24062_South and Hollis LoSo Redevelopment Summary_20230802

https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Akridge/AKR.007 LoSo Brownfields Implementation/Redevelopment Report/2023/24062 - South
and Hollis LoSo - 2023 Annual Redevelopment Report.doc

Via Email
August 2, 2023

NCDEQ – Division of Waste Management
Brownfields Redevelopment Section
Mail Service Center 1646
Raleigh, North Carolina 27699-1646

Attn: Mr. Bill Schmithorst

Re: Redevelopment Summary Report
South and Hollis LoSo
South Boulevard and Hollis Road
Charlotte, North Carolina
Brownfields Project No. 24062-20-060
H&H Job No. AKR-007

Dear Bill:

1.0 Introduction

On behalf of KA LoSo Holdings LLC (Prospective Developer or PD), Hart & Hickman, PC
(H&H) has prepared this Redevelopment Summary Report for the South and Hollis LoSo
Brownfields property (Brownfields Project No. 24062-20-060) located at the intersection of
South Boulevard and Hollis Road in Charlotte, Mecklenburg County, North Carolina (Site). The
Site consists of one parcel (Parcel Identification No. 14905301) that is approximately 2.6 acres
of land located in a mixed-use area of the lower South End of Charlotte. A Site location map is
included as Figure 1, and the Site and surrounding area are shown in Figure 2.

Redevelopment plans include razing the former Site buildings and leveling the Site for
construction of a multi-story residential, commercial retail, and amenity building and associated
parking deck. Redevelopment plans also include construction of new paved access roads and
landscaped areas. Redevelopment activities at the Site are being conducted in accordance with
the North Carolina Department of Environmental Quality (DEQ) Brownfields approved
Mr. Bill Schmithorst
August 2, 2023
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Environmental Management Plan (EMP) dated July 2, 2021. A copy of the Overall Site Plan
prepared by LandDesign that depicts the development plan is provided as Appendix A.

A Brownfields Agreement between the DEQ and the PD was recorded on June 2, 2022. Land
Use Restriction (LUR) 12.c. included in the Brownfields Agreement indicates that within 90
days of each year after the completion of the Brownfields Agreement, for as long as physical
redevelopment of the Brownfields property continues, a report of environment-related activities
will be prepared for submittal to DEQ Brownfields. This report has been prepared in accordance
with LUR 12.c. A summary of environmental-related activities associated with redevelopment
of the Brownfields property is provided in the following sections.

2.0 Environmental Related Redevelopment Activities

Redevelopment activities at the Site are ongoing and have included Site-wide grading activities,
utility installations, and initial construction work on the multi-story residential apartment
building and associated parking deck. In addition, the vapor intrusion mitigation system (VIMS)
is being installed during construction of the proposed apartment building in accordance with
DEQ-approved Vapor Intrusion Mitigation Plan – Revision 2 (VIMP) dated December 17, 2021.

2.1 Orphan Underground Storage Tank Discoveries

During utility installation activities completed in January and March 2023, the on-Site general
contractor identified two (2) approximate 1,500-gallon orphan USTs located side by side in the
southwest corner of the Site. These USTs appeared to be petroleum USTs used at a former gas
station that was previously located in that area. In accordance with the DEQ-approved EMP,
email notifications of the orphan UST discoveries were sent to DEQ within 48-hours of
discovery on January 13, 2023 and March 21, 2023.

The orphan USTs were identified in the southwest corner of the apartment building below a
future retail tenant space and located between two building footers and newly constructed
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August 2, 2023
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subgrade utility PVC piping. In accordance with the DEQ-approved EMP, the PD requested that
the USTs be abandoned in place to reduce potential damages to the newly constructed building
foundations and subgrade utility piping. DEQ Brownfields provided approval to abandon the
USTs in place in emails dated January 20, 2023 and March 22, 2023. The locations of the USTs
in relation to the building footers and subgrade utility piping are shown in Figure 3.

On January 13, 2023, Evo Corporation (Evo) mobilized to the Site with a vacuum truck and
removed approximately 475 gallons of fluids and residual sludge from the orphan UST
discovered in January 2023 for transport and disposal off-Site. On March 22, 2023, Contaminant
Control, Inc. (CCI) mobilized to the Site with a vacuum truck and removed approximately 386
gallons of fluids and residual sludge from the second orphan UST discovered in March 2023 for
transport and disposal off-Site. Copies of the UST fluid disposal manifests are provided in
Appendix B.

After the USTs were emptied, the tanks were uncovered and filled with concrete. After UST
abandonment and while the tanks were uncovered, H&H advanced soil borings along the
perimeter of the tanks to evaluate the potential for impacts that would be left in place. Soil
borings were advanced utilizing a decontaminated stainless steel hand auger to a depth below the
base of the USTs (i.e., 6 feet below ground surface). In general accordance with DEQ UST
Section guidelines, H&H collected two (2) samples along the side of the USTs and one (1)
sample at each end of the USTs for a total of eight (8) samples (UST-1 through UST-8). Boring
logs are provided in Appendix C, and soil sample locations are shown in Figure 3.

Soil samples selected for laboratory analysis were collected directly into laboratory supplied
glassware, labeled with the sample identification, date, time, and requested analyses, and placed
in a laboratory-supplied cooler with ice. The soil samples were delivered to Waypoint
Analytical (Waypoint) under standard chain of custody protocols for analysis of volatile organic
compounds (VOCs) by EPA Method 8260, semi-VOCs (SVOCs) by EPA Method 8270,
Resource Conservation and Recovery Act (RCRA) metals by EPA Methods 6020/7471, and
hexavalent chromium by EPA Method 7199. Soil sample laboratory analytical results are
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August 2, 2023
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summarized as Table 1, and a copy of the laboratory analytical report is provided as Appendix D.

Laboratory analytical results identified naphthalene (up to 22.4 milligrams per kilogram [mg/kg])
at concentrations above the DEQ Residential and Industrial/Commercial Preliminary Soil
Remediation Goals (PSRGs) in one closure soil sample (UST-2). The VOCs ethylbenzene (12.8
mg/kg), 1,2,4-trimethylbenzene (195 mg/kg), 1,3,5-trimethylbenzene (59.3 mg/kg), and total
xylenes (143 mg/kg) were also detected in closure soil sample UST-2 at concentrations
exceeding their respective DEQ Residential PSRGs. No other organic compounds were detected
at concentrations above the DEQ PSRGs in the soil samples collected adjacent to the USTs.

Several metals were detected at concentrations above the laboratory method detection limits in
the closure soil samples. Hexavalent chromium (up to 1.31 mg/kg) was detected at
concentrations exceeding the DEQ Residential PSRG, but below the DEQ Industrial/Commercial
PSRG in two soil samples (UST-4 and UST-7). The remaining concentrations of metals detected
were generally consistent with published concentrations for naturally occurring metals in North
Carolina soil and are considered representative of background conditions.

In accordance with the DEQ-approved EMP, petroleum impacted soil associated with the orphan
USTs was left in place and is covered with an impervious surface (i.e., within the building
footprint). Petroleum compounds were not detected above the DEQ PSRGs is any of the closure
soil samples, with the exception of one soil sample (UST-2) which was collected from a depth
greater than 6 ft below the proposed building slab. In addition, the orphan USTs were identified
in the southwest corner of the apartment building below a future retail tenant space where a
VIMS will be installed. Potential vapor intrusion concerns associated with residual soil impacts
from the orphan USTs can be safely managed through installation of the VIMS during
construction of the apartment building.

2.2 Soil Management

Grading activities to achieve final grade elevations for construction of the apartment building
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August 2, 2023
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and installation of building footers and subgrade utilities generated excess soil that could not be
re-used on-Site as part of construction activities. In accordance with the DEQ-approved EMP,
approximately 996 tons of excess soil were transported to Republic Services Landfill in Concord,
North Carolina, a Subtitle D lined landfill, for off-Site disposal. Copies of the Republic Services
Landfill weight tickets are provided in Appendix E.

2.3 Vapor Intrusion Mitigation System Installation

In accordance with the DEQ-approved VIMP, H&H personnel under the direction of the VIMS
design engineer, completed inspections for sub-slab and above slab components of the VIMS.
Inspections were conducted after placement of each of the VIMS components (i.e., sub-slab
collection piping, vapor barrier, vertical risers, and turbine fans) and prior to their cover to verify
that the VIMS was installed in general accordance with the DEQ-approved VIMS design.
Details associated with the VIMS installation will be documented under separate cover and
submitted at a later date.

3.0 Summary

In summary, redevelopment activities at the South and Hollis LoSo Brownfields property are on-
going and are being conducted in accordance with the DEQ-approved EMP. Two orphan
petroleum USTs were encountered and managed in accordance with the EMP. In addition, vapor
intrusion mitigation systems are being installed during construction of the apartment building in
accordance with the DEQ-approved VIMP.

Upon completion of construction activities and installation of impervious surfaces in exterior
areas surrounding the new building, H&H will observe the Site for unpaved areas. Based on
observations, and if appropriate, H&H will prepare a Work Plan outlining a proposed final grade
soil sampling approach for the DEQ Brownfields Program review and approval. In addition,
following completion of the VIMS installation activities, H&H will prepare a VIMS Installation
Completion Report for submittal to DEQ.
Table 1 Summary of UST Closure Soil Analytical DataSouth and Hollis LoSoCharlotte, North CarolinaH&H Job No. AKR-007Evaluation AreaSample IDUST-1 UST-2 UST-3 UST-4 UST-5 UST-6 UST-7 UST-8Date3/21/2023 3/21/2023 3/21/2023 3/21/2023 3/21/2023 3/21/2023 3/21/2023 3/21/2023Depth (ft bgs)5-6 5-6 5-6 5-6 5-6 5-6 5-6 5-6Sample TypeGrab Grab Grab Grab Grab Grab Grab GrabRange Range UnitsVOCs (8260D)Acetone 0.006 J<0.8230.0470.015 J 0.014 J 0.011 J 0.009 J0.006 J14,000210,000----Benzene 0.001 J<0.1980.002 J 0.001 J 0.004 J0.015<0.00080.001 J1.25.4----n-Butylbenzene<0.000610.50.001 J<0.0007 <0.0006 <0.0007 <0.0006<0.0000778012,000----sec-Butylbenzene<0.00073.330.001 J<0.0008 <0.0007 <0.0008 <0.0007<0.00081,60023,000----1,2-Dichloroethane 0.003 J<0.4730.002 J<0.0010.002 J0.0150.0070.0070.492.2----Ethylbenzene 0.002 J12.80.003 J<0.00080.005 J0.014<0.00080.003 J6.127----Isopropylbenzene 0.001 J5.200.001 J<0.00060.0009 J 0.002 J<0.00060.001 J4102,100----4-Isopropyl toluene <0.0011.82<0.001 <0.001 <0.001 <0.001 <0.001<0.001NENE----Methyl Ethyl Ketone <0.0008 <0.2230.0480.006 J 0.012 J<0.0009 <0.0009<0.00095,50040,000----Methylene Chloride <0.0010.777 J<0.001 <0.002 <0.001 <0.002 <0.001<0.00258650----Naphthalene<0.00122.40.007 J 0.002 J 0.005 J 0.004 J<0.0010.001 J2.18.8----n-Propylbenzene0.003 J22.20.003 J<0.00070.001 J 0.004 J<0.00070.003 J7805,100----Toluene0.0010 J9.790.008<0.00090.003 J0.124<0.0009<0.00099909,700----1,2,4-Trimethylbenzene0.0341950.0800.0180.0170.0520.0120.04363370----1,3,5-Trimethylbenzene0.01259.30.0260.004 J 0.005 J0.0140.0070.01356320----Xylenes (total)0.0571430.0540.0200.0490.2460.010 J0.094120530----SVOCs (8270E)1-Methylnaphthalene<0.1283.26<0.141 <0.145 <0.129 <0.146 <0.139<0.14718 73-- --2-Methylnaphthalene<0.1217.27<0.133 <0.137 <0.121 <0.138 <0.131<0.13948 600-- --Naphthalene <0.17415.9<0.192 <0.198 <0.175 <0.199 <0.189<0.2002.1 8.8-- --Metals (6020B/7471A/7199)Arsenic0.5740.5210.5140.3780.3740.3470.3740.4470.683.01.28 - 3.03 1.0 - 18Barium75.711311795.31301481091563,10047,000 38.1 - 94.6 50 - 1,000Cadmium<0.0314 <0.0355 <0.0346 <0.0356 <0.03150.0387 J<0.03410.0462 J1.420ND - 0.4341.0 - 10Chromium (total)25.136.683.713926.8123123126NENE47.1 - 59.9 7.0 - 300Chromium (VI)<0.171 <0.1930.230 J1.31<0.1740.6951.01<0.1960.316.5ND - 0.540NSChromium (III) *25.136.683.5137.726.8122.312212623,000350,000 47.1 - 59.4NSLead2.1013.42.681.802.271.081.311.144008007.33 - 11.6 ND - 50Mercury<0.0240 <0.0295 <0.0286 <0.0289 <0.0241 <0.0308 <0.0267 <0.03204.7700.0365 - 0.05020.03 - 0.52Selenium0.7170.5450.4510.4420.3940.4370.4820.391781,200 0.586 - 1.04<0.1 - 0.8Silver0.0253 J 0.0128 J 0.0178 J 0.0138 J 0.0182 J 0.0246 J 0.0152 J 0.0204 J 781,200NDND - 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2023. 2) Local metal background soil sample results from Charlotte Van and Storage Brownfields Assessments (Brownfields Project No. 23057-19-060). 3) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils. Soil concentrations are reported in milligrams per kilogram (mg/kg).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.Aside from metals, only constituents detected in at least one sample are shown in the table above.*Chromium (III) is a calculated value.Bold values exceed the Residential PSRG and background levels in the case of metals. Shaded values exceed the Industrial/Commercial PSRG. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface; UST = underground storage tank; NE = not established; NS = not specified; ND = not detected; -- = not applicableJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. mg/kgUSTs Abandoned In-PlaceBackground Metals on Nearby Brownfields (2)Published Background Metals (3) Residential PSRGs (1)Industrial/ Commercial PSRGs (1)Screening Criteria https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Akridge/AKR.007 LoSo Brownfields Implementation/Site Work/Orphan UST ‐ January 2023/Tables/Data Tables_USTTable 1 (Page 1 of 1)Hart & Hickman, PC
USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; USGS Global Ecosystems; U.S. CensusBureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.Department of State Humanitarian Information Unit; and NOAA NationalCenters for Environmental Information, U.S. Coastal Relief Model. Datarefreshed August, 2021.
SITE LOCATION MAP
SOUTH AND HOLLIS LOSOSOUTH BOULEVARD AND HOLLIS ROADCHARLOTTE, NORTH CAROLINA
DATE: 7-25-2023
JOB NO: AKR-007
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Akridge\AKR.007 LoSo Brownfields Implementation\Redevelopment Report\2022\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE EAST, NORTH CAROLINA 2019
CHARLOTTE WEST, NORTH CAROLINA 2019
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. AKR-007
DATE: 7-25-23
FIGURE NO. 2
SOUTH AND HOLLIS LOSO
SOUTH BOULEVARD AND HOLLIS ROAD
CHARLOTTE, NORTH CAROLINA
SITE MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
HO
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CONSTRUCTION
MULTI-TENANT RETAIL(3609 SOUTH BOULEVARD)
RESIDENTIAL
WESTON STREETSOUTH BOULEVARDSOUTH BOULEVARDHA
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NOTES:
1. PARCEL DATA AND AERIAL IMAGERY OBTAINED FROMMECKLENBURG COUNTY GIS, 2023.
SATTO TIRES(3407 SOUTH BOULEVARD)
MASTER AUTO COLLISION(3411 SOUTH BOULEVARD)S:\AAA-Master Projects\Akridge\AKR.007 LoSo Brownfields Implementation\Redevelopment Report\2022\Figures\Site Map_20220810.dwg, FIG.2 (2), 7/25/2023 3:16:16 PM, shaynes
REVISION NO. 0
JOB NO. AKR-007
DATE: 7-25-23
FIGURE NO. 3
SOUTH AND HOLLIS LOSO
SOUTH BOULEVARD AND HOLLIS ROAD
CHARLOTTE, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY LINE
NEW SUBGRADE PVC PIPING
RAILROAD TRACKS
PROPOSED RESIDENTIAL APARTMENTS
PROPOSED RETAIL OR AMENITY SPACE
PROPOSED PARKING DECK
BUILDING FOOTER
UNDERGROUND STORAGE TANK
SOIL BORING
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
NOTES:
1. PARCEL DATA OBTAINED FROM MECKLENBURG
COUNTY GIS, 2021.2. REDEVELOPMENT PLAN PROVIDED BY LANDDESIGN DATED FEBRUARY 2021.3. SOIL SAMPLES COLLECTED BY H&H ON 3/21/2023
4. THE BUILDING FOOTER WAS CONSTRUCTED ABOVE THE ORPHAN UST DEPICTED IN THE INSET. 5. PVC = POLYVINYL CHLORIDE6. UST = UNDERGROUND STORAGE TANK.
PROPOSEDCOURTYARD/POOL WESTON STREETHO
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UST-5
UST-6
UST-7
UST-8
SCALE:1'=10"
UST-4
S:\AAA-Master Projects\Akridge\AKR.007 LoSo Brownfields Implementation\Site Work\Orphan UST - January 2023\Figures\Site and Sample Location Map.dwg, FIG.2 SITE & SAMPLE, 4/24/2023 12:21:19 PM, tmarbueryUST
UST

Appendix A

Overall Site Plan

(Prepared by LandDesign)
VANCCCCVANEVVANVANC C C C C
C CC CUPDNUPDNUPUPFDFDFDFDFDFD4.1%SLOPEDN 3.7%SLOPEDN2.0% SLOPE(MAX.)UP6.5%SLOPEUP
DNDNA5.1-MC3-M1A3-M1A4-M1CORRIDORA5-M1A5-M1B2-M1A4-M1A4-M1B2-M1A1-M1A1-M1B2-M1A3-M1A3-M1A3-M1A4-M2ELEC.STOR.CHEMSTOR.POOL EQELEC.A5-MHCA5-M2A1-M1A1-M1A1-M1RETAIL BRETAIL APET SPAB2-M1A5-M4A1-M1A4-M3B2-M1A1-M1A1-M1ELEC.A3-M2A1-M2A1-M2STOR.MECH.MAINELEC.MECH.STAIR 3CORRIDORRESIDENTTRASHRETAILTRASHMAINTENANCECYCLECENTERSTAIR 1GARAGEELEV.LOBBYSTAIR 2RETAIL BELEC.TRASHOFFICEOFFICEMAILLEASINGMECHWORK ROOMA/VLIBRARY /RIDESHARELOUNGE"THE CUBE"MECH.MECH.JAN.MECH.WOMENMENMECH.MECH.CLUBFITNESSGAME ROOMYOGAMECH.A/VHC STOR.HC STOR.BACKFLOW/SPRINKLEREXITPASSAGEWAYA5-M5OVERSIZEDPACKAGESBORROWER'SROOOMCOWORKGARAGESPRINKLERSTAIR 4RETAIL AELECADDITIONAL FLEXOUTDOORPROGRAMMINGADDITIONAL FLEX OUTDOORPROGRAMMINGFENCESITE WALLFLUSH CURB W/BOLLARDSROADWAY LIGHT, TYP.PROPOSED ROADWAY LIGHT, TYP. TOBE CONFIRMED BY DUKE ENERGYPROPOSEDROADWAY LIGHT,TYP. TO BECONFIRMED BYDUKE ENERGYPROPOSED PED LIGHTPROPOSED PED LIGHTEXISTING POLE + LIGHTTO REMAINPROPOSEDPED LIGHTDOG AREA-SEEMATERIALSPLANDW-2DW-1DW-3TYPE II MODIFIED DRIVEWAYCLDSM 10.25ETYPE II MODIFIED DRIVEWAYCLDSM 10.25EDIRECTIONAL RAMPTIE INTO EXISTINGCURB + GUTTERTIE INTO EXISTINGCURB + GUTTERTIE INTO EXISTINGCURB + GUTTERTIE INTO EXISTINGCURB + GUTTEREX. PIANO STYLE CROSSWALKTYPE II MODIFIED DRIVEWAYCLDSM 10.25ESITE WALLMIN. 26 LONG-TERMSPACES LOCATEDWITHIN CYCLECENTER6 SHORT-TERM BIKE PARKING SPACESPAVING BAND TO ALIGN WITH EDGE OFRECESSED BUILDING AND BE EQUALDISTANCE FROM DOOR CENTERPAVING BAND TO ALIGN WITH EDGE OFRECESSED BUILDING AND BE EQUALDISTANCE FROM DOOR CENTER4 SHORT-TERMBIKE PARKINGSPACESDIRECTIONALCURB RAMPMIN. 576 SFREQUIRED FORRECYCLING797 SF PROVIDEDOUTDOOR KITCHENW/ NATURAL GASGRILLSFUTURE BOC32.5' FROM CL24' SETBACK FROM FUTURE BOC(TRANSIT CORRIDOR)16' SETBACK FROM FUTURE BOC(OTHER FRONTAGE)FUTURE BOC20.5' FROM CL16' SETBACK FROM FUTURE BOC(OTHER FRONTAGE)PROPOSED BOCHOLLIS ROADSECONDARY FRONTAGESOUTH BLVD4+ AVE PRIMARY FRONTAGE
WESTON ST
SECONDARY FRONTAGE TOD-TR10 x 10' SITE TRIANGLE10 x 10' SITE TRIANGLE200' RADIUS FROMSINGLE FAMILY ZONING50 x 50' SITE TRIANGLE(1) 10' x 25' LOADING SPACE8' AMENITY ZONE FROMFUTURE BOC(PLANTING STRIP)MIN. 8' PEDESTRIAN ZONE8' AMENITY ZONE FROM BOC(CURBED PLANTER)ZONING BOUNDARY LINEADDITIONAL FLEX OUTDOORPROGRAMMING8' AMENITY ZONE FROM BOC(PLANTING STRIP)HOLLIS ROADSECONDARY FRONTAGEFIRE ACCESSTRANSFORMERSEXISTING ROWPROPERTY LINEEXISTING ROWPROPERTY LINETOD-CCTOD-TR
TOD-CC
TOD-TR
TOD-CC
TOD-TRTOD-CCBALCONIES ATUPPER LEVELSBALCONIES ATUPPER LEVELSBALCONIES ATUPPER LEVELSBUILDING OVERHANGAT UPPER LEVELSBUILDING OVERHANGAT UPPER LEVELSBUILDING OVERHANGAT UPPER LEVELSMETAL PANELSCREENING- BYARCHITECTURE3441 SOUTHAPARTMENTSKA LOSO HOLDINGS LLC3441 SOUTH BLVD.CHARLOTTE, NC1020155OVERALL SITE PLANN/AKSTAEELDIC1-038/23/2021 11:55 AM CASSIDY FRANKLIN \\CHFILES\PROJECTS\_2020\1020155\CAD\DOCUMENTATION\1020155_PLN_LYOT.DWGKEY MAPSEALSHEET NUMBERSHEET TITLELANDDESIGN PROJ.#SCALEPROJECTNORTHNO. DESCRIPTION DATEREVISION / ISSUANCEORIGINAL SHEET SIZE: 30" X 42"VERT:HORZ:CHECKED BY:DRAWN BY:DESIGNED BY:223 NORTH GRAHAM STREETCHARLOTTE, NC 28202704.333.0325WWW.LANDDESIGN.COMNC ENG. FIRM LICENSE # C-0658ISSUED FORPERMITTING#8/23/2021SEAL103.19.2021SCHEMATIC DESIGN206.11.2021DESIGN DEVELOPMENT308.23.202150% CONSTRUCTIONDOCUMENTS1" = 20'40200 10DEVELOPMENT SUMMARY:PARCEL ID NUMBER (PID#):14905303, 14905302, 14905301, 14905305, 14905306, 14905315, 14905314EXISTING PARCEL SIZE: 2.70 AC TOTALJURISDICTION:CITY OF CHARLOTTEEXISTING ZONING:TOD-CC, TOD-TREXISTING LAND USE:COMMERCIAL/ VACANTPROPOSED PRINCIPAL USE:MULTI-FAMILY APARTMENTS + RETAIL / COMMERCIALPROPOSED GROSS FLOOR AREA: 463,118 SF (10.6 AC)FLOOR AREA RATIO:10.6 AC/ 2.70 AC = 3.9 FARBUILDING SITING :BUILDING SETBACK:24' PRIMARY FRONTAGE (SOUTH BLVD)16' FOR SECONDARY FRONTAGE (HOLLIS ROAD)16' FOR SECONDARY FRONTAGE (WESTON STREET)BUILD-TO ZONE:0-10' (CC), 0-20' (TR)BUILD-TO-PERCENTAGE:80% PRIMARY ENTRANCE60% (CC) OR 40% (TR) SECONDARY ENTRANCEMIN. SIDE SETBACK LINE:NONE (UNLESS ABUTTING SINGLE FAM RES.)MIN. REAR SETBACK LINE:NONE (UNLESS ABUTTING SINGLE FAM RES.)TOTAL PROPOSED UNITS:310 UNITS361 BEDROOMSBUILDING HT. MIN. 24':BUILDING HT. MAX. REFER TO ARCH ELEVATIONS THIS SETTOD CC: 90'73' (ALONG SOUTH)TOD TR: 75' OR 65' * 66'-9" (ALONG HOLLIS)64'-7" (ALONG WESTON)*PURSUING BONUS, WITHIN 200' SINGLE FAMILY RESIDENTIAL-DEVELOPMENT SHALL PURSUE HEIGHT BONUS AS ALLOWED BY CHAPTER 15 OF THE CHARLOTTE ZONING ORDINANCE.PARKING CALCULATIONS :MAXIMUM PARKING: MULTI-FAMILY: 1.1 SPACE/ BEDROOM = 398 MAX. SPACES(EXCLUDING REQ. ADA + ON-STREET PARKING)RETAIL/ COMMERCIAL:9000 SF RETAIL5/1000 GFA MAX 9 X 5 = 45 MAX SPACES RETAILPROVIDED PARKING: 424 TOTAL SPACES (443 MAX ALLOWED)-365 STANDARD SURFACE PARKING SPACES-45 COMPACT SPACES-14 ACCESSIBLE SPACES (4 VAN, 10 REGULAR)- (1) 10' x 25' OFF-STREET LOADING SPACEBIKE PARKING REQUIREMENTSRESIDENTIAL:15 DU OR NOT TO EXCEED 30LONG-TERM SPACES:80%(30)= 24 SPACES LONG-TERM SPACES PROVIDEDSHORT-TERM SPACES:6 SHORT TERM SPACES PROVIDEDCOMMERICAL:1/ 1,500 SF GFA, 9,000 SF/ 1,500 = 6 SPACES REQUIREDLONG-TERM SPACES:25%(6)= 2 LONG-TERM SPACES PROVIDEDSHORT-TERM SPACES:4 SHORT TERM SPACES PROVIDEDOPEN SPACE REQUIREMENTS:OPEN SPACE (10%): REQUIRED: 0.27 ACPROVIDED: 0.28 AC (12,140 SF)OPEN SPACE TO INCLUDE BUT NOT LIMITED TO: HARDSCAPE PLAZA AREAS WITH VARIED SEATING, LIGHTING ANDOVERHEAD SHADE STRUCTURES AND LANDSCAPING. OUTDOOR POOL, KITCHEN AND GRILL AREAS AND FLEXIBLELAWN SPACE.SOLID WASTE SUMMARY:REQUIRED: 8 CU YARD DUMPSTER PER 30 UNITS OR 8 CU YARD COMPACTOR PER 90 UNITS310 UNITS/ 90= 3.44 X 8= 27.5 CU YARDS COMPACTOR REQUIREDPROVIDED: 28 CU YARDS PROVIDEDREQUIRED: 4 RECYCLING STATIONS FOR 241 - 320 UNITS (4 X 144 SQ FT = 576 SQ FT TOTAL)PROVIDED: 797 SQ FT TOTALREFER TO ARCHITECTURE DECK PLANS FOR TRASH COMPACTOR/ RECYCLING AREATREE SAVE REQUIREMENTS:TREE SAVE REQUIRED: N/A- EXEMPT IN TOD DISTRICTTREE MITIGATION PROVIDED:N/A- EXEMPT IN TOD DISTRICTOPENSPACE37.77'36.32'73.18'36.00'PROMINENT ENTRANCEREQUIRED EVERY 150'ON PRIMARY FRONTAGEPROMINENTENTRANCEPROMINENT ENTRANCE NOTREQUIRED ALONG SECONDARYFRONTAGE IN TOD CC/TR80% BUILDING REQUIRED INBUILD-TO-ZONE (PRIMARY)220 LF OUT OF 260 LF WITHINBUILD-TO-ZONE (84%)60% BUILDING REQUIRED INBUILD-TO-ZONE (SECONDARY)190 LF OUT OF 320 LF WITHINBUILD-TO-ZONE (60%)OPEN SPACE(4,925 SF)OPEN SPACE(928 SF)OPEN SPACE(983 SF)PROMINENT ENTRANCE NOTREQUIRED ALONG SECONDARYFRONTAGE IN TOD CC/TR40% BUILDING REQUIRED INBUILD-TO-ZONE (SECONDARY)112 LF OUT OF 112 LF WITHINBUILD-TO-ZONE (100%)PROMINENTENTRANCEPROMINENTENTRANCEPROMINENTENTRANCEPROMINENTENTRANCEOPEN SPACE(1,590 SF)OPEN SPACE(700 SF)OPEN SPACE(310 SF)OPEN SPACE(1,280 SF)OPEN SPACE(1,130 SF)PROMINENTENTRANCE36.00'32.50' CL TO FUTURE BOC18.00' CL
T
O

E
O
P
18.00' CL TO EOPOPEN SPACE(320 SF)32.50' CL TO FUTURE BOC

Appendix B

UST Fluid Disposal Documentation

Appendix C

Boring Logs
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-1
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') SILT (ML); some clay, medium stiff, dry, gray and dark green
(4.0') SILT (ML); trace fine-medium sand, stiff, dry, dark green and brown
(6') Boring terminated
20.2
34.1
25.8
8.2
24.4
26.6 UST-1
0
5
10
SQM
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-2
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') SILT (ML); some clay, medium stiff, dry, gray and dark green
(1.5') Lean CLAY (CL); trace fine-medium sand, some silt, medium plasticity, stiff, dry,
dark green
(4.0') SILT (ML); trace clay, medium stiff, dry, gray and dark brown
(6') Boring terminated
17.8
31.5
50.3
46.0
227.4
1,683 UST-2
0
5
10
SQM
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-3
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') SILT (ML); some clay, medium stiff, dry, gray and dark green
(2.0') Lean CLAY (CL); trace fine-medium sand, some silt, medium plasticity, stiff, dry,
dark gray
(3.5') SILT (ML); some clay, medium stiff, dry, gray and dark brown
(6') Boring terminated
7.0
2.3
2.4
4.0
3.8
9.3 UST-3
0
5
10
SQM
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') Lean CLAY (CL); some silt, medium plasticity, stiff, dry, brown and gray
(1.0') SILT (ML); some clay, medium stiff, dry, dark gray and brown
(3.5') Lean CLAY (CL); trace fine-medium sand, some silt, medium plasticity, stiff, dry, dark brown and gray
(6') Boring terminated
1.3
0.9
1.1
2.8
5.8
6.3 UST-4
0
5
10
SQM
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') SILT (ML); some clay, medium stiff, dry, gray and dark brown
(2.5') Lean CLAY (CL); trace fine-medium sand, some silt, medium plasticity, stiff, dry,
dark brown and gray
(5.0') SILT (ML); trace fine-medium sand, some clay, medium stiff, moist, gray and dark brown
(6') Boring terminated
1.6
1.7
2.6
5.5
14.4
22.2 UST-5
0
5
10
SQM
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') SILT (ML); some clay, medium stiff, dry, dark brown and gray
(2.0') SILT (ML); trace fine-medium sand, trace clay, stiff, dry, gray
(3.0') SILT (ML); some clay, medium stiff, dry, gray, dark brown and dark green
(6') Boring terminated
1.7
3.9
13.6
34.1
59.9
85.1 UST-6
0
5
10
SQM
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') SILT (ML); some clay, medium stiff, dry, dark brown and green
(3.5') SILT (ML); trace clay, medium stiff, moist, dark brown, gray, and dark green
(6') Boring terminated
17.1
19.0
21.3
23.3
16.6
17.9 UST-7
0
5
10
SQM
NOTES: Boring start depth ~3' bgs (top of USTs).
generated using GroundLogs.online
Client:
Project:
Address:
Akridge
AKR-007
South Blvd and Hollis Rd, Charlotte,NC
BORING LOG
Boring No.
Page:
UST-8
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/21/23
3/21/23
Hart and Hickman
Hand Auger
Hand Auger
AML
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
6.0
3.25
Grab
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
GR (0') SILT (ML); some clay, medium stiff, dry, gray and dark green
(1.5') Lean CLAY (CL); trace fine-medium sand, some silt, medium plasticity, stiff, dry,
dark green
(3.5') SILT (ML); some clay, medium stiff, moist, gray and brown
(6') Boring terminated
14.6
22.7
15.6
16.1
11.1
14.3 UST-8
0
5
10
SQM

Appendix D

Laboratory Analytical Report

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/3/2023
Hart & Hickman (Charlotte) Haley Martin
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 23-080-0013 Client Project Description: AKR-007
Dear Haley Martin:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/21/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 117
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-080-0013
Page 2 of 117
Report Number:
Sample Summary Table
Client Project Description:
23-080-0013
AKR-007
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
03/21/2023 09:20Solids 91771 UST-1 (5-6)03/21/2023 14:51
03/21/2023 09:20Solids 91771 UST-1 (5-6)03/21/2023 14:51 7471A WP MTN -
03/21/2023 09:20Solids 91771 UST-1 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
03/21/2023 09:20Solids 91771 UST-1 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 10:00Solids 91772 UST-2 (5-6)03/21/2023 14:51
03/21/2023 10:00Solids 91772 UST-2 (5-6)03/21/2023 14:51 7471A WP MTN -
03/21/2023 10:00Solids 91772 UST-2 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 10:00Solids 91772 UST-2 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
03/21/2023 10:30Solids 91773 UST-3 (5-6)03/21/2023 14:51
03/21/2023 10:30Solids 91773 UST-3 (5-6)03/21/2023 14:51 7471A WP MTN -
03/21/2023 10:30Solids 91773 UST-3 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
03/21/2023 10:30Solids 91773 UST-3 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 11:10Solids 91774 UST-4 (5-6)03/21/2023 14:51
03/21/2023 11:10Solids 91774 UST-4 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
03/21/2023 11:10Solids 91774 UST-4 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 11:10Solids 91774 UST-4 (5-6)03/21/2023 14:51 7471A WP MTN -
03/21/2023 11:55Solids 91775 UST-5 (5-6)03/21/2023 14:51
03/21/2023 11:55Solids 91775 UST-5 (5-6)03/21/2023 14:51 7471A WP MTN -
03/21/2023 11:55Solids 91775 UST-5 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
03/21/2023 11:55Solids 91775 UST-5 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 12:45Solids 91776 UST-6 (5-6)03/21/2023 14:51
03/21/2023 12:45Solids 91776 UST-6 (5-6)03/21/2023 14:51 7471A WP MTN -
03/21/2023 12:45Solids 91776 UST-6 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
03/21/2023 12:45Solids 91776 UST-6 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 13:25Solids 91777 UST-7 (5-6)03/21/2023 14:51
03/21/2023 13:25Solids 91777 UST-7 (5-6)03/21/2023 14:51 7471A WP MTN -
03/21/2023 13:25Solids 91777 UST-7 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 117
Report Number:
Sample Summary Table
Client Project Description:
23-080-0013
AKR-007
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
03/21/2023 13:25Solids 91777 UST-7 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 14:00Solids 91778 UST-8 (5-6)03/21/2023 14:51
03/21/2023 14:00Solids 91778 UST-8 (5-6)03/21/2023 14:51 SW-7199 WP MTN -
03/21/2023 14:00Solids 91778 UST-8 (5-6)03/21/2023 14:51 6020B WP MTN -
03/21/2023 14:00Solids 91778 UST-8 (5-6)03/21/2023 14:51 7471A WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 4 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-080-0013
Report Limit
Project:AKR-007
V 91771UST-1 (5-6)
0.574 03/27/2023 23:196020BArsenicmg/Kg - dry 0.104
75.7 03/27/2023 23:196020BBariummg/Kg - dry 0.051
25.1 03/27/2023 23:196020BChromiummg/Kg - dry 0.140
2.10 03/27/2023 23:196020BLeadmg/Kg - dry 0.0376
0.717 03/27/2023 23:196020BSeleniummg/Kg - dry 0.125
J0.0253 03/27/2023 23:196020BSilvermg/Kg - dry 0.0081
J0.006 03/27/2023 18:168260DAcetonemg/Kg - dry 0.002
J0.001 03/27/2023 18:168260DBenzenemg/Kg - dry 0.0007
J0.003 03/27/2023 18:168260D1,2-Dichloroethane mg/Kg - dry 0.001
J0.002 03/27/2023 18:168260DEthylbenzenemg/Kg - dry 0.0007
J0.001 03/27/2023 18:168260DIsopropylbenzenemg/Kg - dry 0.0006
J0.003 03/27/2023 18:168260Dn-Propylbenzene mg/Kg - dry 0.0007
J0.0010 03/27/2023 18:168260DToluenemg/Kg - dry 0.0008
0.034 03/27/2023 18:168260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
0.012 03/27/2023 18:168260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
0.057 03/27/2023 18:168260Dm,p-Xylene mg/Kg - dry 0.001
0.057 03/27/2023 18:168260DXylene (Total)mg/Kg - dry 0.0006
17.6 03/27/2023 15:04SW-DRYWT Moisture %
V 91772UST-2 (5-6)
0.521 03/27/2023 23:226020BArsenicmg/Kg - dry 0.117
113 03/27/2023 23:226020BBariummg/Kg - dry 0.058
36.6 03/27/2023 23:226020BChromiummg/Kg - dry 0.159
13.4 03/27/2023 23:226020BLeadmg/Kg - dry 0.0425
0.545 03/27/2023 23:226020BSeleniummg/Kg - dry 0.141
J0.0128 03/27/2023 23:226020BSilvermg/Kg - dry 0.0092
10.5 03/27/2023 20:328260Dn-Butylbenzene mg/Kg - dry 0.168
3.33 03/27/2023 20:328260Dsec-Butyl benzene mg/Kg - dry 0.192
12.8 03/27/2023 20:328260DEthylbenzenemg/Kg - dry 0.198
5.20 03/27/2023 20:328260DIsopropylbenzenemg/Kg - dry 0.157
1.82 03/27/2023 20:328260D4-Isopropyl toluene mg/Kg - dry 0.445
J0.777 03/27/2023 20:328260DMethylene Chloride mg/Kg - dry 0.504
22.4 03/27/2023 20:328260DNaphthalenemg/Kg - dry 0.340
22.2 03/27/2023 20:328260Dn-Propylbenzene mg/Kg - dry 0.185
9.79 03/27/2023 20:328260DToluenemg/Kg - dry 0.226
195 03/27/2023 20:598260D1,2,4-Trimethylbenzene mg/Kg - dry 1.69
59.3 03/27/2023 20:328260D1,3,5-Trimethylbenzene mg/Kg - dry 0.185
Page 5 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-080-0013
Report Limit
Project:AKR-007
V 91772UST-2 (5-6)
42.8 03/27/2023 20:328260Do-Xylene mg/Kg - dry 0.171
99.3 03/27/2023 20:328260Dm,p-Xylene mg/Kg - dry 0.432
143 03/27/2023 20:328260DXylene (Total)mg/Kg - dry 0.171
3.26 03/26/2023 20:198270E1-Methylnaphthalene mg/Kg - dry 0.145
7.27 03/26/2023 20:198270E2-Methylnaphthalene mg/Kg - dry 0.137
15.9 03/31/2023 10:418270ENaphthalenemg/Kg - dry 0.790
27.1 03/27/2023 15:04SW-DRYWT Moisture %
V 91773UST-3 (5-6)
0.514 03/27/2023 23:266020BArsenicmg/Kg - dry 0.114
117 03/27/2023 23:266020BBariummg/Kg - dry 0.057
83.7 03/28/2023 20:596020BChromiummg/Kg - dry 0.621
2.68 03/27/2023 23:266020BLeadmg/Kg - dry 0.0414
0.451 03/27/2023 23:266020BSeleniummg/Kg - dry 0.137
J0.0178 03/27/2023 23:266020BSilvermg/Kg - dry 0.0090
0.047 03/25/2023 19:168260DAcetonemg/Kg - dry 0.003
J0.002 03/25/2023 19:168260DBenzenemg/Kg - dry 0.0008
J0.001 03/25/2023 19:168260Dn-Butylbenzene mg/Kg - dry 0.0007
J0.001 03/25/2023 19:168260Dsec-Butyl benzene mg/Kg - dry 0.0007
J0.002 03/25/2023 19:168260D1,2-Dichloroethane mg/Kg - dry 0.001
J0.003 03/25/2023 19:168260DEthylbenzenemg/Kg - dry 0.0008
J0.001 03/25/2023 19:168260DIsopropylbenzenemg/Kg - dry 0.0006
0.048 03/25/2023 19:168260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
J0.007 03/25/2023 19:168260DNaphthalenemg/Kg - dry 0.001
J0.003 03/25/2023 19:168260Dn-Propylbenzene mg/Kg - dry 0.0007
0.008 03/25/2023 19:168260DToluenemg/Kg - dry 0.0009
0.080 03/25/2023 19:168260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
0.026 03/25/2023 19:168260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
0.008 03/25/2023 19:168260Do-Xylene mg/Kg - dry 0.0007
0.046 03/25/2023 19:168260Dm,p-Xylene mg/Kg - dry 0.001
0.054 03/25/2023 19:168260DXylene (Total)mg/Kg - dry 0.0007
J0.230 03/27/2023 16:46SW-7199 Chromium, Hexavalent mg/Kg - dry 0.194
25.3 03/27/2023 15:04SW-DRYWT Moisture %
V 91774UST-4 (5-6)
0.378 03/27/2023 23:376020BArsenicmg/Kg - dry 0.118
95.3 03/27/2023 23:376020BBariummg/Kg - dry 0.058
139 03/28/2023 21:106020BChromiummg/Kg - dry 0.638
Page 6 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-080-0013
Report Limit
Project:AKR-007
V 91774UST-4 (5-6)
1.80 03/27/2023 23:376020BLeadmg/Kg - dry 0.0426
0.442 03/27/2023 23:376020BSeleniummg/Kg - dry 0.141
J0.0138 03/27/2023 23:376020BSilvermg/Kg - dry 0.0092
J0.015 03/25/2023 19:438260DAcetonemg/Kg - dry 0.003
J0.001 03/25/2023 19:438260DBenzenemg/Kg - dry 0.0008
J0.006 03/25/2023 19:438260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
J0.002 03/25/2023 19:438260DNaphthalenemg/Kg - dry 0.001
0.018 03/25/2023 19:438260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.004 03/25/2023 19:438260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
0.020 03/25/2023 19:438260Dm,p-Xylene mg/Kg - dry 0.001
0.020 03/25/2023 19:438260DXylene (Total)mg/Kg - dry 0.0007
1.31 03/27/2023 17:19SW-7199 Chromium, Hexavalent mg/Kg - dry 0.193
27.3 03/27/2023 15:04SW-DRYWT Moisture %
V 91775UST-5 (5-6)
0.374 03/27/2023 23:416020BArsenicmg/Kg - dry 0.104
130 03/27/2023 23:416020BBariummg/Kg - dry 0.052
26.8 03/27/2023 23:416020BChromiummg/Kg - dry 0.141
2.27 03/27/2023 23:416020BLeadmg/Kg - dry 0.0377
0.394 03/27/2023 23:416020BSeleniummg/Kg - dry 0.125
J0.0182 03/27/2023 23:416020BSilvermg/Kg - dry 0.0082
J0.014 03/25/2023 20:118260DAcetonemg/Kg - dry 0.002
J0.004 03/25/2023 20:118260DBenzenemg/Kg - dry 0.0007
J0.002 03/25/2023 20:118260D1,2-Dichloroethane mg/Kg - dry 0.001
J0.005 03/25/2023 20:118260DEthylbenzenemg/Kg - dry 0.0007
J0.0009 03/25/2023 20:118260DIsopropylbenzenemg/Kg - dry 0.0006
J0.012 03/25/2023 20:118260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0008
J0.005 03/25/2023 20:118260DNaphthalenemg/Kg - dry 0.001
J0.001 03/25/2023 20:118260Dn-Propylbenzene mg/Kg - dry 0.0007
J0.003 03/25/2023 20:118260DToluenemg/Kg - dry 0.0008
0.017 03/25/2023 20:118260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
J0.005 03/25/2023 20:118260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
0.049 03/25/2023 20:118260Dm,p-Xylene mg/Kg - dry 0.001
0.049 03/25/2023 20:118260DXylene (Total)mg/Kg - dry 0.0006
17.9 03/27/2023 15:51SW-DRYWT Moisture %
V 91776UST-6 (5-6)
0.347 03/27/2023 23:446020BArsenicmg/Kg - dry 0.118
Page 7 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-080-0013
Report Limit
Project:AKR-007
V 91776UST-6 (5-6)
148 03/27/2023 23:446020BBariummg/Kg - dry 0.059
J0.0387 03/27/2023 23:446020BCadmiummg/Kg - dry 0.0358
123 03/28/2023 21:146020BChromiummg/Kg - dry 0.641
1.08 03/27/2023 23:446020BLeadmg/Kg - dry 0.0428
0.437 03/27/2023 23:446020BSeleniummg/Kg - dry 0.142
J0.0246 03/27/2023 23:446020BSilvermg/Kg - dry 0.0093
J0.011 03/26/2023 02:588260DAcetonemg/Kg - dry 0.003
0.015 03/26/2023 02:588260DBenzenemg/Kg - dry 0.0008
0.015 03/26/2023 02:588260D1,2-Dichloroethane mg/Kg - dry 0.001
0.014 03/26/2023 02:588260DEthylbenzenemg/Kg - dry 0.0008
J0.002 03/26/2023 02:588260DIsopropylbenzenemg/Kg - dry 0.0006
J0.004 03/26/2023 02:588260DNaphthalenemg/Kg - dry 0.001
J0.004 03/26/2023 02:588260Dn-Propylbenzene mg/Kg - dry 0.0007
0.124 03/26/2023 02:588260DToluenemg/Kg - dry 0.0009
0.052 03/26/2023 02:588260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
0.014 03/26/2023 02:588260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
0.035 03/26/2023 02:588260Do-Xylene mg/Kg - dry 0.0007
0.211 03/26/2023 02:588260Dm,p-Xylene mg/Kg - dry 0.001
0.246 03/26/2023 02:588260DXylene (Total)mg/Kg - dry 0.0007
0.695 03/27/2023 17:41SW-7199 Chromium, Hexavalent mg/Kg - dry 0.195
27.7 03/27/2023 15:51SW-DRYWT Moisture %
V 91777UST-7 (5-6)
0.374 03/27/2023 23:486020BArsenicmg/Kg - dry 0.113
109 03/27/2023 23:486020BBariummg/Kg - dry 0.056
123 03/28/2023 21:176020BChromiummg/Kg - dry 0.611
1.31 03/27/2023 23:486020BLeadmg/Kg - dry 0.0408
0.482 03/27/2023 23:486020BSeleniummg/Kg - dry 0.135
J0.0152 03/27/2023 23:486020BSilvermg/Kg - dry 0.0088
J0.009 03/25/2023 20:388260DAcetonemg/Kg - dry 0.003
0.007 03/25/2023 20:388260D1,2-Dichloroethane mg/Kg - dry 0.001
0.012 03/25/2023 20:388260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0006
0.007 03/25/2023 20:388260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0007
J0.010 03/25/2023 20:388260Dm,p-Xylene mg/Kg - dry 0.001
J0.010 03/25/2023 20:388260DXylene (Total)mg/Kg - dry 0.0007
1.01 03/27/2023 17:52SW-7199 Chromium, Hexavalent mg/Kg - dry 0.185
24.1 03/27/2023 15:51SW-DRYWT Moisture %
Page 8 of 117
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-080-0013
Report Limit
Project:AKR-007
V 91778UST-8 (5-6)
0.447 03/27/2023 23:526020BArsenicmg/Kg - dry 0.119
156 03/27/2023 23:526020BBariummg/Kg - dry 0.059
J0.0462 03/27/2023 23:526020BCadmiummg/Kg - dry 0.0360
126 03/28/2023 21:216020BChromiummg/Kg - dry 0.646
1.14 03/27/2023 23:526020BLeadmg/Kg - dry 0.0431
0.391 03/27/2023 23:526020BSeleniummg/Kg - dry 0.143
J0.0204 03/27/2023 23:526020BSilvermg/Kg - dry 0.0093
J0.006 03/25/2023 21:058260DAcetonemg/Kg - dry 0.003
J0.001 03/25/2023 21:058260DBenzenemg/Kg - dry 0.0008
0.007 03/25/2023 21:058260D1,2-Dichloroethane mg/Kg - dry 0.001
J0.003 03/25/2023 21:058260DEthylbenzenemg/Kg - dry 0.0008
J0.001 03/25/2023 21:058260DIsopropylbenzenemg/Kg - dry 0.0006
J0.001 03/25/2023 21:058260DNaphthalenemg/Kg - dry 0.001
J0.003 03/25/2023 21:058260Dn-Propylbenzene mg/Kg - dry 0.0008
0.043 03/25/2023 21:058260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
0.013 03/25/2023 21:058260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0008
0.094 03/25/2023 21:058260Dm,p-Xylene mg/Kg - dry 0.001
0.094 03/25/2023 21:058260DXylene (Total)mg/Kg - dry 0.0007
28.2 03/27/2023 15:51SW-DRYWT Moisture %
Page 9 of 117

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: AKR-007 Lab Report Number: 23-080-0013
Date: 4/3/2023
Metals Analyses Method 6020B Sample 91778 (UST-8 (5-6)) Analyte: Arsenic QC Batch No: L672456/L671954 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91778 (UST-8 (5-6))
Analyte: Barium QC Batch No: L672456/L671954
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 91778 (UST-8 (5-6))
Analyte: Chromium QC Batch No: L672850/L671954
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91778 (UST-8 (5-6)) Analyte: Selenium QC Batch No: L672456/L671954
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected. Hexavalent Chromium by Ion Chromatography Method SW-7199 Analyte: Hexavalent Chromium QC Batch No: L672114 Matrix Spike Recovery Low: A measure of the sample pH and its oxidation reduction potential (ORP) indicate that
the sample has reducing qualities which may not allow for the presence of Hexavalent Chromium. Solids Total Mercury Analysis - CVAA Method 7471A Sample 61457 (NG5) Analyte: Mercury QC Batch No: L672319/L672056 The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control acceptance ranges. Matrix interference is suspected
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Acetone QC Batch No: V31266/V31299 CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. Results are reported but considered estimated.
Page 10 of 117

Analyte: Acetone QC Batch No: V31301/V31299
CCV result is below the control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. Results are reported but considered estimated.
Semivolatile Organic Compounds - GC/MS Method 8270E
Analyte: 2,4-Dimethylphenol QC Batch No: V31378/V31133
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Analyte: 2,4-Dimethylphenol QC Batch No: V31392/V31133
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.

Page 11 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.6 %Moisture 1 03/27/23 15:04 SW-DRYWTPEB
<0.171 mg/Kg - dry 0.171 0.242Chromium, Hexavalent 1 03/27/23 16:24 SW-7199SRJ
0.574 mg/Kg - dry 0.104 0.303Arsenic 5 03/27/23 23:19 6020BCPW
75.7 mg/Kg - dry 0.051 0.303Barium 5 03/27/23 23:19 6020BCPW
<0.0314 mg/Kg - dry 0.0314 0.303Cadmium 5 03/27/23 23:19 6020BCPW
25.1 mg/Kg - dry 0.140 0.303
Chromium 5 03/27/23 23:19 6020BCPW
2.10 mg/Kg - dry 0.0376 0.303Lead 5 03/27/23 23:19 6020BCPW
<0.0240 mg/Kg - dry 0.0240 0.199Mercury (Total)1 03/27/23 12:31 7471AFDS
0.717 mg/Kg - dry 0.125 0.303Selenium 5 03/27/23 23:19 6020BCPW
0.0253 J mg/Kg - dry 0.0081 0.303Silver 5 03/27/23 23:19 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31299 03/27/23 08:00
0.006 J mg/Kg - dry 0.002 0.024Acetone 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 03/27/23 18:16 V31301TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 03/27/23 18:16 V31301TBL
0.001 J mg/Kg - dry 0.0007 0.006Benzene 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 03/27/23 18:16 V31301TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/27/23 18:16 V31301TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/27/23 18:16 V31301TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 03/27/23 18:16 V31301TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/27/23 18:16 V31301TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/27/23 18:16 V31301TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 03/27/23 18:16 V31301TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/27/23 18:16 V31301TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/27/23 18:16 V31301TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31299 03/27/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 03/27/23 18:16 V31301TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 03/27/23 18:16 V31301TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/27/23 18:16 V31301TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/27/23 18:16 V31301TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/27/23 18:16 V31301TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/27/23 18:16 V31301TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 03/27/23 18:16 V31301TBL
0.003 J
mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/27/23 18:16 V31301TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 03/27/23 18:16 V31301TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/27/23 18:16 V31301TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 03/27/23 18:16 V31301TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/27/23 18:16 V31301TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 03/27/23 18:16 V31301TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/27/23 18:16 V31301TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 03/27/23 18:16 V31301TBL
<0.016 mg/Kg - dry 0.016 0.303Ethanol 1 03/27/23 18:16 V31301TBL
0.002 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 03/27/23 18:16 V31301TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 03/27/23 18:16 V31301TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31299 03/27/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/27/23 18:16 V31301TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 03/27/23 18:16 V31301TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/27/23 18:16 V31301TBL
<0.0008 mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 03/27/23 18:16 V31301TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/27/23 18:16 V31301TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.012
Naphthalene 1 03/27/23 18:16 V31301TBL
0.003 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/27/23 18:16 V31301TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/27/23 18:16 V31301TBL
0.0010 J mg/Kg - dry 0.0008 0.006Toluene 1 03/27/23 18:16 V31301TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 03/27/23 18:16 V31301TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/27/23 18:16 V31301TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/27/23 18:16 V31301TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 03/27/23 18:16 V31301TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/27/23 18:16 V31301TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31299 03/27/23 08:00
0.034 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/27/23 18:16 V31301TBL
0.012 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 03/27/23 18:16 V31301TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/27/23 18:16 V31301TBL
0.057 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/27/23 18:16 V31301TBL
0.057 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/27/23 18:16 V31301
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%03/27/23 18:161 TBL V31301
Surrogate: Dibromofluoromethane 106 Limits: 84-123%03/27/23 18:161 TBL V31301
Surrogate: Toluene-d8 96.2 Limits: 76-129%03/27/23 18:161 TBL V31301
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.140 mg/Kg - dry 0.140 0.800Acenaphthene 1 03/26/23 19:56 V31392JMV
<0.127 mg/Kg - dry 0.127 0.800Acenaphthylene 1 03/26/23 19:56 V31392JMV
<0.184 mg/Kg - dry 0.184 0.800Aniline 1 03/26/23 19:56 V31392JMV
<0.173 mg/Kg - dry 0.173 0.800Anthracene 1 03/26/23 19:56 V31392JMV
<0.168 mg/Kg - dry 0.168 0.800
Benzo(a)anthracene 1 03/26/23 19:56 V31392JMV
<0.178 mg/Kg - dry 0.178 0.800Benzo(a)pyrene 1 03/26/23 19:56 V31392JMV
<0.177 mg/Kg - dry 0.177 0.800Benzo(b)fluoranthene 1 03/26/23 19:56 V31392JMV
<0.165 mg/Kg - dry 0.165 0.800Benzo(g,h,i)perylene 1 03/26/23 19:56 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.166 mg/Kg - dry 0.166 0.800Benzo(k)fluoranthene 1 03/26/23 19:56 V31392JMV
<0.703 mg/Kg - dry 0.703 2.43
Benzoic Acid 1 03/26/23 19:56 V31392JMV
<0.127 mg/Kg - dry 0.127 0.800Benzyl alcohol 1 03/26/23 19:56 V31392JMV
<0.143 mg/Kg - dry 0.143 0.800Bis(2-Chloroethoxy)methane 1 03/26/23 19:56 V31392JMV
<0.129 mg/Kg - dry 0.129 0.800Bis(2-Chloroethyl)ether 1 03/26/23 19:56 V31392JMV
<0.165 mg/Kg - dry 0.165 0.400Bis(2-Chloroisopropyl)ether 1 03/26/23 19:56 V31392JMV
<0.145 mg/Kg - dry 0.145 0.800Bis(2-ethylhexyl)phthalate 1 03/26/23 19:56 V31392JMV
<0.132 mg/Kg - dry 0.132 0.8004-Bromophenyl phenyl ether 1 03/26/23 19:56 V31392JMV
<0.137 mg/Kg - dry 0.137 0.400
Butyl benzyl phthalate 1 03/26/23 19:56 V31392JMV
<0.112 mg/Kg - dry 0.112 0.8004-Chloro-3-methylphenol 1 03/26/23 19:56 V31392JMV
<0.135 mg/Kg - dry 0.135 0.4004-Chloroaniline 1 03/26/23 19:56 V31392JMV
<0.140 mg/Kg - dry 0.140 0.8002-Chloronaphthalene 1 03/26/23 19:56 V31392JMV
<0.119 mg/Kg - dry 0.119 0.8002-Chlorophenol 1 03/26/23 19:56 V31392JMV
<0.152 mg/Kg - dry 0.152 1.214-Chlorophenyl phenyl ether 1 03/26/23 19:56 V31392JMV
<0.172 mg/Kg - dry 0.172 0.800Chrysene 1 03/26/23 19:56 V31392JMV
<0.279 mg/Kg - dry 0.279 0.800Dibenz(a,h)anthracene 1 03/26/23 19:56 V31392JMV
<0.144 mg/Kg - dry 0.144 0.800Dibenzofuran 1 03/26/23 19:56 V31392JMV
<0.114 mg/Kg - dry 0.114 0.8001,2-Dichlorobenzene 1 03/26/23 19:56 V31392JMV
<0.118 mg/Kg - dry 0.118 0.8001,3-Dichlorobenzene 1 03/26/23 19:56 V31392JMV
<0.118 mg/Kg - dry 0.118 0.4001,4-Dichlorobenzene 1 03/26/23 19:56 V31392JMV
<0.178 mg/Kg - dry 0.178 0.8003,3'-Dichlorobenzidine 1 03/26/23 19:56 V31392JMV
<0.116 mg/Kg - dry 0.116 0.8002,4-Dichlorophenol 1 03/26/23 19:56 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.218 mg/Kg - dry 0.218 0.800Diethyl phthalate 1 03/26/23 19:56 V31392JMV
<0.211 mg/Kg - dry 0.211 0.800
Dimethyl phthalate 1 03/26/23 19:56 V31392JMV
<0.131 mg/Kg - dry 0.131 0.4002,4-Dimethylphenol 1 03/26/23 19:56 V31392JMV
<0.129 mg/Kg - dry 0.129 0.800Di-n-butyl phthalate 1 03/26/23 19:56 V31392JMV
<0.291 mg/Kg - dry 0.291 1.824,6-Dinitro-2-methylphenol 1 03/26/23 19:56 V31392JMV
<0.631 mg/Kg - dry 0.631 1.822,4-Dinitrophenol 1 03/26/23 19:56 V31392JMV
<0.117 mg/Kg - dry 0.117 0.8002,4-Dinitrotoluene 1 03/26/23 19:56 V31392JMV
<0.131 mg/Kg - dry 0.131 0.8002,6-Dinitrotoluene 1 03/26/23 19:56 V31392JMV
<0.173 mg/Kg - dry 0.173 0.400
Di-n-Octyl Phthalate 1 03/26/23 19:56 V31392JMV
<0.149 mg/Kg - dry 0.149 0.800Fluoranthene 1 03/26/23 19:56 V31392JMV
<0.155 mg/Kg - dry 0.155 0.800Fluorene 1 03/26/23 19:56 V31392JMV
<0.128 mg/Kg - dry 0.128 0.800Hexachlorobenzene 1 03/26/23 19:56 V31392JMV
<0.118 mg/Kg - dry 0.118 0.800Hexachlorobutadiene 1 03/26/23 19:56 V31392JMV
<0.190 mg/Kg - dry 0.190 0.800Hexachlorocyclopentadiene 1 03/26/23 19:56 V31392JMV
<0.096 mg/Kg - dry 0.096 0.800Hexachloroethane 1 03/26/23 19:56 V31392JMV
<0.217 mg/Kg - dry 0.217 0.800Indeno(1,2,3-cd)pyrene 1 03/26/23 19:56 V31392JMV
<0.231 mg/Kg - dry 0.231 0.800Isophorone 1 03/26/23 19:56 V31392JMV
<0.128 mg/Kg - dry 0.128 0.8001-Methylnaphthalene 1 03/26/23 19:56 V31392JMV
<0.121 mg/Kg - dry 0.121 0.8002-Methylnaphthalene 1 03/26/23 19:56 V31392JMV
<0.117 mg/Kg - dry 0.117 0.8002-Methylphenol 1 03/26/23 19:56 V31392JMV
<0.103 mg/Kg - dry 0.103 0.8003&4 Methylphenol 1 03/26/23 19:56 V31392JMV
<0.174 mg/Kg - dry 0.174 0.800Naphthalene 1 03/26/23 19:56 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-1 (5-6)
91771 Matrix:
3/21/2023 9:20
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.117 mg/Kg - dry 0.117 0.8002-Nitroaniline 1 03/26/23 19:56 V31392JMV
<0.145 mg/Kg - dry 0.145 0.800
3-Nitroaniline 1 03/26/23 19:56 V31392JMV
<0.113 mg/Kg - dry 0.113 0.4004-Nitroaniline 1 03/26/23 19:56 V31392JMV
<0.140 mg/Kg - dry 0.140 0.400Nitrobenzene 1 03/26/23 19:56 V31392JMV
<0.107 mg/Kg - dry 0.107 0.8002-Nitrophenol 1 03/26/23 19:56 V31392JMV
<0.141 mg/Kg - dry 0.141 0.8004-Nitrophenol 1 03/26/23 19:56 V31392JMV
<0.319 mg/Kg - dry 0.319 0.800N-Nitrosodimethylamine 1 03/26/23 19:56 V31392JMV
<0.219 mg/Kg - dry 0.219 0.800N-Nitrosodiphenylamine 1 03/26/23 19:56 V31392JMV
<0.143 mg/Kg - dry 0.143 0.800
N-Nitroso-di-n-propylamine 1 03/26/23 19:56 V31392JMV
<0.421 mg/Kg - dry 0.421 1.21Pentachlorophenol 1 03/26/23 19:56 V31392JMV
<0.252 mg/Kg - dry 0.252 0.800Phenanthrene 1 03/26/23 19:56 V31392JMV
<0.135 mg/Kg - dry 0.135 0.800Phenol 1 03/26/23 19:56 V31392JMV
<0.162 mg/Kg - dry 0.162 0.800Pyrene 1 03/26/23 19:56 V31392JMV
<0.096 mg/Kg - dry 0.096 0.400Pyridine 1 03/26/23 19:56 V31392JMV
<0.129 mg/Kg - dry 0.129 0.8001,2,4-Trichlorobenzene 1 03/26/23 19:56 V31392JMV
<0.116 mg/Kg - dry 0.116 0.8002,4,5-Trichlorophenol 1 03/26/23 19:56 V31392JMV
<0.117 mg/Kg - dry 0.117 0.8002,4,6-Trichlorophenol 1 03/26/23 19:56 V31392JMV
8270ESurrogate: Phenol-d5 65.5 Limits: 34-121%03/26/23 19:561 JMV
Surrogate: 2-Fluorobiphenyl 85.6 Limits: 44-115%03/26/23 19:561 JMV V31392
Surrogate: 2-Fluorophenol 71.8 Limits: 35-115%03/26/23 19:561 JMV V31392
Surrogate: Nitrobenzene-d5 75.4 Limits: 37-122%03/26/23 19:561 JMV V31392
Surrogate: 4-Terphenyl-d14 89.8 Limits: 54-127%03/26/23 19:561 JMV V31392
Surrogate: 2,4,6-Tribromophenol 57.1 Limits: 39-132%03/26/23 19:561 JMV V31392
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.1 %Moisture 1 03/27/23 15:04 SW-DRYWTPEB
<0.193 mg/Kg - dry 0.193 0.274Chromium, Hexavalent 1 03/27/23 16:35 SW-7199SRJ
0.521 mg/Kg - dry 0.117 0.343Arsenic 5 03/27/23 23:22 6020BCPW
113 mg/Kg - dry 0.058 0.342Barium 5 03/27/23 23:22 6020BCPW
<0.0355 mg/Kg - dry 0.0355 0.343Cadmium 5 03/27/23 23:22 6020BCPW
36.6 mg/Kg - dry 0.159 0.342
Chromium 5 03/27/23 23:22 6020BCPW
13.4 mg/Kg - dry 0.0425 0.343Lead 5 03/27/23 23:22 6020BCPW
<0.0295 mg/Kg - dry 0.0295 0.244Mercury (Total)1 03/27/23 12:32 7471AFDS
0.545 mg/Kg - dry 0.141 0.342Selenium 5 03/27/23 23:22 6020BCPW
0.0128 J mg/Kg - dry 0.0092 0.343Silver 5 03/27/23 23:22 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31292 03/27/23 08:00
<0.823 mg/Kg - dry 0.823 6.86Acetone 500 03/27/23 20:32 V31293TBL
<0.415 mg/Kg - dry 0.415 6.86
Acrolein 500 03/27/23 20:32 V31293TBL
<0.257 mg/Kg - dry 0.257 6.86Acrylonitrile 500 03/27/23 20:32 V31293TBL
<0.198 mg/Kg - dry 0.198 1.71Benzene 500 03/27/23 20:32 V31293TBL
<0.171 mg/Kg - dry 0.171 1.71Bromobenzene 500 03/27/23 20:32 V31293TBL
<0.274 mg/Kg - dry 0.274 1.71Bromochloromethane 500 03/27/23 20:32 V31293TBL
<0.408 mg/Kg - dry 0.408 1.71Bromodichloromethane 500 03/27/23 20:32 V31293TBL
<0.347 mg/Kg - dry 0.347 1.71Bromoform 500 03/27/23 20:32 V31293TBL
<0.624 mg/Kg - dry 0.624 3.43
Bromomethane 500 03/27/23 20:32 V31293TBL
10.5 mg/Kg - dry 0.168 1.71n-Butylbenzene 500 03/27/23 20:32 V31293TBL
3.33 mg/Kg - dry 0.192 1.71sec-Butyl benzene 500 03/27/23 20:32 V31293TBL
<0.171 mg/Kg - dry 0.171 1.71tert-Butyl benzene 500 03/27/23 20:32 V31293TBL
<0.219 mg/Kg - dry 0.219 1.71Carbon Disulfide 500 03/27/23 20:32 V31293TBL
<0.541 mg/Kg - dry 0.541 1.71Carbon Tetrachloride 500 03/27/23 20:32 V31293TBL
<0.230 mg/Kg - dry 0.230 1.71Chlorobenzene 500 03/27/23 20:32 V31293TBL
<0.305 mg/Kg - dry 0.305 1.71Chlorodibromomethane 500 03/27/23 20:32 V31293TBL
<0.305 mg/Kg - dry 0.305 3.43Chloroethane 500 03/27/23 20:32 V31293TBL
<0.360 mg/Kg - dry 0.360 1.71Chloroform 500 03/27/23 20:32 V31293TBL
<0.216 mg/Kg - dry 0.216 3.43Chloromethane 500 03/27/23 20:32 V31293TBL
<0.175 mg/Kg - dry 0.175 1.712-Chlorotoluene 500 03/27/23 20:32 V31293TBL
<0.133 mg/Kg - dry 0.133 1.714-Chlorotoluene 500 03/27/23 20:32 V31293TBL
<0.251 mg/Kg - dry 0.251 1.71Di-Isopropyl Ether (DIPE)500 03/27/23 20:32 V31293TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31292 03/27/23 08:00
<0.150 mg/Kg - dry 0.150 3.431,2-Dibromo-3-Chloropropane 500 03/27/23 20:32 V31293TBL
<0.203 mg/Kg - dry 0.203 1.71
1,2-Dibromoethane 500 03/27/23 20:32 V31293TBL
<0.340 mg/Kg - dry 0.340 1.71Dibromomethane 500 03/27/23 20:32 V31293TBL
<0.106 mg/Kg - dry 0.106 1.711,2-Dichlorobenzene 500 03/27/23 20:32 V31293TBL
<0.130 mg/Kg - dry 0.130 1.711,3-Dichlorobenzene 500 03/27/23 20:32 V31293TBL
<0.205 mg/Kg - dry 0.205 1.711,4-Dichlorobenzene 500 03/27/23 20:32 V31293TBL
<0.452 mg/Kg - dry 0.452 3.43Dichlorodifluoromethane 500 03/27/23 20:32 V31293TBL
<0.281 mg/Kg - dry 0.281 1.711,1-Dichloroethane 500 03/27/23 20:32 V31293TBL
<0.473 mg/Kg - dry 0.473 1.71
1,2-Dichloroethane 500 03/27/23 20:32 V31293TBL
<0.251 mg/Kg - dry 0.251 1.711,1-Dichloroethene 500 03/27/23 20:32 V31293TBL
<0.271 mg/Kg - dry 0.271 1.71cis-1,2-Dichloroethene 500 03/27/23 20:32 V31293TBL
<0.360 mg/Kg - dry 0.360 1.71trans-1,2-Dichloroethene 500 03/27/23 20:32 V31293TBL
<0.150 mg/Kg - dry 0.150 1.711,2-Dichloropropane 500 03/27/23 20:32 V31293TBL
<0.189 mg/Kg - dry 0.189 1.711,3-Dichloropropane 500 03/27/23 20:32 V31293TBL
<0.436 mg/Kg - dry 0.436 1.712,2-Dichloropropane 500 03/27/23 20:32 V31293TBL
<0.260 mg/Kg - dry 0.260 1.711,1-Dichloropropene 500 03/27/23 20:32 V31293TBL
<0.185 mg/Kg - dry 0.185 1.71cis-1,3-Dichloropropene 500 03/27/23 20:32 V31293TBL
<0.274 mg/Kg - dry 0.274 1.71trans-1,3-Dichloropropene 500 03/27/23 20:32 V31293TBL
<4.98 mg/Kg - dry 4.98 85.7Ethanol 500 03/27/23 20:32 V31293TBL
12.8 mg/Kg - dry 0.198 1.71Ethylbenzene 500 03/27/23 20:32 V31293TBL
<0.285 mg/Kg - dry 0.285 34.3Ethyl Tertiary Butyl Ether (ETBE)500 03/27/23 20:32 V31293TBL
<0.271 mg/Kg - dry 0.271 3.43Hexachlorobutadiene 500 03/27/23 20:32 V31293TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31292 03/27/23 08:00
<0.226 mg/Kg - dry 0.226 3.43n-Hexane 500 03/27/23 20:32 V31293TBL
<0.212 mg/Kg - dry 0.212 6.86
2-Hexanone 500 03/27/23 20:32 V31293TBL
5.20 mg/Kg - dry 0.157 1.71Isopropylbenzene 500 03/27/23 20:32 V31293TBL
1.82 mg/Kg - dry 0.445 1.714-Isopropyl toluene 500 03/27/23 20:32 V31293TBL
<0.223 mg/Kg - dry 0.223 6.86Methyl Ethyl Ketone (MEK)500 03/27/23 20:32 V31293TBL
<0.212 mg/Kg - dry 0.212 1.71Methyl tert-butyl ether (MTBE)500 03/27/23 20:32 V31293TBL
<5.14 mg/Kg - dry 5.14 6.864-Methyl-2-Pentanone 500 03/27/23 20:32 V31293TBL
0.777 J mg/Kg - dry 0.504 1.71Methylene Chloride 500 03/27/23 20:32 V31293TBL
22.4 mg/Kg - dry 0.340 3.43
Naphthalene 500 03/27/23 20:32 V31293TBL
22.2 mg/Kg - dry 0.185 1.71n-Propylbenzene 500 03/27/23 20:32 V31293TBL
<0.486 mg/Kg - dry 0.486 1.71Styrene 500 03/27/23 20:32 V31293TBL
<0.360 mg/Kg - dry 0.360 1.711,1,1,2-Tetrachloroethane 500 03/27/23 20:32 V31293TBL
<0.109 mg/Kg - dry 0.109 1.711,1,2,2-Tetrachloroethane 500 03/27/23 20:32 V31293TBL
<0.308 mg/Kg - dry 0.308 1.71Tetrachloroethene 500 03/27/23 20:32 V31293TBL
9.79 mg/Kg - dry 0.226 1.71Toluene 500 03/27/23 20:32 V31293TBL
<0.185 mg/Kg - dry 0.185 3.431,2,3-Trichlorobenzene 500 03/27/23 20:32 V31293TBL
<0.219 mg/Kg - dry 0.219 3.431,2,4-Trichlorobenzene 500 03/27/23 20:32 V31293TBL
<0.493 mg/Kg - dry 0.493 1.711,1,1-Trichloroethane 500 03/27/23 20:32 V31293TBL
<0.161 mg/Kg - dry 0.161 1.711,1,2-Trichloroethane 500 03/27/23 20:32 V31293TBL
<0.315 mg/Kg - dry 0.315 1.71Trichloroethene 500 03/27/23 20:32 V31293TBL
<0.717 mg/Kg - dry 0.717 3.43Trichlorofluoromethane 500 03/27/23 20:32 V31293TBL
<0.246 mg/Kg - dry 0.246 1.711,2,3-Trichloropropane 500 03/27/23 20:32 V31293TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31292 03/27/23 08:00
195 mg/Kg - dry 1.69 17.11,2,4-Trimethylbenzene 5000 03/27/23 20:59 V31293TBL
59.3 mg/Kg - dry 0.185 1.71
1,3,5-Trimethylbenzene 500 03/27/23 20:32 V31293TBL
<0.157 mg/Kg - dry 0.157 3.43Vinyl Acetate 500 03/27/23 20:32 V31293TBL
<0.164 mg/Kg - dry 0.164 3.43Vinyl Chloride 500 03/27/23 20:32 V31293TBL
42.8 mg/Kg - dry 0.171 1.71o-Xylene 500 03/27/23 20:32 V31293TBL
99.3 mg/Kg - dry 0.432 3.43m,p-Xylene 500 03/27/23 20:32 V31293TBL
143 mg/Kg - dry 0.171 1.71Xylene (Total)500 03/27/23 20:32 V31293
Surrogate: 4-Bromofluorobenzene 99.7 Limits: 70-130%03/27/23 20:32500 TBL V31293
Surrogate: Dibromofluoromethane 101 Limits: 70-130%03/27/23 20:32500 TBL V31293
Surrogate: Toluene-d8 97.8 Limits: 76-129%03/27/23 20:32500 TBL V31293
Surrogate: 4-Bromofluorobenzene 97.5 Limits: 70-130%03/27/23 20:595000 TBL V31293
Surrogate: Dibromofluoromethane 100 Limits: 70-130%03/27/23 20:595000 TBL V31293
Surrogate: Toluene-d8 100 Limits: 76-129%03/27/23 20:595000 TBL V31293
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.159 mg/Kg - dry 0.159 0.905Acenaphthene 1 03/26/23 20:19 V31392JMV
<0.144 mg/Kg - dry 0.144 0.905Acenaphthylene 1 03/26/23 20:19 V31392JMV
<0.208 mg/Kg - dry 0.208 0.905Aniline 1 03/26/23 20:19 V31392JMV
<0.196 mg/Kg - dry 0.196 0.905Anthracene 1 03/26/23 20:19 V31392JMV
<0.190 mg/Kg - dry 0.190 0.905Benzo(a)anthracene 1 03/26/23 20:19 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.201 mg/Kg - dry 0.201 0.905Benzo(a)pyrene 1 03/26/23 20:19 V31392JMV
<0.200 mg/Kg - dry 0.200 0.905
Benzo(b)fluoranthene 1 03/26/23 20:19 V31392JMV
<0.186 mg/Kg - dry 0.186 0.905Benzo(g,h,i)perylene 1 03/26/23 20:19 V31392JMV
<0.187 mg/Kg - dry 0.187 0.905Benzo(k)fluoranthene 1 03/26/23 20:19 V31392JMV
<0.795 mg/Kg - dry 0.795 2.74Benzoic Acid 1 03/26/23 20:19 V31392JMV
<0.144 mg/Kg - dry 0.144 0.905Benzyl alcohol 1 03/26/23 20:19 V31392JMV
<0.161 mg/Kg - dry 0.161 0.905Bis(2-Chloroethoxy)methane 1 03/26/23 20:19 V31392JMV
<0.146 mg/Kg - dry 0.146 0.905Bis(2-Chloroethyl)ether 1 03/26/23 20:19 V31392JMV
<0.186 mg/Kg - dry 0.186 0.452
Bis(2-Chloroisopropyl)ether 1 03/26/23 20:19 V31392JMV
<0.164 mg/Kg - dry 0.164 0.905Bis(2-ethylhexyl)phthalate 1 03/26/23 20:19 V31392JMV
<0.149 mg/Kg - dry 0.149 0.9054-Bromophenyl phenyl ether 1 03/26/23 20:19 V31392JMV
<0.155 mg/Kg - dry 0.155 0.452Butyl benzyl phthalate 1 03/26/23 20:19 V31392JMV
<0.126 mg/Kg - dry 0.126 0.9054-Chloro-3-methylphenol 1 03/26/23 20:19 V31392JMV
<0.153 mg/Kg - dry 0.153 0.4524-Chloroaniline 1 03/26/23 20:19 V31392JMV
<0.159 mg/Kg - dry 0.159 0.9052-Chloronaphthalene 1 03/26/23 20:19 V31392JMV
<0.134 mg/Kg - dry 0.134 0.9052-Chlorophenol 1 03/26/23 20:19 V31392JMV
<0.172 mg/Kg - dry 0.172 1.374-Chlorophenyl phenyl ether 1 03/26/23 20:19 V31392JMV
<0.194 mg/Kg - dry 0.194 0.905Chrysene 1 03/26/23 20:19 V31392JMV
<0.315 mg/Kg - dry 0.315 0.905Dibenz(a,h)anthracene 1 03/26/23 20:19 V31392JMV
<0.163 mg/Kg - dry 0.163 0.905Dibenzofuran 1 03/26/23 20:19 V31392JMV
<0.129 mg/Kg - dry 0.129 0.9051,2-Dichlorobenzene 1 03/26/23 20:19 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9051,3-Dichlorobenzene 1 03/26/23 20:19 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.133 mg/Kg - dry 0.133 0.4521,4-Dichlorobenzene 1 03/26/23 20:19 V31392JMV
<0.201 mg/Kg - dry 0.201 0.905
3,3'-Dichlorobenzidine 1 03/26/23 20:19 V31392JMV
<0.131 mg/Kg - dry 0.131 0.9052,4-Dichlorophenol 1 03/26/23 20:19 V31392JMV
<0.246 mg/Kg - dry 0.246 0.905Diethyl phthalate 1 03/26/23 20:19 V31392JMV
<0.238 mg/Kg - dry 0.238 0.905Dimethyl phthalate 1 03/26/23 20:19 V31392JMV
<0.148 mg/Kg - dry 0.148 0.4522,4-Dimethylphenol 1 03/26/23 20:19 V31392JMV
<0.146 mg/Kg - dry 0.146 0.905Di-n-butyl phthalate 1 03/26/23 20:19 V31392JMV
<0.329 mg/Kg - dry 0.329 2.064,6-Dinitro-2-methylphenol 1 03/26/23 20:19 V31392JMV
<0.713 mg/Kg - dry 0.713 2.06
2,4-Dinitrophenol 1 03/26/23 20:19 V31392JMV
<0.132 mg/Kg - dry 0.132 0.9052,4-Dinitrotoluene 1 03/26/23 20:19 V31392JMV
<0.148 mg/Kg - dry 0.148 0.9052,6-Dinitrotoluene 1 03/26/23 20:19 V31392JMV
<0.196 mg/Kg - dry 0.196 0.452Di-n-Octyl Phthalate 1 03/26/23 20:19 V31392JMV
<0.168 mg/Kg - dry 0.168 0.905Fluoranthene 1 03/26/23 20:19 V31392JMV
<0.175 mg/Kg - dry 0.175 0.905Fluorene 1 03/26/23 20:19 V31392JMV
<0.145 mg/Kg - dry 0.145 0.905Hexachlorobenzene 1 03/26/23 20:19 V31392JMV
<0.133 mg/Kg - dry 0.133 0.905Hexachlorobutadiene 1 03/26/23 20:19 V31392JMV
<0.215 mg/Kg - dry 0.215 0.905Hexachlorocyclopentadiene 1 03/26/23 20:19 V31392JMV
<0.108 mg/Kg - dry 0.108 0.905Hexachloroethane 1 03/26/23 20:19 V31392JMV
<0.245 mg/Kg - dry 0.245 0.905Indeno(1,2,3-cd)pyrene 1 03/26/23 20:19 V31392JMV
<0.262 mg/Kg - dry 0.262 0.905Isophorone 1 03/26/23 20:19 V31392JMV
3.26 mg/Kg - dry 0.145 0.9051-Methylnaphthalene 1 03/26/23 20:19 V31392JMV
7.27 mg/Kg - dry 0.137 0.9052-Methylnaphthalene 1 03/26/23 20:19 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.133 mg/Kg - dry 0.133 0.9052-Methylphenol 1 03/26/23 20:19 V31392JMV
<0.116 mg/Kg - dry 0.116 0.905
3&4 Methylphenol 1 03/26/23 20:19 V31392JMV
15.9 mg/Kg - dry 0.790 3.62Naphthalene 4 03/31/23 10:41 V31392JMV
<0.132 mg/Kg - dry 0.132 0.9052-Nitroaniline 1 03/26/23 20:19 V31392JMV
<0.164 mg/Kg - dry 0.164 0.9053-Nitroaniline 1 03/26/23 20:19 V31392JMV
<0.127 mg/Kg - dry 0.127 0.4524-Nitroaniline 1 03/26/23 20:19 V31392JMV
<0.159 mg/Kg - dry 0.159 0.452Nitrobenzene 1 03/26/23 20:19 V31392JMV
<0.121 mg/Kg - dry 0.121 0.9052-Nitrophenol 1 03/26/23 20:19 V31392JMV
<0.160 mg/Kg - dry 0.160 0.905
4-Nitrophenol 1 03/26/23 20:19 V31392JMV
<0.360 mg/Kg - dry 0.360 0.905N-Nitrosodimethylamine 1 03/26/23 20:19 V31392JMV
<0.248 mg/Kg - dry 0.248 0.905N-Nitrosodiphenylamine 1 03/26/23 20:19 V31392JMV
<0.161 mg/Kg - dry 0.161 0.905N-Nitroso-di-n-propylamine 1 03/26/23 20:19 V31392JMV
<0.475 mg/Kg - dry 0.475 1.37Pentachlorophenol 1 03/26/23 20:19 V31392JMV
<0.285 mg/Kg - dry 0.285 0.905Phenanthrene 1 03/26/23 20:19 V31392JMV
<0.153 mg/Kg - dry 0.153 0.905Phenol 1 03/26/23 20:19 V31392JMV
<0.183 mg/Kg - dry 0.183 0.905Pyrene 1 03/26/23 20:19 V31392JMV
<0.108 mg/Kg - dry 0.108 0.452Pyridine 1 03/26/23 20:19 V31392JMV
<0.146 mg/Kg - dry 0.146 0.9051,2,4-Trichlorobenzene 1 03/26/23 20:19 V31392JMV
<0.131 mg/Kg - dry 0.131 0.9052,4,5-Trichlorophenol 1 03/26/23 20:19 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-2 (5-6)
91772 Matrix:
3/21/2023 10:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.132 mg/Kg - dry 0.132 0.9052,4,6-Trichlorophenol 1 03/26/23 20:19 V31392JMV
8270ESurrogate: Phenol-d5 66.7 Limits: 34-121%03/26/23 20:191 JMV
Surrogate: 2-Fluorobiphenyl 80.1 Limits: 44-115%03/26/23 20:191 JMV V31392
Surrogate: 2-Fluorophenol 66.1 Limits: 35-115%03/26/23 20:191 JMV V31392
Surrogate: Nitrobenzene-d5 45.8 Limits: 37-122%03/26/23 20:191 JMV V31392
Surrogate: 4-Terphenyl-d14 86.7 Limits: 54-127%03/26/23 20:191 JMV V31392
Surrogate: 2,4,6-Tribromophenol 53.8 Limits: 39-132%03/26/23 20:191 JMV V31392
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
25.3 %Moisture 1 03/27/23 15:04 SW-DRYWTPEB
0.230 J mg/Kg - dry 0.194 0.275Chromium, Hexavalent 1 03/27/23 16:46 SW-7199SRJ
0.514 mg/Kg - dry 0.114 0.335Arsenic 5 03/27/23 23:26 6020BCPW
117 mg/Kg - dry 0.057 0.334Barium 5 03/27/23 23:26 6020BCPW
<0.0346 mg/Kg - dry 0.0346 0.335Cadmium 5 03/27/23 23:26 6020BCPW
83.7 mg/Kg - dry 0.621 1.34
Chromium 20 03/28/23 20:59 6020BCPW
2.68 mg/Kg - dry 0.0414 0.335Lead 5 03/27/23 23:26 6020BCPW
<0.0286 mg/Kg - dry 0.0286 0.237Mercury (Total)1 03/27/23 12:34 7471AFDS
0.451 mg/Kg - dry 0.137 0.334Selenium 5 03/27/23 23:26 6020BCPW
0.0178 J mg/Kg - dry 0.0090 0.335Silver 5 03/27/23 23:26 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.047 mg/Kg - dry 0.003 0.026Acetone 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.026Acrylonitrile 1 03/25/23 19:16 V31266TBL
0.002 J mg/Kg - dry 0.0008 0.006Benzene 1 03/25/23 19:16 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/23 19:16 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 03/25/23 19:16 V31266TBL
0.001 J mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 03/25/23 19:16 V31266TBL
0.001 J mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/25/23 19:16 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/25/23 19:16 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 03/25/23 19:16 V31266TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 03/25/23 19:16 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/23 19:16 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 03/25/23 19:16 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 03/25/23 19:16 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/23 19:16 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 03/25/23 19:16 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 03/25/23 19:16 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 03/25/23 19:16 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/25/23 19:16 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/23 19:16 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/23 19:16 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/25/23 19:16 V31266TBL
0.002 J
mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/25/23 19:16 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/23 19:16 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 03/25/23 19:16 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 03/25/23 19:16 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 03/25/23 19:16 V31266TBL
<0.018 mg/Kg - dry 0.018 0.334Ethanol 1 03/25/23 19:16 V31266TBL
0.003 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.066Ethyl Tertiary Butyl Ether (ETBE)1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 03/25/23 19:16 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 03/25/23 19:16 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 03/25/23 19:16 V31266TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/23 19:16 V31266TBL
0.048 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 03/25/23 19:16 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/25/23 19:16 V31266TBL
<0.020 mg/Kg - dry 0.020 0.0264-Methyl-2-Pentanone 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 03/25/23 19:16 V31266TBL
0.007 J
mg/Kg - dry 0.001 0.013
Naphthalene 1 03/25/23 19:16 V31266TBL
0.003 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/23 19:16 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/23 19:16 V31266TBL
0.008 mg/Kg - dry 0.0009 0.006Toluene 1 03/25/23 19:16 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 03/25/23 19:16 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/23 19:16 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/23 19:16 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/23 19:16 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 03/25/23 19:16 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 03/25/23 19:16 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.080 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 03/25/23 19:16 V31266TBL
0.026 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 03/25/23 19:16 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 03/25/23 19:16 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 03/25/23 19:16 V31266TBL
0.008 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/25/23 19:16 V31266TBL
0.046 mg/Kg - dry 0.001 0.013m,p-Xylene 1 03/25/23 19:16 V31266TBL
0.054 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/25/23 19:16 V31266
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%03/25/23 19:161 TBL V31266
Surrogate: Dibromofluoromethane 103 Limits: 84-123%03/25/23 19:161 TBL V31266
Surrogate: Toluene-d8 97.4 Limits: 76-129%03/25/23 19:161 TBL V31266
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.155 mg/Kg - dry 0.155 0.884Acenaphthene 1 03/26/23 20:42 V31392JMV
<0.140 mg/Kg - dry 0.140 0.884Acenaphthylene 1 03/26/23 20:42 V31392JMV
<0.203 mg/Kg - dry 0.203 0.884Aniline 1 03/26/23 20:42 V31392JMV
<0.191 mg/Kg - dry 0.191 0.884Anthracene 1 03/26/23 20:42 V31392JMV
<0.186 mg/Kg - dry 0.186 0.884
Benzo(a)anthracene 1 03/26/23 20:42 V31392JMV
<0.196 mg/Kg - dry 0.196 0.884Benzo(a)pyrene 1 03/26/23 20:42 V31392JMV
<0.195 mg/Kg - dry 0.195 0.884Benzo(b)fluoranthene 1 03/26/23 20:42 V31392JMV
<0.182 mg/Kg - dry 0.182 0.884Benzo(g,h,i)perylene 1 03/26/23 20:42 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.183 mg/Kg - dry 0.183 0.884Benzo(k)fluoranthene 1 03/26/23 20:42 V31392JMV
<0.776 mg/Kg - dry 0.776 2.68
Benzoic Acid 1 03/26/23 20:42 V31392JMV
<0.140 mg/Kg - dry 0.140 0.884Benzyl alcohol 1 03/26/23 20:42 V31392JMV
<0.157 mg/Kg - dry 0.157 0.884Bis(2-Chloroethoxy)methane 1 03/26/23 20:42 V31392JMV
<0.143 mg/Kg - dry 0.143 0.884Bis(2-Chloroethyl)ether 1 03/26/23 20:42 V31392JMV
<0.182 mg/Kg - dry 0.182 0.443Bis(2-Chloroisopropyl)ether 1 03/26/23 20:42 V31392JMV
<0.160 mg/Kg - dry 0.160 0.884Bis(2-ethylhexyl)phthalate 1 03/26/23 20:42 V31392JMV
<0.145 mg/Kg - dry 0.145 0.8844-Bromophenyl phenyl ether 1 03/26/23 20:42 V31392JMV
<0.151 mg/Kg - dry 0.151 0.443
Butyl benzyl phthalate 1 03/26/23 20:42 V31392JMV
<0.123 mg/Kg - dry 0.123 0.8844-Chloro-3-methylphenol 1 03/26/23 20:42 V31392JMV
<0.149 mg/Kg - dry 0.149 0.4434-Chloroaniline 1 03/26/23 20:42 V31392JMV
<0.155 mg/Kg - dry 0.155 0.8842-Chloronaphthalene 1 03/26/23 20:42 V31392JMV
<0.131 mg/Kg - dry 0.131 0.8842-Chlorophenol 1 03/26/23 20:42 V31392JMV
<0.168 mg/Kg - dry 0.168 1.344-Chlorophenyl phenyl ether 1 03/26/23 20:42 V31392JMV
<0.190 mg/Kg - dry 0.190 0.884Chrysene 1 03/26/23 20:42 V31392JMV
<0.307 mg/Kg - dry 0.307 0.884Dibenz(a,h)anthracene 1 03/26/23 20:42 V31392JMV
<0.159 mg/Kg - dry 0.159 0.884Dibenzofuran 1 03/26/23 20:42 V31392JMV
<0.126 mg/Kg - dry 0.126 0.8841,2-Dichlorobenzene 1 03/26/23 20:42 V31392JMV
<0.130 mg/Kg - dry 0.130 0.8841,3-Dichlorobenzene 1 03/26/23 20:42 V31392JMV
<0.130 mg/Kg - dry 0.130 0.4431,4-Dichlorobenzene 1 03/26/23 20:42 V31392JMV
<0.196 mg/Kg - dry 0.196 0.8843,3'-Dichlorobenzidine 1 03/26/23 20:42 V31392JMV
<0.128 mg/Kg - dry 0.128 0.8842,4-Dichlorophenol 1 03/26/23 20:42 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.240 mg/Kg - dry 0.240 0.884Diethyl phthalate 1 03/26/23 20:42 V31392JMV
<0.232 mg/Kg - dry 0.232 0.884
Dimethyl phthalate 1 03/26/23 20:42 V31392JMV
<0.144 mg/Kg - dry 0.144 0.4432,4-Dimethylphenol 1 03/26/23 20:42 V31392JMV
<0.143 mg/Kg - dry 0.143 0.884Di-n-butyl phthalate 1 03/26/23 20:42 V31392JMV
<0.321 mg/Kg - dry 0.321 2.014,6-Dinitro-2-methylphenol 1 03/26/23 20:42 V31392JMV
<0.696 mg/Kg - dry 0.696 2.012,4-Dinitrophenol 1 03/26/23 20:42 V31392JMV
<0.129 mg/Kg - dry 0.129 0.8842,4-Dinitrotoluene 1 03/26/23 20:42 V31392JMV
<0.144 mg/Kg - dry 0.144 0.8842,6-Dinitrotoluene 1 03/26/23 20:42 V31392JMV
<0.191 mg/Kg - dry 0.191 0.443
Di-n-Octyl Phthalate 1 03/26/23 20:42 V31392JMV
<0.164 mg/Kg - dry 0.164 0.884Fluoranthene 1 03/26/23 20:42 V31392JMV
<0.171 mg/Kg - dry 0.171 0.884Fluorene 1 03/26/23 20:42 V31392JMV
<0.141 mg/Kg - dry 0.141 0.884Hexachlorobenzene 1 03/26/23 20:42 V31392JMV
<0.130 mg/Kg - dry 0.130 0.884Hexachlorobutadiene 1 03/26/23 20:42 V31392JMV
<0.210 mg/Kg - dry 0.210 0.884Hexachlorocyclopentadiene 1 03/26/23 20:42 V31392JMV
<0.106 mg/Kg - dry 0.106 0.884Hexachloroethane 1 03/26/23 20:42 V31392JMV
<0.239 mg/Kg - dry 0.239 0.884Indeno(1,2,3-cd)pyrene 1 03/26/23 20:42 V31392JMV
<0.255 mg/Kg - dry 0.255 0.884Isophorone 1 03/26/23 20:42 V31392JMV
<0.141 mg/Kg - dry 0.141 0.8841-Methylnaphthalene 1 03/26/23 20:42 V31392JMV
<0.133 mg/Kg - dry 0.133 0.8842-Methylnaphthalene 1 03/26/23 20:42 V31392JMV
<0.129 mg/Kg - dry 0.129 0.8842-Methylphenol 1 03/26/23 20:42 V31392JMV
<0.113 mg/Kg - dry 0.113 0.8843&4 Methylphenol 1 03/26/23 20:42 V31392JMV
<0.192 mg/Kg - dry 0.192 0.884Naphthalene 1 03/26/23 20:42 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-3 (5-6)
91773 Matrix:
3/21/2023 10:30
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.129 mg/Kg - dry 0.129 0.8842-Nitroaniline 1 03/26/23 20:42 V31392JMV
<0.160 mg/Kg - dry 0.160 0.884
3-Nitroaniline 1 03/26/23 20:42 V31392JMV
<0.125 mg/Kg - dry 0.125 0.4434-Nitroaniline 1 03/26/23 20:42 V31392JMV
<0.155 mg/Kg - dry 0.155 0.443Nitrobenzene 1 03/26/23 20:42 V31392JMV
<0.119 mg/Kg - dry 0.119 0.8842-Nitrophenol 1 03/26/23 20:42 V31392JMV
<0.156 mg/Kg - dry 0.156 0.8844-Nitrophenol 1 03/26/23 20:42 V31392JMV
<0.352 mg/Kg - dry 0.352 0.884N-Nitrosodimethylamine 1 03/26/23 20:42 V31392JMV
<0.242 mg/Kg - dry 0.242 0.884N-Nitrosodiphenylamine 1 03/26/23 20:42 V31392JMV
<0.157 mg/Kg - dry 0.157 0.884
N-Nitroso-di-n-propylamine 1 03/26/23 20:42 V31392JMV
<0.464 mg/Kg - dry 0.464 1.34Pentachlorophenol 1 03/26/23 20:42 V31392JMV
<0.278 mg/Kg - dry 0.278 0.884Phenanthrene 1 03/26/23 20:42 V31392JMV
<0.149 mg/Kg - dry 0.149 0.884Phenol 1 03/26/23 20:42 V31392JMV
<0.179 mg/Kg - dry 0.179 0.884Pyrene 1 03/26/23 20:42 V31392JMV
<0.106 mg/Kg - dry 0.106 0.443Pyridine 1 03/26/23 20:42 V31392JMV
<0.143 mg/Kg - dry 0.143 0.8841,2,4-Trichlorobenzene 1 03/26/23 20:42 V31392JMV
<0.128 mg/Kg - dry 0.128 0.8842,4,5-Trichlorophenol 1 03/26/23 20:42 V31392JMV
<0.129 mg/Kg - dry 0.129 0.8842,4,6-Trichlorophenol 1 03/26/23 20:42 V31392JMV
8270ESurrogate: Phenol-d5 68.6 Limits: 34-121%03/26/23 20:421 JMV
Surrogate: 2-Fluorobiphenyl 90.4 Limits: 44-115%03/26/23 20:421 JMV V31392
Surrogate: 2-Fluorophenol 75.4 Limits: 35-115%03/26/23 20:421 JMV V31392
Surrogate: Nitrobenzene-d5 79.0 Limits: 37-122%03/26/23 20:421 JMV V31392
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%03/26/23 20:421 JMV V31392
Surrogate: 2,4,6-Tribromophenol 61.7 Limits: 39-132%03/26/23 20:421 JMV V31392
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.3 %Moisture 1 03/27/23 15:04 SW-DRYWTPEB
1.31 mg/Kg - dry 0.193 0.275Chromium, Hexavalent 1 03/27/23 17:19 SW-7199SRJ
0.378 mg/Kg - dry 0.118 0.344Arsenic 5 03/27/23 23:37 6020BCPW
95.3 mg/Kg - dry 0.058 0.343Barium 5 03/27/23 23:37 6020BCPW
<0.0356 mg/Kg - dry 0.0356 0.344Cadmium 5 03/27/23 23:37 6020BCPW
139 mg/Kg - dry 0.638 1.38
Chromium 20 03/28/23 21:10 6020BCPW
1.80 mg/Kg - dry 0.0426 0.344Lead 5 03/27/23 23:37 6020BCPW
<0.0289 mg/Kg - dry 0.0289 0.239Mercury (Total)1 03/27/23 12:35 7471AFDS
0.442 mg/Kg - dry 0.141 0.343Selenium 5 03/27/23 23:37 6020BCPW
0.0138 J mg/Kg - dry 0.0092 0.344Silver 5 03/27/23 23:37 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.015 J mg/Kg - dry 0.003 0.027Acetone 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.027
Acrolein 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 03/25/23 19:43 V31266TBL
0.001 J mg/Kg - dry 0.0008 0.006Benzene 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/23 19:43 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 03/25/23 19:43 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/25/23 19:43 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 03/25/23 19:43 V31266TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 03/25/23 19:43 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/23 19:43 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 03/25/23 19:43 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 03/25/23 19:43 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 03/25/23 19:43 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 03/25/23 19:43 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 03/25/23 19:43 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/23 19:43 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/23 19:43 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/23 19:43 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 03/25/23 19:43 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 03/25/23 19:43 V31266TBL
<0.019 mg/Kg - dry 0.019 0.343Ethanol 1 03/25/23 19:43 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.068Ethyl Tertiary Butyl Ether (ETBE)1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 03/25/23 19:43 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 03/25/23 19:43 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.027
2-Hexanone 1 03/25/23 19:43 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/23 19:43 V31266TBL
0.006 J mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 03/25/23 19:43 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/25/23 19:43 V31266TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 03/25/23 19:43 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 03/25/23 19:43 V31266TBL
0.002 J
mg/Kg - dry 0.001 0.013
Naphthalene 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/23 19:43 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/23 19:43 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 03/25/23 19:43 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/23 19:43 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/23 19:43 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/23 19:43 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 03/25/23 19:43 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 03/25/23 19:43 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.018 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 03/25/23 19:43 V31266TBL
0.004 J
mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 03/25/23 19:43 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 03/25/23 19:43 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/25/23 19:43 V31266TBL
0.020 mg/Kg - dry 0.001 0.013m,p-Xylene 1 03/25/23 19:43 V31266TBL
0.020 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/25/23 19:43 V31266
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%03/25/23 19:431 TBL V31266
Surrogate: Dibromofluoromethane 103 Limits: 84-123%03/25/23 19:431 TBL V31266
Surrogate: Toluene-d8 99.1 Limits: 76-129%03/25/23 19:431 TBL V31266
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.159 mg/Kg - dry 0.159 0.909Acenaphthene 1 03/26/23 21:05 V31392JMV
<0.144 mg/Kg - dry 0.144 0.909Acenaphthylene 1 03/26/23 21:05 V31392JMV
<0.209 mg/Kg - dry 0.209 0.909Aniline 1 03/26/23 21:05 V31392JMV
<0.196 mg/Kg - dry 0.196 0.909Anthracene 1 03/26/23 21:05 V31392JMV
<0.191 mg/Kg - dry 0.191 0.909
Benzo(a)anthracene 1 03/26/23 21:05 V31392JMV
<0.202 mg/Kg - dry 0.202 0.909Benzo(a)pyrene 1 03/26/23 21:05 V31392JMV
<0.200 mg/Kg - dry 0.200 0.909Benzo(b)fluoranthene 1 03/26/23 21:05 V31392JMV
<0.187 mg/Kg - dry 0.187 0.909Benzo(g,h,i)perylene 1 03/26/23 21:05 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.188 mg/Kg - dry 0.188 0.909Benzo(k)fluoranthene 1 03/26/23 21:05 V31392JMV
<0.797 mg/Kg - dry 0.797 2.75
Benzoic Acid 1 03/26/23 21:05 V31392JMV
<0.144 mg/Kg - dry 0.144 0.909Benzyl alcohol 1 03/26/23 21:05 V31392JMV
<0.162 mg/Kg - dry 0.162 0.909Bis(2-Chloroethoxy)methane 1 03/26/23 21:05 V31392JMV
<0.147 mg/Kg - dry 0.147 0.909Bis(2-Chloroethyl)ether 1 03/26/23 21:05 V31392JMV
<0.187 mg/Kg - dry 0.187 0.453Bis(2-Chloroisopropyl)ether 1 03/26/23 21:05 V31392JMV
<0.165 mg/Kg - dry 0.165 0.909Bis(2-ethylhexyl)phthalate 1 03/26/23 21:05 V31392JMV
<0.149 mg/Kg - dry 0.149 0.9094-Bromophenyl phenyl ether 1 03/26/23 21:05 V31392JMV
<0.155 mg/Kg - dry 0.155 0.453
Butyl benzyl phthalate 1 03/26/23 21:05 V31392JMV
<0.127 mg/Kg - dry 0.127 0.9094-Chloro-3-methylphenol 1 03/26/23 21:05 V31392JMV
<0.154 mg/Kg - dry 0.154 0.4534-Chloroaniline 1 03/26/23 21:05 V31392JMV
<0.159 mg/Kg - dry 0.159 0.9092-Chloronaphthalene 1 03/26/23 21:05 V31392JMV
<0.135 mg/Kg - dry 0.135 0.9092-Chlorophenol 1 03/26/23 21:05 V31392JMV
<0.173 mg/Kg - dry 0.173 1.384-Chlorophenyl phenyl ether 1 03/26/23 21:05 V31392JMV
<0.195 mg/Kg - dry 0.195 0.909Chrysene 1 03/26/23 21:05 V31392JMV
<0.316 mg/Kg - dry 0.316 0.909Dibenz(a,h)anthracene 1 03/26/23 21:05 V31392JMV
<0.163 mg/Kg - dry 0.163 0.909Dibenzofuran 1 03/26/23 21:05 V31392JMV
<0.129 mg/Kg - dry 0.129 0.9091,2-Dichlorobenzene 1 03/26/23 21:05 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9091,3-Dichlorobenzene 1 03/26/23 21:05 V31392JMV
<0.134 mg/Kg - dry 0.134 0.4531,4-Dichlorobenzene 1 03/26/23 21:05 V31392JMV
<0.202 mg/Kg - dry 0.202 0.9093,3'-Dichlorobenzidine 1 03/26/23 21:05 V31392JMV
<0.131 mg/Kg - dry 0.131 0.9092,4-Dichlorophenol 1 03/26/23 21:05 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.247 mg/Kg - dry 0.247 0.909Diethyl phthalate 1 03/26/23 21:05 V31392JMV
<0.239 mg/Kg - dry 0.239 0.909
Dimethyl phthalate 1 03/26/23 21:05 V31392JMV
<0.148 mg/Kg - dry 0.148 0.4532,4-Dimethylphenol 1 03/26/23 21:05 V31392JMV
<0.147 mg/Kg - dry 0.147 0.909Di-n-butyl phthalate 1 03/26/23 21:05 V31392JMV
<0.330 mg/Kg - dry 0.330 2.064,6-Dinitro-2-methylphenol 1 03/26/23 21:05 V31392JMV
<0.715 mg/Kg - dry 0.715 2.062,4-Dinitrophenol 1 03/26/23 21:05 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9092,4-Dinitrotoluene 1 03/26/23 21:05 V31392JMV
<0.148 mg/Kg - dry 0.148 0.9092,6-Dinitrotoluene 1 03/26/23 21:05 V31392JMV
<0.196 mg/Kg - dry 0.196 0.453
Di-n-Octyl Phthalate 1 03/26/23 21:05 V31392JMV
<0.169 mg/Kg - dry 0.169 0.909Fluoranthene 1 03/26/23 21:05 V31392JMV
<0.176 mg/Kg - dry 0.176 0.909Fluorene 1 03/26/23 21:05 V31392JMV
<0.145 mg/Kg - dry 0.145 0.909Hexachlorobenzene 1 03/26/23 21:05 V31392JMV
<0.134 mg/Kg - dry 0.134 0.909Hexachlorobutadiene 1 03/26/23 21:05 V31392JMV
<0.215 mg/Kg - dry 0.215 0.909Hexachlorocyclopentadiene 1 03/26/23 21:05 V31392JMV
<0.109 mg/Kg - dry 0.109 0.909Hexachloroethane 1 03/26/23 21:05 V31392JMV
<0.246 mg/Kg - dry 0.246 0.909Indeno(1,2,3-cd)pyrene 1 03/26/23 21:05 V31392JMV
<0.262 mg/Kg - dry 0.262 0.909Isophorone 1 03/26/23 21:05 V31392JMV
<0.145 mg/Kg - dry 0.145 0.9091-Methylnaphthalene 1 03/26/23 21:05 V31392JMV
<0.137 mg/Kg - dry 0.137 0.9092-Methylnaphthalene 1 03/26/23 21:05 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9092-Methylphenol 1 03/26/23 21:05 V31392JMV
<0.116 mg/Kg - dry 0.116 0.9093&4 Methylphenol 1 03/26/23 21:05 V31392JMV
<0.198 mg/Kg - dry 0.198 0.909Naphthalene 1 03/26/23 21:05 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-4 (5-6)
91774 Matrix:
3/21/2023 11:10
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.133 mg/Kg - dry 0.133 0.9092-Nitroaniline 1 03/26/23 21:05 V31392JMV
<0.165 mg/Kg - dry 0.165 0.909
3-Nitroaniline 1 03/26/23 21:05 V31392JMV
<0.128 mg/Kg - dry 0.128 0.4534-Nitroaniline 1 03/26/23 21:05 V31392JMV
<0.159 mg/Kg - dry 0.159 0.453Nitrobenzene 1 03/26/23 21:05 V31392JMV
<0.122 mg/Kg - dry 0.122 0.9092-Nitrophenol 1 03/26/23 21:05 V31392JMV
<0.160 mg/Kg - dry 0.160 0.9094-Nitrophenol 1 03/26/23 21:05 V31392JMV
<0.361 mg/Kg - dry 0.361 0.909N-Nitrosodimethylamine 1 03/26/23 21:05 V31392JMV
<0.248 mg/Kg - dry 0.248 0.909N-Nitrosodiphenylamine 1 03/26/23 21:05 V31392JMV
<0.162 mg/Kg - dry 0.162 0.909
N-Nitroso-di-n-propylamine 1 03/26/23 21:05 V31392JMV
<0.477 mg/Kg - dry 0.477 1.38Pentachlorophenol 1 03/26/23 21:05 V31392JMV
<0.286 mg/Kg - dry 0.286 0.909Phenanthrene 1 03/26/23 21:05 V31392JMV
<0.154 mg/Kg - dry 0.154 0.909Phenol 1 03/26/23 21:05 V31392JMV
<0.184 mg/Kg - dry 0.184 0.909Pyrene 1 03/26/23 21:05 V31392JMV
<0.108 mg/Kg - dry 0.108 0.453Pyridine 1 03/26/23 21:05 V31392JMV
<0.147 mg/Kg - dry 0.147 0.9091,2,4-Trichlorobenzene 1 03/26/23 21:05 V31392JMV
<0.132 mg/Kg - dry 0.132 0.9092,4,5-Trichlorophenol 1 03/26/23 21:05 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9092,4,6-Trichlorophenol 1 03/26/23 21:05 V31392JMV
8270ESurrogate: Phenol-d5 68.3 Limits: 34-121%03/26/23 21:051 JMV
Surrogate: 2-Fluorobiphenyl 91.6 Limits: 44-115%03/26/23 21:051 JMV V31392
Surrogate: 2-Fluorophenol 75.4 Limits: 35-115%03/26/23 21:051 JMV V31392
Surrogate: Nitrobenzene-d5 80.2 Limits: 37-122%03/26/23 21:051 JMV V31392
Surrogate: 4-Terphenyl-d14 99.4 Limits: 54-127%03/26/23 21:051 JMV V31392
Surrogate: 2,4,6-Tribromophenol 62.0 Limits: 39-132%03/26/23 21:051 JMV V31392
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
17.9 %Moisture 1 03/27/23 15:51 SW-DRYWTPEB
<0.174 mg/Kg - dry 0.174 0.248Chromium, Hexavalent 1 03/27/23 17:30 SW-7199SRJ
0.374 mg/Kg - dry 0.104 0.305Arsenic 5 03/27/23 23:41 6020BCPW
130 mg/Kg - dry 0.052 0.304Barium 5 03/27/23 23:41 6020BCPW
<0.0315 mg/Kg - dry 0.0315 0.305Cadmium 5 03/27/23 23:41 6020BCPW
26.8 mg/Kg - dry 0.141 0.304
Chromium 5 03/27/23 23:41 6020BCPW
2.27 mg/Kg - dry 0.0377 0.305Lead 5 03/27/23 23:41 6020BCPW
<0.0241 mg/Kg - dry 0.0241 0.200Mercury (Total)1 03/27/23 12:37 7471AFDS
0.394 mg/Kg - dry 0.125 0.304Selenium 5 03/27/23 23:41 6020BCPW
0.0182 J mg/Kg - dry 0.0082 0.305Silver 5 03/27/23 23:41 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.014 J mg/Kg - dry 0.002 0.024Acetone 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.024
Acrolein 1 03/25/23 20:11 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.024Acrylonitrile 1 03/25/23 20:11 V31266TBL
0.004 J mg/Kg - dry 0.0007 0.006Benzene 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 03/25/23 20:11 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.006Bromochloromethane 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/23 20:11 V31266TBL
<0.002 mg/Kg - dry 0.002 0.012
Bromomethane 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/25/23 20:11 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 03/25/23 20:11 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 03/25/23 20:11 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/23 20:11 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 03/25/23 20:11 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/23 20:11 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 03/25/23 20:11 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0005 mg/Kg - dry 0.0005 0.0121,2-Dibromo-3-Chloropropane 1 03/25/23 20:11 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006
1,2-Dibromoethane 1 03/25/23 20:11 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/25/23 20:11 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/23 20:11 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/23 20:11 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,4-Dichlorobenzene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 03/25/23 20:11 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethane 1 03/25/23 20:11 V31266TBL
0.002 J
mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/25/23 20:11 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 03/25/23 20:11 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/23 20:11 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,2-Dichloropropane 1 03/25/23 20:11 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/23 20:11 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloropropene 1 03/25/23 20:11 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/25/23 20:11 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.006trans-1,3-Dichloropropene 1 03/25/23 20:11 V31266TBL
<0.017 mg/Kg - dry 0.017 0.304Ethanol 1 03/25/23 20:11 V31266TBL
0.005 J mg/Kg - dry 0.0007 0.006Ethylbenzene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.060Ethyl Tertiary Butyl Ether (ETBE)1 03/25/23 20:11 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 03/25/23 20:11 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 03/25/23 20:11 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.024
2-Hexanone 1 03/25/23 20:11 V31266TBL
0.0009 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/23 20:11 V31266TBL
0.012 J mg/Kg - dry 0.0008 0.024Methyl Ethyl Ketone (MEK)1 03/25/23 20:11 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/25/23 20:11 V31266TBL
<0.018 mg/Kg - dry 0.018 0.0244-Methyl-2-Pentanone 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 03/25/23 20:11 V31266TBL
0.005 J
mg/Kg - dry 0.001 0.012
Naphthalene 1 03/25/23 20:11 V31266TBL
0.001 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/23 20:11 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/23 20:11 V31266TBL
0.003 J mg/Kg - dry 0.0008 0.006Toluene 1 03/25/23 20:11 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 03/25/23 20:11 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/23 20:11 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/23 20:11 V31266TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 03/25/23 20:11 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/25/23 20:11 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.017 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/25/23 20:11 V31266TBL
0.005 J
mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 03/25/23 20:11 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 03/25/23 20:11 V31266TBL
0.049 mg/Kg - dry 0.001 0.012m,p-Xylene 1 03/25/23 20:11 V31266TBL
0.049 mg/Kg - dry 0.0006 0.006Xylene (Total)1 03/25/23 20:11 V31266
Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%03/25/23 20:111 TBL V31266
Surrogate: Dibromofluoromethane 103 Limits: 84-123%03/25/23 20:111 TBL V31266
Surrogate: Toluene-d8 97.3 Limits: 76-129%03/25/23 20:111 TBL V31266
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.141 mg/Kg - dry 0.141 0.803Acenaphthene 1 03/27/23 13:36 V31392JMV
<0.127 mg/Kg - dry 0.127 0.803Acenaphthylene 1 03/27/23 13:36 V31392JMV
<0.185 mg/Kg - dry 0.185 0.803Aniline 1 03/27/23 13:36 V31392JMV
<0.174 mg/Kg - dry 0.174 0.803Anthracene 1 03/27/23 13:36 V31392JMV
<0.169 mg/Kg - dry 0.169 0.803
Benzo(a)anthracene 1 03/27/23 13:36 V31392JMV
<0.179 mg/Kg - dry 0.179 0.803Benzo(a)pyrene 1 03/27/23 13:36 V31392JMV
<0.177 mg/Kg - dry 0.177 0.803Benzo(b)fluoranthene 1 03/27/23 13:36 V31392JMV
<0.165 mg/Kg - dry 0.165 0.803Benzo(g,h,i)perylene 1 03/27/23 13:36 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.166 mg/Kg - dry 0.166 0.803Benzo(k)fluoranthene 1 03/27/23 13:36 V31392JMV
<0.706 mg/Kg - dry 0.706 2.44
Benzoic Acid 1 03/27/23 13:36 V31392JMV
<0.127 mg/Kg - dry 0.127 0.803Benzyl alcohol 1 03/27/23 13:36 V31392JMV
<0.143 mg/Kg - dry 0.143 0.803Bis(2-Chloroethoxy)methane 1 03/27/23 13:36 V31392JMV
<0.130 mg/Kg - dry 0.130 0.803Bis(2-Chloroethyl)ether 1 03/27/23 13:36 V31392JMV
<0.165 mg/Kg - dry 0.165 0.401Bis(2-Chloroisopropyl)ether 1 03/27/23 13:36 V31392JMV
<0.146 mg/Kg - dry 0.146 0.803Bis(2-ethylhexyl)phthalate 1 03/27/23 13:36 V31392JMV
<0.132 mg/Kg - dry 0.132 0.8034-Bromophenyl phenyl ether 1 03/27/23 13:36 V31392JMV
<0.137 mg/Kg - dry 0.137 0.401
Butyl benzyl phthalate 1 03/27/23 13:36 V31392JMV
<0.112 mg/Kg - dry 0.112 0.8034-Chloro-3-methylphenol 1 03/27/23 13:36 V31392JMV
<0.136 mg/Kg - dry 0.136 0.4014-Chloroaniline 1 03/27/23 13:36 V31392JMV
<0.141 mg/Kg - dry 0.141 0.8032-Chloronaphthalene 1 03/27/23 13:36 V31392JMV
<0.119 mg/Kg - dry 0.119 0.8032-Chlorophenol 1 03/27/23 13:36 V31392JMV
<0.153 mg/Kg - dry 0.153 1.224-Chlorophenyl phenyl ether 1 03/27/23 13:36 V31392JMV
<0.172 mg/Kg - dry 0.172 0.803Chrysene 1 03/27/23 13:36 V31392JMV
<0.280 mg/Kg - dry 0.280 0.803Dibenz(a,h)anthracene 1 03/27/23 13:36 V31392JMV
<0.144 mg/Kg - dry 0.144 0.803Dibenzofuran 1 03/27/23 13:36 V31392JMV
<0.114 mg/Kg - dry 0.114 0.8031,2-Dichlorobenzene 1 03/27/23 13:36 V31392JMV
<0.118 mg/Kg - dry 0.118 0.8031,3-Dichlorobenzene 1 03/27/23 13:36 V31392JMV
<0.118 mg/Kg - dry 0.118 0.4011,4-Dichlorobenzene 1 03/27/23 13:36 V31392JMV
<0.179 mg/Kg - dry 0.179 0.8033,3'-Dichlorobenzidine 1 03/27/23 13:36 V31392JMV
<0.116 mg/Kg - dry 0.116 0.8032,4-Dichlorophenol 1 03/27/23 13:36 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.219 mg/Kg - dry 0.219 0.803Diethyl phthalate 1 03/27/23 13:36 V31392JMV
<0.211 mg/Kg - dry 0.211 0.803
Dimethyl phthalate 1 03/27/23 13:36 V31392JMV
<0.131 mg/Kg - dry 0.131 0.4012,4-Dimethylphenol 1 03/27/23 13:36 V31392JMV
<0.130 mg/Kg - dry 0.130 0.803Di-n-butyl phthalate 1 03/27/23 13:36 V31392JMV
<0.292 mg/Kg - dry 0.292 1.834,6-Dinitro-2-methylphenol 1 03/27/23 13:36 V31392JMV
<0.633 mg/Kg - dry 0.633 1.832,4-Dinitrophenol 1 03/27/23 13:36 V31392JMV
<0.117 mg/Kg - dry 0.117 0.8032,4-Dinitrotoluene 1 03/27/23 13:36 V31392JMV
<0.131 mg/Kg - dry 0.131 0.8032,6-Dinitrotoluene 1 03/27/23 13:36 V31392JMV
<0.174 mg/Kg - dry 0.174 0.401
Di-n-Octyl Phthalate 1 03/27/23 13:36 V31392JMV
<0.149 mg/Kg - dry 0.149 0.803Fluoranthene 1 03/27/23 13:36 V31392JMV
<0.155 mg/Kg - dry 0.155 0.803Fluorene 1 03/27/23 13:36 V31392JMV
<0.129 mg/Kg - dry 0.129 0.803Hexachlorobenzene 1 03/27/23 13:36 V31392JMV
<0.118 mg/Kg - dry 0.118 0.803Hexachlorobutadiene 1 03/27/23 13:36 V31392JMV
<0.191 mg/Kg - dry 0.191 0.803Hexachlorocyclopentadiene 1 03/27/23 13:36 V31392JMV
<0.096 mg/Kg - dry 0.096 0.803Hexachloroethane 1 03/27/23 13:36 V31392JMV
<0.218 mg/Kg - dry 0.218 0.803Indeno(1,2,3-cd)pyrene 1 03/27/23 13:36 V31392JMV
<0.232 mg/Kg - dry 0.232 0.803Isophorone 1 03/27/23 13:36 V31392JMV
<0.129 mg/Kg - dry 0.129 0.8031-Methylnaphthalene 1 03/27/23 13:36 V31392JMV
<0.121 mg/Kg - dry 0.121 0.8032-Methylnaphthalene 1 03/27/23 13:36 V31392JMV
<0.118 mg/Kg - dry 0.118 0.8032-Methylphenol 1 03/27/23 13:36 V31392JMV
<0.103 mg/Kg - dry 0.103 0.8033&4 Methylphenol 1 03/27/23 13:36 V31392JMV
<0.175 mg/Kg - dry 0.175 0.803Naphthalene 1 03/27/23 13:36 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-5 (5-6)
91775 Matrix:
3/21/2023 11:55
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.117 mg/Kg - dry 0.117 0.8032-Nitroaniline 1 03/27/23 13:36 V31392JMV
<0.146 mg/Kg - dry 0.146 0.803
3-Nitroaniline 1 03/27/23 13:36 V31392JMV
<0.113 mg/Kg - dry 0.113 0.4014-Nitroaniline 1 03/27/23 13:36 V31392JMV
<0.141 mg/Kg - dry 0.141 0.401Nitrobenzene 1 03/27/23 13:36 V31392JMV
<0.108 mg/Kg - dry 0.108 0.8032-Nitrophenol 1 03/27/23 13:36 V31392JMV
<0.142 mg/Kg - dry 0.142 0.8034-Nitrophenol 1 03/27/23 13:36 V31392JMV
<0.320 mg/Kg - dry 0.320 0.803N-Nitrosodimethylamine 1 03/27/23 13:36 V31392JMV
<0.220 mg/Kg - dry 0.220 0.803N-Nitrosodiphenylamine 1 03/27/23 13:36 V31392JMV
<0.143 mg/Kg - dry 0.143 0.803
N-Nitroso-di-n-propylamine 1 03/27/23 13:36 V31392JMV
<0.422 mg/Kg - dry 0.422 1.22Pentachlorophenol 1 03/27/23 13:36 V31392JMV
<0.253 mg/Kg - dry 0.253 0.803Phenanthrene 1 03/27/23 13:36 V31392JMV
<0.136 mg/Kg - dry 0.136 0.803Phenol 1 03/27/23 13:36 V31392JMV
<0.163 mg/Kg - dry 0.163 0.803Pyrene 1 03/27/23 13:36 V31392JMV
<0.096 mg/Kg - dry 0.096 0.401Pyridine 1 03/27/23 13:36 V31392JMV
<0.130 mg/Kg - dry 0.130 0.8031,2,4-Trichlorobenzene 1 03/27/23 13:36 V31392JMV
<0.117 mg/Kg - dry 0.117 0.8032,4,5-Trichlorophenol 1 03/27/23 13:36 V31392JMV
<0.117 mg/Kg - dry 0.117 0.8032,4,6-Trichlorophenol 1 03/27/23 13:36 V31392JMV
8270ESurrogate: Phenol-d5 75.4 Limits: 34-121%03/27/23 13:361 JMV
Surrogate: 2-Fluorobiphenyl 97.6 Limits: 44-115%03/27/23 13:361 JMV V31392
Surrogate: 2-Fluorophenol 82.6 Limits: 35-115%03/27/23 13:361 JMV V31392
Surrogate: Nitrobenzene-d5 83.8 Limits: 37-122%03/27/23 13:361 JMV V31392
Surrogate: 4-Terphenyl-d14 111 Limits: 54-127%03/27/23 13:361 JMV V31392
Surrogate: 2,4,6-Tribromophenol 73.1 Limits: 39-132%03/27/23 13:361 JMV V31392
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
27.7 %Moisture 1 03/27/23 15:51 SW-DRYWTPEB
0.695 mg/Kg - dry 0.195 0.276Chromium, Hexavalent 1 03/27/23 17:41 SW-7199SRJ
0.347 mg/Kg - dry 0.118 0.346Arsenic 5 03/27/23 23:44 6020BCPW
148 mg/Kg - dry 0.059 0.345Barium 5 03/27/23 23:44 6020BCPW
0.0387 J mg/Kg - dry 0.0358 0.346Cadmium 5 03/27/23 23:44 6020BCPW
123 mg/Kg - dry 0.641 1.38
Chromium 20 03/28/23 21:14 6020BCPW
1.08 mg/Kg - dry 0.0428 0.346Lead 5 03/27/23 23:44 6020BCPW
<0.0308 mg/Kg - dry 0.0308 0.256Mercury (Total)1 03/27/23 12:38 7471AFDS
0.437 mg/Kg - dry 0.142 0.345Selenium 5 03/27/23 23:44 6020BCPW
0.0246 J mg/Kg - dry 0.0093 0.346Silver 5 03/27/23 23:44 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.011 J mg/Kg - dry 0.003 0.027Acetone 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.027
Acrolein 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 03/26/23 02:58 V31266TBL
0.015 mg/Kg - dry 0.0008 0.006Benzene 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/26/23 02:58 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 03/26/23 02:58 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/26/23 02:58 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 03/26/23 02:58 V31266TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 03/26/23 02:58 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/26/23 02:58 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 03/26/23 02:58 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 03/26/23 02:58 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 54 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 03/26/23 02:58 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 03/26/23 02:58 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 03/26/23 02:58 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/26/23 02:58 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/26/23 02:58 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/26/23 02:58 V31266TBL
0.015 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/26/23 02:58 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 03/26/23 02:58 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 03/26/23 02:58 V31266TBL
<0.019 mg/Kg - dry 0.019 0.345Ethanol 1 03/26/23 02:58 V31266TBL
0.014 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 03/26/23 02:58 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 55 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 03/26/23 02:58 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.027
2-Hexanone 1 03/26/23 02:58 V31266TBL
0.002 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/26/23 02:58 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 03/26/23 02:58 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/26/23 02:58 V31266TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 03/26/23 02:58 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 03/26/23 02:58 V31266TBL
0.004 J
mg/Kg - dry 0.001 0.013
Naphthalene 1 03/26/23 02:58 V31266TBL
0.004 J mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/26/23 02:58 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/26/23 02:58 V31266TBL
0.124 mg/Kg - dry 0.0009 0.006Toluene 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 03/26/23 02:58 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/26/23 02:58 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/26/23 02:58 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 03/26/23 02:58 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 03/26/23 02:58 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 56 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.052 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 03/26/23 02:58 V31266TBL
0.014 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 03/26/23 02:58 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 03/26/23 02:58 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 03/26/23 02:58 V31266TBL
0.035 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/26/23 02:58 V31266TBL
0.211 mg/Kg - dry 0.001 0.013m,p-Xylene 1 03/26/23 02:58 V31266TBL
0.246 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/26/23 02:58 V31266
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%03/26/23 02:581 TBL V31266
Surrogate: Dibromofluoromethane 104 Limits: 84-123%03/26/23 02:581 TBL V31266
Surrogate: Toluene-d8 96.8 Limits: 76-129%03/26/23 02:581 TBL V31266
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.160 mg/Kg - dry 0.160 0.912Acenaphthene 1 03/27/23 10:07 V31392JMV
<0.145 mg/Kg - dry 0.145 0.912Acenaphthylene 1 03/27/23 10:07 V31392JMV
<0.210 mg/Kg - dry 0.210 0.912Aniline 1 03/27/23 10:07 V31392JMV
<0.197 mg/Kg - dry 0.197 0.912Anthracene 1 03/27/23 10:07 V31392JMV
<0.192 mg/Kg - dry 0.192 0.912
Benzo(a)anthracene 1 03/27/23 10:07 V31392JMV
<0.203 mg/Kg - dry 0.203 0.912Benzo(a)pyrene 1 03/27/23 10:07 V31392JMV
<0.201 mg/Kg - dry 0.201 0.912Benzo(b)fluoranthene 1 03/27/23 10:07 V31392JMV
<0.188 mg/Kg - dry 0.188 0.912Benzo(g,h,i)perylene 1 03/27/23 10:07 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 57 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.189 mg/Kg - dry 0.189 0.912Benzo(k)fluoranthene 1 03/27/23 10:07 V31392JMV
<0.802 mg/Kg - dry 0.802 2.77
Benzoic Acid 1 03/27/23 10:07 V31392JMV
<0.145 mg/Kg - dry 0.145 0.912Benzyl alcohol 1 03/27/23 10:07 V31392JMV
<0.163 mg/Kg - dry 0.163 0.912Bis(2-Chloroethoxy)methane 1 03/27/23 10:07 V31392JMV
<0.147 mg/Kg - dry 0.147 0.912Bis(2-Chloroethyl)ether 1 03/27/23 10:07 V31392JMV
<0.188 mg/Kg - dry 0.188 0.456Bis(2-Chloroisopropyl)ether 1 03/27/23 10:07 V31392JMV
<0.165 mg/Kg - dry 0.165 0.912Bis(2-ethylhexyl)phthalate 1 03/27/23 10:07 V31392JMV
<0.150 mg/Kg - dry 0.150 0.9124-Bromophenyl phenyl ether 1 03/27/23 10:07 V31392JMV
<0.156 mg/Kg - dry 0.156 0.456
Butyl benzyl phthalate 1 03/27/23 10:07 V31392JMV
<0.127 mg/Kg - dry 0.127 0.9124-Chloro-3-methylphenol 1 03/27/23 10:07 V31392JMV
<0.154 mg/Kg - dry 0.154 0.4564-Chloroaniline 1 03/27/23 10:07 V31392JMV
<0.160 mg/Kg - dry 0.160 0.9122-Chloronaphthalene 1 03/27/23 10:07 V31392JMV
<0.135 mg/Kg - dry 0.135 0.9122-Chlorophenol 1 03/27/23 10:07 V31392JMV
<0.174 mg/Kg - dry 0.174 1.384-Chlorophenyl phenyl ether 1 03/27/23 10:07 V31392JMV
<0.196 mg/Kg - dry 0.196 0.912Chrysene 1 03/27/23 10:07 V31392JMV
<0.318 mg/Kg - dry 0.318 0.912Dibenz(a,h)anthracene 1 03/27/23 10:07 V31392JMV
<0.164 mg/Kg - dry 0.164 0.912Dibenzofuran 1 03/27/23 10:07 V31392JMV
<0.130 mg/Kg - dry 0.130 0.9121,2-Dichlorobenzene 1 03/27/23 10:07 V31392JMV
<0.134 mg/Kg - dry 0.134 0.9121,3-Dichlorobenzene 1 03/27/23 10:07 V31392JMV
<0.134 mg/Kg - dry 0.134 0.4561,4-Dichlorobenzene 1 03/27/23 10:07 V31392JMV
<0.203 mg/Kg - dry 0.203 0.9123,3'-Dichlorobenzidine 1 03/27/23 10:07 V31392JMV
<0.132 mg/Kg - dry 0.132 0.9122,4-Dichlorophenol 1 03/27/23 10:07 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 58 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.248 mg/Kg - dry 0.248 0.912Diethyl phthalate 1 03/27/23 10:07 V31392JMV
<0.240 mg/Kg - dry 0.240 0.912
Dimethyl phthalate 1 03/27/23 10:07 V31392JMV
<0.149 mg/Kg - dry 0.149 0.4562,4-Dimethylphenol 1 03/27/23 10:07 V31392JMV
<0.147 mg/Kg - dry 0.147 0.912Di-n-butyl phthalate 1 03/27/23 10:07 V31392JMV
<0.331 mg/Kg - dry 0.331 2.074,6-Dinitro-2-methylphenol 1 03/27/23 10:07 V31392JMV
<0.719 mg/Kg - dry 0.719 2.072,4-Dinitrophenol 1 03/27/23 10:07 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9122,4-Dinitrotoluene 1 03/27/23 10:07 V31392JMV
<0.149 mg/Kg - dry 0.149 0.9122,6-Dinitrotoluene 1 03/27/23 10:07 V31392JMV
<0.197 mg/Kg - dry 0.197 0.456
Di-n-Octyl Phthalate 1 03/27/23 10:07 V31392JMV
<0.170 mg/Kg - dry 0.170 0.912Fluoranthene 1 03/27/23 10:07 V31392JMV
<0.177 mg/Kg - dry 0.177 0.912Fluorene 1 03/27/23 10:07 V31392JMV
<0.146 mg/Kg - dry 0.146 0.912Hexachlorobenzene 1 03/27/23 10:07 V31392JMV
<0.134 mg/Kg - dry 0.134 0.912Hexachlorobutadiene 1 03/27/23 10:07 V31392JMV
<0.217 mg/Kg - dry 0.217 0.912Hexachlorocyclopentadiene 1 03/27/23 10:07 V31392JMV
<0.109 mg/Kg - dry 0.109 0.912Hexachloroethane 1 03/27/23 10:07 V31392JMV
<0.247 mg/Kg - dry 0.247 0.912Indeno(1,2,3-cd)pyrene 1 03/27/23 10:07 V31392JMV
<0.264 mg/Kg - dry 0.264 0.912Isophorone 1 03/27/23 10:07 V31392JMV
<0.146 mg/Kg - dry 0.146 0.9121-Methylnaphthalene 1 03/27/23 10:07 V31392JMV
<0.138 mg/Kg - dry 0.138 0.9122-Methylnaphthalene 1 03/27/23 10:07 V31392JMV
<0.134 mg/Kg - dry 0.134 0.9122-Methylphenol 1 03/27/23 10:07 V31392JMV
<0.117 mg/Kg - dry 0.117 0.9123&4 Methylphenol 1 03/27/23 10:07 V31392JMV
<0.199 mg/Kg - dry 0.199 0.912Naphthalene 1 03/27/23 10:07 V31392JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 59 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-6 (5-6)
91776 Matrix:
3/21/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31133 03/24/23 08:26
<0.133 mg/Kg - dry 0.133 0.9122-Nitroaniline 1 03/27/23 10:07 V31392JMV
<0.165 mg/Kg - dry 0.165 0.912
3-Nitroaniline 1 03/27/23 10:07 V31392JMV
<0.129 mg/Kg - dry 0.129 0.4564-Nitroaniline 1 03/27/23 10:07 V31392JMV
<0.160 mg/Kg - dry 0.160 0.456Nitrobenzene 1 03/27/23 10:07 V31392JMV
<0.122 mg/Kg - dry 0.122 0.9122-Nitrophenol 1 03/27/23 10:07 V31392JMV
<0.161 mg/Kg - dry 0.161 0.9124-Nitrophenol 1 03/27/23 10:07 V31392JMV
<0.363 mg/Kg - dry 0.363 0.912N-Nitrosodimethylamine 1 03/27/23 10:07 V31392JMV
<0.250 mg/Kg - dry 0.250 0.912N-Nitrosodiphenylamine 1 03/27/23 10:07 V31392JMV
<0.163 mg/Kg - dry 0.163 0.912
N-Nitroso-di-n-propylamine 1 03/27/23 10:07 V31392JMV
<0.479 mg/Kg - dry 0.479 1.38Pentachlorophenol 1 03/27/23 10:07 V31392JMV
<0.287 mg/Kg - dry 0.287 0.912Phenanthrene 1 03/27/23 10:07 V31392JMV
<0.154 mg/Kg - dry 0.154 0.912Phenol 1 03/27/23 10:07 V31392JMV
<0.185 mg/Kg - dry 0.185 0.912Pyrene 1 03/27/23 10:07 V31392JMV
<0.109 mg/Kg - dry 0.109 0.456Pyridine 1 03/27/23 10:07 V31392JMV
<0.147 mg/Kg - dry 0.147 0.9121,2,4-Trichlorobenzene 1 03/27/23 10:07 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9122,4,5-Trichlorophenol 1 03/27/23 10:07 V31392JMV
<0.133 mg/Kg - dry 0.133 0.9122,4,6-Trichlorophenol 1 03/27/23 10:07 V31392JMV
8270ESurrogate: Phenol-d5 71.2 Limits: 34-121%03/27/23 10:071 JMV
Surrogate: 2-Fluorobiphenyl 92.8 Limits: 44-115%03/27/23 10:071 JMV V31392
Surrogate: 2-Fluorophenol 79.3 Limits: 35-115%03/27/23 10:071 JMV V31392
Surrogate: Nitrobenzene-d5 80.2 Limits: 37-122%03/27/23 10:071 JMV V31392
Surrogate: 4-Terphenyl-d14 100 Limits: 54-127%03/27/23 10:071 JMV V31392
Surrogate: 2,4,6-Tribromophenol 62.8 Limits: 39-132%03/27/23 10:071 JMV V31392
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 60 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
24.1 %Moisture 1 03/27/23 15:51 SW-DRYWTPEB
1.01 mg/Kg - dry 0.185 0.263Chromium, Hexavalent 1 03/27/23 17:52 SW-7199SRJ
0.374 mg/Kg - dry 0.113 0.329Arsenic 5 03/27/23 23:48 6020BCPW
109 mg/Kg - dry 0.056 0.329Barium 5 03/27/23 23:48 6020BCPW
<0.0341 mg/Kg - dry 0.0341 0.329Cadmium 5 03/27/23 23:48 6020BCPW
123 mg/Kg - dry 0.611 1.32
Chromium 20 03/28/23 21:17 6020BCPW
1.31 mg/Kg - dry 0.0408 0.329Lead 5 03/27/23 23:48 6020BCPW
<0.0267 mg/Kg - dry 0.0267 0.221Mercury (Total)1 03/27/23 12:40 7471AFDS
0.482 mg/Kg - dry 0.135 0.329Selenium 5 03/27/23 23:48 6020BCPW
0.0152 J mg/Kg - dry 0.0088 0.329Silver 5 03/27/23 23:48 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 61 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.009 J mg/Kg - dry 0.003 0.026Acetone 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.026
Acrolein 1 03/25/23 20:38 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.026Acrylonitrile 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/23 20:38 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 03/25/23 20:38 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 03/25/23 20:38 V31266TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 03/25/23 20:38 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.013Chloromethane 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 03/25/23 20:38 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/23 20:38 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 03/25/23 20:38 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 62 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 03/25/23 20:38 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/23 20:38 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/25/23 20:38 V31266TBL
0.007 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/25/23 20:38 V31266TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/23 20:38 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 03/25/23 20:38 V31266TBL
<0.018 mg/Kg - dry 0.018 0.329Ethanol 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.065Ethyl Tertiary Butyl Ether (ETBE)1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 03/25/23 20:38 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 63 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.026
2-Hexanone 1 03/25/23 20:38 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/23 20:38 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.026Methyl Ethyl Ketone (MEK)1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/25/23 20:38 V31266TBL
<0.019 mg/Kg - dry 0.019 0.0264-Methyl-2-Pentanone 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Methylene Chloride 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013
Naphthalene 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/23 20:38 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/23 20:38 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 03/25/23 20:38 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,4-Trichlorobenzene 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/25/23 20:38 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/25/23 20:38 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/23 20:38 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 03/25/23 20:38 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 03/25/23 20:38 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 64 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.012 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 03/25/23 20:38 V31266TBL
0.007 mg/Kg - dry 0.0007 0.006
1,3,5-Trimethylbenzene 1 03/25/23 20:38 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 03/25/23 20:38 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Chloride 1 03/25/23 20:38 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/25/23 20:38 V31266TBL
0.010 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 03/25/23 20:38 V31266TBL
0.010 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/25/23 20:38 V31266
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%03/25/23 20:381 TBL V31266
Surrogate: Dibromofluoromethane 104 Limits: 84-123%03/25/23 20:381 TBL V31266
Surrogate: Toluene-d8 97.8 Limits: 76-129%03/25/23 20:381 TBL V31266
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.152 mg/Kg - dry 0.152 0.869Acenaphthene 1 03/29/23 00:31 V31378ANG
<0.138 mg/Kg - dry 0.138 0.869Acenaphthylene 1 03/29/23 00:31 V31378ANG
<0.200 mg/Kg - dry 0.200 0.869Aniline 1 03/29/23 00:31 V31378ANG
<0.188 mg/Kg - dry 0.188 0.869Anthracene 1 03/29/23 00:31 V31378ANG
<0.183 mg/Kg - dry 0.183 0.869
Benzo(a)anthracene 1 03/29/23 00:31 V31378ANG
<0.193 mg/Kg - dry 0.193 0.869Benzo(a)pyrene 1 03/29/23 00:31 V31378ANG
<0.192 mg/Kg - dry 0.192 0.869Benzo(b)fluoranthene 1 03/29/23 00:31 V31378ANG
<0.179 mg/Kg - dry 0.179 0.869Benzo(g,h,i)perylene 1 03/29/23 00:31 V31378ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 65 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.180 mg/Kg - dry 0.180 0.869Benzo(k)fluoranthene 1 03/29/23 00:31 V31378ANG
<0.764 mg/Kg - dry 0.764 2.64
Benzoic Acid 1 03/29/23 00:31 V31378ANG
<0.138 mg/Kg - dry 0.138 0.869Benzyl alcohol 1 03/29/23 00:31 V31378ANG
<0.155 mg/Kg - dry 0.155 0.869Bis(2-Chloroethoxy)methane 1 03/29/23 00:31 V31378ANG
<0.140 mg/Kg - dry 0.140 0.869Bis(2-Chloroethyl)ether 1 03/29/23 00:31 V31378ANG
<0.179 mg/Kg - dry 0.179 0.434Bis(2-Chloroisopropyl)ether 1 03/29/23 00:31 V31378ANG
<0.158 mg/Kg - dry 0.158 0.869Bis(2-ethylhexyl)phthalate 1 03/29/23 00:31 V31378ANG
<0.143 mg/Kg - dry 0.143 0.8694-Bromophenyl phenyl ether 1 03/29/23 00:31 V31378ANG
<0.148 mg/Kg - dry 0.148 0.434
Butyl benzyl phthalate 1 03/29/23 00:31 V31378ANG
<0.121 mg/Kg - dry 0.121 0.8694-Chloro-3-methylphenol 1 03/29/23 00:31 V31378ANG
<0.147 mg/Kg - dry 0.147 0.4344-Chloroaniline 1 03/29/23 00:31 V31378ANG
<0.152 mg/Kg - dry 0.152 0.8692-Chloronaphthalene 1 03/29/23 00:31 V31378ANG
<0.129 mg/Kg - dry 0.129 0.8692-Chlorophenol 1 03/29/23 00:31 V31378ANG
<0.166 mg/Kg - dry 0.166 1.324-Chlorophenyl phenyl ether 1 03/29/23 00:31 V31378ANG
<0.187 mg/Kg - dry 0.187 0.869Chrysene 1 03/29/23 00:31 V31378ANG
<0.303 mg/Kg - dry 0.303 0.869Dibenz(a,h)anthracene 1 03/29/23 00:31 V31378ANG
<0.156 mg/Kg - dry 0.156 0.869Dibenzofuran 1 03/29/23 00:31 V31378ANG
<0.124 mg/Kg - dry 0.124 0.8691,2-Dichlorobenzene 1 03/29/23 00:31 V31378ANG
<0.128 mg/Kg - dry 0.128 0.8691,3-Dichlorobenzene 1 03/29/23 00:31 V31378ANG
<0.128 mg/Kg - dry 0.128 0.4341,4-Dichlorobenzene 1 03/29/23 00:31 V31378ANG
<0.193 mg/Kg - dry 0.193 0.8693,3'-Dichlorobenzidine 1 03/29/23 00:31 V31378ANG
<0.126 mg/Kg - dry 0.126 0.8692,4-Dichlorophenol 1 03/29/23 00:31 V31378ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 66 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.237 mg/Kg - dry 0.237 0.869Diethyl phthalate 1 03/29/23 00:31 V31378ANG
<0.229 mg/Kg - dry 0.229 0.869
Dimethyl phthalate 1 03/29/23 00:31 V31378ANG
<0.142 mg/Kg - dry 0.142 0.4342,4-Dimethylphenol 1 03/29/23 00:31 V31378ANG
<0.140 mg/Kg - dry 0.140 0.869Di-n-butyl phthalate 1 03/29/23 00:31 V31378ANG
<0.316 mg/Kg - dry 0.316 1.984,6-Dinitro-2-methylphenol 1 03/29/23 00:31 V31378ANG
<0.685 mg/Kg - dry 0.685 1.982,4-Dinitrophenol 1 03/29/23 00:31 V31378ANG
<0.127 mg/Kg - dry 0.127 0.8692,4-Dinitrotoluene 1 03/29/23 00:31 V31378ANG
<0.142 mg/Kg - dry 0.142 0.8692,6-Dinitrotoluene 1 03/29/23 00:31 V31378ANG
<0.188 mg/Kg - dry 0.188 0.434
Di-n-Octyl Phthalate 1 03/29/23 00:31 V31378ANG
<0.162 mg/Kg - dry 0.162 0.869Fluoranthene 1 03/29/23 00:31 V31378ANG
<0.168 mg/Kg - dry 0.168 0.869Fluorene 1 03/29/23 00:31 V31378ANG
<0.139 mg/Kg - dry 0.139 0.869Hexachlorobenzene 1 03/29/23 00:31 V31378ANG
<0.128 mg/Kg - dry 0.128 0.869Hexachlorobutadiene 1 03/29/23 00:31 V31378ANG
<0.206 mg/Kg - dry 0.206 0.869Hexachlorocyclopentadiene 1 03/29/23 00:31 V31378ANG
<0.104 mg/Kg - dry 0.104 0.869Hexachloroethane 1 03/29/23 00:31 V31378ANG
<0.235 mg/Kg - dry 0.235 0.869Indeno(1,2,3-cd)pyrene 1 03/29/23 00:31 V31378ANG
<0.251 mg/Kg - dry 0.251 0.869Isophorone 1 03/29/23 00:31 V31378ANG
<0.139 mg/Kg - dry 0.139 0.8691-Methylnaphthalene 1 03/29/23 00:31 V31378ANG
<0.131 mg/Kg - dry 0.131 0.8692-Methylnaphthalene 1 03/29/23 00:31 V31378ANG
<0.127 mg/Kg - dry 0.127 0.8692-Methylphenol 1 03/29/23 00:31 V31378ANG
<0.111 mg/Kg - dry 0.111 0.8693&4 Methylphenol 1 03/29/23 00:31 V31378ANG
<0.189 mg/Kg - dry 0.189 0.869Naphthalene 1 03/29/23 00:31 V31378ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 67 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-7 (5-6)
91777 Matrix:
3/21/2023 13:25
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.127 mg/Kg - dry 0.127 0.8692-Nitroaniline 1 03/29/23 00:31 V31378ANG
<0.158 mg/Kg - dry 0.158 0.869
3-Nitroaniline 1 03/29/23 00:31 V31378ANG
<0.122 mg/Kg - dry 0.122 0.4344-Nitroaniline 1 03/29/23 00:31 V31378ANG
<0.152 mg/Kg - dry 0.152 0.434Nitrobenzene 1 03/29/23 00:31 V31378ANG
<0.116 mg/Kg - dry 0.116 0.8692-Nitrophenol 1 03/29/23 00:31 V31378ANG
<0.154 mg/Kg - dry 0.154 0.8694-Nitrophenol 1 03/29/23 00:31 V31378ANG
<0.346 mg/Kg - dry 0.346 0.869N-Nitrosodimethylamine 1 03/29/23 00:31 V31378ANG
<0.238 mg/Kg - dry 0.238 0.869N-Nitrosodiphenylamine 1 03/29/23 00:31 V31378ANG
<0.155 mg/Kg - dry 0.155 0.869
N-Nitroso-di-n-propylamine 1 03/29/23 00:31 V31378ANG
<0.457 mg/Kg - dry 0.457 1.32Pentachlorophenol 1 03/29/23 00:31 V31378ANG
<0.274 mg/Kg - dry 0.274 0.869Phenanthrene 1 03/29/23 00:31 V31378ANG
<0.147 mg/Kg - dry 0.147 0.869Phenol 1 03/29/23 00:31 V31378ANG
<0.176 mg/Kg - dry 0.176 0.869Pyrene 1 03/29/23 00:31 V31378ANG
<0.104 mg/Kg - dry 0.104 0.434Pyridine 1 03/29/23 00:31 V31378ANG
<0.140 mg/Kg - dry 0.140 0.8691,2,4-Trichlorobenzene 1 03/29/23 00:31 V31378ANG
<0.126 mg/Kg - dry 0.126 0.8692,4,5-Trichlorophenol 1 03/29/23 00:31 V31378ANG
<0.127 mg/Kg - dry 0.127 0.8692,4,6-Trichlorophenol 1 03/29/23 00:31 V31378ANG
8270ESurrogate: Phenol-d5 72.7 Limits: 34-121%03/29/23 00:311 ANG
Surrogate: 2-Fluorobiphenyl 93.4 Limits: 44-115%03/29/23 00:311 ANG V31378
Surrogate: 2-Fluorophenol 79.9 Limits: 35-115%03/29/23 00:311 ANG V31378
Surrogate: Nitrobenzene-d5 85.6 Limits: 37-122%03/29/23 00:311 ANG V31378
Surrogate: 4-Terphenyl-d14 105 Limits: 54-127%03/29/23 00:311 ANG V31378
Surrogate: 2,4,6-Tribromophenol 64.6 Limits: 39-132%03/29/23 00:311 ANG V31378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 68 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.2 %Moisture 1 03/27/23 15:51 SW-DRYWTPEB
<0.196 mg/Kg - dry 0.196 0.278Chromium, Hexavalent 1 03/27/23 18:03 SW-7199SRJ
0.447 mg/Kg - dry 0.119 0.348Arsenic 5 03/27/23 23:52 6020BCPW
156 mg/Kg - dry 0.059 0.348Barium 5 03/27/23 23:52 6020BCPW
0.0462 J mg/Kg - dry 0.0360 0.348Cadmium 5 03/27/23 23:52 6020BCPW
126 mg/Kg - dry 0.646 1.39
Chromium 20 03/28/23 21:21 6020BCPW
1.14 mg/Kg - dry 0.0431 0.348Lead 5 03/27/23 23:52 6020BCPW
<0.0320 mg/Kg - dry 0.0320 0.266Mercury (Total)1 03/27/23 12:41 7471AFDS
0.391 mg/Kg - dry 0.143 0.348Selenium 5 03/27/23 23:52 6020BCPW
0.0204 J mg/Kg - dry 0.0093 0.348Silver 5 03/27/23 23:52 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 69 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.006 J mg/Kg - dry 0.003 0.027Acetone 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.027
Acrolein 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 03/25/23 21:05 V31266TBL
0.001 J mg/Kg - dry 0.0008 0.006Benzene 1 03/25/23 21:05 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/25/23 21:05 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013
Bromomethane 1 03/25/23 21:05 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 03/25/23 21:05 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 03/25/23 21:05 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 03/25/23 21:05 V31266TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 03/25/23 21:05 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 03/25/23 21:05 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 03/25/23 21:05 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 70 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 03/25/23 21:05 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006
1,2-Dibromoethane 1 03/25/23 21:05 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 03/25/23 21:05 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/25/23 21:05 V31266TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/25/23 21:05 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/25/23 21:05 V31266TBL
0.007 mg/Kg - dry 0.001 0.006
1,2-Dichloroethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/25/23 21:05 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 03/25/23 21:05 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 03/25/23 21:05 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 03/25/23 21:05 V31266TBL
<0.019 mg/Kg - dry 0.019 0.348Ethanol 1 03/25/23 21:05 V31266TBL
0.003 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 03/25/23 21:05 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 71 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.027
2-Hexanone 1 03/25/23 21:05 V31266TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/25/23 21:05 V31266TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 03/25/23 21:05 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 03/25/23 21:05 V31266TBL
0.001 J
mg/Kg - dry 0.001 0.013
Naphthalene 1 03/25/23 21:05 V31266TBL
0.003 J mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/25/23 21:05 V31266TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.006Toluene 1 03/25/23 21:05 V31266TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,3-Trichlorobenzene 1 03/25/23 21:05 V31266TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 03/25/23 21:05 V31266TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 03/25/23 21:05 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/25/23 21:05 V31266TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 03/25/23 21:05 V31266TBL
<0.001 mg/Kg - dry 0.001 0.0061,2,3-Trichloropropane 1 03/25/23 21:05 V31266TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 72 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V31265 03/25/23 08:00
0.043 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 03/25/23 21:05 V31266TBL
0.013 mg/Kg - dry 0.0008 0.006
1,3,5-Trimethylbenzene 1 03/25/23 21:05 V31266TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 03/25/23 21:05 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 03/25/23 21:05 V31266TBL
<0.0007 mg/Kg - dry 0.0007 0.006o-Xylene 1 03/25/23 21:05 V31266TBL
0.094 mg/Kg - dry 0.001 0.013m,p-Xylene 1 03/25/23 21:05 V31266TBL
0.094 mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/25/23 21:05 V31266
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 70-130%03/25/23 21:051 TBL V31266
Surrogate: Dibromofluoromethane 103 Limits: 84-123%03/25/23 21:051 TBL V31266
Surrogate: Toluene-d8 97.5 Limits: 76-129%03/25/23 21:051 TBL V31266
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.161 mg/Kg - dry 0.161 0.919Acenaphthene 1 03/29/23 00:54 V31378ANG
<0.146 mg/Kg - dry 0.146 0.919Acenaphthylene 1 03/29/23 00:54 V31378ANG
<0.211 mg/Kg - dry 0.211 0.919Aniline 1 03/29/23 00:54 V31378ANG
<0.199 mg/Kg - dry 0.199 0.919Anthracene 1 03/29/23 00:54 V31378ANG
<0.193 mg/Kg - dry 0.193 0.919
Benzo(a)anthracene 1 03/29/23 00:54 V31378ANG
<0.204 mg/Kg - dry 0.204 0.919Benzo(a)pyrene 1 03/29/23 00:54 V31378ANG
<0.203 mg/Kg - dry 0.203 0.919Benzo(b)fluoranthene 1 03/29/23 00:54 V31378ANG
<0.189 mg/Kg - dry 0.189 0.919Benzo(g,h,i)perylene 1 03/29/23 00:54 V31378ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 73 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.190 mg/Kg - dry 0.190 0.919Benzo(k)fluoranthene 1 03/29/23 00:54 V31378ANG
<0.807 mg/Kg - dry 0.807 2.79
Benzoic Acid 1 03/29/23 00:54 V31378ANG
<0.146 mg/Kg - dry 0.146 0.919Benzyl alcohol 1 03/29/23 00:54 V31378ANG
<0.164 mg/Kg - dry 0.164 0.919Bis(2-Chloroethoxy)methane 1 03/29/23 00:54 V31378ANG
<0.149 mg/Kg - dry 0.149 0.919Bis(2-Chloroethyl)ether 1 03/29/23 00:54 V31378ANG
<0.189 mg/Kg - dry 0.189 0.459Bis(2-Chloroisopropyl)ether 1 03/29/23 00:54 V31378ANG
<0.167 mg/Kg - dry 0.167 0.919Bis(2-ethylhexyl)phthalate 1 03/29/23 00:54 V31378ANG
<0.151 mg/Kg - dry 0.151 0.9194-Bromophenyl phenyl ether 1 03/29/23 00:54 V31378ANG
<0.157 mg/Kg - dry 0.157 0.459
Butyl benzyl phthalate 1 03/29/23 00:54 V31378ANG
<0.128 mg/Kg - dry 0.128 0.9194-Chloro-3-methylphenol 1 03/29/23 00:54 V31378ANG
<0.155 mg/Kg - dry 0.155 0.4594-Chloroaniline 1 03/29/23 00:54 V31378ANG
<0.161 mg/Kg - dry 0.161 0.9192-Chloronaphthalene 1 03/29/23 00:54 V31378ANG
<0.136 mg/Kg - dry 0.136 0.9192-Chlorophenol 1 03/29/23 00:54 V31378ANG
<0.175 mg/Kg - dry 0.175 1.394-Chlorophenyl phenyl ether 1 03/29/23 00:54 V31378ANG
<0.197 mg/Kg - dry 0.197 0.919Chrysene 1 03/29/23 00:54 V31378ANG
<0.320 mg/Kg - dry 0.320 0.919Dibenz(a,h)anthracene 1 03/29/23 00:54 V31378ANG
<0.165 mg/Kg - dry 0.165 0.919Dibenzofuran 1 03/29/23 00:54 V31378ANG
<0.131 mg/Kg - dry 0.131 0.9191,2-Dichlorobenzene 1 03/29/23 00:54 V31378ANG
<0.135 mg/Kg - dry 0.135 0.9191,3-Dichlorobenzene 1 03/29/23 00:54 V31378ANG
<0.135 mg/Kg - dry 0.135 0.4591,4-Dichlorobenzene 1 03/29/23 00:54 V31378ANG
<0.204 mg/Kg - dry 0.204 0.9193,3'-Dichlorobenzidine 1 03/29/23 00:54 V31378ANG
<0.133 mg/Kg - dry 0.133 0.9192,4-Dichlorophenol 1 03/29/23 00:54 V31378ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 74 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.250 mg/Kg - dry 0.250 0.919Diethyl phthalate 1 03/29/23 00:54 V31378ANG
<0.242 mg/Kg - dry 0.242 0.919
Dimethyl phthalate 1 03/29/23 00:54 V31378ANG
<0.150 mg/Kg - dry 0.150 0.4592,4-Dimethylphenol 1 03/29/23 00:54 V31378ANG
<0.149 mg/Kg - dry 0.149 0.919Di-n-butyl phthalate 1 03/29/23 00:54 V31378ANG
<0.334 mg/Kg - dry 0.334 2.094,6-Dinitro-2-methylphenol 1 03/29/23 00:54 V31378ANG
<0.724 mg/Kg - dry 0.724 2.092,4-Dinitrophenol 1 03/29/23 00:54 V31378ANG
<0.134 mg/Kg - dry 0.134 0.9192,4-Dinitrotoluene 1 03/29/23 00:54 V31378ANG
<0.150 mg/Kg - dry 0.150 0.9192,6-Dinitrotoluene 1 03/29/23 00:54 V31378ANG
<0.199 mg/Kg - dry 0.199 0.459
Di-n-Octyl Phthalate 1 03/29/23 00:54 V31378ANG
<0.171 mg/Kg - dry 0.171 0.919Fluoranthene 1 03/29/23 00:54 V31378ANG
<0.178 mg/Kg - dry 0.178 0.919Fluorene 1 03/29/23 00:54 V31378ANG
<0.147 mg/Kg - dry 0.147 0.919Hexachlorobenzene 1 03/29/23 00:54 V31378ANG
<0.135 mg/Kg - dry 0.135 0.919Hexachlorobutadiene 1 03/29/23 00:54 V31378ANG
<0.218 mg/Kg - dry 0.218 0.919Hexachlorocyclopentadiene 1 03/29/23 00:54 V31378ANG
<0.110 mg/Kg - dry 0.110 0.919Hexachloroethane 1 03/29/23 00:54 V31378ANG
<0.249 mg/Kg - dry 0.249 0.919Indeno(1,2,3-cd)pyrene 1 03/29/23 00:54 V31378ANG
<0.266 mg/Kg - dry 0.266 0.919Isophorone 1 03/29/23 00:54 V31378ANG
<0.147 mg/Kg - dry 0.147 0.9191-Methylnaphthalene 1 03/29/23 00:54 V31378ANG
<0.139 mg/Kg - dry 0.139 0.9192-Methylnaphthalene 1 03/29/23 00:54 V31378ANG
<0.135 mg/Kg - dry 0.135 0.9192-Methylphenol 1 03/29/23 00:54 V31378ANG
<0.118 mg/Kg - dry 0.118 0.9193&4 Methylphenol 1 03/29/23 00:54 V31378ANG
<0.200 mg/Kg - dry 0.200 0.919Naphthalene 1 03/29/23 00:54 V31378ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 75 of 117
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
23-080-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Haley Martin
Charlotte
Received : 03/21/2023
AKR-007
Report Date : 04/03/2023
Sample ID :
Lab No :
Sampled:UST-8 (5-6)
91778 Matrix:
3/21/2023 14:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V31269 03/28/23 09:15
<0.134 mg/Kg - dry 0.134 0.9192-Nitroaniline 1 03/29/23 00:54 V31378ANG
<0.167 mg/Kg - dry 0.167 0.919
3-Nitroaniline 1 03/29/23 00:54 V31378ANG
<0.129 mg/Kg - dry 0.129 0.4594-Nitroaniline 1 03/29/23 00:54 V31378ANG
<0.161 mg/Kg - dry 0.161 0.459Nitrobenzene 1 03/29/23 00:54 V31378ANG
<0.123 mg/Kg - dry 0.123 0.9192-Nitrophenol 1 03/29/23 00:54 V31378ANG
<0.162 mg/Kg - dry 0.162 0.9194-Nitrophenol 1 03/29/23 00:54 V31378ANG
<0.366 mg/Kg - dry 0.366 0.919N-Nitrosodimethylamine 1 03/29/23 00:54 V31378ANG
<0.252 mg/Kg - dry 0.252 0.919N-Nitrosodiphenylamine 1 03/29/23 00:54 V31378ANG
<0.164 mg/Kg - dry 0.164 0.919
N-Nitroso-di-n-propylamine 1 03/29/23 00:54 V31378ANG
<0.483 mg/Kg - dry 0.483 1.39Pentachlorophenol 1 03/29/23 00:54 V31378ANG
<0.289 mg/Kg - dry 0.289 0.919Phenanthrene 1 03/29/23 00:54 V31378ANG
<0.155 mg/Kg - dry 0.155 0.919Phenol 1 03/29/23 00:54 V31378ANG
<0.186 mg/Kg - dry 0.186 0.919Pyrene 1 03/29/23 00:54 V31378ANG
<0.110 mg/Kg - dry 0.110 0.459Pyridine 1 03/29/23 00:54 V31378ANG
<0.149 mg/Kg - dry 0.149 0.9191,2,4-Trichlorobenzene 1 03/29/23 00:54 V31378ANG
<0.133 mg/Kg - dry 0.133 0.9192,4,5-Trichlorophenol 1 03/29/23 00:54 V31378ANG
<0.134 mg/Kg - dry 0.134 0.9192,4,6-Trichlorophenol 1 03/29/23 00:54 V31378ANG
8270ESurrogate: Phenol-d5 69.5 Limits: 34-121%03/29/23 00:541 ANG
Surrogate: 2-Fluorobiphenyl 89.8 Limits: 44-115%03/29/23 00:541 ANG V31378
Surrogate: 2-Fluorophenol 76.9 Limits: 35-115%03/29/23 00:541 ANG V31378
Surrogate: Nitrobenzene-d5 81.4 Limits: 37-122%03/29/23 00:541 ANG V31378
Surrogate: 4-Terphenyl-d14 99.4 Limits: 54-127%03/29/23 00:541 ANG V31378
Surrogate: 2,4,6-Tribromophenol 61.7 Limits: 39-132%03/29/23 00:541 ANG V31378
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Page 76 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Metals Analyses
6020B
L672456,L672850QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L671954
Associated Lab Samples: 91771, 91772, 91773, 91774, 91775, 91776, 91777, 91778
LRB-L671954 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/27/23 22:210.2500.0855<0.0855mg/KgArsenic
03/27/23 22:210.2500.042<0.042mg/KgBarium
03/27/23 22:210.2500.0259<0.0259mg/KgCadmium
03/27/23 22:210.2500.1160.121mg/KgChromium
03/27/23 22:210.2500.0310<0.0310mg/KgLead
03/27/23 22:210.2500.103<0.103mg/KgSelenium
03/27/23 22:210.2500.0067<0.0067mg/KgSilver
LCS-L671954Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
89.02.232.50mg/KgArsenic 80-120
89.04.435.00mg/KgBarium 80-120
91.00.4550.500mg/KgCadmium 80-120
96.04.795.00mg/KgChromium 80-120
97.02.432.50mg/KgLead 80-120
95.04.775.00mg/KgSelenium 80-120
93.00.4650.500mg/KgSilver 80-120
V 91778-MS-L671954 V 91778-MSD-L671954Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.68 55.0*1.662.332.490.321mg/KgArsenic 57.0*75-125 1.1 80
110 0.0*1134.674.98112mg/KgBarium 21.0*75-125 2.6 80
0.421 78.00.4150.4670.4980.0332mg/KgCadmium 82.0 75-125 1.4 80
84.8 0.0*1024.674.9890.6mg/KgChromium 244*75-125 18.4 80
Page 1 of 39* QC Fail Date:04/03/2023 02:47 PM
Page 77 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Metals Analyses
6020B
L672456,L672850QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L671954
V 91778-MS-L671954 V 91778-MSD-L671954Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
2.79 79.03.092.332.490.821mg/KgLead 97.0 75-125 10.2 80
3.06 56.0*2.724.674.980.281mg/KgSelenium 52.0*75-125 11.7 80
0.406 79.00.3990.4670.4980.0147mg/KgSilver 82.0 75-125 1.7 80
V 91778-PDS-L671954Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/28/23 00:0392.01.15mg/KgArsenic
03/28/23 00:0310314.0mg/KgBarium
03/28/23 00:0396.00.238mg/KgCadmium
03/28/23 21:3299.04.65mg/KgChromium
03/28/23 00:0398.01.29mg/KgLead
03/28/23 00:0395.02.35mg/KgSelenium
03/28/23 00:0398.00.242mg/KgSilver
Page 2 of 39* QC Fail Date:04/03/2023 02:47 PM
Page 78 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471A
L672319QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471A
QC Prep:L672056
Associated Lab Samples: 91771, 91772, 91773, 91774, 91775, 91776, 91777, 91778
LRB-L672056 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/27/23 12:150.1920.0232<0.0232mg/KgMercury (Total)
LCS-L672056Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1060.4220.400mg/KgMercury (Total)80-120
E 61457-MS-L672056 E 61457-MSD-L672056Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.510 128*0.5110.3720.3980.132mg/KgMercury (Total)137*80-120 0.1 20
E 61457-PDS-L672056Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
03/27/23 12:57129*0.954mg/KgMercury (Total)
Page 3 of 39* QC Fail Date:04/03/2023 02:47 PM
Page 79 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31266QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31265
Associated Lab Samples: 91773, 91774, 91775, 91776, 91777, 91778
LRB-V31265 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/25/23 16:060.0200.002<0.002mg/KgAcetone
03/25/23 16:060.0200.001<0.001mg/KgAcrolein
03/25/23 16:060.0200.0008<0.0008mg/KgAcrylonitrile
03/25/23 16:060.0050.0006<0.0006mg/KgBenzene
03/25/23 16:060.0050.0005<0.0005mg/KgBromobenzene
03/25/23 16:060.0050.0008<0.0008mg/KgBromochloromethane
03/25/23 16:060.0050.001<0.001mg/KgBromodichloromethane
03/25/23 16:060.0050.001<0.001mg/KgBromoform
03/25/23 16:060.0100.001<0.001mg/KgBromomethane
03/25/23 16:060.0050.0005<0.0005mg/Kgn-Butylbenzene
03/25/23 16:060.0050.0006<0.0006mg/Kgsec-Butyl benzene
03/25/23 16:060.0050.0005<0.0005mg/Kgtert-Butyl benzene
03/25/23 16:060.0050.0006<0.0006mg/KgCarbon Disulfide
03/25/23 16:060.0050.001<0.001mg/KgCarbon Tetrachloride
03/25/23 16:060.0050.0007<0.0007mg/KgChlorobenzene
03/25/23 16:060.0050.0009<0.0009mg/KgChlorodibromomethane
03/25/23 16:060.0100.0009<0.0009mg/KgChloroethane
03/25/23 16:060.0050.001<0.001mg/KgChloroform
03/25/23 16:060.0100.0006<0.0006mg/KgChloromethane
03/25/23 16:060.0050.0005<0.0005mg/Kg2-Chlorotoluene
03/25/23 16:060.0050.0004<0.0004mg/Kg4-Chlorotoluene
03/25/23 16:060.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/25/23 16:060.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
03/25/23 16:060.0050.0006<0.0006mg/Kg1,2-Dibromoethane
03/25/23 16:060.0050.0006<0.0006mg/KgDibromomethane
03/25/23 16:060.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
03/25/23 16:060.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 39Date:04/03/2023 02:47 PM
Page 80 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31266QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31265
Associated Lab Samples: 91773, 91774, 91775, 91776, 91777, 91778
LRB-V31265 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/25/23 16:060.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/25/23 16:060.0100.001<0.001mg/KgDichlorodifluoromethane
03/25/23 16:060.0050.0008<0.0008mg/Kg1,1-Dichloroethane
03/25/23 16:060.0050.001<0.001mg/Kg1,2-Dichloroethane
03/25/23 16:060.0050.0007<0.0007mg/Kg1,1-Dichloroethene
03/25/23 16:060.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/25/23 16:060.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
03/25/23 16:060.0050.0004<0.0004mg/Kg1,2-Dichloropropane
03/25/23 16:060.0050.0006<0.0006mg/Kg1,3-Dichloropropane
03/25/23 16:060.0050.001<0.001mg/Kg2,2-Dichloropropane
03/25/23 16:060.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/25/23 16:060.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/25/23 16:060.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
03/25/23 16:060.2500.014<0.014mg/KgEthanol
03/25/23 16:060.0050.0006<0.0006mg/KgEthylbenzene
03/25/23 16:060.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/25/23 16:060.0100.0008<0.0008mg/KgHexachlorobutadiene
03/25/23 16:060.0100.0007<0.0007mg/Kgn-Hexane
03/25/23 16:060.0200.0006<0.0006mg/Kg2-Hexanone
03/25/23 16:060.0050.0005<0.0005mg/KgIsopropylbenzene
03/25/23 16:060.0050.001<0.001mg/Kg4-Isopropyl toluene
03/25/23 16:060.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
03/25/23 16:060.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
03/25/23 16:060.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/25/23 16:060.0100.0010.001mg/KgMethylene Chloride
03/25/23 16:060.0100.0010<0.0010mg/KgNaphthalene
03/25/23 16:060.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 5 of 39Date:04/03/2023 02:47 PM
Page 81 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31266QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31265
Associated Lab Samples: 91773, 91774, 91775, 91776, 91777, 91778
LRB-V31265 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/25/23 16:060.0050.001<0.001mg/KgStyrene
03/25/23 16:060.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
03/25/23 16:060.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
03/25/23 16:060.0050.0009<0.0009mg/KgTetrachloroethene
03/25/23 16:060.0050.0007<0.0007mg/KgToluene
03/25/23 16:060.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
03/25/23 16:060.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
03/25/23 16:060.0050.001<0.001mg/Kg1,1,1-Trichloroethane
03/25/23 16:060.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/25/23 16:060.0050.0009<0.0009mg/KgTrichloroethene
03/25/23 16:060.0100.002<0.002mg/KgTrichlorofluoromethane
03/25/23 16:060.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
03/25/23 16:060.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
03/25/23 16:060.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
03/25/23 16:060.0100.0005<0.0005mg/KgVinyl Acetate
03/25/23 16:060.0100.0005<0.0005mg/KgVinyl Chloride
03/25/23 16:060.0050.0005<0.0005mg/Kgo-Xylene
03/25/23 16:060.0100.001<0.001mg/Kgm,p-Xylene
03/25/23 16:064-Bromofluorobenzene (S)101 70-130
03/25/23 16:06Dibromofluoromethane (S)99.6 84-123
03/25/23 16:06Toluene-d8 (S)99.8 76-129
LCS-V31265 LCSD-V31265Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.074 74.975.50.0750.100mg/KgAcetone 29-198 0.7 20
Page 6 of 39Date:04/03/2023 02:47 PM
Page 82 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31266QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31265
LCS-V31265 LCSD-V31265Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.096 96.297.80.0970.100mg/KgAcrolein 70-130 1.6 20
0.095 95.592.80.0920.100mg/KgAcrylonitrile 65-134 2.8 20
0.046 92.897.60.0480.050mg/KgBenzene 74-127 5.0 20
0.046 93.496.20.0480.050mg/KgBromobenzene 73-125 2.9 20
0.048 97.499.40.0490.050mg/KgBromochloromethane 72-134 2.0 20
0.047 95.898.00.0490.050mg/KgBromodichloromethane 75-122 2.2 20
0.047 95.092.60.0460.050mg/KgBromoform 66-135 2.5 20
0.043 87.61040.0520.050mg/KgBromomethane 20-180 17.1 20
0.047 95.21020.0510.050mg/Kgn-Butylbenzene 65-135 6.8 20
0.047 95.21000.0500.050mg/Kgsec-Butyl benzene 66-131 5.1 20
0.047 94.498.60.0490.050mg/Kgtert-Butyl benzene 67-132 4.3 20
0.044 89.896.80.0480.050mg/KgCarbon Disulfide 61-129 7.5 20
0.044 89.898.20.0490.050mg/KgCarbon Tetrachloride 64-143 8.9 20
0.049 99.498.60.0490.050mg/KgChlorobenzene 74-118 0.8 20
0.048 97.892.60.0460.050mg/KgChlorodibromomethane 73-122 5.4 20
0.054 1081180.0580.050mg/KgChloroethane 33-149 8.3 20
0.047 94.498.60.0490.050mg/KgChloroform 73-127 4.3 20
0.044 88.490.80.0450.050mg/KgChloromethane 45-143 2.6 20
0.046 93.697.80.0480.050mg/Kg2-Chlorotoluene 67-124 4.3 20
0.046 93.697.80.0480.050mg/Kg4-Chlorotoluene 71-126 4.3 20
0.045 90.092.80.0460.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.0 20
0.044 89.685.00.0420.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 5.2 20
0.047 95.698.60.0490.050mg/Kg1,2-Dibromoethane 70-132 3.0 20
0.047 95.894.80.0470.050mg/KgDibromomethane 74-133 1.0 20
0.047 95.499.40.0490.050mg/Kg1,2-Dichlorobenzene 72-123 4.1 20
0.047 95.697.20.0480.050mg/Kg1,3-Dichlorobenzene 71-120 1.6 20
Page 7 of 39Date:04/03/2023 02:47 PM
Page 83 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31266QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31265
LCS-V31265 LCSD-V31265Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.296.40.0480.050mg/Kg1,4-Dichlorobenzene 71-123 4.4 20
0.050 1021110.0550.050mg/KgDichlorodifluoromethane 26-146 8.6 20
0.046 93.898.40.0490.050mg/Kg1,1-Dichloroethane 74-127 4.7 20
0.046 92.494.20.0470.050mg/Kg1,2-Dichloroethane 68-128 1.9 20
0.045 90.097.00.0480.050mg/Kg1,1-Dichloroethene 67-149 7.4 20
0.046 93.297.20.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 4.2 20
0.045 90.697.60.0480.050mg/Kgtrans-1,2-Dichloroethene 73-132 7.4 20
0.046 92.896.80.0480.050mg/Kg1,2-Dichloropropane 73-130 4.2 20
0.047 94.094.80.0470.050mg/Kg1,3-Dichloropropane 75-124 0.8 20
0.044 89.897.60.0480.050mg/Kg2,2-Dichloropropane 50-142 8.3 20
0.045 90.298.00.0490.050mg/Kg1,1-Dichloropropene 71-130 8.2 20
0.046 93.296.40.0480.050mg/Kgcis-1,3-Dichloropropene 71-125 3.3 20
0.049 98.299.40.0490.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.2 20
0.980 78.476.40.9561.25mg/KgEthanol 70-130 2.4 20
0.046 93.698.60.0490.050mg/KgEthylbenzene 74-128 5.2 20
0.091 91.191.60.0910.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.5 20
0.049 98.01060.0530.050mg/KgHexachlorobutadiene 64-125 8.0 20
0.049 99.21050.0520.050mg/Kgn-Hexane 70-130 6.0 20
0.040 80.277.80.0380.050mg/Kg2-Hexanone 61-157 3.0 20
0.046 93.697.60.0480.050mg/KgIsopropylbenzene 68-126 4.1 20
0.047 94.41010.0500.050mg/Kg4-Isopropyl toluene 68-129 6.7 20
0.044 89.894.00.0470.050mg/KgMethyl Ethyl Ketone (MEK)63-149 4.5 20
0.045 90.692.00.0460.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.5 20
0.046 93.693.60.0460.050mg/Kg4-Methyl-2-Pentanone 57-162 0.0 20
0.042 85.890.00.0450.050mg/KgMethylene Chloride 74-129 4.7 20
0.044 89.288.00.0440.050mg/KgNaphthalene 57-157 1.3 20
Page 8 of 39Date:04/03/2023 02:47 PM
Page 84 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31266QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31265
LCS-V31265 LCSD-V31265Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.046 92.298.80.0490.050mg/Kgn-Propylbenzene 67-130 6.9 20
0.049 98.699.40.0490.050mg/KgStyrene 77-121 0.8 20
0.049 98.298.00.0490.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.2 20
0.044 88.087.60.0430.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.4 20
0.048 97.01010.0500.050mg/KgTetrachloroethene 68-130 4.2 20
0.045 91.894.20.0470.050mg/KgToluene 71-129 2.5 20
0.046 93.487.60.0430.050mg/Kg1,2,3-Trichlorobenzene 68-130 6.4 20
0.048 97.896.60.0480.050mg/Kg1,2,4-Trichlorobenzene 66-125 1.2 20
0.046 92.898.80.0490.050mg/Kg1,1,1-Trichloroethane 67-131 6.2 20
0.046 92.891.60.0450.050mg/Kg1,1,2-Trichloroethane 70-133 1.3 20
0.046 93.01010.0500.050mg/KgTrichloroethene 75-133 8.2 20
0.048 96.21070.0530.050mg/KgTrichlorofluoromethane 44-146 10.4 20
0.044 88.687.40.0430.050mg/Kg1,2,3-Trichloropropane 60-137 1.3 20
0.047 95.097.60.0480.050mg/Kg1,2,4-Trimethylbenzene 69-129 2.6 20
0.046 93.498.60.0490.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.4 20
0.050 1011020.0500.050mg/KgVinyl Acetate 60-140 0.7 20
0.044 88.698.20.0490.050mg/KgVinyl Chloride 48-147 10.2 20
0.046 93.698.20.0490.050mg/Kgo-Xylene 74-126 4.7 20
0.096 96.198.10.0980.100mg/Kgm,p-Xylene 75-124 2.0 20
98.21024-Bromofluorobenzene (S)70-130
10199.2Dibromofluoromethane (S)84-123
10299.6Toluene-d8 (S)76-129
Page 9 of 39Date:04/03/2023 02:47 PM
Page 85 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31293QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31292
Associated Lab Samples: 91772
LRB-V31292 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/23 12:220.0200.002<0.002mg/KgAcetone
03/27/23 12:220.0200.001<0.001mg/KgAcrolein
03/27/23 12:220.0200.0008<0.0008mg/KgAcrylonitrile
03/27/23 12:220.0050.0006<0.0006mg/KgBenzene
03/27/23 12:220.0050.0005<0.0005mg/KgBromobenzene
03/27/23 12:220.0050.0008<0.0008mg/KgBromochloromethane
03/27/23 12:220.0050.001<0.001mg/KgBromodichloromethane
03/27/23 12:220.0050.001<0.001mg/KgBromoform
03/27/23 12:220.0100.001<0.001mg/KgBromomethane
03/27/23 12:220.0050.0005<0.0005mg/Kgn-Butylbenzene
03/27/23 12:220.0050.0006<0.0006mg/Kgsec-Butyl benzene
03/27/23 12:220.0050.0005<0.0005mg/Kgtert-Butyl benzene
03/27/23 12:220.0050.0006<0.0006mg/KgCarbon Disulfide
03/27/23 12:220.0050.001<0.001mg/KgCarbon Tetrachloride
03/27/23 12:220.0050.0007<0.0007mg/KgChlorobenzene
03/27/23 12:220.0050.0009<0.0009mg/KgChlorodibromomethane
03/27/23 12:220.0100.0009<0.0009mg/KgChloroethane
03/27/23 12:220.0050.001<0.001mg/KgChloroform
03/27/23 12:220.0100.0006<0.0006mg/KgChloromethane
03/27/23 12:220.0050.0005<0.0005mg/Kg2-Chlorotoluene
03/27/23 12:220.0050.0004<0.0004mg/Kg4-Chlorotoluene
03/27/23 12:220.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/27/23 12:220.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
03/27/23 12:220.0050.0006<0.0006mg/Kg1,2-Dibromoethane
03/27/23 12:220.0050.0010<0.0010mg/KgDibromomethane
03/27/23 12:220.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
03/27/23 12:220.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 10 of 39Date:04/03/2023 02:47 PM
Page 86 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31293QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31292
Associated Lab Samples: 91772
LRB-V31292 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/23 12:220.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/27/23 12:220.0100.001<0.001mg/KgDichlorodifluoromethane
03/27/23 12:220.0050.0008<0.0008mg/Kg1,1-Dichloroethane
03/27/23 12:220.0050.001<0.001mg/Kg1,2-Dichloroethane
03/27/23 12:220.0050.0007<0.0007mg/Kg1,1-Dichloroethene
03/27/23 12:220.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/27/23 12:220.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
03/27/23 12:220.0050.0004<0.0004mg/Kg1,2-Dichloropropane
03/27/23 12:220.0050.0006<0.0006mg/Kg1,3-Dichloropropane
03/27/23 12:220.0050.001<0.001mg/Kg2,2-Dichloropropane
03/27/23 12:220.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/27/23 12:220.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/27/23 12:220.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
03/27/23 12:220.2500.014<0.014mg/KgEthanol
03/27/23 12:220.0050.0006<0.0006mg/KgEthylbenzene
03/27/23 12:220.1000.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/27/23 12:220.0100.0008<0.0008mg/KgHexachlorobutadiene
03/27/23 12:220.0100.0007<0.0007mg/Kgn-Hexane
03/27/23 12:220.0200.0006<0.0006mg/Kg2-Hexanone
03/27/23 12:220.0050.0005<0.0005mg/KgIsopropylbenzene
03/27/23 12:220.0050.001<0.001mg/Kg4-Isopropyl toluene
03/27/23 12:220.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
03/27/23 12:220.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
03/27/23 12:220.0050.0010.001mg/KgMethylene Chloride
03/27/23 12:220.0100.0010<0.0010mg/KgNaphthalene
03/27/23 12:220.0050.0005<0.0005mg/Kgn-Propylbenzene
03/27/23 12:220.0050.001<0.001mg/KgStyrene
Page 11 of 39Date:04/03/2023 02:47 PM
Page 87 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31293QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31292
Associated Lab Samples: 91772
LRB-V31292 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/23 12:220.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
03/27/23 12:220.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
03/27/23 12:220.0050.0009<0.0009mg/KgTetrachloroethene
03/27/23 12:220.0050.0007<0.0007mg/KgToluene
03/27/23 12:220.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
03/27/23 12:220.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
03/27/23 12:220.0050.001<0.001mg/Kg1,1,1-Trichloroethane
03/27/23 12:220.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/27/23 12:220.0050.0009<0.0009mg/KgTrichloroethene
03/27/23 12:220.0100.002<0.002mg/KgTrichlorofluoromethane
03/27/23 12:220.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
03/27/23 12:220.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
03/27/23 12:220.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
03/27/23 12:220.0100.0005<0.0005mg/KgVinyl Acetate
03/27/23 12:220.0100.0005<0.0005mg/KgVinyl Chloride
03/27/23 12:220.0050.0005<0.0005mg/Kgo-Xylene
03/27/23 12:220.0100.001<0.001mg/Kgm,p-Xylene
03/27/23 12:224-Bromofluorobenzene (S)100 70-130
03/27/23 12:22Dibromofluoromethane (S)100 70-130
03/27/23 12:22Toluene-d8 (S)99.0 76-129
LCS-V31292 LCSD-V31292Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.067 67.474.20.0740.100mg/KgAcetone 29-198 9.6 20
0.099 99.11130.1130.100mg/KgAcrolein 70-130 13.1 20
Page 12 of 39Date:04/03/2023 02:47 PM
Page 88 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31293QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31292
LCS-V31292 LCSD-V31292Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.105 1051040.1040.100mg/KgAcrylonitrile 65-134 0.9 20
0.050 1001020.0510.050mg/KgBenzene 74-127 1.9 20
0.050 1021000.0500.050mg/KgBromobenzene 73-125 1.7 20
0.049 99.21020.0510.050mg/KgBromochloromethane 72-134 2.7 20
0.050 1021020.0510.050mg/KgBromodichloromethane 75-122 0.1 20
0.049 99.21020.0500.050mg/KgBromoform 66-135 2.3 20
0.052 1061190.0590.050mg/KgBromomethane 20-180 11.4 20
0.051 1041040.0520.050mg/Kgn-Butylbenzene 65-135 0.5 20
0.050 1021040.0510.050mg/Kgsec-Butyl benzene 66-131 1.7 20
0.050 1001040.0520.050mg/Kgtert-Butyl benzene 67-132 3.5 20
0.049 99.41020.0500.050mg/KgCarbon Disulfide 61-129 2.1 20
0.048 97.21060.0520.050mg/KgCarbon Tetrachloride 64-143 8.2 20
0.053 1081070.0530.050mg/KgChlorobenzene 74-118 0.1 20
0.050 1011030.0510.050mg/KgChlorodibromomethane 73-122 1.9 20
0.059 1181250.0620.050mg/KgChloroethane 33-149 5.7 20
0.050 1001040.0520.050mg/KgChloroform 73-127 3.9 20
0.046 93.898.40.0490.050mg/KgChloromethane 45-143 4.7 20
0.051 1021020.0510.050mg/Kg2-Chlorotoluene 67-124 0.1 20
0.051 1021020.0510.050mg/Kg4-Chlorotoluene 71-126 0.1 20
0.048 97.497.80.0480.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.4 20
0.045 91.897.80.0480.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.3 20
0.052 1041070.0530.050mg/Kg1,2-Dibromoethane 70-132 2.2 20
0.048 96.21060.0530.050mg/KgDibromomethane 74-133 9.8 20
0.051 1031030.0510.050mg/Kg1,2-Dichlorobenzene 72-123 0.1 20
0.051 1031050.0520.050mg/Kg1,3-Dichlorobenzene 71-120 2.1 20
0.050 1011010.0500.050mg/Kg1,4-Dichlorobenzene 71-123 0.5 20
Page 13 of 39Date:04/03/2023 02:47 PM
Page 89 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31293QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31292
LCS-V31292 LCSD-V31292Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1001060.0530.050mg/KgDichlorodifluoromethane 26-146 5.8 20
0.049 98.21020.0500.050mg/Kg1,1-Dichloroethane 74-127 3.6 20
0.049 98.299.00.0490.050mg/Kg1,2-Dichloroethane 68-128 0.8 20
0.048 96.097.80.0480.050mg/Kg1,1-Dichloroethene 67-149 1.8 20
0.049 99.499.60.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 0.2 20
0.048 96.499.60.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.2 20
0.049 98.01010.0500.050mg/Kg1,2-Dichloropropane 73-130 3.4 20
0.049 98.81010.0500.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.049 99.41020.0510.050mg/Kg2,2-Dichloropropane 50-142 2.7 20
0.048 97.61030.0510.050mg/Kg1,1-Dichloropropene 71-130 5.3 20
0.050 1011050.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 4.0 20
0.052 1051040.0520.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.1 20
1.17 93.691.21.141.25mg/KgEthanol 70-130 2.5 20
0.050 1011040.0510.050mg/KgEthylbenzene 74-128 2.9 20
0.098 98.199.50.0990.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.4 20
0.055 1101050.0520.050mg/KgHexachlorobutadiene 64-125 5.0 20
0.048 97.61100.0550.050mg/Kgn-Hexane 70-130 12.3 20
0.041 83.286.80.0430.050mg/Kg2-Hexanone 61-157 4.2 20
0.050 1011020.0510.050mg/KgIsopropylbenzene 68-126 1.3 20
0.050 1021050.0520.050mg/Kg4-Isopropyl toluene 68-129 3.2 20
0.045 90.892.00.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.3 20
0.048 96.697.20.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.6 20
0.043 86.689.00.0440.050mg/KgMethylene Chloride 74-129 2.7 20
0.046 92.094.60.0470.050mg/KgNaphthalene 57-157 2.7 20
0.050 1011030.0510.050mg/Kgn-Propylbenzene 67-130 1.3 20
0.051 1031060.0520.050mg/KgStyrene 77-121 2.2 20
Page 14 of 39Date:04/03/2023 02:47 PM
Page 90 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31293QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31292
LCS-V31292 LCSD-V31292Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1051070.0530.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.8 20
0.046 93.694.00.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.4 20
0.051 1021090.0540.050mg/KgTetrachloroethene 68-130 6.8 20
0.049 98.21010.0500.050mg/KgToluene 71-129 2.6 20
0.048 96.495.60.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.8 20
0.052 1041040.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.0 20
0.050 1021050.0520.050mg/Kg1,1,1-Trichloroethane 67-131 3.2 20
0.048 96.898.60.0490.050mg/Kg1,1,2-Trichloroethane 70-133 1.8 20
0.051 1031050.0520.050mg/KgTrichloroethene 75-133 2.1 20
0.054 1091120.0560.050mg/KgTrichlorofluoromethane 44-146 3.0 20
0.047 94.499.80.0490.050mg/Kg1,2,3-Trichloropropane 60-137 5.5 20
0.050 1021030.0510.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.1 20
0.050 1021050.0520.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.9 20
0.056 1121130.0560.050mg/KgVinyl Acetate 60-140 0.7 20
0.048 97.21020.0500.050mg/KgVinyl Chloride 48-147 4.6 20
0.051 1021050.0520.050mg/Kgo-Xylene 74-126 2.3 20
0.101 1011040.1040.100mg/Kgm,p-Xylene 75-124 2.9 20
10298.64-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)70-130
101101Toluene-d8 (S)76-129
Page 15 of 39Date:04/03/2023 02:47 PM
Page 91 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31301QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31299
Associated Lab Samples: 91771
LRB-V31299 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/23 12:220.0200.002<0.002mg/KgAcetone
03/27/23 12:220.0200.001<0.001mg/KgAcrolein
03/27/23 12:220.0200.0008<0.0008mg/KgAcrylonitrile
03/27/23 12:220.0050.0006<0.0006mg/KgBenzene
03/27/23 12:220.0050.0005<0.0005mg/KgBromobenzene
03/27/23 12:220.0050.0008<0.0008mg/KgBromochloromethane
03/27/23 12:220.0050.001<0.001mg/KgBromodichloromethane
03/27/23 12:220.0050.001<0.001mg/KgBromoform
03/27/23 12:220.0100.001<0.001mg/KgBromomethane
03/27/23 12:220.0050.0005<0.0005mg/Kgn-Butylbenzene
03/27/23 12:220.0050.0006<0.0006mg/Kgsec-Butyl benzene
03/27/23 12:220.0050.0005<0.0005mg/Kgtert-Butyl benzene
03/27/23 12:220.0050.0006<0.0006mg/KgCarbon Disulfide
03/27/23 12:220.0050.001<0.001mg/KgCarbon Tetrachloride
03/27/23 12:220.0050.0007<0.0007mg/KgChlorobenzene
03/27/23 12:220.0050.0009<0.0009mg/KgChlorodibromomethane
03/27/23 12:220.0100.0009<0.0009mg/KgChloroethane
03/27/23 12:220.0050.001<0.001mg/KgChloroform
03/27/23 12:220.0100.0006<0.0006mg/KgChloromethane
03/27/23 12:220.0050.0005<0.0005mg/Kg2-Chlorotoluene
03/27/23 12:220.0050.0004<0.0004mg/Kg4-Chlorotoluene
03/27/23 12:220.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/27/23 12:220.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
03/27/23 12:220.0050.0006<0.0006mg/Kg1,2-Dibromoethane
03/27/23 12:220.0050.0006<0.0006mg/KgDibromomethane
03/27/23 12:220.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
03/27/23 12:220.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 16 of 39Date:04/03/2023 02:47 PM
Page 92 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31301QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31299
Associated Lab Samples: 91771
LRB-V31299 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/23 12:220.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/27/23 12:220.0100.001<0.001mg/KgDichlorodifluoromethane
03/27/23 12:220.0050.0008<0.0008mg/Kg1,1-Dichloroethane
03/27/23 12:220.0050.001<0.001mg/Kg1,2-Dichloroethane
03/27/23 12:220.0050.0007<0.0007mg/Kg1,1-Dichloroethene
03/27/23 12:220.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/27/23 12:220.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
03/27/23 12:220.0050.0004<0.0004mg/Kg1,2-Dichloropropane
03/27/23 12:220.0050.0006<0.0006mg/Kg1,3-Dichloropropane
03/27/23 12:220.0050.001<0.001mg/Kg2,2-Dichloropropane
03/27/23 12:220.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/27/23 12:220.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/27/23 12:220.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
03/27/23 12:220.2500.014<0.014mg/KgEthanol
03/27/23 12:220.0050.0006<0.0006mg/KgEthylbenzene
03/27/23 12:220.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/27/23 12:220.0100.0008<0.0008mg/KgHexachlorobutadiene
03/27/23 12:220.0100.0007<0.0007mg/Kgn-Hexane
03/27/23 12:220.0200.0006<0.0006mg/Kg2-Hexanone
03/27/23 12:220.0050.0005<0.0005mg/KgIsopropylbenzene
03/27/23 12:220.0050.001<0.001mg/Kg4-Isopropyl toluene
03/27/23 12:220.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
03/27/23 12:220.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
03/27/23 12:220.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/27/23 12:220.0100.0010.001mg/KgMethylene Chloride
03/27/23 12:220.0100.0010<0.0010mg/KgNaphthalene
03/27/23 12:220.0050.0005<0.0005mg/Kgn-Propylbenzene
Page 17 of 39Date:04/03/2023 02:47 PM
Page 93 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31301QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31299
Associated Lab Samples: 91771
LRB-V31299 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/27/23 12:220.0050.001<0.001mg/KgStyrene
03/27/23 12:220.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
03/27/23 12:220.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
03/27/23 12:220.0050.0009<0.0009mg/KgTetrachloroethene
03/27/23 12:220.0050.0007<0.0007mg/KgToluene
03/27/23 12:220.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
03/27/23 12:220.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
03/27/23 12:220.0050.001<0.001mg/Kg1,1,1-Trichloroethane
03/27/23 12:220.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/27/23 12:220.0050.0009<0.0009mg/KgTrichloroethene
03/27/23 12:220.0100.002<0.002mg/KgTrichlorofluoromethane
03/27/23 12:220.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
03/27/23 12:220.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
03/27/23 12:220.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
03/27/23 12:220.0100.0005<0.0005mg/KgVinyl Acetate
03/27/23 12:220.0100.0005<0.0005mg/KgVinyl Chloride
03/27/23 12:220.0050.0005<0.0005mg/Kgo-Xylene
03/27/23 12:220.0100.001<0.001mg/Kgm,p-Xylene
03/27/23 12:224-Bromofluorobenzene (S)100 70-130
03/27/23 12:22Dibromofluoromethane (S)100 84-123
03/27/23 12:22Toluene-d8 (S)99.0 76-129
LCS-V31299 LCSD-V31299Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.067 67.474.20.0740.100mg/KgAcetone 29-198 9.6 20
Page 18 of 39Date:04/03/2023 02:47 PM
Page 94 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31301QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31299
LCS-V31299 LCSD-V31299Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.099 99.11130.1130.100mg/KgAcrolein 70-130 13.1 20
0.105 1051040.1040.100mg/KgAcrylonitrile 65-134 0.9 20
0.050 1001020.0510.050mg/KgBenzene 74-127 1.9 20
0.050 1021000.0500.050mg/KgBromobenzene 73-125 1.7 20
0.049 99.21020.0510.050mg/KgBromochloromethane 72-134 2.7 20
0.050 1021020.0510.050mg/KgBromodichloromethane 75-122 0.1 20
0.049 99.21020.0500.050mg/KgBromoform 66-135 2.3 20
0.052 1061190.0590.050mg/KgBromomethane 20-180 11.4 20
0.051 1041040.0520.050mg/Kgn-Butylbenzene 65-135 0.5 20
0.050 1021040.0510.050mg/Kgsec-Butyl benzene 66-131 1.7 20
0.050 1001040.0520.050mg/Kgtert-Butyl benzene 67-132 3.5 20
0.049 99.41020.0500.050mg/KgCarbon Disulfide 61-129 2.1 20
0.048 97.21060.0520.050mg/KgCarbon Tetrachloride 64-143 8.2 20
0.053 1081070.0530.050mg/KgChlorobenzene 74-118 0.1 20
0.050 1011030.0510.050mg/KgChlorodibromomethane 73-122 1.9 20
0.059 1181250.0620.050mg/KgChloroethane 33-149 5.7 20
0.050 1001040.0520.050mg/KgChloroform 73-127 3.9 20
0.046 93.898.40.0490.050mg/KgChloromethane 45-143 4.7 20
0.051 1021020.0510.050mg/Kg2-Chlorotoluene 67-124 0.1 20
0.051 1021020.0510.050mg/Kg4-Chlorotoluene 71-126 0.1 20
0.048 97.497.80.0480.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.4 20
0.045 91.897.80.0480.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.3 20
0.052 1041070.0530.050mg/Kg1,2-Dibromoethane 70-132 2.2 20
0.048 96.21060.0530.050mg/KgDibromomethane 74-133 9.8 20
0.051 1031030.0510.050mg/Kg1,2-Dichlorobenzene 72-123 0.1 20
0.051 1031050.0520.050mg/Kg1,3-Dichlorobenzene 71-120 2.1 20
Page 19 of 39Date:04/03/2023 02:47 PM
Page 95 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31301QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31299
LCS-V31299 LCSD-V31299Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1011010.0500.050mg/Kg1,4-Dichlorobenzene 71-123 0.5 20
0.050 1001060.0530.050mg/KgDichlorodifluoromethane 26-146 5.8 20
0.049 98.21020.0500.050mg/Kg1,1-Dichloroethane 74-127 3.6 20
0.049 98.299.00.0490.050mg/Kg1,2-Dichloroethane 68-128 0.8 20
0.048 96.097.80.0480.050mg/Kg1,1-Dichloroethene 67-149 1.8 20
0.049 99.499.60.0490.050mg/Kgcis-1,2-Dichloroethene 76-134 0.2 20
0.048 96.499.60.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.2 20
0.049 98.01010.0500.050mg/Kg1,2-Dichloropropane 73-130 3.4 20
0.049 98.81010.0500.050mg/Kg1,3-Dichloropropane 75-124 1.8 20
0.049 99.41020.0510.050mg/Kg2,2-Dichloropropane 50-142 2.7 20
0.048 97.61030.0510.050mg/Kg1,1-Dichloropropene 71-130 5.3 20
0.050 1011050.0520.050mg/Kgcis-1,3-Dichloropropene 71-125 4.0 20
0.052 1051040.0520.050mg/Kgtrans-1,3-Dichloropropene 68-123 0.1 20
1.17 93.691.21.141.25mg/KgEthanol 70-130 2.5 20
0.050 1011040.0510.050mg/KgEthylbenzene 74-128 2.9 20
0.098 98.199.50.0990.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.4 20
0.055 1101050.0520.050mg/KgHexachlorobutadiene 64-125 5.0 20
0.048 97.61100.0550.050mg/Kgn-Hexane 70-130 12.3 20
0.041 83.286.80.0430.050mg/Kg2-Hexanone 61-157 4.2 20
0.050 1011020.0510.050mg/KgIsopropylbenzene 68-126 1.3 20
0.050 1021050.0520.050mg/Kg4-Isopropyl toluene 68-129 3.2 20
0.045 90.892.00.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 1.3 20
0.048 96.697.20.0480.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.6 20
0.050 1001040.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 4.1 20
0.043 86.689.00.0440.050mg/KgMethylene Chloride 74-129 2.7 20
0.046 92.094.60.0470.050mg/KgNaphthalene 57-157 2.7 20
Page 20 of 39Date:04/03/2023 02:47 PM
Page 96 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V31301QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V31299
LCS-V31299 LCSD-V31299Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1011030.0510.050mg/Kgn-Propylbenzene 67-130 1.3 20
0.051 1031060.0520.050mg/KgStyrene 77-121 2.2 20
0.052 1051070.0530.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 1.8 20
0.046 93.694.00.0470.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 0.4 20
0.051 1021090.0540.050mg/KgTetrachloroethene 68-130 6.8 20
0.049 98.21010.0500.050mg/KgToluene 71-129 2.6 20
0.048 96.495.60.0470.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.8 20
0.052 1041040.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.0 20
0.050 1021050.0520.050mg/Kg1,1,1-Trichloroethane 67-131 3.2 20
0.048 96.898.60.0490.050mg/Kg1,1,2-Trichloroethane 70-133 1.8 20
0.051 1031050.0520.050mg/KgTrichloroethene 75-133 2.1 20
0.054 1091120.0560.050mg/KgTrichlorofluoromethane 44-146 3.0 20
0.047 94.499.80.0490.050mg/Kg1,2,3-Trichloropropane 60-137 5.5 20
0.050 1021030.0510.050mg/Kg1,2,4-Trimethylbenzene 69-129 1.1 20
0.050 1021050.0520.050mg/Kg1,3,5-Trimethylbenzene 69-128 2.9 20
0.056 1121130.0560.050mg/KgVinyl Acetate 60-140 0.7 20
0.048 97.21020.0500.050mg/KgVinyl Chloride 48-147 4.6 20
0.051 1021050.0520.050mg/Kgo-Xylene 74-126 2.3 20
0.101 1011040.1040.100mg/Kgm,p-Xylene 75-124 2.9 20
10298.64-Bromofluorobenzene (S)70-130
101101Dibromofluoromethane (S)84-123
101101Toluene-d8 (S)76-129
Page 21 of 39Date:04/03/2023 02:47 PM
Page 97 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
Associated Lab Samples: 91771, 91772, 91773, 91774, 91775, 91776
LRB-V31133 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/23 10:180.6610.116<0.116mg/KgAcenaphthene
03/26/23 10:180.6610.105<0.105mg/KgAcenaphthylene
03/26/23 10:180.6610.152<0.152mg/KgAniline
03/26/23 10:180.6610.143<0.143mg/KgAnthracene
03/26/23 10:180.6610.139<0.139mg/KgBenzo(a)anthracene
03/26/23 10:180.6610.147<0.147mg/KgBenzo(a)pyrene
03/26/23 10:180.6610.146<0.146mg/KgBenzo(b)fluoranthene
03/26/23 10:180.6610.136<0.136mg/KgBenzo(g,h,i)perylene
03/26/23 10:180.6610.137<0.137mg/KgBenzo(k)fluoranthene
03/26/23 10:182.000.580<0.580mg/KgBenzoic Acid
03/26/23 10:180.6610.105<0.105mg/KgBenzyl alcohol
03/26/23 10:180.6610.118<0.118mg/KgBis(2-Chloroethoxy)methane
03/26/23 10:180.6610.107<0.107mg/KgBis(2-Chloroethyl)ether
03/26/23 10:180.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
03/26/23 10:180.6610.120<0.120mg/KgBis(2-ethylhexyl)phthalate
03/26/23 10:180.6610.109<0.109mg/Kg4-Bromophenyl phenyl ether
03/26/23 10:180.3300.113<0.113mg/KgButyl benzyl phthalate
03/26/23 10:180.6610.092<0.092mg/Kg4-Chloro-3-methylphenol
03/26/23 10:180.3300.112<0.112mg/Kg4-Chloroaniline
03/26/23 10:180.6610.116<0.116mg/Kg2-Chloronaphthalene
03/26/23 10:180.6610.098<0.098mg/Kg2-Chlorophenol
03/26/23 10:181.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
03/26/23 10:180.6610.142<0.142mg/KgChrysene
03/26/23 10:180.6610.230<0.230mg/KgDibenz(a,h)anthracene
03/26/23 10:180.6610.119<0.119mg/KgDibenzofuran
03/26/23 10:180.6610.094<0.094mg/Kg1,2-Dichlorobenzene
03/26/23 10:180.6610.097<0.097mg/Kg1,3-Dichlorobenzene
Page 22 of 39Date:04/03/2023 02:47 PM
Page 98 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
Associated Lab Samples: 91771, 91772, 91773, 91774, 91775, 91776
LRB-V31133 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/23 10:180.3300.097<0.097mg/Kg1,4-Dichlorobenzene
03/26/23 10:180.6610.147<0.147mg/Kg3,3'-Dichlorobenzidine
03/26/23 10:180.6610.095<0.095mg/Kg2,4-Dichlorophenol
03/26/23 10:180.6610.180<0.180mg/KgDiethyl phthalate
03/26/23 10:180.6610.174<0.174mg/KgDimethyl phthalate
03/26/23 10:180.3300.108<0.108mg/Kg2,4-Dimethylphenol
03/26/23 10:180.6610.107<0.107mg/KgDi-n-butyl phthalate
03/26/23 10:181.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
03/26/23 10:181.500.520<0.520mg/Kg2,4-Dinitrophenol
03/26/23 10:180.6610.096<0.096mg/Kg2,4-Dinitrotoluene
03/26/23 10:180.6610.108<0.108mg/Kg2,6-Dinitrotoluene
03/26/23 10:180.3300.143<0.143mg/KgDi-n-Octyl Phthalate
03/26/23 10:180.6610.123<0.123mg/KgFluoranthene
03/26/23 10:180.6610.128<0.128mg/KgFluorene
03/26/23 10:180.6610.106<0.106mg/KgHexachlorobenzene
03/26/23 10:180.6610.097<0.097mg/KgHexachlorobutadiene
03/26/23 10:180.6610.157<0.157mg/KgHexachlorocyclopentadiene
03/26/23 10:180.6610.079<0.079mg/KgHexachloroethane
03/26/23 10:180.6610.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
03/26/23 10:180.6610.191<0.191mg/KgIsophorone
03/26/23 10:180.6610.106<0.106mg/Kg1-Methylnaphthalene
03/26/23 10:180.6610.100<0.100mg/Kg2-Methylnaphthalene
03/26/23 10:180.6610.097<0.097mg/Kg2-Methylphenol
03/26/23 10:180.6610.085<0.085mg/Kg3&4 Methylphenol
03/26/23 10:180.6610.144<0.144mg/KgNaphthalene
03/26/23 10:180.6610.096<0.096mg/Kg2-Nitroaniline
03/26/23 10:180.6610.120<0.120mg/Kg3-Nitroaniline
Page 23 of 39Date:04/03/2023 02:47 PM
Page 99 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
Associated Lab Samples: 91771, 91772, 91773, 91774, 91775, 91776
LRB-V31133 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/26/23 10:180.3300.093<0.093mg/Kg4-Nitroaniline
03/26/23 10:180.3300.116<0.116mg/KgNitrobenzene
03/26/23 10:180.6610.088<0.088mg/Kg2-Nitrophenol
03/26/23 10:180.6610.117<0.117mg/Kg4-Nitrophenol
03/26/23 10:180.6610.263<0.263mg/KgN-Nitrosodimethylamine
03/26/23 10:180.6610.181<0.181mg/KgN-Nitrosodiphenylamine
03/26/23 10:180.6610.118<0.118mg/KgN-Nitroso-di-n-propylamine
03/26/23 10:181.000.347<0.347mg/KgPentachlorophenol
03/26/23 10:180.6610.208<0.208mg/KgPhenanthrene
03/26/23 10:180.6610.112<0.112mg/KgPhenol
03/26/23 10:180.6610.134<0.134mg/KgPyrene
03/26/23 10:180.3300.079<0.079mg/KgPyridine
03/26/23 10:180.6610.107<0.107mg/Kg1,2,4-Trichlorobenzene
03/26/23 10:180.6610.096<0.096mg/Kg2,4,5-Trichlorophenol
03/26/23 10:180.6610.096<0.096mg/Kg2,4,6-Trichlorophenol
03/26/23 10:182-Fluorobiphenyl (S)95.8 44-115
03/26/23 10:182-Fluorophenol (S)82.3 35-115
03/26/23 10:18Nitrobenzene-d5 (S)89.2 37-122
03/26/23 10:184-Terphenyl-d14 (S)102 54-127
03/26/23 10:182,4,6-Tribromophenol (S)62.8 39-132
03/26/23 10:18Phenol-d5 (S)74.2 34-121
LCS-V31133Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.31.551.66mg/KgAcenaphthene 40-123
96.31.601.66mg/KgAcenaphthylene 32-132
Page 24 of 39Date:04/03/2023 02:47 PM
Page 100 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
LCS-V31133Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1662.751.66mg/KgAniline 12-197
1041.721.66mg/KgAnthracene 47-123
95.11.581.66mg/KgBenzo(a)anthracene 49-126
1071.771.66mg/KgBenzo(a)pyrene 45-129
94.51.571.66mg/KgBenzo(b)fluoranthene 45-132
90.31.501.66mg/KgBenzo(g,h,i)perylene 43-134
99.31.651.66mg/KgBenzo(k)fluoranthene 47-132
38.60.6421.66mg/KgBenzoic Acid 10-83
94.51.571.66mg/KgBenzyl alcohol 29-122
95.71.591.66mg/KgBis(2-Chloroethoxy)methane 36-121
86.71.441.66mg/KgBis(2-Chloroethyl)ether 31-120
85.51.421.66mg/KgBis(2-Chloroisopropyl)ether 33-131
1101.821.66mg/KgBis(2-ethylhexyl)phthalate 51-133
93.31.551.66mg/Kg4-Bromophenyl phenyl ether 46-124
1191.971.66mg/KgButyl benzyl phthalate 48-132
91.51.521.66mg/Kg4-Chloro-3-methylphenol 45-122
1041.721.66mg/Kg4-Chloroaniline 17-106
95.71.591.66mg/Kg2-Chloronaphthalene 41-114
90.91.511.66mg/Kg2-Chlorophenol 34-121
90.31.501.66mg/Kg4-Chlorophenyl phenyl ether 45-121
95.71.591.66mg/KgChrysene 50-124
93.91.561.66mg/KgDibenz(a,h)anthracene 45-134
93.31.551.66mg/KgDibenzofuran 44-120
84.31.401.66mg/Kg1,2-Dichlorobenzene 33-117
82.51.371.66mg/Kg1,3-Dichlorobenzene 30-115
81.91.361.66mg/Kg1,4-Dichlorobenzene 31-115
84.91.411.66mg/Kg3,3'-Dichlorobenzidine 22-121
Page 25 of 39Date:04/03/2023 02:47 PM
Page 101 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
LCS-V31133Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
93.91.561.66mg/Kg2,4-Dichlorophenol 40-122
95.11.581.66mg/KgDiethyl phthalate 50-124
94.51.571.66mg/KgDimethyl phthalate 48-124
127*2.111.66mg/Kg2,4-Dimethylphenol 30-127
1131.881.66mg/KgDi-n-butyl phthalate 51-128
88.51.471.66mg/Kg4,6-Dinitro-2-methylphenol 29-132
75.91.261.66mg/Kg2,4-Dinitrophenol 27-129
95.11.581.66mg/Kg2,4-Dinitrotoluene 48-126
93.91.561.66mg/Kg2,6-Dinitrotoluene 46-124
1161.931.66mg/KgDi-n-Octyl Phthalate 45-140
91.51.521.66mg/KgFluoranthene 50-127
95.11.581.66mg/KgFluorene 43-125
84.91.411.66mg/KgHexachlorobenzene 45-122
87.91.461.66mg/KgHexachlorobutadiene 32-123
86.11.431.66mg/KgHexachlorocyclopentadiene 32-117
83.71.391.66mg/KgHexachloroethane 28-117
89.71.491.66mg/KgIndeno(1,2,3-cd)pyrene 45-133
84.91.411.66mg/KgIsophorone 30-122
87.91.461.66mg/Kg1-Methylnaphthalene 40-119
88.51.471.66mg/Kg2-Methylnaphthalene 38-122
93.31.551.66mg/Kg2-Methylphenol 32-122
83.11.381.66mg/Kg3&4 Methylphenol 34-119
92.71.541.66mg/KgNaphthalene 35-123
95.11.581.66mg/Kg2-Nitroaniline 44-127
95.11.581.66mg/Kg3-Nitroaniline 33-119
1091.811.66mg/Kg4-Nitroaniline 63-147
87.31.451.66mg/KgNitrobenzene 34-122
Page 26 of 39* QC Fail Date:04/03/2023 02:47 PM
Page 102 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
LCS-V31133Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.51.471.66mg/Kg2-Nitrophenol 36-123
1011.671.66mg/Kg4-Nitrophenol 30-132
69.81.161.66mg/KgN-Nitrosodimethylamine 10-146
1191.981.66mg/KgN-Nitrosodiphenylamine 38-127
89.11.481.66mg/KgN-Nitroso-di-n-propylamine 36-120
90.91.511.66mg/KgPentachlorophenol 25-133
1011.671.66mg/KgPhenanthrene 50-121
76.51.271.66mg/KgPhenol 34-121
1001.661.66mg/KgPyrene 47-127
46.90.7801.66mg/KgPyridine 10-80
87.91.461.66mg/Kg1,2,4-Trichlorobenzene 34-118
90.31.501.66mg/Kg2,4,5-Trichlorophenol 41-124
89.71.491.66mg/Kg2,4,6-Trichlorophenol 39-126
1012-Fluorobiphenyl (S)44-115
85.52-Fluorophenol (S)35-115
89.1Nitrobenzene-d5 (S)37-122
1004-Terphenyl-d14 (S)54-127
67.22,4,6-Tribromophenol (S)39-132
78.0Phenol-d5 (S)34-121
V 91691-MS-V31133 V 91691-MSD-V31133Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.47 88.51.521.671.66<0.116mg/KgAcenaphthene 91.0 40-123 3.3 20
1.52 91.51.561.671.66<0.105mg/KgAcenaphthylene 93.4 32-132 2.5 20
2.57 1552.701.671.66<0.152mg/KgAniline 162 12-197 4.9 20
Page 27 of 39Date:04/03/2023 02:47 PM
Page 103 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
V 91691-MS-V31133 V 91691-MSD-V31133Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.68 1011.651.671.66<0.143mg/KgAnthracene 98.8 47-123 1.8 20
1.58 95.11.611.671.66<0.139mg/KgBenzo(a)anthracene 96.4 49-126 1.8 20
1.69 1021.751.671.66<0.147mg/KgBenzo(a)pyrene 105 45-129 3.4 20
1.57 94.51.581.671.66<0.146mg/KgBenzo(b)fluoranthene 94.6 45-132 0.6 20
1.43 86.11.471.671.66<0.136mg/KgBenzo(g,h,i)perylene 88.0 43-134 2.7 20
1.59 95.71.631.671.66<0.137mg/KgBenzo(k)fluoranthene 97.6 47-132 2.4 20
0.657 39.50.6591.671.66<0.580mg/KgBenzoic Acid 39.4 10-83 0.3 20
1.38 83.11.501.671.66<0.105mg/KgBenzyl alcohol 89.8 29-122 8.3 20
1.45 87.31.531.671.66<0.118mg/KgBis(2-Chloroethoxy)methane 91.6 36-121 5.3 20
1.30 78.31.351.671.66<0.107mg/KgBis(2-Chloroethyl)ether 80.8 31-120 3.7 20
1.23 74.01.341.671.66<0.136mg/KgBis(2-Chloroisopropyl)ether 80.2 33-131 8.5 20
1.78 1071.821.671.66<0.120mg/KgBis(2-ethylhexyl)phthalate 109 51-133 2.2 20
1.47 88.51.501.671.66<0.109mg/Kg4-Bromophenyl phenyl ether 89.8 46-124 2.0 20
1.89 1141.921.671.66<0.113mg/KgButyl benzyl phthalate 115 48-132 1.5 20
1.46 87.91.491.671.66<0.092mg/Kg4-Chloro-3-methylphenol 89.2 45-122 2.0 20
1.61 96.91.721.671.66<0.112mg/Kg4-Chloroaniline 103 17-106 6.6 20
1.49 89.71.541.671.66<0.116mg/Kg2-Chloronaphthalene 92.2 41-114 3.3 20
1.35 81.31.431.671.66<0.098mg/Kg2-Chlorophenol 85.6 34-121 5.7 20
1.45 87.31.481.671.66<0.126mg/Kg4-Chlorophenyl phenyl ether 88.6 45-121 2.0 20
1.56 93.91.561.671.66<0.142mg/KgChrysene 93.4 50-124 0.0 20
1.50 90.31.541.671.66<0.230mg/KgDibenz(a,h)anthracene 92.2 45-134 2.6 20
1.48 89.11.531.671.66<0.119mg/KgDibenzofuran 91.6 44-120 3.3 20
1.25 75.31.301.671.66<0.094mg/Kg1,2-Dichlorobenzene 77.8 33-117 3.9 20
1.22 73.41.301.671.66<0.097mg/Kg1,3-Dichlorobenzene 77.8 30-115 6.3 20
1.24 74.61.291.671.66<0.097mg/Kg1,4-Dichlorobenzene 77.2 31-115 3.9 20
1.33 80.11.321.671.66<0.147mg/Kg3,3'-Dichlorobenzidine 79.0 22-121 0.7 20
Page 28 of 39Date:04/03/2023 02:47 PM
Page 104 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
V 91691-MS-V31133 V 91691-MSD-V31133Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.48 89.11.561.671.66<0.095mg/Kg2,4-Dichlorophenol 93.4 40-122 5.2 20
1.55 93.31.571.671.66<0.180mg/KgDiethyl phthalate 94.0 50-124 1.2 20
1.52 91.51.551.671.66<0.174mg/KgDimethyl phthalate 92.8 48-124 1.9 30
1.86 1121.931.671.66<0.108mg/Kg2,4-Dimethylphenol 116 30-127 3.6 20
1.80 1081.801.671.66<0.107mg/KgDi-n-butyl phthalate 108 51-128 0.0 20
1.41 84.91.481.671.66<0.240mg/Kg4,6-Dinitro-2-methylphenol 88.6 29-132 4.8 20
1.18 71.01.231.671.66<0.520mg/Kg2,4-Dinitrophenol 73.6 27-129 4.1 20
1.53 92.11.551.671.66<0.096mg/Kg2,4-Dinitrotoluene 92.8 48-126 1.2 20
1.53 92.11.531.671.66<0.108mg/Kg2,6-Dinitrotoluene 91.6 46-124 0.0 20
1.86 1121.901.671.66<0.143mg/KgDi-n-Octyl Phthalate 114 45-140 2.1 20
1.50 90.31.491.671.66<0.123mg/KgFluoranthene 89.2 50-127 0.6 20
1.52 91.51.551.671.66<0.128mg/KgFluorene 92.8 43-125 1.9 20
1.34 80.71.401.671.66<0.106mg/KgHexachlorobenzene 83.8 45-122 4.3 20
1.32 79.51.451.671.66<0.097mg/KgHexachlorobutadiene 86.8 32-123 9.3 20
1.39 83.71.461.671.66<0.157mg/KgHexachlorocyclopentadiene 87.4 32-117 4.9 20
1.22 73.41.261.671.66<0.079mg/KgHexachloroethane 75.4 28-117 3.2 20
1.43 86.11.481.671.66<0.179mg/KgIndeno(1,2,3-cd)pyrene 88.6 45-133 3.4 20
1.31 78.91.381.671.66<0.191mg/KgIsophorone 82.6 30-122 5.2 20
1.34 80.71.421.671.66<0.106mg/Kg1-Methylnaphthalene 85.0 40-119 5.7 20
1.33 80.11.441.671.66<0.100mg/Kg2-Methylnaphthalene 86.2 38-122 7.9 20
1.41 84.91.441.671.66<0.097mg/Kg2-Methylphenol 86.2 32-122 2.1 20
1.25 75.31.311.671.66<0.084mg/Kg3&4 Methylphenol 78.4 34-119 4.6 20
1.37 82.51.461.671.66<0.144mg/KgNaphthalene 87.4 35-123 6.3 20
1.48 89.11.491.671.66<0.096mg/Kg2-Nitroaniline 89.2 44-127 0.6 20
1.48 89.11.491.671.66<0.120mg/Kg3-Nitroaniline 89.2 33-119 0.6 20
1.69 1021.721.671.66<0.093mg/Kg4-Nitroaniline 103 63-147 1.7 20
Page 29 of 39Date:04/03/2023 02:47 PM
Page 105 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31392QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31133
V 91691-MS-V31133 V 91691-MSD-V31133Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.32 79.51.421.671.66<0.116mg/KgNitrobenzene 85.0 34-122 7.2 20
1.30 78.31.411.671.66<0.088mg/Kg2-Nitrophenol 84.4 32-123 8.1 20
1.58 95.11.591.671.66<0.117mg/Kg4-Nitrophenol 95.2 30-132 0.6 20
1.01 60.81.081.671.66<0.263mg/KgN-Nitrosodimethylamine 64.6 10-146 6.6 30
1.84 1111.871.671.66<0.181mg/KgN-Nitrosodiphenylamine 112 38-127 1.6 20
1.34 80.71.401.671.66<0.118mg/KgN-Nitroso-di-n-propylamine 83.8 36-120 4.3 20
1.48 89.11.561.671.66<0.347mg/KgPentachlorophenol 93.4 25-133 5.2 20
1.58 95.11.611.671.66<0.208mg/KgPhenanthrene 96.4 50-121 1.8 20
1.26 75.91.301.671.66<0.112mg/KgPhenol 77.8 34-121 3.1 20
1.67 1011.671.671.66<0.134mg/KgPyrene 100 47-127 0.0 20
0.958 57.70.9811.671.66<0.079mg/KgPyridine 58.7 10-80 2.3 20
1.28 77.11.381.671.66<0.107mg/Kg1,2,4-Trichlorobenzene 82.6 34-118 7.5 20
1.44 86.71.481.671.66<0.096mg/Kg2,4,5-Trichlorophenol 88.6 41-124 2.7 20
1.43 86.11.441.671.66<0.096mg/Kg2,4,6-Trichlorophenol 86.2 39-126 0.6 20
93.32-Fluorobiphenyl (S)95.8 44-115
75.32-Fluorophenol (S)79.3 35-115
79.5Nitrobenzene-d5 (S)84.4 37-122
97.54-Terphenyl-d14 (S)100 54-127
64.22,4,6-Tribromophenol (S)67.0 39-132
70.5Phenol-d5 (S)72.7 34-121
Page 30 of 39Date:04/03/2023 02:47 PM
Page 106 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31269
Associated Lab Samples: 91777, 91778
LRB-V31269 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/28/23 16:470.6600.116<0.116mg/KgAcenaphthene
03/28/23 16:470.6600.105<0.105mg/KgAcenaphthylene
03/28/23 16:470.6600.152<0.152mg/KgAniline
03/28/23 16:470.6600.143<0.143mg/KgAnthracene
03/28/23 16:470.6600.139<0.139mg/KgBenzo(a)anthracene
03/28/23 16:470.6600.147<0.147mg/KgBenzo(a)pyrene
03/28/23 16:470.6600.146<0.146mg/KgBenzo(b)fluoranthene
03/28/23 16:470.6600.136<0.136mg/KgBenzo(g,h,i)perylene
03/28/23 16:470.6600.137<0.137mg/KgBenzo(k)fluoranthene
03/28/23 16:472.000.580<0.580mg/KgBenzoic Acid
03/28/23 16:470.6600.105<0.105mg/KgBenzyl alcohol
03/28/23 16:470.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
03/28/23 16:470.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
03/28/23 16:470.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
03/28/23 16:470.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
03/28/23 16:470.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
03/28/23 16:470.3300.113<0.113mg/KgButyl benzyl phthalate
03/28/23 16:470.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
03/28/23 16:470.3300.112<0.112mg/Kg4-Chloroaniline
03/28/23 16:470.6600.116<0.116mg/Kg2-Chloronaphthalene
03/28/23 16:470.6600.098<0.098mg/Kg2-Chlorophenol
03/28/23 16:471.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
03/28/23 16:470.6600.142<0.142mg/KgChrysene
03/28/23 16:470.6600.230<0.230mg/KgDibenz(a,h)anthracene
03/28/23 16:470.6600.119<0.119mg/KgDibenzofuran
03/28/23 16:470.6600.094<0.094mg/Kg1,2-Dichlorobenzene
03/28/23 16:470.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 31 of 39Date:04/03/2023 02:47 PM
Page 107 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31269
Associated Lab Samples: 91777, 91778
LRB-V31269 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/28/23 16:470.3300.097<0.097mg/Kg1,4-Dichlorobenzene
03/28/23 16:470.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
03/28/23 16:470.6600.095<0.095mg/Kg2,4-Dichlorophenol
03/28/23 16:470.6600.180<0.180mg/KgDiethyl phthalate
03/28/23 16:470.6600.174<0.174mg/KgDimethyl phthalate
03/28/23 16:470.3300.108<0.108mg/Kg2,4-Dimethylphenol
03/28/23 16:470.6600.107<0.107mg/KgDi-n-butyl phthalate
03/28/23 16:471.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
03/28/23 16:471.500.520<0.520mg/Kg2,4-Dinitrophenol
03/28/23 16:470.6600.096<0.096mg/Kg2,4-Dinitrotoluene
03/28/23 16:470.6600.108<0.108mg/Kg2,6-Dinitrotoluene
03/28/23 16:470.3300.143<0.143mg/KgDi-n-Octyl Phthalate
03/28/23 16:470.6600.123<0.123mg/KgFluoranthene
03/28/23 16:470.6600.128<0.128mg/KgFluorene
03/28/23 16:470.6600.106<0.106mg/KgHexachlorobenzene
03/28/23 16:470.6600.097<0.097mg/KgHexachlorobutadiene
03/28/23 16:470.6600.157<0.157mg/KgHexachlorocyclopentadiene
03/28/23 16:470.6600.079<0.079mg/KgHexachloroethane
03/28/23 16:470.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
03/28/23 16:470.6600.191<0.191mg/KgIsophorone
03/28/23 16:470.6600.106<0.106mg/Kg1-Methylnaphthalene
03/28/23 16:470.6600.100<0.100mg/Kg2-Methylnaphthalene
03/28/23 16:470.6600.097<0.097mg/Kg2-Methylphenol
03/28/23 16:470.6600.084<0.084mg/Kg3&4 Methylphenol
03/28/23 16:470.6600.144<0.144mg/KgNaphthalene
03/28/23 16:470.6600.096<0.096mg/Kg2-Nitroaniline
03/28/23 16:470.6600.120<0.120mg/Kg3-Nitroaniline
Page 32 of 39Date:04/03/2023 02:47 PM
Page 108 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31269
Associated Lab Samples: 91777, 91778
LRB-V31269 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/28/23 16:470.3300.093<0.093mg/Kg4-Nitroaniline
03/28/23 16:470.3300.116<0.116mg/KgNitrobenzene
03/28/23 16:470.6600.088<0.088mg/Kg2-Nitrophenol
03/28/23 16:470.6600.117<0.117mg/Kg4-Nitrophenol
03/28/23 16:470.6600.263<0.263mg/KgN-Nitrosodimethylamine
03/28/23 16:470.6600.181<0.181mg/KgN-Nitrosodiphenylamine
03/28/23 16:470.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
03/28/23 16:471.000.347<0.347mg/KgPentachlorophenol
03/28/23 16:470.6600.208<0.208mg/KgPhenanthrene
03/28/23 16:470.6600.112<0.112mg/KgPhenol
03/28/23 16:470.6600.134<0.134mg/KgPyrene
03/28/23 16:470.3300.079<0.079mg/KgPyridine
03/28/23 16:470.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
03/28/23 16:470.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
03/28/23 16:470.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
03/28/23 16:472-Fluorobiphenyl (S)101 44-115
03/28/23 16:472-Fluorophenol (S)86.4 35-115
03/28/23 16:47Nitrobenzene-d5 (S)91.0 37-122
03/28/23 16:474-Terphenyl-d14 (S)116 54-127
03/28/23 16:472,4,6-Tribromophenol (S)80.4 39-132
03/28/23 16:47Phenol-d5 (S)79.2 34-121
LCS-V31269 LCSD-V31269Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.66 99.495.21.591.67mg/KgAcenaphthene 40-123 4.3 20
Page 33 of 39Date:04/03/2023 02:47 PM
Page 109 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31269
LCS-V31269 LCSD-V31269Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.72 10397.61.631.67mg/KgAcenaphthylene 32-132 5.3 20
2.91 1741602.681.67mg/KgAniline 12-197 8.2 20
2.03 1221041.731.67mg/KgAnthracene 47-123 15.9 20
1.81 1081051.761.67mg/KgBenzo(a)anthracene 49-126 2.8 20
1.94 1161141.901.67mg/KgBenzo(a)pyrene 45-129 2.0 20
1.78 1071031.721.67mg/KgBenzo(b)fluoranthene 45-132 3.4 20
1.69 10199.41.661.67mg/KgBenzo(g,h,i)perylene 43-134 1.7 20
1.82 1091021.701.67mg/KgBenzo(k)fluoranthene 47-132 6.8 20
1.38 82.676.61.281.67mg/KgBenzoic Acid 10-83 7.5 20
1.60 95.889.21.491.67mg/KgBenzyl alcohol 29-122 7.1 20
1.66 99.494.01.571.67mg/KgBis(2-Chloroethoxy)methane 36-121 5.5 20
1.44 86.280.81.351.67mg/KgBis(2-Chloroethyl)ether 31-120 6.4 20
1.45 86.880.81.351.67mg/KgBis(2-Chloroisopropyl)ether 33-131 7.1 20
1.91 1141131.881.67mg/KgBis(2-ethylhexyl)phthalate 51-133 1.5 20
1.68 10197.01.621.67mg/Kg4-Bromophenyl phenyl ether 46-124 3.6 20
1.99 1191131.891.67mg/KgButyl benzyl phthalate 48-132 5.1 20
1.67 10096.41.611.67mg/Kg4-Chloro-3-methylphenol 45-122 3.6 20
1.66 99.494.61.581.67mg/Kg4-Chloroaniline 17-106 4.9 20
1.68 10196.41.611.67mg/Kg2-Chloronaphthalene 41-114 4.2 20
1.53 91.684.41.411.67mg/Kg2-Chlorophenol 34-121 8.1 20
1.70 10296.41.611.67mg/Kg4-Chlorophenyl phenyl ether 45-121 5.4 20
1.76 1051021.701.67mg/KgChrysene 50-124 3.4 20
1.80 1081051.751.67mg/KgDibenz(a,h)anthracene 45-134 2.8 20
1.70 10294.61.581.67mg/KgDibenzofuran 44-120 7.3 20
1.43 85.679.01.321.67mg/Kg1,2-Dichlorobenzene 33-117 8.0 20
1.41 84.477.81.301.67mg/Kg1,3-Dichlorobenzene 30-115 8.1 20
Page 34 of 39Date:04/03/2023 02:47 PM
Page 110 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31269
LCS-V31269 LCSD-V31269Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.41 84.477.81.301.67mg/Kg1,4-Dichlorobenzene 31-115 8.1 20
1.36 81.476.61.281.67mg/Kg3,3'-Dichlorobenzidine 22-121 6.0 20
1.67 10095.81.601.67mg/Kg2,4-Dichlorophenol 40-122 4.2 20
1.77 1061021.701.67mg/KgDiethyl phthalate 50-124 4.0 20
1.79 1071021.701.67mg/KgDimethyl phthalate 48-124 5.1 20
2.22 133*129*2.161.67mg/Kg2,4-Dimethylphenol 30-127 2.7 20
1.99 1191161.931.67mg/KgDi-n-butyl phthalate 51-128 3.0 20
1.58 94.694.01.571.67mg/Kg4,6-Dinitro-2-methylphenol 29-132 0.6 20
1.46 87.485.61.431.67mg/Kg2,4-Dinitrophenol 27-129 2.0 20
1.78 1071011.681.67mg/Kg2,4-Dinitrotoluene 48-126 5.7 20
1.70 10295.81.601.67mg/Kg2,6-Dinitrotoluene 46-124 6.0 20
2.01 1201171.961.67mg/KgDi-n-Octyl Phthalate 45-140 2.5 20
1.67 10098.21.641.67mg/KgFluoranthene 50-127 1.8 20
1.78 10797.61.631.67mg/KgFluorene 43-125 8.7 20
1.59 95.291.61.531.67mg/KgHexachlorobenzene 45-122 3.8 20
1.58 94.691.61.531.67mg/KgHexachlorobutadiene 32-123 3.2 20
1.60 95.889.21.491.67mg/KgHexachlorocyclopentadiene 32-117 7.1 20
1.43 85.677.81.301.67mg/KgHexachloroethane 28-117 9.5 20
1.72 1031011.681.67mg/KgIndeno(1,2,3-cd)pyrene 45-133 2.3 20
1.51 90.485.61.431.67mg/KgIsophorone 30-122 5.4 20
1.51 90.486.81.451.67mg/Kg1-Methylnaphthalene 40-119 4.0 20
1.58 94.685.61.431.67mg/Kg2-Methylnaphthalene 38-122 9.9 20
1.57 94.086.21.441.67mg/Kg2-Methylphenol 32-122 8.6 20
1.41 84.478.41.311.67mg/Kg3&4 Methylphenol 34-119 7.3 20
1.78 10788.61.481.67mg/KgNaphthalene 35-123 18.4 20
1.43 85.681.41.361.67mg/Kg2-Nitroaniline 44-127 5.0 20
Page 35 of 39* QC Fail Date:04/03/2023 02:47 PM
Page 111 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V31378QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V31269
LCS-V31269 LCSD-V31269Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
1.43 85.681.41.361.67mg/Kg3-Nitroaniline 33-119 5.0 20
1.93 1161091.821.67mg/Kg4-Nitroaniline 63-147 5.8 20
1.50 89.885.01.421.67mg/KgNitrobenzene 34-122 5.4 20
1.51 90.485.61.431.67mg/Kg2-Nitrophenol 36-123 5.4 20
1.93 1161131.881.67mg/Kg4-Nitrophenol 30-132 2.6 20
1.01 60.468.21.141.67mg/KgN-Nitrosodimethylamine 10-146 12.0 20
2.06 1231171.961.67mg/KgN-Nitrosodiphenylamine 38-127 4.9 20
1.53 91.684.41.411.67mg/KgN-Nitroso-di-n-propylamine 36-120 8.1 20
1.93 1161081.801.67mg/KgPentachlorophenol 25-133 6.9 20
1.83 1101001.671.67mg/KgPhenanthrene 50-121 9.1 20
1.49 89.283.21.391.67mg/KgPhenol 34-121 6.9 20
1.83 1101041.731.67mg/KgPyrene 47-127 5.6 20
0.831 49.747.00.7861.67mg/KgPyridine 10-80 5.5 20
1.51 90.485.01.421.67mg/Kg1,2,4-Trichlorobenzene 34-118 6.1 20
1.72 10397.61.631.67mg/Kg2,4,5-Trichlorophenol 41-124 5.3 20
1.66 99.493.41.561.67mg/Kg2,4,6-Trichlorophenol 39-126 6.2 20
1051042-Fluorobiphenyl (S)44-115
87.382.82-Fluorophenol (S)35-115
90.490.4Nitrobenzene-d5 (S)37-122
1151164-Terphenyl-d14 (S)54-127
81.081.62,4,6-Tribromophenol (S)39-132
80.776.8Phenol-d5 (S)34-121
Page 36 of 39Date:04/03/2023 02:47 PM
Page 112 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
QC Prep Batch Method:
Hexavalent Chromium by Ion Chromatography
SW-7199
L672114QC Analytical Batch(es):
Analysis Method:
Analysis Description:
SW-3060A
QC Prep:L671902
Associated Lab Samples: 91771, 91772, 91773, 91774, 91775, 91776, 91777, 91778
LRB-L671902 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
03/27/23 15:050.2000.141<0.141mg/KgChromium, Hexavalent
LCS-L671902Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
97.53.904.00mg/KgChromium, Hexavalent 80-120
V 91691-DUP-L671902Duplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/27/23 15:4167.5*0.5110.253mg/KgChromium, Hexavalent
V 91691-MS-L671902Matrix Spike
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
20.2 49.8*40.0< 1.41mg/KgChromium, Hexavalent 75-125
Page 37 of 39* QC Fail Date:04/03/2023 02:47 PM
Page 113 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
Dry Weight Determination
SW-DRYWT
V31239QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91526-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/27/23 15:043.95.995.76%Moisture
V 91534-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/27/23 15:040.76.756.70%Moisture
Page 38 of 39Date:04/03/2023 02:47 PM
Page 114 of 117
Quality Control Data
23-080-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
AKR-007
Dry Weight Determination
SW-DRYWT
V31240QC Analytical Batch:
Analysis Method:
Analysis Description:
V 91768-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/27/23 15:511.519.219.5%Moisture
V 91869-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/27/23 15:510.518.818.7%Moisture
Page 39 of 39Date:04/03/2023 02:47 PM
Page 115 of 117
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-080-0013
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 3.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Paula Blakeborough Date & Time:03/21/2023 15:14:34
Special precautions or instructions included?
Comments:
Page 116 of 117
Waypoint.9
ANALYTICAL
Site Location Name: 4'. ort..<,I • • ~.
Site Location Physical Address:AL-
CLIENT
SAMPLE DESCRIPTION
DATE
COLLECTED
TIME
COLLECTED
MILITARY
HOURS
(Yto-O
,,~r;-
1JLtS-
l ~ JS'"
t'foo
MATRIX
(SOIL,
WATER,OR
SLUDGE)
CHAIN OF CUSTODY RECORD
PAGE j_ OF -L QUOTE# TO ENSURE PROPER BILLING: _______ I
Project Name: 5". /./vdl. -t ;/r-tl,·s ;l,/
Short Hold Analysis (Yes) , @j UST Project: ~ (No)
*Please ATTACH any project specific reporting (QC LEVEL 111111 IV)
prov!sions and/or QC Require':1Js )Ju 11• 1
Invoice To: Mt~? {J rfn•'cAwi/.r>,/n,..,
Address=--------------------1
Purchase Order No./Billing Reference /r/4P.,-oor
Requested Due Date a 1 Day a 2 Days a 3 Days a 4 Days b's Days
"Working Days" a 6-9 Days a Standard 10 days a Rush~ Must Be Pre Approved Samples received after 15:00 will be processed next business day.
Turnaround time is based on business days, excluding weekends and holidays.
{SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES
RENDERED BY WAYPOINT ANALYTICAL, LLC TO CLIENT)
SAMPLE CONTAINER
"TYPE
SEE BELOW NO.
PRESERVA-
TIVES
Affiliation /h-J.J
Samples INTACT upon arrival? '1 NO N/A
Received IN ICE? 4-
PROPER PRESERVATIVES indicated? ..J-Received WITHIN HOLDING TIMES? L __ __
CUSTODY SEALS INTACT? ~
VOLATILES rec'd W/OUT HEADSPACE? __ __ _.;/_
PROPER CONTAINERS used? ...;
TEMP: Therm ID::r:(tt-ts-Observed 3-:-cf:c ~~c
TO BE FILLED IN BY CLIENT/SAMPLING PERSONNEL
Certification: Nc_J(_ SC __
Other __ N/A, __ _
Water Chlorinated: YES_ N0-6...
Samples Iced Upon Collection: YEs)L_No_
/ /
~; ~ N
s~~ -,J,,11)
N 0o .--~ ---~ --c:,, -la:: ~-~~
-~~ -~ ~ -l:ffi -.oz:, ~t: 'S -:l<il
D",MARKS ID NO.
Date I Mllllary/Hours Additional Comments: Site Departure Time:
Date ~ Plei-.-.e. IY:.ro r 1-Field Tech Fee:
~ T>1.µL(TFl~5~). ReUnquislled By: {Signature) ~ .
~ ·2 · 2 - ,
Mileage:
Metnod of Shipment: NOTE: ALL SAMPLE COOLERS SHOULD BE TAPED UT WITH CUSTO S FOR TRANSPORTATION TO THE LABORATORY. COC Group No.
SAMPLES ARE NOT ACCEPTED AND VERIFIED AGAINST COC UNTIL RECEIVED AT THE LABORATORY.
o Fed Ex a UPS a Hancklelr.oered a Waypoint Analytical Field Service a Other.
NPDES: I UST: --I GROUNDWATER:! DRINKING WATER: I SOLID-WASTE: I RCRA: I BRWNFLD I LANDFILL I OTHER:
0 NCO SC Cl NC O SC O NC O SC O NC O SC O NC O SC O NC O SC O NC O SC O NC O SC O NC O SC a ___ o ___ o ___ o ______ o _____ o ___ o ___ o ___ o __ _
*CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon-Lined Cap VOA = Volatile Organics Analysis (Zero Head Space)
SEE REVERSE FOR
TERMS & CONDITIONS
ORIGINAL
Page 117 of 117

Appendix E

Republic Services Weight Tickets
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959531Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/22/23 8:50 am 3/22/23 8:50 am
2203860
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 46,020
25,260 20,760
10.38 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 10.38
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959557Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/22/23 9:27 am 3/22/23 9:27 am
2203861
MT22
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 46,040
29,500 16,540
8.27 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 8.27
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959631Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/22/23 11:14 am 3/22/23 11:14 am
2203802
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 51,080
25,260 25,820
12.91 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.91
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959676Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/22/23 12:29 pm 3/22/23 12:29 pm
2203803
MT22
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 64,280
29,500 34,780
17.39 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 17.39
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959722Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/22/23 1:36 pm 3/22/23 1:36 pm
2203804
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 48,520
25,260 23,260
11.63 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.63
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959793Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/22/23 4:06 pm 3/22/23 4:06 pm
2203805
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 48,000
25,260 22,740
11.37 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.37
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959890Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 8:49 am 3/23/23 8:49 am
2203806
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 44,540
25,260 19,280
9.64 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 9.64
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959915Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 9:33 am 3/23/23 9:33 am
2203807
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 56,420
25,020 31,400
15.70 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.70
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959930Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 9:51 am 3/23/23 9:51 am
2203808
SHO54
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 50,660
23,980 26,680
13.34 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.34
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959948Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 10:11 am 3/23/23 10:11 am
2203809
SHO51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 46,260
30,520 15,740
7.87 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 7.87
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959967Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 10:51 am 3/23/23 10:51 am
2203810
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 59,660
25,260 34,400
17.20 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 17.20
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1959995Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 11:27 am 3/23/23 11:27 am
2203811
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 54,200
25,020 29,180
14.59 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.59
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960016Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 12:01 pm 3/23/23 12:01 pm
2203812
SHO51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 53,020
30,520 22,500
11.25 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.25
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960025Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 12:15 pm 3/23/23 12:15 pm
2203813
SHO54
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,260
23,980 31,280
15.64 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.64
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960076Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 1:24 pm 3/23/23 1:24 pm
2203815
ASH3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 64,240
27,560 36,680
18.34 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 18.34
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960092Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 1:41 pm 3/23/23 1:41 pm
2203814
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 62,500
25,260 37,240
18.62 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 18.62
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960094Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 1:48 pm 3/23/23 1:48 pm
2203816
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 56,460
25,020 31,440
15.72 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.72
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960098Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 1:52 pm 3/23/23 1:52 pm
2203818
SHO51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 46,300
30,520 15,780
7.89 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 7.89
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960112Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 2:08 pm 3/23/23 2:08 pm
2203817
SHO54
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 49,080
23,980 25,100
12.55 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.55
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960177Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 4:15 pm 3/23/23 4:15 pm
2203820
ASH3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 71,480
27,560 43,920
21.96 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 21.96
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960188Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/23/23 4:37 pm 3/23/23 4:37 pm
2203821
SHO51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 42,680
30,520 12,160
6.08 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 6.08
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1960229Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
3/24/23 7:22 am 3/24/23 7:22 am
2203819
mt36
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 59,680
25,260 34,420
17.21 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 17.21
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1962819Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/5/23 9:02 am 4/5/23 9:02 am
2203822
BR3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 52,000
26,520 25,480
12.74 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.74
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1962847Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/5/23 9:33 am 4/5/23 9:58 am
2203825
BRock1
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 52,840
24,940 27,900
13.95 INBOUND
INVOICE
Scale In
Scale Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.95
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1962881Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/5/23 11:01 am 4/5/23 11:01 am
2203823
BR3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 53,540
26,520 27,020
13.51 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.51
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1962899Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/5/23 11:36 am 4/5/23 11:36 am
2203826
BRock1
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,200
24,940 30,260
15.13 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.13
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1962966Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/5/23 2:03 pm 4/5/23 2:03 pm
2203824
BR3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 53,640
26,520 27,120
13.56 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.56
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1962997Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/5/23 2:59 pm 4/5/23 2:59 pm
2203827
BRock1
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,020
24,940 30,080
15.04 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.04
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1963114Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/6/23 9:01 am 4/6/23 9:01 am
2203830
ST704
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 50,100
25,340 24,760
12.38 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.38
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1963131Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/6/23 9:32 am 4/6/23 9:32 am
2203834
scs01
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 54,300
27,180 27,120
13.56 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.56
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1963208Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/6/23 12:10 pm 4/6/23 12:10 pm
2203833
ST704
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 63,140
25,340 37,800
18.90 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 18.90
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1963255Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/6/23 1:31 pm 4/6/23 1:31 pm
2203832
scs01
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 61,780
27,180 34,600
17.30 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 17.30
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1963314Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/6/23 3:11 pm 4/6/23 3:11 pm
2203831
ST704
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,240
25,340 29,900
14.95 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.95
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1963337Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
4/6/23 4:00 pm 4/6/23 4:00 pm
2203829
scs01
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 60,380
27,180 33,200
16.60 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 16.60
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968397Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 9:22 am 5/4/23 9:35 am
2203841
MT18
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 60,580
26,360 34,220
17.11 INBOUND
INVOICE
Scale In
Scale Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 17.11
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968407Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 9:36 am 5/4/23 9:54 am
2203840
Ash5
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 51,380
24,520 26,860
13.43 INBOUND
INVOICE
Scale In
Scale Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.43
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968414Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 10:03 am 5/4/23 10:03 am
2203839
MT48
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 59,480
29,220 30,260
15.13 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.13
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968460Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 11:41 am 5/4/23 11:41 am
2203838
MT18
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 49,020
26,360 22,660
11.33 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.33
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968491Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 12:33 pm 5/4/23 12:33 pm
2203837
Ash5
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 50,320
24,520 25,800
12.90 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.90
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968495Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 12:49 pm 5/4/23 12:49 pm
2203836
MT48
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 57,560
29,220 28,340
14.17 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.17
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968530Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 2:00 pm 5/4/23 2:00 pm
2203835
MT18
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 48,360
26,360 22,000
11.00 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.00
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968553Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 3:00 pm 5/4/23 3:00 pm
2203859
MT48
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 56,480
29,220 27,260
13.63 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.63
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1968573Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/4/23 3:59 pm 5/4/23 3:59 pm
2203858
Ash5
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 45,900
24,520 21,380
10.69 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 10.69
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973568Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 9:02 am 5/30/23 9:02 am
2203853
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 47,980
25,020 22,960
11.48 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.48
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973589Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 9:57 am 5/30/23 9:57 am
2203856
MT61
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 56,260
25,040 31,220
15.61 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.61
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973621Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 10:43 am 5/30/23 11:00 am
2203852
PC51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,600
26,700 28,900
14.45 INBOUND
INVOICE
Scale In
Scale Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.45
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973629Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 11:38 am 5/30/23 11:38 am
2203854
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 51,180
25,020 26,160
13.08 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.08
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973657Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 12:18 pm 5/30/23 12:18 pm
2203850
PC51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 54,920
26,700 28,220
14.11 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.11
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973674Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 1:01 pm 5/30/23 1:01 pm
2203855
MT61
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 49,340
25,040 24,300
12.15 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.15
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973701Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 2:26 pm 5/30/23 2:26 pm
2203842
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 47,420
25,020 22,400
11.20 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.20
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973731Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/30/23 4:10 pm 5/30/23 4:10 pm
2203851
PC51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 54,820
26,700 28,120
14.06 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.06
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973823Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/31/23 9:28 am 5/31/23 9:28 am
2195076
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 53,040
25,020 28,020
14.01 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.01
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973855Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/31/23 10:28 am 5/31/23 10:42 am
2195077
MT8
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 54,880
25,400 29,480
14.74 INBOUND
INVOICE
Scale In
Scale Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.74
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973886Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/31/23 11:32 am 5/31/23 11:32 am
2195081
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 54,340
25,020 29,320
14.66 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.66
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973908Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/31/23 12:28 pm 5/31/23 12:28 pm
2195080
MT8
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 51,060
25,400 25,660
12.83 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.83
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973956Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/31/23 2:32 pm 5/31/23 2:32 pm
2195079
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 44,640
25,020 19,620
9.81 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 9.81
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1973973Y6
Candie E.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
5/31/23 3:34 pm 5/31/23 3:34 pm
2195078
MT8
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 49,240
25,400 23,840
11.92 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.92
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974065Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/1/23 9:26 am 6/1/23 9:26 am
2195083
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 61,480
25,020 36,460
18.23 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 18.23
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974097Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/1/23 10:20 am 6/1/23 10:20 am
2195082
PC51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,480
26,700 28,780
14.39 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.39
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974142Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/1/23 12:09 pm 6/1/23 12:09 pm
2195086
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 50,880
25,020 25,860
12.93 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.93
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974172Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/1/23 1:20 pm 6/1/23 1:20 pm
2195087
PC51
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,720
26,700 29,020
14.51 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 14.51
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974213Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/1/23 3:00 pm 6/1/23 3:00 pm
2195085
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,700
25,020 30,680
15.34 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.34
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974329Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/2/23 8:24 am 6/2/23 8:24 am
2195089
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 47,420
25,020 22,400
11.20 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.20
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974429Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/2/23 11:25 am 6/2/23 11:25 am
2195084
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 55,940
25,020 30,920
15.46 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 15.46
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1974540Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/2/23 3:36 pm 6/2/23 3:36 pm
2195090
MT47
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 50,020
25,020 25,000
12.50 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.50
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1975297Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/7/23 8:54 am 6/7/23 8:54 am
2195091
SHO54
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 41,740
23,980 17,760
8.88 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 8.88
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1975371Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/7/23 11:23 am 6/7/23 11:23 am
2195092
SHO54
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 49,020
23,980 25,040
12.52 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 12.52
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1975828Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/9/23 8:28 am 6/9/23 8:28 am
2195093
BR3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 48,160
26,520 21,640
10.82 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 10.82
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1975838Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/9/23 8:50 am 6/9/23 8:50 am
2195098
MT48
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 64,580
29,400 35,180
17.59 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 17.59
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1975900Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/9/23 10:54 am 6/9/23 10:54 am
2195094
MT48
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 57,220
29,400 27,820
13.91 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.91
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1975943Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/9/23 12:25 pm 6/9/23 12:25 pm
2195095
BR3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 52,760
26,520 26,240
13.12 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 13.12
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1976004Y6
Keri A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/9/23 2:31 pm 6/9/23 2:31 pm
2195097
MT48
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 62,780
29,400 33,380
16.69 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 16.69
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.
BFI/CMS LANDFILL 704-782-2004
5105 MOREHEAD RD CONCORD, NC 28025
REPRINT 1976018Y6
Lisa A.
000744 - SHOWALTER CONSTRUCTION - NO
FEES
P.O. BOX 220289
CHARLOTTE, NC 28222
6/9/23 3:10 pm 6/9/23 3:11 pm
2195096
BR3
Generator:KA LoSo Holdings LLC
Contract:5010220016
GROSS WEIGHT
TARE WEIGHT NET WEIGHT
NET TONS 48,800
26,520 22,280
11.14 INBOUND
INVOICE
Scale In
Tare Out
Tracking QTYYD 0.00
SW-CONT SOIL-ALT DAILY
COVER
tn Origin:MECKLENBURG 100% 11.14
CHANGE:
CHECK :
HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE
WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW
A SET FROM THE SCALE HOUSE. THANK YOU.