MO-7773_36396_CA_CAPR_20230913

Speedway, LLC
500 Speedway Drive
Enon, Ohio 45323
Phone: [phone]
Corrective Action
Performance Report
Speedway Store No. 7971
1343 Rock Barn Road
Conover, Catawba County, North Carolina
Incident No. 36396
Project No. 60690569
September 5, 2023
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Quality Information
Prepared by Reviewed by
Erik Riegel
Environmental Scientist
[e-mail]
Brett G. Schaefer, PE
Project Manager
[e-mail]
Reviewed by
Marie Treiber
Regional Senior Project Manager
[e-mail]
Prepared for:
Speedway, LLC
500 Speedway Drive
Enon, Ohio 45323
Phone: [phone]
Prepared by:
AECOM Technical Services of North Carolina, Inc.
6000 Fairview Road, Suite 200
Charlotte, North Carolina 28210
Phone: [phone]
aecom.com
Copyright © 2023 by AECOM
All rights reserved. No part of this copyrighted work may be reproduced, distributed, or transmitted in any form or by
any means without the prior written permission of AECOM.
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Professional Certification Page
I, Brett G. Schaefer, a Licensed Engineer for AECOM Technical Services of North Carolina, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
_________________________________
Brett G. Schaefer, PE
AECOM Technical Services of North Carolina, Inc.
AECOM Technical Services of North Carolina, Inc. is licensed to practice engineering in North Carolina. The certification
number of the company or corporation is F-0458.
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Table of Contents
1 Introduction .................................................................................................................................................. 1
2 Site Background Information......................................................................................................................... 2
2.1 Site Identification ............................................................................................................................... 2
2.2 Contact Information ........................................................................................................................... 2
2.3 Information about the Release ........................................................................................................... 2
3 Site History and Characterization .................................................................................................................. 4
3.1 Underground Storage Tank Systems .................................................................................................. 4
3.2 Aboveground Storage Tank Systems.................................................................................................. 4
3.3 Historical Releases ............................................................................................................................ 4
3.4 Site Characteristics ........................................................................................................................... 4
3.4.1 Zoning/Receptor Information ................................................................................................... 4
3.4.2 Site Geology and Hydrogeology .............................................................................................. 4
4 Receptor Information .................................................................................................................................... 5
4.1 Water Supply Wells ........................................................................................................................... 5
4.1.1 Private Water Supply Wells ..................................................................................................... 5
4.1.2 Public Water Systems ............................................................................................................. 5
4.2 Surface Water ................................................................................................................................... 5
4.3 Wellhead Protection Areas ................................................................................................................. 5
5 Treatment System Operation and Maintenance ............................................................................................. 6
5.1 System Restart and Treatment System Modifications ......................................................................... 7
5.1.1 Timeline Details ...................................................................................................................... 7
5.2 System Restart.................................................................................................................................. 9
6 Effluent Sample Results ............................................................................................................................. 10
6.1 Air Stack ......................................................................................................................................... 10
6.2 NPDES Discharge ........................................................................................................................... 10
7 Remedial System Operations Summary .......................................................................................................11
7.1 O&M Site Visits ................................................................................................................................11
7.2 Treatment System Operational Data .................................................................................................11
7.3 Mass of Contaminant Removed ........................................................................................................11
7.3.1 Mass Removed as Vapor .......................................................................................................11
7.3.2 Mass Removed as Liquid ...................................................................................................... 12
8 CONCLUSIONS AND RECOMMENDATIONS ............................................................................................ 12
9 References ................................................................................................................................................ 13
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Figures
Figure 1 :Site Location Map
Figure 2 :Site Plan
Tables
Table 1 :Remediation System Air Stack Effluent Samples
Table 2 :Remediation System Effluent Water Samples
Table 3 :DPE System Total BTEX Removal Calculations
Appendices
Appendix A:O&M Field Logs
Appendix B:Laboratory Analytical Reports
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Conover, NCCorrective Action Performance Report September 2023
1 Introduction
As required by the NCDEQ, AECOM Technical Services of North Carolina, Inc. (AECOM) on behalf of Speedway LLC
(Speedway) has prepared this Groundwater Monitoring Report for Speedway Store No. 7971 (Site), located at 1343
Rock Barn Road, Conover, Catawba County, North Carolina.
The site is currently in use as a truck stop, convenience store and retail petroleum dispensing facility, and operates
two 20,000-gallon diesel fuel underground storage tanks (USTs), one 12,000-gallon regular unleaded gasoline UST,
and one 10,000-gallon premium unleaded gasoline UST.
There are two separate releases (gasoline and diesel fuel) associated with this facility. The gasoline release was
reported in September 2007 and the diesel fuel release was reported in January 2010. A Corrective Action Plan
(CAP) proposing air sparge/ vapor extraction (AS/VE) for the gasoline release was prepared in October 2009 and
implemented thereafter but did not address the diesel fuel release since the release had not been discovered at that
time. An initial New Technology Cleanup Plan (NTCP) proposing mobile multi-phase extraction (MMPE) in
conjunction with monitored natural attenuation (MNA) of groundwater was prepared and approved for the diesel fuel
release in August 2010. A total of twenty-four MMPE events were conducted at the site following approval of the
NTCP, with several of the event times split between the diesel fuel and gasoline release areas. The North Carolina
State Trust Fund then indicated that the total costs of MMPE events had approached the purchase price of a dual
phase extraction (DPE) system and, therefore, the Trust Fund would no longer authorize additional rental costs. As a
result, a subsequent NTCP was prepared and approved for the installation of a mobile DPE system to address both
the gasoline and diesel fuel releases.
A mobile DPE system was installed at the site and started for the first time on November 2, 2018, to address both the
gasoline and diesel fuel releases.
In July 2022, AECOM took over remediation responsibilities for the Site and began procedures for restarting the
system. In November 2022 the DPE system was restarted, and regular Operation and Maintenance (O&M) activities
were performed by AECOM staff.
This Corrective Action Performance Report (CAPR) documents the remedial system restart, system operations
(O&M), extraction well installation and supply chain delivery issues during the period from November 2022 through
August 2023. This report is based on limited observations made on the dates noted using the procedures described
herein.
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2 Site Background Information
The following sections provide site background and contact information.
2.1 Site Identification
– Date of Incident Report:September 20, 2007
– Facility ID: 0-034426 Incident Number: 36396
– Site Rank:High
– Site Name:Speedway Store No. 7971
– Site Street Address:1343 Rock Barn Road
– City/Town: Conover Zip Code: 28613 County: Catawba
– Description of Geographical Data Point (e.g., dispenser): Site Property
– Location Method (global positioning system, topographical map, other): Google Earth
– Latitude (decimal degrees): 35.7213 °, Longitude (decimal degrees): -81.1893 °
2.2 Contact Information
– UST Owner: Speedway LLC.
Address: 500 Speedway Drive, Enon, Ohio 45323 Telephone: [phone]
– UST Operator: Speedway LLC.
Address: 500 Speedway Drive, Enon, Ohio 45323 Telephone: [phone]
– Property Owner: PFJ Southeast LLC.
Address: PO Box 54710, Lexington, Kentucky 40555 Telephone: [phone]
– Property Occupant: PFJ Southeast LLC.
Address: PO Box 54710, Lexington, Kentucky 40555 Telephone: [phone]
 Consultant/Contractor: AECOM
Address: 6000 Fairview Road, Suite 200,
Charlotte, North Carolina 28210 Telephone: [phone]
– Analytical Laboratory: Pace Analytical
State Certification No. 5342
Address: 9800 Kincey Avenue, Suite 100,
Huntersville, North Carolina 28078 Telephone: [phone]
2.3 Information about the Release
On September 20, 2007, gasoline was observed leaking from an unleaded gasoline line within a containment sump
during a routine compliance inspection. The damaged line was repaired and WilcoHess (owner/operator at the time)
replaced all UST containment sumps, underground product lines and dispenser sumps. A 24-hour Release and UST
Leak Reporting Form was submitted to the NCDEQ, Division of Waste Management (DWM), UST Section, WSRO on
September 20, 2007, and the site was assigned incident number 36396.
In January 2010, diesel fuel LNAPL was detected for the first time in monitoring well MW-3, which is located near the
truck diesel fuel dispensers. Since then, the extent of the diesel fuel LNAPL plume has expanded to include several
additional monitoring wells.
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On July 6, 2020, Pilot (the current operator of the store) reported a release of diesel fuel from Dispenser #18 to
NCDEQ. LNAPL was present in the under-dispenser containment (UDC) and it was determined that the source of the
fuel was a leaking meter. The UDC did not pass subsequent hydrostatic testing. It is un-known how long the meter
was leaking, but NCDEQ has determined that this release is considered commingled with the existing diesel release,
Incident number 36396.
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3 Site History and Characterization
The following sections provide information on the USTs operated at the Site and follows the general outline
established in UST Section Assessment Guidelines (NCDEQ, 2021a), UST Section Corrective Action Guidelines
(NCDEQ, 2021b) and Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST
Releases (NCDEQ, 2021c) using the Comprehensive Tables for Corrective Action Guidelines Tables (NCDEQ, 2022).
3.1 Underground Storage Tank Systems
UST owner operator and other responsible party information are provided in Table 1. A summary of current and
former USTs maintained at the Site is provided below and summarized in Table 2.
According to the Catawba County, North Carolina Geographic Information System (GIS) mapping service, the current
property owner of the subject site is listed as PFJ Southeast LLC. On October 1, 2014, Speedway purchased the site
from WilcoHess.
3.2 Aboveground Storage Tank Systems
No aboveground storage tank systems (ASTs) are currently present on site. Based on available information, no ASTs
have historically been present at the Site.
3.3 Historical Releases
No information on releases other than Incident 36396 is available for this Site.
3.4 Site Characteristics
The location of the Site is shown on a portion of the United States Geological Survey (USGS), Topo USGS 7.5 Minute
Topographic: Newton, NC (2019) digital raster graphic file (Figure 1). The layout of the Site is found on Figure 2. The
Site is currently operational. The Site is occupied by a PFJ convenience store with Speedway gasoline operations.
The site is located at 1343 Rock Barn Road, Conover, North Carolina and is accessed from Rock Barn Road, located
Southeast of the site. Various commercial and residential properties surround the Site.
3.4.1 Zoning/Receptor Information
The Site and adjoining properties are currently zoned Residential and business (Catawba GIS Viewer).
Receptor information for the site was documented in Mid-Atlantic Associates Inc (Mid-Atlantic)’s (Speedway’s former
consultant) May 15, 2008, Phase II Limited Site Assessment (LSA) Report and amended in Mid-Atlantic’s CAP dated
October 8, 2009. A receptor survey update was not completed for this phase of work. For additional details, please
refer to the LSA report and CAP report.
3.4.2 Site Geology and Hydrogeology
Site geology was evaluated based on historic (Mid-Atlantic) and current investigations. The site is located within the
interlayered rocks of the Carolina Inner Piedmont Belt. The site appears to be in a predominantly metamorphic rock
formation described as “Metamorphosed’. In general, the soils encountered at the Site consist of reddish-brown, light
brown, reddish-orange and black silty clays, and clayey silts, generally getting coarser-grained with depth in the first
sixty feet and then become partially weathered rock and bedrock at approximately eighty feet.
Based on the results of the June 2023 gauging event, groundwater flow is to the north, which is generally consistent
with historical groundwater flow.
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Corrective Action Performance Report September 2023
4 Receptor Information
4.1 Water Supply Wells
The previous consultant (Mid Atlantic) conducted a water supply well survey in 2008 to identify the presence of water
supply wells within a 1,500-foot radius from the Site and is documented in Mid-Atlantic’s May 15, 2008, Phase II LSA
Report and amended in Mid-Atlantic’s October 8, 2009, CAP.
4.1.1 Private Water Supply Wells
It was confirmed that two water supply wells are present within 205 feet of the source areas of the releases, one used
for drinking (user has municipal connection used for everything but drinking water), and one reportedly not in use.
Seven wells were identified between 250 and 1,000, one for drinking, three used for irrigation or cleaning, and three
not in use. And five wells were identified between 1,000 and 1,500 feet of the source areas three of unknown use, one
for drinking, and one for irrigation. For additional details, please refer to the LSA report and CAP report.
4.1.2 Public Water Systems
The Site obtains water from the Conover’s municipal water-supply system, which purchases water from the City of
Hickory drawing water from Lake Hickory on the Catawba River (Conover, 2021).
Based on currently available information, the properties surrounding the Site receive their municipal water supplies
through buried piping that runs beneath the streets and highway easements. A portion of Banner Road according to
Conover’s public works department do not receive service after where the line ended at 102 Banner Road.
4.2 Surface Water
No surface water was observed on the Site. The nearest off-site surface water is an unnamed tributary of Mull Creek
located approximately 1,300 feet to the southwest of the Site. However, drainage from the site appears to be to
generally to the northwest towards an unnamed tributary of Lyle Creek. This unnamed tributary is located
approximately 2,200 feet north of the source area of the release.
4.3 Wellhead Protection Areas
According to the NCDEQ Well Head Protection website, last updated in July 2022, there are no approved wellhead
protection plans located in Catawba County.
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5 Treatment System Operation and Maintenance
The following tasks were performed for the reporting period of performance of November 2022 through August 2023:
•Restart remediation system
•Cleanout of all sight glasses and level switch contacts of encrusted bio-fouling, and adjustments to valves
to control the flow rate;
•Inspect and repair pumps and liquid level controls as needed;
•Tweaked float controls and valve settings as needed;
•Assessed cleanliness of equipment -clean and wipe down as necessary;
•Recorded run time hours;
•Recorded flow meter readings for effluent discharge;
•Evaluated condition of the DPE system (i.e., air filters, particulate filter, etc); and
•Changed oil, filters and belts as needed.
Additional operational data, site visit notes and photographs are available in the O&M Field Logs provided in
Appendix A.
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Corrective Action Performance Report September 2023
5.1 System Restart and Treatment System Modifications
5.1.1 Timeline Details
Date Description
11/17/2022
Attempted to turn system on. System did not start up immediately. Applied penetrating oil on
blower parts to break blower free from corrosion. Checked blower rotation and all filter
housings. Restarted system and observed operation until noticed that the HHL alarm caused
system shutdown. Moisture separator pump was not keeping up with vacuum. It was
determined a new moisture separator pump is required. Took system readings left system off
to re-evaluate operation.
11/29/2022
Installed new M/S pump. Restarted system. Collected readings. Fine-tuned system for
continuous operation after new pump was installed. Restarted system, collected readings, and
left site with system operating.
12/9/2022 Site visit to collect system readings; adjusted valves as necessary to maintain proper vacuum
levels.
12/15/2022 Site visit to collect system readings; adjusted valves as necessary to maintain proper vacuum
levels. Collected effluent air and water samples.
12/20/2022 System was off upon arrival. Reset alarms, restarted system, and collected readings.Adjusted
valves and pressure gauges. System on upon departure.
12/27/2022 Site visit to check on system during freezing weather. System was operating as normal.
Collected system readings. Left site operating.
1/31/2023 Site Visit; collected monthly air stack discharge sample. Collected system readings and
checks.
2/1/2023 Site Visit: collected system readings.
2/9/2023
Site visit: Set up portable pump and hose to pump excess water from the product holding tank
into the system influent tank for treatment and disposal to sewer. Pumped approx. 2/3 of
contents of to the influent tank.
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Date Description
3/27/2023
Site visit: Installed a ball valve on the line between the influent tank and the oil/water separator.
Replaced the leaking vacuum breaker valve on effluent discharge line. Collected monthly air
effluent sample. Collected quarterly water effluent sample.
4/5/2023
Pumped out the water from the product storage tank into the main tank for treatment. Changed
out bag filter. OWS separator was starting to flood again. Shut off flow to the tank and let the
levels normalize with the aeration tank and slowly feed more water through the system. System
operating upon departure.
4/24/2023
System down upon arrival; OWS separator was flooded, MS Level was High-high alarm, and
the product tank is flooded. Pumped product tank into the main equalization tank and pumped
the MS to the equalization tank. Slowly fed the OWS from the EQ tank. Left the vac pump
offline until the system levels returned to normal operating levels. Closed the OWS feed valve
to 50% to prevent potential flooding. Did not collect monthly air discharge sample due to
system operating issues.
5/22/2023
System off upon arrival due to vacuum alarm and the OWS pump not turning on. Replaced the
following system components: Vacuum sensor, OWS float tree. Pumped water from product
tank to system for treatment. Changed bag filter, changed vacuum filter. Cleared alarms and
restarted system. Observed operation and adjusted vac and flows for optimal operation.
System operating upon departure.
6/8/2023
System was down upon arrival. High Level alarms in the OWS and MS. Ran the pumps in
manual to clear the alarms, pumped the product recovery tank which flooded when the OWS
gets a High-High Alarm. Tested the float tree switch for the OWS, it is not activating the OWS
transfer pump properly. The float switch was replaced 2 weeks prior to this visit. System
operated properly as of 2 weeks ago. Will try to replace new float tree to rule out equipment
failure and see if it is an electrical problem. GAC vessels require change outs.
6/14/2023
Worked on getting the OWS float switch to activate the OWS transfer pump. Checked all of the
switch wiring connections, in-line and the control panel. Tightened everything and tested float.
Pump activated. Restart system to observe operation. During observation the OWS transfer
pump operated two times properly and on the third time it failed to activate the pump. Possible
issue at the panel beyond tech’s capabilities. System was left off upon departure.
6/20/2023 Site visit; collected effluent water sample. Collected effluent air stack sample; collected system
readings.
7/24/2023
Site visit; general observation: system does not run consistently potentially due to wiring issues
at the panel. The OWS switch signal operates periodically. Attempted to restart the system but
could not keep it operating due to the High-High level alarms. System could not stay on long
enough to collect proper readings and collect monthly effluent samples.
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5.2 System Restart
As summarized in the Timeline Details section of this report (Section 5.1.1), the treatment system was restarted on
November 29, 2022. The remediation system had operated without much issue until April 2023. System components
were changed out due to age and the system had been operating periodically.
Based on observations with the system operation there may be wiring issues connected to the main control panel and
the Oil/Water separator (OWS) float switch. When the float switch fails to operate the system shuts down and causes
cascading alarms and potentially floods the OWS. The system is also in need of a full cleaning. At the time of this
report (August 2023) the system is not operating and waiting on a schedule date for a deep cleaning with a
subcontractor.
Since system restart on November 29, 2022, the system has suffered multiple shutdowns. A calculated runtime of 52%
was recorded during this reporting period. The below graph summarizes the system performance based on system
logs acquired through the remote login program.
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6 Effluent Sample Results
6.1 Air Stack
Sampling of the DPE effluent stack was performed on December 15, 2022, January 31, 2023, March 27, 2023, and
June 20, 2023, during the current reporting period (November 2022 through August 2023). Samples were shipped
under chain-of-custody control to Pace Analytical in Mt. Juliet, Tennessee for analysis of BTEX according to EPA
Method 18. A copy of the laboratory analytical reports and chain-of-custody records for the effluent stack samples are
provided in Appendix B, with the results summarized in Table 1. As summarized, BTEX compounds were detected in
all effluent stack samples collected during this reporting period.
6.2 NPDES Discharge
Liquid discharge samples were collected from the DPE treatment system on December 15, 2022, March 27, 2023, and
June 20, 2023, during this current reporting period (November 2022 through August 2023). Samples were shipped
under chain-of-custody control to Pace Analytical Services in Charlotte, North Carolina for total suspended solids by
SM2540D-2015, phenols by EPA Method 420.1, oil & grease according to EPA Method 1664B, BTEX by EPA Method
8260D, and lead by EPA Method 6020B. A copy of the laboratory analytical reports and chain-of-custody records for
the effluent stack samples are provided in Appendix B, with the results summarized in Table 2.
AECOM 11
7 Remedial System Operations Summary
7.1 O&M Site Visits
O&M site visits (including extraction well installation visits) were conducted on the following dates during the reporting
period:
7.2 Treatment System Operational Data
Claw pump run hours and water meter totalizer readings obtained during O&M site visits are provided below:
7.3 Mass of Contaminant Removed
7.3.1 Mass Removed as Vapor
Calculations of petroleum hydrocarbon mass removed as vapor were performed using the air stack samples collected
on December 15, 2022, January 31, 2023, March 27, 2023, and June 20, 2023. Based on the mass removal
calculations, Total BTEX removed by operation of the remediation system during this reporting period was 0.16 lbs as
vapor.
Mass removal calculations are provided as Table 3.
Date Date
11/17/2022 3/27/2023
11/29/2022 4/5/2023
12/9/2022 4/24/2023
12/15/2022 5/22/2023
12/20/2022 6/8/2023
12/27/2022 6/14/2023
1/31/2023 6/20/2023
2/1/2023 7/24/2023
2/9/2023
Date LRP Run Hours Water Meter Reading (gal)
11/17/2022 10765 389296
11/29/2022 10767 389344
12/9/2022 10944 399406
12/15/2022 10962 399808
12/20/2022 11057 404612
12/27/2022 11230 410008
2/1/2023 11769.9 426615.67
3/27/2023 12420.1 459720.63
4/24/2023 -482976.20
6/20/2023 13383.8 506157.39
AECOM 12
7.3.2 Mass Removed as Liquid
For the reporting period, approximately 116,861.39 gallons of petroleum-impacted groundwater was treated by the
remediation system. Since the EQ tank was installed, no additional free product has been recovered in the treatment
system's original product tank.
8 CONCLUSIONS AND RECOMMENDATIONS
Based on our observations and activities conducted over the current reporting period, AECOM concludes the
following:
•A total of 116,861.39 gallons gallons of water were extracted from the DPE treatment system during the
period of performance.
•The treatment system has operated at an average runtime of 52% during this reporting period.
•Approximately 0.16 pounds of total BTEX was removed as vapor measured via the air stack effluent at the
claw pump.
•The DPE system currently remains off due to required cleaning of components and a potential electrical
system problem causing the OWS float switch to fail to activate properly. This error causes the OWS to
overflow into the equalization tank used to collect product.
•The electrical system requires an evaluation by an electrician to determine if the PLC at the main control
panel or a wiring issue with the float switch is the cause of pump operation failures.
In lieu of the poor DPE system performance and lack of LNAPL recovery, a Mobile Multiphase Extraction (MMPE)
event was scheduled for September 18 through 22, 2023 to target monitoring wells with significant apparent LNAPL
thicknesses. LNAPL recovery from the event may warrant re-evaluation of the need to continue DPE system
operation or modify the existing system for better performance and LNAPL recovery.
Based on these conclusions, AECOM on behalf of Speedway, recommends the following:
•Keep the DPE system shut down for 6 months (October 2023 through April 2024).
•Perform a deep cleaning of the DPE system during the shutdown period.
•Evaluate electrical components during the shutdown period.
•Continue groundwater sampling on a semi-annual basis.
•Perform and evaluate the September 2023 MMPE event and LNAPL recovery.
•Submittal of this report to the NCDEQ UST Section.
AECOM 13
9 References
NCDEQ, 2021a. UST Section Assessment Guidelines. effective January 19, 2021.
NCDEQ, 2021b. UST Section Corrective Action Guidelines. effective January 19, 2021.
NCDEQ, 2021c. Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement for UST Releases.
Change 11, effective May 17, 2021.
NCDEQ, 2022. Comprehensive Tables for Corrective Action Guidelines Tables. Effective September 7, 2022.
Mid-Atlantic Associates, 2008. Phase II LSA Report. May 15, 2008.
Mid-Atlantic Associates, 2018. Corrective Action Plan. September 25, 2018.
Mid-Atlantic Associates, 2022. Groundwater Monitoring Report. February 27, 2022.
Conover, 2021. 2021 Annual Drinking Water Quality Report, City of Conover,
https://www.conovernc.gov/vertical/sites/%7BBAB0D760-E669-4331-9C22-
9FB14833B6B9%7D/uploads/2021_Annual_Drinking_Water_Quality_Report_-_____.pdf, accessed
September 29, 2022.
Figures
2,0002,000
N
SITE LOCATION
I. DUMITRUAUGUST 2023
SITE LOCATION MAP FIGURE 1
Source: Topo USGS 7.5 Minute Topographic Map
Quadrangle: Newton, NC
Copyright: 2019 National Geographic Society
DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:File: \\na.aecomnet.com\LFS\AMER\Chelmsford-USCHL1\Secure_DCS\Projects\Legacy\711\North Carolina\47293-7971 Conover\60690569\Section 5.0 Reports\Reports\PATA-69_GWMR_2023 07 July_Report\Figures\47293-7971 Conover_2023 07 July_Report.dwg Layout: Figure 1 Date: 21 Aug, 2023 Xrefs:00
SCALE IN FEET:
NOTE: ALL MAP FEATURES ARE APPROXIMATE
IN SCALE AND LOCATION.
E. RIEGEL
Speedway Store #7971
1343 Rock Barn Road
Conover, North Carolina
60690569
Speedway LLC.
SpeedwayStore #7971R o c k B a r n R o a d N o r t h e a s tTank FieldVent PipesDiesel Canopy& Pump IslandsGasoline Canopy& Pump IslandsCAT ScaleConcrete PadConcrete PadFormerPumpIslandTruck ParkingMW-6MW-24MW-23RMW-21MW-20MW-19MW-18MW-22MW-26MW-27MW-28MW-17MW-16MW-9MW-10DMW-2MW-13MW-8MW-14RMW-11DMW-7MW-12MW-5MW-4MW-4MW-3RMW-25MW-1RMW-6MW-15VE-OW-2SCALE IN FEET:40400DATE:DRAWN BY:REVIEWED BY:PROJECT NO.:\\na.aecomnet.com\LFS\AMER\Chelmsford-USCHL1\Secure_DCS\Projects\Legacy\711\North Carolina\47293-7971 Conover\60690569\Section 5.0 Reports\Reports\PATA-69_GWMR_2023 07 July_Report\Figures\47293-7971 Conover_2023 07 July_Report.dwg, 8/21/2023 12:52 PM, Schaefer, Brett, PDF995.pc3, User32767, 1'-0" = 1'-0"NI. DUMITRUE. RIEGELFIGURE 2SITE PLANLEGENDNOTE: ALL MAP FEATURES ARE APPROXIMATEIN SCALE AND LOCATION.Speedway Store #79711343 Rock Barn RoadConover, North Carolina60690569Speedway LLC.Approximate Property BoundaryFenceProduct Dispenser#1, #2#3#4Underground Storage Tank20,000-Gal. Diesel USTs12,000-Gal. RUL Gasoline UST10,000-Gal. PUL Gasoline USTProduct PipingOverhead WireBuried Electric LineBuried Telephone LineWater LineSanitary SewerUtility Pole / Power PoleLight Post / Traffic LightFire HydrantMonitoring WellVapor Extraction Pilot Test WellMonitoring Well (Deep)Recovery WellAUGUST 2023
Tables
Air Stack Effluent 12/15/22 3,930 23,900 3,460 12,300 5,220
Air Stack Effluent 01/31/23 3,420 15,300 2,640 10,000 5,030
Air Stack Effluent 03/27/23 6,010 26,400 11,700 27,200 12,800
Air Stack Effluent 06/20/23 7,220 38,400 5,770 21,900 10,300
Notes:
ND - Not detected at or above laboratory's practical quantitation limit
NA - Not Analyzed for this parameter
All concentrations reported in ug/L - micrograms per liter except where otherwise noted
m&p-
Xylene o-Xylene
TABLE 1
REMEDIATION SYSTEM AIR STACK EFFLUENT SAMPLES
SPEEDWAY 7971
CONOVER, NORTH CAROLINA
INCIDENT NO. 36396
Sample Date Toluene EthylbenzeneBenzeneWell Number
Conover Eflfuent 12/15/22 ND ND ND ND ND 2.2 0.054 ND ND
Conover Eflfuent 03/27/23 ND ND ND ND ND ND ND NA ND
Conover Eflfuent 06/20/23 NA NA NA NA NA ND ND NA 2.5
Notes:
ND - Not detected at or above laboratory's practical quantitation limit
NA - Not Analyzed for this parameter
All concentrations reported in ug/L - micrograms per liter except where otherwise noted
Leadm&p-
Xylene o-Xylene Phenol
(mg/L)
Total
Suspended
Solids (mg/L)
Oil &
Grease
(mg/L)
TABLE 2
REMEDIATION SYSTEM EFFLUENT WATER SAMPLES
SPEEDWAY 7971
CONOVER, NORTH CAROLINA
INCIDENT NO. 36396
Well Number Sample Date Benzene Toluene Ethylbenzene
Conversion Factor3 Total BTEX Mass
Removal per Sample4
(lb-m3/mg-ft3)(lb. recovered per
sample)
12/15/22 Air Stack Effluent 10962.0 195 15 48.81 6.243E-08 0.009
01/31/23 Air Stack Effluent 11769.9 807.9 15 36.39 6.243E-08 0.028
03/27/23 Air Stack Effluent 12420.1 650.2 15 84.11 6.243E-08 0.051
06/20/23 Air Stack Effluent 13383.8 964 15 83.59 6.243E-08 0.075
Average Airflow:15 Total Recovered Total BTEX (lb):0.16
Notes:
5. Sample collected on 12/15/2022 was first sample collected after system restart by AECOM on 11/29/22.
LRP Hour Meter
Reading (min)
1. Air flow rates were extrapolated using system vacuum readings from system main panel.
2. Total BTEX concentrations in the exhaust are based on analytical data collected during site visits.
3. Conversion factor to convert units of concentration from mg/m3 to lb/ft3.
4. Mass removal rate (lb) = (air flow rate) x (Total BTEX Conc.) x (conversion factor) x (elapsed operating time).
TABLE 3
DPE SYSTEM TOTAL BTEX REMOVAL CALCULATIONS
SPEEDWAY 7971 - CONOVER
Sample
Date Air Sample ID
Elapsed
Operating Time
Between Samples
(min)5
Air Flow
Rate1
(ft3/min)Total BTEX(mg/m3)
Appendix A
O&M Field Logs
Site Name:Personnel:
Date:
Arrival Departure
On / Off On / Off
"Hg °F
"H2O PSI
"H2O PSI
Gallons
Remediation System Operation & Maintenance
Inspect entire system for loose bolts, loose connections, broken components, rust, clogging, or leakage:
Project Number:
Departure Time:
Dual Phase Extraction System
Aerator Pump Hour Meter:
Arrival Time:
Repair above issues:
MS Vapor Temperature
Aerator Influent Pressure
Vacuum Blower Hour Meter:MS Pump Hour Meter:
OWS Pump Hour Meter:Aerator Blower Hour Meter:
Aerator Discharge Pressure
Effluent Flow Totalizer:
Influent MS Vacuum:
Page 1 of 2

Date:Site Name:
Log/Notes:
Page 2 of 2
Daily Work Log Page____ of ____
Date:Client:
Project Number:
Weather & Site Conditions:
Equipment:
Personnel Onsite:
Tailgate Safety Meeting Notes:
Instruments & Calibration:
Work Log & Notes:
Daily Objective:
Time Onsite:Time Offsite:
Project Name:Project Location:
Field Personnel:
Project Manager:

Daily Work Log Page____ of ____
Date:Project Number:
Site Name:Personnel:
Date:
Arrival Departure
On / Off On / Off
"Hg °F
"Hg
"H2O PSI
"H2O PSI
Gallons
%%
Inches
DP Vacuum Blower Discharge LEL:Room LEL:
Product Tank Level:
Remediation System Operation & Maintenance
Inspect entire system for loose bolts, loose connections, broken components, rust, clogging, or leakage:
Project Number:
Departure Time:
Dual Phase Extraction System
Aerator Pump Hour Meter:
Arrival Time:
Repair above issues:
MS Vapor Temperature
Aerator Influent Pressure
Effluent Moisture Separator Vacuum:
Vacuum Blower Hour Meter:MS Pump Hour Meter:
OWS Pump Hour Meter:Aerator Blower Hour Meter:
Aerator Discharge Pressure
Effluent Flow Totalizer:
Influent Moisture Separator Vacuum:
Page 1 of 2

SpeedwayConover TimDickey
3127123 60690569
0730 1400
O O
12420.1 1215.4
437.3 17448.4
4454.4
15.5 215
15.5
38 13.5
7 0.25
459720.63
O O
Full
Date:Site Name:
Log/Notes:
Page 2 of 2
3 27 23 SpeedwayConover
CompletedSafetyReview
Installed a ballvalve inthelinebetweentheinfluenttankandows
Replacedthevacuumbreakervalveintheeffluentdischargeline wasleaking
Replacedthevacuumbreakervalvebetweentheowsandtheaeratortank wasleaking
Tried topumpouttheproducttank theportabletransferpumpquitorderedanewpump
Collectedthemonthly aireffluentsample ConoverAirStack Eff
Collected thequarterlywatereffluentsample ConoverEffluent
Daily Work Log Page____ of ____
Date:Client:
Project Number:
Weather & Site Conditions:
Equipment:
Personnel Onsite:
Tailgate Safety Meeting Notes:
Instruments & Calibration:
Work Log & Notes:
Daily Objective:
Time Onsite:Time Offsite:
Project Name:Project Location:
Field Personnel:
Project Manager:

I I
4 5 23 Speedway
SpeedwayConover
TimDickey
ConoverNC
BrettSchaefer 60690569
Pumpwateroutoftheproductstoragetankandsendwaterbackthroughthesystemfortreatment
0830 1530
Verywarmandhumid
Portabletransferpump
NA
Reviewedsafetyprocedures
NA
Setuptransferpumpandpumped thewaterFromtheproductstoragetankintothemaintankfortreatment
ChangedoutthebagfilterOilWaterseparatorwasbeginningtofloodagain shutoff flowto it andletthe
levelsin itandtheaerationtanknormalizeandslowlyfeedmorewaterthroughthe
system
1500 system'soperatingnormallyagain
Daily Work Log Page____ of ____
Date:Project Number:
Daily Work Log Page____ of ____
Date:Client:
Project Number:
Weather & Site Conditions:
Equipment:
Personnel Onsite:
Tailgate Safety Meeting Notes:
Instruments & Calibration:
Work Log & Notes:
Daily Objective:
Time Onsite:Time Offsite:
Project Name:Project Location:
Field Personnel:
Project Manager:

I I
4 24 23 Speedway
Conover ConoverNC
TimDickey
B Schaefer 60690569
MonthlyOM
0830 1620
Clearcooltowarm
NA
NA
ReviewsafetyproceduresandreviewHASP
NA
systemisdown oilwaterseparatorisfloodedMslevelisHighHighalarmandtheproducttankis
floodedPumpeddowntheoilwatersepinstagestonotoverwhelmtheAerationtank
PumpedtheproducttankintothemainEqualizationtankandpumpedtheMstotheEqualizationtank
SlowlyFeedtheonsepfromtheEqualizationtank
LeavethevacuumPumpofflineuntilsystemlevelsreturntonormaloperatinglevels
SpokewiththeprojectmanageraboutcleanthesystemtokeepfromgettingHighlevelsandfloodingandshutingdown
keepslowlyfeedingthewaterthroughthesystem
ClosedthevalvetotheowsepFromtheEqTank toapprox50 totrytokeeptheowSepFromFlooding
TheONSepFloatswitchesmaynotbeoperatingastheyshouldCleanedthefloattreewillhavetoobserve
operationtodetermineiftheyneedtobereplaced
Didnotcollectamonthlyairdischargesampleduetosystemoperationissues
WaterDishargeMeterreading 482,976 20gallons
Daily Work Log Page____ of ____
Date:Project Number:
Daily Work Log Page____ of ____
Date:Client:
Project Number:
Weather & Site Conditions:
Equipment:
Personnel Onsite:
Tailgate Safety Meeting Notes:
Instruments & Calibration:
Work Log & Notes:
Daily Objective:
Time Onsite:Time Offsite:
Project Name:Project Location:
Field Personnel:
Project Manager:

I 1
5122123 Speedway
SpeedwayConover 7971 ConoverNC
TimDickey
BrettSchaefer 60690569
Repairandrestartthesystem
0845
Overcastwarmhumid
n
NA
completedsafetychecksandsafetyproceduresreview
NA
Thesystemisofflineduetovacuumalarmandtheowspumpnotcomingon
ReplacedthevacuumsensorTransmitter Ok
ReplacedtheOwsfloattreeok
PumpedtheProductTankFullofwaterintothesystemprocesstankfortreatment
Chargedoutthebagfilter
Changedoutthevacuumblowerfilter
RestartedthesystemVacuumAlarmhasclearedOwspumpisnowcomingonwhenit issupposedto
Observedoperationand adjustedvacuumandflowsforoptimaloperations
Thesystemseemstobeoperatingwellnow
Daily Work Log Page____ of ____
Date:Project Number:
Daily Work Log Page____ of ____
Date:Client:
Project Number:
Weather & Site Conditions:
Equipment:
Personnel Onsite:
Tailgate Safety Meeting Notes:
Instruments & Calibration:
Work Log & Notes:
Daily Objective:
Time Onsite:Time Offsite:
Project Name:Project Location:
Field Personnel:
Project Manager:

I I
6 8 23 Speedway
SpeedwayConover Conover NC
TimDickey
BrettSchaefer 60690569
TroubleshootandrestarttheDPEsystem
0730 1430
HazyHumidHot
NA
NA
ReviewedSafetyProcedures
NA
Thesystemis downduetoHighlevels intheOwsandMsRonthepumpsinManualto
clearthealarmspumpedtheProductRecoveryTankwhichfloodwhentheOwsgetsa HighHighLevel
TestedthefloattreeswitchfortheOws itisnotactivatingtheowstransferpumpThefloat
treewasreplacedapprox2weeksagoandthesystemranwellfor 2weeksWillreplacetheFloattree
againandseeifthatistheissueoranotherissueincontrolwiring
Alsothe2ndcarbonunitisnotflowingwellprobablyisgettingcloggedupBothCarbonunitsneedtobe
changedout
WillorderanotherFloatswithandtrytorestartafterthegettingtheswitch
Daily Work Log Page____ of ____
Date:Project Number:
Daily Work Log Page____ of ____
Date:Client:
Project Number:
Weather & Site Conditions:
Equipment:
Personnel Onsite:
Tailgate Safety Meeting Notes:
Instruments & Calibration:
Work Log & Notes:
Daily Objective:
Time Onsite:Time Offsite:
Project Name:Project Location:
Field Personnel:
Project Manager:

I
6 14 23 Speedway
Speedway7971Conover ConoverNC
TimDickey
B Schaefer 60690569
TroubleshootandgettheDPEsysteminoperatingcondition
0815
CloudyHumidVeryWarm
NA
NA
ReviewHASPandSafetyProcedures
NA
Arrivedthereis a EasternEnvironmentalManagementvactruckalongwithAtlas
setuponawellbesidetheFronttankpitWorkedongettingtheOwsfloatswitchworkingtoactivatetheowstransferPumpcheckedallofthe
switcheswiringconnectionsinlineandinthecontrolpanelTightenedeverythingandtestedpumpactivated
Restartedthesystemtoobserveoperation
TheOwstransferpumptransferd atimes onthe3rdtimethepumpdidnotactivatewhenthepumpon
Floatwasreached Couldpossiblybeanissueinthecontrolpanel
systemwasleftoff
Daily Work Log Page____ of ____
Date:Project Number:
Site Name:Personnel:
Date:
Arrival Departure
On / Off On / Off
"Hg °F
"Hg
"H2O PSI
"H2O PSI
"Hg "Hg
"Hg
Gallons
%%
Inches
Effluent Flow Totalizer:
Influent Moisture Separator Vacuum:
Well Leg 1 Vacuum:Well Leg 2 Vacuum:
Well Leg 3 Vacuum:
Effluent Moisture Separator Vacuum:
Vacuum Blower Hour Meter:MS Pump Hour Meter:
OWS Pump Hour Meter:Aerator Blower Hour Meter:
Aerator Discharge Pressure
Arrival Time:
Repair above issues:
MS Vapor Temperature
Aerator Influent Pressure
Aerator Pump Hour Meter:
DP Vacuum Blower Discharge LEL:Room LEL:
Product Tank Level:
Remediation System Operation & Maintenance
Inspect entire system for loose bolts, loose connections, broken components, rust, clogging, or leakage:
Project Number:
Departure Time:
Dual Phase Extraction System
Page 1 of 2

ConoverNC 7971 TimDickey
6120123 60690569
0750 1415
O O
13383.8 1255.3
471.9 19245.7
4985.9
16.3 212
16.5
46 1.65
6.5 0.23
11 12.5
5.5
506157.39
O O
10
Carbonvessels lis
cloggedandthe2ndisveryslowgettingclogged
TheowspumphasanissuewithactivatingsometimesitactivatessometimesitdoesnotHavereplacedthe
Floatswitchandthathelpedforawhilebutdidnotsolvetheproblem
stilltroubleshootingwhytheOwsPumpisactivatingperiodicallyandnotallofthetimeMayneedtogetan
electricianinvolvedtofindtheissue
Date:Site Name:
Log/Notes:
Page 2 of 2
phg g
ConoverNC797
Arrived completedsafetyReview
CollectedtheQuart.lyWaterDischargeSample ConoverEffluent 1020hadrunowspumponmanualtomorewater
throughthesystem
CollectedanAirStackEffluentsample ConoverAirstackEFF 1045
TooksampleforanalysistoPaceAnalyticalHuntersvilleNC
Site Name:Personnel:
Date:
Arrival Departure
On / Off On / Off
"Hg °F
"Hg
"H2O PSI
"H2O PSI
"Hg "Hg
"Hg
Gallons
%%
Inches
Log/Notes:
Room LEL:
Product Tank Level:
Remediation System Operation & Maintenance
Project Number:
Departure Time:
Dual Phase Extraction System
Arrival Time:
MS Vapor Temperature
Aerator Influent Pressure
Effluent Moisture Separator Vacuum:
Vacuum Blower Hour Meter:MS Pump Hour Meter:
OWS Pump Hour Meter:Aerator Blower Hour Meter:
Aerator Discharge Pressure
Effluent Flow Totalizer:
pH:
Influent Moisture Separator Vacuum:
Well Leg 1 Vacuum:Well Leg 2 Vacuum:
Well Leg 3 Vacuum:
Aerator Pump Hour Meter:
DP Vacuum Blower Discharge LEL:
Page 1 of 2

SWConoverNC TimDickey
7 2423 60690569
0800 1435
O O
O O
Systemdoesnotrun consistentlydueacontrolwiringcomponent FortheOwsfloat
switchsignaltoturnontheOwstransferPump sometimesthesignalispickedupandsometimesitisnot
Beganmovingthewaterthruthesystemmanually
Couldnotkeepthesystemoperatingdueto HighHighLevel alarms to beable
totakethereadingsandget a monthlyairvapordischargesample
Thecarbonunits arebothclogged I is completelycloggedandtheotheris
notlettingverymuchflow thruandcausing a AeratorTank HighHighLevel
Date:Site Name:
Inspect entire system for loose bolts, loose connections, broken components, rust, clogging, or leakage:
Repair above issues:
Page 2 of 2
7124123
Appendix B
Laboratory Analytical Reports
#=CL#
December 28, 2022
LIMS USE: FR - BRETT SCHAEFER
LIMS OBJECT ID: 92642655
92642655
Project:
Pace Project No.:
RE:
Brett Schaefer
AECOM
6000 Fairview Road
Suite 200
Charlotte, NC 28210
7971 CONOVER
Dear Brett Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 11
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92642655
7971 CONOVER
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Mold Certification #: LAB0152
Texas Certification #: T 104704245-17-14
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 11
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92642655
7971 CONOVER
Lab ID Sample ID Matrix Date Collected Date Received
92642655001 AIR STACK Air 12/15/22 11:00 12/16/22 10:28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 11
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92642655
7971 CONOVER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92642655001 AIR STACK Method 18 Air MeOH & EtOH 8 PANDAH, SDS
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 11
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92642655
7971 CONOVER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92642655001 AIR STACK
Benzene 3930 ug/m3 12/28/22 00:3063.9Method 18 Air MeOH &
EtOH
Toluene 23900 ug/m3 12/28/22 00:30188Method 18 Air MeOH &
EtOH
Ethylbenzene 3460 ug/m3 12/28/22 00:3086.7Method 18 Air MeOH &
EtOH
m&p-Xylene 12300 ug/m3 12/28/22 00:30173Method 18 Air MeOH &
EtOH
o-Xylene 5330 ug/m3 12/28/22 00:3086.7Method 18 Air MeOH &
EtOH
Gasoline Range Organics 283000 ug/m3 12/28/22 00:3082600Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 11
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92642655
7971 CONOVER
Sample:AIR STACK Lab ID:92642655001 Collected:12/15/22 11:00 Received:12/16/22 10:28 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 3930 ug/m3 12/28/22 00:30 71-43-212/28/22 00:3063.9 22.8 100
Toluene 23900 ug/m3 12/28/22 00:30 108-88-312/28/22 00:3018832.8 100
Ethylbenzene 3460 ug/m3 12/28/22 00:30 100-41-412/28/22 00:3086.7 36.2 100
m&p-Xylene 12300 ug/m3 12/28/22 00:30 179601-23-112/28/22 00:3017358.5 100
o-Xylene 5330 ug/m3 12/28/22 00:30 95-47-612/28/22 00:3086.7 35.9 100
Methyl-tert-butyl ether ND ug/m3 12/24/22 19:04 1634-04-412/24/22 19:041.25 0.407 1.74
Gasoline Range Organics 283000 ug/m3 12/28/22 00:30 8006-61-912/28/22 00:308260016400100
Surrogates
1,4-Dichlorobenzene-d4 (IS)176 %12/24/22 19:04 3855-82-1 ST12/24/22 19:0460.0-140 1.74
1,4-Dichlorobenzene-d4 (IS)100 %12/28/22 00:30 3855-82-112/28/22 00:3060.0-140 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 11:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92642655
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1979283
TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92642655001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3875511-3
Associated Lab Samples:92642655001
Matrix:Air
AnalyzedMDL
Methyl-tert-butyl ether ug/m3 ND 0.721 12/24/22 11:360.233
1,4-Dichlorobenzene-d4 (IS)%92.5 60.0-140 12/24/22 11:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3875511-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3875511-2
Methyl-tert-butyl ether ug/m3 15.713.5 117 70.0-13011515.6 1.15 25
1,4-Dichlorobenzene-d4 (IS)%97.5 60.0-14098.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 11:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 11
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92642655
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1979799
TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92642655001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3875739-3
Associated Lab Samples:92642655001
Matrix:Air
AnalyzedMDL
Benzene ug/m3 ND 0.639 12/27/22 12:130.228
Toluene ug/m3 ND 1.88 12/27/22 12:130.328
Ethylbenzene ug/m3 ND 0.867 12/27/22 12:130.362
m&p-Xylene ug/m3 ND 1.73 12/27/22 12:130.585
o-Xylene ug/m3 ND 0.867 12/27/22 12:130.359
Gasoline Range Organics ug/m3 ND 826 12/27/22 12:13164
1,4-Dichlorobenzene-d4 (IS)%95.5 60.0-140 12/27/22 12:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3875739-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3875739-2
Benzene ug/m3 12.412.0 104 70.0-13010412.4 0.00 25
Toluene ug/m3 15.114.1 107 70.0-13010715.2 0.498 25
Ethylbenzene ug/m3 18.016.3 111 70.0-13011218.2 0.719 25
m&p-Xylene ug/m3 36.432.5 112 70.0-13011236.4 0.119 25
o-Xylene ug/m3 17.916.3 110 70.0-13011118.0 0.482 25
Gasoline Range Organics ug/m3 855839 102 70.0-130102855 0.00 25
1,4-Dichlorobenzene-d4 (IS)%97.4 60.0-14097.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 11:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 8 of 11
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92642655
7971 CONOVER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
SAMPLE QUALIFIERS
Sample: 92642655001
Volatile Organic Compounds (MS) by Method M18-Mod - Surrogate failure due to matrix interference.[1]
ANALYTE QUALIFIERS
Surrogate recovery was above laboratory control limits. Results may be biased high.ST
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 11:41 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 11
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92642655
7971 CONOVER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92642655001 1979283 1979283AIR STACK M18-Mod Method 18 Air MeOH &EtOH
92642655001 1979799 1979799AIR STACK M18-Mod Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/28/2022 11:41 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 10 of 11
Page 11 of 11
#=CL#
January 04, 2023
LIMS USE: FR - BRETT SCHAEFER
LIMS OBJECT ID: 92642677
92642677
Project:
Pace Project No.:
RE:
Brett Schaefer
AECOM
6000 Fairview Road
Suite 200
Charlotte, NC 28210
7971 CONOVER
Dear Brett Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 16
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92642677
7971 CONOVER
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 16
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92642677
7971 CONOVER
Lab ID Sample ID Matrix Date Collected Date Received
92642677001 EFF 121522 Water 12/15/22 10:30 12/16/22 10:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 16
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92642677
7971 CONOVER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92642677001 EFF 121522 EPA 1664B 1 PASI-CREL
EPA 6020B 1 PASI-GACW1
EPA 8260D 5 PASI-CSAS
SM 2540D-2015 1 PASI-AJMH1
EPA 420.4 Rev 1.0 1993 1 PASI-AKDF1
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 16
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92642677
7971 CONOVER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92642677001 EFF 121522
Lead 2.2 ug/L 01/03/23 16:431.0EPA 6020B
Phenolics, Total Recoverable 0.054 mg/L 12/21/22 15:040.020EPA 420.4 Rev 1.0 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 16
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92642677
7971 CONOVER
Sample:EFF 121522 Lab ID:92642677001 Collected:12/15/22 10:30 Received:12/16/22 10:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 1664B
Pace Analytical Services - Charlotte
HEM, Oil and Grease
Oil and Grease ND mg/L 12/28/22 00:154.9 1.1 1
Analytical Method: EPA 6020B Preparation Method: EPA 3005A
Pace Analytical Services - Peachtree Corners, GA
6020 MET ICPMS
Lead 2.2 ug/L 01/03/23 16:43 7439-92-112/27/22 17:441.0 0.89 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Diisopropyl ether ND ug/L 12/21/22 03:19 108-20-31.0 0.31 1
Methyl-tert-butyl ether ND ug/L 12/21/22 03:19 1634-04-41.0 0.42 1
Surrogates
4-Bromofluorobenzene (S)98 %12/21/22 03:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %12/21/22 03:19 17060-07-070-130 1
Toluene-d8 (S)117 %12/21/22 03:19 2037-26-570-130 1
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
2540D Total Suspended Solids
Total Suspended Solids ND mg/L 12/21/22 14:212.5 2.5 1
Analytical Method: EPA 420.4 Rev 1.0 1993 Preparation Method: EPA 420.4 Rev 1.0 1993
Pace Analytical Services - Asheville
420.4 Phenolics, Total
Phenolics, Total Recoverable 0.054 mg/L 12/21/22 15:04 64743-03-912/21/22 10:350.020 0.0076 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92642677
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
746031
EPA 1664B
EPA 1664B
1664 HEM, Oil and Grease
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92642677001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3880340
Associated Lab Samples:92642677001
Matrix:Water
AnalyzedMDL
Oil and Grease mg/L ND 5.0 12/28/22 00:151.1
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3880341LABORATORY CONTROL SAMPLE:
LCSSpike
Oil and Grease mg/L 34.640 86 78-114
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3880342MATRIX SPIKE SAMPLE:
MSSpike
Result
92641743001
Oil and Grease mg/L 38.138.5 96 78-114ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92642640002
3880343SAMPLE DUPLICATE:
Oil and Grease mg/L 2.1J 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92642677
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
746005
EPA 3005A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92642677001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3880266
Associated Lab Samples:92642677001
Matrix:Water
AnalyzedMDL
Lead ug/L ND 1.0 01/03/23 14:310.89
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3880267LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 102100 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3880268MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92641696001
3880269
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 94 75-12594 1 20100ND93.9 94.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92642677
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
744441
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92642677001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3873013
Associated Lab Samples:92642677001
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 12/20/22 22:480.31
Methyl-tert-butyl ether ug/L ND 1.0 12/20/22 22:480.42
1,2-Dichloroethane-d4 (S)%97 70-130 12/20/22 22:48
4-Bromofluorobenzene (S)%100 70-130 12/20/22 22:48
Toluene-d8 (S)%113 70-130 12/20/22 22:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3873014LABORATORY CONTROL SAMPLE:
LCSSpike
Diisopropyl ether ug/L 51.150 102 70-130
Methyl-tert-butyl ether ug/L 51.450 103 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3873015MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92642837007
3873016
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Diisopropyl ether ug/L 80 104 67-142108 4 3080ND83.0 86.8
Methyl-tert-butyl ether ug/L 80 98 65-14398 0 3080ND78.1 78.1
1,2-Dichloroethane-d4 (S)%94 70-13094
4-Bromofluorobenzene (S)%97 70-13097
Toluene-d8 (S)%98 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92642677
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
744971
SM 2540D-2015
SM 2540D-2015
2540D Total Suspended Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92642677001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3875620
Associated Lab Samples:92642677001
Matrix:Water
AnalyzedMDL
Total Suspended Solids mg/L ND 2.5 12/21/22 14:202.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3875621LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 248250 99 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92642857005
3875876SAMPLE DUPLICATE:
Total Suspended Solids mg/L 229 3 25235
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92642857006
3875877SAMPLE DUPLICATE:
Total Suspended Solids mg/L 1460 2 251430
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 16
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92642677
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
744609
EPA 420.4 Rev 1.0 1993
EPA 420.4 Rev 1.0 1993
420.4 Phenolics
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92642677001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3873499
Associated Lab Samples:92642677001
Matrix:Water
AnalyzedMDL
Phenolics, Total Recoverable mg/L ND 0.020 12/21/22 13:420.0076
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3873500LABORATORY CONTROL SAMPLE:
LCSSpike
Phenolics, Total Recoverable mg/L 0.0530.05 107 90-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3873501MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92641627001
3873502
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenolics, Total
Recoverable mg/L M1,R10.05 72 90-110106 36 100.05ND 0.040 0.057
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3873503MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92641627002
3873504
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenolics, Total
Recoverable mg/L M1,R10.05 163 90-11089 55 100.05ND 0.085 0.048
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 16
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92642677
7971 CONOVER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 16
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92642677
7971 CONOVER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92642677001 746031EFF 121522 EPA 1664B
92642677001 746005 746121EFF 121522 EPA 3005A EPA 6020B
92642677001 744441EFF 121522 EPA 8260D
92642677001 744971EFF 121522 SM 2540D-2015
92642677001 744609 744932EFF 121522 EPA 420.4 Rev 1.0 1993 EPA 420.4 Rev 1.0 1993
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/04/2023 04:24 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 16
Page 14 of 16
Page 15 of 16
Page 16 of 16
#=CL#
February 06, 2023
LIMS USE: FR - BRETT SCHAEFER
LIMS OBJECT ID: 92649783
92649783
Project:
Pace Project No.:
RE:
Brett Schaefer
AECOM
6000 Fairview Road
Suite 200
Charlotte, NC 28210
7971 CONOVER
Dear Brett Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on February 01, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 12
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92649783
7971 CONOVER
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
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North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
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Ohio VAP Certification #: CL0069
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Oregon Certification #: TN200002
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South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 12
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92649783
7971 CONOVER
Lab ID Sample ID Matrix Date Collected Date Received
92649783001 SW CONOVER AIR STACK Air 01/31/23 19:30 02/01/23 13:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 12
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92649783
7971 CONOVER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92649783001 SW CONOVER AIR STACK Method 18 Air MeOH & EtOH 6 PANDBB
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 12
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92649783
7971 CONOVER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92649783001 SW CONOVER AIR STACK
Benzene 3420 ug/m3 02/04/23 16:2963.9Method 18 Air MeOH &
EtOH
Toluene 15300 ug/m3 02/04/23 16:29188Method 18 Air MeOH &
EtOH
Ethylbenzene 2640 ug/m3 02/04/23 16:2986.7Method 18 Air MeOH &
EtOH
m&p-Xylene 10000 ug/m3 02/04/23 16:29173Method 18 Air MeOH &
EtOH
o-Xylene 5030 ug/m3 02/04/23 16:2986.7Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92649783
7971 CONOVER
Sample:SW CONOVER AIR STACK Lab ID:92649783001 Collected:01/31/23 19:30 Received:02/01/23 13:33 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 3420 ug/m3 02/04/23 16:29 71-43-202/04/23 16:2963.9 22.8 100
Toluene 15300 ug/m3 02/04/23 16:29 108-88-302/04/23 16:2918832.8 100
Ethylbenzene 2640 ug/m3 02/04/23 16:29 100-41-402/04/23 16:2986.7 36.2 100
m&p-Xylene 10000 ug/m3 02/04/23 16:29 179601-23-102/04/23 16:2917358.5 100
o-Xylene 5030 ug/m3 02/04/23 16:29 95-47-602/04/23 16:2986.7 35.9 100
Surrogates
1,4-Dichlorobenzene-d4 (IS)101 %02/04/23 16:29 3855-82-102/04/23 16:2960.0-140 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 01:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92649783
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2000196
TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92649783001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3887777-3
Associated Lab Samples:92649783001
Matrix:Air
AnalyzedMDL
Benzene ug/m3 ND 0.639 02/04/23 08:090.228
Toluene ug/m3 ND 1.88 02/04/23 08:090.328
Ethylbenzene ug/m3 ND 0.867 02/04/23 08:090.362
m&p-Xylene ug/m3 ND 1.73 02/04/23 08:090.585
o-Xylene ug/m3 ND 0.867 02/04/23 08:090.359
1,4-Dichlorobenzene-d4 (IS)%95.9 60.0-140 02/04/23 08:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3887777-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3887777-2
Benzene ug/m3 12.012.0 100 70.0-13010112.0 0.266 25
Toluene ug/m3 14.414.1 102 70.0-13010314.5 0.782 25
Ethylbenzene ug/m3 16.916.3 104 70.0-13010316.8 0.515 25
m&p-Xylene ug/m3 36.232.5 111 70.0-13011035.9 0.842 25
o-Xylene ug/m3 17.816.3 109 70.0-13010817.6 0.980 25
1,4-Dichlorobenzene-d4 (IS)%101 60.0-140103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 01:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 12
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92649783
7971 CONOVER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 01:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 12
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92649783
7971 CONOVER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92649783001 2000196 2000196SW CONOVER AIR STACK M18-Mod Method 18 Air MeOH &EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/06/2023 01:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 12
Page 10 of 12
Page 11 of 12
Page 12 of 12
#=CL#
March 31, 2023
LIMS USE: FR - BRETT SCHAEFER
LIMS OBJECT ID: 92658964
92658964
Project:
Pace Project No.:
RE:
Brett Schaefer
AECOM
6000 Fairview Road
Suite 200
Charlotte, NC 28210
7971 CONOVER
Dear Brett Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on March 27, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 12
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92658964
7971 CONOVER
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 12
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92658964
7971 CONOVER
Lab ID Sample ID Matrix Date Collected Date Received
92658964001 CONOVER AIR STACK EFF Air 03/27/23 11:45 03/27/23 12:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 12
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92658964
7971 CONOVER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92658964001 CONOVER AIR STACK EFF Method 18 Air MeOH & EtOH 6 PANSDS
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 12
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92658964
7971 CONOVER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92658964001 CONOVER AIR STACK EFF
Benzene 6010 ug/m3 03/30/23 23:1363.9Method 18 Air MeOH &
EtOH
Toluene 26400 ug/m3 03/30/23 23:13188Method 18 Air MeOH &
EtOH
Ethylbenzene 11700 ug/m3 03/30/23 23:1386.7Method 18 Air MeOH &
EtOH
m&p-Xylene 27200 ug/m3 03/30/23 23:13173Method 18 Air MeOH &
EtOH
o-Xylene 12800 ug/m3 03/30/23 23:1386.7Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92658964
7971 CONOVER
Sample:CONOVER AIR STACK EFF Lab ID:92658964001 Collected:03/27/23 11:45 Received:03/27/23 12:55 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 6010 ug/m3 03/30/23 23:13 71-43-203/30/23 23:1363.9 22.8 100
Toluene 26400 ug/m3 03/30/23 23:13 108-88-303/30/23 23:1318832.8 100
Ethylbenzene 11700 ug/m3 03/30/23 23:13 100-41-403/30/23 23:1386.7 36.2 100
m&p-Xylene 27200 ug/m3 03/30/23 23:13 179601-23-103/30/23 23:1317358.5 100
o-Xylene 12800 ug/m3 03/30/23 23:13 95-47-603/30/23 23:1386.7 35.9 100
Surrogates
4-Bromofluorobenzene (S)101 %03/30/23 23:13 460-00-403/30/23 23:1360.0-140 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2023 05:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658964
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2032762
M18-Mod/TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92658964001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3907455-3
Associated Lab Samples:92658964001
Matrix:Air
AnalyzedMDL
Benzene ug/m3 ND 0.639 03/30/23 10:090.228
Toluene ug/m3 ND 1.88 03/30/23 10:090.328
Ethylbenzene ug/m3 ND 0.867 03/30/23 10:090.362
m&p-Xylene ug/m3 ND 1.73 03/30/23 10:090.585
o-Xylene ug/m3 ND 0.867 03/30/23 10:090.359
4-Bromofluorobenzene (S)%99.4 60.0-140 03/30/23 10:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3907455-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3907455-2
Benzene ug/m3 12.612.0 105 70.0-13010913.0 3.50 25
Toluene ug/m3 14.414.1 102 70.0-13010715.2 5.61 25
Ethylbenzene ug/m3 17.316.3 106 70.0-13010817.6 1.49 25
m&p-Xylene ug/m3 34.732.5 107 70.0-13010634.4 0.753 25
o-Xylene ug/m3 17.316.3 106 70.0-13010517.0 1.26 25
4-Bromofluorobenzene (S)%101 60.0-14097.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2023 05:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 12
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92658964
7971 CONOVER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2023 05:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 12
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92658964
7971 CONOVER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92658964001 2032762 2032762CONOVER AIR STACK EFF M18-Mod Method 18 Air MeOH &EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/31/2023 05:09 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 12
Page 10 of 12
Page 11 of 12
Page 12 of 12
#=CL#
April 05, 2023
LIMS USE: FR - BRETT SCHAEFER
LIMS OBJECT ID: 92658989
92658989
Project:
Pace Project No.:
RE:
Brett Schaefer
AECOM
6000 Fairview Road
Suite 200
Charlotte, NC 28210
7971 CONOVER
Dear Brett Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on March 27, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92658989
7971 CONOVER
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92658989
7971 CONOVER
Lab ID Sample ID Matrix Date Collected Date Received
92658989001 CONOVER EFFLUENT Water 03/27/23 11:30 03/27/23 12:55
92658989002 TRIP BLANK Water 03/27/23 00:00 03/27/23 12:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92658989
7971 CONOVER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92658989001 CONOVER EFFLUENT EPA 6020B 1 PASI-GACW1
EPA 8270E 4 PASI-CPKS
SM 2540D-2015 1 PASI-AJMH1
92658989002 TRIP BLANK EPA 8260D 63 PASI-CCL
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92658989
7971 CONOVER
Sample:CONOVER EFFLUENT Lab ID:92658989001 Collected:03/27/23 11:30 Received:03/27/23 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3005A
Pace Analytical Services - Peachtree Corners, GA
6020 MET ICPMS
Lead ND ug/L 03/31/23 16:57 7439-92-103/30/23 14:301.0 0.89 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Phenol ND ug/L 04/01/23 02:15 108-95-203/31/23 15:509.1 1.2 1
Surrogates
Phenol-d6 (S)56 %04/01/23 02:15 13127-88-303/31/23 15:5010-130 1
2-Fluorophenol (S)70 %04/01/23 02:15 367-12-403/31/23 15:5010-130 1
2,4,6-Tribromophenol (S)105 %04/01/23 02:15 118-79-603/31/23 15:5010-164 1
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
2540D Total Suspended Solids
Total Suspended Solids ND mg/L 03/29/23 10:462.5 2.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92658989
7971 CONOVER
Sample:TRIP BLANK Lab ID:92658989002 Collected:03/27/23 00:00 Received:03/27/23 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/28/23 16:04 67-64-125.0 5.1 1
Benzene ND ug/L 03/28/23 16:04 71-43-21.0 0.34 1
Bromobenzene ND ug/L 03/28/23 16:04 108-86-11.0 0.29 1
Bromochloromethane ND ug/L 03/28/23 16:04 74-97-51.0 0.47 1
Bromodichloromethane ND ug/L 03/28/23 16:04 75-27-41.0 0.31 1
Bromoform ND ug/L 03/28/23 16:04 75-25-21.0 0.34 1
Bromomethane ND ug/L 03/28/23 16:04 74-83-9 v22.0 1.7 1
2-Butanone (MEK)ND ug/L 03/28/23 16:04 78-93-35.0 4.0 1
Carbon tetrachloride ND ug/L 03/28/23 16:04 56-23-51.0 0.33 1
Chlorobenzene ND ug/L 03/28/23 16:04 108-90-71.0 0.28 1
Chloroethane ND ug/L 03/28/23 16:04 75-00-31.0 0.65 1
Chloroform ND ug/L 03/28/23 16:04 67-66-31.0 0.43 1
Chloromethane ND ug/L 03/28/23 16:04 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 03/28/23 16:04 95-49-81.0 0.32 1
4-Chlorotoluene ND ug/L 03/28/23 16:04 106-43-41.0 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 03/28/23 16:04 96-12-82.0 0.34 1
Dibromochloromethane ND ug/L 03/28/23 16:04 124-48-11.0 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 03/28/23 16:04 106-93-41.0 0.27 1
Dibromomethane ND ug/L 03/28/23 16:04 74-95-31.0 0.39 1
1,2-Dichlorobenzene ND ug/L 03/28/23 16:04 95-50-11.0 0.34 1
1,3-Dichlorobenzene ND ug/L 03/28/23 16:04 541-73-11.0 0.34 1
1,4-Dichlorobenzene ND ug/L 03/28/23 16:04 106-46-71.0 0.33 1
Dichlorodifluoromethane ND ug/L 03/28/23 16:04 75-71-81.0 0.35 1
1,1-Dichloroethane ND ug/L 03/28/23 16:04 75-34-31.0 0.37 1
1,2-Dichloroethane ND ug/L 03/28/23 16:04 107-06-21.0 0.32 1
1,1-Dichloroethene ND ug/L 03/28/23 16:04 75-35-41.0 0.35 1
cis-1,2-Dichloroethene ND ug/L 03/28/23 16:04 156-59-21.0 0.38 1
trans-1,2-Dichloroethene ND ug/L 03/28/23 16:04 156-60-51.0 0.40 1
1,2-Dichloropropane ND ug/L 03/28/23 16:04 78-87-51.0 0.36 1
1,3-Dichloropropane ND ug/L 03/28/23 16:04 142-28-91.0 0.28 1
2,2-Dichloropropane ND ug/L 03/28/23 16:04 594-20-7 v21.0 0.39 1
1,1-Dichloropropene ND ug/L 03/28/23 16:04 563-58-61.0 0.43 1
cis-1,3-Dichloropropene ND ug/L 03/28/23 16:04 10061-01-51.0 0.36 1
trans-1,3-Dichloropropene ND ug/L 03/28/23 16:04 10061-02-61.0 0.36 1
Diisopropyl ether ND ug/L 03/28/23 16:04 108-20-31.0 0.31 1
Ethylbenzene ND ug/L 03/28/23 16:04 100-41-41.0 0.30 1
Hexachloro-1,3-butadiene ND ug/L 03/28/23 16:04 87-68-32.0 1.5 1
2-Hexanone ND ug/L 03/28/23 16:04 591-78-65.0 0.48 1
p-Isopropyltoluene ND ug/L 03/28/23 16:04 99-87-61.0 0.41 1
Methylene Chloride ND ug/L 03/28/23 16:04 75-09-25.0 2.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/28/23 16:04 108-10-15.0 2.7 1
Methyl-tert-butyl ether ND ug/L 03/28/23 16:04 1634-04-41.0 0.42 1
Naphthalene ND ug/L 03/28/23 16:04 91-20-31.0 0.64 1
Styrene ND ug/L 03/28/23 16:04 100-42-51.0 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 03/28/23 16:04 630-20-61.0 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92658989
7971 CONOVER
Sample:TRIP BLANK Lab ID:92658989002 Collected:03/27/23 00:00 Received:03/27/23 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,1,2,2-Tetrachloroethane ND ug/L 03/28/23 16:04 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 03/28/23 16:04 127-18-41.0 0.29 1
Toluene ND ug/L 03/28/23 16:04 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/28/23 16:04 87-61-61.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 03/28/23 16:04 120-82-11.0 0.64 1
1,1,1-Trichloroethane ND ug/L 03/28/23 16:04 71-55-61.0 0.33 1
1,1,2-Trichloroethane ND ug/L 03/28/23 16:04 79-00-51.0 0.32 1
Trichloroethene ND ug/L 03/28/23 16:04 79-01-61.0 0.38 1
Trichlorofluoromethane ND ug/L 03/28/23 16:04 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 03/28/23 16:04 96-18-41.0 0.26 1
Vinyl acetate ND ug/L 03/28/23 16:04 108-05-42.0 1.3 1
Vinyl chloride ND ug/L 03/28/23 16:04 75-01-41.0 0.39 1
Xylene (Total)ND ug/L 03/28/23 16:04 1330-20-71.0 0.34 1
m&p-Xylene ND ug/L 03/28/23 16:04 179601-23-12.0 0.71 1
o-Xylene ND ug/L 03/28/23 16:04 95-47-61.0 0.34 1
Surrogates
4-Bromofluorobenzene (S)96 %03/28/23 16:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %03/28/23 16:04 17060-07-070-130 1
Toluene-d8 (S)99 %03/28/23 16:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
764930
EPA 3005A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92658989001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3971901
Associated Lab Samples:92658989001
Matrix:Water
AnalyzedMDL
Lead ug/L ND 1.0 03/31/23 14:480.89
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3971902LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 100100 100 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3972021MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92658210008
3972022
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 101 75-125100 1 20100ND10199.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
764165
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92658989002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3968257
Associated Lab Samples:92658989002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/28/23 14:510.31
1,1,1-Trichloroethane ug/L ND 1.0 03/28/23 14:510.33
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/28/23 14:510.22
1,1,2-Trichloroethane ug/L ND 1.0 03/28/23 14:510.32
1,1-Dichloroethane ug/L ND 1.0 03/28/23 14:510.37
1,1-Dichloroethene ug/L ND 1.0 03/28/23 14:510.35
1,1-Dichloropropene ug/L ND 1.0 03/28/23 14:510.43
1,2,3-Trichlorobenzene ug/L ND 1.0 03/28/23 14:510.81
1,2,3-Trichloropropane ug/L ND 1.0 03/28/23 14:510.26
1,2,4-Trichlorobenzene ug/L ND 1.0 03/28/23 14:510.64
1,2-Dibromo-3-chloropropane ug/L ND 2.0 03/28/23 14:510.34
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/28/23 14:510.27
1,2-Dichlorobenzene ug/L ND 1.0 03/28/23 14:510.34
1,2-Dichloroethane ug/L ND 1.0 03/28/23 14:510.32
1,2-Dichloropropane ug/L ND 1.0 03/28/23 14:510.36
1,3-Dichlorobenzene ug/L ND 1.0 03/28/23 14:510.34
1,3-Dichloropropane ug/L ND 1.0 03/28/23 14:510.28
1,4-Dichlorobenzene ug/L ND 1.0 03/28/23 14:510.33
2,2-Dichloropropane ug/L ND 1.0 v203/28/23 14:510.39
2-Butanone (MEK)ug/L ND 5.0 03/28/23 14:514.0
2-Chlorotoluene ug/L ND 1.0 03/28/23 14:510.32
2-Hexanone ug/L ND 5.0 03/28/23 14:510.48
4-Chlorotoluene ug/L ND 1.0 03/28/23 14:510.32
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/28/23 14:512.7
Acetone ug/L ND 25.0 03/28/23 14:515.1
Benzene ug/L ND 1.0 03/28/23 14:510.34
Bromobenzene ug/L ND 1.0 03/28/23 14:510.29
Bromochloromethane ug/L ND 1.0 03/28/23 14:510.47
Bromodichloromethane ug/L ND 1.0 03/28/23 14:510.31
Bromoform ug/L ND 1.0 03/28/23 14:510.34
Bromomethane ug/L ND 2.0 v203/28/23 14:511.7
Carbon tetrachloride ug/L ND 1.0 03/28/23 14:510.33
Chlorobenzene ug/L ND 1.0 03/28/23 14:510.28
Chloroethane ug/L ND 1.0 03/28/23 14:510.65
Chloroform ug/L ND 1.0 03/28/23 14:510.43
Chloromethane ug/L ND 1.0 03/28/23 14:510.54
cis-1,2-Dichloroethene ug/L ND 1.0 03/28/23 14:510.38
cis-1,3-Dichloropropene ug/L ND 1.0 03/28/23 14:510.36
Dibromochloromethane ug/L ND 1.0 03/28/23 14:510.36
Dibromomethane ug/L ND 1.0 03/28/23 14:510.39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3968257
Associated Lab Samples:92658989002
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 03/28/23 14:510.35
Diisopropyl ether ug/L ND 1.0 03/28/23 14:510.31
Ethylbenzene ug/L ND 1.0 03/28/23 14:510.30
Hexachloro-1,3-butadiene ug/L ND 2.0 03/28/23 14:511.5
m&p-Xylene ug/L ND 2.0 03/28/23 14:510.71
Methyl-tert-butyl ether ug/L ND 1.0 03/28/23 14:510.42
Methylene Chloride ug/L ND 5.0 03/28/23 14:512.0
Naphthalene ug/L ND 1.0 03/28/23 14:510.64
o-Xylene ug/L ND 1.0 03/28/23 14:510.34
p-Isopropyltoluene ug/L ND 1.0 03/28/23 14:510.41
Styrene ug/L ND 1.0 03/28/23 14:510.29
Tetrachloroethene ug/L ND 1.0 03/28/23 14:510.29
Toluene ug/L ND 1.0 03/28/23 14:510.24
trans-1,2-Dichloroethene ug/L ND 1.0 03/28/23 14:510.40
trans-1,3-Dichloropropene ug/L ND 1.0 03/28/23 14:510.36
Trichloroethene ug/L ND 1.0 03/28/23 14:510.38
Trichlorofluoromethane ug/L ND 1.0 03/28/23 14:510.30
Vinyl acetate ug/L ND 2.0 03/28/23 14:511.3
Vinyl chloride ug/L ND 1.0 03/28/23 14:510.39
Xylene (Total)ug/L ND 1.0 03/28/23 14:510.34
1,2-Dichloroethane-d4 (S)%98 70-130 03/28/23 14:51
4-Bromofluorobenzene (S)%97 70-130 03/28/23 14:51
Toluene-d8 (S)%99 70-130 03/28/23 14:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3968258LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 20.320 102 70-130
1,1,1-Trichloroethane ug/L 19.420 97 70-130
1,1,2,2-Tetrachloroethane ug/L 19.920 100 70-130
1,1,2-Trichloroethane ug/L 19.020 95 70-130
1,1-Dichloroethane ug/L 18.320 92 70-130
1,1-Dichloroethene ug/L 18.020 90 70-130
1,1-Dichloropropene ug/L 19.220 96 70-130
1,2,3-Trichlorobenzene ug/L 19.920 100 70-130
1,2,3-Trichloropropane ug/L 18.620 93 70-130
1,2,4-Trichlorobenzene ug/L 19.420 97 70-130
1,2-Dibromo-3-chloropropane ug/L 20.320 101 70-131
1,2-Dibromoethane (EDB)ug/L 19.620 98 70-130
1,2-Dichlorobenzene ug/L 19.720 98 70-130
1,2-Dichloroethane ug/L 18.220 91 70-130
1,2-Dichloropropane ug/L 18.520 93 70-130
1,3-Dichlorobenzene ug/L 19.520 98 70-130
1,3-Dichloropropane ug/L 19.120 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3968258LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 18.820 94 70-130
2,2-Dichloropropane ug/L 14.5 v3207368-135
2-Butanone (MEK)ug/L 33.240 83 70-134
2-Chlorotoluene ug/L 18.920 94 70-130
2-Hexanone ug/L 37.040 93 70-131
4-Chlorotoluene ug/L 18.920 94 70-130
4-Methyl-2-pentanone (MIBK)ug/L 35.740 89 70-130
Acetone ug/L 33.240 83 70-133
Benzene ug/L 18.720 94 70-130
Bromobenzene ug/L 19.720 98 70-130
Bromochloromethane ug/L 19.220 96 70-130
Bromodichloromethane ug/L 19.120 95 70-130
Bromoform ug/L 20.620 103 70-130
Bromomethane ug/L 14.4 v3207245-151
Carbon tetrachloride ug/L 20.620 103 70-130
Chlorobenzene ug/L 19.620 98 70-130
Chloroethane ug/L 18.420 92 39-152
Chloroform ug/L 18.620 93 70-130
Chloromethane ug/L 20.620 103 58-130
cis-1,2-Dichloroethene ug/L 18.120 90 70-130
cis-1,3-Dichloropropene ug/L 17.820 89 70-130
Dibromochloromethane ug/L 20.220 101 70-130
Dibromomethane ug/L 20.120 101 70-130
Dichlorodifluoromethane ug/L 23.120 115 54-133
Diisopropyl ether ug/L 16.720 84 70-130
Ethylbenzene ug/L 19.020 95 70-130
Hexachloro-1,3-butadiene ug/L 19.920 99 70-135
m&p-Xylene ug/L 38.240 96 70-130
Methyl-tert-butyl ether ug/L 17.320 86 70-130
Methylene Chloride ug/L 17.820 89 66-130
Naphthalene ug/L 19.920 99 70-130
o-Xylene ug/L 19.220 96 70-130
p-Isopropyltoluene ug/L 19.420 97 70-130
Styrene ug/L 19.920 99 70-130
Tetrachloroethene ug/L 19.420 97 70-130
Toluene ug/L 18.820 94 70-130
trans-1,2-Dichloroethene ug/L 18.420 92 70-130
trans-1,3-Dichloropropene ug/L 18.520 92 70-130
Trichloroethene ug/L 19.520 98 70-130
Trichlorofluoromethane ug/L 19.820 99 62-130
Vinyl acetate ug/L 34.640 87 70-144
Vinyl chloride ug/L 16.620 83 62-130
Xylene (Total)ug/L 57.460 96 70-130
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3968259MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92658924015
3968260
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 99 70-141111 12 3020ND19.7 22.1
1,1,1-Trichloroethane ug/L 20 99 70-150116 16 3020ND19.8 23.1
1,1,2,2-Tetrachloroethane ug/L 20 102 69-142116 13 3020ND20.3 23.2
1,1,2-Trichloroethane ug/L 20 105 70-138109 4 3020ND21.0 21.8
1,1-Dichloroethane ug/L 20 91 70-150112 21 3020ND18.3 22.5
1,1-Dichloroethene ug/L 20 79 70-15692 16 3020ND15.7 18.4
1,1-Dichloropropene ug/L 20 103 70-150122 17 3020ND20.6 24.5
1,2,3-Trichlorobenzene ug/L 20 95 70-148117 20 3020ND19.0 23.3
1,2,3-Trichloropropane ug/L 20 98 70-140110 11 3020ND19.7 21.9
1,2,4-Trichlorobenzene ug/L 20 94 70-146118 22 3020ND18.9 23.6
1,2-Dibromo-3-
chloropropane ug/L 20 96 68-146115 19 3020ND19.1 23.0
1,2-Dibromoethane (EDB)ug/L 20 101 70-138107 5 3020ND20.3 21.3
1,2-Dichlorobenzene ug/L 20 97 70-141117 18 3020ND19.4 23.3
1,2-Dichloroethane ug/L 20 96 69-143113 16 3020ND19.3 22.7
1,2-Dichloropropane ug/L 20 96 68-156114 17 3020ND19.3 22.9
1,3-Dichlorobenzene ug/L 20 99 70-143116 17 3020ND19.7 23.3
1,3-Dichloropropane ug/L 20 95 70-138102 7 3020ND19.1 20.4
1,4-Dichlorobenzene ug/L 20 99 70-142114 14 3020ND19.9 22.9
2,2-Dichloropropane ug/L 20 102 52-170118 15 3020ND20.4 23.6
2-Butanone (MEK)ug/L 40 99 60-157109 10 3040ND39.7 43.6
2-Chlorotoluene ug/L 20 98 70-147116 17 3020ND19.7 23.3
2-Hexanone ug/L 40 104 68-146114 9 3040ND41.4 45.4
4-Chlorotoluene ug/L 20 100 70-142119 17 3020ND20.1 23.8
4-Methyl-2-pentanone
(MIBK)ug/L 40 104 70-141103 1 3040ND41.8 41.2
Acetone ug/L 40 80 58-15789 11 3040ND31.9 35.6
Benzene ug/L 20 96 70-142110 14 3020ND19.2 22.0
Bromobenzene ug/L 20 96 70-143113 16 3020ND19.3 22.7
Bromochloromethane ug/L 20 100 70-146117 16 3020ND19.9 23.3
Bromodichloromethane ug/L 20 91 70-139108 17 3020ND18.3 21.6
Bromoform ug/L 20 97 64-140110 13 3020ND19.3 22.0
Bromomethane ug/L 20 52 28-19263 20 3020ND10.4 12.6
Carbon tetrachloride ug/L 20 99 70-148109 9 3020ND19.8 21.7
Chlorobenzene ug/L 20 97 70-141113 15 3020ND19.4 22.5
Chloroethane ug/L 20 73 58-19185 15 3020ND14.6 16.9
Chloroform ug/L 20 99 70-148117 17 3020ND19.8 23.4
Chloromethane ug/L 20 50 43-16255 10 3020ND1011.0
cis-1,2-Dichloroethene ug/L 20 99 68-151115 13 30201.9 21.8 24.9
cis-1,3-Dichloropropene ug/L 20 101 70-139113 11 3020ND20.3 22.6
Dibromochloromethane ug/L 20 97 70-144107 10 3020ND19.3 21.4
Dibromomethane ug/L 20 94 70-139109 15 3020ND18.7 21.7
Dichlorodifluoromethane ug/L M1,v3203439-17138 11 3020ND6.8 7.6
Diisopropyl ether ug/L 20 83 67-142105 23 3020ND16.6 21.0
Ethylbenzene ug/L 20 98 70-143113 15 3020ND19.6 22.7
Hexachloro-1,3-butadiene ug/L 20 99 64-163122 21 3020ND19.8 24.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
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[phone]
Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3968259MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92658924015
3968260
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 98 70-144113 14 3040ND39.1 45.1
Methyl-tert-butyl ether ug/L 20 80 65-14395 17 3020ND16.1 19.0
Methylene Chloride ug/L v1209562-149110 15 3020ND19.0 22.1
Naphthalene ug/L 20 98 67-147124 23 3020ND19.6 24.8
o-Xylene ug/L 20 100 70-145115 15 3020ND19.9 23.0
p-Isopropyltoluene ug/L 20 103 70-147122 17 3020ND20.7 24.5
Styrene ug/L 20 101 70-143117 15 3020ND20.3 23.4
Tetrachloroethene ug/L 20 96 70-145100 5 3020ND19.1 20.1
Toluene ug/L 20 100 70-142112 11 3020ND20.1 22.5
trans-1,2-Dichloroethene ug/L 20 89 70-151102 14 3020ND17.8 20.4
trans-1,3-Dichloropropene ug/L 20 102 70-139107 5 3020ND20.4 21.5
Trichloroethene ug/L 20 98 62-146114 15 3020ND19.6 22.7
Trichlorofluoromethane ug/L v3207563-15385 12 3020ND15.0 17.0
Vinyl acetate ug/L 40 93 61-162108 15 3040ND37.2 43.2
Vinyl chloride ug/L M1,v3204861-16354 10 30200.81J 10.5 11.6
Xylene (Total)ug/L 60 98 70-143114 14 3060ND59.0 68.2
1,2-Dichloroethane-d4 (S)%103 70-130102
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%104 70-130101
REPORT OF LABORATORY ANALYSIS
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Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
765090
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92658989001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3972715
Associated Lab Samples:92658989001
Matrix:Water
AnalyzedMDL
Phenol ug/L ND 10.0 03/31/23 21:071.4
2,4,6-Tribromophenol (S)%107 10-164 03/31/23 21:07
2-Fluorobiphenyl (S)%87 10-130 03/31/23 21:07
2-Fluorophenol (S)%68 10-130 03/31/23 21:07
Nitrobenzene-d5 (S)%92 10-138 03/31/23 21:07
Phenol-d6 (S)%56 10-130 03/31/23 21:07
Terphenyl-d14 (S)%106 19-191 03/31/23 21:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3972716LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol ug/L 30.950 62 19-130
2,4,6-Tribromophenol (S)%129 10-164
2-Fluorobiphenyl (S)%97 10-130
2-Fluorophenol (S)%81 10-130
Nitrobenzene-d5 (S)%104 10-138
Phenol-d6 (S)%72 10-130
Terphenyl-d14 (S)%126 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3973193MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92659368001
3973194
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol ug/L R1502110-13037 55 3050ND10.6 18.7
2,4,6-Tribromophenol (S)%14 10-16427
2-Fluorobiphenyl (S)%47 10-13087
2-Fluorophenol (S)%S0810-13017
Nitrobenzene-d5 (S)%50 10-13891
Phenol-d6 (S)%19 10-13033
Terphenyl-d14 (S)%81 19-19194
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3973964MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92659546005
3973965
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol ug/L 100 56 10-13068 19 30100ND56.1 67.7
REPORT OF LABORATORY ANALYSIS
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Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3973964MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92659546005
3973965
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4,6-Tribromophenol (S)%86 10-16491
2-Fluorobiphenyl (S)%79 10-13074
2-Fluorophenol (S)%63 10-13065
Nitrobenzene-d5 (S)%93 10-13890
Phenol-d6 (S)%51 10-13057
Terphenyl-d14 (S)%84 19-19186
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92658989
7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
764530
SM 2540D-2015
SM 2540D-2015
2540D Total Suspended Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92658989001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3969944
Associated Lab Samples:92658989001
Matrix:Water
AnalyzedMDL
Total Suspended Solids mg/L ND 2.5 03/29/23 10:432.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3969945LABORATORY CONTROL SAMPLE:
LCSSpike
Total Suspended Solids mg/L 240250 96 90-110
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92658936001
3970016SAMPLE DUPLICATE:
Total Suspended Solids mg/L 364 1 25362
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92659144001
3970017SAMPLE DUPLICATE:
Total Suspended Solids mg/L 183 8 25169
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
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Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92658989
7971 CONOVER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
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Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92658989
7971 CONOVER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92658989001 764930 765032CONOVER EFFLUENT EPA 3005A EPA 6020B
92658989001 765090 765320CONOVER EFFLUENT EPA 3510C EPA 8270E
92658989002 764165TRIP BLANK EPA 8260D
92658989001 764530CONOVER EFFLUENT SM 2540D-2015
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/05/2023 04:33 PM
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[phone]
Page 18 of 21
Page 19 of 21
Page 20 of 21
Page 21 of 21
#=CL#
June 26, 2023
LIMS USE: FR - BRETT SCHAEFER
LIMS OBJECT ID: 92673416
92673416
Project:
Pace Project No.:
RE:
Brett Schaefer
AECOM
6000 Fairview Rd
Suite 200
Charlotte, NC 28210
Speedway 7971 CONOVER
Dear Brett Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on June 20, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 13
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Lab ID Sample ID Matrix Date Collected Date Received
92673416001 CONOVER AIR STACK EFF Air 06/20/23 10:45 06/20/23 12:29
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92673416001 CONOVER AIR STACK EFF Method 18 Air MeOH & EtOH 6 PANAA, DAH
PAN = Pace National - Mt. Juliet
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 13
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92673416001 CONOVER AIR STACK EFF
Benzene 7220 ug/m3 06/23/23 04:4563.9Method 18 Air MeOH &
EtOH
Toluene 38400 ug/m3 06/23/23 19:48753Method 18 Air MeOH &
EtOH
Ethylbenzene 5770 ug/m3 06/23/23 04:4586.7Method 18 Air MeOH &
EtOH
m&p-Xylene 21900 ug/m3 06/23/23 04:45173Method 18 Air MeOH &
EtOH
o-Xylene 10300 ug/m3 06/23/23 04:4586.7Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 5 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Sample:CONOVER AIR STACK EFF Lab ID:92673416001 Collected:06/20/23 10:45 Received:06/20/23 12:29 Matrix:Air
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: Method 18 Air MeOH & EtOH Preparation Method: M18-Mod
Pace National - Mt. Juliet
VOA (MS) M18-Mod
Benzene 7220 ug/m3 06/23/23 04:45 71-43-206/23/23 04:4563.9 22.8 100
Toluene 38400 ug/m3 06/23/23 19:48 108-88-306/23/23 19:48753131400
Ethylbenzene 5770 ug/m3 06/23/23 04:45 100-41-406/23/23 04:4586.7 36.2 100
m&p-Xylene 21900 ug/m3 06/23/23 04:45 179601-23-106/23/23 04:4517358.5 100
o-Xylene 10300 ug/m3 06/23/23 04:45 95-47-606/23/23 04:4586.7 35.9 100
Surrogates
4-Bromofluorobenzene (S)106 %06/23/23 04:45 460-00-406/23/23 04:4560.0-140 100
4-Bromofluorobenzene (S)97.2 %06/23/23 19:48 460-00-406/23/23 19:4860.0-140 400
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 11:10 AM
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Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2082610
TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92673416001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3940171-3
Associated Lab Samples:92673416001
Matrix:Air
AnalyzedMDL
Benzene ug/m3 ND 0.639 06/22/23 10:200.228
Ethylbenzene ug/m3 ND 0.867 06/22/23 10:200.362
m&p-Xylene ug/m3 ND 1.73 06/22/23 10:200.585
o-Xylene ug/m3 ND 0.867 06/22/23 10:200.359
4-Bromofluorobenzene (S)%95.9 60.0-140 06/22/23 10:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3940171-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3940171-2
Benzene ug/m3 12.612.0 105 70.0-13010612.7 1.01 25
Ethylbenzene ug/m3 17.716.3 109 70.0-13011017.9 1.46 25
m&p-Xylene ug/m3 36.632.5 113 70.0-13011537.3 1.76 25
o-Xylene ug/m3 18.216.3 112 70.0-13011418.5 1.42 25
4-Bromofluorobenzene (S)%102 60.0-140102
REPORT OF LABORATORY ANALYSIS
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Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2083273
TO-15
Method 18 Air MeOH & EtOH
VOA (MS) M18-Mod
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92673416001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3940558-3
Associated Lab Samples:92673416001
Matrix:Air
AnalyzedMDL
Toluene ug/m3 ND 1.88 06/23/23 09:230.328
4-Bromofluorobenzene (S)%92 60.0-140 06/23/23 09:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3940558-1LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3940558-2
Toluene ug/m3 14.814.1 105 70.0-13010615.0 1.01 25
4-Bromofluorobenzene (S)%101 60.0-14098.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 11:10 AM
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Page 8 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 11:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 13
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92673416
Speedway 7971 CONOVER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92673416001 2082610 2082610CONOVER AIR STACK EFF M18-Mod Method 18 Air MeOH &EtOH
92673416001 2083273 2083273CONOVER AIR STACK EFF M18-Mod Method 18 Air MeOH &
EtOH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 11:10 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 13
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#=CL#
June 26, 2023
LIMS USE: FR - BRETT SCHAEFER
LIMS OBJECT ID: 92673422
92673422
Project:
Pace Project No.:
RE:
Brett Schaefer
AECOM
6000 Fairview Rd
Suite 200
Charlotte, NC 28210
Speedway 7971 CONOVER
Dear Brett Schaefer:
Enclosed are the analytical results for sample(s) received by the laboratory on June 20, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Bonnie Vang
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 14
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 14
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Lab ID Sample ID Matrix Date Collected Date Received
92673422001 CONOVER EFFLUENT Water 06/20/23 10:20 06/20/23 12:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 14
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92673422001 CONOVER EFFLUENT EPA 6010D 1 PASI-ADBB1
EPA 8270E 4 PASI-CPKS
SM 2540D-2015 1 PASI-AMAB2
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 14
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92673422001 CONOVER EFFLUENT
Total Suspended Solids 2.5 mg/L 06/23/23 14:402.5SM 2540D-2015
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 14
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Sample:CONOVER EFFLUENT Lab ID:92673422001 Collected:06/20/23 10:20 Received:06/20/23 12:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6010 MET ICP
Lead ND ug/L 06/22/23 14:40 7439-92-106/21/23 10:505.0 4.5 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Phenol ND ug/L 06/24/23 15:48 108-95-206/22/23 16:228.7 1.2 1
Surrogates
Phenol-d6 (S)36 %06/24/23 15:48 13127-88-306/22/23 16:2210-130 1
2-Fluorophenol (S)48 %06/24/23 15:48 367-12-406/22/23 16:2210-130 1
2,4,6-Tribromophenol (S)84 %06/24/23 15:48 118-79-606/22/23 16:2210-164 1
Analytical Method: SM 2540D-2015
Pace Analytical Services - Asheville
2540D Total Suspended Solids
Total Suspended Solids 2.5 mg/L 06/23/23 14:402.5 2.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 01:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
781913
EPA 3010A
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92673422001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4056224
Associated Lab Samples:92673422001
Matrix:Water
AnalyzedMDL
Lead ug/L ND 5.0 06/22/23 13:534.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4056225LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 526500 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4056226MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92673295001
4056227
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 500 93 75-12596 3 205000.012
mg/L 479 493
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 01:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782338
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92673422001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4058250
Associated Lab Samples:92673422001
Matrix:Water
AnalyzedMDL
Phenol ug/L ND 10.0 06/23/23 10:431.4
2,4,6-Tribromophenol (S)%56 10-164 06/23/23 10:43
2-Fluorobiphenyl (S)%42 10-130 06/23/23 10:43
2-Fluorophenol (S)%37 10-130 06/23/23 10:43
Nitrobenzene-d5 (S)%46 10-138 06/23/23 10:43
Phenol-d6 (S)%30 10-130 06/23/23 10:43
Terphenyl-d14 (S)%58 19-191 06/23/23 10:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4058251LABORATORY CONTROL SAMPLE:
LCSSpike
Phenol ug/L 33.750 67 19-130
2,4,6-Tribromophenol (S)%100 10-164
2-Fluorobiphenyl (S)%85 10-130
2-Fluorophenol (S)%64 10-130
Nitrobenzene-d5 (S)%77 10-138
Phenol-d6 (S)%52 10-130
Terphenyl-d14 (S)%93 19-191
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4058252MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35806987005
4058253
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Phenol ug/L 83.3 32 10-13031 3083.35.6U 26.4J 25.7J
2,4,6-Tribromophenol (S)%13 10-16425
2-Fluorobiphenyl (S)%64 10-13039
2-Fluorophenol (S)%12 10-13017
Nitrobenzene-d5 (S)%D36110-13838
Phenol-d6 (S)%27 10-13022
Terphenyl-d14 (S)%72 19-19141
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 01:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 14
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
782587
SM 2540D-2015
SM 2540D-2015
2540D Total Suspended Solids
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92673422001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4059452
Associated Lab Samples:92673422001
Matrix:Water
AnalyzedMDL
Total Suspended Solids mg/L ND 2.5 06/23/23 14:332.5
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4059453LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
4060095
Total Suspended Solids mg/L 240250 96 90-11091226 6 25
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92673429001
4060096SAMPLE DUPLICATE:
Total Suspended Solids mg/L 49.3 3 2548.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 01:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 14
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 01:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 14
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92673422
Speedway 7971 CONOVER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92673422001 781913 782012CONOVER EFFLUENT EPA 3010A EPA 6010D
92673422001 782338 782473CONOVER EFFLUENT EPA 3510C EPA 8270E
92673422001 782587CONOVER EFFLUENT SM 2540D-2015
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 06/26/2023 01:07 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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