24010_Yandle-Witherspoon Final Grade Assessment_20231023

Via Email
October 10, 2023

NCDEQ – Division of Waste Management
Brownfields Redevelopment Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Attn: Mr. Bill Schmithorst

Re: Final Grade Soil Assessment Report
Yandle Witherspoon Supply Inc.
N. Brevard Street and Belmont Avenue
Charlotte, North Carolina
Brownfields Project No. 24010-20-060
H&H Project No. TCR-001

Dear Bill:

On behalf of AOP II Apartments Venture, LLC, enclosed please find a copy of the Final Grade Soil
Assessment Report prepared for the Yandle Witherspoon Supply Inc. Brownfields property
(Brownfields Project No. 24010-20-060) located in Charlotte, Mecklenburg County.

Should you have questions or need additional information, please do not hesitate to contact us.

Sincerely,
Hart & Hickman, PC
Haley Martin, PG Ralph McGee, PG
Senior Project Geologist Senior Project Manager

Enclosures

cc: Mr. Justin Adams, Trammell Crow Residential (via Email)
Mr. Garrett Wright, Trammell Crow Residential (via Email)
Mr. Jonathan Wells, KMCL, LLP (via Email)

Attachment:
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Final Grade Soil Assessment Report
Yandle Witherspoon Supply Inc. - Optimist II Apartments
Charlotte, North Carolina
Brownfields Project No. 24010-20-060
H&H Job No. TCR-001

Table of Contents

1.0 Introduction 1 
2.0 Final Grade Soil Assessment Activities ................................................................................ 3 
2.1 Final Grade Soil Sampling Methodologies .......................................................................... 3 
2.2 Soil Sample Results .............................................................................................................. 5 
2.3 Soil Direct Exposure Risk Evaluation .................................................................................. 6 
3.0 Summary and Conclusions ................................................................................................... 8 

List of Tables

Table 1 Summary of Final Grade Soil Sampling Lithology
Table 2 Summary of Final Grade Soil Analytical Results

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Final Grade Soil Sample Location Map

List of Appendices

Appendix A Final Planting Plan
Appendix B Laboratory Analytical Report
Appendix C DEQ Risk Calculators

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Final Grade Soil Assessment Report
Yandle Witherspoon Supply Inc. - Optimist II Apartments
Charlotte, North Carolina
Brownfields Project No. 24010-20-060
H&H Job No. TCR-001

1.0 Introduction

On behalf of AOP II Apartments Venture LLC, Hart & Hickman, PC (H&H) has prepared this
report to document final grade soil assessment activities recently completed on a portion of the
Yandle-Witherspoon Supply Inc. Brownfields property (Brownfields Project No. 24010-20-060)
located at N. Brevard Street and Belmont Avenue in Charlotte, Mecklenburg County, North
Carolina. The Yandle-Witherspoon Supply Inc. Brownfields property consists of two (2)
contiguous parcels (Mecklenburg County Parcel Identification Nos. {PINs} 08104106 and
08104107) that collectively total approximately 5.6 acres of land. The Optimist II apartments were
constructed on PIN 08104106 which comprises approximately 4.2 acres of the larger Yandle-
Witherspoon Supply Inc. Brownfields property (Site or subject Site). Redevelopment plans for
remaining portions of the Yandle-Witherspoon Supply Inc. Brownfields property include the
construction of a multi-story commercial building. A Site location map is provided as Figure 1,
and the Site and surrounding area are shown in Figure 2.

Redevelopment of the Site has included the construction of a multifamily residential apartment
building and an associated parking deck. A copy of the Final Planting Plan prepared by Land
Design on August 16, 2021, depicts the proposed redevelopment layout and is provided in
Appendix A. Redevelopment activities at the Site are nearing completion and have been
completed in accordance with the North Carolina Department of Environmental Quality (DEQ)
approved Environmental Management Plan (EMP) dated August 11, 2021.

The EMP for the Site generally states that no occupancy of the Brownfields property may occur
after redevelopment until representative final grade soil samples have been collected in areas at
the Site that are not covered by building foundations, sidewalks, or asphalt or concrete parking
areas and driveways. In accordance with the DEQ-approved EMP, H&H prepared a Final Grade
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Soil Assessment Work Plan (Work Plan) for DEQ review and approval. The Work Plan was
approved by DEQ in a letter dated August 24, 2023. A summary of the final grade sampling
activities is provided in the following sections.

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2.0 Final Grade Soil Assessment Activities

Final grade soil sampling activities were conducted at the Site in August 2023 to evaluate potential
soil direct exposure risks within areas at the Site not will not be covered with impervious materials
upon completion of redevelopment activities. The final grade soil sampling activities were
conducted in general accordance with the DEQ Inactive Hazardous Sites Branch (IHSB)
Guidelines for Assessment and Cleanup of Contaminated Sites (Guidelines) dated September
2022, the most recent versions of the U.S. Environmental Protection Agency (EPA) Region IV
Laboratory Services and Applied Science Division (LSASD) Field Branches Quality System and
Technical Procedures guidance, and the DEQ-approved Work Plan.

2.1 Final Grade Soil Sampling Activities

The Site is predominately covered with hardscape surfaces except for generally isolated or narrow
landscaped areas. To evaluate for the potential presence of shallow soil impacts, landscaped areas
were divided into five evaluation areas (FG-1 through FG-5). Five shallow soil borings were
advanced in each area for collection of aliquot soil samples. The five final grade evaluation areas
and aliquot soil boring locations (designated as “A” through “E” within each evaluation area) are
shown in Figure 3 and are described further below:

 Final grade evaluation area FG-1 includes vegetated areas along the northwestern side of
the parking deck;
 Final grade evaluation area FG-2 includes landscaped areas along the southwestern side of
the apartment building;
 Final grade evaluation area FG-3 includes landscaped areas along the southeastern side of
the apartment building;
 Final grade evaluation area FG-4 includes landscaped areas in the northeastern portion of
the Site on either side of a newly paved asphalt access drive; and
 Final grade evaluation area FG-5 includes landscaped areas within two courtyards located
in the central portion of the Site.

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Each aliquot soil boring was advanced from the surface to approximately two (2) feet below the
ground surface (ft bgs) utilizing a decontaminated stainless steel hand auger. Continuous soil
samples were collected from the center of the hand auger bucket at each boring location. The soil
samples were described for lithologic purposes, observed for obvious evidence of staining and
unusual odors, and field screened for the presence of volatile organic vapors using a calibrated
photoionization detector (PID). Soil lithology generally consisted of moist silt with clay, sand,
and some gravel. Field screening results did not identify obvious evidence of potential impacts in
soil samples collected at the Site. Lithologic descriptions and field screening results for each final
grade aliquot boring are summarized in Table 1.

Soil sample aliquots from each evaluation area were combined and homogenized to form one
composite soil sample representative of shallow soil in that evaluation area. Composite soil
samples selected for laboratory analysis were collected directly into dedicated laboratory supplied
sample containers, labeled with the sample identification, date, and requested analyses, and placed
in a laboratory supplied cooler with ice. The samples were delivered to Waypoint Analytical
(Waypoint) under standard chain of custody protocols for analysis of semi-volatile organic
compounds (SVOCs) by EPA Method 8270 and Resource Conservation and Recovery Act
(RCRA) metals plus hexavalent chromium by EPA Methods 6020/7471/7199.

In addition to the composite soil samples described above, one representative grab soil sample was
collected from each evaluation area from undisturbed portions of soil in the hand auger bucket.
The grab soil samples were placed directly into laboratory supplied glassware, labeled, and placed
in the laboratory supplied sample cooler with ice. The grab soil samples were submitted to
Waypoint for analysis of volatile organic compounds (VOCs) by EPA Method 8260.

For quality assurance and quality control purposes, H&H collected one duplicate soil sample (FG-
DUP) from evaluation area FG-3

Following sampling activities, the soil borings were abandoned, and the surfaces were repaired
similar to pre-drilling conditions. Additionally, the soil boring locations were estimated using a
hand-held global positioning system (GPS) unit.
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2.2 Final Grade Soil Sample Results

A tabular summary of the final grade soil sample analytical results is presented in Table 2, and a
copy of the laboratory analytical report and chain of custody record is provided in Appendix B.
The laboratory analytical results were compared to the DEQ Residential Preliminary Soil
Remediation goals (PSRGs) dated July 2023. In addition to the PSRGs, metals results were
compared to area-specific and published concentrations for naturally occurring metals in North
Carolina soil.

VOCs
Laboratory analytical results indicate that trace levels of acetone and/or n-hexane were detected at
concentrations above the laboratory method detection limits, but well below the DEQ Residential
PSRGs in select final grade soil samples. No other VOCs were detected at concentrations above
the laboratory method detection limits, and no VOCs were detected at concentrations above the
DEQ Residential PSRGs in final grade soil samples collected at the Site.

SVOCs
Laboratory analytical results indicate that low levels of the polynuclear aromatic hydrocarbons
(PAHs) benzo(a) pyrene (up to 0.625 J milligrams per kilogram [mg/kg]) was detected at
concentrations above the DEQ Residential PSRG of 0.11 mg/kg in final grade soil samples FG-1,
FG-2, and FG-3/FG-DUP. Note that the J-flag designation indicates that the compound was
detected at a concentration above the laboratory method detection limit, but below the laboratory
reporting limit and is a laboratory estimated value. Concentrations of several PAHs including
benzo(a) pyrene (6.69 mg/kg), benzo(a)anthracene (6.76 mg/kg), benzo(b)fluoranthene (7.49
mg/kg), and indeno(1,2,3-cd)pyrene (3.88 mg/kg) were detected at concentrations above the DEQ
Residential PSRGs in final grade soil sample FG-4. No other SVOCs were detected at
concentrations above the DEQ Residential PSRGs in the final grade soil samples.

Metals
Several metals including arsenic (up to 1.36 mg/kg), barium (up to 98.7 mg/kg), cadmium (up to
0.143 J mg/kg), trivalent chromium (up to 41.1 mg/kg), hexavalent chromium (0.244 J mg/kg).
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lead 38.9 mg/kg), mercury (up to 0.100 mg/kg), selenium (up to 0.682 mg/kg), and silver (up to
0.0390 J mg/kg) were detected at concentrations consistent with naturally occurring levels and are
considered to be representative of background conditions at the Site.

2.3 Soil Direct Exposure Risk Evaluation

The DEQ PSRGs are very conservative and based upon a Target Cancer Risk (TCR) of 1 x 10-6
for potential carcinogenic effects and a Hazard Quotient (HQ) of 0.2 for potential non-carcinogenic
effects. DEQ and EPA acceptable soil direct exposure risks include a calculated cumulative
lifetime incremental carcinogenic risk (LICR) of 1 x 10-4 or less and a calculated cumulative hazard
index (HI) of 1.0 or less for potential non-carcinogenic risks.

H&H utilized the DEQ Risk Calculator (July 2023) under a residential land use to further evaluate
potential cumulative risks for the soil direct exposure pathway. To model the potential risks under
a hypothetical “worst-case” scenario, H&H conservatively calculated the cumulative risks using
the highest concentration of any compound detected in any final grade soil sample collected at the
Site. In addition, H&H evaluated potential risks for each final grade evaluation area individually.
Risk calculator results are summarized in the table below and copies of the completed risk
calculators are provided in Appendix C.

Evaluation Area Land Use Calculated
Cumulative LICR
Calculated
Cumulative HI
Exceeds
Acceptable Risk
Levels?
FG-1 Residential 4.5 x 10-6 0.063 No
FG-2 Residential 9.1 x 10-6 0.10 No
FG-3 Residential 7.1 x 10-6 0.08 No
FG-4 Residential 7.6 x 10-5 0.46 No
FG-5 Residential 7.5 x 10-7 0.035 No
Cumulative Worst Case Residential 7.8 x 10-5 0.48 No

As shown in the table above, the results of the risk calculations indicate that the calculated
cumulative soil direct exposure risks do not exceed acceptable carcinogenic or noncarcinogenic
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risk levels under a residential use scenario. The Site-wide cumulative risk calculations are
primarily driven by PAH concentrations detected in the FG-4 final grade soil sample. The aliquot
soil borings for the FG-4 final grade soil sample were advanced adjacent to a newly paved asphalt
access drive. H&H attributes the higher concentrations of PAHs in the FG-4 final grade soil
sample to drift associated with recently completed asphalt paving activities within the evaluation
area.

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3.0 Summary and Conclusions

H&H has completed final grade soil sampling activities at the Optimist II apartments portion of
the Yandle Witherspoon Supply Inc. Brownfields property (Brownfields Project No. 24010-20-
060) located at N. Brevard Street and Belmont Avenue in Charlotte, North Carolina. The final
grade soil sampling activities were conducted in general accordance with the DEQ Brownfields
approved Work Plan dated August 24, 2023. Final grade soil sampling activities included the
collection of soil samples to evaluate potential soil direct exposure risks in areas at the Site that
will not be covered by impervious surfaces following completion of redevelopment.

The Site was divided into five final grade evaluation areas and shallow soil samples were collected
for laboratory analysis within each area. Final grade soil sample laboratory analytical results
indicate that several organic compounds were detected at concentrations above the laboratory
method detection limits in each final grade evaluation area. No compounds were detected at
concentrations above the DEQ Residential PSRGs except for background levels of benzo(a)pyrene
in evaluation areas FG-1 through FG-3 and FG-5. Several PAHs were detected at concentrations
above the DEQ Residential PSRGs in final grade soil sample FG-4 collected adjacent to a newly
paved asphalt access drive located in the northeastern portion of the Site. Concentrations of PAHs
detected in the FG-4 final grade soil sample appear to be attributable to drift associated with asphalt
paving activities recently completed adjacent to the FG-4 soil boring locations. Metals
concentrations detected in the final grade soil sample are consistent with published and area-
specific background concentrations and are considered representative of naturally occurring levels.

H&H utilized the most recent version of the DEQ Risk Calculator to further evaluate potential soil
direct exposure risks for a residential occupant. The risk calculations were completed for each
final grade evaluation area individually as well as a hypothetical worst-case scenario using the
highest concentration of any compound detected in any final grade evaluation area.

Results of the residential soil direct exposure risk calculations confirm that cumulative risks are
within acceptable levels for a future residential occupant.

Tables

Table 1 Summary of Final Grade Soil Sampling LithologyYandle-Witherspoon Supply, Inc.Charlotte, North CarolinaH&H Project No. TCR-001Composite Sample AreaComposite Sample AliquotSample DateAliquot Selected for VOC AnalysisDepth (ft bgs)Moisture ContentStiffness Color LithologyPID Readings (ppm) (1)NotesA----0-11-2MoistMoistMedium StiffMedium StiffRed-BrownRed-BrownClayey Silt, some Gravel, trace SandClayey Silt, some Gravel, trace Sand0.00.0----B----0-11-2MoistMoistMedium StiffMedium StiffRed-BrownRed-BrownClayey Silt, some Gravel, few SandClayey Silt, some Gravel, few Sand0.00.0----C----0-11-2MoistMoistMedium StiffMedium StiffRed-BrownRed-BrownSandy Silt with some GravelClayey Silt, little Gravel and Sand0.00.0----D----0-11-2MoistMoistMedium StiffMedium StiffRed-BrownRed-BrownSandy Silt with some GravelSandy Silt with some Gravel0.00.0----E--x0-11-2MoistMoistMedium StiffMedium StiffRed-BrownRed-BrownClayey Silt, some Gravel, trace SandClayey Silt, some Gravel, trace Sand0.20.2Gravel and Sand at top 0-0.5 ftA----0-11-2MoistMoistMedium StiffMedium StiffDark Brown and Red-BrownDark Brown and Red-BrownClayey Silt and Sand, some GravelClayey Silt and Sand, some Gravel0.20.2Gravel and Sand at top 0-0.5 ftB----0-11-2MoistMoistMedium StiffMedium StiffRed-Brown and Light BrownRed-Brown and Light BrownSilt with little GravelSilt with little Gravel0.00.0Gravel and Sand at top 0-0.5 ftC--x0-11-2MoistMoistMedium StiffMedium StiffLight Brown, Black, Red, BrownLight Brown, Black, Red, BrownClayey SiltClayey Silt0.30.3Gravel and Sand at top 0-0.5 ftD----0-11-2MoistMoistMedium StiffMedium StiffLight Red, Red-Brown, Tan, Black, WhiteLight Red, Red-Brown, Tan, Black, WhiteSiltSilt0.10.1----E----0-11-2MoistMoistMedium StiffMedium StiffBrownBrownSandy Silt, some Gravel, little ClaySandy Silt, some Gravel, little Clay0.00.0----A----0-11-2MoistMoistLooseLooseTanTanSilty SandSilty Sand0.10.1Gravel and Sand at top 0-0.5 ftB--x0-11-2MoistMoistMedium StiffMedium StiffBrown, Red-Brown, TanBrown, Red-Brown, TanClayey Silt and trace SandClayey Silt and trace Sand1.41.4----C----0-11-2MoistMoistLooseLooseDark Brown and RedDark Brown and RedSilty Sand, some Gravel, little ClaySilty Sand, some Gravel, little Clay0.10.1----D----0-11-2MoistMoistLooseStiffBrownRedSilty Sand and some GravelSilty Clay and little Gravel0.10.1Gravel and Sand at top 0-0.5 ftE----0-11-2MoistMoistMedium StiffMedium StiffRed and BrownRed and BrownClay, some Sand, little SiltClay, some Sand, little Silt0.20.2----A----0-11-2MoistMoistSoftSoftBrownBrownSandy Clay, some Silt and GravelSandy Clay, some Silt and Gravel0.00.0Collected adjacent to newly paved asphalt access driveB----0-11-2MoistMoistSoftSoftBrownBrownSilty Clay, some Gravel, trace SandSilty Clay, some Gravel, trace Sand0.00.0Collected adjacent to newly paved asphalt access driveC--x0-11-2MoistMoistSoftSoftRed-BrownRed-BrownSilty Clay, some Gravel, trace SandSilty Clay, some Gravel, trace Sand0.10.1Collected adjacent to newly paved asphalt access driveD----0-11-2MoistMoistMedium StiffMedium StiffBrownBrownSandy Silt, little Clay, some GravelSandy Silt, little Clay, some Gravel0.10.1Collected adjacent to newly paved asphalt access driveE----0-11-2MoistMoistSoftSoftBrownBrownSandy Clay, some Gravel, little SiltSandy Clay, some Gravel, little Silt0.00.0Collected adjacent to newly paved asphalt access driveA----0-11-2MoistMoistSoftSoftLight BrownLight BrownSilt, little Clay, trace GravelSilt, little Clay, trace Gravel0.00.0Collected adjacent to newly paved asphalt access driveB--x0-11-2MoistMoistMedium StiffMedium StiffRed-BrownRed-BrownClayey Silt with some GravelClayey Silt with some Gravel0.30.3----C----0-11-2MoistMoistMedium StiffMedium StiffRed-Brown and TanRed-Brown and TanClayey SiltClayey Silt0.00.0----D----0-11-2MoistMoistMedium StiffMedium StiffBrown and Red-BrownBrown and Red-BrownSilty Clay, little Sand, trace GravelSilty Clay, little Sand, trace Gravel0.10.1----E----0-11-2MoistMoistMedium StiffMedium StiffBrown, Red-Brown, TanBrown, Red-Brown, TanSilty Clay, little Sand, trace GravelSilty Clay, little Sand, trace Gravel0.00.0----Notes:1) Background photoionization detector (PID) readings ranged from 0.0 to 0.2 parts per million (ppm). * = selected for duplicate sample; VOC = volatile organic compound; ft bgs = feet below ground surface; -- = not applicable FG-2FG-1FG-3*FG-4FG-58/31/238/31/238/31/238/31/238/31/23https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Trammell Crow Residential - TCR/TCR-001 Yandle Witherspoon/Brownfields/Final Grade/Tables/TCR.001 Final Grade lithologyTable 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Final Grade Soil Sample Analytical ResultsYandle-Witherspoon Supply, Inc. Charlotte, North CarolinaH&H Job No. TCR-001Evaluation AreaScreening CriteriaSample IDDateDepth (ft bgs)1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite UnitsVOCs (8260D)Acetone0.014 JNA0.009 JNA0.010 JNA0.010 JNA0.006 JNA0.007 JNA14,000-- --n−Hexane <0.0008 NA <0.0009 NA <0.0008 NA <0.0008 NA <0.0009 NA0.001 JNA130-- --SVOCs (8270E)Acenaphthene NA <0.146 NA <0.161 NA <0.588 NA <0.136 NA2.59 JNA <0.133720-- --Anthracene NA <0.180 NA <0.198 NA <0.724 NA <0.168 NA3.29 JNA <0.1643,600-- --Benzo(a)anthraceneNA0.207 JNA0.575 JNA <0.704 NA0.446 JNA6.76NA <0.1591.1-- --Benzo(a)pyreneNA0.211 J NA0.625 JNA <0.745 NA0.519 JNA6.69NA <0.1680.11-- --Benzo(b)fluorantheneNA0.284 JNA0.842 JNA <0.740 NA0.640 JNA7.49NA <0.1671.1-- --Benzo(g,h,i)perylene NA <0.171 NA0.378 JNA <0.689 NA0.358 JNA3.28 JNA <0.156NE-- --Benzo(k)fluoranthene NA <0.172 NA0.285 JNA <0.694 NA0.233 JNA2.87 JNA <0.15711-- --ChryseneNA0.210 JNA0.611 JNA <0.719 NA0.447 JNA6.22NA <0.163110-- --DibenzofuranNA <0.149 NA <0.165 NA <0.603 NA <0.139 NA1.06 JNA <0.13616-- --FluorantheneNA0.361 JNA0.972NA <0.623 NA0.609 JNA12.3NA <0.141480-- --FluoreneNA <0.161 NA <0.178 NA <0.648 NA <0.150 NA1.68 JNA <0.147480-- --Indeno(1,2,3-cd)pyreneNA <0.225 NA0.443 JNA <0.907 NA0.366 JNA3.88NA <0.2051.1-- --Naphthalene NA <0.181 NA <0.200 NA <0.730 NA <0.169 NA1.21 JNA <0.1652.1-- --PhenanthreneNA <0.261 NA0.322 JNA <1.05 NA0.256 JNA12.2NA <0.239NE-- --PyreneNA0.352 JNA1.10NA <0.679 NA0.679 JNA11.1NA <0.154360-- --Metals (6020B/7471B/7199)ArsenicNA0.960NA1.36NA0.313 JNA0.857NA0.938NA0.507 0.68 1.1 - 3.0 1.0 - 18BariumNA98.7NA86.1NA21.5NA77.8NA79.4NA94.0 3,100 38 - 110 50 - 1,000CadmiumNA0.0696 JNA0.112 JNA <0.0329 NA0.116 JNA0.143 JNA0.0610 J 1.4ND - 0.36 J1.0 - 10Chromium (total)NA41.3NA28.4NA11.6NA37.4NA41.0NA19.8 NE 14 - 45 7.0 - 300Hexavalent ChromiumNA0.244 JNA <0.198 NA <0.183 NA <0.168 NA <0.186 NA <0.1640.31 0.34 J - 0.98 J NSTrivalent ChromiumNA41.1NA28.4NA11.6NA37.4NA41.0NA19.8 23,000 13.7 - 44.0 NSLeadNA20.0NA29.2NA8.23NA38.9NA36.8NA12.3 400 11 - 36 ND - 50MercuryNA0.0890NA0.0663NA0.0741NA0.0622NA0.0513NA0.100 4.70.024 J - 0.0970.03 - 0.52SeleniumNA0.682NA0.652NA0.166 JNA0.490NA0.427NA0.495 78 ND <0.1 - 0.8SilverNA0.0219 JNA0.0317 JNA <0.0085 NA0.0298 JNA0.0390 JNA0.0173 J 78 0.033 J - 0.60 ND - 5.0Cumulative Risk Calculations (4)Residential LICRResidential Non-Carcinogenic HIWorst Case Residential LICRWorst Case Residential Non-Carcinogenic HINotes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023. 2) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060). 3) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. 4) DEQ Cumulative Risk Calculator dated July 2023 and based upon a TCR of 1 x 10 -6 and THQ of 0.2. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Bold values exceed the Residential PSRGs and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; LICR = lifetime incremental cancer risk; HI = hazard index; TCR = target cancer risk; THQ = target hazard quotient ft bgs= feet below ground surface; NS = not specified; NE = not established; -- = not applicable; ND = not detected; NA = not analyzedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. 8/31/20238/31/2023Nearby Brownfields Property Range (2)Background Metals Final Grade8/31/2023 8/31/2023Published Range (3)mg/kgFG-5FG-4FG-3 / FG-DUPFG-1 FG-28/31/2023Residential PSRGs (1)<1.0 x 10-4<1.0<1.0 x 10-4<1.0Acceptable Risk Levels7.5 x 10-70.487.8 x 10-54.5 x 10-60.0630.0807.1 x 10-60.467.6 x 10-50.0350.109.1 x 10-6https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Trammell Crow Residential - TCR/TCR-001 Yandle Witherspoon/Brownfields/Final Grade/Tables/Data TableTable 2 (Page 1 of 1) Hart & Hickman, PC

