25036_Clariant Corp_Report of Environmental Assessment_20210312

March 12, 2021
Mr. Jason Nail
Parkside Partners
1427 Mayson Street
Atlanta, Georgia 30324

Reference: Report of Environmental Assessment Services
Monroe Road Site
4000 Monroe Road Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:12929-A Dear Mr. Nail: ECS Southeast, LLP (ECS) is pleased to provide Parkside Partners with the results of our environmental assessment for the above-referenced site. ECS’s services were provided in accordance with ECS proposal No. 49:22329P authorized on February 9, 2021. ECS appreciates the opportunity to provide our services to you. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP Scott Young, P.G. Roger A. Smith, P.G.
Environmental Project Manager Principal Geologist
[e-mail] [e-mail]
704-525-5152 704-525-5152
Report of Environmental Assessment
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:12929-A
March 12, 2021

1
TABLE OF CONTENTS 1.0 PROJECT INFORMATION .................................................................................................................... 1
2.0 SCOPE OF SERVICES ............................................................................................................................ 2
2.1 Monitoring Well Permit ....................................................................................................................... 2
2.2 Utility Locate and GPR Survey ............................................................................................................. 2
2.3 Groundwater Sample Collection ......................................................................................................... 2
2.4 Sub-Slab Vapor Sampling..................................................................................................................... 3
3.0 RESULTS .............................................................................................................................................. 4
3.1 Groundwater Samples Analytical Results............................................................................................ 4
3.2 Sub-Slab Vapor Samples Analytical Results ......................................................................................... 4
4.0 CONCLUSIONS .................................................................................................................................... 5
5.0 RECOMMENDATIONS ......................................................................................................................... 5
6.0 QUALIFICATIONS OF REPORT ............................................................................................................. 5
FIGURES Figure 1 USGS Topographic Map Figure 2 Groundwater Sample Locations Map Figure 3 Sub-Slab Sample Locations Map TABLES Table 1 Summary of Groundwater Samples Analytical Results Table 2 Summary of Sub-Slab Soil Gas Samples Analytical Results APPENDICES Appendix A Site Photographs Appendix B NCDEQ Well Permit and Mecklenburg County SIP Information Appendix C Boring Logs and Well Construction/Abandonment Records Appendix D Laboratory Analytical Report and Chain of Custody Record Appendix E NCDEQ Risk Calculator Output Results
Report of Environmental Assessment
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:12929-A
March 12, 2021

1
1.0 PROJECT INFORMATION

The subject property is located at 4000 Monroe Road in Charlotte, Mecklenburg County, North Carolina
(Figure 1). Photographs of the site are included in Appendix A. The subject property is identified by the
Mecklenburg County Geographic Information System (GIS) as Parcel Identification Number (PIN)
15904612 and is owned by Clariant Corporation (Demerger)/Alisa Bradshaw. The approximately 9.799-
acre subject property is developed with Clariant Corporation, a specialty chemical company. The subject
property is developed with an approximate 92,780-square foot building that is subdivided into Buildings
1-4 that was reportedly constructed in 1956; an approximate 75,606-square foot building designated as
Building 5 that was reportedly constructed in 1956; an approximately 391-square foot building designated
as Building 6 that was reportedly constructed in 1994; and an approximate 100-aquare foot structure
designated as Building 7. ECS previously completed a Phase I Environmental Site Assessment (ESA) on the
property, as documented in the report dated January 15, 2021, ECS Project Number 49:12929. The ESA
identified the following recognized environmental conditions (RECs):
• Based on the length of industrial and fueling operations of this facility being around 65 years, the
use of chemicals, and the potential for an undocumented release that could impact the subject
property, ECS considers the historic and current use of the site to represent a REC.
• ECS considers the potential for a release from the wastewater treatment activities in Building 6
which was constructed in 1996 and associated piping to represent a REC.
• Based on the lack of closure documentation and the potential for an undocumented release at
the subject property to impact subsurface conditions, ECS considers four former 4,000-gallon
gasoline underground storage tanks (USTs) to represent a REC.
• ECS considers the potential for additional orphan USTs associated with the former gasoline station
on the northwestern portion of the property that operated from around 1962 to 1993 to
represent a REC.
• Based on distance, measured groundwater flow towards the subject property, and documented
impacts to groundwater above regulatory standards, ECS considers the incident associated with
the former gasoline station that operated on the northeast adjoining property from around 1983-
2005 to represent a REC.
• Based on measured groundwater flow towards the subject property and documented impacts to
groundwater in close proximity to the subject property, ECS considers the potential for
chlorinated solvents to have migrated from the east adjoining Takatori facility to represent a REC.
• ECS considers the documented tetrachloroethene (PCE) impacts in groundwater above regulatory
standards during a Phase II ESA at the north adjacent property in 2019 to represent a REC.
• Based on length of service from approximately 1969 to 1994 and the potential for an
undocumented release that could impact the subject property, ECS considers the former
operation of the north adjacent dry-cleaning facility to represent a REC.

In an effort to determine if the subject property has been adversely affected by the identified RECs, ECS
was requested to submit a proposal to conduct an Environmental Assessment at the site. ECS Project
information is based on information included in the ESA report.

Report of Environmental Assessment
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:12929-A
March 12, 2021

2
2.0 SCOPE OF SERVICES

The environmental assessment included the collection and laboratory analysis of groundwater, and sub-
slab soil gas samples and conducted a limited geophysical survey utilizing ground penetrating radar (GPR)
in an attempt to locate potential remaining underground storage (USTs) in the northwest corner of the
site. Drilling activities were conducted using a Geoprobe® Direct Push Technology (DPT) drill rig. The
drilling subcontractor used for this assessment was 3D Environmental Investigations, LLC. The GPR survey
subcontractor used for this assessment was KCI Technologies (KCI). The GPR survey was conducted on
February 24, 2021. The drilling and groundwater sampling activities were conducted on February 24 and
25, 2021. The sub-slab vapor sampling activities were conducted on March 2 through 4, 2021.

2.1 Monitoring Well Permit

Prior to conducting drilling activities, ECS obtained a monitoring well permit from the North Carolina
Department of Environmental Quality (NCDEQ). In addition, ECS obtained a Subsurface Investigation
Permit (SIP) from the Mecklenburg County Health Department. The NCDEQ well permit and Mecklenburg
County SIP information is included as Appendix B.

2.2 Utility Locate and GPR Survey

Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. Required separation distances between subsurface activities and marked utilities
(typically 30-inches) were maintained during the field activities. In addition, ECS contracted with KCI to
clear the boring areas of private utilities. KCI also conducted the GPR survey in an attempt to locate
previously unknown USTs. The results of the GPR survey did not identify remaining USTs.

2.3 Groundwater Sample Collection

Between February 24 and 25, 2021, 17 borings (GW-1 through GW-17) were advanced at the site at the
locations shown on Figure 2. The borings were advanced by hydraulically driving a five-foot long, 1.5-inch
diameter soil sampling probe into the soil to depths ranging from 12 feet below ground surface or ft-bgs
(GW-15) to 31 ft-bgs (GW-2). Soils were collected continuously from the ground surface to the
termination depth at each of the soil boring locations using a soil sampling probe advanced by the DPT
drill rig. The soil sampling probe was lined with a dedicated disposable clear liner for each sampling
interval. After the soil sampling probe was driven, the liner filled with soil was removed from the probe
and cut open to expose the soil. ECS visually classified the soil collected from each boring and screened
the soils for relative levels of volatile organic vapors using a photoionization detector (PID). Elevated PID
readings were not noted in any of the borings advanced as part of this investigation; therefore, soil
samples were not collected for laboratory analysis. Boring logs for each boring are included in Appendix
C.

Refusal was encountered in borings GW-11 (18 ft-bgs) and GW-15 (12 ft-bgs) prior to encountering
groundwater. Groundwater was encountered at the site at depths ranging from 5 ft-bgs at sample
location GW-10 to 25 ft-bgs at sample location GW-1. The groundwater samples were collected from the
Report of Environmental Assessment
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:12929-A
March 12, 2021

3
remaining borings using a groundwater sampling probe equipped with an exposable stainless-steel
screen, with the exception of sample points GW-10 and GW-12. Temporary monitoring wells were
constructed at sample points GW-10 and GW-12, consisting of one-inch PVC screen and casing due to the
low infiltration of groundwater. The samples were extracted from the subsurface using a peristaltic pump
and dedicated tubing. Sample point construction details are included on the boring logs included in
Appendix C. Well construction records are also included in Appendix C.

The groundwater sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into a cooler with ice to
maintain the samples at approximately four degrees Celsius. The samples were submitted to Pace
Analytical Services, LLC, (Pace), a North Carolina certified laboratory located in Huntersville, North
Carolina, for analysis for Volatile Organic Compounds (VOCs) by EPA Method 8260 and Semi-Volatile
Organic Compounds (SVOCs) by EPA Method 8270. ECS maintained chain-of-custody (COC) procedures
throughout the sample collection and transportation process. A copy of the COC is included in Appendix
D.

Following the completion of the groundwater sampling activities, the groundwater borings were
abandoned by the North Carolina certified driller. The sample point abandonment records are included
in Appendix C.

2.4 Sub-Slab Vapor Sampling

Between March 2 and 4, 2021, 12 sub-slab soil gas sample points (SG-1 and SG-12) were installed in the
interior of the structures on the subject site. The approximate locations of these soil gas samples are
shown on Figure 3.

Each interior sub-slab vapor sample point was collected by drilling a 1 1/2-inch diameter hole through the
floor slabs for the installation of the flush mount cover, then drilling a 5/8-inch diameter hole through,
and approximately 2 inches below, the concrete slab. After drilling, a stainless-steel Vapor Pin® equipped
with an outer air tight seal was installed in general accordance with the manufacturer’s guidelines. A
length of ¼-inch outside diameter (OD) polyethylene tubing was connected to the Vapor Pin®.

Prior to collecting the sub-slab vapor samples, laboratory grade helium gas was used as a quality assurance
control measure to confirm the integrity of the probe seal at each sample location. A plastic cylinder
(approximately 1.75 quarts) was placed and sealed over the sampling point and purged with laboratory
grade helium. The tubing from soil gas sample points and tracer gas tubing was routed through the
cylinder wall. The cylinder was placed over the Vapor Pin® and held securely to the slab with a heavy
weight. During the purging stage, the cylinder was flooded with laboratory grade helium via the hose
placed through the cylinder wall. The concentration of helium inside the cylinder was measured with a
Model MGD-2002 Multi-Gas Leak detector. Immediately after the concentration of helium inside the
cylinder was measured, the detector was connected to the soil gas sample point tubing and the gas stream
being purged was measured for helium. A helium concentration of less than ten percent of helium inside
the cylinder was considered acceptable. If concentrations greater than ten percent helium were
measured, the soil gas sample point seal was reseated, and the leak detection process was repeated.
Report of Environmental Assessment
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:12929-A
March 12, 2021

4
A one Liter, individually Summa canister was fitted with a flow regulator for each sample point. The flow
rate for both purging and sample collection was set at 0.2 liters per minute. The pressure in the canister
was recorded before and after sample collection. Sample collection stopped when the vacuum reached
approximately 10 inches of mercury (Hg). Prior to sample collection, a shut-in test was conducted to assess
for leaks in the fittings and regulator.

The Summa canisters were labeled with ECS project number, sample identification, sample date and time,
and requested laboratory analysis. The soil samples were submitted to Con-Test Analytical Laboratory,
located in East Longmeadow, Massachusetts, for analysis of VOCs including naphthalene using EPA
Method TO-15.

ECS maintained COC procedures throughout the sample collection and transportation process for the sub-
slab soil gas samples. A copy of the COC is included in Appendix D.

3.0 RESULTS

3.1 Groundwater Samples Analytical Results

Review of the laboratory analytical results for the groundwater samples collected indicated one or more
VOCs in the samples collected from borings GW-1, GW-2, GW-4 through GW-7, GW-12, GW-13, GW-16,
and GW-17 at concentrations greater than the laboratory method detection limits. Benzene in the sample
collected from GW-13, methyl tert-butyl ether in the samples collected from GW-12 and GW-13, and
tetrachloroethene (also known as perchloroethene or PCE) in the samples collected from GW-1, GW-2,
GW-5, GW-13, GW-16, and GW-17 were detected at concentrations greater than the North Carolina 2L
Groundwater Quality Standards (NC2LGWQS). In addition, the concentrations of benzene in the sample
collected from GW-13 and PCE in the samples collected from GW-2, GW-5, GW-13, and GW-17 were
detected greater than the NCDEQ Non-Residential Groundwater Vapor Intrusion Screening Level (VISL).
SVOCs were not detected in the samples collected as part of this investigation at concentrations greater
than the laboratory method reporting limits. In addition, VOCs were not detected at concentrations
greater than the laboratory method reporting limits in the samples collected from GW-3, GW-8, GW-9,
GW-10, and GW-14.

The laboratory analytical results are summarized on Table 1. A copy of the laboratory analytical report is
included in Appendix D.

3.2 Sub-Slab Vapor Samples Analytical Results

Review of the laboratory analytical results for the samples collected from the sub-slab sample points
indicated several VOCs at concentrations greater than the laboratory method detection limits in each of
the sub-slab samples collected as part of this investigation. The concentration of chloroform detected in
the SG-A sample was present greater than its NCDEQ Sub-Slab and Exterior Soil Gas VISL. As chloroform
was detected at a concentration greater than its VISL in the SG-A sample and more than five compounds
with non-cancer effects were detected at concentrations greater than the laboratory method reporting
limits in each of the sub-slab soil gas samples collected as part of this investigation, ECS input the
Report of Environmental Assessment
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:12929-A
March 12, 2021

5
laboratory analytical results of each sub-slab soil gas sample collected in to the NCDEQ Risk Calculator.
Based on the results of the NCDEQ Risk Calculator, the concentrations in the sub-slab soil gas samples did
not exceed the risk thresholds. Output from the results of the NCDEQ Risk Calculator are presented in
Appendix E. The laboratory analytical results are summarized on Table 2. A copy of the laboratory
analytical report is included in Appendix D.

4.0 CONCLUSIONS

Based on the results of the baseline assessment, ECS concludes the following:

• Concentrations of benzene in the groundwater sample collected from GW-13 and PCE in the
groundwater samples collected from GW-2, GW-5, GW-13, and GW-17 were detected at
concentrations that were greater than the NCDEQ Non-Residential Groundwater VISLs.
• Soil samples were not collected as part of this investigation, as elevated PID readings and evidence
of release were not noted in the borings advanced on February 24 and 25, 2021.
• Chloroform was detected in soil gas sample SG-A at a concentration greater than its Non-
Residential VISL.
• Based on the results of the NCDEQ Risk Calculator, a vapor risk is not present at the site.

5.0 RECOMMENDATIONS

Based on the results of the environmental assessment, ECS recommends the following:

• Based on the detection of constituents at concentrations greater than their regulatory guidance
levels in site groundwater, it is ECS’ understanding that a reporting obligation exists with the
North Carolina Department of Environmental Quality (NCDEQ). Therefore, ECS further
recommends that a copy of this report be provided to the current property owner and they
consult with an attorney concerning reporting obligations.
• Although groundwater impacts were identified on the site property, based on the locations and
concentration, it appears that at least some of them are due to migration from an offsite source.
• Since redevelopment of the site (excavation, grading, etc.) that would be likely to encounter the
groundwater impacts is not reportedly proposed; the site does not utilize groundwater for
potable and/or non-potable sources; and the results of the sub-slab soil gas sampling and risk
calculator indicates that a vapor intrusion risk does not exist, ECS does not recommend additional
assessment at the time. However, based on the groundwater exceedances, the site should be
eligible for a Brownfields Agreement.

6.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this environmental assessment are consistent with those
normally employed in environmental sub-slab vapor and groundwater assessment projects of this type.
Our evaluation of site conditions has been based on our understanding of the site project information
determined during previous environmental assessments and the data obtained during our field activities.
Report of Environmental Assessment
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:12929-A
March 12, 2021

6
This report was prepared for the express use of Parkside Partners. Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract.

FIGURES

FIGURE 1
USGS TOPOGRAPHIC MAP
MONROE ROAD SITE
4000 and 4010 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:12929-A
SOURCE:
USGS 7.5’ TOPOGRAPHIC MAP
CHARLOTTE WEST, NC
2019
SCALE:
AS SHOWN
SITE LOCATION
FIGURE 2
GROUNDWATER SAMPLE LOCATIONS MAP
MONROE ROAD SITE
4000 and 4010 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:12929-A
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS
WEBSITE ACCESSED JANUARY 19, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE SUB-SLAB VAPOR SAMPLE LOCATION
APPROXIMATE GROUNDWATER BORING LOCATION
Building 6
Former Gasoline
Station and Three 550-
gallon USTs removed
Approximate
location of two
10,000-gallon and
1,000-gallon former
USTs GW-1
GW-2
GW-3 GW-4 GW-5
GW-6
GW-16
GW-17
GW-8
GW-7
GW-9
GW-10
GW-11 GW-15
GW-14
GW-13
GW-12
FIGURE 3
SUB-SLAB SAMPLE LOCATIONS MAP
MONROE ROAD SITE
4000 and 4010 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:12929-A
SOURCE:
CHARLOTTE MECKLENBURG POLARIS GIS
WEBSITE ACCESSED JANUARY 19, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE SUB-SLAB VAPOR SAMPLE LOCATION
APPROXIMATE GROUNDWATER BORING LOCATION
Building 6
Former Gasoline
Station and Three 550-
gallon USTs removed
Approximate
location of two
10,000-gallon and
1,000-gallon former
USTs
SG-K
SG-J
SG-I
SG-G
SG-F
SG-E
SG-H
SG-D
SG-B
SG-C
SG-A

TABLES

Table 1
Summary of Groundwater Samples Analytical Results
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:12929-A
VOCs by EPA Method 8260 SVOCs by EPA
Method 8270
AcetoneBenzeneChloroformcis-1,2-DichloroetheneDiisopropyl etherEthylbenzeneMethyl tert-butyl etherNaphthaleneTetrachloroetheneTrichloroetheneTotal XylenesAll CompoundsNC2LGWQS 6,000 1 70 70 70 600 20 6 0.7 3.0 500 Various
Non-Residential Groundwater VISL 19,000,000 6.9 3.6 NE 5,900 15 2,000 20 48 4.4 320 Various
GW-1 02/24/21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 10.1 <1.0 <1.0 BDL
GW-2 02/24/21 <1.0 <1.0 <1.0 2.3 0.23 J <1.0 <1.0 <1.0 78.2 2.6 <1.0 BDL
GW-3 02/24/21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-4 02/24/21 48.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-5 02/24/21 15.6 J <1.0 5.0 1.7 <1.0 <1.0 <1.0 <1.0 69.0 1.6 <1.0 BDL
GW-6 02/24/21 18.2 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-7 02/24/21 19.2 J <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-8 02/24/21 <25.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-9 02/25/21 <25.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-10 02/25/21 <25.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-12 02/25/21 14.5 J <1.0 <1.0 <1.0 <1.0 <1.0 40.0 <1.0 10.9 <1.0 <1.0 BDL
GW-13 02/25/21 <250 55.9 <10 <10 3.1 J 4.3 J 1,540 4.8 J 198 <10 8.6 J BDL
GW-14 02/25/21 <25.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BDL
GW-16 02/25/21 11.6 J <1.0 12.5 <1.0 <1.0 <1.0 1.6 <1.0 8.6 <1.0 <1.0 BDL
GW-17 02/25/21 28.6 <1.0 3.4 J 0.57 J <1.0 <1.0 5.0 <1.0 75.0 0.50 J <1.0 BDL
Notes:
All results presented in micrograms per liter (mg/L)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
SVOCs = Semi-volatile Organic Compounds
NC2LGWQS = North Carolina 2L Groundwater Quality Standards
Non-Residential Groundwater VISL = NCDEQ Non-Residential Groundwater Vapor Instrusion Screening Level (Janaury 2021)
J = Estimated concentration detected between laboratory method reporting limit and detection limit
BDL = Below Detection Level
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the NC2LGWQS
VALUE = concentration greater than the Non-Residential Groundwater VISL
Sample DateSample ID
Table 2
Summary of Sub-Slab Soil Gas Samples Analytical Results
Monroe Road Site
4000 Monroe Road
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:12929-A
VOCs by EPA Method TO-15 Risk Exceeded?AcetoneBenzeneBromodichloromethane2-Butanone(Methyl ethyl ketone)Carbon TetrachlorideChloroformCyclohexaneDichlorodifluoromethane1,1-DichloroetheneEthanolEthyl acetateEthylbenzeneHeptane2-Hexanone(Methyl butyl ketone)IsopropanolMethylene ChlorideNaphthalenePropeneTetrachloroetheneToluene1,1,1-TrichloroethaneTrichloroetheneTrichlorofluoromethane1,3,5-TrimethylbenzeneTotal XylenesNon-Residential VISLs 2,700,000 160 33 440,000 61,000 53 530,000 NE 18,000 NE 6,100 490 35,000 2,600 18,000 NE 36 260,000 3,500 440,000 440,000 180 NE 5,300 88,000
SG-A 03/02/21 350 <0.64 16 82 2.5 2,000 <0.69 20 <0.79 210 <7.2 0.43 J <0.82 14 31 8.5 <1.0 <14 110 2.5 <1.1 <1.1 2.4 J <0.98 1.5 J NO NO
SG-B 03/02/21 540 <0.64 <1.3 110 <1.3 10 <0.69 <0.99 <0.79 90 41 0.59 J <0.82 23 <20 5.7 J <1.0 <14 6.2 6.8 <1.1 0.49 J 2.0 J <0.98 2.79 NO NO
SG-C 03/02/21 950 6.3 <1.3 180 <1.3 15 <0.69 16 <0.79 330 <7.2 12 3.6 45 50 15 3.2 <14 630 5.1 <1.1 <1.1 3.9 J <0.98 46.4 NO NO
SG-D 03/03/21 570 <0.64 <1.3 110 <1.3 44 <0.69 19 <0.79 110 49 0.52 J <0.82 <0.82 40 15 <1.0 <14 5.0 5.6 <1.1 <1.1 2.2 J <0.98 1.7 J NO NO
SG-E 03/03/21 550 <0.64 <1.3 130 <1.3 5.0 26 22 <0.79 120 <7.2 0.85 J <0.82 <0.82 33 8.0 <1.0 <14 21 7.1 <1.1 <1.1 2.2 J <0.98 5.2 NO NO
SG-F 03/03/21 660 0.68 <1.3 93 <1.3 7.4 <0.69 <0.99 <0.79 110 92 1.3 <0.82 <0.82 <20 <6.9 <1.0 <14 18 15 <1.1 <1.1 2.2 J <0.98 7.2 NO NO
SG-G 03/04/21 740 <0.64 <1.3 130 1.1 J <0.98 <0.69 27 <0.79 130 <7.2 1.3 3.8 <0.82 44 11 <1.0 <14 390 6.1 <1.1 <1.1 3.8 J <0.98 3.5 NO NO
SG-H 03/04/21 270 <0.64 <1.3 64 <1.3 <0.98 <0.69 <0.99 <0.79 100 160 2.0 3.6 <0.82 19 J 4.9 J <1.0 <14 130 47 1.9 <1.1 4.9 <0.98 11.1 NO NO
SG-I 03/04/21 1,300 1.2 <1.3 180 <1.3 <0.98 35 2,200 1.00 220 84 0.92 <0.82 <0.82 <20 25 <1.0 31 11 13 <1.1 <1.1 <4.5 <0.98 1.5 NO NO
SG-J 03/04/21 420 <0.64 <1.3 44 <1.3 <0.98 15 3,600 <0.79 94 31 1.5 <0.82 <0.82 18 J <6.9 <1.0 <14 29 10 <1.1 0.67 J 5.1 1.2 7.2 NO NO
SG-K 03/04/21 240 <0.64 <1.3 52 <1.3 <0.98 <0.69 <0.99 <0.79 100 36 <0.87 <0.82 <0.82 15 J 9.8 <1.0 <14 8.1 28 29 <1.1 1.9 J <0.98 <2.57 NO NO
Notes:
All results presented in micrograms per cubic meter (mg/m3)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
1 = Cumulative Carcenogenic Risk factor established as 1.0 x 10-4
2 = Cumulative Hazard Index factor established as 1
Non-Residential VISLs = NCDEQ Non-Residential Sub-Slab Vapor Instrusion Screening Levels (January 2021)
NE = Not established
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the Non-Residential VISLs
Sample ID Sample
Date
Hazard Index2Carcinogenic Risk1

APPENDIX A

Photo X –View of SG-C sub-slab sample point after installation on 3/2/21.
Photo X –View of SG-C sub-slab sample point during helium leak test; performed at each sample location prior
to sample collection.
PHOTO DOCUMENTATION
MONROE ROAD SITE
4000 and 4010 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:12929-A
Photo X –View of SG-C sub-slab sample point during sample collection.
Photo X –View of SG-C sub-slab sample point during helium leak test
PHOTO DOCUMENTATION
MONROE ROAD SITE
4000 and 4010 MONROE ROAD
CHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:12929-A

APPENDIX B

February 11, 2021 Mr. Jason Nail (via email)
Parkside Partners 1427 Mayson Street Atlanta, GA 30324
RE: Monitoring Well Construction Permit Permit # WM0301100 Monroe Road, Charlotte Mecklenburg
County Dear Mr. Nail,
In accordance with your completed application received on February 10, 2020, we are forwarding herewith Monitoring Well Construction Permit Numbered WM0301100 and issued for the
construction of seventeen monitoring wells located near the subject site in Charlotte, Mecklenburg County. This Permit will be effective for one year from the date of issuance and shall be subject to the conditions and limitations as specified therein. Should you have any questions, please contact Edward Watson at [phone], or by email at [e-mail].
Sincerely,
Andrew H. Pitner, P.G., Assistant Regional Supervisor Mooresville Regional Office Water Quality Regional Operations Section Division of Water Resources
CC: WQROS, Central Office (via Laserfiche) Scott Young, ECS Limited (via email) 3D Environmental Investigations, LLC (via email)

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL
In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws, Rules and Regulations. PERMISSION IS HEREBY GRANTED TO

Parkside Partners (ECS Limited as Agent)
FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of seventeen monitoring wells owned by Parkside Partners near Monroe Road, Charlotte, Mecklenburg County. This Permit is issued in accordance with the application received on October 26, 2020, in conformity with specifications and supporting data, all of which are filed with the Department of Environmental Quality and are considered integral parts of this Permit. This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction
Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well construction.
If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service
Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding. This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions, limitations, or exceptions as follows: 1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as part of an investigation for contamination from an underground storage tank or dry cleaner incident. 2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency. 3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application. 4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o). 5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources’ Information Processing Unit within 30 days of the well completion. 6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a well abandonment record (GW-30) shall be submitted to the Division of Water Resources’ Information Processing Unit within 30 days of the well abandonment. 7. If the well penetrates any water-bearing zone that contains contaminated waters, the upper three feet of the well shall be grouted within one day after the casing is set or the well abandoned. 8. Temporary wells must be permanently abandoned or converted to a permanent well within seven days (168 hours) of completion of drilling the borehole. 9. Adequate permits shall be obtained from Mecklenburg County Groundwater and Wastewater Services. Permit issued the 11th day of February, 2021 FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION
_______________________________________________ Andrew H. Pitner, P.G., Assistant Regional Supervisor Division of Water Resources By Authority of the Environmental Management Commission

Permit No. # WM0301100
SIP Form – revised 2/15/11
Mecklenburg County Health Department Groundwater & Wastewater Services 700 N. Tryon St., Suite 211 Charlotte, NC 28202
Phone: [phone] Fax: [phone] http://groundwater.charmeck.org
Permit Issuance Date: _______________
Permit Number: ____________________ 
SUBSURFACE INVESTIGATION PERMIT
I. Well Owner Information
Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
II. Agent Information (if applicable)

Name: ___________________________________
Attn: _____________________________________
Phone #: _____________________
Address 1: ________________________________
Address 2: ________________________________
City: __________________________ State: _______ Zip: _____________
III. Site Information

Site Name; ________________________________
Parcel ID Number: _____________________
Address: ________________________________
City: __________________________ State: _______ Zip: _____________

General Conditions of This Permit:
• This permit shall be VALID for a period not to exceed twelve (12) months from the date of issuance.
• This permit is VALID for the site specified aboveDQGmust be on-site during the course of the investigation
and made available to a Department representative upon request.
• A North Carolina Certified Well Contrator must perform any well contractor activities associated with this permit.
• All wells shall be constructed and abandoned to the standards of Chapter VI, Section V and Section VIof the Mecklenburg County Groundwater Well Regulations.
• All temporary wells, including those installed using Direct Push Technology, must be abandoned
to the standards of Chapter VI, Section VI of the Mecklenburg County Groundwater Well Regulations.
• Registration information for all wells must be submitted to the Department within thirty (30) days of well completion. If water samples are collected, it is recommended that the well NOT be registered until the
analytical results are received.

Owner
2/12/2021
70002835
Parkside Partners
Jason Nail
404-239-9828
1427 Mayson Street
Atlanta GA 30324
ECS Southeast, LLP
Scott Young
7045255152
1812 Center Park Drive
Suite D
Charlotte NC 28217
4000 Monroe Road
15904612
NC

APPENDIX C

Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.0
0.0
0.0
0.0
0.0 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
SM/MH
SM/MH
SC/CH
SC/CH
SW
DescripƟon
Reddish Brown Sandy SILT; slightly
moist
Reddish Tan and Brown Silty SAND;
slightly moist
Brown and Tannish Orange Silty
SAND; slightly moist
Tannish Brown and Grey Clayey SAND;
with some silt, slightly moist
Tannish Gray and Orange Clayey
SAND; moist
Tannish Gray SAND; saturated
Refusal encountered at 26.0 feet.END OF DRILLING AT 26.0 FT
WELL CONSTRUCTION
Steel Piping
SloƩed Steel Casing
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-1
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.1
0.1
0.2
0.2 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
SM
SC
CL-SC
DescripƟon
Reddish Brown Silty SAND; slightly
moist
Reddish Brown Clayey SAND; moist
Brown Sandy CLAY; moist
Refusal encountered at 24.0 feet.END OF DRILLING AT 24.0 FT
WELL CONSTRUCTION
Schedule 40 PVC
Casing
#2 Filter Sand
Schedule 40 PVC
0.010" SloƩed Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-10
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.1
0.8
0.8 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
SM
CL-SC
CL-SC
CL-SC
DescripƟon
Grayish Brown Silty SAND; slightly
moist
Grayish Tan and Brown Sandy CLAY;
moist
Brown and Tannish Gray Sandy CLAY;
moist
Brown and Tannish Gray Sandy CLAY;
very moist
Refusal encountered at 18.0 feet.END OF DRILLING AT 18.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-11
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.0
0.1
0.1
0.0
0.2 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
ML-CL
ML-CL
CL-SC
CL-SC
DescripƟon
Brownish Red Sandy SILT; slightly
moist
Reddish Brown Clayey SILT; with some
sand, slightly moist
Reddish Brown and Gray Clayey SILT;
with some sand, moist
Tan and Brown Sandy CLAY; slightly
moist
Tan and Brown Sandy CLAY; moist
Refusal encountered at 29.0 feet.END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Schedule 40 PVC
Casing
#2 Filter Sand
Schedule 40 PVC
0.010" SloƩed PVC
Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-12
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.4
0.9
0.6
0.7 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML-CL
MH-SM
MH-SM
DescripƟon
Red Clayey SILT; with some sand,
moist
Reddish Brown Sandy SILT; moist
Reddish Brown Sandy SILT; saturated
END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-13
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading1.1
0.8
0.9
0.9 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML-CL
ML-CL
CL-ML
CL-SC
CL-SC
DescripƟon
Red Clayey SILT; moist
Reddish Brown Clayey SILT; moist
Reddish Brown Silty CLAY; moist
Reddish Brown Sandy CLAY; moist
Reddish Brown Sandy CLAY; saturated
END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-14
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.5
0.1 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML-CL
ML-CL
ML-CL
ML-CL
DescripƟon
Reddish Brown Clayey SILT; with some
sandy; moist
Reddish Brown Clayey SILT; with some
sand, saturated
Reddish Brown Clayey SILT; moist
Reddish Brown Clayey SILT; saturated
Refusal encountered at 12.0 feet.END OF DRILLING AT 12.0 FT
WELL CONSTRUCTION
Schedule 40 PVC
Casing
#2 Filter Sand
Schedule 40 PVC
0.010" SloƩed Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-15
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.3
0.5
1.6
1.6
1.3 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
ML-CL
DescripƟon
Reddish Brown Sandy SILT; moist
Red and Brownish Orange Clayey SILT;
with some sand; moist
Refusal encountered at 28.0 feet.END OF DRILLING AT 28.0 FT
WELL CONSTRUCTION
Steel Screen
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-16
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.4
0.7
1.1
1.1
0.8 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
MH-SM
MH-SM
DescripƟon
Reddish Brown Sandy SILT; moist
Brownish Orange Sandy SILT; slightly
moist
Brownish Orange; moist
END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-17
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.1
0.1
0.0
0.0
0.0 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
MH-SM
CH-SC
CL
DescripƟon
Red Sandy SILT; moist
Reddish Brown Sandy SILT; moist
Reddish Brown Sandy CLAY; moist
Red and Brownish Gray CLAY; moist
CONTINUED ON NEXT PAGE
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 2 Boring No:GW-2
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
35
40
45
50
55
60
ElevaƟon
-35
-40
-45
-50
-55 PID ReadingSample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
Refusal encountered at 31.0 feet.END OF DRILLING AT 31.0 FT
WELL CONSTRUCTION
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:2 of 2 Boring No:GW-2
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.2
0.0
0.1
0.2
0.0 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
SM/MH
SC
CL/SC
DescripƟon
Red Sandy SILT; slightly moist
Brownish Tan Silty SAND; slightly
moist
Tan and Brownish Red Clayey SAND;
slightly moist
Tan and Brownish Orange Sandy CLAY;
moist
END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-3
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.1
0.1
0.4
0.7 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
SM
MH-SM
ML/CL
DescripƟon
Red Sandy SILT; slightly moist
Red and Orangish Brown Silty SAND;
slightly moist
Reddish Brown Sandy SILT; slightly
moist
Reddish Brown Clayey SILT; saturated
END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-4
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.3
0.2
0.1
0.7 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
MH-SM
SM
SC
DescripƟon
Red and Brownish Orange Sandy SILT;
slightly moist
Reddish Brown Sandy SILT; slightly
moist
Tan and Brown Silty SAND; moist
Reddish Brown and Tan Clayey SAND;
saturated
END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-5
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.0
0.0
0.4
0.5 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
SM-MH
SC
SC
DescripƟon
Reddish Brown Sandy SILT; slightly
moist
Reddish Brown and Tan Silty SAND;
slightly moist
Brownish Gray and Tan Clayey SAND;
moist
Brownish Gray Clayey SAND;
saturated
END OF DRILLING AT 29.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-6
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.0
0.2
0.2 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
MH-SM
MH-SM
DescripƟon
Reddish Brown Sandy SILT; slightly
moist
Reddish Brown and Orange Sandy
SILT; moist
Reddish Brown Sandy SILT; saturated
END OF DRILLING AT 24.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-7
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.1
0.0
0.1 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
MH-SM
SM
SM
DescripƟon
Red Sandy SILT; moist
Reddish Brown Sandy SILT; slightly
moist
Brown and Tannish Orange Silty
SAND; moist
Brown and Tannish Orange Silty
SAND; saturated
END OF DRILLING AT 24.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-8
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 24 2021
WL (CompleƟon)Boring Completed:Feb 24 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading0.0
0.0
0.0 Sample NumberSample Recovery (in)Graphic LogSoil ClassiĮcaƟon
MH-SM
CL-SC
CL/ML
CL/ML
DescripƟon
Reddish Brown Sandy SILT; moist
Reddish Brown Sandy CLAY; moist
Brown Silty CLAY; with some sandy,
moist
Brown Silty CLAY; with some sand,
saturated
END OF DRILLING AT 24.0 FT
WELL CONSTRUCTION
Steel Casing
SloƩed Steel Screen
Project Name:Monroe Road Site -Environmental Services
Client:Parkside Partners, LLC
Site LocaƟon:4000 and 4010 Monroe Road, CharloƩe,
North Carolina 28205
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:GW-9
Project No.:49:12929-A
Driller:3D Enviro.Drill Rig:GeoProbe
ElevaƟon:
WL (First Encountered)Boring Started:Feb 25 2021
WL (CompleƟon)Boring Completed:Feb 25 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Mackie H. McMahan
Roger Smith

APPENDIX D

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 11, 2021
Scott Young
ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project Location: Charlotte, NC
Client Job Number:
Project Number: 12929-A
Laboratory Work Order Number: 21C0286
Enclosed are results of analyses for samples received by the laboratory on March 4, 2021. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/11/2021ECS Southeast - Charlotte, NC
1812 Center Park Drive, Suite D
Charlotte, NC 28217
ATTN: Scott Young
12929-A
21C0286
The results of analyses performed on the following samples submitted to Con-Test, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
SG-C 21C0286-01 Soil Gas EPA TO-15
SG-B 21C0286-02 Soil Gas EPA TO-15
SG-A 21C0286-03 Soil Gas EPA TO-15
SG-D 21C0286-04 Soil Gas EPA TO-15
SG-E 21C0286-05 Soil Gas EPA TO-15
SG-G 21C0286-06 Soil Gas EPA TO-15
SG-F 21C0286-07 Soil Gas EPA TO-15
SG-H 21C0286-08 Soil Gas EPA TO-15
SG-I 21C0286-09 Soil Gas EPA TO-15
SG-J 21C0286-10 Soil Gas EPA TO-15
SG-K 21C0286-11 Soil Gas EPA TO-15
Page 2 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
Page 3 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EPA TO-15
Qualifications:
Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not
detected" for all samples in this batch for this compound and bias is on the high side.
Analyte & Samples(s) Qualified:
Hexachlorobutadiene
B277883-BS1
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the low side.
Analyte & Samples(s) Qualified:
1,4-Dioxane
21C0286-01[SG-C], 21C0286-02[SG-B], 21C0286-03[SG-A], 21C0286-04[SG-D], 21C0286-05[SG-E], 21C0286-06[SG-G], 21C0286-07[SG-F], 21C0286-08[SG-H],
21C0286-09[SG-I], 21C0286-10[SG-J], 21C0286-11[SG-K], B277883-BLK1, B277883-BS1
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be
biased on the high side.
Analyte & Samples(s) Qualified:
Acetone, Trichlorofluoromethane (Freon 11)
21C0286-10[SG-J], B277883-BS1, 21C0286-01[SG-C], 21C0286-02[SG-B], 21C0286-03[SG-A], 21C0286-04[SG-D], 21C0286-05[SG-E], 21C0286-06[SG-G],
21C0286-07[SG-F], 21C0286-08[SG-H], 21C0286-11[SG-K]
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
1,4-Dioxane, Naphthalene
21C0286-01[SG-C], 21C0286-02[SG-B], 21C0286-03[SG-A], 21C0286-04[SG-D], 21C0286-05[SG-E], 21C0286-06[SG-G], 21C0286-07[SG-F], 21C0286-08[SG-H],
21C0286-09[SG-I], 21C0286-10[SG-J], 21C0286-11[SG-K], B277883-BLK1, B277883-BS1, S057690-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
Acetone
21C0286-10[SG-J], B277883-BS1, S057690-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
Bromoform
B277883-BS1, S057690-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
Ethanol
21C0286-01[SG-C], 21C0286-02[SG-B], 21C0286-03[SG-A], 21C0286-04[SG-D], 21C0286-05[SG-E], 21C0286-06[SG-G], 21C0286-07[SG-F], 21C0286-08[SG-H],
21C0286-09[SG-I], 21C0286-10[SG-J], 21C0286-11[SG-K], B277883-BLK1, B277883-BS1, S057690-CCV1
Calibrations RSD for this compound is >30% but <40%.
Analyte & Samples(s) Qualified:
Naphthalene
21C0286-01[SG-C], 21C0286-02[SG-B], 21C0286-03[SG-A], 21C0286-04[SG-D], 21C0286-05[SG-E], 21C0286-06[SG-G], 21C0286-07[SG-F], 21C0286-08[SG-H],
21C0286-09[SG-I], 21C0286-10[SG-J], 21C0286-11[SG-K], B277883-BLK1, B277883-BS1, S057690-CCV1
Page 4 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 5 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-C
Sample ID: 21C0286-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -8.7
Sampled: 3/2/2021 15:44
Canister ID: 2125
Flow Controller ID: 4120
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 400 60 3/11/21 6:50 BRF950 301403686
Benzene 2.0 0.20 3/11/21 0:44 BRF6.3 40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 0:44 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 0:44 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 0:44 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 0:44 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 0:44 BRFND40.440.15 0.32
2-Butanone (MEK)61 8.0 3/11/21 0:44 BRF180 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 0:44 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 0:44 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 0:44 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 0:44 BRFND40.530.20 0.52
Chloroform 3.1 0.20 3/11/21 0:44 BRF15 40.980.048 0.24
Chloromethane ND 0.40 3/11/21 0:44 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 0:44 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 0:44 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 0:44 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 0:44 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 0:44 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 0:44 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)3.2 0.20 3/11/21 0:44 BRF16 40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 0:44 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 0:44 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 0:44 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 0:44 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 0:44 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 0:44 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 0:44 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 0:44 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 0:44 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 0:44 BRFV-05, L-03 ND 47.20.56 2.0
Ethanol 180 8.0 3/11/21 0:44 BRFV-34 330 4152.4 4.6
Ethyl Acetate ND 2.0 3/11/21 0:44 BRFND47.21.2 4.3
Ethylbenzene 2.8 0.20 3/11/21 0:44 BRF12 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 0:44 BRFND40.980.062 0.30
Heptane 0.87 0.20 3/11/21 0:44 BRF3.6 40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 0:44 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 0:44 BRFND4280.36 1.3
2-Hexanone (MBK)11 0.20 3/11/21 0:44 BRF45 40.820.11 0.46
Isopropanol 20 8.0 3/11/21 0:44 BRF50 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 0:44 BRFND40.720.080 0.29
Methylene Chloride 4.4 2.0 3/11/21 0:44 BRF15 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 0:44 BRFND40.820.10 0.43
Naphthalene 0.62 0.20 3/11/21 0:44 BRFV-05, Z-01 3.2 41.00.11 0.59
Propene ND 8.0 3/11/21 0:44 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 0:44 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 0:44 BRFND41.40.053 0.37
Page 6 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-C
Sample ID: 21C0286-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -8.7
Sampled: 3/2/2021 15:44
Canister ID: 2125
Flow Controller ID: 4120
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 93 0.20 3/11/21 0:44 BRF630 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 0:44 BRFND45.90.49 1.5
Toluene 1.4 0.20 3/11/21 0:44 BRF5.1 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 0:44 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 0:44 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 0:44 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 0:44 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.70 0.80 3/11/21 0:44 BRFL-05, J 3.9 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 0:44 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 0:44 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 0:44 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 0:44 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 0:44 BRFND40.510.11 0.29
m&p-Xylene 8.6 0.40 3/11/21 0:44 BRF37 41.70.070 0.30
o-Xylene 2.2 0.20 3/11/21 0:44 BRF9.4 40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)99.1 3/11/21 6:5070-130
4-Bromofluorobenzene (1)113 3/11/21 0:4470-130
Page 7 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-B
Sample ID: 21C0286-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.3
Sampled: 3/2/2021 16:13
Canister ID: 2119
Flow Controller ID: 432
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 230 40 3/11/21 7:16 BRF540 20952457
Benzene ND 0.20 3/11/21 2:04 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 2:04 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 2:04 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 2:04 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 2:04 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 2:04 BRFND40.440.15 0.32
2-Butanone (MEK)39 8.0 3/11/21 2:04 BRF110 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 2:04 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 2:04 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 2:04 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 2:04 BRFND40.530.20 0.52
Chloroform 2.1 0.20 3/11/21 2:04 BRF10 40.980.048 0.24
Chloromethane ND 0.40 3/11/21 2:04 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 2:04 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 2:04 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 2:04 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 2:04 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 2:04 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 2:04 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)ND 0.20 3/11/21 2:04 BRFND40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 2:04 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 2:04 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 2:04 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 2:04 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 2:04 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 2:04 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 2:04 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 2:04 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 2:04 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 2:04 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 48 8.0 3/11/21 2:04 BRFV-34 90 4152.4 4.6
Ethyl Acetate 11 2.0 3/11/21 2:04 BRF41 47.21.2 4.3
Ethylbenzene 0.14 0.20 3/11/21 2:04 BRFJ0.59 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 2:04 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 2:04 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 2:04 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 2:04 BRFND4280.36 1.3
2-Hexanone (MBK)5.7 0.20 3/11/21 2:04 BRF23 40.820.11 0.46
Isopropanol ND 8.0 3/11/21 2:04 BRFND4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 2:04 BRFND40.720.080 0.29
Methylene Chloride 1.6 2.0 3/11/21 2:04 BRFJ5.7 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 2:04 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 2:04 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 2:04 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 2:04 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 2:04 BRFND41.40.053 0.37
Page 8 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-B
Sample ID: 21C0286-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.3
Sampled: 3/2/2021 16:13
Canister ID: 2119
Flow Controller ID: 432
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.91 0.20 3/11/21 2:04 BRF6.2 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 2:04 BRFND45.90.49 1.5
Toluene 1.8 0.20 3/11/21 2:04 BRF6.8 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 2:04 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 2:04 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 2:04 BRFND41.10.073 0.40
Trichloroethylene 0.092 0.20 3/11/21 2:04 BRFJ0.49 41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.36 0.80 3/11/21 2:04 BRFL-05, J 2.0 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 2:04 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 2:04 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 2:04 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 2:04 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 2:04 BRFND40.510.11 0.29
m&p-Xylene 0.44 0.40 3/11/21 2:04 BRF1.9 41.70.070 0.30
o-Xylene 0.20 0.20 3/11/21 2:04 BRF0.89 40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)99.6 3/11/21 7:1670-130
4-Bromofluorobenzene (1)119 3/11/21 2:0470-130
Page 9 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-A
Sample ID: 21C0286-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -25
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.6
Sampled: 3/2/2021 16:35
Canister ID: 2124
Flow Controller ID: 4141
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 150 40 3/11/21 7:42 BRF350 20952457
Benzene ND 0.20 3/11/21 2:45 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 2:45 BRFND41.00.090 0.47
Bromodichloromethane 2.3 0.20 3/11/21 2:45 BRF16 41.30.056 0.37
Bromoform ND 0.20 3/11/21 2:45 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 2:45 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 2:45 BRFND40.440.15 0.32
2-Butanone (MEK)28 8.0 3/11/21 2:45 BRF82 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 2:45 BRFND46.20.51 1.6
Carbon Tetrachloride 0.40 0.20 3/11/21 2:45 BRF2.5 41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 2:45 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 2:45 BRFND40.530.20 0.52
Chloroform 420 1.0 3/11/21 7:42 BRF2000 204.90.24 1.2
Chloromethane ND 0.40 3/11/21 2:45 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 2:45 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 2:45 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 2:45 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 2:45 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 2:45 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 2:45 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)4.0 0.20 3/11/21 2:45 BRF20 40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 2:45 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 2:45 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 2:45 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 2:45 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 2:45 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 2:45 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 2:45 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 2:45 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 2:45 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 2:45 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 110 8.0 3/11/21 2:45 BRFV-34 210 4152.4 4.6
Ethyl Acetate ND 2.0 3/11/21 2:45 BRFND47.21.2 4.3
Ethylbenzene 0.10 0.20 3/11/21 2:45 BRFJ0.43 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 2:45 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 2:45 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 2:45 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 2:45 BRFND4280.36 1.3
2-Hexanone (MBK)3.5 0.20 3/11/21 2:45 BRF14 40.820.11 0.46
Isopropanol 12 8.0 3/11/21 2:45 BRF31 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 2:45 BRFND40.720.080 0.29
Methylene Chloride 2.4 2.0 3/11/21 2:45 BRF8.5 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 2:45 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 2:45 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 2:45 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 2:45 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 2:45 BRFND41.40.053 0.37
Page 10 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-A
Sample ID: 21C0286-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -25
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.6
Sampled: 3/2/2021 16:35
Canister ID: 2124
Flow Controller ID: 4141
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 17 0.20 3/11/21 2:45 BRF110 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 2:45 BRFND45.90.49 1.5
Toluene 0.67 0.20 3/11/21 2:45 BRF2.5 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 2:45 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 2:45 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 2:45 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 2:45 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.42 0.80 3/11/21 2:45 BRFL-05, J 2.4 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 2:45 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 2:45 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 2:45 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 2:45 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 2:45 BRFND40.510.11 0.29
m&p-Xylene 0.34 0.40 3/11/21 2:45 BRFJ1.5 41.70.070 0.30
o-Xylene ND 0.20 3/11/21 2:45 BRFND40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)120 3/11/21 2:4570-130
4-Bromofluorobenzene (1)104 3/11/21 7:4270-130
Page 11 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-D
Sample ID: 21C0286-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -9.5
Sampled: 3/3/2021 14:31
Canister ID: 2562
Flow Controller ID: 4403
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 240 40 3/11/21 8:07 BRF570 20952457
Benzene ND 0.20 3/11/21 3:26 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 3:26 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 3:26 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 3:26 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 3:26 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 3:26 BRFND40.440.15 0.32
2-Butanone (MEK)39 8.0 3/11/21 3:26 BRF110 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 3:26 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 3:26 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 3:26 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 3:26 BRFND40.530.20 0.52
Chloroform 8.9 0.20 3/11/21 3:26 BRF44 40.980.048 0.24
Chloromethane ND 0.40 3/11/21 3:26 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 3:26 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 3:26 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 3:26 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 3:26 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 3:26 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 3:26 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)3.9 0.20 3/11/21 3:26 BRF19 40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 3:26 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 3:26 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 3:26 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 3:26 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 3:26 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 3:26 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 3:26 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 3:26 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 3:26 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 3:26 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 58 8.0 3/11/21 3:26 BRFV-34 110 4152.4 4.6
Ethyl Acetate 14 2.0 3/11/21 3:26 BRF49 47.21.2 4.3
Ethylbenzene 0.12 0.20 3/11/21 3:26 BRFJ0.52 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 3:26 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 3:26 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 3:26 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 3:26 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 3:26 BRFND40.820.11 0.46
Isopropanol 16 8.0 3/11/21 3:26 BRF40 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 3:26 BRFND40.720.080 0.29
Methylene Chloride 4.3 2.0 3/11/21 3:26 BRF15 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 3:26 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 3:26 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 3:26 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 3:26 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 3:26 BRFND41.40.053 0.37
Page 12 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-D
Sample ID: 21C0286-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -6
Receipt Vacuum(in Hg): -9.5
Sampled: 3/3/2021 14:31
Canister ID: 2562
Flow Controller ID: 4403
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.73 0.20 3/11/21 3:26 BRF5.0 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 3:26 BRFND45.90.49 1.5
Toluene 1.5 0.20 3/11/21 3:26 BRF5.6 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 3:26 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 3:26 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 3:26 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 3:26 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.39 0.80 3/11/21 3:26 BRFL-05, J 2.2 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 3:26 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 3:26 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 3:26 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 3:26 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 3:26 BRFND40.510.11 0.29
m&p-Xylene 0.39 0.40 3/11/21 3:26 BRFJ1.7 41.70.070 0.30
o-Xylene ND 0.20 3/11/21 3:26 BRFND40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)102 3/11/21 8:0770-130
4-Bromofluorobenzene (1)121 3/11/21 3:2670-130
Page 13 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-E
Sample ID: 21C0286-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -8.0
Sampled: 3/3/2021 14:59
Canister ID: 2570
Flow Controller ID: 4417
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 230 40 3/11/21 8:33 BRF550 20952457
Benzene ND 0.20 3/11/21 4:06 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 4:06 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 4:06 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 4:06 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 4:06 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 4:06 BRFND40.440.15 0.32
2-Butanone (MEK)43 8.0 3/11/21 4:06 BRF130 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 4:06 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 4:06 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 4:06 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 4:06 BRFND40.530.20 0.52
Chloroform 1.0 0.20 3/11/21 4:06 BRF5.0 40.980.048 0.24
Chloromethane ND 0.40 3/11/21 4:06 BRFND40.830.15 0.32
Cyclohexane 7.7 0.20 3/11/21 4:06 BRF26 40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 4:06 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 4:06 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 4:06 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 4:06 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 4:06 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)4.5 0.20 3/11/21 4:06 BRF22 40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 4:06 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 4:06 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 4:06 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 4:06 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 4:06 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 4:06 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 4:06 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 4:06 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 4:06 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 4:06 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 64 8.0 3/11/21 4:06 BRFV-34 120 4152.4 4.6
Ethyl Acetate ND 2.0 3/11/21 4:06 BRFND47.21.2 4.3
Ethylbenzene 0.20 0.20 3/11/21 4:06 BRFJ0.85 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 4:06 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 4:06 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 4:06 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 4:06 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 4:06 BRFND40.820.11 0.46
Isopropanol 13 8.0 3/11/21 4:06 BRF33 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 4:06 BRFND40.720.080 0.29
Methylene Chloride 2.3 2.0 3/11/21 4:06 BRF8.0 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 4:06 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 4:06 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 4:06 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 4:06 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 4:06 BRFND41.40.053 0.37
Page 14 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-E
Sample ID: 21C0286-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -8.0
Sampled: 3/3/2021 14:59
Canister ID: 2570
Flow Controller ID: 4417
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 3.1 0.20 3/11/21 4:06 BRF21 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 4:06 BRFND45.90.49 1.5
Toluene 1.9 0.20 3/11/21 4:06 BRF7.1 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 4:06 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 4:06 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 4:06 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 4:06 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.39 0.80 3/11/21 4:06 BRFJ, L-05 2.2 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 4:06 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 4:06 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 4:06 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 4:06 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 4:06 BRFND40.510.11 0.29
m&p-Xylene 0.60 0.40 3/11/21 4:06 BRF2.6 41.70.070 0.30
o-Xylene 0.60 0.20 3/11/21 4:06 BRF2.6 40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)99.4 3/11/21 8:3370-130
4-Bromofluorobenzene (1)118 3/11/21 4:0670-130
Page 15 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-G
Sample ID: 21C0286-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.7
Sampled: 3/3/2021 15:33
Canister ID: 2319
Flow Controller ID: 4410
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 310 60 3/11/21 8:58 BRF740 301403686
Benzene ND 0.20 3/11/21 4:47 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 4:47 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 4:47 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 4:47 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 4:47 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 4:47 BRFND40.440.15 0.32
2-Butanone (MEK)44 8.0 3/11/21 4:47 BRF130 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 4:47 BRFND46.20.51 1.6
Carbon Tetrachloride 0.18 0.20 3/11/21 4:47 BRFJ1.1 41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 4:47 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 4:47 BRFND40.530.20 0.52
Chloroform ND 0.20 3/11/21 4:47 BRFND40.980.048 0.24
Chloromethane ND 0.40 3/11/21 4:47 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 4:47 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 4:47 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 4:47 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 4:47 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 4:47 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 4:47 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)5.5 0.20 3/11/21 4:47 BRF27 40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 4:47 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 4:47 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 4:47 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 4:47 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 4:47 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 4:47 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 4:47 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 4:47 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 4:47 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 4:47 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 69 8.0 3/11/21 4:47 BRFV-34 130 4152.4 4.6
Ethyl Acetate ND 2.0 3/11/21 4:47 BRFND47.21.2 4.3
Ethylbenzene 0.29 0.20 3/11/21 4:47 BRF1.3 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 4:47 BRFND40.980.062 0.30
Heptane 0.92 0.20 3/11/21 4:47 BRF3.8 40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 4:47 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 4:47 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 4:47 BRFND40.820.11 0.46
Isopropanol 18 8.0 3/11/21 4:47 BRF44 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 4:47 BRFND40.720.080 0.29
Methylene Chloride 3.1 2.0 3/11/21 4:47 BRF11 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 4:47 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 4:47 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 4:47 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 4:47 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 4:47 BRFND41.40.053 0.37
Page 16 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-G
Sample ID: 21C0286-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.7
Sampled: 3/3/2021 15:33
Canister ID: 2319
Flow Controller ID: 4410
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 58 0.20 3/11/21 4:47 BRF390 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 4:47 BRFND45.90.49 1.5
Toluene 1.6 0.20 3/11/21 4:47 BRF6.1 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 4:47 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 4:47 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 4:47 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 4:47 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.67 0.80 3/11/21 4:47 BRFL-05, J 3.8 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 4:47 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 4:47 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 4:47 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 4:47 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 4:47 BRFND40.510.11 0.29
m&p-Xylene 0.81 0.40 3/11/21 4:47 BRF3.5 41.70.070 0.30
o-Xylene ND 0.20 3/11/21 4:47 BRFND40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)120 3/11/21 4:4770-130
4-Bromofluorobenzene (1)100 3/11/21 8:5870-130
Page 17 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-F
Sample ID: 21C0286-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.4
Sampled: 3/3/2021 16:11
Canister ID: 2525
Flow Controller ID: 4408
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 280 40 3/11/21 9:24 BRF660 20952457
Benzene 0.21 0.20 3/11/21 6:07 BRF0.68 40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 6:07 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 6:07 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 6:07 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 6:07 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 6:07 BRFND40.440.15 0.32
2-Butanone (MEK)31 8.0 3/11/21 6:07 BRF93 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 6:07 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 6:07 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 6:07 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 6:07 BRFND40.530.20 0.52
Chloroform 1.5 0.20 3/11/21 6:07 BRF7.4 40.980.048 0.24
Chloromethane ND 0.40 3/11/21 6:07 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 6:07 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 6:07 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 6:07 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 6:07 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 6:07 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 6:07 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)ND 0.20 3/11/21 6:07 BRFND40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 6:07 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 6:07 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 6:07 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 6:07 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 6:07 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 6:07 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 6:07 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 6:07 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 6:07 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 6:07 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 59 8.0 3/11/21 6:07 BRFV-34 110 4152.4 4.6
Ethyl Acetate 26 2.0 3/11/21 6:07 BRF92 47.21.2 4.3
Ethylbenzene 0.30 0.20 3/11/21 6:07 BRF1.3 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 6:07 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 6:07 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 6:07 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 6:07 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 6:07 BRFND40.820.11 0.46
Isopropanol ND 8.0 3/11/21 6:07 BRFND4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 6:07 BRFND40.720.080 0.29
Methylene Chloride ND 2.0 3/11/21 6:07 BRFND46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 6:07 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 6:07 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 6:07 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 6:07 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 6:07 BRFND41.40.053 0.37
Page 18 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-F
Sample ID: 21C0286-07
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -29
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.4
Sampled: 3/3/2021 16:11
Canister ID: 2525
Flow Controller ID: 4408
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 20 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 2.7 0.20 3/11/21 6:07 BRF18 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 6:07 BRFND45.90.49 1.5
Toluene 3.9 0.20 3/11/21 6:07 BRF15 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 6:07 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 6:07 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 6:07 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 6:07 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.40 0.80 3/11/21 6:07 BRFJ, L-05 2.2 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 6:07 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 6:07 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 6:07 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 6:07 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 6:07 BRFND40.510.11 0.29
m&p-Xylene 0.95 0.40 3/11/21 6:07 BRF4.1 41.70.070 0.30
o-Xylene 0.71 0.20 3/11/21 6:07 BRF3.1 40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)98.9 3/11/21 9:2470-130
4-Bromofluorobenzene (1)121 3/11/21 6:0770-130
Page 19 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-H
Sample ID: 21C0286-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.2
Sampled: 3/4/2021 09:45
Canister ID: 2323
Flow Controller ID: 4055
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 110 20 3/11/21 9:50 BRF270 10481229
Benzene ND 0.20 3/11/21 6:47 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 6:47 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 6:47 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 6:47 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 6:47 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 6:47 BRFND40.440.15 0.32
2-Butanone (MEK)22 8.0 3/11/21 6:47 BRF64 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 6:47 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 6:47 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 6:47 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 6:47 BRFND40.530.20 0.52
Chloroform ND 0.20 3/11/21 6:47 BRFND40.980.048 0.24
Chloromethane ND 0.40 3/11/21 6:47 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 6:47 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 6:47 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 6:47 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 6:47 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 6:47 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 6:47 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)ND 0.20 3/11/21 6:47 BRFND40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 6:47 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 6:47 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 6:47 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 6:47 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 6:47 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 6:47 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 6:47 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 6:47 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 6:47 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 6:47 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 55 8.0 3/11/21 6:47 BRFV-34 100 4152.4 4.6
Ethyl Acetate 43 2.0 3/11/21 6:47 BRF160 47.21.2 4.3
Ethylbenzene 0.47 0.20 3/11/21 6:47 BRF2.0 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 6:47 BRFND40.980.062 0.30
Heptane 0.87 0.20 3/11/21 6:47 BRF3.6 40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 6:47 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 6:47 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 6:47 BRFND40.820.11 0.46
Isopropanol 7.6 8.0 3/11/21 6:47 BRFJ19 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 6:47 BRFND40.720.080 0.29
Methylene Chloride 1.4 2.0 3/11/21 6:47 BRFJ4.9 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 6:47 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 6:47 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 6:47 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 6:47 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 6:47 BRFND41.40.053 0.37
Page 20 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-H
Sample ID: 21C0286-08
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -30
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -7.2
Sampled: 3/4/2021 09:45
Canister ID: 2323
Flow Controller ID: 4055
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 19 0.20 3/11/21 6:47 BRF130 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 6:47 BRFND45.90.49 1.5
Toluene 12 0.20 3/11/21 6:47 BRF47 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 6:47 BRFND41.50.12 0.91
1,1,1-Trichloroethane 0.35 0.20 3/11/21 6:47 BRF1.9 41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 6:47 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 6:47 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.87 0.80 3/11/21 6:47 BRFL-05 4.9 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 6:47 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 6:47 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 6:47 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 6:47 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 6:47 BRFND40.510.11 0.29
m&p-Xylene 1.5 0.40 3/11/21 6:47 BRF6.5 41.70.070 0.30
o-Xylene 1.1 0.20 3/11/21 6:47 BRF4.6 40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)101 3/11/21 9:5070-130
4-Bromofluorobenzene (1)122 3/11/21 6:4770-130
Page 21 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-I
Sample ID: 21C0286-09
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -22
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -8.2
Sampled: 3/4/2021 10:08
Canister ID: 2096
Flow Controller ID: 4255
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 540 40 3/11/21 10:16 BRF1300 20952457
Benzene 0.38 0.20 3/11/21 7:27 BRF1.2 40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 7:27 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 7:27 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 7:27 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 7:27 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 7:27 BRFND40.440.15 0.32
2-Butanone (MEK)62 8.0 3/11/21 7:27 BRF180 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 7:27 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 7:27 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 7:27 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 7:27 BRFND40.530.20 0.52
Chloroform ND 0.20 3/11/21 7:27 BRFND40.980.048 0.24
Chloromethane ND 0.40 3/11/21 7:27 BRFND40.830.15 0.32
Cyclohexane 10 0.20 3/11/21 7:27 BRF35 40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 7:27 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 7:27 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 7:27 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 7:27 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 7:27 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)450 1.0 3/11/21 10:16 BRF2200 204.90.31 1.6
1,1-Dichloroethane ND 0.20 3/11/21 7:27 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 7:27 BRFND40.810.073 0.30
1,1-Dichloroethylene 0.25 0.20 3/11/21 7:27 BRF1.00 40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 7:27 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 7:27 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 7:27 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 7:27 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 7:27 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 7:27 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 7:27 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 120 8.0 3/11/21 7:27 BRFV-34 220 4152.4 4.6
Ethyl Acetate 23 2.0 3/11/21 7:27 BRF84 47.21.2 4.3
Ethylbenzene 0.21 0.20 3/11/21 7:27 BRF0.92 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 7:27 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 7:27 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 7:27 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 7:27 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 7:27 BRFND40.820.11 0.46
Isopropanol ND 8.0 3/11/21 7:27 BRFND4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 7:27 BRFND40.720.080 0.29
Methylene Chloride 7.2 2.0 3/11/21 7:27 BRF25 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 7:27 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 7:27 BRFV-05, Z-01 ND 41.00.11 0.59
Propene 18 8.0 3/11/21 7:27 BRF31 4140.67 1.2
Styrene ND 0.20 3/11/21 7:27 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 7:27 BRFND41.40.053 0.37
Page 22 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-I
Sample ID: 21C0286-09
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -22
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -8.2
Sampled: 3/4/2021 10:08
Canister ID: 2096
Flow Controller ID: 4255
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 1.6 0.20 3/11/21 7:27 BRF11 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 7:27 BRFND45.90.49 1.5
Toluene 3.4 0.20 3/11/21 7:27 BRF13 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 7:27 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 7:27 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 7:27 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 7:27 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)ND 0.80 3/11/21 7:27 BRFND44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 7:27 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 7:27 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 7:27 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 7:27 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 7:27 BRFND40.510.11 0.29
m&p-Xylene ND 0.40 3/11/21 7:27 BRFND41.70.070 0.30
o-Xylene 0.35 0.20 3/11/21 7:27 BRF1.5 40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)99.6 3/11/21 10:1670-130
4-Bromofluorobenzene (1)124 3/11/21 7:2770-130
Page 23 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-J
Sample ID: 21C0286-10
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -33
Final Vacuum(in Hg): -3
Receipt Vacuum(in Hg): -3.9
Sampled: 3/4/2021 10:39
Canister ID: 2122
Flow Controller ID: 4248
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 180 8.0 3/11/21 8:07 BRFL-05, V-06 420 4194.8 11
Benzene ND 0.20 3/11/21 8:07 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 8:07 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 8:07 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 8:07 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 8:07 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 8:07 BRFND40.440.15 0.32
2-Butanone (MEK)15 8.0 3/11/21 8:07 BRF44 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 8:07 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 8:07 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 8:07 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 8:07 BRFND40.530.20 0.52
Chloroform ND 0.20 3/11/21 8:07 BRFND40.980.048 0.24
Chloromethane ND 0.40 3/11/21 8:07 BRFND40.830.15 0.32
Cyclohexane 4.3 0.20 3/11/21 8:07 BRF15 40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 8:07 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 8:07 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 8:07 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 8:07 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 8:07 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)720 1.0 3/11/21 10:41 BRF3600 204.90.31 1.6
1,1-Dichloroethane ND 0.20 3/11/21 8:07 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 8:07 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 8:07 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 8:07 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 8:07 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 8:07 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 8:07 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 8:07 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 8:07 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 8:07 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 50 8.0 3/11/21 8:07 BRFV-34 94 4152.4 4.6
Ethyl Acetate 8.5 2.0 3/11/21 8:07 BRF31 47.21.2 4.3
Ethylbenzene 0.35 0.20 3/11/21 8:07 BRF1.5 40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 8:07 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 8:07 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 8:07 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 8:07 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 8:07 BRFND40.820.11 0.46
Isopropanol 7.3 8.0 3/11/21 8:07 BRFJ18 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 8:07 BRFND40.720.080 0.29
Methylene Chloride ND 2.0 3/11/21 8:07 BRFND46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 8:07 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 8:07 BRFV-05, Z-01 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 8:07 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 8:07 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 8:07 BRFND41.40.053 0.37
Page 24 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-J
Sample ID: 21C0286-10
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -33
Final Vacuum(in Hg): -3
Receipt Vacuum(in Hg): -3.9
Sampled: 3/4/2021 10:39
Canister ID: 2122
Flow Controller ID: 4248
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 4.2 0.20 3/11/21 8:07 BRF29 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 8:07 BRFND45.90.49 1.5
Toluene 2.7 0.20 3/11/21 8:07 BRF10 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 8:07 BRFND41.50.12 0.91
1,1,1-Trichloroethane ND 0.20 3/11/21 8:07 BRFND41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 8:07 BRFND41.10.073 0.40
Trichloroethylene 0.12 0.20 3/11/21 8:07 BRFJ0.67 41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.91 0.80 3/11/21 8:07 BRFL-05 5.1 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 8:07 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 8:07 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene 0.24 0.20 3/11/21 8:07 BRF1.2 40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 8:07 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 8:07 BRFND40.510.11 0.29
m&p-Xylene 0.98 0.40 3/11/21 8:07 BRF4.3 41.70.070 0.30
o-Xylene 0.67 0.20 3/11/21 8:07 BRF2.9 40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)100 3/11/21 10:4170-130
4-Bromofluorobenzene (1)124 3/11/21 8:0770-130
Page 25 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-K
Sample ID: 21C0286-11
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.5
Sampled: 3/4/2021 11:15
Canister ID: 2099
Flow Controller ID: 4322
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 100 20 3/11/21 11:08 BRF240 10481229
Benzene ND 0.20 3/11/21 8:47 BRFND40.640.058 0.19
Benzyl chloride ND 0.20 3/11/21 8:47 BRFND41.00.090 0.47
Bromodichloromethane ND 0.20 3/11/21 8:47 BRFND41.30.056 0.37
Bromoform ND 0.20 3/11/21 8:47 BRFND42.10.069 0.71
Bromomethane ND 0.20 3/11/21 8:47 BRFND40.780.11 0.41
1,3-Butadiene ND 0.20 3/11/21 8:47 BRFND40.440.15 0.32
2-Butanone (MEK)18 8.0 3/11/21 8:47 BRF52 4240.66 2.0
Carbon Disulfide ND 2.0 3/11/21 8:47 BRFND46.20.51 1.6
Carbon Tetrachloride ND 0.20 3/11/21 8:47 BRFND41.30.053 0.33
Chlorobenzene ND 0.20 3/11/21 8:47 BRFND40.920.048 0.22
Chloroethane ND 0.20 3/11/21 8:47 BRFND40.530.20 0.52
Chloroform ND 0.20 3/11/21 8:47 BRFND40.980.048 0.24
Chloromethane ND 0.40 3/11/21 8:47 BRFND40.830.15 0.32
Cyclohexane ND 0.20 3/11/21 8:47 BRFND40.690.098 0.34
Dibromochloromethane ND 0.20 3/11/21 8:47 BRFND41.70.067 0.57
1,2-Dibromoethane (EDB)ND 0.20 3/11/21 8:47 BRFND41.50.052 0.40
1,2-Dichlorobenzene ND 0.20 3/11/21 8:47 BRFND41.20.074 0.44
1,3-Dichlorobenzene ND 0.20 3/11/21 8:47 BRFND41.20.073 0.44
1,4-Dichlorobenzene ND 0.20 3/11/21 8:47 BRFND41.20.045 0.27
Dichlorodifluoromethane (Freon 12)ND 0.20 3/11/21 8:47 BRFND40.990.063 0.31
1,1-Dichloroethane ND 0.20 3/11/21 8:47 BRFND40.810.063 0.25
1,2-Dichloroethane ND 0.20 3/11/21 8:47 BRFND40.810.073 0.30
1,1-Dichloroethylene ND 0.20 3/11/21 8:47 BRFND40.790.11 0.43
cis-1,2-Dichloroethylene ND 0.20 3/11/21 8:47 BRFND40.790.068 0.27
trans-1,2-Dichloroethylene ND 0.20 3/11/21 8:47 BRFND40.790.059 0.23
1,2-Dichloropropane ND 0.20 3/11/21 8:47 BRFND40.920.072 0.33
cis-1,3-Dichloropropene ND 0.20 3/11/21 8:47 BRFND40.910.093 0.42
trans-1,3-Dichloropropene ND 0.20 3/11/21 8:47 BRFND40.910.067 0.30
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 3/11/21 8:47 BRFND41.40.11 0.79
1,4-Dioxane ND 2.0 3/11/21 8:47 BRFL-03, V-05 ND 47.20.56 2.0
Ethanol 54 8.0 3/11/21 8:47 BRFV-34 100 4152.4 4.6
Ethyl Acetate 10 2.0 3/11/21 8:47 BRF36 47.21.2 4.3
Ethylbenzene ND 0.20 3/11/21 8:47 BRFND40.870.042 0.18
4-Ethyltoluene ND 0.20 3/11/21 8:47 BRFND40.980.062 0.30
Heptane ND 0.20 3/11/21 8:47 BRFND40.820.086 0.35
Hexachlorobutadiene ND 0.20 3/11/21 8:47 BRFND42.10.088 0.94
Hexane ND 8.0 3/11/21 8:47 BRFND4280.36 1.3
2-Hexanone (MBK)ND 0.20 3/11/21 8:47 BRFND40.820.11 0.46
Isopropanol 6.1 8.0 3/11/21 8:47 BRFJ15 4201.8 4.5
Methyl tert-Butyl Ether (MTBE)ND 0.20 3/11/21 8:47 BRFND40.720.080 0.29
Methylene Chloride 2.8 2.0 3/11/21 8:47 BRF9.8 46.90.46 1.6
4-Methyl-2-pentanone (MIBK)ND 0.20 3/11/21 8:47 BRFND40.820.10 0.43
Naphthalene ND 0.20 3/11/21 8:47 BRFZ-01, V-05 ND 41.00.11 0.59
Propene ND 8.0 3/11/21 8:47 BRFND4140.67 1.2
Styrene ND 0.20 3/11/21 8:47 BRFND40.850.057 0.24
1,1,2,2-Tetrachloroethane ND 0.20 3/11/21 8:47 BRFND41.40.053 0.37
Page 26 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: Charlotte, NC
Date Received: 3/4/2021
Work Order: 21C0286Sample Description/Location:
Field Sample #: SG-K
Sample ID: 21C0286-11
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -5
Receipt Vacuum(in Hg): -6.5
Sampled: 3/4/2021 11:15
Canister ID: 2099
Flow Controller ID: 4322
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 1.2 0.20 3/11/21 8:47 BRF8.1 41.40.065 0.44
Tetrahydrofuran ND 2.0 3/11/21 8:47 BRFND45.90.49 1.5
Toluene 7.5 0.20 3/11/21 8:47 BRF28 40.750.058 0.22
1,2,4-Trichlorobenzene ND 0.20 3/11/21 8:47 BRFND41.50.12 0.91
1,1,1-Trichloroethane 5.3 0.20 3/11/21 8:47 BRF29 41.10.065 0.36
1,1,2-Trichloroethane ND 0.20 3/11/21 8:47 BRFND41.10.073 0.40
Trichloroethylene ND 0.20 3/11/21 8:47 BRFND41.10.074 0.40
Trichlorofluoromethane (Freon 11)0.34 0.80 3/11/21 8:47 BRFL-05, J 1.9 44.50.15 0.85
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 3/11/21 8:47 BRFND46.10.15 1.2
1,2,4-Trimethylbenzene ND 0.20 3/11/21 8:47 BRFND40.980.046 0.22
1,3,5-Trimethylbenzene ND 0.20 3/11/21 8:47 BRFND40.980.052 0.26
Vinyl Acetate ND 4.0 3/11/21 8:47 BRFND4140.56 2.0
Vinyl Chloride ND 0.20 3/11/21 8:47 BRFND40.510.11 0.29
m&p-Xylene ND 0.40 3/11/21 8:47 BRFND41.70.070 0.30
o-Xylene ND 0.20 3/11/21 8:47 BRFND40.870.054 0.23
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)101 3/11/21 11:0870-130
4-Bromofluorobenzene (1)121 3/11/21 8:4770-130
Page 27 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
21C0286-01 [SG-C]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-02 [SG-B]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-03 [SG-A]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-04 [SG-D]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-05 [SG-E]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-06 [SG-G]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-07 [SG-F]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-08 [SG-H]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-09 [SG-I]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-10 [SG-J]B277883 1.5 1 N/A 1000 400 150 03/10/21
21C0286-11 [SG-K]B277883 1.5 1 N/A 1000 400 150 03/10/21
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
21C0286-01RE1 [SG-C]B277891 1.5 1 N/A 1000 200 10 03/10/21
21C0286-02RE1 [SG-B]B277891 1.5 1 N/A 1000 200 15 03/10/21
21C0286-03RE1 [SG-A]B277891 1.5 1 N/A 1000 200 15 03/10/21
21C0286-04RE1 [SG-D]B277891 1.5 1 N/A 1000 200 15 03/10/21
21C0286-05RE1 [SG-E]B277891 1.5 1 N/A 1000 200 15 03/10/21
21C0286-06RE1 [SG-G]B277891 1.5 1 N/A 1000 200 10 03/10/21
21C0286-07RE1 [SG-F]B277891 1.5 1 N/A 1000 200 15 03/10/21
21C0286-08RE1 [SG-H]B277891 1.5 1 N/A 1000 200 30 03/10/21
21C0286-09RE1 [SG-I]B277891 1.5 1 N/A 1000 200 15 03/10/21
21C0286-10RE1 [SG-J]B277891 1.5 1 N/A 1000 200 15 03/10/21
21C0286-11RE1 [SG-K]B277891 1.5 1 N/A 1000 200 30 03/10/21
Page 28 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B277883 - TO-15 Prep
Blank (B277883-BLK1)Prepared & Analyzed: 03/10/21
0.80NDAcetone
0.020NDBenzene
0.020NDBenzyl chloride
0.020NDBromodichloromethane
0.020NDBromoform
0.020NDBromomethane
0.020ND1,3-Butadiene
0.80ND2-Butanone (MEK)
0.20NDCarbon Disulfide
0.020NDCarbon Tetrachloride
0.020NDChlorobenzene
0.020NDChloroethane
0.020NDChloroform
0.040NDChloromethane
0.020NDCyclohexane
0.020NDDibromochloromethane
0.020ND1,2-Dibromoethane (EDB)
0.020ND1,2-Dichlorobenzene
0.020ND1,3-Dichlorobenzene
0.020ND1,4-Dichlorobenzene
0.020NDDichlorodifluoromethane (Freon 12)
0.020ND1,1-Dichloroethane
0.020ND1,2-Dichloroethane
0.020ND1,1-Dichloroethylene
0.020NDcis-1,2-Dichloroethylene
0.020NDtrans-1,2-Dichloroethylene
0.020ND1,2-Dichloropropane
0.020NDcis-1,3-Dichloropropene
0.020NDtrans-1,3-Dichloropropene
0.020ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.20 L-03, V-05ND1,4-Dioxane
0.80 V-34NDEthanol
0.20NDEthyl Acetate
0.020NDEthylbenzene
0.020ND4-Ethyltoluene
0.020NDHeptane
0.020NDHexachlorobutadiene
0.80NDHexane
0.020ND2-Hexanone (MBK)
0.80NDIsopropanol
0.020NDMethyl tert-Butyl Ether (MTBE)
0.20NDMethylene Chloride
0.020ND4-Methyl-2-pentanone (MIBK)
0.020 V-05, Z-01NDNaphthalene
0.80NDPropene
0.020NDStyrene
Page 29 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B277883 - TO-15 Prep
Blank (B277883-BLK1)Prepared & Analyzed: 03/10/21
0.020ND1,1,2,2-Tetrachloroethane
0.020NDTetrachloroethylene
0.20NDTetrahydrofuran
0.020NDToluene
0.020ND1,2,4-Trichlorobenzene
0.020ND1,1,1-Trichloroethane
0.020ND1,1,2-Trichloroethane
0.020NDTrichloroethylene
0.080NDTrichlorofluoromethane (Freon 11)
0.080ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.020ND1,2,4-Trimethylbenzene
0.020ND1,3,5-Trimethylbenzene
0.40NDVinyl Acetate
0.020NDVinyl Chloride
0.040NDm&p-Xylene
0.020NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1128.97
LCS (B277883-BS1)Prepared & Analyzed: 03/10/21
5.00 V-06, L-0570-1301477.34Acetone *
5.00 70-13078.23.91Benzene
5.00 70-1301095.46Benzyl chloride
5.00 70-13089.94.50Bromodichloromethane
5.00 V-2070-1301256.24Bromoform
5.00 70-13084.74.24Bromomethane
5.00 70-1301035.141,3-Butadiene
5.00 70-13089.34.462-Butanone (MEK)
5.00 70-13089.84.49Carbon Disulfide
5.00 70-1301165.81Carbon Tetrachloride
5.00 70-13085.84.29Chlorobenzene
5.00 70-13098.44.92Chloroethane
5.00 70-13094.94.75Chloroform
5.00 70-1301025.10Chloromethane
5.00 70-13071.73.59Cyclohexane
5.00 70-1301125.58Dibromochloromethane
5.00 70-13085.04.251,2-Dibromoethane (EDB)
5.00 70-1301105.481,2-Dichlorobenzene
5.00 70-1301125.621,3-Dichlorobenzene
5.00 70-1301095.461,4-Dichlorobenzene
5.00 70-1301155.74Dichlorodifluoromethane (Freon 12)
5.00 70-13085.84.291,1-Dichloroethane
5.00 70-1301085.411,2-Dichloroethane
5.00 70-13092.54.621,1-Dichloroethylene
5.00 70-13081.54.08cis-1,2-Dichloroethylene
5.00 70-13086.14.30trans-1,2-Dichloroethylene
5.00 70-13072.43.621,2-Dichloropropane
Page 30 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B277883 - TO-15 Prep
LCS (B277883-BS1)Prepared & Analyzed: 03/10/21
5.00 70-13073.33.66cis-1,3-Dichloropropene
5.00 70-13086.34.31trans-1,3-Dichloropropene
5.00 70-13089.74.481,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 V-05, L-0370-13066.73.331,4-Dioxane *
5.00 V-3470-1301095.47Ethanol
5.00 70-13078.43.92Ethyl Acetate
5.00 70-13083.44.17Ethylbenzene
5.00 70-13089.34.464-Ethyltoluene
5.00 70-13077.53.88Heptane
5.00 L-0170-1301477.36Hexachlorobutadiene *
5.00 70-1301135.67Hexane
5.00 70-13076.83.842-Hexanone (MBK)
5.00 70-1301155.74Isopropanol
5.00 70-13086.24.31Methyl tert-Butyl Ether (MTBE)
5.00 70-1301025.11Methylene Chloride
5.00 70-13081.54.084-Methyl-2-pentanone (MIBK)
5.00 Z-01, V-0570-13096.84.84Naphthalene
5.00 70-13093.04.65Propene
5.00 70-13085.04.25Styrene
5.00 70-13075.43.771,1,2,2-Tetrachloroethane
5.00 70-13096.34.81Tetrachloroethylene
5.00 70-13078.33.91Tetrahydrofuran
5.00 70-13081.74.08Toluene
5.00 70-1301306.491,2,4-Trichlorobenzene
5.00 70-13094.44.721,1,1-Trichloroethane
5.00 70-13082.14.111,1,2-Trichloroethane
5.00 70-13083.64.18Trichloroethylene
5.00 L-0570-1301316.56Trichlorofluoromethane (Freon 11)*
5.00 70-13097.94.901,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-13093.04.651,2,4-Trimethylbenzene
5.00 70-13095.84.791,3,5-Trimethylbenzene
5.00 70-13090.24.51Vinyl Acetate
5.00 70-13090.64.53Vinyl Chloride
10.0 70-13090.09.00m&p-Xylene
5.00 70-13089.24.46o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1149.09
Page 31 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B277891 - TO-15 Prep
Blank (B277891-BLK1)Prepared & Analyzed: 03/10/21
0.80NDAcetone
0.020NDChloroform
0.020NDDichlorodifluoromethane (Freon 12)
0.80NDEthanol
0.80NDIsopropanol
0.020NDTetrachloroethylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1008.00
LCS (B277891-BS1)Prepared & Analyzed: 03/10/21
5.00 70-13085.24.26Acetone
5.00 70-1301095.46Chloroform
5.00 70-1301226.12Dichlorodifluoromethane (Freon 12)
5.00 70-13076.03.80Ethanol
5.00 70-13073.43.67Isopropanol
5.00 70-13089.04.45Tetrachloroethylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1048.29
Page 32 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not
affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high
side.
L-01
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this
compound is likely to be biased on the low side.
L-03
Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this
compound is likely to be biased on the high side.
L-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
Page 33 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
Calibrations RSD for this compound is >30% but <40%.Z-01
ANALYST
Thomas P. HniteckiTPH
Raisa A. PetraitisRAP
PDF Management StationSTATION
Kerry K. McGeeKKM
Brittany R. FiskBRF
Page 34 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S055345-ICV1 )Lab File ID: G2034717.D Analyzed: 12/12/20 20:54
Bromochloromethane (1)505996 8.515 488099 8.515 60 - 140104 0.0000 +/-0.50
1,4-Difluorobenzene (1)1450373 10.289 1376596 10.289 60 - 140105 0.0000 +/-0.50
Chlorobenzene-d5 (1)1360732 14.667 1307205 14.666 60 - 140104 0.0010 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S057255-ICV1 )Lab File ID: K2104723.D Analyzed: 02/17/21 16:51
Bromochloromethane (1)107800 2.968 111919 2.968 60 - 14096 0.0000 +/-0.50
1,4-Difluorobenzene (1)442785 3.58 454201 3.581 60 - 14097 -0.0010 +/-0.50
Chlorobenzene-d5 (1)339053 5.18 349429 5.183 60 - 14097 -0.0030 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S057690-CCV1 )Lab File ID: G2106904.D Analyzed: 03/10/21 12:43
Bromochloromethane (1)386986 8.509 488099 8.515 60 - 14079 -0.0060 +/-0.50
1,4-Difluorobenzene (1)1131004 10.289 1376596 10.289 60 - 14082 0.0000 +/-0.50
Chlorobenzene-d5 (1)966730 14.66 1307205 14.666 60 - 14074 -0.0060 +/-0.50
LCS (B277883-BS1 )Lab File ID: G2106906.D Analyzed: 03/10/21 14:01
Bromochloromethane (1)383860 8.509 386986 8.509 60 - 14099 0.0000 +/-0.50
1,4-Difluorobenzene (1)1122586 10.289 1131004 10.289 60 - 14099 0.0000 +/-0.50
Chlorobenzene-d5 (1)1012204 14.66 966730 14.66 60 - 140105 0.0000 +/-0.50
Blank (B277883-BLK1 )Lab File ID: G2106912.D Analyzed: 03/10/21 18:11
Bromochloromethane (1)374011 8.515 386986 8.509 60 - 14097 0.0060 +/-0.50
1,4-Difluorobenzene (1)1047037 10.289 1131004 10.289 60 - 14093 0.0000 +/-0.50
Chlorobenzene-d5 (1)958107 14.66 966730 14.66 60 - 14099 0.0000 +/-0.50
SG-C (21C0286-01 )Lab File ID: G2106922.D Analyzed: 03/11/21 00:44
Bromochloromethane (1)357474 8.509 386986 8.509 60 - 14092 0.0000 +/-0.50
1,4-Difluorobenzene (1)1069095 10.289 1131004 10.289 60 - 14095 0.0000 +/-0.50
Chlorobenzene-d5 (1)981794 14.661 966730 14.66 60 - 140102 0.0010 +/-0.50
SG-B (21C0286-02 )Lab File ID: G2106924.D Analyzed: 03/11/21 02:04
Bromochloromethane (1)290595 8.509 386986 8.509 60 - 14075 0.0000 +/-0.50
1,4-Difluorobenzene (1)923072 10.283 1131004 10.289 60 - 14082 -0.0060 +/-0.50
Chlorobenzene-d5 (1)851078 14.66 966730 14.66 60 - 14088 0.0000 +/-0.50
Page 35 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SG-A (21C0286-03 )Lab File ID: G2106925.D Analyzed: 03/11/21 02:45
Bromochloromethane (1)277336 8.509 386986 8.509 60 - 14072 0.0000 +/-0.50
1,4-Difluorobenzene (1)906902 10.289 1131004 10.289 60 - 14080 0.0000 +/-0.50
Chlorobenzene-d5 (1)828561 14.66 966730 14.66 60 - 14086 0.0000 +/-0.50
SG-D (21C0286-04 )Lab File ID: G2106926.D Analyzed: 03/11/21 03:26
Bromochloromethane (1)269792 8.509 386986 8.509 60 - 14070 0.0000 +/-0.50
1,4-Difluorobenzene (1)861948 10.283 1131004 10.289 60 - 14076 -0.0060 +/-0.50
Chlorobenzene-d5 (1)804099 14.66 966730 14.66 60 - 14083 0.0000 +/-0.50
SG-E (21C0286-05 )Lab File ID: G2106927.D Analyzed: 03/11/21 04:06
Bromochloromethane (1)267187 8.509 386986 8.509 60 - 14069 0.0000 +/-0.50
1,4-Difluorobenzene (1)866737 10.289 1131004 10.289 60 - 14077 0.0000 +/-0.50
Chlorobenzene-d5 (1)809415 14.66 966730 14.66 60 - 14084 0.0000 +/-0.50
SG-G (21C0286-06 )Lab File ID: G2106928.D Analyzed: 03/11/21 04:47
Bromochloromethane (1)262707 8.509 386986 8.509 60 - 14068 0.0000 +/-0.50
1,4-Difluorobenzene (1)837542 10.283 1131004 10.289 60 - 14074 -0.0060 +/-0.50
Chlorobenzene-d5 (1)790421 14.661 966730 14.66 60 - 14082 0.0010 +/-0.50
SG-F (21C0286-07 )Lab File ID: G2106930.D Analyzed: 03/11/21 06:07
Bromochloromethane (1)261503 8.509 386986 8.509 60 - 14068 0.0000 +/-0.50
1,4-Difluorobenzene (1)856579 10.289 1131004 10.289 60 - 14076 0.0000 +/-0.50
Chlorobenzene-d5 (1)795857 14.66 966730 14.66 60 - 14082 0.0000 +/-0.50
SG-H (21C0286-08 )Lab File ID: G2106929.D Analyzed: 03/11/21 06:47
Bromochloromethane (1)293606 8.509 386986 8.509 60 - 14076 0.0000 +/-0.50
1,4-Difluorobenzene (1)937061 10.289 1131004 10.289 60 - 14083 0.0000 +/-0.50
Chlorobenzene-d5 (1)889565 14.66 966730 14.66 60 - 14092 0.0000 +/-0.50
SG-I (21C0286-09 )Lab File ID: G2106931.D Analyzed: 03/11/21 07:27
Bromochloromethane (1)317645 8.509 386986 8.509 60 - 14082 0.0000 +/-0.50
1,4-Difluorobenzene (1)999078 10.289 1131004 10.289 60 - 14088 0.0000 +/-0.50
Chlorobenzene-d5 (1)932657 14.66 966730 14.66 60 - 14096 0.0000 +/-0.50
SG-J (21C0286-10 )Lab File ID: G2106932.D Analyzed: 03/11/21 08:07
Bromochloromethane (1)332770 8.509 386986 8.509 60 - 14086 0.0000 +/-0.50
1,4-Difluorobenzene (1)1064961 10.283 1131004 10.289 60 - 14094 -0.0060 +/-0.50
Chlorobenzene-d5 (1)995133 14.66 966730 14.66 60 - 140103 0.0000 +/-0.50
SG-K (21C0286-11 )Lab File ID: G2106933.D Analyzed: 03/11/21 08:47
Bromochloromethane (1)374454 8.515 386986 8.509 60 - 14097 0.0060 +/-0.50
1,4-Difluorobenzene (1)1159857 10.289 1131004 10.289 60 - 140103 0.0000 +/-0.50
Chlorobenzene-d5 (1)1120619 14.66 966730 14.66 60 - 140116 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
Page 36 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S057700-CCV1 )Lab File ID: K2106904.D Analyzed: 03/10/21 12:24
Bromochloromethane (1)83047 2.968 111919 2.968 60 - 14074 0.0000 +/-0.50
1,4-Difluorobenzene (1)461444 3.58 454201 3.581 60 - 140102 -0.0010 +/-0.50
Chlorobenzene-d5 (1)357744 5.18 349429 5.183 60 - 140102 -0.0030 +/-0.50
LCS (B277891-BS1 )Lab File ID: K2106905.D Analyzed: 03/10/21 12:49
Bromochloromethane (1)82970 2.965 83047 2.968 60 - 140100 -0.0030 +/-0.50
1,4-Difluorobenzene (1)464621 3.577 461444 3.58 60 - 140101 -0.0030 +/-0.50
Chlorobenzene-d5 (1)358804 5.18 357744 5.18 60 - 140100 0.0000 +/-0.50
Blank (B277891-BLK1 )Lab File ID: K2106909.D Analyzed: 03/10/21 14:43
Bromochloromethane (1)93169 2.965 83047 2.968 60 - 140112 -0.0030 +/-0.50
1,4-Difluorobenzene (1)505871 3.58 461444 3.58 60 - 140110 0.0000 +/-0.50
Chlorobenzene-d5 (1)371615 5.18 357744 5.18 60 - 140104 0.0000 +/-0.50
SG-C (21C0286-01RE1 )Lab File ID: K2106920.D Analyzed: 03/11/21 06:50
Bromochloromethane (1)98528 2.965 83047 2.968 60 - 140119 -0.0030 +/-0.50
1,4-Difluorobenzene (1)511168 3.577 461444 3.58 60 - 140111 -0.0030 +/-0.50
Chlorobenzene-d5 (1)368993 5.18 357744 5.18 60 - 140103 0.0000 +/-0.50
SG-B (21C0286-02RE1 )Lab File ID: K2106921.D Analyzed: 03/11/21 07:16
Bromochloromethane (1)87421 2.968 83047 2.968 60 - 140105 0.0000 +/-0.50
1,4-Difluorobenzene (1)473376 3.58 461444 3.58 60 - 140103 0.0000 +/-0.50
Chlorobenzene-d5 (1)351161 5.183 357744 5.18 60 - 14098 0.0030 +/-0.50
SG-A (21C0286-03RE1 )Lab File ID: K2106922.D Analyzed: 03/11/21 07:42
Bromochloromethane (1)84468 2.971 83047 2.968 60 - 140102 0.0030 +/-0.50
1,4-Difluorobenzene (1)457404 3.584 461444 3.58 60 - 14099 0.0040 +/-0.50
Chlorobenzene-d5 (1)344488 5.183 357744 5.18 60 - 14096 0.0030 +/-0.50
SG-D (21C0286-04RE1 )Lab File ID: K2106923.D Analyzed: 03/11/21 08:07
Bromochloromethane (1)85440 2.968 83047 2.968 60 - 140103 0.0000 +/-0.50
1,4-Difluorobenzene (1)484811 3.58 461444 3.58 60 - 140105 0.0000 +/-0.50
Chlorobenzene-d5 (1)354769 5.18 357744 5.18 60 - 14099 0.0000 +/-0.50
SG-E (21C0286-05RE1 )Lab File ID: K2106924.D Analyzed: 03/11/21 08:33
Bromochloromethane (1)86354 2.965 83047 2.968 60 - 140104 -0.0030 +/-0.50
1,4-Difluorobenzene (1)479984 3.58 461444 3.58 60 - 140104 0.0000 +/-0.50
Chlorobenzene-d5 (1)357386 5.183 357744 5.18 60 - 140100 0.0030 +/-0.50
SG-G (21C0286-06RE1 )Lab File ID: K2106925.D Analyzed: 03/11/21 08:58
Bromochloromethane (1)84357 2.968 83047 2.968 60 - 140102 0.0000 +/-0.50
1,4-Difluorobenzene (1)478061 3.581 461444 3.58 60 - 140104 0.0010 +/-0.50
Chlorobenzene-d5 (1)353918 5.183 357744 5.18 60 - 14099 0.0030 +/-0.50
Page 37 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SG-F (21C0286-07RE1 )Lab File ID: K2106926.D Analyzed: 03/11/21 09:24
Bromochloromethane (1)83543 2.968 83047 2.968 60 - 140101 0.0000 +/-0.50
1,4-Difluorobenzene (1)486424 3.58 461444 3.58 60 - 140105 0.0000 +/-0.50
Chlorobenzene-d5 (1)356062 5.183 357744 5.18 60 - 140100 0.0030 +/-0.50
SG-H (21C0286-08RE1 )Lab File ID: K2106927.D Analyzed: 03/11/21 09:50
Bromochloromethane (1)83143 2.968 83047 2.968 60 - 140100 0.0000 +/-0.50
1,4-Difluorobenzene (1)482587 3.58 461444 3.58 60 - 140105 0.0000 +/-0.50
Chlorobenzene-d5 (1)356182 5.183 357744 5.18 60 - 140100 0.0030 +/-0.50
SG-I (21C0286-09RE1 )Lab File ID: K2106928.D Analyzed: 03/11/21 10:16
Bromochloromethane (1)82100 2.971 83047 2.968 60 - 14099 0.0030 +/-0.50
1,4-Difluorobenzene (1)475886 3.58 461444 3.58 60 - 140103 0.0000 +/-0.50
Chlorobenzene-d5 (1)352289 5.183 357744 5.18 60 - 14098 0.0030 +/-0.50
SG-J (21C0286-10RE1 )Lab File ID: K2106929.D Analyzed: 03/11/21 10:41
Bromochloromethane (1)82237 2.971 83047 2.968 60 - 14099 0.0030 +/-0.50
1,4-Difluorobenzene (1)472888 3.584 461444 3.58 60 - 140102 0.0040 +/-0.50
Chlorobenzene-d5 (1)351048 5.183 357744 5.18 60 - 14098 0.0030 +/-0.50
SG-K (21C0286-11RE1 )Lab File ID: K2106930.D Analyzed: 03/11/21 11:08
Bromochloromethane (1)79714 2.975 83047 2.968 60 - 14096 0.0070 +/-0.50
1,4-Difluorobenzene (1)478624 3.587 461444 3.58 60 - 140104 0.0070 +/-0.50
Chlorobenzene-d5 (1)360265 5.183 357744 5.18 60 - 140101 0.0030 +/-0.50
Page 38 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S057690-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
1.151467A 41.9 *307.09 0.81158015.00Acetone
0.6343419A -23.1 303.84 0.82539185.00Benzene
0.7481402A 21.7 306.09 0.61455625.00Benzyl chloride
0.5206899A -9.9 304.50 0.57784985.00Bromodichloromethane
0.5891399A 40.5 *307.03 0.41926245.00Bromoform
0.5629434A -17.2 304.14 0.67955115.00Bromomethane
0.4694702A 0.5 305.03 0.46703095.001,3-Butadiene
1.210673A -13.0 304.35 1.3919855.002-Butanone (MEK)
1.763115A -13.4 304.33 2.0360965.00Carbon Disulfide
0.5301994A 19.5 305.98 0.44360025.00Carbon Tetrachloride
0.7495057A -6.8 304.66 0.80444835.00Chlorobenzene
0.2977761A -5.5 304.73 0.31500645.00Chloroethane
1.441772A -5.2 304.74 1.5205565.00Chloroform
0.5779806A 4.8 305.24 0.55128855.00Chloromethane
0.2645536A -28.1 303.60 0.36786055.00Cyclohexane
0.6259998A 21.1 306.05 0.51699025.00Dibromochloromethane
0.4963785A -8.3 304.58 0.54157795.001,2-Dibromoethane (EDB)
0.5666575A 22.3 306.12 0.46329595.001,2-Dichlorobenzene
0.6882931A 27.5 306.37 0.53996995.001,3-Dichlorobenzene
0.6644155A 23.2 306.16 0.53943395.001,4-Dichlorobenzene
1.696516A 13.6 305.68 1.4931215.00Dichlorodifluoromethane (Freon 12)
1.117953A -16.7 304.17 1.34195.001,1-Dichloroethane
0.9253337A 5.5 305.28 0.87669355.001,2-Dichloroethane
0.9906715A -9.6 304.52 1.095815.001,1-Dichloroethylene
0.7883613A -19.4 304.03 0.97787355.00cis-1,2-Dichloroethylene
0.8215863A -18.0 304.10 1.0013645.00trans-1,2-Dichloroethylene
0.230941A -32.7 *303.67 0.34291475.001,2-Dichloropropane
0.3764712A -23.5 303.83 0.491855.00cis-1,3-Dichloropropene
0.326123A -14.2 304.29 0.38030865.00trans-1,3-Dichloropropene
1.617212A -3.6 304.82 1.6774395.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1241134A -34.8 *303.26 0.19025475.001,4-Dioxane
0.1629372A -8.3 304.58 0.17771145.00Ethanol
0.2099756A -17.0 304.15 0.25311635.00Ethyl Acetate
1.124126A -10.4 304.48 1.2541855.00Ethylbenzene
1.173485A 0.7 305.04 1.1654355.004-Ethyltoluene
0.1972067A -20.7 303.96 0.24866565.00Heptane
0.312726A 24.2 306.21 0.25177355.00Hexachlorobutadiene
0.797358A 12.9 305.64 0.73067145.00Hexane
Page 39 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S057690-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.5383973A -16.7 304.16 0.64633365.002-Hexanone (MBK)
1.13927A 22.4 306.12 0.93093635.00Isopropanol
1.577971A -15.1 304.24 1.8596235.00Methyl tert-Butyl Ether (MTBE)
0.7528748A -0.3 304.98 0.75519945.00Methylene Chloride
0.5230694A -14.5 304.27 0.61201125.004-Methyl-2-pentanone (MIBK)
0.4704321A -37.6 *303.12 0.75346765.00Naphthalene
0.5151277A -1.9 304.91 0.52484025.00Propene
0.6680202A -6.4 304.68 0.71348735.00Styrene
0.6684522A -16.1 304.20 0.79680455.001,1,2,2-Tetrachloroethane
0.4486001A 2.5 305.13 0.43751765.00Tetrachloroethylene
0.2437339A -22.4 303.88 0.31401185.00Tetrahydrofuran
0.8586704A -16.4 304.18 1.0266415.00Toluene
0.2489812A -4.8 304.76 0.2614095.001,2,4-Trichlorobenzene
0.5000739A 2.2 305.11 0.48942785.001,1,1-Trichloroethane
0.3248957A -11.3 304.44 0.36615875.001,1,2-Trichloroethane
0.3056371A -16.2 304.19 0.36472025.00Trichloroethylene
1.750964A 28.5 306.42 1.3629225.00Trichlorofluoromethane (Freon 11)
1.353955A -0.6 304.97 1.3623125.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.936609A 7.2 305.36 0.8733095.001,2,4-Trimethylbenzene
1.008584A 8.7 305.44 0.92773195.001,3,5-Trimethylbenzene
1.456917A -15.5 304.22 1.7245595.00Vinyl Acetate
0.6182301A -10.3 304.48 0.68915255.00Vinyl Chloride
0.9201841A -1.9 309.81 0.937867510.0m&p-Xylene
0.9315528A -2.5 304.87 0.95582245.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 40 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S057700-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.9813624A -10.7 304.46 1.0990455.00Acetone
1.980681A 12.7 305.63 1.7575365.00Chloroform
2.822421A 25.5 306.28 2.2485385.00Dichlorodifluoromethane (Freon 12)
0.1725481A -14.8 304.26 0.20259395.00Ethanol
1.122391A -14.2 304.29 1.3086415.00Isopropanol
0.4595957A -4.5 304.77 0.48139555.00Tetrachloroethylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 41 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 42 of 47
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2021
PH-0165Connecticut Department of Publilc HealthCT 12/31/2022
10899 NELAPNew York State Department of HealthNY 04/1/2021
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2022
LAO00112Rhode Island Department of HealthRI 12/30/2021
652North Carolina Div. of Water QualityNC 12/31/2021
MA007 NELAPNew Jersey DEPNJ 06/30/2021
E871027 NELAPFlorida Department of HealthFL 06/30/2021
LL720741Vermont Department of Health Lead LaboratoryVT 07/30/2021
MA00100State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2021
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2021
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2021
25703North Carolina Department of HealthNC-DW 07/31/2021
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2021
9100Dept. of Env, Great Lakes, and EnergyMI 09/6/2021
Page 43 of 47
Page 44 of 47
Page 45 of 47
Page 46 of 47
Page 47 of 47
#=CL#
March 05, 2021
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92524499
92524499
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
Monroe Road Site
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on February 26, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 98
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92524499
Monroe Road Site
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 98
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92524499
Monroe Road Site
Lab ID Sample ID Matrix Date Collected Date Received
92524499001 GW-1 Water 02/24/21 10:25 02/26/21 12:55
92524499002 GW-2 Water 02/24/21 11:00 02/26/21 12:55
92524499003 GW-3 Water 02/24/21 11:45 02/26/21 12:55
92524499004 GW-4 Water 02/24/21 12:20 02/26/21 12:55
92524499005 GW-5 Water 02/24/21 13:10 02/26/21 12:55
92524499006 GW-6 Water 02/24/21 13:40 02/26/21 12:55
92524499007 GW-7 Water 02/24/21 14:40 02/26/21 12:55
92524499008 GW-8 Water 02/24/21 15:15 02/26/21 12:55
92524499009 GW-9 Water 02/25/21 10:05 02/26/21 12:55
92524499010 GW-10 Water 02/25/21 16:20 02/26/21 12:55
92524499011 GW-14 Water 02/25/21 13:30 02/26/21 12:55
92524499012 GW-12 Water 02/25/21 11:55 02/26/21 12:55
92524499013 GW-13 Water 02/25/21 13:00 02/26/21 12:55
92524499014 GW-16 Water 02/25/21 14:50 02/26/21 12:55
92524499015 GW-17 Water 02/25/21 15:30 02/26/21 12:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 98
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92524499
Monroe Road Site
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92524499001 GW-1 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499002 GW-2 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499003 GW-3 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499004 GW-4 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499005 GW-5 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499006 GW-6 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499007 GW-7 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499008 GW-8 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499009 GW-9 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92524499010 GW-10 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CBSH
92524499011 GW-14 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CBSH
92524499012 GW-12 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92524499013 GW-13 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92524499014 GW-16 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92524499015 GW-17 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CBSH
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 98
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92524499
Monroe Road Site
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92524499001 GW-1
Tetrachloroethene 10.1 ug/L 02/27/21 00:191.0EPA 8260D
92524499002 GW-2
cis-1,2-Dichloroethene 2.3 ug/L 02/27/21 00:381.0EPA 8260D
Diisopropyl ether 0.23J ug/L 02/27/21 00:381.0EPA 8260D
Tetrachloroethene 78.2 ug/L 02/27/21 00:381.0EPA 8260D
Trichloroethene 2.6 ug/L 02/27/21 00:381.0EPA 8260D
92524499004 GW-4
Acetone 48.8 ug/L 02/27/21 01:1425.0EPA 8260D
92524499005 GW-5
Acetone 15.6J ug/L 02/27/21 01:3225.0EPA 8260D
Chloroform 5.0 ug/L 02/27/21 01:325.0EPA 8260D
cis-1,2-Dichloroethene 1.7 ug/L 02/27/21 01:321.0EPA 8260D
Tetrachloroethene 69.0 ug/L 02/27/21 01:321.0EPA 8260D
Trichloroethene 1.6 ug/L 02/27/21 01:321.0EPA 8260D
92524499006 GW-6
Acetone 18.1J ug/L 02/27/21 01:5025.0EPA 8260D
92524499007 GW-7
Acetone 19.2J ug/L 02/27/21 02:0825.0EPA 8260D
92524499012 GW-12
Acetone 14.5J ug/L 03/01/21 12:15 v125.0EPA 8260D
Methyl-tert-butyl ether 40.0 ug/L 03/01/21 12:151.0EPA 8260D
Tetrachloroethene 10.9 ug/L 03/01/21 12:151.0EPA 8260D
92524499013 GW-13
Benzene 55.9 ug/L 03/01/21 16:4810.0EPA 8260D
Diisopropyl ether 3.1J ug/L 03/01/21 16:4810.0EPA 8260D
Ethylbenzene 4.3J ug/L 03/01/21 16:4810.0EPA 8260D
Methyl-tert-butyl ether 1540 ug/L 03/01/21 16:4810.0EPA 8260D
Naphthalene 4.8J ug/L 03/01/21 16:48 v110.0EPA 8260D
Tetrachloroethene 198 ug/L 03/01/21 16:4810.0EPA 8260D
Xylene (Total)8.6J ug/L 03/01/21 16:4810.0EPA 8260D
o-Xylene 8.6J ug/L 03/01/21 16:4810.0EPA 8260D
92524499014 GW-16
Acetone 11.6J ug/L 03/01/21 12:33 v125.0EPA 8260D
Chloroform 12.5 ug/L 03/01/21 12:335.0EPA 8260D
Methyl-tert-butyl ether 1.6 ug/L 03/01/21 12:331.0EPA 8260D
Tetrachloroethene 8.6 ug/L 03/01/21 12:331.0EPA 8260D
92524499015 GW-17
Acetone 28.6 ug/L 02/27/21 16:2625.0EPA 8260D
Chloroform 3.4J ug/L 02/27/21 16:265.0EPA 8260D
cis-1,2-Dichloroethene 0.57J ug/L 02/27/21 16:261.0EPA 8260D
Methyl-tert-butyl ether 5.0 ug/L 02/27/21 16:261.0EPA 8260D
Tetrachloroethene 75.0 ug/L 02/27/21 16:261.0EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 98
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92524499
Monroe Road Site
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92524499015 GW-17
Trichloroethene 0.50J ug/L 02/27/21 16:261.0EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-1 Lab ID:92524499001 Collected:02/24/21 10:25 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 19:33 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 19:33 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 19:33 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 19:33 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 19:33 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 19:33 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 19:33 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 19:33 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 19:33 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 19:33 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 19:33 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 19:33 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 19:33 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 19:33 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 19:33 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 19:33 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 19:33 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 19:33 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 19:33 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 19:33 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 19:33 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 19:33 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 19:33 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 19:33 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 19:33 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 19:33 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 19:33 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 19:33 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 19:33 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 19:33 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 19:33 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 19:33 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 19:33 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 19:33 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 19:33 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 19:33 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 19:33 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 19:33 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 19:33 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 19:33 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 19:33 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 19:33 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 19:33 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 19:33 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 19:33 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-1 Lab ID:92524499001 Collected:02/24/21 10:25 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 19:33 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 19:33 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 19:33 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 19:33 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 19:33 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 19:33 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 19:33 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 19:33 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 19:33 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 19:33 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 19:33 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 19:33 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 19:33 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 19:33 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 19:33 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 19:33 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 19:33 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 19:33 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 19:33 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 19:33 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 19:33 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 19:33 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 19:33 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)66 %03/02/21 19:33 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)61 %03/02/21 19:33 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)96 %03/02/21 19:33 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)39 %03/02/21 19:33 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)48 %03/02/21 19:33 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)82 %03/02/21 19:33 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/27/21 00:19 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 00:19 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 00:19 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 00:19 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 00:19 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 00:19 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 00:19 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 00:19 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 00:19 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 00:19 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 00:19 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 00:19 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-1 Lab ID:92524499001 Collected:02/24/21 10:25 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 00:19 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 00:19 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 00:19 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 00:19 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 00:19 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 00:19 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 00:19 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 00:19 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 00:19 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 00:19 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 00:19 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 00:19 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 00:19 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 00:19 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 00:19 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 00:19 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 00:19 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 00:19 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 00:19 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 00:19 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 00:19 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 00:19 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 00:19 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 00:19 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 00:19 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 00:19 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 00:19 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 00:19 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 00:19 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 00:19 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 00:19 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 00:19 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 00:19 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 00:19 79-34-51.0 0.22 1
Tetrachloroethene 10.1 ug/L 02/27/21 00:19 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 00:19 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 00:19 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 00:19 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 00:19 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 00:19 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 00:19 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 00:19 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 00:19 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 00:19 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 00:19 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-1 Lab ID:92524499001 Collected:02/24/21 10:25 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 00:19 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 00:19 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 00:19 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)93 %02/27/21 00:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/27/21 00:19 17060-07-070-130 1
Toluene-d8 (S)98 %02/27/21 00:19 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-2 Lab ID:92524499002 Collected:02/24/21 11:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 19:59 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 19:59 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 19:59 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 19:59 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 19:59 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 19:59 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 19:59 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 19:59 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 19:59 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 19:59 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 19:59 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 19:59 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 19:59 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 19:59 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 19:59 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 19:59 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 19:59 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 19:59 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 19:59 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 19:59 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 19:59 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 19:59 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 19:59 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 19:59 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 19:59 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 19:59 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 19:59 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 19:59 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 19:59 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 19:59 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 19:59 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 19:59 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 19:59 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 19:59 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 19:59 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 19:59 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 19:59 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 19:59 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 19:59 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 19:59 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 19:59 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 19:59 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 19:59 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 19:59 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 19:59 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-2 Lab ID:92524499002 Collected:02/24/21 11:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 19:59 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 19:59 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 19:59 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 19:59 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 19:59 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 19:59 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 19:59 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 19:59 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 19:59 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 19:59 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 19:59 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 19:59 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 19:59 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 19:59 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 19:59 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 19:59 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 19:59 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 19:59 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 19:59 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 19:59 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 19:59 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 19:59 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 19:59 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)68 %03/02/21 19:59 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)66 %03/02/21 19:59 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)95 %03/02/21 19:59 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)34 %03/02/21 19:59 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)46 %03/02/21 19:59 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)75 %03/02/21 19:59 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/27/21 00:38 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 00:38 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 00:38 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 00:38 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 00:38 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 00:38 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 00:38 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 00:38 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 00:38 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 00:38 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 00:38 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 00:38 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-2 Lab ID:92524499002 Collected:02/24/21 11:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 00:38 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 00:38 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 00:38 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 00:38 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 00:38 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 00:38 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 00:38 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 00:38 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 00:38 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 00:38 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 00:38 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 00:38 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 00:38 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 00:38 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 2.3 ug/L 02/27/21 00:38 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 00:38 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 00:38 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 00:38 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 00:38 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 00:38 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 00:38 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 00:38 10061-02-61.0 0.31 1
Diisopropyl ether 0.23J ug/L 02/27/21 00:38 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 00:38 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 00:38 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 00:38 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 00:38 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 00:38 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 00:38 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 00:38 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 00:38 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 00:38 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 00:38 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 00:38 79-34-51.0 0.22 1
Tetrachloroethene 78.2 ug/L 02/27/21 00:38 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 00:38 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 00:38 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 00:38 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 00:38 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 00:38 79-00-51.0 0.24 1
Trichloroethene 2.6 ug/L 02/27/21 00:38 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 00:38 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 00:38 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 00:38 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 00:38 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-2 Lab ID:92524499002 Collected:02/24/21 11:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 00:38 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 00:38 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 00:38 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)94 %02/27/21 00:38 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/27/21 00:38 17060-07-070-130 1
Toluene-d8 (S)99 %02/27/21 00:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-3 Lab ID:92524499003 Collected:02/24/21 11:45 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 20:24 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 20:24 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 20:24 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 20:24 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 20:24 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 20:24 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 20:24 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 20:24 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 20:24 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 20:24 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 20:24 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 20:24 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 20:24 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 20:24 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 20:24 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 20:24 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 20:24 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 20:24 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 20:24 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 20:24 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 20:24 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 20:24 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 20:24 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 20:24 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 20:24 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 20:24 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 20:24 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 20:24 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 20:24 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 20:24 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 20:24 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 20:24 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 20:24 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 20:24 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 20:24 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 20:24 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 20:24 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 20:24 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 20:24 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 20:24 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 20:24 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 20:24 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 20:24 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 20:24 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 20:24 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-3 Lab ID:92524499003 Collected:02/24/21 11:45 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 20:24 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 20:24 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 20:24 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 20:24 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 20:24 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 20:24 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 20:24 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 20:24 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 20:24 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 20:24 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 20:24 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 20:24 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 20:24 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 20:24 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 20:24 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 20:24 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 20:24 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 20:24 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 20:24 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 20:24 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 20:24 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 20:24 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 20:24 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)60 %03/02/21 20:24 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)58 %03/02/21 20:24 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)80 %03/02/21 20:24 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)33 %03/02/21 20:24 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)43 %03/02/21 20:24 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)64 %03/02/21 20:24 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/27/21 00:55 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 00:55 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 00:55 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 00:55 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 00:55 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 00:55 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 00:55 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 00:55 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 00:55 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 00:55 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 00:55 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 00:55 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-3 Lab ID:92524499003 Collected:02/24/21 11:45 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 00:55 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 00:55 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 00:55 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 00:55 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 00:55 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 00:55 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 00:55 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 00:55 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 00:55 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 00:55 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 00:55 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 00:55 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 00:55 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 00:55 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 00:55 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 00:55 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 00:55 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 00:55 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 00:55 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 00:55 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 00:55 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 00:55 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 00:55 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 00:55 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 00:55 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 00:55 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 00:55 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 00:55 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 00:55 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 00:55 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 00:55 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 00:55 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 00:55 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 00:55 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 00:55 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 00:55 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 00:55 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 00:55 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 00:55 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 00:55 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 00:55 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 00:55 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 00:55 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 00:55 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 00:55 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-3 Lab ID:92524499003 Collected:02/24/21 11:45 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 00:55 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 00:55 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 00:55 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/21 00:55 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/27/21 00:55 17060-07-070-130 1
Toluene-d8 (S)99 %02/27/21 00:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-4 Lab ID:92524499004 Collected:02/24/21 12:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 17:28 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 17:28 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 17:28 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 17:28 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 17:28 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 17:28 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 17:28 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 17:28 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 17:28 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 17:28 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 17:28 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 17:28 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 17:28 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 17:28 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 17:28 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 17:28 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 17:28 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 17:28 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 17:28 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 17:28 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 17:28 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 17:28 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 17:28 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 17:28 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 17:28 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 17:28 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 17:28 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 17:28 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 17:28 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 17:28 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 17:28 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 17:28 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 17:28 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 17:28 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 17:28 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 17:28 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 17:28 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 17:28 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 17:28 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 17:28 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 17:28 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 17:28 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 17:28 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 17:28 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 17:28 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-4 Lab ID:92524499004 Collected:02/24/21 12:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 17:28 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 17:28 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 17:28 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 17:28 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 17:28 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 17:28 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 17:28 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 17:28 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 17:28 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 17:28 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 17:28 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 17:28 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 17:28 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 17:28 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 17:28 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 17:28 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 17:28 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 17:28 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 17:28 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 17:28 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 17:28 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 17:28 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 17:28 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)63 %03/02/21 17:28 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)60 %03/02/21 17:28 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)106 %03/02/21 17:28 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)35 %03/02/21 17:28 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)45 %03/02/21 17:28 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)66 %03/02/21 17:28 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 48.8 ug/L 02/27/21 01:14 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 01:14 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 01:14 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 01:14 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 01:14 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 01:14 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 01:14 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 01:14 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 01:14 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 01:14 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 01:14 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 01:14 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-4 Lab ID:92524499004 Collected:02/24/21 12:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 01:14 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 01:14 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 01:14 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 01:14 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 01:14 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 01:14 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 01:14 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 01:14 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 01:14 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 01:14 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 01:14 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 01:14 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 01:14 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 01:14 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 01:14 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 01:14 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 01:14 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 01:14 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 01:14 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 01:14 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 01:14 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 01:14 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 01:14 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 01:14 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 01:14 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 01:14 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 01:14 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 01:14 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 01:14 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 01:14 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 01:14 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 01:14 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 01:14 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 01:14 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 01:14 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 01:14 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 01:14 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 01:14 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 01:14 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 01:14 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 01:14 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 01:14 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 01:14 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 01:14 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 01:14 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-4 Lab ID:92524499004 Collected:02/24/21 12:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 01:14 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 01:14 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 01:14 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/21 01:14 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/27/21 01:14 17060-07-070-130 1
Toluene-d8 (S)101 %02/27/21 01:14 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-5 Lab ID:92524499005 Collected:02/24/21 13:10 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 17:53 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 17:53 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 17:53 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 17:53 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 17:53 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 17:53 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 17:53 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 17:53 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 17:53 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 17:53 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 17:53 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 17:53 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 17:53 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 17:53 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 17:53 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 17:53 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 17:53 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 17:53 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 17:53 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 17:53 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 17:53 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 17:53 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 17:53 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 17:53 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 17:53 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 17:53 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 17:53 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 17:53 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 17:53 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 17:53 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 17:53 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 17:53 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 17:53 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 17:53 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 17:53 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 17:53 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 17:53 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 17:53 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 17:53 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 17:53 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 17:53 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 17:53 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 17:53 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 17:53 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 17:53 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-5 Lab ID:92524499005 Collected:02/24/21 13:10 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 17:53 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 17:53 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 17:53 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 17:53 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 17:53 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 17:53 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 17:53 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 17:53 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 17:53 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 17:53 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 17:53 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 17:53 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 17:53 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 17:53 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 17:53 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 17:53 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 17:53 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 17:53 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 17:53 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 17:53 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 17:53 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 17:53 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 17:53 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)75 %03/02/21 17:53 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)71 %03/02/21 17:53 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)110 %03/02/21 17:53 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)45 %03/02/21 17:53 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)53 %03/02/21 17:53 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)74 %03/02/21 17:53 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 15.6J ug/L 02/27/21 01:32 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 01:32 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 01:32 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 01:32 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 01:32 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 01:32 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 01:32 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 01:32 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 01:32 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 01:32 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 01:32 75-00-31.0 0.49 1
Chloroform 5.0 ug/L 02/27/21 01:32 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-5 Lab ID:92524499005 Collected:02/24/21 13:10 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 01:32 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 01:32 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 01:32 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 01:32 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 01:32 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 01:32 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 01:32 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 01:32 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 01:32 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 01:32 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 01:32 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 01:32 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 01:32 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 01:32 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 1.7 ug/L 02/27/21 01:32 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 01:32 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 01:32 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 01:32 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 01:32 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 01:32 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 01:32 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 01:32 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 01:32 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 01:32 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 01:32 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 01:32 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 01:32 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 01:32 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 01:32 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 01:32 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 01:32 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 01:32 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 01:32 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 01:32 79-34-51.0 0.22 1
Tetrachloroethene 69.0 ug/L 02/27/21 01:32 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 01:32 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 01:32 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 01:32 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 01:32 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 01:32 79-00-51.0 0.24 1
Trichloroethene 1.6 ug/L 02/27/21 01:32 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 01:32 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 01:32 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 01:32 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 01:32 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-5 Lab ID:92524499005 Collected:02/24/21 13:10 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 01:32 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 01:32 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 01:32 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/21 01:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/27/21 01:32 17060-07-070-130 1
Toluene-d8 (S)101 %02/27/21 01:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-6 Lab ID:92524499006 Collected:02/24/21 13:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 18:19 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 18:19 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 18:19 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 18:19 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 18:19 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 18:19 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 18:19 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 18:19 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 18:19 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 18:19 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 18:19 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 18:19 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 18:19 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 18:19 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 18:19 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 18:19 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 18:19 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 18:19 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 18:19 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 18:19 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 18:19 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 18:19 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 18:19 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 18:19 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 18:19 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 18:19 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 18:19 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 18:19 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 18:19 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 18:19 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 18:19 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 18:19 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 18:19 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 18:19 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 18:19 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 18:19 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 18:19 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 18:19 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 18:19 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 18:19 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 18:19 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 18:19 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 18:19 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 18:19 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 18:19 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-6 Lab ID:92524499006 Collected:02/24/21 13:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 18:19 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 18:19 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 18:19 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 18:19 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 18:19 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 18:19 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 18:19 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 18:19 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 18:19 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 18:19 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 18:19 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 18:19 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 18:19 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 18:19 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 18:19 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 18:19 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 18:19 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 18:19 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 18:19 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 18:19 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 18:19 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 18:19 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 18:19 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)66 %03/02/21 18:19 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)65 %03/02/21 18:19 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)103 %03/02/21 18:19 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)35 %03/02/21 18:19 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)44 %03/02/21 18:19 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)62 %03/02/21 18:19 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 18.1J ug/L 02/27/21 01:50 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 01:50 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 01:50 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 01:50 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 01:50 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 01:50 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 01:50 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 01:50 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 01:50 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 01:50 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 01:50 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 01:50 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-6 Lab ID:92524499006 Collected:02/24/21 13:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 01:50 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 01:50 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 01:50 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 01:50 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 01:50 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 01:50 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 01:50 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 01:50 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 01:50 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 01:50 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 01:50 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 01:50 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 01:50 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 01:50 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 01:50 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 01:50 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 01:50 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 01:50 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 01:50 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 01:50 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 01:50 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 01:50 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 01:50 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 01:50 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 01:50 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 01:50 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 01:50 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 01:50 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 01:50 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 01:50 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 01:50 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 01:50 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 01:50 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 01:50 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 01:50 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 01:50 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 01:50 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 01:50 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 01:50 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 01:50 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 01:50 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 01:50 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 01:50 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 01:50 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 01:50 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-6 Lab ID:92524499006 Collected:02/24/21 13:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 01:50 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 01:50 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 01:50 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/21 01:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)97 %02/27/21 01:50 17060-07-070-130 1
Toluene-d8 (S)102 %02/27/21 01:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-7 Lab ID:92524499007 Collected:02/24/21 14:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 18:44 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 18:44 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 18:44 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 18:44 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 18:44 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 18:44 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 18:44 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 18:44 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 18:44 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 18:44 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 18:44 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 18:44 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 18:44 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 18:44 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 18:44 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 18:44 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 18:44 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 18:44 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 18:44 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 18:44 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 18:44 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 18:44 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 18:44 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 18:44 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 18:44 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 18:44 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 18:44 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 18:44 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 18:44 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 18:44 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 18:44 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 18:44 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 18:44 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 18:44 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 18:44 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 18:44 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 18:44 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 18:44 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 18:44 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 18:44 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 18:44 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 18:44 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 18:44 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 18:44 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 18:44 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-7 Lab ID:92524499007 Collected:02/24/21 14:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 18:44 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 18:44 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 18:44 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 18:44 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 18:44 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 18:44 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 18:44 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 18:44 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 18:44 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 18:44 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 18:44 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 18:44 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 18:44 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 18:44 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 18:44 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 18:44 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 18:44 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 18:44 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 18:44 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 18:44 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 18:44 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 18:44 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 18:44 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)60 %03/02/21 18:44 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)53 %03/02/21 18:44 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)98 %03/02/21 18:44 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)32 %03/02/21 18:44 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)41 %03/02/21 18:44 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)55 %03/02/21 18:44 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 19.2J ug/L 02/27/21 02:08 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 02:08 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 02:08 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 02:08 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 02:08 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 02:08 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 02:08 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 02:08 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 02:08 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 02:08 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 02:08 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 02:08 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-7 Lab ID:92524499007 Collected:02/24/21 14:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 02:08 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 02:08 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 02:08 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 02:08 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 02:08 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 02:08 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 02:08 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 02:08 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 02:08 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 02:08 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 02:08 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 02:08 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 02:08 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 02:08 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 02:08 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 02:08 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 02:08 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 02:08 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 02:08 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 02:08 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 02:08 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 02:08 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 02:08 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 02:08 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 02:08 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 02:08 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 02:08 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 02:08 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 02:08 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 02:08 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 02:08 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 02:08 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 02:08 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 02:08 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 02:08 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 02:08 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 02:08 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 02:08 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 02:08 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 02:08 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 02:08 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 02:08 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 02:08 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 02:08 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 02:08 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-7 Lab ID:92524499007 Collected:02/24/21 14:40 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 02:08 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 02:08 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 02:08 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/21 02:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %02/27/21 02:08 17060-07-070-130 1
Toluene-d8 (S)99 %02/27/21 02:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-8 Lab ID:92524499008 Collected:02/24/21 15:15 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 19:09 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 19:09 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 19:09 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 19:09 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 19:09 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 19:09 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 19:09 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 19:09 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 19:09 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 19:09 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 19:09 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 19:09 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 19:09 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 19:09 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 19:09 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 19:09 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 19:09 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 19:09 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 19:09 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 19:09 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 19:09 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 19:09 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 19:09 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 19:09 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 19:09 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 19:09 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 19:09 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 19:09 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 19:09 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 19:09 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 19:09 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 19:09 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 19:09 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 19:09 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 19:09 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 19:09 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 19:09 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 19:09 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 19:09 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 19:09 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 19:09 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 19:09 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 19:09 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 19:09 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 19:09 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-8 Lab ID:92524499008 Collected:02/24/21 15:15 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 19:09 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 19:09 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 19:09 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 19:09 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 19:09 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 19:09 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 19:09 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 19:09 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 19:09 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 19:09 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 19:09 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 19:09 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 19:09 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 19:09 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 19:09 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 19:09 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 19:09 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 19:09 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 19:09 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 19:09 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 19:09 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 19:09 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 19:09 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)83 %03/02/21 19:09 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)80 %03/02/21 19:09 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)122 %03/02/21 19:09 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)49 %03/02/21 19:09 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)54 %03/02/21 19:09 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)77 %03/02/21 19:09 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/27/21 02:26 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 02:26 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 02:26 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 02:26 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 02:26 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 02:26 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 02:26 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 02:26 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 02:26 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 02:26 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 02:26 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 02:26 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-8 Lab ID:92524499008 Collected:02/24/21 15:15 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 02:26 74-87-3 v21.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 02:26 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 02:26 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 02:26 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 02:26 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 02:26 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 02:26 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 02:26 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 02:26 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 02:26 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 02:26 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 02:26 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 02:26 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 02:26 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 02:26 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 02:26 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 02:26 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 02:26 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 02:26 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 02:26 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 02:26 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 02:26 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 02:26 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 02:26 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 02:26 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 02:26 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 02:26 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 02:26 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 02:26 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 02:26 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 02:26 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 02:26 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 02:26 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 02:26 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 02:26 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 02:26 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 02:26 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 02:26 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 02:26 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 02:26 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 02:26 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 02:26 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 02:26 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 02:26 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 02:26 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-8 Lab ID:92524499008 Collected:02/24/21 15:15 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 02:26 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 02:26 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 02:26 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/21 02:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %02/27/21 02:26 17060-07-070-130 1
Toluene-d8 (S)100 %02/27/21 02:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-9 Lab ID:92524499009 Collected:02/25/21 10:05 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 19:34 83-32-903/02/21 14:4350.0 10.0 1
Acenaphthylene ND ug/L 03/02/21 19:34 208-96-803/02/21 14:4350.0 9.8 1
Aniline ND ug/L 03/02/21 19:34 62-53-303/02/21 14:4350.0 8.2 1
Anthracene ND ug/L 03/02/21 19:34 120-12-703/02/21 14:4350.0 11.6 1
Benzo(a)anthracene ND ug/L 03/02/21 19:34 56-55-303/02/21 14:4350.0 13.4 1
Benzo(a)pyrene ND ug/L 03/02/21 19:34 50-32-803/02/21 14:4350.0 13.9 1
Benzo(b)fluoranthene ND ug/L 03/02/21 19:34 205-99-203/02/21 14:4350.0 13.0 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 19:34 191-24-203/02/21 14:4350.0 14.2 1
Benzo(k)fluoranthene ND ug/L 03/02/21 19:34 207-08-903/02/21 14:4350.0 13.6 1
Benzoic Acid ND ug/L 03/02/21 19:34 65-85-003/02/21 14:4325017.0 1
Benzyl alcohol ND ug/L 03/02/21 19:34 100-51-603/02/21 14:4310014.5 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 19:34 101-55-303/02/21 14:4350.0 8.8 1
Butylbenzylphthalate ND ug/L 03/02/21 19:34 85-68-703/02/21 14:4350.0 15.7 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 19:34 59-50-703/02/21 14:4350.0 16.7 1
4-Chloroaniline ND ug/L 03/02/21 19:34 106-47-803/02/21 14:4310018.2 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 19:34 111-91-103/02/21 14:4350.0 9.1 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 19:34 111-44-403/02/21 14:4350.0 9.6 1
2-Chloronaphthalene ND ug/L 03/02/21 19:34 91-58-703/02/21 14:4350.0 8.6 1
2-Chlorophenol ND ug/L 03/02/21 19:34 95-57-803/02/21 14:4350.0 6.0 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 19:34 7005-72-303/02/21 14:4350.0 10.0 1
Chrysene ND ug/L 03/02/21 19:34 218-01-903/02/21 14:4350.0 13.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 19:34 53-70-303/02/21 14:4350.0 14.8 1
Dibenzofuran ND ug/L 03/02/21 19:34 132-64-903/02/21 14:4350.0 10.5 1
1,2-Dichlorobenzene ND ug/L 03/02/21 19:34 95-50-103/02/21 14:4350.0 9.0 1
1,3-Dichlorobenzene ND ug/L 03/02/21 19:34 541-73-103/02/21 14:4350.0 8.0 1
1,4-Dichlorobenzene ND ug/L 03/02/21 19:34 106-46-703/02/21 14:4350.0 8.4 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 19:34 91-94-103/02/21 14:4310040.6 1
2,4-Dichlorophenol ND ug/L 03/02/21 19:34 120-83-203/02/21 14:4350.0 7.0 1
Diethylphthalate ND ug/L 03/02/21 19:34 84-66-203/02/21 14:4350.0 10.2 1
2,4-Dimethylphenol ND ug/L 03/02/21 19:34 105-67-903/02/21 14:4350.0 8.5 1
Dimethylphthalate ND ug/L 03/02/21 19:34 131-11-303/02/21 14:4350.0 10.6 1
Di-n-butylphthalate ND ug/L 03/02/21 19:34 84-74-203/02/21 14:4350.0 11.0 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 19:34 534-52-103/02/21 14:4310017.0 1
2,4-Dinitrophenol ND ug/L 03/02/21 19:34 51-28-503/02/21 14:432501301
2,4-Dinitrotoluene ND ug/L 03/02/21 19:34 121-14-203/02/21 14:4350.0 8.1 1
2,6-Dinitrotoluene ND ug/L 03/02/21 19:34 606-20-203/02/21 14:4350.0 8.6 1
Di-n-octylphthalate ND ug/L 03/02/21 19:34 117-84-003/02/21 14:4350.0 19.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 19:34 117-81-703/02/21 14:4330.0 18.6 1
Fluoranthene ND ug/L 03/02/21 19:34 206-44-003/02/21 14:4350.0 11.0 1
Fluorene ND ug/L 03/02/21 19:34 86-73-703/02/21 14:4350.0 10.4 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 19:34 87-68-303/02/21 14:4350.0 8.8 1
Hexachlorobenzene ND ug/L 03/02/21 19:34 118-74-103/02/21 14:4350.0 10.8 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 19:34 77-47-403/02/21 14:4350.0 8.0 1
Hexachloroethane ND ug/L 03/02/21 19:34 67-72-103/02/21 14:4350.0 6.9 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 19:34 193-39-503/02/21 14:4350.0 14.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-9 Lab ID:92524499009 Collected:02/25/21 10:05 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 19:34 78-59-103/02/21 14:4350.0 8.3 1
1-Methylnaphthalene ND ug/L 03/02/21 19:34 90-12-003/02/21 14:4350.0 10.2 1
2-Methylnaphthalene ND ug/L 03/02/21 19:34 91-57-603/02/21 14:4350.0 9.4 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 19:34 95-48-703/02/21 14:4350.0 9.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 19:34 15831-10-403/02/21 14:4350.0 6.1 1
Naphthalene ND ug/L 03/02/21 19:34 91-20-303/02/21 14:4350.0 10.4 1
2-Nitroaniline ND ug/L 03/02/21 19:34 88-74-403/02/21 14:4310014.9 1
3-Nitroaniline ND ug/L 03/02/21 19:34 99-09-203/02/21 14:4310018.8 1
4-Nitroaniline ND ug/L 03/02/21 19:34 100-01-603/02/21 14:4310025.5 1
Nitrobenzene ND ug/L 03/02/21 19:34 98-95-303/02/21 14:4350.0 9.4 1
2-Nitrophenol ND ug/L 03/02/21 19:34 88-75-503/02/21 14:4350.0 7.0 1
4-Nitrophenol ND ug/L 03/02/21 19:34 100-02-703/02/21 14:4325033.0 1
N-Nitrosodimethylamine ND ug/L 03/02/21 19:34 62-75-903/02/21 14:4350.0 9.4 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 19:34 621-64-703/02/21 14:4350.0 6.6 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 19:34 86-30-603/02/21 14:4350.0 15.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 19:34 108-60-103/02/21 14:4350.0 5.8 1
Pentachlorophenol ND ug/L 03/02/21 19:34 87-86-503/02/21 14:4310018.8 1
Phenanthrene ND ug/L 03/02/21 19:34 85-01-803/02/21 14:4350.0 10.0 1
Phenol ND ug/L 03/02/21 19:34 108-95-203/02/21 14:4350.0 6.8 1
Pyrene ND ug/L 03/02/21 19:34 129-00-003/02/21 14:4350.0 11.0 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 19:34 120-82-103/02/21 14:4350.0 8.6 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 19:34 95-95-403/02/21 14:4350.0 7.1 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 19:34 88-06-203/02/21 14:4350.0 7.8 1
Surrogates
Nitrobenzene-d5 (S)67 %03/02/21 19:34 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)62 %03/02/21 19:34 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)118 %03/02/21 19:34 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)43 %03/02/21 19:34 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)51 %03/02/21 19:34 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)73 %03/02/21 19:34 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/27/21 02:44 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 02:44 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 02:44 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 02:44 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 02:44 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 02:44 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 02:44 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 02:44 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 02:44 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 02:44 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 02:44 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 02:44 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-9 Lab ID:92524499009 Collected:02/25/21 10:05 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 02:44 74-87-3 v2,v31.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 02:44 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 02:44 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 02:44 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 02:44 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 02:44 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 02:44 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 02:44 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 02:44 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 02:44 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 02:44 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 02:44 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 02:44 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 02:44 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 02:44 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 02:44 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 02:44 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 02:44 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 02:44 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 02:44 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 02:44 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 02:44 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 02:44 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 02:44 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 02:44 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 02:44 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 02:44 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 02:44 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 02:44 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 02:44 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 02:44 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 02:44 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 02:44 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 02:44 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 02:44 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 02:44 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 02:44 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 02:44 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 02:44 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 02:44 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 02:44 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 02:44 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 02:44 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 02:44 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 02:44 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-9 Lab ID:92524499009 Collected:02/25/21 10:05 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 02:44 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 02:44 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 02:44 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %02/27/21 02:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %02/27/21 02:44 17060-07-070-130 1
Toluene-d8 (S)102 %02/27/21 02:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-10 Lab ID:92524499010 Collected:02/25/21 16:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 19:59 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 19:59 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 19:59 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 19:59 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 19:59 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 19:59 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 19:59 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 19:59 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 19:59 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 19:59 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 19:59 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 19:59 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 19:59 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 19:59 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 19:59 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 19:59 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 19:59 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 19:59 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 19:59 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 19:59 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 19:59 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 19:59 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 19:59 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 19:59 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 19:59 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 19:59 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 19:59 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 19:59 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 19:59 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 19:59 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 19:59 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 19:59 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 19:59 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 19:59 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 19:59 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 19:59 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 19:59 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 19:59 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 19:59 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 19:59 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 19:59 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 19:59 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 19:59 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 19:59 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 19:59 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-10 Lab ID:92524499010 Collected:02/25/21 16:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 19:59 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 19:59 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 19:59 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 19:59 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 19:59 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 19:59 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 19:59 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 19:59 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 19:59 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 19:59 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 19:59 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 19:59 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 19:59 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 19:59 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 19:59 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 19:59 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 19:59 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 19:59 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 19:59 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 19:59 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 19:59 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 19:59 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 19:59 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)69 %03/02/21 19:59 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)69 %03/02/21 19:59 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)102 %03/02/21 19:59 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)54 %03/02/21 19:59 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)58 %03/02/21 19:59 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)86 %03/02/21 19:59 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/27/21 15:49 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 15:49 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 15:49 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 15:49 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 15:49 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 15:49 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 15:49 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 15:49 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 15:49 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 15:49 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 15:49 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 15:49 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-10 Lab ID:92524499010 Collected:02/25/21 16:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 15:49 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 15:49 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 15:49 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 15:49 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 15:49 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 15:49 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 15:49 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 15:49 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 15:49 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 15:49 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 15:49 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 15:49 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 15:49 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 15:49 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 15:49 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 15:49 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 15:49 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 15:49 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 15:49 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 15:49 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 15:49 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 15:49 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 15:49 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 15:49 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 15:49 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 15:49 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 15:49 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 15:49 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 15:49 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 15:49 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 15:49 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 15:49 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 15:49 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 15:49 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 15:49 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 15:49 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 15:49 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 15:49 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 15:49 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 15:49 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 15:49 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 15:49 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 15:49 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 15:49 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 15:49 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-10 Lab ID:92524499010 Collected:02/25/21 16:20 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 15:49 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 15:49 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 15:49 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)101 %02/27/21 15:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %02/27/21 15:49 17060-07-070-130 1
Toluene-d8 (S)101 %02/27/21 15:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-14 Lab ID:92524499011 Collected:02/25/21 13:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 20:25 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 20:25 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 20:25 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 20:25 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 20:25 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 20:25 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 20:25 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 20:25 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 20:25 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 20:25 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 20:25 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 20:25 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 20:25 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 20:25 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 20:25 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 20:25 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 20:25 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 20:25 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 20:25 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 20:25 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 20:25 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 20:25 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 20:25 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 20:25 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 20:25 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 20:25 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 20:25 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 20:25 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 20:25 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 20:25 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 20:25 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 20:25 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 20:25 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 20:25 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 20:25 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 20:25 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 20:25 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 20:25 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 20:25 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 20:25 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 20:25 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 20:25 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 20:25 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 20:25 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 20:25 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-14 Lab ID:92524499011 Collected:02/25/21 13:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 20:25 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 20:25 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 20:25 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 20:25 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 20:25 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 20:25 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 20:25 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 20:25 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 20:25 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 20:25 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 20:25 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 20:25 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 20:25 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 20:25 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 20:25 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 20:25 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 20:25 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 20:25 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 20:25 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 20:25 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 20:25 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 20:25 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 20:25 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)60 %03/02/21 20:25 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)56 %03/02/21 20:25 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)92 %03/02/21 20:25 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)34 %03/02/21 20:25 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)43 %03/02/21 20:25 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)60 %03/02/21 20:25 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 02/27/21 16:08 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 16:08 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 16:08 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 16:08 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 16:08 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 16:08 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 16:08 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 16:08 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 16:08 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 16:08 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 16:08 75-00-31.0 0.49 1
Chloroform ND ug/L 02/27/21 16:08 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-14 Lab ID:92524499011 Collected:02/25/21 13:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 16:08 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 16:08 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 16:08 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 16:08 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 16:08 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 16:08 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 16:08 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 16:08 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 16:08 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 16:08 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 16:08 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 16:08 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 16:08 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 16:08 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 02/27/21 16:08 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 16:08 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 16:08 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 16:08 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 16:08 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 16:08 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 16:08 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 16:08 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 16:08 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 16:08 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 16:08 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 16:08 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 16:08 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 16:08 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 16:08 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 02/27/21 16:08 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 16:08 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 16:08 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 16:08 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 16:08 79-34-51.0 0.22 1
Tetrachloroethene ND ug/L 02/27/21 16:08 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 16:08 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 16:08 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 16:08 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 16:08 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 16:08 79-00-51.0 0.24 1
Trichloroethene ND ug/L 02/27/21 16:08 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 16:08 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 16:08 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 16:08 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 16:08 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-14 Lab ID:92524499011 Collected:02/25/21 13:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 16:08 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 16:08 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 16:08 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)102 %02/27/21 16:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %02/27/21 16:08 17060-07-070-130 1
Toluene-d8 (S)101 %02/27/21 16:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-12 Lab ID:92524499012 Collected:02/25/21 11:55 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 20:50 83-32-903/02/21 14:4320.0 4.0 1
Acenaphthylene ND ug/L 03/02/21 20:50 208-96-803/02/21 14:4320.0 3.9 1
Aniline ND ug/L 03/02/21 20:50 62-53-303/02/21 14:4320.0 3.3 1
Anthracene ND ug/L 03/02/21 20:50 120-12-703/02/21 14:4320.0 4.6 1
Benzo(a)anthracene ND ug/L 03/02/21 20:50 56-55-303/02/21 14:4320.0 5.4 1
Benzo(a)pyrene ND ug/L 03/02/21 20:50 50-32-803/02/21 14:4320.0 5.6 1
Benzo(b)fluoranthene ND ug/L 03/02/21 20:50 205-99-203/02/21 14:4320.0 5.2 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 20:50 191-24-203/02/21 14:4320.0 5.7 1
Benzo(k)fluoranthene ND ug/L 03/02/21 20:50 207-08-903/02/21 14:4320.0 5.4 1
Benzoic Acid ND ug/L 03/02/21 20:50 65-85-003/02/21 14:431006.8 1
Benzyl alcohol ND ug/L 03/02/21 20:50 100-51-603/02/21 14:4340.0 5.8 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 20:50 101-55-303/02/21 14:4320.0 3.5 1
Butylbenzylphthalate ND ug/L 03/02/21 20:50 85-68-703/02/21 14:4320.0 6.3 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 20:50 59-50-703/02/21 14:4320.0 6.7 1
4-Chloroaniline ND ug/L 03/02/21 20:50 106-47-803/02/21 14:4340.0 7.3 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 20:50 111-91-103/02/21 14:4320.0 3.6 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 20:50 111-44-403/02/21 14:4320.0 3.8 1
2-Chloronaphthalene ND ug/L 03/02/21 20:50 91-58-703/02/21 14:4320.0 3.4 1
2-Chlorophenol ND ug/L 03/02/21 20:50 95-57-803/02/21 14:4320.0 2.4 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 20:50 7005-72-303/02/21 14:4320.0 4.0 1
Chrysene ND ug/L 03/02/21 20:50 218-01-903/02/21 14:4320.0 5.5 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 20:50 53-70-303/02/21 14:4320.0 5.9 1
Dibenzofuran ND ug/L 03/02/21 20:50 132-64-903/02/21 14:4320.0 4.2 1
1,2-Dichlorobenzene ND ug/L 03/02/21 20:50 95-50-103/02/21 14:4320.0 3.6 1
1,3-Dichlorobenzene ND ug/L 03/02/21 20:50 541-73-103/02/21 14:4320.0 3.2 1
1,4-Dichlorobenzene ND ug/L 03/02/21 20:50 106-46-703/02/21 14:4320.0 3.3 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 20:50 91-94-103/02/21 14:4340.0 16.2 1
2,4-Dichlorophenol ND ug/L 03/02/21 20:50 120-83-203/02/21 14:4320.0 2.8 1
Diethylphthalate ND ug/L 03/02/21 20:50 84-66-203/02/21 14:4320.0 4.1 1
2,4-Dimethylphenol ND ug/L 03/02/21 20:50 105-67-903/02/21 14:4320.0 3.4 1
Dimethylphthalate ND ug/L 03/02/21 20:50 131-11-303/02/21 14:4320.0 4.3 1
Di-n-butylphthalate ND ug/L 03/02/21 20:50 84-74-203/02/21 14:4320.0 4.4 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 20:50 534-52-103/02/21 14:4340.0 6.8 1
2,4-Dinitrophenol ND ug/L 03/02/21 20:50 51-28-503/02/21 14:4310052.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 20:50 121-14-203/02/21 14:4320.0 3.2 1
2,6-Dinitrotoluene ND ug/L 03/02/21 20:50 606-20-203/02/21 14:4320.0 3.4 1
Di-n-octylphthalate ND ug/L 03/02/21 20:50 117-84-003/02/21 14:4320.0 7.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 20:50 117-81-703/02/21 14:4312.0 7.5 1
Fluoranthene ND ug/L 03/02/21 20:50 206-44-003/02/21 14:4320.0 4.4 1
Fluorene ND ug/L 03/02/21 20:50 86-73-703/02/21 14:4320.0 4.2 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 20:50 87-68-303/02/21 14:4320.0 3.5 1
Hexachlorobenzene ND ug/L 03/02/21 20:50 118-74-103/02/21 14:4320.0 4.3 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 20:50 77-47-403/02/21 14:4320.0 3.2 1
Hexachloroethane ND ug/L 03/02/21 20:50 67-72-103/02/21 14:4320.0 2.8 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 20:50 193-39-503/02/21 14:4320.0 5.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-12 Lab ID:92524499012 Collected:02/25/21 11:55 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 20:50 78-59-103/02/21 14:4320.0 3.3 1
1-Methylnaphthalene ND ug/L 03/02/21 20:50 90-12-003/02/21 14:4320.0 4.1 1
2-Methylnaphthalene ND ug/L 03/02/21 20:50 91-57-603/02/21 14:4320.0 3.7 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 20:50 95-48-703/02/21 14:4320.0 3.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 20:50 15831-10-403/02/21 14:4320.0 2.4 1
Naphthalene ND ug/L 03/02/21 20:50 91-20-303/02/21 14:4320.0 4.2 1
2-Nitroaniline ND ug/L 03/02/21 20:50 88-74-403/02/21 14:4340.0 6.0 1
3-Nitroaniline ND ug/L 03/02/21 20:50 99-09-203/02/21 14:4340.0 7.5 1
4-Nitroaniline ND ug/L 03/02/21 20:50 100-01-603/02/21 14:4340.0 10.2 1
Nitrobenzene ND ug/L 03/02/21 20:50 98-95-303/02/21 14:4320.0 3.7 1
2-Nitrophenol ND ug/L 03/02/21 20:50 88-75-503/02/21 14:4320.0 2.8 1
4-Nitrophenol ND ug/L 03/02/21 20:50 100-02-703/02/21 14:4310013.2 1
N-Nitrosodimethylamine ND ug/L 03/02/21 20:50 62-75-903/02/21 14:4320.0 3.8 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 20:50 621-64-703/02/21 14:4320.0 2.7 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 20:50 86-30-603/02/21 14:4320.0 6.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 20:50 108-60-103/02/21 14:4320.0 2.3 1
Pentachlorophenol ND ug/L 03/02/21 20:50 87-86-503/02/21 14:4340.0 7.5 1
Phenanthrene ND ug/L 03/02/21 20:50 85-01-803/02/21 14:4320.0 4.0 1
Phenol ND ug/L 03/02/21 20:50 108-95-203/02/21 14:4320.0 2.7 1
Pyrene ND ug/L 03/02/21 20:50 129-00-003/02/21 14:4320.0 4.4 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 20:50 120-82-103/02/21 14:4320.0 3.5 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 20:50 95-95-403/02/21 14:4320.0 2.8 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 20:50 88-06-203/02/21 14:4320.0 3.1 1
Surrogates
Nitrobenzene-d5 (S)84 %03/02/21 20:50 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)78 %03/02/21 20:50 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)139 %03/02/21 20:50 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)44 %03/02/21 20:50 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)55 %03/02/21 20:50 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)99 %03/02/21 20:50 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 14.5J ug/L 03/01/21 12:15 67-64-1 v125.0 6.2 1
Benzene ND ug/L 03/01/21 12:15 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/01/21 12:15 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 03/01/21 12:15 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/01/21 12:15 75-27-41.0 0.26 1
Bromoform ND ug/L 03/01/21 12:15 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/01/21 12:15 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 03/01/21 12:15 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/01/21 12:15 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/01/21 12:15 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/01/21 12:15 75-00-31.0 0.49 1
Chloroform ND ug/L 03/01/21 12:15 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-12 Lab ID:92524499012 Collected:02/25/21 11:55 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 03/01/21 12:15 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/01/21 12:15 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/01/21 12:15 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/01/21 12:15 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/01/21 12:15 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/01/21 12:15 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/01/21 12:15 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/01/21 12:15 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/01/21 12:15 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/01/21 12:15 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/01/21 12:15 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 03/01/21 12:15 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/01/21 12:15 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/01/21 12:15 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/01/21 12:15 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/01/21 12:15 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/01/21 12:15 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/01/21 12:15 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/01/21 12:15 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 03/01/21 12:15 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/01/21 12:15 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/01/21 12:15 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/01/21 12:15 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/01/21 12:15 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/01/21 12:15 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/01/21 12:15 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/01/21 12:15 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/01/21 12:15 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/01/21 12:15 108-10-15.0 4.5 1
Methyl-tert-butyl ether 40.0 ug/L 03/01/21 12:15 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/01/21 12:15 91-20-3 v11.0 0.35 1
Styrene ND ug/L 03/01/21 12:15 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/01/21 12:15 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/01/21 12:15 79-34-51.0 0.22 1
Tetrachloroethene 10.9 ug/L 03/01/21 12:15 127-18-41.0 0.16 1
Toluene ND ug/L 03/01/21 12:15 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/01/21 12:15 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 03/01/21 12:15 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/01/21 12:15 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/01/21 12:15 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/01/21 12:15 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/01/21 12:15 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/01/21 12:15 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/01/21 12:15 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 03/01/21 12:15 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-12 Lab ID:92524499012 Collected:02/25/21 11:55 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 03/01/21 12:15 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/01/21 12:15 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/01/21 12:15 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)95 %03/01/21 12:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %03/01/21 12:15 17060-07-070-130 1
Toluene-d8 (S)99 %03/01/21 12:15 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-13 Lab ID:92524499013 Collected:02/25/21 13:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/02/21 21:15 83-32-903/02/21 14:4310.0 2.0 1
Acenaphthylene ND ug/L 03/02/21 21:15 208-96-803/02/21 14:4310.0 2.0 1
Aniline ND ug/L 03/02/21 21:15 62-53-303/02/21 14:4310.0 1.6 1
Anthracene ND ug/L 03/02/21 21:15 120-12-703/02/21 14:4310.0 2.3 1
Benzo(a)anthracene ND ug/L 03/02/21 21:15 56-55-303/02/21 14:4310.0 2.7 1
Benzo(a)pyrene ND ug/L 03/02/21 21:15 50-32-803/02/21 14:4310.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/02/21 21:15 205-99-203/02/21 14:4310.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/02/21 21:15 191-24-203/02/21 14:4310.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/02/21 21:15 207-08-903/02/21 14:4310.0 2.7 1
Benzoic Acid ND ug/L 03/02/21 21:15 65-85-003/02/21 14:4350.0 3.4 1
Benzyl alcohol ND ug/L 03/02/21 21:15 100-51-603/02/21 14:4320.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/02/21 21:15 101-55-303/02/21 14:4310.0 1.8 1
Butylbenzylphthalate ND ug/L 03/02/21 21:15 85-68-703/02/21 14:4310.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/02/21 21:15 59-50-703/02/21 14:4310.0 3.3 1
4-Chloroaniline ND ug/L 03/02/21 21:15 106-47-803/02/21 14:4320.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/02/21 21:15 111-91-103/02/21 14:4310.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/02/21 21:15 111-44-403/02/21 14:4310.0 1.9 1
2-Chloronaphthalene ND ug/L 03/02/21 21:15 91-58-703/02/21 14:4310.0 1.7 1
2-Chlorophenol ND ug/L 03/02/21 21:15 95-57-803/02/21 14:4310.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/02/21 21:15 7005-72-303/02/21 14:4310.0 2.0 1
Chrysene ND ug/L 03/02/21 21:15 218-01-903/02/21 14:4310.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/02/21 21:15 53-70-303/02/21 14:4310.0 3.0 1
Dibenzofuran ND ug/L 03/02/21 21:15 132-64-903/02/21 14:4310.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/02/21 21:15 95-50-103/02/21 14:4310.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/02/21 21:15 541-73-103/02/21 14:4310.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/02/21 21:15 106-46-703/02/21 14:4310.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/02/21 21:15 91-94-103/02/21 14:4320.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/02/21 21:15 120-83-203/02/21 14:4310.0 1.4 1
Diethylphthalate ND ug/L 03/02/21 21:15 84-66-203/02/21 14:4310.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/02/21 21:15 105-67-903/02/21 14:4310.0 1.7 1
Dimethylphthalate ND ug/L 03/02/21 21:15 131-11-303/02/21 14:4310.0 2.1 1
Di-n-butylphthalate ND ug/L 03/02/21 21:15 84-74-203/02/21 14:4310.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/02/21 21:15 534-52-103/02/21 14:4320.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/02/21 21:15 51-28-503/02/21 14:4350.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/02/21 21:15 121-14-203/02/21 14:4310.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/02/21 21:15 606-20-203/02/21 14:4310.0 1.7 1
Di-n-octylphthalate ND ug/L 03/02/21 21:15 117-84-003/02/21 14:4310.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/02/21 21:15 117-81-703/02/21 14:436.0 3.7 1
Fluoranthene ND ug/L 03/02/21 21:15 206-44-003/02/21 14:4310.0 2.2 1
Fluorene ND ug/L 03/02/21 21:15 86-73-703/02/21 14:4310.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/02/21 21:15 87-68-303/02/21 14:4310.0 1.8 1
Hexachlorobenzene ND ug/L 03/02/21 21:15 118-74-103/02/21 14:4310.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/02/21 21:15 77-47-403/02/21 14:4310.0 1.6 1
Hexachloroethane ND ug/L 03/02/21 21:15 67-72-103/02/21 14:4310.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/02/21 21:15 193-39-503/02/21 14:4310.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-13 Lab ID:92524499013 Collected:02/25/21 13:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/02/21 21:15 78-59-103/02/21 14:4310.0 1.7 1
1-Methylnaphthalene ND ug/L 03/02/21 21:15 90-12-003/02/21 14:4310.0 2.0 1
2-Methylnaphthalene ND ug/L 03/02/21 21:15 91-57-603/02/21 14:4310.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/02/21 21:15 95-48-703/02/21 14:4310.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/02/21 21:15 15831-10-403/02/21 14:4310.0 1.2 1
Naphthalene ND ug/L 03/02/21 21:15 91-20-303/02/21 14:4310.0 2.1 1
2-Nitroaniline ND ug/L 03/02/21 21:15 88-74-403/02/21 14:4320.0 3.0 1
3-Nitroaniline ND ug/L 03/02/21 21:15 99-09-203/02/21 14:4320.0 3.8 1
4-Nitroaniline ND ug/L 03/02/21 21:15 100-01-603/02/21 14:4320.0 5.1 1
Nitrobenzene ND ug/L 03/02/21 21:15 98-95-303/02/21 14:4310.0 1.9 1
2-Nitrophenol ND ug/L 03/02/21 21:15 88-75-503/02/21 14:4310.0 1.4 1
4-Nitrophenol ND ug/L 03/02/21 21:15 100-02-703/02/21 14:4350.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/02/21 21:15 62-75-903/02/21 14:4310.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/02/21 21:15 621-64-703/02/21 14:4310.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/02/21 21:15 86-30-603/02/21 14:4310.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/02/21 21:15 108-60-103/02/21 14:4310.0 1.2 1
Pentachlorophenol ND ug/L 03/02/21 21:15 87-86-503/02/21 14:4320.0 3.8 1
Phenanthrene ND ug/L 03/02/21 21:15 85-01-803/02/21 14:4310.0 2.0 1
Phenol ND ug/L 03/02/21 21:15 108-95-203/02/21 14:4310.0 1.4 1
Pyrene ND ug/L 03/02/21 21:15 129-00-003/02/21 14:4310.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/02/21 21:15 120-82-103/02/21 14:4310.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/02/21 21:15 95-95-403/02/21 14:4310.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/02/21 21:15 88-06-203/02/21 14:4310.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)67 %03/02/21 21:15 4165-60-003/02/21 14:4310-144 1
2-Fluorobiphenyl (S)60 %03/02/21 21:15 321-60-803/02/21 14:4310-130 1
Terphenyl-d14 (S)124 %03/02/21 21:15 1718-51-003/02/21 14:4334-163 1
Phenol-d6 (S)40 %03/02/21 21:15 13127-88-303/02/21 14:4310-130 1
2-Fluorophenol (S)48 %03/02/21 21:15 367-12-403/02/21 14:4310-130 1
2,4,6-Tribromophenol (S)77 %03/02/21 21:15 118-79-603/02/21 14:4310-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 03/01/21 16:48 67-64-1 v125061.7 10
Benzene 55.9 ug/L 03/01/21 16:48 71-43-210.0 1.5 10
Bromobenzene ND ug/L 03/01/21 16:48 108-86-110.0 2.2 10
Bromochloromethane ND ug/L 03/01/21 16:48 74-97-510.0 3.4 10
Bromodichloromethane ND ug/L 03/01/21 16:48 75-27-410.0 2.6 10
Bromoform ND ug/L 03/01/21 16:48 75-25-210.0 6.2 10
Bromomethane ND ug/L 03/01/21 16:48 74-83-9 v220.0 6.2 10
2-Butanone (MEK)ND ug/L 03/01/21 16:48 78-93-350.0 33.3 10
Carbon tetrachloride ND ug/L 03/01/21 16:48 56-23-510.0 2.2 10
Chlorobenzene ND ug/L 03/01/21 16:48 108-90-710.0 2.3 10
Chloroethane ND ug/L 03/01/21 16:48 75-00-310.0 4.9 10
Chloroform ND ug/L 03/01/21 16:48 67-66-350.0 23.4 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-13 Lab ID:92524499013 Collected:02/25/21 13:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 03/01/21 16:48 74-87-310.0 3.9 10
2-Chlorotoluene ND ug/L 03/01/21 16:48 95-49-810.0 2.0 10
4-Chlorotoluene ND ug/L 03/01/21 16:48 106-43-410.0 2.0 10
1,2-Dibromo-3-chloropropane ND ug/L 03/01/21 16:48 96-12-850.0 2.6 10
Dibromochloromethane ND ug/L 03/01/21 16:48 124-48-110.0 4.1 10
1,2-Dibromoethane (EDB)ND ug/L 03/01/21 16:48 106-93-410.0 2.6 10
Dibromomethane ND ug/L 03/01/21 16:48 74-95-310.0 4.6 10
1,2-Dichlorobenzene ND ug/L 03/01/21 16:48 95-50-110.0 2.9 10
1,3-Dichlorobenzene ND ug/L 03/01/21 16:48 541-73-110.0 2.2 10
1,4-Dichlorobenzene ND ug/L 03/01/21 16:48 106-46-710.0 2.6 10
Dichlorodifluoromethane ND ug/L 03/01/21 16:48 75-71-8 v110.0 2.3 10
1,1-Dichloroethane ND ug/L 03/01/21 16:48 75-34-310.0 2.7 10
1,2-Dichloroethane ND ug/L 03/01/21 16:48 107-06-210.0 3.4 10
1,1-Dichloroethene ND ug/L 03/01/21 16:48 75-35-410.0 2.4 10
cis-1,2-Dichloroethene ND ug/L 03/01/21 16:48 156-59-210.0 2.9 10
trans-1,2-Dichloroethene ND ug/L 03/01/21 16:48 156-60-510.0 2.5 10
1,2-Dichloropropane ND ug/L 03/01/21 16:48 78-87-510.0 1.9 10
1,3-Dichloropropane ND ug/L 03/01/21 16:48 142-28-910.0 1.6 10
2,2-Dichloropropane ND ug/L 03/01/21 16:48 594-20-710.0 2.7 10
1,1-Dichloropropene ND ug/L 03/01/21 16:48 563-58-610.0 2.1 10
cis-1,3-Dichloropropene ND ug/L 03/01/21 16:48 10061-01-510.0 3.0 10
trans-1,3-Dichloropropene ND ug/L 03/01/21 16:48 10061-02-610.0 3.1 10
Diisopropyl ether 3.1J ug/L 03/01/21 16:48 108-20-310.0 2.2 10
Ethylbenzene 4.3J ug/L 03/01/21 16:48 100-41-410.0 2.6 10
Hexachloro-1,3-butadiene ND ug/L 03/01/21 16:48 87-68-310.0 4.4 10
2-Hexanone ND ug/L 03/01/21 16:48 591-78-650.0 5.7 10
p-Isopropyltoluene ND ug/L 03/01/21 16:48 99-87-610.0 2.1 10
Methylene Chloride ND ug/L 03/01/21 16:48 75-09-250.0 36.9 10
4-Methyl-2-pentanone (MIBK)ND ug/L 03/01/21 16:48 108-10-150.0 45.3 10
Methyl-tert-butyl ether 1540 ug/L 03/01/21 16:48 1634-04-410.0 2.8 10
Naphthalene 4.8J ug/L 03/01/21 16:48 91-20-3 v110.0 3.5 10
Styrene ND ug/L 03/01/21 16:48 100-42-510.0 2.7 10
1,1,1,2-Tetrachloroethane ND ug/L 03/01/21 16:48 630-20-610.0 3.4 10
1,1,2,2-Tetrachloroethane ND ug/L 03/01/21 16:48 79-34-510.0 2.2 10
Tetrachloroethene 198 ug/L 03/01/21 16:48 127-18-410.0 1.6 10
Toluene ND ug/L 03/01/21 16:48 108-88-310.0 2.4 10
1,2,3-Trichlorobenzene ND ug/L 03/01/21 16:48 87-61-610.0 3.4 10
1,2,4-Trichlorobenzene ND ug/L 03/01/21 16:48 120-82-110.0 2.2 10
1,1,1-Trichloroethane ND ug/L 03/01/21 16:48 71-55-610.0 1.8 10
1,1,2-Trichloroethane ND ug/L 03/01/21 16:48 79-00-510.0 2.4 10
Trichloroethene ND ug/L 03/01/21 16:48 79-01-610.0 2.2 10
Trichlorofluoromethane ND ug/L 03/01/21 16:48 75-69-410.0 3.1 10
1,2,3-Trichloropropane ND ug/L 03/01/21 16:48 96-18-410.0 3.5 10
Vinyl acetate ND ug/L 03/01/21 16:48 108-05-420.0 14.5 10
Vinyl chloride ND ug/L 03/01/21 16:48 75-01-410.0 2.4 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-13 Lab ID:92524499013 Collected:02/25/21 13:00 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)8.6J ug/L 03/01/21 16:48 1330-20-710.0 6.3 10
m&p-Xylene ND ug/L 03/01/21 16:48 179601-23-120.0 4.1 10
o-Xylene 8.6J ug/L 03/01/21 16:48 95-47-610.0 2.2 10
Surrogates
4-Bromofluorobenzene (S)80 %03/01/21 16:48 460-00-470-130 10
1,2-Dichloroethane-d4 (S)95 %03/01/21 16:48 17060-07-070-130 10
Toluene-d8 (S)108 %03/01/21 16:48 2037-26-570-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-16 Lab ID:92524499014 Collected:02/25/21 14:50 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/04/21 12:02 83-32-903/03/21 10:0410.0 2.0 1
Acenaphthylene ND ug/L 03/04/21 12:02 208-96-803/03/21 10:0410.0 2.0 1
Aniline ND ug/L 03/04/21 12:02 62-53-303/03/21 10:0410.0 1.6 1
Anthracene ND ug/L 03/04/21 12:02 120-12-703/03/21 10:0410.0 2.3 1
Benzo(a)anthracene ND ug/L 03/04/21 12:02 56-55-303/03/21 10:0410.0 2.7 1
Benzo(a)pyrene ND ug/L 03/04/21 12:02 50-32-803/03/21 10:0410.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/04/21 12:02 205-99-203/03/21 10:0410.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/04/21 12:02 191-24-203/03/21 10:0410.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/04/21 12:02 207-08-903/03/21 10:0410.0 2.7 1
Benzoic Acid ND ug/L 03/04/21 12:02 65-85-003/03/21 10:0450.0 3.4 1
Benzyl alcohol ND ug/L 03/04/21 12:02 100-51-603/03/21 10:0420.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/04/21 12:02 101-55-303/03/21 10:0410.0 1.8 1
Butylbenzylphthalate ND ug/L 03/04/21 12:02 85-68-703/03/21 10:0410.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/04/21 12:02 59-50-703/03/21 10:0410.0 3.3 1
4-Chloroaniline ND ug/L 03/04/21 12:02 106-47-803/03/21 10:0420.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/04/21 12:02 111-91-103/03/21 10:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/04/21 12:02 111-44-403/03/21 10:0410.0 1.9 1
2-Chloronaphthalene ND ug/L 03/04/21 12:02 91-58-703/03/21 10:0410.0 1.7 1
2-Chlorophenol ND ug/L 03/04/21 12:02 95-57-803/03/21 10:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/04/21 12:02 7005-72-303/03/21 10:0410.0 2.0 1
Chrysene ND ug/L 03/04/21 12:02 218-01-903/03/21 10:0410.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/04/21 12:02 53-70-303/03/21 10:0410.0 3.0 1
Dibenzofuran ND ug/L 03/04/21 12:02 132-64-903/03/21 10:0410.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/04/21 12:02 95-50-103/03/21 10:0410.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/04/21 12:02 541-73-103/03/21 10:0410.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/04/21 12:02 106-46-703/03/21 10:0410.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/04/21 12:02 91-94-103/03/21 10:0420.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/04/21 12:02 120-83-203/03/21 10:0410.0 1.4 1
Diethylphthalate ND ug/L 03/04/21 12:02 84-66-203/03/21 10:0410.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/04/21 12:02 105-67-903/03/21 10:0410.0 1.7 1
Dimethylphthalate ND ug/L 03/04/21 12:02 131-11-303/03/21 10:0410.0 2.1 1
Di-n-butylphthalate ND ug/L 03/04/21 12:02 84-74-203/03/21 10:0410.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/04/21 12:02 534-52-103/03/21 10:0420.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/04/21 12:02 51-28-503/03/21 10:0450.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/04/21 12:02 121-14-203/03/21 10:0410.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/04/21 12:02 606-20-203/03/21 10:0410.0 1.7 1
Di-n-octylphthalate ND ug/L 03/04/21 12:02 117-84-003/03/21 10:0410.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/04/21 12:02 117-81-703/03/21 10:046.0 3.7 1
Fluoranthene ND ug/L 03/04/21 12:02 206-44-003/03/21 10:0410.0 2.2 1
Fluorene ND ug/L 03/04/21 12:02 86-73-703/03/21 10:0410.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/04/21 12:02 87-68-303/03/21 10:0410.0 1.8 1
Hexachlorobenzene ND ug/L 03/04/21 12:02 118-74-103/03/21 10:0410.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/04/21 12:02 77-47-403/03/21 10:0410.0 1.6 1
Hexachloroethane ND ug/L 03/04/21 12:02 67-72-103/03/21 10:0410.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/04/21 12:02 193-39-503/03/21 10:0410.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-16 Lab ID:92524499014 Collected:02/25/21 14:50 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/04/21 12:02 78-59-103/03/21 10:0410.0 1.7 1
1-Methylnaphthalene ND ug/L 03/04/21 12:02 90-12-003/03/21 10:0410.0 2.0 1
2-Methylnaphthalene ND ug/L 03/04/21 12:02 91-57-603/03/21 10:0410.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/04/21 12:02 95-48-703/03/21 10:0410.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/04/21 12:02 15831-10-403/03/21 10:0410.0 1.2 1
Naphthalene ND ug/L 03/04/21 12:02 91-20-303/03/21 10:0410.0 2.1 1
2-Nitroaniline ND ug/L 03/04/21 12:02 88-74-403/03/21 10:0420.0 3.0 1
3-Nitroaniline ND ug/L 03/04/21 12:02 99-09-203/03/21 10:0420.0 3.8 1
4-Nitroaniline ND ug/L 03/04/21 12:02 100-01-603/03/21 10:0420.0 5.1 1
Nitrobenzene ND ug/L 03/04/21 12:02 98-95-303/03/21 10:0410.0 1.9 1
2-Nitrophenol ND ug/L 03/04/21 12:02 88-75-503/03/21 10:0410.0 1.4 1
4-Nitrophenol ND ug/L 03/04/21 12:02 100-02-703/03/21 10:0450.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/04/21 12:02 62-75-903/03/21 10:0410.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/04/21 12:02 621-64-703/03/21 10:0410.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/04/21 12:02 86-30-603/03/21 10:0410.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/04/21 12:02 108-60-103/03/21 10:0410.0 1.2 1
Pentachlorophenol ND ug/L 03/04/21 12:02 87-86-503/03/21 10:0420.0 3.8 1
Phenanthrene ND ug/L 03/04/21 12:02 85-01-803/03/21 10:0410.0 2.0 1
Phenol ND ug/L 03/04/21 12:02 108-95-203/03/21 10:0410.0 1.4 1
Pyrene ND ug/L 03/04/21 12:02 129-00-003/03/21 10:0410.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/04/21 12:02 120-82-103/03/21 10:0410.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/04/21 12:02 95-95-403/03/21 10:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/04/21 12:02 88-06-203/03/21 10:0410.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)66 %03/04/21 12:02 4165-60-003/03/21 10:0410-144 1
2-Fluorobiphenyl (S)63 %03/04/21 12:02 321-60-803/03/21 10:0410-130 1
Terphenyl-d14 (S)137 %03/04/21 12:02 1718-51-003/03/21 10:0434-163 1
Phenol-d6 (S)41 %03/04/21 12:02 13127-88-303/03/21 10:0410-130 1
2-Fluorophenol (S)49 %03/04/21 12:02 367-12-403/03/21 10:0410-130 1
2,4,6-Tribromophenol (S)64 %03/04/21 12:02 118-79-603/03/21 10:0410-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 11.6J ug/L 03/01/21 12:33 67-64-1 v125.0 6.2 1
Benzene ND ug/L 03/01/21 12:33 71-43-21.0 0.15 1
Bromobenzene ND ug/L 03/01/21 12:33 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 03/01/21 12:33 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 03/01/21 12:33 75-27-41.0 0.26 1
Bromoform ND ug/L 03/01/21 12:33 75-25-21.0 0.62 1
Bromomethane ND ug/L 03/01/21 12:33 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 03/01/21 12:33 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 03/01/21 12:33 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 03/01/21 12:33 108-90-71.0 0.23 1
Chloroethane ND ug/L 03/01/21 12:33 75-00-31.0 0.49 1
Chloroform 12.5 ug/L 03/01/21 12:33 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-16 Lab ID:92524499014 Collected:02/25/21 14:50 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 03/01/21 12:33 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 03/01/21 12:33 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 03/01/21 12:33 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 03/01/21 12:33 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 03/01/21 12:33 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 03/01/21 12:33 106-93-41.0 0.26 1
Dibromomethane ND ug/L 03/01/21 12:33 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 03/01/21 12:33 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 03/01/21 12:33 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 03/01/21 12:33 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 03/01/21 12:33 75-71-8 v11.0 0.23 1
1,1-Dichloroethane ND ug/L 03/01/21 12:33 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 03/01/21 12:33 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 03/01/21 12:33 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 03/01/21 12:33 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 03/01/21 12:33 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 03/01/21 12:33 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 03/01/21 12:33 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 03/01/21 12:33 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 03/01/21 12:33 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 03/01/21 12:33 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 03/01/21 12:33 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 03/01/21 12:33 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 03/01/21 12:33 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 03/01/21 12:33 87-68-31.0 0.44 1
2-Hexanone ND ug/L 03/01/21 12:33 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 03/01/21 12:33 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 03/01/21 12:33 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 03/01/21 12:33 108-10-15.0 4.5 1
Methyl-tert-butyl ether 1.6 ug/L 03/01/21 12:33 1634-04-41.0 0.28 1
Naphthalene ND ug/L 03/01/21 12:33 91-20-3 v11.0 0.35 1
Styrene ND ug/L 03/01/21 12:33 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 03/01/21 12:33 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 03/01/21 12:33 79-34-51.0 0.22 1
Tetrachloroethene 8.6 ug/L 03/01/21 12:33 127-18-41.0 0.16 1
Toluene ND ug/L 03/01/21 12:33 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 03/01/21 12:33 87-61-6 v11.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 03/01/21 12:33 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 03/01/21 12:33 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 03/01/21 12:33 79-00-51.0 0.24 1
Trichloroethene ND ug/L 03/01/21 12:33 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 03/01/21 12:33 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 03/01/21 12:33 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 03/01/21 12:33 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 03/01/21 12:33 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-16 Lab ID:92524499014 Collected:02/25/21 14:50 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 03/01/21 12:33 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 03/01/21 12:33 179601-23-12.0 0.41 1
o-Xylene ND ug/L 03/01/21 12:33 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)96 %03/01/21 12:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %03/01/21 12:33 17060-07-070-130 1
Toluene-d8 (S)113 %03/01/21 12:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-17 Lab ID:92524499015 Collected:02/25/21 15:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 03/04/21 12:27 83-32-903/03/21 10:0410.0 2.0 1
Acenaphthylene ND ug/L 03/04/21 12:27 208-96-803/03/21 10:0410.0 2.0 1
Aniline ND ug/L 03/04/21 12:27 62-53-303/03/21 10:0410.0 1.6 1
Anthracene ND ug/L 03/04/21 12:27 120-12-703/03/21 10:0410.0 2.3 1
Benzo(a)anthracene ND ug/L 03/04/21 12:27 56-55-303/03/21 10:0410.0 2.7 1
Benzo(a)pyrene ND ug/L 03/04/21 12:27 50-32-803/03/21 10:0410.0 2.8 1
Benzo(b)fluoranthene ND ug/L 03/04/21 12:27 205-99-203/03/21 10:0410.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 03/04/21 12:27 191-24-203/03/21 10:0410.0 2.8 1
Benzo(k)fluoranthene ND ug/L 03/04/21 12:27 207-08-903/03/21 10:0410.0 2.7 1
Benzoic Acid ND ug/L 03/04/21 12:27 65-85-003/03/21 10:0450.0 3.4 1
Benzyl alcohol ND ug/L 03/04/21 12:27 100-51-603/03/21 10:0420.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 03/04/21 12:27 101-55-303/03/21 10:0410.0 1.8 1
Butylbenzylphthalate ND ug/L 03/04/21 12:27 85-68-703/03/21 10:0410.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 03/04/21 12:27 59-50-703/03/21 10:0410.0 3.3 1
4-Chloroaniline ND ug/L 03/04/21 12:27 106-47-803/03/21 10:0420.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 03/04/21 12:27 111-91-103/03/21 10:0410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 03/04/21 12:27 111-44-403/03/21 10:0410.0 1.9 1
2-Chloronaphthalene ND ug/L 03/04/21 12:27 91-58-703/03/21 10:0410.0 1.7 1
2-Chlorophenol ND ug/L 03/04/21 12:27 95-57-803/03/21 10:0410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 03/04/21 12:27 7005-72-303/03/21 10:0410.0 2.0 1
Chrysene ND ug/L 03/04/21 12:27 218-01-903/03/21 10:0410.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 03/04/21 12:27 53-70-303/03/21 10:0410.0 3.0 1
Dibenzofuran ND ug/L 03/04/21 12:27 132-64-903/03/21 10:0410.0 2.1 1
1,2-Dichlorobenzene ND ug/L 03/04/21 12:27 95-50-103/03/21 10:0410.0 1.8 1
1,3-Dichlorobenzene ND ug/L 03/04/21 12:27 541-73-103/03/21 10:0410.0 1.6 1
1,4-Dichlorobenzene ND ug/L 03/04/21 12:27 106-46-703/03/21 10:0410.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 03/04/21 12:27 91-94-103/03/21 10:0420.0 8.1 1
2,4-Dichlorophenol ND ug/L 03/04/21 12:27 120-83-203/03/21 10:0410.0 1.4 1
Diethylphthalate ND ug/L 03/04/21 12:27 84-66-203/03/21 10:0410.0 2.0 1
2,4-Dimethylphenol ND ug/L 03/04/21 12:27 105-67-903/03/21 10:0410.0 1.7 1
Dimethylphthalate ND ug/L 03/04/21 12:27 131-11-303/03/21 10:0410.0 2.1 1
Di-n-butylphthalate ND ug/L 03/04/21 12:27 84-74-203/03/21 10:0410.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 03/04/21 12:27 534-52-103/03/21 10:0420.0 3.4 1
2,4-Dinitrophenol ND ug/L 03/04/21 12:27 51-28-503/03/21 10:0450.0 26.0 1
2,4-Dinitrotoluene ND ug/L 03/04/21 12:27 121-14-203/03/21 10:0410.0 1.6 1
2,6-Dinitrotoluene ND ug/L 03/04/21 12:27 606-20-203/03/21 10:0410.0 1.7 1
Di-n-octylphthalate ND ug/L 03/04/21 12:27 117-84-003/03/21 10:0410.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 03/04/21 12:27 117-81-703/03/21 10:046.0 3.7 1
Fluoranthene ND ug/L 03/04/21 12:27 206-44-003/03/21 10:0410.0 2.2 1
Fluorene ND ug/L 03/04/21 12:27 86-73-703/03/21 10:0410.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 03/04/21 12:27 87-68-303/03/21 10:0410.0 1.8 1
Hexachlorobenzene ND ug/L 03/04/21 12:27 118-74-103/03/21 10:0410.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 03/04/21 12:27 77-47-403/03/21 10:0410.0 1.6 1
Hexachloroethane ND ug/L 03/04/21 12:27 67-72-103/03/21 10:0410.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 03/04/21 12:27 193-39-503/03/21 10:0410.0 2.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-17 Lab ID:92524499015 Collected:02/25/21 15:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Isophorone ND ug/L 03/04/21 12:27 78-59-103/03/21 10:0410.0 1.7 1
1-Methylnaphthalene ND ug/L 03/04/21 12:27 90-12-003/03/21 10:0410.0 2.0 1
2-Methylnaphthalene ND ug/L 03/04/21 12:27 91-57-603/03/21 10:0410.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 03/04/21 12:27 95-48-703/03/21 10:0410.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 03/04/21 12:27 15831-10-403/03/21 10:0410.0 1.2 1
Naphthalene ND ug/L 03/04/21 12:27 91-20-303/03/21 10:0410.0 2.1 1
2-Nitroaniline ND ug/L 03/04/21 12:27 88-74-403/03/21 10:0420.0 3.0 1
3-Nitroaniline ND ug/L 03/04/21 12:27 99-09-203/03/21 10:0420.0 3.8 1
4-Nitroaniline ND ug/L 03/04/21 12:27 100-01-603/03/21 10:0420.0 5.1 1
Nitrobenzene ND ug/L 03/04/21 12:27 98-95-303/03/21 10:0410.0 1.9 1
2-Nitrophenol ND ug/L 03/04/21 12:27 88-75-503/03/21 10:0410.0 1.4 1
4-Nitrophenol ND ug/L 03/04/21 12:27 100-02-703/03/21 10:0450.0 6.6 1
N-Nitrosodimethylamine ND ug/L 03/04/21 12:27 62-75-903/03/21 10:0410.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 03/04/21 12:27 621-64-703/03/21 10:0410.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 03/04/21 12:27 86-30-603/03/21 10:0410.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 03/04/21 12:27 108-60-103/03/21 10:0410.0 1.2 1
Pentachlorophenol ND ug/L 03/04/21 12:27 87-86-503/03/21 10:0420.0 3.8 1
Phenanthrene ND ug/L 03/04/21 12:27 85-01-803/03/21 10:0410.0 2.0 1
Phenol ND ug/L 03/04/21 12:27 108-95-203/03/21 10:0410.0 1.4 1
Pyrene ND ug/L 03/04/21 12:27 129-00-003/03/21 10:0410.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 03/04/21 12:27 120-82-103/03/21 10:0410.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 03/04/21 12:27 95-95-403/03/21 10:0410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 03/04/21 12:27 88-06-203/03/21 10:0410.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)47 %03/04/21 12:27 4165-60-003/03/21 10:0410-144 1
2-Fluorobiphenyl (S)44 %03/04/21 12:27 321-60-803/03/21 10:0410-130 1
Terphenyl-d14 (S)83 %03/04/21 12:27 1718-51-003/03/21 10:0434-163 1
Phenol-d6 (S)27 %03/04/21 12:27 13127-88-303/03/21 10:0410-130 1
2-Fluorophenol (S)33 %03/04/21 12:27 367-12-403/03/21 10:0410-130 1
2,4,6-Tribromophenol (S)40 %03/04/21 12:27 118-79-603/03/21 10:0410-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone 28.6 ug/L 02/27/21 16:26 67-64-125.0 6.2 1
Benzene ND ug/L 02/27/21 16:26 71-43-21.0 0.15 1
Bromobenzene ND ug/L 02/27/21 16:26 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 02/27/21 16:26 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 02/27/21 16:26 75-27-41.0 0.26 1
Bromoform ND ug/L 02/27/21 16:26 75-25-21.0 0.62 1
Bromomethane ND ug/L 02/27/21 16:26 74-83-9 v22.0 0.62 1
2-Butanone (MEK)ND ug/L 02/27/21 16:26 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 02/27/21 16:26 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 02/27/21 16:26 108-90-71.0 0.23 1
Chloroethane ND ug/L 02/27/21 16:26 75-00-31.0 0.49 1
Chloroform 3.4J ug/L 02/27/21 16:26 67-66-35.0 2.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-17 Lab ID:92524499015 Collected:02/25/21 15:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Chloromethane ND ug/L 02/27/21 16:26 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 02/27/21 16:26 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 02/27/21 16:26 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 02/27/21 16:26 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 02/27/21 16:26 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 02/27/21 16:26 106-93-41.0 0.26 1
Dibromomethane ND ug/L 02/27/21 16:26 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 02/27/21 16:26 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 02/27/21 16:26 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 02/27/21 16:26 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 02/27/21 16:26 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 02/27/21 16:26 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 02/27/21 16:26 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 02/27/21 16:26 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 0.57J ug/L 02/27/21 16:26 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 02/27/21 16:26 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 02/27/21 16:26 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 02/27/21 16:26 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 02/27/21 16:26 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 02/27/21 16:26 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 02/27/21 16:26 10061-01-51.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 02/27/21 16:26 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 02/27/21 16:26 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 02/27/21 16:26 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 02/27/21 16:26 87-68-31.0 0.44 1
2-Hexanone ND ug/L 02/27/21 16:26 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 02/27/21 16:26 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 02/27/21 16:26 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 02/27/21 16:26 108-10-15.0 4.5 1
Methyl-tert-butyl ether 5.0 ug/L 02/27/21 16:26 1634-04-41.0 0.28 1
Naphthalene ND ug/L 02/27/21 16:26 91-20-31.0 0.35 1
Styrene ND ug/L 02/27/21 16:26 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 02/27/21 16:26 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 02/27/21 16:26 79-34-51.0 0.22 1
Tetrachloroethene 75.0 ug/L 02/27/21 16:26 127-18-41.0 0.16 1
Toluene ND ug/L 02/27/21 16:26 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 02/27/21 16:26 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 02/27/21 16:26 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 02/27/21 16:26 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 02/27/21 16:26 79-00-51.0 0.24 1
Trichloroethene 0.50J ug/L 02/27/21 16:26 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 02/27/21 16:26 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 02/27/21 16:26 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 02/27/21 16:26 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 02/27/21 16:26 75-01-41.0 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 98
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92524499
Monroe Road Site
Sample:GW-17 Lab ID:92524499015 Collected:02/25/21 15:30 Received:02/26/21 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Xylene (Total)ND ug/L 02/27/21 16:26 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 02/27/21 16:26 179601-23-12.0 0.41 1
o-Xylene ND ug/L 02/27/21 16:26 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)101 %02/27/21 16:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %02/27/21 16:26 17060-07-070-130 1
Toluene-d8 (S)99 %02/27/21 16:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
603004
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92524499001, 92524499002, 92524499003, 92524499004, 92524499005, 92524499006, 92524499007,
92524499008, 92524499009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3177302
Associated Lab Samples:92524499001, 92524499002, 92524499003, 92524499004, 92524499005, 92524499006, 92524499007,
92524499008, 92524499009
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/26/21 21:550.34
1,1,1-Trichloroethane ug/L ND 1.0 02/26/21 21:550.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/26/21 21:550.22
1,1,2-Trichloroethane ug/L ND 1.0 02/26/21 21:550.24
1,1-Dichloroethane ug/L ND 1.0 02/26/21 21:550.27
1,1-Dichloroethene ug/L ND 1.0 02/26/21 21:550.24
1,1-Dichloropropene ug/L ND 1.0 02/26/21 21:550.21
1,2,3-Trichlorobenzene ug/L 0.43J 1.0 02/26/21 21:550.34
1,2,3-Trichloropropane ug/L ND 1.0 02/26/21 21:550.35
1,2,4-Trichlorobenzene ug/L ND 1.0 02/26/21 21:550.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/26/21 21:550.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/26/21 21:550.26
1,2-Dichlorobenzene ug/L ND 1.0 02/26/21 21:550.29
1,2-Dichloroethane ug/L ND 1.0 02/26/21 21:550.34
1,2-Dichloropropane ug/L ND 1.0 02/26/21 21:550.19
1,3-Dichlorobenzene ug/L ND 1.0 02/26/21 21:550.22
1,3-Dichloropropane ug/L ND 1.0 02/26/21 21:550.16
1,4-Dichlorobenzene ug/L ND 1.0 02/26/21 21:550.26
2,2-Dichloropropane ug/L ND 1.0 02/26/21 21:550.27
2-Butanone (MEK)ug/L ND 5.0 02/26/21 21:553.3
2-Chlorotoluene ug/L ND 1.0 02/26/21 21:550.20
2-Hexanone ug/L ND 5.0 02/26/21 21:550.57
4-Chlorotoluene ug/L ND 1.0 02/26/21 21:550.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/26/21 21:554.5
Acetone ug/L ND 25.0 02/26/21 21:556.2
Benzene ug/L ND 1.0 02/26/21 21:550.15
Bromobenzene ug/L ND 1.0 02/26/21 21:550.22
Bromochloromethane ug/L ND 1.0 02/26/21 21:550.34
Bromodichloromethane ug/L ND 1.0 02/26/21 21:550.26
Bromoform ug/L ND 1.0 02/26/21 21:550.62
Bromomethane ug/L ND 2.0 02/26/21 21:550.62
Carbon tetrachloride ug/L ND 1.0 02/26/21 21:550.22
Chlorobenzene ug/L ND 1.0 02/26/21 21:550.23
Chloroethane ug/L ND 1.0 02/26/21 21:550.49
Chloroform ug/L ND 5.0 02/26/21 21:552.3
Chloromethane ug/L ND 1.0 v202/26/21 21:550.39
cis-1,2-Dichloroethene ug/L ND 1.0 02/26/21 21:550.29
cis-1,3-Dichloropropene ug/L ND 1.0 02/26/21 21:550.30
Dibromochloromethane ug/L ND 1.0 02/26/21 21:550.41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3177302
Associated Lab Samples:92524499001, 92524499002, 92524499003, 92524499004, 92524499005, 92524499006, 92524499007,
92524499008, 92524499009
Matrix:Water
AnalyzedMDL
Dibromomethane ug/L ND 1.0 02/26/21 21:550.46
Dichlorodifluoromethane ug/L ND 1.0 02/26/21 21:550.23
Diisopropyl ether ug/L ND 1.0 02/26/21 21:550.22
Ethylbenzene ug/L ND 1.0 02/26/21 21:550.26
Hexachloro-1,3-butadiene ug/L ND 1.0 02/26/21 21:550.44
m&p-Xylene ug/L ND 2.0 02/26/21 21:550.41
Methyl-tert-butyl ether ug/L ND 1.0 02/26/21 21:550.28
Methylene Chloride ug/L ND 5.0 02/26/21 21:553.7
Naphthalene ug/L ND 1.0 02/26/21 21:550.35
o-Xylene ug/L ND 1.0 02/26/21 21:550.22
p-Isopropyltoluene ug/L ND 1.0 02/26/21 21:550.21
Styrene ug/L ND 1.0 02/26/21 21:550.27
Tetrachloroethene ug/L ND 1.0 02/26/21 21:550.16
Toluene ug/L ND 1.0 02/26/21 21:550.24
trans-1,2-Dichloroethene ug/L ND 1.0 02/26/21 21:550.25
trans-1,3-Dichloropropene ug/L ND 1.0 02/26/21 21:550.31
Trichloroethene ug/L ND 1.0 02/26/21 21:550.22
Trichlorofluoromethane ug/L ND 1.0 02/26/21 21:550.31
Vinyl acetate ug/L ND 2.0 02/26/21 21:551.4
Vinyl chloride ug/L ND 1.0 02/26/21 21:550.24
Xylene (Total)ug/L ND 1.0 02/26/21 21:550.63
1,2-Dichloroethane-d4 (S)%99 70-130 02/26/21 21:55
4-Bromofluorobenzene (S)%96 70-130 02/26/21 21:55
Toluene-d8 (S)%100 70-130 02/26/21 21:55
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3177303LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.850 106 70-130
1,1,1-Trichloroethane ug/L 48.750 97 70-130
1,1,2,2-Tetrachloroethane ug/L 51.250 102 70-130
1,1,2-Trichloroethane ug/L 51.250 102 70-130
1,1-Dichloroethane ug/L 48.650 97 70-130
1,1-Dichloroethene ug/L 50.450 101 70-132
1,1-Dichloropropene ug/L 48.550 97 70-131
1,2,3-Trichlorobenzene ug/L 46.950 94 70-134
1,2,3-Trichloropropane ug/L 49.850 100 70-130
1,2,4-Trichlorobenzene ug/L 50.750 101 70-130
1,2-Dibromo-3-chloropropane ug/L 55.250 110 70-132
1,2-Dibromoethane (EDB)ug/L 51.650 103 70-130
1,2-Dichlorobenzene ug/L 51.750 103 70-130
1,2-Dichloroethane ug/L 47.950 96 70-130
1,2-Dichloropropane ug/L 53.050 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3177303LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 51.450 103 70-130
1,3-Dichloropropane ug/L 50.950 102 70-130
1,4-Dichlorobenzene ug/L 50.250 100 70-130
2,2-Dichloropropane ug/L 49.050 98 70-130
2-Butanone (MEK)ug/L 98.8100 99 70-133
2-Chlorotoluene ug/L 51.350 103 70-130
2-Hexanone ug/L 106100 106 70-130
4-Chlorotoluene ug/L 49.650 99 70-130
4-Methyl-2-pentanone (MIBK)ug/L 102100 102 70-130
Acetone ug/L 103100 103 70-144
Benzene ug/L 49.450 99 70-130
Bromobenzene ug/L 50.250 100 70-130
Bromochloromethane ug/L 51.350 103 70-130
Bromodichloromethane ug/L 49.650 99 70-130
Bromoform ug/L 53.950 108 70-131
Bromomethane ug/L 50.450 101 30-177
Carbon tetrachloride ug/L 52.450 105 70-130
Chlorobenzene ug/L 51.550 103 70-130
Chloroethane ug/L 45.350 91 46-131
Chloroform ug/L 48.350 97 70-130
Chloromethane ug/L 39.7 v3507949-130
cis-1,2-Dichloroethene ug/L 47.550 95 70-130
cis-1,3-Dichloropropene ug/L 53.150 106 70-130
Dibromochloromethane ug/L 53.250 106 70-130
Dibromomethane ug/L 52.850 106 70-130
Dichlorodifluoromethane ug/L 44.550 89 52-134
Diisopropyl ether ug/L 48.050 96 70-131
Ethylbenzene ug/L 50.050 100 70-130
Hexachloro-1,3-butadiene ug/L 49.450 99 70-131
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 50.950 102 70-130
Methylene Chloride ug/L 47.350 95 68-130
Naphthalene ug/L 51.550 103 70-133
o-Xylene ug/L 50.150 100 70-130
p-Isopropyltoluene ug/L 49.450 99 70-130
Styrene ug/L 51.750 103 70-130
Tetrachloroethene ug/L 49.050 98 70-130
Toluene ug/L 49.950 100 70-130
trans-1,2-Dichloroethene ug/L 48.650 97 70-130
trans-1,3-Dichloropropene ug/L 53.050 106 70-130
Trichloroethene ug/L 51.650 103 70-130
Trichlorofluoromethane ug/L 43.650 87 61-130
Vinyl acetate ug/L 110100 110 70-140
Vinyl chloride ug/L 42.450 85 59-142
Xylene (Total)ug/L 151150 101 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3177303LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3177304MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524499009
3177305
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 111 70-135120 7 3020ND22.3 23.9
1,1,1-Trichloroethane ug/L 20 118 70-148125 6 3020ND23.5 25.0
1,1,2,2-Tetrachloroethane ug/L 20 102 70-131112 9 3020ND20.4 22.4
1,1,2-Trichloroethane ug/L 20 105 70-136112 7 3020ND20.9 22.5
1,1-Dichloroethane ug/L 20 109 70-147120 9 3020ND21.9 23.9
1,1-Dichloroethene ug/L 20 118 70-158128 8 3020ND23.6 25.5
1,1-Dichloropropene ug/L 20 113 70-149123 8 3020ND22.7 24.7
1,2,3-Trichlorobenzene ug/L 20 114 68-140112 1 3020ND22.8 22.5
1,2,3-Trichloropropane ug/L 20 101 67-137106 5 3020ND20.1 21.2
1,2,4-Trichlorobenzene ug/L 20 114 70-139117 3 3020ND22.8 23.4
1,2-Dibromo-3-
chloropropane
ug/L 20 115 69-136121 5 3020ND23.1 24.3
1,2-Dibromoethane (EDB)ug/L 20 110 70-137117 6 3020ND22.1 23.4
1,2-Dichlorobenzene ug/L 20 107 70-133114 6 3020ND21.4 22.8
1,2-Dichloroethane ug/L 20 104 67-138115 10 3020ND20.8 23.0
1,2-Dichloropropane ug/L 20 115 70-138116 1 3020ND23.0 23.3
1,3-Dichlorobenzene ug/L 20 110 70-133116 5 3020ND22.0 23.1
1,3-Dichloropropane ug/L 20 107 70-136118 10 3020ND21.3 23.7
1,4-Dichlorobenzene ug/L 20 105 70-133111 6 3020ND21.1 22.3
2,2-Dichloropropane ug/L 20 121 52-155129 7 3020ND24.1 25.8
2-Butanone (MEK)ug/L 40 98 61-147114 15 3040ND39.3 45.5
2-Chlorotoluene ug/L 20 110 70-141115 5 3020ND21.9 23.1
2-Hexanone ug/L 40 102 67-139117 14 3040ND40.7 46.7
4-Chlorotoluene ug/L 20 107 70-135113 6 3020ND21.3 22.6
4-Methyl-2-pentanone
(MIBK)
ug/L 40 101 67-136109 8 3040ND40.4 43.7
Acetone ug/L 40 113 55-159126 11 3040ND45.4 50.6
Benzene ug/L 20 112 67-150116 3 3020ND22.4 23.1
Bromobenzene ug/L 20 110 70-134116 6 3020ND21.9 23.2
Bromochloromethane ug/L 20 108 70-146117 8 3020ND21.6 23.5
Bromodichloromethane ug/L 20 107 70-138115 7 3020ND21.4 23.0
Bromoform ug/L 20 97 57-138106 9 3020ND19.5 21.2
Bromomethane ug/L 20 125 10-200134 7 3020ND25.0 26.8
Carbon tetrachloride ug/L 20 125 70-147127 2 3020ND25.0 25.4
Chlorobenzene ug/L 20 111 70-137120 7 3020ND22.2 23.9
Chloroethane ug/L 20 102 51-166117 13 3020ND20.5 23.4
Chloroform ug/L 20 109 70-144119 10 3020ND21.7 23.9
Chloromethane ug/L v3208524-16192 9 3020ND16.9 18.4
cis-1,2-Dichloroethene ug/L 20 104 67-148112 7 3020ND20.9 22.3
cis-1,3-Dichloropropene ug/L 20 113 70-142119 5 3020ND22.6 23.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3177304MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524499009
3177305
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dibromochloromethane ug/L 20 113 68-138122 7 3020ND22.6 24.4
Dibromomethane ug/L 20 110 70-134120 9 3020ND22.0 24.0
Dichlorodifluoromethane ug/L 20 90 43-15598 9 3020ND18.0 19.6
Diisopropyl ether ug/L 20 101 65-146113 11 3020ND20.3 22.7
Ethylbenzene ug/L 20 111 68-143117 5 3020ND22.2 23.4
Hexachloro-1,3-butadiene ug/L 20 135 62-151132 2 3020ND26.9 26.4
m&p-Xylene ug/L 40 113 53-157119 5 3040ND45.2 47.7
Methyl-tert-butyl ether ug/L 20 107 59-156118 10 3020ND21.3 23.6
Methylene Chloride ug/L 20 103 64-148109 6 3020ND20.5 21.7
Naphthalene ug/L 20 113 57-150113 0 3020ND22.6 22.7
o-Xylene ug/L 20 107 68-143119 10 3020ND21.5 23.7
p-Isopropyltoluene ug/L 20 114 70-141117 3 3020ND22.8 23.5
Styrene ug/L 20 108 70-136117 8 3020ND21.5 23.3
Tetrachloroethene ug/L 20 118 70-139122 4 3020ND23.5 24.4
Toluene ug/L 20 110 47-157118 7 3020ND22.0 23.5
trans-1,2-Dichloroethene ug/L 20 114 70-149126 10 3020ND22.9 25.2
trans-1,3-Dichloropropene ug/L 20 115 70-138118 3 3020ND23.0 23.7
Trichloroethene ug/L 20 120 70-149122 2 3020ND24.0 24.4
Trichlorofluoromethane ug/L 20 115 61-154124 7 3020ND23.0 24.7
Vinyl acetate ug/L 40 113 48-156126 11 3040ND45.1 50.3
Vinyl chloride ug/L 20 97 55-172103 6 3020ND19.4 20.6
Xylene (Total)ug/L 60 111 66-145119 7 3060ND66.7 71.5
1,2-Dichloroethane-d4 (S)%100 70-130101
4-Bromofluorobenzene (S)%97 70-13099
Toluene-d8 (S)%101 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
603119
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92524499010, 92524499011, 92524499015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3177803
Associated Lab Samples:92524499010, 92524499011, 92524499015
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 02/27/21 13:430.34
1,1,1-Trichloroethane ug/L ND 1.0 02/27/21 13:430.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 02/27/21 13:430.22
1,1,2-Trichloroethane ug/L ND 1.0 02/27/21 13:430.24
1,1-Dichloroethane ug/L ND 1.0 02/27/21 13:430.27
1,1-Dichloroethene ug/L ND 1.0 02/27/21 13:430.24
1,1-Dichloropropene ug/L ND 1.0 02/27/21 13:430.21
1,2,3-Trichlorobenzene ug/L ND 1.0 02/27/21 13:430.34
1,2,3-Trichloropropane ug/L ND 1.0 02/27/21 13:430.35
1,2,4-Trichlorobenzene ug/L ND 1.0 02/27/21 13:430.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 02/27/21 13:430.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 02/27/21 13:430.26
1,2-Dichlorobenzene ug/L ND 1.0 02/27/21 13:430.29
1,2-Dichloroethane ug/L ND 1.0 02/27/21 13:430.34
1,2-Dichloropropane ug/L ND 1.0 02/27/21 13:430.19
1,3-Dichlorobenzene ug/L ND 1.0 02/27/21 13:430.22
1,3-Dichloropropane ug/L ND 1.0 02/27/21 13:430.16
1,4-Dichlorobenzene ug/L ND 1.0 02/27/21 13:430.26
2,2-Dichloropropane ug/L ND 1.0 02/27/21 13:430.27
2-Butanone (MEK)ug/L ND 5.0 02/27/21 13:433.3
2-Chlorotoluene ug/L ND 1.0 02/27/21 13:430.20
2-Hexanone ug/L ND 5.0 02/27/21 13:430.57
4-Chlorotoluene ug/L ND 1.0 02/27/21 13:430.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 02/27/21 13:434.5
Acetone ug/L ND 25.0 02/27/21 13:436.2
Benzene ug/L ND 1.0 02/27/21 13:430.15
Bromobenzene ug/L ND 1.0 02/27/21 13:430.22
Bromochloromethane ug/L ND 1.0 02/27/21 13:430.34
Bromodichloromethane ug/L ND 1.0 02/27/21 13:430.26
Bromoform ug/L ND 1.0 02/27/21 13:430.62
Bromomethane ug/L ND 2.0 v202/27/21 13:430.62
Carbon tetrachloride ug/L ND 1.0 02/27/21 13:430.22
Chlorobenzene ug/L ND 1.0 02/27/21 13:430.23
Chloroethane ug/L ND 1.0 02/27/21 13:430.49
Chloroform ug/L ND 5.0 02/27/21 13:432.3
Chloromethane ug/L ND 1.0 02/27/21 13:430.39
cis-1,2-Dichloroethene ug/L ND 1.0 02/27/21 13:430.29
cis-1,3-Dichloropropene ug/L ND 1.0 02/27/21 13:430.30
Dibromochloromethane ug/L ND 1.0 02/27/21 13:430.41
Dibromomethane ug/L ND 1.0 02/27/21 13:430.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3177803
Associated Lab Samples:92524499010, 92524499011, 92524499015
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 02/27/21 13:430.23
Diisopropyl ether ug/L ND 1.0 02/27/21 13:430.22
Ethylbenzene ug/L ND 1.0 02/27/21 13:430.26
Hexachloro-1,3-butadiene ug/L ND 1.0 02/27/21 13:430.44
m&p-Xylene ug/L ND 2.0 02/27/21 13:430.41
Methyl-tert-butyl ether ug/L ND 1.0 02/27/21 13:430.28
Methylene Chloride ug/L ND 5.0 02/27/21 13:433.7
Naphthalene ug/L ND 1.0 02/27/21 13:430.35
o-Xylene ug/L ND 1.0 02/27/21 13:430.22
p-Isopropyltoluene ug/L ND 1.0 02/27/21 13:430.21
Styrene ug/L ND 1.0 02/27/21 13:430.27
Tetrachloroethene ug/L ND 1.0 02/27/21 13:430.16
Toluene ug/L ND 1.0 02/27/21 13:430.24
trans-1,2-Dichloroethene ug/L ND 1.0 02/27/21 13:430.25
trans-1,3-Dichloropropene ug/L ND 1.0 02/27/21 13:430.31
Trichloroethene ug/L ND 1.0 02/27/21 13:430.22
Trichlorofluoromethane ug/L ND 1.0 02/27/21 13:430.31
Vinyl acetate ug/L ND 2.0 02/27/21 13:431.4
Vinyl chloride ug/L ND 1.0 02/27/21 13:430.24
Xylene (Total)ug/L ND 1.0 02/27/21 13:430.63
1,2-Dichloroethane-d4 (S)%103 70-130 02/27/21 13:43
4-Bromofluorobenzene (S)%103 70-130 02/27/21 13:43
Toluene-d8 (S)%101 70-130 02/27/21 13:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3177804LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.150 108 70-130
1,1,1-Trichloroethane ug/L 51.750 103 70-130
1,1,2,2-Tetrachloroethane ug/L 53.450 107 70-130
1,1,2-Trichloroethane ug/L 52.050 104 70-130
1,1-Dichloroethane ug/L 52.750 105 70-130
1,1-Dichloroethene ug/L 54.850 110 70-132
1,1-Dichloropropene ug/L 53.450 107 70-131
1,2,3-Trichlorobenzene ug/L 51.850 104 70-134
1,2,3-Trichloropropane ug/L 51.450 103 70-130
1,2,4-Trichlorobenzene ug/L 51.450 103 70-130
1,2-Dibromo-3-chloropropane ug/L 55.950 112 70-132
1,2-Dibromoethane (EDB)ug/L 53.150 106 70-130
1,2-Dichlorobenzene ug/L 53.950 108 70-130
1,2-Dichloroethane ug/L 50.150 100 70-130
1,2-Dichloropropane ug/L 52.450 105 70-130
1,3-Dichlorobenzene ug/L 54.050 108 70-130
1,3-Dichloropropane ug/L 51.550 103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3177804LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 52.550 105 70-130
2,2-Dichloropropane ug/L 55.850 112 70-130
2-Butanone (MEK)ug/L 110100 110 70-133
2-Chlorotoluene ug/L 52.850 106 70-130
2-Hexanone ug/L 111100 111 70-130
4-Chlorotoluene ug/L 52.250 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 109100 109 70-130
Acetone ug/L 114100 114 70-144
Benzene ug/L 50.550 101 70-130
Bromobenzene ug/L 51.250 102 70-130
Bromochloromethane ug/L 52.950 106 70-130
Bromodichloromethane ug/L 51.150 102 70-130
Bromoform ug/L 48.750 97 70-131
Bromomethane ug/L 42.9 v3508630-177
Carbon tetrachloride ug/L 51.550 103 70-130
Chlorobenzene ug/L 52.150 104 70-130
Chloroethane ug/L 44.050 88 46-131
Chloroform ug/L 50.750 101 70-130
Chloromethane ug/L 46.450 93 49-130
cis-1,2-Dichloroethene ug/L 50.450 101 70-130
cis-1,3-Dichloropropene ug/L 55.450 111 70-130
Dibromochloromethane ug/L 56.050 112 70-130
Dibromomethane ug/L 52.850 106 70-130
Dichlorodifluoromethane ug/L 46.450 93 52-134
Diisopropyl ether ug/L 51.750 103 70-131
Ethylbenzene ug/L 51.550 103 70-130
Hexachloro-1,3-butadiene ug/L 51.650 103 70-131
m&p-Xylene ug/L 102100 102 70-130
Methyl-tert-butyl ether ug/L 50.950 102 70-130
Methylene Chloride ug/L 49.550 99 68-130
Naphthalene ug/L 52.850 106 70-133
o-Xylene ug/L 51.450 103 70-130
p-Isopropyltoluene ug/L 53.450 107 70-130
Styrene ug/L 52.650 105 70-130
Tetrachloroethene ug/L 52.350 105 70-130
Toluene ug/L 51.150 102 70-130
trans-1,2-Dichloroethene ug/L 53.450 107 70-130
trans-1,3-Dichloropropene ug/L 54.750 109 70-130
Trichloroethene ug/L 53.350 107 70-130
Trichlorofluoromethane ug/L 48.050 96 61-130
Vinyl acetate ug/L 118100 118 70-140
Vinyl chloride ug/L 45.950 92 59-142
Xylene (Total)ug/L 154150 103 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3177805MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524136004
3177806
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 109 70-135120 9 3020ND21.8 23.9
1,1,1-Trichloroethane ug/L 20 114 70-148124 9 3020ND22.8 24.9
1,1,2,2-Tetrachloroethane ug/L 20 107 70-131112 5 3020ND21.3 22.5
1,1,2-Trichloroethane ug/L 20 107 70-136112 5 3020ND21.4 22.4
1,1-Dichloroethane ug/L 20 115 70-147122 6 3020ND22.9 24.4
1,1-Dichloroethene ug/L 20 121 70-158129 6 3020ND24.2 25.8
1,1-Dichloropropene ug/L 20 118 70-149127 7 3020ND23.6 25.4
1,2,3-Trichlorobenzene ug/L 20 105 68-140109 4 3020ND20.9 21.7
1,2,3-Trichloropropane ug/L 20 102 67-137108 6 3020ND20.3 21.6
1,2,4-Trichlorobenzene ug/L 20 105 70-139108 3 3020ND21.1 21.6
1,2-Dibromo-3-
chloropropane ug/L 20 113 69-136120 6 3020ND22.6 23.9
1,2-Dibromoethane (EDB)ug/L 20 107 70-137116 7 3020ND21.5 23.1
1,2-Dichlorobenzene ug/L 20 111 70-133114 3 3020ND22.2 22.9
1,2-Dichloroethane ug/L 20 111 67-138115 4 3020ND22.1 23.0
1,2-Dichloropropane ug/L 20 113 70-138117 4 3020ND22.6 23.5
1,3-Dichlorobenzene ug/L 20 111 70-133114 3 3020ND22.1 22.9
1,3-Dichloropropane ug/L 20 108 70-136116 7 3020ND21.7 23.2
1,4-Dichlorobenzene ug/L 20 108 70-133113 5 3020ND21.6 22.6
2,2-Dichloropropane ug/L 20 124 52-155133 7 3020ND24.9 26.6
2-Butanone (MEK)ug/L 40 112 61-147114 2 3040ND44.6 45.6
2-Chlorotoluene ug/L 20 111 70-141115 4 3020ND22.2 23.1
2-Hexanone ug/L v14011067-139112 2 3040ND43.9 44.7
4-Chlorotoluene ug/L 20 111 70-135111 0 3020ND22.2 22.2
4-Methyl-2-pentanone
(MIBK)ug/L 40 111 67-136114 2 3040ND44.4 45.5
Acetone ug/L 40 109 55-159114 4 3040ND43.6 45.5
Benzene ug/L 20 109 67-150117 7 3020ND21.9 23.4
Bromobenzene ug/L 20 108 70-134111 3 3020ND21.6 22.3
Bromochloromethane ug/L 20 116 70-146126 9 3020ND23.1 25.2
Bromodichloromethane ug/L 20 106 70-138114 7 3020ND21.3 22.7
Bromoform ug/L 20 96 57-138103 7 3020ND19.1 20.5
Bromomethane ug/L 20 104 10-200113 9 3020ND20.7 22.7
Carbon tetrachloride ug/L 20 115 70-147121 6 3020ND22.9 24.3
Chlorobenzene ug/L 20 109 70-137118 8 3020ND21.8 23.5
Chloroethane ug/L 20 108 51-166113 4 3020ND21.6 22.5
Chloroform ug/L 20 114 70-144121 6 3020ND22.8 24.2
Chloromethane ug/L 20 107 24-161111 3 3020ND21.4 22.2
cis-1,2-Dichloroethene ug/L 20 111 67-148120 8 3020ND22.1 24.0
cis-1,3-Dichloropropene ug/L 20 113 70-142122 7 3020ND22.7 24.3
Dibromochloromethane ug/L 20 111 68-138119 7 3020ND22.3 23.9
Dibromomethane ug/L 20 111 70-134118 7 3020ND22.1 23.7
Dichlorodifluoromethane ug/L 20 101 43-155106 5 3020ND20.1 21.2
Diisopropyl ether ug/L 20 109 65-146118 8 3020ND21.8 23.6
Ethylbenzene ug/L 20 108 68-143117 8 3020ND21.6 23.3
Hexachloro-1,3-butadiene ug/L 20 112 62-151114 2 3020ND22.4 22.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3177805MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524136004
3177806
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 40 107 53-157114 6 3040ND42.9 45.6
Methyl-tert-butyl ether ug/L 20 109 59-156116 6 3020ND21.9 23.1
Methylene Chloride ug/L 20 108 64-148116 7 3020ND21.6 23.2
Naphthalene ug/L 20 110 57-150112 2 3020ND22.0 22.5
o-Xylene ug/L 20 108 68-143113 5 3020ND21.6 22.7
p-Isopropyltoluene ug/L 20 113 70-141115 2 3020ND22.6 23.0
Styrene ug/L 20 105 70-136113 7 3020ND21.1 22.5
Tetrachloroethene ug/L 20 109 70-139118 8 3020ND21.8 23.6
Toluene ug/L 20 109 47-157116 6 3020ND21.8 23.2
trans-1,2-Dichloroethene ug/L 20 119 70-149124 4 3020ND23.9 24.9
trans-1,3-Dichloropropene ug/L 20 113 70-138118 4 3020ND22.5 23.6
Trichloroethene ug/L 20 114 70-149120 5 3020ND22.7 24.0
Trichlorofluoromethane ug/L 20 111 61-154117 6 3020ND22.1 23.5
Vinyl acetate ug/L v14012548-156131 5 3040ND49.9 52.3
Vinyl chloride ug/L 20 106 55-172110 4 3020ND21.2 22.1
Xylene (Total)ug/L 60 107 66-145114 6 3060ND64.5 68.3
1,2-Dichloroethane-d4 (S)%102 70-130105
4-Bromofluorobenzene (S)%99 70-130101
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
603258
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92524499012, 92524499013, 92524499014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3178516
Associated Lab Samples:92524499012, 92524499013, 92524499014
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 03/01/21 11:570.34
1,1,1-Trichloroethane ug/L ND 1.0 03/01/21 11:570.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 03/01/21 11:570.22
1,1,2-Trichloroethane ug/L ND 1.0 03/01/21 11:570.24
1,1-Dichloroethane ug/L ND 1.0 03/01/21 11:570.27
1,1-Dichloroethene ug/L ND 1.0 03/01/21 11:570.24
1,1-Dichloropropene ug/L ND 1.0 03/01/21 11:570.21
1,2,3-Trichlorobenzene ug/L ND 1.0 v103/01/21 11:570.34
1,2,3-Trichloropropane ug/L ND 1.0 03/01/21 11:570.35
1,2,4-Trichlorobenzene ug/L ND 1.0 03/01/21 11:570.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 03/01/21 11:570.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 03/01/21 11:570.26
1,2-Dichlorobenzene ug/L ND 1.0 03/01/21 11:570.29
1,2-Dichloroethane ug/L ND 1.0 03/01/21 11:570.34
1,2-Dichloropropane ug/L ND 1.0 03/01/21 11:570.19
1,3-Dichlorobenzene ug/L ND 1.0 03/01/21 11:570.22
1,3-Dichloropropane ug/L ND 1.0 03/01/21 11:570.16
1,4-Dichlorobenzene ug/L ND 1.0 03/01/21 11:570.26
2,2-Dichloropropane ug/L ND 1.0 03/01/21 11:570.27
2-Butanone (MEK)ug/L ND 5.0 03/01/21 11:573.3
2-Chlorotoluene ug/L ND 1.0 03/01/21 11:570.20
2-Hexanone ug/L ND 5.0 03/01/21 11:570.57
4-Chlorotoluene ug/L ND 1.0 03/01/21 11:570.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 03/01/21 11:574.5
Acetone ug/L ND 25.0 v103/01/21 11:576.2
Benzene ug/L ND 1.0 03/01/21 11:570.15
Bromobenzene ug/L ND 1.0 03/01/21 11:570.22
Bromochloromethane ug/L ND 1.0 03/01/21 11:570.34
Bromodichloromethane ug/L ND 1.0 03/01/21 11:570.26
Bromoform ug/L ND 1.0 03/01/21 11:570.62
Bromomethane ug/L ND 2.0 v203/01/21 11:570.62
Carbon tetrachloride ug/L ND 1.0 03/01/21 11:570.22
Chlorobenzene ug/L ND 1.0 03/01/21 11:570.23
Chloroethane ug/L ND 1.0 03/01/21 11:570.49
Chloroform ug/L ND 5.0 03/01/21 11:572.3
Chloromethane ug/L ND 1.0 03/01/21 11:570.39
cis-1,2-Dichloroethene ug/L ND 1.0 03/01/21 11:570.29
cis-1,3-Dichloropropene ug/L ND 1.0 03/01/21 11:570.30
Dibromochloromethane ug/L ND 1.0 03/01/21 11:570.41
Dibromomethane ug/L ND 1.0 03/01/21 11:570.46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3178516
Associated Lab Samples:92524499012, 92524499013, 92524499014
Matrix:Water
AnalyzedMDL
Dichlorodifluoromethane ug/L ND 1.0 v103/01/21 11:570.23
Diisopropyl ether ug/L ND 1.0 03/01/21 11:570.22
Ethylbenzene ug/L ND 1.0 03/01/21 11:570.26
Hexachloro-1,3-butadiene ug/L ND 1.0 03/01/21 11:570.44
m&p-Xylene ug/L ND 2.0 03/01/21 11:570.41
Methyl-tert-butyl ether ug/L ND 1.0 03/01/21 11:570.28
Methylene Chloride ug/L ND 5.0 03/01/21 11:573.7
Naphthalene ug/L ND 1.0 v103/01/21 11:570.35
o-Xylene ug/L ND 1.0 03/01/21 11:570.22
p-Isopropyltoluene ug/L ND 1.0 03/01/21 11:570.21
Styrene ug/L ND 1.0 03/01/21 11:570.27
Tetrachloroethene ug/L ND 1.0 03/01/21 11:570.16
Toluene ug/L ND 1.0 03/01/21 11:570.24
trans-1,2-Dichloroethene ug/L ND 1.0 03/01/21 11:570.25
trans-1,3-Dichloropropene ug/L ND 1.0 03/01/21 11:570.31
Trichloroethene ug/L ND 1.0 03/01/21 11:570.22
Trichlorofluoromethane ug/L ND 1.0 03/01/21 11:570.31
Vinyl acetate ug/L ND 2.0 03/01/21 11:571.4
Vinyl chloride ug/L ND 1.0 03/01/21 11:570.24
Xylene (Total)ug/L ND 1.0 03/01/21 11:570.63
1,2-Dichloroethane-d4 (S)%114 70-130 03/01/21 11:57
4-Bromofluorobenzene (S)%98 70-130 03/01/21 11:57
Toluene-d8 (S)%102 70-130 03/01/21 11:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3178517LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.150 100 70-130
1,1,1-Trichloroethane ug/L 47.150 94 70-130
1,1,2,2-Tetrachloroethane ug/L 49.150 98 70-130
1,1,2-Trichloroethane ug/L 55.050 110 70-130
1,1-Dichloroethane ug/L 53.650 107 70-130
1,1-Dichloroethene ug/L 41.850 84 70-132
1,1-Dichloropropene ug/L 44.950 90 70-131
1,2,3-Trichlorobenzene ug/L 48.6 v1509770-134
1,2,3-Trichloropropane ug/L 50.650 101 70-130
1,2,4-Trichlorobenzene ug/L 49.450 99 70-130
1,2-Dibromo-3-chloropropane ug/L 51.650 103 70-132
1,2-Dibromoethane (EDB)ug/L 50.550 101 70-130
1,2-Dichlorobenzene ug/L 49.250 98 70-130
1,2-Dichloroethane ug/L 51.550 103 70-130
1,2-Dichloropropane ug/L 51.850 104 70-130
1,3-Dichlorobenzene ug/L 50.050 100 70-130
1,3-Dichloropropane ug/L 50.550 101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3178517LABORATORY CONTROL SAMPLE:
LCSSpike
1,4-Dichlorobenzene ug/L 49.050 98 70-130
2,2-Dichloropropane ug/L 49.550 99 70-130
2-Butanone (MEK)ug/L 95.5100 96 70-133
2-Chlorotoluene ug/L 51.150 102 70-130
2-Hexanone ug/L 128100 128 70-130
4-Chlorotoluene ug/L 50.750 101 70-130
4-Methyl-2-pentanone (MIBK)ug/L 123100 123 70-130
Acetone ug/L 126 v110012670-144
Benzene ug/L 44.550 89 70-130
Bromobenzene ug/L 48.450 97 70-130
Bromochloromethane ug/L 48.050 96 70-130
Bromodichloromethane ug/L 49.350 99 70-130
Bromoform ug/L 47.950 96 70-131
Bromomethane ug/L 39.4 v3507930-177
Carbon tetrachloride ug/L 45.350 91 70-130
Chlorobenzene ug/L 48.750 97 70-130
Chloroethane ug/L 49.750 99 46-131
Chloroform ug/L 50.850 102 70-130
Chloromethane ug/L 42.750 85 49-130
cis-1,2-Dichloroethene ug/L 54.150 108 70-130
cis-1,3-Dichloropropene ug/L 45.850 92 70-130
Dibromochloromethane ug/L 50.950 102 70-130
Dibromomethane ug/L 45.350 91 70-130
Dichlorodifluoromethane ug/L 46.3 v1509352-134
Diisopropyl ether ug/L 60.650 121 70-131
Ethylbenzene ug/L 48.850 98 70-130
Hexachloro-1,3-butadiene ug/L 45.750 91 70-131
m&p-Xylene ug/L 97.2100 97 70-130
Methyl-tert-butyl ether ug/L 50.050 100 70-130
Methylene Chloride ug/L 44.750 89 68-130
Naphthalene ug/L 52.1 v15010470-133
o-Xylene ug/L 48.650 97 70-130
p-Isopropyltoluene ug/L 50.450 101 70-130
Styrene ug/L 51.050 102 70-130
Tetrachloroethene ug/L 40.350 81 70-130
Toluene ug/L 46.150 92 70-130
trans-1,2-Dichloroethene ug/L 51.450 103 70-130
trans-1,3-Dichloropropene ug/L 53.850 108 70-130
Trichloroethene ug/L 45.050 90 70-130
Trichlorofluoromethane ug/L 38.750 77 61-130
Vinyl acetate ug/L 130100 130 70-140
Vinyl chloride ug/L 37.250 74 59-142
Xylene (Total)ug/L 146150 97 70-130
1,2-Dichloroethane-d4 (S)%116 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%92 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3178518MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524138017
3178519
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 4000 115 70-135124 8 304000ND46004970
1,1,1-Trichloroethane ug/L 4000 119 70-148107 9 30400027750204570
1,1,2,2-Tetrachloroethane ug/L M1400011970-131138 14 304000ND47805510
1,1,2-Trichloroethane ug/L R140008970-136125 33 304000ND35805000
1,1-Dichloroethane ug/L 4000 130 70-147116 11 304000ND51904630
1,1-Dichloroethene ug/L 4000 107 70-158111 3 30400022145204650
1,1-Dichloropropene ug/L 4000 115 70-149119 4 304000ND45904750
1,2,3-Trichlorobenzene ug/L v1400010268-140128 22 304000ND40905110
1,2,3-Trichloropropane ug/L M1400011967-137154 26 304000ND47506150
1,2,4-Trichlorobenzene ug/L 4000 106 70-139131 21 304000ND42305240
1,2-Dibromo-3-
chloropropane ug/L 4000 110 69-136134 19 304000ND43905340
1,2-Dibromoethane (EDB)ug/L R140008670-137126 38 304000ND34305040
1,2-Dichlorobenzene ug/L 4000 113 70-133106 6 304000ND45204240
1,2-Dichloroethane ug/L M1400012967-138142 9 304000ND51705680
1,2-Dichloropropane ug/L 4000 107 70-138118 10 304000ND42704700
1,3-Dichlorobenzene ug/L 4000 116 70-133126 8 304000ND46305030
1,3-Dichloropropane ug/L R140008070-136129 47 304000ND32005180
1,4-Dichlorobenzene ug/L 4000 111 70-133124 11 304000ND44404960
2,2-Dichloropropane ug/L 4000 117 52-155120 3 304000ND46804800
2-Butanone (MEK)ug/L 8000 115 61-147119 4 308000ND91809510
2-Chlorotoluene ug/L 4000 117 70-141129 10 304000ND46605140
2-Hexanone ug/L 8000 110 67-139113 3 308000ND87909050
4-Chlorotoluene ug/L 4000 116 70-135129 10 304000ND46505160
4-Methyl-2-pentanone
(MIBK)ug/L R180008667-136119 32 308000ND68809500
Acetone ug/L R1,v1800013355-15998 31 308000ND107007830
Benzene ug/L R140009267-150129 33 304000ND36905180
Bromobenzene ug/L 4000 108 70-134118 9 304000ND43304720
Bromochloromethane ug/L 4000 104 70-146104 0 304000ND41704160
Bromodichloromethane ug/L 4000 109 70-138119 8 304000ND43804750
Bromoform ug/L 4000 113 57-138125 9 304000ND45304980
Bromomethane ug/L v3400010110-200104 3 304000ND40504160
Carbon tetrachloride ug/L 4000 96 70-147122 23 304000ND38604870
Chlorobenzene ug/L 4000 112 70-137123 9 304000ND45004920
Chloroethane ug/L 4000 110 51-166107 4 304000ND44104260
Chloroform ug/L 4000 112 70-144117 4 304000ND44704660
Chloromethane ug/L 4000 101 24-16197 4 304000ND40603890
cis-1,2-Dichloroethene ug/L 4000 133 67-148111 14 304000116064605590
cis-1,3-Dichloropropene ug/L R140009070-142129 35 304000ND36205170
Dibromochloromethane ug/L R140008568-138133 44 304000ND34105310
Dibromomethane ug/L 4000 105 70-134122 15 304000ND42104890
Dichlorodifluoromethane ug/L v1400011643-155118 1 304000ND46404710
Diisopropyl ether ug/L 4000 134 65-146115 15 304000ND53604590
Ethylbenzene ug/L 4000 114 68-143120 5 304000ND45704820
Hexachloro-1,3-butadiene ug/L 4000 107 62-151132 21 304000ND42905300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3178518MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524138017
3178519
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
m&p-Xylene ug/L 8000 119 53-157120 1 308000ND94909580
Methyl-tert-butyl ether ug/L 4000 120 59-156101 16 304000ND47804050
Methylene Chloride ug/L 4000 115 64-14892 23 304000ND46103680
Naphthalene ug/L v1400010657-150132 21 304000ND43905410
o-Xylene ug/L 4000 118 68-143125 6 304000ND47405010
p-Isopropyltoluene ug/L 4000 117 70-141116 1 304000ND46804640
Styrene ug/L 4000 123 70-136132 7 304000ND49405280
Tetrachloroethene ug/L M1,R140005570-139139 40 3040004570676010100
Toluene ug/L 4000 100 47-157126 23 304000ND40005050
trans-1,2-Dichloroethene ug/L 4000 130 70-149106 20 304000ND51904230
trans-1,3-Dichloropropene ug/L R140008670-138122 34 304000ND34504870
Trichloroethene ug/L M1400010670-149196 12 304000233002760031200
Trichlorofluoromethane ug/L 4000 101 61-154100 1 304000ND40404000
Vinyl acetate ug/L 8000 153 48-156133 15 308000ND1230010600
Vinyl chloride ug/L 4000 99 55-17295 3 304000ND39403810
Xylene (Total)ug/L 12000 119 66-145122 3 3012000ND1420014600
1,2-Dichloroethane-d4 (S)%110 70-130116
4-Bromofluorobenzene (S)%107 70-130116
Toluene-d8 (S)%84 70-130107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
603611
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92524499001, 92524499002, 92524499003, 92524499004, 92524499005, 92524499006, 92524499007,
92524499008, 92524499009, 92524499010, 92524499011, 92524499012, 92524499013
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3179890
Associated Lab Samples:92524499001, 92524499002, 92524499003, 92524499004, 92524499005, 92524499006, 92524499007,
92524499008, 92524499009, 92524499010, 92524499011, 92524499012, 92524499013
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 03/02/21 16:361.7
1,2-Dichlorobenzene ug/L ND 10.0 03/02/21 16:361.8
1,3-Dichlorobenzene ug/L ND 10.0 03/02/21 16:361.6
1,4-Dichlorobenzene ug/L ND 10.0 03/02/21 16:361.7
1-Methylnaphthalene ug/L ND 10.0 03/02/21 16:362.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 03/02/21 16:361.2
2,4,5-Trichlorophenol ug/L ND 10.0 03/02/21 16:361.4
2,4,6-Trichlorophenol ug/L ND 10.0 03/02/21 16:361.6
2,4-Dichlorophenol ug/L ND 10.0 03/02/21 16:361.4
2,4-Dimethylphenol ug/L ND 10.0 03/02/21 16:361.7
2,4-Dinitrophenol ug/L ND 50.0 03/02/21 16:3626.0
2,4-Dinitrotoluene ug/L ND 10.0 03/02/21 16:361.6
2,6-Dinitrotoluene ug/L ND 10.0 03/02/21 16:361.7
2-Chloronaphthalene ug/L ND 10.0 03/02/21 16:361.7
2-Chlorophenol ug/L ND 10.0 03/02/21 16:361.2
2-Methylnaphthalene ug/L ND 10.0 03/02/21 16:361.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/02/21 16:361.9
2-Nitroaniline ug/L ND 20.0 03/02/21 16:363.0
2-Nitrophenol ug/L ND 10.0 03/02/21 16:361.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/02/21 16:361.2
3,3'-Dichlorobenzidine ug/L ND 20.0 03/02/21 16:368.1
3-Nitroaniline ug/L ND 20.0 03/02/21 16:363.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/02/21 16:363.4
4-Bromophenylphenyl ether ug/L ND 10.0 03/02/21 16:361.8
4-Chloro-3-methylphenol ug/L ND 10.0 03/02/21 16:363.3
4-Chloroaniline ug/L ND 20.0 03/02/21 16:363.6
4-Chlorophenylphenyl ether ug/L ND 10.0 03/02/21 16:362.0
4-Nitroaniline ug/L ND 20.0 03/02/21 16:365.1
4-Nitrophenol ug/L ND 50.0 03/02/21 16:366.6
Acenaphthene ug/L ND 10.0 03/02/21 16:362.0
Acenaphthylene ug/L ND 10.0 03/02/21 16:362.0
Aniline ug/L ND 10.0 03/02/21 16:361.6
Anthracene ug/L ND 10.0 03/02/21 16:362.3
Benzo(a)anthracene ug/L ND 10.0 03/02/21 16:362.7
Benzo(a)pyrene ug/L ND 10.0 03/02/21 16:362.8
Benzo(b)fluoranthene ug/L ND 10.0 03/02/21 16:362.6
Benzo(g,h,i)perylene ug/L ND 10.0 03/02/21 16:362.8
Benzo(k)fluoranthene ug/L ND 10.0 03/02/21 16:362.7
Benzoic Acid ug/L ND 50.0 03/02/21 16:363.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3179890
Associated Lab Samples:92524499001, 92524499002, 92524499003, 92524499004, 92524499005, 92524499006, 92524499007,
92524499008, 92524499009, 92524499010, 92524499011, 92524499012, 92524499013
Matrix:Water
AnalyzedMDL
Benzyl alcohol ug/L ND 20.0 03/02/21 16:362.9
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/02/21 16:361.8
bis(2-Chloroethyl) ether ug/L ND 10.0 03/02/21 16:361.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/02/21 16:363.7
Butylbenzylphthalate ug/L ND 10.0 03/02/21 16:363.1
Chrysene ug/L ND 10.0 03/02/21 16:362.8
Di-n-butylphthalate ug/L ND 10.0 03/02/21 16:362.2
Di-n-octylphthalate ug/L ND 10.0 03/02/21 16:363.9
Dibenz(a,h)anthracene ug/L ND 10.0 03/02/21 16:363.0
Dibenzofuran ug/L ND 10.0 03/02/21 16:362.1
Diethylphthalate ug/L ND 10.0 03/02/21 16:362.0
Dimethylphthalate ug/L ND 10.0 03/02/21 16:362.1
Fluoranthene ug/L ND 10.0 03/02/21 16:362.2
Fluorene ug/L ND 10.0 03/02/21 16:362.1
Hexachloro-1,3-butadiene ug/L ND 10.0 03/02/21 16:361.8
Hexachlorobenzene ug/L ND 10.0 03/02/21 16:362.2
Hexachlorocyclopentadiene ug/L ND 10.0 03/02/21 16:361.6
Hexachloroethane ug/L ND 10.0 03/02/21 16:361.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/02/21 16:362.9
Isophorone ug/L ND 10.0 03/02/21 16:361.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/02/21 16:361.3
N-Nitrosodimethylamine ug/L ND 10.0 03/02/21 16:361.9
N-Nitrosodiphenylamine ug/L ND 10.0 03/02/21 16:363.0
Naphthalene ug/L ND 10.0 03/02/21 16:362.1
Nitrobenzene ug/L ND 10.0 03/02/21 16:361.9
Pentachlorophenol ug/L ND 20.0 03/02/21 16:363.8
Phenanthrene ug/L ND 10.0 03/02/21 16:362.0
Phenol ug/L ND 10.0 03/02/21 16:361.4
Pyrene ug/L ND 10.0 03/02/21 16:362.2
2,4,6-Tribromophenol (S)%111 10-144 03/02/21 16:36
2-Fluorobiphenyl (S)%88 10-130 03/02/21 16:36
2-Fluorophenol (S)%71 10-130 03/02/21 16:36
Nitrobenzene-d5 (S)%100 10-144 03/02/21 16:36
Phenol-d6 (S)%54 10-130 03/02/21 16:36
Terphenyl-d14 (S)%140 34-163 03/02/21 16:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3179891LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 20.650 41 18-130
1,2-Dichlorobenzene ug/L 22.150 44 20-130
1,3-Dichlorobenzene ug/L 21.150 42 18-130
1,4-Dichlorobenzene ug/L 22.350 45 18-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3179891LABORATORY CONTROL SAMPLE:
LCSSpike
1-Methylnaphthalene ug/L 24.750 49 29-130
2,2'-Oxybis(1-chloropropane)ug/L 30.850 62 28-130
2,4,5-Trichlorophenol ug/L 34.650 69 35-130
2,4,6-Trichlorophenol ug/L 32.450 65 31-130
2,4-Dichlorophenol ug/L 32.150 64 35-130
2,4-Dimethylphenol ug/L 33.350 67 34-130
2,4-Dinitrophenol ug/L 190250 76 10-153
2,4-Dinitrotoluene ug/L 42.150 84 37-136
2,6-Dinitrotoluene ug/L 36.850 74 33-136
2-Chloronaphthalene ug/L 24.450 49 26-130
2-Chlorophenol ug/L 31.150 62 37-130
2-Methylnaphthalene ug/L 23.950 48 29-130
2-Methylphenol(o-Cresol)ug/L 30.350 61 35-130
2-Nitroaniline ug/L 72.0100 72 37-130
2-Nitrophenol ug/L 33.250 66 32-130
3&4-Methylphenol(m&p Cresol)ug/L 28.450 57 34-130
3,3'-Dichlorobenzidine ug/L 85.1100 85 34-136
3-Nitroaniline ug/L 78.9100 79 37-138
4,6-Dinitro-2-methylphenol ug/L 86.5100 86 21-157
4-Bromophenylphenyl ether ug/L 36.750 73 38-130
4-Chloro-3-methylphenol ug/L 67.4100 67 37-130
4-Chloroaniline ug/L 62.9100 63 38-130
4-Chlorophenylphenyl ether ug/L 30.750 61 33-130
4-Nitroaniline ug/L 87.4100 87 42-137
4-Nitrophenol ug/L 144250 57 10-130
Acenaphthene ug/L 28.850 58 33-130
Acenaphthylene ug/L 29.950 60 35-130
Aniline ug/L 28.150 56 22-130
Anthracene ug/L 43.650 87 48-130
Benzo(a)anthracene ug/L 46.850 94 48-137
Benzo(a)pyrene ug/L 48.050 96 49-138
Benzo(b)fluoranthene ug/L 47.950 96 52-138
Benzo(g,h,i)perylene ug/L 48.350 97 48-140
Benzo(k)fluoranthene ug/L 48.650 97 48-139
Benzoic Acid ug/L 111250 45 10-130
Benzyl alcohol ug/L 62.9100 63 35-130
bis(2-Chloroethoxy)methane ug/L 32.950 66 34-130
bis(2-Chloroethyl) ether ug/L 34.750 69 36-130
bis(2-Ethylhexyl)phthalate ug/L 46.750 93 32-165
Butylbenzylphthalate ug/L 45.450 91 34-161
Chrysene ug/L 47.450 95 47-131
Di-n-butylphthalate ug/L 46.050 92 39-144
Di-n-octylphthalate ug/L 44.550 89 30-170
Dibenz(a,h)anthracene ug/L 49.550 99 49-138
Dibenzofuran ug/L 30.450 61 33-130
Diethylphthalate ug/L 40.550 81 38-131
Dimethylphthalate ug/L 36.850 74 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3179891LABORATORY CONTROL SAMPLE:
LCSSpike
Fluoranthene ug/L 47.750 95 46-137
Fluorene ug/L 33.350 67 37-130
Hexachloro-1,3-butadiene ug/L 17.750 35 11-130
Hexachlorobenzene ug/L 39.150 78 38-130
Hexachlorocyclopentadiene ug/L 15.350 31 10-130
Hexachloroethane ug/L 18.850 38 14-130
Indeno(1,2,3-cd)pyrene ug/L 49.550 99 41-130
Isophorone ug/L 31.850 64 33-130
N-Nitroso-di-n-propylamine ug/L 32.950 66 36-130
N-Nitrosodimethylamine ug/L 30.850 62 34-130
N-Nitrosodiphenylamine ug/L 39.150 78 37-130
Naphthalene ug/L 26.450 53 30-130
Nitrobenzene ug/L 32.950 66 36-130
Pentachlorophenol ug/L 100100 100 23-149
Phenanthrene ug/L 42.350 85 44-130
Phenol ug/L 20.050 40 18-130
Pyrene ug/L 46.150 92 47-134
2,4,6-Tribromophenol (S)%102 10-144
2-Fluorobiphenyl (S)%59 10-130
2-Fluorophenol (S)%49 10-130
Nitrobenzene-d5 (S)%68 10-144
Phenol-d6 (S)%39 10-130
Terphenyl-d14 (S)%111 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3179892MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524445019
3179893
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 84 10-13079 6 3050ND41.9 39.6
1,2-Dichlorobenzene ug/L 50 86 10-13079 9 3050ND42.9 39.3
1,3-Dichlorobenzene ug/L 50 82 10-13076 8 3050ND41.2 38.2
1,4-Dichlorobenzene ug/L 50 85 10-13078 9 3050ND42.7 38.9
1-Methylnaphthalene ug/L 50 95 10-13089 6 3050ND47.4 44.6
2,2'-Oxybis(1-
chloropropane)ug/L 50 109 12-142100 8 3050ND54.3 49.9
2,4,5-Trichlorophenol ug/L 50 123 10-143119 4 3050ND61.7 59.6
2,4,6-Trichlorophenol ug/L 50 117 10-147111 5 3050ND58.5 55.5
2,4-Dichlorophenol ug/L 50 112 10-138107 4 3050ND55.8 53.6
2,4-Dimethylphenol ug/L 50 112 25-130105 6 3050ND55.8 52.7
2,4-Dinitrophenol ug/L R125011010-16555 67 30250ND276138
2,4-Dinitrotoluene ug/L 50 122 29-148120 2 3050ND61.1 59.9
2,6-Dinitrotoluene ug/L 50 123 26-146119 3 3050ND61.3 59.4
2-Chloronaphthalene ug/L 50 97 11-13092 5 3050ND48.4 46.1
2-Chlorophenol ug/L 50 106 10-133100 5 3050ND52.8 50.0
2-Methylnaphthalene ug/L 50 94 13-13090 4 3050ND46.8 44.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3179892MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524445019
3179893
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/L 50 103 20-13097 6 3050ND51.6 48.5
2-Nitroaniline ug/L 100 120 24-136116 4 30100ND120116
2-Nitrophenol ug/L 50 120 10-153118 1 3050ND59.8 59.2
3&4-Methylphenol(m&p
Cresol)ug/L 50 99 16-13092 7 3050ND49.4 46.1
3,3'-Dichlorobenzidine ug/L 100 111 10-153103 8 30100ND111103
3-Nitroaniline ug/L 100 117 22-151118 1 30100ND117118
4,6-Dinitro-2-methylphenol ug/L 100 121 10-180103 16 30100ND121103
4-Bromophenylphenyl ether ug/L 50 120 25-130118 2 3050ND60.2 58.9
4-Chloro-3-methylphenol ug/L 100 114 25-133109 4 30100ND114109
4-Chloroaniline ug/L 100 107 14-13299 8 30100ND10798.6
4-Chlorophenylphenyl ether ug/L 50 112 19-130106 5 3050ND56.1 53.1
4-Nitroaniline ug/L 100 121 29-150118 3 30100ND121118
4-Nitrophenol ug/L 250 75 10-13062 19 30250ND188154
Acenaphthene ug/L 50 108 16-130104 4 3050ND53.9 51.8
Acenaphthylene ug/L 50 108 15-137105 3 3050ND53.9 52.4
Aniline ug/L 50 89 10-13083 6 3050ND44.3 41.6
Anthracene ug/L 50 121 37-136118 2 3050ND60.3 59.0
Benzo(a)anthracene ug/L 50 122 40-145123 1 3050ND61.0 61.3
Benzo(a)pyrene ug/L 50 126 41-146126 0 3050ND63.1 63.1
Benzo(b)fluoranthene ug/L 50 126 39-151129 2 3050ND62.9 64.3
Benzo(g,h,i)perylene ug/L 50 127 40-147127 1 3050ND63.7 63.3
Benzo(k)fluoranthene ug/L 50 129 40-146130 1 3050ND64.5 65.0
Benzoic Acid ug/L 250 67 10-13014 30250ND16934.4J
Benzyl alcohol ug/L 100 106 25-130102 3 30100ND106102
bis(2-
Chloroethoxy)methane ug/L 50 116 23-130111 4 3050ND58.0 55.6
bis(2-Chloroethyl) ether ug/L 50 122 25-130114 6 3050ND60.8 57.0
bis(2-Ethylhexyl)phthalate ug/L 50 119 28-166121 2 3050ND59.6 60.6
Butylbenzylphthalate ug/L 50 121 33-165125 3 3050ND60.7 62.5
Chrysene ug/L 50 123 38-141122 1 3050ND61.6 61.1
Di-n-butylphthalate ug/L 50 118 32-153118 0 3050ND59.0 59.2
Di-n-octylphthalate ug/L 50 121 30-175123 2 3050ND60.4 61.4
Dibenz(a,h)anthracene ug/L 50 130 39-148126 3 3050ND65.0 63.2
Dibenzofuran ug/L 50 109 20-130105 4 3050ND54.6 52.7
Diethylphthalate ug/L 50 114 28-142113 1 3050ND57.0 56.4
Dimethylphthalate ug/L 50 114 26-136111 3 3050ND57.0 55.6
Fluoranthene ug/L 50 124 39-143122 2 3050ND61.9 60.9
Fluorene ug/L 50 115 24-132110 5 3050ND57.5 54.8
Hexachloro-1,3-butadiene ug/L 50 79 10-13074 6 3050ND39.6 37.2
Hexachlorobenzene ug/L 50 119 29-130115 4 3050ND59.5 57.4
Hexachlorocyclopentadiene ug/L 50 76 10-13072 5 3050ND37.8 35.8
Hexachloroethane ug/L 50 79 10-13073 9 3050ND39.6 36.3
Indeno(1,2,3-cd)pyrene ug/L 50 130 39-148128 1 3050ND64.8 63.9
Isophorone ug/L 50 109 23-130106 3 3050ND54.7 53.0
N-Nitroso-di-n-propylamine ug/L 50 118 25-130111 7 3050ND59.2 55.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3179892MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92524445019
3179893
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/L 50 101 22-13097 4 3050ND50.4 48.4
N-Nitrosodiphenylamine ug/L 50 114 26-134108 5 3050ND57.2 54.1
Naphthalene ug/L 50 96 14-13091 6 3050ND48.0 45.3
Nitrobenzene ug/L 50 110 25-130106 4 3050ND55.1 53.0
Pentachlorophenol ug/L 100 140 10-175127 9 30100ND140127
Phenanthrene ug/L 50 120 36-133117 3 3050ND60.2 58.5
Phenol ug/L 50 66 10-13063 6 3050ND33.1 31.3
Pyrene ug/L 50 122 40-143122 0 3050ND60.9 60.9
2,4,6-Tribromophenol (S)%S014810-144139
2-Fluorobiphenyl (S)%105 10-130100
2-Fluorophenol (S)%79 10-13073
Nitrobenzene-d5 (S)%111 10-144107
Phenol-d6 (S)%63 10-13059
Terphenyl-d14 (S)%142 34-163143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
603795
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92524499014, 92524499015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3180817
Associated Lab Samples:92524499014, 92524499015
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 03/04/21 11:111.7
1,2-Dichlorobenzene ug/L ND 10.0 03/04/21 11:111.8
1,3-Dichlorobenzene ug/L ND 10.0 03/04/21 11:111.6
1,4-Dichlorobenzene ug/L ND 10.0 03/04/21 11:111.7
1-Methylnaphthalene ug/L ND 10.0 03/04/21 11:112.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 03/04/21 11:111.2
2,4,5-Trichlorophenol ug/L ND 10.0 03/04/21 11:111.4
2,4,6-Trichlorophenol ug/L ND 10.0 03/04/21 11:111.6
2,4-Dichlorophenol ug/L ND 10.0 03/04/21 11:111.4
2,4-Dimethylphenol ug/L ND 10.0 03/04/21 11:111.7
2,4-Dinitrophenol ug/L ND 50.0 03/04/21 11:1126.0
2,4-Dinitrotoluene ug/L ND 10.0 03/04/21 11:111.6
2,6-Dinitrotoluene ug/L ND 10.0 03/04/21 11:111.7
2-Chloronaphthalene ug/L ND 10.0 03/04/21 11:111.7
2-Chlorophenol ug/L ND 10.0 03/04/21 11:111.2
2-Methylnaphthalene ug/L ND 10.0 03/04/21 11:111.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 03/04/21 11:111.9
2-Nitroaniline ug/L ND 20.0 03/04/21 11:113.0
2-Nitrophenol ug/L ND 10.0 03/04/21 11:111.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 03/04/21 11:111.2
3,3'-Dichlorobenzidine ug/L ND 20.0 03/04/21 11:118.1
3-Nitroaniline ug/L ND 20.0 03/04/21 11:113.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 03/04/21 11:113.4
4-Bromophenylphenyl ether ug/L ND 10.0 03/04/21 11:111.8
4-Chloro-3-methylphenol ug/L ND 10.0 03/04/21 11:113.3
4-Chloroaniline ug/L ND 20.0 03/04/21 11:113.6
4-Chlorophenylphenyl ether ug/L ND 10.0 03/04/21 11:112.0
4-Nitroaniline ug/L ND 20.0 03/04/21 11:115.1
4-Nitrophenol ug/L ND 50.0 03/04/21 11:116.6
Acenaphthene ug/L ND 10.0 03/04/21 11:112.0
Acenaphthylene ug/L ND 10.0 03/04/21 11:112.0
Aniline ug/L ND 10.0 03/04/21 11:111.6
Anthracene ug/L ND 10.0 03/04/21 11:112.3
Benzo(a)anthracene ug/L ND 10.0 03/04/21 11:112.7
Benzo(a)pyrene ug/L ND 10.0 03/04/21 11:112.8
Benzo(b)fluoranthene ug/L ND 10.0 03/04/21 11:112.6
Benzo(g,h,i)perylene ug/L ND 10.0 03/04/21 11:112.8
Benzo(k)fluoranthene ug/L ND 10.0 03/04/21 11:112.7
Benzoic Acid ug/L ND 50.0 03/04/21 11:113.4
Benzyl alcohol ug/L ND 20.0 03/04/21 11:112.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3180817
Associated Lab Samples:92524499014, 92524499015
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 03/04/21 11:111.8
bis(2-Chloroethyl) ether ug/L ND 10.0 03/04/21 11:111.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 03/04/21 11:113.7
Butylbenzylphthalate ug/L ND 10.0 03/04/21 11:113.1
Chrysene ug/L ND 10.0 03/04/21 11:112.8
Di-n-butylphthalate ug/L ND 10.0 03/04/21 11:112.2
Di-n-octylphthalate ug/L ND 10.0 03/04/21 11:113.9
Dibenz(a,h)anthracene ug/L ND 10.0 03/04/21 11:113.0
Dibenzofuran ug/L ND 10.0 03/04/21 11:112.1
Diethylphthalate ug/L ND 10.0 03/04/21 11:112.0
Dimethylphthalate ug/L ND 10.0 03/04/21 11:112.1
Fluoranthene ug/L ND 10.0 03/04/21 11:112.2
Fluorene ug/L ND 10.0 03/04/21 11:112.1
Hexachloro-1,3-butadiene ug/L ND 10.0 03/04/21 11:111.8
Hexachlorobenzene ug/L ND 10.0 03/04/21 11:112.2
Hexachlorocyclopentadiene ug/L ND 10.0 03/04/21 11:111.6
Hexachloroethane ug/L ND 10.0 03/04/21 11:111.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 03/04/21 11:112.9
Isophorone ug/L ND 10.0 03/04/21 11:111.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 03/04/21 11:111.3
N-Nitrosodimethylamine ug/L ND 10.0 03/04/21 11:111.9
N-Nitrosodiphenylamine ug/L ND 10.0 03/04/21 11:113.0
Naphthalene ug/L ND 10.0 03/04/21 11:112.1
Nitrobenzene ug/L ND 10.0 03/04/21 11:111.9
Pentachlorophenol ug/L ND 20.0 03/04/21 11:113.8
Phenanthrene ug/L ND 10.0 03/04/21 11:112.0
Phenol ug/L ND 10.0 03/04/21 11:111.4
Pyrene ug/L ND 10.0 03/04/21 11:112.2
2,4,6-Tribromophenol (S)%82 10-144 03/04/21 11:11
2-Fluorobiphenyl (S)%82 10-130 03/04/21 11:11
2-Fluorophenol (S)%67 10-130 03/04/21 11:11
Nitrobenzene-d5 (S)%87 10-144 03/04/21 11:11
Phenol-d6 (S)%55 10-130 03/04/21 11:11
Terphenyl-d14 (S)%149 34-163 03/04/21 11:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3180818LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 27.450 55 18-130
1,2-Dichlorobenzene ug/L 29.150 58 20-130
1,3-Dichlorobenzene ug/L 27.250 54 18-130
1,4-Dichlorobenzene ug/L 28.750 57 18-130
1-Methylnaphthalene ug/L 35.050 70 29-130
2,2'-Oxybis(1-chloropropane)ug/L 38.550 77 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3180818LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 52.150 104 35-130
2,4,6-Trichlorophenol ug/L 48.450 97 31-130
2,4-Dichlorophenol ug/L 46.150 92 35-130
2,4-Dimethylphenol ug/L 47.750 95 34-130
2,4-Dinitrophenol ug/L 267250 107 10-153
2,4-Dinitrotoluene ug/L 59.650 119 37-136
2,6-Dinitrotoluene ug/L 56.350 113 33-136
2-Chloronaphthalene ug/L 34.750 69 26-130
2-Chlorophenol ug/L 42.450 85 37-130
2-Methylnaphthalene ug/L 35.150 70 29-130
2-Methylphenol(o-Cresol)ug/L 44.350 89 35-130
2-Nitroaniline ug/L 102100 102 37-130
2-Nitrophenol ug/L 47.150 94 32-130
3&4-Methylphenol(m&p Cresol)ug/L 44.250 88 34-130
3,3'-Dichlorobenzidine ug/L 117100 117 34-136
3-Nitroaniline ug/L 110100 110 37-138
4,6-Dinitro-2-methylphenol ug/L 107100 107 21-157
4-Bromophenylphenyl ether ug/L 50.250 100 38-130
4-Chloro-3-methylphenol ug/L 103100 103 37-130
4-Chloroaniline ug/L 88.8100 89 38-130
4-Chlorophenylphenyl ether ug/L 48.850 98 33-130
4-Nitroaniline ug/L 118100 118 42-137
4-Nitrophenol ug/L 176250 70 10-130
Acenaphthene ug/L 42.850 86 33-130
Acenaphthylene ug/L 43.850 88 35-130
Aniline ug/L 36.250 72 22-130
Anthracene ug/L 56.250 112 48-130
Benzo(a)anthracene ug/L 63.350 127 48-137
Benzo(a)pyrene ug/L 63.750 127 49-138
Benzo(b)fluoranthene ug/L 63.350 127 52-138
Benzo(g,h,i)perylene ug/L 63.650 127 48-140
Benzo(k)fluoranthene ug/L 64.450 129 48-139
Benzoic Acid ug/L 165250 66 10-130
Benzyl alcohol ug/L 95.2100 95 35-130
bis(2-Chloroethoxy)methane ug/L 47.550 95 34-130
bis(2-Chloroethyl) ether ug/L 46.150 92 36-130
bis(2-Ethylhexyl)phthalate ug/L 61.450 123 32-165
Butylbenzylphthalate ug/L 63.950 128 34-161
Chrysene ug/L 61.350 123 47-131
Di-n-butylphthalate ug/L 68.750 137 39-144
Di-n-octylphthalate ug/L 57.750 115 30-170
Dibenz(a,h)anthracene ug/L 65.750 131 49-138
Dibenzofuran ug/L 44.950 90 33-130
Diethylphthalate ug/L 60.750 121 38-131
Dimethylphthalate ug/L 54.150 108 37-130
Fluoranthene ug/L 62.750 125 46-137
Fluorene ug/L 50.950 102 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 98
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92524499
Monroe Road Site
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3180818LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 23.550 47 11-130
Hexachlorobenzene ug/L 48.050 96 38-130
Hexachlorocyclopentadiene ug/L 21.950 44 10-130
Hexachloroethane ug/L 25.950 52 14-130
Indeno(1,2,3-cd)pyrene ug/L 64.350 129 41-130
Isophorone ug/L 47.450 95 33-130
N-Nitroso-di-n-propylamine ug/L 50.150 100 36-130
N-Nitrosodimethylamine ug/L 36.650 73 34-130
N-Nitrosodiphenylamine ug/L 53.350 107 37-130
Naphthalene ug/L 34.350 69 30-130
Nitrobenzene ug/L 41.750 83 36-130
Pentachlorophenol ug/L 106100 106 23-149
Phenanthrene ug/L 55.950 112 44-130
Phenol ug/L 29.550 59 18-130
Pyrene ug/L 63.450 127 47-134
2,4,6-Tribromophenol (S)%118 10-144
2-Fluorobiphenyl (S)%81 10-130
2-Fluorophenol (S)%65 10-130
Nitrobenzene-d5 (S)%88 10-144
Phenol-d6 (S)%56 10-130
Terphenyl-d14 (S)%149 34-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 98
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92524499
Monroe Road Site
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 98
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92524499
Monroe Road Site
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92524499001 603611 603688GW-1 EPA 3510C EPA 8270E
92524499002 603611 603688GW-2 EPA 3510C EPA 8270E
92524499003 603611 603688GW-3 EPA 3510C EPA 8270E
92524499004 603611 603688GW-4 EPA 3510C EPA 8270E
92524499005 603611 603688GW-5 EPA 3510C EPA 8270E
92524499006 603611 603688GW-6 EPA 3510C EPA 8270E
92524499007 603611 603688GW-7 EPA 3510C EPA 8270E
92524499008 603611 603688GW-8 EPA 3510C EPA 8270E
92524499009 603611 603688GW-9 EPA 3510C EPA 8270E
92524499010 603611 603688GW-10 EPA 3510C EPA 8270E
92524499011 603611 603688GW-14 EPA 3510C EPA 8270E
92524499012 603611 603688GW-12 EPA 3510C EPA 8270E
92524499013 603611 603688GW-13 EPA 3510C EPA 8270E
92524499014 603795 604241GW-16 EPA 3510C EPA 8270E
92524499015 603795 604241GW-17 EPA 3510C EPA 8270E
92524499001 603004GW-1 EPA 8260D
92524499002 603004GW-2 EPA 8260D
92524499003 603004GW-3 EPA 8260D
92524499004 603004GW-4 EPA 8260D
92524499005 603004GW-5 EPA 8260D
92524499006 603004GW-6 EPA 8260D
92524499007 603004GW-7 EPA 8260D
92524499008 603004GW-8 EPA 8260D
92524499009 603004GW-9 EPA 8260D
92524499010 603119GW-10 EPA 8260D
92524499011 603119GW-14 EPA 8260D
92524499012 603258GW-12 EPA 8260D
92524499013 603258GW-13 EPA 8260D
92524499014 603258GW-16 EPA 8260D
92524499015 603119GW-17 EPA 8260D
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/05/2021 10:09 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 98
Page 94 of 98
Page 95 of 98
Page 96 of 98
Page 97 of 98
Page 98 of 98

APPENDIX E

Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-A
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.8E-05 5.5E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-B
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.9E-07 4.4E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-C
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 5.7E-07 4.5E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-D
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 8.3E-07 4.0E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-E
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.0E-07 2.5E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-F
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.5E-07 4.5E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-G
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 9.1E-08 2.4E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-H
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 3.2E-08 1.3E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-I
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.2E-08 5.4E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-J
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.1E-08 8.6E-02 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: Monroe Road Site
Exposure Unit ID: SG-K
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.8E-09 1.9E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator