27011_Revels Esso_Phase II ESA 20210830_sealed

September 21, 2023

Mrs. Carolyn Minnich NCDEQ, DWM, Brownfields Redevelopment Section 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115

Reference: Report of Environmental Assessment Services
Graham and 6th Site
301 North Graham Street and 420 West 6th Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:13734-A

Mrs. Minnich:

On behalf of our client, Daniel Realty Company, LLC, ECS has prepared this sealed cover letter for the
above-referenced report. As such, I Scott Young, a Licensed Geologist for ECS Southeast, LLP, do certify
that the information contained in the referenced report is correct and accurate to the best of my
knowledge, and at the time of the completion of the report.

Respectfully,

ECS SOUTHEAST, LLP as represented by:

Scott Young, P.G. Joseph P. Nestor, P.G., P.E.
Senior Environmental Project Manager Environmental Principal
[e-mail] [e-mail]
704-525-5152 704-525-5152

August 30, 2021 Mr. Scott Wearren Daniel Realty Company, LLC 505 20th Street N, Suite 100 Birmingham, Alabama 35203 Reference: Report of Environmental Assessment Services Graham and 6th Site 301 North Graham Street and 420 West 6th Street Charlotte, Mecklenburg County, North Carolina ECS Project No. 49:13734-A Dear Mr. Wearren: ECS Southeast, LLP (ECS) is pleased to provide Daniel Realty Company, LLC with the results of our environmental assessment for the above-referenced site. ECS’s services were provided in accordance with ECS proposal No. 49:25356P authorized on August 2, 2021. ECS appreciates the opportunity to provide our services to you. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP
Scott Young, P.G. Joseph P. Nestor, P.G., P.E.
Environmental Project Manager Environmental Principal
[e-mail] [e-mail]
704-525-5152 704-280-7422
Report of Environmental Assessment Services
Graham and 6th Site
301 N. Graham St. and 420 W. 6th St.
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:13734-A
August 30, 2021

1
TABLE OF CONTENTS 1.0 PROJECT INFORMATION .................................................................................................................... 1
2.0 SCOPE OF SERVICES ............................................................................................................................ 2
2.1 Monitoring Well Permit ....................................................................................................................... 2
2.2 Utility Locate and GPR Survey ............................................................................................................. 2
2.3 Groundwater Sample Collection ......................................................................................................... 2
2.4 Soil Boring Activities ............................................................................................................................ 3
2.5 Soil Sample Collection ......................................................................................................................... 3
3.0 RESULTS .............................................................................................................................................. 3
3.1 Groundwater Samples Analytical Results............................................................................................ 3
3.2 Soil Samples Analytical Results............................................................................................................ 4
4.0 CONCLUSIONS .................................................................................................................................... 4
5.0 RECOMMENDATIONS ......................................................................................................................... 4
6.0 QUALIFICATIONS OF REPORT ............................................................................................................. 5
FIGURES Figure 1 USGS Topographic Map Figure 2 Sample Locations Map TABLES Table 1 Summary of Soil Samples Analytical Results Table 2 Summary of Groundwater Samples Analytical Results APPENDICES Appendix A NCDEQ Well Permit and Mecklenburg County SIP Information Appendix B Laboratory Analytical Report and Chain of Custody Record Appendix C Boring Logs and Construction/Abandonment Records Appendix D NCDEQ Risk Calculator Output
Report of Environmental Assessment Services
Graham and 6th Site
301 N. Graham St. and 420 W. 6th St.
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:13734-A
August 30, 2021

1
1.0 PROJECT INFORMATION

The subject property is located at 301 North Graham Street and 420 West 6th Street, Charlotte,
Mecklenburg County, North Carolina (Figure 1) and identified by Mecklenburg County GIS as Parcel
Identification Numbers 07806401 and 07806402 and is owned by Gerrard Family LLC & Mant Properties
LLC. The subject property is approximately 1.64 acres in size. The on-site buildings are reported as being
constructed in 1928 and 1950 and contain approximately 18,400 and 7,000 square feet of space,
respectively. The buildings were vacant at the time of the field reconnaissance, and formerly were used
as a tire service business. The buildings consisted of offices, warehouse space, service areas, and a
basement. The remaining portions of the subject property consisted of grassed and paved parking areas.
ECS previously conducted a Phase I Environmental Site Assessment (Phase I ESA) for the subject property
(ECS Project No. 49:13734, dated April 28, 2021). ECS noted the following Recognized Environmental
Conditions (RECs) in the Phase I ESA:
• ECS observed staining in the location of a former above ground storage tank (AST) that was
associated with the former auto service operations. ECS considered the potential for the observed
staining to impact the subject property to be a REC.
• ECS observed a potential former underground hydraulic lift that appeared to have been filled. ECS
considered the potential for the apparent former underground hydraulic lift to impact the subject
property to be a REC.
• ECS considered the potential for the reported former heating oil underground storage tank (UST)
at the subject property to impact the subject property to be a REC.
• ECS considered the historical use of the subject property as a gasoline station to be a REC based
on the potential for an undocumented release to impact the subject property.
• ECS considered the historical use of the subject property for auto repair and servicing to be a REC
based on the potential for an undocumented release to impact the subject property.
• ECS considered the historical use of the subject property as a junkyard to be a REC based on the
potential for an undocumented release to impact the subject property.
• ECS considered the Leaking Underground Storage Tank (LUST) incidents at surrounding and
upgradient properties to be RECs based on documented groundwater contamination, the inferred
direction of groundwater flow toward the subject property based on surface topography, and the
potential for contaminants to migrate and impact the subject property.
• ECS considered the surrounding, upgradient dry-cleaning and historical dry-cleaning facilities to
be RECs for the subject property based on the potential for undocumented releases of dry-
cleaning solvents from these facilities to migrate and impact the subject property.
• ECS considered the surrounding and upgradient historical auto stations to be RECs based on the
potential for undocumented releases to migrate and impact the subject property.

In an effort to determine if the subject property has been adversely affected by the identified RECs and
CREC, ECS was requested to conduct an environmental assessment of the site.

Report of Environmental Assessment Services
Graham and 6th Site
301 N. Graham St. and 420 W. 6th St.
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:13734-A
August 30, 2021

2
2.0 SCOPE OF SERVICES

The environmental assessment included the collection and laboratory analysis of soil and groundwater
samples. Drilling activities were conducted using a Geoprobe® Direct Push Technology (DPT) drill rig. The
drilling subcontractor used for this assessment was 3D Environmental Investigations, LLC (3D). Drilling
and sampling activities were conducted on August 16 and 17, 2021.

2.1 Monitoring Well Permit

Prior to conducting drilling activities, ECS obtained a monitoring well permit from the North Carolina
Department of Environmental Quality (NCDEQ). In addition, ECS obtained a Subsurface Investigation
Permit (SIP) from the Mecklenburg County Health Department. The NCDEQ well permit and Mecklenburg
County SIP information is included as Appendix A.

2.2 Utility Locate and GPR Survey

Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. Required separation distances between subsurface activities and marked utilities
(typically 30-inches) were maintained during the field activities. In addition, ECS contracted with KCI to
clear the boring areas of private utilities. KCI also conducted a ground penetrating radar (GPR) survey in
an attempt to locate the former fueling system components. The results of the GPR survey identified an
approximately eight feet by eight feet anomaly near the intersection of North Graham Street and West
6th Street. No metal was indicated; however, it is assumed a former UST may have been present in this
area. The approximate location of the anomaly is indicated on Figure 2.

2.3 Groundwater Sample Collection

ECS observed the advancement of 11 borings (GW-1 through GW-11) for the collection of groundwater
samples. The borings were advanced to depths ranging from 26 feet below ground surface (bgs) at boring
location GW-2 to 34 feet below ground surface at boring locations GW-1 and GW-3. The locations of
groundwater samples are shown on Figure 2.

The groundwater samples were collected using a groundwater sampling probe equipped with an
exposable stainless-steel screen and a peristaltic pump and dedicated tubing. At each sample point, the
groundwater sampling probe was advanced by DPT to a depth approximately 5 feet below the apparent
water table at the time of drilling. The hollow DPT rods were then extracted approximately 4 feet exposing
the screen.

The groundwater sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into a cooler with ice to
maintain the samples at approximately four degrees Celsius. The groundwater samples were submitted
to Pace Analytical Services, LLC (Pace), a North Carolina certified laboratory located in Huntersville, North
Carolina, for analysis for volatile organic compounds (VOCs) by EPA Method 8260 and semi-volatile
organic compounds (SVOCs) by EPA Method 8270. ECS maintained chain-of-custody (COC) procedures
Report of Environmental Assessment Services
Graham and 6th Site
301 N. Graham St. and 420 W. 6th St.
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:13734-A
August 30, 2021

3
throughout the sample collection and transportation process. A copy of the COC is included in Appendix
B.

Following the completion of the groundwater sampling activities, the groundwater sample locations were
abandoned by the North Carolina certified driller. Copies of the construction and abandonment records
are included in Appendix C.

2.4 Soil Boring Activities
Six soil borings (SB-1 through SB-6) were advanced at the site. The locations of the soil borings are
indicated on Figure 2.

The soil borings were advanced by hydraulically driving a five-foot long, 1.5-inch diameter soil sampling
probe into the soil to depths of 10 to 15 feet below the ground surface (bgs). The soil sampling probe was
lined with a dedicated disposable clear liner for each sampling interval. After the soil sampling probe was
driven, the liner filled with soil was removed from the probe and cut open to expose the soil. Soils were
collected continuously from the ground surface to the termination depth at each of the soil boring
locations. ECS visually classified the soil collected from each boring and screened the soils for evidence of
staining, odors, as well as relative levels of volatile organic vapors using a photoionization detector (PID).
Boring logs for each soil boring are included in Appendix C.

2.5 Soil Sample Collection

The soil samples from soil borings SS-1 through SS-6 were collected by a sampler from the liner retrieved
from the soil sample probe and placed directly into laboratory provided containers. The soil sample
selected from soil boring SS-1 was collected from the five to 10 feet bgs interval, and the soil samples
selected from soil borings SS-2 through SS-6 were collected from the 10 to 15 feet bgs intervals.

The soil sample containers were labeled with ECS project number, sample identification, sample date and
time, and requested analytical analysis. The containers were placed into a cooler with ice to maintain the
samples at approximately four degrees Celsius. The soil samples were submitted to Pace for analysis for
VOCs by EPA Method 8260 and SVOCs by EPA Method 8270. ECS maintained chain-of-custody (COC)
procedures throughout the sample collection and transportation process. A copy of the COC is included
in Appendix C.

3.0 RESULTS

3.1 Groundwater Samples Analytical Results

Review of the laboratory analytical results for the groundwater samples collected indicated
concentrations of benzene in the GW-8 and GW-9 groundwater samples greater than its North Carolina
2L Groundwater Quality Standards (NC2LGWQS) and Residential Groundwater Vapor Intrusion Screening
Level (VISL). Also, chloroform was detected in groundwater samples GW-1, GW-2, GW-3, GW-4, GW-6,
GW-7, GW-9, and GW-11 at concentrations greater than its Residential Groundwater VISL, with the
Report of Environmental Assessment Services
Graham and 6th Site
301 N. Graham St. and 420 W. 6th St.
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:13734-A
August 30, 2021

4
concentrations detected in the GW-3, GW-4, and GW-9 samples greater than its Non-Residential
Groundwater VISL. Concentrations of diisopropyl ether in the GW-8 groundwater sample and
naphthalene, toluene, and total xylenes in the GW-9 groundwater were detected greater than the
laboratory method reporting limits, but less than their respective NC2LGWQS and VISLs. Additional
compounds were not indicated at concentrations greater than the laboratory method reporting limits in
the eleven groundwater samples collected. The laboratory analytical results are summarized on Table 1.
A copy of the laboratory analytical report is included in Appendix B.

In light of the groundwater sample results, ECS input the laboratory analytical results of the GW-1, GW-2,
GW-3, GW-4, GW-6, GW-7, GW-9, and GW-11 groundwater samples in to the NCDEQ Risk Calculator.
Based on the results of the NCDEQ Risk Calculator, the concentrations detected in the samples did not
exceed the risk thresholds. Output from the results of the NCDEQ Risk Calculator are presented in
Appendix D.

3.2 Soil Samples Analytical Results

Review of the laboratory analytical results for the soil samples collected indicated a total of 11 compounds
in the SS-2 soil sample at concentrations greater than the laboratory method reporting limits, with the
concentrations of benzene, 1,2-dibromoethane, methylene chloride, and naphthalene greater than their
respective Protection of Groundwater Preliminary Soil Remediation Goals (PSRGs) and Soil-to-
Groundwater Maximum Soil Contaminant Concentrations (MSCCs). In addition, methylene chloride was
also detected in the SS-1, SS-3, SS-4, and SS-5 soil samples at concentrations greater than its Protection
of Groundwater PSRG and Soil-to-Water MSCC. It should be noted that methylene chloride is a common
laboratory contaminant. Additional compounds were not detected at concentrations greater than their
respective PSRGs or MSCCs. The soil sample analytical results are summarized on Table 2. A copy of the
laboratory analytical report is included in Appendix B.

4.0 CONCLUSIONS

Based on the results of the environmental assessment, ECS concludes the following:

• Groundwater and soil contamination were noted in the vicinity of the approximate former heating
oil UST location and the GPR survey anomaly.
• A reporting obligation may exist due to the detection of contaminants in soil and groundwater.
• Evidence of additional releases associated with the remaining RECs was not indicated in the soil
and groundwater samples collected as part of these assessment activities.

5.0 RECOMMENDATIONS

Based on the results of the environmental assessment, ECS recommends the following:

• ECS recommends that a copy of this report be maintained for your records.
• ECS recommends that a copy of this report be provided to the current property owner, and they
consult with an environmental attorney regarding potential reporting obligations.
Report of Environmental Assessment Services
Graham and 6th Site
301 N. Graham St. and 420 W. 6th St.
Charlotte, Mecklenburg County, North Carolina
ECS Project No. 49:13734-A
August 30, 2021

5
• ECS recommends conducting soil gas sampling near the former heating oil UST location and the
GPR survey anomaly and near the site structure to assess if vapors at the site are a risk.
• ECS does not recommend further sampling at this time for the additional previously mentioned
RECs.

6.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this environmental assessment are consistent with those normally employed in environmental soil and groundwater assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information determined during previous environmental assessments and the data obtained during our field activities. This report was prepared for the express use of Daniel Realty Company, LLC. Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract.

FIGURES

FIGURE 1USGS TOPOGRAPHIC MAP
GRAHAM AND 6th STREET SITE301 N GRAHAM ST & 420 W 6th STCHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:13734-A
SOURCE:
USGS 7.5’ TOPOGRAPHIC MAP
CHARLOTTE EAST, NC
2019
SCALE:
AS SHOWN
SITE
LOCATION
FIGURE 1PROPOSED SAMPLE LOCATIONS MAP
GRAHAM AND 6th STREET SITE301 N GRAHAM ST & 420 W 6th STCHARLOTTE, NORTH CAROLINA
ECS PROJECT NO. 49:13734-A
SOURCE:
MECKLENBURG COUNTY GIS WEBSITE
ACCESSED JULY 6, 2021
SCALE:
AS SHOWN
APPROXIMATE SITE BOUNDARY
LEGEND
APPROXIMATE SOIL SAMPLE LOCATION
APPROXIMATE GROUNDWATER BORING LOCATION
APPROXIMATE
FORMER AST
LOCATION
APPROXIMATE FORMER UNDERGROUND HYDRAULIC LIFT LOCATION
THE VUE (LUST –REC)
FORMER
DRYCLEANERS AND
FORMER GASOLINE
STATION (REC)
FORMER
HOLLAND
HOUSE
(LUST –REC)
FORMER EDEN CLEANERS (REC)FORMER GASOLINE STATION (REC)
FORMER
DRYCLEANER (REC)
APPROXIMATE FORMER HEATING OIL UST LOCATION
GW-1 GW-2
GW-3
GW-4
GW-5
GW-6
GW-7
SS-1/GW-8 SS-2/GW-9
SS-4/GW-10
SS-3
GW-11
SS-5
GPR ANOMALY

TABLES

Table 1
Summary of Groundwater Samples Analytical Results
Graham and 6th Site
301 North Graham Street and 420 West 6th Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:13734-A
VOCs by EPA Method 8260 SVOCs by EPA
Method 8270
BenzeneChloroformDiisopropyl etherNaphthaleneTolueneTotal XylenesAll CompoundsNC2LGWQS 1 70 70 6 600 500 Various
Residential Groundwater VISL 1.6 0.81 1,400 4.6 3,800 77 Various
Non-Residential Groundwater VISL 6.9 3.6 5,900 20 16,000 320 Various
GW-1 08/16/21 <1.0 1.5 <1.0 <1.0 <1.0 <1.0 BRL
GW-2 08/16/21 <1.0 1.4 <1.0 <1.0 <1.0 <1.0 BRL
GW-3 08/16/21 <1.0 4.2 <1.0 <1.0 <1.0 <1.0 BRL
GW-4 08/16/21 <1.0 4.4 <1.0 <1.0 <1.0 <1.0 BRL
GW-5 08/16/21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BRL
GW-6 08/16/21 <1.0 2.7 <1.0 <1.0 <1.0 <1.0 BRL
GW-7 08/16/21 <1.0 3.5 <1.0 <1.0 <1.0 <1.0 BRL
GW-8 08/16/21 3.0 <1.0 2.7 <1.0 <1.0 <1.0 BRL
GW-9 08/16/21 6.8 3.9 <1.0 1.4 1.2 3.1 BRL
GW-10 08/17/21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 BRL
GW-11 08/17/21 <1.0 1.4 <1.0 <1.0 <1.0 <1.0 BRL
Notes:
All results presented in micrograms per liter (mg/L)
Compounds not shown were not detected
VOCs = Volatile Organic Compounds
SVOCs = Semi-volatile Organic Compounds
NC2LGWQS = North Carolina 2L Groundwater Quality Standards (October 2020)
Residential Groundwater VISL = NCDEQ Groundwater Residential Vapor Intrusion Screening Level (June 2021)
Non-Residential Groundwater VISL = NCDEQ Groundwater Non-Residential Vapor Intrusion Screening Level (June 2021)
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the NC2LGWQS
VALUE = concentration greater than the Residential Groundwater VISL
VALUE = concentration greater than the Non-Residential Groundwater VISL
Sample DateSample ID
Table 2
Summary of Soil Samples Analytical Results
Graham and 6th Site
301 North Graham Street and 420 West 6th Street
Charlotte, Mecklenburg County, North Carolina
ECS Project No.: 49:13734-A
VOCs by EPA Method 8260 SVOCs by EPA
Method 8270
Benzene2-Butanone (MEK)sec-Butylbenzene1,2-Dibromoethane(EDB)EthylbenzeneIsopropylbenzeneMethylene ChlorideNaphthalenen-PropylbenzeneTolueneTotal XylenesAll CompoundsProtection of Groundwater PSRG 0.10 17 4.1 0.00011 13 2.3 0.025 0.39 2.6 8.3 9.9 Various
Residential PSRG 1.2 5,500 1,600 0.038 6.1 410 58 2.1 780 990 120 Various
Industrial/Commercial PSRG 5.4 40,000 23,000 0.17 27 2,100 650 8.8 5,100 9,700 530 Various
Soil-To-Water MSCC 0.0072 16 2.2 0.000096 8.0 1.3 0.023 0.2 1.4 5.4 6.0 Various
Residential MSCC 12 9,380 1,560 0.33 60.3 1,560 93.8 5.5 1,560 1,250 3,120 Various
Industrial/Commercial MSCC 59.4 140,000 23,300 1.63 297 23,300 1,400 27 23,300 18,600 46,700 Various
SS-1 08/16/21 5 - 10 <0.032 <0.64 0.18 <0.032 <0.032 <0.032 0.67 <0.032 <0.032 <0.032 0.096 BRL
SS-2 08/16/21 10 - 15 0.22 0.18 0.16 0.010 0.11 0.59 0.071 0.64 0.75 0.068 0.36 BRL
SS-3 08/17/21 10 - 15 <0.0068 <0.14 <0.0068 <0.0068 <0.0068 <0.0068 0.075 0.0079 <0.0068 <0.0068 <0.014 BRL
SS-4 08/17/21 10 - 15 <0.0063 <0.13 <0.0063 <0.0063 <0.0063 <0.0063 0.075 <0.0063 <0.0063 <0.0063 <0.013 BRL
SS-5 08/17/21 10 - 15 <0.0056 <0.11 <0.0056 <0.0056 <0.0056 <0.0056 0.041 <0.0056 <0.0056 <0.0056 <0.011 BRL
Notes:
All results presented in milligrams per kilogram (mg/kg)
Compounds not shown were not detected
ft bgs = feet below ground surface
VOCs = Volatile Organic Compounds
SVOCs = Semi-volatile Organic Compounds
PSRG = Preliminary Soil Remediation Goal (January 2021)
MSCC = Maximum Soil Contaminant Concentration (October 2020)
NE = Not Established
VALUE = concentration greater than the laboratory method reporting limit
VALUE = concentration greater than the Protection of Groundwater PSRG
VALUE = concentration greater than the Soil-to-Water MSCC
Sample ID Sample Date Sample Depth
(x to y ft bgs)

APPENDIX A

August 2, 2021 Mr. Scott Wearren (via email) Daniel Realty Company, LLC
505 20th St. North Suite 100 Birmingham, AL 35203
RE: Monitoring Well Construction Permit Permit # WM0301140 301 N. Graham St and 420 W. 6th St.
Charlotte, Mecklenburg County Dear Mr. Wearren, In accordance with your completed application received on August 2, 2021, we are forwarding herewith Monitoring Well Construction Permit Numbered WM0301140 and issued for the construction of six monitoring wells located near the subject site in Charlotte, Mecklenburg County.
This Permit will be effective for one year from the date of issuance and shall be subject to the conditions and limitations as specified therein. Should you have any questions, please contact Edward Watson at [phone], or by email at [e-mail].
Sincerely,
Andrew H. Pitner, P.G., Assistant Regional Supervisor
Mooresville Regional Office Water Quality Regional Operations Section Division of Water Resources CC: WQROS, Central Office (via Laserfiche) Scott Young, ECS Limited (via email)

NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL
In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and other applicable Laws, Rules and Regulations. PERMISSION IS HEREBY GRANTED TO

Daniel Realty Company, LLC (ECS Limited as Agent)
FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of six monitoring wells owned by Daniel Realty
Company, LLC at the subject site near N. Graham St. and W. 6th St., in Charlotte, Mecklenburg County. This Permit is issued in accordance with the application received on August 2, 2021, in conformity with specifications and supporting data,
all of which are filed with the Department of Environmental Quality and are considered integral parts of this Permit. This Permit is for well construction only, and does not waive any provision or requirement of any other applicable law or regulation. Construction of any well under this Permit shall be in strict compliance with the North Carolina Well Construction Regulations and Standards (15A NCAC 02C .0100), and other State and Local Laws and regulations pertaining to well construction. If any requirements or limitations specified in this Permit are unacceptable, you have a right to an adjudicatory hearing upon written request within 30 days of receipt of this Permit. The request must be in the form of a written petition conforming to Chapter 150B of the North Carolina General Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service Center, Raleigh, North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding. This Permit will be effective for one year from the date of its issuance and shall be subject to other specified conditions,
limitations, or exceptions as follows:
1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these wells are being installed as part of an investigation for contamination from an underground storage tank or dry cleaner incident. 2. Issuance of this Permit does not supersede any other agreement, permit, or requirement issued by another agency. 3. The well(s) shall be located and constructed as shown on the attachments submitted as part of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC 02C .0108(o). 5. Well construction records (GW-1) for each well shall be submitted to the Division of Water Resources’ Information
Processing Unit within 30 days of the well completion. 6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A NCAC 02C .0113 and a well abandonment record (GW-30) shall be submitted to the Division of Water Resources’ Information Processing Unit within 30 days of the well abandonment.
7. If the well penetrates any water-bearing zone that contains contaminated waters, the upper three feet of the well shall be grouted within one day after the casing is set or the well abandoned.
8. Temporary wells must be permanently abandoned or converted to a permanent well within seven days (168 hours) of completion of drilling the borehole. 9. Adequate permits shall be obtained from Mecklenburg County Groundwater and Wastewater Services.
Permit issued the 2nd day of August, 2021 FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION _______________________________________________
Andrew H. Pitner, P.G., Assistant Regional Supervisor
Division of Water Resources By Authority of the Environmental Management Commission
Permit No. # WM0301140

APPENDIX B

#=CL#
August 26, 2021
LIMS USE: FR - SCOTT YOUNG
LIMS OBJECT ID: 92556378
92556378
Project:
Pace Project No.:
RE:
Scott Young
ECS Southeast, LLP
1812 Center Park Drive
Suite D
Charlotte, NC 28217
N. Graham & 6th
Dear Scott Young:
Enclosed are the analytical results for sample(s) received by the laboratory on August 18, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 94
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 94
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92556378
N. Graham & 6th
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92556378001 GW-1 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378002 GW-2 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378003 GW-3 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378004 GW-4 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378005 GW-5 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378006 GW-6 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378007 GW-7 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378008 GW-8 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378009 GW-9 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378010 GW-10 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378011 GW-11 EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CPM1
92556378012 SS-1 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92556378013 SS-2 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92556378014 SS-3 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92556378015 SS-4 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92556378016 SS-5 EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 94
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92556378
N. Graham & 6th
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-1 Lab ID:92556378001 Collected:08/16/21 09:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 15:50 83-32-908/20/21 12:078.4 1
Acenaphthylene ND ug/L 08/24/21 15:50 208-96-808/20/21 12:078.4 1
Aniline ND ug/L 08/24/21 15:50 62-53-308/20/21 12:078.4 1
Anthracene ND ug/L 08/24/21 15:50 120-12-708/20/21 12:078.4 1
Benzo(a)anthracene ND ug/L 08/24/21 15:50 56-55-308/20/21 12:078.4 1
Benzo(a)pyrene ND ug/L 08/24/21 15:50 50-32-808/20/21 12:078.4 1
Benzo(b)fluoranthene ND ug/L 08/24/21 15:50 205-99-208/20/21 12:078.4 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 15:50 191-24-208/20/21 12:078.4 1
Benzo(k)fluoranthene ND ug/L 08/24/21 15:50 207-08-908/20/21 12:078.4 1
Benzoic Acid ND ug/L 08/24/21 15:50 65-85-008/20/21 12:0742.0 1
Benzyl alcohol ND ug/L 08/24/21 15:50 100-51-608/20/21 12:0716.8 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 15:50 101-55-308/20/21 12:078.4 1
Butylbenzylphthalate ND ug/L 08/24/21 15:50 85-68-708/20/21 12:078.4 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 15:50 59-50-708/20/21 12:078.4 1
4-Chloroaniline ND ug/L 08/24/21 15:50 106-47-808/20/21 12:0716.8 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 15:50 111-91-108/20/21 12:078.4 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 15:50 111-44-408/20/21 12:078.4 1
2-Chloronaphthalene ND ug/L 08/24/21 15:50 91-58-708/20/21 12:078.4 1
2-Chlorophenol ND ug/L 08/24/21 15:50 95-57-808/20/21 12:078.4 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 15:50 7005-72-308/20/21 12:078.4 1
Chrysene ND ug/L 08/24/21 15:50 218-01-908/20/21 12:078.4 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 15:50 53-70-308/20/21 12:078.4 1
Dibenzofuran ND ug/L 08/24/21 15:50 132-64-908/20/21 12:078.4 1
1,2-Dichlorobenzene ND ug/L 08/24/21 15:50 95-50-108/20/21 12:078.4 1
1,3-Dichlorobenzene ND ug/L 08/24/21 15:50 541-73-108/20/21 12:078.4 1
1,4-Dichlorobenzene ND ug/L 08/24/21 15:50 106-46-708/20/21 12:078.4 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 15:50 91-94-108/20/21 12:0716.8 1
2,4-Dichlorophenol ND ug/L 08/24/21 15:50 120-83-208/20/21 12:078.4 1
Diethylphthalate ND ug/L 08/24/21 15:50 84-66-208/20/21 12:078.4 1
2,4-Dimethylphenol ND ug/L 08/24/21 15:50 105-67-908/20/21 12:078.4 1
Dimethylphthalate ND ug/L 08/24/21 15:50 131-11-308/20/21 12:078.4 1
Di-n-butylphthalate ND ug/L 08/24/21 15:50 84-74-208/20/21 12:078.4 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 15:50 534-52-108/20/21 12:0716.8 1
2,4-Dinitrophenol ND ug/L 08/24/21 15:50 51-28-508/20/21 12:0742.0 1
2,4-Dinitrotoluene ND ug/L 08/24/21 15:50 121-14-208/20/21 12:078.4 1
2,6-Dinitrotoluene ND ug/L 08/24/21 15:50 606-20-208/20/21 12:078.4 1
Di-n-octylphthalate ND ug/L 08/24/21 15:50 117-84-008/20/21 12:078.4 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 15:50 117-81-708/20/21 12:075.0 1
Fluoranthene ND ug/L 08/24/21 15:50 206-44-008/20/21 12:078.4 1
Fluorene ND ug/L 08/24/21 15:50 86-73-708/20/21 12:078.4 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 15:50 87-68-308/20/21 12:078.4 1
Hexachlorobenzene ND ug/L 08/24/21 15:50 118-74-108/20/21 12:078.4 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 15:50 77-47-408/20/21 12:078.4 1
Hexachloroethane ND ug/L 08/24/21 15:50 67-72-108/20/21 12:078.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 15:50 193-39-508/20/21 12:078.4 1
Isophorone ND ug/L 08/24/21 15:50 78-59-108/20/21 12:078.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-1 Lab ID:92556378001 Collected:08/16/21 09:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
1-Methylnaphthalene ND ug/L 08/24/21 15:50 90-12-008/20/21 12:078.4 1
2-Methylnaphthalene ND ug/L 08/24/21 15:50 91-57-608/20/21 12:078.4 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 15:50 95-48-708/20/21 12:078.4 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 15:50 15831-10-408/20/21 12:078.4 1
Naphthalene ND ug/L 08/24/21 15:50 91-20-308/20/21 12:078.4 1
2-Nitroaniline ND ug/L 08/24/21 15:50 88-74-408/20/21 12:0716.8 1
3-Nitroaniline ND ug/L 08/24/21 15:50 99-09-208/20/21 12:0716.8 1
4-Nitroaniline ND ug/L 08/24/21 15:50 100-01-608/20/21 12:0716.8 1
Nitrobenzene ND ug/L 08/24/21 15:50 98-95-308/20/21 12:078.4 1
2-Nitrophenol ND ug/L 08/24/21 15:50 88-75-508/20/21 12:078.4 1
4-Nitrophenol ND ug/L 08/24/21 15:50 100-02-708/20/21 12:0742.0 1
N-Nitrosodimethylamine ND ug/L 08/24/21 15:50 62-75-908/20/21 12:078.4 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 15:50 621-64-708/20/21 12:078.4 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 15:50 86-30-608/20/21 12:078.4 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 15:50 108-60-108/20/21 12:078.4 1
Pentachlorophenol ND ug/L 08/24/21 15:50 87-86-508/20/21 12:0716.8 1
Phenanthrene ND ug/L 08/24/21 15:50 85-01-808/20/21 12:078.4 1
Phenol ND ug/L 08/24/21 15:50 108-95-208/20/21 12:078.4 1
Pyrene ND ug/L 08/24/21 15:50 129-00-008/20/21 12:078.4 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 15:50 120-82-108/20/21 12:078.4 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 15:50 95-95-408/20/21 12:078.4 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 15:50 88-06-208/20/21 12:078.4 1
Surrogates
Nitrobenzene-d5 (S)38 %08/24/21 15:50 4165-60-008/20/21 12:0710-144 1
2-Fluorobiphenyl (S)28 %08/24/21 15:50 321-60-808/20/21 12:0710-130 1
Terphenyl-d14 (S)75 %08/24/21 15:50 1718-51-008/20/21 12:0734-163 1
Phenol-d6 (S)17 %08/24/21 15:50 13127-88-308/20/21 12:0710-130 1
2-Fluorophenol (S)25 %08/24/21 15:50 367-12-408/20/21 12:0710-130 1
2,4,6-Tribromophenol (S)48 %08/24/21 15:50 118-79-608/20/21 12:0710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 02:33 67-64-125.0 1
Benzene ND ug/L 08/20/21 02:33 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 02:33 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 02:33 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 02:33 75-27-41.0 1
Bromoform ND ug/L 08/20/21 02:33 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 02:33 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 02:33 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 02:33 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 02:33 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 02:33 75-00-3 IL1.0 1
Chloroform 1.5 ug/L 08/20/21 02:33 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 02:33 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 02:33 95-49-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-1 Lab ID:92556378001 Collected:08/16/21 09:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Chlorotoluene ND ug/L 08/20/21 02:33 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 02:33 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 02:33 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 02:33 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 02:33 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 02:33 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 02:33 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 02:33 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 02:33 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 02:33 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 02:33 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 02:33 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 02:33 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 02:33 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 02:33 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 02:33 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 02:33 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 02:33 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 02:33 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 02:33 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 02:33 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 02:33 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 02:33 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 02:33 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 02:33 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 02:33 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 02:33 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 02:33 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 02:33 91-20-31.0 1
Styrene ND ug/L 08/20/21 02:33 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 02:33 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 02:33 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 02:33 127-18-41.0 1
Toluene ND ug/L 08/20/21 02:33 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 02:33 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 02:33 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 02:33 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 02:33 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 02:33 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 02:33 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 02:33 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 02:33 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 02:33 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 02:33 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 02:33 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 02:33 95-47-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-1 Lab ID:92556378001 Collected:08/16/21 09:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Surrogates
4-Bromofluorobenzene (S)100 %08/20/21 02:33 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/20/21 02:33 17060-07-070-130 1
Toluene-d8 (S)105 %08/20/21 02:33 2037-26-570-130 1
Sample:GW-2 Lab ID:92556378002 Collected:08/16/21 10:15 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 16:16 83-32-908/20/21 12:078.7 1
Acenaphthylene ND ug/L 08/24/21 16:16 208-96-808/20/21 12:078.7 1
Aniline ND ug/L 08/24/21 16:16 62-53-308/20/21 12:078.7 1
Anthracene ND ug/L 08/24/21 16:16 120-12-708/20/21 12:078.7 1
Benzo(a)anthracene ND ug/L 08/24/21 16:16 56-55-308/20/21 12:078.7 1
Benzo(a)pyrene ND ug/L 08/24/21 16:16 50-32-808/20/21 12:078.7 1
Benzo(b)fluoranthene ND ug/L 08/24/21 16:16 205-99-208/20/21 12:078.7 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 16:16 191-24-208/20/21 12:078.7 1
Benzo(k)fluoranthene ND ug/L 08/24/21 16:16 207-08-908/20/21 12:078.7 1
Benzoic Acid ND ug/L 08/24/21 16:16 65-85-008/20/21 12:0743.5 1
Benzyl alcohol ND ug/L 08/24/21 16:16 100-51-608/20/21 12:0717.4 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 16:16 101-55-308/20/21 12:078.7 1
Butylbenzylphthalate ND ug/L 08/24/21 16:16 85-68-708/20/21 12:078.7 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 16:16 59-50-708/20/21 12:078.7 1
4-Chloroaniline ND ug/L 08/24/21 16:16 106-47-808/20/21 12:0717.4 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 16:16 111-91-108/20/21 12:078.7 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 16:16 111-44-408/20/21 12:078.7 1
2-Chloronaphthalene ND ug/L 08/24/21 16:16 91-58-708/20/21 12:078.7 1
2-Chlorophenol ND ug/L 08/24/21 16:16 95-57-808/20/21 12:078.7 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 16:16 7005-72-308/20/21 12:078.7 1
Chrysene ND ug/L 08/24/21 16:16 218-01-908/20/21 12:078.7 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 16:16 53-70-308/20/21 12:078.7 1
Dibenzofuran ND ug/L 08/24/21 16:16 132-64-908/20/21 12:078.7 1
1,2-Dichlorobenzene ND ug/L 08/24/21 16:16 95-50-108/20/21 12:078.7 1
1,3-Dichlorobenzene ND ug/L 08/24/21 16:16 541-73-108/20/21 12:078.7 1
1,4-Dichlorobenzene ND ug/L 08/24/21 16:16 106-46-708/20/21 12:078.7 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 16:16 91-94-108/20/21 12:0717.4 1
2,4-Dichlorophenol ND ug/L 08/24/21 16:16 120-83-208/20/21 12:078.7 1
Diethylphthalate ND ug/L 08/24/21 16:16 84-66-208/20/21 12:078.7 1
2,4-Dimethylphenol ND ug/L 08/24/21 16:16 105-67-908/20/21 12:078.7 1
Dimethylphthalate ND ug/L 08/24/21 16:16 131-11-308/20/21 12:078.7 1
Di-n-butylphthalate ND ug/L 08/24/21 16:16 84-74-208/20/21 12:078.7 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 16:16 534-52-108/20/21 12:0717.4 1
2,4-Dinitrophenol ND ug/L 08/24/21 16:16 51-28-508/20/21 12:0743.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-2 Lab ID:92556378002 Collected:08/16/21 10:15 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dinitrotoluene ND ug/L 08/24/21 16:16 121-14-208/20/21 12:078.7 1
2,6-Dinitrotoluene ND ug/L 08/24/21 16:16 606-20-208/20/21 12:078.7 1
Di-n-octylphthalate ND ug/L 08/24/21 16:16 117-84-008/20/21 12:078.7 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 16:16 117-81-708/20/21 12:075.2 1
Fluoranthene ND ug/L 08/24/21 16:16 206-44-008/20/21 12:078.7 1
Fluorene ND ug/L 08/24/21 16:16 86-73-708/20/21 12:078.7 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 16:16 87-68-308/20/21 12:078.7 1
Hexachlorobenzene ND ug/L 08/24/21 16:16 118-74-108/20/21 12:078.7 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 16:16 77-47-408/20/21 12:078.7 1
Hexachloroethane ND ug/L 08/24/21 16:16 67-72-108/20/21 12:078.7 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 16:16 193-39-508/20/21 12:078.7 1
Isophorone ND ug/L 08/24/21 16:16 78-59-108/20/21 12:078.7 1
1-Methylnaphthalene ND ug/L 08/24/21 16:16 90-12-008/20/21 12:078.7 1
2-Methylnaphthalene ND ug/L 08/24/21 16:16 91-57-608/20/21 12:078.7 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 16:16 95-48-708/20/21 12:078.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 16:16 15831-10-408/20/21 12:078.7 1
Naphthalene ND ug/L 08/24/21 16:16 91-20-308/20/21 12:078.7 1
2-Nitroaniline ND ug/L 08/24/21 16:16 88-74-408/20/21 12:0717.4 1
3-Nitroaniline ND ug/L 08/24/21 16:16 99-09-208/20/21 12:0717.4 1
4-Nitroaniline ND ug/L 08/24/21 16:16 100-01-608/20/21 12:0717.4 1
Nitrobenzene ND ug/L 08/24/21 16:16 98-95-308/20/21 12:078.7 1
2-Nitrophenol ND ug/L 08/24/21 16:16 88-75-508/20/21 12:078.7 1
4-Nitrophenol ND ug/L 08/24/21 16:16 100-02-708/20/21 12:0743.5 1
N-Nitrosodimethylamine ND ug/L 08/24/21 16:16 62-75-908/20/21 12:078.7 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 16:16 621-64-708/20/21 12:078.7 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 16:16 86-30-608/20/21 12:078.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 16:16 108-60-108/20/21 12:078.7 1
Pentachlorophenol ND ug/L 08/24/21 16:16 87-86-508/20/21 12:0717.4 1
Phenanthrene ND ug/L 08/24/21 16:16 85-01-808/20/21 12:078.7 1
Phenol ND ug/L 08/24/21 16:16 108-95-208/20/21 12:078.7 1
Pyrene ND ug/L 08/24/21 16:16 129-00-008/20/21 12:078.7 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 16:16 120-82-108/20/21 12:078.7 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 16:16 95-95-408/20/21 12:078.7 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 16:16 88-06-208/20/21 12:078.7 1
Surrogates
Nitrobenzene-d5 (S)76 %08/24/21 16:16 4165-60-0 1g08/20/21 12:0710-144 1
2-Fluorobiphenyl (S)59 %08/24/21 16:16 321-60-808/20/21 12:0710-130 1
Terphenyl-d14 (S)89 %08/24/21 16:16 1718-51-008/20/21 12:0734-163 1
Phenol-d6 (S)1 %08/24/21 16:16 13127-88-3 S008/20/21 12:0710-130 1
2-Fluorophenol (S)5 %08/24/21 16:16 367-12-4 S008/20/21 12:0710-130 1
2,4,6-Tribromophenol (S)76 %08/24/21 16:16 118-79-608/20/21 12:0710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 02:50 67-64-125.0 1
Benzene ND ug/L 08/20/21 02:50 71-43-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-2 Lab ID:92556378002 Collected:08/16/21 10:15 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Bromobenzene ND ug/L 08/20/21 02:50 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 02:50 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 02:50 75-27-41.0 1
Bromoform ND ug/L 08/20/21 02:50 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 02:50 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 02:50 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 02:50 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 02:50 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 02:50 75-00-3 IL1.0 1
Chloroform 1.4 ug/L 08/20/21 02:50 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 02:50 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 02:50 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 02:50 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 02:50 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 02:50 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 02:50 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 02:50 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 02:50 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 02:50 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 02:50 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 02:50 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 02:50 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 02:50 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 02:50 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 02:50 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 02:50 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 02:50 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 02:50 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 02:50 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 02:50 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 02:50 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 02:50 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 02:50 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 02:50 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 02:50 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 02:50 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 02:50 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 02:50 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 02:50 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 02:50 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 02:50 91-20-31.0 1
Styrene ND ug/L 08/20/21 02:50 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 02:50 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 02:50 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 02:50 127-18-41.0 1
Toluene ND ug/L 08/20/21 02:50 108-88-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-2 Lab ID:92556378002 Collected:08/16/21 10:15 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2,3-Trichlorobenzene ND ug/L 08/20/21 02:50 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 02:50 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 02:50 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 02:50 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 02:50 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 02:50 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 02:50 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 02:50 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 02:50 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 02:50 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 02:50 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 02:50 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/20/21 02:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %08/20/21 02:50 17060-07-070-130 1
Toluene-d8 (S)104 %08/20/21 02:50 2037-26-570-130 1
Sample:GW-3 Lab ID:92556378003 Collected:08/16/21 10:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 16:43 83-32-908/20/21 12:078.8 1
Acenaphthylene ND ug/L 08/24/21 16:43 208-96-808/20/21 12:078.8 1
Aniline ND ug/L 08/24/21 16:43 62-53-308/20/21 12:078.8 1
Anthracene ND ug/L 08/24/21 16:43 120-12-708/20/21 12:078.8 1
Benzo(a)anthracene ND ug/L 08/24/21 16:43 56-55-308/20/21 12:078.8 1
Benzo(a)pyrene ND ug/L 08/24/21 16:43 50-32-808/20/21 12:078.8 1
Benzo(b)fluoranthene ND ug/L 08/24/21 16:43 205-99-208/20/21 12:078.8 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 16:43 191-24-208/20/21 12:078.8 1
Benzo(k)fluoranthene ND ug/L 08/24/21 16:43 207-08-908/20/21 12:078.8 1
Benzoic Acid ND ug/L 08/24/21 16:43 65-85-008/20/21 12:0743.9 1
Benzyl alcohol ND ug/L 08/24/21 16:43 100-51-608/20/21 12:0717.5 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 16:43 101-55-308/20/21 12:078.8 1
Butylbenzylphthalate ND ug/L 08/24/21 16:43 85-68-708/20/21 12:078.8 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 16:43 59-50-708/20/21 12:078.8 1
4-Chloroaniline ND ug/L 08/24/21 16:43 106-47-808/20/21 12:0717.5 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 16:43 111-91-108/20/21 12:078.8 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 16:43 111-44-408/20/21 12:078.8 1
2-Chloronaphthalene ND ug/L 08/24/21 16:43 91-58-708/20/21 12:078.8 1
2-Chlorophenol ND ug/L 08/24/21 16:43 95-57-808/20/21 12:078.8 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 16:43 7005-72-308/20/21 12:078.8 1
Chrysene ND ug/L 08/24/21 16:43 218-01-908/20/21 12:078.8 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 16:43 53-70-308/20/21 12:078.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-3 Lab ID:92556378003 Collected:08/16/21 10:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Dibenzofuran ND ug/L 08/24/21 16:43 132-64-908/20/21 12:078.8 1
1,2-Dichlorobenzene ND ug/L 08/24/21 16:43 95-50-108/20/21 12:078.8 1
1,3-Dichlorobenzene ND ug/L 08/24/21 16:43 541-73-108/20/21 12:078.8 1
1,4-Dichlorobenzene ND ug/L 08/24/21 16:43 106-46-708/20/21 12:078.8 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 16:43 91-94-108/20/21 12:0717.5 1
2,4-Dichlorophenol ND ug/L 08/24/21 16:43 120-83-208/20/21 12:078.8 1
Diethylphthalate ND ug/L 08/24/21 16:43 84-66-208/20/21 12:078.8 1
2,4-Dimethylphenol ND ug/L 08/24/21 16:43 105-67-908/20/21 12:078.8 1
Dimethylphthalate ND ug/L 08/24/21 16:43 131-11-308/20/21 12:078.8 1
Di-n-butylphthalate ND ug/L 08/24/21 16:43 84-74-208/20/21 12:078.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 16:43 534-52-108/20/21 12:0717.5 1
2,4-Dinitrophenol ND ug/L 08/24/21 16:43 51-28-508/20/21 12:0743.9 1
2,4-Dinitrotoluene ND ug/L 08/24/21 16:43 121-14-208/20/21 12:078.8 1
2,6-Dinitrotoluene ND ug/L 08/24/21 16:43 606-20-208/20/21 12:078.8 1
Di-n-octylphthalate ND ug/L 08/24/21 16:43 117-84-008/20/21 12:078.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 16:43 117-81-708/20/21 12:075.3 1
Fluoranthene ND ug/L 08/24/21 16:43 206-44-008/20/21 12:078.8 1
Fluorene ND ug/L 08/24/21 16:43 86-73-708/20/21 12:078.8 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 16:43 87-68-308/20/21 12:078.8 1
Hexachlorobenzene ND ug/L 08/24/21 16:43 118-74-108/20/21 12:078.8 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 16:43 77-47-408/20/21 12:078.8 1
Hexachloroethane ND ug/L 08/24/21 16:43 67-72-108/20/21 12:078.8 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 16:43 193-39-508/20/21 12:078.8 1
Isophorone ND ug/L 08/24/21 16:43 78-59-108/20/21 12:078.8 1
1-Methylnaphthalene ND ug/L 08/24/21 16:43 90-12-008/20/21 12:078.8 1
2-Methylnaphthalene ND ug/L 08/24/21 16:43 91-57-608/20/21 12:078.8 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 16:43 95-48-708/20/21 12:078.8 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 16:43 15831-10-408/20/21 12:078.8 1
Naphthalene ND ug/L 08/24/21 16:43 91-20-308/20/21 12:078.8 1
2-Nitroaniline ND ug/L 08/24/21 16:43 88-74-408/20/21 12:0717.5 1
3-Nitroaniline ND ug/L 08/24/21 16:43 99-09-208/20/21 12:0717.5 1
4-Nitroaniline ND ug/L 08/24/21 16:43 100-01-608/20/21 12:0717.5 1
Nitrobenzene ND ug/L 08/24/21 16:43 98-95-308/20/21 12:078.8 1
2-Nitrophenol ND ug/L 08/24/21 16:43 88-75-508/20/21 12:078.8 1
4-Nitrophenol ND ug/L 08/24/21 16:43 100-02-708/20/21 12:0743.9 1
N-Nitrosodimethylamine ND ug/L 08/24/21 16:43 62-75-908/20/21 12:078.8 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 16:43 621-64-708/20/21 12:078.8 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 16:43 86-30-608/20/21 12:078.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 16:43 108-60-108/20/21 12:078.8 1
Pentachlorophenol ND ug/L 08/24/21 16:43 87-86-508/20/21 12:0717.5 1
Phenanthrene ND ug/L 08/24/21 16:43 85-01-808/20/21 12:078.8 1
Phenol ND ug/L 08/24/21 16:43 108-95-208/20/21 12:078.8 1
Pyrene ND ug/L 08/24/21 16:43 129-00-008/20/21 12:078.8 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 16:43 120-82-108/20/21 12:078.8 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 16:43 95-95-408/20/21 12:078.8 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 16:43 88-06-208/20/21 12:078.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-3 Lab ID:92556378003 Collected:08/16/21 10:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
Nitrobenzene-d5 (S)24 %08/24/21 16:43 4165-60-008/20/21 12:0710-144 1
2-Fluorobiphenyl (S)19 %08/24/21 16:43 321-60-808/20/21 12:0710-130 1
Terphenyl-d14 (S)47 %08/24/21 16:43 1718-51-008/20/21 12:0734-163 1
Phenol-d6 (S)9 %08/24/21 16:43 13127-88-3 S008/20/21 12:0710-130 1
2-Fluorophenol (S)13 %08/24/21 16:43 367-12-408/20/21 12:0710-130 1
2,4,6-Tribromophenol (S)31 %08/24/21 16:43 118-79-608/20/21 12:0710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 03:08 67-64-125.0 1
Benzene ND ug/L 08/20/21 03:08 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 03:08 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 03:08 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 03:08 75-27-41.0 1
Bromoform ND ug/L 08/20/21 03:08 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 03:08 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 03:08 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 03:08 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 03:08 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 03:08 75-00-3 IL1.0 1
Chloroform 4.2 ug/L 08/20/21 03:08 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 03:08 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 03:08 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 03:08 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 03:08 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 03:08 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 03:08 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 03:08 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 03:08 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 03:08 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 03:08 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 03:08 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 03:08 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 03:08 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 03:08 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 03:08 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 03:08 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 03:08 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 03:08 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 03:08 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 03:08 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 03:08 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 03:08 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 03:08 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 03:08 100-41-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-3 Lab ID:92556378003 Collected:08/16/21 10:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 08/20/21 03:08 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 03:08 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 03:08 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 03:08 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 03:08 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 03:08 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 03:08 91-20-31.0 1
Styrene ND ug/L 08/20/21 03:08 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 03:08 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 03:08 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 03:08 127-18-41.0 1
Toluene ND ug/L 08/20/21 03:08 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 03:08 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 03:08 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 03:08 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 03:08 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 03:08 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 03:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 03:08 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 03:08 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 03:08 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 03:08 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 03:08 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 03:08 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)104 %08/20/21 03:08 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/20/21 03:08 17060-07-070-130 1
Toluene-d8 (S)103 %08/20/21 03:08 2037-26-570-130 1
Sample:GW-4 Lab ID:92556378004 Collected:08/16/21 10:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 17:09 83-32-908/20/21 12:078.3 1
Acenaphthylene ND ug/L 08/24/21 17:09 208-96-808/20/21 12:078.3 1
Aniline ND ug/L 08/24/21 17:09 62-53-308/20/21 12:078.3 1
Anthracene ND ug/L 08/24/21 17:09 120-12-708/20/21 12:078.3 1
Benzo(a)anthracene ND ug/L 08/24/21 17:09 56-55-308/20/21 12:078.3 1
Benzo(a)pyrene ND ug/L 08/24/21 17:09 50-32-808/20/21 12:078.3 1
Benzo(b)fluoranthene ND ug/L 08/24/21 17:09 205-99-208/20/21 12:078.3 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 17:09 191-24-208/20/21 12:078.3 1
Benzo(k)fluoranthene ND ug/L 08/24/21 17:09 207-08-908/20/21 12:078.3 1
Benzoic Acid ND ug/L 08/24/21 17:09 65-85-008/20/21 12:0741.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-4 Lab ID:92556378004 Collected:08/16/21 10:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzyl alcohol ND ug/L 08/24/21 17:09 100-51-608/20/21 12:0716.7 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 17:09 101-55-308/20/21 12:078.3 1
Butylbenzylphthalate ND ug/L 08/24/21 17:09 85-68-708/20/21 12:078.3 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 17:09 59-50-708/20/21 12:078.3 1
4-Chloroaniline ND ug/L 08/24/21 17:09 106-47-808/20/21 12:0716.7 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 17:09 111-91-108/20/21 12:078.3 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 17:09 111-44-408/20/21 12:078.3 1
2-Chloronaphthalene ND ug/L 08/24/21 17:09 91-58-708/20/21 12:078.3 1
2-Chlorophenol ND ug/L 08/24/21 17:09 95-57-808/20/21 12:078.3 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 17:09 7005-72-308/20/21 12:078.3 1
Chrysene ND ug/L 08/24/21 17:09 218-01-908/20/21 12:078.3 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 17:09 53-70-308/20/21 12:078.3 1
Dibenzofuran ND ug/L 08/24/21 17:09 132-64-908/20/21 12:078.3 1
1,2-Dichlorobenzene ND ug/L 08/24/21 17:09 95-50-108/20/21 12:078.3 1
1,3-Dichlorobenzene ND ug/L 08/24/21 17:09 541-73-108/20/21 12:078.3 1
1,4-Dichlorobenzene ND ug/L 08/24/21 17:09 106-46-708/20/21 12:078.3 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 17:09 91-94-108/20/21 12:0716.7 1
2,4-Dichlorophenol ND ug/L 08/24/21 17:09 120-83-208/20/21 12:078.3 1
Diethylphthalate ND ug/L 08/24/21 17:09 84-66-208/20/21 12:078.3 1
2,4-Dimethylphenol ND ug/L 08/24/21 17:09 105-67-908/20/21 12:078.3 1
Dimethylphthalate ND ug/L 08/24/21 17:09 131-11-308/20/21 12:078.3 1
Di-n-butylphthalate ND ug/L 08/24/21 17:09 84-74-208/20/21 12:078.3 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 17:09 534-52-108/20/21 12:0716.7 1
2,4-Dinitrophenol ND ug/L 08/24/21 17:09 51-28-508/20/21 12:0741.7 1
2,4-Dinitrotoluene ND ug/L 08/24/21 17:09 121-14-208/20/21 12:078.3 1
2,6-Dinitrotoluene ND ug/L 08/24/21 17:09 606-20-208/20/21 12:078.3 1
Di-n-octylphthalate ND ug/L 08/24/21 17:09 117-84-008/20/21 12:078.3 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 17:09 117-81-708/20/21 12:075.0 1
Fluoranthene ND ug/L 08/24/21 17:09 206-44-008/20/21 12:078.3 1
Fluorene ND ug/L 08/24/21 17:09 86-73-708/20/21 12:078.3 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 17:09 87-68-308/20/21 12:078.3 1
Hexachlorobenzene ND ug/L 08/24/21 17:09 118-74-108/20/21 12:078.3 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 17:09 77-47-408/20/21 12:078.3 1
Hexachloroethane ND ug/L 08/24/21 17:09 67-72-108/20/21 12:078.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 17:09 193-39-508/20/21 12:078.3 1
Isophorone ND ug/L 08/24/21 17:09 78-59-108/20/21 12:078.3 1
1-Methylnaphthalene ND ug/L 08/24/21 17:09 90-12-008/20/21 12:078.3 1
2-Methylnaphthalene ND ug/L 08/24/21 17:09 91-57-608/20/21 12:078.3 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 17:09 95-48-708/20/21 12:078.3 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 17:09 15831-10-408/20/21 12:078.3 1
Naphthalene ND ug/L 08/24/21 17:09 91-20-308/20/21 12:078.3 1
2-Nitroaniline ND ug/L 08/24/21 17:09 88-74-408/20/21 12:0716.7 1
3-Nitroaniline ND ug/L 08/24/21 17:09 99-09-208/20/21 12:0716.7 1
4-Nitroaniline ND ug/L 08/24/21 17:09 100-01-608/20/21 12:0716.7 1
Nitrobenzene ND ug/L 08/24/21 17:09 98-95-308/20/21 12:078.3 1
2-Nitrophenol ND ug/L 08/24/21 17:09 88-75-508/20/21 12:078.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-4 Lab ID:92556378004 Collected:08/16/21 10:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
4-Nitrophenol ND ug/L 08/24/21 17:09 100-02-708/20/21 12:0741.7 1
N-Nitrosodimethylamine ND ug/L 08/24/21 17:09 62-75-908/20/21 12:078.3 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 17:09 621-64-708/20/21 12:078.3 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 17:09 86-30-608/20/21 12:078.3 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 17:09 108-60-108/20/21 12:078.3 1
Pentachlorophenol ND ug/L 08/24/21 17:09 87-86-508/20/21 12:0716.7 1
Phenanthrene ND ug/L 08/24/21 17:09 85-01-808/20/21 12:078.3 1
Phenol ND ug/L 08/24/21 17:09 108-95-208/20/21 12:078.3 1
Pyrene ND ug/L 08/24/21 17:09 129-00-008/20/21 12:078.3 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 17:09 120-82-108/20/21 12:078.3 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 17:09 95-95-408/20/21 12:078.3 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 17:09 88-06-208/20/21 12:078.3 1
Surrogates
Nitrobenzene-d5 (S)61 %08/24/21 17:09 4165-60-008/20/21 12:0710-144 1
2-Fluorobiphenyl (S)48 %08/24/21 17:09 321-60-808/20/21 12:0710-130 1
Terphenyl-d14 (S)111 %08/24/21 17:09 1718-51-008/20/21 12:0734-163 1
Phenol-d6 (S)15 %08/24/21 17:09 13127-88-308/20/21 12:0710-130 1
2-Fluorophenol (S)29 %08/24/21 17:09 367-12-408/20/21 12:0710-130 1
2,4,6-Tribromophenol (S)86 %08/24/21 17:09 118-79-608/20/21 12:0710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 03:26 67-64-125.0 1
Benzene ND ug/L 08/20/21 03:26 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 03:26 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 03:26 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 03:26 75-27-41.0 1
Bromoform ND ug/L 08/20/21 03:26 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 03:26 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 03:26 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 03:26 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 03:26 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 03:26 75-00-3 IL1.0 1
Chloroform 4.4 ug/L 08/20/21 03:26 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 03:26 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 03:26 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 03:26 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 03:26 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 03:26 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 03:26 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 03:26 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 03:26 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 03:26 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 03:26 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 03:26 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 03:26 75-34-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-4 Lab ID:92556378004 Collected:08/16/21 10:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dichloroethane ND ug/L 08/20/21 03:26 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 03:26 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 03:26 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 03:26 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 03:26 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 03:26 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 03:26 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 03:26 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 03:26 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 03:26 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 03:26 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 03:26 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 03:26 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 03:26 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 03:26 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 03:26 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 03:26 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 03:26 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 03:26 91-20-31.0 1
Styrene ND ug/L 08/20/21 03:26 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 03:26 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 03:26 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 03:26 127-18-41.0 1
Toluene ND ug/L 08/20/21 03:26 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 03:26 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 03:26 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 03:26 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 03:26 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 03:26 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 03:26 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 03:26 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 03:26 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 03:26 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 03:26 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 03:26 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 03:26 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)100 %08/20/21 03:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/20/21 03:26 17060-07-070-130 1
Toluene-d8 (S)104 %08/20/21 03:26 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-5 Lab ID:92556378005 Collected:08/16/21 11:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 20:52 83-32-908/20/21 12:078.5 1
Acenaphthylene ND ug/L 08/24/21 20:52 208-96-808/20/21 12:078.5 1
Aniline ND ug/L 08/24/21 20:52 62-53-308/20/21 12:078.5 1
Anthracene ND ug/L 08/24/21 20:52 120-12-708/20/21 12:078.5 1
Benzo(a)anthracene ND ug/L 08/24/21 20:52 56-55-308/20/21 12:078.5 1
Benzo(a)pyrene ND ug/L 08/24/21 20:52 50-32-808/20/21 12:078.5 1
Benzo(b)fluoranthene ND ug/L 08/24/21 20:52 205-99-208/20/21 12:078.5 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 20:52 191-24-208/20/21 12:078.5 1
Benzo(k)fluoranthene ND ug/L 08/24/21 20:52 207-08-908/20/21 12:078.5 1
Benzoic Acid ND ug/L 08/24/21 20:52 65-85-008/20/21 12:0742.7 1
Benzyl alcohol ND ug/L 08/24/21 20:52 100-51-608/20/21 12:0717.1 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 20:52 101-55-308/20/21 12:078.5 1
Butylbenzylphthalate ND ug/L 08/24/21 20:52 85-68-708/20/21 12:078.5 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 20:52 59-50-708/20/21 12:078.5 1
4-Chloroaniline ND ug/L 08/24/21 20:52 106-47-808/20/21 12:0717.1 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 20:52 111-91-108/20/21 12:078.5 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 20:52 111-44-408/20/21 12:078.5 1
2-Chloronaphthalene ND ug/L 08/24/21 20:52 91-58-708/20/21 12:078.5 1
2-Chlorophenol ND ug/L 08/24/21 20:52 95-57-808/20/21 12:078.5 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 20:52 7005-72-308/20/21 12:078.5 1
Chrysene ND ug/L 08/24/21 20:52 218-01-908/20/21 12:078.5 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 20:52 53-70-308/20/21 12:078.5 1
Dibenzofuran ND ug/L 08/24/21 20:52 132-64-908/20/21 12:078.5 1
1,2-Dichlorobenzene ND ug/L 08/24/21 20:52 95-50-108/20/21 12:078.5 1
1,3-Dichlorobenzene ND ug/L 08/24/21 20:52 541-73-108/20/21 12:078.5 1
1,4-Dichlorobenzene ND ug/L 08/24/21 20:52 106-46-708/20/21 12:078.5 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 20:52 91-94-108/20/21 12:0717.1 1
2,4-Dichlorophenol ND ug/L 08/24/21 20:52 120-83-208/20/21 12:078.5 1
Diethylphthalate ND ug/L 08/24/21 20:52 84-66-208/20/21 12:078.5 1
2,4-Dimethylphenol ND ug/L 08/24/21 20:52 105-67-908/20/21 12:078.5 1
Dimethylphthalate ND ug/L 08/24/21 20:52 131-11-308/20/21 12:078.5 1
Di-n-butylphthalate ND ug/L 08/24/21 20:52 84-74-208/20/21 12:078.5 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 20:52 534-52-108/20/21 12:0717.1 1
2,4-Dinitrophenol ND ug/L 08/24/21 20:52 51-28-508/20/21 12:0742.7 1
2,4-Dinitrotoluene ND ug/L 08/24/21 20:52 121-14-208/20/21 12:078.5 1
2,6-Dinitrotoluene ND ug/L 08/24/21 20:52 606-20-208/20/21 12:078.5 1
Di-n-octylphthalate ND ug/L 08/24/21 20:52 117-84-008/20/21 12:078.5 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 20:52 117-81-708/20/21 12:075.1 1
Fluoranthene ND ug/L 08/24/21 20:52 206-44-008/20/21 12:078.5 1
Fluorene ND ug/L 08/24/21 20:52 86-73-708/20/21 12:078.5 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 20:52 87-68-308/20/21 12:078.5 1
Hexachlorobenzene ND ug/L 08/24/21 20:52 118-74-108/20/21 12:078.5 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 20:52 77-47-408/20/21 12:078.5 1
Hexachloroethane ND ug/L 08/24/21 20:52 67-72-108/20/21 12:078.5 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 20:52 193-39-508/20/21 12:078.5 1
Isophorone ND ug/L 08/24/21 20:52 78-59-108/20/21 12:078.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-5 Lab ID:92556378005 Collected:08/16/21 11:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
1-Methylnaphthalene ND ug/L 08/24/21 20:52 90-12-008/20/21 12:078.5 1
2-Methylnaphthalene ND ug/L 08/24/21 20:52 91-57-608/20/21 12:078.5 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 20:52 95-48-708/20/21 12:078.5 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 20:52 15831-10-408/20/21 12:078.5 1
Naphthalene ND ug/L 08/24/21 20:52 91-20-308/20/21 12:078.5 1
2-Nitroaniline ND ug/L 08/24/21 20:52 88-74-408/20/21 12:0717.1 1
3-Nitroaniline ND ug/L 08/24/21 20:52 99-09-208/20/21 12:0717.1 1
4-Nitroaniline ND ug/L 08/24/21 20:52 100-01-608/20/21 12:0717.1 1
Nitrobenzene ND ug/L 08/24/21 20:52 98-95-308/20/21 12:078.5 1
2-Nitrophenol ND ug/L 08/24/21 20:52 88-75-508/20/21 12:078.5 1
4-Nitrophenol ND ug/L 08/24/21 20:52 100-02-708/20/21 12:0742.7 1
N-Nitrosodimethylamine ND ug/L 08/24/21 20:52 62-75-908/20/21 12:078.5 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 20:52 621-64-708/20/21 12:078.5 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 20:52 86-30-608/20/21 12:078.5 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 20:52 108-60-108/20/21 12:078.5 1
Pentachlorophenol ND ug/L 08/24/21 20:52 87-86-508/20/21 12:0717.1 1
Phenanthrene ND ug/L 08/24/21 20:52 85-01-808/20/21 12:078.5 1
Phenol ND ug/L 08/24/21 20:52 108-95-208/20/21 12:078.5 1
Pyrene ND ug/L 08/24/21 20:52 129-00-008/20/21 12:078.5 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 20:52 120-82-108/20/21 12:078.5 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 20:52 95-95-408/20/21 12:078.5 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 20:52 88-06-208/20/21 12:078.5 1
Surrogates
Nitrobenzene-d5 (S)28 %08/24/21 20:52 4165-60-008/20/21 12:0710-144 1
2-Fluorobiphenyl (S)23 %08/24/21 20:52 321-60-808/20/21 12:0710-130 1
Terphenyl-d14 (S)99 %08/24/21 20:52 1718-51-008/20/21 12:0734-163 1
Phenol-d6 (S)24 %08/24/21 20:52 13127-88-308/20/21 12:0710-130 1
2-Fluorophenol (S)23 %08/24/21 20:52 367-12-408/20/21 12:0710-130 1
2,4,6-Tribromophenol (S)78 %08/24/21 20:52 118-79-608/20/21 12:0710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 03:43 67-64-125.0 1
Benzene ND ug/L 08/20/21 03:43 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 03:43 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 03:43 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 03:43 75-27-41.0 1
Bromoform ND ug/L 08/20/21 03:43 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 03:43 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 03:43 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 03:43 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 03:43 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 03:43 75-00-3 IL1.0 1
Chloroform ND ug/L 08/20/21 03:43 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 03:43 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 03:43 95-49-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-5 Lab ID:92556378005 Collected:08/16/21 11:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Chlorotoluene ND ug/L 08/20/21 03:43 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 03:43 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 03:43 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 03:43 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 03:43 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 03:43 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 03:43 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 03:43 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 03:43 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 03:43 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 03:43 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 03:43 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 03:43 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 03:43 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 03:43 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 03:43 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 03:43 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 03:43 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 03:43 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 03:43 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 03:43 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 03:43 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 03:43 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 03:43 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 03:43 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 03:43 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 03:43 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 03:43 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 03:43 91-20-31.0 1
Styrene ND ug/L 08/20/21 03:43 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 03:43 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 03:43 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 03:43 127-18-41.0 1
Toluene ND ug/L 08/20/21 03:43 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 03:43 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 03:43 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 03:43 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 03:43 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 03:43 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 03:43 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 03:43 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 03:43 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 03:43 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 03:43 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 03:43 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 03:43 95-47-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-5 Lab ID:92556378005 Collected:08/16/21 11:30 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Surrogates
4-Bromofluorobenzene (S)100 %08/20/21 03:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/20/21 03:43 17060-07-070-130 1
Toluene-d8 (S)105 %08/20/21 03:43 2037-26-570-130 1
Sample:GW-6 Lab ID:92556378006 Collected:08/16/21 11:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 21:18 83-32-908/20/21 12:078.8 1
Acenaphthylene ND ug/L 08/24/21 21:18 208-96-808/20/21 12:078.8 1
Aniline ND ug/L 08/24/21 21:18 62-53-308/20/21 12:078.8 1
Anthracene ND ug/L 08/24/21 21:18 120-12-708/20/21 12:078.8 1
Benzo(a)anthracene ND ug/L 08/24/21 21:18 56-55-308/20/21 12:078.8 1
Benzo(a)pyrene ND ug/L 08/24/21 21:18 50-32-808/20/21 12:078.8 1
Benzo(b)fluoranthene ND ug/L 08/24/21 21:18 205-99-208/20/21 12:078.8 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 21:18 191-24-208/20/21 12:078.8 1
Benzo(k)fluoranthene ND ug/L 08/24/21 21:18 207-08-908/20/21 12:078.8 1
Benzoic Acid ND ug/L 08/24/21 21:18 65-85-008/20/21 12:0743.9 1
Benzyl alcohol ND ug/L 08/24/21 21:18 100-51-608/20/21 12:0717.5 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 21:18 101-55-308/20/21 12:078.8 1
Butylbenzylphthalate ND ug/L 08/24/21 21:18 85-68-708/20/21 12:078.8 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 21:18 59-50-708/20/21 12:078.8 1
4-Chloroaniline ND ug/L 08/24/21 21:18 106-47-808/20/21 12:0717.5 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 21:18 111-91-108/20/21 12:078.8 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 21:18 111-44-408/20/21 12:078.8 1
2-Chloronaphthalene ND ug/L 08/24/21 21:18 91-58-708/20/21 12:078.8 1
2-Chlorophenol ND ug/L 08/24/21 21:18 95-57-808/20/21 12:078.8 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 21:18 7005-72-308/20/21 12:078.8 1
Chrysene ND ug/L 08/24/21 21:18 218-01-908/20/21 12:078.8 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 21:18 53-70-308/20/21 12:078.8 1
Dibenzofuran ND ug/L 08/24/21 21:18 132-64-908/20/21 12:078.8 1
1,2-Dichlorobenzene ND ug/L 08/24/21 21:18 95-50-108/20/21 12:078.8 1
1,3-Dichlorobenzene ND ug/L 08/24/21 21:18 541-73-108/20/21 12:078.8 1
1,4-Dichlorobenzene ND ug/L 08/24/21 21:18 106-46-708/20/21 12:078.8 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 21:18 91-94-108/20/21 12:0717.5 1
2,4-Dichlorophenol ND ug/L 08/24/21 21:18 120-83-208/20/21 12:078.8 1
Diethylphthalate ND ug/L 08/24/21 21:18 84-66-208/20/21 12:078.8 1
2,4-Dimethylphenol ND ug/L 08/24/21 21:18 105-67-908/20/21 12:078.8 1
Dimethylphthalate ND ug/L 08/24/21 21:18 131-11-308/20/21 12:078.8 1
Di-n-butylphthalate ND ug/L 08/24/21 21:18 84-74-208/20/21 12:078.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 21:18 534-52-108/20/21 12:0717.5 1
2,4-Dinitrophenol ND ug/L 08/24/21 21:18 51-28-508/20/21 12:0743.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-6 Lab ID:92556378006 Collected:08/16/21 11:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dinitrotoluene ND ug/L 08/24/21 21:18 121-14-208/20/21 12:078.8 1
2,6-Dinitrotoluene ND ug/L 08/24/21 21:18 606-20-208/20/21 12:078.8 1
Di-n-octylphthalate ND ug/L 08/24/21 21:18 117-84-008/20/21 12:078.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 21:18 117-81-708/20/21 12:075.3 1
Fluoranthene ND ug/L 08/24/21 21:18 206-44-008/20/21 12:078.8 1
Fluorene ND ug/L 08/24/21 21:18 86-73-708/20/21 12:078.8 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 21:18 87-68-308/20/21 12:078.8 1
Hexachlorobenzene ND ug/L 08/24/21 21:18 118-74-108/20/21 12:078.8 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 21:18 77-47-408/20/21 12:078.8 1
Hexachloroethane ND ug/L 08/24/21 21:18 67-72-108/20/21 12:078.8 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 21:18 193-39-508/20/21 12:078.8 1
Isophorone ND ug/L 08/24/21 21:18 78-59-108/20/21 12:078.8 1
1-Methylnaphthalene ND ug/L 08/24/21 21:18 90-12-008/20/21 12:078.8 1
2-Methylnaphthalene ND ug/L 08/24/21 21:18 91-57-608/20/21 12:078.8 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 21:18 95-48-708/20/21 12:078.8 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 21:18 15831-10-408/20/21 12:078.8 1
Naphthalene ND ug/L 08/24/21 21:18 91-20-308/20/21 12:078.8 1
2-Nitroaniline ND ug/L 08/24/21 21:18 88-74-408/20/21 12:0717.5 1
3-Nitroaniline ND ug/L 08/24/21 21:18 99-09-208/20/21 12:0717.5 1
4-Nitroaniline ND ug/L 08/24/21 21:18 100-01-608/20/21 12:0717.5 1
Nitrobenzene ND ug/L 08/24/21 21:18 98-95-308/20/21 12:078.8 1
2-Nitrophenol ND ug/L 08/24/21 21:18 88-75-508/20/21 12:078.8 1
4-Nitrophenol ND ug/L 08/24/21 21:18 100-02-708/20/21 12:0743.9 1
N-Nitrosodimethylamine ND ug/L 08/24/21 21:18 62-75-908/20/21 12:078.8 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 21:18 621-64-708/20/21 12:078.8 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 21:18 86-30-608/20/21 12:078.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 21:18 108-60-108/20/21 12:078.8 1
Pentachlorophenol ND ug/L 08/24/21 21:18 87-86-508/20/21 12:0717.5 1
Phenanthrene ND ug/L 08/24/21 21:18 85-01-808/20/21 12:078.8 1
Phenol ND ug/L 08/24/21 21:18 108-95-208/20/21 12:078.8 1
Pyrene ND ug/L 08/24/21 21:18 129-00-008/20/21 12:078.8 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 21:18 120-82-108/20/21 12:078.8 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 21:18 95-95-408/20/21 12:078.8 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 21:18 88-06-208/20/21 12:078.8 1
Surrogates
Nitrobenzene-d5 (S)62 %08/24/21 21:18 4165-60-008/20/21 12:0710-144 1
2-Fluorobiphenyl (S)45 %08/24/21 21:18 321-60-808/20/21 12:0710-130 1
Terphenyl-d14 (S)122 %08/24/21 21:18 1718-51-008/20/21 12:0734-163 1
Phenol-d6 (S)47 %08/24/21 21:18 13127-88-308/20/21 12:0710-130 1
2-Fluorophenol (S)53 %08/24/21 21:18 367-12-408/20/21 12:0710-130 1
2,4,6-Tribromophenol (S)91 %08/24/21 21:18 118-79-608/20/21 12:0710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 04:01 67-64-125.0 1
Benzene ND ug/L 08/20/21 04:01 71-43-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-6 Lab ID:92556378006 Collected:08/16/21 11:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Bromobenzene ND ug/L 08/20/21 04:01 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 04:01 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 04:01 75-27-41.0 1
Bromoform ND ug/L 08/20/21 04:01 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 04:01 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 04:01 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 04:01 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 04:01 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 04:01 75-00-3 IL1.0 1
Chloroform 2.7 ug/L 08/20/21 04:01 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 04:01 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 04:01 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 04:01 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 04:01 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 04:01 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 04:01 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 04:01 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 04:01 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 04:01 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 04:01 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 04:01 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 04:01 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 04:01 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 04:01 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 04:01 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 04:01 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 04:01 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 04:01 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 04:01 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 04:01 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 04:01 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 04:01 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 04:01 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 04:01 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 04:01 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 04:01 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 04:01 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 04:01 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 04:01 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 04:01 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 04:01 91-20-31.0 1
Styrene ND ug/L 08/20/21 04:01 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 04:01 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 04:01 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 04:01 127-18-41.0 1
Toluene ND ug/L 08/20/21 04:01 108-88-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-6 Lab ID:92556378006 Collected:08/16/21 11:50 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2,3-Trichlorobenzene ND ug/L 08/20/21 04:01 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 04:01 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 04:01 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 04:01 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 04:01 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 04:01 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 04:01 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 04:01 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 04:01 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 04:01 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 04:01 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 04:01 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/20/21 04:01 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/20/21 04:01 17060-07-070-130 1
Toluene-d8 (S)105 %08/20/21 04:01 2037-26-570-130 1
Sample:GW-7 Lab ID:92556378007 Collected:08/16/21 12:10 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 21:45 83-32-908/20/21 12:078.8 1
Acenaphthylene ND ug/L 08/24/21 21:45 208-96-808/20/21 12:078.8 1
Aniline ND ug/L 08/24/21 21:45 62-53-308/20/21 12:078.8 1
Anthracene ND ug/L 08/24/21 21:45 120-12-708/20/21 12:078.8 1
Benzo(a)anthracene ND ug/L 08/24/21 21:45 56-55-308/20/21 12:078.8 1
Benzo(a)pyrene ND ug/L 08/24/21 21:45 50-32-808/20/21 12:078.8 1
Benzo(b)fluoranthene ND ug/L 08/24/21 21:45 205-99-208/20/21 12:078.8 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 21:45 191-24-208/20/21 12:078.8 1
Benzo(k)fluoranthene ND ug/L 08/24/21 21:45 207-08-908/20/21 12:078.8 1
Benzoic Acid ND ug/L 08/24/21 21:45 65-85-008/20/21 12:0744.2 1
Benzyl alcohol ND ug/L 08/24/21 21:45 100-51-608/20/21 12:0717.7 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 21:45 101-55-308/20/21 12:078.8 1
Butylbenzylphthalate ND ug/L 08/24/21 21:45 85-68-708/20/21 12:078.8 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 21:45 59-50-708/20/21 12:078.8 1
4-Chloroaniline ND ug/L 08/24/21 21:45 106-47-808/20/21 12:0717.7 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 21:45 111-91-108/20/21 12:078.8 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 21:45 111-44-408/20/21 12:078.8 1
2-Chloronaphthalene ND ug/L 08/24/21 21:45 91-58-708/20/21 12:078.8 1
2-Chlorophenol ND ug/L 08/24/21 21:45 95-57-808/20/21 12:078.8 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 21:45 7005-72-308/20/21 12:078.8 1
Chrysene ND ug/L 08/24/21 21:45 218-01-908/20/21 12:078.8 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 21:45 53-70-308/20/21 12:078.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-7 Lab ID:92556378007 Collected:08/16/21 12:10 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Dibenzofuran ND ug/L 08/24/21 21:45 132-64-908/20/21 12:078.8 1
1,2-Dichlorobenzene ND ug/L 08/24/21 21:45 95-50-108/20/21 12:078.8 1
1,3-Dichlorobenzene ND ug/L 08/24/21 21:45 541-73-108/20/21 12:078.8 1
1,4-Dichlorobenzene ND ug/L 08/24/21 21:45 106-46-708/20/21 12:078.8 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 21:45 91-94-108/20/21 12:0717.7 1
2,4-Dichlorophenol ND ug/L 08/24/21 21:45 120-83-208/20/21 12:078.8 1
Diethylphthalate ND ug/L 08/24/21 21:45 84-66-208/20/21 12:078.8 1
2,4-Dimethylphenol ND ug/L 08/24/21 21:45 105-67-908/20/21 12:078.8 1
Dimethylphthalate ND ug/L 08/24/21 21:45 131-11-308/20/21 12:078.8 1
Di-n-butylphthalate ND ug/L 08/24/21 21:45 84-74-208/20/21 12:078.8 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 21:45 534-52-108/20/21 12:0717.7 1
2,4-Dinitrophenol ND ug/L 08/24/21 21:45 51-28-508/20/21 12:0744.2 1
2,4-Dinitrotoluene ND ug/L 08/24/21 21:45 121-14-208/20/21 12:078.8 1
2,6-Dinitrotoluene ND ug/L 08/24/21 21:45 606-20-208/20/21 12:078.8 1
Di-n-octylphthalate ND ug/L 08/24/21 21:45 117-84-008/20/21 12:078.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 21:45 117-81-708/20/21 12:075.3 1
Fluoranthene ND ug/L 08/24/21 21:45 206-44-008/20/21 12:078.8 1
Fluorene ND ug/L 08/24/21 21:45 86-73-708/20/21 12:078.8 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 21:45 87-68-308/20/21 12:078.8 1
Hexachlorobenzene ND ug/L 08/24/21 21:45 118-74-108/20/21 12:078.8 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 21:45 77-47-408/20/21 12:078.8 1
Hexachloroethane ND ug/L 08/24/21 21:45 67-72-108/20/21 12:078.8 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 21:45 193-39-508/20/21 12:078.8 1
Isophorone ND ug/L 08/24/21 21:45 78-59-108/20/21 12:078.8 1
1-Methylnaphthalene ND ug/L 08/24/21 21:45 90-12-008/20/21 12:078.8 1
2-Methylnaphthalene ND ug/L 08/24/21 21:45 91-57-608/20/21 12:078.8 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 21:45 95-48-708/20/21 12:078.8 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 21:45 15831-10-408/20/21 12:078.8 1
Naphthalene ND ug/L 08/24/21 21:45 91-20-308/20/21 12:078.8 1
2-Nitroaniline ND ug/L 08/24/21 21:45 88-74-408/20/21 12:0717.7 1
3-Nitroaniline ND ug/L 08/24/21 21:45 99-09-208/20/21 12:0717.7 1
4-Nitroaniline ND ug/L 08/24/21 21:45 100-01-608/20/21 12:0717.7 1
Nitrobenzene ND ug/L 08/24/21 21:45 98-95-308/20/21 12:078.8 1
2-Nitrophenol ND ug/L 08/24/21 21:45 88-75-508/20/21 12:078.8 1
4-Nitrophenol ND ug/L 08/24/21 21:45 100-02-708/20/21 12:0744.2 1
N-Nitrosodimethylamine ND ug/L 08/24/21 21:45 62-75-908/20/21 12:078.8 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 21:45 621-64-708/20/21 12:078.8 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 21:45 86-30-608/20/21 12:078.8 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 21:45 108-60-108/20/21 12:078.8 1
Pentachlorophenol ND ug/L 08/24/21 21:45 87-86-508/20/21 12:0717.7 1
Phenanthrene ND ug/L 08/24/21 21:45 85-01-808/20/21 12:078.8 1
Phenol ND ug/L 08/24/21 21:45 108-95-208/20/21 12:078.8 1
Pyrene ND ug/L 08/24/21 21:45 129-00-008/20/21 12:078.8 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 21:45 120-82-108/20/21 12:078.8 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 21:45 95-95-408/20/21 12:078.8 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 21:45 88-06-208/20/21 12:078.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-7 Lab ID:92556378007 Collected:08/16/21 12:10 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
Nitrobenzene-d5 (S)58 %08/24/21 21:45 4165-60-008/20/21 12:0710-144 1
2-Fluorobiphenyl (S)40 %08/24/21 21:45 321-60-808/20/21 12:0710-130 1
Terphenyl-d14 (S)95 %08/24/21 21:45 1718-51-008/20/21 12:0734-163 1
Phenol-d6 (S)36 %08/24/21 21:45 13127-88-308/20/21 12:0710-130 1
2-Fluorophenol (S)45 %08/24/21 21:45 367-12-408/20/21 12:0710-130 1
2,4,6-Tribromophenol (S)79 %08/24/21 21:45 118-79-608/20/21 12:0710-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 04:19 67-64-125.0 1
Benzene ND ug/L 08/20/21 04:19 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 04:19 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 04:19 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 04:19 75-27-41.0 1
Bromoform ND ug/L 08/20/21 04:19 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 04:19 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 04:19 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 04:19 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 04:19 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 04:19 75-00-3 IL1.0 1
Chloroform 3.5 ug/L 08/20/21 04:19 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 04:19 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 04:19 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 04:19 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 04:19 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 04:19 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 04:19 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 04:19 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 04:19 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 04:19 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 04:19 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 04:19 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 04:19 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 04:19 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 04:19 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 04:19 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 04:19 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 04:19 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 04:19 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 04:19 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 04:19 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 04:19 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 04:19 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 04:19 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 04:19 100-41-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-7 Lab ID:92556378007 Collected:08/16/21 12:10 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 08/20/21 04:19 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 04:19 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 04:19 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 04:19 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 04:19 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 04:19 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 04:19 91-20-31.0 1
Styrene ND ug/L 08/20/21 04:19 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 04:19 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 04:19 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 04:19 127-18-41.0 1
Toluene ND ug/L 08/20/21 04:19 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 04:19 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 04:19 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 04:19 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 04:19 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 04:19 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 04:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 04:19 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 04:19 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 04:19 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 04:19 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 04:19 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 04:19 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %08/20/21 04:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)100 %08/20/21 04:19 17060-07-070-130 1
Toluene-d8 (S)105 %08/20/21 04:19 2037-26-570-130 1
Sample:GW-8 Lab ID:92556378008 Collected:08/16/21 12:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 22:11 83-32-908/23/21 07:249.1 1
Acenaphthylene ND ug/L 08/24/21 22:11 208-96-808/23/21 07:249.1 1
Aniline ND ug/L 08/24/21 22:11 62-53-308/23/21 07:249.1 1
Anthracene ND ug/L 08/24/21 22:11 120-12-708/23/21 07:249.1 1
Benzo(a)anthracene ND ug/L 08/24/21 22:11 56-55-308/23/21 07:249.1 1
Benzo(a)pyrene ND ug/L 08/24/21 22:11 50-32-808/23/21 07:249.1 1
Benzo(b)fluoranthene ND ug/L 08/24/21 22:11 205-99-208/23/21 07:249.1 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 22:11 191-24-208/23/21 07:249.1 1
Benzo(k)fluoranthene ND ug/L 08/24/21 22:11 207-08-908/23/21 07:249.1 1
Benzoic Acid ND ug/L 08/24/21 22:11 65-85-008/23/21 07:2445.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-8 Lab ID:92556378008 Collected:08/16/21 12:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Benzyl alcohol ND ug/L 08/24/21 22:11 100-51-608/23/21 07:2418.2 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 22:11 101-55-308/23/21 07:249.1 1
Butylbenzylphthalate ND ug/L 08/24/21 22:11 85-68-708/23/21 07:249.1 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 22:11 59-50-708/23/21 07:249.1 1
4-Chloroaniline ND ug/L 08/24/21 22:11 106-47-808/23/21 07:2418.2 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 22:11 111-91-108/23/21 07:249.1 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 22:11 111-44-408/23/21 07:249.1 1
2-Chloronaphthalene ND ug/L 08/24/21 22:11 91-58-708/23/21 07:249.1 1
2-Chlorophenol ND ug/L 08/24/21 22:11 95-57-808/23/21 07:249.1 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 22:11 7005-72-308/23/21 07:249.1 1
Chrysene ND ug/L 08/24/21 22:11 218-01-908/23/21 07:249.1 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 22:11 53-70-308/23/21 07:249.1 1
Dibenzofuran ND ug/L 08/24/21 22:11 132-64-908/23/21 07:249.1 1
1,2-Dichlorobenzene ND ug/L 08/24/21 22:11 95-50-108/23/21 07:249.1 1
1,3-Dichlorobenzene ND ug/L 08/24/21 22:11 541-73-108/23/21 07:249.1 1
1,4-Dichlorobenzene ND ug/L 08/24/21 22:11 106-46-708/23/21 07:249.1 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 22:11 91-94-108/23/21 07:2418.2 1
2,4-Dichlorophenol ND ug/L 08/24/21 22:11 120-83-208/23/21 07:249.1 1
Diethylphthalate ND ug/L 08/24/21 22:11 84-66-208/23/21 07:249.1 1
2,4-Dimethylphenol ND ug/L 08/24/21 22:11 105-67-908/23/21 07:249.1 1
Dimethylphthalate ND ug/L 08/24/21 22:11 131-11-308/23/21 07:249.1 1
Di-n-butylphthalate ND ug/L 08/24/21 22:11 84-74-208/23/21 07:249.1 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 22:11 534-52-108/23/21 07:2418.2 1
2,4-Dinitrophenol ND ug/L 08/24/21 22:11 51-28-508/23/21 07:2445.5 1
2,4-Dinitrotoluene ND ug/L 08/24/21 22:11 121-14-208/23/21 07:249.1 1
2,6-Dinitrotoluene ND ug/L 08/24/21 22:11 606-20-208/23/21 07:249.1 1
Di-n-octylphthalate ND ug/L 08/24/21 22:11 117-84-008/23/21 07:249.1 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 22:11 117-81-708/23/21 07:245.5 1
Fluoranthene ND ug/L 08/24/21 22:11 206-44-008/23/21 07:249.1 1
Fluorene ND ug/L 08/24/21 22:11 86-73-708/23/21 07:249.1 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 22:11 87-68-308/23/21 07:249.1 1
Hexachlorobenzene ND ug/L 08/24/21 22:11 118-74-108/23/21 07:249.1 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 22:11 77-47-408/23/21 07:249.1 1
Hexachloroethane ND ug/L 08/24/21 22:11 67-72-108/23/21 07:249.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 22:11 193-39-508/23/21 07:249.1 1
Isophorone ND ug/L 08/24/21 22:11 78-59-108/23/21 07:249.1 1
1-Methylnaphthalene ND ug/L 08/24/21 22:11 90-12-008/23/21 07:249.1 1
2-Methylnaphthalene ND ug/L 08/24/21 22:11 91-57-608/23/21 07:249.1 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 22:11 95-48-708/23/21 07:249.1 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 22:11 15831-10-408/23/21 07:249.1 1
Naphthalene ND ug/L 08/24/21 22:11 91-20-308/23/21 07:249.1 1
2-Nitroaniline ND ug/L 08/24/21 22:11 88-74-408/23/21 07:2418.2 1
3-Nitroaniline ND ug/L 08/24/21 22:11 99-09-208/23/21 07:2418.2 1
4-Nitroaniline ND ug/L 08/24/21 22:11 100-01-608/23/21 07:2418.2 1
Nitrobenzene ND ug/L 08/24/21 22:11 98-95-308/23/21 07:249.1 1
2-Nitrophenol ND ug/L 08/24/21 22:11 88-75-508/23/21 07:249.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-8 Lab ID:92556378008 Collected:08/16/21 12:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
4-Nitrophenol ND ug/L 08/24/21 22:11 100-02-708/23/21 07:2445.5 1
N-Nitrosodimethylamine ND ug/L 08/24/21 22:11 62-75-908/23/21 07:249.1 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 22:11 621-64-708/23/21 07:249.1 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 22:11 86-30-608/23/21 07:249.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 22:11 108-60-108/23/21 07:249.1 1
Pentachlorophenol ND ug/L 08/24/21 22:11 87-86-508/23/21 07:2418.2 1
Phenanthrene ND ug/L 08/24/21 22:11 85-01-808/23/21 07:249.1 1
Phenol ND ug/L 08/24/21 22:11 108-95-208/23/21 07:249.1 1
Pyrene ND ug/L 08/24/21 22:11 129-00-008/23/21 07:249.1 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 22:11 120-82-108/23/21 07:249.1 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 22:11 95-95-408/23/21 07:249.1 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 22:11 88-06-208/23/21 07:249.1 1
Surrogates
Nitrobenzene-d5 (S)65 %08/24/21 22:11 4165-60-008/23/21 07:2410-144 1
2-Fluorobiphenyl (S)47 %08/24/21 22:11 321-60-808/23/21 07:2410-130 1
Terphenyl-d14 (S)85 %08/24/21 22:11 1718-51-008/23/21 07:2434-163 1
Phenol-d6 (S)36 %08/24/21 22:11 13127-88-308/23/21 07:2410-130 1
2-Fluorophenol (S)49 %08/24/21 22:11 367-12-408/23/21 07:2410-130 1
2,4,6-Tribromophenol (S)72 %08/24/21 22:11 118-79-608/23/21 07:2410-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 04:36 67-64-125.0 1
Benzene 3.0 ug/L 08/20/21 04:36 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 04:36 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 04:36 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 04:36 75-27-41.0 1
Bromoform ND ug/L 08/20/21 04:36 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 04:36 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 04:36 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 04:36 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 04:36 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 04:36 75-00-3 IL1.0 1
Chloroform ND ug/L 08/20/21 04:36 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 04:36 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 04:36 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 04:36 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 04:36 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 04:36 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 04:36 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 04:36 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 04:36 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 04:36 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 04:36 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 04:36 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 04:36 75-34-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-8 Lab ID:92556378008 Collected:08/16/21 12:45 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2-Dichloroethane ND ug/L 08/20/21 04:36 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 04:36 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 04:36 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 04:36 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 04:36 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 04:36 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 04:36 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 04:36 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 04:36 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 04:36 10061-02-61.0 1
Diisopropyl ether 2.7 ug/L 08/20/21 04:36 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 04:36 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 04:36 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 04:36 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 04:36 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 04:36 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 04:36 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 04:36 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 04:36 91-20-31.0 1
Styrene ND ug/L 08/20/21 04:36 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 04:36 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 04:36 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 04:36 127-18-41.0 1
Toluene ND ug/L 08/20/21 04:36 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 04:36 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 04:36 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 04:36 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 04:36 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 04:36 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 04:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 04:36 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 04:36 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 04:36 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 04:36 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 04:36 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 04:36 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %08/20/21 04:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/20/21 04:36 17060-07-070-130 1
Toluene-d8 (S)105 %08/20/21 04:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-9 Lab ID:92556378009 Collected:08/16/21 13:20 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 22:37 83-32-908/23/21 07:249.1 1
Acenaphthylene ND ug/L 08/24/21 22:37 208-96-808/23/21 07:249.1 1
Aniline ND ug/L 08/24/21 22:37 62-53-308/23/21 07:249.1 1
Anthracene ND ug/L 08/24/21 22:37 120-12-708/23/21 07:249.1 1
Benzo(a)anthracene ND ug/L 08/24/21 22:37 56-55-308/23/21 07:249.1 1
Benzo(a)pyrene ND ug/L 08/24/21 22:37 50-32-808/23/21 07:249.1 1
Benzo(b)fluoranthene ND ug/L 08/24/21 22:37 205-99-208/23/21 07:249.1 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 22:37 191-24-208/23/21 07:249.1 1
Benzo(k)fluoranthene ND ug/L 08/24/21 22:37 207-08-908/23/21 07:249.1 1
Benzoic Acid ND ug/L 08/24/21 22:37 65-85-008/23/21 07:2445.5 1
Benzyl alcohol ND ug/L 08/24/21 22:37 100-51-608/23/21 07:2418.2 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 22:37 101-55-308/23/21 07:249.1 1
Butylbenzylphthalate ND ug/L 08/24/21 22:37 85-68-708/23/21 07:249.1 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 22:37 59-50-708/23/21 07:249.1 1
4-Chloroaniline ND ug/L 08/24/21 22:37 106-47-808/23/21 07:2418.2 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 22:37 111-91-108/23/21 07:249.1 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 22:37 111-44-408/23/21 07:249.1 1
2-Chloronaphthalene ND ug/L 08/24/21 22:37 91-58-708/23/21 07:249.1 1
2-Chlorophenol ND ug/L 08/24/21 22:37 95-57-808/23/21 07:249.1 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 22:37 7005-72-308/23/21 07:249.1 1
Chrysene ND ug/L 08/24/21 22:37 218-01-908/23/21 07:249.1 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 22:37 53-70-308/23/21 07:249.1 1
Dibenzofuran ND ug/L 08/24/21 22:37 132-64-908/23/21 07:249.1 1
1,2-Dichlorobenzene ND ug/L 08/24/21 22:37 95-50-108/23/21 07:249.1 1
1,3-Dichlorobenzene ND ug/L 08/24/21 22:37 541-73-108/23/21 07:249.1 1
1,4-Dichlorobenzene ND ug/L 08/24/21 22:37 106-46-708/23/21 07:249.1 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 22:37 91-94-108/23/21 07:2418.2 1
2,4-Dichlorophenol ND ug/L 08/24/21 22:37 120-83-208/23/21 07:249.1 1
Diethylphthalate ND ug/L 08/24/21 22:37 84-66-208/23/21 07:249.1 1
2,4-Dimethylphenol ND ug/L 08/24/21 22:37 105-67-908/23/21 07:249.1 1
Dimethylphthalate ND ug/L 08/24/21 22:37 131-11-308/23/21 07:249.1 1
Di-n-butylphthalate ND ug/L 08/24/21 22:37 84-74-208/23/21 07:249.1 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 22:37 534-52-108/23/21 07:2418.2 1
2,4-Dinitrophenol ND ug/L 08/24/21 22:37 51-28-508/23/21 07:2445.5 1
2,4-Dinitrotoluene ND ug/L 08/24/21 22:37 121-14-208/23/21 07:249.1 1
2,6-Dinitrotoluene ND ug/L 08/24/21 22:37 606-20-208/23/21 07:249.1 1
Di-n-octylphthalate ND ug/L 08/24/21 22:37 117-84-008/23/21 07:249.1 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 22:37 117-81-708/23/21 07:245.5 1
Fluoranthene ND ug/L 08/24/21 22:37 206-44-008/23/21 07:249.1 1
Fluorene ND ug/L 08/24/21 22:37 86-73-708/23/21 07:249.1 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 22:37 87-68-308/23/21 07:249.1 1
Hexachlorobenzene ND ug/L 08/24/21 22:37 118-74-108/23/21 07:249.1 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 22:37 77-47-408/23/21 07:249.1 1
Hexachloroethane ND ug/L 08/24/21 22:37 67-72-108/23/21 07:249.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 22:37 193-39-508/23/21 07:249.1 1
Isophorone ND ug/L 08/24/21 22:37 78-59-108/23/21 07:249.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-9 Lab ID:92556378009 Collected:08/16/21 13:20 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
1-Methylnaphthalene ND ug/L 08/24/21 22:37 90-12-008/23/21 07:249.1 1
2-Methylnaphthalene ND ug/L 08/24/21 22:37 91-57-608/23/21 07:249.1 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 22:37 95-48-708/23/21 07:249.1 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 22:37 15831-10-408/23/21 07:249.1 1
Naphthalene ND ug/L 08/24/21 22:37 91-20-308/23/21 07:249.1 1
2-Nitroaniline ND ug/L 08/24/21 22:37 88-74-408/23/21 07:2418.2 1
3-Nitroaniline ND ug/L 08/24/21 22:37 99-09-208/23/21 07:2418.2 1
4-Nitroaniline ND ug/L 08/24/21 22:37 100-01-608/23/21 07:2418.2 1
Nitrobenzene ND ug/L 08/24/21 22:37 98-95-308/23/21 07:249.1 1
2-Nitrophenol ND ug/L 08/24/21 22:37 88-75-508/23/21 07:249.1 1
4-Nitrophenol ND ug/L 08/24/21 22:37 100-02-708/23/21 07:2445.5 1
N-Nitrosodimethylamine ND ug/L 08/24/21 22:37 62-75-908/23/21 07:249.1 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 22:37 621-64-708/23/21 07:249.1 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 22:37 86-30-608/23/21 07:249.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 22:37 108-60-108/23/21 07:249.1 1
Pentachlorophenol ND ug/L 08/24/21 22:37 87-86-508/23/21 07:2418.2 1
Phenanthrene ND ug/L 08/24/21 22:37 85-01-808/23/21 07:249.1 1
Phenol ND ug/L 08/24/21 22:37 108-95-208/23/21 07:249.1 1
Pyrene ND ug/L 08/24/21 22:37 129-00-008/23/21 07:249.1 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 22:37 120-82-108/23/21 07:249.1 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 22:37 95-95-408/23/21 07:249.1 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 22:37 88-06-208/23/21 07:249.1 1
Surrogates
Nitrobenzene-d5 (S)69 %08/24/21 22:37 4165-60-008/23/21 07:2410-144 1
2-Fluorobiphenyl (S)52 %08/24/21 22:37 321-60-808/23/21 07:2410-130 1
Terphenyl-d14 (S)85 %08/24/21 22:37 1718-51-008/23/21 07:2434-163 1
Phenol-d6 (S)39 %08/24/21 22:37 13127-88-308/23/21 07:2410-130 1
2-Fluorophenol (S)52 %08/24/21 22:37 367-12-408/23/21 07:2410-130 1
2,4,6-Tribromophenol (S)69 %08/24/21 22:37 118-79-608/23/21 07:2410-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 04:54 67-64-125.0 1
Benzene 6.8 ug/L 08/20/21 04:54 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 04:54 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 04:54 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 04:54 75-27-41.0 1
Bromoform ND ug/L 08/20/21 04:54 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 04:54 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 04:54 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 04:54 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 04:54 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 04:54 75-00-3 IL1.0 1
Chloroform 3.9 ug/L 08/20/21 04:54 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 04:54 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 04:54 95-49-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-9 Lab ID:92556378009 Collected:08/16/21 13:20 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
4-Chlorotoluene ND ug/L 08/20/21 04:54 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 04:54 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 04:54 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 04:54 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 04:54 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 04:54 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 04:54 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 04:54 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 04:54 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 04:54 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 04:54 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 04:54 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 04:54 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 04:54 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 04:54 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 04:54 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 04:54 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 04:54 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 04:54 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 04:54 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 04:54 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 04:54 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 04:54 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 04:54 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 04:54 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 04:54 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 04:54 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 04:54 1634-04-41.0 1
Naphthalene 1.4 ug/L 08/20/21 04:54 91-20-31.0 1
Styrene ND ug/L 08/20/21 04:54 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 04:54 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 04:54 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 04:54 127-18-41.0 1
Toluene 1.2 ug/L 08/20/21 04:54 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 04:54 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 04:54 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 04:54 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 04:54 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 04:54 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 04:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 04:54 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 04:54 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 04:54 75-01-41.0 1
Xylene (Total)3.1 ug/L 08/20/21 04:54 1330-20-71.0 1
m&p-Xylene 3.1 ug/L 08/20/21 04:54 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 04:54 95-47-61.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-9 Lab ID:92556378009 Collected:08/16/21 13:20 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Surrogates
4-Bromofluorobenzene (S)101 %08/20/21 04:54 460-00-470-130 1
1,2-Dichloroethane-d4 (S)101 %08/20/21 04:54 17060-07-070-130 1
Toluene-d8 (S)103 %08/20/21 04:54 2037-26-570-130 1
Sample:GW-10 Lab ID:92556378010 Collected:08/17/21 10:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 23:04 83-32-908/23/21 07:249.1 1
Acenaphthylene ND ug/L 08/24/21 23:04 208-96-808/23/21 07:249.1 1
Aniline ND ug/L 08/24/21 23:04 62-53-308/23/21 07:249.1 1
Anthracene ND ug/L 08/24/21 23:04 120-12-708/23/21 07:249.1 1
Benzo(a)anthracene ND ug/L 08/24/21 23:04 56-55-308/23/21 07:249.1 1
Benzo(a)pyrene ND ug/L 08/24/21 23:04 50-32-808/23/21 07:249.1 1
Benzo(b)fluoranthene ND ug/L 08/24/21 23:04 205-99-208/23/21 07:249.1 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 23:04 191-24-208/23/21 07:249.1 1
Benzo(k)fluoranthene ND ug/L 08/24/21 23:04 207-08-908/23/21 07:249.1 1
Benzoic Acid ND ug/L 08/24/21 23:04 65-85-008/23/21 07:2445.5 1
Benzyl alcohol ND ug/L 08/24/21 23:04 100-51-608/23/21 07:2418.2 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 23:04 101-55-308/23/21 07:249.1 1
Butylbenzylphthalate ND ug/L 08/24/21 23:04 85-68-708/23/21 07:249.1 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 23:04 59-50-708/23/21 07:249.1 1
4-Chloroaniline ND ug/L 08/24/21 23:04 106-47-808/23/21 07:2418.2 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 23:04 111-91-108/23/21 07:249.1 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 23:04 111-44-408/23/21 07:249.1 1
2-Chloronaphthalene ND ug/L 08/24/21 23:04 91-58-708/23/21 07:249.1 1
2-Chlorophenol ND ug/L 08/24/21 23:04 95-57-808/23/21 07:249.1 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 23:04 7005-72-308/23/21 07:249.1 1
Chrysene ND ug/L 08/24/21 23:04 218-01-908/23/21 07:249.1 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 23:04 53-70-308/23/21 07:249.1 1
Dibenzofuran ND ug/L 08/24/21 23:04 132-64-908/23/21 07:249.1 1
1,2-Dichlorobenzene ND ug/L 08/24/21 23:04 95-50-108/23/21 07:249.1 1
1,3-Dichlorobenzene ND ug/L 08/24/21 23:04 541-73-108/23/21 07:249.1 1
1,4-Dichlorobenzene ND ug/L 08/24/21 23:04 106-46-708/23/21 07:249.1 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 23:04 91-94-108/23/21 07:2418.2 1
2,4-Dichlorophenol ND ug/L 08/24/21 23:04 120-83-208/23/21 07:249.1 1
Diethylphthalate ND ug/L 08/24/21 23:04 84-66-208/23/21 07:249.1 1
2,4-Dimethylphenol ND ug/L 08/24/21 23:04 105-67-908/23/21 07:249.1 1
Dimethylphthalate ND ug/L 08/24/21 23:04 131-11-308/23/21 07:249.1 1
Di-n-butylphthalate ND ug/L 08/24/21 23:04 84-74-208/23/21 07:249.1 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 23:04 534-52-108/23/21 07:2418.2 1
2,4-Dinitrophenol ND ug/L 08/24/21 23:04 51-28-508/23/21 07:2445.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-10 Lab ID:92556378010 Collected:08/17/21 10:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
2,4-Dinitrotoluene ND ug/L 08/24/21 23:04 121-14-208/23/21 07:249.1 1
2,6-Dinitrotoluene ND ug/L 08/24/21 23:04 606-20-208/23/21 07:249.1 1
Di-n-octylphthalate ND ug/L 08/24/21 23:04 117-84-008/23/21 07:249.1 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 23:04 117-81-708/23/21 07:245.5 1
Fluoranthene ND ug/L 08/24/21 23:04 206-44-008/23/21 07:249.1 1
Fluorene ND ug/L 08/24/21 23:04 86-73-708/23/21 07:249.1 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 23:04 87-68-308/23/21 07:249.1 1
Hexachlorobenzene ND ug/L 08/24/21 23:04 118-74-108/23/21 07:249.1 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 23:04 77-47-408/23/21 07:249.1 1
Hexachloroethane ND ug/L 08/24/21 23:04 67-72-108/23/21 07:249.1 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 23:04 193-39-508/23/21 07:249.1 1
Isophorone ND ug/L 08/24/21 23:04 78-59-108/23/21 07:249.1 1
1-Methylnaphthalene ND ug/L 08/24/21 23:04 90-12-008/23/21 07:249.1 1
2-Methylnaphthalene ND ug/L 08/24/21 23:04 91-57-608/23/21 07:249.1 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 23:04 95-48-708/23/21 07:249.1 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 23:04 15831-10-408/23/21 07:249.1 1
Naphthalene ND ug/L 08/24/21 23:04 91-20-308/23/21 07:249.1 1
2-Nitroaniline ND ug/L 08/24/21 23:04 88-74-408/23/21 07:2418.2 1
3-Nitroaniline ND ug/L 08/24/21 23:04 99-09-208/23/21 07:2418.2 1
4-Nitroaniline ND ug/L 08/24/21 23:04 100-01-608/23/21 07:2418.2 1
Nitrobenzene ND ug/L 08/24/21 23:04 98-95-308/23/21 07:249.1 1
2-Nitrophenol ND ug/L 08/24/21 23:04 88-75-508/23/21 07:249.1 1
4-Nitrophenol ND ug/L 08/24/21 23:04 100-02-708/23/21 07:2445.5 1
N-Nitrosodimethylamine ND ug/L 08/24/21 23:04 62-75-908/23/21 07:249.1 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 23:04 621-64-708/23/21 07:249.1 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 23:04 86-30-608/23/21 07:249.1 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 23:04 108-60-108/23/21 07:249.1 1
Pentachlorophenol ND ug/L 08/24/21 23:04 87-86-508/23/21 07:2418.2 1
Phenanthrene ND ug/L 08/24/21 23:04 85-01-808/23/21 07:249.1 1
Phenol ND ug/L 08/24/21 23:04 108-95-208/23/21 07:249.1 1
Pyrene ND ug/L 08/24/21 23:04 129-00-008/23/21 07:249.1 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 23:04 120-82-108/23/21 07:249.1 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 23:04 95-95-408/23/21 07:249.1 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 23:04 88-06-208/23/21 07:249.1 1
Surrogates
Nitrobenzene-d5 (S)87 %08/24/21 23:04 4165-60-008/23/21 07:2410-144 1
2-Fluorobiphenyl (S)67 %08/24/21 23:04 321-60-808/23/21 07:2410-130 1
Terphenyl-d14 (S)103 %08/24/21 23:04 1718-51-008/23/21 07:2434-163 1
Phenol-d6 (S)49 %08/24/21 23:04 13127-88-308/23/21 07:2410-130 1
2-Fluorophenol (S)68 %08/24/21 23:04 367-12-408/23/21 07:2410-130 1
2,4,6-Tribromophenol (S)95 %08/24/21 23:04 118-79-608/23/21 07:2410-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 05:12 67-64-125.0 1
Benzene ND ug/L 08/20/21 05:12 71-43-21.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-10 Lab ID:92556378010 Collected:08/17/21 10:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Bromobenzene ND ug/L 08/20/21 05:12 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 05:12 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 05:12 75-27-41.0 1
Bromoform ND ug/L 08/20/21 05:12 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 05:12 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 05:12 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 05:12 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 05:12 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 05:12 75-00-3 IL1.0 1
Chloroform ND ug/L 08/20/21 05:12 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 05:12 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 05:12 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 05:12 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 05:12 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 05:12 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 05:12 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 05:12 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 05:12 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 05:12 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 05:12 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 05:12 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 05:12 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 05:12 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 05:12 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 05:12 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 05:12 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 05:12 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 05:12 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 05:12 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 05:12 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 05:12 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 05:12 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 05:12 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 05:12 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 08/20/21 05:12 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 05:12 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 05:12 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 05:12 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 05:12 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 05:12 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 05:12 91-20-31.0 1
Styrene ND ug/L 08/20/21 05:12 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 05:12 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 05:12 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 05:12 127-18-41.0 1
Toluene ND ug/L 08/20/21 05:12 108-88-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-10 Lab ID:92556378010 Collected:08/17/21 10:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
1,2,3-Trichlorobenzene ND ug/L 08/20/21 05:12 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 05:12 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 05:12 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 05:12 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 05:12 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 05:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 05:12 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 05:12 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 05:12 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 05:12 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 05:12 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 05:12 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)102 %08/20/21 05:12 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %08/20/21 05:12 17060-07-070-130 1
Toluene-d8 (S)105 %08/20/21 05:12 2037-26-570-130 1
Sample:GW-11 Lab ID:92556378011 Collected:08/17/21 11:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 08/24/21 23:30 83-32-908/23/21 07:2410.0 1
Acenaphthylene ND ug/L 08/24/21 23:30 208-96-808/23/21 07:2410.0 1
Aniline ND ug/L 08/24/21 23:30 62-53-308/23/21 07:2410.0 1
Anthracene ND ug/L 08/24/21 23:30 120-12-708/23/21 07:2410.0 1
Benzo(a)anthracene ND ug/L 08/24/21 23:30 56-55-308/23/21 07:2410.0 1
Benzo(a)pyrene ND ug/L 08/24/21 23:30 50-32-808/23/21 07:2410.0 1
Benzo(b)fluoranthene ND ug/L 08/24/21 23:30 205-99-208/23/21 07:2410.0 1
Benzo(g,h,i)perylene ND ug/L 08/24/21 23:30 191-24-208/23/21 07:2410.0 1
Benzo(k)fluoranthene ND ug/L 08/24/21 23:30 207-08-908/23/21 07:2410.0 1
Benzoic Acid ND ug/L 08/24/21 23:30 65-85-008/23/21 07:2450.0 1
Benzyl alcohol ND ug/L 08/24/21 23:30 100-51-608/23/21 07:2420.0 1
4-Bromophenylphenyl ether ND ug/L 08/24/21 23:30 101-55-308/23/21 07:2410.0 1
Butylbenzylphthalate ND ug/L 08/24/21 23:30 85-68-708/23/21 07:2410.0 1
4-Chloro-3-methylphenol ND ug/L 08/24/21 23:30 59-50-708/23/21 07:2410.0 1
4-Chloroaniline ND ug/L 08/24/21 23:30 106-47-808/23/21 07:2420.0 1
bis(2-Chloroethoxy)methane ND ug/L 08/24/21 23:30 111-91-108/23/21 07:2410.0 1
bis(2-Chloroethyl) ether ND ug/L 08/24/21 23:30 111-44-408/23/21 07:2410.0 1
2-Chloronaphthalene ND ug/L 08/24/21 23:30 91-58-708/23/21 07:2410.0 1
2-Chlorophenol ND ug/L 08/24/21 23:30 95-57-808/23/21 07:2410.0 1
4-Chlorophenylphenyl ether ND ug/L 08/24/21 23:30 7005-72-308/23/21 07:2410.0 1
Chrysene ND ug/L 08/24/21 23:30 218-01-908/23/21 07:2410.0 1
Dibenz(a,h)anthracene ND ug/L 08/24/21 23:30 53-70-308/23/21 07:2410.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-11 Lab ID:92556378011 Collected:08/17/21 11:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Dibenzofuran ND ug/L 08/24/21 23:30 132-64-908/23/21 07:2410.0 1
1,2-Dichlorobenzene ND ug/L 08/24/21 23:30 95-50-108/23/21 07:2410.0 1
1,3-Dichlorobenzene ND ug/L 08/24/21 23:30 541-73-108/23/21 07:2410.0 1
1,4-Dichlorobenzene ND ug/L 08/24/21 23:30 106-46-708/23/21 07:2410.0 1
3,3'-Dichlorobenzidine ND ug/L 08/24/21 23:30 91-94-108/23/21 07:2420.0 1
2,4-Dichlorophenol ND ug/L 08/24/21 23:30 120-83-208/23/21 07:2410.0 1
Diethylphthalate ND ug/L 08/24/21 23:30 84-66-208/23/21 07:2410.0 1
2,4-Dimethylphenol ND ug/L 08/24/21 23:30 105-67-908/23/21 07:2410.0 1
Dimethylphthalate ND ug/L 08/24/21 23:30 131-11-308/23/21 07:2410.0 1
Di-n-butylphthalate ND ug/L 08/24/21 23:30 84-74-208/23/21 07:2410.0 1
4,6-Dinitro-2-methylphenol ND ug/L 08/24/21 23:30 534-52-108/23/21 07:2420.0 1
2,4-Dinitrophenol ND ug/L 08/24/21 23:30 51-28-508/23/21 07:2450.0 1
2,4-Dinitrotoluene ND ug/L 08/24/21 23:30 121-14-208/23/21 07:2410.0 1
2,6-Dinitrotoluene ND ug/L 08/24/21 23:30 606-20-208/23/21 07:2410.0 1
Di-n-octylphthalate ND ug/L 08/24/21 23:30 117-84-008/23/21 07:2410.0 1
bis(2-Ethylhexyl)phthalate ND ug/L 08/24/21 23:30 117-81-708/23/21 07:246.0 1
Fluoranthene ND ug/L 08/24/21 23:30 206-44-008/23/21 07:2410.0 1
Fluorene ND ug/L 08/24/21 23:30 86-73-708/23/21 07:2410.0 1
Hexachloro-1,3-butadiene ND ug/L 08/24/21 23:30 87-68-308/23/21 07:2410.0 1
Hexachlorobenzene ND ug/L 08/24/21 23:30 118-74-108/23/21 07:2410.0 1
Hexachlorocyclopentadiene ND ug/L 08/24/21 23:30 77-47-408/23/21 07:2410.0 1
Hexachloroethane ND ug/L 08/24/21 23:30 67-72-108/23/21 07:2410.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 08/24/21 23:30 193-39-508/23/21 07:2410.0 1
Isophorone ND ug/L 08/24/21 23:30 78-59-108/23/21 07:2410.0 1
1-Methylnaphthalene ND ug/L 08/24/21 23:30 90-12-008/23/21 07:2410.0 1
2-Methylnaphthalene ND ug/L 08/24/21 23:30 91-57-608/23/21 07:2410.0 1
2-Methylphenol(o-Cresol)ND ug/L 08/24/21 23:30 95-48-708/23/21 07:2410.0 1
3&4-Methylphenol(m&p Cresol)ND ug/L 08/24/21 23:30 15831-10-408/23/21 07:2410.0 1
Naphthalene ND ug/L 08/24/21 23:30 91-20-308/23/21 07:2410.0 1
2-Nitroaniline ND ug/L 08/24/21 23:30 88-74-408/23/21 07:2420.0 1
3-Nitroaniline ND ug/L 08/24/21 23:30 99-09-208/23/21 07:2420.0 1
4-Nitroaniline ND ug/L 08/24/21 23:30 100-01-608/23/21 07:2420.0 1
Nitrobenzene ND ug/L 08/24/21 23:30 98-95-308/23/21 07:2410.0 1
2-Nitrophenol ND ug/L 08/24/21 23:30 88-75-508/23/21 07:2410.0 1
4-Nitrophenol ND ug/L 08/24/21 23:30 100-02-708/23/21 07:2450.0 1
N-Nitrosodimethylamine ND ug/L 08/24/21 23:30 62-75-908/23/21 07:2410.0 1
N-Nitroso-di-n-propylamine ND ug/L 08/24/21 23:30 621-64-708/23/21 07:2410.0 1
N-Nitrosodiphenylamine ND ug/L 08/24/21 23:30 86-30-608/23/21 07:2410.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 08/24/21 23:30 108-60-108/23/21 07:2410.0 1
Pentachlorophenol ND ug/L 08/24/21 23:30 87-86-508/23/21 07:2420.0 1
Phenanthrene ND ug/L 08/24/21 23:30 85-01-808/23/21 07:2410.0 1
Phenol ND ug/L 08/24/21 23:30 108-95-208/23/21 07:2410.0 1
Pyrene ND ug/L 08/24/21 23:30 129-00-008/23/21 07:2410.0 1
1,2,4-Trichlorobenzene ND ug/L 08/24/21 23:30 120-82-108/23/21 07:2410.0 1
2,4,5-Trichlorophenol ND ug/L 08/24/21 23:30 95-95-408/23/21 07:2410.0 1
2,4,6-Trichlorophenol ND ug/L 08/24/21 23:30 88-06-208/23/21 07:2410.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-11 Lab ID:92556378011 Collected:08/17/21 11:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Surrogates
Nitrobenzene-d5 (S)79 %08/24/21 23:30 4165-60-008/23/21 07:2410-144 1
2-Fluorobiphenyl (S)61 %08/24/21 23:30 321-60-808/23/21 07:2410-130 1
Terphenyl-d14 (S)100 %08/24/21 23:30 1718-51-008/23/21 07:2434-163 1
Phenol-d6 (S)42 %08/24/21 23:30 13127-88-308/23/21 07:2410-130 1
2-Fluorophenol (S)56 %08/24/21 23:30 367-12-408/23/21 07:2410-130 1
2,4,6-Tribromophenol (S)84 %08/24/21 23:30 118-79-608/23/21 07:2410-144 1
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Acetone ND ug/L 08/20/21 05:29 67-64-125.0 1
Benzene ND ug/L 08/20/21 05:29 71-43-21.0 1
Bromobenzene ND ug/L 08/20/21 05:29 108-86-11.0 1
Bromochloromethane ND ug/L 08/20/21 05:29 74-97-51.0 1
Bromodichloromethane ND ug/L 08/20/21 05:29 75-27-41.0 1
Bromoform ND ug/L 08/20/21 05:29 75-25-21.0 1
Bromomethane ND ug/L 08/20/21 05:29 74-83-92.0 1
2-Butanone (MEK)ND ug/L 08/20/21 05:29 78-93-35.0 1
Carbon tetrachloride ND ug/L 08/20/21 05:29 56-23-51.0 1
Chlorobenzene ND ug/L 08/20/21 05:29 108-90-71.0 1
Chloroethane ND ug/L 08/20/21 05:29 75-00-3 IL1.0 1
Chloroform 1.4 ug/L 08/20/21 05:29 67-66-31.0 1
Chloromethane ND ug/L 08/20/21 05:29 74-87-3 v21.0 1
2-Chlorotoluene ND ug/L 08/20/21 05:29 95-49-81.0 1
4-Chlorotoluene ND ug/L 08/20/21 05:29 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 08/20/21 05:29 96-12-82.0 1
Dibromochloromethane ND ug/L 08/20/21 05:29 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 08/20/21 05:29 106-93-41.0 1
Dibromomethane ND ug/L 08/20/21 05:29 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 08/20/21 05:29 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 08/20/21 05:29 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 08/20/21 05:29 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 08/20/21 05:29 75-71-81.0 1
1,1-Dichloroethane ND ug/L 08/20/21 05:29 75-34-31.0 1
1,2-Dichloroethane ND ug/L 08/20/21 05:29 107-06-21.0 1
1,1-Dichloroethene ND ug/L 08/20/21 05:29 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 08/20/21 05:29 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 08/20/21 05:29 156-60-51.0 1
1,2-Dichloropropane ND ug/L 08/20/21 05:29 78-87-51.0 1
1,3-Dichloropropane ND ug/L 08/20/21 05:29 142-28-91.0 1
2,2-Dichloropropane ND ug/L 08/20/21 05:29 594-20-71.0 1
1,1-Dichloropropene ND ug/L 08/20/21 05:29 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 08/20/21 05:29 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 08/20/21 05:29 10061-02-61.0 1
Diisopropyl ether ND ug/L 08/20/21 05:29 108-20-31.0 1
Ethylbenzene ND ug/L 08/20/21 05:29 100-41-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:GW-11 Lab ID:92556378011 Collected:08/17/21 11:00 Received:08/18/21 11:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV Low Level
Hexachloro-1,3-butadiene ND ug/L 08/20/21 05:29 87-68-32.0 1
2-Hexanone ND ug/L 08/20/21 05:29 591-78-65.0 1
p-Isopropyltoluene ND ug/L 08/20/21 05:29 99-87-61.0 1
Methylene Chloride ND ug/L 08/20/21 05:29 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 08/20/21 05:29 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 08/20/21 05:29 1634-04-41.0 1
Naphthalene ND ug/L 08/20/21 05:29 91-20-31.0 1
Styrene ND ug/L 08/20/21 05:29 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 08/20/21 05:29 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 08/20/21 05:29 79-34-51.0 1
Tetrachloroethene ND ug/L 08/20/21 05:29 127-18-41.0 1
Toluene ND ug/L 08/20/21 05:29 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 08/20/21 05:29 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 08/20/21 05:29 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 08/20/21 05:29 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 08/20/21 05:29 79-00-51.0 1
Trichloroethene ND ug/L 08/20/21 05:29 79-01-61.0 1
Trichlorofluoromethane ND ug/L 08/20/21 05:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 08/20/21 05:29 96-18-41.0 1
Vinyl acetate ND ug/L 08/20/21 05:29 108-05-42.0 1
Vinyl chloride ND ug/L 08/20/21 05:29 75-01-41.0 1
Xylene (Total)ND ug/L 08/20/21 05:29 1330-20-71.0 1
m&p-Xylene ND ug/L 08/20/21 05:29 179601-23-12.0 1
o-Xylene ND ug/L 08/20/21 05:29 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)101 %08/20/21 05:29 460-00-470-130 1
1,2-Dichloroethane-d4 (S)99 %08/20/21 05:29 17060-07-070-130 1
Toluene-d8 (S)104 %08/20/21 05:29 2037-26-570-130 1
Sample:SS-1 Lab ID:92556378012 Collected:08/16/21 12:30 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/26/21 07:22 83-32-908/25/21 14:150.44 1
Acenaphthylene ND mg/kg 08/26/21 07:22 208-96-808/25/21 14:150.44 1
Aniline ND mg/kg 08/26/21 07:22 62-53-308/25/21 14:150.44 1
Anthracene ND mg/kg 08/26/21 07:22 120-12-708/25/21 14:150.44 1
Benzo(a)anthracene ND mg/kg 08/26/21 07:22 56-55-308/25/21 14:150.44 1
Benzo(a)pyrene ND mg/kg 08/26/21 07:22 50-32-808/25/21 14:150.44 1
Benzo(b)fluoranthene ND mg/kg 08/26/21 07:22 205-99-208/25/21 14:150.44 1
Benzo(g,h,i)perylene ND mg/kg 08/26/21 07:22 191-24-208/25/21 14:150.44 1
Benzo(k)fluoranthene ND mg/kg 08/26/21 07:22 207-08-908/25/21 14:150.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-1 Lab ID:92556378012 Collected:08/16/21 12:30 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Benzoic Acid ND mg/kg 08/26/21 07:22 65-85-008/25/21 14:152.2 1
Benzyl alcohol ND mg/kg 08/26/21 07:22 100-51-608/25/21 14:150.89 1
4-Bromophenylphenyl ether ND mg/kg 08/26/21 07:22 101-55-308/25/21 14:150.44 1
Butylbenzylphthalate ND mg/kg 08/26/21 07:22 85-68-708/25/21 14:150.44 1
4-Chloro-3-methylphenol ND mg/kg 08/26/21 07:22 59-50-708/25/21 14:150.89 1
4-Chloroaniline ND mg/kg 08/26/21 07:22 106-47-808/25/21 14:150.89 1
bis(2-Chloroethoxy)methane ND mg/kg 08/26/21 07:22 111-91-108/25/21 14:150.44 1
bis(2-Chloroethyl) ether ND mg/kg 08/26/21 07:22 111-44-408/25/21 14:150.44 1
2-Chloronaphthalene ND mg/kg 08/26/21 07:22 91-58-708/25/21 14:150.44 1
2-Chlorophenol ND mg/kg 08/26/21 07:22 95-57-808/25/21 14:150.44 1
4-Chlorophenylphenyl ether ND mg/kg 08/26/21 07:22 7005-72-308/25/21 14:150.44 1
Chrysene ND mg/kg 08/26/21 07:22 218-01-908/25/21 14:150.44 1
Dibenz(a,h)anthracene ND mg/kg 08/26/21 07:22 53-70-308/25/21 14:150.44 1
Dibenzofuran ND mg/kg 08/26/21 07:22 132-64-908/25/21 14:150.44 1
1,2-Dichlorobenzene ND mg/kg 08/26/21 07:22 95-50-108/25/21 14:150.44 1
1,3-Dichlorobenzene ND mg/kg 08/26/21 07:22 541-73-108/25/21 14:150.44 1
1,4-Dichlorobenzene ND mg/kg 08/26/21 07:22 106-46-708/25/21 14:150.44 1
3,3'-Dichlorobenzidine ND mg/kg 08/26/21 07:22 91-94-1 IL08/25/21 14:150.89 1
2,4-Dichlorophenol ND mg/kg 08/26/21 07:22 120-83-208/25/21 14:150.44 1
Diethylphthalate ND mg/kg 08/26/21 07:22 84-66-208/25/21 14:150.44 1
2,4-Dimethylphenol ND mg/kg 08/26/21 07:22 105-67-908/25/21 14:150.44 1
Dimethylphthalate ND mg/kg 08/26/21 07:22 131-11-308/25/21 14:150.44 1
Di-n-butylphthalate ND mg/kg 08/26/21 07:22 84-74-208/25/21 14:150.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/26/21 07:22 534-52-1 v108/25/21 14:150.89 1
2,4-Dinitrophenol ND mg/kg 08/26/21 07:22 51-28-5 v108/25/21 14:152.2 1
2,4-Dinitrotoluene ND mg/kg 08/26/21 07:22 121-14-208/25/21 14:150.44 1
2,6-Dinitrotoluene ND mg/kg 08/26/21 07:22 606-20-208/25/21 14:150.44 1
Di-n-octylphthalate ND mg/kg 08/26/21 07:22 117-84-008/25/21 14:150.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/26/21 07:22 117-81-708/25/21 14:150.44 1
Fluoranthene ND mg/kg 08/26/21 07:22 206-44-008/25/21 14:150.44 1
Fluorene ND mg/kg 08/26/21 07:22 86-73-708/25/21 14:150.44 1
Hexachloro-1,3-butadiene ND mg/kg 08/26/21 07:22 87-68-308/25/21 14:150.44 1
Hexachlorobenzene ND mg/kg 08/26/21 07:22 118-74-108/25/21 14:150.44 1
Hexachlorocyclopentadiene ND mg/kg 08/26/21 07:22 77-47-408/25/21 14:150.44 1
Hexachloroethane ND mg/kg 08/26/21 07:22 67-72-108/25/21 14:150.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/26/21 07:22 193-39-508/25/21 14:150.44 1
Isophorone ND mg/kg 08/26/21 07:22 78-59-108/25/21 14:150.44 1
1-Methylnaphthalene ND mg/kg 08/26/21 07:22 90-12-008/25/21 14:150.44 1
2-Methylnaphthalene ND mg/kg 08/26/21 07:22 91-57-608/25/21 14:150.44 1
2-Methylphenol(o-Cresol)ND mg/kg 08/26/21 07:22 95-48-708/25/21 14:150.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/26/21 07:22 15831-10-408/25/21 14:150.44 1
Naphthalene ND mg/kg 08/26/21 07:22 91-20-308/25/21 14:150.44 1
2-Nitroaniline ND mg/kg 08/26/21 07:22 88-74-408/25/21 14:152.2 1
3-Nitroaniline ND mg/kg 08/26/21 07:22 99-09-2 IL08/25/21 14:152.2 1
4-Nitroaniline ND mg/kg 08/26/21 07:22 100-01-608/25/21 14:150.89 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-1 Lab ID:92556378012 Collected:08/16/21 12:30 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Nitrobenzene ND mg/kg 08/26/21 07:22 98-95-308/25/21 14:150.44 1
2-Nitrophenol ND mg/kg 08/26/21 07:22 88-75-508/25/21 14:150.44 1
4-Nitrophenol ND mg/kg 08/26/21 07:22 100-02-708/25/21 14:152.2 1
N-Nitrosodimethylamine ND mg/kg 08/26/21 07:22 62-75-9 v108/25/21 14:150.44 1
N-Nitroso-di-n-propylamine ND mg/kg 08/26/21 07:22 621-64-708/25/21 14:150.44 1
N-Nitrosodiphenylamine ND mg/kg 08/26/21 07:22 86-30-608/25/21 14:150.44 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/26/21 07:22 108-60-108/25/21 14:150.44 1
Pentachlorophenol ND mg/kg 08/26/21 07:22 87-86-508/25/21 14:150.89 1
Phenanthrene ND mg/kg 08/26/21 07:22 85-01-808/25/21 14:150.44 1
Phenol ND mg/kg 08/26/21 07:22 108-95-2 v108/25/21 14:150.44 1
Pyrene ND mg/kg 08/26/21 07:22 129-00-008/25/21 14:150.44 1
Pyridine ND mg/kg 08/26/21 07:22 110-86-1 v108/25/21 14:150.44 1
1,2,4-Trichlorobenzene ND mg/kg 08/26/21 07:22 120-82-108/25/21 14:150.44 1
2,4,5-Trichlorophenol ND mg/kg 08/26/21 07:22 95-95-408/25/21 14:150.44 1
2,4,6-Trichlorophenol ND mg/kg 08/26/21 07:22 88-06-208/25/21 14:150.44 1
Surrogates
Nitrobenzene-d5 (S)40 %08/26/21 07:22 4165-60-008/25/21 14:1521-130 1
2-Fluorobiphenyl (S)22 %08/26/21 07:22 321-60-808/25/21 14:1519-130 1
Terphenyl-d14 (S)17 %08/26/21 07:22 1718-51-008/25/21 14:1515-130 1
Phenol-d6 (S)45 %08/26/21 07:22 13127-88-308/25/21 14:1518-130 1
2-Fluorophenol (S)44 %08/26/21 07:22 367-12-408/25/21 14:1518-130 1
2,4,6-Tribromophenol (S)42 %08/26/21 07:22 118-79-608/25/21 14:1518-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/23/21 21:23 67-64-108/23/21 13:030.64 4
Benzene ND mg/kg 08/23/21 21:23 71-43-208/23/21 13:030.032 4
Bromobenzene ND mg/kg 08/23/21 21:23 108-86-108/23/21 13:030.032 4
Bromochloromethane ND mg/kg 08/23/21 21:23 74-97-508/23/21 13:030.032 4
Bromodichloromethane ND mg/kg 08/23/21 21:23 75-27-408/23/21 13:030.032 4
Bromoform ND mg/kg 08/23/21 21:23 75-25-208/23/21 13:030.032 4
Bromomethane ND mg/kg 08/23/21 21:23 74-83-9 v108/23/21 13:030.064 4
2-Butanone (MEK)ND mg/kg 08/23/21 21:23 78-93-308/23/21 13:030.64 4
n-Butylbenzene ND mg/kg 08/23/21 21:23 104-51-808/23/21 13:030.032 4
sec-Butylbenzene 0.18 mg/kg 08/23/21 21:23 135-98-808/23/21 13:030.032 4
tert-Butylbenzene ND mg/kg 08/23/21 21:23 98-06-608/23/21 13:030.032 4
Carbon tetrachloride ND mg/kg 08/23/21 21:23 56-23-508/23/21 13:030.032 4
Chlorobenzene ND mg/kg 08/23/21 21:23 108-90-708/23/21 13:030.032 4
Chloroethane ND mg/kg 08/23/21 21:23 75-00-3 v108/23/21 13:030.064 4
Chloroform ND mg/kg 08/23/21 21:23 67-66-308/23/21 13:030.032 4
Chloromethane ND mg/kg 08/23/21 21:23 74-87-308/23/21 13:030.064 4
2-Chlorotoluene ND mg/kg 08/23/21 21:23 95-49-808/23/21 13:030.032 4
4-Chlorotoluene ND mg/kg 08/23/21 21:23 106-43-408/23/21 13:030.032 4
1,2-Dibromo-3-chloropropane ND mg/kg 08/23/21 21:23 96-12-808/23/21 13:030.032 4
Dibromochloromethane ND mg/kg 08/23/21 21:23 124-48-108/23/21 13:030.032 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-1 Lab ID:92556378012 Collected:08/16/21 12:30 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dibromoethane (EDB)ND mg/kg 08/23/21 21:23 106-93-408/23/21 13:030.032 4
Dibromomethane ND mg/kg 08/23/21 21:23 74-95-308/23/21 13:030.032 4
1,2-Dichlorobenzene ND mg/kg 08/23/21 21:23 95-50-108/23/21 13:030.032 4
1,3-Dichlorobenzene ND mg/kg 08/23/21 21:23 541-73-108/23/21 13:030.032 4
1,4-Dichlorobenzene ND mg/kg 08/23/21 21:23 106-46-708/23/21 13:030.032 4
Dichlorodifluoromethane ND mg/kg 08/23/21 21:23 75-71-8 IK,v108/23/21 13:030.064 4
1,1-Dichloroethane ND mg/kg 08/23/21 21:23 75-34-308/23/21 13:030.032 4
1,2-Dichloroethane ND mg/kg 08/23/21 21:23 107-06-208/23/21 13:030.032 4
1,1-Dichloroethene ND mg/kg 08/23/21 21:23 75-35-408/23/21 13:030.032 4
cis-1,2-Dichloroethene ND mg/kg 08/23/21 21:23 156-59-208/23/21 13:030.032 4
trans-1,2-Dichloroethene ND mg/kg 08/23/21 21:23 156-60-508/23/21 13:030.032 4
1,2-Dichloropropane ND mg/kg 08/23/21 21:23 78-87-508/23/21 13:030.032 4
1,3-Dichloropropane ND mg/kg 08/23/21 21:23 142-28-908/23/21 13:030.032 4
2,2-Dichloropropane ND mg/kg 08/23/21 21:23 594-20-708/23/21 13:030.032 4
1,1-Dichloropropene ND mg/kg 08/23/21 21:23 563-58-608/23/21 13:030.032 4
cis-1,3-Dichloropropene ND mg/kg 08/23/21 21:23 10061-01-508/23/21 13:030.032 4
trans-1,3-Dichloropropene ND mg/kg 08/23/21 21:23 10061-02-608/23/21 13:030.032 4
Diisopropyl ether ND mg/kg 08/23/21 21:23 108-20-308/23/21 13:030.032 4
Ethylbenzene ND mg/kg 08/23/21 21:23 100-41-408/23/21 13:030.032 4
Hexachloro-1,3-butadiene ND mg/kg 08/23/21 21:23 87-68-308/23/21 13:030.064 4
2-Hexanone ND mg/kg 08/23/21 21:23 591-78-608/23/21 13:030.32 4
Isopropylbenzene (Cumene)ND mg/kg 08/23/21 21:23 98-82-808/23/21 13:030.032 4
p-Isopropyltoluene ND mg/kg 08/23/21 21:23 99-87-608/23/21 13:030.032 4
Methylene Chloride 0.67 mg/kg 08/23/21 21:23 75-09-208/23/21 13:030.13 4
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/23/21 21:23 108-10-108/23/21 13:030.32 4
Methyl-tert-butyl ether ND mg/kg 08/23/21 21:23 1634-04-408/23/21 13:030.032 4
Naphthalene ND mg/kg 08/23/21 21:23 91-20-308/23/21 13:030.032 4
n-Propylbenzene ND mg/kg 08/23/21 21:23 103-65-108/23/21 13:030.032 4
Styrene ND mg/kg 08/23/21 21:23 100-42-508/23/21 13:030.032 4
1,1,1,2-Tetrachloroethane ND mg/kg 08/23/21 21:23 630-20-608/23/21 13:030.032 4
1,1,2,2-Tetrachloroethane ND mg/kg 08/23/21 21:23 79-34-508/23/21 13:030.032 4
Tetrachloroethene ND mg/kg 08/23/21 21:23 127-18-408/23/21 13:030.032 4
Toluene ND mg/kg 08/23/21 21:23 108-88-308/23/21 13:030.032 4
1,2,3-Trichlorobenzene ND mg/kg 08/23/21 21:23 87-61-608/23/21 13:030.032 4
1,2,4-Trichlorobenzene ND mg/kg 08/23/21 21:23 120-82-108/23/21 13:030.032 4
1,1,1-Trichloroethane ND mg/kg 08/23/21 21:23 71-55-608/23/21 13:030.032 4
1,1,2-Trichloroethane ND mg/kg 08/23/21 21:23 79-00-508/23/21 13:030.032 4
Trichloroethene ND mg/kg 08/23/21 21:23 79-01-608/23/21 13:030.032 4
Trichlorofluoromethane ND mg/kg 08/23/21 21:23 75-69-408/23/21 13:030.032 4
1,2,3-Trichloropropane ND mg/kg 08/23/21 21:23 96-18-408/23/21 13:030.032 4
1,2,4-Trimethylbenzene ND mg/kg 08/23/21 21:23 95-63-608/23/21 13:030.032 4
1,3,5-Trimethylbenzene ND mg/kg 08/23/21 21:23 108-67-808/23/21 13:030.032 4
Vinyl acetate ND mg/kg 08/23/21 21:23 108-05-408/23/21 13:030.32 4
Vinyl chloride ND mg/kg 08/23/21 21:23 75-01-4 v108/23/21 13:030.064 4
Xylene (Total)0.096 mg/kg 08/23/21 21:23 1330-20-708/23/21 13:030.064 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-1 Lab ID:92556378012 Collected:08/16/21 12:30 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
m&p-Xylene 0.096 mg/kg 08/23/21 21:23 179601-23-108/23/21 13:030.064 4
o-Xylene ND mg/kg 08/23/21 21:23 95-47-608/23/21 13:030.032 4
Surrogates
Toluene-d8 (S)101 %08/23/21 21:23 2037-26-5 D308/23/21 13:0370-130 4
4-Bromofluorobenzene (S)111 %08/23/21 21:23 460-00-408/23/21 13:0369-134 4
1,2-Dichloroethane-d4 (S)108 %08/23/21 21:23 17060-07-008/23/21 13:0370-130 4
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.9 %08/18/21 18:04 N20.10 1
Sample:SS-2 Lab ID:92556378013 Collected:08/16/21 13:10 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/26/21 07:48 83-32-908/25/21 14:150.43 1
Acenaphthylene ND mg/kg 08/26/21 07:48 208-96-808/25/21 14:150.43 1
Aniline ND mg/kg 08/26/21 07:48 62-53-308/25/21 14:150.43 1
Anthracene ND mg/kg 08/26/21 07:48 120-12-708/25/21 14:150.43 1
Benzo(a)anthracene ND mg/kg 08/26/21 07:48 56-55-308/25/21 14:150.43 1
Benzo(a)pyrene ND mg/kg 08/26/21 07:48 50-32-808/25/21 14:150.43 1
Benzo(b)fluoranthene ND mg/kg 08/26/21 07:48 205-99-208/25/21 14:150.43 1
Benzo(g,h,i)perylene ND mg/kg 08/26/21 07:48 191-24-208/25/21 14:150.43 1
Benzo(k)fluoranthene ND mg/kg 08/26/21 07:48 207-08-908/25/21 14:150.43 1
Benzoic Acid ND mg/kg 08/26/21 07:48 65-85-008/25/21 14:152.2 1
Benzyl alcohol ND mg/kg 08/26/21 07:48 100-51-608/25/21 14:150.86 1
4-Bromophenylphenyl ether ND mg/kg 08/26/21 07:48 101-55-308/25/21 14:150.43 1
Butylbenzylphthalate ND mg/kg 08/26/21 07:48 85-68-708/25/21 14:150.43 1
4-Chloro-3-methylphenol ND mg/kg 08/26/21 07:48 59-50-708/25/21 14:150.86 1
4-Chloroaniline ND mg/kg 08/26/21 07:48 106-47-808/25/21 14:150.86 1
bis(2-Chloroethoxy)methane ND mg/kg 08/26/21 07:48 111-91-108/25/21 14:150.43 1
bis(2-Chloroethyl) ether ND mg/kg 08/26/21 07:48 111-44-408/25/21 14:150.43 1
2-Chloronaphthalene ND mg/kg 08/26/21 07:48 91-58-708/25/21 14:150.43 1
2-Chlorophenol ND mg/kg 08/26/21 07:48 95-57-808/25/21 14:150.43 1
4-Chlorophenylphenyl ether ND mg/kg 08/26/21 07:48 7005-72-308/25/21 14:150.43 1
Chrysene ND mg/kg 08/26/21 07:48 218-01-908/25/21 14:150.43 1
Dibenz(a,h)anthracene ND mg/kg 08/26/21 07:48 53-70-308/25/21 14:150.43 1
Dibenzofuran ND mg/kg 08/26/21 07:48 132-64-908/25/21 14:150.43 1
1,2-Dichlorobenzene ND mg/kg 08/26/21 07:48 95-50-108/25/21 14:150.43 1
1,3-Dichlorobenzene ND mg/kg 08/26/21 07:48 541-73-108/25/21 14:150.43 1
1,4-Dichlorobenzene ND mg/kg 08/26/21 07:48 106-46-708/25/21 14:150.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-2 Lab ID:92556378013 Collected:08/16/21 13:10 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3,3'-Dichlorobenzidine ND mg/kg 08/26/21 07:48 91-94-1 IL08/25/21 14:150.86 1
2,4-Dichlorophenol ND mg/kg 08/26/21 07:48 120-83-208/25/21 14:150.43 1
Diethylphthalate ND mg/kg 08/26/21 07:48 84-66-208/25/21 14:150.43 1
2,4-Dimethylphenol ND mg/kg 08/26/21 07:48 105-67-908/25/21 14:150.43 1
Dimethylphthalate ND mg/kg 08/26/21 07:48 131-11-308/25/21 14:150.43 1
Di-n-butylphthalate ND mg/kg 08/26/21 07:48 84-74-208/25/21 14:150.43 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/26/21 07:48 534-52-1 v108/25/21 14:150.86 1
2,4-Dinitrophenol ND mg/kg 08/26/21 07:48 51-28-5 v108/25/21 14:152.2 1
2,4-Dinitrotoluene ND mg/kg 08/26/21 07:48 121-14-208/25/21 14:150.43 1
2,6-Dinitrotoluene ND mg/kg 08/26/21 07:48 606-20-208/25/21 14:150.43 1
Di-n-octylphthalate ND mg/kg 08/26/21 07:48 117-84-008/25/21 14:150.43 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/26/21 07:48 117-81-708/25/21 14:150.43 1
Fluoranthene ND mg/kg 08/26/21 07:48 206-44-008/25/21 14:150.43 1
Fluorene ND mg/kg 08/26/21 07:48 86-73-708/25/21 14:150.43 1
Hexachloro-1,3-butadiene ND mg/kg 08/26/21 07:48 87-68-308/25/21 14:150.43 1
Hexachlorobenzene ND mg/kg 08/26/21 07:48 118-74-108/25/21 14:150.43 1
Hexachlorocyclopentadiene ND mg/kg 08/26/21 07:48 77-47-408/25/21 14:150.43 1
Hexachloroethane ND mg/kg 08/26/21 07:48 67-72-108/25/21 14:150.43 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/26/21 07:48 193-39-508/25/21 14:150.43 1
Isophorone ND mg/kg 08/26/21 07:48 78-59-108/25/21 14:150.43 1
1-Methylnaphthalene ND mg/kg 08/26/21 07:48 90-12-008/25/21 14:150.43 1
2-Methylnaphthalene ND mg/kg 08/26/21 07:48 91-57-608/25/21 14:150.43 1
2-Methylphenol(o-Cresol)ND mg/kg 08/26/21 07:48 95-48-708/25/21 14:150.43 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/26/21 07:48 15831-10-408/25/21 14:150.43 1
Naphthalene ND mg/kg 08/26/21 07:48 91-20-308/25/21 14:150.43 1
2-Nitroaniline ND mg/kg 08/26/21 07:48 88-74-408/25/21 14:152.2 1
3-Nitroaniline ND mg/kg 08/26/21 07:48 99-09-2 IL08/25/21 14:152.2 1
4-Nitroaniline ND mg/kg 08/26/21 07:48 100-01-608/25/21 14:150.86 1
Nitrobenzene ND mg/kg 08/26/21 07:48 98-95-308/25/21 14:150.43 1
2-Nitrophenol ND mg/kg 08/26/21 07:48 88-75-508/25/21 14:150.43 1
4-Nitrophenol ND mg/kg 08/26/21 07:48 100-02-708/25/21 14:152.2 1
N-Nitrosodimethylamine ND mg/kg 08/26/21 07:48 62-75-9 v108/25/21 14:150.43 1
N-Nitroso-di-n-propylamine ND mg/kg 08/26/21 07:48 621-64-708/25/21 14:150.43 1
N-Nitrosodiphenylamine ND mg/kg 08/26/21 07:48 86-30-608/25/21 14:150.43 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/26/21 07:48 108-60-108/25/21 14:150.43 1
Pentachlorophenol ND mg/kg 08/26/21 07:48 87-86-508/25/21 14:150.86 1
Phenanthrene ND mg/kg 08/26/21 07:48 85-01-808/25/21 14:150.43 1
Phenol ND mg/kg 08/26/21 07:48 108-95-2 v108/25/21 14:150.43 1
Pyrene ND mg/kg 08/26/21 07:48 129-00-008/25/21 14:150.43 1
Pyridine ND mg/kg 08/26/21 07:48 110-86-1 v108/25/21 14:150.43 1
1,2,4-Trichlorobenzene ND mg/kg 08/26/21 07:48 120-82-108/25/21 14:150.43 1
2,4,5-Trichlorophenol ND mg/kg 08/26/21 07:48 95-95-408/25/21 14:150.43 1
2,4,6-Trichlorophenol ND mg/kg 08/26/21 07:48 88-06-208/25/21 14:150.43 1
Surrogates
Nitrobenzene-d5 (S)72 %08/26/21 07:48 4165-60-008/25/21 14:1521-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-2 Lab ID:92556378013 Collected:08/16/21 13:10 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorobiphenyl (S)38 %08/26/21 07:48 321-60-808/25/21 14:1519-130 1
Terphenyl-d14 (S)50 %08/26/21 07:48 1718-51-008/25/21 14:1515-130 1
Phenol-d6 (S)67 %08/26/21 07:48 13127-88-308/25/21 14:1518-130 1
2-Fluorophenol (S)67 %08/26/21 07:48 367-12-408/25/21 14:1518-130 1
2,4,6-Tribromophenol (S)59 %08/26/21 07:48 118-79-608/25/21 14:1518-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/23/21 19:03 67-64-108/23/21 13:030.14 1
Benzene 0.22 mg/kg 08/23/21 19:03 71-43-208/23/21 13:030.0071 1
Bromobenzene ND mg/kg 08/23/21 19:03 108-86-108/23/21 13:030.0071 1
Bromochloromethane ND mg/kg 08/23/21 19:03 74-97-508/23/21 13:030.0071 1
Bromodichloromethane ND mg/kg 08/23/21 19:03 75-27-408/23/21 13:030.0071 1
Bromoform ND mg/kg 08/23/21 19:03 75-25-208/23/21 13:030.0071 1
Bromomethane ND mg/kg 08/23/21 19:03 74-83-9 v108/23/21 13:030.014 1
2-Butanone (MEK)0.18 mg/kg 08/23/21 19:03 78-93-308/23/21 13:030.14 1
n-Butylbenzene ND mg/kg 08/23/21 19:03 104-51-808/23/21 13:030.0071 1
sec-Butylbenzene 0.16 mg/kg 08/23/21 19:03 135-98-808/23/21 13:030.0071 1
tert-Butylbenzene ND mg/kg 08/23/21 19:03 98-06-608/23/21 13:030.0071 1
Carbon tetrachloride ND mg/kg 08/23/21 19:03 56-23-508/23/21 13:030.0071 1
Chlorobenzene ND mg/kg 08/23/21 19:03 108-90-708/23/21 13:030.0071 1
Chloroethane ND mg/kg 08/23/21 19:03 75-00-3 v108/23/21 13:030.014 1
Chloroform ND mg/kg 08/23/21 19:03 67-66-308/23/21 13:030.0071 1
Chloromethane ND mg/kg 08/23/21 19:03 74-87-308/23/21 13:030.014 1
2-Chlorotoluene ND mg/kg 08/23/21 19:03 95-49-808/23/21 13:030.0071 1
4-Chlorotoluene ND mg/kg 08/23/21 19:03 106-43-408/23/21 13:030.0071 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/23/21 19:03 96-12-808/23/21 13:030.0071 1
Dibromochloromethane ND mg/kg 08/23/21 19:03 124-48-108/23/21 13:030.0071 1
1,2-Dibromoethane (EDB)0.010 mg/kg 08/23/21 19:03 106-93-408/23/21 13:030.0071 1
Dibromomethane ND mg/kg 08/23/21 19:03 74-95-308/23/21 13:030.0071 1
1,2-Dichlorobenzene ND mg/kg 08/23/21 19:03 95-50-108/23/21 13:030.0071 1
1,3-Dichlorobenzene ND mg/kg 08/23/21 19:03 541-73-108/23/21 13:030.0071 1
1,4-Dichlorobenzene ND mg/kg 08/23/21 19:03 106-46-708/23/21 13:030.0071 1
Dichlorodifluoromethane ND mg/kg 08/23/21 19:03 75-71-8 IK,v108/23/21 13:030.014 1
1,1-Dichloroethane ND mg/kg 08/23/21 19:03 75-34-308/23/21 13:030.0071 1
1,2-Dichloroethane ND mg/kg 08/23/21 19:03 107-06-208/23/21 13:030.0071 1
1,1-Dichloroethene ND mg/kg 08/23/21 19:03 75-35-408/23/21 13:030.0071 1
cis-1,2-Dichloroethene ND mg/kg 08/23/21 19:03 156-59-208/23/21 13:030.0071 1
trans-1,2-Dichloroethene ND mg/kg 08/23/21 19:03 156-60-508/23/21 13:030.0071 1
1,2-Dichloropropane ND mg/kg 08/23/21 19:03 78-87-508/23/21 13:030.0071 1
1,3-Dichloropropane ND mg/kg 08/23/21 19:03 142-28-908/23/21 13:030.0071 1
2,2-Dichloropropane ND mg/kg 08/23/21 19:03 594-20-708/23/21 13:030.0071 1
1,1-Dichloropropene ND mg/kg 08/23/21 19:03 563-58-608/23/21 13:030.0071 1
cis-1,3-Dichloropropene ND mg/kg 08/23/21 19:03 10061-01-508/23/21 13:030.0071 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-2 Lab ID:92556378013 Collected:08/16/21 13:10 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
trans-1,3-Dichloropropene ND mg/kg 08/23/21 19:03 10061-02-608/23/21 13:030.0071 1
Diisopropyl ether ND mg/kg 08/23/21 19:03 108-20-308/23/21 13:030.0071 1
Ethylbenzene 0.11 mg/kg 08/23/21 19:03 100-41-408/23/21 13:030.0071 1
Hexachloro-1,3-butadiene ND mg/kg 08/23/21 19:03 87-68-308/23/21 13:030.014 1
2-Hexanone ND mg/kg 08/23/21 19:03 591-78-608/23/21 13:030.071 1
Isopropylbenzene (Cumene)0.59 mg/kg 08/23/21 19:03 98-82-808/23/21 13:030.0071 1
p-Isopropyltoluene ND mg/kg 08/23/21 19:03 99-87-608/23/21 13:030.0071 1
Methylene Chloride 0.071 mg/kg 08/23/21 19:03 75-09-208/23/21 13:030.028 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/23/21 19:03 108-10-108/23/21 13:030.071 1
Methyl-tert-butyl ether ND mg/kg 08/23/21 19:03 1634-04-408/23/21 13:030.0071 1
Naphthalene 0.64 mg/kg 08/23/21 19:03 91-20-308/23/21 13:030.0071 1
n-Propylbenzene 0.75 mg/kg 08/23/21 19:03 103-65-108/23/21 13:030.0071 1
Styrene ND mg/kg 08/23/21 19:03 100-42-508/23/21 13:030.0071 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/23/21 19:03 630-20-608/23/21 13:030.0071 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/23/21 19:03 79-34-508/23/21 13:030.0071 1
Tetrachloroethene ND mg/kg 08/23/21 19:03 127-18-408/23/21 13:030.0071 1
Toluene 0.068 mg/kg 08/23/21 19:03 108-88-308/23/21 13:030.0071 1
1,2,3-Trichlorobenzene ND mg/kg 08/23/21 19:03 87-61-608/23/21 13:030.0071 1
1,2,4-Trichlorobenzene ND mg/kg 08/23/21 19:03 120-82-108/23/21 13:030.0071 1
1,1,1-Trichloroethane ND mg/kg 08/23/21 19:03 71-55-608/23/21 13:030.0071 1
1,1,2-Trichloroethane ND mg/kg 08/23/21 19:03 79-00-508/23/21 13:030.0071 1
Trichloroethene ND mg/kg 08/23/21 19:03 79-01-608/23/21 13:030.0071 1
Trichlorofluoromethane ND mg/kg 08/23/21 19:03 75-69-408/23/21 13:030.0071 1
1,2,3-Trichloropropane ND mg/kg 08/23/21 19:03 96-18-408/23/21 13:030.0071 1
1,2,4-Trimethylbenzene ND mg/kg 08/23/21 19:03 95-63-608/23/21 13:030.0071 1
1,3,5-Trimethylbenzene ND mg/kg 08/23/21 19:03 108-67-808/23/21 13:030.0071 1
Vinyl acetate ND mg/kg 08/23/21 19:03 108-05-408/23/21 13:030.071 1
Vinyl chloride ND mg/kg 08/23/21 19:03 75-01-4 v108/23/21 13:030.014 1
Xylene (Total)0.36 mg/kg 08/23/21 19:03 1330-20-708/23/21 13:030.014 1
m&p-Xylene 0.34 mg/kg 08/23/21 19:03 179601-23-108/23/21 13:030.014 1
o-Xylene 0.019 mg/kg 08/23/21 19:03 95-47-608/23/21 13:030.0071 1
Surrogates
Toluene-d8 (S)102 %08/23/21 19:03 2037-26-508/23/21 13:0370-130 1
4-Bromofluorobenzene (S)100 %08/23/21 19:03 460-00-408/23/21 13:0369-134 1
1,2-Dichloroethane-d4 (S)106 %08/23/21 19:03 17060-07-008/23/21 13:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.6 %08/18/21 18:04 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-3 Lab ID:92556378014 Collected:08/17/21 09:40 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/26/21 08:15 83-32-908/25/21 14:150.42 1
Acenaphthylene ND mg/kg 08/26/21 08:15 208-96-808/25/21 14:150.42 1
Aniline ND mg/kg 08/26/21 08:15 62-53-308/25/21 14:150.42 1
Anthracene ND mg/kg 08/26/21 08:15 120-12-708/25/21 14:150.42 1
Benzo(a)anthracene ND mg/kg 08/26/21 08:15 56-55-308/25/21 14:150.42 1
Benzo(a)pyrene ND mg/kg 08/26/21 08:15 50-32-808/25/21 14:150.42 1
Benzo(b)fluoranthene ND mg/kg 08/26/21 08:15 205-99-208/25/21 14:150.42 1
Benzo(g,h,i)perylene ND mg/kg 08/26/21 08:15 191-24-208/25/21 14:150.42 1
Benzo(k)fluoranthene ND mg/kg 08/26/21 08:15 207-08-908/25/21 14:150.42 1
Benzoic Acid ND mg/kg 08/26/21 08:15 65-85-008/25/21 14:152.1 1
Benzyl alcohol ND mg/kg 08/26/21 08:15 100-51-608/25/21 14:150.84 1
4-Bromophenylphenyl ether ND mg/kg 08/26/21 08:15 101-55-308/25/21 14:150.42 1
Butylbenzylphthalate ND mg/kg 08/26/21 08:15 85-68-708/25/21 14:150.42 1
4-Chloro-3-methylphenol ND mg/kg 08/26/21 08:15 59-50-708/25/21 14:150.84 1
4-Chloroaniline ND mg/kg 08/26/21 08:15 106-47-808/25/21 14:150.84 1
bis(2-Chloroethoxy)methane ND mg/kg 08/26/21 08:15 111-91-108/25/21 14:150.42 1
bis(2-Chloroethyl) ether ND mg/kg 08/26/21 08:15 111-44-408/25/21 14:150.42 1
2-Chloronaphthalene ND mg/kg 08/26/21 08:15 91-58-708/25/21 14:150.42 1
2-Chlorophenol ND mg/kg 08/26/21 08:15 95-57-808/25/21 14:150.42 1
4-Chlorophenylphenyl ether ND mg/kg 08/26/21 08:15 7005-72-308/25/21 14:150.42 1
Chrysene ND mg/kg 08/26/21 08:15 218-01-908/25/21 14:150.42 1
Dibenz(a,h)anthracene ND mg/kg 08/26/21 08:15 53-70-308/25/21 14:150.42 1
Dibenzofuran ND mg/kg 08/26/21 08:15 132-64-908/25/21 14:150.42 1
1,2-Dichlorobenzene ND mg/kg 08/26/21 08:15 95-50-108/25/21 14:150.42 1
1,3-Dichlorobenzene ND mg/kg 08/26/21 08:15 541-73-108/25/21 14:150.42 1
1,4-Dichlorobenzene ND mg/kg 08/26/21 08:15 106-46-708/25/21 14:150.42 1
3,3'-Dichlorobenzidine ND mg/kg 08/26/21 08:15 91-94-1 IL08/25/21 14:150.84 1
2,4-Dichlorophenol ND mg/kg 08/26/21 08:15 120-83-208/25/21 14:150.42 1
Diethylphthalate ND mg/kg 08/26/21 08:15 84-66-208/25/21 14:150.42 1
2,4-Dimethylphenol ND mg/kg 08/26/21 08:15 105-67-908/25/21 14:150.42 1
Dimethylphthalate ND mg/kg 08/26/21 08:15 131-11-308/25/21 14:150.42 1
Di-n-butylphthalate ND mg/kg 08/26/21 08:15 84-74-208/25/21 14:150.42 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/26/21 08:15 534-52-1 v108/25/21 14:150.84 1
2,4-Dinitrophenol ND mg/kg 08/26/21 08:15 51-28-5 v108/25/21 14:152.1 1
2,4-Dinitrotoluene ND mg/kg 08/26/21 08:15 121-14-208/25/21 14:150.42 1
2,6-Dinitrotoluene ND mg/kg 08/26/21 08:15 606-20-208/25/21 14:150.42 1
Di-n-octylphthalate ND mg/kg 08/26/21 08:15 117-84-008/25/21 14:150.42 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/26/21 08:15 117-81-708/25/21 14:150.42 1
Fluoranthene ND mg/kg 08/26/21 08:15 206-44-008/25/21 14:150.42 1
Fluorene ND mg/kg 08/26/21 08:15 86-73-708/25/21 14:150.42 1
Hexachloro-1,3-butadiene ND mg/kg 08/26/21 08:15 87-68-308/25/21 14:150.42 1
Hexachlorobenzene ND mg/kg 08/26/21 08:15 118-74-108/25/21 14:150.42 1
Hexachlorocyclopentadiene ND mg/kg 08/26/21 08:15 77-47-408/25/21 14:150.42 1
Hexachloroethane ND mg/kg 08/26/21 08:15 67-72-108/25/21 14:150.42 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/26/21 08:15 193-39-508/25/21 14:150.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-3 Lab ID:92556378014 Collected:08/17/21 09:40 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND mg/kg 08/26/21 08:15 78-59-108/25/21 14:150.42 1
1-Methylnaphthalene ND mg/kg 08/26/21 08:15 90-12-008/25/21 14:150.42 1
2-Methylnaphthalene ND mg/kg 08/26/21 08:15 91-57-608/25/21 14:150.42 1
2-Methylphenol(o-Cresol)ND mg/kg 08/26/21 08:15 95-48-708/25/21 14:150.42 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/26/21 08:15 15831-10-408/25/21 14:150.42 1
Naphthalene ND mg/kg 08/26/21 08:15 91-20-308/25/21 14:150.42 1
2-Nitroaniline ND mg/kg 08/26/21 08:15 88-74-408/25/21 14:152.1 1
3-Nitroaniline ND mg/kg 08/26/21 08:15 99-09-2 IL08/25/21 14:152.1 1
4-Nitroaniline ND mg/kg 08/26/21 08:15 100-01-608/25/21 14:150.84 1
Nitrobenzene ND mg/kg 08/26/21 08:15 98-95-308/25/21 14:150.42 1
2-Nitrophenol ND mg/kg 08/26/21 08:15 88-75-508/25/21 14:150.42 1
4-Nitrophenol ND mg/kg 08/26/21 08:15 100-02-708/25/21 14:152.1 1
N-Nitrosodimethylamine ND mg/kg 08/26/21 08:15 62-75-9 v108/25/21 14:150.42 1
N-Nitroso-di-n-propylamine ND mg/kg 08/26/21 08:15 621-64-708/25/21 14:150.42 1
N-Nitrosodiphenylamine ND mg/kg 08/26/21 08:15 86-30-608/25/21 14:150.42 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/26/21 08:15 108-60-108/25/21 14:150.42 1
Pentachlorophenol ND mg/kg 08/26/21 08:15 87-86-508/25/21 14:150.84 1
Phenanthrene ND mg/kg 08/26/21 08:15 85-01-808/25/21 14:150.42 1
Phenol ND mg/kg 08/26/21 08:15 108-95-2 v108/25/21 14:150.42 1
Pyrene ND mg/kg 08/26/21 08:15 129-00-008/25/21 14:150.42 1
Pyridine ND mg/kg 08/26/21 08:15 110-86-1 v108/25/21 14:150.42 1
1,2,4-Trichlorobenzene ND mg/kg 08/26/21 08:15 120-82-108/25/21 14:150.42 1
2,4,5-Trichlorophenol ND mg/kg 08/26/21 08:15 95-95-408/25/21 14:150.42 1
2,4,6-Trichlorophenol ND mg/kg 08/26/21 08:15 88-06-208/25/21 14:150.42 1
Surrogates
Nitrobenzene-d5 (S)68 %08/26/21 08:15 4165-60-008/25/21 14:1521-130 1
2-Fluorobiphenyl (S)29 %08/26/21 08:15 321-60-808/25/21 14:1519-130 1
Terphenyl-d14 (S)24 %08/26/21 08:15 1718-51-008/25/21 14:1515-130 1
Phenol-d6 (S)69 %08/26/21 08:15 13127-88-308/25/21 14:1518-130 1
2-Fluorophenol (S)69 %08/26/21 08:15 367-12-408/25/21 14:1518-130 1
2,4,6-Tribromophenol (S)52 %08/26/21 08:15 118-79-608/25/21 14:1518-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/23/21 19:21 67-64-108/23/21 13:030.14 1
Benzene ND mg/kg 08/23/21 19:21 71-43-208/23/21 13:030.0068 1
Bromobenzene ND mg/kg 08/23/21 19:21 108-86-108/23/21 13:030.0068 1
Bromochloromethane ND mg/kg 08/23/21 19:21 74-97-508/23/21 13:030.0068 1
Bromodichloromethane ND mg/kg 08/23/21 19:21 75-27-408/23/21 13:030.0068 1
Bromoform ND mg/kg 08/23/21 19:21 75-25-208/23/21 13:030.0068 1
Bromomethane ND mg/kg 08/23/21 19:21 74-83-9 v108/23/21 13:030.014 1
2-Butanone (MEK)ND mg/kg 08/23/21 19:21 78-93-308/23/21 13:030.14 1
n-Butylbenzene ND mg/kg 08/23/21 19:21 104-51-808/23/21 13:030.0068 1
sec-Butylbenzene ND mg/kg 08/23/21 19:21 135-98-808/23/21 13:030.0068 1
tert-Butylbenzene ND mg/kg 08/23/21 19:21 98-06-608/23/21 13:030.0068 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-3 Lab ID:92556378014 Collected:08/17/21 09:40 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Carbon tetrachloride ND mg/kg 08/23/21 19:21 56-23-508/23/21 13:030.0068 1
Chlorobenzene ND mg/kg 08/23/21 19:21 108-90-708/23/21 13:030.0068 1
Chloroethane ND mg/kg 08/23/21 19:21 75-00-3 v108/23/21 13:030.014 1
Chloroform ND mg/kg 08/23/21 19:21 67-66-308/23/21 13:030.0068 1
Chloromethane ND mg/kg 08/23/21 19:21 74-87-308/23/21 13:030.014 1
2-Chlorotoluene ND mg/kg 08/23/21 19:21 95-49-808/23/21 13:030.0068 1
4-Chlorotoluene ND mg/kg 08/23/21 19:21 106-43-408/23/21 13:030.0068 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/23/21 19:21 96-12-808/23/21 13:030.0068 1
Dibromochloromethane ND mg/kg 08/23/21 19:21 124-48-108/23/21 13:030.0068 1
1,2-Dibromoethane (EDB)ND mg/kg 08/23/21 19:21 106-93-408/23/21 13:030.0068 1
Dibromomethane ND mg/kg 08/23/21 19:21 74-95-308/23/21 13:030.0068 1
1,2-Dichlorobenzene ND mg/kg 08/23/21 19:21 95-50-108/23/21 13:030.0068 1
1,3-Dichlorobenzene ND mg/kg 08/23/21 19:21 541-73-108/23/21 13:030.0068 1
1,4-Dichlorobenzene ND mg/kg 08/23/21 19:21 106-46-708/23/21 13:030.0068 1
Dichlorodifluoromethane ND mg/kg 08/23/21 19:21 75-71-8 IK,v108/23/21 13:030.014 1
1,1-Dichloroethane ND mg/kg 08/23/21 19:21 75-34-308/23/21 13:030.0068 1
1,2-Dichloroethane ND mg/kg 08/23/21 19:21 107-06-208/23/21 13:030.0068 1
1,1-Dichloroethene ND mg/kg 08/23/21 19:21 75-35-408/23/21 13:030.0068 1
cis-1,2-Dichloroethene ND mg/kg 08/23/21 19:21 156-59-208/23/21 13:030.0068 1
trans-1,2-Dichloroethene ND mg/kg 08/23/21 19:21 156-60-508/23/21 13:030.0068 1
1,2-Dichloropropane ND mg/kg 08/23/21 19:21 78-87-508/23/21 13:030.0068 1
1,3-Dichloropropane ND mg/kg 08/23/21 19:21 142-28-908/23/21 13:030.0068 1
2,2-Dichloropropane ND mg/kg 08/23/21 19:21 594-20-708/23/21 13:030.0068 1
1,1-Dichloropropene ND mg/kg 08/23/21 19:21 563-58-608/23/21 13:030.0068 1
cis-1,3-Dichloropropene ND mg/kg 08/23/21 19:21 10061-01-508/23/21 13:030.0068 1
trans-1,3-Dichloropropene ND mg/kg 08/23/21 19:21 10061-02-608/23/21 13:030.0068 1
Diisopropyl ether ND mg/kg 08/23/21 19:21 108-20-308/23/21 13:030.0068 1
Ethylbenzene ND mg/kg 08/23/21 19:21 100-41-408/23/21 13:030.0068 1
Hexachloro-1,3-butadiene ND mg/kg 08/23/21 19:21 87-68-308/23/21 13:030.014 1
2-Hexanone ND mg/kg 08/23/21 19:21 591-78-608/23/21 13:030.068 1
Isopropylbenzene (Cumene)ND mg/kg 08/23/21 19:21 98-82-808/23/21 13:030.0068 1
p-Isopropyltoluene ND mg/kg 08/23/21 19:21 99-87-608/23/21 13:030.0068 1
Methylene Chloride 0.075 mg/kg 08/23/21 19:21 75-09-208/23/21 13:030.027 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/23/21 19:21 108-10-108/23/21 13:030.068 1
Methyl-tert-butyl ether ND mg/kg 08/23/21 19:21 1634-04-408/23/21 13:030.0068 1
Naphthalene 0.0079 mg/kg 08/23/21 19:21 91-20-308/23/21 13:030.0068 1
n-Propylbenzene ND mg/kg 08/23/21 19:21 103-65-108/23/21 13:030.0068 1
Styrene ND mg/kg 08/23/21 19:21 100-42-508/23/21 13:030.0068 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/23/21 19:21 630-20-608/23/21 13:030.0068 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/23/21 19:21 79-34-508/23/21 13:030.0068 1
Tetrachloroethene ND mg/kg 08/23/21 19:21 127-18-408/23/21 13:030.0068 1
Toluene ND mg/kg 08/23/21 19:21 108-88-308/23/21 13:030.0068 1
1,2,3-Trichlorobenzene ND mg/kg 08/23/21 19:21 87-61-608/23/21 13:030.0068 1
1,2,4-Trichlorobenzene ND mg/kg 08/23/21 19:21 120-82-108/23/21 13:030.0068 1
1,1,1-Trichloroethane ND mg/kg 08/23/21 19:21 71-55-608/23/21 13:030.0068 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-3 Lab ID:92556378014 Collected:08/17/21 09:40 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1,2-Trichloroethane ND mg/kg 08/23/21 19:21 79-00-508/23/21 13:030.0068 1
Trichloroethene ND mg/kg 08/23/21 19:21 79-01-608/23/21 13:030.0068 1
Trichlorofluoromethane ND mg/kg 08/23/21 19:21 75-69-408/23/21 13:030.0068 1
1,2,3-Trichloropropane ND mg/kg 08/23/21 19:21 96-18-408/23/21 13:030.0068 1
1,2,4-Trimethylbenzene ND mg/kg 08/23/21 19:21 95-63-608/23/21 13:030.0068 1
1,3,5-Trimethylbenzene ND mg/kg 08/23/21 19:21 108-67-808/23/21 13:030.0068 1
Vinyl acetate ND mg/kg 08/23/21 19:21 108-05-408/23/21 13:030.068 1
Vinyl chloride ND mg/kg 08/23/21 19:21 75-01-4 v108/23/21 13:030.014 1
Xylene (Total)ND mg/kg 08/23/21 19:21 1330-20-708/23/21 13:030.014 1
m&p-Xylene ND mg/kg 08/23/21 19:21 179601-23-108/23/21 13:030.014 1
o-Xylene ND mg/kg 08/23/21 19:21 95-47-608/23/21 13:030.0068 1
Surrogates
Toluene-d8 (S)102 %08/23/21 19:21 2037-26-508/23/21 13:0370-130 1
4-Bromofluorobenzene (S)97 %08/23/21 19:21 460-00-408/23/21 13:0369-134 1
1,2-Dichloroethane-d4 (S)106 %08/23/21 19:21 17060-07-008/23/21 13:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.3 %08/18/21 18:04 N20.10 1
Sample:SS-4 Lab ID:92556378015 Collected:08/17/21 09:55 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/26/21 08:42 83-32-908/25/21 14:150.39 1
Acenaphthylene ND mg/kg 08/26/21 08:42 208-96-808/25/21 14:150.39 1
Aniline ND mg/kg 08/26/21 08:42 62-53-308/25/21 14:150.39 1
Anthracene ND mg/kg 08/26/21 08:42 120-12-708/25/21 14:150.39 1
Benzo(a)anthracene ND mg/kg 08/26/21 08:42 56-55-308/25/21 14:150.39 1
Benzo(a)pyrene ND mg/kg 08/26/21 08:42 50-32-808/25/21 14:150.39 1
Benzo(b)fluoranthene ND mg/kg 08/26/21 08:42 205-99-208/25/21 14:150.39 1
Benzo(g,h,i)perylene ND mg/kg 08/26/21 08:42 191-24-208/25/21 14:150.39 1
Benzo(k)fluoranthene ND mg/kg 08/26/21 08:42 207-08-908/25/21 14:150.39 1
Benzoic Acid ND mg/kg 08/26/21 08:42 65-85-008/25/21 14:152.0 1
Benzyl alcohol ND mg/kg 08/26/21 08:42 100-51-608/25/21 14:150.78 1
4-Bromophenylphenyl ether ND mg/kg 08/26/21 08:42 101-55-308/25/21 14:150.39 1
Butylbenzylphthalate ND mg/kg 08/26/21 08:42 85-68-708/25/21 14:150.39 1
4-Chloro-3-methylphenol ND mg/kg 08/26/21 08:42 59-50-708/25/21 14:150.78 1
4-Chloroaniline ND mg/kg 08/26/21 08:42 106-47-808/25/21 14:150.78 1
bis(2-Chloroethoxy)methane ND mg/kg 08/26/21 08:42 111-91-108/25/21 14:150.39 1
bis(2-Chloroethyl) ether ND mg/kg 08/26/21 08:42 111-44-408/25/21 14:150.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-4 Lab ID:92556378015 Collected:08/17/21 09:55 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Chloronaphthalene ND mg/kg 08/26/21 08:42 91-58-708/25/21 14:150.39 1
2-Chlorophenol ND mg/kg 08/26/21 08:42 95-57-808/25/21 14:150.39 1
4-Chlorophenylphenyl ether ND mg/kg 08/26/21 08:42 7005-72-308/25/21 14:150.39 1
Chrysene ND mg/kg 08/26/21 08:42 218-01-908/25/21 14:150.39 1
Dibenz(a,h)anthracene ND mg/kg 08/26/21 08:42 53-70-308/25/21 14:150.39 1
Dibenzofuran ND mg/kg 08/26/21 08:42 132-64-908/25/21 14:150.39 1
1,2-Dichlorobenzene ND mg/kg 08/26/21 08:42 95-50-108/25/21 14:150.39 1
1,3-Dichlorobenzene ND mg/kg 08/26/21 08:42 541-73-108/25/21 14:150.39 1
1,4-Dichlorobenzene ND mg/kg 08/26/21 08:42 106-46-708/25/21 14:150.39 1
3,3'-Dichlorobenzidine ND mg/kg 08/26/21 08:42 91-94-1 IL08/25/21 14:150.78 1
2,4-Dichlorophenol ND mg/kg 08/26/21 08:42 120-83-208/25/21 14:150.39 1
Diethylphthalate ND mg/kg 08/26/21 08:42 84-66-208/25/21 14:150.39 1
2,4-Dimethylphenol ND mg/kg 08/26/21 08:42 105-67-908/25/21 14:150.39 1
Dimethylphthalate ND mg/kg 08/26/21 08:42 131-11-308/25/21 14:150.39 1
Di-n-butylphthalate ND mg/kg 08/26/21 08:42 84-74-208/25/21 14:150.39 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/26/21 08:42 534-52-1 v108/25/21 14:150.78 1
2,4-Dinitrophenol ND mg/kg 08/26/21 08:42 51-28-5 v108/25/21 14:152.0 1
2,4-Dinitrotoluene ND mg/kg 08/26/21 08:42 121-14-208/25/21 14:150.39 1
2,6-Dinitrotoluene ND mg/kg 08/26/21 08:42 606-20-208/25/21 14:150.39 1
Di-n-octylphthalate ND mg/kg 08/26/21 08:42 117-84-008/25/21 14:150.39 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/26/21 08:42 117-81-708/25/21 14:150.39 1
Fluoranthene ND mg/kg 08/26/21 08:42 206-44-008/25/21 14:150.39 1
Fluorene ND mg/kg 08/26/21 08:42 86-73-708/25/21 14:150.39 1
Hexachloro-1,3-butadiene ND mg/kg 08/26/21 08:42 87-68-308/25/21 14:150.39 1
Hexachlorobenzene ND mg/kg 08/26/21 08:42 118-74-108/25/21 14:150.39 1
Hexachlorocyclopentadiene ND mg/kg 08/26/21 08:42 77-47-408/25/21 14:150.39 1
Hexachloroethane ND mg/kg 08/26/21 08:42 67-72-108/25/21 14:150.39 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/26/21 08:42 193-39-508/25/21 14:150.39 1
Isophorone ND mg/kg 08/26/21 08:42 78-59-108/25/21 14:150.39 1
1-Methylnaphthalene ND mg/kg 08/26/21 08:42 90-12-008/25/21 14:150.39 1
2-Methylnaphthalene ND mg/kg 08/26/21 08:42 91-57-608/25/21 14:150.39 1
2-Methylphenol(o-Cresol)ND mg/kg 08/26/21 08:42 95-48-708/25/21 14:150.39 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/26/21 08:42 15831-10-408/25/21 14:150.39 1
Naphthalene ND mg/kg 08/26/21 08:42 91-20-308/25/21 14:150.39 1
2-Nitroaniline ND mg/kg 08/26/21 08:42 88-74-408/25/21 14:152.0 1
3-Nitroaniline ND mg/kg 08/26/21 08:42 99-09-2 IL08/25/21 14:152.0 1
4-Nitroaniline ND mg/kg 08/26/21 08:42 100-01-608/25/21 14:150.78 1
Nitrobenzene ND mg/kg 08/26/21 08:42 98-95-308/25/21 14:150.39 1
2-Nitrophenol ND mg/kg 08/26/21 08:42 88-75-508/25/21 14:150.39 1
4-Nitrophenol ND mg/kg 08/26/21 08:42 100-02-708/25/21 14:152.0 1
N-Nitrosodimethylamine ND mg/kg 08/26/21 08:42 62-75-9 v108/25/21 14:150.39 1
N-Nitroso-di-n-propylamine ND mg/kg 08/26/21 08:42 621-64-708/25/21 14:150.39 1
N-Nitrosodiphenylamine ND mg/kg 08/26/21 08:42 86-30-608/25/21 14:150.39 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/26/21 08:42 108-60-108/25/21 14:150.39 1
Pentachlorophenol ND mg/kg 08/26/21 08:42 87-86-508/25/21 14:150.78 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-4 Lab ID:92556378015 Collected:08/17/21 09:55 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Phenanthrene ND mg/kg 08/26/21 08:42 85-01-808/25/21 14:150.39 1
Phenol ND mg/kg 08/26/21 08:42 108-95-2 v108/25/21 14:150.39 1
Pyrene ND mg/kg 08/26/21 08:42 129-00-008/25/21 14:150.39 1
Pyridine ND mg/kg 08/26/21 08:42 110-86-1 v108/25/21 14:150.39 1
1,2,4-Trichlorobenzene ND mg/kg 08/26/21 08:42 120-82-108/25/21 14:150.39 1
2,4,5-Trichlorophenol ND mg/kg 08/26/21 08:42 95-95-408/25/21 14:150.39 1
2,4,6-Trichlorophenol ND mg/kg 08/26/21 08:42 88-06-208/25/21 14:150.39 1
Surrogates
Nitrobenzene-d5 (S)75 %08/26/21 08:42 4165-60-008/25/21 14:1521-130 1
2-Fluorobiphenyl (S)58 %08/26/21 08:42 321-60-808/25/21 14:1519-130 1
Terphenyl-d14 (S)70 %08/26/21 08:42 1718-51-008/25/21 14:1515-130 1
Phenol-d6 (S)75 %08/26/21 08:42 13127-88-308/25/21 14:1518-130 1
2-Fluorophenol (S)73 %08/26/21 08:42 367-12-408/25/21 14:1518-130 1
2,4,6-Tribromophenol (S)77 %08/26/21 08:42 118-79-608/25/21 14:1518-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/23/21 19:38 67-64-108/23/21 13:030.13 1
Benzene ND mg/kg 08/23/21 19:38 71-43-208/23/21 13:030.0063 1
Bromobenzene ND mg/kg 08/23/21 19:38 108-86-108/23/21 13:030.0063 1
Bromochloromethane ND mg/kg 08/23/21 19:38 74-97-508/23/21 13:030.0063 1
Bromodichloromethane ND mg/kg 08/23/21 19:38 75-27-408/23/21 13:030.0063 1
Bromoform ND mg/kg 08/23/21 19:38 75-25-208/23/21 13:030.0063 1
Bromomethane ND mg/kg 08/23/21 19:38 74-83-9 v108/23/21 13:030.013 1
2-Butanone (MEK)ND mg/kg 08/23/21 19:38 78-93-308/23/21 13:030.13 1
n-Butylbenzene ND mg/kg 08/23/21 19:38 104-51-808/23/21 13:030.0063 1
sec-Butylbenzene ND mg/kg 08/23/21 19:38 135-98-808/23/21 13:030.0063 1
tert-Butylbenzene ND mg/kg 08/23/21 19:38 98-06-608/23/21 13:030.0063 1
Carbon tetrachloride ND mg/kg 08/23/21 19:38 56-23-508/23/21 13:030.0063 1
Chlorobenzene ND mg/kg 08/23/21 19:38 108-90-708/23/21 13:030.0063 1
Chloroethane ND mg/kg 08/23/21 19:38 75-00-3 v108/23/21 13:030.013 1
Chloroform ND mg/kg 08/23/21 19:38 67-66-308/23/21 13:030.0063 1
Chloromethane ND mg/kg 08/23/21 19:38 74-87-308/23/21 13:030.013 1
2-Chlorotoluene ND mg/kg 08/23/21 19:38 95-49-808/23/21 13:030.0063 1
4-Chlorotoluene ND mg/kg 08/23/21 19:38 106-43-408/23/21 13:030.0063 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/23/21 19:38 96-12-808/23/21 13:030.0063 1
Dibromochloromethane ND mg/kg 08/23/21 19:38 124-48-108/23/21 13:030.0063 1
1,2-Dibromoethane (EDB)ND mg/kg 08/23/21 19:38 106-93-408/23/21 13:030.0063 1
Dibromomethane ND mg/kg 08/23/21 19:38 74-95-308/23/21 13:030.0063 1
1,2-Dichlorobenzene ND mg/kg 08/23/21 19:38 95-50-108/23/21 13:030.0063 1
1,3-Dichlorobenzene ND mg/kg 08/23/21 19:38 541-73-108/23/21 13:030.0063 1
1,4-Dichlorobenzene ND mg/kg 08/23/21 19:38 106-46-708/23/21 13:030.0063 1
Dichlorodifluoromethane ND mg/kg 08/23/21 19:38 75-71-8 IK,v108/23/21 13:030.013 1
1,1-Dichloroethane ND mg/kg 08/23/21 19:38 75-34-308/23/21 13:030.0063 1
1,2-Dichloroethane ND mg/kg 08/23/21 19:38 107-06-208/23/21 13:030.0063 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-4 Lab ID:92556378015 Collected:08/17/21 09:55 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,1-Dichloroethene ND mg/kg 08/23/21 19:38 75-35-408/23/21 13:030.0063 1
cis-1,2-Dichloroethene ND mg/kg 08/23/21 19:38 156-59-208/23/21 13:030.0063 1
trans-1,2-Dichloroethene ND mg/kg 08/23/21 19:38 156-60-508/23/21 13:030.0063 1
1,2-Dichloropropane ND mg/kg 08/23/21 19:38 78-87-508/23/21 13:030.0063 1
1,3-Dichloropropane ND mg/kg 08/23/21 19:38 142-28-908/23/21 13:030.0063 1
2,2-Dichloropropane ND mg/kg 08/23/21 19:38 594-20-708/23/21 13:030.0063 1
1,1-Dichloropropene ND mg/kg 08/23/21 19:38 563-58-608/23/21 13:030.0063 1
cis-1,3-Dichloropropene ND mg/kg 08/23/21 19:38 10061-01-508/23/21 13:030.0063 1
trans-1,3-Dichloropropene ND mg/kg 08/23/21 19:38 10061-02-608/23/21 13:030.0063 1
Diisopropyl ether ND mg/kg 08/23/21 19:38 108-20-308/23/21 13:030.0063 1
Ethylbenzene ND mg/kg 08/23/21 19:38 100-41-408/23/21 13:030.0063 1
Hexachloro-1,3-butadiene ND mg/kg 08/23/21 19:38 87-68-308/23/21 13:030.013 1
2-Hexanone ND mg/kg 08/23/21 19:38 591-78-608/23/21 13:030.063 1
Isopropylbenzene (Cumene)ND mg/kg 08/23/21 19:38 98-82-808/23/21 13:030.0063 1
p-Isopropyltoluene ND mg/kg 08/23/21 19:38 99-87-608/23/21 13:030.0063 1
Methylene Chloride 0.075 mg/kg 08/23/21 19:38 75-09-208/23/21 13:030.025 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/23/21 19:38 108-10-108/23/21 13:030.063 1
Methyl-tert-butyl ether ND mg/kg 08/23/21 19:38 1634-04-408/23/21 13:030.0063 1
Naphthalene ND mg/kg 08/23/21 19:38 91-20-308/23/21 13:030.0063 1
n-Propylbenzene ND mg/kg 08/23/21 19:38 103-65-108/23/21 13:030.0063 1
Styrene ND mg/kg 08/23/21 19:38 100-42-508/23/21 13:030.0063 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/23/21 19:38 630-20-608/23/21 13:030.0063 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/23/21 19:38 79-34-508/23/21 13:030.0063 1
Tetrachloroethene ND mg/kg 08/23/21 19:38 127-18-408/23/21 13:030.0063 1
Toluene ND mg/kg 08/23/21 19:38 108-88-308/23/21 13:030.0063 1
1,2,3-Trichlorobenzene ND mg/kg 08/23/21 19:38 87-61-608/23/21 13:030.0063 1
1,2,4-Trichlorobenzene ND mg/kg 08/23/21 19:38 120-82-108/23/21 13:030.0063 1
1,1,1-Trichloroethane ND mg/kg 08/23/21 19:38 71-55-608/23/21 13:030.0063 1
1,1,2-Trichloroethane ND mg/kg 08/23/21 19:38 79-00-508/23/21 13:030.0063 1
Trichloroethene ND mg/kg 08/23/21 19:38 79-01-608/23/21 13:030.0063 1
Trichlorofluoromethane ND mg/kg 08/23/21 19:38 75-69-408/23/21 13:030.0063 1
1,2,3-Trichloropropane ND mg/kg 08/23/21 19:38 96-18-408/23/21 13:030.0063 1
1,2,4-Trimethylbenzene ND mg/kg 08/23/21 19:38 95-63-608/23/21 13:030.0063 1
1,3,5-Trimethylbenzene ND mg/kg 08/23/21 19:38 108-67-808/23/21 13:030.0063 1
Vinyl acetate ND mg/kg 08/23/21 19:38 108-05-408/23/21 13:030.063 1
Vinyl chloride ND mg/kg 08/23/21 19:38 75-01-4 v108/23/21 13:030.013 1
Xylene (Total)ND mg/kg 08/23/21 19:38 1330-20-708/23/21 13:030.013 1
m&p-Xylene ND mg/kg 08/23/21 19:38 179601-23-108/23/21 13:030.013 1
o-Xylene ND mg/kg 08/23/21 19:38 95-47-608/23/21 13:030.0063 1
Surrogates
Toluene-d8 (S)100 %08/23/21 19:38 2037-26-508/23/21 13:0370-130 1
4-Bromofluorobenzene (S)99 %08/23/21 19:38 460-00-408/23/21 13:0369-134 1
1,2-Dichloroethane-d4 (S)105 %08/23/21 19:38 17060-07-008/23/21 13:0370-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-4 Lab ID:92556378015 Collected:08/17/21 09:55 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.9 %08/18/21 18:04 N20.10 1
Sample:SS-5 Lab ID:92556378016 Collected:08/17/21 10:35 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 08/26/21 09:09 83-32-908/25/21 14:150.37 1
Acenaphthylene ND mg/kg 08/26/21 09:09 208-96-808/25/21 14:150.37 1
Aniline ND mg/kg 08/26/21 09:09 62-53-308/25/21 14:150.37 1
Anthracene ND mg/kg 08/26/21 09:09 120-12-708/25/21 14:150.37 1
Benzo(a)anthracene ND mg/kg 08/26/21 09:09 56-55-308/25/21 14:150.37 1
Benzo(a)pyrene ND mg/kg 08/26/21 09:09 50-32-808/25/21 14:150.37 1
Benzo(b)fluoranthene ND mg/kg 08/26/21 09:09 205-99-208/25/21 14:150.37 1
Benzo(g,h,i)perylene ND mg/kg 08/26/21 09:09 191-24-208/25/21 14:150.37 1
Benzo(k)fluoranthene ND mg/kg 08/26/21 09:09 207-08-908/25/21 14:150.37 1
Benzoic Acid ND mg/kg 08/26/21 09:09 65-85-008/25/21 14:151.9 1
Benzyl alcohol ND mg/kg 08/26/21 09:09 100-51-608/25/21 14:150.74 1
4-Bromophenylphenyl ether ND mg/kg 08/26/21 09:09 101-55-308/25/21 14:150.37 1
Butylbenzylphthalate ND mg/kg 08/26/21 09:09 85-68-708/25/21 14:150.37 1
4-Chloro-3-methylphenol ND mg/kg 08/26/21 09:09 59-50-708/25/21 14:150.74 1
4-Chloroaniline ND mg/kg 08/26/21 09:09 106-47-808/25/21 14:150.74 1
bis(2-Chloroethoxy)methane ND mg/kg 08/26/21 09:09 111-91-108/25/21 14:150.37 1
bis(2-Chloroethyl) ether ND mg/kg 08/26/21 09:09 111-44-408/25/21 14:150.37 1
2-Chloronaphthalene ND mg/kg 08/26/21 09:09 91-58-708/25/21 14:150.37 1
2-Chlorophenol ND mg/kg 08/26/21 09:09 95-57-808/25/21 14:150.37 1
4-Chlorophenylphenyl ether ND mg/kg 08/26/21 09:09 7005-72-308/25/21 14:150.37 1
Chrysene ND mg/kg 08/26/21 09:09 218-01-908/25/21 14:150.37 1
Dibenz(a,h)anthracene ND mg/kg 08/26/21 09:09 53-70-308/25/21 14:150.37 1
Dibenzofuran ND mg/kg 08/26/21 09:09 132-64-908/25/21 14:150.37 1
1,2-Dichlorobenzene ND mg/kg 08/26/21 09:09 95-50-108/25/21 14:150.37 1
1,3-Dichlorobenzene ND mg/kg 08/26/21 09:09 541-73-108/25/21 14:150.37 1
1,4-Dichlorobenzene ND mg/kg 08/26/21 09:09 106-46-708/25/21 14:150.37 1
3,3'-Dichlorobenzidine ND mg/kg 08/26/21 09:09 91-94-1 IL08/25/21 14:150.74 1
2,4-Dichlorophenol ND mg/kg 08/26/21 09:09 120-83-208/25/21 14:150.37 1
Diethylphthalate ND mg/kg 08/26/21 09:09 84-66-208/25/21 14:150.37 1
2,4-Dimethylphenol ND mg/kg 08/26/21 09:09 105-67-908/25/21 14:150.37 1
Dimethylphthalate ND mg/kg 08/26/21 09:09 131-11-308/25/21 14:150.37 1
Di-n-butylphthalate ND mg/kg 08/26/21 09:09 84-74-208/25/21 14:150.37 1
4,6-Dinitro-2-methylphenol ND mg/kg 08/26/21 09:09 534-52-1 v108/25/21 14:150.74 1
2,4-Dinitrophenol ND mg/kg 08/26/21 09:09 51-28-5 v108/25/21 14:151.9 1
2,4-Dinitrotoluene ND mg/kg 08/26/21 09:09 121-14-208/25/21 14:150.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-5 Lab ID:92556378016 Collected:08/17/21 10:35 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2,6-Dinitrotoluene ND mg/kg 08/26/21 09:09 606-20-208/25/21 14:150.37 1
Di-n-octylphthalate ND mg/kg 08/26/21 09:09 117-84-008/25/21 14:150.37 1
bis(2-Ethylhexyl)phthalate ND mg/kg 08/26/21 09:09 117-81-708/25/21 14:150.37 1
Fluoranthene ND mg/kg 08/26/21 09:09 206-44-008/25/21 14:150.37 1
Fluorene ND mg/kg 08/26/21 09:09 86-73-708/25/21 14:150.37 1
Hexachloro-1,3-butadiene ND mg/kg 08/26/21 09:09 87-68-308/25/21 14:150.37 1
Hexachlorobenzene ND mg/kg 08/26/21 09:09 118-74-108/25/21 14:150.37 1
Hexachlorocyclopentadiene ND mg/kg 08/26/21 09:09 77-47-408/25/21 14:150.37 1
Hexachloroethane ND mg/kg 08/26/21 09:09 67-72-108/25/21 14:150.37 1
Indeno(1,2,3-cd)pyrene ND mg/kg 08/26/21 09:09 193-39-508/25/21 14:150.37 1
Isophorone ND mg/kg 08/26/21 09:09 78-59-108/25/21 14:150.37 1
1-Methylnaphthalene ND mg/kg 08/26/21 09:09 90-12-008/25/21 14:150.37 1
2-Methylnaphthalene ND mg/kg 08/26/21 09:09 91-57-608/25/21 14:150.37 1
2-Methylphenol(o-Cresol)ND mg/kg 08/26/21 09:09 95-48-708/25/21 14:150.37 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 08/26/21 09:09 15831-10-408/25/21 14:150.37 1
Naphthalene ND mg/kg 08/26/21 09:09 91-20-308/25/21 14:150.37 1
2-Nitroaniline ND mg/kg 08/26/21 09:09 88-74-408/25/21 14:151.9 1
3-Nitroaniline ND mg/kg 08/26/21 09:09 99-09-2 IL08/25/21 14:151.9 1
4-Nitroaniline ND mg/kg 08/26/21 09:09 100-01-608/25/21 14:150.74 1
Nitrobenzene ND mg/kg 08/26/21 09:09 98-95-308/25/21 14:150.37 1
2-Nitrophenol ND mg/kg 08/26/21 09:09 88-75-508/25/21 14:150.37 1
4-Nitrophenol ND mg/kg 08/26/21 09:09 100-02-708/25/21 14:151.9 1
N-Nitrosodimethylamine ND mg/kg 08/26/21 09:09 62-75-9 v108/25/21 14:150.37 1
N-Nitroso-di-n-propylamine ND mg/kg 08/26/21 09:09 621-64-708/25/21 14:150.37 1
N-Nitrosodiphenylamine ND mg/kg 08/26/21 09:09 86-30-608/25/21 14:150.37 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 08/26/21 09:09 108-60-108/25/21 14:150.37 1
Pentachlorophenol ND mg/kg 08/26/21 09:09 87-86-508/25/21 14:150.74 1
Phenanthrene ND mg/kg 08/26/21 09:09 85-01-808/25/21 14:150.37 1
Phenol ND mg/kg 08/26/21 09:09 108-95-2 v108/25/21 14:150.37 1
Pyrene ND mg/kg 08/26/21 09:09 129-00-008/25/21 14:150.37 1
Pyridine ND mg/kg 08/26/21 09:09 110-86-1 v108/25/21 14:150.37 1
1,2,4-Trichlorobenzene ND mg/kg 08/26/21 09:09 120-82-108/25/21 14:150.37 1
2,4,5-Trichlorophenol ND mg/kg 08/26/21 09:09 95-95-408/25/21 14:150.37 1
2,4,6-Trichlorophenol ND mg/kg 08/26/21 09:09 88-06-208/25/21 14:150.37 1
Surrogates
Nitrobenzene-d5 (S)69 %08/26/21 09:09 4165-60-008/25/21 14:1521-130 1
2-Fluorobiphenyl (S)52 %08/26/21 09:09 321-60-808/25/21 14:1519-130 1
Terphenyl-d14 (S)56 %08/26/21 09:09 1718-51-008/25/21 14:1515-130 1
Phenol-d6 (S)72 %08/26/21 09:09 13127-88-308/25/21 14:1518-130 1
2-Fluorophenol (S)68 %08/26/21 09:09 367-12-408/25/21 14:1518-130 1
2,4,6-Tribromophenol (S)68 %08/26/21 09:09 118-79-608/25/21 14:1518-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND mg/kg 08/23/21 19:56 67-64-108/23/21 13:030.11 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-5 Lab ID:92556378016 Collected:08/17/21 10:35 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Benzene ND mg/kg 08/23/21 19:56 71-43-208/23/21 13:030.0056 1
Bromobenzene ND mg/kg 08/23/21 19:56 108-86-108/23/21 13:030.0056 1
Bromochloromethane ND mg/kg 08/23/21 19:56 74-97-508/23/21 13:030.0056 1
Bromodichloromethane ND mg/kg 08/23/21 19:56 75-27-408/23/21 13:030.0056 1
Bromoform ND mg/kg 08/23/21 19:56 75-25-208/23/21 13:030.0056 1
Bromomethane ND mg/kg 08/23/21 19:56 74-83-9 v108/23/21 13:030.011 1
2-Butanone (MEK)ND mg/kg 08/23/21 19:56 78-93-308/23/21 13:030.11 1
n-Butylbenzene ND mg/kg 08/23/21 19:56 104-51-808/23/21 13:030.0056 1
sec-Butylbenzene ND mg/kg 08/23/21 19:56 135-98-808/23/21 13:030.0056 1
tert-Butylbenzene ND mg/kg 08/23/21 19:56 98-06-608/23/21 13:030.0056 1
Carbon tetrachloride ND mg/kg 08/23/21 19:56 56-23-508/23/21 13:030.0056 1
Chlorobenzene ND mg/kg 08/23/21 19:56 108-90-708/23/21 13:030.0056 1
Chloroethane ND mg/kg 08/23/21 19:56 75-00-3 v108/23/21 13:030.011 1
Chloroform ND mg/kg 08/23/21 19:56 67-66-308/23/21 13:030.0056 1
Chloromethane ND mg/kg 08/23/21 19:56 74-87-308/23/21 13:030.011 1
2-Chlorotoluene ND mg/kg 08/23/21 19:56 95-49-808/23/21 13:030.0056 1
4-Chlorotoluene ND mg/kg 08/23/21 19:56 106-43-408/23/21 13:030.0056 1
1,2-Dibromo-3-chloropropane ND mg/kg 08/23/21 19:56 96-12-808/23/21 13:030.0056 1
Dibromochloromethane ND mg/kg 08/23/21 19:56 124-48-108/23/21 13:030.0056 1
1,2-Dibromoethane (EDB)ND mg/kg 08/23/21 19:56 106-93-408/23/21 13:030.0056 1
Dibromomethane ND mg/kg 08/23/21 19:56 74-95-308/23/21 13:030.0056 1
1,2-Dichlorobenzene ND mg/kg 08/23/21 19:56 95-50-108/23/21 13:030.0056 1
1,3-Dichlorobenzene ND mg/kg 08/23/21 19:56 541-73-108/23/21 13:030.0056 1
1,4-Dichlorobenzene ND mg/kg 08/23/21 19:56 106-46-708/23/21 13:030.0056 1
Dichlorodifluoromethane ND mg/kg 08/23/21 19:56 75-71-8 IK,v108/23/21 13:030.011 1
1,1-Dichloroethane ND mg/kg 08/23/21 19:56 75-34-308/23/21 13:030.0056 1
1,2-Dichloroethane ND mg/kg 08/23/21 19:56 107-06-208/23/21 13:030.0056 1
1,1-Dichloroethene ND mg/kg 08/23/21 19:56 75-35-408/23/21 13:030.0056 1
cis-1,2-Dichloroethene ND mg/kg 08/23/21 19:56 156-59-208/23/21 13:030.0056 1
trans-1,2-Dichloroethene ND mg/kg 08/23/21 19:56 156-60-508/23/21 13:030.0056 1
1,2-Dichloropropane ND mg/kg 08/23/21 19:56 78-87-508/23/21 13:030.0056 1
1,3-Dichloropropane ND mg/kg 08/23/21 19:56 142-28-908/23/21 13:030.0056 1
2,2-Dichloropropane ND mg/kg 08/23/21 19:56 594-20-708/23/21 13:030.0056 1
1,1-Dichloropropene ND mg/kg 08/23/21 19:56 563-58-608/23/21 13:030.0056 1
cis-1,3-Dichloropropene ND mg/kg 08/23/21 19:56 10061-01-508/23/21 13:030.0056 1
trans-1,3-Dichloropropene ND mg/kg 08/23/21 19:56 10061-02-608/23/21 13:030.0056 1
Diisopropyl ether ND mg/kg 08/23/21 19:56 108-20-308/23/21 13:030.0056 1
Ethylbenzene ND mg/kg 08/23/21 19:56 100-41-408/23/21 13:030.0056 1
Hexachloro-1,3-butadiene ND mg/kg 08/23/21 19:56 87-68-308/23/21 13:030.011 1
2-Hexanone ND mg/kg 08/23/21 19:56 591-78-608/23/21 13:030.056 1
Isopropylbenzene (Cumene)ND mg/kg 08/23/21 19:56 98-82-808/23/21 13:030.0056 1
p-Isopropyltoluene ND mg/kg 08/23/21 19:56 99-87-608/23/21 13:030.0056 1
Methylene Chloride 0.041 mg/kg 08/23/21 19:56 75-09-208/23/21 13:030.022 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 08/23/21 19:56 108-10-108/23/21 13:030.056 1
Methyl-tert-butyl ether ND mg/kg 08/23/21 19:56 1634-04-408/23/21 13:030.0056 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 94
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92556378
N. Graham & 6th
Sample:SS-5 Lab ID:92556378016 Collected:08/17/21 10:35 Received:08/18/21 11:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Naphthalene ND mg/kg 08/23/21 19:56 91-20-308/23/21 13:030.0056 1
n-Propylbenzene ND mg/kg 08/23/21 19:56 103-65-108/23/21 13:030.0056 1
Styrene ND mg/kg 08/23/21 19:56 100-42-508/23/21 13:030.0056 1
1,1,1,2-Tetrachloroethane ND mg/kg 08/23/21 19:56 630-20-608/23/21 13:030.0056 1
1,1,2,2-Tetrachloroethane ND mg/kg 08/23/21 19:56 79-34-508/23/21 13:030.0056 1
Tetrachloroethene ND mg/kg 08/23/21 19:56 127-18-408/23/21 13:030.0056 1
Toluene ND mg/kg 08/23/21 19:56 108-88-308/23/21 13:030.0056 1
1,2,3-Trichlorobenzene ND mg/kg 08/23/21 19:56 87-61-608/23/21 13:030.0056 1
1,2,4-Trichlorobenzene ND mg/kg 08/23/21 19:56 120-82-108/23/21 13:030.0056 1
1,1,1-Trichloroethane ND mg/kg 08/23/21 19:56 71-55-608/23/21 13:030.0056 1
1,1,2-Trichloroethane ND mg/kg 08/23/21 19:56 79-00-508/23/21 13:030.0056 1
Trichloroethene ND mg/kg 08/23/21 19:56 79-01-608/23/21 13:030.0056 1
Trichlorofluoromethane ND mg/kg 08/23/21 19:56 75-69-408/23/21 13:030.0056 1
1,2,3-Trichloropropane ND mg/kg 08/23/21 19:56 96-18-408/23/21 13:030.0056 1
1,2,4-Trimethylbenzene ND mg/kg 08/23/21 19:56 95-63-608/23/21 13:030.0056 1
1,3,5-Trimethylbenzene ND mg/kg 08/23/21 19:56 108-67-808/23/21 13:030.0056 1
Vinyl acetate ND mg/kg 08/23/21 19:56 108-05-408/23/21 13:030.056 1
Vinyl chloride ND mg/kg 08/23/21 19:56 75-01-4 v108/23/21 13:030.011 1
Xylene (Total)ND mg/kg 08/23/21 19:56 1330-20-708/23/21 13:030.011 1
m&p-Xylene ND mg/kg 08/23/21 19:56 179601-23-108/23/21 13:030.011 1
o-Xylene ND mg/kg 08/23/21 19:56 95-47-608/23/21 13:030.0056 1
Surrogates
Toluene-d8 (S)101 %08/23/21 19:56 2037-26-508/23/21 13:0370-130 1
4-Bromofluorobenzene (S)94 %08/23/21 19:56 460-00-408/23/21 13:0369-134 1
1,2-Dichloroethane-d4 (S)106 %08/23/21 19:56 17060-07-008/23/21 13:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 12.3 %08/18/21 18:04 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
642240
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92556378012, 92556378013, 92556378014, 92556378015, 92556378016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3370685
Associated Lab Samples:92556378012, 92556378013, 92556378014, 92556378015, 92556378016
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 08/23/21 13:48
1,1,1-Trichloroethane mg/kg ND 0.0050 08/23/21 13:48
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 08/23/21 13:48
1,1,2-Trichloroethane mg/kg ND 0.0050 08/23/21 13:48
1,1-Dichloroethane mg/kg ND 0.0050 08/23/21 13:48
1,1-Dichloroethene mg/kg ND 0.0050 08/23/21 13:48
1,1-Dichloropropene mg/kg ND 0.0050 08/23/21 13:48
1,2,3-Trichlorobenzene mg/kg ND 0.0050 08/23/21 13:48
1,2,3-Trichloropropane mg/kg ND 0.0050 08/23/21 13:48
1,2,4-Trichlorobenzene mg/kg ND 0.0050 08/23/21 13:48
1,2,4-Trimethylbenzene mg/kg ND 0.0050 08/23/21 13:48
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 08/23/21 13:48
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 08/23/21 13:48
1,2-Dichlorobenzene mg/kg ND 0.0050 08/23/21 13:48
1,2-Dichloroethane mg/kg ND 0.0050 08/23/21 13:48
1,2-Dichloropropane mg/kg ND 0.0050 08/23/21 13:48
1,3,5-Trimethylbenzene mg/kg ND 0.0050 08/23/21 13:48
1,3-Dichlorobenzene mg/kg ND 0.0050 08/23/21 13:48
1,3-Dichloropropane mg/kg ND 0.0050 08/23/21 13:48
1,4-Dichlorobenzene mg/kg ND 0.0050 08/23/21 13:48
2,2-Dichloropropane mg/kg ND 0.0050 08/23/21 13:48
2-Butanone (MEK)mg/kg ND 0.10 08/23/21 13:48
2-Chlorotoluene mg/kg ND 0.0050 08/23/21 13:48
2-Hexanone mg/kg ND 0.050 08/23/21 13:48
4-Chlorotoluene mg/kg ND 0.0050 08/23/21 13:48
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 08/23/21 13:48
Acetone mg/kg ND 0.10 08/23/21 13:48
Benzene mg/kg ND 0.0050 08/23/21 13:48
Bromobenzene mg/kg ND 0.0050 08/23/21 13:48
Bromochloromethane mg/kg ND 0.0050 08/23/21 13:48
Bromodichloromethane mg/kg ND 0.0050 08/23/21 13:48
Bromoform mg/kg ND 0.0050 08/23/21 13:48
Bromomethane mg/kg ND 0.010 v108/23/21 13:48
Carbon tetrachloride mg/kg ND 0.0050 08/23/21 13:48
Chlorobenzene mg/kg ND 0.0050 08/23/21 13:48
Chloroethane mg/kg ND 0.010 v108/23/21 13:48
Chloroform mg/kg ND 0.0050 08/23/21 13:48
Chloromethane mg/kg ND 0.010 08/23/21 13:48
cis-1,2-Dichloroethene mg/kg ND 0.0050 08/23/21 13:48
cis-1,3-Dichloropropene mg/kg ND 0.0050 08/23/21 13:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3370685
Associated Lab Samples:92556378012, 92556378013, 92556378014, 92556378015, 92556378016
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 08/23/21 13:48
Dibromomethane mg/kg ND 0.0050 08/23/21 13:48
Dichlorodifluoromethane mg/kg ND 0.010 IK,v108/23/21 13:48
Diisopropyl ether mg/kg ND 0.0050 08/23/21 13:48
Ethylbenzene mg/kg ND 0.0050 08/23/21 13:48
Hexachloro-1,3-butadiene mg/kg ND 0.010 08/23/21 13:48
Isopropylbenzene (Cumene)mg/kg ND 0.0050 08/23/21 13:48
m&p-Xylene mg/kg ND 0.010 08/23/21 13:48
Methyl-tert-butyl ether mg/kg ND 0.0050 08/23/21 13:48
Methylene Chloride mg/kg ND 0.020 08/23/21 13:48
n-Butylbenzene mg/kg ND 0.0050 08/23/21 13:48
n-Propylbenzene mg/kg ND 0.0050 08/23/21 13:48
Naphthalene mg/kg ND 0.0050 08/23/21 13:48
o-Xylene mg/kg ND 0.0050 08/23/21 13:48
p-Isopropyltoluene mg/kg ND 0.0050 08/23/21 13:48
sec-Butylbenzene mg/kg ND 0.0050 08/23/21 13:48
Styrene mg/kg ND 0.0050 08/23/21 13:48
tert-Butylbenzene mg/kg ND 0.0050 08/23/21 13:48
Tetrachloroethene mg/kg ND 0.0050 08/23/21 13:48
Toluene mg/kg ND 0.0050 08/23/21 13:48
trans-1,2-Dichloroethene mg/kg ND 0.0050 08/23/21 13:48
trans-1,3-Dichloropropene mg/kg ND 0.0050 08/23/21 13:48
Trichloroethene mg/kg ND 0.0050 08/23/21 13:48
Trichlorofluoromethane mg/kg ND 0.0050 08/23/21 13:48
Vinyl acetate mg/kg ND 0.050 08/23/21 13:48
Vinyl chloride mg/kg ND 0.010 v108/23/21 13:48
Xylene (Total)mg/kg ND 0.010 08/23/21 13:48
1,2-Dichloroethane-d4 (S)%109 70-130 08/23/21 13:48
4-Bromofluorobenzene (S)%99 69-134 08/23/21 13:48
Toluene-d8 (S)%102 70-130 08/23/21 13:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3370686LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 1.21.2 100 70-130
1,1,1-Trichloroethane mg/kg 1.31.2 104 70-130
1,1,2,2-Tetrachloroethane mg/kg 1.21.2 99 70-130
1,1,2-Trichloroethane mg/kg 1.31.2 102 70-130
1,1-Dichloroethane mg/kg 1.31.2 105 70-130
1,1-Dichloroethene mg/kg 1.31.2 107 70-130
1,1-Dichloropropene mg/kg 1.31.2 106 70-130
1,2,3-Trichlorobenzene mg/kg 1.51.2 116 65-130
1,2,3-Trichloropropane mg/kg 1.31.2 107 70-130
1,2,4-Trichlorobenzene mg/kg 1.41.2 114 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3370686LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene mg/kg 1.41.2 114 70-130
1,2-Dibromo-3-chloropropane mg/kg 1.41.2 112 70-130
1,2-Dibromoethane (EDB)mg/kg 1.21.2 96 70-130
1,2-Dichlorobenzene mg/kg 1.31.2 102 70-130
1,2-Dichloroethane mg/kg 1.21.2 100 63-130
1,2-Dichloropropane mg/kg 1.31.2 102 70-130
1,3,5-Trimethylbenzene mg/kg 1.31.2 107 70-130
1,3-Dichlorobenzene mg/kg 1.51.2 117 70-130
1,3-Dichloropropane mg/kg 1.21.2 95 70-130
1,4-Dichlorobenzene mg/kg 1.41.2 114 70-130
2,2-Dichloropropane mg/kg 1.31.2 105 66-130
2-Butanone (MEK)mg/kg 2.22.5 90 70-130
2-Chlorotoluene mg/kg 1.31.2 106 70-130
2-Hexanone mg/kg 2.62.5 104 70-130
4-Chlorotoluene mg/kg 1.31.2 101 70-130
4-Methyl-2-pentanone (MIBK)mg/kg 2.52.5 99 70-130
Acetone mg/kg 2.82.5 112 69-130
Benzene mg/kg 1.31.2 102 70-130
Bromobenzene mg/kg 1.31.2 104 70-130
Bromochloromethane mg/kg 1.31.2 107 70-130
Bromodichloromethane mg/kg 1.31.2 104 69-130
Bromoform mg/kg 1.41.2 108 70-130
Bromomethane mg/kg 1.6 v11.2 126 52-130
Carbon tetrachloride mg/kg 1.41.2 111 70-130
Chlorobenzene mg/kg 1.31.2 101 70-130
Chloroethane mg/kg 1.6 v11.2 127 65-130
Chloroform mg/kg 1.41.2 110 70-130
Chloromethane mg/kg 1.41.2 113 55-130
cis-1,2-Dichloroethene mg/kg 1.31.2 102 70-130
cis-1,3-Dichloropropene mg/kg 1.31.2 102 70-130
Dibromochloromethane mg/kg 1.41.2 108 70-130
Dibromomethane mg/kg 1.31.2 103 70-130
Dichlorodifluoromethane mg/kg 1.7 IK,v11.2 138 45-156
Diisopropyl ether mg/kg 1.21.2 98 70-130
Ethylbenzene mg/kg 1.41.2 109 70-130
Hexachloro-1,3-butadiene mg/kg 1.51.2 118 66-130
Isopropylbenzene (Cumene)mg/kg 1.31.2 105 70-130
m&p-Xylene mg/kg 2.52.5 101 70-130
Methyl-tert-butyl ether mg/kg 1.31.2 105 70-130
Methylene Chloride mg/kg 1.31.2 107 65-130
n-Butylbenzene mg/kg 1.51.2 117 67-130
n-Propylbenzene mg/kg 1.31.2 105 70-130
Naphthalene mg/kg 1.31.2 103 70-130
o-Xylene mg/kg 1.21.2 99 70-130
p-Isopropyltoluene mg/kg 1.41.2 115 67-130
sec-Butylbenzene mg/kg 1.31.2 107 69-130
Styrene mg/kg 1.31.2 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3370686LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene mg/kg 1.41.2 114 67-130
Tetrachloroethene mg/kg 1.31.2 107 70-130
Toluene mg/kg 1.31.2 101 70-130
trans-1,2-Dichloroethene mg/kg 1.31.2 107 70-130
trans-1,3-Dichloropropene mg/kg 1.41.2 109 68-130
Trichloroethene mg/kg 1.31.2 100 70-130
Trichlorofluoromethane mg/kg 1.41.2 109 70-130
Vinyl acetate mg/kg 2.82.5 111 70-130
Vinyl chloride mg/kg 1.5 v11.2 123 61-130
Xylene (Total)mg/kg 3.83.8 100 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%96 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3370687MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92555973010
3370688
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane mg/kg 57.7 105 70-131103 157.7ND 60.4 59.7
1,1,1-Trichloroethane mg/kg 57.7 112 65-133115 257.7ND 64.5 66.1
1,1,2,2-Tetrachloroethane mg/kg 57.7 106 66-130105 157.7ND 60.9 60.4
1,1,2-Trichloroethane mg/kg 57.7 109 66-133108 157.7ND 62.9 62.5
1,1-Dichloroethane mg/kg 57.7 113 65-130115 257.7ND 65.1 66.6
1,1-Dichloroethene mg/kg 57.7 119 10-158119 057.7ND 68.7 68.6
1,1-Dichloropropene mg/kg 57.7 113 68-133118 457.7ND 65.3 67.9
1,2,3-Trichlorobenzene mg/kg 57.7 111 27-138103 757.7ND 63.9 59.3
1,2,3-Trichloropropane mg/kg 57.7 111 67-130108 357.7ND 64.3 62.2
1,2,4-Trichlorobenzene mg/kg 57.7 113 51-134108 557.7ND 65.0 62.0
1,2,4-Trimethylbenzene mg/kg M157.7 128 63-136145 457.7162000
ug/kg 235 246
1,2-Dibromo-3-chloropropane mg/kg 57.7 113 32-130111 257.7ND 65.3 64.1
1,2-Dibromoethane (EDB)mg/kg 57.7 103 70-13099 457.7ND 59.3 57.1
1,2-Dichlorobenzene mg/kg 57.7 103 69-13099 457.7ND 59.2 56.8
1,2-Dichloroethane mg/kg 57.7 106 59-130107 157.7ND 61.1 61.5
1,2-Dichloropropane mg/kg 57.7 106 70-130105 157.7ND 61.4 60.6
1,3,5-Trimethylbenzene mg/kg M157.7 182 65-137182 057.7ND 105 105
1,3-Dichlorobenzene mg/kg 57.7 115 70-130110 457.7ND 66.1 63.6
1,3-Dichloropropane mg/kg 57.7 98 70-13099 157.7ND 56.8 57.3
1,4-Dichlorobenzene mg/kg 57.7 117 68-130109 757.7ND 67.2 63.0
2,2-Dichloropropane mg/kg 57.7 109 32-130113 457.7ND 62.9 65.1
2-Butanone (MEK)mg/kg 115 106 10-136104 2115ND123120
2-Chlorotoluene mg/kg 57.7 113 69-141108 457.7ND 65.1 62.4
2-Hexanone mg/kg 115 112 10-144110 2115ND129127
4-Chlorotoluene mg/kg 57.7 110 70-132106 457.7ND 63.7 61.3
4-Methyl-2-pentanone (MIBK)mg/kg 115 103 25-143102 1115ND119118
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3370687MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92555973010
3370688
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Acetone mg/kg 115 116 10-130121 411525600
ug/kg 159 165
Benzene mg/kg 57.7 105 67-130112 457.734700
ug/kg 95.5 99.5
Bromobenzene mg/kg 57.7 105 70-130102 357.7ND 60.5 59.0
Bromochloromethane mg/kg 57.7 109 69-134113 357.7ND 63.1 65.3
Bromodichloromethane mg/kg 57.7 104 64-130105 157.7ND 59.9 60.4
Bromoform mg/kg 57.7 109 62-130106 357.7ND 62.9 61.2
Bromomethane mg/kg v157.7 133 20-176130 257.7ND 76.7 74.9
Carbon tetrachloride mg/kg 57.7 114 65-140111 357.7ND 66.0 64.2
Chlorobenzene mg/kg 57.7 106 70-130104 157.7ND 60.9 60.1
Chloroethane mg/kg M1,v157.7 134 10-130135 157.7ND 77.3 78.0
Chloroform mg/kg 57.7 119 63-130121 157.7ND 68.9 69.9
Chloromethane mg/kg 57.7 125 58-130127 157.7ND 72.4 73.4
cis-1,2-Dichloroethene mg/kg 57.7 108 66-130112 357.7ND 62.5 64.5
cis-1,3-Dichloropropene mg/kg 57.7 102 67-130102 057.7ND 58.7 58.6
Dibromochloromethane mg/kg 57.7 109 67-130110 057.7ND 63.2 63.2
Dibromomethane mg/kg 57.7 104 63-131100 457.7ND 60.1 57.7
Dichlorodifluoromethane mg/kg IK,v157.7 150 44-180152 157.7ND 86.4 87.6
Diisopropyl ether mg/kg 57.7 105 63-130106 057.7ND 60.6 60.9
Ethylbenzene mg/kg 57.7 113 66-130125 557.782200
ug/kg 147 154
Hexachloro-1,3-butadiene mg/kg 57.7 114 64-150112 257.7ND 65.8 64.4
Isopropylbenzene (Cumene)mg/kg 57.7 107 69-135105 157.77050
ug/kg 68.5 67.6
m&p-Xylene mg/kg 115 107 60-133125 5115291000
ug/kg
415 435
Methyl-tert-butyl ether mg/kg 57.7 109 65-130112 357.7ND 62.8 64.5
Methylene Chloride mg/kg 57.7 127 61-130125 157.7ND 73.1 72.1
n-Butylbenzene mg/kg 57.7 138 65-140121 1257.78910
ug/kg
88.4 78.5
n-Propylbenzene mg/kg 57.7 104 67-140104 057.726600
ug/kg 86.5 86.5
Naphthalene mg/kg 57.7 103 15-145100 257.717600
ug/kg 77.0 75.5
o-Xylene mg/kg 57.7 107 66-133119 457.7111000
ug/kg 172 180
p-Isopropyltoluene mg/kg 57.7 117 56-147111 457.76520
ug/kg 73.7 70.6
sec-Butylbenzene mg/kg 57.7 110 65-139108 257.7ND 63.6 62.1
Styrene mg/kg 57.7 109 70-132107 257.73190
ug/kg 66.0 64.9
tert-Butylbenzene mg/kg 57.7 116 62-135113 357.7ND 66.9 65.0
Tetrachloroethene mg/kg 57.7 111 70-135105 557.7ND 63.9 60.8
Toluene mg/kg M157.7 113 67-130161 857.7259000
ug/kg 324 352
trans-1,2-Dichloroethene mg/kg 57.7 113 69-130113 057.7ND 65.3 65.4
trans-1,3-Dichloropropene mg/kg 57.7 108 62-130107 157.7ND 62.4 61.7
Trichloroethene mg/kg 57.7 103 70-135103 057.7ND 59.5 59.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3370687MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92555973010
3370688
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Trichlorofluoromethane mg/kg 57.7 117 10-130120 257.7ND 67.3 69.0
Vinyl acetate mg/kg 115 110 53-130108 1115ND127125
Vinyl chloride mg/kg v157.7 129 61-148132 357.7ND 74.4 76.4
Xylene (Total)mg/kg 173 107 63-132123 5173402000
ug/kg 587 615
1,2-Dichloroethane-d4 (S)%107 70-130110
4-Bromofluorobenzene (S)%101 69-13499
Toluene-d8 (S)%102 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
641729
EPA 8260D
EPA 8260D
8260D MSV Low Level
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92556378001, 92556378002, 92556378003, 92556378004, 92556378005, 92556378006, 92556378007,
92556378008, 92556378009, 92556378010, 92556378011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3368212
Associated Lab Samples:92556378001, 92556378002, 92556378003, 92556378004, 92556378005, 92556378006, 92556378007,
92556378008, 92556378009, 92556378010, 92556378011
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 08/20/21 00:29
1,1,1-Trichloroethane ug/L ND 1.0 08/20/21 00:29
1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/20/21 00:29
1,1,2-Trichloroethane ug/L ND 1.0 08/20/21 00:29
1,1-Dichloroethane ug/L ND 1.0 08/20/21 00:29
1,1-Dichloroethene ug/L ND 1.0 08/20/21 00:29
1,1-Dichloropropene ug/L ND 1.0 08/20/21 00:29
1,2,3-Trichlorobenzene ug/L ND 1.0 08/20/21 00:29
1,2,3-Trichloropropane ug/L ND 1.0 08/20/21 00:29
1,2,4-Trichlorobenzene ug/L ND 1.0 08/20/21 00:29
1,2-Dibromo-3-chloropropane ug/L ND 2.0 08/20/21 00:29
1,2-Dibromoethane (EDB)ug/L ND 1.0 08/20/21 00:29
1,2-Dichlorobenzene ug/L ND 1.0 08/20/21 00:29
1,2-Dichloroethane ug/L ND 1.0 08/20/21 00:29
1,2-Dichloropropane ug/L ND 1.0 08/20/21 00:29
1,3-Dichlorobenzene ug/L ND 1.0 08/20/21 00:29
1,3-Dichloropropane ug/L ND 1.0 08/20/21 00:29
1,4-Dichlorobenzene ug/L ND 1.0 08/20/21 00:29
2,2-Dichloropropane ug/L ND 1.0 08/20/21 00:29
2-Butanone (MEK)ug/L ND 5.0 08/20/21 00:29
2-Chlorotoluene ug/L ND 1.0 08/20/21 00:29
2-Hexanone ug/L ND 5.0 08/20/21 00:29
4-Chlorotoluene ug/L ND 1.0 08/20/21 00:29
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 08/20/21 00:29
Acetone ug/L ND 25.0 08/20/21 00:29
Benzene ug/L ND 1.0 08/20/21 00:29
Bromobenzene ug/L ND 1.0 08/20/21 00:29
Bromochloromethane ug/L ND 1.0 08/20/21 00:29
Bromodichloromethane ug/L ND 1.0 08/20/21 00:29
Bromoform ug/L ND 1.0 08/20/21 00:29
Bromomethane ug/L ND 2.0 08/20/21 00:29
Carbon tetrachloride ug/L ND 1.0 08/20/21 00:29
Chlorobenzene ug/L ND 1.0 08/20/21 00:29
Chloroethane ug/L ND 1.0 IL08/20/21 00:29
Chloroform ug/L ND 1.0 08/20/21 00:29
Chloromethane ug/L ND 1.0 v208/20/21 00:29
cis-1,2-Dichloroethene ug/L ND 1.0 08/20/21 00:29
cis-1,3-Dichloropropene ug/L ND 1.0 08/20/21 00:29
Dibromochloromethane ug/L ND 1.0 08/20/21 00:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3368212
Associated Lab Samples:92556378001, 92556378002, 92556378003, 92556378004, 92556378005, 92556378006, 92556378007,
92556378008, 92556378009, 92556378010, 92556378011
Matrix:Water
Analyzed
Dibromomethane ug/L ND 1.0 08/20/21 00:29
Dichlorodifluoromethane ug/L ND 1.0 08/20/21 00:29
Diisopropyl ether ug/L ND 1.0 08/20/21 00:29
Ethylbenzene ug/L ND 1.0 08/20/21 00:29
Hexachloro-1,3-butadiene ug/L ND 2.0 08/20/21 00:29
m&p-Xylene ug/L ND 2.0 08/20/21 00:29
Methyl-tert-butyl ether ug/L ND 1.0 08/20/21 00:29
Methylene Chloride ug/L ND 5.0 08/20/21 00:29
Naphthalene ug/L ND 1.0 08/20/21 00:29
o-Xylene ug/L ND 1.0 08/20/21 00:29
p-Isopropyltoluene ug/L ND 1.0 08/20/21 00:29
Styrene ug/L ND 1.0 08/20/21 00:29
Tetrachloroethene ug/L ND 1.0 08/20/21 00:29
Toluene ug/L ND 1.0 08/20/21 00:29
trans-1,2-Dichloroethene ug/L ND 1.0 08/20/21 00:29
trans-1,3-Dichloropropene ug/L ND 1.0 08/20/21 00:29
Trichloroethene ug/L ND 1.0 08/20/21 00:29
Trichlorofluoromethane ug/L ND 1.0 08/20/21 00:29
Vinyl acetate ug/L ND 2.0 08/20/21 00:29
Vinyl chloride ug/L ND 1.0 08/20/21 00:29
Xylene (Total)ug/L ND 1.0 08/20/21 00:29
1,2-Dichloroethane-d4 (S)%98 70-130 08/20/21 00:29
4-Bromofluorobenzene (S)%102 70-130 08/20/21 00:29
Toluene-d8 (S)%103 70-130 08/20/21 00:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3368213LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.750 101 70-130
1,1,1-Trichloroethane ug/L 51.050 102 70-130
1,1,2,2-Tetrachloroethane ug/L 51.150 102 70-130
1,1,2-Trichloroethane ug/L 52.650 105 70-130
1,1-Dichloroethane ug/L 52.050 104 70-130
1,1-Dichloroethene ug/L 51.050 102 70-132
1,1-Dichloropropene ug/L 48.650 97 70-131
1,2,3-Trichlorobenzene ug/L 56.350 113 70-134
1,2,3-Trichloropropane ug/L 48.950 98 70-130
1,2,4-Trichlorobenzene ug/L 53.850 108 70-130
1,2-Dibromo-3-chloropropane ug/L 50.950 102 70-132
1,2-Dibromoethane (EDB)ug/L 51.950 104 70-130
1,2-Dichlorobenzene ug/L 49.850 100 70-130
1,2-Dichloroethane ug/L 49.050 98 70-130
1,2-Dichloropropane ug/L 50.950 102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3368213LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.750 99 70-130
1,3-Dichloropropane ug/L 52.250 104 70-130
1,4-Dichlorobenzene ug/L 50.350 101 70-130
2,2-Dichloropropane ug/L 51.250 102 70-130
2-Butanone (MEK)ug/L 111100 111 70-133
2-Chlorotoluene ug/L 50.050 100 70-130
2-Hexanone ug/L 104100 104 70-130
4-Chlorotoluene ug/L 47.650 95 70-130
4-Methyl-2-pentanone (MIBK)ug/L 107100 107 70-130
Acetone ug/L 99.4100 99 70-144
Benzene ug/L 50.050 100 70-130
Bromobenzene ug/L 50.750 101 70-130
Bromochloromethane ug/L 51.850 104 70-130
Bromodichloromethane ug/L 49.050 98 70-130
Bromoform ug/L 45.250 90 70-131
Bromomethane ug/L 54.250 108 30-177
Carbon tetrachloride ug/L 50.650 101 70-130
Chlorobenzene ug/L 49.950 100 70-130
Chloroethane ug/L 36.9 IL507446-131
Chloroform ug/L 48.850 98 70-130
Chloromethane ug/L 35.6 v3507149-130
cis-1,2-Dichloroethene ug/L 51.050 102 70-130
cis-1,3-Dichloropropene ug/L 49.950 100 70-130
Dibromochloromethane ug/L 46.850 94 70-130
Dibromomethane ug/L 49.550 99 70-130
Dichlorodifluoromethane ug/L 41.950 84 52-134
Diisopropyl ether ug/L 47.050 94 70-131
Ethylbenzene ug/L 49.950 100 70-130
Hexachloro-1,3-butadiene ug/L 52.850 106 70-131
m&p-Xylene ug/L 101100 101 70-130
Methyl-tert-butyl ether ug/L 53.850 108 70-130
Methylene Chloride ug/L 48.750 97 68-130
Naphthalene ug/L 52.450 105 70-133
o-Xylene ug/L 50.150 100 70-130
p-Isopropyltoluene ug/L 52.250 104 70-130
Styrene ug/L 50.550 101 70-130
Tetrachloroethene ug/L 49.450 99 70-130
Toluene ug/L 49.950 100 70-130
trans-1,2-Dichloroethene ug/L 53.050 106 70-130
trans-1,3-Dichloropropene ug/L 48.850 98 70-130
Trichloroethene ug/L 51.750 103 70-130
Trichlorofluoromethane ug/L 46.950 94 61-130
Vinyl acetate ug/L 116100 116 70-140
Vinyl chloride ug/L 47.150 94 59-142
Xylene (Total)ug/L 151150 101 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3368213LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3368214MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92556367009
3368215
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 105 70-135100 520ND21.0 20.0
1,1,1-Trichloroethane ug/L 20 108 70-148104 420ND21.6 20.8
1,1,2,2-Tetrachloroethane ug/L 20 98 70-13198 020ND19.7 19.6
1,1,2-Trichloroethane ug/L 20 99 70-13697 220ND19.7 19.4
1,1-Dichloroethane ug/L 20 108 70-147104 3200.41J 22.0 21.3
1,1-Dichloroethene ug/L 20 112 70-158108 420ND22.5 21.7
1,1-Dichloropropene ug/L 20 108 70-149106 220ND21.7 21.2
1,2,3-Trichlorobenzene ug/L 20 100 68-140100 020ND20.0 20.0
1,2,3-Trichloropropane ug/L 20 99 67-13799 120ND19.8 19.9
1,2,4-Trichlorobenzene ug/L 20 101 70-139102 120ND20.2 20.4
1,2-Dibromo-3-chloropropane ug/L 20 95 69-136100 520ND19.0 19.9
1,2-Dibromoethane (EDB)ug/L 20 101 70-13798 220ND20.1 19.6
1,2-Dichlorobenzene ug/L 20 99 70-13399 020ND19.9 19.9
1,2-Dichloroethane ug/L 20 104 67-138101 220ND20.7 20.3
1,2-Dichloropropane ug/L 20 103 70-138101 120ND20.5 20.3
1,3-Dichlorobenzene ug/L 20 104 70-133102 220ND20.9 20.4
1,3-Dichloropropane ug/L 20 103 70-13699 420ND20.5 19.7
1,4-Dichlorobenzene ug/L 20 102 70-133102 020ND20.3 20.3
2,2-Dichloropropane ug/L 20 118 52-155113 420ND23.5 22.6
2-Butanone (MEK)ug/L 40 86 61-14787 140ND34.2 34.6
2-Chlorotoluene ug/L 20 107 70-141106 120ND21.4 21.2
2-Hexanone ug/L 40 93 67-13994 140ND37.4 37.7
4-Chlorotoluene ug/L 20 101 70-135100 120ND20.2 20.0
4-Methyl-2-pentanone (MIBK)ug/L 40 93 67-13695 240ND37.2 38.0
Acetone ug/L 40 92 55-15992 040ND36.6 36.6
Benzene ug/L 20 100 67-15098 220ND19.9 19.6
Bromobenzene ug/L 20 103 70-134102 120ND20.7 20.4
Bromochloromethane ug/L 20 117 70-146111 520ND23.5 22.3
Bromodichloromethane ug/L 20 101 70-138100 120ND20.2 20.0
Bromoform ug/L 20 100 57-138100 020ND20.1 20.1
Bromomethane ug/L 20 99 10-200100 120ND20.4 20.6
Carbon tetrachloride ug/L 20 105 70-147101 320ND21.0 20.3
Chlorobenzene ug/L 20 103 70-137101 220ND20.6 20.2
Chloroethane ug/L IK,IL2011851-166113 520ND23.6 22.5
Chloroform ug/L 20 100 70-14496 420ND20.1 19.2
Chloromethane ug/L 20 99 24-16196 320ND19.8 19.1
cis-1,2-Dichloroethene ug/L 20 107 67-148103 320ND21.3 20.6
cis-1,3-Dichloropropene ug/L 20 102 70-142100 220ND20.4 19.9
Dibromochloromethane ug/L 20 105 68-138102 320ND21.0 20.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3368214MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92556367009
3368215
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Dibromomethane ug/L 20 100 70-134100 020ND20.0 20.0
Dichlorodifluoromethane ug/L 20 85 43-15585 020ND17.1 17.0
Diisopropyl ether ug/L 20 101 65-14699 320ND20.3 19.7
Ethylbenzene ug/L 20 106 68-143102 420ND21.2 20.4
Hexachloro-1,3-butadiene ug/L 20 109 62-151103 620ND22.6 21.2
m&p-Xylene ug/L 40 106 53-157102 340ND42.4 41.0
Methyl-tert-butyl ether ug/L 20 100 59-15698 120ND19.9 19.7
Methylene Chloride ug/L 20 102 64-14899 320ND20.4 19.8
Naphthalene ug/L 20 93 57-15099 720ND18.5 19.9
o-Xylene ug/L 20 104 68-143101 320ND20.8 20.1
p-Isopropyltoluene ug/L 20 108 70-141106 220ND21.6 21.1
Styrene ug/L 20 104 70-136104 020ND20.9 20.8
Tetrachloroethene ug/L 20 103 70-139101 220ND20.7 20.2
Toluene ug/L 20 98 47-15796 220ND19.6 19.3
trans-1,2-Dichloroethene ug/L 20 113 70-149109 320ND22.6 21.8
trans-1,3-Dichloropropene ug/L 20 102 70-138100 220ND20.5 20.0
Trichloroethene ug/L 20 102 70-14999 320ND20.4 19.8
Trichlorofluoromethane ug/L 20 106 61-154101 520ND21.2 20.2
Vinyl acetate ug/L 40 112 48-156110 240ND44.6 43.9
Vinyl chloride ug/L 20 104 55-172102 220ND20.7 20.4
Xylene (Total)ug/L 60 105 66-145102 360ND63.2 61.1
1,2-Dichloroethane-d4 (S)%104 70-130103
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
641867
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92556378001, 92556378002, 92556378003, 92556378004, 92556378005, 92556378006, 92556378007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3368622
Associated Lab Samples:92556378001, 92556378002, 92556378003, 92556378004, 92556378005, 92556378006, 92556378007
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 08/24/21 11:31
1,2-Dichlorobenzene ug/L ND 10.0 08/24/21 11:31
1,3-Dichlorobenzene ug/L ND 10.0 08/24/21 11:31
1,4-Dichlorobenzene ug/L ND 10.0 08/24/21 11:31
1-Methylnaphthalene ug/L ND 10.0 08/24/21 11:31
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 08/24/21 11:31
2,4,5-Trichlorophenol ug/L ND 10.0 08/24/21 11:31
2,4,6-Trichlorophenol ug/L ND 10.0 08/24/21 11:31
2,4-Dichlorophenol ug/L ND 10.0 08/24/21 11:31
2,4-Dimethylphenol ug/L ND 10.0 08/24/21 11:31
2,4-Dinitrophenol ug/L ND 50.0 08/24/21 11:31
2,4-Dinitrotoluene ug/L ND 10.0 08/24/21 11:31
2,6-Dinitrotoluene ug/L ND 10.0 08/24/21 11:31
2-Chloronaphthalene ug/L ND 10.0 08/24/21 11:31
2-Chlorophenol ug/L ND 10.0 08/24/21 11:31
2-Methylnaphthalene ug/L ND 10.0 08/24/21 11:31
2-Methylphenol(o-Cresol)ug/L ND 10.0 08/24/21 11:31
2-Nitroaniline ug/L ND 20.0 08/24/21 11:31
2-Nitrophenol ug/L ND 10.0 08/24/21 11:31
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 08/24/21 11:31
3,3'-Dichlorobenzidine ug/L ND 20.0 08/24/21 11:31
3-Nitroaniline ug/L ND 20.0 08/24/21 11:31
4,6-Dinitro-2-methylphenol ug/L ND 20.0 08/24/21 11:31
4-Bromophenylphenyl ether ug/L ND 10.0 08/24/21 11:31
4-Chloro-3-methylphenol ug/L ND 10.0 08/24/21 11:31
4-Chloroaniline ug/L ND 20.0 08/24/21 11:31
4-Chlorophenylphenyl ether ug/L ND 10.0 08/24/21 11:31
4-Nitroaniline ug/L ND 20.0 08/24/21 11:31
4-Nitrophenol ug/L ND 50.0 08/24/21 11:31
Acenaphthene ug/L ND 10.0 08/24/21 11:31
Acenaphthylene ug/L ND 10.0 08/24/21 11:31
Aniline ug/L ND 10.0 08/24/21 11:31
Anthracene ug/L ND 10.0 08/24/21 11:31
Benzo(a)anthracene ug/L ND 10.0 08/24/21 11:31
Benzo(a)pyrene ug/L ND 10.0 08/24/21 11:31
Benzo(b)fluoranthene ug/L ND 10.0 08/24/21 11:31
Benzo(g,h,i)perylene ug/L ND 10.0 08/24/21 11:31
Benzo(k)fluoranthene ug/L ND 10.0 08/24/21 11:31
Benzoic Acid ug/L ND 50.0 08/24/21 11:31
Benzyl alcohol ug/L ND 20.0 08/24/21 11:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3368622
Associated Lab Samples:92556378001, 92556378002, 92556378003, 92556378004, 92556378005, 92556378006, 92556378007
Matrix:Water
Analyzed
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/24/21 11:31
bis(2-Chloroethyl) ether ug/L ND 10.0 08/24/21 11:31
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 08/24/21 11:31
Butylbenzylphthalate ug/L ND 10.0 08/24/21 11:31
Chrysene ug/L ND 10.0 08/24/21 11:31
Di-n-butylphthalate ug/L ND 10.0 08/24/21 11:31
Di-n-octylphthalate ug/L ND 10.0 08/24/21 11:31
Dibenz(a,h)anthracene ug/L ND 10.0 08/24/21 11:31
Dibenzofuran ug/L ND 10.0 08/24/21 11:31
Diethylphthalate ug/L ND 10.0 08/24/21 11:31
Dimethylphthalate ug/L ND 10.0 08/24/21 11:31
Fluoranthene ug/L ND 10.0 08/24/21 11:31
Fluorene ug/L ND 10.0 08/24/21 11:31
Hexachloro-1,3-butadiene ug/L ND 10.0 08/24/21 11:31
Hexachlorobenzene ug/L ND 10.0 08/24/21 11:31
Hexachlorocyclopentadiene ug/L ND 10.0 08/24/21 11:31
Hexachloroethane ug/L ND 10.0 08/24/21 11:31
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/24/21 11:31
Isophorone ug/L ND 10.0 08/24/21 11:31
N-Nitroso-di-n-propylamine ug/L ND 10.0 08/24/21 11:31
N-Nitrosodimethylamine ug/L ND 10.0 08/24/21 11:31
N-Nitrosodiphenylamine ug/L ND 10.0 08/24/21 11:31
Naphthalene ug/L ND 10.0 08/24/21 11:31
Nitrobenzene ug/L ND 10.0 08/24/21 11:31
Pentachlorophenol ug/L ND 20.0 08/24/21 11:31
Phenanthrene ug/L ND 10.0 08/24/21 11:31
Phenol ug/L ND 10.0 08/24/21 11:31
Pyrene ug/L ND 10.0 08/24/21 11:31
2,4,6-Tribromophenol (S)%89 10-144 08/24/21 11:31
2-Fluorobiphenyl (S)%60 10-130 08/24/21 11:31
2-Fluorophenol (S)%57 10-130 08/24/21 11:31
Nitrobenzene-d5 (S)%83 10-144 08/24/21 11:31
Phenol-d6 (S)%45 10-130 08/24/21 11:31
Terphenyl-d14 (S)%114 34-163 08/24/21 11:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3368623LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 19.750 39 18-130
1,2-Dichlorobenzene ug/L 15.850 32 20-130
1,3-Dichlorobenzene ug/L 13.850 28 18-130
1,4-Dichlorobenzene ug/L 14.950 30 18-130
1-Methylnaphthalene ug/L 31.550 63 29-130
2,2'-Oxybis(1-chloropropane)ug/L 31.850 64 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3368623LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 46.150 92 35-130
2,4,6-Trichlorophenol ug/L 45.850 92 31-130
2,4-Dichlorophenol ug/L 42.950 86 35-130
2,4-Dimethylphenol ug/L 43.450 87 34-130
2,4-Dinitrophenol ug/L 189250 76 10-153
2,4-Dinitrotoluene ug/L 47.350 95 37-136
2,6-Dinitrotoluene ug/L 48.250 96 33-136
2-Chloronaphthalene ug/L 35.350 71 26-130
2-Chlorophenol ug/L 37.850 76 37-130
2-Methylnaphthalene ug/L 28.850 58 29-130
2-Methylphenol(o-Cresol)ug/L 37.750 75 35-130
2-Nitroaniline ug/L 87.7100 88 37-130
2-Nitrophenol ug/L 41.650 83 32-130
3&4-Methylphenol(m&p Cresol)ug/L 34.350 69 34-130
3,3'-Dichlorobenzidine ug/L 91.2100 91 34-136
3-Nitroaniline ug/L 88.6100 89 37-138
4,6-Dinitro-2-methylphenol ug/L 83.5100 84 21-157
4-Bromophenylphenyl ether ug/L 44.350 89 38-130
4-Chloro-3-methylphenol ug/L 87.9100 88 37-130
4-Chloroaniline ug/L 79.3100 79 38-130
4-Chlorophenylphenyl ether ug/L 41.950 84 33-130
4-Nitroaniline ug/L 84.2100 84 42-137
4-Nitrophenol ug/L 130250 52 10-130
Acenaphthene ug/L 41.450 83 33-130
Acenaphthylene ug/L 43.050 86 35-130
Aniline ug/L 33.450 67 22-130
Anthracene ug/L 47.750 95 48-130
Benzo(a)anthracene ug/L 46.450 93 48-137
Benzo(a)pyrene ug/L 50.850 102 49-138
Benzo(b)fluoranthene ug/L 49.950 100 52-138
Benzo(g,h,i)perylene ug/L 42.050 84 48-140
Benzo(k)fluoranthene ug/L 50.950 102 48-139
Benzoic Acid ug/L 116250 46 10-130
Benzyl alcohol ug/L 81.3100 81 35-130
bis(2-Chloroethoxy)methane ug/L 41.750 83 34-130
bis(2-Chloroethyl) ether ug/L 42.550 85 36-130
bis(2-Ethylhexyl)phthalate ug/L 50.850 102 32-165
Butylbenzylphthalate ug/L 50.450 101 34-161
Chrysene ug/L 47.050 94 47-131
Di-n-butylphthalate ug/L 52.450 105 39-144
Di-n-octylphthalate ug/L 48.850 98 30-170
Dibenz(a,h)anthracene ug/L 42.850 86 49-138
Dibenzofuran ug/L 41.250 82 33-130
Diethylphthalate ug/L 45.750 91 38-131
Dimethylphthalate ug/L 45.250 90 37-130
Fluoranthene ug/L 49.750 99 46-137
Fluorene ug/L 44.150 88 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3368623LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 13.450 27 11-130
Hexachlorobenzene ug/L 40.550 81 38-130
Hexachlorocyclopentadiene ug/L 18.450 37 10-130
Hexachloroethane ug/L 11.450 23 14-130
Indeno(1,2,3-cd)pyrene ug/L 44.850 90 41-130
Isophorone ug/L 46.250 92 33-130
N-Nitroso-di-n-propylamine ug/L 42.550 85 36-130
N-Nitrosodimethylamine ug/L 37.450 75 34-130
N-Nitrosodiphenylamine ug/L 45.050 90 37-130
Naphthalene ug/L 28.150 56 30-130
Nitrobenzene ug/L 41.150 82 36-130
Pentachlorophenol ug/L 83.5100 84 23-149
Phenanthrene ug/L 46.250 92 44-130
Phenol ug/L 22.350 45 18-130
Pyrene ug/L 46.550 93 47-134
2,4,6-Tribromophenol (S)%110 10-144
2-Fluorobiphenyl (S)%89 10-130
2-Fluorophenol (S)%63 10-130
Nitrobenzene-d5 (S)%95 10-144
Phenol-d6 (S)%52 10-130
Terphenyl-d14 (S)%100 34-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
642143
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92556378008, 92556378009, 92556378010, 92556378011
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3370202
Associated Lab Samples:92556378008, 92556378009, 92556378010, 92556378011
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 10.0 08/24/21 18:14
1,2-Dichlorobenzene ug/L ND 10.0 08/24/21 18:14
1,3-Dichlorobenzene ug/L ND 10.0 08/24/21 18:14
1,4-Dichlorobenzene ug/L ND 10.0 08/24/21 18:14
1-Methylnaphthalene ug/L ND 10.0 08/24/21 18:14
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 08/24/21 18:14
2,4,5-Trichlorophenol ug/L ND 10.0 08/24/21 18:14
2,4,6-Trichlorophenol ug/L ND 10.0 08/24/21 18:14
2,4-Dichlorophenol ug/L ND 10.0 08/24/21 18:14
2,4-Dimethylphenol ug/L ND 10.0 08/24/21 18:14
2,4-Dinitrophenol ug/L ND 50.0 08/24/21 18:14
2,4-Dinitrotoluene ug/L ND 10.0 08/24/21 18:14
2,6-Dinitrotoluene ug/L ND 10.0 08/24/21 18:14
2-Chloronaphthalene ug/L ND 10.0 08/24/21 18:14
2-Chlorophenol ug/L ND 10.0 08/24/21 18:14
2-Methylnaphthalene ug/L ND 10.0 08/24/21 18:14
2-Methylphenol(o-Cresol)ug/L ND 10.0 08/24/21 18:14
2-Nitroaniline ug/L ND 20.0 08/24/21 18:14
2-Nitrophenol ug/L ND 10.0 08/24/21 18:14
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 08/24/21 18:14
3,3'-Dichlorobenzidine ug/L ND 20.0 08/24/21 18:14
3-Nitroaniline ug/L ND 20.0 08/24/21 18:14
4,6-Dinitro-2-methylphenol ug/L ND 20.0 08/24/21 18:14
4-Bromophenylphenyl ether ug/L ND 10.0 08/24/21 18:14
4-Chloro-3-methylphenol ug/L ND 10.0 08/24/21 18:14
4-Chloroaniline ug/L ND 20.0 08/24/21 18:14
4-Chlorophenylphenyl ether ug/L ND 10.0 08/24/21 18:14
4-Nitroaniline ug/L ND 20.0 08/24/21 18:14
4-Nitrophenol ug/L ND 50.0 08/24/21 18:14
Acenaphthene ug/L ND 10.0 08/24/21 18:14
Acenaphthylene ug/L ND 10.0 08/24/21 18:14
Aniline ug/L ND 10.0 08/24/21 18:14
Anthracene ug/L ND 10.0 08/24/21 18:14
Benzo(a)anthracene ug/L ND 10.0 08/24/21 18:14
Benzo(a)pyrene ug/L ND 10.0 08/24/21 18:14
Benzo(b)fluoranthene ug/L ND 10.0 08/24/21 18:14
Benzo(g,h,i)perylene ug/L ND 10.0 08/24/21 18:14
Benzo(k)fluoranthene ug/L ND 10.0 08/24/21 18:14
Benzoic Acid ug/L ND 50.0 08/24/21 18:14
Benzyl alcohol ug/L ND 20.0 08/24/21 18:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3370202
Associated Lab Samples:92556378008, 92556378009, 92556378010, 92556378011
Matrix:Water
Analyzed
bis(2-Chloroethoxy)methane ug/L ND 10.0 08/24/21 18:14
bis(2-Chloroethyl) ether ug/L ND 10.0 08/24/21 18:14
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 08/24/21 18:14
Butylbenzylphthalate ug/L ND 10.0 08/24/21 18:14
Chrysene ug/L ND 10.0 08/24/21 18:14
Di-n-butylphthalate ug/L ND 10.0 08/24/21 18:14
Di-n-octylphthalate ug/L ND 10.0 08/24/21 18:14
Dibenz(a,h)anthracene ug/L ND 10.0 08/24/21 18:14
Dibenzofuran ug/L ND 10.0 08/24/21 18:14
Diethylphthalate ug/L ND 10.0 08/24/21 18:14
Dimethylphthalate ug/L ND 10.0 08/24/21 18:14
Fluoranthene ug/L ND 10.0 08/24/21 18:14
Fluorene ug/L ND 10.0 08/24/21 18:14
Hexachloro-1,3-butadiene ug/L ND 10.0 08/24/21 18:14
Hexachlorobenzene ug/L ND 10.0 08/24/21 18:14
Hexachlorocyclopentadiene ug/L ND 10.0 08/24/21 18:14
Hexachloroethane ug/L ND 10.0 08/24/21 18:14
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/24/21 18:14
Isophorone ug/L ND 10.0 08/24/21 18:14
N-Nitroso-di-n-propylamine ug/L ND 10.0 08/24/21 18:14
N-Nitrosodimethylamine ug/L ND 10.0 08/24/21 18:14
N-Nitrosodiphenylamine ug/L ND 10.0 08/24/21 18:14
Naphthalene ug/L ND 10.0 08/24/21 18:14
Nitrobenzene ug/L ND 10.0 08/24/21 18:14
Pentachlorophenol ug/L ND 20.0 08/24/21 18:14
Phenanthrene ug/L ND 10.0 08/24/21 18:14
Phenol ug/L ND 10.0 08/24/21 18:14
Pyrene ug/L ND 10.0 08/24/21 18:14
2,4,6-Tribromophenol (S)%94 10-144 08/24/21 18:14
2-Fluorobiphenyl (S)%81 10-130 08/24/21 18:14
2-Fluorophenol (S)%64 10-130 08/24/21 18:14
Nitrobenzene-d5 (S)%97 10-144 08/24/21 18:14
Phenol-d6 (S)%45 10-130 08/24/21 18:14
Terphenyl-d14 (S)%104 34-163 08/24/21 18:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3370203LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 20.750 41 18-130
1,2-Dichlorobenzene ug/L 20.150 40 20-130
1,3-Dichlorobenzene ug/L 18.950 38 18-130
1,4-Dichlorobenzene ug/L 19.350 39 18-130
1-Methylnaphthalene ug/L 29.550 59 29-130
2,2'-Oxybis(1-chloropropane)ug/L 34.350 69 28-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3370203LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 45.550 91 35-130
2,4,6-Trichlorophenol ug/L 44.550 89 31-130
2,4-Dichlorophenol ug/L 43.850 88 35-130
2,4-Dimethylphenol ug/L 45.350 91 34-130
2,4-Dinitrophenol ug/L 192250 77 10-153
2,4-Dinitrotoluene ug/L 50.250 100 37-136
2,6-Dinitrotoluene ug/L 49.350 99 33-136
2-Chloronaphthalene ug/L 33.650 67 26-130
2-Chlorophenol ug/L 40.650 81 37-130
2-Methylnaphthalene ug/L 28.150 56 29-130
2-Methylphenol(o-Cresol)ug/L 39.350 79 35-130
2-Nitroaniline ug/L 87.7100 88 37-130
2-Nitrophenol ug/L 41.750 83 32-130
3&4-Methylphenol(m&p Cresol)ug/L 37.050 74 34-130
3,3'-Dichlorobenzidine ug/L 92.0100 92 34-136
3-Nitroaniline ug/L 94.2100 94 37-138
4,6-Dinitro-2-methylphenol ug/L 91.1100 91 21-157
4-Bromophenylphenyl ether ug/L 45.850 92 38-130
4-Chloro-3-methylphenol ug/L 89.9100 90 37-130
4-Chloroaniline ug/L 84.1100 84 38-130
4-Chlorophenylphenyl ether ug/L 41.650 83 33-130
4-Nitroaniline ug/L 94.9100 95 42-137
4-Nitrophenol ug/L 127250 51 10-130
Acenaphthene ug/L 40.250 80 33-130
Acenaphthylene ug/L 41.450 83 35-130
Aniline ug/L 34.350 69 22-130
Anthracene ug/L 47.450 95 48-130
Benzo(a)anthracene ug/L 47.050 94 48-137
Benzo(a)pyrene ug/L 50.550 101 49-138
Benzo(b)fluoranthene ug/L 48.550 97 52-138
Benzo(g,h,i)perylene ug/L 44.550 89 48-140
Benzo(k)fluoranthene ug/L 51.250 102 48-139
Benzoic Acid ug/L 60.5250 24 10-130
Benzyl alcohol ug/L 85.8100 86 35-130
bis(2-Chloroethoxy)methane ug/L 42.750 85 34-130
bis(2-Chloroethyl) ether ug/L 47.350 95 36-130
bis(2-Ethylhexyl)phthalate ug/L 50.950 102 32-165
Butylbenzylphthalate ug/L 52.250 104 34-161
Chrysene ug/L 46.850 94 47-131
Di-n-butylphthalate ug/L 50.950 102 39-144
Di-n-octylphthalate ug/L 50.750 101 30-170
Dibenz(a,h)anthracene ug/L 45.850 92 49-138
Dibenzofuran ug/L 41.750 83 33-130
Diethylphthalate ug/L 46.350 93 38-131
Dimethylphthalate ug/L 44.850 90 37-130
Fluoranthene ug/L 49.650 99 46-137
Fluorene ug/L 44.150 88 37-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3370203LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 17.850 36 11-130
Hexachlorobenzene ug/L 42.150 84 38-130
Hexachlorocyclopentadiene ug/L 18.150 36 10-130
Hexachloroethane ug/L 18.050 36 14-130
Indeno(1,2,3-cd)pyrene ug/L 45.950 92 41-130
Isophorone ug/L 47.050 94 33-130
N-Nitroso-di-n-propylamine ug/L 46.050 92 36-130
N-Nitrosodimethylamine ug/L 39.250 78 34-130
N-Nitrosodiphenylamine ug/L 45.950 92 37-130
Naphthalene ug/L 26.850 54 30-130
Nitrobenzene ug/L 42.050 84 36-130
Pentachlorophenol ug/L 87.1100 87 23-149
Phenanthrene ug/L 46.650 93 44-130
Phenol ug/L 20.850 42 18-130
Pyrene ug/L 47.150 94 47-134
2,4,6-Tribromophenol (S)%108 10-144
2-Fluorobiphenyl (S)%97 10-130
2-Fluorophenol (S)%69 10-130
Nitrobenzene-d5 (S)%99 10-144
Phenol-d6 (S)%54 10-130
Terphenyl-d14 (S)%103 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3370204MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92550821005
3370205
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L R1502510-13039 4450ND12.6 19.7
1,2-Dichlorobenzene ug/L R1502710-13041 4150ND13.7 20.7
1,3-Dichlorobenzene ug/L R1502510-13036 3650ND12.4 17.8
1,4-Dichlorobenzene ug/L R1502710-13038 3650ND13.3 19.0
1-Methylnaphthalene ug/L R1504110-13056 3250ND20.4 28.2
2,2'-Oxybis(1-chloropropane)ug/L R1504012-14256 3350ND19.9 27.9
2,4,5-Trichlorophenol ug/L R1503410-14355 4750ND17.1 27.6
2,4,6-Trichlorophenol ug/L 50 17 10-1473250ND8.6J 15.9
2,4-Dichlorophenol ug/L R1503310-13855 4950ND16.6 27.4
2,4-Dimethylphenol ug/L R1504125-13062 4150ND20.3 30.9
2,4-Dinitrophenol ug/L M1250010-1650250NDNDND
2,4-Dinitrotoluene ug/L R1504729-14869 3950ND23.5 34.7
2,6-Dinitrotoluene ug/L R1504726-14670 3950ND23.6 34.9
2-Chloronaphthalene ug/L R1503711-13058 4550ND18.5 29.2
2-Chlorophenol ug/L R1503710-13352 3550ND18.3 26.0
2-Methylnaphthalene ug/L R1503813-13054 3550ND18.9 26.9
2-Methylphenol(o-Cresol)ug/L R1504220-13060 3650ND20.8 30.0
2-Nitroaniline ug/L R11003824-13658 42100ND37.8 57.6
2-Nitrophenol ug/L R1503910-15358 3950ND19.4 28.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3370204MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92550821005
3370205
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
3&4-Methylphenol(m&p
Cresol)ug/L R1503716-13053 3450ND18.6 26.3
3,3'-Dichlorobenzidine ug/L R11002310-15335 42100ND23.2 35.4
3-Nitroaniline ug/L R11002722-15144 46100ND27.3 43.8
4,6-Dinitro-2-methylphenol ug/L M1100010-18010100NDND10.4J
4-Bromophenylphenyl ether ug/L R1504925-13067 3250ND24.3 33.5
4-Chloro-3-methylphenol ug/L 100 54 25-13373 29100ND54.4 73.1
4-Chloroaniline ug/L R11003414-13247 33100ND33.6 46.8
4-Chlorophenylphenyl ether ug/L R1504119-13060 3750ND20.7 30.1
4-Nitroaniline ug/L M11001829-15039100ND18.4J 38.6
4-Nitrophenol ug/L M1250010-1300250NDNDND
Acenaphthene ug/L R1504316-13065 4150ND21.5 32.5
Acenaphthylene ug/L R1504015-13761 4250ND19.9 30.6
Aniline ug/L 50 36 10-13047 2850ND17.9 23.7
Anthracene ug/L 50 57 37-13676 2950ND28.4 38.1
Benzo(a)anthracene ug/L R1506140-14589 3650ND30.7 44.3
Benzo(a)pyrene ug/L R1506641-14692 3450ND32.9 46.2
Benzo(b)fluoranthene ug/L R1506339-15193 3850ND31.5 46.4
Benzo(g,h,i)perylene ug/L R1506240-14788 3550ND30.9 44.2
Benzo(k)fluoranthene ug/L R1506340-14694 3950ND31.4 46.8
Benzoic Acid ug/L M1250010-1300250NDNDND
Benzyl alcohol ug/L R11004625-13063 32100ND45.7 63.1
bis(2-Chloroethoxy)methane ug/L R1504523-13062 3350ND22.3 31.0
bis(2-Chloroethyl) ether ug/L 50 53 25-13070 2750ND26.7 35.0
bis(2-Ethylhexyl)phthalate ug/L R1506528-16694 3750ND32.4 47.2
Butylbenzylphthalate ug/L R1507033-165105 4050ND35.0 52.7
Chrysene ug/L R1506238-14188 3550ND30.9 43.9
Di-n-butylphthalate ug/L R1506732-15396 3750ND33.3 48.1
Di-n-octylphthalate ug/L R1506730-17597 3850ND33.3 48.7
Dibenz(a,h)anthracene ug/L R1505939-14888 4050ND29.4 44.2
Dibenzofuran ug/L R1504220-13064 4250ND20.8 31.8
Diethylphthalate ug/L R1504828-14271 3850ND24.1 35.3
Dimethylphthalate ug/L R1504326-13665 3950ND21.7 32.3
Fluoranthene ug/L R1506539-14393 3550ND32.7 46.3
Fluorene ug/L R1504424-13267 4150ND22.0 33.5
Hexachloro-1,3-butadiene ug/L R1502010-13033 4750ND10.2 16.5
Hexachlorobenzene ug/L R1504429-13061 3350ND21.8 30.6
Hexachlorocyclopentadiene ug/L 50 19 10-1303650ND9.7J 18.2
Hexachloroethane ug/L R1502210-13033 4250ND10.9 16.7
Indeno(1,2,3-cd)pyrene ug/L R1506339-14893 3950ND31.3 46.6
Isophorone ug/L 50 51 23-13069 3050ND25.7 34.7
N-Nitroso-di-n-propylamine ug/L 50 52 25-13070 2950ND26.1 35.1
N-Nitrosodimethylamine ug/L 50 46 22-13059 2550ND23.0 29.7
N-Nitrosodiphenylamine ug/L R1504426-13461 3250ND22.1 30.7
Naphthalene ug/L R1503414-13051 3850ND17.2 25.3
Nitrobenzene ug/L 50 54 25-13072 2950ND26.9 35.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3370204MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92550821005
3370205
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Pentachlorophenol ug/L M1100310-1758100NDND8.3J
Phenanthrene ug/L R1505636-13377 3250ND28.0 38.6
Phenol ug/L R1502310-13035 4050ND11.5 17.3
Pyrene ug/L R1506440-14387 3150ND31.9 43.6
2,4,6-Tribromophenol (S)%36 10-14463
2-Fluorobiphenyl (S)%41 10-13064
2-Fluorophenol (S)%22 10-13034
Nitrobenzene-d5 (S)%50 10-14469
Phenol-d6 (S)%27 10-13038
Terphenyl-d14 (S)%64 34-16392
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
642890
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92556378012, 92556378013, 92556378014, 92556378015, 92556378016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3373554
Associated Lab Samples:92556378012, 92556378013, 92556378014, 92556378015, 92556378016
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 08/26/21 06:30
1,2-Dichlorobenzene mg/kg ND 0.33 08/26/21 06:30
1,3-Dichlorobenzene mg/kg ND 0.33 08/26/21 06:30
1,4-Dichlorobenzene mg/kg ND 0.33 08/26/21 06:30
1-Methylnaphthalene mg/kg ND 0.33 08/26/21 06:30
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 08/26/21 06:30
2,4,5-Trichlorophenol mg/kg ND 0.33 08/26/21 06:30
2,4,6-Trichlorophenol mg/kg ND 0.33 08/26/21 06:30
2,4-Dichlorophenol mg/kg ND 0.33 08/26/21 06:30
2,4-Dimethylphenol mg/kg ND 0.33 08/26/21 06:30
2,4-Dinitrophenol mg/kg ND 1.6 v108/26/21 06:30
2,4-Dinitrotoluene mg/kg ND 0.33 08/26/21 06:30
2,6-Dinitrotoluene mg/kg ND 0.33 08/26/21 06:30
2-Chloronaphthalene mg/kg ND 0.33 08/26/21 06:30
2-Chlorophenol mg/kg ND 0.33 08/26/21 06:30
2-Methylnaphthalene mg/kg ND 0.33 08/26/21 06:30
2-Methylphenol(o-Cresol)mg/kg ND 0.33 08/26/21 06:30
2-Nitroaniline mg/kg ND 1.6 08/26/21 06:30
2-Nitrophenol mg/kg ND 0.33 08/26/21 06:30
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 08/26/21 06:30
3,3'-Dichlorobenzidine mg/kg ND 0.65 IL08/26/21 06:30
3-Nitroaniline mg/kg ND 1.6 IL08/26/21 06:30
4,6-Dinitro-2-methylphenol mg/kg ND 0.65 v108/26/21 06:30
4-Bromophenylphenyl ether mg/kg ND 0.33 08/26/21 06:30
4-Chloro-3-methylphenol mg/kg ND 0.65 08/26/21 06:30
4-Chloroaniline mg/kg ND 0.65 08/26/21 06:30
4-Chlorophenylphenyl ether mg/kg ND 0.33 08/26/21 06:30
4-Nitroaniline mg/kg ND 0.65 08/26/21 06:30
4-Nitrophenol mg/kg ND 1.6 08/26/21 06:30
Acenaphthene mg/kg ND 0.33 08/26/21 06:30
Acenaphthylene mg/kg ND 0.33 08/26/21 06:30
Aniline mg/kg ND 0.33 08/26/21 06:30
Anthracene mg/kg ND 0.33 08/26/21 06:30
Benzo(a)anthracene mg/kg ND 0.33 08/26/21 06:30
Benzo(a)pyrene mg/kg ND 0.33 08/26/21 06:30
Benzo(b)fluoranthene mg/kg ND 0.33 08/26/21 06:30
Benzo(g,h,i)perylene mg/kg ND 0.33 08/26/21 06:30
Benzo(k)fluoranthene mg/kg ND 0.33 08/26/21 06:30
Benzoic Acid mg/kg ND 1.6 08/26/21 06:30
Benzyl alcohol mg/kg ND 0.65 08/26/21 06:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3373554
Associated Lab Samples:92556378012, 92556378013, 92556378014, 92556378015, 92556378016
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 08/26/21 06:30
bis(2-Chloroethyl) ether mg/kg ND 0.33 08/26/21 06:30
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 08/26/21 06:30
Butylbenzylphthalate mg/kg ND 0.33 08/26/21 06:30
Chrysene mg/kg ND 0.33 08/26/21 06:30
Di-n-butylphthalate mg/kg ND 0.33 08/26/21 06:30
Di-n-octylphthalate mg/kg ND 0.33 08/26/21 06:30
Dibenz(a,h)anthracene mg/kg ND 0.33 08/26/21 06:30
Dibenzofuran mg/kg ND 0.33 08/26/21 06:30
Diethylphthalate mg/kg ND 0.33 08/26/21 06:30
Dimethylphthalate mg/kg ND 0.33 08/26/21 06:30
Fluoranthene mg/kg ND 0.33 08/26/21 06:30
Fluorene mg/kg ND 0.33 08/26/21 06:30
Hexachloro-1,3-butadiene mg/kg ND 0.33 08/26/21 06:30
Hexachlorobenzene mg/kg ND 0.33 08/26/21 06:30
Hexachlorocyclopentadiene mg/kg ND 0.33 08/26/21 06:30
Hexachloroethane mg/kg ND 0.33 08/26/21 06:30
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 08/26/21 06:30
Isophorone mg/kg ND 0.33 08/26/21 06:30
N-Nitroso-di-n-propylamine mg/kg ND 0.33 08/26/21 06:30
N-Nitrosodimethylamine mg/kg ND 0.33 v108/26/21 06:30
N-Nitrosodiphenylamine mg/kg ND 0.33 08/26/21 06:30
Naphthalene mg/kg ND 0.33 08/26/21 06:30
Nitrobenzene mg/kg ND 0.33 08/26/21 06:30
Pentachlorophenol mg/kg ND 0.65 08/26/21 06:30
Phenanthrene mg/kg ND 0.33 08/26/21 06:30
Phenol mg/kg ND 0.33 v108/26/21 06:30
Pyrene mg/kg ND 0.33 08/26/21 06:30
Pyridine mg/kg ND 0.33 v108/26/21 06:30
2,4,6-Tribromophenol (S)%74 18-130 08/26/21 06:30
2-Fluorobiphenyl (S)%70 19-130 08/26/21 06:30
2-Fluorophenol (S)%75 18-130 08/26/21 06:30
Nitrobenzene-d5 (S)%79 21-130 08/26/21 06:30
Phenol-d6 (S)%78 18-130 08/26/21 06:30
Terphenyl-d14 (S)%86 15-130 08/26/21 06:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3373555LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.7 74 47-130
1,2-Dichlorobenzene mg/kg 1.21.7 73 49-130
1,3-Dichlorobenzene mg/kg 1.31.7 75 48-130
1,4-Dichlorobenzene mg/kg 1.31.7 76 49-130
1-Methylnaphthalene mg/kg 1.31.7 75 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3373555LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.31.7 80 38-130
2,4,5-Trichlorophenol mg/kg 1.41.7 82 49-130
2,4,6-Trichlorophenol mg/kg 1.41.7 83 50-130
2,4-Dichlorophenol mg/kg 1.31.7 77 51-130
2,4-Dimethylphenol mg/kg 1.41.7 85 53-130
2,4-Dinitrophenol mg/kg 7.7 v18.4 91 39-130
2,4-Dinitrotoluene mg/kg 1.41.7 83 53-130
2,6-Dinitrotoluene mg/kg 1.41.7 86 55-130
2-Chloronaphthalene mg/kg 1.31.7 79 48-130
2-Chlorophenol mg/kg 1.41.7 83 54-130
2-Methylnaphthalene mg/kg 1.31.7 76 57-130
2-Methylphenol(o-Cresol)mg/kg 1.41.7 85 50-130
2-Nitroaniline mg/kg 2.93.3 86 49-130
2-Nitrophenol mg/kg 1.51.7 87 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.31.7 79 50-130
3,3'-Dichlorobenzidine mg/kg 2.6 IL3.3 79 47-130
3-Nitroaniline mg/kg 2.7 IL3.3 81 45-130
4,6-Dinitro-2-methylphenol mg/kg 3.6 v13.3 108 50-142
4-Bromophenylphenyl ether mg/kg 1.41.7 81 55-130
4-Chloro-3-methylphenol mg/kg 2.73.3 82 52-130
4-Chloroaniline mg/kg 2.43.3 73 49-130
4-Chlorophenylphenyl ether mg/kg 1.31.7 77 53-130
4-Nitroaniline mg/kg 2.73.3 80 51-130
4-Nitrophenol mg/kg 7.38.4 88 40-130
Acenaphthene mg/kg 1.41.7 81 56-130
Acenaphthylene mg/kg 1.41.7 83 58-130
Aniline mg/kg 1.41.7 84 44-130
Anthracene mg/kg 1.41.7 84 60-130
Benzo(a)anthracene mg/kg 1.51.7 88 59-130
Benzo(a)pyrene mg/kg 1.61.7 94 57-130
Benzo(b)fluoranthene mg/kg 1.61.7 93 54-130
Benzo(g,h,i)perylene mg/kg 1.61.7 97 59-130
Benzo(k)fluoranthene mg/kg 1.61.7 94 54-130
Benzoic Acid mg/kg 5.68.4 67 19-130
Benzyl alcohol mg/kg 2.73.3 81 50-130
bis(2-Chloroethoxy)methane mg/kg 1.41.7 85 55-130
bis(2-Chloroethyl) ether mg/kg 1.61.7 95 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.41.7 84 58-130
Butylbenzylphthalate mg/kg 1.61.7 93 46-138
Chrysene mg/kg 1.41.7 83 57-130
Di-n-butylphthalate mg/kg 1.41.7 86 57-130
Di-n-octylphthalate mg/kg 1.61.7 93 57-130
Dibenz(a,h)anthracene mg/kg 1.61.7 98 60-130
Dibenzofuran mg/kg 1.31.7 79 54-130
Diethylphthalate mg/kg 1.41.7 84 55-130
Dimethylphthalate mg/kg 1.41.7 82 57-130
Fluoranthene mg/kg 1.51.7 87 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3373555LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.31.7 78 56-130
Hexachloro-1,3-butadiene mg/kg 1.21.7 74 41-130
Hexachlorobenzene mg/kg 1.41.7 81 53-130
Hexachlorocyclopentadiene mg/kg 0.951.7 57 23-130
Hexachloroethane mg/kg 1.41.7 82 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.71.7 100 61-130
Isophorone mg/kg 1.51.7 87 49-130
N-Nitroso-di-n-propylamine mg/kg 1.41.7 83 52-130
N-Nitrosodimethylamine mg/kg 1.6 v11.7 99 45-130
N-Nitrosodiphenylamine mg/kg 1.41.7 84 56-130
Naphthalene mg/kg 1.31.7 79 56-130
Nitrobenzene mg/kg 1.51.7 87 50-130
Pentachlorophenol mg/kg 2.53.3 74 33-130
Phenanthrene mg/kg 1.41.7 84 60-130
Phenol mg/kg 1.6 v11.7 93 54-130
Pyrene mg/kg 1.41.7 86 61-130
Pyridine mg/kg 1.3 v11.7 77 35-130
2,4,6-Tribromophenol (S)%91 18-130
2-Fluorobiphenyl (S)%81 19-130
2-Fluorophenol (S)%90 18-130
Nitrobenzene-d5 (S)%90 21-130
Phenol-d6 (S)%90 18-130
Terphenyl-d14 (S)%88 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3373556MATRIX SPIKE SAMPLE:
MSSpike
Result
92556387001
1,2,4-Trichlorobenzene mg/kg 1.01.9 51 22-130ND
1,2-Dichlorobenzene mg/kg 1.11.9 54 23-130ND
1,3-Dichlorobenzene mg/kg 1.11.9 55 26-130ND
1,4-Dichlorobenzene mg/kg 1.11.9 56 27-130ND
1-Methylnaphthalene mg/kg 1.01.9 51 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.21.9 60 30-130ND
2,4,5-Trichlorophenol mg/kg 1.21.9 60 26-130ND
2,4,6-Trichlorophenol mg/kg 1.21.9 61 23-130ND
2,4-Dichlorophenol mg/kg 1.21.9 58 29-130ND
2,4-Dimethylphenol mg/kg 1.31.9 66 13-130ND
2,4-Dinitrophenol mg/kg 7.1 v1107110-131ND
2,4-Dinitrotoluene mg/kg 1.21.9 60 28-130ND
2,6-Dinitrotoluene mg/kg 1.31.9 63 36-130ND
2-Chloronaphthalene mg/kg 1.11.9 54 27-130ND
2-Chlorophenol mg/kg 1.31.9 63 29-130ND
2-Methylnaphthalene mg/kg 1.01.9 52 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.31.9 65 20-130ND
2-Nitroaniline mg/kg 2.64 64 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3373556MATRIX SPIKE SAMPLE:
MSSpike
Result
92556387001
2-Nitrophenol mg/kg 1.31.9 67 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.21.9 60 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.2 IL45415-130ND
3-Nitroaniline mg/kg 2.3 IL45828-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.1 v147815-132ND
4-Bromophenylphenyl ether mg/kg 1.01.9 50 35-130ND
4-Chloro-3-methylphenol mg/kg 2.44 61 30-130ND
4-Chloroaniline mg/kg 2.14 53 28-130ND
4-Chlorophenylphenyl ether mg/kg 0.991.9 49 32-130ND
4-Nitroaniline mg/kg 2.34 58 30-130ND
4-Nitrophenol mg/kg 6.410 64 17-130ND
Acenaphthene mg/kg 1.11.9 54 29-130ND
Acenaphthylene mg/kg 1.11.9 57 31-130ND
Aniline mg/kg 1.21.9 61 10-130ND
Anthracene mg/kg 1.11.9 53 33-130ND
Benzo(a)anthracene mg/kg 1.11.9 54 32-130ND
Benzo(a)pyrene mg/kg 1.11.9 55 32-130ND
Benzo(b)fluoranthene mg/kg 1.11.9 54 33-130ND
Benzo(g,h,i)perylene mg/kg 1.11.9 56 28-130ND
Benzo(k)fluoranthene mg/kg 1.11.9 54 31-130ND
Benzoic Acid mg/kg 5.210 52 10-130ND
Benzyl alcohol mg/kg 2.44 61 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.31.9 64 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.51.9 74 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.01.9 52 40-130ND
Butylbenzylphthalate mg/kg 1.21.9 58 40-130ND
Chrysene mg/kg 1.01.9 52 30-130ND
Di-n-butylphthalate mg/kg 1.11.9 53 41-130ND
Di-n-octylphthalate mg/kg 1.21.9 57 42-130ND
Dibenz(a,h)anthracene mg/kg 1.21.9 59 27-130ND
Dibenzofuran mg/kg 1.11.9 53 32-130ND
Diethylphthalate mg/kg 1.21.9 58 40-130ND
Dimethylphthalate mg/kg 1.21.9 61 37-130ND
Fluoranthene mg/kg 1.01.9 52 26-130ND
Fluorene mg/kg 1.01.9 51 31-130ND
Hexachloro-1,3-butadiene mg/kg 0.981.9 49 20-130ND
Hexachlorobenzene mg/kg 1.01.9 50 29-130ND
Hexachlorocyclopentadiene mg/kg 0.691.9 35 10-130ND
Hexachloroethane mg/kg 1.11.9 57 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.21.9 57 28-130ND
Isophorone mg/kg 1.31.9 66 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.31.9 64 31-130ND
N-Nitrosodimethylamine mg/kg 1.5 v11.9 74 20-130ND
N-Nitrosodiphenylamine mg/kg 1.11.9 57 32-130ND
Naphthalene mg/kg 1.11.9 56 30-130ND
Nitrobenzene mg/kg 1.31.9 66 25-130ND
Pentachlorophenol mg/kg 2.04 51 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3373556MATRIX SPIKE SAMPLE:
MSSpike
Result
92556387001
Phenanthrene mg/kg 1.11.9 53 34-130ND
Phenol mg/kg 1.4 v11.9 70 14-130ND
Pyrene mg/kg 1.11.9 56 31-130ND
Pyridine mg/kg 0.87 v11.9 44 10-130ND
2,4,6-Tribromophenol (S)%61 18-130
2-Fluorobiphenyl (S)%47 19-130
2-Fluorophenol (S)%68 18-130
Nitrobenzene-d5 (S)%67 21-130
Phenol-d6 (S)%67 18-130
Terphenyl-d14 (S)%50 15-130
Parameter Units
Dup
Result QualifiersRPDResult
92556387002
3373557SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg ND v1ND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg ND ILND
3-Nitroaniline mg/kg ND ILND
4,6-Dinitro-2-methylphenol mg/kg ND v1ND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92556387002
3373557SAMPLE DUPLICATE:
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg NDND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg NDND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg ND v1ND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg ND v1ND
Pyrene mg/kg NDND
Pyridine mg/kg ND v1ND
2,4,6-Tribromophenol (S)%3 S03
2-Fluorobiphenyl (S)%4142
2-Fluorophenol (S)%5 S07
Nitrobenzene-d5 (S)%4753
Phenol-d6 (S)%2230
Terphenyl-d14 (S)%5458
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 94
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92556378
N. Graham & 6th
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
641386
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92556378012, 92556378013, 92556378014, 92556378015, 92556378016
Parameter Units
Dup
Result QualifiersRPDResult
92556011002
3366735SAMPLE DUPLICATE:
Percent Moisture %40.6 N2339.5
Parameter Units
Dup
Result QualifiersRPDResult
92555809002
3366736SAMPLE DUPLICATE:
Percent Moisture %43.9 N2044.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 94
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92556378
N. Graham & 6th
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Re-extraction conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.1g
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 94
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92556378
N. Graham & 6th
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92556378001 641867 642546GW-1 EPA 3510C EPA 8270E
92556378002 641867 642546GW-2 EPA 3510C EPA 8270E
92556378003 641867 642546GW-3 EPA 3510C EPA 8270E
92556378004 641867 642546GW-4 EPA 3510C EPA 8270E
92556378005 641867 642546GW-5 EPA 3510C EPA 8270E
92556378006 641867 642546GW-6 EPA 3510C EPA 8270E
92556378007 641867 642546GW-7 EPA 3510C EPA 8270E
92556378008 642143 642649GW-8 EPA 3510C EPA 8270E
92556378009 642143 642649GW-9 EPA 3510C EPA 8270E
92556378010 642143 642649GW-10 EPA 3510C EPA 8270E
92556378011 642143 642649GW-11 EPA 3510C EPA 8270E
92556378012 642890 643133SS-1 EPA 3546 EPA 8270E
92556378013 642890 643133SS-2 EPA 3546 EPA 8270E
92556378014 642890 643133SS-3 EPA 3546 EPA 8270E
92556378015 642890 643133SS-4 EPA 3546 EPA 8270E
92556378016 642890 643133SS-5 EPA 3546 EPA 8270E
92556378012 642240 642245SS-1 EPA 5035A/5030B EPA 8260D
92556378013 642240 642245SS-2 EPA 5035A/5030B EPA 8260D
92556378014 642240 642245SS-3 EPA 5035A/5030B EPA 8260D
92556378015 642240 642245SS-4 EPA 5035A/5030B EPA 8260D
92556378016 642240 642245SS-5 EPA 5035A/5030B EPA 8260D
92556378001 641729GW-1 EPA 8260D
92556378002 641729GW-2 EPA 8260D
92556378003 641729GW-3 EPA 8260D
92556378004 641729GW-4 EPA 8260D
92556378005 641729GW-5 EPA 8260D
92556378006 641729GW-6 EPA 8260D
92556378007 641729GW-7 EPA 8260D
92556378008 641729GW-8 EPA 8260D
92556378009 641729GW-9 EPA 8260D
92556378010 641729GW-10 EPA 8260D
92556378011 641729GW-11 EPA 8260D
92556378012 641386SS-1 SW-846
92556378013 641386SS-2 SW-846
92556378014 641386SS-3 SW-846
92556378015 641386SS-4 SW-846
92556378016 641386SS-5 SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/26/2021 12:58 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 94
Page 90 of 94
Page 91 of 94
Page 92 of 94
Page 93 of 94
Page 94 of 94

APPENDIX C

Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading78.6
755.0 Sample NumberSS-1 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
DescripƟon
Brown Clayey Silt. PHC Odor
Brown Silt, Wet. PHC Odor
END OF DRILLING AT 10.0 FT
Project Name:Graham and 6th Site
Client:Daniel Realty Company, LLC
Site LocaƟon:301 North Graham Street and 420 West 6th,
CharloƩe, North Carolina 28202
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-1
Project No.:49:13734-A
Driller:3D Enviro Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Aug 16 2021
WL (CompleƟon)Boring Completed:Aug 16 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavallier
ScoƩ Werley
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading61.5
338.0
1075.0 Sample NumberSS-2 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
ML
DescripƟon
Brown Clayey Silt. PHC Odor
Brown Silt. PHC Odor
Brown Silt. PHC Odor
END OF DRILLING AT 15.0 FT
Project Name:Graham and 6th Site
Client:Daniel Realty Company, LLC
Site LocaƟon:301 North Graham Street and 420 West 6th,
CharloƩe, North Carolina 28202
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-2
Project No.:49:13734-A
Driller:3D Enviro Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Aug 16 2021
WL (CompleƟon)Boring Completed:Aug 16 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavallier
ScoƩ Werley
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading440.0
354.0
1651.0 Sample NumberSS-3 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML/CL
ML
SM/MH
DescripƟon
Brown Clayey Silt
Gray/Brown Silt
Gray Sandy Silt, Wet
END OF DRILLING AT 15.0 FT
Project Name:Graham and 6th Site
Client:Daniel Realty Company, LLC
Site LocaƟon:301 North Graham Street and 420 West 6th,
CharloƩe, North Carolina 28202
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-3
Project No.:49:13734-A
Driller:3D Enviro Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Aug 17 2021
WL (CompleƟon)Boring Completed:Aug 17 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavallier
ScoƩ Werley
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading11.4
11.8
12.5 Sample NumberSS-4 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon DescripƟon
END OF DRILLING AT 15.0 FT
Project Name:Graham and 6th Site
Client:Daniel Realty Company, LLC
Site LocaƟon:301 North Graham Street and 420 West 6th,
CharloƩe, North Carolina 28202
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-4
Project No.:49:13734-A
Driller:3D Enviro Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Aug 17 2021
WL (CompleƟon)Boring Completed:Aug 17 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavallier
ScoƩ Werley
Depth/
5
10
15
20
25
30
ElevaƟon
-5
-10
-15
-20
-25 PID Reading12.1
19.2 Sample NumberSS-5 Sample Recovery (in)Graphic LogSoil ClassiĮcaƟon
ML-CL
SM-MH
DescripƟon
No Recovery
Brown Clayey Silt
Brown Sandy Silt
END OF DRILLING AT 15.0 FT
Project Name:Graham and 6th Site
Client:Daniel Realty Company, LLC
Site LocaƟon:301 North Graham Street and 420 West 6th,
CharloƩe, North Carolina 28202
LaƟtude/Longitude:
Sheet:1 of 1 Boring No:SS-5
Project No.:49:13734-A
Driller:3D Enviro Drill Rig:GeoProbe
WL (First Encountered)Boring Started:Aug 17 2021
WL (CompleƟon)Boring Completed:Aug 17 2021
Remarks:Logged By:
Principal Engineer/
Responsible PG:
Randy Cavallier
ScoƩ Werley

APPENDIX D

Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-1
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 1.8E-06 2.2E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 4.2E-07 5.2E-04 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-2
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 1.7E-06 2.1E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 3.9E-07 4.9E-04 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-3
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 5.2E-06 6.2E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 1.2E-06 1.5E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-4
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 5.4E-06 6.5E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 1.2E-06 1.5E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-6
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 3.3E-06 4.0E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 7.6E-07 9.4E-04 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-7
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 3.3E-06 4.0E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 7.6E-07 9.4E-04 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-8
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 1.9E-06 2.2E-02 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 4.3E-07 5.3E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-8
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 9.4E-06 7.1E-02 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 2.1E-06 1.7E-02 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: June 2021
Basis: May 2021 EPA RSL Table
Site ID: Graham and 6th Site
Exposure Unit ID: GW-11
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air 1.7E-06 2.1E-03 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 3.9E-07 4.9E-04 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator