27017_Stateville Rd_Environmental Services Rpt Update_20181221

December 21, 2018 Mr. Chris Varela First Citizens Bank & Trust Company 4300 Six Forks Road FCB Mail Code: FCC52 Raleigh, North Carolina 27609 Reference: Report of Environmental Services - Vaughn Gittin Jr. Motorsports 8718 Statesville Road Charlotte, Mecklenburg County, North Carolina RIMS No. 18-019638-01-2 ECS Project: 49:8122-A Dear Mr. Varela: ECS Southeast, LLP (ECS) is pleased to provide First Citizens Bank & Trust Company with the results of our groundwater assessment for the above-referenced site. ECS’s services were provided in accordance with ECS proposal No. 49-12291P authorized on November 27, 2018. ECS appreciates the opportunity to provide our services to you. If there are questions regarding this report, or a need for further information, please contact us. Respectfully submitted, ECS SOUTHEAST, LLP
Shaun Andrew Brewer Christopher D. Orrell, P.G.
Assistant Staff Project Manager Staff Project Manager
[e-mail] [e-mail]
980-242-9916 704-525-51525
Matthew H. McDuffie, P. G.
Principal Geologist
[e-mail]
704-525-5152
Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
1

TABLE OF CONTENTS
1.0 PROJECT INFORMATION .................................................................................................................... 1
2.0 SCOPE OF SERVICES ............................................................................................................................ 3
3.0 RESULTS .............................................................................................................................................. 5
4.0 CONCLUSIONS .................................................................................................................................... 6
5.0 RECOMMENDATIONS ......................................................................................................................... 6
6.0 QUALIFICATIONS OF REPORT ............................................................................................................. 7
FIGURES Figure 1 Site Topographic Map Figure 2 Site Features Map Figure 3 Sample Location Map TABLES Table 1 Summary of Soil Analytical Results Table 2 Summary of Groundwater Analytical Results APPENDICES Appendix A Site Photograph Log Appendix B Laboratory Analytical Data and Chain of Custody (COC) Record
Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
1

1.0 PROJECT INFORMATION

The subject site is located at 8718 Statesville Road in Charlotte, Mecklenburg County, North Carolina
(Figures 1 and 2). The approximate 4.99-acre site currently is identified by the Mecklenburg County
Geographic Information System (GIS) website as Parcel Identification Number (PIN) 02502203 and
owned by RJH Investments LLC. The subject property is currently developed with an approximate 5,880-
square foot building that was constructed in 1971; an approximate 7,000-square foot building that was
constructed in 1974; an approximate 15,300-square foot building that was constructed in 1978; and two
approximate 7,500-square foot buildings that were constructed in 1987. The buildings are occupied by
auto repair businesses, a lawn care business, and a motorsports fabrication business which includes
storage space and offices.

A Phase I Environmental Site Assessment (ESA) was previously completed by ECS on October 19, 2018
(ECS Project No. 49-7927). The findings of the Phase I ESA identified the following Recognized
Environmental Conditions (RECs):

• Based on the current use of the subject property, ECS considers the potential for an
undocumented release at the subject property to be a REC of the subject property.
• ECS observed an apparent septic tank system located on the western portion of the subject
property. According to the property owner, Mr. Ron Hutcherson, there are approximately 5 or 6
septic tank systems at the subject property. He indicated that a septic tank services each
building. There is the potential for waste oil and other fluids associated with the auto repair
businesses to discharge into the septic system and drain field. ECS considers the potential for a
release from the septic tanks to impact the subject property to be a REC of the subject property.
• Based on the distance from the subject property and length of service, ECS considers the
potential for an undocumented release migrating on to the subject site from the southern
adjoining automotive repair facility to be a REC of the subject property.
• ECS considers the potential for migration from the documented release involving the Parker Nall
Well SWHS listing (solvent-impacted water supply well on the south adjoining property) to be a
REC of the subject property.
• ECS considers the potential for migration from the documented release associated with the
Alterman Transport Lines, Inc. (west adjacent property) LUST incident to be a REC of the subject
property.

The following Historical Recognized Environmental Condition (HREC) was identified during this
assessment:

• ECS considers the RJH Enterprises LUST listing associated with a former heating oil UST to be a
HREC of the subject property.

The following Business Environmental Risks (BERs) were identified during this assessment:

• ECS considers the potential for asbestos containing materials, lead in drinking water, lead based
paint, mold, and wetlands at the subject property to be BERs for the subject site.

Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
2

As part of a pending real estate transaction, ECS was contracted to conduct additional assessment to
determine whether the RECs and HRECs identified in the Phase I ESA have impacted the subject
property. Project information is based on correspondence between Mr. Varela with First Citizens Bank,
Mrs. Erika Frey of ECS, and the previously cited Phase I ESA report.

On November 8, 2018, ECS conducted a ground penetration radar survey (GPR) to locate potential septic
tanks and drain fields and collected soil and groundwater samples from the subject site. The GPR survey
confirmed the apparent septic tank system located on the western portion of the subject site identified
during the Phase I ESA as well as an additional septic system located on the southern portion of the
subject site. Four soil borings, SB-1 through SB-4, and three groundwater borings for temporary
groundwater monitoring wells, TW-1 through TW-3, were advance at the site. The borings were located
in the vicinity of the possible drain fields associated with the septic tank systems. The soil and
groundwater samples were submitted to Prism Laboratories for analysis for volatile organic compounds
(VOCs), semi-volatile organic compounds (SVOCs), and Resource Conservation and Recovery Act (RCEA)
Metals using EPA Methods 8260, 8270, and 6010, respectively.

Laboratory analysis of soil samples SB-1, SB-3, and SB-4 detected several VOCs and SVOCs at
concentration above laboratory reporting limits but below their respective Preliminary Soil Remediation
Goals (PSRGs) for residential and industrial/commercial sites. An estimated concentration of isophorone
and a concentration of ¾-methylphenol were reported at a concentration above its protection of
groundwater PSRG in soil sample SB-1. Concentrations of VOCS and SVOCS were not detected above
the laboratory reporting limit in the soil sample SB-2.

Laboratory analysis of each of the soil samples SB-1 through SB-4 detected concentrations of several
RCRA metals above laboratory reporting limits.

• Laboratory analysis of soil samples SB-1, SB-2, and SB-4 reported concentrations of arsenic
above its residential PSRG but below its protection of groundwater PSRG. Laboratory analysis of
soil sample SB-3 reported arsenic at a concentration above its residential and
industrial/commercial PSRG but below its protection of groundwater PSRG.
• Laboratory analysis of soil samples SB-2, SB-3, and SB-4 reported concentrations of total
chromium above its protection of groundwater, residential, and industrial/commercial PSRG.
Laboratory analysis of soil sample SB-1 reported total chromium at a concentration above its
protection of groundwater and residential PSRG but below its industrial/commercial PSRG.
• Laboratory analysis of soil sample SB-2 reported selenium at a concentration above its
protection of groundwater PSRG but below its residential and industrial/commercial PSRG.

Laboratory analysis of the groundwater sample collected from temporary monitoring wells TW-2 and
TW-3 detected several targeted VOCs at concentrations above laboratory reporting limits. Benzene was
detected in the groundwater sample collected from temporary monitoring well TW-2 at a concentration
(2 micrograms per liter (µg/l)) above its North Carolina 2L Groundwater Quality Standard (NC2LGWQS)
(1µg/l) but below its groundwater screening level for vapor intrusion (GWSL) at residential and non-
residential sites. Acetone, a common laboratory contaminant, was detected in the groundwater sample
collected from temporary monitoring wells TW-1 and TW-3 at concentrations below its NC2LGWQS.

Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
3

Several RCRA metals were detected in the groundwater samples collected from temporary monitoring
wells TW-1 through TW-3 at concentrations above the laboratory reporting limit but below their
respective NC2LGWQS. Concentrations of targeted SVOCs were not detected above the laboratory
reporting limit in the groundwater samples collected from each of the temporary monitoring wells.

ECS noted that the buildings on-site reportedly utilize an active private water supply well and are not
connected to municipal water or sanitary sewer. Additionally, the site contains numerous ASTs which
were used to contain heating oil. In 2008, a 1,000-gallon heating oil UST and approximately 30.33 tons
of petroleum-impacted soil was excavated. Confirmatory soil samples were collected from the base and
the side was of the excavation. The soil samples did not exceed the soil to groundwater standard for the
targeted constituents. No groundwater or surface water samples were collected for this assessment. On
July 17, 2018, the NCDEQ issued this facility a letter of No Further Action. According to the letter the soil
contamination did not exceed the lower of the soil to groundwater or residential maximum soil
contaminant concentrations (MSCCs). The source of the release is undetermined and warrants further
investigation.

ECS has been requested to conduct additional assessment activities in an effort to investigate the
contaminant exceedances at the subject site.

2.0 SCOPE OF SERVICES

The environmental assessment included the collection of soil and groundwater samples, the completion
of a relative temporary monitoring well survey, and the submittal of the previously collected soil
samples for analysis of hexavalent chromium. Drilling activities were conducted using a Geoprobe® drill
rig. The drilling subcontractor used for this assessment was 3D Environmental Investigations, LLC (3D).
Drilling and sampling were conducted on December 3, 2018. A photographic log documenting the field
sampling activities is provided in Appendix A.

2.1 Public Utility Locate
Prior to commencing with field activities, ECS contacted North Carolina One-Call to locate/mark public
utilities at the site. Required separation distances between subsurface activities and marked utilities
(typically 30-inches) were maintained during the field activities.

2.2 Monitoring Well Permit
Prior to commencing with field activities, ECS obtained a monitoring well permit from the Mooresville
Regional office of the North Carolina Department of Environmental Quality (NCDEQ). In accordance
with the NCDEQ permit, the GW-1 and GW-30 forms (well construction and well abandonment forms)
were submitted to the NCDEQ. The GW-1 and GW-30 forms were completed by the North Carolina
certified well driller.

2.3 Private Utility Locate
The private utility locate was conducted by Priority Underground Utility Locate across the subject
property as North Carolina One-Call does not mark private utilities.

Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
4

2.4 Soil Boring Activities
Three soil borings, SB-5, BKG-1, and BKG-2, was advanced at the site in the vicinity of the former soil
boring SB-1 and in two discrete background locations. The boring/sample locations are depicted on
Figure 3.

The soil borings were advanced by hydraulically driving a five-foot long, 1.5-inch diameter soil sampling
probe into the soil to a depth of 15 feet below the ground surface (bgs). Continuous soil samples were
collected from the soil borings using a soil sampling probe lined with a dedicated disposable clear plastic
tube. After the soil sampling probe was driven, the clear plastic tube filled with soil was removed from
the probe and cut open to expose the soil. ECS visually classified the soil collected and screened the soil
samples for relative levels of volatile organic vapors using a photoionization detector (PID). Soil samples
were collected from the bottom of the boring (10-15 feet bgs) of SB-5 in an effort to vertically delineate
the previously identified soil impacts. Soil samples were collected at random from the two background
boring locations (BKG-1 and BKG-2).

2.5 Temporary Monitoring Well Installation Activities
After soil sampling activities were complete, three borings were advanced to the water table for the
installation of temporary monitoring wells. Temporary monitoring well TW-4 was advanced in the vicinity
of the former TW-2 boring while TW-5 and TW-6 were advanced in more central locations of the site. The
locations of the temporary groundwater monitoring wells are shown on Figure 3.

The temporary monitoring wells were installed in boreholes drilled using a Geoprobe® in a manner
consistent with the borings described above. The temporary wells were constructed with one-inch inside
diameter Schedule 40 PVC flush-threaded casing and screen. Temporary monitoring wells TW-4 through
TW-6 were set to a total depth of 30 feet bgs. A fifteen-foot length of slotted well screen with machined
0.010-inch slot widths and a threaded bottom plug was installed at the bottom of each well. The screens
were installed to a depth that intercepted the groundwater surface, as estimated during drilling, or at the
top of drilling refusal.

Upon the completion of the temporary monitoring well installation activities, a top of casing (TOC) survey
was conducted in an effort to determine the relative direction of groundwater flow across the site.

Following the completion of the groundwater sampling and surveying, the temporary monitoring wells were
removed and the borings were properly abandoned.

2.6 Soil and Groundwater Sample Collection
The soil samples were collected by a sampler wearing dedicated disposable nitrile gloves from the clear
plastic tubes retrieved from the soil sample probe. New sleeves were used for each sample. The soil
samples were placed directly into laboratory provided containers.

Groundwater was purged and sampled subsequent to being pumped to the surface using a peristaltic
pump with dedicated disposable polyethylene tubing lowered through the temporary monitoring well
casing. Groundwater samples were placed directly into laboratory prepared containers at each sample
location.

Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
5

The soil and groundwater sample containers were labeled with ECS project number, sample
identification, sample date and time, and requested analytical analysis. The containers were placed into
a cooler with ice to maintain the samples at approximately 4° Celsius. The soil and groundwater samples
were submitted to Prism Laboratories for analysis. The soil sample collected from SB-5 was submitted
for analysis of semi-volatile organic compounds (SVOCs) using EPA Method 8270, while the two
background soil samples (BKG-1 and BKG-2) were submitted for analysis of arsenic and selenium using
EPA Method 6010. The groundwater samples were submitted for laboratory analysis of volatile organic
compounds (VOCs) and SVOCs using EPA Methods 8260 and 8270.

Additionally, the previously collected soil samples SB-1 through SB-4 were re-submitted for laboratory
analysis of hexavalent chromium using EPA Method 7199.
3.0 RESULTS
3.1 Soil Analytical Results
Laboratory analysis of the soil sample collected from SB-2 detected hexavalent chromium at an
estimated concentration of 0.48 mg/kg which is above the NCDEQ Residential Health Based PSRG of
0.31 mg/kg. Hexavalent chromium was detected in each of the other soil borings at estimated
concentrations below the NCDEQ Residential Health Based PSRG.

Arsenic was detected at a concentration of 6.2 mg/kg is the soil sample collected from BKG-1 which is
above the NCDEQ Industrial/Commercial Health Based PSRG of 3.0 mg/kg and the NCDEQ Protection of
Groundwater PSRG of 5.8 mg/kg. Arsenic was detected at a concentration of 4.2 mg/kg in the soil
sample collected from BKG-2 which is above the Industrial/Commercial Health Based PSRG but below
the Protection of Groundwater PSRG. Selenium was detected at concentrations ranging from 5.1 mg/kg
(BKG-2) to 5.6 mg/kg (BKG-2) which is above the Protection of Groundwater PSRG of 2.1 mg/kg, but
below the Residential Health Based PSRG of 78 mg/kg.

Laboratory analysis of the soil sample collected from SB-5 detected ¾-methylnaphthalene at an
estimated concentration of 0.13 mg/kg, which is below the NCDEQ Protection of Groundwater and
Residential Health Based PSRGs of 17 mg/kg and 1,300 mg/kg.

A summary of the soil analytical results are provided on Table 1. The laboratory data sheets are included
in Appendix B.

3.2 Groundwater Analytical Results
Laboratory analysis of each of the groundwater samples (TW-4 through TW-6) detected
tetrachloroethylene, a chlorinated solvent, at concentrations ranging from 0.98 ug/L (TW-6) to 6.8 ug/L
(TW-5), which is above the NC2LGWQS of 0.7 ug/L, but below the NCDEQ Residential Vapor Intrusion
Screening Level (VISL) Groundwater Screening Level (GWSL) of 12 ug/L.

Additionally, several other VOCs were detected in the groundwater sample collected from TW-6 at
concentrations exceeding their respective NCDEQ Residential VISL GWSLs and NC2LGWQSs.

Acetone, a common laboratory contaminant, was detected at a concentration below its applicable
standards in the groundwater sample collected from TW-5.
Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
6

4.0 CONCLUSIONS

Based on the results of the environmental assessment, ECS concludes the following:

• It appears that the soil impacts previously identified in SB-1 have been vertically delineated to
below the applicable screening levels at a depth of 10-15 feet via the soil sample collected from
SB-5.
• Based on the consistency of the detections of arsenic and selenium in the background soil
samples collected (BKG-1 and BKG-2) to that of the soil samples previously collected, the
detections of arsenic and selenium appear to be consistent with naturally occurring
concentrations of arsenic and selenium.
• Based on the detection of hexavalent chromium in the soil sample collected from SB-2 at a
concentration exceeding the NCDEQ Residential Health Based PSRG but below the Protection of
Groundwater and Industrial/Commercial Health Based PSRG, it appears that the site has been
impacted where the soil sample was collected.
• Based on the results of the relative site survey, groundwater appears to be flowing to the south-
southeast.
• Based on the detections of tetrachloroethylene in each of the wells, and various other VOCs in
the anticipated upgradient well at concentrations exceeding their applicable NC2LGWQSs and
NCDEQ Residential VISL GWSLs (but below the NCDEQ Non-Residential VISL GWSLs), it appears
that groundwater at the site has been impacted by either onsite operations or a potential
upgradient source.

5.0 RECOMMENDATIONS

Based on the results of the environmental assessment, ECS recommends the following:

• ECS understands that based on the detections of contaminants in soil and groundwater at the
site, a reporting obligation to the NCDEQ may exist. ECS recommends a copy of this report be
submitted to the property owner and they consult legal counsel regarding potential reporting
obligations.
• ECS does not recommend additional assessment of the arsenic and selenium detections at the
site.
• Based on the proposed commercial/industrial redevelopment activities, it does not appear that
additional assessment is warranted for the identified soil impacts.

Report of Environmental Assessment - Vaughn Gittin Jr. Motorsport
Charlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No. 49:8122-A
7

6.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this environmental assessment are consistent with those normally employed in environmental soil and groundwater assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information determined during previous environmental assessments and the data obtained during our field activities. This report was prepared for the express use of First Citizens Bank & Trust Company. Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract.
FIGURES
FIGURE 1
SITE TOPOGRAPHIC MAP
8718 Statesville RoadCharlotte, Mecklenburg County, North Carolina
RIMS No. 18-019638-01-2
ECS Project No: 49:8122-A
SOURCE:
USGS TOPOGRAPHIC MAPDERITA, NC QUADRANGLE 2016
SCALE:AS SHOWN
SITE
LEGEND
Approximate Subject Property
Boundary
LEGEND
FIGURE 2
SITE FEATURES MAP
8718 Statesville Road
Charlotte, Mecklenburg County, North CarolinaRIMS No. 18-019638-01-2
ECS Project No: 49:8122-A-A
Approximate Subject Property Boundary
Approximate AST Location
Approximate Septic Drain Field Location
SOURCE:
GOOGLE EARTH IMAGEDATED 2018
SCALE:AS SHOWN
LEGEND
SOURCE:
GOOGLE EARTH IMAGEDATED 2018
SCALE:AS SHOWN
FIGURE 3
SAMPLE LOCATION MAP
8718 Statesville Road
Charlotte, Mecklenburg County, North CarolinaRIMS No. 18-019638-01-2
ECS Project No: 49:8122-A
TW-4
TW-5 TW-6
Approximate Background Sample Location
Approximate Groundwater Sample
Location
BKG-2
BKG-1
Approximate Groundwater Flow Direction
Approximate Subject Property Boundary
TABLES
TABLE 1: SUMMARY OF SOIL ANALYTICAL RESULTS
VAUGHN GITTIN JR MOTORSPORT
8718 STATESVILLE ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-8122-A

Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 BKG-1 BKG-2
Sample Depth (ft)5-10'5-10'5-5.5'7.5-8.5'10-15'5-10'5-5.5'
Collection Date
3/4-Methylphenol 2.7 BRL BRL BRL 0.13 J BRL BRL 17 1,300 16,000
Arsenic 2.5 2.2 3.1 1.9 NA 6.2 4.2 5.8 0.68 3.0
Hexavalent Chromium 0.1 J 0.48 J 0.23 J 0.07 J NA NA NA 3.8 0.31 6.5
Selenium 1.6 2.1 0.93 1.1 NA 5.6 5.1 2.1 78 1,200
Notes:
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
NCDEQ PSRG = North Carolina Department of Environmental Quality Preliminary Soil Remediation Goals as of February 2018

Bold = Denotes exceedances above the NCDEQ PSRG for Residential soil
BOLD UNDERLINE = Denotes exceedances above or equal to the NCDEQ PSRG for Industrial/Commercial soil
Italics = Denotes exceedances above the Protection of Groundwater PSRG
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration
ft = feet
12/3/18
Semi-Volatile Organic Compounds by EPA Method 8270
ANALYTICAL RESULTS
Resource Conservation and Recovery Act (RCRA) Metals by EPA Method 6010
Residential Health
Based PSRG
Industrial/Commercial
Health Based PSRG
COMPARISON CRITERIA
Protection of
Groundwater
PSRG11/8/18
TABLE 2: SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
VAUGHN GITTIN JR MOTORSPORT
8718 STATESVILLE ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-8122-A
Sample ID TW-4 TW-5 TW-6
Collection Date
Targeted SVOCs BRL BRL BRL ---
Acetone BRL 5.1 BRL 6,000 4,500,000 19,000,000
1,1,2-Trichloroethane BRL BRL 4.0 NS 1.2 5.2
1,1-Dichloroethane BRL BRL 9.7 6 76 330
1,1-Dichloroethylene BRL BRL 8.2 7 39 160
1,2-Dichloroethane BRL BRL 0.93 0.4 22 98
Methyl-tert-Butyl Ether BRL BRL 1.9 20 4,500 20,000
Tetrachloroethylene 1.3 6.8 0.98 0.7 12 48
Trichloroethylene BRL BRL 2.2 3 1 4.4
Notes:
Results presented in milligrams per kilogram (ug/L), analogous to parts per billion (ppb)
NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013
NCDEQ = North Carolina Department of Environmental Quality
BRL = Below Reporting Limits
VISL GWSL = Vapor Intrustion Screening Levels Groundwater Screening Level as of February 2018
Bold denotes an exceedance of the NC2LGWQS
Italics denotes an exceedance of the Residential VISL GWSL
Underline denotes an exceedance of the Industrial VISL GWSL
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration
NE = Not Established
Volatile Organic Compounds (VOCs) By EPA Method 8260B
NCDEQ NON-
RESIDENTIAL VISL
GWSL
NC2LGWQS NCDEQ RESIDENTIAL
VISL GWSL
ANALYTICAL RESULTS
11/8/18
Semi-Volatile Organic Compounds (SVOCs) By EPA Method 8270
APPENDIX A
PHOTOGRAPHIC LOG
VAUGHN GITTINS JR MOTORSPORT
8718 STATESVILLE ROAD
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-8122-A
Photograph 1: General view of TW-4 formerly TW-2 location looking toward the southeast
Photograph 2: General view of TW-5 location looking toward the northwest
APPENDIX B
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
12/17/2018
ECS Carolinas, LLP (Charlotte)
Shaun Brewer
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: Vaughn Grittin Jr.
Lab Submittal Date: 11/09/2018
Prism Work Order: 8110180
Method 7199analysis was subcontracted to ALS Global. Laboratory report is attached.
Narrative Notes:
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Angela D. Overcash
VP Laboratory Services
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Data Qualifiers Key Reference:
A Analyte detected in MB, due to contaminated DI water. Samples not prepped in lab unaffected.
Aa The ICV response factor is below the method recommended guidance criteria. The analyte is not detected down to
the MDL.
B Analyte is found in the associated blank at a concentration >1/2 RL.
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
D RPD value outside of the control limits.
ICV ICV result is above the control limits. Analyte not detected in the sample. No further action taken.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L Parameter reported with possible low bias. LCS recovery below the QC limit.
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
LH High LCS recovery. Analyte not detected in the sample(s). No further action taken.
SR Surrogate recovery outside the QC limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Receipt Summary
12/17/2018
Prism Work Order: 8110180
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
8110180-01 11/08/18 10:15SB-1 11/09/18 15:00Solid
8110180-02 11/08/18 11:25SB-2 11/09/18 15:00Solid
8110180-03 11/08/18 12:20SB-3 11/09/18 15:00Solid
8110180-04 11/08/18 12:50SB-4 11/09/18 15:00Solid
8110180-05 11/08/18 14:15TW-1 11/09/18 15:00Water
8110180-06 11/08/18 14:35TW-2 11/09/18 15:00Water
8110180-07 11/08/18 15:05TW-3 11/09/18 15:00Water
Samples were received in good condition at 2.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8110180
12/17/2018
Summary of Detections
2.7 mg/kg dry8110180-01 SB-1 3/4-Methylphenol 8270D
0.44 J mg/kg dry8110180-01 SB-1 Isophorone 8270D
2.5 mg/kg dry8110180-01 SB-1 Arsenic *6010D
86 mg/kg dry8110180-01 SB-1 Barium *6010D
5.1 mg/kg dry8110180-01 SB-1 Chromium *6010D
6.7 mg/kg dry8110180-01 SB-1 Lead *6010D
1.6 mg/kg dry8110180-01 SB-1 Selenium *6010D
0.083 mg/kg dry8110180-01 SB-1 Acetone 8260B
2.2 mg/kg dry8110180-02 SB-2 Arsenic *6010D
38 mg/kg dry8110180-02 SB-2 Barium *6010D
42 mg/kg dry8110180-02 SB-2 Chromium *6010D
5.2 mg/kg dry8110180-02 SB-2 Lead *6010D
2.1 mg/kg dry8110180-02 SB-2 Selenium *6010D
0.038 mg/kg dry8110180-03 SB-3 Mercury *7471B
3.1 mg/kg dry8110180-03 SB-3 Arsenic *6010D
37 mg/kg dry8110180-03 SB-3 Barium *6010D
37 mg/kg dry8110180-03 SB-3 Chromium *6010D
4.4 mg/kg dry8110180-03 SB-3 Lead *6010D
0.93 mg/kg dry8110180-03 SB-3 Selenium *6010D
0.061 mg/kg dry8110180-03 SB-3 Acetone 8260B
0.14 J mg/kg dry8110180-04 SB-4 Benzoic Acid 8270D
1.9 mg/kg dry8110180-04 SB-4 Arsenic *6010D
39 mg/kg dry8110180-04 SB-4 Barium *6010D
36 mg/kg dry8110180-04 SB-4 Chromium *6010D
4.0 mg/kg dry8110180-04 SB-4 Lead *6010D
1.1 mg/kg dry8110180-04 SB-4 Selenium *6010D
0.0088 mg/kg dry8110180-04 SB-4 4-Isopropyltoluene 8260B
0.042 mg/kg dry8110180-04 SB-4 Acetone 8260B
0.75 mg/L8110180-05 TW-1 Barium *6010D
0.052 mg/L8110180-05 TW-1 Chromium *6010D
11 ug/L8110180-05 TW-1 Acetone 8260B
0.048 mg/L8110180-06 TW-2 Arsenic *6010D
3.6 mg/L8110180-06 TW-2 Barium *6010D
0.71 mg/L8110180-06 TW-2 Chromium *6010D
0.031 mg/L8110180-06 TW-2 Lead *6010D
2.0 ug/L8110180-06 TW-2 Benzene 8260B
1.1 ug/L8110180-06 TW-2 m,p-Xylenes 8260B
0.37 J ug/L8110180-06 TW-2 Methyl Isobutyl Ketone 8260B
0.51 ug/L8110180-06 TW-2 Methyl-tert-Butyl Ether 8260B
0.96 ug/L8110180-06 TW-2 o-Xylene 8260B
0.76 ug/L8110180-06 TW-2 Toluene 8260B
2.1 ug/L8110180-06 TW-2 Xylenes, total 8260B
0.35 mg/L8110180-07 TW-3 Barium *6010D
0.028 mg/L8110180-07 TW-3 Chromium *6010D
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8110180
12/17/2018
Summary of Detections
5.6 ug/L8110180-07 TW-3 Acetone 8260B
2.8 ug/L8110180-07 TW-3 cis-1,2-Dichloroethylene 8260B
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-1
Prism Sample ID: 8110180-01
Prism Work Order: 8110180
Time Collected: 11/08/18 10:15
Time Submitted: 11/09/18 15:00
General Chemistry Parameters
69.6 *SM2540 G P8K021910.100 11/12/18 16:00 TJY% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0741,2,4-Trichlorobenzene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0721,2-Dichlorobenzene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0671,3-Dichlorobenzene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0691,4-Dichlorobenzene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0911-Methylnaphthalene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0892,4,6-Trichlorophenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0912,4-Dichlorophenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0722,4-Dimethylphenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0662,4-Dinitrophenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0572,4-Dinitrotoluene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0632,6-Dinitrotoluene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0682-Chloronaphthalene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0672-Chlorophenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0762-Methylnaphthalene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0612-Methylphenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0862-Nitrophenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVICVmg/kg dry 0.0933,3’-Dichlorobenzidine
2.7 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0583/4-Methylphenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0714,6-Dinitro-2-methylphenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0814-Bromophenyl phenyl ether
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0664-Chloro-3-methylphenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0574-Chloroaniline
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0614-Chlorophenyl phenyl ether
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.0734-Nitrophenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.064Acenaphthene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.068Acenaphthylene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.076Anthracene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.062Azobenzene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.062Benzo(a)anthracene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.051Benzo(a)pyrene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.055Benzo(b)fluoranthene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.052Benzo(g,h,i)perylene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.062Benzo(k)fluoranthene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.040Benzoic Acid
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.062Benzyl alcohol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.082bis(2-Chloroethoxy)methane
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.067Bis(2-Chloroethyl)ether
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.081Bis(2-chloroisopropyl)ether
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.070Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-1
Prism Sample ID: 8110180-01
Prism Work Order: 8110180
Time Collected: 11/08/18 10:15
Time Submitted: 11/09/18 15:00
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.067Butyl benzyl phthalate
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.060Chrysene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.058Dibenzo(a,h)anthracene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.072Dibenzofuran
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.065Diethyl phthalate
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.062Dimethyl phthalate
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.067Di-n-butyl phthalate
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.058Di-n-octyl phthalate
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.060Fluoranthene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.068Fluorene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.075Hexachlorobenzene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.085Hexachlorobutadiene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.084Hexachlorocyclopentadiene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.079Hexachloroethane
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.054Indeno(1,2,3-cd)pyrene
0.44 8270D P8K024910.47 11/15/18 23:31 JMVJmg/kg dry 0.064Isophorone
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.076Naphthalene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.067Nitrobenzene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVAamg/kg dry 0.074N-Nitroso-di-n-propylamine
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.072N-Nitrosodiphenylamine
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.056Pentachlorophenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.061Phenanthrene
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.070Phenol
BRL 8270D P8K024910.47 11/15/18 23:31 JMVmg/kg dry 0.063Pyrene
Surrogate Recovery Control Limits
39-13260 %2,4,6-Tribromophenol
44-11588 %2-Fluorobiphenyl
35-11570 %2-Fluorophenol
37-12275 %Nitrobenzene-d5
34-12166 %Phenol-d5
54-12786 %Terphenyl-d14
Total Metals
BRL *7471B P8K026810.028 11/15/18 13:32 MMRmg/kg dry 0.0026Mercury
2.5 *6010D P8K021310.72 11/13/18 19:42 JABmg/kg dry 0.044Arsenic
86 *6010D P8K021310.72 11/13/18 19:42 JABmg/kg dry 0.10Barium
BRL *6010D P8K021310.36 11/13/18 19:42 JABmg/kg dry 0.0096Cadmium
5.1 *6010D P8K021310.36 11/13/18 19:42 JABmg/kg dry 0.060Chromium
6.7 *6010D P8K021310.36 11/13/18 19:42 JABmg/kg dry 0.067Lead
1.6 *6010D P8K021310.72 11/13/18 19:42 JABmg/kg dry 0.17Selenium
BRL *6010D P8K021310.36 11/13/18 19:42 JABmg/kg dry 0.0089Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000611,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-1
Prism Sample ID: 8110180-01
Prism Work Order: 8110180
Time Collected: 11/08/18 10:15
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000361,1,1-Trichloroethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000501,1,2,2-Tetrachloroethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000651,1,2-Trichloroethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000201,1-Dichloroethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000331,1-Dichloroethylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000401,1-Dichloropropylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000421,2,3-Trichlorobenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000941,2,3-Trichloropropane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000551,2,4-Trichlorobenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000561,2,4-Trimethylbenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000301,2-Dibromoethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000351,2-Dichlorobenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000441,2-Dichloroethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000461,2-Dichloropropane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000561,3,5-Trimethylbenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000491,3-Dichlorobenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000371,3-Dichloropropane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000291,4-Dichlorobenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000352,2-Dichloropropane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000382-Chlorotoluene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000444-Chlorotoluene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.000364-Isopropyltoluene
0.083 8260B P8K027610.074 11/15/18 17:57 ANGmg/kg dry 0.0018Acetone
BRL 8260B P8K027610.0044 11/15/18 17:57 ANGmg/kg dry 0.00043Benzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00061Bromobenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00041Bromochloromethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00041Bromodichloromethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00084Bromoform
BRL 8260B P8K027610.015 11/15/18 17:57 ANGmg/kg dry 0.00091Bromomethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00037Carbon Tetrachloride
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00039Chlorobenzene
BRL 8260B P8K027610.015 11/15/18 17:57 ANGmg/kg dry 0.00061Chloroethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00053Chloroform
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00050Chloromethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00031cis-1,2-Dichloroethylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00025cis-1,3-Dichloropropylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00030Dibromochloromethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00033Dichlorodifluoromethane
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00028Ethylbenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00030Isopropyl Ether
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00044Isopropylbenzene (Cumene)
BRL 8260B P8K027610.015 11/15/18 17:57 ANGmg/kg dry 0.00068m,p-Xylenes
BRL 8260B P8K027610.074 11/15/18 17:57 ANGmg/kg dry 0.00067Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-1
Prism Sample ID: 8110180-01
Prism Work Order: 8110180
Time Collected: 11/08/18 10:15
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.15 11/15/18 17:57 ANGmg/kg dry 0.00067Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8K027610.074 11/15/18 17:57 ANGmg/kg dry 0.00063Methyl Isobutyl Ketone
BRL 8260B P8K027610.015 11/15/18 17:57 ANGmg/kg dry 0.00041Methylene Chloride
BRL 8260B P8K027610.015 11/15/18 17:57 ANGmg/kg dry 0.00024Methyl-tert-Butyl Ether
BRL 8260B P8K027610.015 11/15/18 17:57 ANGmg/kg dry 0.00023Naphthalene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00038n-Butylbenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00044n-Propylbenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00030o-Xylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00036sec-Butylbenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00044Styrene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00025tert-Butylbenzene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00035Tetrachloroethylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00042Toluene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00044trans-1,2-Dichloroethylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00039trans-1,3-Dichloropropylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00048Trichloroethylene
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00048Trichlorofluoromethane
BRL 8260B P8K027610.037 11/15/18 17:57 ANGmg/kg dry 0.0010Vinyl acetate
BRL 8260B P8K027610.0074 11/15/18 17:57 ANGmg/kg dry 0.00036Vinyl chloride
BRL 8260B P8K027610.022 11/15/18 17:57 ANGmg/kg dry 0.0014Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
84-123109 %Dibromofluoromethane
76-129102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-2
Prism Sample ID: 8110180-02
Prism Work Order: 8110180
Time Collected: 11/08/18 11:25
Time Submitted: 11/09/18 15:00
General Chemistry Parameters
69.9 *SM2540 G P8K021910.100 11/12/18 16:00 TJY% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0741,2,4-Trichlorobenzene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0721,2-Dichlorobenzene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0661,3-Dichlorobenzene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0691,4-Dichlorobenzene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0911-Methylnaphthalene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0882,4,6-Trichlorophenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0912,4-Dichlorophenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0722,4-Dimethylphenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0662,4-Dinitrophenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0572,4-Dinitrotoluene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0632,6-Dinitrotoluene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0682-Chloronaphthalene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0672-Chlorophenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0752-Methylnaphthalene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0602-Methylphenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0862-Nitrophenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVCCVmg/kg dry 0.0933,3’-Dichlorobenzidine
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0583/4-Methylphenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0714,6-Dinitro-2-methylphenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0814-Bromophenyl phenyl ether
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0664-Chloro-3-methylphenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0574-Chloroaniline
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0614-Chlorophenyl phenyl ether
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.0734-Nitrophenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.064Acenaphthene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.068Acenaphthylene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.076Anthracene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.062Azobenzene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.062Benzo(a)anthracene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.051Benzo(a)pyrene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.055Benzo(b)fluoranthene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.052Benzo(g,h,i)perylene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.062Benzo(k)fluoranthene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.040Benzoic Acid
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.062Benzyl alcohol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.082bis(2-Chloroethoxy)methane
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.067Bis(2-Chloroethyl)ether
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.081Bis(2-chloroisopropyl)ether
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.070Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-2
Prism Sample ID: 8110180-02
Prism Work Order: 8110180
Time Collected: 11/08/18 11:25
Time Submitted: 11/09/18 15:00
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.067Butyl benzyl phthalate
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.059Chrysene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.057Dibenzo(a,h)anthracene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.072Dibenzofuran
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.065Diethyl phthalate
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.062Dimethyl phthalate
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.067Di-n-butyl phthalate
BRL 8270D P8K029910.47 11/16/18 13:29 JMVCCVmg/kg dry 0.058Di-n-octyl phthalate
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.060Fluoranthene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.068Fluorene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.075Hexachlorobenzene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.085Hexachlorobutadiene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.084Hexachlorocyclopentadiene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.079Hexachloroethane
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.054Indeno(1,2,3-cd)pyrene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.064Isophorone
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.076Naphthalene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.067Nitrobenzene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVAamg/kg dry 0.074N-Nitroso-di-n-propylamine
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.072N-Nitrosodiphenylamine
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.056Pentachlorophenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.061Phenanthrene
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.070Phenol
BRL 8270D P8K029910.47 11/16/18 13:29 JMVmg/kg dry 0.062Pyrene
Surrogate Recovery Control Limits
39-13254 %2,4,6-Tribromophenol
44-11575 %2-Fluorobiphenyl
35-11571 %2-Fluorophenol
37-12261 %Nitrobenzene-d5
34-12166 %Phenol-d5
54-12760 %Terphenyl-d14
Total Metals
BRL *7471B P8K026810.028 11/15/18 13:36 MMRmg/kg dry 0.0027Mercury
2.2 *6010D P8K021310.72 11/13/18 19:51 JABmg/kg dry 0.044Arsenic
38 *6010D P8K021310.72 11/13/18 19:51 JABmg/kg dry 0.10Barium
BRL *6010D P8K021310.36 11/13/18 19:51 JABmg/kg dry 0.0096Cadmium
42 *6010D P8K021310.36 11/13/18 19:51 JABmg/kg dry 0.060Chromium
5.2 *6010D P8K021310.36 11/13/18 19:51 JABmg/kg dry 0.067Lead
2.1 *6010D P8K021310.72 11/13/18 19:51 JABmg/kg dry 0.17Selenium
BRL *6010D P8K021310.36 11/13/18 19:51 JABmg/kg dry 0.0089Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000721,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-2
Prism Sample ID: 8110180-02
Prism Work Order: 8110180
Time Collected: 11/08/18 11:25
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000431,1,1-Trichloroethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000591,1,2,2-Tetrachloroethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000781,1,2-Trichloroethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000241,1-Dichloroethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000391,1-Dichloroethylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000481,1-Dichloropropylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000501,2,3-Trichlorobenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00111,2,3-Trichloropropane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000651,2,4-Trichlorobenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000671,2,4-Trimethylbenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000351,2-Dibromoethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000411,2-Dichlorobenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000521,2-Dichloroethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000541,2-Dichloropropane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000661,3,5-Trimethylbenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000581,3-Dichlorobenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000441,3-Dichloropropane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000351,4-Dichlorobenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000422,2-Dichloropropane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000452-Chlorotoluene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000524-Chlorotoluene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.000424-Isopropyltoluene
BRL 8260B P8K027610.088 11/15/18 18:25 ANGmg/kg dry 0.0021Acetone
BRL 8260B P8K027610.0053 11/15/18 18:25 ANGmg/kg dry 0.00051Benzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00073Bromobenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00048Bromochloromethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00049Bromodichloromethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.0010Bromoform
BRL 8260B P8K027610.018 11/15/18 18:25 ANGmg/kg dry 0.0011Bromomethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00044Carbon Tetrachloride
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00047Chlorobenzene
BRL 8260B P8K027610.018 11/15/18 18:25 ANGmg/kg dry 0.00073Chloroethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00063Chloroform
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00059Chloromethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00037cis-1,2-Dichloroethylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00030cis-1,3-Dichloropropylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00036Dibromochloromethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00040Dichlorodifluoromethane
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00034Ethylbenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00036Isopropyl Ether
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00052Isopropylbenzene (Cumene)
BRL 8260B P8K027610.018 11/15/18 18:25 ANGmg/kg dry 0.00081m,p-Xylenes
BRL 8260B P8K027610.088 11/15/18 18:25 ANGmg/kg dry 0.00079Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-2
Prism Sample ID: 8110180-02
Prism Work Order: 8110180
Time Collected: 11/08/18 11:25
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.18 11/15/18 18:25 ANGmg/kg dry 0.00079Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8K027610.088 11/15/18 18:25 ANGmg/kg dry 0.00075Methyl Isobutyl Ketone
BRL 8260B P8K027610.018 11/15/18 18:25 ANGmg/kg dry 0.00049Methylene Chloride
BRL 8260B P8K027610.018 11/15/18 18:25 ANGmg/kg dry 0.00028Methyl-tert-Butyl Ether
BRL 8260B P8K027610.018 11/15/18 18:25 ANGmg/kg dry 0.00028Naphthalene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00045n-Butylbenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00052n-Propylbenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00036o-Xylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00043sec-Butylbenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00053Styrene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00030tert-Butylbenzene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00042Tetrachloroethylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00050Toluene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00053trans-1,2-Dichloroethylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00046trans-1,3-Dichloropropylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00057Trichloroethylene
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00057Trichlorofluoromethane
BRL 8260B P8K027610.044 11/15/18 18:25 ANGmg/kg dry 0.0012Vinyl acetate
BRL 8260B P8K027610.0088 11/15/18 18:25 ANGmg/kg dry 0.00043Vinyl chloride
BRL 8260B P8K027610.026 11/15/18 18:25 ANGmg/kg dry 0.0016Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
84-123110 %Dibromofluoromethane
76-129102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-3
Prism Sample ID: 8110180-03
Prism Work Order: 8110180
Time Collected: 11/08/18 12:20
Time Submitted: 11/09/18 15:00
General Chemistry Parameters
77.8 *SM2540 G P8K028410.100 11/14/18 14:56 TJY% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0661,2,4-Trichlorobenzene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0641,2-Dichlorobenzene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0601,3-Dichlorobenzene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0621,4-Dichlorobenzene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0821-Methylnaphthalene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0792,4,6-Trichlorophenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0822,4-Dichlorophenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0652,4-Dimethylphenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0592,4-Dinitrophenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0512,4-Dinitrotoluene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0562,6-Dinitrotoluene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0612-Chloronaphthalene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0602-Chlorophenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0682-Methylnaphthalene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0542-Methylphenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0772-Nitrophenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVICVmg/kg dry 0.0843,3’-Dichlorobenzidine
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0523/4-Methylphenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0644,6-Dinitro-2-methylphenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0734-Bromophenyl phenyl ether
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0594-Chloro-3-methylphenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0514-Chloroaniline
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0554-Chlorophenyl phenyl ether
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.0654-Nitrophenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.058Acenaphthene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.061Acenaphthylene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.068Anthracene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.056Azobenzene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.055Benzo(a)anthracene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.046Benzo(a)pyrene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.049Benzo(b)fluoranthene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.046Benzo(g,h,i)perylene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.056Benzo(k)fluoranthene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.036Benzoic Acid
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.056Benzyl alcohol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.073bis(2-Chloroethoxy)methane
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.060Bis(2-Chloroethyl)ether
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.072Bis(2-chloroisopropyl)ether
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.063Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-3
Prism Sample ID: 8110180-03
Prism Work Order: 8110180
Time Collected: 11/08/18 12:20
Time Submitted: 11/09/18 15:00
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.060Butyl benzyl phthalate
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.053Chrysene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.052Dibenzo(a,h)anthracene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.064Dibenzofuran
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.058Diethyl phthalate
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.056Dimethyl phthalate
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.060Di-n-butyl phthalate
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.052Di-n-octyl phthalate
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.054Fluoranthene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.061Fluorene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.067Hexachlorobenzene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.076Hexachlorobutadiene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.076Hexachlorocyclopentadiene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.071Hexachloroethane
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.049Indeno(1,2,3-cd)pyrene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.057Isophorone
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.068Naphthalene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.060Nitrobenzene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVAamg/kg dry 0.067N-Nitroso-di-n-propylamine
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.064N-Nitrosodiphenylamine
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.050Pentachlorophenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.055Phenanthrene
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.062Phenol
BRL 8270D P8K024910.42 11/15/18 23:54 JMVmg/kg dry 0.056Pyrene
Surrogate Recovery Control Limits
39-13286 %2,4,6-Tribromophenol
44-11595 %2-Fluorobiphenyl
35-11591 %2-Fluorophenol
37-12229 %Nitrobenzene-d5 SR
34-12190 %Phenol-d5
54-12795 %Terphenyl-d14
Total Metals
0.038 *7471B P8K026810.026 11/15/18 13:41 MMRmg/kg dry 0.0024Mercury
3.1 *6010D P8K021310.64 11/13/18 19:59 JABmg/kg dry 0.039Arsenic
37 *6010D P8K021310.64 11/13/18 19:59 JABmg/kg dry 0.094Barium
BRL *6010D P8K021310.32 11/13/18 19:59 JABmg/kg dry 0.0086Cadmium
37 *6010D P8K021310.32 11/13/18 19:59 JABmg/kg dry 0.054Chromium
4.4 *6010D P8K021310.32 11/13/18 19:59 JABmg/kg dry 0.060Lead
0.93 *6010D P8K021310.64 11/13/18 19:59 JABmg/kg dry 0.15Selenium
BRL *6010D P8K021310.32 11/13/18 19:59 JABmg/kg dry 0.0080Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000461,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-3
Prism Sample ID: 8110180-03
Prism Work Order: 8110180
Time Collected: 11/08/18 12:20
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000271,1,1-Trichloroethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000381,1,2,2-Tetrachloroethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000501,1,2-Trichloroethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000161,1-Dichloroethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000251,1-Dichloroethylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000311,1-Dichloropropylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000321,2,3-Trichlorobenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000721,2,3-Trichloropropane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000421,2,4-Trichlorobenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000431,2,4-Trimethylbenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000231,2-Dibromoethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000261,2-Dichlorobenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000331,2-Dichloroethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000351,2-Dichloropropane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000421,3,5-Trimethylbenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000371,3-Dichlorobenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000281,3-Dichloropropane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000221,4-Dichlorobenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000272,2-Dichloropropane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000292-Chlorotoluene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000334-Chlorotoluene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.000274-Isopropyltoluene
0.061 8260B P8K027610.056 11/15/18 18:53 ANGmg/kg dry 0.0014Acetone
BRL 8260B P8K027610.0034 11/15/18 18:53 ANGmg/kg dry 0.00033Benzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00047Bromobenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00031Bromochloromethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00031Bromodichloromethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00064Bromoform
BRL 8260B P8K027610.011 11/15/18 18:53 ANGmg/kg dry 0.00069Bromomethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00028Carbon Tetrachloride
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00030Chlorobenzene
BRL 8260B P8K027610.011 11/15/18 18:53 ANGmg/kg dry 0.00047Chloroethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00041Chloroform
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00038Chloromethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00024cis-1,2-Dichloroethylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00019cis-1,3-Dichloropropylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00023Dibromochloromethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00025Dichlorodifluoromethane
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00022Ethylbenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00023Isopropyl Ether
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00033Isopropylbenzene (Cumene)
BRL 8260B P8K027610.011 11/15/18 18:53 ANGmg/kg dry 0.00052m,p-Xylenes
BRL 8260B P8K027610.056 11/15/18 18:53 ANGmg/kg dry 0.00051Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-3
Prism Sample ID: 8110180-03
Prism Work Order: 8110180
Time Collected: 11/08/18 12:20
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.11 11/15/18 18:53 ANGmg/kg dry 0.00051Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8K027610.056 11/15/18 18:53 ANGmg/kg dry 0.00048Methyl Isobutyl Ketone
BRL 8260B P8K027610.011 11/15/18 18:53 ANGmg/kg dry 0.00032Methylene Chloride
BRL 8260B P8K027610.011 11/15/18 18:53 ANGmg/kg dry 0.00018Methyl-tert-Butyl Ether
BRL 8260B P8K027610.011 11/15/18 18:53 ANGmg/kg dry 0.00018Naphthalene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00029n-Butylbenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00033n-Propylbenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00023o-Xylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00027sec-Butylbenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00034Styrene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00019tert-Butylbenzene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00027Tetrachloroethylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00032Toluene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00034trans-1,2-Dichloroethylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00030trans-1,3-Dichloropropylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00036Trichloroethylene
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00036Trichlorofluoromethane
BRL 8260B P8K027610.028 11/15/18 18:53 ANGmg/kg dry 0.00077Vinyl acetate
BRL 8260B P8K027610.0056 11/15/18 18:53 ANGmg/kg dry 0.00027Vinyl chloride
BRL 8260B P8K027610.017 11/15/18 18:53 ANGmg/kg dry 0.0011Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
84-123109 %Dibromofluoromethane
76-129102 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-4
Prism Sample ID: 8110180-04
Prism Work Order: 8110180
Time Collected: 11/08/18 12:50
Time Submitted: 11/09/18 15:00
General Chemistry Parameters
81.0 *SM2540 G P8K028410.100 11/14/18 14:56 TJY% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0641,2,4-Trichlorobenzene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0621,2-Dichlorobenzene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0571,3-Dichlorobenzene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0601,4-Dichlorobenzene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0781-Methylnaphthalene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0762,4,6-Trichlorophenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0792,4-Dichlorophenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0622,4-Dimethylphenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0572,4-Dinitrophenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0492,4-Dinitrotoluene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0542,6-Dinitrotoluene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0592-Chloronaphthalene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0582-Chlorophenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0652-Methylnaphthalene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0522-Methylphenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0742-Nitrophenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVICVmg/kg dry 0.0803,3’-Dichlorobenzidine
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0503/4-Methylphenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0614,6-Dinitro-2-methylphenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0704-Bromophenyl phenyl ether
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0574-Chloro-3-methylphenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0494-Chloroaniline
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0534-Chlorophenyl phenyl ether
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.0634-Nitrophenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.055Acenaphthene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.059Acenaphthylene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.066Anthracene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.054Azobenzene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.053Benzo(a)anthracene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.044Benzo(a)pyrene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.047Benzo(b)fluoranthene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.045Benzo(g,h,i)perylene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.053Benzo(k)fluoranthene
0.14 8270D P8K024910.41 11/16/18 0:17 JMVJmg/kg dry 0.034Benzoic Acid
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.054Benzyl alcohol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.071bis(2-Chloroethoxy)methane
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.058Bis(2-Chloroethyl)ether
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.070Bis(2-chloroisopropyl)ether
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.060Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-4
Prism Sample ID: 8110180-04
Prism Work Order: 8110180
Time Collected: 11/08/18 12:50
Time Submitted: 11/09/18 15:00
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.058Butyl benzyl phthalate
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.051Chrysene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.050Dibenzo(a,h)anthracene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.062Dibenzofuran
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.056Diethyl phthalate
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.054Dimethyl phthalate
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.058Di-n-butyl phthalate
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.050Di-n-octyl phthalate
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.052Fluoranthene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.058Fluorene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.065Hexachlorobenzene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.073Hexachlorobutadiene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.073Hexachlorocyclopentadiene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.068Hexachloroethane
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.047Indeno(1,2,3-cd)pyrene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.055Isophorone
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.066Naphthalene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.058Nitrobenzene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVAamg/kg dry 0.064N-Nitroso-di-n-propylamine
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.062N-Nitrosodiphenylamine
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.048Pentachlorophenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.053Phenanthrene
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.060Phenol
BRL 8270D P8K024910.41 11/16/18 0:17 JMVmg/kg dry 0.054Pyrene
Surrogate Recovery Control Limits
39-13265 %2,4,6-Tribromophenol
44-11577 %2-Fluorobiphenyl
35-11571 %2-Fluorophenol
37-12226 %Nitrobenzene-d5 SR
34-12164 %Phenol-d5
54-12778 %Terphenyl-d14
Total Metals
BRL *7471B P8K026810.024 11/15/18 13:45 MMRmg/kg dry 0.0023Mercury
1.9 *6010D P8K021310.61 11/13/18 20:08 JABmg/kg dry 0.037Arsenic
39 *6010D P8K021310.61 11/13/18 20:08 JABmg/kg dry 0.090Barium
BRL *6010D P8K021310.31 11/13/18 20:08 JABmg/kg dry 0.0082Cadmium
36 *6010D P8K021310.31 11/13/18 20:08 JABmg/kg dry 0.051Chromium
4.0 *6010D P8K021310.31 11/13/18 20:08 JABmg/kg dry 0.057Lead
1.1 *6010D P8K021310.61 11/13/18 20:08 JABmg/kg dry 0.15Selenium
BRL *6010D P8K021310.31 11/13/18 20:08 JABmg/kg dry 0.0076Silver
Volatile Organic Compounds by GC/MS
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000341,1,1,2-Tetrachloroethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-4
Prism Sample ID: 8110180-04
Prism Work Order: 8110180
Time Collected: 11/08/18 12:50
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000201,1,1-Trichloroethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000281,1,2,2-Tetrachloroethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000361,1,2-Trichloroethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000111,1-Dichloroethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000181,1-Dichloroethylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000221,1-Dichloropropylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000231,2,3-Trichlorobenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000521,2,3-Trichloropropane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000301,2,4-Trichlorobenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000311,2,4-Trimethylbenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000161,2-Dibromoethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000191,2-Dichlorobenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000241,2-Dichloroethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000251,2-Dichloropropane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000311,3,5-Trimethylbenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000271,3-Dichlorobenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000201,3-Dichloropropane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000161,4-Dichlorobenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000192,2-Dichloropropane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000212-Chlorotoluene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000244-Chlorotoluene
0.0088 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.000204-Isopropyltoluene
0.042 8260B P8K027610.041 11/15/18 19:20 ANGmg/kg dry 0.0010Acetone
BRL 8260B P8K027610.0024 11/15/18 19:20 ANGmg/kg dry 0.00024Benzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00034Bromobenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00022Bromochloromethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00023Bromodichloromethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00046Bromoform
BRL 8260B P8K027610.0082 11/15/18 19:20 ANGmg/kg dry 0.00050Bromomethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00020Carbon Tetrachloride
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00022Chlorobenzene
BRL 8260B P8K027610.0082 11/15/18 19:20 ANGmg/kg dry 0.00034Chloroethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00029Chloroform
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00027Chloromethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00017cis-1,2-Dichloroethylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00014cis-1,3-Dichloropropylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00017Dibromochloromethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00019Dichlorodifluoromethane
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00016Ethylbenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00017Isopropyl Ether
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00024Isopropylbenzene (Cumene)
BRL 8260B P8K027610.0082 11/15/18 19:20 ANGmg/kg dry 0.00038m,p-Xylenes
BRL 8260B P8K027610.041 11/15/18 19:20 ANGmg/kg dry 0.00037Methyl Butyl Ketone (2-Hexanone)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-4
Prism Sample ID: 8110180-04
Prism Work Order: 8110180
Time Collected: 11/08/18 12:50
Time Submitted: 11/09/18 15:00
BRL 8260B P8K027610.082 11/15/18 19:20 ANGmg/kg dry 0.00037Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8K027610.041 11/15/18 19:20 ANGmg/kg dry 0.00035Methyl Isobutyl Ketone
BRL 8260B P8K027610.0082 11/15/18 19:20 ANGmg/kg dry 0.00023Methylene Chloride
BRL 8260B P8K027610.0082 11/15/18 19:20 ANGmg/kg dry 0.00013Methyl-tert-Butyl Ether
BRL 8260B P8K027610.0082 11/15/18 19:20 ANGmg/kg dry 0.00013Naphthalene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00021n-Butylbenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00024n-Propylbenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00017o-Xylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00020sec-Butylbenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00025Styrene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00014tert-Butylbenzene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00019Tetrachloroethylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00023Toluene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00024trans-1,2-Dichloroethylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00021trans-1,3-Dichloropropylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00026Trichloroethylene
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00026Trichlorofluoromethane
BRL 8260B P8K027610.020 11/15/18 19:20 ANGmg/kg dry 0.00056Vinyl acetate
BRL 8260B P8K027610.0041 11/15/18 19:20 ANGmg/kg dry 0.00020Vinyl chloride
BRL 8260B P8K027610.012 11/15/18 19:20 ANGmg/kg dry 0.00076Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
84-123110 %Dibromofluoromethane
76-129103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-1
Prism Sample ID: 8110180-05
Prism Work Order: 8110180
Time Collected: 11/08/18 14:15
Time Submitted: 11/09/18 15:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.41,2,4-Trichlorobenzene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.31,2-Dichlorobenzene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.61,3-Dichlorobenzene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.31,4-Dichlorobenzene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.61-Methylnaphthalene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.22,4,5-Trichlorophenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.62,4,6-Trichlorophenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.62,4-Dichlorophenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 4.82,4-Dimethylphenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.82,4-Dinitrophenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.02,4-Dinitrotoluene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.62,6-Dinitrotoluene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.82-Chloronaphthalene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.62-Chlorophenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.32-Methylnaphthalene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.52-Methylphenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.02-Nitroaniline
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.32-Nitrophenol
BRL 8270D P8K026511411/16/18 1:48 JMVICVug/L 2.03,3’-Dichlorobenzidine
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.13/4-Methylphenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.93-Nitroaniline
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.94,6-Dinitro-2-methylphenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.84-Bromophenyl phenyl ether
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.34-Chloro-3-methylphenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.44-Chloroaniline
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.84-Chlorophenyl phenyl ether
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.34-Nitroaniline
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 0.834-Nitrophenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.5Acenaphthene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.8Acenaphthylene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.3Aniline
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.0Anthracene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.5Azobenzene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.0Benzo(a)anthracene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.0Benzo(a)pyrene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.6Benzo(b)fluoranthene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.9Benzo(g,h,i)perylene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.0Benzo(k)fluoranthene
BRL 8270D P8K0265114011/16/18 1:48 JMVug/L 6.5Benzoic Acid
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.0Benzyl alcohol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.6bis(2-Chloroethoxy)methane
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.2Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-1
Prism Sample ID: 8110180-05
Prism Work Order: 8110180
Time Collected: 11/08/18 14:15
Time Submitted: 11/09/18 15:00
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.7Bis(2-chloroisopropyl)ether
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.8Bis(2-Ethylhexyl)phthalate
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.9Butyl benzyl phthalate
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.0Chrysene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.7Dibenzo(a,h)anthracene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.4Dibenzofuran
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 4.6Diethyl phthalate
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.9Dimethyl phthalate
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.3Di-n-butyl phthalate
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.8Di-n-octyl phthalate
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.3Fluoranthene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.3Fluorene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.8Hexachlorobenzene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.0Hexachlorobutadiene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.4Hexachlorocyclopentadiene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.4Hexachloroethane
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 5.4Indeno(1,2,3-cd)pyrene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.5Isophorone
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.6Naphthalene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 3.6Nitrobenzene
BRL 8270D P8K026511411/16/18 1:48 JMVAaug/L 3.0N-Nitroso-di-n-propylamine
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.8N-Nitrosodiphenylamine
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.7Pentachlorophenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.0Phenanthrene
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 1.4Phenol
BRL 8270D P8K026511411/16/18 1:48 JMVug/L 2.0Pyrene
Surrogate Recovery Control Limits
43-140105 %2,4,6-Tribromophenol
44-11996 %2-Fluorobiphenyl
19-11966 %2-Fluorophenol
44-12089 %Nitrobenzene-d5
11-5248 %Phenol-d5
50-134105 %Terphenyl-d14
Total Metals
BRL *7470A P8K023810.00020 11/14/18 18:14 MMRmg/L 0.000036Mercury
BRL *6010D P8K021110.020 11/13/18 16:57 JABmg/L 0.0031Arsenic
0.75 *6010D P8K021110.010 11/13/18 16:57 JABmg/L 0.00080Barium
BRL *6010D P8K021110.0010 11/13/18 16:57 JABmg/L 0.00015Cadmium
0.052 *6010D P8K021110.0050 11/13/18 16:57 JABmg/L 0.00036Chromium
BRL *6010D P8K021110.0050 11/13/18 16:57 JABmg/L 0.00080Lead
BRL *6010D P8K021110.020 11/13/18 16:57 JABmg/L 0.0056Selenium
BRL *6010D P8K021110.0050 11/13/18 16:57 JABmg/L 0.00039Silver
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-1
Prism Sample ID: 8110180-05
Prism Work Order: 8110180
Time Collected: 11/08/18 14:15
Time Submitted: 11/09/18 15:00
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P8K026412.0 11/14/18 20:25 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P8K026412.0 11/14/18 20:25 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P8K026412.0 11/14/18 20:25 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.0894-Isopropyltoluene
11 8260B P8K026415.0 11/14/18 20:25 KDMug/L 0.31Acetone
BRL 8260B P8K026412011/14/18 20:25 KDMug/L 0.20Acrolein
BRL 8260B P8K026412011/14/18 20:25 KDMug/L 0.20Acrylonitrile
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.048Benzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.057Bromobenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.14Bromochloromethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.062Bromodichloromethane
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.040Bromoform
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.18Bromomethane
BRL 8260B P8K026415.0 11/14/18 20:25 KDMug/L 0.075Carbon disulfide
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.062Chlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.22Chloroethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.076Chloroform
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.079Chloromethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.081Dibromochloromethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.065Dibromomethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-1
Prism Sample ID: 8110180-05
Prism Work Order: 8110180
Time Collected: 11/08/18 14:15
Time Submitted: 11/09/18 15:00
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.061Ethylbenzene
BRL 8260B P8K026412.0 11/14/18 20:25 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.050Isopropyl Ether
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.12m,p-Xylenes
BRL 8260B P8K026415.0 11/14/18 20:25 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P8K026415.0 11/14/18 20:25 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8K026415.0 11/14/18 20:25 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.083Methylene Chloride
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.19Naphthalene
BRL 8260B P8K026411.0 11/14/18 20:25 KDMug/L 0.076n-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.087n-Propylbenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.044o-Xylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.047Styrene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.044Toluene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.078Trichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P8K026412.0 11/14/18 20:25 KDMug/L 0.060Vinyl acetate
BRL 8260B P8K026410.50 11/14/18 20:25 KDMug/L 0.097Vinyl chloride
BRL 8260B P8K026411.5 11/14/18 20:25 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12496 %4-Bromofluorobenzene
75-12998 %Dibromofluoromethane
77-12393 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-2
Prism Sample ID: 8110180-06
Prism Work Order: 8110180
Time Collected: 11/08/18 14:35
Time Submitted: 11/09/18 15:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.21,2,4-Trichlorobenzene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.11,2-Dichlorobenzene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.41,3-Dichlorobenzene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.11,4-Dichlorobenzene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.31-Methylnaphthalene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.02,4,5-Trichlorophenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.32,4,6-Trichlorophenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.22,4-Dichlorophenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 4.42,4-Dimethylphenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.42,4-Dinitrophenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.82,4-Dinitrotoluene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.42,6-Dinitrotoluene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.42-Chloronaphthalene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.42-Chlorophenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.02-Methylnaphthalene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.32-Methylphenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.82-Nitroaniline
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.02-Nitrophenol
BRL 8270D P8K026511311/16/18 2:11 JMVICVug/L 1.83,3’-Dichlorobenzidine
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.93/4-Methylphenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.83-Nitroaniline
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.74,6-Dinitro-2-methylphenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.64-Bromophenyl phenyl ether
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.04-Chloro-3-methylphenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.14-Chloroaniline
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.74-Chlorophenyl phenyl ether
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.24-Nitroaniline
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 0.764-Nitrophenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.3Acenaphthene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.6Acenaphthylene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.0Aniline
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.8Anthracene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.3Azobenzene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.8Benzo(a)anthracene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.8Benzo(a)pyrene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.4Benzo(b)fluoranthene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.7Benzo(g,h,i)perylene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.8Benzo(k)fluoranthene
BRL 8270D P8K0265113011/16/18 2:11 JMVug/L 5.9Benzoic Acid
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.7Benzyl alcohol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.3bis(2-Chloroethoxy)methane
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.9Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-2
Prism Sample ID: 8110180-06
Prism Work Order: 8110180
Time Collected: 11/08/18 14:35
Time Submitted: 11/09/18 15:00
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.5Bis(2-chloroisopropyl)ether
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.7Bis(2-Ethylhexyl)phthalate
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.7Butyl benzyl phthalate
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.8Chrysene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.5Dibenzo(a,h)anthracene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.2Dibenzofuran
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 4.2Diethyl phthalate
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.8Dimethyl phthalate
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.1Di-n-butyl phthalate
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.6Di-n-octyl phthalate
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.1Fluoranthene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.1Fluorene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.6Hexachlorobenzene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.7Hexachlorobutadiene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.2Hexachlorocyclopentadiene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 2.2Hexachloroethane
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 4.9Indeno(1,2,3-cd)pyrene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.2Isophorone
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.3Naphthalene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 3.2Nitrobenzene
BRL 8270D P8K026511311/16/18 2:11 JMVAaug/L 2.8N-Nitroso-di-n-propylamine
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.7N-Nitrosodiphenylamine
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.6Pentachlorophenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.9Phenanthrene
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.2Phenol
BRL 8270D P8K026511311/16/18 2:11 JMVug/L 1.8Pyrene
Surrogate Recovery Control Limits
43-140104 %2,4,6-Tribromophenol
44-11999 %2-Fluorobiphenyl
19-11966 %2-Fluorophenol
44-12094 %Nitrobenzene-d5
11-5246 %Phenol-d5
50-134106 %Terphenyl-d14
Total Metals
BRL *7470A P8K023810.00020 11/14/18 18:18 MMRmg/L 0.000036Mercury
0.048 *6010D P8K021110.020 11/13/18 17:07 JABmg/L 0.0031Arsenic
3.6 *6010D P8K021110.010 11/13/18 17:07 JABmg/L 0.00080Barium
BRL *6010D P8K021110.0010 11/13/18 17:07 JABmg/L 0.00015Cadmium
0.71 *6010D P8K021110.0050 11/13/18 17:07 JABmg/L 0.00036Chromium
0.031 *6010D P8K021110.0050 11/13/18 17:07 JABmg/L 0.00080Lead
BRL *6010D P8K021110.020 11/13/18 17:07 JABmg/L 0.0056Selenium
BRL *6010D P8K021110.0050 11/13/18 17:07 JABmg/L 0.00039Silver
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-2
Prism Sample ID: 8110180-06
Prism Work Order: 8110180
Time Collected: 11/08/18 14:35
Time Submitted: 11/09/18 15:00
Volatile Organic Compounds by GC/MS
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P8K026412.0 11/14/18 20:51 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P8K026412.0 11/14/18 20:51 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P8K026412.0 11/14/18 20:51 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.0894-Isopropyltoluene
BRL 8260B P8K026415.0 11/14/18 20:51 KDMug/L 0.31Acetone
BRL 8260B P8K026412011/14/18 20:51 KDMug/L 0.20Acrolein
BRL 8260B P8K026412011/14/18 20:51 KDMug/L 0.20Acrylonitrile
2.0 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.048Benzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.057Bromobenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.14Bromochloromethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.062Bromodichloromethane
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.040Bromoform
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.18Bromomethane
BRL 8260B P8K026415.0 11/14/18 20:51 KDMug/L 0.075Carbon disulfide
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.062Chlorobenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.22Chloroethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.076Chloroform
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.079Chloromethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-2
Prism Sample ID: 8110180-06
Prism Work Order: 8110180
Time Collected: 11/08/18 14:35
Time Submitted: 11/09/18 15:00
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.065Dibromomethane
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.061Ethylbenzene
BRL 8260B P8K026412.0 11/14/18 20:51 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.050Isopropyl Ether
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.054Isopropylbenzene (Cumene)
1.1 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.12m,p-Xylenes
BRL 8260B P8K026415.0 11/14/18 20:51 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P8K026415.0 11/14/18 20:51 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
0.37 8260B P8K026415.0 11/14/18 20:51 KDMJug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.083Methylene Chloride
0.51 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.19Naphthalene
BRL 8260B P8K026411.0 11/14/18 20:51 KDMug/L 0.076n-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.087n-Propylbenzene
0.96 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.044o-Xylene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.047Styrene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.098Tetrachloroethylene
0.76 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.044Toluene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.078Trichloroethylene
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P8K026412.0 11/14/18 20:51 KDMug/L 0.060Vinyl acetate
BRL 8260B P8K026410.50 11/14/18 20:51 KDMug/L 0.097Vinyl chloride
2.1 8260B P8K026411.5 11/14/18 20:51 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124100 %4-Bromofluorobenzene
75-12994 %Dibromofluoromethane
77-12394 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-3
Prism Sample ID: 8110180-07
Prism Work Order: 8110180
Time Collected: 11/08/18 15:05
Time Submitted: 11/09/18 15:00
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.01,2,4-Trichlorobenzene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.91,2-Dichlorobenzene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.21,3-Dichlorobenzene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.91,4-Dichlorobenzene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.01-Methylnaphthalene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.92,4,5-Trichlorophenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.12,4,6-Trichlorophenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.02,4-Dichlorophenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 4.02,4-Dimethylphenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.12,4-Dinitrophenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.72,4-Dinitrotoluene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.32,6-Dinitrotoluene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.22-Chloronaphthalene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.22-Chlorophenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.82-Methylnaphthalene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.12-Methylphenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.62-Nitroaniline
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.82-Nitrophenol
BRL 8270D P8K026511211/16/18 2:34 JMVICVug/L 1.73,3’-Dichlorobenzidine
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.83/4-Methylphenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.63-Nitroaniline
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.64,6-Dinitro-2-methylphenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.54-Bromophenyl phenyl ether
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.84-Chloro-3-methylphenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.84-Chloroaniline
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.54-Chlorophenyl phenyl ether
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.14-Nitroaniline
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 0.704-Nitrophenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.1Acenaphthene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.4Acenaphthylene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.8Aniline
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.7Anthracene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.1Azobenzene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.7Benzo(a)anthracene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.7Benzo(a)pyrene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.3Benzo(b)fluoranthene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.6Benzo(g,h,i)perylene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.6Benzo(k)fluoranthene
BRL 8270D P8K0265112011/16/18 2:34 JMVug/L 5.4Benzoic Acid
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.5Benzyl alcohol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.0bis(2-Chloroethoxy)methane
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.7Bis(2-Chloroethyl)ether
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-3
Prism Sample ID: 8110180-07
Prism Work Order: 8110180
Time Collected: 11/08/18 15:05
Time Submitted: 11/09/18 15:00
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.3Bis(2-chloroisopropyl)ether
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.5Bis(2-Ethylhexyl)phthalate
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.6Butyl benzyl phthalate
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.7Chrysene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.4Dibenzo(a,h)anthracene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.0Dibenzofuran
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.9Diethyl phthalate
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.6Dimethyl phthalate
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.0Di-n-butyl phthalate
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.5Di-n-octyl phthalate
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.0Fluoranthene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.0Fluorene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.5Hexachlorobenzene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.5Hexachlorobutadiene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.0Hexachlorocyclopentadiene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.0Hexachloroethane
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 4.5Indeno(1,2,3-cd)pyrene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 2.9Isophorone
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.0Naphthalene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 3.0Nitrobenzene
BRL 8270D P8K026511211/16/18 2:34 JMVAaug/L 2.5N-Nitroso-di-n-propylamine
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.5N-Nitrosodiphenylamine
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.4Pentachlorophenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.7Phenanthrene
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.1Phenol
BRL 8270D P8K026511211/16/18 2:34 JMVug/L 1.7Pyrene
Surrogate Recovery Control Limits
43-14090 %2,4,6-Tribromophenol
44-11985 %2-Fluorobiphenyl
19-11956 %2-Fluorophenol
44-12084 %Nitrobenzene-d5
11-5239 %Phenol-d5
50-13498 %Terphenyl-d14
Total Metals
BRL *7470A P8K023810.00020 11/14/18 18:22 MMRmg/L 0.000036Mercury
BRL *6010D P8K021110.020 11/13/18 17:15 JABmg/L 0.0031Arsenic
0.35 *6010D P8K021110.010 11/13/18 17:15 JABmg/L 0.00080Barium
BRL *6010D P8K021110.0010 11/13/18 17:15 JABmg/L 0.00015Cadmium
0.028 *6010D P8K021110.0050 11/13/18 17:15 JABmg/L 0.00036Chromium
BRL *6010D P8K021110.0050 11/13/18 17:15 JABmg/L 0.00080Lead
BRL *6010D P8K021110.020 11/13/18 17:15 JABmg/L 0.0056Selenium
BRL *6010D P8K021110.0050 11/13/18 17:15 JABmg/L 0.00039Silver
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-3
Prism Sample ID: 8110180-07
Prism Work Order: 8110180
Time Collected: 11/08/18 15:05
Time Submitted: 11/09/18 15:00
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0611,1,1-Trichloroethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0661,1,2-Trichloroethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0831,1-Dichloroethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0831,1-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0511,1-Dichloropropylene
BRL 8260B P8K026412.0 11/14/18 21:16 KDMug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.141,2,3-Trichloropropane
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P8K026412.0 11/14/18 21:16 KDMug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0511,2-Dibromoethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0761,2-Dichlorobenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0661,2-Dichloroethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.111,2-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0541,3-Dichlorobenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0431,3-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0501,4-Dichlorobenzene
BRL 8260B P8K026412.0 11/14/18 21:16 KDMug/L 0.112,2-Dichloropropane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0662-Chlorotoluene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0504-Chlorotoluene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.0894-Isopropyltoluene
5.6 8260B P8K026415.0 11/14/18 21:16 KDMug/L 0.31Acetone
BRL 8260B P8K026412011/14/18 21:16 KDMug/L 0.20Acrolein
BRL 8260B P8K026412011/14/18 21:16 KDMug/L 0.20Acrylonitrile
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.048Benzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.057Bromobenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.14Bromochloromethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.062Bromodichloromethane
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.040Bromoform
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.18Bromomethane
BRL 8260B P8K026415.0 11/14/18 21:16 KDMug/L 0.075Carbon disulfide
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.11Carbon Tetrachloride
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.062Chlorobenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.22Chloroethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.076Chloroform
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.079Chloromethane
2.8 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.081Dibromochloromethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.065Dibromomethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
12/17/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-3
Prism Sample ID: 8110180-07
Prism Work Order: 8110180
Time Collected: 11/08/18 15:05
Time Submitted: 11/09/18 15:00
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.11Dichlorodifluoromethane
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.061Ethylbenzene
BRL 8260B P8K026412.0 11/14/18 21:16 KDMug/L 0.16Hexachlorobutadiene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.050Isopropyl Ether
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.12m,p-Xylenes
BRL 8260B P8K026415.0 11/14/18 21:16 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P8K026415.0 11/14/18 21:16 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8K026415.0 11/14/18 21:16 KDMug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.083Methylene Chloride
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.19Naphthalene
BRL 8260B P8K026411.0 11/14/18 21:16 KDMug/L 0.076n-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.087n-Propylbenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.044o-Xylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.076sec-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.047Styrene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.088tert-Butylbenzene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.098Tetrachloroethylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.044Toluene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.078Trichloroethylene
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.062Trichlorofluoromethane
BRL 8260B P8K026412.0 11/14/18 21:16 KDMug/L 0.060Vinyl acetate
BRL 8260B P8K026410.50 11/14/18 21:16 KDMug/L 0.097Vinyl chloride
BRL 8260B P8K026411.5 11/14/18 21:16 KDMug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-12498 %4-Bromofluorobenzene
75-12994 %Dibromofluoromethane
77-12395 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0264 - 5030B
Blank (P8K0264-BLK1)Prepared & Analyzed: 11/14/18
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/L1.75 0.50 A
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0264 - 5030B
Blank (P8K0264-BLK1)Prepared & Analyzed: 11/14/18
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL1.0
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9949.3
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0264 - 5030B
LCS (P8K0264-BS1)Prepared & Analyzed: 11/14/18
1,1,1,2-Tetrachloroethane ug/L19.6 0.50 20.00 79-13498
1,1,1-Trichloroethane ug/L18.2 0.50 20.00 75-13691
1,1,2,2-Tetrachloroethane ug/L18.8 0.50 20.00 62-12794
1,1,2-Trichloroethane ug/L20.8 0.50 20.00 70-140104
1,1-Dichloroethane ug/L19.0 0.50 20.00 78-13095
1,1-Dichloroethylene ug/L18.1 0.50 20.00 70-15490
1,1-Dichloropropylene ug/L18.7 0.50 20.00 71-13694
1,2,3-Trichlorobenzene ug/L19.0 2.0 20.00 58-14495
1,2,3-Trichloropropane ug/L18.8 1.0 20.00 71-12794
1,2,4-Trichlorobenzene ug/L18.6 1.0 20.00 66-13993
1,2,4-Trimethylbenzene ug/L18.9 0.50 20.00 75-13394
1,2-Dibromo-3-chloropropane ug/L17.1 2.0 20.00 63-13486
1,2-Dibromoethane ug/L19.5 0.50 20.00 77-13598
1,2-Dichlorobenzene ug/L18.6 0.50 20.00 78-12893
1,2-Dichloroethane ug/L20.8 0.50 20.00 68-131104
1,2-Dichloropropane ug/L20.3 0.50 20.00 77-130101
1,3,5-Trimethylbenzene ug/L18.2 0.50 20.00 75-13191
1,3-Dichlorobenzene ug/L17.9 0.50 20.00 77-12590
1,3-Dichloropropane ug/L19.6 0.50 20.00 76-13298
1,4-Dichlorobenzene ug/L18.4 0.50 20.00 75-12692
2,2-Dichloropropane ug/L20.0 2.0 20.00 29-149100
2-Chlorotoluene ug/L17.8 0.50 20.00 74-12689
4-Chlorotoluene ug/L18.7 0.50 20.00 78-12994
4-Isopropyltoluene ug/L18.4 0.50 20.00 69-13292
Acetone ug/L42.4 5.0 40.00 40-166106
Acrolein ug/L39.4 20 40.00 70-13098
Acrylonitrile ug/L41.0 20 40.00 81-127102
Benzene ug/L20.2 0.50 20.00 77-128101
Bromobenzene ug/L18.3 0.50 20.00 78-12992
Bromochloromethane ug/L20.2 0.50 20.00 78-135101
Bromodichloromethane ug/L20.8 0.50 20.00 76-138104
Bromoform ug/L20.8 1.0 20.00 71-135104
Bromomethane ug/L16.7 1.0 20.00 41-16883
Carbon disulfide ug/L19.0 5.0 20.00 59-13595
Carbon Tetrachloride ug/L18.0 0.50 20.00 72-14290
Chlorobenzene ug/L18.9 0.50 20.00 78-11994
Chloroethane ug/L19.9 0.50 20.00 57-14299
Chloroform ug/L21.7 0.50 20.00 B77-130108
Chloromethane ug/L20.3 0.50 20.00 47-145102
cis-1,2-Dichloroethylene ug/L19.8 0.50 20.00 76-14199
cis-1,3-Dichloropropylene ug/L20.5 0.50 20.00 65-140102
Dibromochloromethane ug/L17.6 0.50 20.00 75-13488
Dibromomethane ug/L20.8 0.50 20.00 76-138104
Dichlorodifluoromethane ug/L19.3 1.0 20.00 28-16396
Ethylbenzene ug/L19.1 0.50 20.00 80-12795
Hexachlorobutadiene ug/L16.4 2.0 20.00 61-13482
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0264 - 5030B
LCS (P8K0264-BS1)Prepared & Analyzed: 11/14/18
Isopropyl Ether ug/L20.2 0.50 20.00 60-154101
Isopropylbenzene (Cumene)ug/L18.7 0.50 20.00 70-13094
m,p-Xylenes ug/L37.5 1.0 40.00 77-13394
Methyl Butyl Ketone (2-Hexanone)ug/L19.0 5.0 20.00 64-13795
Methyl Ethyl Ketone (2-Butanone)ug/L19.9 5.0 20.00 71-13499
Methyl Isobutyl Ketone ug/L21.3 5.0 20.00 69-134106
Methylene Chloride ug/L20.4 1.0 20.00 73-131102
Methyl-tert-Butyl Ether ug/L20.0 0.50 20.00 68-135100
Naphthalene ug/L18.7 1.0 20.00 64-13694
n-Butylbenzene ug/L19.0 1.0 20.00 68-13495
n-Propylbenzene ug/L18.8 0.50 20.00 72-13294
o-Xylene ug/L18.7 0.50 20.00 78-12894
sec-Butylbenzene ug/L18.5 0.50 20.00 71-13192
Styrene ug/L18.9 0.50 20.00 78-12995
tert-Butylbenzene ug/L18.1 0.50 20.00 70-13291
Tetrachloroethylene ug/L16.5 0.50 20.00 80-12982
Toluene ug/L20.3 0.50 20.00 76-131101
trans-1,2-Dichloroethylene ug/L20.1 0.50 20.00 76-135100
trans-1,3-Dichloropropylene ug/L22.6 0.50 20.00 67-140113
Trichloroethylene ug/L20.0 0.50 20.00 77-133100
Trichlorofluoromethane ug/L21.9 0.50 20.00 62-148109
Vinyl acetate ug/L22.6 2.0 20.00 34-167113
Vinyl chloride ug/L20.2 0.50 20.00 57-141101
Xylenes, total ug/L56.3 1.5 60.00 77-13394
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9849.2
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9647.9
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0264 - 5030B
LCS Dup (P8K0264-BSD1)Prepared & Analyzed: 11/14/18
1,1,1,2-Tetrachloroethane ug/L19.0 0.50 20.00 2079-13495 3
1,1,1-Trichloroethane ug/L17.0 0.50 20.00 2075-13685 7
1,1,2,2-Tetrachloroethane ug/L17.8 0.50 20.00 2062-12789 5
1,1,2-Trichloroethane ug/L19.6 0.50 20.00 2070-14098 6
1,1-Dichloroethane ug/L17.6 0.50 20.00 2078-13088 8
1,1-Dichloroethylene ug/L17.3 0.50 20.00 2070-15486 5
1,1-Dichloropropylene ug/L17.5 0.50 20.00 2071-13688 7
1,2,3-Trichlorobenzene ug/L17.0 2.0 20.00 2058-14485 11
1,2,3-Trichloropropane ug/L18.0 1.0 20.00 2071-12790 4
1,2,4-Trichlorobenzene ug/L16.9 1.0 20.00 2066-13985 10
1,2,4-Trimethylbenzene ug/L17.5 0.50 20.00 2075-13387 8
1,2-Dibromo-3-chloropropane ug/L16.4 2.0 20.00 2063-13482 5
1,2-Dibromoethane ug/L18.5 0.50 20.00 2077-13592 6
1,2-Dichlorobenzene ug/L17.2 0.50 20.00 2078-12886 8
1,2-Dichloroethane ug/L19.2 0.50 20.00 2068-13196 8
1,2-Dichloropropane ug/L20.0 0.50 20.00 2077-130100 2
1,3,5-Trimethylbenzene ug/L16.9 0.50 20.00 2075-13185 7
1,3-Dichlorobenzene ug/L16.4 0.50 20.00 2077-12582 9
1,3-Dichloropropane ug/L18.9 0.50 20.00 2076-13294 4
1,4-Dichlorobenzene ug/L16.7 0.50 20.00 2075-12683 10
2,2-Dichloropropane ug/L18.4 2.0 20.00 2029-14992 8
2-Chlorotoluene ug/L16.5 0.50 20.00 2074-12682 8
4-Chlorotoluene ug/L17.1 0.50 20.00 2078-12985 9
4-Isopropyltoluene ug/L16.5 0.50 20.00 2069-13283 11
Acetone ug/L39.4 5.0 40.00 2040-16698 7
Acrolein ug/L37.3 20 40.00 2070-13093 5
Acrylonitrile ug/L39.4 20 40.00 2081-12798 4
Benzene ug/L19.1 0.50 20.00 2077-12896 5
Bromobenzene ug/L17.1 0.50 20.00 2078-12985 7
Bromochloromethane ug/L19.3 0.50 20.00 2078-13596 5
Bromodichloromethane ug/L19.9 0.50 20.00 2076-13899 5
Bromoform ug/L20.5 1.0 20.00 2071-135103 1
Bromomethane ug/L15.7 1.0 20.00 2041-16878 6
Carbon disulfide ug/L17.9 5.0 20.00 2059-13590 6
Carbon Tetrachloride ug/L17.0 0.50 20.00 2072-14285 6
Chlorobenzene ug/L17.9 0.50 20.00 2078-11990 5
Chloroethane ug/L18.5 0.50 20.00 2057-14292 7
Chloroform ug/L20.1 0.50 20.00 20 B77-130100 8
Chloromethane ug/L19.1 0.50 20.00 2047-14596 6
cis-1,2-Dichloroethylene ug/L18.8 0.50 20.00 2076-14194 5
cis-1,3-Dichloropropylene ug/L18.9 0.50 20.00 2065-14095 8
Dibromochloromethane ug/L17.8 0.50 20.00 2075-13489 0.8
Dibromomethane ug/L19.4 0.50 20.00 2076-13897 7
Dichlorodifluoromethane ug/L18.1 1.0 20.00 2028-16391 6
Ethylbenzene ug/L18.4 0.50 20.00 2080-12792 4
Hexachlorobutadiene ug/L15.3 2.0 20.00 2061-13476 7
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0264 - 5030B
LCS Dup (P8K0264-BSD1)Prepared & Analyzed: 11/14/18
Isopropyl Ether ug/L19.0 0.50 20.00 2060-15495 6
Isopropylbenzene (Cumene)ug/L16.8 0.50 20.00 2070-13084 11
m,p-Xylenes ug/L36.1 1.0 40.00 2077-13390 4
Methyl Butyl Ketone (2-Hexanone)ug/L18.6 5.0 20.00 2064-13793 2
Methyl Ethyl Ketone (2-Butanone)ug/L19.2 5.0 20.00 2071-13496 3
Methyl Isobutyl Ketone ug/L19.9 5.0 20.00 2069-13499 7
Methylene Chloride ug/L18.8 1.0 20.00 2073-13194 9
Methyl-tert-Butyl Ether ug/L19.3 0.50 20.00 2068-13596 4
Naphthalene ug/L17.3 1.0 20.00 2064-13686 8
n-Butylbenzene ug/L16.4 1.0 20.00 2068-13482 14
n-Propylbenzene ug/L17.5 0.50 20.00 2072-13288 7
o-Xylene ug/L18.1 0.50 20.00 2078-12891 3
sec-Butylbenzene ug/L17.0 0.50 20.00 2071-13185 8
Styrene ug/L18.3 0.50 20.00 2078-12991 3
tert-Butylbenzene ug/L16.6 0.50 20.00 2070-13283 9
Tetrachloroethylene ug/L15.3 0.50 20.00 20 L280-12977 7
Toluene ug/L18.6 0.50 20.00 2076-13193 8
trans-1,2-Dichloroethylene ug/L18.8 0.50 20.00 2076-13594 7
trans-1,3-Dichloropropylene ug/L21.8 0.50 20.00 2067-140109 4
Trichloroethylene ug/L18.8 0.50 20.00 2077-13394 6
Trichlorofluoromethane ug/L21.1 0.50 20.00 2062-148105 4
Vinyl acetate ug/L21.3 2.0 20.00 2034-167107 6
Vinyl chloride ug/L18.6 0.50 20.00 2057-14193 8
Xylenes, total ug/L54.2 1.5 60.00 2077-13390 4
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 9547.6
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9447.0
ug/L 50.00 77-123Surrogate: Toluene-d8 9346.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0276 - 5035
Blank (P8K0276-BLK1)Prepared & Analyzed: 11/15/18
1,1,1,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,1-Trichloroethane mg/kg wetBRL0.0050
1,1,2,2-Tetrachloroethane mg/kg wetBRL0.0050
1,1,2-Trichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethane mg/kg wetBRL0.0050
1,1-Dichloroethylene mg/kg wetBRL0.0050
1,1-Dichloropropylene mg/kg wetBRL0.0050
1,2,3-Trichlorobenzene mg/kg wetBRL0.0050
1,2,3-Trichloropropane mg/kg wetBRL0.0050
1,2,4-Trichlorobenzene mg/kg wetBRL0.0050
1,2,4-Trimethylbenzene mg/kg wetBRL0.0050
1,2-Dibromoethane mg/kg wetBRL0.0050
1,2-Dichlorobenzene mg/kg wetBRL0.0050
1,2-Dichloroethane mg/kg wetBRL0.0050
1,2-Dichloropropane mg/kg wetBRL0.0050
1,3,5-Trimethylbenzene mg/kg wetBRL0.0050
1,3-Dichlorobenzene mg/kg wetBRL0.0050
1,3-Dichloropropane mg/kg wetBRL0.0050
1,4-Dichlorobenzene mg/kg wetBRL0.0050
2,2-Dichloropropane mg/kg wetBRL0.0050
2-Chlorotoluene mg/kg wetBRL0.0050
4-Chlorotoluene mg/kg wetBRL0.0050
4-Isopropyltoluene mg/kg wetBRL0.0050
Acetone mg/kg wetBRL0.050
Benzene mg/kg wetBRL0.0030
Bromobenzene mg/kg wetBRL0.0050
Bromochloromethane mg/kg wetBRL0.0050
Bromodichloromethane mg/kg wetBRL0.0050
Bromoform mg/kg wetBRL0.0050
Bromomethane mg/kg wetBRL0.010
Carbon Tetrachloride mg/kg wetBRL0.0050
Chlorobenzene mg/kg wetBRL0.0050
Chloroethane mg/kg wetBRL0.010
Chloroform mg/kg wetBRL0.0050
Chloromethane mg/kg wetBRL0.0050
cis-1,2-Dichloroethylene mg/kg wetBRL0.0050
cis-1,3-Dichloropropylene mg/kg wetBRL0.0050
Dibromochloromethane mg/kg wetBRL0.0050
Dichlorodifluoromethane mg/kg wetBRL0.0050
Ethylbenzene mg/kg wetBRL0.0050
Isopropyl Ether mg/kg wetBRL0.0050
Isopropylbenzene (Cumene)mg/kg wetBRL0.0050
m,p-Xylenes mg/kg wetBRL0.010
Methyl Butyl Ketone (2-Hexanone)mg/kg wetBRL0.050
Methyl Ethyl Ketone (2-Butanone)mg/kg wetBRL0.10
Methyl Isobutyl Ketone mg/kg wetBRL0.050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0276 - 5035
Blank (P8K0276-BLK1)Prepared & Analyzed: 11/15/18
Methylene Chloride mg/kg wetBRL0.010
Methyl-tert-Butyl Ether mg/kg wetBRL0.010
Naphthalene mg/kg wetBRL0.010
n-Butylbenzene mg/kg wetBRL0.0050
n-Propylbenzene mg/kg wetBRL0.0050
o-Xylene mg/kg wetBRL0.0050
sec-Butylbenzene mg/kg wetBRL0.0050
Styrene mg/kg wetBRL0.0050
tert-Butylbenzene mg/kg wetBRL0.0050
Tetrachloroethylene mg/kg wetBRL0.0050
Toluene mg/kg wetBRL0.0050
trans-1,2-Dichloroethylene mg/kg wetBRL0.0050
trans-1,3-Dichloropropylene mg/kg wetBRL0.0050
Trichloroethylene mg/kg wetBRL0.0050
Trichlorofluoromethane mg/kg wetBRL0.0050
Vinyl acetate mg/kg wetBRL0.025
Vinyl chloride mg/kg wetBRL0.0050
Xylenes, total mg/kg wetBRL0.015
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.3
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10753.4
ug/L 50.00 76-129Surrogate: Toluene-d8 10351.6
LCS (P8K0276-BS1)Prepared & Analyzed: 11/15/18
1,1,1,2-Tetrachloroethane mg/kg wet0.0461 0.0050 0.05000 72-11592
1,1,1-Trichloroethane mg/kg wet0.0420 0.0050 0.05000 67-13184
1,1,2,2-Tetrachloroethane mg/kg wet0.0498 0.0050 0.05000 56-126100
1,1,2-Trichloroethane mg/kg wet0.0459 0.0050 0.05000 70-13392
1,1-Dichloroethane mg/kg wet0.0418 0.0050 0.05000 74-12784
1,1-Dichloroethylene mg/kg wet0.0382 0.0050 0.05000 67-14976
1,1-Dichloropropylene mg/kg wet0.0425 0.0050 0.05000 71-13085
1,2,3-Trichlorobenzene mg/kg wet0.0484 0.0050 0.05000 68-13097
1,2,3-Trichloropropane mg/kg wet0.0491 0.0050 0.05000 60-13798
1,2,4-Trichlorobenzene mg/kg wet0.0490 0.0050 0.05000 66-12598
1,2,4-Trimethylbenzene mg/kg wet0.0490 0.0050 0.05000 69-12998
1,2-Dibromoethane mg/kg wet0.0468 0.0050 0.05000 70-13294
1,2-Dichlorobenzene mg/kg wet0.0478 0.0050 0.05000 72-12396
1,2-Dichloroethane mg/kg wet0.0433 0.0050 0.05000 68-12887
1,2-Dichloropropane mg/kg wet0.0436 0.0050 0.05000 73-13087
1,3,5-Trimethylbenzene mg/kg wet0.0489 0.0050 0.05000 69-12898
1,3-Dichlorobenzene mg/kg wet0.0481 0.0050 0.05000 71-12096
1,3-Dichloropropane mg/kg wet0.0459 0.0050 0.05000 75-12492
1,4-Dichlorobenzene mg/kg wet0.0471 0.0050 0.05000 71-12394
2,2-Dichloropropane mg/kg wet0.0424 0.0050 0.05000 50-14285
2-Chlorotoluene mg/kg wet0.0482 0.0050 0.05000 67-12496
4-Chlorotoluene mg/kg wet0.0483 0.0050 0.05000 71-12697
4-Isopropyltoluene mg/kg wet0.0501 0.0050 0.05000 68-129100
Acetone mg/kg wet0.0922 0.050 0.1000 29-19892
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0276 - 5035
LCS (P8K0276-BS1)Prepared & Analyzed: 11/15/18
Benzene mg/kg wet0.0431 0.0030 0.05000 74-12786
Bromobenzene mg/kg wet0.0470 0.0050 0.05000 73-12594
Bromochloromethane mg/kg wet0.0432 0.0050 0.05000 72-13486
Bromodichloromethane mg/kg wet0.0444 0.0050 0.05000 75-12289
Bromoform mg/kg wet0.0484 0.0050 0.05000 66-13597
Bromomethane mg/kg wet0.0317 0.010 0.05000 20-18063
Carbon Tetrachloride mg/kg wet0.0423 0.0050 0.05000 64-14385
Chlorobenzene mg/kg wet0.0452 0.0050 0.05000 74-11890
Chloroethane mg/kg wet0.0374 0.010 0.05000 33-14975
Chloroform mg/kg wet0.0439 0.0050 0.05000 73-12788
Chloromethane mg/kg wet0.0302 0.0050 0.05000 45-14360
cis-1,2-Dichloroethylene mg/kg wet0.0422 0.0050 0.05000 76-13484
cis-1,3-Dichloropropylene mg/kg wet0.0450 0.0050 0.05000 71-12590
Dibromochloromethane mg/kg wet0.0471 0.0050 0.05000 73-12294
Dichlorodifluoromethane mg/kg wet0.0326 0.0050 0.05000 26-14665
Ethylbenzene mg/kg wet0.0454 0.0050 0.05000 74-12891
Isopropyl Ether mg/kg wet0.0451 0.0050 0.05000 59-15990
Isopropylbenzene (Cumene)mg/kg wet0.0491 0.0050 0.05000 68-12698
m,p-Xylenes mg/kg wet0.0947 0.010 0.1000 75-12495
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0516 0.050 0.05000 61-157103
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0460 0.10 0.05000 J63-14992
Methyl Isobutyl Ketone mg/kg wet0.0486 0.050 0.05000 J57-16297
Methylene Chloride mg/kg wet0.0414 0.010 0.05000 74-12983
Methyl-tert-Butyl Ether mg/kg wet0.0464 0.010 0.05000 70-13093
Naphthalene mg/kg wet0.0507 0.010 0.05000 57-157101
n-Butylbenzene mg/kg wet0.0504 0.0050 0.05000 65-135101
n-Propylbenzene mg/kg wet0.0489 0.0050 0.05000 67-13098
o-Xylene mg/kg wet0.0463 0.0050 0.05000 74-12693
sec-Butylbenzene mg/kg wet0.0488 0.0050 0.05000 66-13198
Styrene mg/kg wet0.0472 0.0050 0.05000 77-12194
tert-Butylbenzene mg/kg wet0.0486 0.0050 0.05000 67-13297
Tetrachloroethylene mg/kg wet0.0432 0.0050 0.05000 68-13086
Toluene mg/kg wet0.0426 0.0050 0.05000 71-12985
trans-1,2-Dichloroethylene mg/kg wet0.0407 0.0050 0.05000 73-13281
trans-1,3-Dichloropropylene mg/kg wet0.0456 0.0050 0.05000 68-12391
Trichloroethylene mg/kg wet0.0435 0.0050 0.05000 75-13387
Trichlorofluoromethane mg/kg wet0.0373 0.0050 0.05000 44-14675
Vinyl acetate mg/kg wet0.0511 0.025 0.05000 85-161102
Vinyl chloride mg/kg wet0.0356 0.0050 0.05000 48-14771
Xylenes, total mg/kg wet0.141 0.015 0.1500 74-12694
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.1
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.5
ug/L 50.00 76-129Surrogate: Toluene-d8 10351.3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0276 - 5035
LCS Dup (P8K0276-BSD1)Prepared & Analyzed: 11/15/18
1,1,1,2-Tetrachloroethane mg/kg wet0.0464 0.0050 0.05000 2072-11593 0.5
1,1,1-Trichloroethane mg/kg wet0.0415 0.0050 0.05000 2067-13183 1
1,1,2,2-Tetrachloroethane mg/kg wet0.0498 0.0050 0.05000 2056-126100 0.06
1,1,2-Trichloroethane mg/kg wet0.0471 0.0050 0.05000 2070-13394 3
1,1-Dichloroethane mg/kg wet0.0418 0.0050 0.05000 2074-12784 0
1,1-Dichloroethylene mg/kg wet0.0377 0.0050 0.05000 2067-14975 1
1,1-Dichloropropylene mg/kg wet0.0419 0.0050 0.05000 2071-13084 1
1,2,3-Trichlorobenzene mg/kg wet0.0492 0.0050 0.05000 2068-13098 2
1,2,3-Trichloropropane mg/kg wet0.0485 0.0050 0.05000 2060-13797 1
1,2,4-Trichlorobenzene mg/kg wet0.0492 0.0050 0.05000 2066-12598 0.4
1,2,4-Trimethylbenzene mg/kg wet0.0485 0.0050 0.05000 2069-12997 1
1,2-Dibromoethane mg/kg wet0.0472 0.0050 0.05000 2070-13294 0.8
1,2-Dichlorobenzene mg/kg wet0.0478 0.0050 0.05000 2072-12396 0.06
1,2-Dichloroethane mg/kg wet0.0441 0.0050 0.05000 2068-12888 2
1,2-Dichloropropane mg/kg wet0.0444 0.0050 0.05000 2073-13089 2
1,3,5-Trimethylbenzene mg/kg wet0.0484 0.0050 0.05000 2069-12897 1
1,3-Dichlorobenzene mg/kg wet0.0479 0.0050 0.05000 2071-12096 0.3
1,3-Dichloropropane mg/kg wet0.0467 0.0050 0.05000 2075-12493 2
1,4-Dichlorobenzene mg/kg wet0.0474 0.0050 0.05000 2071-12395 0.5
2,2-Dichloropropane mg/kg wet0.0421 0.0050 0.05000 2050-14284 0.6
2-Chlorotoluene mg/kg wet0.0477 0.0050 0.05000 2067-12495 1
4-Chlorotoluene mg/kg wet0.0481 0.0050 0.05000 2071-12696 0.3
4-Isopropyltoluene mg/kg wet0.0489 0.0050 0.05000 2068-12998 3
Acetone mg/kg wet0.0907 0.050 0.1000 2029-19891 2
Benzene mg/kg wet0.0432 0.0030 0.05000 2074-12786 0.3
Bromobenzene mg/kg wet0.0474 0.0050 0.05000 2073-12595 0.8
Bromochloromethane mg/kg wet0.0435 0.0050 0.05000 2072-13487 0.7
Bromodichloromethane mg/kg wet0.0454 0.0050 0.05000 2075-12291 2
Bromoform mg/kg wet0.0485 0.0050 0.05000 2066-13597 0.2
Bromomethane mg/kg wet0.0362 0.010 0.05000 2020-18072 13
Carbon Tetrachloride mg/kg wet0.0414 0.0050 0.05000 2064-14383 2
Chlorobenzene mg/kg wet0.0451 0.0050 0.05000 2074-11890 0.2
Chloroethane mg/kg wet0.0375 0.010 0.05000 2033-14975 0.2
Chloroform mg/kg wet0.0442 0.0050 0.05000 2073-12788 0.9
Chloromethane mg/kg wet0.0322 0.0050 0.05000 2045-14364 7
cis-1,2-Dichloroethylene mg/kg wet0.0429 0.0050 0.05000 2076-13486 2
cis-1,3-Dichloropropylene mg/kg wet0.0461 0.0050 0.05000 2071-12592 2
Dibromochloromethane mg/kg wet0.0479 0.0050 0.05000 2073-12296 2
Dichlorodifluoromethane mg/kg wet0.0318 0.0050 0.05000 2026-14664 3
Ethylbenzene mg/kg wet0.0449 0.0050 0.05000 2074-12890 0.9
Isopropyl Ether mg/kg wet0.0460 0.0050 0.05000 2059-15992 2
Isopropylbenzene (Cumene)mg/kg wet0.0485 0.0050 0.05000 2068-12697 1
m,p-Xylenes mg/kg wet0.0940 0.010 0.1000 2075-12494 0.7
Methyl Butyl Ketone (2-Hexanone)mg/kg wet0.0499 0.050 0.05000 20 J61-157100 3
Methyl Ethyl Ketone (2-Butanone)mg/kg wet0.0452 0.10 0.05000 20 J63-14990 2
Methyl Isobutyl Ketone mg/kg wet0.0476 0.050 0.05000 20 J57-16295 2
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8K0276 - 5035
LCS Dup (P8K0276-BSD1)Prepared & Analyzed: 11/15/18
Methylene Chloride mg/kg wet0.0426 0.010 0.05000 2074-12985 3
Methyl-tert-Butyl Ether mg/kg wet0.0461 0.010 0.05000 2070-13092 0.5
Naphthalene mg/kg wet0.0504 0.010 0.05000 2057-157101 0.7
n-Butylbenzene mg/kg wet0.0494 0.0050 0.05000 2065-13599 2
n-Propylbenzene mg/kg wet0.0480 0.0050 0.05000 2067-13096 2
o-Xylene mg/kg wet0.0466 0.0050 0.05000 2074-12693 0.8
sec-Butylbenzene mg/kg wet0.0479 0.0050 0.05000 2066-13196 2
Styrene mg/kg wet0.0478 0.0050 0.05000 2077-12196 1
tert-Butylbenzene mg/kg wet0.0476 0.0050 0.05000 2067-13295 2
Tetrachloroethylene mg/kg wet0.0424 0.0050 0.05000 2068-13085 2
Toluene mg/kg wet0.0426 0.0050 0.05000 2071-12985 0.09
trans-1,2-Dichloroethylene mg/kg wet0.0406 0.0050 0.05000 2073-13281 0.3
trans-1,3-Dichloropropylene mg/kg wet0.0466 0.0050 0.05000 2068-12393 2
Trichloroethylene mg/kg wet0.0432 0.0050 0.05000 2075-13386 0.8
Trichlorofluoromethane mg/kg wet0.0360 0.0050 0.05000 2044-14672 4
Vinyl acetate mg/kg wet0.0506 0.025 0.05000 2085-161101 0.8
Vinyl chloride mg/kg wet0.0350 0.0050 0.05000 2048-14770 2
Xylenes, total mg/kg wet0.141 0.015 0.1500 2074-12694 0.2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.7
ug/L 50.00 84-123Surrogate: Dibromofluoromethane 10351.6
ug/L 50.00 76-129Surrogate: Toluene-d8 10351.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0249 - 3546
Blank (P8K0249-BLK1)Prepared: 11/14/18 Analyzed: 11/15/18
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0249 - 3546
Blank (P8K0249-BLK1)Prepared: 11/14/18 Analyzed: 11/15/18
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 872.89
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 961.61
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 923.08
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 871.44
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 913.05
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 961.61
LCS (P8K0249-BS1)Prepared: 11/14/18 Analyzed: 11/15/18
1,2,4-Trichlorobenzene mg/kg wet1.09 0.33 1.667 34-11866
1,2-Dichlorobenzene mg/kg wet1.13 0.33 1.667 33-11768
1,3-Dichlorobenzene mg/kg wet1.07 0.33 1.667 30-11564
1,4-Dichlorobenzene mg/kg wet1.11 0.33 1.667 31-11566
1-Methylnaphthalene mg/kg wet1.26 0.33 1.667 40-11976
2,4,6-Trichlorophenol mg/kg wet1.43 0.33 1.667 39-12686
2,4-Dichlorophenol mg/kg wet1.21 0.33 1.667 40-12272
2,4-Dimethylphenol mg/kg wet1.68 0.33 1.667 30-127101
2,4-Dinitrophenol mg/kg wet0.831 0.33 1.667 27-12950
2,4-Dinitrotoluene mg/kg wet1.54 0.33 1.667 48-12693
2,6-Dinitrotoluene mg/kg wet1.50 0.33 1.667 46-12490
2-Chloronaphthalene mg/kg wet1.39 0.33 1.667 41-11483
2-Chlorophenol mg/kg wet1.30 0.33 1.667 34-12178
2-Methylnaphthalene mg/kg wet1.22 0.33 1.667 38-12273
2-Methylphenol mg/kg wet1.40 0.33 1.667 32-12284
2-Nitrophenol mg/kg wet1.13 0.33 1.667 36-12368
3,3’-Dichlorobenzidine mg/kg wet1.82 0.33 1.667 22-121109
3/4-Methylphenol mg/kg wet1.25 0.33 1.667 34-11975
4,6-Dinitro-2-methylphenol mg/kg wet1.13 0.33 1.667 29-13268
4-Bromophenyl phenyl ether mg/kg wet1.53 0.33 1.667 46-12492
4-Chloro-3-methylphenol mg/kg wet1.27 0.33 1.667 45-12276
4-Chloroaniline mg/kg wet1.37 0.33 1.667 17-10682
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0249 - 3546
LCS (P8K0249-BS1)Prepared: 11/14/18 Analyzed: 11/15/18
4-Chlorophenyl phenyl ether mg/kg wet1.47 0.33 1.667 45-12188
4-Nitrophenol mg/kg wet1.42 0.33 1.667 30-13285
Acenaphthene mg/kg wet1.45 0.33 1.667 40-12387
Acenaphthylene mg/kg wet1.52 0.33 1.667 32-13291
Anthracene mg/kg wet1.69 0.33 1.667 47-123101
Azobenzene mg/kg wet1.50 0.33 1.667 39-12590
Benzo(a)anthracene mg/kg wet1.64 0.33 1.667 49-12698
Benzo(a)pyrene mg/kg wet1.68 0.33 1.667 45-129101
Benzo(b)fluoranthene mg/kg wet1.61 0.33 1.667 45-13297
Benzo(g,h,i)perylene mg/kg wet1.64 0.33 1.667 43-13499
Benzo(k)fluoranthene mg/kg wet1.64 0.33 1.667 47-13298
Benzoic Acid mg/kg wet0.385 0.33 1.667 10-8323
Benzyl alcohol mg/kg wet1.35 0.33 1.667 29-12281
bis(2-Chloroethoxy)methane mg/kg wet1.29 0.33 1.667 36-12177
Bis(2-Chloroethyl)ether mg/kg wet0.997 0.33 1.667 31-12060
Bis(2-chloroisopropyl)ether mg/kg wet1.26 0.33 1.667 33-13175
Bis(2-Ethylhexyl)phthalate mg/kg wet1.73 0.33 1.667 51-133104
Butyl benzyl phthalate mg/kg wet1.65 0.33 1.667 48-13299
Chrysene mg/kg wet1.63 0.33 1.667 50-12498
Dibenzo(a,h)anthracene mg/kg wet1.06 0.33 1.667 45-13464
Dibenzofuran mg/kg wet1.49 0.33 1.667 44-12090
Diethyl phthalate mg/kg wet1.56 0.33 1.667 50-12494
Dimethyl phthalate mg/kg wet1.52 0.33 1.667 48-12491
Di-n-butyl phthalate mg/kg wet1.67 0.33 1.667 51-128100
Di-n-octyl phthalate mg/kg wet1.81 0.33 1.667 45-140109
Fluoranthene mg/kg wet1.60 0.33 1.667 50-12796
Fluorene mg/kg wet1.56 0.33 1.667 43-12593
Hexachlorobenzene mg/kg wet1.48 0.33 1.667 45-12289
Hexachlorobutadiene mg/kg wet1.19 0.33 1.667 32-12371
Hexachlorocyclopentadiene mg/kg wet1.25 0.33 1.667 32-11775
Hexachloroethane mg/kg wet1.08 0.33 1.667 28-11765
Indeno(1,2,3-cd)pyrene mg/kg wet1.82 0.33 1.667 45-133109
Isophorone mg/kg wet1.35 0.33 1.667 30-12281
Naphthalene mg/kg wet1.22 0.33 1.667 35-12373
Nitrobenzene mg/kg wet1.18 0.33 1.667 34-12271
N-Nitroso-di-n-propylamine mg/kg wet1.26 0.33 1.667 36-12075
N-Nitrosodiphenylamine mg/kg wet1.90 0.33 1.667 38-127114
Pentachlorophenol mg/kg wet1.20 0.33 1.667 25-13372
Phenanthrene mg/kg wet1.62 0.33 1.667 50-12197
Phenol mg/kg wet1.33 0.33 1.667 34-12180
Pyrene mg/kg wet1.64 0.33 1.667 47-12798
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 902.99
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 831.39
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 782.60
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 651.09
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 782.61
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0249 - 3546
LCS (P8K0249-BS1)Prepared: 11/14/18 Analyzed: 11/15/18
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 901.50
LCS Dup (P8K0249-BSD1)Prepared: 11/14/18 Analyzed: 11/15/18
1,2,4-Trichlorobenzene mg/kg wet1.21 0.33 1.667 2034-11873 10
1,2-Dichlorobenzene mg/kg wet1.25 0.33 1.667 2033-11775 10
1,3-Dichlorobenzene mg/kg wet1.18 0.33 1.667 2030-11571 10
1,4-Dichlorobenzene mg/kg wet1.23 0.33 1.667 2031-11574 11
1-Methylnaphthalene mg/kg wet1.39 0.33 1.667 2040-11983 10
2,4,6-Trichlorophenol mg/kg wet1.58 0.33 1.667 2039-12695 10
2,4-Dichlorophenol mg/kg wet1.38 0.33 1.667 2040-12283 14
2,4-Dimethylphenol mg/kg wet1.84 0.33 1.667 2030-127110 9
2,4-Dinitrophenol mg/kg wet1.05 0.33 1.667 20 D27-12963 24
2,4-Dinitrotoluene mg/kg wet1.68 0.33 1.667 2048-126101 9
2,6-Dinitrotoluene mg/kg wet1.65 0.33 1.667 2046-12499 10
2-Chloronaphthalene mg/kg wet1.56 0.33 1.667 2041-11494 11
2-Chlorophenol mg/kg wet1.46 0.33 1.667 2034-12188 12
2-Methylnaphthalene mg/kg wet1.35 0.33 1.667 2038-12281 10
2-Methylphenol mg/kg wet1.58 0.33 1.667 2032-12295 12
2-Nitrophenol mg/kg wet1.27 0.33 1.667 2036-12376 12
3,3’-Dichlorobenzidine mg/kg wet1.93 0.33 1.667 2022-121116 6
3/4-Methylphenol mg/kg wet1.41 0.33 1.667 2034-11985 12
4,6-Dinitro-2-methylphenol mg/kg wet1.39 0.33 1.667 20 D29-13284 21
4-Bromophenyl phenyl ether mg/kg wet1.68 0.33 1.667 2046-124101 9
4-Chloro-3-methylphenol mg/kg wet1.37 0.33 1.667 2045-12282 8
4-Chloroaniline mg/kg wet1.52 0.33 1.667 2017-10691 10
4-Chlorophenyl phenyl ether mg/kg wet1.61 0.33 1.667 2045-12197 9
4-Nitrophenol mg/kg wet1.49 0.33 1.667 2030-13289 4
Acenaphthene mg/kg wet1.61 0.33 1.667 2040-12396 10
Acenaphthylene mg/kg wet1.66 0.33 1.667 2032-132100 9
Anthracene mg/kg wet1.84 0.33 1.667 2047-123111 9
Azobenzene mg/kg wet1.62 0.33 1.667 2039-12597 8
Benzo(a)anthracene mg/kg wet1.77 0.33 1.667 2049-126106 8
Benzo(a)pyrene mg/kg wet1.82 0.33 1.667 2045-129109 8
Benzo(b)fluoranthene mg/kg wet1.72 0.33 1.667 2045-132103 6
Benzo(g,h,i)perylene mg/kg wet1.80 0.33 1.667 2043-134108 9
Benzo(k)fluoranthene mg/kg wet1.77 0.33 1.667 2047-132106 8
Benzoic Acid mg/kg wet0.756 0.33 1.667 20 D10-8345 65
Benzyl alcohol mg/kg wet1.57 0.33 1.667 2029-12294 15
bis(2-Chloroethoxy)methane mg/kg wet1.44 0.33 1.667 2036-12186 11
Bis(2-Chloroethyl)ether mg/kg wet1.36 0.33 1.667 20 D31-12082 31
Bis(2-chloroisopropyl)ether mg/kg wet1.40 0.33 1.667 2033-13184 11
Bis(2-Ethylhexyl)phthalate mg/kg wet1.82 0.33 1.667 2051-133109 5
Butyl benzyl phthalate mg/kg wet1.77 0.33 1.667 2048-132106 7
Chrysene mg/kg wet1.77 0.33 1.667 2050-124106 8
Dibenzo(a,h)anthracene mg/kg wet1.36 0.33 1.667 20 D45-13482 25
Dibenzofuran mg/kg wet1.64 0.33 1.667 2044-12098 9
Diethyl phthalate mg/kg wet1.70 0.33 1.667 2050-124102 8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0249 - 3546
LCS Dup (P8K0249-BSD1)Prepared: 11/14/18 Analyzed: 11/15/18
Dimethyl phthalate mg/kg wet1.66 0.33 1.667 2048-12499 9
Di-n-butyl phthalate mg/kg wet1.80 0.33 1.667 2051-128108 8
Di-n-octyl phthalate mg/kg wet1.93 0.33 1.667 2045-140116 6
Fluoranthene mg/kg wet1.73 0.33 1.667 2050-127104 7
Fluorene mg/kg wet1.69 0.33 1.667 2043-125102 8
Hexachlorobenzene mg/kg wet1.63 0.33 1.667 2045-12298 10
Hexachlorobutadiene mg/kg wet1.29 0.33 1.667 2032-12378 8
Hexachlorocyclopentadiene mg/kg wet1.46 0.33 1.667 2032-11788 16
Hexachloroethane mg/kg wet1.19 0.33 1.667 2028-11772 10
Indeno(1,2,3-cd)pyrene mg/kg wet1.74 0.33 1.667 2045-133105 4
Isophorone mg/kg wet1.50 0.33 1.667 2030-12290 10
Naphthalene mg/kg wet1.30 0.33 1.667 2035-12378 7
Nitrobenzene mg/kg wet1.28 0.33 1.667 2034-12277 8
N-Nitroso-di-n-propylamine mg/kg wet1.43 0.33 1.667 2036-12086 13
N-Nitrosodiphenylamine mg/kg wet2.05 0.33 1.667 2038-127123 8
Pentachlorophenol mg/kg wet1.40 0.33 1.667 2025-13384 16
Phenanthrene mg/kg wet1.73 0.33 1.667 2050-121104 6
Phenol mg/kg wet1.51 0.33 1.667 2034-12191 12
Pyrene mg/kg wet1.76 0.33 1.667 2047-127106 7
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 983.27
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 941.56
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 872.89
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 721.19
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 872.89
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 961.60
Batch P8K0265 - 3510C MS
Blank (P8K0265-BLK1)Prepared & Analyzed: 11/15/18
1,2,4-Trichlorobenzene ug/LBRL10
1,2-Dichlorobenzene ug/LBRL10
1,3-Dichlorobenzene ug/LBRL10
1,4-Dichlorobenzene ug/LBRL10
1-Methylnaphthalene ug/LBRL10
2,4,5-Trichlorophenol ug/LBRL10
2,4,6-Trichlorophenol ug/LBRL10
2,4-Dichlorophenol ug/LBRL10
2,4-Dimethylphenol ug/LBRL10
2,4-Dinitrophenol ug/LBRL10
2,4-Dinitrotoluene ug/LBRL10
2,6-Dinitrotoluene ug/LBRL10
2-Chloronaphthalene ug/LBRL10
2-Chlorophenol ug/LBRL10
2-Methylnaphthalene ug/LBRL10
2-Methylphenol ug/LBRL10
2-Nitroaniline ug/LBRL10
2-Nitrophenol ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0265 - 3510C MS
Blank (P8K0265-BLK1)Prepared & Analyzed: 11/15/18
3,3’-Dichlorobenzidine ug/LBRL10
3/4-Methylphenol ug/LBRL10
3-Nitroaniline ug/LBRL10
4,6-Dinitro-2-methylphenol ug/LBRL10
4-Bromophenyl phenyl ether ug/LBRL10
4-Chloro-3-methylphenol ug/LBRL10
4-Chloroaniline ug/LBRL10
4-Chlorophenyl phenyl ether ug/LBRL10
4-Nitroaniline ug/LBRL10
4-Nitrophenol ug/LBRL10
Acenaphthene ug/LBRL10
Acenaphthylene ug/LBRL10
Aniline ug/LBRL10
Anthracene ug/LBRL10
Azobenzene ug/LBRL10
Benzo(a)anthracene ug/LBRL10
Benzo(a)pyrene ug/LBRL10
Benzo(b)fluoranthene ug/LBRL10
Benzo(g,h,i)perylene ug/LBRL10
Benzo(k)fluoranthene ug/LBRL10
Benzoic Acid ug/LBRL100
Benzyl alcohol ug/LBRL10
bis(2-Chloroethoxy)methane ug/LBRL10
Bis(2-Chloroethyl)ether ug/LBRL10
Bis(2-chloroisopropyl)ether ug/LBRL10
Bis(2-Ethylhexyl)phthalate ug/LBRL10
Butyl benzyl phthalate ug/LBRL10
Chrysene ug/LBRL10
Dibenzo(a,h)anthracene ug/LBRL10
Dibenzofuran ug/LBRL10
Diethyl phthalate ug/LBRL10
Dimethyl phthalate ug/LBRL10
Di-n-butyl phthalate ug/LBRL10
Di-n-octyl phthalate ug/LBRL10
Fluoranthene ug/LBRL10
Fluorene ug/LBRL10
Hexachlorobenzene ug/LBRL10
Hexachlorobutadiene ug/LBRL10
Hexachlorocyclopentadiene ug/LBRL10
Hexachloroethane ug/LBRL10
Indeno(1,2,3-cd)pyrene ug/LBRL10
Isophorone ug/LBRL10
Naphthalene ug/LBRL10
Nitrobenzene ug/LBRL10
N-Nitroso-di-n-propylamine ug/LBRL10
N-Nitrosodiphenylamine ug/LBRL10
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0265 - 3510C MS
Blank (P8K0265-BLK1)Prepared & Analyzed: 11/15/18
Pentachlorophenol ug/LBRL10
Phenanthrene ug/LBRL10
Phenol ug/LBRL10
Pyrene ug/LBRL10
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 122122
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 11758.3
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 7877.5
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 11255.8
ug/L 100.0 11-52Surrogate: Phenol-d5 4949.1
ug/L 50.00 50-134Surrogate: Terphenyl-d14 12562.3
LCS (P8K0265-BS1)Prepared & Analyzed: 11/15/18
1,2,4-Trichlorobenzene ug/L37.3 10 50.00 29-12675
1,2-Dichlorobenzene ug/L39.1 10 50.00 32-11178
1,3-Dichlorobenzene ug/L37.1 10 50.00 28-11074
1,4-Dichlorobenzene ug/L38.4 10 50.00 29-11277
1-Methylnaphthalene ug/L44.7 10 50.00 41-11989
2,4,5-Trichlorophenol ug/L52.5 10 50.00 53-123105
2,4,6-Trichlorophenol ug/L52.2 10 50.00 50-125104
2,4-Dichlorophenol ug/L44.3 10 50.00 47-12189
2,4-Dimethylphenol ug/L54.8 10 50.00 31-124110
2,4-Dinitrophenol ug/L42.4 10 50.00 23-14385
2,4-Dinitrotoluene ug/L55.9 10 50.00 57-128112
2,6-Dinitrotoluene ug/L55.6 10 50.00 57-124111
2-Chloronaphthalene ug/L50.1 10 50.00 40-116100
2-Chlorophenol ug/L46.7 10 50.00 38-11793
2-Methylnaphthalene ug/L42.2 10 50.00 40-12184
2-Methylphenol ug/L45.0 10 50.00 30-11790
2-Nitroaniline ug/L53.7 10 50.00 55-127107
2-Nitrophenol ug/L42.7 10 50.00 47-12385
3,3’-Dichlorobenzidine ug/L66.7 10 50.00 LH27-129133
3/4-Methylphenol ug/L36.9 10 50.00 29-11074
3-Nitroaniline ug/L54.8 10 50.00 41-128110
4,6-Dinitro-2-methylphenol ug/L51.3 10 50.00 44-137103
4-Bromophenyl phenyl ether ug/L56.1 10 50.00 55-124112
4-Chloro-3-methylphenol ug/L43.0 10 50.00 52-11986
4-Chloroaniline ug/L50.6 10 50.00 33-117101
4-Chlorophenyl phenyl ether ug/L52.7 10 50.00 53-121105
4-Nitroaniline ug/L54.0 10 50.00 45-135108
4-Nitrophenol ug/L24.8 10 50.00 10-7750
Acenaphthene ug/L51.9 10 50.00 47-122104
Acenaphthylene ug/L53.6 10 50.00 41-130107
Aniline ug/L91.5 10 50.00 12-197183
Anthracene ug/L61.2 10 50.00 57-123122
Azobenzene ug/L54.0 10 50.00 61-116108
Benzo(a)anthracene ug/L58.6 10 50.00 58-125117
Benzo(a)pyrene ug/L58.5 10 50.00 54-128117
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0265 - 3510C MS
LCS (P8K0265-BS1)Prepared & Analyzed: 11/15/18
Benzo(b)fluoranthene ug/L58.6 10 50.00 53-131117
Benzo(g,h,i)perylene ug/L58.8 10 50.00 50-134118
Benzo(k)fluoranthene ug/L55.9 10 50.00 57-129112
Benzoic Acid ug/LBRL100 50.00 L10-125
Benzyl alcohol ug/L46.7 10 50.00 31-11293
bis(2-Chloroethoxy)methane ug/L50.2 10 50.00 48-120100
Bis(2-Chloroethyl)ether ug/L43.4 10 50.00 43-11887
Bis(2-chloroisopropyl)ether ug/L49.4 10 50.00 37-13099
Bis(2-Ethylhexyl)phthalate ug/L60.3 10 50.00 55-135121
Butyl benzyl phthalate ug/L59.3 10 50.00 53-134119
Chrysene ug/L59.3 10 50.00 59-123119
Dibenzo(a,h)anthracene ug/L41.2 10 50.00 51-13482
Dibenzofuran ug/L52.8 10 50.00 53-118106
Diethyl phthalate ug/L55.4 10 50.00 56-125111
Dimethyl phthalate ug/L54.5 10 50.00 45-127109
Di-n-butyl phthalate ug/L59.2 10 50.00 59-127118
Di-n-octyl phthalate ug/L62.2 10 50.00 51-140124
Fluoranthene ug/L57.2 10 50.00 57-128114
Fluorene ug/L55.2 10 50.00 52-124110
Hexachlorobenzene ug/L54.2 10 50.00 53-125108
Hexachlorobutadiene ug/L37.1 10 50.00 22-12474
Hexachlorocyclopentadiene ug/L42.8 10 50.00 32-11786
Hexachloroethane ug/L36.3 10 50.00 21-11573
Indeno(1,2,3-cd)pyrene ug/L64.9 10 50.00 52-134130
Isophorone ug/L50.9 10 50.00 42-124102
Naphthalene ug/L42.0 10 50.00 40-12184
Nitrobenzene ug/L45.6 10 50.00 45-12191
N-Nitroso-di-n-propylamine ug/L46.8 10 50.00 49-11994
N-Nitrosodiphenylamine ug/L66.8 10 50.00 LH51-123134
Pentachlorophenol ug/L54.8 10 50.00 35-138110
Phenanthrene ug/L57.4 10 50.00 59-120115
Phenol ug/L24.8 10 50.00 12-5850
Pyrene ug/L58.6 10 50.00 57-126117
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 107107
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 9849.2
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 6565.0
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8542.7
ug/L 100.0 11-52Surrogate: Phenol-d5 4241.8
ug/L 50.00 50-134Surrogate: Terphenyl-d14 10853.9
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0265 - 3510C MS
LCS Dup (P8K0265-BSD1)Prepared & Analyzed: 11/15/18
1,2,4-Trichlorobenzene ug/L36.5 10 50.00 2029-12673 2
1,2-Dichlorobenzene ug/L38.8 10 50.00 2032-11178 0.8
1,3-Dichlorobenzene ug/L36.9 10 50.00 2028-11074 0.5
1,4-Dichlorobenzene ug/L37.3 10 50.00 2029-11275 3
1-Methylnaphthalene ug/L44.6 10 50.00 2041-11989 0.2
2,4,5-Trichlorophenol ug/L49.3 10 50.00 2053-12399 6
2,4,6-Trichlorophenol ug/L46.5 10 50.00 2050-12593 12
2,4-Dichlorophenol ug/L41.2 10 50.00 2047-12182 7
2,4-Dimethylphenol ug/L53.9 10 50.00 2031-124108 2
2,4-Dinitrophenol ug/L28.7 10 50.00 20 D23-14357 39
2,4-Dinitrotoluene ug/L55.9 10 50.00 2057-128112 0
2,6-Dinitrotoluene ug/L56.3 10 50.00 2057-124113 1
2-Chloronaphthalene ug/L50.3 10 50.00 2040-116101 0.5
2-Chlorophenol ug/L43.8 10 50.00 2038-11788 6
2-Methylnaphthalene ug/L42.0 10 50.00 2040-12184 0.4
2-Methylphenol ug/L46.2 10 50.00 2030-11792 3
2-Nitroaniline ug/L54.3 10 50.00 2055-127109 1
2-Nitrophenol ug/L41.2 10 50.00 2047-12382 4
3,3’-Dichlorobenzidine ug/L68.1 10 50.00 20 LH27-129136 2
3/4-Methylphenol ug/L37.2 10 50.00 2029-11074 0.8
3-Nitroaniline ug/L55.3 10 50.00 2041-128111 0.9
4,6-Dinitro-2-methylphenol ug/L39.8 10 50.00 20 D44-13780 25
4-Bromophenyl phenyl ether ug/L56.8 10 50.00 2055-124114 1
4-Chloro-3-methylphenol ug/L43.7 10 50.00 2052-11987 2
4-Chloroaniline ug/L51.4 10 50.00 2033-117103 2
4-Chlorophenyl phenyl ether ug/L52.7 10 50.00 2053-121105 0.02
4-Nitroaniline ug/L56.2 10 50.00 2045-135112 4
4-Nitrophenol ug/L23.1 10 50.00 2010-7746 7
Acenaphthene ug/L52.7 10 50.00 2047-122105 2
Acenaphthylene ug/L54.2 10 50.00 2041-130108 1
Aniline ug/L96.3 10 50.00 2012-197193 5
Anthracene ug/L61.8 10 50.00 20 L157-123124 0.8
Azobenzene ug/L55.5 10 50.00 2061-116111 3
Benzo(a)anthracene ug/L59.2 10 50.00 2058-125118 1
Benzo(a)pyrene ug/L61.1 10 50.00 2054-128122 4
Benzo(b)fluoranthene ug/L57.8 10 50.00 2053-131116 1
Benzo(g,h,i)perylene ug/L60.8 10 50.00 2050-134122 3
Benzo(k)fluoranthene ug/L60.7 10 50.00 2057-129121 8
Benzoic Acid ug/LBRL100 50.00 20 L10-125
Benzyl alcohol ug/L46.9 10 50.00 2031-11294 0.4
bis(2-Chloroethoxy)methane ug/L48.8 10 50.00 2048-12098 3
Bis(2-Chloroethyl)ether ug/L42.1 10 50.00 2043-11884 3
Bis(2-chloroisopropyl)ether ug/L50.6 10 50.00 2037-130101 2
Bis(2-Ethylhexyl)phthalate ug/L60.5 10 50.00 2055-135121 0.4
Butyl benzyl phthalate ug/L59.3 10 50.00 2053-134119 0
Chrysene ug/L59.7 10 50.00 2059-123119 0.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0265 - 3510C MS
LCS Dup (P8K0265-BSD1)Prepared & Analyzed: 11/15/18
Dibenzo(a,h)anthracene ug/L42.3 10 50.00 2051-13485 3
Dibenzofuran ug/L54.1 10 50.00 2053-118108 2
Diethyl phthalate ug/L56.7 10 50.00 2056-125113 2
Dimethyl phthalate ug/L55.4 10 50.00 2045-127111 2
Di-n-butyl phthalate ug/L60.6 10 50.00 2059-127121 2
Di-n-octyl phthalate ug/L65.3 10 50.00 2051-140131 5
Fluoranthene ug/L58.7 10 50.00 2057-128117 3
Fluorene ug/L56.0 10 50.00 2052-124112 1
Hexachlorobenzene ug/L55.5 10 50.00 2053-125111 2
Hexachlorobutadiene ug/L36.9 10 50.00 2022-12474 0.6
Hexachlorocyclopentadiene ug/L43.2 10 50.00 2032-11786 0.9
Hexachloroethane ug/L35.9 10 50.00 2021-11572 0.9
Indeno(1,2,3-cd)pyrene ug/L67.3 10 50.00 20 L252-134135 4
Isophorone ug/L50.7 10 50.00 2042-124101 0.4
Naphthalene ug/L41.9 10 50.00 2040-12184 0.2
Nitrobenzene ug/L45.5 10 50.00 2045-12191 0.2
N-Nitroso-di-n-propylamine ug/L48.8 10 50.00 2049-11998 4
N-Nitrosodiphenylamine ug/L67.9 10 50.00 20 LH51-123136 2
Pentachlorophenol ug/L39.9 10 50.00 20 D35-13880 31
Phenanthrene ug/L59.0 10 50.00 2059-120118 3
Phenol ug/L24.6 10 50.00 2012-5849 0.8
Pyrene ug/L58.9 10 50.00 2057-126118 0.5
ug/L 100.0 43-140Surrogate: 2,4,6-Tribromophenol 100100
ug/L 50.00 44-119Surrogate: 2-Fluorobiphenyl 9949.4
ug/L 100.0 19-119Surrogate: 2-Fluorophenol 5757.0
ug/L 50.00 44-120Surrogate: Nitrobenzene-d5 8441.8
ug/L 100.0 11-52Surrogate: Phenol-d5 4040.5
ug/L 50.00 50-134Surrogate: Terphenyl-d14 10853.8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0299 - 3546
Blank (P8K0299-BLK1)Prepared & Analyzed: 11/16/18
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0299 - 3546
Blank (P8K0299-BLK1)Prepared & Analyzed: 11/16/18
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 1013.35
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 1021.70
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 1003.33
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 911.51
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 973.23
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 1051.76
LCS (P8K0299-BS1)Prepared & Analyzed: 11/16/18
1,2,4-Trichlorobenzene mg/kg wet1.36 0.33 1.667 34-11881
1,2-Dichlorobenzene mg/kg wet1.45 0.33 1.667 33-11787
1,3-Dichlorobenzene mg/kg wet1.38 0.33 1.667 30-11583
1,4-Dichlorobenzene mg/kg wet1.43 0.33 1.667 31-11586
1-Methylnaphthalene mg/kg wet1.52 0.33 1.667 40-11991
2,4,6-Trichlorophenol mg/kg wet1.71 0.33 1.667 39-126103
2,4-Dichlorophenol mg/kg wet1.48 0.33 1.667 40-12289
2,4-Dimethylphenol mg/kg wet2.06 0.33 1.667 30-127123
2,4-Dinitrophenol mg/kg wet0.942 0.33 1.667 27-12957
2,4-Dinitrotoluene mg/kg wet1.78 0.33 1.667 48-126107
2,6-Dinitrotoluene mg/kg wet1.80 0.33 1.667 46-124108
2-Chloronaphthalene mg/kg wet1.69 0.33 1.667 41-114101
2-Chlorophenol mg/kg wet1.63 0.33 1.667 34-12198
2-Methylnaphthalene mg/kg wet1.45 0.33 1.667 38-12287
2-Methylphenol mg/kg wet1.75 0.33 1.667 32-122105
2-Nitrophenol mg/kg wet1.38 0.33 1.667 36-12383
3,3’-Dichlorobenzidine mg/kg wet1.84 0.33 1.667 22-121111
3/4-Methylphenol mg/kg wet1.54 0.33 1.667 34-11992
4,6-Dinitro-2-methylphenol mg/kg wet1.34 0.33 1.667 29-13280
4-Bromophenyl phenyl ether mg/kg wet1.81 0.33 1.667 46-124109
4-Chloro-3-methylphenol mg/kg wet1.48 0.33 1.667 45-12289
4-Chloroaniline mg/kg wet1.50 0.33 1.667 17-10690
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0299 - 3546
LCS (P8K0299-BS1)Prepared & Analyzed: 11/16/18
4-Chlorophenyl phenyl ether mg/kg wet1.74 0.33 1.667 45-121105
4-Nitrophenol mg/kg wet1.58 0.33 1.667 30-13295
Acenaphthene mg/kg wet1.74 0.33 1.667 40-123104
Acenaphthylene mg/kg wet1.82 0.33 1.667 32-132109
Anthracene mg/kg wet1.97 0.33 1.667 47-123118
Azobenzene mg/kg wet1.77 0.33 1.667 39-125106
Benzo(a)anthracene mg/kg wet1.91 0.33 1.667 49-126115
Benzo(a)pyrene mg/kg wet1.92 0.33 1.667 45-129115
Benzo(b)fluoranthene mg/kg wet1.86 0.33 1.667 45-132112
Benzo(g,h,i)perylene mg/kg wet1.91 0.33 1.667 43-134115
Benzo(k)fluoranthene mg/kg wet1.86 0.33 1.667 47-132112
Benzoic Acid mg/kg wet0.836 0.33 1.667 10-8350
Benzyl alcohol mg/kg wet1.74 0.33 1.667 29-122105
bis(2-Chloroethoxy)methane mg/kg wet1.56 0.33 1.667 36-12194
Bis(2-Chloroethyl)ether mg/kg wet1.47 0.33 1.667 31-12088
Bis(2-chloroisopropyl)ether mg/kg wet1.58 0.33 1.667 33-13195
Bis(2-Ethylhexyl)phthalate mg/kg wet1.96 0.33 1.667 51-133118
Butyl benzyl phthalate mg/kg wet1.90 0.33 1.667 48-132114
Chrysene mg/kg wet1.88 0.33 1.667 50-124113
Dibenzo(a,h)anthracene mg/kg wet1.33 0.33 1.667 45-13480
Dibenzofuran mg/kg wet1.75 0.33 1.667 44-120105
Diethyl phthalate mg/kg wet1.82 0.33 1.667 50-124109
Dimethyl phthalate mg/kg wet1.77 0.33 1.667 48-124106
Di-n-butyl phthalate mg/kg wet1.92 0.33 1.667 51-128115
Di-n-octyl phthalate mg/kg wet2.10 0.33 1.667 45-140126
Fluoranthene mg/kg wet1.88 0.33 1.667 50-127113
Fluorene mg/kg wet1.83 0.33 1.667 43-125110
Hexachlorobenzene mg/kg wet1.79 0.33 1.667 45-122108
Hexachlorobutadiene mg/kg wet1.48 0.33 1.667 32-12388
Hexachlorocyclopentadiene mg/kg wet1.53 0.33 1.667 32-11792
Hexachloroethane mg/kg wet1.40 0.33 1.667 28-11784
Indeno(1,2,3-cd)pyrene mg/kg wet2.12 0.33 1.667 45-133127
Isophorone mg/kg wet1.61 0.33 1.667 30-12297
Naphthalene mg/kg wet1.46 0.33 1.667 35-12387
Nitrobenzene mg/kg wet1.42 0.33 1.667 34-12285
N-Nitroso-di-n-propylamine mg/kg wet1.53 0.33 1.667 36-12092
N-Nitrosodiphenylamine mg/kg wet2.22 0.33 1.667 LH38-127133
Pentachlorophenol mg/kg wet1.37 0.33 1.667 25-13382
Phenanthrene mg/kg wet1.88 0.33 1.667 50-121113
Phenol mg/kg wet1.65 0.33 1.667 34-12199
Pyrene mg/kg wet1.89 0.33 1.667 47-127114
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 1053.49
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 1031.71
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 993.29
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 811.35
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 973.23
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0299 - 3546
LCS (P8K0299-BS1)Prepared & Analyzed: 11/16/18
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 1051.75
LCS Dup (P8K0299-BSD1)Prepared & Analyzed: 11/16/18
1,2,4-Trichlorobenzene mg/kg wet1.53 0.33 1.667 2034-11892 12
1,2-Dichlorobenzene mg/kg wet1.63 0.33 1.667 2033-11798 12
1,3-Dichlorobenzene mg/kg wet1.55 0.33 1.667 2030-11593 11
1,4-Dichlorobenzene mg/kg wet1.59 0.33 1.667 2031-11595 10
1-Methylnaphthalene mg/kg wet1.73 0.33 1.667 2040-119104 13
2,4,6-Trichlorophenol mg/kg wet1.99 0.33 1.667 2039-126119 15
2,4-Dichlorophenol mg/kg wet1.67 0.33 1.667 2040-122100 12
2,4-Dimethylphenol mg/kg wet2.26 0.33 1.667 20 L230-127136 10
2,4-Dinitrophenol mg/kg wet1.09 0.33 1.667 2027-12965 15
2,4-Dinitrotoluene mg/kg wet2.08 0.33 1.667 2048-126125 16
2,6-Dinitrotoluene mg/kg wet2.09 0.33 1.667 20 L246-124125 15
2-Chloronaphthalene mg/kg wet1.92 0.33 1.667 20 L241-114115 13
2-Chlorophenol mg/kg wet1.83 0.33 1.667 2034-121110 12
2-Methylnaphthalene mg/kg wet1.64 0.33 1.667 2038-12298 12
2-Methylphenol mg/kg wet1.93 0.33 1.667 2032-122116 10
2-Nitrophenol mg/kg wet1.58 0.33 1.667 2036-12395 13
3,3’-Dichlorobenzidine mg/kg wet2.17 0.33 1.667 20 L222-121130 16
3/4-Methylphenol mg/kg wet1.71 0.33 1.667 2034-119103 11
4,6-Dinitro-2-methylphenol mg/kg wet1.56 0.33 1.667 2029-13293 15
4-Bromophenyl phenyl ether mg/kg wet2.10 0.33 1.667 20 L246-124126 15
4-Chloro-3-methylphenol mg/kg wet1.70 0.33 1.667 2045-122102 14
4-Chloroaniline mg/kg wet1.74 0.33 1.667 2017-106104 15
4-Chlorophenyl phenyl ether mg/kg wet2.02 0.33 1.667 2045-121121 15
4-Nitrophenol mg/kg wet1.88 0.33 1.667 2030-132113 17
Acenaphthene mg/kg wet2.02 0.33 1.667 2040-123121 15
Acenaphthylene mg/kg wet2.09 0.33 1.667 2032-132125 14
Anthracene mg/kg wet2.29 0.33 1.667 20 L247-123138 15
Azobenzene mg/kg wet2.01 0.33 1.667 2039-125121 13
Benzo(a)anthracene mg/kg wet2.23 0.33 1.667 20 L249-126134 15
Benzo(a)pyrene mg/kg wet2.29 0.33 1.667 20 L245-129138 17
Benzo(b)fluoranthene mg/kg wet2.20 0.33 1.667 2045-132132 17
Benzo(g,h,i)perylene mg/kg wet2.24 0.33 1.667 2043-134134 16
Benzo(k)fluoranthene mg/kg wet2.23 0.33 1.667 20 L247-132134 18
Benzoic Acid mg/kg wet0.885 0.33 1.667 2010-8353 6
Benzyl alcohol mg/kg wet1.96 0.33 1.667 2029-122117 12
bis(2-Chloroethoxy)methane mg/kg wet1.75 0.33 1.667 2036-121105 11
Bis(2-Chloroethyl)ether mg/kg wet1.65 0.33 1.667 2031-12099 12
Bis(2-chloroisopropyl)ether mg/kg wet1.78 0.33 1.667 2033-131107 12
Bis(2-Ethylhexyl)phthalate mg/kg wet2.33 0.33 1.667 20 L251-133140 17
Butyl benzyl phthalate mg/kg wet2.26 0.33 1.667 20 L248-132136 17
Chrysene mg/kg wet2.23 0.33 1.667 20 L250-124134 17
Dibenzo(a,h)anthracene mg/kg wet1.57 0.33 1.667 2045-13494 17
Dibenzofuran mg/kg wet2.03 0.33 1.667 20 L244-120122 14
Diethyl phthalate mg/kg wet2.10 0.33 1.667 20 L250-124126 14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8K0299 - 3546
LCS Dup (P8K0299-BSD1)Prepared & Analyzed: 11/16/18
Dimethyl phthalate mg/kg wet2.05 0.33 1.667 2048-124123 15
Di-n-butyl phthalate mg/kg wet2.25 0.33 1.667 20 L251-128135 16
Di-n-octyl phthalate mg/kg wet2.45 0.33 1.667 20 L245-140147 16
Fluoranthene mg/kg wet2.17 0.33 1.667 20 L250-127130 15
Fluorene mg/kg wet2.10 0.33 1.667 20 L243-125126 14
Hexachlorobenzene mg/kg wet2.07 0.33 1.667 20 L245-122124 15
Hexachlorobutadiene mg/kg wet1.68 0.33 1.667 2032-123101 13
Hexachlorocyclopentadiene mg/kg wet1.80 0.33 1.667 2032-117108 16
Hexachloroethane mg/kg wet1.59 0.33 1.667 2028-11796 13
Indeno(1,2,3-cd)pyrene mg/kg wet2.48 0.33 1.667 20 L245-133149 16
Isophorone mg/kg wet1.80 0.33 1.667 2030-122108 11
Naphthalene mg/kg wet1.64 0.33 1.667 2035-12398 11
Nitrobenzene mg/kg wet1.61 0.33 1.667 2034-12296 13
N-Nitroso-di-n-propylamine mg/kg wet1.77 0.33 1.667 2036-120106 15
N-Nitrosodiphenylamine mg/kg wet2.59 0.33 1.667 20 L238-127156 16
Pentachlorophenol mg/kg wet1.62 0.33 1.667 2025-13397 17
Phenanthrene mg/kg wet2.20 0.33 1.667 20 L250-121132 16
Phenol mg/kg wet1.87 0.33 1.667 2034-121112 12
Pyrene mg/kg wet2.25 0.33 1.667 20 L247-127135 17
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 1224.07
mg/kg wet 1.667 L244-115Surrogate: 2-Fluorobiphenyl 1161.93
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 1093.64
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 891.49
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 1083.59
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 1201.99
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8K0211 - 3010A
Blank (P8K0211-BLK1)Prepared & Analyzed: 11/13/18
Arsenic mg/LBRL0.020
Barium mg/LBRL0.010
Cadmium mg/LBRL0.0010
Chromium mg/LBRL0.0050
Lead mg/LBRL0.0050
Selenium mg/LBRL0.020
Silver mg/LBRL0.0050
LCS (P8K0211-BS1)Prepared & Analyzed: 11/13/18
Arsenic mg/L0.495 0.020 0.5001 80-12099
Barium mg/L0.508 0.010 0.5000 80-120102
Cadmium mg/L0.498 0.0010 0.5000 80-120100
Chromium mg/L0.509 0.0050 0.5001 80-120102
Lead mg/L0.501 0.0050 0.5001 80-120100
Selenium mg/L0.476 0.020 0.4999 80-12095
Silver mg/L0.202 0.0050 0.2000 80-120101
Batch P8K0213 - 3050B
Blank (P8K0213-BLK1)Prepared & Analyzed: 11/13/18
Arsenic mg/kg wetBRL0.50
Barium mg/kg wetBRL0.50
Cadmium mg/kg wetBRL0.25
Chromium mg/kg wetBRL0.25
Lead mg/kg wetBRL0.25
Selenium mg/kg wetBRL0.50
Silver mg/kg wetBRL0.25
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
12/17/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8110180
Time Submitted: 11/9/2018 3:00:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8K0213 - 3050B
LCS (P8K0213-BS1)Prepared & Analyzed: 11/13/18
Arsenic mg/kg wet12.0 0.50 12.50 80-12096
Barium mg/kg wet12.6 0.50 12.50 80-120101
Cadmium mg/kg wet11.9 0.25 12.50 80-12095
Chromium mg/kg wet12.6 0.25 12.50 80-120101
Lead mg/kg wet11.9 0.25 12.50 80-12095
Selenium mg/kg wet11.4 0.50 12.50 80-12091
Silver mg/kg wet4.83 0.25 5.000 80-12097
Batch P8K0238 - 7470A
Blank (P8K0238-BLK1)Prepared & Analyzed: 11/14/18
Mercury mg/LBRL0.00020
LCS (P8K0238-BS1)Prepared & Analyzed: 11/14/18
Mercury mg/L0.00905 0.00020 0.009375 80-12097
Batch P8K0268 - 7471B
Blank (P8K0268-BLK1)Prepared & Analyzed: 11/15/18
Mercury mg/kg wetBRL0.020
LCS (P8K0268-BS1)Prepared & Analyzed: 11/15/18
Mercury mg/kg wet0.413 0.020 0.4167 80-12099
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P8K02198110180-01 11/12/18 16:0030 30g g
P8K02198110180-02 11/12/18 16:0030 30g g
P8K02848110180-03 11/14/18 14:5630 30g g
P8K02848110180-04 11/14/18 14:5630 30g g
Prep Method: 3510C MS
Lab Number Batch Date/TimeInitialFinal
P8K02658110180-05 11/15/18 9:357201mL mL
P8K02658110180-06 11/15/18 9:357901mL mL
P8K02658110180-07 11/15/18 9:358601mL mL
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P8K02498110180-01 11/14/18 10:3530.08 1g mL
P8K02998110180-02 11/16/18 9:3030.04 1g mL
P8K02498110180-03 11/14/18 10:3530.05 1g mL
P8K02498110180-04 11/14/18 10:3530.03 1g mL
Prep Method: 3010A
Lab Number Batch Date/TimeInitialFinal
P8K02118110180-05 11/13/18 7:4550 50mL mL
P8K02118110180-06 11/13/18 7:4550 50mL mL
P8K02118110180-07 11/13/18 7:4550 50mL mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P8K02138110180-01 11/13/18 8:252 50g mL
P8K02138110180-02 11/13/18 8:252 50g mL
P8K02138110180-03 11/13/18 8:252 50g mL
P8K02138110180-04 11/13/18 8:252.01 50g mL
Prep Method: 7470A
Lab Number Batch Date/TimeInitialFinal
P8K02388110180-05 11/14/18 8:1520 30mL mL
P8K02388110180-06 11/14/18 8:1520 30mL mL
P8K02388110180-07 11/14/18 8:1520 30mL mL
Prep Method: 7471B
Lab Number Batch Date/TimeInitialFinal
P8K02688110180-01 11/15/18 9:350.62 50g mL
P8K02688110180-02 11/15/18 9:350.61 50g mL
P8K02688110180-03 11/15/18 9:350.6 50g mL
P8K02688110180-04 11/15/18 9:350.61 50g mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P8K02648110180-05 11/14/18 8:2510 10mL mL
P8K02648110180-06 11/14/18 8:2510 10mL mL
P8K02648110180-07 11/14/18 8:2510 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Extraction Data
Prep Method: 5035
Lab Number Batch Date/TimeInitialFinal
P8K02768110180-01 11/15/18 11:114.87 5g mL
P8K02768110180-02 11/15/18 11:114.07 5g mL
P8K02768110180-03 11/15/18 11:115.72 5g mL
P8K02768110180-04 11/15/18 11:117.57 5g mL
Subcontracted Analyses
Lab Number
The following analyses were subcontracted to ALS - Rochester, NY
Analysis
8110180-01 Hexavalent Chromium (Sub)
8110180-02 Hexavalent Chromium (Sub)
8110180-03 Hexavalent Chromium (Sub)
8110180-04 Hexavalent Chromium (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
12/11/2018
ECS Carolinas, LLP (Charlotte)
Shaun Brewer
1812 Center Park Drive, Suite D
Charlotte, NC 28217
Project: Vaughn Grittin Jr.
Lab Submittal Date: 12/03/2018
Prism Work Order: 8120022
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
VP Laboratory Services
Reviewed ByAngela D. Overcash Robbi A. Jones For Angela D. Overcash
President/Project Manager
Data Qualifiers Key Reference:
CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken.
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L1 LCS recovery outside of the QC limits. LCSD recovery within the limits. No further action taken.
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 27
Sample Receipt Summary
12/11/2018
Prism Work Order: 8120022
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
8120022-01 12/03/18 12:10TW-4 12/03/18 14:40Water
8120022-02 12/03/18 12:45TW-5 12/03/18 14:40Water
8120022-03 12/03/18 13:00TW-6 12/03/18 14:40Water
8120022-04 12/03/18 13:20SB-5 12/03/18 14:40Solid
8120022-05 12/03/18 13:30BKG-1 12/03/18 14:40Solid
8120022-06 12/03/18 13:35BKG-2 12/03/18 14:40Solid
Samples were received in good condition at 4.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 27
Client ID ResultParameterMethod UnitsPrism ID
Prism Work Order: 8120022
12/11/2018
Summary of Detections
1.3 ug/L8120022-01 TW-4 Tetrachloroethylene 8260B
5.1 ug/L8120022-02 TW-5 Acetone 8260B
6.8 ug/L8120022-02 TW-5 Tetrachloroethylene 8260B
4.0 ug/L8120022-03 TW-6 1,1,2-Trichloroethane 8260B
9.7 ug/L8120022-03 TW-6 1,1-Dichloroethane 8260B
8.2 ug/L8120022-03 TW-6 1,1-Dichloroethylene 8260B
0.93 ug/L8120022-03 TW-6 1,2-Dichloroethane 8260B
1.9 ug/L8120022-03 TW-6 Methyl-tert-Butyl Ether 8260B
0.98 ug/L8120022-03 TW-6 Tetrachloroethylene 8260B
2.2 ug/L8120022-03 TW-6 Trichloroethylene 8260B
0.13 J mg/kg dry8120022-04 SB-5 3/4-Methylphenol 8270D
6.2 mg/kg dry8120022-05 BKG-1 Arsenic 6010D
5.6 mg/kg dry8120022-05 BKG-1 Selenium 6010D
4.2 mg/kg dry8120022-06 BKG-2 Arsenic 6010D
5.1 mg/kg dry8120022-06 BKG-2 Selenium 6010D
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-4
Prism Sample ID: 8120022-01
Prism Work Order: 8120022
Time Collected: 12/03/18 12:10
Time Submitted: 12/03/18 14:40
Volatile Organic Compounds by GC/MS
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0611,1,1-Trichloroethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0661,1,2-Trichloroethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0831,1-Dichloroethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0831,1-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0511,1-Dichloropropylene
BRL 8260B P8L011212.0 12/10/18 17:53 ANGug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.141,2,3-Trichloropropane
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P8L011212.0 12/10/18 17:53 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0511,2-Dibromoethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0761,2-Dichlorobenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0661,2-Dichloroethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.111,2-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0541,3-Dichlorobenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0431,3-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0501,4-Dichlorobenzene
BRL 8260B P8L011212.0 12/10/18 17:53 ANGug/L 0.112,2-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0662-Chlorotoluene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0504-Chlorotoluene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.0894-Isopropyltoluene
BRL 8260B P8L011215.0 12/10/18 17:53 ANGug/L 0.31Acetone
BRL 8260B P8L011212012/10/18 17:53 ANGug/L 0.20Acrolein
BRL 8260B P8L011212012/10/18 17:53 ANGug/L 0.20Acrylonitrile
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.048Benzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.057Bromobenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.14Bromochloromethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.062Bromodichloromethane
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.040Bromoform
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.18Bromomethane
BRL 8260B P8L011215.0 12/10/18 17:53 ANGug/L 0.075Carbon disulfide
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.11Carbon Tetrachloride
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.062Chlorobenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.22Chloroethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.076Chloroform
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.079Chloromethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-4
Prism Sample ID: 8120022-01
Prism Work Order: 8120022
Time Collected: 12/03/18 12:10
Time Submitted: 12/03/18 14:40
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.065Dibromomethane
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.11Dichlorodifluoromethane
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.061Ethylbenzene
BRL 8260B P8L011212.0 12/10/18 17:53 ANGug/L 0.16Hexachlorobutadiene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.050Isopropyl Ether
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.12m,p-Xylenes
BRL 8260B P8L011215.0 12/10/18 17:53 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P8L011215.0 12/10/18 17:53 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8L011215.0 12/10/18 17:53 ANGug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.083Methylene Chloride
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.19Naphthalene
BRL 8260B P8L011211.0 12/10/18 17:53 ANGug/L 0.076n-Butylbenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.087n-Propylbenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.044o-Xylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.076sec-Butylbenzene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.047Styrene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.088tert-Butylbenzene
1.3 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.098Tetrachloroethylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.044Toluene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.078Trichloroethylene
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.062Trichlorofluoromethane
BRL 8260B P8L011212.0 12/10/18 17:53 ANGug/L 0.060Vinyl acetate
BRL 8260B P8L011210.50 12/10/18 17:53 ANGug/L 0.097Vinyl chloride
BRL 8260B P8L011211.5 12/10/18 17:53 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124109 %4-Bromofluorobenzene
75-12998 %Dibromofluoromethane
77-123101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-5
Prism Sample ID: 8120022-02
Prism Work Order: 8120022
Time Collected: 12/03/18 12:45
Time Submitted: 12/03/18 14:40
Volatile Organic Compounds by GC/MS
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0611,1,1-Trichloroethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0661,1,2-Trichloroethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0831,1-Dichloroethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0831,1-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0511,1-Dichloropropylene
BRL 8260B P8L011212.0 12/10/18 18:20 ANGug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.141,2,3-Trichloropropane
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P8L011212.0 12/10/18 18:20 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0511,2-Dibromoethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0761,2-Dichlorobenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0661,2-Dichloroethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.111,2-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0541,3-Dichlorobenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0431,3-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0501,4-Dichlorobenzene
BRL 8260B P8L011212.0 12/10/18 18:20 ANGug/L 0.112,2-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0662-Chlorotoluene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0504-Chlorotoluene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.0894-Isopropyltoluene
5.1 8260B P8L011215.0 12/10/18 18:20 ANGug/L 0.31Acetone
BRL 8260B P8L011212012/10/18 18:20 ANGug/L 0.20Acrolein
BRL 8260B P8L011212012/10/18 18:20 ANGug/L 0.20Acrylonitrile
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.048Benzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.057Bromobenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.14Bromochloromethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.062Bromodichloromethane
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.040Bromoform
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.18Bromomethane
BRL 8260B P8L011215.0 12/10/18 18:20 ANGug/L 0.075Carbon disulfide
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.11Carbon Tetrachloride
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.062Chlorobenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.22Chloroethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.076Chloroform
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.079Chloromethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-5
Prism Sample ID: 8120022-02
Prism Work Order: 8120022
Time Collected: 12/03/18 12:45
Time Submitted: 12/03/18 14:40
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.065Dibromomethane
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.11Dichlorodifluoromethane
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.061Ethylbenzene
BRL 8260B P8L011212.0 12/10/18 18:20 ANGug/L 0.16Hexachlorobutadiene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.050Isopropyl Ether
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.12m,p-Xylenes
BRL 8260B P8L011215.0 12/10/18 18:20 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P8L011215.0 12/10/18 18:20 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8L011215.0 12/10/18 18:20 ANGug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.083Methylene Chloride
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.19Naphthalene
BRL 8260B P8L011211.0 12/10/18 18:20 ANGug/L 0.076n-Butylbenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.087n-Propylbenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.044o-Xylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.076sec-Butylbenzene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.047Styrene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.088tert-Butylbenzene
6.8 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.098Tetrachloroethylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.044Toluene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.070trans-1,3-Dichloropropylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.078Trichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.062Trichlorofluoromethane
BRL 8260B P8L011212.0 12/10/18 18:20 ANGug/L 0.060Vinyl acetate
BRL 8260B P8L011210.50 12/10/18 18:20 ANGug/L 0.097Vinyl chloride
BRL 8260B P8L011211.5 12/10/18 18:20 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-123100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-6
Prism Sample ID: 8120022-03
Prism Work Order: 8120022
Time Collected: 12/03/18 13:00
Time Submitted: 12/03/18 14:40
Volatile Organic Compounds by GC/MS
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0611,1,1-Trichloroethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0361,1,2,2-Tetrachloroethane
4.0 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0661,1,2-Trichloroethane
9.7 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0831,1-Dichloroethane
8.2 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0831,1-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0511,1-Dichloropropylene
BRL 8260B P8L011212.0 12/10/18 18:46 ANGug/L 0.401,2,3-Trichlorobenzene
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.141,2,3-Trichloropropane
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.131,2,4-Trichlorobenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL 8260B P8L011212.0 12/10/18 18:46 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0511,2-Dibromoethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0761,2-Dichlorobenzene
0.93 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0661,2-Dichloroethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.111,2-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0541,3-Dichlorobenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0431,3-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0501,4-Dichlorobenzene
BRL 8260B P8L011212.0 12/10/18 18:46 ANGug/L 0.112,2-Dichloropropane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0662-Chlorotoluene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0504-Chlorotoluene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.0894-Isopropyltoluene
BRL 8260B P8L011215.0 12/10/18 18:46 ANGug/L 0.31Acetone
BRL 8260B P8L011212012/10/18 18:46 ANGug/L 0.20Acrolein
BRL 8260B P8L011212012/10/18 18:46 ANGug/L 0.20Acrylonitrile
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.048Benzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.057Bromobenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.14Bromochloromethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.062Bromodichloromethane
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.040Bromoform
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.18Bromomethane
BRL 8260B P8L011215.0 12/10/18 18:46 ANGug/L 0.075Carbon disulfide
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.11Carbon Tetrachloride
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.062Chlorobenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.22Chloroethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.076Chloroform
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.079Chloromethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.081Dibromochloromethane
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Water
Client Sample ID: TW-6
Prism Sample ID: 8120022-03
Prism Work Order: 8120022
Time Collected: 12/03/18 13:00
Time Submitted: 12/03/18 14:40
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.065Dibromomethane
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.11Dichlorodifluoromethane
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.061Ethylbenzene
BRL 8260B P8L011212.0 12/10/18 18:46 ANGug/L 0.16Hexachlorobutadiene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.050Isopropyl Ether
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.12m,p-Xylenes
BRL 8260B P8L011215.0 12/10/18 18:46 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL 8260B P8L011215.0 12/10/18 18:46 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL 8260B P8L011215.0 12/10/18 18:46 ANGug/L 0.078Methyl Isobutyl Ketone
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.083Methylene Chloride
1.9 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.19Naphthalene
BRL 8260B P8L011211.0 12/10/18 18:46 ANGug/L 0.076n-Butylbenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.087n-Propylbenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.044o-Xylene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.076sec-Butylbenzene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.047Styrene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.088tert-Butylbenzene
0.98 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.098Tetrachloroethylene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.044Toluene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.094trans-1,2-Dichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.070trans-1,3-Dichloropropylene
2.2 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.078Trichloroethylene
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.062Trichlorofluoromethane
BRL 8260B P8L011212.0 12/10/18 18:46 ANGug/L 0.060Vinyl acetate
BRL 8260B P8L011210.50 12/10/18 18:46 ANGug/L 0.097Vinyl chloride
BRL 8260B P8L011211.5 12/10/18 18:46 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
80-124111 %4-Bromofluorobenzene
75-129100 %Dibromofluoromethane
77-123103 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-5
Prism Sample ID: 8120022-04
Prism Work Order: 8120022
Time Collected: 12/03/18 13:20
Time Submitted: 12/03/18 14:40
General Chemistry Parameters
82.8 SM2540 G P8L008710.100 12/5/18 14:24 TJY% by
Weight
0.100% Solids
Semivolatile Organic Compounds by GC/MS
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0621,2,4-Trichlorobenzene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0601,2-Dichlorobenzene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0561,3-Dichlorobenzene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0581,4-Dichlorobenzene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0771-Methylnaphthalene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0752,4,6-Trichlorophenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0772,4-Dichlorophenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0612,4-Dimethylphenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVCCVmg/kg dry 0.0562,4-Dinitrophenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0482,4-Dinitrotoluene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0532,6-Dinitrotoluene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0582-Chloronaphthalene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0562-Chlorophenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0642-Methylnaphthalene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0512-Methylphenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0732-Nitrophenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0793,3’-Dichlorobenzidine
0.13 8270D P8L003810.40 12/5/18 20:16 JMVJmg/kg dry 0.0493/4-Methylphenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0604,6-Dinitro-2-methylphenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0684-Bromophenyl phenyl ether
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0564-Chloro-3-methylphenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0484-Chloroaniline
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0524-Chlorophenyl phenyl ether
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.0614-Nitrophenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.054Acenaphthene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.058Acenaphthylene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.064Anthracene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.053Azobenzene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.052Benzo(a)anthracene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.043Benzo(a)pyrene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.046Benzo(b)fluoranthene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.044Benzo(g,h,i)perylene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.052Benzo(k)fluoranthene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.034Benzoic Acid
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.053Benzyl alcohol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.069bis(2-Chloroethoxy)methane
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.056Bis(2-Chloroethyl)ether
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.068Bis(2-chloroisopropyl)ether
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.059Bis(2-Ethylhexyl)phthalate
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: SB-5
Prism Sample ID: 8120022-04
Prism Work Order: 8120022
Time Collected: 12/03/18 13:20
Time Submitted: 12/03/18 14:40
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.057Butyl benzyl phthalate
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.050Chrysene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.049Dibenzo(a,h)anthracene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.061Dibenzofuran
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.055Diethyl phthalate
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.053Dimethyl phthalate
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.057Di-n-butyl phthalate
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.049Di-n-octyl phthalate
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.051Fluoranthene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.057Fluorene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.063Hexachlorobenzene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.072Hexachlorobutadiene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.071Hexachlorocyclopentadiene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.067Hexachloroethane
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.046Indeno(1,2,3-cd)pyrene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.054Isophorone
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.064Naphthalene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.057Nitrobenzene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.063N-Nitroso-di-n-propylamine
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.061N-Nitrosodiphenylamine
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.047Pentachlorophenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.052Phenanthrene
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.059Phenol
BRL 8270D P8L003810.40 12/5/18 20:16 JMVmg/kg dry 0.053Pyrene
Surrogate Recovery Control Limits
39-13282 %2,4,6-Tribromophenol
44-11584 %2-Fluorobiphenyl
35-11571 %2-Fluorophenol
37-12268 %Nitrobenzene-d5
34-12165 %Phenol-d5
54-12775 %Terphenyl-d14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: BKG-1
Prism Sample ID: 8120022-05
Prism Work Order: 8120022
Time Collected: 12/03/18 13:30
Time Submitted: 12/03/18 14:40
General Chemistry Parameters
70.8 SM2540 G P8L008710.100 12/5/18 14:24 TJY% by
Weight
0.100% Solids
Total Metals
6.2 6010D P8L004210.70 12/5/18 15:41 JABmg/kg dry 0.043Arsenic
5.6 6010D P8L004210.70 12/6/18 13:41 JABmg/kg dry 0.17Selenium
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 27
Laboratory Report
12/11/2018
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Sample Matrix: Solid
Client Sample ID: BKG-2
Prism Sample ID: 8120022-06
Prism Work Order: 8120022
Time Collected: 12/03/18 13:35
Time Submitted: 12/03/18 14:40
General Chemistry Parameters
79.0 SM2540 G P8L008710.100 12/5/18 14:24 TJY% by
Weight
0.100% Solids
Total Metals
4.2 6010D P8L004210.63 12/5/18 16:09 JABmg/kg dry 0.039Arsenic
5.1 6010D P8L004210.63 12/6/18 13:50 JABmg/kg dry 0.15Selenium
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8L0112 - 5030B
Blank (P8L0112-BLK1)Prepared & Analyzed: 12/10/18
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL2.0
1,2,3-Trichloropropane ug/LBRL1.0
1,2,4-Trichlorobenzene ug/LBRL1.0
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL5.0
Acrolein ug/LBRL20
Acrylonitrile ug/LBRL20
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL1.0
Bromomethane ug/LBRL1.0
Carbon disulfide ug/LBRL5.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8L0112 - 5030B
Blank (P8L0112-BLK1)Prepared & Analyzed: 12/10/18
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL5.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL5.0
Methylene Chloride ug/LBRL1.0
Methyl-tert-Butyl Ether ug/LBRL0.50
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL1.0
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL2.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10954.4
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 9949.7
ug/L 50.00 77-123Surrogate: Toluene-d8 10251.1
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8L0112 - 5030B
LCS (P8L0112-BS1)Prepared & Analyzed: 12/10/18
1,1,1,2-Tetrachloroethane ug/L20.5 0.50 20.00 79-134103
1,1,1-Trichloroethane ug/L18.4 0.50 20.00 75-13692
1,1,2,2-Tetrachloroethane ug/L22.5 0.50 20.00 62-127112
1,1,2-Trichloroethane ug/L21.8 0.50 20.00 70-140109
1,1-Dichloroethane ug/L22.0 0.50 20.00 78-130110
1,1-Dichloroethylene ug/L23.2 0.50 20.00 70-154116
1,1-Dichloropropylene ug/L18.5 0.50 20.00 71-13692
1,2,3-Trichlorobenzene ug/L19.2 2.0 20.00 58-14496
1,2,3-Trichloropropane ug/L21.0 1.0 20.00 71-127105
1,2,4-Trichlorobenzene ug/L19.7 1.0 20.00 66-13998
1,2,4-Trimethylbenzene ug/L21.4 0.50 20.00 75-133107
1,2-Dibromo-3-chloropropane ug/L20.6 2.0 20.00 63-134103
1,2-Dibromoethane ug/L21.1 0.50 20.00 77-135106
1,2-Dichlorobenzene ug/L18.8 0.50 20.00 78-12894
1,2-Dichloroethane ug/L20.9 0.50 20.00 68-131105
1,2-Dichloropropane ug/L20.9 0.50 20.00 77-130104
1,3,5-Trimethylbenzene ug/L20.2 0.50 20.00 75-131101
1,3-Dichlorobenzene ug/L19.5 0.50 20.00 77-12597
1,3-Dichloropropane ug/L21.4 0.50 20.00 76-132107
1,4-Dichlorobenzene ug/L19.4 0.50 20.00 75-12697
2,2-Dichloropropane ug/L18.4 2.0 20.00 29-14992
2-Chlorotoluene ug/L20.1 0.50 20.00 74-126100
4-Chlorotoluene ug/L20.9 0.50 20.00 78-129104
4-Isopropyltoluene ug/L19.8 0.50 20.00 69-13299
Acetone ug/L54.6 5.0 40.00 40-166136
Acrolein ug/L53.0 20 40.00 L170-130133
Acrylonitrile ug/L53.7 20 40.00 L181-127134
Benzene ug/L20.4 0.50 20.00 77-128102
Bromobenzene ug/L20.9 0.50 20.00 78-129105
Bromochloromethane ug/L19.6 0.50 20.00 78-13598
Bromodichloromethane ug/L21.0 0.50 20.00 76-138105
Bromoform ug/L20.6 1.0 20.00 71-135103
Bromomethane ug/L18.0 1.0 20.00 41-16890
Carbon disulfide ug/L21.6 5.0 20.00 59-135108
Carbon Tetrachloride ug/L20.0 0.50 20.00 72-142100
Chlorobenzene ug/L20.0 0.50 20.00 78-119100
Chloroethane ug/L24.8 0.50 20.00 57-142124
Chloroform ug/L21.0 0.50 20.00 77-130105
Chloromethane ug/L23.3 0.50 20.00 47-145117
cis-1,2-Dichloroethylene ug/L19.6 0.50 20.00 76-14198
cis-1,3-Dichloropropylene ug/L20.3 0.50 20.00 65-140102
Dibromochloromethane ug/L20.8 0.50 20.00 75-134104
Dibromomethane ug/L21.6 0.50 20.00 76-138108
Dichlorodifluoromethane ug/L18.6 1.0 20.00 28-16393
Ethylbenzene ug/L20.5 0.50 20.00 80-127102
Hexachlorobutadiene ug/L18.2 2.0 20.00 61-13491
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8L0112 - 5030B
LCS (P8L0112-BS1)Prepared & Analyzed: 12/10/18
Isopropyl Ether ug/L22.9 0.50 20.00 60-154115
Isopropylbenzene (Cumene)ug/L20.5 0.50 20.00 70-130102
m,p-Xylenes ug/L41.3 1.0 40.00 77-133103
Methyl Butyl Ketone (2-Hexanone)ug/L21.1 5.0 20.00 64-137106
Methyl Ethyl Ketone (2-Butanone)ug/L22.9 5.0 20.00 71-134115
Methyl Isobutyl Ketone ug/L21.4 5.0 20.00 69-134107
Methylene Chloride ug/L24.0 1.0 20.00 73-131120
Methyl-tert-Butyl Ether ug/L23.7 0.50 20.00 68-135119
Naphthalene ug/L20.8 1.0 20.00 64-136104
n-Butylbenzene ug/L20.9 1.0 20.00 68-134104
n-Propylbenzene ug/L20.9 0.50 20.00 72-132104
o-Xylene ug/L20.5 0.50 20.00 78-128102
sec-Butylbenzene ug/L20.6 0.50 20.00 71-131103
Styrene ug/L20.8 0.50 20.00 78-129104
tert-Butylbenzene ug/L20.2 0.50 20.00 70-132101
Tetrachloroethylene ug/L17.1 0.50 20.00 80-12985
Toluene ug/L20.4 0.50 20.00 76-131102
trans-1,2-Dichloroethylene ug/L24.6 0.50 20.00 76-135123
trans-1,3-Dichloropropylene ug/L20.2 0.50 20.00 67-140101
Trichloroethylene ug/L19.7 0.50 20.00 77-13399
Trichlorofluoromethane ug/L19.7 0.50 20.00 62-14898
Vinyl acetate ug/L24.9 2.0 20.00 34-167124
Vinyl chloride ug/L20.7 0.50 20.00 57-141103
Xylenes, total ug/L61.8 1.5 60.00 77-133103
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10452.0
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10451.8
ug/L 50.00 77-123Surrogate: Toluene-d8 10351.6
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8L0112 - 5030B
LCS Dup (P8L0112-BSD1)Prepared & Analyzed: 12/10/18
1,1,1,2-Tetrachloroethane ug/L20.6 0.50 20.00 2079-134103 0.1
1,1,1-Trichloroethane ug/L17.7 0.50 20.00 2075-13689 4
1,1,2,2-Tetrachloroethane ug/L22.3 0.50 20.00 2062-127111 1
1,1,2-Trichloroethane ug/L21.1 0.50 20.00 2070-140106 3
1,1-Dichloroethane ug/L18.4 0.50 20.00 2078-13092 18
1,1-Dichloroethylene ug/L17.5 0.50 20.00 20 D70-15488 28
1,1-Dichloropropylene ug/L17.9 0.50 20.00 2071-13690 3
1,2,3-Trichlorobenzene ug/L19.5 2.0 20.00 2058-14498 2
1,2,3-Trichloropropane ug/L20.6 1.0 20.00 2071-127103 2
1,2,4-Trichlorobenzene ug/L18.7 1.0 20.00 2066-13994 5
1,2,4-Trimethylbenzene ug/L20.8 0.50 20.00 2075-133104 3
1,2-Dibromo-3-chloropropane ug/L21.2 2.0 20.00 2063-134106 3
1,2-Dibromoethane ug/L20.7 0.50 20.00 2077-135103 2
1,2-Dichlorobenzene ug/L18.9 0.50 20.00 2078-12895 0.6
1,2-Dichloroethane ug/L20.0 0.50 20.00 2068-131100 5
1,2-Dichloropropane ug/L20.1 0.50 20.00 2077-130101 4
1,3,5-Trimethylbenzene ug/L19.7 0.50 20.00 2075-13199 2
1,3-Dichlorobenzene ug/L18.6 0.50 20.00 2077-12593 4
1,3-Dichloropropane ug/L21.0 0.50 20.00 2076-132105 2
1,4-Dichlorobenzene ug/L19.0 0.50 20.00 2075-12695 2
2,2-Dichloropropane ug/L17.8 2.0 20.00 2029-14989 3
2-Chlorotoluene ug/L19.1 0.50 20.00 2074-12696 5
4-Chlorotoluene ug/L20.6 0.50 20.00 2078-129103 1
4-Isopropyltoluene ug/L19.4 0.50 20.00 2069-13297 2
Acetone ug/L41.4 5.0 40.00 20 D40-166104 27
Acrolein ug/L44.5 20 40.00 2070-130111 18
Acrylonitrile ug/L45.2 20 40.00 2081-127113 17
Benzene ug/L19.5 0.50 20.00 2077-12898 5
Bromobenzene ug/L20.0 0.50 20.00 2078-129100 4
Bromochloromethane ug/L19.1 0.50 20.00 2078-13596 2
Bromodichloromethane ug/L20.6 0.50 20.00 2076-138103 2
Bromoform ug/L20.4 1.0 20.00 2071-135102 0.7
Bromomethane ug/L19.5 1.0 20.00 2041-16898 8
Carbon disulfide ug/L18.4 5.0 20.00 2059-13592 16
Carbon Tetrachloride ug/L19.4 0.50 20.00 2072-14297 3
Chlorobenzene ug/L19.6 0.50 20.00 2078-11998 2
Chloroethane ug/L24.1 0.50 20.00 2057-142120 3
Chloroform ug/L20.2 0.50 20.00 2077-130101 4
Chloromethane ug/L22.0 0.50 20.00 2047-145110 6
cis-1,2-Dichloroethylene ug/L19.4 0.50 20.00 2076-14197 1
cis-1,3-Dichloropropylene ug/L19.6 0.50 20.00 2065-14098 4
Dibromochloromethane ug/L20.3 0.50 20.00 2075-134101 2
Dibromomethane ug/L20.9 0.50 20.00 2076-138105 3
Dichlorodifluoromethane ug/L17.8 1.0 20.00 2028-16389 4
Ethylbenzene ug/L20.0 0.50 20.00 2080-127100 2
Hexachlorobutadiene ug/L17.3 2.0 20.00 2061-13486 5
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P8L0112 - 5030B
LCS Dup (P8L0112-BSD1)Prepared & Analyzed: 12/10/18
Isopropyl Ether ug/L18.9 0.50 20.00 2060-15495 19
Isopropylbenzene (Cumene)ug/L19.9 0.50 20.00 2070-130100 3
m,p-Xylenes ug/L40.3 1.0 40.00 2077-133101 2
Methyl Butyl Ketone (2-Hexanone)ug/L21.1 5.0 20.00 2064-137105 0.1
Methyl Ethyl Ketone (2-Butanone)ug/L22.8 5.0 20.00 2071-134114 0.5
Methyl Isobutyl Ketone ug/L21.7 5.0 20.00 2069-134108 1
Methylene Chloride ug/L19.4 1.0 20.00 20 D73-13197 21
Methyl-tert-Butyl Ether ug/L19.8 0.50 20.00 2068-13599 18
Naphthalene ug/L20.3 1.0 20.00 2064-136101 3
n-Butylbenzene ug/L20.4 1.0 20.00 2068-134102 3
n-Propylbenzene ug/L20.5 0.50 20.00 2072-132102 2
o-Xylene ug/L20.2 0.50 20.00 2078-128101 1
sec-Butylbenzene ug/L19.6 0.50 20.00 2071-13198 5
Styrene ug/L20.3 0.50 20.00 2078-129102 3
tert-Butylbenzene ug/L19.7 0.50 20.00 2070-13298 3
Tetrachloroethylene ug/L16.9 0.50 20.00 2080-12984 1
Toluene ug/L19.4 0.50 20.00 2076-13197 5
trans-1,2-Dichloroethylene ug/L20.0 0.50 20.00 2076-135100 20
trans-1,3-Dichloropropylene ug/L19.9 0.50 20.00 2067-14099 1
Trichloroethylene ug/L18.5 0.50 20.00 2077-13392 7
Trichlorofluoromethane ug/L18.1 0.50 20.00 2062-14891 8
Vinyl acetate ug/L20.6 2.0 20.00 2034-167103 19
Vinyl chloride ug/L19.7 0.50 20.00 2057-14198 5
Xylenes, total ug/L60.5 1.5 60.00 2077-133101 2
ug/L 50.00 80-124Surrogate: 4-Bromofluorobenzene 10552.4
ug/L 50.00 75-129Surrogate: Dibromofluoromethane 10351.7
ug/L 50.00 77-123Surrogate: Toluene-d8 10251.0
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8L0038 - 3546
Blank (P8L0038-BLK1)Prepared: 12/04/18 Analyzed: 12/05/18
1,2,4-Trichlorobenzene mg/kg wetBRL0.33
1,2-Dichlorobenzene mg/kg wetBRL0.33
1,3-Dichlorobenzene mg/kg wetBRL0.33
1,4-Dichlorobenzene mg/kg wetBRL0.33
1-Methylnaphthalene mg/kg wetBRL0.33
2,4,6-Trichlorophenol mg/kg wetBRL0.33
2,4-Dichlorophenol mg/kg wetBRL0.33
2,4-Dimethylphenol mg/kg wetBRL0.33
2,4-Dinitrophenol mg/kg wetBRL0.33
2,4-Dinitrotoluene mg/kg wetBRL0.33
2,6-Dinitrotoluene mg/kg wetBRL0.33
2-Chloronaphthalene mg/kg wetBRL0.33
2-Chlorophenol mg/kg wetBRL0.33
2-Methylnaphthalene mg/kg wetBRL0.33
2-Methylphenol mg/kg wetBRL0.33
2-Nitrophenol mg/kg wetBRL0.33
3,3’-Dichlorobenzidine mg/kg wetBRL0.33
3/4-Methylphenol mg/kg wetBRL0.33
4,6-Dinitro-2-methylphenol mg/kg wetBRL0.33
4-Bromophenyl phenyl ether mg/kg wetBRL0.33
4-Chloro-3-methylphenol mg/kg wetBRL0.33
4-Chloroaniline mg/kg wetBRL0.33
4-Chlorophenyl phenyl ether mg/kg wetBRL0.33
4-Nitrophenol mg/kg wetBRL0.33
Acenaphthene mg/kg wetBRL0.33
Acenaphthylene mg/kg wetBRL0.33
Anthracene mg/kg wetBRL0.33
Azobenzene mg/kg wetBRL0.33
Benzo(a)anthracene mg/kg wetBRL0.33
Benzo(a)pyrene mg/kg wetBRL0.33
Benzo(b)fluoranthene mg/kg wetBRL0.33
Benzo(g,h,i)perylene mg/kg wetBRL0.33
Benzo(k)fluoranthene mg/kg wetBRL0.33
Benzoic Acid mg/kg wetBRL0.33
Benzyl alcohol mg/kg wetBRL0.33
bis(2-Chloroethoxy)methane mg/kg wetBRL0.33
Bis(2-Chloroethyl)ether mg/kg wetBRL0.33
Bis(2-chloroisopropyl)ether mg/kg wetBRL0.33
Bis(2-Ethylhexyl)phthalate mg/kg wetBRL0.33
Butyl benzyl phthalate mg/kg wetBRL0.33
Chrysene mg/kg wetBRL0.33
Dibenzo(a,h)anthracene mg/kg wetBRL0.33
Dibenzofuran mg/kg wetBRL0.33
Diethyl phthalate mg/kg wetBRL0.33
Dimethyl phthalate mg/kg wetBRL0.33
Di-n-butyl phthalate mg/kg wetBRL0.33
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8L0038 - 3546
Blank (P8L0038-BLK1)Prepared: 12/04/18 Analyzed: 12/05/18
Di-n-octyl phthalate mg/kg wetBRL0.33
Fluoranthene mg/kg wetBRL0.33
Fluorene mg/kg wetBRL0.33
Hexachlorobenzene mg/kg wetBRL0.33
Hexachlorobutadiene mg/kg wetBRL0.33
Hexachlorocyclopentadiene mg/kg wetBRL0.33
Hexachloroethane mg/kg wetBRL0.33
Indeno(1,2,3-cd)pyrene mg/kg wetBRL0.33
Isophorone mg/kg wetBRL0.33
Naphthalene mg/kg wetBRL0.33
Nitrobenzene mg/kg wetBRL0.33
N-Nitroso-di-n-propylamine mg/kg wetBRL0.33
N-Nitrosodiphenylamine mg/kg wetBRL0.33
Pentachlorophenol mg/kg wetBRL0.33
Phenanthrene mg/kg wetBRL0.33
Phenol mg/kg wetBRL0.33
Pyrene mg/kg wetBRL0.33
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 1063.53
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 941.57
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 913.03
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 761.27
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 872.90
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 861.43
LCS (P8L0038-BS1)Prepared: 12/04/18 Analyzed: 12/05/18
1,2,4-Trichlorobenzene mg/kg wet1.28 0.33 1.667 34-11877
1,2-Dichlorobenzene mg/kg wet1.32 0.33 1.667 33-11779
1,3-Dichlorobenzene mg/kg wet1.26 0.33 1.667 30-11575
1,4-Dichlorobenzene mg/kg wet1.27 0.33 1.667 31-11576
1-Methylnaphthalene mg/kg wet1.42 0.33 1.667 40-11985
2,4,6-Trichlorophenol mg/kg wet1.75 0.33 1.667 39-126105
2,4-Dichlorophenol mg/kg wet1.42 0.33 1.667 40-12285
2,4-Dimethylphenol mg/kg wet1.81 0.33 1.667 30-127108
2,4-Dinitrophenol mg/kg wet1.68 0.33 1.667 27-129101
2,4-Dinitrotoluene mg/kg wet1.71 0.33 1.667 48-126102
2,6-Dinitrotoluene mg/kg wet1.77 0.33 1.667 46-124106
2-Chloronaphthalene mg/kg wet1.56 0.33 1.667 41-11494
2-Chlorophenol mg/kg wet1.51 0.33 1.667 34-12191
2-Methylnaphthalene mg/kg wet1.35 0.33 1.667 38-12281
2-Methylphenol mg/kg wet1.56 0.33 1.667 32-12294
2-Nitrophenol mg/kg wet1.41 0.33 1.667 36-12385
3,3’-Dichlorobenzidine mg/kg wet1.89 0.33 1.667 22-121114
3/4-Methylphenol mg/kg wet1.37 0.33 1.667 34-11982
4,6-Dinitro-2-methylphenol mg/kg wet1.62 0.33 1.667 29-13297
4-Bromophenyl phenyl ether mg/kg wet1.72 0.33 1.667 46-124103
4-Chloro-3-methylphenol mg/kg wet1.39 0.33 1.667 45-12283
4-Chloroaniline mg/kg wet1.56 0.33 1.667 17-10693
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8L0038 - 3546
LCS (P8L0038-BS1)Prepared: 12/04/18 Analyzed: 12/05/18
4-Chlorophenyl phenyl ether mg/kg wet1.67 0.33 1.667 45-121100
4-Nitrophenol mg/kg wet1.61 0.33 1.667 30-13297
Acenaphthene mg/kg wet1.65 0.33 1.667 40-12399
Acenaphthylene mg/kg wet1.68 0.33 1.667 32-132101
Anthracene mg/kg wet1.83 0.33 1.667 47-123110
Azobenzene mg/kg wet1.54 0.33 1.667 39-12593
Benzo(a)anthracene mg/kg wet1.58 0.33 1.667 49-12695
Benzo(a)pyrene mg/kg wet1.78 0.33 1.667 45-129107
Benzo(b)fluoranthene mg/kg wet1.61 0.33 1.667 45-13296
Benzo(g,h,i)perylene mg/kg wet1.98 0.33 1.667 43-134119
Benzo(k)fluoranthene mg/kg wet1.58 0.33 1.667 47-13295
Benzoic Acid mg/kg wet0.863 0.33 1.667 10-8352
Benzyl alcohol mg/kg wet1.50 0.33 1.667 29-12290
bis(2-Chloroethoxy)methane mg/kg wet1.49 0.33 1.667 36-12189
Bis(2-Chloroethyl)ether mg/kg wet1.44 0.33 1.667 31-12086
Bis(2-chloroisopropyl)ether mg/kg wet1.33 0.33 1.667 33-13180
Bis(2-Ethylhexyl)phthalate mg/kg wet1.61 0.33 1.667 51-13397
Butyl benzyl phthalate mg/kg wet1.52 0.33 1.667 48-13291
Chrysene mg/kg wet1.64 0.33 1.667 50-12498
Dibenzo(a,h)anthracene mg/kg wet1.88 0.33 1.667 45-134113
Dibenzofuran mg/kg wet1.63 0.33 1.667 44-12098
Diethyl phthalate mg/kg wet1.67 0.33 1.667 50-124100
Dimethyl phthalate mg/kg wet1.64 0.33 1.667 48-12499
Di-n-butyl phthalate mg/kg wet1.73 0.33 1.667 51-128104
Di-n-octyl phthalate mg/kg wet1.74 0.33 1.667 45-140105
Fluoranthene mg/kg wet1.76 0.33 1.667 50-127106
Fluorene mg/kg wet1.74 0.33 1.667 43-125105
Hexachlorobenzene mg/kg wet1.69 0.33 1.667 45-122101
Hexachlorobutadiene mg/kg wet1.38 0.33 1.667 32-12383
Hexachlorocyclopentadiene mg/kg wet1.88 0.33 1.667 32-117113
Hexachloroethane mg/kg wet1.24 0.33 1.667 28-11775
Indeno(1,2,3-cd)pyrene mg/kg wet1.92 0.33 1.667 45-133115
Isophorone mg/kg wet1.51 0.33 1.667 30-12290
Naphthalene mg/kg wet1.37 0.33 1.667 35-12382
Nitrobenzene mg/kg wet1.30 0.33 1.667 34-12278
N-Nitroso-di-n-propylamine mg/kg wet1.47 0.33 1.667 36-12088
N-Nitrosodiphenylamine mg/kg wet2.06 0.33 1.667 38-127123
Pentachlorophenol mg/kg wet1.69 0.33 1.667 25-133101
Phenanthrene mg/kg wet1.77 0.33 1.667 50-121106
Phenol mg/kg wet1.44 0.33 1.667 34-12187
Pyrene mg/kg wet1.54 0.33 1.667 47-12793
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 1103.65
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 951.59
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 913.05
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 691.15
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 872.91
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8L0038 - 3546
LCS (P8L0038-BS1)Prepared: 12/04/18 Analyzed: 12/05/18
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 861.43
LCS Dup (P8L0038-BSD1)Prepared: 12/04/18 Analyzed: 12/05/18
1,2,4-Trichlorobenzene mg/kg wet1.31 0.33 1.667 2034-11879 2
1,2-Dichlorobenzene mg/kg wet1.34 0.33 1.667 2033-11780 1
1,3-Dichlorobenzene mg/kg wet1.29 0.33 1.667 2030-11577 2
1,4-Dichlorobenzene mg/kg wet1.32 0.33 1.667 2031-11579 4
1-Methylnaphthalene mg/kg wet1.46 0.33 1.667 2040-11988 3
2,4,6-Trichlorophenol mg/kg wet1.86 0.33 1.667 2039-126112 6
2,4-Dichlorophenol mg/kg wet1.50 0.33 1.667 2040-12290 6
2,4-Dimethylphenol mg/kg wet1.93 0.33 1.667 2030-127116 6
2,4-Dinitrophenol mg/kg wet1.83 0.33 1.667 2027-129110 9
2,4-Dinitrotoluene mg/kg wet1.80 0.33 1.667 2048-126108 5
2,6-Dinitrotoluene mg/kg wet1.84 0.33 1.667 2046-124110 4
2-Chloronaphthalene mg/kg wet1.64 0.33 1.667 2041-11498 5
2-Chlorophenol mg/kg wet1.57 0.33 1.667 2034-12194 4
2-Methylnaphthalene mg/kg wet1.41 0.33 1.667 2038-12285 4
2-Methylphenol mg/kg wet1.61 0.33 1.667 2032-12297 3
2-Nitrophenol mg/kg wet1.48 0.33 1.667 2036-12389 5
3,3’-Dichlorobenzidine mg/kg wet1.99 0.33 1.667 2022-121119 5
3/4-Methylphenol mg/kg wet1.45 0.33 1.667 2034-11987 6
4,6-Dinitro-2-methylphenol mg/kg wet1.66 0.33 1.667 2029-132100 2
4-Bromophenyl phenyl ether mg/kg wet1.75 0.33 1.667 2046-124105 2
4-Chloro-3-methylphenol mg/kg wet1.46 0.33 1.667 2045-12287 5
4-Chloroaniline mg/kg wet1.63 0.33 1.667 2017-10698 5
4-Chlorophenyl phenyl ether mg/kg wet1.74 0.33 1.667 2045-121105 4
4-Nitrophenol mg/kg wet1.72 0.33 1.667 2030-132103 6
Acenaphthene mg/kg wet1.77 0.33 1.667 2040-123106 7
Acenaphthylene mg/kg wet1.78 0.33 1.667 2032-132107 6
Anthracene mg/kg wet1.85 0.33 1.667 2047-123111 0.9
Azobenzene mg/kg wet1.56 0.33 1.667 2039-12594 1
Benzo(a)anthracene mg/kg wet1.68 0.33 1.667 2049-126100 6
Benzo(a)pyrene mg/kg wet1.85 0.33 1.667 2045-129111 4
Benzo(b)fluoranthene mg/kg wet1.68 0.33 1.667 2045-132101 5
Benzo(g,h,i)perylene mg/kg wet2.01 0.33 1.667 2043-134121 1
Benzo(k)fluoranthene mg/kg wet1.65 0.33 1.667 2047-13299 4
Benzoic Acid mg/kg wet0.976 0.33 1.667 2010-8359 12
Benzyl alcohol mg/kg wet1.56 0.33 1.667 2029-12294 4
bis(2-Chloroethoxy)methane mg/kg wet1.56 0.33 1.667 2036-12194 5
Bis(2-Chloroethyl)ether mg/kg wet1.44 0.33 1.667 2031-12087 0.2
Bis(2-chloroisopropyl)ether mg/kg wet1.37 0.33 1.667 2033-13182 3
Bis(2-Ethylhexyl)phthalate mg/kg wet1.64 0.33 1.667 2051-13398 2
Butyl benzyl phthalate mg/kg wet1.54 0.33 1.667 2048-13292 1
Chrysene mg/kg wet1.67 0.33 1.667 2050-124100 2
Dibenzo(a,h)anthracene mg/kg wet1.87 0.33 1.667 2045-134112 0.4
Dibenzofuran mg/kg wet1.71 0.33 1.667 2044-120102 5
Diethyl phthalate mg/kg wet1.72 0.33 1.667 2050-124103 3
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
Batch P8L0038 - 3546
LCS Dup (P8L0038-BSD1)Prepared: 12/04/18 Analyzed: 12/05/18
Dimethyl phthalate mg/kg wet1.73 0.33 1.667 2048-124104 5
Di-n-butyl phthalate mg/kg wet1.74 0.33 1.667 2051-128104 0.7
Di-n-octyl phthalate mg/kg wet1.79 0.33 1.667 2045-140107 3
Fluoranthene mg/kg wet1.74 0.33 1.667 2050-127105 1
Fluorene mg/kg wet1.82 0.33 1.667 2043-125109 4
Hexachlorobenzene mg/kg wet1.70 0.33 1.667 2045-122102 0.4
Hexachlorobutadiene mg/kg wet1.42 0.33 1.667 2032-12385 3
Hexachlorocyclopentadiene mg/kg wet1.97 0.33 1.667 20 L232-117118 5
Hexachloroethane mg/kg wet1.28 0.33 1.667 2028-11777 3
Indeno(1,2,3-cd)pyrene mg/kg wet2.45 0.33 1.667 20 D, L245-133147 24
Isophorone mg/kg wet1.56 0.33 1.667 2030-12294 4
Naphthalene mg/kg wet1.43 0.33 1.667 2035-12386 4
Nitrobenzene mg/kg wet1.34 0.33 1.667 2034-12280 3
N-Nitroso-di-n-propylamine mg/kg wet1.55 0.33 1.667 2036-12093 6
N-Nitrosodiphenylamine mg/kg wet2.07 0.33 1.667 2038-127124 0.9
Pentachlorophenol mg/kg wet1.76 0.33 1.667 2025-133106 4
Phenanthrene mg/kg wet1.78 0.33 1.667 2050-121107 0.9
Phenol mg/kg wet1.51 0.33 1.667 2034-12191 5
Pyrene mg/kg wet1.58 0.33 1.667 2047-12795 2
mg/kg wet 3.333 39-132Surrogate: 2,4,6-Tribromophenol 1143.81
mg/kg wet 1.667 44-115Surrogate: 2-Fluorobiphenyl 1001.67
mg/kg wet 3.333 35-115Surrogate: 2-Fluorophenol 933.11
mg/kg wet 1.667 37-122Surrogate: Nitrobenzene-d5 761.27
mg/kg wet 3.333 34-121Surrogate: Phenol-d5 913.04
mg/kg wet 1.667 54-127Surrogate: Terphenyl-d14 871.44
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Total Metals - Quality Control
Batch P8L0042 - 3050B
Blank (P8L0042-BLK1)Prepared & Analyzed: 12/05/18
Arsenic mg/kg wetBRL0.50
Selenium mg/kg wetBRL0.50
LCS (P8L0042-BS1)Prepared & Analyzed: 12/05/18
Arsenic mg/kg wet11.6 0.50 12.50 80-12093
Selenium mg/kg wet10.6 0.50 12.50 80-12085
Matrix Spike (P8L0042-MS1)Prepared & Analyzed: 12/05/18 Source: 8120022-05
Arsenic mg/kg dry16.7 0.71 17.66 6.23 M75-12559
Selenium mg/kg dry9.12 0.71 17.65 5.63 M75-12520
Matrix Spike Dup (P8L0042-MSD1)Prepared & Analyzed: 12/05/18 Source: 8120022-05
Arsenic mg/kg dry16.1 0.71 17.66 6.23 20 M75-12556 4
Selenium mg/kg dry8.22 0.71 17.65 5.63 20 M75-12515 10
Post Spike (P8L0042-PS1)Prepared & Analyzed: 12/05/18 Source: 8120022-05
Arsenic mg/L0.553 0.5001 0.176 M80-12075
Selenium mg/L0.272 0.4999 0.160 M80-12022
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 27
12/11/18
Level II QC Report
1812 Center Park Drive, Suite D
Project: Vaughn Grittin Jr.ECS Carolinas, LLP (Charlotte)
Charlotte, NC 28217
Attn: Shaun Brewer
Prism Work Order: 8120022
Time Submitted: 12/3/2018 2:40:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
General Chemistry Parameters - Quality Control
Batch P8L0087 - Solids, Dry Weight
Duplicate (P8L0087-DUP1)Prepared & Analyzed: 12/05/18 Source: 8120022-05
% Solids % by Weight72.3 0.100 70.8 202
Sample Extraction Data
Prep Method: Solids, Dry Weight
Lab Number Batch Date/TimeInitialFinal
P8L00878120022-04 12/05/18 14:2430 30g g
P8L00878120022-05 12/05/18 14:2430 30g g
P8L00878120022-06 12/05/18 14:2430 30g g
Prep Method: 3546
Lab Number Batch Date/TimeInitialFinal
P8L00388120022-04 12/04/18 16:4030 1g mL
Prep Method: 3050B
Lab Number Batch Date/TimeInitialFinal
P8L00428120022-05 12/05/18 7:502.01 50g mL
P8L00428120022-05 12/05/18 7:502.01 50g mL
P8L00428120022-06 12/05/18 7:502 50g mL
P8L00428120022-06 12/05/18 7:502 50g mL
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P8L01128120022-01 12/10/18 8:5910 10mL mL
P8L01128120022-02 12/10/18 8:5910 10mL mL
P8L01128120022-03 12/10/18 8:5910 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 27
Page 27 of 27