Figures

REVISION NO. 0
JOB NO. TCR-001
DATE: 10-3-23
FIGURE NO. 2
YANDLE-WITHERSPOON SUPPLY INC.
N. BREVARD STREET AND BELMONT AVENUE
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
RAILROAD TRACK
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOR
T
H
B
R
E
V
A
R
D
S
T
R
E
E
T BE
LMON
T

A
V
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NUE
NOTES:
1.AERIAL IMAGERY AND PARCEL DATA OBTAINED FROM
MECKLENBURG COUNTY GIS, 2023.
2.NCBP = NORTH CAROLINA BROWNFIELDS PROPERTY
TRIBUTARY OF LITTLE
SUGAR CREEK
PROPOSED
PARKING DECK
PROPOSED
COURTYARD
PROPOSED POOL/
COURTYARD
COTTON WAREHOUSE
(NCBP NO. 24013-20-060)
HIGHLAND PARK MILL
(NCBP NO. 2005-16-060)
ALTON OPTIMIST PARK - PORTION
OF HIGHLAND PARK MILL
(NCBP NO. 2005-16-060)
ALPHA MILLS
(NCBP NO. 07009-03-060)
SOUTH
E
R
N

R
A
I
L
W
A
Y
LYNX
B
L
U
E
LI
N
E
LI
G
H
T
R
AIL
HIGHLAND PARK MILL
(NCBP NO. 2005-16-060)S:\AAA-Master Projects\Trammell Crow Residential - TCR\TCR-001 Yandle Witherspoon\Brownfields\Final Grade\Figures\TCR.001_20230906.dwg, Figure 2, 10/3/2023 11:28:49 AM, draburn
REVISION NO. 0
JOB NO. TCR-001
DATE: 10-3-23
FIGURE NO. 3
YANDLE-WITHERSPOON SUPPLY INC.
N. BREVARD STREET AND BELMONT AVENUE
CHARLOTTE, NORTH CAROLINA
FINAL GRADE SOIL
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
RAILROAD TRACK
PROPOSED MULTI-FAMILY RESIDENTIAL
BUILDING
PROPOSED OFFICE BUILDING
PROPOSED LANDSCAPING AREA
PROPOSED PARKING DECK
ALIQUOT SOIL SAMPLE LOCATIONS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOR
T
H
B
R
E
V
A
R
D
S
T
R
E
E
T BE
LMON
T

A
V
E
NUE
TRIBUTARY OF LITTLE
SUGAR CREEK
PROPOSED
PARKING DECK
PROPOSED
COURTYARD
PROPOSED POOL/
COURTYARD
NOTES:
1.PARCEL DATA OBTAINED FROM MECKLENBURG
COUNTY GIS, 2023.
2.APPROXIMATE EXTENT OF PROPOSED BUILDING
FOOTPRINTS BASED ON PRELIMINARY SITE PLAN
PROVIDED BY THE PD DATED 3/4/22.
3.FINAL GRADE SOIL SAMPLES COLLECTED BY H&H
PERSONNEL ON AUGUST 31, 2023.
FG-4
FG-5
FG-3
FG-2
FG-1
FG-1E
FG-1D
FG-1C
FG-1B
FG-1A
FG-2A
FG-2B
FG-2C
FG-2D
FG-2E
FG-3A
FG-3B
FG-3C
FG-3D
FG-3E
FG-4E
FG-4D
FG-4C
FG-4A
FG-4B
FG-5EFG-5D
FG-5A FG-5B
FG-5C
SOUTH
E
R
N

R
A
I
L
W
A
Y
LYN
X
B
L
U
E
LI
N
E
LI
G
H
T
R
AIL
S:\AAA-Master Projects\Trammell Crow Residential - TCR\TCR-001 Yandle Witherspoon\Brownfields\Final Grade\Figures\TCR.001_20230906.dwg, Figure 3, 10/3/2023 11:39:34 AM, draburn

Appendix A
Final Planting Plan

710' - 11 11/32"
UP
UP UP UP
UP
UP
UP
UP
ADJACENT
OPTIMIST HALL
DEVELOPMENT
BELMONT AVEN BREVARD STREET
PARKING DECK
SEE B  C STUDIO
PLANS FOR
COURTYARD
DESIGN
SEE B  C STUDIO
PLANS FOR
COURTYARD 
BREEZEWAY
DESIGN
EXISTING LIGHT RAIL
RAILROAD ROW
TOP OFCREEK BANK
PROPERTY LINETOP OF CREEK BANKCENTERLINE
10' BUILD TO ZONE
16' SETBACK
MULTI
FAMILY
RESIDENTIAL
ADJACENT
ALTON OPTIMIST PARK
DEVELOPMENT OFFICE
L
IM
ITS
OF
WORK
10' SETBACK
10' SETBACK
15' LANDSCAPE BUFFER ALONG PARKING DECK
35' POST CONSTRUCTION /
SWIM BUFFER
STORM DRAINAGE
EASEMENT
CLUB /
AMENITY
T
T
T
FREIGHT RAIL
CPROPERTY LINEPROPERTY LINE
FUTURE
OFFICE
DEVELOPMENT
30' POST-CONSTRUCTION
BUFFER
PROPERTY LINE
PROPERTY LINE
RAILROAD R/W
FREIGHT RAILWhite Point PacesPartners LLC
Parcel AZoned: TOD-MOZoned: TOD-UCSeaboard Air Line Railroad Co.
Seaboard Air Line Railroad Co.Zoned: I-2Zoned: TOD-UCEXISTING
POWER POLE
TO REMAIN
EXISTING
POWER POLE
TO REMAIN
EXISTING
POWER POLE
TO REMAIN
EXISTING
POWER POLE
TO REMAIN
6 LARGE MATURING
TREES TO BE PLACED
WITHIN 2 INTERIOR
COURTYARDS - SEE
BC STUDIO PLANS
FOR PROPOSED
LOCATIONS.
ADDITIONAL 8
RE4UIRED INTERNAL
TREES TO BE PLACED
PER THIS PLAN.
PROPOSED
PED LIGHT
TYP.
PROPOSED
PED LIGHT
TYP.
PROPOSED
PED LIGHT
TYP.
PROPOSED
PED LIGHT
TYP.
RE4UIRED PLANTING BUFFER,
SEE RE4UIRED PLANTING PLAN
TREES CODE 4TY BOTANICAL NAME COMMON NAME CONT.SIZE SPEC SIZE REMARKS
LTG 3 LLULRGHQGURQ WXOLSLIHUD 'GOHQ GROG'GOHQ GROG TXOLS PRSODU B B 1.5"MATCHED SPECIMEN, STRONG
CENTRAL LEADER
4VI 7 4XHUFXV YLUJLQLDQD SRXWKHUQ LLYH ODN B B 3"10-12C MATCHED SPECIMEN, STRONG
CENTRAL LEADER
UPA 17 UOPXV SDUYLIROLD 'AOOHH' TM AOOHH LDFHEDUN EOP B B 3"10-12C MATCHED SPECIMEN, STRONG
CENTRAL LEADER
SHRUBS CODE 4TY BOTANICAL NAME COMMON NAME CONT SPACING SPEC SIZE REMARKS
AGO 1,246 AFRUXV JUDPLQHXV 'OJRQ'GROGHQ VDULHJDWHG SZHHWIODJ 3 GAL AV SKRZQ MATCHED SPECIMEN
ARS 190 AVWLOEH [ 'RLVH DQG SKLQH'RLVH DQG SKLQH AVWLOEH 3 GAL AV SKRZQ MATCHED SPECIMEN
CSA 20 CDPHOOLD VDVDQTXD 'GUHHQ 02-004' TM OFWREHU MDJLF WKLWH SKL-SKL CDPHOOLD -AV SKRZQ 2-3C MATCHED SPECIMEN
CSK 26 CDPHOOLD VDVDQTXD 'KDQMLUR'KDQMLUR CDPHOOLD 7 GAL AV SKRZQ MATCHED SPECIMEN
DXR 132 DLVW\OLXP [ 'RLH-DM1ER' TM BOXHVFDSH DLVW\OLXP 5 GAL AV SKRZQ MATCHED SPECIMEN
HPI 19 H\GUDQJHD SDQLFXODWD 'ILVOBO' TM BRER PDQLFOH H\GUDQJHD 5 GAL AV SKRZQ MATCHED SPECIMEN
H4U 13 H\GUDQJHD TXHUFLIROLD 'MXQFKNLQ'ODNOHDI H\GUDQJHD -AV SKRZQ 2-3C MATCHED SPECIMEN
MSA 259 MLVFDQWKXV VLQHQVLV 'AGDJLR'AGDJLR EXODOLD GUDVV 5 GAL AV SKRZQ MATCHED SPECIMEN
OFC 11 OVPDQWKXV [ IRUWXQHL 'CDUO WKHHOHU'CDUO WKHHOHU FRUWXQH OVPDQWKXV 30 GAL AV SKRZQ 36"MATCHED SPECIMEN, STRONG
CENTRAL LEADER
PGA 13 PKRWLQLD JODEUD 'PDUVXU'D\QDPR RHG PKRWLQLD -AV SKRZQ 2-3C MATCHED SPECIMEN
TOS 87 TKXMD RFFLGHQWDOLV 'SPDUDJG'EPHUDOG GUHHQ AUERUYLWDH B B AV SKRZQ 36-48"MATCHED SPECIMEN, STRONG
CENTRAL LEADER
VTI 26 VLEXUQXP WLQXV 'LLVDURVH'LLVDURVH LDXUXVWLQXV -AV SKRZQ 2-3C MATCHED SPECIMEN
VML 119 VLEXUQXP [ 'MRRQOLW LDFH'MRRQOLW LDFH VLEXUQXP 5 GAL AV SKRZQ MATCHED SPECIMEN
SHRUB AREAS CODE 4TY BOTANICAL NAME COMMON NAME CONT SPACING MIN HT REMARKS
RO 456 VI RRFN MXOFK RRFN MXOFK -TO BE DETERMINED
GROUND COVERS CODE 4TY BOTANICAL NAME COMMON NAME CONT SPACING MIN HT REMARKS
ZXZ 9,027 VI ZR\VLD [ CZHRQC ZHRQ ZR\VLD SOD SOD
ZZE 25,051 VI ZR\VLD [ 'ZHRQ'ZHRQ ZR\VLD SEED SEED
PLANT SCHEDULE PLNT
ALEXAN OPTIMIST
PARK II
TRAMMELL CROW RESIDENTIAL
3715 NORTHSIDE PARKWAY,
BUILDING 100, SUIT 200
ATLANTA, GA 30327
1020346
FINAL PLANTING PLAN
N/A
LD
LD
LD
C11.03
3/4/2022 1:51 PM IGNACIO NUÑEZ N:\_2020\1020346\CAD\DOCUMENTATION\1020346_PLN_FPLNT.DWG
KEY MAP
SEAL
SHEET NUMBER
SHEET TITLE
LANDDESIGN PROJ.#
SCALE
PROJECT
NORTH
NO.DESCRIPTION DATE
REVISION / ISSUANCE
ORIGINAL SHEET SIZE: 24" X 36"
VERT:
HORZ:
CHECKED BY:
DRAWN BY:
DESIGNED BY:
223 NORTH GRAHAM STREET
CHARLOTTE, NC 28202
704.333.0325
WWW.LANDDESIGN.COM
NC ENG. FIRM LICENSE # C-0658
ISSUED FOR
PERMITTING
03/04/2022

1"=30'
6030015
90% GMP 07/20/2021
LAND DEVELOPMENT 08/16/2021

Appendix B
Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

10/24/2023
Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100
Charlotte, NC, 28203
Ref: Analytical Testing Revised Lab Report Number: 23-243-0019
Client Project Description: TCR-001
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/31/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 80
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202484002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2024T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/23-243-0019
Page 2 of 80
Report Number:
Sample Summary Table
Client Project Description:
23-243-0019
TCR-001
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
08/31/2023 09:10Solids 93827 FG-1 08/31/2023 15:00
08/31/2023 09:10Solids 93827 FG-1 08/31/2023 15:00 6020B WP MTN -
08/31/2023 09:10Solids 93827 FG-1 08/31/2023 15:00 SW-7199 WP MTN -
08/31/2023 14:05Solids 93828 FG-2 08/31/2023 15:00
08/31/2023 14:05Solids 93828 FG-2 08/31/2023 15:00 SW-7199 WP MTN -
08/31/2023 14:05Solids 93828 FG-2 08/31/2023 15:00 6020B WP MTN -
08/31/2023 11:20Solids 93829 FG-3 08/31/2023 15:00
08/31/2023 11:20Solids 93829 FG-3 08/31/2023 15:00 SW-7199 WP MTN -
08/31/2023 11:20Solids 93829 FG-3 08/31/2023 15:00 6020B WP MTN -
08/31/2023 10:20Solids 93830 FG-4 08/31/2023 15:00
08/31/2023 10:20Solids 93830 FG-4 08/31/2023 15:00 SW-7199 WP MTN -
08/31/2023 10:20Solids 93830 FG-4 08/31/2023 15:00 6020B WP MTN -
08/31/2023 12:50Solids 93831 FG-5 08/31/2023 15:00
08/31/2023 12:50Solids 93831 FG-5 08/31/2023 15:00 SW-7199 WP MTN -
08/31/2023 12:50Solids 93831 FG-5 08/31/2023 15:00 6020B WP MTN -
08/31/2023Solids 93832 FG-DUP 08/31/2023 15:00
08/31/2023Solids 93832 FG-DUP 08/31/2023 15:00 SW-7199 WP MTN -
08/31/2023Solids 93832 FG-DUP 08/31/2023 15:00 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 80
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-243-0019
Report Limit
Project:TCR-001
V 93827FG-1
0.960 09/06/2023 17:566020BArsenicmg/Kg - dry 0.108
98.7 09/06/2023 17:566020BBariummg/Kg - dry 0.053
J0.0696 09/06/2023 17:566020BCadmiummg/Kg - dry 0.0327
41.3 09/06/2023 17:566020BChromiummg/Kg - dry 0.146
20.0 09/06/2023 17:566020BLeadmg/Kg - dry 0.0390
0.682 09/06/2023 17:566020BSeleniummg/Kg - dry 0.129
J0.0219 09/07/2023 17:016020BSilvermg/Kg - dry 0.0084
0.0890 09/06/2023 15:227471BMercury (Total)mg/Kg - dry 0.0151
J0.014 09/01/2023 15:108260DAcetonemg/Kg - dry 0.003
J0.207 09/06/2023 23:408270EBenzo(a)anthracene mg/Kg - dry 0.175
J0.211 09/06/2023 23:408270EBenzo(a)pyrene mg/Kg - dry 0.185
J0.284 09/06/2023 23:408270EBenzo(b)fluoranthene mg/Kg - dry 0.183
J0.210 09/06/2023 23:408270EChrysenemg/Kg - dry 0.178
J0.361 09/06/2023 23:408270EFluoranthenemg/Kg - dry 0.154
J0.352 09/06/2023 23:408270EPyrenemg/Kg - dry 0.168
J0.244 09/08/2023 15:44SW-7199 Chromium, Hexavalent mg/Kg - dry 0.178
20.6 09/01/2023 09:16SW-DRYWT Moisture %
V 93828FG-2
1.36 09/06/2023 18:006020BArsenicmg/Kg - dry 0.119
86.1 09/06/2023 18:006020BBariummg/Kg - dry 0.059
J0.112 09/06/2023 18:006020BCadmiummg/Kg - dry 0.0361
28.4 09/06/2023 18:006020BChromiummg/Kg - dry 0.161
29.2 09/06/2023 18:006020BLeadmg/Kg - dry 0.0431
0.652 09/06/2023 18:006020BSeleniummg/Kg - dry 0.143
J0.0317 09/07/2023 17:056020BSilvermg/Kg - dry 0.0093
0.0663 09/06/2023 15:247471BMercury (Total)mg/Kg - dry 0.0167
J0.009 09/01/2023 15:378260DAcetonemg/Kg - dry 0.003
J0.575 09/07/2023 00:038270EBenzo(a)anthracene mg/Kg - dry 0.193
J0.625 09/07/2023 00:038270EBenzo(a)pyrene mg/Kg - dry 0.204
J0.842 09/07/2023 00:038270EBenzo(b)fluoranthene mg/Kg - dry 0.203
J0.378 09/07/2023 00:038270EBenzo(g,h,i)perylene mg/Kg - dry 0.189
J0.285 09/07/2023 00:038270EBenzo(k)fluoranthene mg/Kg - dry 0.190
J0.611 09/07/2023 00:038270EChrysenemg/Kg - dry 0.197
0.972 09/07/2023 00:038270EFluoranthenemg/Kg - dry 0.171
J0.443 09/07/2023 00:038270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.248
J0.322 09/07/2023 00:038270EPhenanthrenemg/Kg - dry 0.289
Page 4 of 80
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-243-0019
Report Limit
Project:TCR-001
V 93828FG-2
1.10 09/07/2023 00:038270EPyrenemg/Kg - dry 0.186
28.1 09/01/2023 09:16SW-DRYWT Moisture %
V 93829FG-3
J0.313 09/06/2023 18:046020BArsenicmg/Kg - dry 0.108
21.5 09/06/2023 18:046020BBariummg/Kg - dry 0.054
11.6 09/06/2023 18:046020BChromiummg/Kg - dry 0.147
8.23 09/06/2023 18:046020BLeadmg/Kg - dry 0.0392
J0.166 09/06/2023 18:046020BSeleniummg/Kg - dry 0.130
0.0741 09/06/2023 15:277471BMercury (Total)mg/Kg - dry 0.0152
J0.010 09/01/2023 16:048260DAcetonemg/Kg - dry 0.003
21.1 09/01/2023 09:16SW-DRYWT Moisture %
V 93830FG-4
0.938 09/06/2023 18:086020BArsenicmg/Kg - dry 0.113
79.4 09/06/2023 18:086020BBariummg/Kg - dry 0.056
J0.143 09/06/2023 18:086020BCadmiummg/Kg - dry 0.0343
41.0 09/06/2023 18:086020BChromiummg/Kg - dry 0.153
36.8 09/06/2023 18:086020BLeadmg/Kg - dry 0.0410
0.427 09/06/2023 18:086020BSeleniummg/Kg - dry 0.136
J0.0390 09/07/2023 17:136020BSilvermg/Kg - dry 0.0089
0.0513 09/06/2023 15:297471BMercury (Total)mg/Kg - dry 0.0159
J0.006 09/01/2023 16:318260DAcetonemg/Kg - dry 0.003
J2.59 09/07/2023 15:228270EAcenaphthenemg/Kg - dry 0.613
J3.29 09/07/2023 15:228270EAnthracenemg/Kg - dry 0.756
6.76 09/07/2023 15:228270EBenzo(a)anthracene mg/Kg - dry 0.735
6.69 09/07/2023 15:228270EBenzo(a)pyrene mg/Kg - dry 0.777
7.49 09/07/2023 15:228270EBenzo(b)fluoranthene mg/Kg - dry 0.772
J3.28 09/07/2023 15:228270EBenzo(g,h,i)perylene mg/Kg - dry 0.719
J2.87 09/07/2023 15:228270EBenzo(k)fluoranthene mg/Kg - dry 0.724
6.22 09/07/2023 15:228270EChrysenemg/Kg - dry 0.751
J1.06 09/07/2023 15:228270EDibenzofuranmg/Kg - dry 0.629
12.3 09/07/2023 15:228270EFluoranthenemg/Kg - dry 0.650
J1.68 09/07/2023 15:228270EFluorenemg/Kg - dry 0.677
3.88 09/07/2023 15:228270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.947
J1.21 09/07/2023 15:228270ENaphthalenemg/Kg - dry 0.761
12.2 09/07/2023 15:228270EPhenanthrenemg/Kg - dry 1.10
11.1 09/07/2023 15:228270EPyrenemg/Kg - dry 0.708
Page 5 of 80
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-243-0019
Report Limit
Project:TCR-001
V 93830FG-4
24.4 09/01/2023 09:16SW-DRYWT Moisture %
V 93831FG-5
0.507 09/06/2023 18:126020BArsenicmg/Kg - dry 0.0982
94.0 09/06/2023 18:126020BBariummg/Kg - dry 0.049
J0.0610 09/06/2023 18:126020BCadmiummg/Kg - dry 0.0298
19.8 09/06/2023 18:126020BChromiummg/Kg - dry 0.133
12.3 09/06/2023 18:126020BLeadmg/Kg - dry 0.0356
0.495 09/06/2023 18:126020BSeleniummg/Kg - dry 0.118
J0.0173 09/07/2023 17:176020BSilvermg/Kg - dry 0.0077
0.100 09/06/2023 15:327471BMercury (Total)mg/Kg - dry 0.0138
J0.007 09/01/2023 16:588260DAcetonemg/Kg - dry 0.002
J0.001 09/01/2023 16:588260Dn-Hexane mg/Kg - dry 0.0008
13.0 09/01/2023 09:16SW-DRYWT Moisture %
V 93832FG-DUP
0.857 09/06/2023 18:166020BArsenicmg/Kg - dry 0.100
77.8 09/06/2023 18:166020BBariummg/Kg - dry 0.050
J0.116 09/06/2023 18:166020BCadmiummg/Kg - dry 0.0305
37.4 09/06/2023 18:166020BChromiummg/Kg - dry 0.136
38.9 09/06/2023 18:166020BLeadmg/Kg - dry 0.0364
0.490 09/06/2023 18:166020BSeleniummg/Kg - dry 0.121
J0.0298 09/07/2023 17:216020BSilvermg/Kg - dry 0.0079
0.0622 09/06/2023 15:347471BMercury (Total)mg/Kg - dry 0.0141
J0.010 09/01/2023 17:268260DAcetonemg/Kg - dry 0.002
J0.446 09/07/2023 00:268270EBenzo(a)anthracene mg/Kg - dry 0.163
J0.519 09/07/2023 00:268270EBenzo(a)pyrene mg/Kg - dry 0.172
J0.640 09/07/2023 00:268270EBenzo(b)fluoranthene mg/Kg - dry 0.171
J0.358 09/07/2023 00:268270EBenzo(g,h,i)perylene mg/Kg - dry 0.159
J0.233 09/07/2023 00:268270EBenzo(k)fluoranthene mg/Kg - dry 0.160
J0.447 09/07/2023 00:268270EChrysenemg/Kg - dry 0.166
J0.609 09/07/2023 00:268270EFluoranthenemg/Kg - dry 0.144
J0.366 09/07/2023 00:268270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.210
J0.256 09/07/2023 00:268270EPhenanthrenemg/Kg - dry 0.244
J0.679 09/07/2023 00:268270EPyrenemg/Kg - dry 0.157
14.9 09/01/2023 09:16SW-DRYWT Moisture %
Page 6 of 80

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: TCR-001 Lab Report Number: 23-243-0019
Date: 9/13/2023
Metals Analyses Method 6020B Sample 93832 (FG-DUP) Analyte: Arsenic
QC Batch No: L702982/L702308 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93832 (FG-DUP)
Analyte: Barium QC Batch No: L702982/L702308
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 93832 (FG-DUP)
Analyte: Chromium QC Batch No: L702982/L702308
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 93832 (FG-DUP) Analyte: Lead QC Batch No: L702982/L702308
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 93832 (FG-DUP)
Analyte: Selenium QC Batch No: L702982/L702308 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected. Semivolatile Organic Compounds - GC/MS Method 8270E Sample 93829 (FG-3) QC Batch No: V37467/V37441 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Analyte: Aniline
QC Batch No: V37467/V37441 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Page 7 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.6 %Moisture 1 09/01/23 09:16 SW-DRYWTCNC
0.244 J mg/Kg - dry 0.178 0.254Chromium, Hexavalent 1 09/08/23 15:44 SW-7199SDS
0.960 mg/Kg - dry 0.108 0.315Arsenic 5 09/06/23 17:56 6020BCPW
98.7 mg/Kg - dry 0.053 0.314Barium 5 09/06/23 17:56 6020BCPW
0.0696 J mg/Kg - dry 0.0327 0.315Cadmium 5 09/06/23 17:56 6020BCPW
41.3 mg/Kg - dry 0.146 0.314
Chromium 5 09/06/23 17:56 6020BCPW
20.0 mg/Kg - dry 0.0390 0.315Lead 5 09/06/23 17:56 6020BCPW
0.0890 mg/Kg - dry 0.0151 0.0378Mercury (Total)1 09/06/23 15:22 7471BJKC
0.682 mg/Kg - dry 0.129 0.314Selenium 5 09/06/23 17:56 6020BCPW
0.0219 J mg/Kg - dry 0.0084 0.315Silver 5 09/07/23 17:01 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.014 J mg/Kg - dry 0.003 0.025Acetone 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/01/23 15:10 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 15:10 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/01/23 15:10 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 15:10 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 15:10 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 15:10 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 15:10 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/01/23 15:10 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/01/23 15:10 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 15:10 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 15:10 V37419TBL
<0.017 mg/Kg - dry 0.017 0.314Ethanol 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 15:10 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/01/23 15:10 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 15:10 V37419TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 15:10 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 09/01/23 15:10 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 15:10 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/01/23 15:10 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/01/23 15:10 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 15:10 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/01/23 15:10 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/01/23 15:10 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/01/23 15:10 V37419
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/01/23 15:101 TBL V37419
Surrogate: Dibromofluoromethane 105 Limits: 84-123%09/01/23 15:101 TBL V37419
Surrogate: Toluene-d8 99.1 Limits: 76-129%09/01/23 15:101 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.146 mg/Kg - dry 0.146 0.831Acenaphthene 1 09/06/23 23:40 V37467AMP
<0.132 mg/Kg - dry 0.132 0.831Acenaphthylene 1 09/06/23 23:40 V37467AMP
<0.191 mg/Kg - dry 0.191 0.831Aniline 1 09/06/23 23:40 V37467AMP
<0.180 mg/Kg - dry 0.180 0.831Anthracene 1 09/06/23 23:40 V37467AMP
0.207 J
mg/Kg - dry 0.175 0.831
Benzo(a)anthracene 1 09/06/23 23:40 V37467AMP
0.211 J mg/Kg - dry 0.185 0.831Benzo(a)pyrene 1 09/06/23 23:40 V37467AMP
0.284 J mg/Kg - dry 0.183 0.831Benzo(b)fluoranthene 1 09/06/23 23:40 V37467AMP
<0.171 mg/Kg - dry 0.171 0.831Benzo(g,h,i)perylene 1 09/06/23 23:40 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.172 mg/Kg - dry 0.172 0.831Benzo(k)fluoranthene 1 09/06/23 23:40 V37467AMP
<0.730 mg/Kg - dry 0.730 2.52Benzoic Acid 1 09/06/23 23:40 V37467AMP
<0.132 mg/Kg - dry 0.132 0.831Benzyl alcohol 1 09/06/23 23:40 V37467AMP
<0.148 mg/Kg - dry 0.148 0.831Bis(2-Chloroethoxy)methane 1 09/06/23 23:40 V37467AMP
<0.134 mg/Kg - dry 0.134 0.831Bis(2-Chloroethyl)ether 1 09/06/23 23:40 V37467AMP
<0.171 mg/Kg - dry 0.171 0.415Bis(2-Chloroisopropyl)ether 1 09/06/23 23:40 V37467AMP
<0.151 mg/Kg - dry 0.151 0.831Bis(2-ethylhexyl)phthalate 1 09/06/23 23:40 V37467AMP
<0.137 mg/Kg - dry 0.137 0.8314-Bromophenyl phenyl ether 1 09/06/23 23:40 V37467AMP
<0.142 mg/Kg - dry 0.142 0.415
Butyl benzyl phthalate 1 09/06/23 23:40 V37467AMP
<0.116 mg/Kg - dry 0.116 0.8314-Chloro-3-methylphenol 1 09/06/23 23:40 V37467AMP
<0.141 mg/Kg - dry 0.141 0.4154-Chloroaniline 1 09/06/23 23:40 V37467AMP
<0.146 mg/Kg - dry 0.146 0.8312-Chloronaphthalene 1 09/06/23 23:40 V37467AMP
<0.123 mg/Kg - dry 0.123 0.8312-Chlorophenol 1 09/06/23 23:40 V37467AMP
<0.158 mg/Kg - dry 0.158 1.264-Chlorophenyl phenyl ether 1 09/06/23 23:40 V37467AMP
0.210 J mg/Kg - dry 0.178 0.831Chrysene 1 09/06/23 23:40 V37467AMP
<0.289 mg/Kg - dry 0.289 0.831
Dibenz(a,h)anthracene 1 09/06/23 23:40 V37467AMP
<0.149 mg/Kg - dry 0.149 0.831Dibenzofuran 1 09/06/23 23:40 V37467AMP
<0.118 mg/Kg - dry 0.118 0.8311,2-Dichlorobenzene 1 09/06/23 23:40 V37467AMP
<0.122 mg/Kg - dry 0.122 0.8311,3-Dichlorobenzene 1 09/06/23 23:40 V37467AMP
<0.122 mg/Kg - dry 0.122 0.4151,4-Dichlorobenzene 1 09/06/23 23:40 V37467AMP
<0.185 mg/Kg - dry 0.185 0.8313,3'-Dichlorobenzidine 1 09/06/23 23:40 V37467AMP
<0.120 mg/Kg - dry 0.120 0.8312,4-Dichlorophenol 1 09/06/23 23:40 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.226 mg/Kg - dry 0.226 0.831Diethyl phthalate 1 09/06/23 23:40 V37467AMP
<0.219 mg/Kg - dry 0.219 0.831Dimethyl phthalate 1 09/06/23 23:40 V37467AMP
<0.136 mg/Kg - dry 0.136 0.4152,4-Dimethylphenol 1 09/06/23 23:40 V37467AMP
<0.134 mg/Kg - dry 0.134 0.831Di-n-butyl phthalate 1 09/06/23 23:40 V37467AMP
<0.302 mg/Kg - dry 0.302 1.894,6-Dinitro-2-methylphenol 1 09/06/23 23:40 V37467AMP
<0.654 mg/Kg - dry 0.654 1.892,4-Dinitrophenol 1 09/06/23 23:40 V37467AMP
<0.121 mg/Kg - dry 0.121 0.8312,4-Dinitrotoluene 1 09/06/23 23:40 V37467AMP
<0.136 mg/Kg - dry 0.136 0.8312,6-Dinitrotoluene 1 09/06/23 23:40 V37467AMP
<0.180 mg/Kg - dry 0.180 0.415
Di-n-Octyl Phthalate 1 09/06/23 23:40 V37467AMP
0.361 J mg/Kg - dry 0.154 0.831Fluoranthene 1 09/06/23 23:40 V37467AMP
<0.161 mg/Kg - dry 0.161 0.831Fluorene 1 09/06/23 23:40 V37467AMP
<0.133 mg/Kg - dry 0.133 0.831Hexachlorobenzene 1 09/06/23 23:40 V37467AMP
<0.122 mg/Kg - dry 0.122 0.831Hexachlorobutadiene 1 09/06/23 23:40 V37467AMP
<0.197 mg/Kg - dry 0.197 0.831Hexachlorocyclopentadiene 1 09/06/23 23:40 V37467AMP
<0.099 mg/Kg - dry 0.099 0.831Hexachloroethane 1 09/06/23 23:40 V37467AMP
<0.225 mg/Kg - dry 0.225 0.831
Indeno(1,2,3-cd)pyrene 1 09/06/23 23:40 V37467AMP
<0.240 mg/Kg - dry 0.240 0.831Isophorone 1 09/06/23 23:40 V37467AMP
<0.133 mg/Kg - dry 0.133 0.8311-Methylnaphthalene 1 09/06/23 23:40 V37467AMP
<0.125 mg/Kg - dry 0.125 0.8312-Methylnaphthalene 1 09/06/23 23:40 V37467AMP
<0.122 mg/Kg - dry 0.122 0.8312-Methylphenol 1 09/06/23 23:40 V37467AMP
<0.106 mg/Kg - dry 0.106 0.8313&4 Methylphenol 1 09/06/23 23:40 V37467AMP
<0.181 mg/Kg - dry 0.181 0.831Naphthalene 1 09/06/23 23:40 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-1
93827 Matrix:
8/31/2023 9:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.121 mg/Kg - dry 0.121 0.8312-Nitroaniline 1 09/06/23 23:40 V37467AMP
<0.151 mg/Kg - dry 0.151 0.8313-Nitroaniline 1 09/06/23 23:40 V37467AMP
<0.117 mg/Kg - dry 0.117 0.4154-Nitroaniline 1 09/06/23 23:40 V37467AMP
<0.146 mg/Kg - dry 0.146 0.415Nitrobenzene 1 09/06/23 23:40 V37467AMP
<0.111 mg/Kg - dry 0.111 0.8312-Nitrophenol 1 09/06/23 23:40 V37467AMP
<0.147 mg/Kg - dry 0.147 0.8314-Nitrophenol 1 09/06/23 23:40 V37467AMP
<0.331 mg/Kg - dry 0.331 0.831N-Nitrosodimethylamine 1 09/06/23 23:40 V37467AMP
<0.227 mg/Kg - dry 0.227 0.831N-Nitrosodiphenylamine 1 09/06/23 23:40 V37467AMP
<0.148 mg/Kg - dry 0.148 0.831
N-Nitroso-di-n-propylamine 1 09/06/23 23:40 V37467AMP
<0.437 mg/Kg - dry 0.437 1.26Pentachlorophenol 1 09/06/23 23:40 V37467AMP
<0.261 mg/Kg - dry 0.261 0.831Phenanthrene 1 09/06/23 23:40 V37467AMP
<0.141 mg/Kg - dry 0.141 0.831Phenol 1 09/06/23 23:40 V37467AMP
0.352 J mg/Kg - dry 0.168 0.831Pyrene 1 09/06/23 23:40 V37467AMP
<0.099 mg/Kg - dry 0.099 0.415Pyridine 1 09/06/23 23:40 V37467AMP
<0.134 mg/Kg - dry 0.134 0.8311,2,4-Trichlorobenzene 1 09/06/23 23:40 V37467AMP
<0.121 mg/Kg - dry 0.121 0.831
2,4,5-Trichlorophenol 1 09/06/23 23:40 V37467AMP
<0.121 mg/Kg - dry 0.121 0.8312,4,6-Trichlorophenol 1 09/06/23 23:40 V37467AMP
8270ESurrogate: Phenol-d5 81.4 Limits: 34-121%09/06/23 23:401 AMP
Surrogate: 2-Fluorobiphenyl 94.6 Limits: 44-115%09/06/23 23:401 AMP V37467
Surrogate: 2-Fluorophenol 87.1 Limits: 35-115%09/06/23 23:401 AMP V37467
Surrogate: Nitrobenzene-d5 91.6 Limits: 37-122%09/06/23 23:401 AMP V37467
Surrogate: 4-Terphenyl-d14 105 Limits: 54-127%09/06/23 23:401 AMP V37467
Surrogate: 2,4,6-Tribromophenol 85.6 Limits: 39-132%09/06/23 23:401 AMP V37467
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.1 %Moisture 1 09/01/23 09:16 SW-DRYWTCNC
<0.198 mg/Kg - dry 0.198 0.282Chromium, Hexavalent 1 09/08/23 16:49 SW-7199SDS
1.36 mg/Kg - dry 0.119 0.348Arsenic 5 09/06/23 18:00 6020BCPW
86.1 mg/Kg - dry 0.059 0.347Barium 5 09/06/23 18:00 6020BCPW
0.112 J mg/Kg - dry 0.0361 0.348Cadmium 5 09/06/23 18:00 6020BCPW
28.4 mg/Kg - dry 0.161 0.347
Chromium 5 09/06/23 18:00 6020BCPW
29.2 mg/Kg - dry 0.0431 0.348Lead 5 09/06/23 18:00 6020BCPW
0.0663 mg/Kg - dry 0.0167 0.0417Mercury (Total)1 09/06/23 15:24 7471BJKC
0.652 mg/Kg - dry 0.143 0.347Selenium 5 09/06/23 18:00 6020BCPW
0.0317 J mg/Kg - dry 0.0093 0.348Silver 5 09/07/23 17:05 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.009 J mg/Kg - dry 0.003 0.027Acetone 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 15:37 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 09/01/23 15:37 V37419TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/01/23 15:37 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 15:37 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 09/01/23 15:37 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 15:37 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 15:37 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 15:37 V37419TBL
<0.019 mg/Kg - dry 0.019 0.347Ethanol 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/01/23 15:37 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 09/01/23 15:37 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 15:37 V37419TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 09/01/23 15:37 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 15:37 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.013
1,2,3-Trichlorobenzene 1 09/01/23 15:37 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 09/01/23 15:37 V37419TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 15:37 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,2,3-Trichloropropane 1 09/01/23 15:37 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 09/01/23 15:37 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 09/01/23 15:37 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 09/01/23 15:37 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/01/23 15:37 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/01/23 15:37 V37419
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/01/23 15:371 TBL V37419
Surrogate: Dibromofluoromethane 106 Limits: 84-123%09/01/23 15:371 TBL V37419
Surrogate: Toluene-d8 98.1 Limits: 76-129%09/01/23 15:371 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.161 mg/Kg - dry 0.161 0.917Acenaphthene 1 09/07/23 00:03 V37467AMP
<0.146 mg/Kg - dry 0.146 0.917Acenaphthylene 1 09/07/23 00:03 V37467AMP
<0.211 mg/Kg - dry 0.211 0.917Aniline 1 09/07/23 00:03 V37467AMP
<0.198 mg/Kg - dry 0.198 0.917Anthracene 1 09/07/23 00:03 V37467AMP
0.575 J
mg/Kg - dry 0.193 0.917
Benzo(a)anthracene 1 09/07/23 00:03 V37467AMP
0.625 J mg/Kg - dry 0.204 0.917Benzo(a)pyrene 1 09/07/23 00:03 V37467AMP
0.842 J mg/Kg - dry 0.203 0.917Benzo(b)fluoranthene 1 09/07/23 00:03 V37467AMP
0.378 J mg/Kg - dry 0.189 0.917Benzo(g,h,i)perylene 1 09/07/23 00:03 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
0.285 J mg/Kg - dry 0.190 0.917Benzo(k)fluoranthene 1 09/07/23 00:03 V37467AMP
<0.806 mg/Kg - dry 0.806 2.78Benzoic Acid 1 09/07/23 00:03 V37467AMP
<0.146 mg/Kg - dry 0.146 0.917Benzyl alcohol 1 09/07/23 00:03 V37467AMP
<0.164 mg/Kg - dry 0.164 0.917Bis(2-Chloroethoxy)methane 1 09/07/23 00:03 V37467AMP
<0.148 mg/Kg - dry 0.148 0.917Bis(2-Chloroethyl)ether 1 09/07/23 00:03 V37467AMP
<0.189 mg/Kg - dry 0.189 0.458Bis(2-Chloroisopropyl)ether 1 09/07/23 00:03 V37467AMP
<0.166 mg/Kg - dry 0.166 0.917Bis(2-ethylhexyl)phthalate 1 09/07/23 00:03 V37467AMP
<0.151 mg/Kg - dry 0.151 0.9174-Bromophenyl phenyl ether 1 09/07/23 00:03 V37467AMP
<0.157 mg/Kg - dry 0.157 0.458
Butyl benzyl phthalate 1 09/07/23 00:03 V37467AMP
<0.128 mg/Kg - dry 0.128 0.9174-Chloro-3-methylphenol 1 09/07/23 00:03 V37467AMP
<0.155 mg/Kg - dry 0.155 0.4584-Chloroaniline 1 09/07/23 00:03 V37467AMP
<0.161 mg/Kg - dry 0.161 0.9172-Chloronaphthalene 1 09/07/23 00:03 V37467AMP
<0.136 mg/Kg - dry 0.136 0.9172-Chlorophenol 1 09/07/23 00:03 V37467AMP
<0.175 mg/Kg - dry 0.175 1.394-Chlorophenyl phenyl ether 1 09/07/23 00:03 V37467AMP
0.611 J mg/Kg - dry 0.197 0.917Chrysene 1 09/07/23 00:03 V37467AMP
<0.319 mg/Kg - dry 0.319 0.917
Dibenz(a,h)anthracene 1 09/07/23 00:03 V37467AMP
<0.165 mg/Kg - dry 0.165 0.917Dibenzofuran 1 09/07/23 00:03 V37467AMP
<0.131 mg/Kg - dry 0.131 0.9171,2-Dichlorobenzene 1 09/07/23 00:03 V37467AMP
<0.135 mg/Kg - dry 0.135 0.9171,3-Dichlorobenzene 1 09/07/23 00:03 V37467AMP
<0.135 mg/Kg - dry 0.135 0.4581,4-Dichlorobenzene 1 09/07/23 00:03 V37467AMP
<0.204 mg/Kg - dry 0.204 0.9173,3'-Dichlorobenzidine 1 09/07/23 00:03 V37467AMP
<0.133 mg/Kg - dry 0.133 0.9172,4-Dichlorophenol 1 09/07/23 00:03 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.250 mg/Kg - dry 0.250 0.917Diethyl phthalate 1 09/07/23 00:03 V37467AMP
<0.242 mg/Kg - dry 0.242 0.917Dimethyl phthalate 1 09/07/23 00:03 V37467AMP
<0.150 mg/Kg - dry 0.150 0.4582,4-Dimethylphenol 1 09/07/23 00:03 V37467AMP
<0.148 mg/Kg - dry 0.148 0.917Di-n-butyl phthalate 1 09/07/23 00:03 V37467AMP
<0.333 mg/Kg - dry 0.333 2.094,6-Dinitro-2-methylphenol 1 09/07/23 00:03 V37467AMP
<0.723 mg/Kg - dry 0.723 2.092,4-Dinitrophenol 1 09/07/23 00:03 V37467AMP
<0.134 mg/Kg - dry 0.134 0.9172,4-Dinitrotoluene 1 09/07/23 00:03 V37467AMP
<0.150 mg/Kg - dry 0.150 0.9172,6-Dinitrotoluene 1 09/07/23 00:03 V37467AMP
<0.198 mg/Kg - dry 0.198 0.458
Di-n-Octyl Phthalate 1 09/07/23 00:03 V37467AMP
0.972 mg/Kg - dry 0.171 0.917Fluoranthene 1 09/07/23 00:03 V37467AMP
<0.178 mg/Kg - dry 0.178 0.917Fluorene 1 09/07/23 00:03 V37467AMP
<0.147 mg/Kg - dry 0.147 0.917Hexachlorobenzene 1 09/07/23 00:03 V37467AMP
<0.135 mg/Kg - dry 0.135 0.917Hexachlorobutadiene 1 09/07/23 00:03 V37467AMP
<0.218 mg/Kg - dry 0.218 0.917Hexachlorocyclopentadiene 1 09/07/23 00:03 V37467AMP
<0.110 mg/Kg - dry 0.110 0.917Hexachloroethane 1 09/07/23 00:03 V37467AMP
0.443 J
mg/Kg - dry 0.248 0.917
Indeno(1,2,3-cd)pyrene 1 09/07/23 00:03 V37467AMP
<0.265 mg/Kg - dry 0.265 0.917Isophorone 1 09/07/23 00:03 V37467AMP
<0.147 mg/Kg - dry 0.147 0.9171-Methylnaphthalene 1 09/07/23 00:03 V37467AMP
<0.139 mg/Kg - dry 0.139 0.9172-Methylnaphthalene 1 09/07/23 00:03 V37467AMP
<0.134 mg/Kg - dry 0.134 0.9172-Methylphenol 1 09/07/23 00:03 V37467AMP
<0.118 mg/Kg - dry 0.118 0.9173&4 Methylphenol 1 09/07/23 00:03 V37467AMP
<0.200 mg/Kg - dry 0.200 0.917Naphthalene 1 09/07/23 00:03 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-2
93828 Matrix:
8/31/2023 14:05
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.134 mg/Kg - dry 0.134 0.9172-Nitroaniline 1 09/07/23 00:03 V37467AMP
<0.166 mg/Kg - dry 0.166 0.9173-Nitroaniline 1 09/07/23 00:03 V37467AMP
<0.129 mg/Kg - dry 0.129 0.4584-Nitroaniline 1 09/07/23 00:03 V37467AMP
<0.161 mg/Kg - dry 0.161 0.458Nitrobenzene 1 09/07/23 00:03 V37467AMP
<0.123 mg/Kg - dry 0.123 0.9172-Nitrophenol 1 09/07/23 00:03 V37467AMP
<0.162 mg/Kg - dry 0.162 0.9174-Nitrophenol 1 09/07/23 00:03 V37467AMP
<0.365 mg/Kg - dry 0.365 0.917N-Nitrosodimethylamine 1 09/07/23 00:03 V37467AMP
<0.251 mg/Kg - dry 0.251 0.917N-Nitrosodiphenylamine 1 09/07/23 00:03 V37467AMP
<0.164 mg/Kg - dry 0.164 0.917
N-Nitroso-di-n-propylamine 1 09/07/23 00:03 V37467AMP
<0.482 mg/Kg - dry 0.482 1.39Pentachlorophenol 1 09/07/23 00:03 V37467AMP
0.322 J mg/Kg - dry 0.289 0.917Phenanthrene 1 09/07/23 00:03 V37467AMP
<0.155 mg/Kg - dry 0.155 0.917Phenol 1 09/07/23 00:03 V37467AMP
1.10 mg/Kg - dry 0.186 0.917Pyrene 1 09/07/23 00:03 V37467AMP
<0.110 mg/Kg - dry 0.110 0.458Pyridine 1 09/07/23 00:03 V37467AMP
<0.148 mg/Kg - dry 0.148 0.9171,2,4-Trichlorobenzene 1 09/07/23 00:03 V37467AMP
<0.133 mg/Kg - dry 0.133 0.917
2,4,5-Trichlorophenol 1 09/07/23 00:03 V37467AMP
<0.134 mg/Kg - dry 0.134 0.9172,4,6-Trichlorophenol 1 09/07/23 00:03 V37467AMP
8270ESurrogate: Phenol-d5 76.3 Limits: 34-121%09/07/23 00:031 AMP
Surrogate: 2-Fluorobiphenyl 92.2 Limits: 44-115%09/07/23 00:031 AMP V37467
Surrogate: 2-Fluorophenol 76.9 Limits: 35-115%09/07/23 00:031 AMP V37467
Surrogate: Nitrobenzene-d5 83.2 Limits: 37-122%09/07/23 00:031 AMP V37467
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%09/07/23 00:031 AMP V37467
Surrogate: 2,4,6-Tribromophenol 81.1 Limits: 39-132%09/07/23 00:031 AMP V37467
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.1 %Moisture 1 09/01/23 09:16 SW-DRYWTCNC
<0.183 mg/Kg - dry 0.183 0.262Chromium, Hexavalent 1 09/08/23 17:00 SW-7199SDS
0.313 J mg/Kg - dry 0.108 0.317Arsenic 5 09/06/23 18:04 6020BCPW
21.5 mg/Kg - dry 0.054 0.316Barium 5 09/06/23 18:04 6020BCPW
<0.0329 mg/Kg - dry 0.0329 0.317Cadmium 5 09/06/23 18:04 6020BCPW
11.6 mg/Kg - dry 0.147 0.316
Chromium 5 09/06/23 18:04 6020BCPW
8.23 mg/Kg - dry 0.0392 0.317Lead 5 09/06/23 18:04 6020BCPW
0.0741 mg/Kg - dry 0.0152 0.0380Mercury (Total)1 09/06/23 15:27 7471BJKC
0.166 J mg/Kg - dry 0.130 0.316Selenium 5 09/06/23 18:04 6020BCPW
<0.0085 mg/Kg - dry 0.0085 0.317Silver 5 09/07/23 17:09 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.010 J mg/Kg - dry 0.003 0.025Acetone 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/01/23 16:04 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 16:04 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 16:04 V37419TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/01/23 16:04 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 16:04 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 16:04 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 16:04 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 16:04 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/01/23 16:04 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 16:04 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 16:04 V37419TBL
<0.017 mg/Kg - dry 0.017 0.316Ethanol 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/01/23 16:04 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 16:04 V37419TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 16:04 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 09/01/23 16:04 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 16:04 V37419TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/01/23 16:04 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/01/23 16:04 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 16:04 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/01/23 16:04 V37419TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/01/23 16:04 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/01/23 16:04 V37419
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/01/23 16:041 TBL V37419
Surrogate: Dibromofluoromethane 108 Limits: 84-123%09/01/23 16:041 TBL V37419
Surrogate: Toluene-d8 99.5 Limits: 76-129%09/01/23 16:041 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.588 mg/Kg - dry 0.588 3.35Acenaphthene 4 09/07/23 15:45 V37467AMP
<0.532 mg/Kg - dry 0.532 3.35Acenaphthylene 4 09/07/23 15:45 V37467AMP
<0.770 mg/Kg - dry 0.770 3.35Aniline 4 09/07/23 15:45 V37467AMP
<0.724 mg/Kg - dry 0.724 3.35Anthracene 4 09/07/23 15:45 V37467AMP
<0.704 mg/Kg - dry 0.704 3.35
Benzo(a)anthracene 4 09/07/23 15:45 V37467AMP
<0.745 mg/Kg - dry 0.745 3.35Benzo(a)pyrene 4 09/07/23 15:45 V37467AMP
<0.740 mg/Kg - dry 0.740 3.35Benzo(b)fluoranthene 4 09/07/23 15:45 V37467AMP
<0.689 mg/Kg - dry 0.689 3.35Benzo(g,h,i)perylene 4 09/07/23 15:45 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.694 mg/Kg - dry 0.694 3.35Benzo(k)fluoranthene 4 09/07/23 15:45 V37467AMP
<2.94 mg/Kg - dry 2.94 10.2Benzoic Acid 4 09/07/23 15:45 V37467AMP
<0.532 mg/Kg - dry 0.532 3.35Benzyl alcohol 4 09/07/23 15:45 V37467AMP
<0.598 mg/Kg - dry 0.598 3.35Bis(2-Chloroethoxy)methane 4 09/07/23 15:45 V37467AMP
<0.542 mg/Kg - dry 0.542 3.35Bis(2-Chloroethyl)ether 4 09/07/23 15:45 V37467AMP
<0.689 mg/Kg - dry 0.689 1.67Bis(2-Chloroisopropyl)ether 4 09/07/23 15:45 V37467AMP
<0.608 mg/Kg - dry 0.608 3.35Bis(2-ethylhexyl)phthalate 4 09/07/23 15:45 V37467AMP
<0.552 mg/Kg - dry 0.552 3.354-Bromophenyl phenyl ether 4 09/07/23 15:45 V37467AMP
<0.572 mg/Kg - dry 0.572 1.67
Butyl benzyl phthalate 4 09/07/23 15:45 V37467AMP
<0.468 mg/Kg - dry 0.468 3.354-Chloro-3-methylphenol 4 09/07/23 15:45 V37467AMP
<0.567 mg/Kg - dry 0.567 1.674-Chloroaniline 4 09/07/23 15:45 V37467AMP
<0.588 mg/Kg - dry 0.588 3.352-Chloronaphthalene 4 09/07/23 15:45 V37467AMP
<0.498 mg/Kg - dry 0.498 3.352-Chlorophenol 4 09/07/23 15:45 V37467AMP
<0.638 mg/Kg - dry 0.638 5.074-Chlorophenyl phenyl ether 4 09/07/23 15:45 V37467AMP
<0.719 mg/Kg - dry 0.719 3.35Chrysene 4 09/07/23 15:45 V37467AMP
<1.17 mg/Kg - dry 1.17 3.35
Dibenz(a,h)anthracene 4 09/07/23 15:45 V37467AMP
<0.603 mg/Kg - dry 0.603 3.35Dibenzofuran 4 09/07/23 15:45 V37467AMP
<0.479 mg/Kg - dry 0.479 3.351,2-Dichlorobenzene 4 09/07/23 15:45 V37467AMP
<0.493 mg/Kg - dry 0.493 3.351,3-Dichlorobenzene 4 09/07/23 15:45 V37467AMP
<0.494 mg/Kg - dry 0.494 1.671,4-Dichlorobenzene 4 09/07/23 15:45 V37467AMP
<0.745 mg/Kg - dry 0.745 3.353,3'-Dichlorobenzidine 4 09/07/23 15:45 V37467AMP
<0.485 mg/Kg - dry 0.485 3.352,4-Dichlorophenol 4 09/07/23 15:45 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.912 mg/Kg - dry 0.912 3.35Diethyl phthalate 4 09/07/23 15:45 V37467AMP
<0.882 mg/Kg - dry 0.882 3.35Dimethyl phthalate 4 09/07/23 15:45 V37467AMP
<0.547 mg/Kg - dry 0.547 1.672,4-Dimethylphenol 4 09/07/23 15:45 V37467AMP
<0.542 mg/Kg - dry 0.542 3.35Di-n-butyl phthalate 4 09/07/23 15:45 V37467AMP
<1.22 mg/Kg - dry 1.22 7.604,6-Dinitro-2-methylphenol 4 09/07/23 15:45 V37467AMP
<2.64 mg/Kg - dry 2.64 7.602,4-Dinitrophenol 4 09/07/23 15:45 V37467AMP
<0.489 mg/Kg - dry 0.489 3.352,4-Dinitrotoluene 4 09/07/23 15:45 V37467AMP
<0.547 mg/Kg - dry 0.547 3.352,6-Dinitrotoluene 4 09/07/23 15:45 V37467AMP
<0.724 mg/Kg - dry 0.724 1.67
Di-n-Octyl Phthalate 4 09/07/23 15:45 V37467AMP
<0.623 mg/Kg - dry 0.623 3.35Fluoranthene 4 09/07/23 15:45 V37467AMP
<0.648 mg/Kg - dry 0.648 3.35Fluorene 4 09/07/23 15:45 V37467AMP
<0.537 mg/Kg - dry 0.537 3.35Hexachlorobenzene 4 09/07/23 15:45 V37467AMP
<0.494 mg/Kg - dry 0.494 3.35Hexachlorobutadiene 4 09/07/23 15:45 V37467AMP
<0.795 mg/Kg - dry 0.795 3.35Hexachlorocyclopentadiene 4 09/07/23 15:45 V37467AMP
<0.401 mg/Kg - dry 0.401 3.35Hexachloroethane 4 09/07/23 15:45 V37467AMP
<0.907 mg/Kg - dry 0.907 3.35
Indeno(1,2,3-cd)pyrene 4 09/07/23 15:45 V37467AMP
<0.968 mg/Kg - dry 0.968 3.35Isophorone 4 09/07/23 15:45 V37467AMP
<0.537 mg/Kg - dry 0.537 3.351-Methylnaphthalene 4 09/07/23 15:45 V37467AMP
<0.506 mg/Kg - dry 0.506 3.352-Methylnaphthalene 4 09/07/23 15:45 V37467AMP
<0.491 mg/Kg - dry 0.491 3.352-Methylphenol 4 09/07/23 15:45 V37467AMP
<0.430 mg/Kg - dry 0.430 3.353&4 Methylphenol 4 09/07/23 15:45 V37467AMP
<0.730 mg/Kg - dry 0.730 3.35Naphthalene 4 09/07/23 15:45 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-3
93829 Matrix:
8/31/2023 11:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.490 mg/Kg - dry 0.490 3.352-Nitroaniline 4 09/07/23 15:45 V37467AMP
<0.608 mg/Kg - dry 0.608 3.353-Nitroaniline 4 09/07/23 15:45 V37467AMP
<0.472 mg/Kg - dry 0.472 1.674-Nitroaniline 4 09/07/23 15:45 V37467AMP
<0.588 mg/Kg - dry 0.588 1.67Nitrobenzene 4 09/07/23 15:45 V37467AMP
<0.449 mg/Kg - dry 0.449 3.352-Nitrophenol 4 09/07/23 15:45 V37467AMP
<0.593 mg/Kg - dry 0.593 3.354-Nitrophenol 4 09/07/23 15:45 V37467AMP
<1.33 mg/Kg - dry 1.33 3.35N-Nitrosodimethylamine 4 09/07/23 15:45 V37467AMP
<0.917 mg/Kg - dry 0.917 3.35N-Nitrosodiphenylamine 4 09/07/23 15:45 V37467AMP
<0.598 mg/Kg - dry 0.598 3.35
N-Nitroso-di-n-propylamine 4 09/07/23 15:45 V37467AMP
<1.76 mg/Kg - dry 1.76 5.07Pentachlorophenol 4 09/07/23 15:45 V37467AMP
<1.05 mg/Kg - dry 1.05 3.35Phenanthrene 4 09/07/23 15:45 V37467AMP
<0.567 mg/Kg - dry 0.567 3.35Phenol 4 09/07/23 15:45 V37467AMP
<0.679 mg/Kg - dry 0.679 3.35Pyrene 4 09/07/23 15:45 V37467AMP
<0.401 mg/Kg - dry 0.401 1.67Pyridine 4 09/07/23 15:45 V37467AMP
<0.542 mg/Kg - dry 0.542 3.351,2,4-Trichlorobenzene 4 09/07/23 15:45 V37467AMP
<0.487 mg/Kg - dry 0.487 3.35
2,4,5-Trichlorophenol 4 09/07/23 15:45 V37467AMP
<0.489 mg/Kg - dry 0.489 3.352,4,6-Trichlorophenol 4 09/07/23 15:45 V37467AMP
8270ESurrogate: Phenol-d5 72.8 Limits: 34-121%09/07/23 15:454 AMP
Surrogate: 2-Fluorobiphenyl 82.6 Limits: 44-115%09/07/23 15:454 AMP V37467
Surrogate: 2-Fluorophenol 75.1 Limits: 35-115%09/07/23 15:454 AMP V37467
Surrogate: Nitrobenzene-d5 79.0 Limits: 37-122%09/07/23 15:454 AMP V37467
Surrogate: 4-Terphenyl-d14 88.6 Limits: 54-127%09/07/23 15:454 AMP V37467
Surrogate: 2,4,6-Tribromophenol 63.2 Limits: 39-132%09/07/23 15:454 AMP V37467
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.4 %Moisture 1 09/01/23 09:16 SW-DRYWTCNC
<0.186 mg/Kg - dry 0.186 0.264Chromium, Hexavalent 1 09/08/23 17:11 SW-7199SDS
0.938 mg/Kg - dry 0.113 0.331Arsenic 5 09/06/23 18:08 6020BCPW
79.4 mg/Kg - dry 0.056 0.330Barium 5 09/06/23 18:08 6020BCPW
0.143 J mg/Kg - dry 0.0343 0.331Cadmium 5 09/06/23 18:08 6020BCPW
41.0 mg/Kg - dry 0.153 0.330
Chromium 5 09/06/23 18:08 6020BCPW
36.8 mg/Kg - dry 0.0410 0.331Lead 5 09/06/23 18:08 6020BCPW
0.0513 mg/Kg - dry 0.0159 0.0397Mercury (Total)1 09/06/23 15:29 7471BJKC
0.427 mg/Kg - dry 0.136 0.330Selenium 5 09/06/23 18:08 6020BCPW
0.0390 J mg/Kg - dry 0.0089 0.331Silver 5 09/07/23 17:13 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.006 J mg/Kg - dry 0.003 0.026Acetone 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.026Acrolein 1 09/01/23 16:31 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/01/23 16:31 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 09/01/23 16:31 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/01/23 16:31 V37419TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/01/23 16:31 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/01/23 16:31 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/01/23 16:31 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 09/01/23 16:31 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/01/23 16:31 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/01/23 16:31 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/01/23 16:31 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/01/23 16:31 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006
1,1-Dichloropropene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/01/23 16:31 V37419TBL
<0.018 mg/Kg - dry 0.018 0.330Ethanol 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 09/01/23 16:31 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0262-Hexanone 1 09/01/23 16:31 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/01/23 16:31 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/01/23 16:31 V37419TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/01/23 16:31 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/01/23 16:31 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.013
1,2,3-Trichlorobenzene 1 09/01/23 16:31 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/01/23 16:31 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/01/23 16:31 V37419TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 09/01/23 16:31 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 09/01/23 16:31 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/01/23 16:31 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 09/01/23 16:31 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 09/01/23 16:31 V37419TBL
<0.001 mg/Kg - dry 0.001 0.013m,p-Xylene 1 09/01/23 16:31 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.006Xylene (Total)1 09/01/23 16:31 V37419
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/01/23 16:311 TBL V37419
Surrogate: Dibromofluoromethane 109 Limits: 84-123%09/01/23 16:311 TBL V37419
Surrogate: Toluene-d8 99.2 Limits: 76-129%09/01/23 16:311 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
2.59 J mg/Kg - dry 0.613 3.49Acenaphthene 4 09/07/23 15:22 V37467AMP
<0.555 mg/Kg - dry 0.555 3.49Acenaphthylene 4 09/07/23 15:22 V37467AMP
<0.804 mg/Kg - dry 0.804 3.49Aniline 4 09/07/23 15:22 V37467AMP
3.29 J mg/Kg - dry 0.756 3.49Anthracene 4 09/07/23 15:22 V37467AMP
6.76 mg/Kg - dry 0.735 3.49
Benzo(a)anthracene 4 09/07/23 15:22 V37467AMP
6.69 mg/Kg - dry 0.777 3.49Benzo(a)pyrene 4 09/07/23 15:22 V37467AMP
7.49 mg/Kg - dry 0.772 3.49Benzo(b)fluoranthene 4 09/07/23 15:22 V37467AMP
3.28 J mg/Kg - dry 0.719 3.49Benzo(g,h,i)perylene 4 09/07/23 15:22 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
2.87 J mg/Kg - dry 0.724 3.49Benzo(k)fluoranthene 4 09/07/23 15:22 V37467AMP
<3.07 mg/Kg - dry 3.07 10.6Benzoic Acid 4 09/07/23 15:22 V37467AMP
<0.555 mg/Kg - dry 0.555 3.49Benzyl alcohol 4 09/07/23 15:22 V37467AMP
<0.624 mg/Kg - dry 0.624 3.49Bis(2-Chloroethoxy)methane 4 09/07/23 15:22 V37467AMP
<0.566 mg/Kg - dry 0.566 3.49Bis(2-Chloroethyl)ether 4 09/07/23 15:22 V37467AMP
<0.719 mg/Kg - dry 0.719 1.75Bis(2-Chloroisopropyl)ether 4 09/07/23 15:22 V37467AMP
<0.634 mg/Kg - dry 0.634 3.49Bis(2-ethylhexyl)phthalate 4 09/07/23 15:22 V37467AMP
<0.576 mg/Kg - dry 0.576 3.494-Bromophenyl phenyl ether 4 09/07/23 15:22 V37467AMP
<0.597 mg/Kg - dry 0.597 1.75
Butyl benzyl phthalate 4 09/07/23 15:22 V37467AMP
<0.489 mg/Kg - dry 0.489 3.494-Chloro-3-methylphenol 4 09/07/23 15:22 V37467AMP
<0.592 mg/Kg - dry 0.592 1.754-Chloroaniline 4 09/07/23 15:22 V37467AMP
<0.613 mg/Kg - dry 0.613 3.492-Chloronaphthalene 4 09/07/23 15:22 V37467AMP
<0.519 mg/Kg - dry 0.519 3.492-Chlorophenol 4 09/07/23 15:22 V37467AMP
<0.666 mg/Kg - dry 0.666 5.294-Chlorophenyl phenyl ether 4 09/07/23 15:22 V37467AMP
6.22 mg/Kg - dry 0.751 3.49Chrysene 4 09/07/23 15:22 V37467AMP
<1.22 mg/Kg - dry 1.22 3.49
Dibenz(a,h)anthracene 4 09/07/23 15:22 V37467AMP
1.06 J mg/Kg - dry 0.629 3.49Dibenzofuran 4 09/07/23 15:22 V37467AMP
<0.500 mg/Kg - dry 0.500 3.491,2-Dichlorobenzene 4 09/07/23 15:22 V37467AMP
<0.514 mg/Kg - dry 0.514 3.491,3-Dichlorobenzene 4 09/07/23 15:22 V37467AMP
<0.515 mg/Kg - dry 0.515 1.751,4-Dichlorobenzene 4 09/07/23 15:22 V37467AMP
<0.777 mg/Kg - dry 0.777 3.493,3'-Dichlorobenzidine 4 09/07/23 15:22 V37467AMP
<0.506 mg/Kg - dry 0.506 3.492,4-Dichlorophenol 4 09/07/23 15:22 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.952 mg/Kg - dry 0.952 3.49Diethyl phthalate 4 09/07/23 15:22 V37467AMP
<0.920 mg/Kg - dry 0.920 3.49Dimethyl phthalate 4 09/07/23 15:22 V37467AMP
<0.571 mg/Kg - dry 0.571 1.752,4-Dimethylphenol 4 09/07/23 15:22 V37467AMP
<0.566 mg/Kg - dry 0.566 3.49Di-n-butyl phthalate 4 09/07/23 15:22 V37467AMP
<1.27 mg/Kg - dry 1.27 7.944,6-Dinitro-2-methylphenol 4 09/07/23 15:22 V37467AMP
<2.75 mg/Kg - dry 2.75 7.942,4-Dinitrophenol 4 09/07/23 15:22 V37467AMP
<0.510 mg/Kg - dry 0.510 3.492,4-Dinitrotoluene 4 09/07/23 15:22 V37467AMP
<0.571 mg/Kg - dry 0.571 3.492,6-Dinitrotoluene 4 09/07/23 15:22 V37467AMP
<0.756 mg/Kg - dry 0.756 1.75
Di-n-Octyl Phthalate 4 09/07/23 15:22 V37467AMP
12.3 mg/Kg - dry 0.650 3.49Fluoranthene 4 09/07/23 15:22 V37467AMP
1.68 J mg/Kg - dry 0.677 3.49Fluorene 4 09/07/23 15:22 V37467AMP
<0.560 mg/Kg - dry 0.560 3.49Hexachlorobenzene 4 09/07/23 15:22 V37467AMP
<0.515 mg/Kg - dry 0.515 3.49Hexachlorobutadiene 4 09/07/23 15:22 V37467AMP
<0.830 mg/Kg - dry 0.830 3.49Hexachlorocyclopentadiene 4 09/07/23 15:22 V37467AMP
<0.419 mg/Kg - dry 0.419 3.49Hexachloroethane 4 09/07/23 15:22 V37467AMP
3.88 mg/Kg - dry 0.947 3.49
Indeno(1,2,3-cd)pyrene 4 09/07/23 15:22 V37467AMP
<1.01 mg/Kg - dry 1.01 3.49Isophorone 4 09/07/23 15:22 V37467AMP
<0.560 mg/Kg - dry 0.560 3.491-Methylnaphthalene 4 09/07/23 15:22 V37467AMP
<0.529 mg/Kg - dry 0.529 3.492-Methylnaphthalene 4 09/07/23 15:22 V37467AMP
<0.513 mg/Kg - dry 0.513 3.492-Methylphenol 4 09/07/23 15:22 V37467AMP
<0.449 mg/Kg - dry 0.449 3.493&4 Methylphenol 4 09/07/23 15:22 V37467AMP
1.21 J mg/Kg - dry 0.761 3.49Naphthalene 4 09/07/23 15:22 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-4
93830 Matrix:
8/31/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.511 mg/Kg - dry 0.511 3.492-Nitroaniline 4 09/07/23 15:22 V37467AMP
<0.634 mg/Kg - dry 0.634 3.493-Nitroaniline 4 09/07/23 15:22 V37467AMP
<0.493 mg/Kg - dry 0.493 1.754-Nitroaniline 4 09/07/23 15:22 V37467AMP
<0.613 mg/Kg - dry 0.613 1.75Nitrobenzene 4 09/07/23 15:22 V37467AMP
<0.469 mg/Kg - dry 0.469 3.492-Nitrophenol 4 09/07/23 15:22 V37467AMP
<0.619 mg/Kg - dry 0.619 3.494-Nitrophenol 4 09/07/23 15:22 V37467AMP
<1.39 mg/Kg - dry 1.39 3.49N-Nitrosodimethylamine 4 09/07/23 15:22 V37467AMP
<0.957 mg/Kg - dry 0.957 3.49N-Nitrosodiphenylamine 4 09/07/23 15:22 V37467AMP
<0.624 mg/Kg - dry 0.624 3.49
N-Nitroso-di-n-propylamine 4 09/07/23 15:22 V37467AMP
<1.84 mg/Kg - dry 1.84 5.29Pentachlorophenol 4 09/07/23 15:22 V37467AMP
12.2 mg/Kg - dry 1.10 3.49Phenanthrene 4 09/07/23 15:22 V37467AMP
<0.592 mg/Kg - dry 0.592 3.49Phenol 4 09/07/23 15:22 V37467AMP
11.1 mg/Kg - dry 0.708 3.49Pyrene 4 09/07/23 15:22 V37467AMP
<0.419 mg/Kg - dry 0.419 1.75Pyridine 4 09/07/23 15:22 V37467AMP
<0.566 mg/Kg - dry 0.566 3.491,2,4-Trichlorobenzene 4 09/07/23 15:22 V37467AMP
<0.509 mg/Kg - dry 0.509 3.49
2,4,5-Trichlorophenol 4 09/07/23 15:22 V37467AMP
<0.510 mg/Kg - dry 0.510 3.492,4,6-Trichlorophenol 4 09/07/23 15:22 V37467AMP
8270ESurrogate: Phenol-d5 65.2 Limits: 34-121%09/07/23 15:224 AMP
Surrogate: 2-Fluorobiphenyl 82.0 Limits: 44-115%09/07/23 15:224 AMP V37467
Surrogate: 2-Fluorophenol 64.6 Limits: 35-115%09/07/23 15:224 AMP V37467
Surrogate: Nitrobenzene-d5 67.7 Limits: 37-122%09/07/23 15:224 AMP V37467
Surrogate: 4-Terphenyl-d14 90.4 Limits: 54-127%09/07/23 15:224 AMP V37467
Surrogate: 2,4,6-Tribromophenol 64.6 Limits: 39-132%09/07/23 15:224 AMP V37467
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.0 %Moisture 1 09/01/23 09:16 SW-DRYWTCNC
<0.164 mg/Kg - dry 0.164 0.234Chromium, Hexavalent 1 09/08/23 17:22 SW-7199SDS
0.507 mg/Kg - dry 0.0982 0.287Arsenic 5 09/06/23 18:12 6020BCPW
94.0 mg/Kg - dry 0.049 0.287Barium 5 09/06/23 18:12 6020BCPW
0.0610 J mg/Kg - dry 0.0298 0.287Cadmium 5 09/06/23 18:12 6020BCPW
19.8 mg/Kg - dry 0.133 0.287
Chromium 5 09/06/23 18:12 6020BCPW
12.3 mg/Kg - dry 0.0356 0.287Lead 5 09/06/23 18:12 6020BCPW
0.100 mg/Kg - dry 0.0138 0.0345Mercury (Total)1 09/06/23 15:32 7471BJKC
0.495 mg/Kg - dry 0.118 0.287Selenium 5 09/06/23 18:12 6020BCPW
0.0173 J mg/Kg - dry 0.0077 0.287Silver 5 09/07/23 17:17 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.007 J mg/Kg - dry 0.002 0.022Acetone 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 09/01/23 16:58 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 09/01/23 16:58 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/01/23 16:58 V37419TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/01/23 16:58 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 09/01/23 16:58 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 09/01/23 16:58 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 09/01/23 16:58 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 09/01/23 16:58 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 09/01/23 16:58 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 09/01/23 16:58 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/01/23 16:58 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 09/01/23 16:58 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/01/23 16:58 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/01/23 16:58 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/01/23 16:58 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/01/23 16:58 V37419TBL
<0.016 mg/Kg - dry 0.016 0.287Ethanol 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 09/01/23 16:58 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.057Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 16:58 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 09/01/23 16:58 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.001 J mg/Kg - dry 0.0008 0.011n-Hexane 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 09/01/23 16:58 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/01/23 16:58 V37419TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/01/23 16:58 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 09/01/23 16:58 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 09/01/23 16:58 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/01/23 16:58 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 09/01/23 16:58 V37419TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 09/01/23 16:58 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/01/23 16:58 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 09/01/23 16:58 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 09/01/23 16:58 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 09/01/23 16:58 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 09/01/23 16:58 V37419
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/01/23 16:581 TBL V37419
Surrogate: Dibromofluoromethane 106 Limits: 84-123%09/01/23 16:581 TBL V37419
Surrogate: Toluene-d8 99.8 Limits: 76-129%09/01/23 16:581 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.133 mg/Kg - dry 0.133 0.758Acenaphthene 1 09/06/23 21:24 V37467AMP
<0.120 mg/Kg - dry 0.120 0.758Acenaphthylene 1 09/06/23 21:24 V37467AMP
<0.174 mg/Kg - dry 0.174 0.758Aniline 1 09/06/23 21:24 V37467AMP
<0.164 mg/Kg - dry 0.164 0.758Anthracene 1 09/06/23 21:24 V37467AMP
<0.159 mg/Kg - dry 0.159 0.758
Benzo(a)anthracene 1 09/06/23 21:24 V37467AMP
<0.168 mg/Kg - dry 0.168 0.758Benzo(a)pyrene 1 09/06/23 21:24 V37467AMP
<0.167 mg/Kg - dry 0.167 0.758Benzo(b)fluoranthene 1 09/06/23 21:24 V37467AMP
<0.156 mg/Kg - dry 0.156 0.758Benzo(g,h,i)perylene 1 09/06/23 21:24 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.157 mg/Kg - dry 0.157 0.758Benzo(k)fluoranthene 1 09/06/23 21:24 V37467AMP
<0.666 mg/Kg - dry 0.666 2.30Benzoic Acid 1 09/06/23 21:24 V37467AMP
<0.120 mg/Kg - dry 0.120 0.758Benzyl alcohol 1 09/06/23 21:24 V37467AMP
<0.135 mg/Kg - dry 0.135 0.758Bis(2-Chloroethoxy)methane 1 09/06/23 21:24 V37467AMP
<0.122 mg/Kg - dry 0.122 0.758Bis(2-Chloroethyl)ether 1 09/06/23 21:24 V37467AMP
<0.156 mg/Kg - dry 0.156 0.379Bis(2-Chloroisopropyl)ether 1 09/06/23 21:24 V37467AMP
<0.137 mg/Kg - dry 0.137 0.758Bis(2-ethylhexyl)phthalate 1 09/06/23 21:24 V37467AMP
<0.125 mg/Kg - dry 0.125 0.7584-Bromophenyl phenyl ether 1 09/06/23 21:24 V37467AMP
<0.129 mg/Kg - dry 0.129 0.379
Butyl benzyl phthalate 1 09/06/23 21:24 V37467AMP
<0.106 mg/Kg - dry 0.106 0.7584-Chloro-3-methylphenol 1 09/06/23 21:24 V37467AMP
<0.128 mg/Kg - dry 0.128 0.3794-Chloroaniline 1 09/06/23 21:24 V37467AMP
<0.133 mg/Kg - dry 0.133 0.7582-Chloronaphthalene 1 09/06/23 21:24 V37467AMP
<0.112 mg/Kg - dry 0.112 0.7582-Chlorophenol 1 09/06/23 21:24 V37467AMP
<0.144 mg/Kg - dry 0.144 1.154-Chlorophenyl phenyl ether 1 09/06/23 21:24 V37467AMP
<0.163 mg/Kg - dry 0.163 0.758Chrysene 1 09/06/23 21:24 V37467AMP
<0.264 mg/Kg - dry 0.264 0.758
Dibenz(a,h)anthracene 1 09/06/23 21:24 V37467AMP
<0.136 mg/Kg - dry 0.136 0.758Dibenzofuran 1 09/06/23 21:24 V37467AMP
<0.108 mg/Kg - dry 0.108 0.7581,2-Dichlorobenzene 1 09/06/23 21:24 V37467AMP
<0.111 mg/Kg - dry 0.111 0.7581,3-Dichlorobenzene 1 09/06/23 21:24 V37467AMP
<0.112 mg/Kg - dry 0.112 0.3791,4-Dichlorobenzene 1 09/06/23 21:24 V37467AMP
<0.168 mg/Kg - dry 0.168 0.7583,3'-Dichlorobenzidine 1 09/06/23 21:24 V37467AMP
<0.110 mg/Kg - dry 0.110 0.7582,4-Dichlorophenol 1 09/06/23 21:24 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.206 mg/Kg - dry 0.206 0.758Diethyl phthalate 1 09/06/23 21:24 V37467AMP
<0.200 mg/Kg - dry 0.200 0.758Dimethyl phthalate 1 09/06/23 21:24 V37467AMP
<0.124 mg/Kg - dry 0.124 0.3792,4-Dimethylphenol 1 09/06/23 21:24 V37467AMP
<0.122 mg/Kg - dry 0.122 0.758Di-n-butyl phthalate 1 09/06/23 21:24 V37467AMP
<0.275 mg/Kg - dry 0.275 1.724,6-Dinitro-2-methylphenol 1 09/06/23 21:24 V37467AMP
<0.597 mg/Kg - dry 0.597 1.722,4-Dinitrophenol 1 09/06/23 21:24 V37467AMP
<0.111 mg/Kg - dry 0.111 0.7582,4-Dinitrotoluene 1 09/06/23 21:24 V37467AMP
<0.124 mg/Kg - dry 0.124 0.7582,6-Dinitrotoluene 1 09/06/23 21:24 V37467AMP
<0.164 mg/Kg - dry 0.164 0.379
Di-n-Octyl Phthalate 1 09/06/23 21:24 V37467AMP
<0.141 mg/Kg - dry 0.141 0.758Fluoranthene 1 09/06/23 21:24 V37467AMP
<0.147 mg/Kg - dry 0.147 0.758Fluorene 1 09/06/23 21:24 V37467AMP
<0.121 mg/Kg - dry 0.121 0.758Hexachlorobenzene 1 09/06/23 21:24 V37467AMP
<0.112 mg/Kg - dry 0.112 0.758Hexachlorobutadiene 1 09/06/23 21:24 V37467AMP
<0.180 mg/Kg - dry 0.180 0.758Hexachlorocyclopentadiene 1 09/06/23 21:24 V37467AMP
<0.091 mg/Kg - dry 0.091 0.758Hexachloroethane 1 09/06/23 21:24 V37467AMP
<0.205 mg/Kg - dry 0.205 0.758
Indeno(1,2,3-cd)pyrene 1 09/06/23 21:24 V37467AMP
<0.219 mg/Kg - dry 0.219 0.758Isophorone 1 09/06/23 21:24 V37467AMP
<0.121 mg/Kg - dry 0.121 0.7581-Methylnaphthalene 1 09/06/23 21:24 V37467AMP
<0.114 mg/Kg - dry 0.114 0.7582-Methylnaphthalene 1 09/06/23 21:24 V37467AMP
<0.111 mg/Kg - dry 0.111 0.7582-Methylphenol 1 09/06/23 21:24 V37467AMP
<0.097 mg/Kg - dry 0.097 0.7583&4 Methylphenol 1 09/06/23 21:24 V37467AMP
<0.165 mg/Kg - dry 0.165 0.758Naphthalene 1 09/06/23 21:24 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-5
93831 Matrix:
8/31/2023 12:50
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.111 mg/Kg - dry 0.111 0.7582-Nitroaniline 1 09/06/23 21:24 V37467AMP
<0.137 mg/Kg - dry 0.137 0.7583-Nitroaniline 1 09/06/23 21:24 V37467AMP
<0.107 mg/Kg - dry 0.107 0.3794-Nitroaniline 1 09/06/23 21:24 V37467AMP
<0.133 mg/Kg - dry 0.133 0.379Nitrobenzene 1 09/06/23 21:24 V37467AMP
<0.102 mg/Kg - dry 0.102 0.7582-Nitrophenol 1 09/06/23 21:24 V37467AMP
<0.134 mg/Kg - dry 0.134 0.7584-Nitrophenol 1 09/06/23 21:24 V37467AMP
<0.302 mg/Kg - dry 0.302 0.758N-Nitrosodimethylamine 1 09/06/23 21:24 V37467AMP
<0.208 mg/Kg - dry 0.208 0.758N-Nitrosodiphenylamine 1 09/06/23 21:24 V37467AMP
<0.135 mg/Kg - dry 0.135 0.758
N-Nitroso-di-n-propylamine 1 09/06/23 21:24 V37467AMP
<0.398 mg/Kg - dry 0.398 1.15Pentachlorophenol 1 09/06/23 21:24 V37467AMP
<0.239 mg/Kg - dry 0.239 0.758Phenanthrene 1 09/06/23 21:24 V37467AMP
<0.128 mg/Kg - dry 0.128 0.758Phenol 1 09/06/23 21:24 V37467AMP
<0.154 mg/Kg - dry 0.154 0.758Pyrene 1 09/06/23 21:24 V37467AMP
<0.091 mg/Kg - dry 0.091 0.379Pyridine 1 09/06/23 21:24 V37467AMP
<0.122 mg/Kg - dry 0.122 0.7581,2,4-Trichlorobenzene 1 09/06/23 21:24 V37467AMP
<0.110 mg/Kg - dry 0.110 0.758
2,4,5-Trichlorophenol 1 09/06/23 21:24 V37467AMP
<0.111 mg/Kg - dry 0.111 0.7582,4,6-Trichlorophenol 1 09/06/23 21:24 V37467AMP
8270ESurrogate: Phenol-d5 77.2 Limits: 34-121%09/06/23 21:241 AMP
Surrogate: 2-Fluorobiphenyl 91.0 Limits: 44-115%09/06/23 21:241 AMP V37467
Surrogate: 2-Fluorophenol 79.6 Limits: 35-115%09/06/23 21:241 AMP V37467
Surrogate: Nitrobenzene-d5 87.3 Limits: 37-122%09/06/23 21:241 AMP V37467
Surrogate: 4-Terphenyl-d14 98.8 Limits: 54-127%09/06/23 21:241 AMP V37467
Surrogate: 2,4,6-Tribromophenol 79.9 Limits: 39-132%09/06/23 21:241 AMP V37467
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.9 %Moisture 1 09/01/23 09:16 SW-DRYWTCNC
<0.168 mg/Kg - dry 0.168 0.239Chromium, Hexavalent 1 09/08/23 17:33 SW-7199SDS
0.857 mg/Kg - dry 0.100 0.294Arsenic 5 09/06/23 18:16 6020BCPW
77.8 mg/Kg - dry 0.050 0.293Barium 5 09/06/23 18:16 6020BCPW
0.116 J mg/Kg - dry 0.0305 0.294Cadmium 5 09/06/23 18:16 6020BCPW
37.4 mg/Kg - dry 0.136 0.293
Chromium 5 09/06/23 18:16 6020BCPW
38.9 mg/Kg - dry 0.0364 0.294Lead 5 09/06/23 18:16 6020BCPW
0.0622 mg/Kg - dry 0.0141 0.0353Mercury (Total)1 09/06/23 15:34 7471BJKC
0.490 mg/Kg - dry 0.121 0.293Selenium 5 09/06/23 18:16 6020BCPW
0.0298 J mg/Kg - dry 0.0079 0.294Silver 5 09/07/23 17:21 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
0.010 J mg/Kg - dry 0.002 0.023Acetone 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 09/01/23 17:26 V37419TBL
<0.002 mg/Kg - dry 0.002 0.011
Bromomethane 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 09/01/23 17:26 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 09/01/23 17:26 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005
Chlorodibromomethane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 09/01/23 17:26 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 09/01/23 17:26 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 09/01/23 17:26 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 09/01/23 17:26 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 09/01/23 17:26 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005
1,2-Dichloroethane 1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 09/01/23 17:26 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005
1,1-Dichloropropene 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 09/01/23 17:26 V37419TBL
<0.016 mg/Kg - dry 0.016 0.293Ethanol 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 09/01/23 17:26 V37419TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 09/01/23 17:26 V37419TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 09/01/23 17:26 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 09/01/23 17:26 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 09/01/23 17:26 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 09/01/23 17:26 V37419TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 09/01/23 17:26 V37419TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011
Naphthalene 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 09/01/23 17:26 V37419TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 09/01/23 17:26 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.011
1,2,3-Trichlorobenzene 1 09/01/23 17:26 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 09/01/23 17:26 V37419TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 09/01/23 17:26 V37419TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 09/01/23 17:26 V37419TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37418 09/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 09/01/23 17:26 V37419TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 09/01/23 17:26 V37419TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 09/01/23 17:26 V37419TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 09/01/23 17:26 V37419
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%09/01/23 17:261 TBL V37419
Surrogate: Dibromofluoromethane 107 Limits: 84-123%09/01/23 17:261 TBL V37419
Surrogate: Toluene-d8 99.8 Limits: 76-129%09/01/23 17:261 TBL V37419
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.136 mg/Kg - dry 0.136 0.775Acenaphthene 1 09/07/23 00:26 V37467AMP
<0.123 mg/Kg - dry 0.123 0.775Acenaphthylene 1 09/07/23 00:26 V37467AMP
<0.178 mg/Kg - dry 0.178 0.775Aniline 1 09/07/23 00:26 V37467AMP
<0.168 mg/Kg - dry 0.168 0.775Anthracene 1 09/07/23 00:26 V37467AMP
0.446 J
mg/Kg - dry 0.163 0.775
Benzo(a)anthracene 1 09/07/23 00:26 V37467AMP
0.519 J mg/Kg - dry 0.172 0.775Benzo(a)pyrene 1 09/07/23 00:26 V37467AMP
0.640 J mg/Kg - dry 0.171 0.775Benzo(b)fluoranthene 1 09/07/23 00:26 V37467AMP
0.358 J mg/Kg - dry 0.159 0.775Benzo(g,h,i)perylene 1 09/07/23 00:26 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
0.233 J mg/Kg - dry 0.160 0.775Benzo(k)fluoranthene 1 09/07/23 00:26 V37467AMP
<0.681 mg/Kg - dry 0.681 2.35Benzoic Acid 1 09/07/23 00:26 V37467AMP
<0.123 mg/Kg - dry 0.123 0.775Benzyl alcohol 1 09/07/23 00:26 V37467AMP
<0.138 mg/Kg - dry 0.138 0.775Bis(2-Chloroethoxy)methane 1 09/07/23 00:26 V37467AMP
<0.125 mg/Kg - dry 0.125 0.775Bis(2-Chloroethyl)ether 1 09/07/23 00:26 V37467AMP
<0.159 mg/Kg - dry 0.159 0.387Bis(2-Chloroisopropyl)ether 1 09/07/23 00:26 V37467AMP
<0.141 mg/Kg - dry 0.141 0.775Bis(2-ethylhexyl)phthalate 1 09/07/23 00:26 V37467AMP
<0.128 mg/Kg - dry 0.128 0.7754-Bromophenyl phenyl ether 1 09/07/23 00:26 V37467AMP
<0.132 mg/Kg - dry 0.132 0.387
Butyl benzyl phthalate 1 09/07/23 00:26 V37467AMP
<0.108 mg/Kg - dry 0.108 0.7754-Chloro-3-methylphenol 1 09/07/23 00:26 V37467AMP
<0.131 mg/Kg - dry 0.131 0.3874-Chloroaniline 1 09/07/23 00:26 V37467AMP
<0.136 mg/Kg - dry 0.136 0.7752-Chloronaphthalene 1 09/07/23 00:26 V37467AMP
<0.115 mg/Kg - dry 0.115 0.7752-Chlorophenol 1 09/07/23 00:26 V37467AMP
<0.148 mg/Kg - dry 0.148 1.184-Chlorophenyl phenyl ether 1 09/07/23 00:26 V37467AMP
0.447 J mg/Kg - dry 0.166 0.775Chrysene 1 09/07/23 00:26 V37467AMP
<0.270 mg/Kg - dry 0.270 0.775
Dibenz(a,h)anthracene 1 09/07/23 00:26 V37467AMP
<0.139 mg/Kg - dry 0.139 0.775Dibenzofuran 1 09/07/23 00:26 V37467AMP
<0.110 mg/Kg - dry 0.110 0.7751,2-Dichlorobenzene 1 09/07/23 00:26 V37467AMP
<0.114 mg/Kg - dry 0.114 0.7751,3-Dichlorobenzene 1 09/07/23 00:26 V37467AMP
<0.114 mg/Kg - dry 0.114 0.3871,4-Dichlorobenzene 1 09/07/23 00:26 V37467AMP
<0.172 mg/Kg - dry 0.172 0.7753,3'-Dichlorobenzidine 1 09/07/23 00:26 V37467AMP
<0.112 mg/Kg - dry 0.112 0.7752,4-Dichlorophenol 1 09/07/23 00:26 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.211 mg/Kg - dry 0.211 0.775Diethyl phthalate 1 09/07/23 00:26 V37467AMP
<0.204 mg/Kg - dry 0.204 0.775Dimethyl phthalate 1 09/07/23 00:26 V37467AMP
<0.126 mg/Kg - dry 0.126 0.3872,4-Dimethylphenol 1 09/07/23 00:26 V37467AMP
<0.125 mg/Kg - dry 0.125 0.775Di-n-butyl phthalate 1 09/07/23 00:26 V37467AMP
<0.282 mg/Kg - dry 0.282 1.764,6-Dinitro-2-methylphenol 1 09/07/23 00:26 V37467AMP
<0.611 mg/Kg - dry 0.611 1.762,4-Dinitrophenol 1 09/07/23 00:26 V37467AMP
<0.113 mg/Kg - dry 0.113 0.7752,4-Dinitrotoluene 1 09/07/23 00:26 V37467AMP
<0.126 mg/Kg - dry 0.126 0.7752,6-Dinitrotoluene 1 09/07/23 00:26 V37467AMP
<0.168 mg/Kg - dry 0.168 0.387
Di-n-Octyl Phthalate 1 09/07/23 00:26 V37467AMP
0.609 J mg/Kg - dry 0.144 0.775Fluoranthene 1 09/07/23 00:26 V37467AMP
<0.150 mg/Kg - dry 0.150 0.775Fluorene 1 09/07/23 00:26 V37467AMP
<0.124 mg/Kg - dry 0.124 0.775Hexachlorobenzene 1 09/07/23 00:26 V37467AMP
<0.114 mg/Kg - dry 0.114 0.775Hexachlorobutadiene 1 09/07/23 00:26 V37467AMP
<0.184 mg/Kg - dry 0.184 0.775Hexachlorocyclopentadiene 1 09/07/23 00:26 V37467AMP
<0.093 mg/Kg - dry 0.093 0.775Hexachloroethane 1 09/07/23 00:26 V37467AMP
0.366 J
mg/Kg - dry 0.210 0.775
Indeno(1,2,3-cd)pyrene 1 09/07/23 00:26 V37467AMP
<0.224 mg/Kg - dry 0.224 0.775Isophorone 1 09/07/23 00:26 V37467AMP
<0.124 mg/Kg - dry 0.124 0.7751-Methylnaphthalene 1 09/07/23 00:26 V37467AMP
<0.117 mg/Kg - dry 0.117 0.7752-Methylnaphthalene 1 09/07/23 00:26 V37467AMP
<0.113 mg/Kg - dry 0.113 0.7752-Methylphenol 1 09/07/23 00:26 V37467AMP
<0.099 mg/Kg - dry 0.099 0.7753&4 Methylphenol 1 09/07/23 00:26 V37467AMP
<0.169 mg/Kg - dry 0.169 0.775Naphthalene 1 09/07/23 00:26 V37467AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 80
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-243-0019
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Charlotte
Received : 08/31/2023
TCR-001
Revised Report Date: 10/24/2023
Original Report Date : 09/13/2023
Sample ID :
Lab No :
Sampled:FG-DUP
93832 Matrix:
8/31/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37441 09/05/23 10:20
<0.113 mg/Kg - dry 0.113 0.7752-Nitroaniline 1 09/07/23 00:26 V37467AMP
<0.141 mg/Kg - dry 0.141 0.7753-Nitroaniline 1 09/07/23 00:26 V37467AMP
<0.109 mg/Kg - dry 0.109 0.3874-Nitroaniline 1 09/07/23 00:26 V37467AMP
<0.136 mg/Kg - dry 0.136 0.387Nitrobenzene 1 09/07/23 00:26 V37467AMP
<0.104 mg/Kg - dry 0.104 0.7752-Nitrophenol 1 09/07/23 00:26 V37467AMP
<0.137 mg/Kg - dry 0.137 0.7754-Nitrophenol 1 09/07/23 00:26 V37467AMP
<0.309 mg/Kg - dry 0.309 0.775N-Nitrosodimethylamine 1 09/07/23 00:26 V37467AMP
<0.212 mg/Kg - dry 0.212 0.775N-Nitrosodiphenylamine 1 09/07/23 00:26 V37467AMP
<0.138 mg/Kg - dry 0.138 0.775
N-Nitroso-di-n-propylamine 1 09/07/23 00:26 V37467AMP
<0.407 mg/Kg - dry 0.407 1.18Pentachlorophenol 1 09/07/23 00:26 V37467AMP
0.256 J mg/Kg - dry 0.244 0.775Phenanthrene 1 09/07/23 00:26 V37467AMP
<0.131 mg/Kg - dry 0.131 0.775Phenol 1 09/07/23 00:26 V37467AMP
0.679 J mg/Kg - dry 0.157 0.775Pyrene 1 09/07/23 00:26 V37467AMP
<0.093 mg/Kg - dry 0.093 0.387Pyridine 1 09/07/23 00:26 V37467AMP
<0.125 mg/Kg - dry 0.125 0.7751,2,4-Trichlorobenzene 1 09/07/23 00:26 V37467AMP
<0.113 mg/Kg - dry 0.113 0.775
2,4,5-Trichlorophenol 1 09/07/23 00:26 V37467AMP
<0.113 mg/Kg - dry 0.113 0.7752,4,6-Trichlorophenol 1 09/07/23 00:26 V37467AMP
8270ESurrogate: Phenol-d5 72.7 Limits: 34-121%09/07/23 00:261 AMP
Surrogate: 2-Fluorobiphenyl 86.2 Limits: 44-115%09/07/23 00:261 AMP V37467
Surrogate: 2-Fluorophenol 74.8 Limits: 35-115%09/07/23 00:261 AMP V37467
Surrogate: Nitrobenzene-d5 80.2 Limits: 37-122%09/07/23 00:261 AMP V37467
Surrogate: 4-Terphenyl-d14 95.2 Limits: 54-127%09/07/23 00:261 AMP V37467
Surrogate: 2,4,6-Tribromophenol 75.4 Limits: 39-132%09/07/23 00:261 AMP V37467
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 55 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Metals Analyses
6020B
L702982,L703242QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L702308
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-L702308 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/06/23 17:350.2500.0855<0.0855mg/KgArsenic
09/06/23 17:350.2500.0420.118mg/KgBarium
09/06/23 17:350.2500.0260<0.0260mg/KgCadmium
09/06/23 17:350.2500.1160.118mg/KgChromium
09/06/23 17:350.2500.0310<0.0310mg/KgLead
09/06/23 17:350.2500.103<0.103mg/KgSelenium
09/06/23 17:350.2500.0067<0.0067mg/KgSilver
LCS-L702308Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.02.302.50mg/KgArsenic 80-120
89.04.475.00mg/KgBarium 80-120
93.00.4640.500mg/KgCadmium 80-120
98.04.905.00mg/KgChromium 80-120
96.02.412.50mg/KgLead 80-120
92.04.625.00mg/KgSelenium 80-120
94.00.4700.500mg/KgSilver 80-120
V 93832-MS-L702308 V 93832-MSD-L702308Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.68 39.0*1.352.402.420.729mg/KgArsenic 26.0*75-125 21.7 80
51.1 0.0*68.54.794.8466.2mg/KgBarium 48.0*75-125 29.0 80
0.526 88.00.5090.4790.4840.0988mg/KgCadmium 86.0 75-125 3.2 80
26.0 0.0*27.04.794.8431.8mg/KgChromium 0.0*75-125 3.7 80
Page 1 of 23* QC Fail Date:10/24/2023 02:11 PM
Page 56 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Metals Analyses
6020B
L702982,L703242QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L702308
V 93832-MS-L702308 V 93832-MSD-L702308Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
35.3 91.031.92.402.4233.1mg/KgLead 0.0*75-125 10.1 80
0.922 10.0*0.9874.794.840.417mg/KgSelenium 12.0*75-125 6.8 80
0.470 92.00.4370.4790.4840.0254mg/KgSilver 86.0 75-125 7.2 80
V 93832-PDS-L702308Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/06/23 18:4095.01.20mg/KgArsenic
09/06/23 18:4086.07.70mg/KgBarium
09/06/23 18:4094.00.234mg/KgCadmium
09/06/23 18:4086.04.81mg/KgChromium
09/06/23 18:4083.03.74mg/KgLead
09/06/23 18:4094.02.27mg/KgSelenium
09/06/23 18:4097.00.235mg/KgSilver
Page 2 of 23* QC Fail Date:10/24/2023 02:11 PM
Page 57 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V37531QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V37406
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-V37406 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/06/23 14:350.03000.0120<0.0120mg/KgMercury (Total)
LCS-V37406Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1040.4330.417mg/KgMercury (Total)80-120
V 93785-MS-V37406 V 93785-MSD-V37406Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.435 1060.4450.4100.4100.0186mg/KgMercury (Total)109 80-120 2.2 20
V 93785-PDS-V37406Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/06/23 14:471120.215mg/KgMercury (Total)
Page 3 of 23Date:10/24/2023 02:11 PM
Page 58 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-V37418 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0200.002<0.002mg/KgAcetone
09/01/23 11:050.0200.001<0.001mg/KgAcrolein
09/01/23 11:050.0200.0008<0.0008mg/KgAcrylonitrile
09/01/23 11:050.0050.0006<0.0006mg/KgBenzene
09/01/23 11:050.0050.0005<0.0005mg/KgBromobenzene
09/01/23 11:050.0050.0008<0.0008mg/KgBromochloromethane
09/01/23 11:050.0050.001<0.001mg/KgBromodichloromethane
09/01/23 11:050.0050.001<0.001mg/KgBromoform
09/01/23 11:050.0100.001<0.001mg/KgBromomethane
09/01/23 11:050.0050.0005<0.0005mg/Kgn-Butylbenzene
09/01/23 11:050.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/01/23 11:050.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/01/23 11:050.0050.0006<0.0006mg/KgCarbon Disulfide
09/01/23 11:050.0050.001<0.001mg/KgCarbon Tetrachloride
09/01/23 11:050.0050.0007<0.0007mg/KgChlorobenzene
09/01/23 11:050.0050.0009<0.0009mg/KgChlorodibromomethane
09/01/23 11:050.0100.0009<0.0009mg/KgChloroethane
09/01/23 11:050.0050.001<0.001mg/KgChloroform
09/01/23 11:050.0100.0006<0.0006mg/KgChloromethane
09/01/23 11:050.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/01/23 11:050.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/01/23 11:050.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/01/23 11:050.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/01/23 11:050.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/01/23 11:050.0050.0006<0.0006mg/KgDibromomethane
09/01/23 11:050.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/01/23 11:050.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 23Date:10/24/2023 02:11 PM
Page 59 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-V37418 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/01/23 11:050.0100.001<0.001mg/KgDichlorodifluoromethane
09/01/23 11:050.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/01/23 11:050.0050.001<0.001mg/Kg1,2-Dichloroethane
09/01/23 11:050.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/01/23 11:050.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/01/23 11:050.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/01/23 11:050.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/01/23 11:050.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/01/23 11:050.0050.001<0.001mg/Kg2,2-Dichloropropane
09/01/23 11:050.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/01/23 11:050.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/01/23 11:050.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/01/23 11:050.2500.014<0.014mg/KgEthanol
09/01/23 11:050.0050.0006<0.0006mg/KgEthylbenzene
09/01/23 11:050.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/01/23 11:050.0100.0008<0.0008mg/KgHexachlorobutadiene
09/01/23 11:050.0100.0007<0.0007mg/Kgn-Hexane
09/01/23 11:050.0200.0006<0.0006mg/Kg2-Hexanone
09/01/23 11:050.0050.0005<0.0005mg/KgIsopropylbenzene
09/01/23 11:050.0050.001<0.001mg/Kg4-Isopropyl toluene
09/01/23 11:050.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/01/23 11:050.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/01/23 11:050.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/01/23 11:050.0100.001<0.001mg/KgMethylene Chloride
09/01/23 11:050.0100.0010<0.0010mg/KgNaphthalene
09/01/23 11:050.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 23Date:10/24/2023 02:11 PM
Page 60 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-V37418 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/01/23 11:050.0050.001<0.001mg/KgStyrene
09/01/23 11:050.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/01/23 11:050.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/01/23 11:050.0050.0009<0.0009mg/KgTetrachloroethene
09/01/23 11:050.0050.0007<0.0007mg/KgToluene
09/01/23 11:050.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/01/23 11:050.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/01/23 11:050.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/01/23 11:050.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/01/23 11:050.0050.0009<0.0009mg/KgTrichloroethene
09/01/23 11:050.0100.002<0.002mg/KgTrichlorofluoromethane
09/01/23 11:050.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/01/23 11:050.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/01/23 11:050.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/01/23 11:050.0100.0005<0.0005mg/KgVinyl Acetate
09/01/23 11:050.0100.0005<0.0005mg/KgVinyl Chloride
09/01/23 11:050.0050.0005<0.0005mg/Kgo-Xylene
09/01/23 11:050.0100.001<0.001mg/Kgm,p-Xylene
09/01/23 11:054-Bromofluorobenzene (S)103 70-130
09/01/23 11:05Dibromofluoromethane (S)105 84-123
09/01/23 11:05Toluene-d8 (S)99.2 76-129
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
96.50.0960.100mg/KgAcetone 29-198
1060.1060.100mg/KgAcrolein 70-130
Page 6 of 23Date:10/24/2023 02:11 PM
Page 61 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1120.1120.100mg/KgAcrylonitrile 65-134
96.40.0480.050mg/KgBenzene 74-127
99.00.0490.050mg/KgBromobenzene 73-125
1040.0510.050mg/KgBromochloromethane 72-134
98.20.0490.050mg/KgBromodichloromethane 75-122
1060.0520.050mg/KgBromoform 66-135
91.00.0450.050mg/KgBromomethane 20-180
1010.0500.050mg/Kgn-Butylbenzene 65-135
99.00.0490.050mg/Kgsec-Butyl benzene 66-131
99.60.0490.050mg/Kgtert-Butyl benzene 67-132
85.40.0420.050mg/KgCarbon Disulfide 61-129
96.00.0480.050mg/KgCarbon Tetrachloride 64-143
98.60.0490.050mg/KgChlorobenzene 74-118
1020.0500.050mg/KgChlorodibromomethane 73-122
95.60.0470.050mg/KgChloroethane 33-149
94.60.0470.050mg/KgChloroform 73-127
83.60.0410.050mg/KgChloromethane 45-143
98.80.0490.050mg/Kg2-Chlorotoluene 67-124
98.80.0490.050mg/Kg4-Chlorotoluene 71-126
92.20.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159
1160.0570.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157
1050.0520.050mg/Kg1,2-Dibromoethane 70-132
99.80.0490.050mg/KgDibromomethane 74-133
1060.0530.050mg/Kg1,2-Dichlorobenzene 72-123
1040.0520.050mg/Kg1,3-Dichlorobenzene 71-120
1000.0500.050mg/Kg1,4-Dichlorobenzene 71-123
1010.0500.050mg/KgDichlorodifluoromethane 26-146
Page 7 of 23Date:10/24/2023 02:11 PM
Page 62 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.00.0470.050mg/Kg1,1-Dichloroethane 74-127
93.00.0460.050mg/Kg1,2-Dichloroethane 68-128
88.00.0440.050mg/Kg1,1-Dichloroethene 67-149
96.60.0480.050mg/Kgcis-1,2-Dichloroethene 76-134
91.00.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132
96.80.0480.050mg/Kg1,2-Dichloropropane 73-130
1020.0500.050mg/Kg1,3-Dichloropropane 75-124
92.20.0460.050mg/Kg2,2-Dichloropropane 50-142
93.60.0460.050mg/Kg1,1-Dichloropropene 71-130
1030.0510.050mg/Kgcis-1,3-Dichloropropene 71-125
1060.0530.050mg/Kgtrans-1,3-Dichloropropene 68-123
84.81.061.25mg/KgEthanol 70-130
94.60.0470.050mg/KgEthylbenzene 74-128
96.60.0960.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130
1060.0520.050mg/KgHexachlorobutadiene 64-125
98.60.0490.050mg/Kgn-Hexane 70-130
93.40.0460.050mg/Kg2-Hexanone 61-157
98.80.0490.050mg/KgIsopropylbenzene 68-126
1010.0500.050mg/Kg4-Isopropyl toluene 68-129
80.40.0400.050mg/KgMethyl Ethyl Ketone (MEK)63-149
99.60.0490.050mg/KgMethyl tert-butyl ether (MTBE)70-130
1000.0500.050mg/Kg4-Methyl-2-Pentanone 57-162
86.00.0430.050mg/KgMethylene Chloride 74-129
1170.0580.050mg/KgNaphthalene 57-157
97.20.0480.050mg/Kgn-Propylbenzene 67-130
1030.0510.050mg/KgStyrene 77-121
1010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115
Page 8 of 23Date:10/24/2023 02:11 PM
Page 63 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
LCS-V37418Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1040.0520.050mg/Kg1,1,2,2-Tetrachloroethane 56-126
98.60.0490.050mg/KgTetrachloroethene 68-130
96.00.0480.050mg/KgToluene 71-129
1130.0560.050mg/Kg1,2,3-Trichlorobenzene 68-130
1120.0560.050mg/Kg1,2,4-Trichlorobenzene 66-125
91.60.0450.050mg/Kg1,1,1-Trichloroethane 67-131
1000.0500.050mg/Kg1,1,2-Trichloroethane 70-133
96.60.0480.050mg/KgTrichloroethene 75-133
81.20.0400.050mg/KgTrichlorofluoromethane 44-146
1100.0540.050mg/Kg1,2,3-Trichloropropane 60-137
1020.0510.050mg/Kg1,2,4-Trimethylbenzene 69-129
1000.0500.050mg/Kg1,3,5-Trimethylbenzene 69-128
1070.0530.050mg/KgVinyl Acetate 60-140
79.00.0390.050mg/KgVinyl Chloride 48-147
98.40.0490.050mg/Kgo-Xylene 74-126
96.70.0960.100mg/Kgm,p-Xylene 75-124
1034-Bromofluorobenzene (S)70-130
104Dibromofluoromethane (S)84-123
102Toluene-d8 (S)76-129
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.022 16.7*0.0260.1000.1000.005mg/KgAcetone 21.0*34-143 17.6 49
0.018 18.7*0.0360.1000.100<0.001mg/KgAcrolein 36.0*70-130 63.2*20
0.050 50.1*0.0600.1000.100<0.0008mg/KgAcrylonitrile 60.0*65-134 17.9 30
Page 9 of 23* QC Fail Date:10/24/2023 02:11 PM
Page 64 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.027 55.0*0.0240.0500.050<0.0006mg/KgBenzene 48.0*60-135 13.5 20
0.024 48.00.0230.0500.050<0.0005mg/KgBromobenzene 46.8 45-135 2.5 25
0.027 54.2*0.0270.0500.050<0.0008mg/KgBromochloromethane 55.2 55-136 1.8 18
0.025 51.6*0.0250.0500.050<0.001mg/KgBromodichloromethane 50.0*55-127 3.1 17
0.026 52.20.0280.0500.050<0.001mg/KgBromoform 56.6 40-136 8.0 35
0.029 58.00.0240.0500.050<0.001mg/KgBromomethane 49.6 30-137 15.6 30
0.023 46.60.0210.0500.050<0.0005mg/Kgn-Butylbenzene 42.8 23-148 8.5 39
0.025 50.80.0220.0500.050<0.0006mg/Kgsec-Butyl benzene 45.4 34-144 11.2 28
0.026 52.20.0230.0500.050<0.0005mg/Kgtert-Butyl benzene 47.2 36-150 10.0 29
0.026 52.40.0210.0500.050<0.0006mg/KgCarbon Disulfide 43.0*49-139 19.7 26
0.029 58.00.0240.0500.050<0.001mg/KgCarbon Tetrachloride 49.4 48-153 16.0 23
0.026 52.8*0.0240.0500.050<0.0007mg/KgChlorobenzene 48.8*57-125 7.8 14
0.025 51.40.0260.0500.050<0.0009mg/KgChlorodibromomethane 53.6 49-127 4.1 24
0.030 60.40.0240.0500.050<0.0009mg/KgChloroethane 49.4 16-177 20.0 47
0.027 54.6*0.0240.0500.050<0.001mg/KgChloroform 49.8*56-137 9.1 18
0.020 41.20.0170.0500.050<0.0006mg/KgChloromethane 34.6*40-145 17.4 26
0.024 49.20.0220.0500.050<0.0005mg/Kg2-Chlorotoluene 45.8*46-132 7.1 29
0.024 49.20.0220.0500.050<0.0004mg/Kg4-Chlorotoluene 45.6 44-135 7.5 23
0.023 46.4*0.0220.0500.050<0.0007mg/KgDi-Isopropyl Ether (DIPE)44.8*51-155 3.5 13
0.025 51.00.0300.0500.050<0.0004mg/Kg1,2-Dibromo-3-Chloropropane 60.6 27-132 17.2 25
0.026 53.40.0280.0500.050<0.0006mg/Kg1,2-Dibromoethane 57.0 49-132 6.5 15
0.025 51.4*0.0260.0500.050<0.0006mg/KgDibromomethane 53.6*59-133 4.1 15
0.024 48.80.0240.0500.050<0.0003mg/Kg1,2-Dichlorobenzene 48.6 42-130 0.4 21
0.023 47.00.0230.0500.050<0.0004mg/Kg1,3-Dichlorobenzene 46.2 41-129 1.7 24
0.022 45.60.0220.0500.050<0.0006mg/Kg1,4-Dichlorobenzene 45.8 44-134 0.4 21
0.016 33.00.0130.0500.050<0.001mg/KgDichlorodifluoromethane 26.4 25-151 22.2 37
Page 10 of 23* QC Fail Date:10/24/2023 02:11 PM
Page 65 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.026 53.6*0.0230.0500.050<0.0008mg/Kg1,1-Dichloroethane 47.2*59-137 12.6 21
0.024 48.6*0.0230.0500.050<0.001mg/Kg1,2-Dichloroethane 47.6*51-131 2.0 13
0.027 54.20.0230.0500.050<0.0007mg/Kg1,1-Dichloroethene 46.4*54-162 15.5 22
0.026 52.6*0.0230.0500.050<0.0008mg/Kgcis-1,2-Dichloroethene 47.2*58-140 10.8 28
0.027 54.6*0.0230.0500.050<0.001mg/Kgtrans-1,2-Dichloroethene 46.6*57-141 15.8 18
0.025 51.2*0.0240.0500.050<0.0004mg/Kg1,2-Dichloropropane 49.2*55-138 3.9 16
0.025 51.0*0.0260.0500.050<0.0006mg/Kg1,3-Dichloropropane 52.2*53-129 2.3 15
0.026 53.60.0220.0500.050<0.001mg/Kg2,2-Dichloropropane 44.8 30-147 17.8 20
0.028 56.40.0230.0500.050<0.0008mg/Kg1,1-Dichloropropene 47.8*55-137 16.5 19
0.025 51.40.0250.0500.050<0.0005mg/Kgcis-1,3-Dichloropropene 50.4 42-135 1.9 32
0.025 50.60.0260.0500.050<0.0008mg/Kgtrans-1,3-Dichloropropene 52.0 41-124 2.7 20
0.673 53.8*0.7391.251.25<0.014mg/KgEthanol 59.1*70-130 9.3 20
0.026 53.20.0230.0500.050<0.0006mg/KgEthylbenzene 46.6 44-144 13.2 19
0.048 48.7*0.0490.1000.100<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)49.4*70-130 1.4 20
0.021 43.60.0210.0500.050<0.0008mg/KgHexachlorobutadiene 43.4 30-126 0.4 26
0.028 56.0*0.0240.0500.050<0.0007mg/Kgn-Hexane 48.0*70-130 15.3 20
0.011 23.6*0.0170.0500.050<0.0006mg/Kg2-Hexanone 35.6 30-147 40.5 42
0.026 53.40.0230.0500.050<0.0005mg/KgIsopropylbenzene 47.0 41-140 12.7 27
0.024 49.80.0220.0500.050<0.001mg/Kg4-Isopropyl toluene 45.6 32-144 8.8 22
0.010 20.0*0.0120.0500.050<0.0007mg/KgMethyl Ethyl Ketone (MEK)25.8 24-160 25.3 42
0.025 50.20.0260.0500.050<0.0006mg/KgMethyl tert-butyl ether (MTBE)52.4 49-135 4.2 22
0.021 42.00.0280.0500.050<0.015mg/Kg4-Methyl-2-Pentanone 56.0 25-163 28.5 44
0.024 48.8*0.0220.0500.050<0.001mg/KgMethylene Chloride 45.8*53-144 6.3 14
0.026 52.60.0280.0500.050<0.0010mg/KgNaphthalene 56.6 32-127 7.3 44
0.025 50.60.0220.0500.050<0.0005mg/Kgn-Propylbenzene 44.6 35-144 12.6 27
0.026 53.20.0240.0500.050<0.001mg/KgStyrene 48.4 42-132 9.4 28
Page 11 of 23* QC Fail Date:10/24/2023 02:11 PM
Page 66 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37419QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37418
V 93785-MS-V37418 V 93785-MSD-V37418Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.026 53.4*0.0250.0500.050<0.001mg/Kg1,1,1,2-Tetrachloroethane 50.6*60-120 5.3 15
0.025 50.40.0270.0500.050<0.0003mg/Kg1,1,2,2-Tetrachloroethane 55.2 39-135 9.0 22
0.028 56.80.0240.0500.050<0.0009mg/KgTetrachloroethene 49.2 47-142 14.3 26
0.027 55.0*0.0240.0500.050<0.0007mg/KgToluene 48.6*57-135 12.3 22
0.021 42.20.0220.0500.050<0.0005mg/Kg1,2,3-Trichlorobenzene 45.8 34-120 8.1 41
0.020 41.40.0210.0500.050<0.0006mg/Kg1,2,4-Trichlorobenzene 43.0 35-116 3.7 62
0.028 56.40.0240.0500.050<0.001mg/Kg1,1,1-Trichloroethane 48.6*52-139 14.8 21
0.024 49.40.0260.0500.050<0.0005mg/Kg1,1,2-Trichloroethane 53.0 44-140 7.0 21
0.028 56.20.0240.0500.050<0.0009mg/KgTrichloroethene 48.4 38-164 14.9 18
0.026 52.20.0210.0500.050<0.002mg/KgTrichlorofluoromethane 42.8 30-157 19.7 27
0.025 51.60.0290.0500.050<0.0007mg/Kg1,2,3-Trichloropropane 59.4 45-139 14.0 25
0.025 50.60.0230.0500.050<0.0005mg/Kg1,2,4-Trimethylbenzene 46.2 38-142 9.0 24
0.025 51.00.0230.0500.050<0.0005mg/Kg1,3,5-Trimethylbenzene 46.2 44-140 9.8 29
<0.0005 0.0*0.0030.0500.050<0.0005mg/KgVinyl Acetate 6.6*61-154 151*35
0.023 47.40.0170.0500.050<0.0005mg/KgVinyl Chloride 35.4*40-156 28.9 35
0.026 52.80.0240.0500.050<0.0005mg/Kgo-Xylene 48.0 43-143 9.5 17
0.052 52.70.0460.1000.100<0.001mg/Kgm,p-Xylene 46.9 36-148 11.6 20
1024-Bromofluorobenzene (S)101 70-130
105Dibromofluoromethane (S)106 84-123
102Toluene-d8 (S)100 76-129
Page 12 of 23* QC Fail Date:10/24/2023 02:11 PM
Page 67 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-V37441 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 17:150.6600.116<0.116mg/KgAcenaphthene
09/06/23 17:150.6600.105<0.105mg/KgAcenaphthylene
09/06/23 17:150.6600.152<0.152mg/KgAniline
09/06/23 17:150.6600.143<0.143mg/KgAnthracene
09/06/23 17:150.6600.139<0.139mg/KgBenzo(a)anthracene
09/06/23 17:150.6600.147<0.147mg/KgBenzo(a)pyrene
09/06/23 17:150.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/06/23 17:150.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/06/23 17:150.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/06/23 17:152.000.580<0.580mg/KgBenzoic Acid
09/06/23 17:150.6600.105<0.105mg/KgBenzyl alcohol
09/06/23 17:150.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/06/23 17:150.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/06/23 17:150.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/06/23 17:150.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/06/23 17:150.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/06/23 17:150.3300.113<0.113mg/KgButyl benzyl phthalate
09/06/23 17:150.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/06/23 17:150.3300.112<0.112mg/Kg4-Chloroaniline
09/06/23 17:150.6600.116<0.116mg/Kg2-Chloronaphthalene
09/06/23 17:150.6600.098<0.098mg/Kg2-Chlorophenol
09/06/23 17:151.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/06/23 17:150.6600.142<0.142mg/KgChrysene
09/06/23 17:150.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/06/23 17:150.6600.119<0.119mg/KgDibenzofuran
09/06/23 17:150.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/06/23 17:150.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 13 of 23Date:10/24/2023 02:11 PM
Page 68 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-V37441 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 17:150.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/06/23 17:150.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/06/23 17:150.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/06/23 17:150.6600.180<0.180mg/KgDiethyl phthalate
09/06/23 17:150.6600.174<0.174mg/KgDimethyl phthalate
09/06/23 17:150.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/06/23 17:150.6600.107<0.107mg/KgDi-n-butyl phthalate
09/06/23 17:151.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/06/23 17:151.500.520<0.520mg/Kg2,4-Dinitrophenol
09/06/23 17:150.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/06/23 17:150.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/06/23 17:150.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/06/23 17:150.6600.123<0.123mg/KgFluoranthene
09/06/23 17:150.6600.128<0.128mg/KgFluorene
09/06/23 17:150.6600.106<0.106mg/KgHexachlorobenzene
09/06/23 17:150.6600.097<0.097mg/KgHexachlorobutadiene
09/06/23 17:150.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/06/23 17:150.6600.079<0.079mg/KgHexachloroethane
09/06/23 17:150.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/06/23 17:150.6600.191<0.191mg/KgIsophorone
09/06/23 17:150.6600.106<0.106mg/Kg1-Methylnaphthalene
09/06/23 17:150.6600.100<0.100mg/Kg2-Methylnaphthalene
09/06/23 17:150.6600.097<0.097mg/Kg2-Methylphenol
09/06/23 17:150.6600.084<0.084mg/Kg3&4 Methylphenol
09/06/23 17:150.6600.144<0.144mg/KgNaphthalene
09/06/23 17:150.6600.096<0.096mg/Kg2-Nitroaniline
09/06/23 17:150.6600.120<0.120mg/Kg3-Nitroaniline
Page 14 of 23Date:10/24/2023 02:11 PM
Page 69 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-V37441 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/06/23 17:150.3300.093<0.093mg/Kg4-Nitroaniline
09/06/23 17:150.3300.116<0.116mg/KgNitrobenzene
09/06/23 17:150.6600.088<0.088mg/Kg2-Nitrophenol
09/06/23 17:150.6600.117<0.117mg/Kg4-Nitrophenol
09/06/23 17:150.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/06/23 17:150.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/06/23 17:150.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/06/23 17:151.000.347<0.347mg/KgPentachlorophenol
09/06/23 17:150.6600.208<0.208mg/KgPhenanthrene
09/06/23 17:150.6600.112<0.112mg/KgPhenol
09/06/23 17:150.6600.134<0.134mg/KgPyrene
09/06/23 17:150.3300.079<0.079mg/KgPyridine
09/06/23 17:150.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/06/23 17:150.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/06/23 17:150.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/06/23 17:152-Fluorobiphenyl (S)77.8 44-115
09/06/23 17:152-Fluorophenol (S)65.7 35-115
09/06/23 17:15Nitrobenzene-d5 (S)74.8 37-122
09/06/23 17:154-Terphenyl-d14 (S)83.8 54-127
09/06/23 17:152,4,6-Tribromophenol (S)65.4 39-132
09/06/23 17:15Phenol-d5 (S)66.6 34-121
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
79.61.331.67mg/KgAcenaphthene 40-123
76.61.281.67mg/KgAcenaphthylene 32-132
Page 15 of 23Date:10/24/2023 02:11 PM
Page 70 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
210*3.501.67mg/KgAniline 12-197
86.21.441.67mg/KgAnthracene 47-123
84.41.411.67mg/KgBenzo(a)anthracene 49-126
94.61.581.67mg/KgBenzo(a)pyrene 45-129
89.81.501.67mg/KgBenzo(b)fluoranthene 45-132
82.01.371.67mg/KgBenzo(g,h,i)perylene 43-134
86.21.441.67mg/KgBenzo(k)fluoranthene 47-132
61.61.031.67mg/KgBenzoic Acid 10-83
83.81.401.67mg/KgBenzyl alcohol 29-122
74.21.241.67mg/KgBis(2-Chloroethoxy)methane 36-121
73.61.231.67mg/KgBis(2-Chloroethyl)ether 31-120
82.01.371.67mg/KgBis(2-Chloroisopropyl)ether 33-131
86.81.451.67mg/KgBis(2-ethylhexyl)phthalate 51-133
86.21.441.67mg/Kg4-Bromophenyl phenyl ether 46-124
91.61.531.67mg/KgButyl benzyl phthalate 48-132
77.81.301.67mg/Kg4-Chloro-3-methylphenol 45-122
93.41.561.67mg/Kg4-Chloroaniline 17-106
77.81.301.67mg/Kg2-Chloronaphthalene 41-114
79.61.331.67mg/Kg2-Chlorophenol 34-121
83.81.401.67mg/Kg4-Chlorophenyl phenyl ether 45-121
83.21.391.67mg/KgChrysene 50-124
66.41.111.67mg/KgDibenz(a,h)anthracene 45-134
78.41.311.67mg/KgDibenzofuran 44-120
73.61.231.67mg/Kg1,2-Dichlorobenzene 33-117
71.21.191.67mg/Kg1,3-Dichlorobenzene 30-115
70.61.181.67mg/Kg1,4-Dichlorobenzene 31-115
77.81.301.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 16 of 23* QC Fail Date:10/24/2023 02:11 PM
Page 71 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.81.301.67mg/Kg2,4-Dichlorophenol 40-122
86.21.441.67mg/KgDiethyl phthalate 50-124
83.21.391.67mg/KgDimethyl phthalate 48-124
91.61.531.67mg/Kg2,4-Dimethylphenol 30-127
94.01.571.67mg/KgDi-n-butyl phthalate 51-128
85.01.421.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
88.61.481.67mg/Kg2,4-Dinitrophenol 27-129
86.21.441.67mg/Kg2,4-Dinitrotoluene 48-126
85.01.421.67mg/Kg2,6-Dinitrotoluene 46-124
93.41.561.67mg/KgDi-n-Octyl Phthalate 45-140
79.01.321.67mg/KgFluoranthene 50-127
81.41.361.67mg/KgFluorene 43-125
85.01.421.67mg/KgHexachlorobenzene 45-122
69.41.161.67mg/KgHexachlorobutadiene 32-123
67.01.121.67mg/KgHexachlorocyclopentadiene 32-117
70.61.181.67mg/KgHexachloroethane 28-117
83.81.401.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
67.01.121.67mg/KgIsophorone 30-122
68.21.141.67mg/Kg1-Methylnaphthalene 40-119
68.21.141.67mg/Kg2-Methylnaphthalene 38-122
82.01.371.67mg/Kg2-Methylphenol 32-122
75.41.261.67mg/Kg3&4 Methylphenol 34-119
66.41.111.67mg/KgNaphthalene 35-123
87.41.461.67mg/Kg2-Nitroaniline 44-127
87.41.461.67mg/Kg3-Nitroaniline 33-119
88.01.471.67mg/Kg4-Nitroaniline 63-147
67.61.131.67mg/KgNitrobenzene 34-122
Page 17 of 23Date:10/24/2023 02:11 PM
Page 72 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
LCS-V37441Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
72.41.211.67mg/Kg2-Nitrophenol 36-123
91.01.521.67mg/Kg4-Nitrophenol 30-132
61.61.031.67mg/KgN-Nitrosodimethylamine 10-146
1031.721.67mg/KgN-Nitrosodiphenylamine 38-127
80.81.351.67mg/KgN-Nitroso-di-n-propylamine 36-120
99.41.661.67mg/KgPentachlorophenol 25-133
83.21.391.67mg/KgPhenanthrene 50-121
77.21.291.67mg/KgPhenol 34-121
83.81.401.67mg/KgPyrene 47-127
53.30.8911.67mg/KgPyridine 10-80
67.01.121.67mg/Kg1,2,4-Trichlorobenzene 34-118
79.01.321.67mg/Kg2,4,5-Trichlorophenol 41-124
79.01.321.67mg/Kg2,4,6-Trichlorophenol 39-126
77.22-Fluorobiphenyl (S)44-115
70.22-Fluorophenol (S)35-115
70.6Nitrobenzene-d5 (S)37-122
85.64-Terphenyl-d14 (S)54-127
72.02,4,6-Tribromophenol (S)39-132
69.9Phenol-d5 (S)34-121
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.18 70.61.211.661.67<0.116mg/KgAcenaphthene 72.8 40-123 2.5 20
1.16 69.41.191.661.67<0.105mg/KgAcenaphthylene 71.6 32-132 2.5 20
2.86 1712.861.661.67<0.152mg/KgAniline 172 12-197 0.0 20
Page 18 of 23Date:10/24/2023 02:11 PM
Page 73 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.30 77.81.291.661.67<0.143mg/KgAnthracene 77.7 47-123 0.7 20
1.25 74.81.251.661.67<0.139mg/KgBenzo(a)anthracene 75.3 49-126 0.0 20
1.43 85.61.401.661.67<0.147mg/KgBenzo(a)pyrene 84.3 45-129 2.1 20
1.30 77.81.281.661.67<0.146mg/KgBenzo(b)fluoranthene 77.1 45-132 1.5 20
1.26 75.41.241.661.67<0.136mg/KgBenzo(g,h,i)perylene 74.6 43-134 1.6 20
1.32 79.01.301.661.67<0.137mg/KgBenzo(k)fluoranthene 78.3 47-132 1.5 20
1.12 67.01.041.661.67<0.580mg/KgBenzoic Acid 62.6 10-83 7.4 20
1.23 73.61.191.661.67<0.105mg/KgBenzyl alcohol 71.6 29-122 3.3 20
1.10 65.81.101.661.67<0.118mg/KgBis(2-Chloroethoxy)methane 66.2 36-121 0.0 20
1.04 62.21.061.661.67<0.107mg/KgBis(2-Chloroethyl)ether 63.8 31-120 1.9 20
1.18 70.61.201.661.67<0.136mg/KgBis(2-Chloroisopropyl)ether 72.2 33-131 1.6 20
1.31 78.41.301.661.67<0.120mg/KgBis(2-ethylhexyl)phthalate 78.3 51-133 0.7 20
1.29 77.21.251.661.67<0.109mg/Kg4-Bromophenyl phenyl ether 75.3 46-124 3.1 20
1.39 83.21.371.661.67<0.113mg/KgButyl benzyl phthalate 82.5 48-132 1.4 20
1.16 69.41.161.661.67<0.092mg/Kg4-Chloro-3-methylphenol 69.8 45-122 0.0 20
1.32 79.01.331.661.67<0.112mg/Kg4-Chloroaniline 80.1 17-106 0.7 20
1.17 70.01.191.661.67<0.116mg/Kg2-Chloronaphthalene 71.6 41-114 1.6 20
1.16 69.41.171.661.67<0.098mg/Kg2-Chlorophenol 70.4 34-121 0.8 20
1.27 76.01.271.661.67<0.126mg/Kg4-Chlorophenyl phenyl ether 76.5 45-121 0.0 20
1.27 76.01.251.661.67<0.142mg/KgChrysene 75.3 50-124 1.5 20
1.02 61.01.011.661.67<0.230mg/KgDibenz(a,h)anthracene 60.8 45-134 0.9 20
1.19 71.21.201.661.67<0.119mg/KgDibenzofuran 72.2 44-120 0.8 20
1.07 64.01.051.661.67<0.094mg/Kg1,2-Dichlorobenzene 63.2 33-117 1.8 20
1.01 60.41.001.661.67<0.097mg/Kg1,3-Dichlorobenzene 60.2 30-115 0.9 20
0.998 59.71.001.661.67<0.097mg/Kg1,4-Dichlorobenzene 60.2 31-115 0.2 20
1.15 68.81.141.661.67<0.147mg/Kg3,3'-Dichlorobenzidine 68.6 22-121 0.8 20
Page 19 of 23Date:10/24/2023 02:11 PM
Page 74 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.12 67.01.161.661.67<0.095mg/Kg2,4-Dichlorophenol 69.8 40-122 3.5 20
1.29 77.21.261.661.67<0.180mg/KgDiethyl phthalate 75.9 50-124 2.3 20
1.25 74.81.261.661.67<0.174mg/KgDimethyl phthalate 75.9 48-124 0.7 30
1.49 89.21.481.661.67<0.108mg/Kg2,4-Dimethylphenol 89.1 30-127 0.6 20
1.42 85.01.381.661.67<0.107mg/KgDi-n-butyl phthalate 83.1 51-128 2.8 20
1.29 77.21.191.661.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 71.6 29-132 8.0 20
1.29 77.21.241.661.67<0.520mg/Kg2,4-Dinitrophenol 74.6 27-129 3.9 20
1.28 76.61.261.661.67<0.096mg/Kg2,4-Dinitrotoluene 75.9 48-126 1.5 20
1.26 75.41.261.661.67<0.108mg/Kg2,6-Dinitrotoluene 75.9 46-124 0.0 20
1.41 84.41.371.661.67<0.143mg/KgDi-n-Octyl Phthalate 82.5 45-140 2.8 20
1.21 72.41.171.661.67<0.123mg/KgFluoranthene 70.4 50-127 3.3 20
1.23 73.61.241.661.67<0.128mg/KgFluorene 74.6 43-125 0.8 20
1.24 74.21.231.661.67<0.106mg/KgHexachlorobenzene 74.0 45-122 0.8 20
1.00 59.81.041.661.67<0.097mg/KgHexachlorobutadiene 62.6 32-123 3.9 20
1.05 62.81.051.661.67<0.157mg/KgHexachlorocyclopentadiene 63.2 32-117 0.0 20
1.00 59.81.021.661.67<0.079mg/KgHexachloroethane 61.4 28-117 1.9 20
1.27 76.01.241.661.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 74.6 45-133 2.3 20
0.961 57.50.9761.661.67<0.191mg/KgIsophorone 58.7 30-122 1.5 20
1.04 62.21.061.661.67<0.106mg/Kg1-Methylnaphthalene 63.8 40-119 1.9 20
1.00 59.81.041.661.67<0.100mg/Kg2-Methylnaphthalene 62.6 38-122 3.9 20
1.16 69.41.201.661.67<0.097mg/Kg2-Methylphenol 72.2 32-122 3.3 20
1.06 63.41.081.661.67<0.084mg/Kg3&4 Methylphenol 65.0 34-119 1.8 20
0.974 58.30.9871.661.67<0.144mg/KgNaphthalene 59.4 35-123 1.3 20
1.33 79.61.311.661.67<0.096mg/Kg2-Nitroaniline 78.9 44-127 1.5 20
1.28 76.61.301.661.67<0.120mg/Kg3-Nitroaniline 78.3 33-119 1.5 20
1.29 77.21.311.661.67<0.093mg/Kg4-Nitroaniline 78.9 63-147 1.5 20
Page 20 of 23Date:10/24/2023 02:11 PM
Page 75 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37467QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37441
V 93785-MS-V37441 V 93785-MSD-V37441Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.983 58.80.9801.661.67<0.116mg/KgNitrobenzene 59.0 34-122 0.3 20
1.05 62.81.041.661.67<0.088mg/Kg2-Nitrophenol 62.6 32-123 0.9 20
1.39 83.21.351.661.67<0.117mg/Kg4-Nitrophenol 81.3 30-132 2.9 20
0.918 54.90.9111.661.67<0.263mg/KgN-Nitrosodimethylamine 54.8 10-146 0.7 30
1.53 91.61.511.661.67<0.181mg/KgN-Nitrosodiphenylamine 90.9 38-127 1.3 20
1.14 68.21.181.661.67<0.118mg/KgN-Nitroso-di-n-propylamine 71.0 36-120 3.4 20
1.60 95.81.571.661.67<0.347mg/KgPentachlorophenol 94.5 25-133 1.8 20
1.27 76.01.221.661.67<0.208mg/KgPhenanthrene 73.4 50-121 4.0 20
1.12 67.01.131.661.67<0.112mg/KgPhenol 68.0 34-121 0.8 20
1.30 77.81.301.661.67<0.134mg/KgPyrene 78.3 47-127 0.0 20
0.801 47.90.7941.661.67<0.079mg/KgPyridine 47.8 10-80 0.8 20
0.994 59.50.9911.661.67<0.107mg/Kg1,2,4-Trichlorobenzene 59.6 34-118 0.3 20
1.23 73.61.211.661.67<0.096mg/Kg2,4,5-Trichlorophenol 72.8 41-124 1.6 20
1.23 73.61.201.661.67<0.096mg/Kg2,4,6-Trichlorophenol 72.2 39-126 2.4 20
68.82-Fluorobiphenyl (S)68.0 44-115
61.52-Fluorophenol (S)60.9 35-115
59.8Nitrobenzene-d5 (S)57.2 37-122
77.24-Terphenyl-d14 (S)74.6 54-127
64.82,4,6-Tribromophenol (S)62.1 39-132
60.6Phenol-d5 (S)58.2 34-121
Page 21 of 23Date:10/24/2023 02:11 PM
Page 76 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L703608QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L703066
Associated Lab Samples: 93827, 93828, 93829, 93830, 93831, 93832
LRB-L703066 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/08/23 15:220.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L703066Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
84.73.394.00mg/KgChromium, Hexavalent 80-120
V 93827-DUP-L703066Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/08/23 15:5411.20.226< 0.204mg/KgChromium, Hexavalent
V 93827-MS-L703066Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
27.3 66.4*41.1< 1.45mg/KgChromium, Hexavalent 75-125
Page 22 of 23Date:10/24/2023 02:11 PM
Page 77 of 80
Quality Control Data
23-243-0019Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
TCR-001
Dry Weight Determination
SW-DRYWT
V37349QC Analytical Batch:
Analysis Method:
Analysis Description:
V 93785-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/01/23 09:161.029.529.8%Moisture
V 93829-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/01/23 09:165.922.421.1%Moisture
Page 23 of 23Date:10/24/2023 02:11 PM
Page 78 of 80
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-243-0019
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 1.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:08/31/2023 15:27:15
Special precautions or instructions included?
Comments:
Page 79 of 80
Page 80 of 80

Appendix C
DEQ Risk Calculators
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Final Grade Evaluation Area 1
North Carolina Department of Environmental Quality
Risk Calculator
Yandle-Witherspoon Supply Inc.
1001 N. Brevard Street
Brownfields Redevelopment Section
24010-20-060
July 2023
May 2023 EPA RSL Table
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 1
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 1
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 1
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration (mg/kg)Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration (Qualifier)
Maximum
Concentration (Qualifier)Units
Location of
Maximum Concentration
Detection Frequency Range of Detection Limits
Concentration
Used for Screening
Background Value
Screening
Toxicity Value (Screening
Level) (n/c)
Potential
ARAR/TBC Value
Potential
ARAR/TBC Source
COPC
Flag (Y/N)
Rationale for
Selection or Deletion
0.014 67-64-1 Acetone mg/kg
0.96 7440-38-2 Arsenic, Inorganic mg/kg
98.7 7440-39-3 Barium mg/kg0.0696 7440-43-9 Cadmium (Diet)mg/kg
41.1 16065-83-1 Chromium(III), Insoluble Salts mg/kg0.244 18540-29-9 Chromium(VI)mg/kg
20 7439-92-1 ~Lead and Compounds mg/kg0.089 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.207 56-55-3 ~Benz[a]anthracene mg/kg0.211 50-32-8 ~Benzo[a]pyrene mg/kg
0.284 205-99-2 ~Benzo[b]fluoranthene mg/kg0.21 218-01-9 ~Chrysene mg/kg
0.361 206-44-0 ~Fluoranthene mg/kg0.352 129-00-0 ~Pyrene mg/kg
0.682 7782-49-2 Selenium mg/kg0.0219 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 1
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 4.5E-06 6.3E-02 NO
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 1
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk*
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient*
Calculated Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.014 0.014 0.014 2.0E-07 2.0E-07
7440-38-2 Arsenic, Inorganic 0.96 0.96 0.96 1.2E-06 1.7E-07 2.5E-11 1.4E-06 2.5E-02 2.9E-03 1.0E-06 2.7E-027440-39-3 Barium 98.7 98.7 98.7 6.3E-03 3.2E-06 6.3E-037440-43-9 Cadmium (Diet)0.0696 0.0696 0.0696 7.5E-13 7.5E-13 8.9E-03 8.4E-04 1.1E-07 9.7E-0316065-83-1 Chromium(III), Insoluble Salts 41.1 41.1 41.1 3.5E-04 3.5E-0418540-29-9 Chromium(VI)0.244 0.244 0.244 8.0E-07 3.4E-10 8.0E-07 1.0E-03 3.9E-08 1.0E-03
132-64-9 ~Dibenzofuran110-54-3 Hexane, N-7439-92-1 ~Lead and Compounds 20 20 20 <SL**<SL**<SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.089 0.089 0.089 3.8E-03 4.8E-09 3.8E-0383-32-9 ~Acenaphthene
120-12-7 ~Anthracene56-55-3 ~Benz[a]anthracene 0.207 0.207 0.207 1.4E-07 4.5E-08 2.6E-09 1.8E-0750-32-8 ~Benzo[a]pyrene 0.211 0.211 0.211 1.4E-06 4.6E-07 2.1E-12 1.8E-06 9.0E-03 2.8E-03 1.7E-06 1.2E-02205-99-2 ~Benzo[b]fluoranthene 0.284 0.284 0.284 1.9E-07 6.2E-08 2.8E-13 2.5E-07207-08-9 ~Benzo[k]fluoranthene
218-01-9 ~Chrysene 0.21 0.21 0.21 1.4E-09 4.6E-10 2.1E-15 1.8E-09206-44-0 ~Fluoranthene 0.361 0.361 0.361 1.2E-04 3.6E-05 1.5E-0486-73-7 ~Fluorene193-39-5 ~Indeno[1,2,3-cd]pyrene91-20-3 ~Naphthalene
129-00-0 ~Pyrene 0.352 0.352 0.352 1.5E-04 4.6E-05 2.0E-047782-49-2 Selenium 0.682 0.682 0.682 1.7E-03 5.5E-10 1.7E-03
7440-22-4 Silver 0.0219 0.0219 0.0219 5.6E-05 5.6E-05
Cumulative:4.5E-06 6.3E-02
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
Final Grade Evaluation Area 2
North Carolina Department of Environmental Quality
Risk Calculator
Yandle-Witherspoon Supply Inc.
1001 N. Brevard Street
Brownfields Redevelopment Section
24010-20-060
July 2023
May 2023 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 2
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 2
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 2
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration (mg/kg)Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration (Qualifier)
Maximum
Concentration (Qualifier)Units
Location of
Maximum Concentration
Detection Frequency Range of Detection Limits
Concentration
Used for Screening
Background Value
Screening
Toxicity Value (Screening
Level) (n/c)
Potential
ARAR/TBC Value
Potential
ARAR/TBC Source
COPC
Flag (Y/N)
Rationale for
Selection or Deletion
0.009 67-64-1 Acetone mg/kg
1.36 7440-38-2 Arsenic, Inorganic mg/kg
86.1 7440-39-3 Barium mg/kg0.112 7440-43-9 Cadmium (Diet)mg/kg
28.4 16065-83-1 Chromium(III), Insoluble Salts mg/kg29.2 7439-92-1 ~Lead and Compounds mg/kg
0.0663 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg0.575 56-55-3 ~Benz[a]anthracene mg/kg
0.625 50-32-8 ~Benzo[a]pyrene mg/kg0.842 205-99-2 ~Benzo[b]fluoranthene mg/kg
0.285 207-08-9 ~Benzo[k]fluoranthene mg/kg0.611 218-01-9 ~Chrysene mg/kg
0.972 206-44-0 ~Fluoranthene mg/kg0.443 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg
1.1 129-00-0 ~Pyrene mg/kg0.652 7782-49-2 Selenium mg/kg
0.0317 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 2
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 9.1E-06 1.0E-01 NO
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 2
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk*
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient*
Calculated Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.009 0.009 0.009 1.3E-07 1.3E-07
7440-38-2 Arsenic, Inorganic 1.36 1.36 1.36 1.8E-06 2.5E-07 3.5E-11 2.0E-06 3.5E-02 4.1E-03 1.5E-06 3.9E-027440-39-3 Barium 86.1 86.1 86.1 5.5E-03 2.8E-06 5.5E-037440-43-9 Cadmium (Diet)0.112 0.112 0.112 1.2E-12 1.2E-12 1.4E-02 1.4E-03 1.8E-07 1.6E-0216065-83-1 Chromium(III), Insoluble Salts 28.4 28.4 28.4 2.4E-04 2.4E-0418540-29-9 Chromium(VI)
132-64-9 ~Dibenzofuran110-54-3 Hexane, N-7439-92-1 ~Lead and Compounds 29.2 29.2 29.2 <SL**<SL**<SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.0663 0.0663 0.0663 2.8E-03 3.6E-09 2.8E-0383-32-9 ~Acenaphthene
120-12-7 ~Anthracene56-55-3 ~Benz[a]anthracene 0.575 0.575 0.575 3.8E-07 1.3E-07 7.3E-09 5.1E-0750-32-8 ~Benzo[a]pyrene 0.625 0.625 0.625 4.1E-06 1.4E-06 6.2E-12 5.4E-06 2.7E-02 8.2E-03 5.1E-06 3.5E-02205-99-2 ~Benzo[b]fluoranthene 0.842 0.842 0.842 5.5E-07 1.8E-07 8.4E-13 7.3E-07207-08-9 ~Benzo[k]fluoranthene 0.285 0.285 0.285 1.9E-08 6.2E-09 2.8E-14 2.5E-08
218-01-9 ~Chrysene 0.611 0.611 0.611 4.0E-09 1.3E-09 6.1E-15 5.3E-09206-44-0 ~Fluoranthene 0.972 0.972 0.972 3.1E-04 9.6E-05 4.1E-0486-73-7 ~Fluorene193-39-5 ~Indeno[1,2,3-cd]pyrene 0.443 0.443 0.443 2.9E-07 9.7E-08 4.4E-13 3.9E-0791-20-3 ~Naphthalene
129-00-0 ~Pyrene 1.1 1.1 1.1 4.7E-04 1.4E-04 6.1E-047782-49-2 Selenium 0.652 0.652 0.652 1.7E-03 5.3E-10 1.7E-03
7440-22-4 Silver 0.0317 0.0317 0.0317 8.1E-05 8.1E-05
Cumulative:9.1E-06 1.0E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Final Grade Evaluation Area 3
North Carolina Department of Environmental Quality
Risk Calculator
Yandle-Witherspoon Supply Inc.
1001 N. Brevard Street
Brownfields Redevelopment Section
24010-20-060
July 2023
May 2023 EPA RSL Table
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 3
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 3
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 3
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration (mg/kg)Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration (Qualifier)
Maximum
Concentration (Qualifier)Units
Location of
Maximum Concentration
Detection Frequency Range of Detection Limits
Concentration
Used for Screening
Background Value
Screening
Toxicity Value (Screening
Level) (n/c)
Potential
ARAR/TBC Value
Potential
ARAR/TBC Source
COPC
Flag (Y/N)
Rationale for
Selection or Deletion
0.01 67-64-1 Acetone mg/kg
0.857 7440-38-2 Arsenic, Inorganic mg/kg
77.8 7440-39-3 Barium mg/kg0.116 7440-43-9 Cadmium (Diet)mg/kg
37.4 16065-83-1 Chromium(III), Insoluble Salts mg/kg38.9 7439-92-1 ~Lead and Compounds mg/kg
0.0741 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg0.446 56-55-3 ~Benz[a]anthracene mg/kg
0.519 50-32-8 ~Benzo[a]pyrene mg/kg0.64 205-99-2 ~Benzo[b]fluoranthene mg/kg
0.233 207-08-9 ~Benzo[k]fluoranthene mg/kg0.447 218-01-9 ~Chrysene mg/kg
0.609 206-44-0 ~Fluoranthene mg/kg0.366 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg
0.679 129-00-0 ~Pyrene mg/kg0.49 7782-49-2 Selenium mg/kg
0.0298 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 3
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 7.1E-06 8.0E-02 NO
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 3
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk*
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient*
Calculated Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.01 0.01 0.01 1.4E-07 1.4E-07
7440-38-2 Arsenic, Inorganic 0.857 0.857 0.857 1.1E-06 1.6E-07 2.2E-11 1.3E-06 2.2E-02 2.6E-03 9.2E-07 2.5E-027440-39-3 Barium 77.8 77.8 77.8 5.0E-03 2.5E-06 5.0E-037440-43-9 Cadmium (Diet)0.116 0.116 0.116 1.3E-12 1.3E-12 1.5E-02 1.4E-03 1.9E-07 1.6E-0216065-83-1 Chromium(III), Insoluble Salts 37.4 37.4 37.4 3.2E-04 3.2E-0418540-29-9 Chromium(VI)
132-64-9 ~Dibenzofuran110-54-3 Hexane, N-7439-92-1 ~Lead and Compounds 38.9 38.9 38.9 <SL**<SL**<SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.0741 0.0741 0.0741 3.2E-03 4.0E-09 3.2E-0383-32-9 ~Acenaphthene
120-12-7 ~Anthracene56-55-3 ~Benz[a]anthracene 0.446 0.446 0.446 2.9E-07 9.7E-08 5.6E-09 3.9E-0750-32-8 ~Benzo[a]pyrene 0.519 0.519 0.519 3.4E-06 1.1E-06 5.2E-12 4.5E-06 2.2E-02 6.8E-03 4.2E-06 2.9E-02205-99-2 ~Benzo[b]fluoranthene 0.64 0.64 0.64 4.2E-07 1.4E-07 6.4E-13 5.6E-07207-08-9 ~Benzo[k]fluoranthene 0.233 0.233 0.233 1.5E-08 5.1E-09 2.3E-14 2.0E-08
218-01-9 ~Chrysene 0.447 0.447 0.447 2.9E-09 9.7E-10 4.5E-15 3.9E-09206-44-0 ~Fluoranthene 0.609 0.609 0.609 1.9E-04 6.0E-05 2.5E-0486-73-7 ~Fluorene193-39-5 ~Indeno[1,2,3-cd]pyrene 0.366 0.366 0.366 2.4E-07 8.0E-08 3.7E-13 3.2E-0791-20-3 ~Naphthalene
129-00-0 ~Pyrene 0.679 0.679 0.679 2.9E-04 8.9E-05 3.8E-047782-49-2 Selenium 0.49 0.49 0.49 1.3E-03 4.0E-10 1.3E-03
7440-22-4 Silver 0.0298 0.0298 0.0298 7.6E-05 7.6E-05
Cumulative:7.1E-06 8.0E-02
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
Final Grade Evaluation Area 4
North Carolina Department of Environmental Quality
Risk Calculator
Yandle-Witherspoon Supply Inc.
1001 N. Brevard Street
Brownfields Redevelopment Section
24010-20-060
July 2023
May 2023 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 4
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 4
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 4
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration (mg/kg)Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration (Qualifier)
Maximum
Concentration (Qualifier)Units
Location of
Maximum Concentration
Detection Frequency Range of Detection Limits
Concentration
Used for Screening
Background Value
Screening
Toxicity Value (Screening
Level) (n/c)
Potential
ARAR/TBC Value
Potential
ARAR/TBC Source
COPC
Flag (Y/N)
Rationale for
Selection or Deletion
0.006 67-64-1 Acetone mg/kg
0.938 7440-38-2 Arsenic, Inorganic mg/kg
79.4 7440-39-3 Barium mg/kg0.143 7440-43-9 Cadmium (Diet)mg/kg
41 16065-83-1 Chromium(III), Insoluble Salts mg/kg1.06 132-64-9 ~Dibenzofuran mg/kg
36.8 7439-92-1 ~Lead and Compounds mg/kg0.0513 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
2.59 83-32-9 ~Acenaphthene mg/kg3.29 120-12-7 ~Anthracene mg/kg
6.76 56-55-3 ~Benz[a]anthracene mg/kg6.69 50-32-8 ~Benzo[a]pyrene mg/kg
7.49 205-99-2 ~Benzo[b]fluoranthene mg/kg2.87 207-08-9 ~Benzo[k]fluoranthene mg/kg
6.22 218-01-9 ~Chrysene mg/kg12.3 206-44-0 ~Fluoranthene mg/kg
1.68 86-73-7 ~Fluorene mg/kg3.88 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg
1.21 91-20-3 ~Naphthalene mg/kg11.1 129-00-0 ~Pyrene mg/kg
0.427 7782-49-2 Selenium mg/kg0.039 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 4
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 7.6E-05 4.6E-01 NO
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 4
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk*
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient*
Calculated Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.006 0.006 0.006 8.5E-08 8.5E-08
7440-38-2 Arsenic, Inorganic 0.938 0.938 0.938 1.2E-06 1.7E-07 2.4E-11 1.4E-06 2.4E-02 2.8E-03 1.0E-06 2.7E-027440-39-3 Barium 79.4 79.4 79.4 5.1E-03 2.6E-06 5.1E-037440-43-9 Cadmium (Diet)0.143 0.143 0.143 1.5E-12 1.5E-12 1.8E-02 1.7E-03 2.3E-07 2.0E-0216065-83-1 Chromium(III), Insoluble Salts 41 41 41 3.5E-04 3.5E-0418540-29-9 Chromium(VI)
132-64-9 ~Dibenzofuran 1.06 1.06 1.06 1.4E-02 1.4E-02110-54-3 Hexane, N-7439-92-1 ~Lead and Compounds 36.8 36.8 36.8 <SL**<SL**<SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.0513 0.0513 0.0513 2.2E-03 2.8E-09 2.2E-0383-32-9 ~Acenaphthene 2.59 2.59 2.59 5.5E-04 1.7E-04 7.2E-04
120-12-7 ~Anthracene 3.29 3.29 3.29 1.4E-04 4.3E-05 1.8E-0456-55-3 ~Benz[a]anthracene 6.76 6.76 6.76 4.4E-06 1.5E-06 8.5E-08 6.0E-0650-32-8 ~Benzo[a]pyrene 6.69 6.69 6.69 4.4E-05 1.5E-05 6.7E-11 5.8E-05 2.9E-01 8.8E-02 5.4E-05 3.7E-01205-99-2 ~Benzo[b]fluoranthene 7.49 7.49 7.49 4.9E-06 1.6E-06 7.5E-12 6.5E-06207-08-9 ~Benzo[k]fluoranthene 2.87 2.87 2.87 1.9E-07 6.3E-08 2.9E-13 2.5E-07
218-01-9 ~Chrysene 6.22 6.22 6.22 4.1E-08 1.4E-08 6.2E-14 5.4E-08206-44-0 ~Fluoranthene 12.3 12.3 12.3 3.9E-03 1.2E-03 5.1E-0386-73-7 ~Fluorene 1.68 1.68 1.68 5.4E-04 1.7E-04 7.0E-04193-39-5 ~Indeno[1,2,3-cd]pyrene 3.88 3.88 3.88 2.5E-06 8.5E-07 3.9E-12 3.4E-0691-20-3 ~Naphthalene 1.21 1.21 1.21 2.1E-07 7.6E-08 3.0E-07 5.8E-07 7.7E-04 2.4E-04 7.8E-03 8.9E-03
129-00-0 ~Pyrene 11.1 11.1 11.1 4.7E-03 1.5E-03 6.2E-037782-49-2 Selenium 0.427 0.427 0.427 1.1E-03 3.5E-10 1.1E-03
7440-22-4 Silver 0.039 0.039 0.039 1.0E-04 1.0E-04
Cumulative:7.6E-05 4.6E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Final Grade Evaluation Area 5
North Carolina Department of Environmental Quality
Risk Calculator
Yandle-Witherspoon Supply Inc.
1001 N. Brevard Street
Brownfields Redevelopment Section
24010-20-060
July 2023
May 2023 EPA RSL Table
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 5
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 5
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 5
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration (mg/kg)Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration (Qualifier)
Maximum
Concentration (Qualifier)Units
Location of
Maximum Concentration
Detection Frequency Range of Detection Limits
Concentration
Used for Screening
Background Value
Screening
Toxicity Value (Screening
Level) (n/c)
Potential
ARAR/TBC Value
Potential
ARAR/TBC Source
COPC
Flag (Y/N)
Rationale for
Selection or Deletion
0.007 67-64-1 Acetone mg/kg
0.507 7440-38-2 Arsenic, Inorganic mg/kg
94 7440-39-3 Barium mg/kg0.061 7440-43-9 Cadmium (Diet)mg/kg
19.8 16065-83-1 Chromium(III), Insoluble Salts mg/kg0.001 110-54-3 Hexane, N-mg/kg
12.3 7439-92-1 ~Lead and Compounds mg/kg0.1 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.495 7782-49-2 Selenium mg/kg0.0173 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 5
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 7.5E-07 3.5E-02 NO
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Final Grade Evaluation Area 5
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk*
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient*
Calculated Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.007 0.007 0.007 9.9E-08 9.9E-08
7440-38-2 Arsenic, Inorganic 0.507 0.507 0.507 6.6E-07 9.2E-08 1.3E-11 7.5E-07 1.3E-02 1.5E-03 5.5E-07 1.5E-027440-39-3 Barium 94 94 94 6.0E-03 3.0E-06 6.0E-037440-43-9 Cadmium (Diet)0.061 0.061 0.061 6.6E-13 6.6E-13 7.8E-03 7.4E-04 9.9E-08 8.5E-0316065-83-1 Chromium(III), Insoluble Salts 19.8 19.8 19.8 1.7E-04 1.7E-0418540-29-9 Chromium(VI)
132-64-9 ~Dibenzofuran110-54-3 Hexane, N-0.001 0.001 0.001 4.4E-07 4.4E-077439-92-1 ~Lead and Compounds 12.3 12.3 12.3 <SL**<SL**<SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.1 0.1 0.1 4.3E-03 5.4E-09 4.3E-0383-32-9 ~Acenaphthene
120-12-7 ~Anthracene56-55-3 ~Benz[a]anthracene50-32-8 ~Benzo[a]pyrene205-99-2 ~Benzo[b]fluoranthene207-08-9 ~Benzo[k]fluoranthene
218-01-9 ~Chrysene206-44-0 ~Fluoranthene86-73-7 ~Fluorene193-39-5 ~Indeno[1,2,3-cd]pyrene91-20-3 ~Naphthalene
129-00-0 ~Pyrene7782-49-2 Selenium 0.495 0.495 0.495 1.3E-03 4.0E-10 1.3E-03
7440-22-4 Silver 0.0173 0.0173 0.0173 4.4E-05 4.4E-05
Cumulative:7.5E-07 3.5E-02
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:Hart and Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
Hypothetical Worst Case Soil
North Carolina Department of Environmental Quality
Risk Calculator
Yandle-Witherspoon Supply Inc.
1001 N. Brevard Street
Brownfields Redevelopment Section
24010-20-060
July 2023
May 2023 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Hypothetical Worst Case Soil
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Hypothetical Worst Case Soil
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Hypothetical Worst Case Soil
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration (mg/kg)Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration (Qualifier)
Maximum
Concentration (Qualifier)Units
Location of
Maximum Concentration
Detection Frequency Range of Detection Limits
Concentration
Used for Screening
Background Value
Screening
Toxicity Value (Screening
Level) (n/c)
Potential
ARAR/TBC Value
Potential
ARAR/TBC Source
COPC
Flag (Y/N)
Rationale for
Selection or Deletion
0.014 FG-1 67-64-1 Acetone mg/kg1.36 FG-2 7440-38-2 Arsenic, Inorganic mg/kg
98.7 FG-1 7440-39-3 Barium mg/kg0.143 FG-4 7440-43-9 Cadmium (Diet)mg/kg
41.1 FG-1 16065-83-1 Chromium(III), Insoluble Salts mg/kg0.244 FG-1 18540-29-9 Chromium(VI)mg/kg
1.06 FG-4 132-64-9 ~Dibenzofuran mg/kg0.001 FG-5 110-54-3 Hexane, N-mg/kg
38.9 FG-3 7439-92-1 ~Lead and Compounds mg/kg0.1 FG-5 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
2.59 FG-4 83-32-9 ~Acenaphthene mg/kg3.29 FG-4 120-12-7 ~Anthracene mg/kg
6.76 FG-4 56-55-3 ~Benz[a]anthracene mg/kg6.69 FG-4 50-32-8 ~Benzo[a]pyrene mg/kg
7.49 FG-4 205-99-2 ~Benzo[b]fluoranthene mg/kg2.87 FG-4 207-08-9 ~Benzo[k]fluoranthene mg/kg
6.22 FG-4 218-01-9 ~Chrysene mg/kg12.3 FG-4 206-44-0 ~Fluoranthene mg/kg
1.68 FG-4 86-73-7 ~Fluorene mg/kg3.88 FG-4 193-39-5 ~Indeno[1,2,3-cd]pyrene mg/kg
1.21 FG-4 91-20-3 ~Naphthalene mg/kg11.1 FG-4 129-00-0 ~Pyrene mg/kg
0.682 FG-1 7782-49-2 Selenium mg/kg0.039 FG-4 7440-22-4 Silver mg/kg
Input Form 2A
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Hypothetical Worst Case Soil
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 7.8E-05 4.8E-01 NO
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: July 2023
Basis: May 2023 EPA RSL Table
Site ID: 24010-20-060
Exposure Unit ID: Hypothetical Worst Case Soil
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS #Chemical Name:Ingestion Concentration (mg/kg)
Dermal Concentration (mg/kg)
Inhalation Concentration (mg/kg)*
Ingestion Carcinogenic Risk
Dermal Carcinogenic Risk
Inhalation Carcinogenic Risk*
Calculated Carcinogenic Risk
Ingestion Hazard Quotient
Dermal Hazard Quotient
Inhalation Hazard Quotient*
Calculated Non-Carcinogenic Hazard Quotient67-64-1 Acetone 0.014 0.014 0.014 2.0E-07 2.0E-07
7440-38-2 Arsenic, Inorganic 1.36 1.36 1.36 1.8E-06 2.5E-07 3.5E-11 2.0E-06 3.5E-02 4.1E-03 1.5E-06 3.9E-027440-39-3 Barium 98.7 98.7 98.7 6.3E-03 3.2E-06 6.3E-037440-43-9 Cadmium (Diet)0.143 0.143 0.143 1.5E-12 1.5E-12 1.8E-02 1.7E-03 2.3E-07 2.0E-0216065-83-1 Chromium(III), Insoluble Salts 41.1 41.1 41.1 3.5E-04 3.5E-0418540-29-9 Chromium(VI)0.244 0.244 0.244 8.0E-07 3.4E-10 8.0E-07 1.0E-03 3.9E-08 1.0E-03
132-64-9 ~Dibenzofuran 1.06 1.06 1.06 1.4E-02 1.4E-02110-54-3 Hexane, N-0.001 0.001 0.001 4.4E-07 4.4E-077439-92-1 ~Lead and Compounds 38.9 38.9 38.9 <SL**<SL**<SL**7487-94-7 ~Mercuric Chloride (and other Mercury salts)0.1 0.1 0.1 4.3E-03 5.4E-09 4.3E-0383-32-9 ~Acenaphthene 2.59 2.59 2.59 5.5E-04 1.7E-04 7.2E-04
120-12-7 ~Anthracene 3.29 3.29 3.29 1.4E-04 4.3E-05 1.8E-0456-55-3 ~Benz[a]anthracene 6.76 6.76 6.76 4.4E-06 1.5E-06 8.5E-08 6.0E-0650-32-8 ~Benzo[a]pyrene 6.69 6.69 6.69 4.4E-05 1.5E-05 6.7E-11 5.8E-05 2.9E-01 8.8E-02 5.4E-05 3.7E-01205-99-2 ~Benzo[b]fluoranthene 7.49 7.49 7.49 4.9E-06 1.6E-06 7.5E-12 6.5E-06207-08-9 ~Benzo[k]fluoranthene 2.87 2.87 2.87 1.9E-07 6.3E-08 2.9E-13 2.5E-07
218-01-9 ~Chrysene 6.22 6.22 6.22 4.1E-08 1.4E-08 6.2E-14 5.4E-08206-44-0 ~Fluoranthene 12.3 12.3 12.3 3.9E-03 1.2E-03 5.1E-0386-73-7 ~Fluorene 1.68 1.68 1.68 5.4E-04 1.7E-04 7.0E-04193-39-5 ~Indeno[1,2,3-cd]pyrene 3.88 3.88 3.88 2.5E-06 8.5E-07 3.9E-12 3.4E-0691-20-3 ~Naphthalene 1.21 1.21 1.21 2.1E-07 7.6E-08 3.0E-07 5.8E-07 7.7E-04 2.4E-04 7.8E-03 8.9E-03
129-00-0 ~Pyrene 11.1 11.1 11.1 4.7E-03 1.5E-03 6.2E-037782-49-2 Selenium 0.682 0.682 0.682 1.7E-03 5.5E-10 1.7E-03
7440-22-4 Silver 0.039 0.039 0.039 1.0E-04 1.0E-04
Cumulative:7.8E-05 4.8E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator