20026 Kaiser Fluids_soil export request approval SP4_20230929

September 29, 2023 Sent Via E-mail
Hank Farmer Trailhead 530 Owner, LLC Charlotte, NC 28203 [e-mail]
Subject: Soil Management Export Approval Kaiser Fluids Tech II 530 East Sugar Creek Road
Charlotte, Mecklenburg County
Brownfields Project No 20026-16-060
Dear Mr. Farmer: The North Carolina Department of Environmental Quality Brownfields Redevelopment Section (DEQ Brownfields) received a request to export up to 1000 cubic yards of soil from the above referenced
Brownfields Property. This request was submitted on your behalf by Mr. Matt Bramlett of Hart &
Hickman. (H&H) on September 29, 2023 via email. Based on our review of the data provided, DEQ Brownfields agrees that the soils from Soil Pile 4 may be exported to the following options. Stockpiled soils characterized by Soil Pile 4 data may be managed
at Old 27 Landfill (1222 Old 27 Highway, Mount Holly, Gaston County, Permit No. 36A-LCOD-2010),
or a Construction & Demolition (C&D) Landfill, or a Municipal Solid Waste (MSW) Landfill, or at another Brownfields Property with prior DEQ Brownfields approval. Other options may be available; however, DEQ requires that the receiving facility be identified and approved prior to export.
All soil export must be conducted under a DEQ Brownfields approved Environmental Management Plan
(EMP). Soils should be field screened during excavation prior to export from the property. If unanticipated impacts are identified during excavation, please refer to the EMP for further actions and cease transfer until appropriate characterization can be completed. In addition, in accordance with the Kaiser Fluids Tech II Road EMP, an annual Redevelopment Summary Report will be submitted to DEQ
Brownfields. Details related to the disposition of this soil including but not limited to, total volume, general description of field screening efforts, etc. should be included with the Redevelopment Summary Report.
Page 2 of 2

Please be advised that this compliance review from DEQ Brownfields does not waive any applicable requirement to obtain any necessary permits, licenses or certifications which may be required from other state or local entities. If you have any questions, please contact me at (704) 661-10330, or via e-mail at [e-mail].
Sincerely,
Carolyn Minnich Project Manager Brownfields Redevelopment Section ec: Matt Ingalls [e-mail] Kyle McDaniel [e-mail]

From:Matt Ingalls
To:Minnich, Carolyn
Cc:Kyle McDaniel
Subject:[External] Soil Export Request for Kaiser Fluids Tech II BFs (20026-16-060)
Date:Friday, September 29, 2023 9:23:39 AM
Attachments:image007.pngimage013.pngimage008.png
image009.png
image012.pngimage014.pngSoil Stockpile 3&4 Results.pdfTU-004_20230920-FIG 3.pdfTU -004PDFreport_far361-362.PDF
CAUTION: External email. Do not click links or open attachments unless verified. Report suspicious emails with the
Report Message button located on your Outlook menu bar on the Home tab.
Hi Carolyn – based on the results of the recent soil characterization activities, the contractor NVR is
requesting disposal of Soil Pile 4 generated at the former Kaiser Fluids portion of the Kaiser Fluids
Tech II Brownfields Property (#20026-16-060) located in Charlotte, NC to the Old 27 Land Clearing and
Inert Debris (LCID) landfill facility. Soil Pile 4 is approximately 800 cubic yards in size and was
generated during recent grading activities. H&H inspected soil that comprised the soil pile during
recent grading activities and collected samples from the soil pile for characterization purposes.

The Soil Pile 4 sample was derived from five (5) aliquot soil samples collected on September 12, 2023
and no obvious odors, evidence of soil staining, or elevated PID readings were identified during the
characterization sampling activities. Soil pile sampling activities was conducted in accordance with
the DEQ-approved EMP prepared for the Site. The semi-volatile organic compound (SVOC by EPA
Method 8270) and the RCRA metals (plus hexavalent chromium) samples were generated from five
(5) soil aliquot samples (A-E) and composited. The volatile organic compound (VOC) sample was
selected from the aliquot exhibiting the highest PID reading (aliquot C = 3.2 mg/kg).

Laboratory results indicated that VOCs and SVOCs were not detected at concentrations above PSRGs
in the Soil Pile 4 soil sample. Arsenic (2.4 mg/kg) was detected in the Soil Pile 4 sample at a
concentration slightly above the residential PSRG (0.68 mg/kg) and consistent with regional
background concentrations. Based on this information, we request written approval for DEQ to allow
export of soil from Soil Pile 4 to the Highway 29 LCID Landfill. Note, the soil in Soil Pile 3 will be sent
to the Republic Services Speedway MSWLF based on the results of the soil characterization sampling
activities.

From: Kyle McDaniel <[e-mail]>
Sent: Wednesday, September 20, 2023 1:19 PM
To: Matt Ingalls <[e-mail]>
Subject: RE: PDF H&H - T&U -004 23-255-0005

Matt,

Please find attached tabulated results for Soil Pile 3 and Soil Pile 4. I’ve also attached figures showing
where Soil Piles 3 & 4 are located (one with the proposed building footprint and one without).

The duplicate results are a little wonky.

Please let me know if there’s anything else you need.

Sincerely,
Kyle

Kyle McDaniel, Assistant Project GeologistHart & Hickman, PC2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-887-4632 · Mobile: [phone]
www.harthickman.com

From: Matt Ingalls <[e-mail]>
Sent: Wednesday, September 20, 2023 11:27 AM
To: Kyle McDaniel <[e-mail]>
Subject: RE: PDF H&H - T&U -004 23-255-0005

Thanks.

From: Kyle McDaniel <[e-mail]>
Sent: Wednesday, September 20, 2023 8:39 AM
To: Matt Ingalls <[e-mail]>
Subject: RE: PDF H&H - T&U -004 23-255-0005

Thanks, Matt. I’ll get this tabulated and get a table and figure over to you today.

Sincerely,
Kyle

Kyle McDaniel, Assistant Project Geologist
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 · Charlotte, NC 28203
Direct: 704-887-4632 · Mobile: [phone]
www.harthickman.com

From: Matt Ingalls <[e-mail]>
Sent: Tuesday, September 19, 2023 6:56 PM
To: Kyle McDaniel <[e-mail]>
Subject: FW: PDF H&H - T&U -004 23-255-0005

Kyle – lab data attached for 530 E Sugar Creek soil piles.

From: Waypoint Analytical, Inc. <[e-mail]>
Sent: Tuesday, September 19, 2023 2:32 PM
To: Matt Ingalls <[e-mail]>
Subject: PDF H&H - T&U -004 23-255-0005

XFMRHHSB-1
HHSB-2
HHSB-29
HHSB-3
HHSB-4
HHSB-5
HHSB-6
HHSB-9
HHSB-7 HHSB-8
HHSB-10
HHSB-11
MW-11
MW-5
RW-2
RW-1
RW-4
RW-3
MW-1
MW-2
MW-8
MW-3
MW-7
MW-4
MW-6
SB-6/TMW-2
RW-1A
SB-9/TMW-3
MW-9
SB-1/TMW-1
MW-10
HHTMW-1
HHTMW-3
HHTMW-4
HHTMW-2
SB-3
SB-2
SB-4
SB-5
SB-7
SB-8
SB-12
SB-13
SB-11
SB-10
REVISION NO. 0
JOB NO. T&U-004
DATE: 9-20-23
FIGURE NO. 3
KAISER FLUIDS TECH II
BROWNFIELDS PROPERTY
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
530 E. SUGAR CREEK ROAD
(FORMER KAISER FLUIDS)
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1.AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS, 2023.
2.PROPOSED BUILDING FOOTPRINT OBTAINED FROM NILES
BOLTON ASSOCIATES, DATED 7-25-2022.
KEITH CLINIC ESTRAMONTE
CHIROPRACTIC
(402 E. SUGAR CREEK ROAD)
CONCRETE SUPPLY CO.
(3940 GREENSBORO STREET)
MULTI-TENANT WAREHOUSE /
INDUSTRIAL BUILDING
(4001 RALEIGH STREET)
VACANT COMMERCIAL BUILDING -
FORMER TRYON MALL CLEANING
CENTER DRY CLEANER
(451 E. SUGAR CREEK ROAD)
RALEIGH STRE
E
T E.
SUGAR
CREEK
ROAD
NORTH
COURTYARD
PARKING
DECK
SOUTH
COURTYARD
BUILDING
300
BUILDING
100B
BUILDING
100A
BUILDING
200
PLACEMENT OF
SOILS FROM 4100
RALEIGH STREET
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
ABANDONED GROUNDWATER MONITORING
WELL
SOIL BORING (SEPTEMBER 2011)
CO-LOCATED SOIL BORING AND TEMPORARY
MONITORING WELL (SEPTEMBER 2011)
SOIL BORING (OCTOBER 2018)
TEMPORARY MONITORING WELL (OCTOBER
2018)
SOIL GAS SAMPLE (OCTOBER 2018)
SUB-SLAB VAPOR SAMPLE (OCTOBER 2018)
FORMER SETTLING TANK EXCAVATION
SOIL PILE 4
SOIL PILE 3
S:\AAA-Master Projects\Third & Urban\T&U-004 530 Sugar Creek (Kaiser Fluids Tech)\Soil Management\Figures\TU-004_20230905.dwg, FIG 3, 9/20/2023 9:26:53 AM, tmarbuery
Table 1
Summary of Soil Stockpile Analytical Results
Kaiser Fluids Tech II
Charlotte, North Carolina
H&H Job No. T&U-004
Sample ID Soil Pile 4
Estimated Volume (cy)1,000
Date Collected 9/12/2023
VOCs (8260D)
Acetone 0.012 J 0.013 J 0.018 J 25 14,000 210,000 ----
n-Hexane 0.001 J 0.001 J <0.0008 55 130 540 ----
Methylene Chloride 0.009 J 0.008 J 0.002 J 0.025 58 650 ----
SVOCs (8270)
Benzo(a)anthracene <0.170 0.253 J <0.178 0.35 1.1 21 ----
Benzo(a)pyrene <0.180 0.212 J <0.188 0.12 0.11 2.1 ----
Benzo(b)fluoranthene <0.179 0.299 J <0.187 1.2 1.1 21 ----
Chrysene <0.174 0.228 J <0.182 36 11 2,100 ----
Fluoranthene 0.187 J 0.376 J 0.246 J 670 480 6,000 ----Pyrene 0.168 J 0.339 J 0.206 J 440 360 4,500 ----
RCRA Metals (6020B/7471B/7199)
Arsenic 2.25 2.26 2.40 5.8 0.68 3.0 3.1 - 3.7 3.4Barium64.2 63.4 75.0 580 3,100 47,000 58 - 79 66Cadmium0.168 J 0.179 J 0.150 J 3.0 1.4 20 0.38 - 1.1 0.87
Chromium (Total)53.6 41.2 48.4 360,000 NE NE 35 - 50 42
Hexavalent Chromium <0.173 <0.178 <0.181 3.8 0.31 6.5 0.18 - 0.44 0.31Trivalent Chromium**53.6 41.2 48.4 360,000 23,000 350,000 36.62 - 49.56 41.7
Lead 17.4 19.1 19.8 270 400 800 5.8 - 30 14.6Mercury0.0317 J 0.0427 0.0433 1.0 2.3 9.7 0.014 - 0.037 0.025Selenium0.747 0.718 0.738 2.1 78 1,200 2.9 - 6.7 4.7Silver0.0749 J 0.0736 J 0.0872 J 3.4 78 1,200 0.078 - 0.20 0.15
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs), dated July 2023
Soil concentrations are reported in milligrams per kilogram (mg/kg)
**Trivalent Chromium = Chromium (Total) - Hexavalent Chromium
Laboratory analytical methods are shown in parentheses
VOCs = volatile organic compounds
SVOCs = semi-volatile organic compounds
RCRA = Resource Conservation and Recovery ActBold values exceed DEQ Protection of Groundwater PSRGs
Underlined values exceed Residential PSRGs
J = estimated value between the laboratory detection limit and the laboratory reporting limit
cy = cubic yards
With the exception of metals, only those compounds detected in at least one sample are shown above
NE = not established
-- = not applicable
Sample Location
Screening Criteria (1)Site Specific Background
Generated on-Site
10/2/2018
Protection of
Groundwater
PSRGs
Range Mean
Soil Stockpile
Soil Pile 3 / Soil Pile Dup
1,000
9/12/2023
Residential
PSRGs
Industrial/
Commercial
PSRGs
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Third & Urban/T&U-004 530 Sugar Creek (Kaiser Fluids Tech)/Soil Management/Table/Soil Stockpile Results
9/20/2023
Table 1 (Page 1 of 1)
Hart & Hickman, PC

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

9/19/2023
Hart & Hickman (Charlotte) Matt Ingalls
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-255-0005 Client Project Description: T&U -004
Dear Matt Ingalls:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 9/12/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 49
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202437735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202499012State ProgramSouth Carolina
12/31/202399012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20242904State ProgramCalifornia
06/30/2024E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202404015State ProgramGeorgia
10/31/2024200078State Program - NELAPIllinois
06/30/202480215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202404015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202447701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202400106State ProgramVirginia
09/14/2024460181State Program - NELAPVirginia
Page 1 of 1 00016/23-255-0005
Page 2 of 49
Report Number:
Sample Summary Table
Client Project Description:
23-255-0005
T&U -004
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
09/12/2023 09:55Solids 94734 Soil Pile 3 09/12/2023 10:50
09/12/2023 09:55Solids 94734 Soil Pile 3 09/12/2023 10:50 6020B WP MTN -
09/12/2023 09:55Solids 94734 Soil Pile 3 09/12/2023 10:50 SW-7199 WP MTN -
09/12/2023 10:20Solids 94735 Soil Pile 4 09/12/2023 10:50
09/12/2023 10:20Solids 94735 Soil Pile 4 09/12/2023 10:50 SW-7199 WP MTN -
09/12/2023 10:20Solids 94735 Soil Pile 4 09/12/2023 10:50 6020B WP MTN -
09/12/2023Solids 94736 Soil Pile Dup 09/12/2023 10:50
09/12/2023Solids 94736 Soil Pile Dup 09/12/2023 10:50 SW-7199 WP MTN -
09/12/2023Solids 94736 Soil Pile Dup 09/12/2023 10:50 6020B WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 49
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-255-0005
Report Limit
Project:T&U -004
V 94734Soil Pile 3
2.25 09/15/2023 02:376020BArsenicmg/Kg - dry 0.105
64.2 09/15/2023 02:376020BBariummg/Kg - dry 0.052
J0.168 09/15/2023 02:376020BCadmiummg/Kg - dry 0.0319
53.6 09/15/2023 02:376020BChromiummg/Kg - dry 0.142
17.4 09/15/2023 19:496020BLeadmg/Kg - dry 0.0380
0.747 09/15/2023 02:376020BSeleniummg/Kg - dry 0.126
J0.0749 09/15/2023 02:376020BSilvermg/Kg - dry 0.0082
J0.0317 09/13/2023 15:317471BMercury (Total)mg/Kg - dry 0.0147
J0.012 09/12/2023 15:288260DAcetonemg/Kg - dry 0.002
J0.001 09/12/2023 15:288260Dn-Hexane mg/Kg - dry 0.0008
J0.009 09/12/2023 15:288260DMethylene Chloride mg/Kg - dry 0.001
J0.187 09/14/2023 15:508270EFluoranthenemg/Kg - dry 0.150
J0.168 09/14/2023 15:508270EPyrenemg/Kg - dry 0.164
18.5 09/14/2023 10:10SW-DRYWT Moisture %
V 94735Soil Pile 4
2.40 09/15/2023 02:416020BArsenicmg/Kg - dry 0.110
75.0 09/15/2023 02:416020BBariummg/Kg - dry 0.054
J0.150 09/15/2023 02:416020BCadmiummg/Kg - dry 0.0333
48.4 09/15/2023 02:416020BChromiummg/Kg - dry 0.148
19.8 09/15/2023 19:536020BLeadmg/Kg - dry 0.0397
0.738 09/15/2023 02:416020BSeleniummg/Kg - dry 0.132
J0.0872 09/15/2023 02:416020BSilvermg/Kg - dry 0.0086
0.0433 09/13/2023 15:347471BMercury (Total)mg/Kg - dry 0.0154
J0.018 09/12/2023 16:508260DAcetonemg/Kg - dry 0.003
J0.002 09/12/2023 16:508260DMethylene Chloride mg/Kg - dry 0.001
J0.246 09/14/2023 16:138270EFluoranthenemg/Kg - dry 0.157
J0.206 09/14/2023 16:138270EPyrenemg/Kg - dry 0.172
22.1 09/14/2023 10:10SW-DRYWT Moisture %
V 94736Soil Pile Dup
2.26 09/15/2023 02:456020BArsenicmg/Kg - dry 0.108
63.4 09/15/2023 02:456020BBariummg/Kg - dry 0.054
J0.179 09/15/2023 02:456020BCadmiummg/Kg - dry 0.0329
41.2 09/15/2023 02:456020BChromiummg/Kg - dry 0.147
19.1 09/15/2023 19:576020BLeadmg/Kg - dry 0.0392
0.718 09/15/2023 02:456020BSeleniummg/Kg - dry 0.130
J0.0736 09/15/2023 02:456020BSilvermg/Kg - dry 0.0085
Page 4 of 49
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-255-0005
Report Limit
Project:T&U -004
V 94736Soil Pile Dup
0.0427 09/13/2023 15:367471BMercury (Total)mg/Kg - dry 0.0152
J0.013 09/12/2023 16:238260DAcetonemg/Kg - dry 0.003
J0.001 09/12/2023 16:238260Dn-Hexane mg/Kg - dry 0.0008
J0.008 09/12/2023 16:238260DMethylene Chloride mg/Kg - dry 0.001
J0.253 09/14/2023 16:368270EBenzo(a)anthracene mg/Kg - dry 0.176
J0.212 09/14/2023 16:368270EBenzo(a)pyrene mg/Kg - dry 0.186
J0.299 09/14/2023 16:368270EBenzo(b)fluoranthene mg/Kg - dry 0.185
J0.228 09/14/2023 16:368270EChrysenemg/Kg - dry 0.179
J0.376 09/14/2023 16:368270EFluoranthenemg/Kg - dry 0.155
J0.339 09/14/2023 16:368270EPyrenemg/Kg - dry 0.169
21.1 09/14/2023 10:10SW-DRYWT Moisture %
Page 5 of 49

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: T&U -004 Lab Report Number: 23-255-0005
Date: 9/18/2023
Metals Analyses Method 6020B Sample 94708 (SB-1) Analyte: Arsenic
QC Batch No: L704586/L704365 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94708 (SB-1)
Analyte: Barium QC Batch No: L704586/L704365
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94708 (SB-1)
Analyte: Chromium QC Batch No: L704586/L704365
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94708 (SB-1) Analyte: Lead QC Batch No: L704856/L704365
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 94708 (SB-1) Analyte: Selenium QC Batch No: L704586/L704365 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Aniline QC Batch No: V37800/V37786 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Page 6 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
18.5 %Moisture 1 09/14/23 10:10 SW-DRYWTCNC
<0.173 mg/Kg - dry 0.173 0.245Chromium, Hexavalent 1 09/17/23 12:27 SW-7199NFP
2.25 mg/Kg - dry 0.105 0.307Arsenic 5 09/15/23 02:37 6020BCPW
64.2 mg/Kg - dry 0.052 0.306Barium 5 09/15/23 02:37 6020BCPW
0.168 J mg/Kg - dry 0.0319 0.307Cadmium 5 09/15/23 02:37 6020BCPW
53.6 mg/Kg - dry 0.142 0.306
Chromium 5 09/15/23 02:37 6020BCPW
17.4 mg/Kg - dry 0.0380 0.307Lead 5 09/15/23 19:49 6020BCPW
0.0317 J mg/Kg - dry 0.0147 0.0368Mercury (Total)1 09/13/23 15:31 7471BJKC
0.747 mg/Kg - dry 0.126 0.306Selenium 5 09/15/23 02:37 6020BCPW
0.0749 J mg/Kg - dry 0.0082 0.307Silver 5 09/15/23 02:37 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
0.012 J mg/Kg - dry 0.002 0.024Acetone 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.024Acrolein 1 09/12/23 15:28 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/12/23 15:28 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/12/23 15:28 V37758TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/12/23 15:28 V37758TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/12/23 15:28 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/12/23 15:28 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/12/23 15:28 V37758TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/12/23 15:28 V37758TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/12/23 15:28 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/12/23 15:28 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/12/23 15:28 V37758TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/12/23 15:28 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.006
1,1-Dichloropropene 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/12/23 15:28 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 09/12/23 15:28 V37758TBL
<0.017 mg/Kg - dry 0.017 0.306Ethanol 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.061Ethyl Tertiary Butyl Ether (ETBE)1 09/12/23 15:28 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 09/12/23 15:28 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0242-Hexanone 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/12/23 15:28 V37758TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 09/12/23 15:28 V37758TBL
0.009 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/12/23 15:28 V37758TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 09/12/23 15:28 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/12/23 15:28 V37758TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/12/23 15:28 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/12/23 15:28 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/12/23 15:28 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/12/23 15:28 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/12/23 15:28 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/12/23 15:28 V37758
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%09/12/23 15:281 TBL V37758
Surrogate: Dibromofluoromethane 106 Limits: 84-123%09/12/23 15:281 TBL V37758
Surrogate: Toluene-d8 95.5 Limits: 76-129%09/12/23 15:281 TBL V37758
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.142 mg/Kg - dry 0.142 0.809Acenaphthene 1 09/14/23 15:50 V37800AMP
<0.128 mg/Kg - dry 0.128 0.809Acenaphthylene 1 09/14/23 15:50 V37800AMP
<0.186 mg/Kg - dry 0.186 0.809Aniline 1 09/14/23 15:50 V37800AMP
<0.175 mg/Kg - dry 0.175 0.809Anthracene 1 09/14/23 15:50 V37800AMP
<0.170 mg/Kg - dry 0.170 0.809
Benzo(a)anthracene 1 09/14/23 15:50 V37800AMP
<0.180 mg/Kg - dry 0.180 0.809Benzo(a)pyrene 1 09/14/23 15:50 V37800AMP
<0.179 mg/Kg - dry 0.179 0.809Benzo(b)fluoranthene 1 09/14/23 15:50 V37800AMP
<0.166 mg/Kg - dry 0.166 0.809Benzo(g,h,i)perylene 1 09/14/23 15:50 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.168 mg/Kg - dry 0.168 0.809Benzo(k)fluoranthene 1 09/14/23 15:50 V37800AMP
<0.711 mg/Kg - dry 0.711 2.45Benzoic Acid 1 09/14/23 15:50 V37800AMP
<0.128 mg/Kg - dry 0.128 0.809Benzyl alcohol 1 09/14/23 15:50 V37800AMP
<0.144 mg/Kg - dry 0.144 0.809Bis(2-Chloroethoxy)methane 1 09/14/23 15:50 V37800AMP
<0.131 mg/Kg - dry 0.131 0.809Bis(2-Chloroethyl)ether 1 09/14/23 15:50 V37800AMP
<0.166 mg/Kg - dry 0.166 0.404Bis(2-Chloroisopropyl)ether 1 09/14/23 15:50 V37800AMP
<0.147 mg/Kg - dry 0.147 0.809Bis(2-ethylhexyl)phthalate 1 09/14/23 15:50 V37800AMP
<0.133 mg/Kg - dry 0.133 0.8094-Bromophenyl phenyl ether 1 09/14/23 15:50 V37800AMP
<0.138 mg/Kg - dry 0.138 0.404
Butyl benzyl phthalate 1 09/14/23 15:50 V37800AMP
<0.113 mg/Kg - dry 0.113 0.8094-Chloro-3-methylphenol 1 09/14/23 15:50 V37800AMP
<0.137 mg/Kg - dry 0.137 0.4044-Chloroaniline 1 09/14/23 15:50 V37800AMP
<0.142 mg/Kg - dry 0.142 0.8092-Chloronaphthalene 1 09/14/23 15:50 V37800AMP
<0.120 mg/Kg - dry 0.120 0.8092-Chlorophenol 1 09/14/23 15:50 V37800AMP
<0.154 mg/Kg - dry 0.154 1.234-Chlorophenyl phenyl ether 1 09/14/23 15:50 V37800AMP
<0.174 mg/Kg - dry 0.174 0.809Chrysene 1 09/14/23 15:50 V37800AMP
<0.282 mg/Kg - dry 0.282 0.809
Dibenz(a,h)anthracene 1 09/14/23 15:50 V37800AMP
<0.146 mg/Kg - dry 0.146 0.809Dibenzofuran 1 09/14/23 15:50 V37800AMP
<0.115 mg/Kg - dry 0.115 0.8091,2-Dichlorobenzene 1 09/14/23 15:50 V37800AMP
<0.119 mg/Kg - dry 0.119 0.8091,3-Dichlorobenzene 1 09/14/23 15:50 V37800AMP
<0.119 mg/Kg - dry 0.119 0.4041,4-Dichlorobenzene 1 09/14/23 15:50 V37800AMP
<0.180 mg/Kg - dry 0.180 0.8093,3'-Dichlorobenzidine 1 09/14/23 15:50 V37800AMP
<0.117 mg/Kg - dry 0.117 0.8092,4-Dichlorophenol 1 09/14/23 15:50 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.220 mg/Kg - dry 0.220 0.809Diethyl phthalate 1 09/14/23 15:50 V37800AMP
<0.213 mg/Kg - dry 0.213 0.809Dimethyl phthalate 1 09/14/23 15:50 V37800AMP
<0.132 mg/Kg - dry 0.132 0.4042,4-Dimethylphenol 1 09/14/23 15:50 V37800AMP
<0.131 mg/Kg - dry 0.131 0.809Di-n-butyl phthalate 1 09/14/23 15:50 V37800AMP
<0.294 mg/Kg - dry 0.294 1.844,6-Dinitro-2-methylphenol 1 09/14/23 15:50 V37800AMP
<0.638 mg/Kg - dry 0.638 1.842,4-Dinitrophenol 1 09/14/23 15:50 V37800AMP
<0.118 mg/Kg - dry 0.118 0.8092,4-Dinitrotoluene 1 09/14/23 15:50 V37800AMP
<0.132 mg/Kg - dry 0.132 0.8092,6-Dinitrotoluene 1 09/14/23 15:50 V37800AMP
<0.175 mg/Kg - dry 0.175 0.404
Di-n-Octyl Phthalate 1 09/14/23 15:50 V37800AMP
0.187 J mg/Kg - dry 0.150 0.809Fluoranthene 1 09/14/23 15:50 V37800AMP
<0.157 mg/Kg - dry 0.157 0.809Fluorene 1 09/14/23 15:50 V37800AMP
<0.130 mg/Kg - dry 0.130 0.809Hexachlorobenzene 1 09/14/23 15:50 V37800AMP
<0.119 mg/Kg - dry 0.119 0.809Hexachlorobutadiene 1 09/14/23 15:50 V37800AMP
<0.192 mg/Kg - dry 0.192 0.809Hexachlorocyclopentadiene 1 09/14/23 15:50 V37800AMP
<0.097 mg/Kg - dry 0.097 0.809Hexachloroethane 1 09/14/23 15:50 V37800AMP
<0.219 mg/Kg - dry 0.219 0.809
Indeno(1,2,3-cd)pyrene 1 09/14/23 15:50 V37800AMP
<0.234 mg/Kg - dry 0.234 0.809Isophorone 1 09/14/23 15:50 V37800AMP
<0.130 mg/Kg - dry 0.130 0.8091-Methylnaphthalene 1 09/14/23 15:50 V37800AMP
<0.122 mg/Kg - dry 0.122 0.8092-Methylnaphthalene 1 09/14/23 15:50 V37800AMP
<0.119 mg/Kg - dry 0.119 0.8092-Methylphenol 1 09/14/23 15:50 V37800AMP
<0.104 mg/Kg - dry 0.104 0.8093&4 Methylphenol 1 09/14/23 15:50 V37800AMP
<0.176 mg/Kg - dry 0.176 0.809Naphthalene 1 09/14/23 15:50 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 3
94734 Matrix:
9/12/2023 9:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.118 mg/Kg - dry 0.118 0.8092-Nitroaniline 1 09/14/23 15:50 V37800AMP
<0.147 mg/Kg - dry 0.147 0.8093-Nitroaniline 1 09/14/23 15:50 V37800AMP
<0.114 mg/Kg - dry 0.114 0.4044-Nitroaniline 1 09/14/23 15:50 V37800AMP
<0.142 mg/Kg - dry 0.142 0.404Nitrobenzene 1 09/14/23 15:50 V37800AMP
<0.108 mg/Kg - dry 0.108 0.8092-Nitrophenol 1 09/14/23 15:50 V37800AMP
<0.143 mg/Kg - dry 0.143 0.8094-Nitrophenol 1 09/14/23 15:50 V37800AMP
<0.322 mg/Kg - dry 0.322 0.809N-Nitrosodimethylamine 1 09/14/23 15:50 V37800AMP
<0.222 mg/Kg - dry 0.222 0.809N-Nitrosodiphenylamine 1 09/14/23 15:50 V37800AMP
<0.144 mg/Kg - dry 0.144 0.809
N-Nitroso-di-n-propylamine 1 09/14/23 15:50 V37800AMP
<0.425 mg/Kg - dry 0.425 1.23Pentachlorophenol 1 09/14/23 15:50 V37800AMP
<0.255 mg/Kg - dry 0.255 0.809Phenanthrene 1 09/14/23 15:50 V37800AMP
<0.137 mg/Kg - dry 0.137 0.809Phenol 1 09/14/23 15:50 V37800AMP
0.168 J mg/Kg - dry 0.164 0.809Pyrene 1 09/14/23 15:50 V37800AMP
<0.097 mg/Kg - dry 0.097 0.404Pyridine 1 09/14/23 15:50 V37800AMP
<0.131 mg/Kg - dry 0.131 0.8091,2,4-Trichlorobenzene 1 09/14/23 15:50 V37800AMP
<0.118 mg/Kg - dry 0.118 0.809
2,4,5-Trichlorophenol 1 09/14/23 15:50 V37800AMP
<0.118 mg/Kg - dry 0.118 0.8092,4,6-Trichlorophenol 1 09/14/23 15:50 V37800AMP
8270ESurrogate: Phenol-d5 62.5 Limits: 34-121%09/14/23 15:501 AMP
Surrogate: 2-Fluorobiphenyl 75.4 Limits: 44-115%09/14/23 15:501 AMP V37800
Surrogate: 2-Fluorophenol 64.6 Limits: 35-115%09/14/23 15:501 AMP V37800
Surrogate: Nitrobenzene-d5 70.7 Limits: 37-122%09/14/23 15:501 AMP V37800
Surrogate: 4-Terphenyl-d14 77.8 Limits: 54-127%09/14/23 15:501 AMP V37800
Surrogate: 2,4,6-Tribromophenol 68.5 Limits: 39-132%09/14/23 15:501 AMP V37800
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
22.1 %Moisture 1 09/14/23 10:10 SW-DRYWTCNC
<0.181 mg/Kg - dry 0.181 0.256Chromium, Hexavalent 1 09/17/23 12:38 SW-7199NFP
2.40 mg/Kg - dry 0.110 0.321Arsenic 5 09/15/23 02:41 6020BCPW
75.0 mg/Kg - dry 0.054 0.320Barium 5 09/15/23 02:41 6020BCPW
0.150 J mg/Kg - dry 0.0333 0.321Cadmium 5 09/15/23 02:41 6020BCPW
48.4 mg/Kg - dry 0.148 0.320
Chromium 5 09/15/23 02:41 6020BCPW
19.8 mg/Kg - dry 0.0397 0.321Lead 5 09/15/23 19:53 6020BCPW
0.0433 mg/Kg - dry 0.0154 0.0385Mercury (Total)1 09/13/23 15:34 7471BJKC
0.738 mg/Kg - dry 0.132 0.320Selenium 5 09/15/23 02:41 6020BCPW
0.0872 J mg/Kg - dry 0.0086 0.321Silver 5 09/15/23 02:41 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
0.018 J mg/Kg - dry 0.003 0.025Acetone 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/12/23 16:50 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/12/23 16:50 V37758TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/12/23 16:50 V37758TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/12/23 16:50 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 09/12/23 16:50 V37758TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/12/23 16:50 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/12/23 16:50 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/12/23 16:50 V37758TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/12/23 16:50 V37758TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/12/23 16:50 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/12/23 16:50 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/12/23 16:50 V37758TBL
<0.017 mg/Kg - dry 0.017 0.320Ethanol 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.064Ethyl Tertiary Butyl Ether (ETBE)1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/12/23 16:50 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/12/23 16:50 V37758TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/12/23 16:50 V37758TBL
0.002 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/12/23 16:50 V37758TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 09/12/23 16:50 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/12/23 16:50 V37758TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/12/23 16:50 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/12/23 16:50 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/12/23 16:50 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/12/23 16:50 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/12/23 16:50 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/12/23 16:50 V37758
Surrogate: 4-Bromofluorobenzene 110 Limits: 70-130%09/12/23 16:501 TBL V37758
Surrogate: Dibromofluoromethane 105 Limits: 84-123%09/12/23 16:501 TBL V37758
Surrogate: Toluene-d8 97.0 Limits: 76-129%09/12/23 16:501 TBL V37758
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.148 mg/Kg - dry 0.148 0.847Acenaphthene 1 09/14/23 16:13 V37800AMP
<0.134 mg/Kg - dry 0.134 0.847Acenaphthylene 1 09/14/23 16:13 V37800AMP
<0.195 mg/Kg - dry 0.195 0.847Aniline 1 09/14/23 16:13 V37800AMP
<0.183 mg/Kg - dry 0.183 0.847Anthracene 1 09/14/23 16:13 V37800AMP
<0.178 mg/Kg - dry 0.178 0.847
Benzo(a)anthracene 1 09/14/23 16:13 V37800AMP
<0.188 mg/Kg - dry 0.188 0.847Benzo(a)pyrene 1 09/14/23 16:13 V37800AMP
<0.187 mg/Kg - dry 0.187 0.847Benzo(b)fluoranthene 1 09/14/23 16:13 V37800AMP
<0.174 mg/Kg - dry 0.174 0.847Benzo(g,h,i)perylene 1 09/14/23 16:13 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.175 mg/Kg - dry 0.175 0.847Benzo(k)fluoranthene 1 09/14/23 16:13 V37800AMP
<0.744 mg/Kg - dry 0.744 2.57Benzoic Acid 1 09/14/23 16:13 V37800AMP
<0.134 mg/Kg - dry 0.134 0.847Benzyl alcohol 1 09/14/23 16:13 V37800AMP
<0.151 mg/Kg - dry 0.151 0.847Bis(2-Chloroethoxy)methane 1 09/14/23 16:13 V37800AMP
<0.137 mg/Kg - dry 0.137 0.847Bis(2-Chloroethyl)ether 1 09/14/23 16:13 V37800AMP
<0.174 mg/Kg - dry 0.174 0.423Bis(2-Chloroisopropyl)ether 1 09/14/23 16:13 V37800AMP
<0.154 mg/Kg - dry 0.154 0.847Bis(2-ethylhexyl)phthalate 1 09/14/23 16:13 V37800AMP
<0.139 mg/Kg - dry 0.139 0.8474-Bromophenyl phenyl ether 1 09/14/23 16:13 V37800AMP
<0.145 mg/Kg - dry 0.145 0.423
Butyl benzyl phthalate 1 09/14/23 16:13 V37800AMP
<0.118 mg/Kg - dry 0.118 0.8474-Chloro-3-methylphenol 1 09/14/23 16:13 V37800AMP
<0.143 mg/Kg - dry 0.143 0.4234-Chloroaniline 1 09/14/23 16:13 V37800AMP
<0.148 mg/Kg - dry 0.148 0.8472-Chloronaphthalene 1 09/14/23 16:13 V37800AMP
<0.126 mg/Kg - dry 0.126 0.8472-Chlorophenol 1 09/14/23 16:13 V37800AMP
<0.161 mg/Kg - dry 0.161 1.284-Chlorophenyl phenyl ether 1 09/14/23 16:13 V37800AMP
<0.182 mg/Kg - dry 0.182 0.847Chrysene 1 09/14/23 16:13 V37800AMP
<0.295 mg/Kg - dry 0.295 0.847
Dibenz(a,h)anthracene 1 09/14/23 16:13 V37800AMP
<0.152 mg/Kg - dry 0.152 0.847Dibenzofuran 1 09/14/23 16:13 V37800AMP
<0.121 mg/Kg - dry 0.121 0.8471,2-Dichlorobenzene 1 09/14/23 16:13 V37800AMP
<0.124 mg/Kg - dry 0.124 0.8471,3-Dichlorobenzene 1 09/14/23 16:13 V37800AMP
<0.125 mg/Kg - dry 0.125 0.4231,4-Dichlorobenzene 1 09/14/23 16:13 V37800AMP
<0.188 mg/Kg - dry 0.188 0.8473,3'-Dichlorobenzidine 1 09/14/23 16:13 V37800AMP
<0.122 mg/Kg - dry 0.122 0.8472,4-Dichlorophenol 1 09/14/23 16:13 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.231 mg/Kg - dry 0.231 0.847Diethyl phthalate 1 09/14/23 16:13 V37800AMP
<0.223 mg/Kg - dry 0.223 0.847Dimethyl phthalate 1 09/14/23 16:13 V37800AMP
<0.138 mg/Kg - dry 0.138 0.4232,4-Dimethylphenol 1 09/14/23 16:13 V37800AMP
<0.137 mg/Kg - dry 0.137 0.847Di-n-butyl phthalate 1 09/14/23 16:13 V37800AMP
<0.308 mg/Kg - dry 0.308 1.934,6-Dinitro-2-methylphenol 1 09/14/23 16:13 V37800AMP
<0.667 mg/Kg - dry 0.667 1.932,4-Dinitrophenol 1 09/14/23 16:13 V37800AMP
<0.124 mg/Kg - dry 0.124 0.8472,4-Dinitrotoluene 1 09/14/23 16:13 V37800AMP
<0.138 mg/Kg - dry 0.138 0.8472,6-Dinitrotoluene 1 09/14/23 16:13 V37800AMP
<0.183 mg/Kg - dry 0.183 0.423
Di-n-Octyl Phthalate 1 09/14/23 16:13 V37800AMP
0.246 J mg/Kg - dry 0.157 0.847Fluoranthene 1 09/14/23 16:13 V37800AMP
<0.164 mg/Kg - dry 0.164 0.847Fluorene 1 09/14/23 16:13 V37800AMP
<0.136 mg/Kg - dry 0.136 0.847Hexachlorobenzene 1 09/14/23 16:13 V37800AMP
<0.125 mg/Kg - dry 0.125 0.847Hexachlorobutadiene 1 09/14/23 16:13 V37800AMP
<0.201 mg/Kg - dry 0.201 0.847Hexachlorocyclopentadiene 1 09/14/23 16:13 V37800AMP
<0.101 mg/Kg - dry 0.101 0.847Hexachloroethane 1 09/14/23 16:13 V37800AMP
<0.229 mg/Kg - dry 0.229 0.847
Indeno(1,2,3-cd)pyrene 1 09/14/23 16:13 V37800AMP
<0.245 mg/Kg - dry 0.245 0.847Isophorone 1 09/14/23 16:13 V37800AMP
<0.136 mg/Kg - dry 0.136 0.8471-Methylnaphthalene 1 09/14/23 16:13 V37800AMP
<0.128 mg/Kg - dry 0.128 0.8472-Methylnaphthalene 1 09/14/23 16:13 V37800AMP
<0.124 mg/Kg - dry 0.124 0.8472-Methylphenol 1 09/14/23 16:13 V37800AMP
<0.108 mg/Kg - dry 0.108 0.8473&4 Methylphenol 1 09/14/23 16:13 V37800AMP
<0.184 mg/Kg - dry 0.184 0.847Naphthalene 1 09/14/23 16:13 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile 4
94735 Matrix:
9/12/2023 10:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.124 mg/Kg - dry 0.124 0.8472-Nitroaniline 1 09/14/23 16:13 V37800AMP
<0.154 mg/Kg - dry 0.154 0.8473-Nitroaniline 1 09/14/23 16:13 V37800AMP
<0.119 mg/Kg - dry 0.119 0.4234-Nitroaniline 1 09/14/23 16:13 V37800AMP
<0.148 mg/Kg - dry 0.148 0.423Nitrobenzene 1 09/14/23 16:13 V37800AMP
<0.113 mg/Kg - dry 0.113 0.8472-Nitrophenol 1 09/14/23 16:13 V37800AMP
<0.150 mg/Kg - dry 0.150 0.8474-Nitrophenol 1 09/14/23 16:13 V37800AMP
<0.337 mg/Kg - dry 0.337 0.847N-Nitrosodimethylamine 1 09/14/23 16:13 V37800AMP
<0.232 mg/Kg - dry 0.232 0.847N-Nitrosodiphenylamine 1 09/14/23 16:13 V37800AMP
<0.151 mg/Kg - dry 0.151 0.847
N-Nitroso-di-n-propylamine 1 09/14/23 16:13 V37800AMP
<0.445 mg/Kg - dry 0.445 1.28Pentachlorophenol 1 09/14/23 16:13 V37800AMP
<0.267 mg/Kg - dry 0.267 0.847Phenanthrene 1 09/14/23 16:13 V37800AMP
<0.143 mg/Kg - dry 0.143 0.847Phenol 1 09/14/23 16:13 V37800AMP
0.206 J mg/Kg - dry 0.172 0.847Pyrene 1 09/14/23 16:13 V37800AMP
<0.101 mg/Kg - dry 0.101 0.423Pyridine 1 09/14/23 16:13 V37800AMP
<0.137 mg/Kg - dry 0.137 0.8471,2,4-Trichlorobenzene 1 09/14/23 16:13 V37800AMP
<0.123 mg/Kg - dry 0.123 0.847
2,4,5-Trichlorophenol 1 09/14/23 16:13 V37800AMP
<0.124 mg/Kg - dry 0.124 0.8472,4,6-Trichlorophenol 1 09/14/23 16:13 V37800AMP
8270ESurrogate: Phenol-d5 53.2 Limits: 34-121%09/14/23 16:131 AMP
Surrogate: 2-Fluorobiphenyl 62.7 Limits: 44-115%09/14/23 16:131 AMP V37800
Surrogate: 2-Fluorophenol 55.3 Limits: 35-115%09/14/23 16:131 AMP V37800
Surrogate: Nitrobenzene-d5 64.5 Limits: 37-122%09/14/23 16:131 AMP V37800
Surrogate: 4-Terphenyl-d14 63.9 Limits: 54-127%09/14/23 16:131 AMP V37800
Surrogate: 2,4,6-Tribromophenol 58.9 Limits: 39-132%09/14/23 16:131 AMP V37800
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
21.1 %Moisture 1 09/14/23 10:10 SW-DRYWTCNC
<0.178 mg/Kg - dry 0.178 0.253Chromium, Hexavalent 1 09/17/23 12:49 SW-7199NFP
2.26 mg/Kg - dry 0.108 0.317Arsenic 5 09/15/23 02:45 6020BCPW
63.4 mg/Kg - dry 0.054 0.316Barium 5 09/15/23 02:45 6020BCPW
0.179 J mg/Kg - dry 0.0329 0.317Cadmium 5 09/15/23 02:45 6020BCPW
41.2 mg/Kg - dry 0.147 0.316
Chromium 5 09/15/23 02:45 6020BCPW
19.1 mg/Kg - dry 0.0392 0.317Lead 5 09/15/23 19:57 6020BCPW
0.0427 mg/Kg - dry 0.0152 0.0380Mercury (Total)1 09/13/23 15:36 7471BJKC
0.718 mg/Kg - dry 0.130 0.316Selenium 5 09/15/23 02:45 6020BCPW
0.0736 J mg/Kg - dry 0.0085 0.317Silver 5 09/15/23 02:45 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
0.013 J mg/Kg - dry 0.003 0.025Acetone 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 09/12/23 16:23 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.025Acrylonitrile 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 09/12/23 16:23 V37758TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 09/12/23 16:23 V37758TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006
Chlorodibromomethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 09/12/23 16:23 V37758TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 09/12/23 16:23 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 09/12/23 16:23 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 09/12/23 16:23 V37758TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 09/12/23 16:23 V37758TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 09/12/23 16:23 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 09/12/23 16:23 V37758TBL
<0.0010 mg/Kg - dry 0.0010 0.006
1,1-Dichloropropene 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 09/12/23 16:23 V37758TBL
<0.017 mg/Kg - dry 0.017 0.316Ethanol 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.063Ethyl Tertiary Butyl Ether (ETBE)1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012Hexachlorobutadiene 1 09/12/23 16:23 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
0.001 J mg/Kg - dry 0.0008 0.012n-Hexane 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 09/12/23 16:23 V37758TBL
<0.019 mg/Kg - dry 0.019 0.0254-Methyl-2-Pentanone 1 09/12/23 16:23 V37758TBL
0.008 J mg/Kg - dry 0.001 0.012Methylene Chloride 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 09/12/23 16:23 V37758TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.012
1,2,3-Trichlorobenzene 1 09/12/23 16:23 V37758TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 09/12/23 16:23 V37758TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 09/12/23 16:23 V37758TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 09/12/23 16:23 V37758TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V37757 09/12/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 09/12/23 16:23 V37758TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 09/12/23 16:23 V37758TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 09/12/23 16:23 V37758TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 09/12/23 16:23 V37758
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%09/12/23 16:231 TBL V37758
Surrogate: Dibromofluoromethane 103 Limits: 84-123%09/12/23 16:231 TBL V37758
Surrogate: Toluene-d8 95.5 Limits: 76-129%09/12/23 16:231 TBL V37758
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.147 mg/Kg - dry 0.147 0.836Acenaphthene 1 09/14/23 16:36 V37800AMP
<0.133 mg/Kg - dry 0.133 0.836Acenaphthylene 1 09/14/23 16:36 V37800AMP
<0.192 mg/Kg - dry 0.192 0.836Aniline 1 09/14/23 16:36 V37800AMP
<0.181 mg/Kg - dry 0.181 0.836Anthracene 1 09/14/23 16:36 V37800AMP
0.253 J
mg/Kg - dry 0.176 0.836
Benzo(a)anthracene 1 09/14/23 16:36 V37800AMP
0.212 J mg/Kg - dry 0.186 0.836Benzo(a)pyrene 1 09/14/23 16:36 V37800AMP
0.299 J mg/Kg - dry 0.185 0.836Benzo(b)fluoranthene 1 09/14/23 16:36 V37800AMP
<0.172 mg/Kg - dry 0.172 0.836Benzo(g,h,i)perylene 1 09/14/23 16:36 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.173 mg/Kg - dry 0.173 0.836Benzo(k)fluoranthene 1 09/14/23 16:36 V37800AMP
<0.735 mg/Kg - dry 0.735 2.53Benzoic Acid 1 09/14/23 16:36 V37800AMP
<0.133 mg/Kg - dry 0.133 0.836Benzyl alcohol 1 09/14/23 16:36 V37800AMP
<0.149 mg/Kg - dry 0.149 0.836Bis(2-Chloroethoxy)methane 1 09/14/23 16:36 V37800AMP
<0.135 mg/Kg - dry 0.135 0.836Bis(2-Chloroethyl)ether 1 09/14/23 16:36 V37800AMP
<0.172 mg/Kg - dry 0.172 0.418Bis(2-Chloroisopropyl)ether 1 09/14/23 16:36 V37800AMP
<0.152 mg/Kg - dry 0.152 0.836Bis(2-ethylhexyl)phthalate 1 09/14/23 16:36 V37800AMP
<0.138 mg/Kg - dry 0.138 0.8364-Bromophenyl phenyl ether 1 09/14/23 16:36 V37800AMP
<0.143 mg/Kg - dry 0.143 0.418
Butyl benzyl phthalate 1 09/14/23 16:36 V37800AMP
<0.117 mg/Kg - dry 0.117 0.8364-Chloro-3-methylphenol 1 09/14/23 16:36 V37800AMP
<0.141 mg/Kg - dry 0.141 0.4184-Chloroaniline 1 09/14/23 16:36 V37800AMP
<0.147 mg/Kg - dry 0.147 0.8362-Chloronaphthalene 1 09/14/23 16:36 V37800AMP
<0.124 mg/Kg - dry 0.124 0.8362-Chlorophenol 1 09/14/23 16:36 V37800AMP
<0.159 mg/Kg - dry 0.159 1.274-Chlorophenyl phenyl ether 1 09/14/23 16:36 V37800AMP
0.228 J mg/Kg - dry 0.179 0.836Chrysene 1 09/14/23 16:36 V37800AMP
<0.291 mg/Kg - dry 0.291 0.836
Dibenz(a,h)anthracene 1 09/14/23 16:36 V37800AMP
<0.150 mg/Kg - dry 0.150 0.836Dibenzofuran 1 09/14/23 16:36 V37800AMP
<0.119 mg/Kg - dry 0.119 0.8361,2-Dichlorobenzene 1 09/14/23 16:36 V37800AMP
<0.123 mg/Kg - dry 0.123 0.8361,3-Dichlorobenzene 1 09/14/23 16:36 V37800AMP
<0.123 mg/Kg - dry 0.123 0.4181,4-Dichlorobenzene 1 09/14/23 16:36 V37800AMP
<0.186 mg/Kg - dry 0.186 0.8363,3'-Dichlorobenzidine 1 09/14/23 16:36 V37800AMP
<0.121 mg/Kg - dry 0.121 0.8362,4-Dichlorophenol 1 09/14/23 16:36 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.228 mg/Kg - dry 0.228 0.836Diethyl phthalate 1 09/14/23 16:36 V37800AMP
<0.220 mg/Kg - dry 0.220 0.836Dimethyl phthalate 1 09/14/23 16:36 V37800AMP
<0.136 mg/Kg - dry 0.136 0.4182,4-Dimethylphenol 1 09/14/23 16:36 V37800AMP
<0.135 mg/Kg - dry 0.135 0.836Di-n-butyl phthalate 1 09/14/23 16:36 V37800AMP
<0.304 mg/Kg - dry 0.304 1.904,6-Dinitro-2-methylphenol 1 09/14/23 16:36 V37800AMP
<0.659 mg/Kg - dry 0.659 1.902,4-Dinitrophenol 1 09/14/23 16:36 V37800AMP
<0.122 mg/Kg - dry 0.122 0.8362,4-Dinitrotoluene 1 09/14/23 16:36 V37800AMP
<0.136 mg/Kg - dry 0.136 0.8362,6-Dinitrotoluene 1 09/14/23 16:36 V37800AMP
<0.181 mg/Kg - dry 0.181 0.418
Di-n-Octyl Phthalate 1 09/14/23 16:36 V37800AMP
0.376 J mg/Kg - dry 0.155 0.836Fluoranthene 1 09/14/23 16:36 V37800AMP
<0.162 mg/Kg - dry 0.162 0.836Fluorene 1 09/14/23 16:36 V37800AMP
<0.134 mg/Kg - dry 0.134 0.836Hexachlorobenzene 1 09/14/23 16:36 V37800AMP
<0.123 mg/Kg - dry 0.123 0.836Hexachlorobutadiene 1 09/14/23 16:36 V37800AMP
<0.198 mg/Kg - dry 0.198 0.836Hexachlorocyclopentadiene 1 09/14/23 16:36 V37800AMP
<0.100 mg/Kg - dry 0.100 0.836Hexachloroethane 1 09/14/23 16:36 V37800AMP
<0.226 mg/Kg - dry 0.226 0.836
Indeno(1,2,3-cd)pyrene 1 09/14/23 16:36 V37800AMP
<0.242 mg/Kg - dry 0.242 0.836Isophorone 1 09/14/23 16:36 V37800AMP
<0.134 mg/Kg - dry 0.134 0.8361-Methylnaphthalene 1 09/14/23 16:36 V37800AMP
<0.126 mg/Kg - dry 0.126 0.8362-Methylnaphthalene 1 09/14/23 16:36 V37800AMP
<0.122 mg/Kg - dry 0.122 0.8362-Methylphenol 1 09/14/23 16:36 V37800AMP
<0.107 mg/Kg - dry 0.107 0.8363&4 Methylphenol 1 09/14/23 16:36 V37800AMP
<0.182 mg/Kg - dry 0.182 0.836Naphthalene 1 09/14/23 16:36 V37800AMP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 49
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-255-0005
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Matt Ingalls
Charlotte
Received : 09/12/2023
T&U -004
Report Date : 09/19/2023
Sample ID :
Lab No :
Sampled:Soil Pile Dup
94736 Matrix:
9/12/2023 0:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V37786 09/13/23 12:10
<0.122 mg/Kg - dry 0.122 0.8362-Nitroaniline 1 09/14/23 16:36 V37800AMP
<0.152 mg/Kg - dry 0.152 0.8363-Nitroaniline 1 09/14/23 16:36 V37800AMP
<0.118 mg/Kg - dry 0.118 0.4184-Nitroaniline 1 09/14/23 16:36 V37800AMP
<0.147 mg/Kg - dry 0.147 0.418Nitrobenzene 1 09/14/23 16:36 V37800AMP
<0.112 mg/Kg - dry 0.112 0.8362-Nitrophenol 1 09/14/23 16:36 V37800AMP
<0.148 mg/Kg - dry 0.148 0.8364-Nitrophenol 1 09/14/23 16:36 V37800AMP
<0.333 mg/Kg - dry 0.333 0.836N-Nitrosodimethylamine 1 09/14/23 16:36 V37800AMP
<0.229 mg/Kg - dry 0.229 0.836N-Nitrosodiphenylamine 1 09/14/23 16:36 V37800AMP
<0.149 mg/Kg - dry 0.149 0.836
N-Nitroso-di-n-propylamine 1 09/14/23 16:36 V37800AMP
<0.439 mg/Kg - dry 0.439 1.27Pentachlorophenol 1 09/14/23 16:36 V37800AMP
<0.263 mg/Kg - dry 0.263 0.836Phenanthrene 1 09/14/23 16:36 V37800AMP
<0.141 mg/Kg - dry 0.141 0.836Phenol 1 09/14/23 16:36 V37800AMP
0.339 J mg/Kg - dry 0.169 0.836Pyrene 1 09/14/23 16:36 V37800AMP
<0.100 mg/Kg - dry 0.100 0.418Pyridine 1 09/14/23 16:36 V37800AMP
<0.135 mg/Kg - dry 0.135 0.8361,2,4-Trichlorobenzene 1 09/14/23 16:36 V37800AMP
<0.121 mg/Kg - dry 0.121 0.836
2,4,5-Trichlorophenol 1 09/14/23 16:36 V37800AMP
<0.122 mg/Kg - dry 0.122 0.8362,4,6-Trichlorophenol 1 09/14/23 16:36 V37800AMP
8270ESurrogate: Phenol-d5 63.1 Limits: 34-121%09/14/23 16:361 AMP
Surrogate: 2-Fluorobiphenyl 73.5 Limits: 44-115%09/14/23 16:361 AMP V37800
Surrogate: 2-Fluorophenol 64.9 Limits: 35-115%09/14/23 16:361 AMP V37800
Surrogate: Nitrobenzene-d5 71.1 Limits: 37-122%09/14/23 16:361 AMP V37800
Surrogate: 4-Terphenyl-d14 80.7 Limits: 54-127%09/14/23 16:361 AMP V37800
Surrogate: 2,4,6-Tribromophenol 71.2 Limits: 39-132%09/14/23 16:361 AMP V37800
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 30 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Metals Analyses
6020B
L704586,L704856QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L704365
Associated Lab Samples: 94734, 94735, 94736
LRB-L704365 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/15/23 02:120.2500.0855<0.0855mg/KgArsenic
09/15/23 02:120.2500.042<0.042mg/KgBarium
09/15/23 02:120.2500.0260<0.0260mg/KgCadmium
09/15/23 02:120.2500.116<0.116mg/KgChromium
09/15/23 19:000.2500.03100.0382mg/KgLead
09/15/23 02:120.2500.103<0.103mg/KgSelenium
09/15/23 02:120.2500.0067<0.0067mg/KgSilver
LCS-L704365Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.02.362.50mg/KgArsenic 80-120
94.04.705.00mg/KgBarium 80-120
1000.4990.500mg/KgCadmium 80-120
95.04.775.00mg/KgChromium 80-120
96.02.402.50mg/KgLead 80-120
93.04.665.00mg/KgSelenium 80-120
96.00.4780.500mg/KgSilver 80-120
V 94708-MS-L704365 V 94708-MSD-L704365Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.92 44.0*2.092.432.320.889mg/KgArsenic 49.0*75-125 8.4 80
94.4 91.01114.874.6490.2mg/KgBarium 427*75-125 16.1 80
0.418 84.00.4280.4870.4640.0261mg/KgCadmium 83.0 75-125 2.3 80
53.0 0.0*54.74.874.6468.7mg/KgChromium 0.0*75-125 3.1 80
Page 1 of 17* QC Fail Date:09/19/2023 02:23 PM
Page 31 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Metals Analyses
6020B
L704586,L704856QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L704365
V 94708-MS-L704365 V 94708-MSD-L704365Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
7.31 87.08.882.432.325.30mg/KgLead 147*75-125 19.3 80
3.04 44.0*3.254.874.640.986mg/KgSelenium 47.0*75-125 6.6 80
0.423 83.00.4400.4870.4640.0370mg/KgSilver 83.0 75-125 3.9 80
V 94708-PDS-L704365Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/15/23 04:1693.01.23mg/KgArsenic
09/15/23 04:1610311.8mg/KgBarium
09/15/23 04:1695.00.239mg/KgCadmium
09/15/23 04:1699.09.28mg/KgChromium
09/15/23 18:1997.01.73mg/KgLead
09/15/23 04:1688.02.29mg/KgSelenium
09/15/23 04:1693.00.235mg/KgSilver
Page 2 of 17* QC Fail Date:09/19/2023 02:23 PM
Page 32 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471B
V37816QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471B (Prep)
QC Prep:V37754
Associated Lab Samples: 94734, 94735, 94736
LRB-V37754 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/13/23 15:240.03000.0120<0.0120mg/KgMercury (Total)
LCS-V37754Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1020.4240.417mg/KgMercury (Total)80-120
V 94711-MS-V37754 V 94711-MSD-V37754Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.458 95.00.4270.3970.4100.0683mg/KgMercury (Total)90.0 80-120 7.0 20
V 94711-PDS-V37754Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
09/13/23 15:4994.00.221mg/KgMercury (Total)
Page 3 of 17Date:09/19/2023 02:23 PM
Page 33 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37758QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37757
Associated Lab Samples: 94734, 94735, 94736
LRB-V37757 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/12/23 10:070.0200.002<0.002mg/KgAcetone
09/12/23 10:070.0200.001<0.001mg/KgAcrolein
09/12/23 10:070.0200.0008<0.0008mg/KgAcrylonitrile
09/12/23 10:070.0050.0006<0.0006mg/KgBenzene
09/12/23 10:070.0050.0005<0.0005mg/KgBromobenzene
09/12/23 10:070.0050.0008<0.0008mg/KgBromochloromethane
09/12/23 10:070.0050.001<0.001mg/KgBromodichloromethane
09/12/23 10:070.0050.001<0.001mg/KgBromoform
09/12/23 10:070.0100.001<0.001mg/KgBromomethane
09/12/23 10:070.0050.0005<0.0005mg/Kgn-Butylbenzene
09/12/23 10:070.0050.0006<0.0006mg/Kgsec-Butyl benzene
09/12/23 10:070.0050.0005<0.0005mg/Kgtert-Butyl benzene
09/12/23 10:070.0050.0006<0.0006mg/KgCarbon Disulfide
09/12/23 10:070.0050.001<0.001mg/KgCarbon Tetrachloride
09/12/23 10:070.0050.0007<0.0007mg/KgChlorobenzene
09/12/23 10:070.0050.0009<0.0009mg/KgChlorodibromomethane
09/12/23 10:070.0100.0009<0.0009mg/KgChloroethane
09/12/23 10:070.0050.001<0.001mg/KgChloroform
09/12/23 10:070.0100.0006<0.0006mg/KgChloromethane
09/12/23 10:070.0050.0005<0.0005mg/Kg2-Chlorotoluene
09/12/23 10:070.0050.0004<0.0004mg/Kg4-Chlorotoluene
09/12/23 10:070.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
09/12/23 10:070.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
09/12/23 10:070.0050.0006<0.0006mg/Kg1,2-Dibromoethane
09/12/23 10:070.0050.0006<0.0006mg/KgDibromomethane
09/12/23 10:070.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
09/12/23 10:070.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 17Date:09/19/2023 02:23 PM
Page 34 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37758QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37757
Associated Lab Samples: 94734, 94735, 94736
LRB-V37757 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/12/23 10:070.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
09/12/23 10:070.0100.001<0.001mg/KgDichlorodifluoromethane
09/12/23 10:070.0050.0008<0.0008mg/Kg1,1-Dichloroethane
09/12/23 10:070.0050.001<0.001mg/Kg1,2-Dichloroethane
09/12/23 10:070.0050.0007<0.0007mg/Kg1,1-Dichloroethene
09/12/23 10:070.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
09/12/23 10:070.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
09/12/23 10:070.0050.0004<0.0004mg/Kg1,2-Dichloropropane
09/12/23 10:070.0050.0006<0.0006mg/Kg1,3-Dichloropropane
09/12/23 10:070.0050.001<0.001mg/Kg2,2-Dichloropropane
09/12/23 10:070.0050.0008<0.0008mg/Kg1,1-Dichloropropene
09/12/23 10:070.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
09/12/23 10:070.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
09/12/23 10:070.2500.014<0.014mg/KgEthanol
09/12/23 10:070.0050.0006<0.0006mg/KgEthylbenzene
09/12/23 10:070.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
09/12/23 10:070.0100.0008<0.0008mg/KgHexachlorobutadiene
09/12/23 10:070.0100.0007<0.0007mg/Kgn-Hexane
09/12/23 10:070.0200.0006<0.0006mg/Kg2-Hexanone
09/12/23 10:070.0050.0005<0.0005mg/KgIsopropylbenzene
09/12/23 10:070.0050.001<0.001mg/Kg4-Isopropyl toluene
09/12/23 10:070.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
09/12/23 10:070.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
09/12/23 10:070.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
09/12/23 10:070.0100.001<0.001mg/KgMethylene Chloride
09/12/23 10:070.0100.0010<0.0010mg/KgNaphthalene
09/12/23 10:070.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 17Date:09/19/2023 02:23 PM
Page 35 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37758QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37757
Associated Lab Samples: 94734, 94735, 94736
LRB-V37757 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/12/23 10:070.0050.001<0.001mg/KgStyrene
09/12/23 10:070.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
09/12/23 10:070.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
09/12/23 10:070.0050.0009<0.0009mg/KgTetrachloroethene
09/12/23 10:070.0050.0007<0.0007mg/KgToluene
09/12/23 10:070.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
09/12/23 10:070.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
09/12/23 10:070.0050.001<0.001mg/Kg1,1,1-Trichloroethane
09/12/23 10:070.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
09/12/23 10:070.0050.0009<0.0009mg/KgTrichloroethene
09/12/23 10:070.0100.002<0.002mg/KgTrichlorofluoromethane
09/12/23 10:070.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
09/12/23 10:070.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
09/12/23 10:070.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
09/12/23 10:070.0100.0005<0.0005mg/KgVinyl Acetate
09/12/23 10:070.0100.0005<0.0005mg/KgVinyl Chloride
09/12/23 10:070.0050.0005<0.0005mg/Kgo-Xylene
09/12/23 10:070.0100.001<0.001mg/Kgm,p-Xylene
09/12/23 10:074-Bromofluorobenzene (S)102 70-130
09/12/23 10:07Dibromofluoromethane (S)102 84-123
09/12/23 10:07Toluene-d8 (S)96.2 76-129
LCS-V37757 LCSD-V37757Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.081 81.778.00.0780.100mg/KgAcetone 29-198 4.6 20
Page 6 of 17Date:09/19/2023 02:23 PM
Page 36 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37758QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37757
LCS-V37757 LCSD-V37757Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.298.10.0980.100mg/KgAcrolein 70-130 5.1 20
0.102 1021010.1010.100mg/KgAcrylonitrile 65-134 0.9 20
0.045 90.693.40.0460.050mg/KgBenzene 74-127 3.0 20
0.043 87.887.20.0430.050mg/KgBromobenzene 73-125 0.6 20
0.051 1041020.0510.050mg/KgBromochloromethane 72-134 1.3 20
0.047 94.894.80.0470.050mg/KgBromodichloromethane 75-122 0.0 20
0.053 1061020.0510.050mg/KgBromoform 66-135 3.6 20
0.049 98.494.60.0470.050mg/KgBromomethane 20-180 3.9 20
0.043 87.090.60.0450.050mg/Kgn-Butylbenzene 65-135 4.0 20
0.043 86.288.40.0440.050mg/Kgsec-Butyl benzene 66-131 2.5 20
0.043 86.688.40.0440.050mg/Kgtert-Butyl benzene 67-132 2.0 20
0.042 84.088.80.0440.050mg/KgCarbon Disulfide 61-129 5.5 20
0.045 91.896.80.0480.050mg/KgCarbon Tetrachloride 64-143 5.3 20
0.046 92.293.60.0460.050mg/KgChlorobenzene 74-118 1.5 20
0.049 98.298.80.0490.050mg/KgChlorodibromomethane 73-122 0.6 20
0.047 95.899.20.0490.050mg/KgChloroethane 33-149 3.4 20
0.046 92.492.40.0460.050mg/KgChloroform 73-127 0.0 20
0.040 80.683.40.0410.050mg/KgChloromethane 45-143 3.4 20
0.042 85.688.40.0440.050mg/Kg2-Chlorotoluene 67-124 3.2 20
0.042 85.688.20.0440.050mg/Kg4-Chlorotoluene 71-126 2.9 20
0.042 85.085.00.0420.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.0 20
0.051 1021020.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 0.1 20
0.051 1031030.0510.050mg/Kg1,2-Dibromoethane 70-132 0.0 20
0.048 96.896.80.0480.050mg/KgDibromomethane 74-133 0.0 20
0.047 94.695.20.0470.050mg/Kg1,2-Dichlorobenzene 72-123 0.6 20
0.046 92.692.80.0460.050mg/Kg1,3-Dichlorobenzene 71-120 0.2 20
Page 7 of 17Date:09/19/2023 02:23 PM
Page 37 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37758QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37757
LCS-V37757 LCSD-V37757Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.044 89.690.80.0450.050mg/Kg1,4-Dichlorobenzene 71-123 1.3 20
0.049 99.61030.0510.050mg/KgDichlorodifluoromethane 26-146 2.9 20
0.044 88.689.80.0440.050mg/Kg1,1-Dichloroethane 74-127 1.3 20
0.044 89.689.20.0440.050mg/Kg1,2-Dichloroethane 68-128 0.4 20
0.040 81.286.40.0430.050mg/Kg1,1-Dichloroethene 67-149 6.2 20
0.044 88.691.80.0450.050mg/Kgcis-1,2-Dichloroethene 76-134 3.5 20
0.043 87.091.00.0450.050mg/Kgtrans-1,2-Dichloroethene 73-132 4.4 20
0.045 91.891.20.0450.050mg/Kg1,2-Dichloropropane 73-130 0.6 20
0.046 93.694.40.0470.050mg/Kg1,3-Dichloropropane 75-124 0.8 20
0.044 88.091.40.0450.050mg/Kg2,2-Dichloropropane 50-142 3.7 20
0.042 85.892.00.0460.050mg/Kg1,1-Dichloropropene 71-130 6.9 20
0.049 99.299.40.0490.050mg/Kgcis-1,3-Dichloropropene 71-125 0.2 20
0.051 1021000.0500.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.9 20
1.19 95.290.41.131.25mg/KgEthanol 70-130 5.1 20
0.043 86.689.80.0440.050mg/KgEthylbenzene 74-128 3.6 20
0.091 91.791.10.0910.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.6 20
0.045 91.295.60.0470.050mg/KgHexachlorobutadiene 64-125 4.7 20
0.047 95.81020.0510.050mg/Kgn-Hexane 70-130 6.2 20
0.039 79.679.00.0390.050mg/Kg2-Hexanone 61-157 0.7 20
0.043 86.088.60.0440.050mg/KgIsopropylbenzene 68-126 2.9 20
0.044 88.690.80.0450.050mg/Kg4-Isopropyl toluene 68-129 2.4 20
0.047 94.093.20.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.8 20
0.048 96.294.80.0470.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.4 20
0.045 91.690.20.0450.050mg/Kg4-Methyl-2-Pentanone 57-162 1.5 20
0.040 80.080.80.0400.050mg/KgMethylene Chloride 74-129 0.9 20
0.050 10099.40.0490.050mg/KgNaphthalene 57-157 0.8 20
Page 8 of 17Date:09/19/2023 02:23 PM
Page 38 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V37758QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V37757
LCS-V37757 LCSD-V37757Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 85.087.60.0430.050mg/Kgn-Propylbenzene 67-130 3.0 20
0.048 96.499.20.0490.050mg/KgStyrene 77-121 2.8 20
0.048 96.496.80.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.4 20
0.046 92.490.80.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.7 20
0.045 91.096.40.0480.050mg/KgTetrachloroethene 68-130 5.7 20
0.045 90.293.20.0460.050mg/KgToluene 71-129 3.2 20
0.047 94.696.00.0480.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.4 20
0.048 97.498.80.0490.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.4 20
0.042 85.490.80.0450.050mg/Kg1,1,1-Trichloroethane 67-131 6.1 20
0.047 95.296.20.0480.050mg/Kg1,1,2-Trichloroethane 70-133 1.0 20
0.046 92.697.20.0480.050mg/KgTrichloroethene 75-133 4.8 20
0.038 76.081.40.0400.050mg/KgTrichlorofluoromethane 44-146 6.8 20
0.048 96.094.80.0470.050mg/Kg1,2,3-Trichloropropane 60-137 1.2 20
0.044 89.490.60.0450.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.3 20
0.044 88.890.00.0450.050mg/Kg1,3,5-Trimethylbenzene 69-128 1.3 20
0.052 1051100.0550.050mg/KgVinyl Acetate 60-140 4.8 20
0.036 72.685.20.0420.050mg/KgVinyl Chloride 48-147 15.9 20
0.045 90.693.40.0460.050mg/Kgo-Xylene 74-126 3.0 20
0.088 88.491.10.0910.100mg/Kgm,p-Xylene 75-124 3.0 20
1011004-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
97.298.0Toluene-d8 (S)76-129
Page 9 of 17Date:09/19/2023 02:23 PM
Page 39 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37800QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37786
Associated Lab Samples: 94734, 94735, 94736
LRB-V37786 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/14/23 12:450.6600.116<0.116mg/KgAcenaphthene
09/14/23 12:450.6600.105<0.105mg/KgAcenaphthylene
09/14/23 12:450.6600.152<0.152mg/KgAniline
09/14/23 12:450.6600.143<0.143mg/KgAnthracene
09/14/23 12:450.6600.139<0.139mg/KgBenzo(a)anthracene
09/14/23 12:450.6600.147<0.147mg/KgBenzo(a)pyrene
09/14/23 12:450.6600.146<0.146mg/KgBenzo(b)fluoranthene
09/14/23 12:450.6600.136<0.136mg/KgBenzo(g,h,i)perylene
09/14/23 12:450.6600.137<0.137mg/KgBenzo(k)fluoranthene
09/14/23 12:452.000.580<0.580mg/KgBenzoic Acid
09/14/23 12:450.6600.105<0.105mg/KgBenzyl alcohol
09/14/23 12:450.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
09/14/23 12:450.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
09/14/23 12:450.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
09/14/23 12:450.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
09/14/23 12:450.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
09/14/23 12:450.3300.113<0.113mg/KgButyl benzyl phthalate
09/14/23 12:450.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
09/14/23 12:450.3300.112<0.112mg/Kg4-Chloroaniline
09/14/23 12:450.6600.116<0.116mg/Kg2-Chloronaphthalene
09/14/23 12:450.6600.098<0.098mg/Kg2-Chlorophenol
09/14/23 12:451.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
09/14/23 12:450.6600.142<0.142mg/KgChrysene
09/14/23 12:450.6600.230<0.230mg/KgDibenz(a,h)anthracene
09/14/23 12:450.6600.119<0.119mg/KgDibenzofuran
09/14/23 12:450.6600.094<0.094mg/Kg1,2-Dichlorobenzene
09/14/23 12:450.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 10 of 17Date:09/19/2023 02:23 PM
Page 40 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37800QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37786
Associated Lab Samples: 94734, 94735, 94736
LRB-V37786 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/14/23 12:450.3300.097<0.097mg/Kg1,4-Dichlorobenzene
09/14/23 12:450.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
09/14/23 12:450.6600.095<0.095mg/Kg2,4-Dichlorophenol
09/14/23 12:450.6600.180<0.180mg/KgDiethyl phthalate
09/14/23 12:450.6600.174<0.174mg/KgDimethyl phthalate
09/14/23 12:450.3300.108<0.108mg/Kg2,4-Dimethylphenol
09/14/23 12:450.6600.107<0.107mg/KgDi-n-butyl phthalate
09/14/23 12:451.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
09/14/23 12:451.500.520<0.520mg/Kg2,4-Dinitrophenol
09/14/23 12:450.6600.096<0.096mg/Kg2,4-Dinitrotoluene
09/14/23 12:450.6600.108<0.108mg/Kg2,6-Dinitrotoluene
09/14/23 12:450.3300.143<0.143mg/KgDi-n-Octyl Phthalate
09/14/23 12:450.6600.123<0.123mg/KgFluoranthene
09/14/23 12:450.6600.128<0.128mg/KgFluorene
09/14/23 12:450.6600.106<0.106mg/KgHexachlorobenzene
09/14/23 12:450.6600.097<0.097mg/KgHexachlorobutadiene
09/14/23 12:450.6600.157<0.157mg/KgHexachlorocyclopentadiene
09/14/23 12:450.6600.079<0.079mg/KgHexachloroethane
09/14/23 12:450.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
09/14/23 12:450.6600.191<0.191mg/KgIsophorone
09/14/23 12:450.6600.106<0.106mg/Kg1-Methylnaphthalene
09/14/23 12:450.6600.100<0.100mg/Kg2-Methylnaphthalene
09/14/23 12:450.6600.097<0.097mg/Kg2-Methylphenol
09/14/23 12:450.6600.084<0.084mg/Kg3&4 Methylphenol
09/14/23 12:450.6600.144<0.144mg/KgNaphthalene
09/14/23 12:450.6600.096<0.096mg/Kg2-Nitroaniline
09/14/23 12:450.6600.120<0.120mg/Kg3-Nitroaniline
Page 11 of 17Date:09/19/2023 02:23 PM
Page 41 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37800QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37786
Associated Lab Samples: 94734, 94735, 94736
LRB-V37786 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
09/14/23 12:450.3300.093<0.093mg/Kg4-Nitroaniline
09/14/23 12:450.3300.116<0.116mg/KgNitrobenzene
09/14/23 12:450.6600.088<0.088mg/Kg2-Nitrophenol
09/14/23 12:450.6600.117<0.117mg/Kg4-Nitrophenol
09/14/23 12:450.6600.263<0.263mg/KgN-Nitrosodimethylamine
09/14/23 12:450.6600.181<0.181mg/KgN-Nitrosodiphenylamine
09/14/23 12:450.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
09/14/23 12:451.000.347<0.347mg/KgPentachlorophenol
09/14/23 12:450.6600.208<0.208mg/KgPhenanthrene
09/14/23 12:450.6600.112<0.112mg/KgPhenol
09/14/23 12:450.6600.134<0.134mg/KgPyrene
09/14/23 12:450.3300.079<0.079mg/KgPyridine
09/14/23 12:450.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
09/14/23 12:450.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
09/14/23 12:450.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
09/14/23 12:452-Fluorobiphenyl (S)65.2 44-115
09/14/23 12:452-Fluorophenol (S)57.3 35-115
09/14/23 12:45Nitrobenzene-d5 (S)62.8 37-122
09/14/23 12:454-Terphenyl-d14 (S)71.2 54-127
09/14/23 12:452,4,6-Tribromophenol (S)62.1 39-132
09/14/23 12:45Phenol-d5 (S)55.2 34-121
LCS-V37786 LCSD-V37786Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.11 66.464.01.071.67mg/KgAcenaphthene 40-123 3.6 20
Page 12 of 17Date:09/19/2023 02:23 PM
Page 42 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37800QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37786
LCS-V37786 LCSD-V37786Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.14 68.267.01.121.67mg/KgAcenaphthylene 32-132 1.7 20
3.35 201*1933.221.67mg/KgAniline 12-197 3.9 20
1.25 74.873.61.231.67mg/KgAnthracene 47-123 1.6 20
1.26 75.473.01.221.67mg/KgBenzo(a)anthracene 49-126 3.2 20
1.36 81.479.01.321.67mg/KgBenzo(a)pyrene 45-129 2.9 20
1.29 77.277.21.291.67mg/KgBenzo(b)fluoranthene 45-132 0.0 20
1.21 72.471.21.191.67mg/KgBenzo(g,h,i)perylene 43-134 1.6 20
1.18 70.670.01.171.67mg/KgBenzo(k)fluoranthene 47-132 0.8 20
0.758 45.351.70.8641.67mg/KgBenzoic Acid 10-83 13.0 20
1.15 68.865.81.101.67mg/KgBenzyl alcohol 29-122 4.4 20
1.17 70.067.61.131.67mg/KgBis(2-Chloroethoxy)methane 36-121 3.4 20
1.04 62.259.81.001.67mg/KgBis(2-Chloroethyl)ether 31-120 3.9 20
1.16 69.466.41.111.67mg/KgBis(2-Chloroisopropyl)ether 33-131 4.4 20
1.35 80.879.61.331.67mg/KgBis(2-ethylhexyl)phthalate 51-133 1.4 20
1.23 73.673.61.231.67mg/Kg4-Bromophenyl phenyl ether 46-124 0.0 20
1.33 79.676.61.281.67mg/KgButyl benzyl phthalate 48-132 3.8 20
1.20 71.869.41.161.67mg/Kg4-Chloro-3-methylphenol 45-122 3.3 20
1.48 88.685.61.431.67mg/Kg4-Chloroaniline 17-106 3.4 20
1.12 67.064.01.071.67mg/Kg2-Chloronaphthalene 41-114 4.5 20
1.13 67.665.21.091.67mg/Kg2-Chlorophenol 34-121 3.6 20
1.20 71.868.21.141.67mg/Kg4-Chlorophenyl phenyl ether 45-121 5.1 20
1.17 70.068.21.141.67mg/KgChrysene 50-124 2.5 20
0.794 47.547.40.7921.67mg/KgDibenz(a,h)anthracene 45-134 0.2 20
1.13 67.664.01.071.67mg/KgDibenzofuran 44-120 5.4 20
1.01 60.457.40.9601.67mg/Kg1,2-Dichlorobenzene 33-117 5.0 20
0.983 58.856.30.9411.67mg/Kg1,3-Dichlorobenzene 30-115 4.3 20
Page 13 of 17* QC Fail Date:09/19/2023 02:23 PM
Page 43 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37800QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37786
LCS-V37786 LCSD-V37786Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.989 59.256.40.9431.67mg/Kg1,4-Dichlorobenzene 31-115 4.7 20
1.21 72.467.61.131.67mg/Kg3,3'-Dichlorobenzidine 22-121 6.8 20
1.20 71.868.21.141.67mg/Kg2,4-Dichlorophenol 40-122 5.1 20
1.22 73.071.21.191.67mg/KgDiethyl phthalate 50-124 2.4 20
1.23 73.671.21.191.67mg/KgDimethyl phthalate 48-124 3.3 20
1.62 97.091.61.531.67mg/Kg2,4-Dimethylphenol 30-127 5.7 20
1.31 78.479.01.321.67mg/KgDi-n-butyl phthalate 51-128 0.7 20
1.14 68.265.21.091.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 4.4 20
1.06 63.464.61.081.67mg/Kg2,4-Dinitrophenol 27-129 1.8 20
1.30 77.876.01.271.67mg/Kg2,4-Dinitrotoluene 48-126 2.3 20
1.31 78.473.61.231.67mg/Kg2,6-Dinitrotoluene 46-124 6.2 20
1.33 79.678.41.311.67mg/KgDi-n-Octyl Phthalate 45-140 1.5 20
1.16 69.468.21.141.67mg/KgFluoranthene 50-127 1.7 20
1.18 70.667.61.131.67mg/KgFluorene 43-125 4.3 20
1.24 74.273.01.221.67mg/KgHexachlorobenzene 45-122 1.6 20
1.11 66.462.21.041.67mg/KgHexachlorobutadiene 32-123 6.5 20
0.988 59.154.10.9051.67mg/KgHexachlorocyclopentadiene 32-117 8.7 20
0.979 58.656.60.9461.67mg/KgHexachloroethane 28-117 3.4 20
1.25 74.871.21.191.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 4.9 20
1.08 64.662.21.041.67mg/KgIsophorone 30-122 3.7 20
1.08 64.661.61.031.67mg/Kg1-Methylnaphthalene 40-119 4.7 20
1.08 64.662.21.041.67mg/Kg2-Methylnaphthalene 38-122 3.7 20
1.13 67.665.21.091.67mg/Kg2-Methylphenol 32-122 3.6 20
1.04 62.259.81.001.67mg/Kg3&4 Methylphenol 34-119 3.9 20
1.08 64.661.01.021.67mg/KgNaphthalene 35-123 5.7 20
1.34 80.276.61.281.67mg/Kg2-Nitroaniline 44-127 4.5 20
Page 14 of 17Date:09/19/2023 02:23 PM
Page 44 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V37800QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V37786
LCS-V37786 LCSD-V37786Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.34 80.276.61.281.67mg/Kg3-Nitroaniline 33-119 4.5 20
1.25 74.872.41.211.67mg/Kg4-Nitroaniline 63-147 3.2 20
1.06 63.461.01.021.67mg/KgNitrobenzene 34-122 3.8 20
1.16 69.465.81.101.67mg/Kg2-Nitrophenol 36-123 5.3 20
1.15 68.867.01.121.67mg/Kg4-Nitrophenol 30-132 2.6 20
0.896 53.651.50.8611.67mg/KgN-Nitrosodimethylamine 10-146 3.9 20
1.48 88.688.01.471.67mg/KgN-Nitrosodiphenylamine 38-127 0.6 20
1.08 64.661.61.031.67mg/KgN-Nitroso-di-n-propylamine 36-120 4.7 20
1.46 87.481.41.361.67mg/KgPentachlorophenol 25-133 7.0 20
1.21 72.470.61.181.67mg/KgPhenanthrene 50-121 2.5 20
1.03 61.659.30.9911.67mg/KgPhenol 34-121 3.8 20
1.22 73.071.81.201.67mg/KgPyrene 47-127 1.6 20
0.718 42.943.80.7331.67mg/KgPyridine 10-80 2.0 20
1.06 63.460.41.011.67mg/Kg1,2,4-Trichlorobenzene 34-118 4.8 20
1.19 71.268.81.151.67mg/Kg2,4,5-Trichlorophenol 41-124 3.4 20
1.18 70.667.61.131.67mg/Kg2,4,6-Trichlorophenol 39-126 4.3 20
65.263.42-Fluorobiphenyl (S)44-115
58.258.52-Fluorophenol (S)35-115
63.463.4Nitrobenzene-d5 (S)37-122
71.271.84-Terphenyl-d14 (S)54-127
65.163.92,4,6-Tribromophenol (S)39-132
55.556.4Phenol-d5 (S)34-121
Page 15 of 17Date:09/19/2023 02:23 PM
Page 45 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L704912QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L704344
Associated Lab Samples: 94734, 94735, 94736
LRB-L704344 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
09/17/23 11:220.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L704344Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
86.53.464.00mg/KgChromium, Hexavalent 80-120
V 94711-DUP-L704344Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/17/23 11:540.0<0.200< 0.200mg/KgChromium, Hexavalent
V 94711-MS-L704344Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
32.9 85.038.7< 0.141mg/KgChromium, Hexavalent 75-125
Page 16 of 17Date:09/19/2023 02:23 PM
Page 46 of 49
Quality Control Data
23-255-0005Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
T&U -004
Dry Weight Determination
SW-DRYWT
V37805QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94900-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 09/14/23 10:101.827.427.9%Moisture
Page 17 of 17Date:09/19/2023 02:23 PM
Page 47 of 49
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-255-0005
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 3.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:09/12/2023 11:36:17
Special precautions or instructions included?
Comments:
Page 48 of 49
Page 49 of 49