26081_United Air Filter_ Limited Site Investigation_Final

Limited Site Investigation
United Air Filter Facility
1000 West Palmer Street
Charlotte, Mecklenburg County, North Carolina
August 11, 2022
Terracon Project No. 71227290

Prepared for:
United Air Filter Company
Charlotte, North Carolina

Prepared by:
Terracon Consultants, Inc.
Charlotte, North Carolina

Terracon Consultants, Inc. 2701 Westport Road Charlotte, NC 28208
P [phone] F [phone] terracon.com
August 11, 2022

United Air Filter Company
1000 West Palmer Street
Charlotte, North Carolina 28208

Attn: Mr. William Kinney
E: [e-mail]
P: 704-334-5311

Re: Limited Site Investigation
United Air Filter Facility
1000 West Palmer Street
Charlotte, Mecklenburg County, North Carolina 28208
Terracon Project No. 71227290

Dear Mr. Kinney:

Terracon Consultants, Inc. (Terracon) is pleased to submit this summary report of Limited Site
Investigation (LSI) activities completed at the above referenced site. This report presents data
from recent field activities that included collection of groundwater samples for laboratory analysis.
Terracon conducted the LSI in general accordance with Terracon proposal P71227290, dated
June 29, 2022.

Terracon appreciates this opportunity to provide environmental consulting services to United Air
Filter Company. If you have any questions or require additional information, please do not hesitate
to contact our office at [phone].

Sincerely,
Terracon Consultants, Inc.

Alex Chinery, PE Robert Brookshire
Environmental Group Manager Environmental Department Manager

Justin L. Fabriziani, RSM
Environmental Department Manager

Attachments

ii

TABLE OF CONTENTS
1.0 SITE DESCRIPTION ....................................................................................................... 1 1.1 Standard of Care.................................................................................................. 1 1.2 Additional Scope of Limitations ............................................................................ 2 1.3 Reliance ............................................................................................................... 2 2.0 FIELD INVESTIGATION METHODS ............................................................................... 2 2.1 Utility Location and Site Observations .................................................................. 2
2.2 Groundwater Investigation ................................................................................... 3 3.0 FIELD INVESTIGATION RESULTS ................................................................................ 4 3.1 Groundwater Analytical Results ........................................................................... 4 4.0 CONCLUSIONS .............................................................................................................. 4 5.0 RECOMMENDATIONS ................................................................................................... 5

Figures
Exhibit 1 – Topographic Map
Exhibit 2 – Sample Location Map

Table
Table 1 – Summary of Temporary Monitoring Well Construction
Table 2 – Summary of Groundwater Analytical Results

Appendices
APPENDIX A – SOIL BORING LOGS/FIELD FORMS

APPENDIX B – ANALYTICAL REPORTS AND CHAINS OF CUSTODY
Groundwater Analytical Report

Responsive ■ Resourceful ■ Reliable 1
LIMITED SITE INVESTIGATION
UNITED AIR FILTER FACILITY
1000 WEST PALMER STREET
CHARLOTTE, NORTH CAROLINA

TERRACON PROJECT NO. 71227290
AUGUST 11, 2022

1.0 SITE DESCRIPTION

The site consists of a 2.130-acre parcel located at 1000 West Palmer Street in Charlotte,
Mecklenburg County, North Carolina, identified on Mecklenburg County GIS Polaris database as
Parcel ID: 07325204 (the Site). The subject property is developed with a 44,520 square foot (sf)
warehouse, constructed in 1920. The remaining portions of the Site consist of asphalt parking
spaces, gravel areas, and limited vegetation.

Terracon previously completed a Phase I Environmental Site Assessment (ESA; Terracon Project
No. 71217171, May 17, 2022). The Phase I ESA identified the following recognized environmental
conditions (RECs):

 The long-term (100+ years) industrial/commercial operation at the Site and
surrounding properties is a REC.

 The documented groundwater impacts associated with the adjacent Clarkson
Street Brownfields project is an off-site REC.

 The documented groundwater impacts associated with the up-gradient Worth
Keeter facility (1117 South Clarkson Avenue) is an off-site REC.

Terracon performed the initial assessment activities described in this report to evaluate
groundwater conditions as it relates to the adjacent and off-site RECs identified during the ESA.

1.1 Standard of Care

Terracon’s services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same time.
Terracon makes no warranties, expressed or implied, regarding the findings, conclusions, or
recommendations. Please note that Terracon does not warrant the work of laboratories,
regulatory agencies, or other third parties supplying information to prepare the report. The
services were performed in accordance with the scope of work authorized by our client, as
reflected in our proposal and were not conducted in accordance with ASTM E1903-11.

Limited Site Investigation
United Air Filter Facility ■ Charlotte, North Carolina August 11, 2022 ■ Terracon Project No. 71227290
Responsive ■ Resourceful ■ Reliable 2
1.2 Additional Scope of Limitations

Findings, conclusions, and recommendations resulting from these services are based upon
information derived from the on-site activities and other services performed under this scope of
work; such information is subject to change over time. Certain indicators of the presence of
hazardous substances, petroleum products, or other constituents may have been latent,
inaccessible, unobservable, non-detectable, or not present during these services. We cannot
represent that the site is free of hazardous substances, toxic materials, petroleum products, or
other latent conditions beyond those identified during this investigation. Subsurface conditions
may vary from those encountered at specific borings or wells or during other surveys, tests,
assessments, investigations, or exploratory services. The data, interpretations, findings, and our
recommendations are based solely upon data obtained at the time and within the scope of these
services.

1.3 Reliance

This report is for the exclusive use of United Air Filter Company (United). Any authorization for
use or reliance by another party (except a governmental entity having jurisdiction over the site) is
prohibited without the expressed written authorization of United and Terracon. Any unauthorized
distribution or reuse is at the sole risk of United. Reliance by authorized parties will be subject to
the terms, conditions, and limitations stated in our proposal.

2.0 FIELD INVESTIGATION METHODS

On June 30, 2022, Terracon mobilized to the Site to install three temporary monitoring wells and
collect groundwater samples. Terracon conducted the fieldwork under a health and safety plan
developed for this project. Work was performed using United States Environmental Protection
Agency (USEPA) Level D work attire consisting of a hard hat, safety glasses, safety vest,
protective gloves, and protective boots.

2.1 Utility Location and Site Observations

Prior to intrusive activities, Terracon contacted North Carolina 811, the public utility locator, to
mark subsurface utilities throughout the Site. In addition, Terracon contracted Ground Penetrating
Radar Systems LLC, to identify and mark private utility lines, confirm public utility lines, and utility
clear the proposed boring locations using ground-penetrating radar (GPR) and electromagnetic
methods.

Limited Site Investigation
United Air Filter Facility ■ Charlotte, North Carolina August 11, 2022 ■ Terracon Project No. 71227290
Responsive ■ Resourceful ■ Reliable 3
2.2 Groundwater Investigation

On June 30, 2022, Terracon directed Carolina Soil Investigations (CSI), a North Carolina licensed
drilling company to install three temporary monitoring wells in the following locations:

 TW-1 was installed adjacent to the northeastern corner of the on-site building;
 TW-2 was installed in the northeastern corner of the property; and
 TW-3 was installed in the northwestern corner of the property.

Temporary monitoring well locations are presented in Exhibit 2.

The temporary monitoring wells were installed using direct-push technology (DPT) drilling
methods to advance the borings until sufficient groundwater was encountered. During temporary
well installation activities, the soil cuttings were observed for soil lithology, staining and odors,
and field-screened for the presence of volatile organic vapors using a calibrated photoionization
detector (PID). Terracon did not observe staining, odors, or elevated PID readings while
advancing the temporary monitoring wells. Boring logs summarizing field observations are
provided in Appendix A.

Temporary monitoring wells TW-1 and TW-2 were advanced to a total depth of 28 feet below
ground surface (ft bgs). Temporary monitoring well TW-3 was advanced to a total depth of 23 ft
bgs. The temporary monitoring wells were constructed per the following details:

 Installation of a 10-foot section of 1-inch diameter, 0.010-inch machine slotted PVC well
screen;
 Installation of a 1-inch diameter, threaded, flush-joint PVC riser pipe to the ground surface;
and
 Placement of sand in the borehole annulus to approximately two feet above the screened
interval, followed by a layer of hydrated bentonite.

Well construction details are provided in Table 1.

After installing the temporary monitoring wells, groundwater within the wells was allowed to
equilibrate to static conditions. Terracon used a decontaminated electronic water level meter to
measure groundwater depth. Groundwater in temporary monitoring wells TW-1 to TW-3 was
measured at 19.38 ft below top of casing (bTOC), 23.21 ft bTOC, and 19.21 ft bTOC, respectively.

The temporary monitoring wells were purged via a peristatic pump and dedicated disposable
tubing until field parameters (temperature, pH, specific conductivity, and oxidation-reduction
potential [ORP]) stabilized to within +/- 10%. Samples were collected in laboratory-provided
sample containers and packed on ice for shipment to Pace Analytical for analysis of volatile
Limited Site Investigation
United Air Filter Facility ■ Charlotte, North Carolina August 11, 2022 ■ Terracon Project No. 71227290
Responsive ■ Resourceful ■ Reliable 4
organic compounds (VOCs) by EPA Method 8260, semi-volatile organic compounds (SVOCs) by
EPA Method 8270, and RCRA metals by EPA Methods 6010/6020/7471.

After the sampling activities were completed, the temporary monitoring wells were abandoned,
and the surfaces were repaired to match pre-drilling conditions.
3.0 FIELD INVESTIGATION RESULTS

Soils encountered at the Site generally consisted of reddish and yellowish-brown silts with varying
sand. The groundwater analytical results are summarized in Table 2. Copies of the laboratory
analytical reports are provided in Appendix B.

3.1 Groundwater Analytical Results

Detected concentrations of constituents of concern were compared to North Carolina Department
of Environmental Quality (NCDEQ) 15A NCAC 02L .0202 Groundwater Standards (2L Standards)
updated April 1, 2022 and Gross Contamination Levels for Groundwater (GCLs) updated March
2022 and are summarized below:

 Trichloroethene (TCE) was detected at a concentration above the 2L Standard in
groundwater from temporary well TW-2.
 TCE was detected in groundwater from temporary well TW-1 and TW-3 at concentrations
below the 2L Standard.
 Additional VOCs were not detected at concentrations above their respective method
detection limits (MDLs) in groundwater from TW-1, TW-2 and TW-3.
 Arsenic, Barium, Cadmium, Chromium, Lead, and Selenium were detected at
concentrations above their respective 2L Standards in groundwater from temporary
monitoring well TW-1.
 Arsenic and Chromium were detected at concentrations above their respective 2L
Standards in groundwater from temporary monitoring wells TW-2 and TW-3.
 Lead was detected at concentrations above the 2L Standard in groundwater from
temporary monitoring well TW-3.
 None of the detected compounds were above the GCLs.
 SVOCs were not detected at concentrations above 2L Standards or GCLs in groundwater
from temporary monitoring wells TW-1, TW-2, or TW-3.

4.0 CONCLUSIONS

On June 30, 2022, Terracon collected three groundwater samples from three temporary
monitoring wells.

Limited Site Investigation
United Air Filter Facility ■ Charlotte, North Carolina August 11, 2022 ■ Terracon Project No. 71227290
Responsive ■ Resourceful ■ Reliable 5
 TCE was detected in groundwater from temporary monitoring well TW-2 at a concentration
above the 2L Standard. Additional VOCs or SVOCs were not detected above the MDLs.
 Multiple detections of metals above 2L Standards were identified in the on-site temporary
monitoring wells; likely due to high turbidity observed in the groundwater.

5.0 RECOMMENDATIONS

Based on the findings of the LSI and Terracon’s understanding of the operations of the site, the
reported impacts may be attributable to off-site sources. Prior to site redevelopment, additional
environmental sampling should be completed to further evaluate the limits of the TCE plume in
groundwater and potential risk posed by vapor intrusion. Additionally, further investigation may
be necessary to manage the presence of heavy metals in the on-site soil and/or groundwater. A
site management plan may be necessary prior to site redevelopment to outline protocols for the
proper management of potentially impacted soil, groundwater, and soil vapor during future
redevelopment.

TOPOGRAPHIC MAP
United Air Filter
1000 West Palmer Street Charlotte, NC
TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY QUADRANGLES INCLUDE: MOUNTAIN ISLAND LAKE, NC (1/1/1997), DERITA, NC (1/1/1993), CHARLOTTE WEST, NC (1/1/1993) and CHARLOTTE EAST, NC (1/1/1988).
2701 Westport Rd
Charlotte, NC 28208-3608
71227290 Project Manager:
Drawn by:
Checked by:
Approved by:
SAC
RSB
RSB
1”=2,000’
Figure1
August 2022
Project No.
Scale:
File Name:
Date: 1
Exhibit SAC
APPROXIMATE
SITE BOUNDARY
2
Exhibit
2701 Westport Road
Charlotte, NC
SAMPLE LOCATION MAPProject Manager:
Drawn by:
Checked by:
Approved by:
SAC Proposal No.
File Name:
Date:
Scale:
P71227240
SAC
June 2022SAC
MNM
NTS
Figure 1
United Air Filter Facility 1000 West Palmer StreetCharlotte, North Carolina
LEGEND:
SITE BOUNDARY
Image obtained from Google Earth.
Checked by:
CLARKSON STREETBROWNFIELDS
CHARLOTTE PIPE & FOUNDRY
CHARLOTTE PIPE & FOUNDRY
CHARLOTTE PIPE & FOUNDRY
-MONITORING WELL LOCATIONS
TW-1
TW-2
TW-3
Table 1
Summary of Temporary Well Construction
United Air Filter Facility
1000 West Palmer Street
Charlotte, North Carolina
Terracon Project Number: 71227290
Well Well Screen Water
Diameter Depth Interval Table Depth
(inches)(ft)(ft)(ft bgs)
TW-01 6/30/2022 1 28 18-28 Soil 19.38
TW-02 6/30/2022 1 28 18-28 Soil 23.21
TW-03 6/30/2022 1 23 13-23 Soil 19.21
Notes:
ft bgs = feet below ground surface
TW= temporary monitoring well
Installation Date
Depth to groundwater measurements were collected from temporary monitoring wells TW-01, TW-
02, and TW-03 on June 30, 2022. The temporary monitoring wells were abandoned on June 30,
2022 after sampling activities were completed.
Monitoring Well
Identification Lithology
\\charlotte1\Data\Projects\2022\71227290\Working Files\Laboratory-Field Data-Boring Logs\LSI Tables8/11/2022 Table 1
Table 2
Summary of Groundwater Analytical Results
United Air Filter Facility
1000 West Palmer Street
Charlotte, North Carolina
Terracon Project Number: 71227290
Sample Location
Adjacent to NE
Corner of Building
Adjacent to NE
Corner of Property
Adjacent to NW
Corner of Property
Sample ID TW-1 TW-2 TW-3
Date 6/30/2022 6/30/2022 6/30/2022
VOCs (6200B) µg/L
Trichloroethene (TCE)0.75 3.4 0.48J 3 3,000
Metals (6020B) µg/L
Arsenic 46.8J 13.1J 15.6J 10 NE
Barium 4,390 110 575 700 700,000
Cadmium 2.0J <0.57 <0.57 2 NE
Chromium 183 13.7J 374 10 10,000
Lead 80.4 <4.4 21.0 15 15,000
Selenium 24.9J <6.8 <6.8 20 NE
Notes:
1) North Carolina Department of Environmental Quality (NCDEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 2022.
2) NCDEQ Gross Contaminant Levels (GCLs) revised March 7, 2022.
Bolded values exceed 2L Standards
Method detection limits are shown above for non-detections
Constituents detected in at least one sample are shown above; refer to the laboratory report
TW= temporary monitoring well
µg/L = micrograms/liter
VOCs = volatile organic compounds
J = estimated concentrations above the adjusted method detection limit and below the adjusted reporting limit
<0.38 = below method detection limits
NE = Not Established
2L Standards (1)GCLs (2)
Screening Criteria
\\charlotte1\Data\Projects\2022\71227290\Working Files\Laboratory-Field Data-Boring Logs\LSI Tables8/11/2022
Table 2

APPENDIX A – SOIL BORING LOGS/FIELD FORMS

Client: United Air Filter Drilling Co: CSI
Site: United Air Filter Facility - Charlotte Lead Driller:
Project No: 71227290 Time Started:
Time Finished:
Logged By: Alex Chinery
Weather: Sunny, 90's Depth of Boring: 34 ft
Drilling
Method / Dia.
Blow
Counts (per 6 in)
Recovery
(ft)PID (ppm)Geologic
ID U.S.C.S.
NOTES: Checked by: RSB Date:8/11/2022
Boring ID:TW-1
Rig make / type: 9:30
Site Address: 1000 West Palmer Street, Charlotte, Mecklenburg
County, NC 10:15
15-20 feet: SILTY SAND, brown,
micaceous material
20
Groundwater encountered at approx. 20 feet
20-25 feet: SILTY SAND, brown, micaceous material, indications of PWR
Depth (ft)Description of Drill Cuttings
Hand AugerNot ApplicableNot ApplicableML
0-10 feet: SANDY CLAY, light brown/yellowish orange, dry
60
Static water level measured at 19.38 feet bgs.
Temporary monitoring well depth = 28 feet bgs.
Boring terminated at 34' bgs
0.0
0.0
0.0
0.0
Not Collected30
40
50 Direct-push TechnologySM
10
10-15 feet: SANDY SILT, light brown,
fine, dry
Client: United Air Filter Drilling Co: CSI
Site: United Air Filter Facility - Charlotte Lead Driller:
Project No: 71227290 Time Started:
Time Finished:
Logged By: Alex Chinery
Weather: Sunny, 90's Depth of Boring: 28 ft
Drilling
Method / Dia.
Blow
Counts (per 6 in)
Recovery
(ft)PID (ppm)Geologic
ID U.S.C.S.
NOTES: Checked by: RSB Date:8/11/2022
Boring ID:TW-2
Rig make / type: 10:30
Site Address: 1000 West Palmer Street, Charlotte, Mecklenburg
County, NC 11:45
10-15 feet: SANDY SILT, light brown,
fine, dry
0.0 15-20 feet: SILTY SAND, brown,
micaceous material
20
Depth (ft)Description of Drill Cuttings
Hand AugerNot ApplicableNot Applicable0.0
ML
0-10 feet: SANDY SILT, light brown/yellowish orange, dry
60
Static water level measured at 23.21 feet bgs.
Temporary monitoring well depth = 28 feet bgs.
Boring terminated at 28' bgsDirect-push TechnologyGroundwater encountered at approx. 20 feet
20-25 feet: SILTY SAND, brown, micaceous material, indications of PWR
SM0.0
Not Collected30
40
50
0.0
10
0.0
Client: United Air Filter Drilling Co: CSI
Site: United Air Filter Facility - Charlotte Lead Driller:
Project No: 71227290 Time Started:
Time Finished:
Logged By: Alex Chinery
Weather: Sunny, 90's Depth of Boring: 23 ft
Drilling
Method / Dia.
Blow
Counts (per 6 in)
Recovery
(ft)PID (ppm)Geologic
ID U.S.C.S.
NOTES: Checked by: RSB Date:8/11/2022
Boring ID:TW-3
Rig make / type: 12:00
Site Address: 1000 West Palmer Street, Charlotte, Mecklenburg
County, NC 13:30
Depth (ft)Description of Drill Cuttings
Hand AugerNot ApplicableNot Applicable0.0
ML
0-10 feet: SILTY clay, light brown/yellowish orange, dry
Groundwater encountered at approx. 20 feet
20-23 feet: SILTY SAND, brown, micaceous material, indications of PWR
0.0
10
0.0 10-15 feet: SANDY SILT, light brown,
fine, dry
0.0 15-20 feet: SILTY SAND, brown,
micaceous material
20
Not CollectedDirect-push TechnologySM
60
Static water level measured at 19.21 feet bgs.
Temporary monitoring well depth = 23 feet bgs.
30
40
50
Boring terminated at 23' bgs
_Groundwc!!er Samplin 9 Log_ lrerracon ------
ProJect No.---~~---------
Site Location -:---::-'-:~UJ:bf!--f-,-..1--_________ _
Date ___,,y~/_S-=-Q __
Weather --h~'-'L-J.J_ ___________ _
Well ID __ --r'...!.....:w=--_-...Jr[__ ____ _
Sample Collect,on T,me
Casing
Diameter Gal/ft Lift
D 6 1.47 5.56
D 4 653 2.47
D 3 367 1.39
D 2 163 .618 g ~ .04 1 .154
.023 .087
~
mple Method
Peristaltic D Grundfos
Bladder D Monsoon
D Bailer D PDB D Monsoon
Field Parameters
Evacuation Data
Screen Length (ft bis)
Well Length (ft bTOC)
Depth to water (ft bTOC)
Water column length (ft )
Well Volume
Evacuation Volu me (x
Purge Device
Dedicated D Disposable D Decontaminated
QA/QC Samples
D Duplicate D MS/MSD D Equipment Blank D Field Blank
o ·
7 :0 '
\9 3 f2 '
Sample ID for QA/QC
Time Purge Temp pH DO Cond. Turb. Redox Flow Drawdown
1/"1_
11; t:iO I /7,,
I 7., lo_ I .$'
, (°C) {S_!J_) {!!!9&)
_ ?D . \ _ W~ Z-'1 5""
. l,\i .(; 0 W. 1 .J '!::> . V . \D _ &-"Q.L 7 S1::__
(µmhos/cm) , {NTI:J..L _ d mY.) {mUmill)
~3?.:..ltz > -t.J1.l..f. Y. Z,o. y__ :;,_ -J.;. )
<,,(1,,B . q_ 7 -:Js_, s--__ _
(I!)
------------
Laboratory Analyses
Analytical Parameter
D voes
D PAHs
D
D
D
D
SVOCs
TPH
Metals
--------
Method I B ottle Size/Type I Preservative
Bottles 1
8260 3 __ 40 ml glass _ HCI
8270 2 1 L amber none
6010 250 ml Plastic nitric acid
Notes: __ -.--!\jj.i,..\l~JW:,___!\J+--'---'-'~'-41\Q...L..!.\ Jl--+----------
Sampling Personnel: __ __:__4.J--__ C_J/l-=-~----------------
Groundwater Sampling Log 1rerracon
Project No.-~-~----------
Site Location _.:::G~f_f\-_!_-________ _ Date __ 0~/-~_u __ _
Well ID __ ::P-:::'..1....-_-_'-____ _
Weather ___ -1..fo _ _..:::lf _________ _ Sample Collection Time \~. '7t°
Casing
Diameter Gal/ft Uft Evacuation Data
6 1.47 5.56 Screen Length (ft bis) ~o'
4 .653 2.47 Well Length (ft bTOC) Z...6
3 .367 1.39 Depth to water (ft bTOC) 7...3 · 7.-\ a~ .1 63 .618 Water column length (ft)
.041 .154 Well Volume
¾ .023 .087 Evacuation Volume (x
~
pie Method
Peristaltic D Grundfos
fu;ge Device
1:1" Dedicated
D Disposable
QA/QC Samples
D Duplicate
Sample ID for QA/QC rw-~
Bladder D Monsoon 0 Bailer O PDB D Monsoon
Field Parameters
D Decontaminated
0 MS/MSD D Equipment Blank
0 Field Blank
Time Purge Temp pH DO Cond. I Turb. : Redox Flow Drawdown
(OC) _(SU) (my/L) . (µm~os/cm) 1 (NTU) (mV) , (mUmiaj_ j Jft) J1,·Th°. . 'll, ~. (o .l'.]q . Y 7'1,, "s 3D,(e l
j ,-QD . 0 :'l.S 2 )_, .0 f~,1: 3 0 ":}. ) IP . '1-'
1·-~_ . .9f Z5S.o .~.'1'. 3°.1-3. la>.3 .
Laboratory Analyses --
Analytical Parameter
voes
PAHs
SVOCs
TPH
Metals
-~-Method 7
j 82~0
!
8270
6010
. it7. . .lS.7-~
I YJ D ,
_ ___J
I
L
j
No. Bottle Size/Type
Bottles J
3 40 ml glass I -
2 1 lamber
250 ml Plastic
Notes: 1\JwvPt-il J) RH Q ,C M ' u:s fcXOu& h PY
Preservative
HCI
1 none ...---
nitric acid
Sampling Personnel: ---~--''-+-~.3;:):::2r-:::3>-------------------
Groundwater Sampling Log l ferracon
Project No. _____________ _
Site Location --~~J.:.lil:ftr..t:~--------
Weather __ --10:::JLuifCJ.JL ________ _ Sample Collection Time
Casing
Diameter Gal/ft Uft D 6 1.47 5.56 D 4 .653 2.47 D 3 .367 1.39 D 2 .163 .618
~1 .041 .154 D ¾ .023 .087
Sample Method
Jg' Peristaltic D Grundfos b Bladder O Monsoon D Bailer O PDB
0 Monsoon
Field Parameters
Evacuation Data
Screen Length (ft bis)
Well Length (ft bTOC)
Depth to water (ft bTOC)
Water column length (ft)
Well Volume
Evacuation Volume (x ')
Purge Device
0 Dedicated
0 Disposable
0 Decontaminated
QA/QC Samples
0 Duplicate D MS/MSD
0 Equipment Blank
0 Field Blank
i4 -1,I
o -15
Sample ID for QA/QC
Time Purge Temp pH I DO I Cond. 1 Turb. ,• Redox Flow Drawdown
(°CJ _.JSU) _ (r!!_g/L) 1 (µm hos/cm) , (NTU). _ _,_ _ _,_(m"-V)'-L-_ _,(=m=U=m'-"in,,_)-'-'1 ("'ft,_) __ _ -~s J ·-5~-(J_._1.J -i~ {\~----03-,--:lf70 \--~ss .,_,___\ __ __._-10_g -1,,_,___ ___ _
1 \~ v, _ l.O ·li) ___ ·1 _l-',Q::,. 1.9 ,. -1~ .,,,,
\. ~0i ~--VJ ,J__ ia_fil__i.-:.10 . 1A .1L ~-..:.._1 --------'1,---°''6'-,v=---------
~w ct( t\,----1JL,-v 1 !£.:_5)j__ l , OU l _~~ S 1 1i.~
_· . \ :~ _L,~IQ,_*_µtO I 2,'.'.Ko----=U.L-.-------.:_~'J._.'-'---"'------'---
Laboratory Analyses
Analytical Parameter
D voes
0 PAHs
0 SVOCs
D TPH
0 Metals
D
I I
I
I
I
i I
Method No. Bottle Size/Type Preservative
Bottles
8260 40 ml glass . HCI
8270 ---"-l-'-1 Lamber none
6010 7--------------
250 ml Plastic nitric acid
Sampling Personnel: __________________________ _

APPENDIX B –ANALYTICAL REPORT AND CHAIN OF
CUSTODY

Groundwater Sample Analytical Report – Pace Laboratory
#=CL#
July 11, 2022
LIMS USE: FR - ALEX CHINERY
LIMS OBJECT ID: 92612736
92612736
Project:
Pace Project No.:
RE:
Alex Chinery
Terracon
2701 Westport Rd
Charlotte, NC 28208
UAF/71227290
Dear Alex Chinery:
Enclosed are the analytical results for sample(s) received by the laboratory on July 01, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyler Forney
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 40
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92612736
UAF/71227290
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 40
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92612736
UAF/71227290
Lab ID Sample ID Matrix Date Collected Date Received
92612736001 TW-1 Water 06/30/22 12:30 07/01/22 09:05
92612736002 TW-2 Water 06/30/22 13:25 07/01/22 09:05
92612736003 TW-3 Water 06/30/22 14:15 07/01/22 09:05
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 40
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92612736
UAF/71227290
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92612736001 TW-1 EPA 6020B 7 PASI-GACW1
EPA 7470A 1 PASI-GAVB
EPA 8270E 74 PASI-CPKS
SM 6200B 63 PASI-CSAS
92612736002 TW-2 EPA 6020B 7 PASI-GACW1
EPA 7470A 1 PASI-GAVB
EPA 8270E 74 PASI-CPKS
SM 6200B 63 PASI-CSAS
92612736003 TW-3 EPA 6020B 7 PASI-GACW1
EPA 7470A 1 PASI-GAVB
EPA 8270E 74 PASI-CPKS
SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 40
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92612736
UAF/71227290
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92612736001 TW-1
Arsenic 46.8J ug/L 07/08/22 17:39 D350.0EPA 6020B
Barium 4390 ug/L 07/08/22 17:3950.0EPA 6020B
Cadmium 2.0J ug/L 07/08/22 17:39 D35.0EPA 6020B
Chromium 183 ug/L 07/08/22 17:3950.0EPA 6020B
Lead 80.4 ug/L 07/08/22 17:3910.0EPA 6020B
Selenium 24.9J ug/L 07/08/22 17:39 D350.0EPA 6020B
Trichloroethene 0.75 ug/L 07/02/22 02:410.50SM 6200B
92612736002 TW-2
Arsenic 13.1J ug/L 07/08/22 17:45 D325.0EPA 6020B
Barium 110 ug/L 07/08/22 17:4525.0EPA 6020B
Chromium 13.7J ug/L 07/08/22 17:45 D325.0EPA 6020B
Trichloroethene 3.4 ug/L 07/02/22 03:000.50SM 6200B
92612736003 TW-3
Arsenic 15.6J ug/L 07/08/22 17:51 D325.0EPA 6020B
Barium 575 ug/L 07/08/22 17:5125.0EPA 6020B
Chromium 374 ug/L 07/08/22 17:5125.0EPA 6020B
Lead 21.0 ug/L 07/08/22 17:515.0EPA 6020B
Trichloroethene 0.48J ug/L 07/02/22 03:180.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 40
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92612736
UAF/71227290
Method:
Client:Terracon - Charlotte, NC
EPA 6020B
Date:July 11, 2022
Description:6020 MET ICPMS
General Information:
3 samples were analyzed for EPA 6020B by Pace Analytical Services Peachtree Corners, GA. All samples were received in acceptable
condition with any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attachedat the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3005A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 708819
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• TW-1 (Lab ID: 92612736001)
• Silver
• Arsenic
• Cadmium
• Selenium
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 40
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92612736
UAF/71227290
Method:
Client:Terracon - Charlotte, NC
EPA 6020B
Date:July 11, 2022
Description:6020 MET ICPMS
Analyte Comments:
QC Batch: 708819
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• TW-2 (Lab ID: 92612736002)
• Silver
• Arsenic
• Cadmium
• Chromium
• Lead
• Selenium
• TW-3 (Lab ID: 92612736003)
• Silver
• Arsenic
• Cadmium
• Selenium
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 40
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92612736
UAF/71227290
Method:
Client:Terracon - Charlotte, NC
EPA 7470A
Date:July 11, 2022
Description:7470 Mercury
General Information:
3 samples were analyzed for EPA 7470A by Pace Analytical Services Peachtree Corners, GA. All samples were received in acceptable
condition with any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attachedat the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 7470A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 40
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92612736
UAF/71227290
Method:
Client:Terracon - Charlotte, NC
EPA 8270E
Date:July 11, 2022
Description:8270E RVE
General Information:
3 samples were analyzed for EPA 8270E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3510C with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 709032
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samplesmay be biased high.
• LCS (Lab ID: 3697505)
• 4-Bromophenylphenyl ether
• Anthracene
• Benzo(a)anthracene
• Benzo(a)pyrene
• Benzo(b)fluoranthene
• Benzo(g,h,i)perylene
• Benzo(k)fluoranthene
• Butylbenzylphthalate
• Chrysene
• Di-n-octylphthalate
• Dibenz(a,h)anthracene
• Fluoranthene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 40
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92612736
UAF/71227290
Method:
Client:Terracon - Charlotte, NC
EPA 8270E
Date:July 11, 2022
Description:8270E RVE
QC Batch: 709032
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• Hexachlorobenzene
• Indeno(1,2,3-cd)pyrene
• Phenanthrene
• Pyrene
• bis(2-Ethylhexyl)phthalate
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 709032
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92613441001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3699118)
• Benzoic Acid
R1: RPD value was outside control limits.
• MSD (Lab ID: 3699119)
• 1,2,4-Trichlorobenzene
• 1-Methylnaphthalene
• 2,2'-Oxybis(1-chloropropane)
• 2,4-Dichlorophenol
• 2,4-Dimethylphenol
• 2-Chloronaphthalene
• 2-Chlorophenol
• 2-Methylnaphthalene
• 2-Methylphenol(o-Cresol)
• 2-Nitrophenol
• 3&4-Methylphenol(m&p Cresol)
• 4-Chloroaniline
• Aniline
• Benzo(a)pyrene
• Benzo(k)fluoranthene
• Benzyl alcohol
• Chrysene
• Dibenz(a,h)anthracene
• Hexachlorocyclopentadiene
• Indeno(1,2,3-cd)pyrene
• Isophorone
• N-Nitroso-di-n-propylamine
• N-Nitrosodimethylamine
• Naphthalene
• Nitrobenzene
• bis(2-Chloroethoxy)methane
• bis(2-Chloroethyl) ether
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 40
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92612736
UAF/71227290
Method:
Client:Terracon - Charlotte, NC
EPA 8270E
Date:July 11, 2022
Description:8270E RVE
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 40
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92612736
UAF/71227290
Method:
Client:Terracon - Charlotte, NC
SM 6200B
Date:July 11, 2022
Description:6200B MSV
General Information:
3 samples were analyzed for SM 6200B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-1 Lab ID:92612736001 Collected:06/30/22 12:30 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3005A
Pace Analytical Services - Peachtree Corners, GA
6020 MET ICPMS
Arsenic 46.8J ug/L 07/08/22 17:39 7440-38-2 D307/06/22 08:0850.0 21.6 1
Barium 4390 ug/L 07/08/22 17:39 7440-39-307/06/22 08:0850.0 6.7 1
Cadmium 2.0J ug/L 07/08/22 17:39 7440-43-9 D307/06/22 08:085.0 1.1 1
Chromium 183 ug/L 07/08/22 17:39 7440-47-307/06/22 08:0850.0 11.0 1
Lead 80.4 ug/L 07/08/22 17:39 7439-92-107/06/22 08:0810.0 8.9 1
Selenium 24.9J ug/L 07/08/22 17:39 7782-49-2 D307/06/22 08:0850.0 13.7 1
Silver ND ug/L 07/08/22 17:39 7440-22-4 D307/06/22 08:0850.0 4.4 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 07/06/22 10:26 7439-97-607/05/22 15:150.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/08/22 12:46 83-32-907/07/22 10:4810.0 2.0 1
Acenaphthylene ND ug/L 07/08/22 12:46 208-96-807/07/22 10:4810.0 2.0 1
Aniline ND ug/L 07/08/22 12:46 62-53-307/07/22 10:4810.0 1.6 1
Anthracene ND ug/L 07/08/22 12:46 120-12-7 L107/07/22 10:4810.0 2.3 1
Benzo(a)anthracene ND ug/L 07/08/22 12:46 56-55-3 L107/07/22 10:4810.0 2.7 1
Benzo(a)pyrene ND ug/L 07/08/22 12:46 50-32-8 L107/07/22 10:4810.0 2.8 1
Benzo(b)fluoranthene ND ug/L 07/08/22 12:46 205-99-2 L107/07/22 10:4810.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 07/08/22 12:46 191-24-2 L107/07/22 10:4810.0 2.8 1
Benzo(k)fluoranthene ND ug/L 07/08/22 12:46 207-08-9 L107/07/22 10:4810.0 2.7 1
Benzoic Acid ND ug/L 07/08/22 12:46 65-85-007/07/22 10:4850.0 22.0 1
Benzyl alcohol ND ug/L 07/08/22 12:46 100-51-607/07/22 10:4820.0 2.9 1
4-Bromophenylphenyl ether ND ug/L 07/08/22 12:46 101-55-3 L107/07/22 10:4810.0 1.8 1
Butylbenzylphthalate ND ug/L 07/08/22 12:46 85-68-7 L107/07/22 10:4810.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 07/08/22 12:46 59-50-707/07/22 10:4810.0 3.3 1
4-Chloroaniline ND ug/L 07/08/22 12:46 106-47-807/07/22 10:4820.0 3.6 1
bis(2-Chloroethoxy)methane ND ug/L 07/08/22 12:46 111-91-107/07/22 10:4810.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 07/08/22 12:46 111-44-407/07/22 10:4810.0 1.9 1
2-Chloronaphthalene ND ug/L 07/08/22 12:46 91-58-707/07/22 10:4810.0 1.7 1
2-Chlorophenol ND ug/L 07/08/22 12:46 95-57-807/07/22 10:4810.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 07/08/22 12:46 7005-72-307/07/22 10:4810.0 2.0 1
Chrysene ND ug/L 07/08/22 12:46 218-01-9 L107/07/22 10:4810.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 07/08/22 12:46 53-70-3 L107/07/22 10:4810.0 3.0 1
Dibenzofuran ND ug/L 07/08/22 12:46 132-64-907/07/22 10:4810.0 2.1 1
1,2-Dichlorobenzene ND ug/L 07/08/22 12:46 95-50-107/07/22 10:4810.0 1.8 1
1,3-Dichlorobenzene ND ug/L 07/08/22 12:46 541-73-107/07/22 10:4810.0 1.6 1
1,4-Dichlorobenzene ND ug/L 07/08/22 12:46 106-46-707/07/22 10:4810.0 1.7 1
3,3'-Dichlorobenzidine ND ug/L 07/08/22 12:46 91-94-107/07/22 10:4820.0 8.1 1
2,4-Dichlorophenol ND ug/L 07/08/22 12:46 120-83-207/07/22 10:4810.0 1.4 1
Diethylphthalate ND ug/L 07/08/22 12:46 84-66-207/07/22 10:4810.0 2.0 1
2,4-Dimethylphenol ND ug/L 07/08/22 12:46 105-67-907/07/22 10:4810.0 1.7 1
Dimethylphthalate ND ug/L 07/08/22 12:46 131-11-307/07/22 10:4810.0 2.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-1 Lab ID:92612736001 Collected:06/30/22 12:30 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/08/22 12:46 84-74-207/07/22 10:4810.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 07/08/22 12:46 534-52-107/07/22 10:4820.0 7.8 1
2,4-Dinitrophenol ND ug/L 07/08/22 12:46 51-28-507/07/22 10:4850.0 26.0 1
2,4-Dinitrotoluene ND ug/L 07/08/22 12:46 121-14-207/07/22 10:4810.0 1.6 1
2,6-Dinitrotoluene ND ug/L 07/08/22 12:46 606-20-207/07/22 10:4810.0 1.7 1
Di-n-octylphthalate ND ug/L 07/08/22 12:46 117-84-0 L107/07/22 10:4810.0 3.9 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/08/22 12:46 117-81-7 L107/07/22 10:486.0 3.7 1
Fluoranthene ND ug/L 07/08/22 12:46 206-44-0 L107/07/22 10:4810.0 2.2 1
Fluorene ND ug/L 07/08/22 12:46 86-73-707/07/22 10:4810.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 07/08/22 12:46 87-68-307/07/22 10:4810.0 1.8 1
Hexachlorobenzene ND ug/L 07/08/22 12:46 118-74-1 L107/07/22 10:4810.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 07/08/22 12:46 77-47-407/07/22 10:4810.0 1.6 1
Hexachloroethane ND ug/L 07/08/22 12:46 67-72-107/07/22 10:4810.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/08/22 12:46 193-39-5 L107/07/22 10:4810.0 2.9 1
Isophorone ND ug/L 07/08/22 12:46 78-59-107/07/22 10:4810.0 1.7 1
1-Methylnaphthalene ND ug/L 07/08/22 12:46 90-12-007/07/22 10:4810.0 2.0 1
2-Methylnaphthalene ND ug/L 07/08/22 12:46 91-57-607/07/22 10:4810.0 1.9 1
2-Methylphenol(o-Cresol)ND ug/L 07/08/22 12:46 95-48-707/07/22 10:4810.0 1.9 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/08/22 12:46 15831-10-407/07/22 10:4810.0 1.2 1
Naphthalene ND ug/L 07/08/22 12:46 91-20-307/07/22 10:4810.0 2.1 1
2-Nitroaniline ND ug/L 07/08/22 12:46 88-74-407/07/22 10:4820.0 3.0 1
3-Nitroaniline ND ug/L 07/08/22 12:46 99-09-207/07/22 10:4820.0 3.8 1
4-Nitroaniline ND ug/L 07/08/22 12:46 100-01-607/07/22 10:4820.0 5.1 1
Nitrobenzene ND ug/L 07/08/22 12:46 98-95-307/07/22 10:4810.0 1.9 1
2-Nitrophenol ND ug/L 07/08/22 12:46 88-75-507/07/22 10:4810.0 1.4 1
4-Nitrophenol ND ug/L 07/08/22 12:46 100-02-707/07/22 10:4850.0 6.6 1
N-Nitrosodimethylamine ND ug/L 07/08/22 12:46 62-75-907/07/22 10:4810.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 07/08/22 12:46 621-64-707/07/22 10:4810.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 07/08/22 12:46 86-30-607/07/22 10:4810.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/08/22 12:46 108-60-107/07/22 10:4810.0 1.2 1
Pentachlorophenol ND ug/L 07/08/22 12:46 87-86-507/07/22 10:4820.0 3.8 1
Phenanthrene ND ug/L 07/08/22 12:46 85-01-8 L107/07/22 10:4810.0 2.0 1
Phenol ND ug/L 07/08/22 12:46 108-95-207/07/22 10:4810.0 1.4 1
Pyrene ND ug/L 07/08/22 12:46 129-00-0 L107/07/22 10:4810.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 07/08/22 12:46 120-82-107/07/22 10:4810.0 1.7 1
2,4,5-Trichlorophenol ND ug/L 07/08/22 12:46 95-95-407/07/22 10:4810.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 07/08/22 12:46 88-06-207/07/22 10:4810.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)83 %07/08/22 12:46 4165-60-007/07/22 10:4810-144 1
2-Fluorobiphenyl (S)70 %07/08/22 12:46 321-60-807/07/22 10:4810-130 1
Terphenyl-d14 (S)105 %07/08/22 12:46 1718-51-007/07/22 10:4834-163 1
Phenol-d6 (S)49 %07/08/22 12:46 13127-88-307/07/22 10:4810-130 1
2-Fluorophenol (S)59 %07/08/22 12:46 367-12-407/07/22 10:4810-130 1
2,4,6-Tribromophenol (S)81 %07/08/22 12:46 118-79-607/07/22 10:4810-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-1 Lab ID:92612736001 Collected:06/30/22 12:30 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 07/02/22 02:41 71-43-20.50 0.34 1
Bromobenzene ND ug/L 07/02/22 02:41 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 07/02/22 02:41 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 07/02/22 02:41 75-27-40.50 0.31 1
Bromoform ND ug/L 07/02/22 02:41 75-25-20.50 0.34 1
Bromomethane ND ug/L 07/02/22 02:41 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 07/02/22 02:41 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 07/02/22 02:41 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 07/02/22 02:41 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 07/02/22 02:41 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 07/02/22 02:41 108-90-70.50 0.28 1
Chloroethane ND ug/L 07/02/22 02:41 75-00-31.0 0.65 1
Chloroform ND ug/L 07/02/22 02:41 67-66-30.50 0.43 1
Chloromethane ND ug/L 07/02/22 02:41 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 07/02/22 02:41 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 07/02/22 02:41 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 07/02/22 02:41 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 07/02/22 02:41 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 07/02/22 02:41 106-93-40.50 0.27 1
Dibromomethane ND ug/L 07/02/22 02:41 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 07/02/22 02:41 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 07/02/22 02:41 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 07/02/22 02:41 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 07/02/22 02:41 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 07/02/22 02:41 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 07/02/22 02:41 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 07/02/22 02:41 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 07/02/22 02:41 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 07/02/22 02:41 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 07/02/22 02:41 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 07/02/22 02:41 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 07/02/22 02:41 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 07/02/22 02:41 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 07/02/22 02:41 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 07/02/22 02:41 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 07/02/22 02:41 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 07/02/22 02:41 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 07/02/22 02:41 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 07/02/22 02:41 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 07/02/22 02:41 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 07/02/22 02:41 1634-04-40.50 0.42 1
Naphthalene ND ug/L 07/02/22 02:41 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 07/02/22 02:41 103-65-10.50 0.34 1
Styrene ND ug/L 07/02/22 02:41 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 07/02/22 02:41 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-1 Lab ID:92612736001 Collected:06/30/22 12:30 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 07/02/22 02:41 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 07/02/22 02:41 127-18-40.50 0.29 1
Toluene ND ug/L 07/02/22 02:41 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene ND ug/L 07/02/22 02:41 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 07/02/22 02:41 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 07/02/22 02:41 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 07/02/22 02:41 79-00-50.50 0.32 1
Trichloroethene 0.75 ug/L 07/02/22 02:41 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 07/02/22 02:41 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 07/02/22 02:41 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 07/02/22 02:41 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 07/02/22 02:41 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 07/02/22 02:41 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 07/02/22 02:41 179601-23-11.0 0.71 1
o-Xylene ND ug/L 07/02/22 02:41 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %07/02/22 02:41 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %07/02/22 02:41 460-00-470-130 1
Toluene-d8 (S)100 %07/02/22 02:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-2 Lab ID:92612736002 Collected:06/30/22 13:25 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3005A
Pace Analytical Services - Peachtree Corners, GA
6020 MET ICPMS
Arsenic 13.1J ug/L 07/08/22 17:45 7440-38-2 D307/06/22 08:0825.0 10.8 1
Barium 110 ug/L 07/08/22 17:45 7440-39-307/06/22 08:0825.0 3.4 1
Cadmium ND ug/L 07/08/22 17:45 7440-43-9 D307/06/22 08:082.5 0.57 1
Chromium 13.7J ug/L 07/08/22 17:45 7440-47-3 D307/06/22 08:0825.0 5.5 1
Lead ND ug/L 07/08/22 17:45 7439-92-1 D307/06/22 08:085.0 4.4 1
Selenium ND ug/L 07/08/22 17:45 7782-49-2 D307/06/22 08:0825.0 6.8 1
Silver ND ug/L 07/08/22 17:45 7440-22-4 D307/06/22 08:0825.0 2.2 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 07/06/22 10:29 7439-97-607/05/22 15:150.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/08/22 13:11 83-32-907/07/22 10:489.1 1.8 1
Acenaphthylene ND ug/L 07/08/22 13:11 208-96-807/07/22 10:489.1 1.8 1
Aniline ND ug/L 07/08/22 13:11 62-53-307/07/22 10:489.1 1.5 1
Anthracene ND ug/L 07/08/22 13:11 120-12-7 L107/07/22 10:489.1 2.1 1
Benzo(a)anthracene ND ug/L 07/08/22 13:11 56-55-3 L107/07/22 10:489.1 2.4 1
Benzo(a)pyrene ND ug/L 07/08/22 13:11 50-32-8 L107/07/22 10:489.1 2.5 1
Benzo(b)fluoranthene ND ug/L 07/08/22 13:11 205-99-2 L107/07/22 10:489.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 07/08/22 13:11 191-24-2 L107/07/22 10:489.1 2.6 1
Benzo(k)fluoranthene ND ug/L 07/08/22 13:11 207-08-9 L107/07/22 10:489.1 2.5 1
Benzoic Acid ND ug/L 07/08/22 13:11 65-85-007/07/22 10:4845.5 20.0 1
Benzyl alcohol ND ug/L 07/08/22 13:11 100-51-607/07/22 10:4818.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 07/08/22 13:11 101-55-3 L107/07/22 10:489.1 1.6 1
Butylbenzylphthalate ND ug/L 07/08/22 13:11 85-68-7 L107/07/22 10:489.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 07/08/22 13:11 59-50-707/07/22 10:489.1 3.0 1
4-Chloroaniline ND ug/L 07/08/22 13:11 106-47-807/07/22 10:4818.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 07/08/22 13:11 111-91-107/07/22 10:489.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/08/22 13:11 111-44-407/07/22 10:489.1 1.7 1
2-Chloronaphthalene ND ug/L 07/08/22 13:11 91-58-707/07/22 10:489.1 1.6 1
2-Chlorophenol ND ug/L 07/08/22 13:11 95-57-807/07/22 10:489.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 07/08/22 13:11 7005-72-307/07/22 10:489.1 1.8 1
Chrysene ND ug/L 07/08/22 13:11 218-01-9 L107/07/22 10:489.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 07/08/22 13:11 53-70-3 L107/07/22 10:489.1 2.7 1
Dibenzofuran ND ug/L 07/08/22 13:11 132-64-907/07/22 10:489.1 1.9 1
1,2-Dichlorobenzene ND ug/L 07/08/22 13:11 95-50-107/07/22 10:489.1 1.6 1
1,3-Dichlorobenzene ND ug/L 07/08/22 13:11 541-73-107/07/22 10:489.1 1.5 1
1,4-Dichlorobenzene ND ug/L 07/08/22 13:11 106-46-707/07/22 10:489.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 07/08/22 13:11 91-94-107/07/22 10:4818.2 7.4 1
2,4-Dichlorophenol ND ug/L 07/08/22 13:11 120-83-207/07/22 10:489.1 1.3 1
Diethylphthalate ND ug/L 07/08/22 13:11 84-66-207/07/22 10:489.1 1.9 1
2,4-Dimethylphenol ND ug/L 07/08/22 13:11 105-67-907/07/22 10:489.1 1.5 1
Dimethylphthalate ND ug/L 07/08/22 13:11 131-11-307/07/22 10:489.1 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-2 Lab ID:92612736002 Collected:06/30/22 13:25 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/08/22 13:11 84-74-207/07/22 10:489.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 07/08/22 13:11 534-52-107/07/22 10:4818.2 7.1 1
2,4-Dinitrophenol ND ug/L 07/08/22 13:11 51-28-507/07/22 10:4845.5 23.6 1
2,4-Dinitrotoluene ND ug/L 07/08/22 13:11 121-14-207/07/22 10:489.1 1.5 1
2,6-Dinitrotoluene ND ug/L 07/08/22 13:11 606-20-207/07/22 10:489.1 1.6 1
Di-n-octylphthalate ND ug/L 07/08/22 13:11 117-84-0 L107/07/22 10:489.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/08/22 13:11 117-81-7 L107/07/22 10:485.5 3.4 1
Fluoranthene ND ug/L 07/08/22 13:11 206-44-0 L107/07/22 10:489.1 2.0 1
Fluorene ND ug/L 07/08/22 13:11 86-73-707/07/22 10:489.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 07/08/22 13:11 87-68-307/07/22 10:489.1 1.6 1
Hexachlorobenzene ND ug/L 07/08/22 13:11 118-74-1 L107/07/22 10:489.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 07/08/22 13:11 77-47-407/07/22 10:489.1 1.4 1
Hexachloroethane ND ug/L 07/08/22 13:11 67-72-107/07/22 10:489.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/08/22 13:11 193-39-5 L107/07/22 10:489.1 2.6 1
Isophorone ND ug/L 07/08/22 13:11 78-59-107/07/22 10:489.1 1.5 1
1-Methylnaphthalene ND ug/L 07/08/22 13:11 90-12-007/07/22 10:489.1 1.8 1
2-Methylnaphthalene ND ug/L 07/08/22 13:11 91-57-607/07/22 10:489.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 07/08/22 13:11 95-48-707/07/22 10:489.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/08/22 13:11 15831-10-407/07/22 10:489.1 1.1 1
Naphthalene ND ug/L 07/08/22 13:11 91-20-307/07/22 10:489.1 1.9 1
2-Nitroaniline ND ug/L 07/08/22 13:11 88-74-407/07/22 10:4818.2 2.7 1
3-Nitroaniline ND ug/L 07/08/22 13:11 99-09-207/07/22 10:4818.2 3.4 1
4-Nitroaniline ND ug/L 07/08/22 13:11 100-01-607/07/22 10:4818.2 4.6 1
Nitrobenzene ND ug/L 07/08/22 13:11 98-95-307/07/22 10:489.1 1.7 1
2-Nitrophenol ND ug/L 07/08/22 13:11 88-75-507/07/22 10:489.1 1.3 1
4-Nitrophenol ND ug/L 07/08/22 13:11 100-02-707/07/22 10:4845.5 6.0 1
N-Nitrosodimethylamine ND ug/L 07/08/22 13:11 62-75-907/07/22 10:489.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 07/08/22 13:11 621-64-707/07/22 10:489.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 07/08/22 13:11 86-30-607/07/22 10:489.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/08/22 13:11 108-60-107/07/22 10:489.1 1.0 1
Pentachlorophenol ND ug/L 07/08/22 13:11 87-86-507/07/22 10:4818.2 3.4 1
Phenanthrene ND ug/L 07/08/22 13:11 85-01-8 L107/07/22 10:489.1 1.8 1
Phenol ND ug/L 07/08/22 13:11 108-95-207/07/22 10:489.1 1.2 1
Pyrene ND ug/L 07/08/22 13:11 129-00-0 L107/07/22 10:489.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 07/08/22 13:11 120-82-107/07/22 10:489.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/08/22 13:11 95-95-407/07/22 10:489.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 07/08/22 13:11 88-06-207/07/22 10:489.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)33 %07/08/22 13:11 4165-60-007/07/22 10:4810-144 1
2-Fluorobiphenyl (S)28 %07/08/22 13:11 321-60-807/07/22 10:4810-130 1
Terphenyl-d14 (S)85 %07/08/22 13:11 1718-51-007/07/22 10:4834-163 1
Phenol-d6 (S)20 %07/08/22 13:11 13127-88-307/07/22 10:4810-130 1
2-Fluorophenol (S)24 %07/08/22 13:11 367-12-407/07/22 10:4810-130 1
2,4,6-Tribromophenol (S)55 %07/08/22 13:11 118-79-607/07/22 10:4810-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-2 Lab ID:92612736002 Collected:06/30/22 13:25 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 07/02/22 03:00 71-43-20.50 0.34 1
Bromobenzene ND ug/L 07/02/22 03:00 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 07/02/22 03:00 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 07/02/22 03:00 75-27-40.50 0.31 1
Bromoform ND ug/L 07/02/22 03:00 75-25-20.50 0.34 1
Bromomethane ND ug/L 07/02/22 03:00 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 07/02/22 03:00 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 07/02/22 03:00 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 07/02/22 03:00 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 07/02/22 03:00 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 07/02/22 03:00 108-90-70.50 0.28 1
Chloroethane ND ug/L 07/02/22 03:00 75-00-31.0 0.65 1
Chloroform ND ug/L 07/02/22 03:00 67-66-30.50 0.43 1
Chloromethane ND ug/L 07/02/22 03:00 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 07/02/22 03:00 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 07/02/22 03:00 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 07/02/22 03:00 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 07/02/22 03:00 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 07/02/22 03:00 106-93-40.50 0.27 1
Dibromomethane ND ug/L 07/02/22 03:00 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 07/02/22 03:00 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 07/02/22 03:00 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 07/02/22 03:00 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 07/02/22 03:00 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 07/02/22 03:00 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 07/02/22 03:00 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 07/02/22 03:00 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 07/02/22 03:00 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 07/02/22 03:00 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 07/02/22 03:00 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 07/02/22 03:00 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 07/02/22 03:00 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 07/02/22 03:00 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 07/02/22 03:00 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 07/02/22 03:00 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 07/02/22 03:00 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 07/02/22 03:00 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 07/02/22 03:00 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 07/02/22 03:00 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 07/02/22 03:00 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 07/02/22 03:00 1634-04-40.50 0.42 1
Naphthalene ND ug/L 07/02/22 03:00 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 07/02/22 03:00 103-65-10.50 0.34 1
Styrene ND ug/L 07/02/22 03:00 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 07/02/22 03:00 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-2 Lab ID:92612736002 Collected:06/30/22 13:25 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 07/02/22 03:00 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 07/02/22 03:00 127-18-40.50 0.29 1
Toluene ND ug/L 07/02/22 03:00 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene ND ug/L 07/02/22 03:00 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 07/02/22 03:00 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 07/02/22 03:00 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 07/02/22 03:00 79-00-50.50 0.32 1
Trichloroethene 3.4 ug/L 07/02/22 03:00 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 07/02/22 03:00 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 07/02/22 03:00 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 07/02/22 03:00 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 07/02/22 03:00 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 07/02/22 03:00 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 07/02/22 03:00 179601-23-11.0 0.71 1
o-Xylene ND ug/L 07/02/22 03:00 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)103 %07/02/22 03:00 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %07/02/22 03:00 460-00-470-130 1
Toluene-d8 (S)100 %07/02/22 03:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-3 Lab ID:92612736003 Collected:06/30/22 14:15 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3005A
Pace Analytical Services - Peachtree Corners, GA
6020 MET ICPMS
Arsenic 15.6J ug/L 07/08/22 17:51 7440-38-2 D307/06/22 08:0825.0 10.8 1
Barium 575 ug/L 07/08/22 17:51 7440-39-307/06/22 08:0825.0 3.4 1
Cadmium ND ug/L 07/08/22 17:51 7440-43-9 D307/06/22 08:082.5 0.57 1
Chromium 374 ug/L 07/08/22 17:51 7440-47-307/06/22 08:0825.0 5.5 1
Lead 21.0 ug/L 07/08/22 17:51 7439-92-107/06/22 08:085.0 4.4 1
Selenium ND ug/L 07/08/22 17:51 7782-49-2 D307/06/22 08:0825.0 6.8 1
Silver ND ug/L 07/08/22 17:51 7440-22-4 D307/06/22 08:0825.0 2.2 1
Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services - Peachtree Corners, GA
7470 Mercury
Mercury ND ug/L 07/06/22 10:31 7439-97-607/05/22 15:150.20 0.13 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Acenaphthene ND ug/L 07/08/22 13:37 83-32-907/07/22 10:489.1 1.8 1
Acenaphthylene ND ug/L 07/08/22 13:37 208-96-807/07/22 10:489.1 1.8 1
Aniline ND ug/L 07/08/22 13:37 62-53-307/07/22 10:489.1 1.5 1
Anthracene ND ug/L 07/08/22 13:37 120-12-7 L107/07/22 10:489.1 2.1 1
Benzo(a)anthracene ND ug/L 07/08/22 13:37 56-55-3 L107/07/22 10:489.1 2.4 1
Benzo(a)pyrene ND ug/L 07/08/22 13:37 50-32-8 L107/07/22 10:489.1 2.5 1
Benzo(b)fluoranthene ND ug/L 07/08/22 13:37 205-99-2 L107/07/22 10:489.1 2.4 1
Benzo(g,h,i)perylene ND ug/L 07/08/22 13:37 191-24-2 L107/07/22 10:489.1 2.6 1
Benzo(k)fluoranthene ND ug/L 07/08/22 13:37 207-08-9 L107/07/22 10:489.1 2.5 1
Benzoic Acid ND ug/L 07/08/22 13:37 65-85-007/07/22 10:4845.5 20.0 1
Benzyl alcohol ND ug/L 07/08/22 13:37 100-51-607/07/22 10:4818.2 2.6 1
4-Bromophenylphenyl ether ND ug/L 07/08/22 13:37 101-55-3 L107/07/22 10:489.1 1.6 1
Butylbenzylphthalate ND ug/L 07/08/22 13:37 85-68-7 L107/07/22 10:489.1 2.9 1
4-Chloro-3-methylphenol ND ug/L 07/08/22 13:37 59-50-707/07/22 10:489.1 3.0 1
4-Chloroaniline ND ug/L 07/08/22 13:37 106-47-807/07/22 10:4818.2 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 07/08/22 13:37 111-91-107/07/22 10:489.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 07/08/22 13:37 111-44-407/07/22 10:489.1 1.7 1
2-Chloronaphthalene ND ug/L 07/08/22 13:37 91-58-707/07/22 10:489.1 1.6 1
2-Chlorophenol ND ug/L 07/08/22 13:37 95-57-807/07/22 10:489.1 1.1 1
4-Chlorophenylphenyl ether ND ug/L 07/08/22 13:37 7005-72-307/07/22 10:489.1 1.8 1
Chrysene ND ug/L 07/08/22 13:37 218-01-9 L107/07/22 10:489.1 2.5 1
Dibenz(a,h)anthracene ND ug/L 07/08/22 13:37 53-70-3 L107/07/22 10:489.1 2.7 1
Dibenzofuran ND ug/L 07/08/22 13:37 132-64-907/07/22 10:489.1 1.9 1
1,2-Dichlorobenzene ND ug/L 07/08/22 13:37 95-50-107/07/22 10:489.1 1.6 1
1,3-Dichlorobenzene ND ug/L 07/08/22 13:37 541-73-107/07/22 10:489.1 1.5 1
1,4-Dichlorobenzene ND ug/L 07/08/22 13:37 106-46-707/07/22 10:489.1 1.5 1
3,3'-Dichlorobenzidine ND ug/L 07/08/22 13:37 91-94-107/07/22 10:4818.2 7.4 1
2,4-Dichlorophenol ND ug/L 07/08/22 13:37 120-83-207/07/22 10:489.1 1.3 1
Diethylphthalate ND ug/L 07/08/22 13:37 84-66-207/07/22 10:489.1 1.9 1
2,4-Dimethylphenol ND ug/L 07/08/22 13:37 105-67-907/07/22 10:489.1 1.5 1
Dimethylphthalate ND ug/L 07/08/22 13:37 131-11-307/07/22 10:489.1 1.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-3 Lab ID:92612736003 Collected:06/30/22 14:15 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C
Pace Analytical Services - Charlotte
8270E RVE
Di-n-butylphthalate ND ug/L 07/08/22 13:37 84-74-207/07/22 10:489.1 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 07/08/22 13:37 534-52-107/07/22 10:4818.2 7.1 1
2,4-Dinitrophenol ND ug/L 07/08/22 13:37 51-28-507/07/22 10:4845.5 23.6 1
2,4-Dinitrotoluene ND ug/L 07/08/22 13:37 121-14-207/07/22 10:489.1 1.5 1
2,6-Dinitrotoluene ND ug/L 07/08/22 13:37 606-20-207/07/22 10:489.1 1.6 1
Di-n-octylphthalate ND ug/L 07/08/22 13:37 117-84-0 L107/07/22 10:489.1 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 07/08/22 13:37 117-81-7 L107/07/22 10:485.5 3.4 1
Fluoranthene ND ug/L 07/08/22 13:37 206-44-0 L107/07/22 10:489.1 2.0 1
Fluorene ND ug/L 07/08/22 13:37 86-73-707/07/22 10:489.1 1.9 1
Hexachloro-1,3-butadiene ND ug/L 07/08/22 13:37 87-68-307/07/22 10:489.1 1.6 1
Hexachlorobenzene ND ug/L 07/08/22 13:37 118-74-1 L107/07/22 10:489.1 2.0 1
Hexachlorocyclopentadiene ND ug/L 07/08/22 13:37 77-47-407/07/22 10:489.1 1.4 1
Hexachloroethane ND ug/L 07/08/22 13:37 67-72-107/07/22 10:489.1 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 07/08/22 13:37 193-39-5 L107/07/22 10:489.1 2.6 1
Isophorone ND ug/L 07/08/22 13:37 78-59-107/07/22 10:489.1 1.5 1
1-Methylnaphthalene ND ug/L 07/08/22 13:37 90-12-007/07/22 10:489.1 1.8 1
2-Methylnaphthalene ND ug/L 07/08/22 13:37 91-57-607/07/22 10:489.1 1.7 1
2-Methylphenol(o-Cresol)ND ug/L 07/08/22 13:37 95-48-707/07/22 10:489.1 1.7 1
3&4-Methylphenol(m&p Cresol)ND ug/L 07/08/22 13:37 15831-10-407/07/22 10:489.1 1.1 1
Naphthalene ND ug/L 07/08/22 13:37 91-20-307/07/22 10:489.1 1.9 1
2-Nitroaniline ND ug/L 07/08/22 13:37 88-74-407/07/22 10:4818.2 2.7 1
3-Nitroaniline ND ug/L 07/08/22 13:37 99-09-207/07/22 10:4818.2 3.4 1
4-Nitroaniline ND ug/L 07/08/22 13:37 100-01-607/07/22 10:4818.2 4.6 1
Nitrobenzene ND ug/L 07/08/22 13:37 98-95-307/07/22 10:489.1 1.7 1
2-Nitrophenol ND ug/L 07/08/22 13:37 88-75-507/07/22 10:489.1 1.3 1
4-Nitrophenol ND ug/L 07/08/22 13:37 100-02-707/07/22 10:4845.5 6.0 1
N-Nitrosodimethylamine ND ug/L 07/08/22 13:37 62-75-907/07/22 10:489.1 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 07/08/22 13:37 621-64-707/07/22 10:489.1 1.2 1
N-Nitrosodiphenylamine ND ug/L 07/08/22 13:37 86-30-607/07/22 10:489.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 07/08/22 13:37 108-60-107/07/22 10:489.1 1.0 1
Pentachlorophenol ND ug/L 07/08/22 13:37 87-86-507/07/22 10:4818.2 3.4 1
Phenanthrene ND ug/L 07/08/22 13:37 85-01-8 L107/07/22 10:489.1 1.8 1
Phenol ND ug/L 07/08/22 13:37 108-95-207/07/22 10:489.1 1.2 1
Pyrene ND ug/L 07/08/22 13:37 129-00-0 L107/07/22 10:489.1 2.0 1
1,2,4-Trichlorobenzene ND ug/L 07/08/22 13:37 120-82-107/07/22 10:489.1 1.6 1
2,4,5-Trichlorophenol ND ug/L 07/08/22 13:37 95-95-407/07/22 10:489.1 1.3 1
2,4,6-Trichlorophenol ND ug/L 07/08/22 13:37 88-06-207/07/22 10:489.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)81 %07/08/22 13:37 4165-60-007/07/22 10:4810-144 1
2-Fluorobiphenyl (S)70 %07/08/22 13:37 321-60-807/07/22 10:4810-130 1
Terphenyl-d14 (S)105 %07/08/22 13:37 1718-51-007/07/22 10:4834-163 1
Phenol-d6 (S)51 %07/08/22 13:37 13127-88-307/07/22 10:4810-130 1
2-Fluorophenol (S)61 %07/08/22 13:37 367-12-407/07/22 10:4810-130 1
2,4,6-Tribromophenol (S)85 %07/08/22 13:37 118-79-607/07/22 10:4810-144 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-3 Lab ID:92612736003 Collected:06/30/22 14:15 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 07/02/22 03:18 71-43-20.50 0.34 1
Bromobenzene ND ug/L 07/02/22 03:18 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 07/02/22 03:18 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 07/02/22 03:18 75-27-40.50 0.31 1
Bromoform ND ug/L 07/02/22 03:18 75-25-20.50 0.34 1
Bromomethane ND ug/L 07/02/22 03:18 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 07/02/22 03:18 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 07/02/22 03:18 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 07/02/22 03:18 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 07/02/22 03:18 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 07/02/22 03:18 108-90-70.50 0.28 1
Chloroethane ND ug/L 07/02/22 03:18 75-00-31.0 0.65 1
Chloroform ND ug/L 07/02/22 03:18 67-66-30.50 0.43 1
Chloromethane ND ug/L 07/02/22 03:18 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 07/02/22 03:18 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 07/02/22 03:18 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 07/02/22 03:18 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 07/02/22 03:18 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 07/02/22 03:18 106-93-40.50 0.27 1
Dibromomethane ND ug/L 07/02/22 03:18 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 07/02/22 03:18 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 07/02/22 03:18 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 07/02/22 03:18 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 07/02/22 03:18 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 07/02/22 03:18 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 07/02/22 03:18 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 07/02/22 03:18 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 07/02/22 03:18 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 07/02/22 03:18 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 07/02/22 03:18 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 07/02/22 03:18 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 07/02/22 03:18 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 07/02/22 03:18 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 07/02/22 03:18 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 07/02/22 03:18 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 07/02/22 03:18 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 07/02/22 03:18 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 07/02/22 03:18 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 07/02/22 03:18 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 07/02/22 03:18 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 07/02/22 03:18 1634-04-40.50 0.42 1
Naphthalene ND ug/L 07/02/22 03:18 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 07/02/22 03:18 103-65-10.50 0.34 1
Styrene ND ug/L 07/02/22 03:18 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 07/02/22 03:18 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 40
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92612736
UAF/71227290
Sample:TW-3 Lab ID:92612736003 Collected:06/30/22 14:15 Received:07/01/22 09:05 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 07/02/22 03:18 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 07/02/22 03:18 127-18-40.50 0.29 1
Toluene ND ug/L 07/02/22 03:18 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene ND ug/L 07/02/22 03:18 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 07/02/22 03:18 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 07/02/22 03:18 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 07/02/22 03:18 79-00-50.50 0.32 1
Trichloroethene 0.48J ug/L 07/02/22 03:18 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 07/02/22 03:18 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 07/02/22 03:18 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 07/02/22 03:18 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 07/02/22 03:18 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 07/02/22 03:18 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 07/02/22 03:18 179601-23-11.0 0.71 1
o-Xylene ND ug/L 07/02/22 03:18 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %07/02/22 03:18 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %07/02/22 03:18 460-00-470-130 1
Toluene-d8 (S)100 %07/02/22 03:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
708819
EPA 3005A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92612736001, 92612736002, 92612736003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3696535
Associated Lab Samples:92612736001, 92612736002, 92612736003
Matrix:Water
AnalyzedMDL
Arsenic ug/L 2.4J 5.0 07/08/22 17:272.2
Barium ug/L ND 5.0 07/08/22 17:270.67
Cadmium ug/L ND 0.50 07/08/22 17:270.11
Chromium ug/L ND 5.0 07/08/22 17:271.1
Lead ug/L ND 1.0 07/08/22 17:270.89
Selenium ug/L ND 5.0 07/08/22 17:271.4
Silver ug/L ND 5.0 07/08/22 17:270.44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3696536LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic ug/L 100100 100 80-120
Barium ug/L 101100 101 80-120
Cadmium ug/L 99.4100 99 80-120
Chromium ug/L 99.0100 99 80-120
Lead ug/L 104100 104 80-120
Selenium ug/L 96.4100 96 80-120
Silver ug/L 101100 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3696594MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92612593001
3696595
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic ug/L 100 100 75-125103 3 20100ND102105
Barium ug/L 100 104 75-125107 2 20100ND117120
Cadmium ug/L 100 103 75-125104 1 20100ND103104
Chromium ug/L 100 107 75-125108 1 20100ND107108
Lead ug/L 100 106 75-125109 3 20100ND106109
Selenium ug/L 100 100 75-125102 2 20100ND100102
Silver ug/L 100 104 75-125106 3 20100ND104107
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
708696
EPA 7470A
EPA 7470A
7470 Mercury
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples:92612736001, 92612736002, 92612736003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3696075
Associated Lab Samples:92612736001, 92612736002, 92612736003
Matrix:Water
AnalyzedMDL
Mercury ug/L ND 0.20 07/06/22 09:300.13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3696076LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury ug/L 2.52.5 98 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3696077MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92609807002
3696078
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury ug/L 2.5 92 75-12589 3 202.5ND 2.4 2.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
708425
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92612736001, 92612736002, 92612736003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3694898
Associated Lab Samples:92612736001, 92612736002, 92612736003
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 07/01/22 22:260.31
1,1,1-Trichloroethane ug/L ND 0.50 07/01/22 22:260.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 07/01/22 22:260.22
1,1,2-Trichloroethane ug/L ND 0.50 07/01/22 22:260.32
1,1-Dichloroethane ug/L ND 0.50 07/01/22 22:260.37
1,1-Dichloroethene ug/L ND 0.50 07/01/22 22:260.35
1,1-Dichloropropene ug/L ND 0.50 07/01/22 22:260.43
1,2,3-Trichlorobenzene ug/L ND 2.0 07/01/22 22:260.81
1,2,3-Trichloropropane ug/L ND 0.50 07/01/22 22:260.26
1,2,4-Trichlorobenzene ug/L ND 2.0 07/01/22 22:260.64
1,2,4-Trimethylbenzene ug/L ND 0.50 07/01/22 22:260.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 07/01/22 22:260.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 07/01/22 22:260.27
1,2-Dichlorobenzene ug/L ND 0.50 07/01/22 22:260.34
1,2-Dichloroethane ug/L ND 0.50 07/01/22 22:260.32
1,2-Dichloropropane ug/L ND 0.50 07/01/22 22:260.36
1,3,5-Trimethylbenzene ug/L ND 0.50 07/01/22 22:260.33
1,3-Dichlorobenzene ug/L ND 0.50 07/01/22 22:260.34
1,3-Dichloropropane ug/L ND 0.50 07/01/22 22:260.28
1,4-Dichlorobenzene ug/L ND 0.50 07/01/22 22:260.33
2,2-Dichloropropane ug/L ND 0.50 07/01/22 22:260.39
2-Chlorotoluene ug/L ND 0.50 07/01/22 22:260.32
4-Chlorotoluene ug/L ND 0.50 07/01/22 22:260.32
Benzene ug/L ND 0.50 07/01/22 22:260.34
Bromobenzene ug/L ND 0.50 07/01/22 22:260.29
Bromochloromethane ug/L ND 0.50 07/01/22 22:260.47
Bromodichloromethane ug/L ND 0.50 07/01/22 22:260.31
Bromoform ug/L ND 0.50 07/01/22 22:260.34
Bromomethane ug/L ND 5.0 07/01/22 22:261.7
Carbon tetrachloride ug/L ND 0.50 07/01/22 22:260.33
Chlorobenzene ug/L ND 0.50 07/01/22 22:260.28
Chloroethane ug/L ND 1.0 07/01/22 22:260.65
Chloroform ug/L ND 0.50 07/01/22 22:260.43
Chloromethane ug/L ND 1.0 07/01/22 22:260.54
cis-1,2-Dichloroethene ug/L ND 0.50 07/01/22 22:260.38
cis-1,3-Dichloropropene ug/L ND 0.50 07/01/22 22:260.36
Dibromochloromethane ug/L ND 0.50 07/01/22 22:260.36
Dibromomethane ug/L ND 0.50 07/01/22 22:260.39
Dichlorodifluoromethane ug/L ND 0.50 07/01/22 22:260.35
Diisopropyl ether ug/L ND 0.50 07/01/22 22:260.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3694898
Associated Lab Samples:92612736001, 92612736002, 92612736003
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 07/01/22 22:260.30
Hexachloro-1,3-butadiene ug/L ND 2.0 07/01/22 22:261.5
Isopropylbenzene (Cumene)ug/L ND 0.50 07/01/22 22:260.33
m&p-Xylene ug/L ND 1.0 07/01/22 22:260.71
Methyl-tert-butyl ether ug/L ND 0.50 07/01/22 22:260.42
Methylene Chloride ug/L ND 2.0 07/01/22 22:262.0
n-Butylbenzene ug/L ND 0.50 07/01/22 22:260.49
n-Propylbenzene ug/L ND 0.50 07/01/22 22:260.34
Naphthalene ug/L ND 2.0 07/01/22 22:260.64
o-Xylene ug/L ND 0.50 07/01/22 22:260.34
sec-Butylbenzene ug/L ND 0.50 07/01/22 22:260.40
Styrene ug/L ND 0.50 07/01/22 22:260.29
tert-Butylbenzene ug/L ND 0.50 07/01/22 22:260.32
Tetrachloroethene ug/L ND 0.50 07/01/22 22:260.29
Toluene ug/L ND 0.50 07/01/22 22:260.48
trans-1,2-Dichloroethene ug/L ND 0.50 07/01/22 22:260.40
trans-1,3-Dichloropropene ug/L ND 0.50 07/01/22 22:260.36
Trichloroethene ug/L ND 0.50 07/01/22 22:260.38
Trichlorofluoromethane ug/L ND 1.0 07/01/22 22:260.30
Vinyl chloride ug/L ND 1.0 07/01/22 22:260.39
1,2-Dichloroethane-d4 (S)%107 70-130 07/01/22 22:26
4-Bromofluorobenzene (S)%93 70-130 07/01/22 22:26
Toluene-d8 (S)%100 70-130 07/01/22 22:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3694899LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.550 111 60-140
1,1,1-Trichloroethane ug/L 48.350 97 60-140
1,1,2,2-Tetrachloroethane ug/L 51.250 102 60-140
1,1,2-Trichloroethane ug/L 48.850 98 60-140
1,1-Dichloroethane ug/L 43.350 87 60-140
1,1-Dichloroethene ug/L 44.150 88 60-140
1,1-Dichloropropene ug/L 47.550 95 60-140
1,2,3-Trichlorobenzene ug/L 49.450 99 60-140
1,2,3-Trichloropropane ug/L 50.450 101 60-140
1,2,4-Trichlorobenzene ug/L 50.750 101 60-140
1,2,4-Trimethylbenzene ug/L 49.650 99 60-140
1,2-Dibromo-3-chloropropane ug/L 52.050 104 60-140
1,2-Dibromoethane (EDB)ug/L 54.250 108 60-140
1,2-Dichlorobenzene ug/L 51.050 102 60-140
1,2-Dichloroethane ug/L 44.250 88 60-140
1,2-Dichloropropane ug/L 47.850 96 60-140
1,3,5-Trimethylbenzene ug/L 49.950 100 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3694899LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 51.350 103 60-140
1,3-Dichloropropane ug/L 49.950 100 60-140
1,4-Dichlorobenzene ug/L 50.350 101 60-140
2,2-Dichloropropane ug/L 45.550 91 60-140
2-Chlorotoluene ug/L 50.050 100 60-140
4-Chlorotoluene ug/L 49.950 100 60-140
Benzene ug/L 46.550 93 60-140
Bromobenzene ug/L 48.750 97 60-140
Bromochloromethane ug/L 45.750 91 60-140
Bromodichloromethane ug/L 50.750 101 60-140
Bromoform ug/L 43.650 87 60-140
Bromomethane ug/L 53.550 107 60-140
Carbon tetrachloride ug/L 53.750 107 60-140
Chlorobenzene ug/L 50.450 101 60-140
Chloroethane ug/L 43.250 86 60-140
Chloroform ug/L 43.750 87 60-140
Chloromethane ug/L 45.250 90 60-140
cis-1,2-Dichloroethene ug/L 44.350 89 60-140
cis-1,3-Dichloropropene ug/L 50.850 102 60-140
Dibromochloromethane ug/L 54.450 109 60-140
Dibromomethane ug/L 52.750 105 60-140
Dichlorodifluoromethane ug/L 34.850 70 60-140
Diisopropyl ether ug/L 45.050 90 60-140
Ethylbenzene ug/L 50.150 100 60-140
Hexachloro-1,3-butadiene ug/L 52.050 104 60-140
Isopropylbenzene (Cumene)ug/L 50.250 100 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 42.650 85 60-140
Methylene Chloride ug/L 44.450 89 60-140
n-Butylbenzene ug/L 51.050 102 60-140
n-Propylbenzene ug/L 48.150 96 60-140
Naphthalene ug/L 51.150 102 60-140
o-Xylene ug/L 51.150 102 60-140
sec-Butylbenzene ug/L 49.650 99 60-140
Styrene ug/L 54.350 109 60-140
tert-Butylbenzene ug/L 42.250 84 60-140
Tetrachloroethene ug/L 51.050 102 60-140
Toluene ug/L 46.650 93 60-140
trans-1,2-Dichloroethene ug/L 43.950 88 60-140
trans-1,3-Dichloropropene ug/L 50.550 101 60-140
Trichloroethene ug/L 51.950 104 60-140
Trichlorofluoromethane ug/L 45.150 90 60-140
Vinyl chloride ug/L 44.150 88 60-140
1,2-Dichloroethane-d4 (S)%87 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3694900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611903001
3694901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 115 60-140115 0 302000ND23002300
1,1,1-Trichloroethane ug/L 2000 108 60-140108 0 302000ND21702160
1,1,2,2-Tetrachloroethane ug/L 2000 108 60-140106 3 302000ND21702120
1,1,2-Trichloroethane ug/L 2000 97 60-140101 5 302000ND19302030
1,1-Dichloroethane ug/L 2000 97 60-14097 1 302000ND19301940
1,1-Dichloroethene ug/L 2000 104 60-140104 0 302000ND20902080
1,1-Dichloropropene ug/L 2000 107 60-140106 1 302000ND21402120
1,2,3-Trichlorobenzene ug/L 2000 98 60-140103 5 302000ND19602050
1,2,3-Trichloropropane ug/L 2000 102 60-140103 1 302000ND20302050
1,2,4-Trichlorobenzene ug/L 2000 102 60-140106 3 302000ND20402110
1,2,4-Trimethylbenzene ug/L 2000 107 60-140109 1 30200099231303170
1,2-Dibromo-3-
chloropropane ug/L 2000 103 60-140103 1 302000ND20502070
1,2-Dibromoethane (EDB)ug/L 2000 113 60-140112 1 302000ND22602240
1,2-Dichlorobenzene ug/L 2000 103 60-140104 0 302000ND20702080
1,2-Dichloroethane ug/L 2000 99 60-14099 0 30200020521802180
1,2-Dichloropropane ug/L 2000 98 60-140105 7 302000ND19702110
1,3,5-Trimethylbenzene ug/L 2000 108 60-140109 1 30200033125002510
1,3-Dichlorobenzene ug/L 2000 106 60-140108 2 302000ND21102150
1,3-Dichloropropane ug/L 2000 104 60-140104 0 302000ND20902080
1,4-Dichlorobenzene ug/L 2000 103 60-140101 2 302000ND20502010
2,2-Dichloropropane ug/L 2000 93 60-14091 2 302000ND18601820
2-Chlorotoluene ug/L 2000 91 60-14093 3 302000ND18201870
4-Chlorotoluene ug/L 2000 102 60-140103 1 302000ND20402060
Benzene ug/L 2000 80 60-140110 5 30200096901130011900
Bromobenzene ug/L 2000 99 60-140102 3 302000ND19902050
Bromochloromethane ug/L 2000 106 60-140109 4 302000ND21102190
Bromodichloromethane ug/L 2000 103 60-140106 3 302000ND20602120
Bromoform ug/L 2000 85 60-14086 0 302000ND17101710
Bromomethane ug/L 2000 110 60-140119 7 302000ND22102370
Carbon tetrachloride ug/L 2000 111 60-140117 5 302000ND22202340
Chlorobenzene ug/L 2000 108 60-140107 1 302000ND21602140
Chloroethane ug/L 2000 96 60-14096 0 302000ND19101910
Chloroform ug/L 2000 94 60-140100 6 302000ND19202030
Chloromethane ug/L 2000 85 60-14093 8 302000ND17101850
cis-1,2-Dichloroethene ug/L 2000 96 60-14099 4 302000ND19201990
cis-1,3-Dichloropropene ug/L 2000 98 60-140102 4 302000ND19502030
Dibromochloromethane ug/L 2000 101 60-140105 4 302000ND20202100
Dibromomethane ug/L 2000 105 60-140110 4 302000ND20902190
Dichlorodifluoromethane ug/L 2000 80 60-14082 3 302000ND16001640
Diisopropyl ether ug/L 2000 92 60-14098 4 302000103028702990
Ethylbenzene ug/L 2000 109 60-140115 3 302000131035003620
Hexachloro-1,3-butadiene ug/L 2000 110 60-140117 6 302000ND22002330
Isopropylbenzene(Cumene)ug/L 2000 106 60-140109 3 30200080.8 2200 2260
m&p-Xylene ug/L 4000 114 60-140119 2 304000348080308230
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3694900MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92611903001
3694901
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 2000 86 60-14095 5 302000183035503740
Methylene Chloride ug/L 2000 85 60-14090 5 302000ND17001800
n-Butylbenzene ug/L 2000 108 60-140111 2 302000ND21702220
n-Propylbenzene ug/L 2000 102 60-140105 2 30200018122302270
Naphthalene ug/L 2000 101 60-140107 5 30200046324802610
o-Xylene ug/L 2000 115 60-140116 1 302000121035103530
sec-Butylbenzene ug/L 2000 108 60-140109 1 302000ND21602170
Styrene ug/L 2000 110 60-140111 0 302000ND22302240
tert-Butylbenzene ug/L 2000 91 60-14090 1 302000ND18201800
Tetrachloroethene ug/L 2000 112 60-140112 1 302000ND22302250
Toluene ug/L 2000 93 60-140109 5 302000404059006230
trans-1,2-Dichloroethene ug/L 2000 98 60-140102 4 302000ND19702040
trans-1,3-Dichloropropene ug/L 2000 99 60-140100 1 302000ND19701990
Trichloroethene ug/L 2000 110 60-140111 1 302000ND22002230
Trichlorofluoromethane ug/L 2000 90 60-14091 0 302000ND18101820
Vinyl chloride ug/L 2000 103 60-140102 1 302000ND20602040
1,2-Dichloroethane-d4 (S)%89 70-13091
4-Bromofluorobenzene (S)%102 70-130104
Toluene-d8 (S)%96 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
709032
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92612736001, 92612736002, 92612736003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3697504
Associated Lab Samples:92612736001, 92612736002, 92612736003
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 07/08/22 10:361.7
1,2-Dichlorobenzene ug/L ND 10.0 07/08/22 10:361.8
1,3-Dichlorobenzene ug/L ND 10.0 07/08/22 10:361.6
1,4-Dichlorobenzene ug/L ND 10.0 07/08/22 10:361.7
1-Methylnaphthalene ug/L ND 10.0 07/08/22 10:362.0
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 07/08/22 10:361.2
2,4,5-Trichlorophenol ug/L ND 10.0 07/08/22 10:361.4
2,4,6-Trichlorophenol ug/L ND 10.0 07/08/22 10:361.6
2,4-Dichlorophenol ug/L ND 10.0 07/08/22 10:361.4
2,4-Dimethylphenol ug/L ND 10.0 07/08/22 10:361.7
2,4-Dinitrophenol ug/L ND 50.0 07/08/22 10:3626.0
2,4-Dinitrotoluene ug/L ND 10.0 07/08/22 10:361.6
2,6-Dinitrotoluene ug/L ND 10.0 07/08/22 10:361.7
2-Chloronaphthalene ug/L ND 10.0 07/08/22 10:361.7
2-Chlorophenol ug/L ND 10.0 07/08/22 10:361.2
2-Methylnaphthalene ug/L ND 10.0 07/08/22 10:361.9
2-Methylphenol(o-Cresol)ug/L ND 10.0 07/08/22 10:361.9
2-Nitroaniline ug/L ND 20.0 07/08/22 10:363.0
2-Nitrophenol ug/L ND 10.0 07/08/22 10:361.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 07/08/22 10:361.2
3,3'-Dichlorobenzidine ug/L ND 20.0 07/08/22 10:368.1
3-Nitroaniline ug/L ND 20.0 07/08/22 10:363.8
4,6-Dinitro-2-methylphenol ug/L ND 20.0 07/08/22 10:367.8
4-Bromophenylphenyl ether ug/L ND 10.0 07/08/22 10:361.8
4-Chloro-3-methylphenol ug/L ND 10.0 07/08/22 10:363.3
4-Chloroaniline ug/L ND 20.0 07/08/22 10:363.6
4-Chlorophenylphenyl ether ug/L ND 10.0 07/08/22 10:362.0
4-Nitroaniline ug/L ND 20.0 07/08/22 10:365.1
4-Nitrophenol ug/L ND 50.0 07/08/22 10:366.6
Acenaphthene ug/L ND 10.0 07/08/22 10:362.0
Acenaphthylene ug/L ND 10.0 07/08/22 10:362.0
Aniline ug/L ND 10.0 07/08/22 10:361.6
Anthracene ug/L ND 10.0 07/08/22 10:362.3
Benzo(a)anthracene ug/L ND 10.0 07/08/22 10:362.7
Benzo(a)pyrene ug/L ND 10.0 07/08/22 10:362.8
Benzo(b)fluoranthene ug/L ND 10.0 07/08/22 10:362.6
Benzo(g,h,i)perylene ug/L ND 10.0 07/08/22 10:362.8
Benzo(k)fluoranthene ug/L ND 10.0 07/08/22 10:362.7
Benzoic Acid ug/L ND 50.0 07/08/22 10:3622.0
Benzyl alcohol ug/L ND 20.0 07/08/22 10:362.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3697504
Associated Lab Samples:92612736001, 92612736002, 92612736003
Matrix:Water
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/L ND 10.0 07/08/22 10:361.8
bis(2-Chloroethyl) ether ug/L ND 10.0 07/08/22 10:361.9
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 07/08/22 10:363.7
Butylbenzylphthalate ug/L ND 10.0 07/08/22 10:363.1
Chrysene ug/L ND 10.0 07/08/22 10:362.8
Di-n-butylphthalate ug/L ND 10.0 07/08/22 10:362.2
Di-n-octylphthalate ug/L ND 10.0 07/08/22 10:363.9
Dibenz(a,h)anthracene ug/L ND 10.0 07/08/22 10:363.0
Dibenzofuran ug/L ND 10.0 07/08/22 10:362.1
Diethylphthalate ug/L ND 10.0 07/08/22 10:362.0
Dimethylphthalate ug/L ND 10.0 07/08/22 10:362.1
Fluoranthene ug/L ND 10.0 07/08/22 10:362.2
Fluorene ug/L ND 10.0 07/08/22 10:362.1
Hexachloro-1,3-butadiene ug/L ND 10.0 07/08/22 10:361.8
Hexachlorobenzene ug/L ND 10.0 07/08/22 10:362.2
Hexachlorocyclopentadiene ug/L ND 10.0 07/08/22 10:361.6
Hexachloroethane ug/L ND 10.0 07/08/22 10:361.4
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 07/08/22 10:362.9
Isophorone ug/L ND 10.0 07/08/22 10:361.7
N-Nitroso-di-n-propylamine ug/L ND 10.0 07/08/22 10:361.3
N-Nitrosodimethylamine ug/L ND 10.0 07/08/22 10:361.9
N-Nitrosodiphenylamine ug/L ND 10.0 07/08/22 10:363.0
Naphthalene ug/L ND 10.0 07/08/22 10:362.1
Nitrobenzene ug/L ND 10.0 07/08/22 10:361.9
Pentachlorophenol ug/L ND 20.0 07/08/22 10:363.8
Phenanthrene ug/L ND 10.0 07/08/22 10:362.0
Phenol ug/L ND 10.0 07/08/22 10:361.4
Pyrene ug/L ND 10.0 07/08/22 10:362.2
2,4,6-Tribromophenol (S)%75 10-144 07/08/22 10:36
2-Fluorobiphenyl (S)%63 10-130 07/08/22 10:36
2-Fluorophenol (S)%46 10-130 07/08/22 10:36
Nitrobenzene-d5 (S)%72 10-144 07/08/22 10:36
Phenol-d6 (S)%35 10-130 07/08/22 10:36
Terphenyl-d14 (S)%114 34-163 07/08/22 10:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3697505LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 34.250 68 18-130
1,2-Dichlorobenzene ug/L 26.050 52 20-130
1,3-Dichlorobenzene ug/L 23.250 46 18-130
1,4-Dichlorobenzene ug/L 24.650 49 18-130
1-Methylnaphthalene ug/L 42.750 85 29-130
2,2'-Oxybis(1-chloropropane)ug/L 36.450 73 28-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
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Page 33 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3697505LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/L 50.150 100 35-130
2,4,6-Trichlorophenol ug/L 49.050 98 31-130
2,4-Dichlorophenol ug/L 44.150 88 35-130
2,4-Dimethylphenol ug/L 50.850 102 34-130
2,4-Dinitrophenol ug/L 204250 82 10-153
2,4-Dinitrotoluene ug/L 55.550 111 37-136
2,6-Dinitrotoluene ug/L 51.850 104 33-136
2-Chloronaphthalene ug/L 46.750 93 26-130
2-Chlorophenol ug/L 40.750 81 37-130
2-Methylnaphthalene ug/L 41.250 82 29-130
2-Methylphenol(o-Cresol)ug/L 38.850 78 35-130
2-Nitroaniline ug/L 98.6100 99 37-130
2-Nitrophenol ug/L 43.550 87 32-130
3&4-Methylphenol(m&p Cresol)ug/L 37.250 74 34-130
3,3'-Dichlorobenzidine ug/L 108100 108 34-136
3-Nitroaniline ug/L 106100 106 37-138
4,6-Dinitro-2-methylphenol ug/L 104100 104 21-157
4-Bromophenylphenyl ether ug/L 67.0 L15013438-130
4-Chloro-3-methylphenol ug/L 92.8100 93 37-130
4-Chloroaniline ug/L 86.8100 87 38-130
4-Chlorophenylphenyl ether ug/L 57.350 115 33-130
4-Nitroaniline ug/L 104100 104 42-137
4-Nitrophenol ug/L 141250 56 10-130
Acenaphthene ug/L 48.550 97 33-130
Acenaphthylene ug/L 47.050 94 35-130
Aniline ug/L 34.650 69 22-130
Anthracene ug/L 70.2 L15014048-130
Benzo(a)anthracene ug/L 83.3 L15016748-137
Benzo(a)pyrene ug/L 84.5 L15016949-138
Benzo(b)fluoranthene ug/L 83.7 L15016752-138
Benzo(g,h,i)perylene ug/L 85.6 L15017148-140
Benzo(k)fluoranthene ug/L 88.4 L15017748-139
Benzoic Acid ug/L 69.6250 28 10-130
Benzyl alcohol ug/L 79.6100 80 35-130
bis(2-Chloroethoxy)methane ug/L 44.450 89 34-130
bis(2-Chloroethyl) ether ug/L 41.750 83 36-130
bis(2-Ethylhexyl)phthalate ug/L 84.7 L15016932-165
Butylbenzylphthalate ug/L 85.3 L15017134-161
Chrysene ug/L 87.1 L15017447-131
Di-n-butylphthalate ug/L 69.450 139 39-144
Di-n-octylphthalate ug/L 90.4 L15018130-170
Dibenz(a,h)anthracene ug/L 88.5 L15017749-138
Dibenzofuran ug/L 52.650 105 33-130
Diethylphthalate ug/L 51.550 103 38-131
Dimethylphthalate ug/L 49.150 98 37-130
Fluoranthene ug/L 78.2 L15015646-137
Fluorene ug/L 57.950 116 37-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
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Huntersville, NC 28078
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Page 34 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3697505LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/L 27.250 54 11-130
Hexachlorobenzene ug/L 72.2 L15014438-130
Hexachlorocyclopentadiene ug/L 39.050 78 10-130
Hexachloroethane ug/L 21.650 43 14-130
Indeno(1,2,3-cd)pyrene ug/L 88.5 L15017741-130
Isophorone ug/L 46.750 93 33-130
N-Nitroso-di-n-propylamine ug/L 45.550 91 36-130
N-Nitrosodimethylamine ug/L 35.550 71 34-130
N-Nitrosodiphenylamine ug/L 53.450 107 37-130
Naphthalene ug/L 35.550 71 30-130
Nitrobenzene ug/L 45.350 91 36-130
Pentachlorophenol ug/L 123100 123 23-149
Phenanthrene ug/L 70.1 L15014044-130
Phenol ug/L 24.150 48 18-130
Pyrene ug/L 84.1 L15016847-134
2,4,6-Tribromophenol (S)%101 10-144
2-Fluorobiphenyl (S)%82 10-130
2-Fluorophenol (S)%59 10-130
Nitrobenzene-d5 (S)%87 10-144
Phenol-d6 (S)%48 10-130
Terphenyl-d14 (S)%142 34-163
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3699118MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441001
3699119
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L R1502110-13037 55 3050ND10.5 18.4
1,2-Dichlorobenzene ug/L 50 17 10-13027 3050ND8.6J 13.4
1,3-Dichlorobenzene ug/L 50 16 10-13024 3050ND7.8J 11.9
1,4-Dichlorobenzene ug/L 50 16 10-13026 3050ND8.1J 13.0
1-Methylnaphthalene ug/L R1502910-13045 45 3050ND14.3 22.7
2,2'-Oxybis(1-
chloropropane)
ug/L R1502512-14236 38 3050ND12.3 18.0
2,4,5-Trichlorophenol ug/L 50 51 10-14360 15 3050ND25.6 29.8
2,4,6-Trichlorophenol ug/L 50 45 10-14761 29 3050ND22.7 30.3
2,4-Dichlorophenol ug/L R1503610-13853 37 3050ND18.2 26.6
2,4-Dimethylphenol ug/L R1504425-13062 34 3050ND21.9 30.8
2,4-Dinitrophenol ug/L 250 39 10-16537 4 30250ND96.3 92.8
2,4-Dinitrotoluene ug/L 50 48 29-14856 15 3050ND24.0 28.0
2,6-Dinitrotoluene ug/L 50 59 26-14664 8 3050ND29.3 31.8
2-Chloronaphthalene ug/L R1503811-13053 32 3050ND19.2 26.5
2-Chlorophenol ug/L R1503210-13347 38 3050ND16.1 23.6
2-Methylnaphthalene ug/L R1502813-13045 45 3050ND14.1 22.4
2-Methylphenol(o-Cresol)ug/L R1503120-13046 40 3050ND15.3 22.9
2-Nitroaniline ug/L 100 58 24-13665 12 30100ND57.8 64.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
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[phone]
Page 35 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3699118MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441001
3699119
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitrophenol ug/L R1503610-15353 38 3050ND18.1 26.7
3&4-Methylphenol(m&p
Cresol)ug/L R1502916-13044 41 3050ND14.6 22.0
3,3'-Dichlorobenzidine ug/L 100 78 10-15363 22 30100ND78.1 62.8
3-Nitroaniline ug/L 100 64 22-15162 4 30100ND64.5 61.8
4,6-Dinitro-2-methylphenol ug/L 100 74 10-18064 14 30100ND74.1 64.2
4-Bromophenylphenyl ether ug/L 50 68 25-13069 0 3050ND34.2 34.4
4-Chloro-3-methylphenol ug/L 100 42 25-13353 24 30100ND41.8 53.1
4-Chloroaniline ug/L R11003114-13247 40 30100ND31.2 46.6
4-Chlorophenylphenyl ether ug/L 50 48 19-13056 15 3050ND24.1 28.1
4-Nitroaniline ug/L 100 73 29-15060 19 30100ND73.0 60.3
4-Nitrophenol ug/L 250 33 10-13031 8 30250ND82.6 76.3
Acenaphthene ug/L 50 39 16-13051 27 3050ND19.5 25.6
Acenaphthylene ug/L 50 40 15-13752 27 3050ND19.8 25.9
Aniline ug/L R1502610-13039 41 3050ND12.9 19.6
Anthracene ug/L 50 71 37-13662 13 3050ND35.5 31.2
Benzo(a)anthracene ug/L 50 94 40-14572 27 3050ND47.2 36.1
Benzo(a)pyrene ug/L R1509941-14673 31 3050ND49.7 36.5
Benzo(b)fluoranthene ug/L 50 95 39-15174 24 3050ND47.3 37.0
Benzo(g,h,i)perylene ug/L 50 97 40-14772 29 3050ND48.3 36.2
Benzo(k)fluoranthene ug/L R1509840-14671 32 3050ND49.1 35.6
Benzoic Acid ug/L M1250910-13011 30250NDND26.5J
Benzyl alcohol ug/L R11003325-13051 42 30100ND33.3 51.0
bis(2-
Chloroethoxy)methane
ug/L R1503523-13050 34 3050ND17.7 25.0
bis(2-Chloroethyl) ether ug/L R1503425-13050 39 3050ND16.9 24.9
bis(2-Ethylhexyl)phthalate ug/L 50 111 28-16682 30 3050ND55.6 41.0
Butylbenzylphthalate ug/L 50 120 33-16594 24 3050ND60.1 47.0
Chrysene ug/L R1509338-14167 33 3050ND46.7 33.3
Di-n-butylphthalate ug/L 50 99 32-15377 26 3050ND49.5 38.3
Di-n-octylphthalate ug/L 50 109 30-17583 27 3050ND54.5 41.5
Dibenz(a,h)anthracene ug/L R1509339-14868 31 3050ND46.3 33.9
Dibenzofuran ug/L 50 44 20-13054 21 3050ND21.9 27.1
Diethylphthalate ug/L 50 71 28-14264 11 3050ND35.5 31.9
Dimethylphthalate ug/L 50 56 26-13660 6 3050ND28.2 29.9
Fluoranthene ug/L 50 88 39-14367 27 3050ND43.9 33.6
Fluorene ug/L 50 48 24-13256 15 3050ND24.2 28.2
Hexachloro-1,3-butadiene ug/L 50 15 10-13028 3050ND7.3J 14.2
Hexachlorobenzene ug/L 50 72 29-13069 5 3050ND36.0 34.3
Hexachlorocyclopentadiene ug/L R1502510-13045 55 3050ND12.7 22.3
Hexachloroethane ug/L 50 13 10-13020 3050ND6.3J 10J
Indeno(1,2,3-cd)pyrene ug/L R1509839-14871 31 3050ND48.8 35.6
Isophorone ug/L R1503723-13052 33 3050ND18.7 26.0
N-Nitroso-di-n-propylamine ug/L R1503625-13051 36 3050ND17.8 25.6
N-Nitrosodimethylamine ug/L R1502622-13043 47 3050ND13.2 21.3
N-Nitrosodiphenylamine ug/L 50 65 26-13464 1 3050ND32.3 31.9
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
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Huntersville, NC 28078
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Page 36 of 40
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92612736
UAF/71227290
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3699118MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92613441001
3699119
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Naphthalene ug/L R1502414-13039 47 3050ND12.2 19.7
Nitrobenzene ug/L R1503825-13054 35 3050ND18.9 27.0
Pentachlorophenol ug/L 100 77 10-17565 18 30100ND77.0 64.6
Phenanthrene ug/L 50 78 36-13368 14 3050ND38.9 33.8
Phenol ug/L 50 18 10-13031 3050ND9.1J 15.4
Pyrene ug/L 50 108 40-14383 26 3050ND53.9 41.5
2,4,6-Tribromophenol (S)%79 10-14472
2-Fluorobiphenyl (S)%36 10-13045
2-Fluorophenol (S)%24 10-13037
Nitrobenzene-d5 (S)%39 10-14452
Phenol-d6 (S)%18 10-13030
Terphenyl-d14 (S)%115 34-16386
REPORT OF LABORATORY ANALYSIS
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Page 37 of 40
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92612736
UAF/71227290
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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Page 38 of 40
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92612736
UAF/71227290
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92612736001 708819 708917TW-1 EPA 3005A EPA 6020B
92612736002 708819 708917TW-2 EPA 3005A EPA 6020B
92612736003 708819 708917TW-3 EPA 3005A EPA 6020B
92612736001 708696 708827TW-1 EPA 7470A EPA 7470A
92612736002 708696 708827TW-2 EPA 7470A EPA 7470A
92612736003 708696 708827TW-3 EPA 7470A EPA 7470A
92612736001 709032 709366TW-1 EPA 3510C EPA 8270E
92612736002 709032 709366TW-2 EPA 3510C EPA 8270E
92612736003 709032 709366TW-3 EPA 3510C EPA 8270E
92612736001 708425TW-1 SM 6200B
92612736002 708425TW-2 SM 6200B
92612736003 708425TW-3 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 07/11/2022 12:17 PM
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[phone]
Page 39 of 40
Page 40 of 40