Loading...
HomeMy WebLinkAbout23076_RalMGP2II_PostConstVIReport_20230818POST-CONSTRUCTION/PRE-OCCUPANCY VIMS REPORT FORMER RALEIGH MGP NO. 2 AKA PLATFORM, PHASE I REDEVELOPMENT 600 WEST CABARRUS STREET RALEIGH, NORTH CAROLINA BROWNFIELDS PROJECT NO.: 23076-19-092 FORMERLY 13022-09-92 MID -ATLANTIC PE LICENSE: F-0967 REVISION NO.: 0 MID -ATLANTIC JOB NO. OOOR3746.00 August 16, 2023 Prospective Developer: KL Platform Owner, LLC Allen McCollum 4321 Lassiter at North Hills Avenue, Suite 250 Raleigh, North Carolina 27609 Phone: 919-833-7755 Email: amccollumAkanerealtycorp.com Consultant: Mid -Atlantic Associates, Inc. Daniel H. Nielsen, PE 409 Rogers View Court Raleigh, North Carolina, 27610 Phone: 919-250-9918 Email: dnielsen(cDmaaonline.com Brownfields Project Manager: Sharon Eckard, PG Mail Service Center 1646 Raleigh, North Carolina, 27699 Phone: 919-707-8379 Email: sharon.eckard(cDdeg.nc.gov The Vapor Intrusion Mitigation System (VIMS) detailed herein is designed to mitigate intrusion of subsurface vapors into the subject building from known Brownfields Property contaminants in a manner that is in accordance with the most recent and applicable guidelines including, but not limited to, DWM Vapor Intrusion Guidance, Interstate Technology & Regulatory Council (ITRC) guidance, and American National Standards Institute (ANSI)/American Association of Radon Scientists and Technologists (AARST) standards. The sealing professional engineer below is satisfied that the design and its installation are fully protective of public health from known Brownfields Property contaminants. 6elni 1 S 4 �1, Nolen Barefoot Project Scientist Ift Mid Atlantic TABLE OF CONTENTS 1.0 GENERAL INFORMATION....................................................................................1 2.0 VIMS CONSTRUCTION..........................................................................................2 2.1 VIMS Design Changes......................................................................................... 2 2.2 VIMS Construction Inspections.............................................................................2 2.3 VIMS Influence Testing........................................................................................ 2 3.0 PRE -OCCUPANCY ANALYTICAL TESTING........................................................ 3 3.1 Indoor Air Sample Collection................................................................................ 4 3.2 Sub -Slab Soil Gas Sample Collection.................................................................. 5 4.0 SUMMARY OF LABORATORY ANALYTICAL RESULTS....................................6 4.1 Indoor Air Sampling Results................................................................................. 6 4.2 Soil Gas Sampling Results................................................................................... 7 4.3 Risk Evaluation Methodology............................................................................... 7 4.3.1 Indoor Air Risk Evaluation and Results......................................................... 8 4.3.2 Sub -Slab Soil Gas Risk Evaluation and Results .......................................... 14 5.0 QUALITY ASSURANCE.......................................................................................14 6.0 SUMMARY AND CONCLUSIONS.......................................................................15 FIGURES Figure 1 Topographic Site Map Figure 2 Site Redevelopment Plan Figure 3 As -Built VIMS Monitoring Network Figure 4 As -Built VIMS Sub -Slab Components — Building A Figure 5 As -Built VIMS Sub -Slab Components — Building B Figure 6 Exposure Units TABLES Table 1 Sub -Slab Depressurization Influence Results Table 2 Monitoring Point and Indoor Air Sample Summary Table 3 Chemical Constituents Analyzed in Indoor Air Table 4 Chemical Constituents Analyzed in Soil Gas Table 5 Pre -Occupancy Indoor Air/Soil Gas Testing Risk Assessment Summary APPENDICES Appendix A VIMS Inspection Logs Appendix B Indoor Air Building Survey and Sampling Form Appendix C Field Notes Appendix D Laboratory Analytical Reports and Chain -of -Custody Records for Indoor/Ambient Air Appendix E Laboratory Analytical Reports and Chain -of -Custody Records for Sub -Slab Soil Gas Samples Appendix F Indoor Air and Sub -Slab Soil Gas Vapor Intrusion Risk Calculations 0 Mid Atlantic 1.0 GENERAL INFORMATION The subject site is on 5.7 acres located at the northwest quadrant of the intersection of West Cabarrus Street and South West Street in Raleigh, North Carolina (Figure 1). Data collected during assessment activities associated with historical use of the site as a manufactured gas plant (MGP), lumber facility, and equipment maintenance facility have identified impacts to soil, groundwater, and soil gas. The contaminants include volatile organic compounds (VOCs), both chlorinated solvents and petroleum compounds. In April 2021, sub -slab soil gas sampling activities were conducted that are summarized in Mid -Atlantic's Sub -Slab Soil Gas Assessment Report, dated May 28, 2021 (revised May 26, 2023). The VOCs detected in soil gas and groundwater on and near the subject site suggest that a vapor encroachment condition exists. Therefore, a Vapor Intrusion Mitigation System (VIMS) has been constructed in conjunction with redevelopment. The VIMS was constructed in accordance with the Vapor Intrusion Mitigation System Design Submittal, Revision 1 dated February 7, 2022 (VIMS Plan). This VIMS Plan was developed for Phase I Redevelopment, which is located on the western portion of the site (600 West Cabarrus Street) and also known as Platform (a separate VIMS Plan was developed for Phase II Redevelopment on the eastern portion of the site). This VIMS Plan was approved by the Brownfields Program (now known as Brownfields Redevelopment Section (BRS)) on March 3, 2022. Section 4 of the VIMS Plan outlines the Post-Construction/Pre-Occupation System Effectiveness Testing requirements. The VIMS Plan outlines a sequential sampling approach where the initial sampling is limited to sampling the 25 sub -slab monitoring points included in the VIMS design. Under this BRS-approved VIMS Plan, indoor air sampling would only be conducted if/where the sub -slab soil gas testing results indicated it was warranted. After approval of the VIMS Plan, and in consultation with the BRS, the Prospective Developer elected to add indoor air sampling to the initial pre -occupancy testing regime in order to expedite BRS's occupancy approval process. Addendum 1 to the VIMS Plan, dated May 25, 2023, documented that the indoor air sampling would be conducted just prior to the sub -slab sampling versus the original sequential approach. This addendum was approved by the BRS on May 26, 2023. The site is being redeveloped for mixed commercial/residential use. The new development is seven stories tall and built around an inner courtyard with pedestrian entrances to the courtyard from the south, east, and west. The designers have divided the structure into three buildings (A, B, and C, Figure 2). Building A is on the southern portion of the site and is divided by the southern courtyard entrance. This creates two areas of ground contact of nearly equal size. These two areas will be occupied on the ground floor by commercial enterprises and building support facilities. The foundation of Building A is slab -on -grade. Residential use is planned for the floors above ground floor. Building B, located north of Building A, is separated from Building A on the ground floor by the eastern and western pedestrian entrances to the courtyard. Building B is U-shaped, wrapping around the courtyard and its swimming pool. The slab -on -grade ground floor of Building B will be occupied by commercial enterprises to the west, recreational and fitness facilities to the north, and offices to the east. Floors 2 through 7 of Building B are planned for residential use and connect to Buildings A and C. Building C is the northernmost building. The ground floor of Building C is slab -on -grade parking with portions dedicated ft Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 2 to apartment building support facilities. Floors 2 through 7 of Building C include parking facilities in the center surrounded by residential apartments around the perimeter of each floor. There are no ground floor residential or commercial uses in Building C. 2.0 VIMS CONSTRUCTION Section 3 of the VIMS Plan outlines quality control and quality assurance measures required to assure the VIMS will operate effectively. The following is a summary of construction -related activities associated with the VIMS. 2.1 VIMS Design Changes As construction has progressed, design changes to the buildings were required. The design changes were minor and did not require changes to the monitoring point network or VIMS construction. Attached Figure 3 illustrates the monitoring point network, and Figures 4 and 5 illustrate the sub -slab vapor collection pit and piping locations. The VIMS was constructed in general accordance with the design. 2.2 VIMS Construction Inspections In accordance with the VIMS Plan, inspections of the VIMS were conducted at key times by Mid -Atlantic personnel. The project general contractor was Clancy and Theys Construction Company (C&T). The vapor barrier used for this project was VaporBlock Plus 20, which was installed by C&T's concrete subcontractor. Vent piping was installed by C&T's plumbing subcontractor. Barrier integrity smoke testing was conducted by RDH Environmental Consultants (RDH) and witnessed by Mid -Atlantic. An inspection log was completed for each inspection by Mid -Atlantic personnel (Appendix A). Each inspection log contains a checklist, notes describing the inspections, and photographs. Where the depressurization system was constructed (Buildings A and B), the gravel layer, sub -slab piping, and vapor collection pits were inspected by Mid -Atlantic personnel prior to placement of the VaporBlock Plus 20 vapor barrier. For all areas with vapor mitigation infrastructure, inspections were also conducted after placement and during smoke testing of the VaporBlock Plus 20 but prior to pouring the concrete floor. In total, 25 inspections were conducted during the construction of the VIMS. 2.3 VIMS Influence Testing The VIMS that includes sub -slab depressurization is in portions of Buildings A and B. The VIMS in Building C is barrier only. The influence testing was conducted in sub -slab depressurization areas to demonstrate that the VIMS could provide acceptable depressurization beneath the building floor slabs. It was initially conducted after the Ift Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase I Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 3 installation of the concrete floors and monitoring points, but prior to the completion of the risers. To test the influence of the sub -slab depressurization system, fans were placed on the risers and activated. With the fan running, the pressure differential between the sub - slab and the interior space directly above the monitoring point was measured using a TSI DP Calc meter. These measurements were recorded at six locations (MP-1, 2, 3, 5, 6 and 7, Figure 3) in Building A and 11 locations (MP-10 thru 20, Figure 3) in Building B. The design goal is to achieve a -4 pascal (pa) or greater pressure differential across the slab (less pressure below slab than above). The results of the final testing conducted on May 31, 2023, after the riser construction was completed, are summarized in Table 1, and show differential pressures ranging from -22.3 pa to -803.7 pa. These results indicate that the design goal was achieved at all 17 monitoring points. 3.0 PRE -OCCUPANCY ANALYTICAL TESTING The objective of this testing was to provide pre -occupancy data from Buildings A, B, and C to support evaluation of possible vapor intrusion risks and based on those risks, to provide the basis for approval for building occupancy and determine whether the active VIMS (i.e., sub -slab depressurization) should be activated. As detailed in the VIMS Plan and Addendum 1, pre -occupancy data consists of testing paired sub -slab soil gas and indoor air samples for the presence of VOCs by EPA Method TO-15. The evaluation included collection of 25 paired indoor air/sub-slab soil gas samples, one ambient outdoor air sample, two duplicate indoor air samples, and two duplicate sub -slab soil gas samples. Due to a transit -damaged canister, one planned indoor air sample (IA- 20) was not tested. Table 2 provides summary information for all sampling points and Figure 3 illustrates sample locations. Sampling was performed in general accordance with the Vapor Intrusion Mitigation System Design Submittal, Revision 1, including Addendum 1, as well as the following published documents: • NCDEQ, Brownfields Redevelopment Section, Vapor Intrusion Assessment Work Plan & Report Checklist (February 2023); • NCDEQ, Inactive Hazardous Sites Branch, Guidelines for Assessment and Cleanup of Contaminated Sites (September 2022); • NCDEQ, Division of Waste Management, Vapor Intrusion Guidance (March 2018); and • The Interstate Technology & Regulatory Council Vapor Intrusion Mitigation Training Team Technical Resources for Vapor Mitigation Training (December 2020). All indoor air and sub -slab soil gas sample points were co -located and sampling was closely sequenced such that the indoor air samples were collected just prior to the soil gas 0 Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 4 samples. This sequencing prevented the opening and purging of the sub -slab monitoring points from inadvertently introducing sub -slab contamination and influencing indoor air test results. 3.1 Indoor Air Sample Collection On May 30, 2023, Mid -Atlantic conducted site reconnaissance to identify potential sources (materials and activities) of indoor air VOC contaminants inside relevant portions of Buildings A, B, and C. The objective was to differentiate VOCs detected in indoor air associated with construction activities from possible vapor intrusion sources. The results of the survey are included in the Indoor Air Building Survey and Sampling Form attached in Appendix B. During the performance of the survey, small quantities (<5 gallons) of latex paint, primer, adhesives, grout, and joint compound were found throughout the buildings. Minor painting and finishing associated with typical construction activities had been performed throughout the buildings. Diesel and gasoline -powered equipment was in the courtyard, which is surrounded by Buildings A and B. Some doors and windows were yet to be installed. At these locations, plastic sheeting was taped in place to enclose the space and simulate the presence of these doors and windows. The HVAC systems were not operational at the time of sampling. The HVAC systems for the commercial areas of Buildings A and B will not be constructed until tenants for these spaces are under contract. On June 3-4, 2023, Mid -Atlantic collected 25 indoor air samples (IA-1 through IA-25), one outdoor (ambient) air sample (OA), and two duplicate samples (duplicates of IA-7 and IA- 25, Appendix C). These sample locations are summarized in Table 2 and shown in Figure 3. During sampling, the buildings were kept locked/sealed to prevent access to the testing areas. The procedures used to collect these samples are described in detail in Addendum 1 to the VIMS Plan. All indoor air samples were collected using laboratory -supplied 6-liter, individually certified, stainless -steel Summa canisters and flow regulators designed to restrict the maximum flow rate to 3-4 milliliters per minute (mL/min). The intakes for the canisters were set approximately between 3-5 feet above the floor and the initial vacuums displayed on the laboratory -supplied vacuum gauges on the flow regulators were recorded. The canisters used during indoor air sampling activities were confirmed to have retained greater than 90% of their initial volume (>27" Hg) prior to sampling. The canisters were left open over an approximately 24-hour period and closed once 24 hours had passed or a vacuum of 5" Hg was achieved. The duplicate indoor air samples were collected concurrently with the primary sample and the ambient outdoor air sample was collected at an unwind location. Upon collection, the indoor air samples were shipped to Con -Test, a Pace Analytical Laboratory, in East Longmeadow, Massachusetts under chain -of -custody control for analysis. The canisters were analyzed in the laboratory for VOCs according to EPA Method TO-15 (full list). 0 Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 3.2 Sub -Slab Soil Gas Sample Collection August 16, 2023 Page 5 Mid -Atlantic returned to the site on June 7, 2023, to collect 25 sub -slab soil gas samples (MP-1 through 25) and two duplicate samples (duplicates of MP-1 and MP-13, Appendix C). These sample locations are summarized in Table 2 and shown in Figure 3. The procedures used to collect these samples are described in detail in the VIMS Plan. As detailed in the VIMS Plan, a leak check was conducted at each of the sub -slab soil gas monitoring points prior to sample collection. Helium concentrations of at least 100,000 parts per million (ppm) were maintained in the shroud during purging. Helium was not detected within the Tedlar bag at a concentration exceeding NCDEQ's acceptable guideline of ten percent of the helium concentration under the plastic shroud at any of the sampling locations. As such, unacceptable leaks were not detected prior to soil gas sample collection. The results of Mid -Atlantic's helium leak checks at each sample location are as follows: Sample ID Helium Concentration Under Shroud Helium Concentration in Tedlar Bag MP-1 10.5 % (105,000 ppm) 50 ppm MP-1 DUP 15.8 % 158,000 m 2800 ppm MP-2 10.0 % 100,000 ppm 150 ppm MP-3 12.2 % 122,000 m 0 ppm MP-4 11.2 % 112,000 m 0 ppm MP-5 10.0 % 100,000 m 0 ppm MP-6 11.3 % 113,000 m 0 ppm MP-7 11.6 % 116,000 ppm 0 ppm MP-8 10.4 % (104,000 ppm) 0 ppm MP-9 12.8 % 128,000 m 0 ppm MP-10 12.7 % 127,000 m 0 ppm MP-11 10.2% 102,000 m 0 ppm MP-12 10.0% 100,000 m 0 ppm MP-13 10.5% (105,000 ppm) 0 ppm MP-13 DUP 10.0% 100,000 m 100 ppm MP-14 11.9% 119,000 m 150 ppm MP-15 23.4% 234,000 m 0 ppm MP-16 11.1% 111,000 m 0 ppm MP-17 12.0% 120,000 ppm 0 ppm MP-18 12.3% (123,000 m) 75 ppm MP-19 12.8% 128,000 m 0 ppm MP-20 12.5% 125,000 m 725 ppm MP-21 11.6% 116,000 m 0 ppm MP-22 18.5% 185,000 m 75 ppm MP-23 12.4% (124,000 ppm) 0 ppm ft Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 6 Sample ID Helium Concentration Helium Concentration Under Shroud in Tedlar Bag MP-24 13.5% (135,000 ppm) 0 ppm MP-25 15.3% 153,000 m 0 ppm After performing the helium leak check at each sub -slab soil gas sample location, soil gas samples were collected using laboratory -supplied 1-liter, batch -certified, stainless -steel Summa canisters and flow regulators at a maximum flow rate of 200 mL/min. The canisters used during soil gas sampling activities were confirmed to have retained greater than 90% of their initial volume (>27" Hg) prior to sampling. The initial vacuums displayed on the laboratory -supplied vacuum gauges on the flow controllers were recorded. The canisters were left open over an approximately five-minute period and closed once a vacuum of 5" Hg was achieved. Once primary samples MP-1 and MP-13 were collected, the Summa canister was disconnected. The duplicate canister was then connected to the sample location and leak tested as described above. The seal around the vapor probe was determined to be acceptable and duplicates MP-1 DUP and MP-13 DUP were collected using a Summa canister identical to the ones used for the primary samples. Upon collection, the soil gas samples were shipped to Con -Test under chain -of -custody control for analysis. The canisters were analyzed in the laboratory for VOCs according to EPA Method TO-15 (full list). Mercury contamination was not expected at the site; therefore, samples were not submitted for mercury vapor analysis. 4.0 SUMMARY OF LABORATORY ANALYTICAL RESULTS The laboratory analytical reports and chain -of -custody records for the indoor/ambient air samples and sub -slab soil gas samples are provided in Appendix D and Appendix E with results summarized in Tables 3 and 4, respectively. The ground floor use of Buildings A and B is commercial, and the ground floor use of Building C is primarily parking. However, the second through seventh floor of each building is residential use. Therefore, sample results were compared to the NCDEQ Division of Waste Management (DWM) January 2023 Residential Indoor Air Screening Levels (IASLs) and Soil Gas Screening Levels (SGSLs). 4.1 Indoor Air Sampling Results Indoor air sample results are summarized in Table 3. During the sampling event conducted on June 3-4, 2023, eight compounds were detected at concentrations exceeding Residential IASLs. Of the eight compounds, four are petroleum -related: benzene, ethylbenzene, naphthalene, and m,p-xylene; three are solvents: carbon tetrachloride, chloroform and 1,2-dichloroethane; and one is a solvent stabilizer: 1,4-dioxane. Chloroform is also known to form as a byproduct of disinfecting water supplies, while 1,2- ft Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 7 dichloroethane is used in manufacturing PVC pipes. The petroleum compounds were identified in all samples collected. Of the solvents, carbon tetrachloride was detected in all samples; chloroform was detected in 15 of 25 samples; and 1,2-dichloroethane was detected in 19 of 25 samples. 1,4-dioxane was detected in five of the 25 samples. The concentrations of the petroleum and solvent -related compounds were consistent throughout the buildings. In weeks leading up to the sampling events, a series of sealants, cleaners, caulks, adhesives, grouts, cements, paints, and other building materials containing VOCs had been used, stored, or installed in the buildings, which likely contributed to these compounds detected in indoor air. Trichloroethylene, also known as trichloroethene or TCE, is a contaminant of particular concern due to the potential for adverse health effects in sensitive populations following short-term exposure. Trichloroethylene was detected above its method detection limit (MDL) in four of the 25 samples. Three of the samples were located in the eastern portion of Building A. The fourth sample was collected in the Building C trash room. The maximum concentration detected was 0.34 ug/m3 (micrograms per cubic meter), which is below the IASL of 0.42 ug/m3 for TCE. The outdoor ambient air sample OA showed detections of 21 compounds. Both petroleum and chlorinated solvent -related compounds were detected. One compound, benzene (0.52 ug/m3), was detected at a concentration above the Residential IASL (0.36 ug/m3). This suggests that VOCs were in the outdoor/ambient air during the testing but, with the exception of benzene, not at significant concentrations. 4.2 Soil Gas Sampling Results Sub -slab soil gas sample results are summarized in Table 4. During the sampling on June 7, 2023, no compounds were detected at concentrations exceeding their Residential SGSL. TCE was detected in seven of the 25 sub -slab soil gas samples with a maximum concentration of 1.6 ug/m3, which is approximately 1/9 of the Residential SGSL of 14 ug/m3. 4.3 Risk Evaluation Methodol The cumulative risk is calculated by entering the maximum concentrations of all contaminants detected in each established exposure unit (EU) into the DEQ Risk Calculator. An EU is a defined area of a site represented by a specific set of use(s), receptors, contaminant concentrations, and exposure pathways.' The DEQ Risk Calculator determines the cancer risk sum for all carcinogens and the cumulative hazard index for all non -carcinogens under Residential and Non -Residential (industrial/commercial) exposure NCDEQ Technical Guidance for Risk -Based Environmental Remediation of Sites. March 2017. Page 40 Ift Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 8 scenarios. The BRS allows a maximum cumulative cancer risk for all carcinogens of 1.0E- 4 and a maximum cumulative hazard index (HI) of 1 for all non -carcinogens. The hazard index is the sum of the hazard quotient (HQ) calculated for each compound detected. 4.3.1 Indoor Air Risk Evaluation and Results For this assessment, eight EUs (EU-1 through EU-8) were identified in the buildings. Each EU is isolated and conditioned separately from adjacent and surrounding spaces. The EUs are depicted in Figure 6 and comprised of the spaces and samples listed in Table 2. To evaluate risk in each EU, the following data was entered into the Risk Calculator to produce each output: 1. The highest concentration of each compound detected in indoor air above MDLs was entered into the Risk Calculator. *2. These concentrations were then compared to those detected in the corresponding soil gas sample(s). If a compound was detected at a greater concentration in the indoor air than in the corresponding soil gas sample(s), thus indicating an indoor source, then the concentration detected in the soil gas was used in the risk calculation in lieu of the concentration detected in the indoor air. 3. For compounds not detected in indoor air but with MDLs above Residential IASLs, if the compound was not detected in the corresponding paired soil gas sample(s), then the compound was assumed not to be present in indoor air and was excluded from the risk calculation. If the compound was detected in the corresponding paired soil gas sample(s), then a concentration equal to the MDL from laboratory analysis of the indoor air sample was entered into the risk calculation. *This is a conservative approach because it assumes the entire concentration of a compound detected in sub -slab soil gas is contributed to the concentration detected in indoor air and does not account for attenuation provided by the chemical resistant barrier at the site, which has been sealed, inspected, and smoke -tested to confirm its integrity and effectiveness. Thus, risk is overestimated. Risk calculations for each EU are included in Appendix F. A summary of risk assessment parameters and the cumulative Residential and Non -Residential exposure cancer risk sum and non -cancer hazard index for each EU is included in Table 5. Further discussion regarding results from each EU is included below. Exposure Unit 1, Building A, East Side In EU-1, 37 compounds were detected in the indoor air. Seven of these compounds - benzene, carbon tetrachloride, chloroform, 1,2-dichloroethane, 1,4-dioxane, ethylbenzene, ft Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 9 and naphthalene- were detected at concentrations exceeding their Residential IASL. Each of these compounds was either not detected or detected at a lower concentration in the sub slab soil gas than the indoor air. This indicates that an indoor air source of these compounds is present in EU-1. Six compounds- benzyl chloride, bromodichloromethane, 1,2-dibromoethane (EDB), hexachlorobutadiene, 1,1,2,2-tetrachloroethane, and 1,1,2-trichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 1.4E-05 6.1 E-01 Non -Residential Calculated Non -Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 3.1 E-06 1.4E-01 As indicated, the cancer risk sum and cumulative non -cancer hazard index using the maximum concentrations for the indoor air samples in EU-1 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non -cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Exposure Unit 2, Building A, West Side In EU-2, 35 compounds were detected in the indoor air. Six of these compounds- benzene, carbon tetrachloride, chloroform, 1,2-dichloroethane, ethylbenzene, and naphthalene- were detected at concentrations exceeding their Residential IASL. None of these compounds were detected in the sub slab soil gas. This indicates that an indoor air source of these compounds is present in EU-2. Six compounds- benzyl chloride, bromodichloromethane, 1,2-dibromoethane (EDB), hexachlorobutadiene, 1,1,2,2-tetrachloroethane, and 1,1,2-trichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 1.8E-05 5.2E-01 EU-2 Non -Residential Calculated Non -Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 4.1 E-06 1.2E-01 0 Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 10 As indicated, the cancer risk sum and cumulative non -cancer hazard index using the maximum concentrations for the indoor air samples in EU-2 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non -cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Exposure Unit 3, Building B, West Side In EU-3, 34 compounds were detected in the indoor air. Eight of these compounds - benzene, carbon tetrachloride, chloroform, 1,2-dichloroethane, 1,4-dioxane, ethylbenzene, naphthalene, and m,p-xylene- were detected at concentrations exceeding their Residential IASL. Seven of the eight compounds were not detected in the sub slab soil gas samples. Naphthalene was detected in the sub -slab soil gas at a greater concentration than that detected in the indoor air. The data indicates that an indoor air source of seven of these compounds is present in EU-3 and that the naphthalene detected in the indoor air may have originated from soil gas. Six compounds- benzyl chloride, bromodichloromethane, 1,2-dibromoethane (EDB), hexachlorobutadiene, 1,1,2,2-tetrachloroethane, and 1,1,2-tichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 1.6E-05 5.1 E-01 Non -Residential Calculated Non -Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 3.6E-06 1.2E-01 As indicated, the cancer risk sum and cumulative non -cancer hazard index using the maximum concentrations for the indoor air samples in EU-3 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non -cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Exposure Unit 4, Building B, Move In Area In EU-4, 32 compounds were detected in the indoor air. Six of these compounds- benzene, carbon tetrachloride, 1,2-dichloroethane, 1,4-dioxane, ethylbenzene, and naphthalene - were detected at concentrations exceeding their Residential IASL. None of these compounds were detected in the sub slab soil gas. This indicates that an indoor air source of these compounds is present in EU-4. 46 Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 11 Seven compounds- benzyl chloride, bromodichloromethane, chloroform, 1,2- dibromoethane (EDB), hexachlorobutadiene, 1,1,2,2-tetrachloroethane, and 1,1,2- trichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 1.1 E-05 3.7E-01 Non -Residential Calculated Non -Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 2.6E-06 8.8E-02 As indicated, the cancer risk sum and cumulative non -cancer hazard index for the indoor air sample in EU-4 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non - cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Exposure Unit 5, Building B, Amenities Area In EU-5, 32 compounds were detected in the indoor air. Six of these compounds- benzene, carbon tetrachloride, chloroform, 1,2-dichloroethane, ethylbenzene, and naphthalene- were detected at concentrations exceeding their Residential IASL. Five of the six compounds were not detected in the sub slab soil gas samples. Chloroform was detected in the sub - slab soil gas at a greater concentration than that detected in the indoor air. The data indicates that an indoor air source of five of these compounds is present in EU-5 and that the chloroform detected in the indoor air may have originated from soil gas. Six compounds- benzyl chloride, bromodichloromethane, 1,2-dibromoethane (EDB), hexachlorobutadiene, 1,1,2,2-tetrachloroethane, and 1,1,2-trichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 1.4E-05 4.9E-01 Non -Residential Calculated Non -Residential Cumulative Non- EU-5 Carcinogenic Risk Sum Carcinogenic Hazard Index 3.2E-06 1.2E-01 0 Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 12 As indicated, the cancer risk sum and cumulative non -cancer hazard index using the maximum concentrations for the indoor air samples in EU-5 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non -cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Exposure Unit 6, Building C, Lobby, Stair, Elevator In EU-6, 26 compounds were detected in the indoor air. Three of these compounds - benzene, carbon tetrachloride, and ethylbenzene- were detected at concentrations exceeding their Residential IASL. Each of these compounds was either not detected or detected at a lower concentration in the sub slab soil gas than the indoor air. This indicates that an indoor air source of these compounds is present in EU-6. Nine compounds- benzyl chloride, bromodichloromethane, chloroform, 1,2-dibromoethane (EDB), 1,2-dichloroethane, hexachlorobutadiene, naphthalene, 1,1,2,2-tetrachloroethane, and 1,1,2-trichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 3.0E-06 1.9E-01 Non -Residential Calculated Non -Residential Cumulative Non- EU-6 Carcinogenic Risk Sum Carcinogenic Hazard Index 6.9E-07 4.6E-02 As indicated, the cancer risk sum and cumulative non -cancer hazard index using the maximum concentrations for the indoor air samples in EU-6 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non -cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Exposure Unit 7, Building C, Trash and Pump Rooms In EU-7, 32 compounds were detected in the indoor air. Six of these compounds- benzene, carbon tetrachloride, chloroform, ethylbenzene, naphthalene, and m,p-xylene- were detected at concentrations exceeding their Residential IASL. None of these compounds were detected in the sub slab soil gas. This indicates that an indoor air source of these compounds is present in EU-7. Seven compounds- benzyl chloride, bromodichloromethane, 1,2-dibromoethane (EDB), 1,2-dichloroethane, hexachlorobutadiene, 1,1,2,2-tetrachloroethane, and 1,1,2- 0 Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 13 trichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 8.3E-06 5.7E-01 Non -Residential Calculated Non -Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 1.9E-06 1.4E-01 As indicated, the cancer risk sum and cumulative non -cancer hazard index for the indoor air sample in EU-7 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non - cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Exposure Unit 8, Building C, Support Offices, Storage In EU-8, 26 compounds were detected in the indoor air. Two of these compounds- benzene and carbon tetrachloride- were detected at concentrations exceeding their Residential IASL. Neither of these compounds were detected in the sub slab soil gas. This indicates that an indoor air source of these compounds is present in EU-8. Nine compounds- benzyl chloride, bromodichloromethane, chloroform, 1,2-dibromoethane (EDB), 1,2-dichloroethane, hexachlorobutadiene, naphthalene, 1,1,2,2-tetrachloroethane, and 1,1,2-trichloroethane- had MDLs above Residential IASLs, but were not detected in soil gas; therefore, they were excluded from the risk calculation. Indoor Air Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 2.9E-06 1.6E-01 Non -Residential Calculated Non -Residential Cumulative Non - EU-8 Carcinogenic Risk Sum Carcinogenic Hazard Index 6.5E-07 3.8E-02 As indicated, the cancer risk sum and cumulative non -cancer hazard index using the maximum concentrations for the indoor air samples in EU-8 did not exceed the target risk sum of 1.0E-4 nor the target cumulative non -cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. Ift Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 4.3.2 Sub -Slab Soil Gas Risk Evaluation and Results August 16, 2023 Page 14 Section 5 of the approved VIMS Plan states that if pre -occupancy sub -slab soil gas testing and subsequent evaluation using the DWM Risk Calculator shows no unacceptable risk, that the active VIMS (i.e., sub -slab depressurization) will not be activated. Because the buildings at the site are not underlain by one contiguous foundation, communication of sub - slab soil gas between the buildings is not likely. Therefore, the site could be separated into multiple EUs. However, based on the concentrations observed and to provide a conservative evaluation, site -wide sub -slab soil gas was treated as one EU to provide a "worst -case" exposure scenario. Additionally, one analyte in sub -slab soil gas samples (1,2- dibromoethane) had an MDL above its SGSL. For the purposes of risk evaluation, a concentration of this compound equal to its MDL was assumed. Risk calculations for site - wide sub -slab soil gas samples are included in Appendix F. The cumulative Residential and Non -Residential exposure cancer risk sum and non -cancer hazard index for site -wide sub -slab soil gas are summarized in the following table: Sub -Slab Soil Gas Risk Calculations Exposure Unit Residential Calculated Residential Cumulative Non - Carcinogenic Risk Sum Carcinogenic Hazard Index 7.1 E-06 7.4E-02 Non -Residential Calculated Non -Residential Cumulative Non - Site -Wide Carcino enic Risk Sum Carcinogenic Hazard Index 5.4E-07 5.9E-03 As indicated, the cancer risk sum and cumulative non -cancer hazard index using the maximum concentrations for the sub -slab soil gas samples throughout the site did not exceed the target risk sum of 1.0E-4 nor the target cumulative non -cancer hazard index of 1 for the Residential or Non -Residential exposure scenario. 5.0 QUALITY ASSURANCE Two duplicate indoor air samples and two duplicate sub -slab soil gas samples were collected during each sampling event and analyzed for VOCs by EPA Method TO-15 (full list). Duplicate samples were collected using laboratory -provided Summa canisters and submitted to the laboratory with a vacuum of at least 5" Hg remaining in the canisters. All samples were submitted to the laboratory under chain -of -custody control for analysis. The laboratory analytical reports were reported to level II QA/QC including the reporting of J- flags (where the laboratory reported concentration is an estimated value greater than the MDL but lower than the reporting limit). Efforts were made to ensure that soil gas samples were analyzed with the lowest feasible MDLs under EPA Method TO-15. In general, duplicate samples did not appear to exhibit high variability in concentrations when ft Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 15 compared to the primary samples. There were no limitations on which constituents were reported by the laboratory (except for acrolein). 6.0 SUMMARY AND CONCLUSIONS The overall objective of this assessment was to provide pre -occupancy data from Buildings A, B, and C of Phase I Redevelopment of the former Raleigh MGP No. 2 site to evaluate whether vapor intrusion is occurring which could pose unacceptable risk to building occupants and whether the active VIMS (i.e., sub -slab depressurization) should be activated. Mid -Atlantic offers the following summary of assessment activities and results: • A total of 24 paired indoor air/sub-slab soil gas samples, one unpaired sub -slab soil gas sample (not paired due to indoor air sample canister damage during return shipping), one ambient outdoor air sample, two duplicate indoor air samples, and two duplicate sub -slab soil gas samples were collected from Buildings A, B, and C; • Site -wide, a total of eight compounds were detected in various indoor air samples at concentrations exceeding their respective Residential IASLs. These compounds were typically detected in indoor air at concentrations greater than those observed in paired soil gas samples, indicating indoor air source contributions, including being introduced from building materials associated with onsite construction; • There were no compounds detected in the soil gas at concentrations exceeding SGSLs, which indicates relatively low risk of unacceptable vapor intrusion; • TCE, a contaminant of particular concern due to the potential for adverse health effects in sensitive populations following short-term exposure, was detected in four of the 24 indoor air samples. Three of these samples were collected in EU-1 and the fourth in EU-7. The highest detected concentration of TCE was 0.34 ug/m3 in EU-7, which is below the TCE IASL of 0.42 ug/m3. Of note, TCE was not detected in the corresponding sub -slab soil gas sample from EU-7; • TCE was detected in seven of the 25 soil gas samples at low concentrations ranging from 0.84J to 1.6 ug/m3, which is approximately 11 % of the Residential SGSL of 14 ug/m3; • Risk evaluations using indoor air and soil gas data were performed on eight EUs throughout Buildings A, B, and C (EU-1 through EU-8), each isolated and conditioned separately from adjacent and surrounding spaces; • Risk evaluations using indoor air and soil gas data from each EU identified no unacceptable exposure risk under Residential use scenarios in all eight EUs; I% Mid Atlantic Post-Construction/Pre-Occupancy VIMS Report Former Raleigh MGP 2, Phase 1 Redevelopment Raleigh, North Carolina Brownfields Project Number 23076-19-092 August 16, 2023 Page 16 • Many construction materials containing VOCs had been used, stored, or installed in the buildings in the days and weeks leading up to the sampling events and likely contributed to the concentrations detected in indoor air; • A risk evaluation using site -wide sub -slab soil gas data was performed to provide a "worst -case" exposure scenario; and • The risk evaluation using site -wide sub -slab soil gas data identified no unacceptable exposure risk under a Residential use scenario. Based on the results of this assessment, Mid -Atlantic concludes the following: • Occupancy of Buildings A, B, and C for residential use does not pose an unacceptable exposure risk; • The active VIMS at the site does not need to be activated; and • A follow up sub -slab soil gas sampling event should be conducted within six months of this initial event to confirm the acceptable risk results and that operation of the active VIMS is not necessary. U Mid Atlantic FIGURES ft Mid Atlantic a REFERENCES: 1. RALEIGH WEST, NC DIGITAL RASTER GRAPHICS, USGS. SCANNED FROM 1:24,000-SCALE WAKE, NC TOPOGRAPHIC MAPS, PUBLISHED 2019, USGS. SCALE: 1:9,000 2. INSET MAP DIGITAL DATA FROM 2002 NATIONAL TRANSPORTATION ATLAS, Feet BUREAU OF TRANSPORTATION STATISTICS, WASHINGTON, D.C. 6OO 1,ZOO 3. PROPERTY BOUNDARY DATA FROM WAKE COUNTY GIS. DRAWN DATE: TOPOGRAPHIC SITE MAP BY: GCH AUGUST2023 FORMER RALEIGH MGP NO. 2 DRAFT JOB NO: Mid Atlantic 600 WEST CABARRUS STREET CHECK: OOOR3746.00 Engineering & Environmental Solutions ENG. GIS NO: RALEIGH, NORTH CAROLINA �HFrK- 9G-R374Fi_DO-1 O O N Qo I \ O / N N / \ cl) p (D N \ CD BE IDEO Q I \ 0 0 Z \ Z _ \ O 45"F-E \ � SHORT R.) - \ x \ \ Y UW Y U I � — = W 2 U LL' U aFp \ \ ® Z _ W W Z j o' PUMP < \ � r r z r� r a000N DENT ,� �,/ am am Wm am BUILDING A GROUND FLOOR: BUILDING OPERATIONAL M I� NCER SUPPORT AND COMMERCIAL N W BUILDING B GROUND FLOOR: BUILDING LEASING, r ; s pUp / 4Z W Q J O Of z c RECREATION AND COMMERCIAL I � IPME T f 11 FITNESS CHBNI TOF GE V� /��( / �l EN W :2 � U BUILDING C GROUND FLOOR: PARKING AND BUILDING OPERATIONS SUPPORT Np BE a ` � � _ 6 � a O m ERC sT ® RIGOR g ; Q o of)f �_= I. ��w� ED J Ij Lli � O� ING -MEET �OF O( O OA-1 YM O W aN EETIN Q Leo I ,I Z ' Vo VAUL _� i�,Z 4 0 A • A Co " . �IN . .® . . .I �r _ TR4SH E C Q 1 Z — TENANT�° . y G `/Il l W (n W ---------- J------- --------- �_ d0 W Z J N w 0 oN �•i, i W Of 0 64' LWi W SCALE: 1/64"=1'—O" (if MP-1 SUB -SLAB MONITORING POINT O IA-1 INDOOR AIR SAMPLE LOCATION ❑❑ OA-1 OUTDOOR AIR SAMPLE LOCATION 4 0 64' SCALE: 1/64"=1'-O" O O r7 O O N I O N r\ N r7 O 0 � cn O D � O O I Q O o � z z c� 0 O0 U Y Y U U w LLJ 2 = LL U U > of z LLd d � E Z_ � Q Q U' 0 �r �r zr �r a om wm Qm N O N Ln \ O r) LLJ Q C.� Z_ Q ry 0 Q Z (n LLJ W Z J U L�..I U Z LLJ W LL LLJ Lol 4 MP-7 ELECTRICAL VAULT PIT 3 � � 0 0 � � MAIN ELECTRICAL o MP-9 J COMMERCIAL TRASH b 0 MP-8 c2� 0 o MP-6 6" DIAMETER SCH 40 PVC PIT 4 COMMERCIAL TENANT 0 VAPOR BARRIER AREAS 0 VAPOR BARRIER AND SUB -SLAB DEPRESSURIZATION AREAS o MP-1 SUB -SLAB MONITORING POINT ❑ VAPOR PIT PIT 1 0 o MP-5 " i. _ 110, s' 10' SCALE: 3/32"=l'-0" N-) O O N O O O Q N � � � N � O cn Q O O O O Q I 0 0 z Z4� z 0 0 u o W Z 0 m Y U W U z �r 0 m Y U W U w zr W m o o dr Q m cn LLJ cn un N W � • W z � o Or-z o ZZ I__� � III (n o < z n Q CD (n a D U o = Q I=- z u 0 m m o LL_I Q o U z cn Q Q m I___ - m cn w 0 Or- z m w w m cn m oQ 0 0 om IZ L - Q0 Q m cn Q drr1a�SE0v3T.?Ply+ CA RC. �•� 0 w c� z w w w w ry i DOMESTIC PUMP ROOM r7 O O N O O o I N � � I� � N RESIDENTIAL 00� CD � MOVE -IN Q o ELEV 1 o CD "IY ELEV 2 MP-15 0 P TO TENENT STORAGE ROOM ON THIRD FLOOR o MP-14 0 Y 1' U U W W W U U LOBBY CD a- Z w > Z oa � Z5-: a- Q m c� m W M Q m 0 VAPOR BARRIER AREAS o VAPOR BARRIER AND SUB -SLAB DEPRESSURIZATION AREAS WORKSHOP MP-16 o MP-12 SUB -SLAB MONITORING POINT Q VAPOR PIT 0 GROUP PIT 5 W ° TRAINING P TO AREA BEHIND SHOWER ON THIRD FLOOR u� PIT 6 0 un N W M P —13 z U� LLJ z I— O m — LzL_I z v O O< z 0 cn < ° o 0 ❑ MEN'S cl- :�i D O FITNESS ROOM 0 zz MP-17 z v CDm Q:� ° � 0 y r S�O Lz<LI (Q- O ° O z ROOM u COMMERCIAL Y'SY,�' � .Z TENANT o �ELEV 3 _ �-= Y �S�SY � SY =Y =� � S� � � WII J u) m O Q 0 PIT 7 TV � ELEV 4 O O o _ Y Z-Y OUNGE Q Eo O MP-18 1 � WJ x CLUB CORRIDOR P TO CLOSET ON THIRD FLOOR P TO ELECTRICAL ROOM ON THIRD FLOOR R t '�Vener�y��aot;�r''�n MAIL ROOM O M P —19 PIT 5� Lu CD Q Y 0 d aSS8x8x3/8 0 0 0 PHONE ROOM MEETING o ❑ PIT 8 SS8x80/8EJ WORK / OFFICE LEASING BREAK O L 0 MP-11 Z lJ MP-10 06 o Y o O 0 o 3: c O OFFICEcu o MP-20 MEETING N El 0 F1 w LLi U Z 1 ' 0' 5' 10' W W SCALE: 3/32"=V-0" � J r7 O O O O \ o co I EU S N NO cl) p O MP-25 \ IA-25 \ O O STORAGE • • Q I O o O A 24 - - \ H m � � 0NCE MAOFF E 'RAGE , , • a O Q ST 0 \ LECTRICAL / TERM) X x • \ Y U Y U / \ LL1 W EU 7_W U U ui R ots \ \ Z> Z LiRo O G DES MP-23 ® r r zr CIE �r R ROOM IA-23 am o m w m Q m IA-15 EU 4 E RESIDENTIAL MP-15 RISER 0 IA-1 R°° MP-16 / MP-1 SUB -SLAB MONITORING POINT MP-14 IA-16 N O IA-1 INDOOR AIR SAMPLE LOCATION ��li 3 8a. � W Q o o- z ❑❑ OA-1 OUTDOOR AIR SAMPLE LOCATION . , ff GR°°, TRAINING ° / �/'� J V / O ❑ EU 2 EXPOSURE UNIT IA-13 • IA-13 O ` CUP W Q EU 3 . �\ EITM1E� REN '^ MP-2 s U (n f OIA-17 oREM IA-22 EU 6 = � I MP-12 . 00 IA-12 MP-17 • Lus W O Q COMM-1 A�TAL TEN9776 IA-i 8 GE LIJ Q O J U Z N O SE MP-18 MP-21 N • IA-21 O Df ® a_ V) Z W n1P919 � J II ® oo" MEETING(If ROOM O Q O oOf O MP-11 IA-10 00IA-11 r ° 0 EaSI" GI EU 5 W p ® MP-10 aR�k IA-20 0 LiOA-1 MP-20 E ° EI 11 0LID Q DIN -- -• t0 L I • • • U 4 • ■ MP-3 �+ o Of IAP 77 O ■ • _ I 0O IA-3 _ • • 0 ELECATRI L -- ® ■ . O EU 2 " IA-9 • MP-9 ® ® • EU 1 cd c EL IGAL $8 MP-4 IA-4 j E Q TFASR MP o Z P - — ......7ERA"T . °P • I > c C0 szSE iy � COMMERCIAL TENANT SF SMP-1 c MP-6 MP IA- I -5 • MP-2 • f --—--- — — —— J L ——————----— — — — — —— N c J w (� O" W (if 0 64' LWi W SCALE: 1/64"=1'-O" (Y TABLES 0 Mid Atlantic r TABLE 1 SUB -SLAB DEPRESSURIZATION INFLUENCE RESULTS FORMER RALEIGH MGP NO. 2 PHASEIREDEVELOPMENT RALEIGH, NORTH CAROLINA MID -ATLANTIC JOB NO. R3746.00 Monitoring Point Vacuum Reading (pascals, pa) MP-1 -448.1 MP-2 -664.3 MP-3 -685.5 MP-5 -800.6 MP-6 -803.7 MP-7 -786.2 MP-10 -31.5 MP-11 -22.3 MP-12 -88.7 MP-13 -129.5 MP-14 -78.6 MP-15 -96.6 MP-16 -203.7 MP-17 -233.6 MP-18 -217.3 MP-19 -151.2 M P-20 -211.5 TABLE 2 MONITORING POINT AND INDOOR AIR SAMPLE SUMMARY FORMER RALEIGH MGP NO. 2 PHASEIREDEVELOPMENT RALEIGH, NORTH CAROLINA MID -ATLANTIC JOB NO. R3746.00 Description/Use Indoor Air Samples Sub -Slab Monitoring Points Building A, east side, commercial IA-1, IA-2, IA-3, IA-4 MP-1, MP-1 DUP, MP-2, MP-3, M P-4 Building A, west side, commercial IA-5, IA-6, IA-7, IA-7 DUP, MP-5, MP-6, MP-7, MP-8, MP-9 IA-8,IA-9 Building B, west side, commercial IA-10, IA-11, IA-12, IA-13, MP-10, MP-11, MP-12, MP-13, IA-14 MP-13 DUP, MP-14 Building B, north end, move -in IA-15 MP-15 Building B, northeast side, amenities, office IA-16, , , IA-17IA-18IA-19 MP-16, MP-17, MP-18, MP-19, MP-20 Building C, east end, lobby, stair, elevator IA-21, IA-22 MP-21, MP-22 Building C, west end, trash IA-23 MP-23 Building C, north end, maintenance office IA-24 MP-24 Building C, north end, storage IA-25, IA-25 DUP MP-25 TABLE 3 CHEMICAL CONSTITUENTS ANALYZED IN INDOOR AIR FORMER RALEIGH MGP NO. 2 PHASEIREDEVELOPMENT RALEIGH, NORTH CAROLINA MID -ATLANTIC JOB NO. R3746.00 EU1 EU2 EU3 Sample ID P IA-1 IA-2 IA-3 ll Greatest Concentration IA-5 IA-6 IA-7 IA-7 DUP IA-8 IA-9 Greatest Concentration IA-10 IA-11 IA-12 IA-13 IA-14 Greatest Concentration NCDEQ DWM Residential Indoor Air Screening Levels January 2023 (ug/m') NCDEQ DWM Non-Residental Indoor Air Screening Levels January 2023 (ug/m') Sampling Date 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 11 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 Acetone 130 130 120 51 130 290 E 290 E 290 E 290 E 120 E 260 E 290 340 E 330 E 330 E 330 E 330 E 340 HE NE Benzene 0.74 0.76 0.69 0.63 0.76 0.78 0.77 0.76 0.69 0.74 0.49 0.78 0.76 0.78 0.74 0.76 0.78 0.78 0.36 1.6 Benzyl Chloride- <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 <0.16 0.16 0.057 0.25 Bromodichloromethene' <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 <0.16 0.16 0.076 0.33 Bromoform <0.25 <0.25 <0.25 <0.25 NO <0.25 <0.25 <0.25 <0.24 <0.25 <0.25 NO <0.25 <0.24 <0.25 <0.25 <0.25 ND 2.6 11 Bromomethane <0.090 0.101 <0.090 <0.090 0.10 <0.090 <0.090 0.092J <0.090 <0.090 <0.090 0.092 <0.090 <0.090 <0.090 <0.090 <0.090 NO 1.0 4.4 1,3-Butadiene <0.065 <0.065 <0.065 <0.065 NO <0.065 <0.065 <0.065 <0.065 <0.065 <0.065 NO <0.065 <0.065 <0.065 <0.065 <0.065 NO 0.094 0.41 2-Butanone (MEK) 60 55 55 7.0 L-05 60 53 48 47 34 12 L-05 29 53 47 39 42 32 L-05 40 L-05 47 1000 4400 Carbon Disulfide 1.5 1.5 1.8 0.111 1.8 2.8 2.8 2.9 0.75J 0.57J 0.651 2.9 1.2 1.2 1.1 1.2 1.11 1.2 150 610 Carbon Tetrachloride 0.49 0.56 0.50 0.47 0.56 0.53 0.53 0.50 0.57 0.48 0.49 0.57 0.52 0.50 0.47 0.49 0.51 0.52 0.47 2.0 Chlorobenzene <0.11 <0.11 <0.11 <0.11 NO <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 NO <0.11 <0.11 <0.11 <0.11 <0.11 NO 10 44 Chloroethane <0.082 0.14 0.11 <0.082 0.14 <0.082 <0.082 0.085 J <0.081 <0.082 <0.082 0.085 0.42 0.45 0.44 0.51 0.42 0.51 830 3500 Chloroform 0.17 0.20 0.17 <0.16 0.20 0.51 0.29 0.32 0.19 0.17 J <0.16 0.51 0.24 0.27 0.25 0.26 0.24 0.27 0.12 0.53 Chloromethane 1.2 1.4 1.3 1.2 1.4 1.2 1.2 1.3 1.3 1.3 1.2 1.3 1.1 1.1 1.2 1.2 1.2 1.2 19 79 Cyclohexane 0.34 0.44 0.37 1.3 1.3 0.51 1.3 0.50 0.26 1.1 0.22 1.3 1.2 1.2 1.2 1.2 1.2 1.2 1300 5300 Dibromochloromethane -0.20 -0.20 -0.20 -0.20 NO -0.20 -0.20 -0.20 -0.20 <0.20 <0.20 NO -0.20 -0.20 -0.20 -0.20 <0.20 NO HE HE 1,2-Dibromoethane(EDB)* <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 <0.16 0.16 0.0047 0.02 1,2-Dichlorobenzene -0.12 -0.12 -0.12 -0.12 NO -0.12 -0.12 -0.12 -0.12 -0.12 -0.12 NO -0.12 <0.12 <0.12 <0.12 <0.12 NO 42 180 1,3-Dichlorobenzene <0.12 <0.12 <0.12 <0.12 NO <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 NO <0.12 <0.12 <0.12 <0.12 <0.12 ND NE NE 1,4-Dichlorob---us <0.14 <0.14 <0.14 <0.14 ND <0.14 <0.14 <0.14 <0.14 <0.14 -0.14 ND <0.14 <0.14 <0.14 <0.14 -0.14 ND 0.26 1.1 Dlchlorodi uoromelhane Freon 121 27 27 2.6 2.6 2.7 2.7 2.7 2.8 3.0 2.6 2.6 3.0 2.8 2.7 2.8 2.8 2.6 2.8 21 88 1,1-Dichlomethane <0.12 <0.12 <0.12 <0.12 ND <0.12 <0.12 <0.12 <0.12 <0.12 <0.12 ND <0.12 <0.12 <0.12 <0.12 <0.12 ND 1.8 7.7 1,2-Dichlomethane 0.19 0.19 0.18 0.17 0.19 0.29 0.31 0.29 0.18 0.24 0.16 0.31 0.24 0.28 0.24 0.28 0.27 0.27 0.11 0.47 1,1-Dichloroelhylene <0.11 <0.11 <0.11 <0.11 ND <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 ND <0.11 <0.11 <0.11 <0.11 <0.11 ND 42 180 is-1,2-Dichloroelhylene <0.10 <0.10 <0.10 <0.10 NO <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NO <0.10 <0.10 <0.10 <0.10 <0.10 NO 8.3 35 trans-1,2-Dichloroelhylene <0.11 <0.11 <0.11 <0.11 ND <0.11 <0.11 <0.11 <0.11 <0.11 <0.11 ND <0.11 <0.11 <0.11 <0.11 <0.11 ND 8.3 35 1,2-Dichloropropane 0.097J <0.087 <0.087 <0.087 0.097 0.17 0.16 0.17 0.111 0.093J 0.101 0.17 0.29 0.30 0.29 0.30 0.27 0.30 0.76 3.3 cis-1,3-Dichloropropene <0.082 <0.082 <0.082 <0.082 ND <0.082 <0.082 <0.082 <0.082 <0.082 <0.082 ND <0.082 <0.082 <0.082 <0.082 <0.082 ND HE HE trans-1,3-Dichloropropene <0.081 <0.081 <0.081 <0.081 NO <0.081 <0.081 <0.081 <0.081 <0.081 <0.081 NO <0.081 <0.081 <0.081 <0.081 <0.081 NO HE HE 1,2-Dichloro-1,1,2,2- tetrafluoroethane Freon 114' <0.24 <0.24 <0.24 <0.24 ND <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 ND <0.24 <0.24 <0.24 <0.24 <0.24 ND NE HE 1,4-Dioxane 0.69 J 0.70 J 0.86 J <0.10 0.88 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 ND 1.3 <0.10 <0.10 <0,10 <0,10 1.3 0.56 2.5 Ethanol 61 59 59 44 61 83 E 82 E 79 E 37 87 E 32 87 67 68 66 68 68 68 HE HE Ethyl Acetate 0.911 1.7 1.0 J 1.2 J 1.7 2.3 2.2 1.7 0.88 J 2.2 0.94 J 2.3 2.0 2.3 2.0 2.3 2.0 2.3 15 61 Ethylbenzene 2.4 2.5 2.5 0.63 2.5 4.0 4.1 4.1 2.4 1.9 2.0 4.1 5.4 5.0 5.2 5.3 5.4 5.4 1.1 4.9 4-Ethyltoluene 0.27 0.28 0.23 <0.11 0.28 0.36 0.44 0.43 0.22 0.25 0.17 0.44 0.49 0.46 0.50 0.49 0.40 0.50 NE HE Heptane 2.4 2.5 2.3 1.1 2.5 26 27 26 30 4.9 26 30 6.2 6.0 5.9 6.2 6.0 6.2 83 350 Hexachlorobutadiene' <0.31 <0.31 <0.31 <0.31 0.31 <0.31 <0.31 <0.31 0.31 <0.31 0.31 0.31 <0.31 <0.31 <0.31 <0.31 <0.31 0.31 0.13 0.56 Hexane 1.6 J 2.0 J 2.0 J <0.64 2.0 2.1 J 1.6 J 1.8 J 0.80 J 0.78 J <0.64 2.1 8.7 9.0 8.1 6.3 5.2 9.0 150 610 2-Hexanone(MBK) 0.85 0.62 0.48J 0.61 0.85 1.1 0.73 0.63 0.29J 0.78 0.20J 1.1 0.63 0.66 0.75 0.77 0.75 0.77 6.3 26 Isopmpanol 8.9 8.9 8.7 4.7 8.9 12 12 11 5.3 10.0 4.5 12 6.6 7.1 6.2 6.5 6.6 7.1 42 180 Methyl tert-Butyl Ether (Ml <0.097 <0.097 <0.097 <0.097 NO <0.097 <0.097 <0.097 <0.097 <0.097 <0.097 NO <0.097 <0.097 <0.097 <0.097 <0.097 NO 11 47 Methylene Chloride <0.56 <0.56 <0.56 <0.56 NO <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 NO <0.56 <0.56 <0.56 <0.56 <0.56 NO 100 530 4-Methyl-2-pentanone (MIBK) 0.76 0.81 0.68 0.98 0.98 <0.076 <0.076 <0.076 <0.076 1.6 <0.076 1.6 1.3 1.3 1.3 1.4 1.4 1.4 630 2600 Naphthalene 0.36 V-08 1 0.34 V-08 1 0.23 V-08 1 0.15 J LZ-01 -0 V46 0 36 OA4 V-08 1 0.61 V-08 1 OAS V-08 1 0.23 V46 1 0.17 J L-0 V-06Z-01 0.18 J V-06 1 0 67 OA2 V-08 1 0.55 V-06 1 OAS V-08 1 OAO L-0 V-0 Z41 0.30 L-65V-66Z-61 0.55 0.083 0.36 Propene <0.53 1.7 J 1.6 J 0.86 J 1.7 2.2 J 2.1 J <0.53 <0.53 1.2 J 1.11 2.2 2.3 J 2.1 J <0.53 2.3 J <0.53 2.3 630 2600 Styrene 2.0 2.1 2.1 0.55 2.1 5.4 5.6 5.8 5.9 5.7 5.1 5.9 4.0 3.7 3.7 3.9 3.8 4.0 210 880 1,1,2,2-Tetrachloroethane' <0.13 <0.13 <0.13 <0.13 0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.13 0.048 0.21 Tetrechloroethylene 0.21 J 0.24 0.22 J <0.18 0.24 0.30 0.30 0.27 <0.18 <0.18 -0.18 0.30 <0.18 1.0 -0.18 -0.18 -0.18 1.0 8.3 35 Tetrahydmfumn 97 92 90 3.7 97 74 74 79 100 8.0 87 100 100 99 97 100 100 100 420 1800 Toluene 20 19 19 4.7 20 63 64 62 56 23 48 64 120 110 110 120 120 120 1000 4400 1,2,4-Trichlorobenzene <0.24 <0.24 <0.24 <0.24 ND <0.24 <0.24 <0.24 <0.24 <0.24 <0.24 ND <0.24 <0.24 <0.24 <0.24 <0.24 ND 0.42 1.8 1,1,1-Trichloroethane <0.15 <0.15 <0.15 <0.15 NO <0.15 <0.15 <0.15 <0.15 <0.15 <0.15 NO <0.15 <0.15 <0.15 <0.15 <0.15 NO 1000 4400 1,1,2-Trichloroethane' <0.13 <0.13 <0.13 <0.13 0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.13 0.042 0.18 Trichloroethylene 0.29 0.15 J 0.18 J <0.13 0.29 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NO <0.13 <0.13 <0.13 <0.13 <0.13 NO 0.42 1.8 Trichloro uoromet ane r on 11) 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.4 1.2 1.2 1.4 1.2 1.2 1.2 1.2 1.2 1.2 NE HE 1,1,2-Tdchloro-1,2,2- tdfluoroethane Freon 113' 0.50 J 0.53 J 0.44 J 0.48 J 0.53 0.48 J 0.511 0.511 0.59 J 0.50 J 0.48 J 0.59 0.49 J 0.47 J 0.49 J 0.48 J 0.49 J 0.49 1000 4400 1,2,4-Tdmethylbenzene 1.6 1.7 1.5 0.46 1.7 2.7 2.9 2.8 1.4 1.4 1.2 2.9 3.2 3.0 3.0 3.1 3.1 3.2 13 53 1,3,5-Trimethylbenzene 0.40 0.39 0.35 0.111 0.40 0.66 0.69 0.66 0.32 0.37 0.27 0.69 0.80 0.71 0.78 0.73 0.73 0.80 13 53 Vinyl Acetate 6.0 <0.66 <0.66 2.6 6.0 7.0 6.7 <0.66 <0.66 3.1 <0.66 7.0 <0.66 <0.66 <0.66 <0.66 <0.66 NO 42 180 Vinyl Chloride <0.080 <0.080 <0.080 <0.080 ND <0.080 <0.080 <0.080 <0.080 <0.080 <0.080 ND <0.080 <0.080 <0.080 <0.080 <0.080 ND 0.17 2.8 m&p-Xylene 9.7 9.8 10 2.3 10 16 16 16 9.4 7.2 8.0 16 22 20 20 21 21 22 21 88 o-Xylene 3.8 3.8 3.9 1.0 3.9 6.0 6.0 6.0 3.5 2.5 2.9 6.0 7.4 6.9 7.0 7.3 7.2 7.4 21 88 Nate.: Concentration units: pg/m' NCDEQ DWM = North Carolina Department of Environmental Quality Division of Waste Management J = Estimated Concentration E = Reported result is estimated. Value reported over verified calibration range. HE = Not Established -= Compound was not detected, but had a lab method detection limit (MDL) over the Residential Indoor Air Screening Level. For the purpose of risk evaluation, concentrations of this compound equal to its MDL were assumed. L-05 = Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the high side. V-06 = Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. Z-01 = Calibrations relative standard deviation (RSD) for this compound is>30 % but <40%. Bolded concentrations exceed the Residential Indoor Air Screening Level Shaded concentrations exceed the Non -Residential Indoor Air Screening Level <0.34 = Not detected above the lab method detection limit MDL TABLE 3 CHEMICAL CONSTITUENTS ANALYZED IN INDOOR AIR FORMER RALEIGH MGP NO. 2 PHASEIREDEVELOPMENT RALEIGH, NORTH CAROLINA MID -ATLANTIC JOB NO. R3746.00 Sample ID EU 4 EU 5 EU 6 EU 7 EU 8 CA NCDEQ DWM Residential Indoor Air Screening Levels January 2023 (ug/m') NCDEQ DWM Non -Residential Indoor Air Screening Levels January 2023 (ug/m') IA-15 IA-16 IA-17 IA-18 IA-19 Greatest Concentration IA-21 IA-22 Greatest Concentration IA-23 IA-24 IA-25 IA-25 DUP Greatest Concentration Sampling Date 6/4/2023 1 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 11 6/4/2023 6/4/2023 6/4/2023 6/4/2023 6/4/2023 Acetone 130 50 47 89 79 89 41 39 41 210 22 33 32 33 14 NE NE Benzene 0.85 1.7 1.7 0.79 0.70 1.7 0.66 0.59 0.66 0.47 0.64 0.55 0.47 0.64 0.52 0.36 1.6 Benzyl Chloride' <0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 0.057 0.25 Bromodichloromethane' <0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 0.076 0.33 Bromoform -0.25 <0.25 <0.25 <0.25 <0.25 NO <0.25 <0.25 NO <0.25 <0.25 <0.25 <0.25 NO <0.25 2.6 11 Bromomethane <0.090 <0.090 <0.090 <0.090 <0.090 NO <0.090 <0.090 NO 0.36 <0.090 <0.090 <0.090 NO <0.090 1.0 4.4 1,3.Butadiene <0.065 <0.065 <0.065 <0.065 <0.065 NO <0.065 <0.065 NO <0.065 <0.065 <0.065 <0.065 NO <0.065 0.094 0.41 2-Butanone (MEK) 28 L-05 9.7 L-05 9.6 L-05 160 93 160 19 L-05 23 L-05 23 22 L-05 11 L-05 11 L-05 11 L-05 11 2.0 L-05,J 1000 4400 Carbon Disulfide 0.17 J 0.13 J 0.16 J 0.64 J 0.64 J 0.64 0.111 <0.10 0.11 0.101 <0.10 <0.10 <0.10 NO <0.10 150 610 Carbon Tetrachloride 0.50 0.48 0.- 0.48 0.43 0.- 0.48 0.51 0.51 0.50 0.- 0.50 0.50 0.50 0.47 0.47 2.0 Chlorobenzene <0.11 <0.11 <0.11 <0.11 <0.11 NO <0.11 <0.11 NO <0.11 <0.11 <0.11 <0.11 NO <0.11 10 44 Chlomethane 0.092 <0.082 <0.082 0.11 0.11 0.11 <0.082 <0.082 NO <0.082 <0.082 <0.082 <0.082 NO <0.082 830 3500 Chloroform <0.16' <0.16 <0.16 0.17 0.18 0.18 <0.16 <0.16 0.16- 0.16 J <0.16 <0.16 <0.16 0.16' <0.16- 0.12 0.53 Chloromethane 1.2 1.2 1.1 1.3 1.2 1.3 1.1 1.2 1.2 1.2 1.1 1.2 1.2 1.2 1.3 19 79 Cyclohexane 1.5 1.7 2.1 2.6 1.9 2.6 0.52 0.79 0.79 4.2 0.098 J 0.12 J 0.14 0.14 <0.073 1300 5300 Dibromochloromethane <0.20 <0.20 <0.20 <0.20 <0.20 NO <0.20 <0.20 NO <0.20 <0.20 <0.20 <0.20 NO <0.20 NE NE 1,2.Dibromoethane(EDB)' <0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 <0.16 0.16 <0.16 <0.16 <0.16 <0.16 0.16 <0.16 0.0047 0.02 1,2.Dichlorobenzene -0.12 <0.12 -0.12 <0.12 <0.12 ND <0.12 <0.12 ND <0.12 <0.12 <0.12 <0.12 ND <0.12 42 180 1,3-Dichlorobenzene <0.12 <0.12 <0.12 <0.12 <0.12 ND <0.12 <0.12 ND <0.12 <0.12 <0.12 <0.12 ND <0.12 NE NE 14-Dichlorobenzene <0.14 <0.14 <0.14 <0.14 <0.14 ND <0.14 <0.14 ND <0.14 <0.14 <0.14 <0.14 ND <0.14 0.26 1.1 Dlchlonedi uoromelhane Freon 121 26 2.6 2.6 3.1 2.5 3.1 2.6 2.6 2.6 2.5 2.6 2.6 2.8 2.8 2.6 21 88 1,1-Dichlomethane -0.12 <0.12 <0.12 <0.12 <0.12 ND <0.12 <0.12 ND <0.12 <0.12 <0.12 <0.12 ND <0.12 1.8 7.7 1,2-Dichlomelhane 0.27 0.27 0.27 0.32 0.28 0.32 <0.13 <0.13 0.13' <0.13' <0.13 <0.13 <0.13 0.13' <0.13' 0.11 0.47 1,1-Dichloroethylene <0.11 <0.11 <0.11 <0.11 <0.11 ND <0.11 <0.11 ND <0.11 <0.11 <0.11 <0.11 ND <0.11 42 180 cis-1,2-Dichloroethylene -0.10 <0.10 <0.10 <0.10 <0.10 ND <0.10 <0.10 ND <0.10 <0.10 <0.10 <0.10 ND <0.10 8.3 35 trans-1,2-Dichloroelhylene <0.11 <0.11 <0.11 <0.11 <0.11 ND <0.11 <0.11 ND <0.11 <0.11 <0,11 <0.11 ND <0,11 8.3 35 1,2-Dichloropropane 0.111 <0.087 <0.087 <0.087 <0.087 ND <0.087 <0.087 ND 0.151 <0.087 <0.087 <0.087 ND <0.087 0.76 3.3 cis-1,3-Dichloropropene <0.082 <0.082 <0.082 <0.082 <0.082 ND <0.082 <0.082 ND <0.082 <0.082 <0.082 <0.082 ND <0,082 NE HE trans-1,3-Dichloropropene <0.081 <0.081 <0.081 <0.081 <0.081 ND <0.081 <0.081 ND <0.081 <0.081 <0.081 <0.081 ND <0.081 NE HE 1,2-Dichloeth.m 2,2- tetra8uoroethane Freon 114' <0.24 <0.24 <0.24 <0.24 <0.24 ND <0.24 <0.24 ND <0.24 <0.24 <0.24 <0.24 ND <0.24 NE HE 1,4-Dioxane 0.67 J <0.10 <0.10 <0.10 <0.10 ND <0.10 <0.10 ND <0.10 <0.10 <0.10 <0.10 ND <0.10 0.56 2.5 Ethanol 110 100 E 130 E 570 E 640 E 640 21 22 22 240 17 14 15 17 8.9 HE HE Ethyl Acetate 0.97 J 1.9 2.0 3.4 3.0 3.4 0.76 J 2.0 2.0 <0,64 0.97 J <0,64 0.65 J 0.97 <0,64 15 61 Ethylbenzene 3.0 1.3 1.4 4.1 3.2 4.1 1.2 1.9 1.9 7.1 0.28 0.78 0.77 0.78 0.25 1.1 4.9 4-Ethyltoluene 0.20 0.14 J 0.15 J 1 0.50 0.74 0.74 0.19 0.20 0.20 0.17 <0.11 0.15 J 0.16 J 1 0.16 <0.11 NE HE Heptsne 5.4 14 20 35 24 35 0.54 0.63 0.63 13 0.27 0.23 0.21 0.27 0.35 83 350 Hexachlorobutadiene' <0.31 <0.31 <0.31 <0.31 <0.31 0.31 <0.31 <0.31 0.31 <0.31 <0.31 <0.31 <0.31 0.31 <0.31 0.13 0.56 Hexane 5.4 1.9 J 2.0 J 2.2 J 1.7 J 2.2 1.6 J <0.64 1.6 15 <0.64 <0.64 <0.64 NO <0.64 150 610 2-Hexanone (MBK) 0.67 0.51 J 0.37 J 0.81 0.79 0.81 0.27 J 0.44 J 0.44 0.85 0.41 J 0.35 J 0.34 J 0.41 0.13 J 6.3 26 Isopropanol 9.0 4.0 4.0 6.3 5.8 6.3 1.2J 1.9J 1.9 21 1.2J 1.4J 1.2J 1.4 0.69J 42 180 Methyl tert-Butyl Ether (MTBE) <0,097 <0.097 <0.097 <0.097 <0.097 NO <0.097 <0.097 NO <0.097 <0.097 <0.097 <0.097 NO <0.097 11 47 Methylene Chloride <0.56 -0.56 <0.56 <0.56 <0.56 NO <0.56 <0.56 NO <0.56 -0.56 <0.56 <0.56 NO <0.56 100 530 4-Methyl-2-pentanone (MIBK) 2.3 1.8 2.6 10 9.9 10 0.28 0.37 0.37 5.1 0.23 0.25 0.25 0.25 0.083J 630 2600 Naphthalene 0.39 L4V-06 Z-0t 0.25 L.05 V-06 Z-01 0.31 L4V416 Z-01 0.53 L4V-06 Z-01 0.57 L4V-06 Z-Ot 0.57 <0.14 Z-01 <0.14 Z-01 0.14' 0.27 1_41V-06 Z-01 <0.14 Z-01 <0.14 Z-01 <0.14 Z-01 0.14' <0.14Z-01' 0.083 0.36 Propene 1.61 1.7J 1.5J 1.81 1.4J 1.8 1.11 1.7J 1.7 1.11 0.87J 0.67J 0.67J 0.87 0.57J 630 2600 Styrene 6.4 1.8 1.9 3.8 3.3 3.8 0.38 0.39 0.39 20 0.98 0.66 0.66 0.98 0.12 J 210 880 1,1,2,2-Tetrachloroethane' <0.13 <0.13 <0.13 <0.13 <0.13 0.13 <0.13 <0.13 0.13 <0.13 <0.13 <0.13 <0.13 0.13 <0.13 0.048 0.21 Tetrachloroethylene <0.18 <0.18 <0.18 <0.18 <0.18 NO <0.18 <0.18 ND 0.211 <0.18 <0.18 <0.18 ND <0.18 8.3 35 Tetrahydrefuran 170 18 18 48 50 50 39 32 39 200 21 40 41 41 0.73J 420 1800 Toluene 190 50 63 110 80 110 4.4 4.0 4.4 690 4.7 29 29 29 1.3 1000 4400 1,2,4-Trichlorobenzene <0.24 <0.24 <0.24 <0.24 <0.24 ND <0.24 <0.24 ND <0.24 <0.24 <0.24 <0,24 ND <0.24 0.42 1.8 1,1,1-Tdchloroethane <0.15 <0.15 <0.15 <0.15 <0.15 NO <0.15 <0.15 NO <0.15 <0.15 <0.15 <0.15 NO <0.15 1000 4400 1,1,2-Tdchloroelhane' <0.13 <0.13 <0.13 <0.13 <0.13 0.13 <0.13 <0.13 0.13 <0.113 <0.113 <0.13 <0.13 0.13 <0.13 0.042 0.18 Trichloroethylene <0.13 <0.13 <0.13 <0.13 <0.13 NO <0.13 <0.13 NO 0.34 <0.13 <0.13 <0.13 NO <0.13 0.42 1.8 Trichloro uorome a on 11) 1.2 1.2 1.2 1.1 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 1.2 NE HE 1,1,2-Trichloro-1,2,2- trifluoroethane Freon 113' 0.50 J 0.48 J 0.47 J 0.50 J 0.52 J 0.52 0.44 J 0.46 J 0.46 0.47 J 0.50 J 0.48 J 0.47 J 0.50 0.47 J 1000 4400 1,2,4-Trimethylbenzene 1.3 0.83 0.86 3.1 4.0 4.0 1.2 1.3 1.3 0.88 0.28 0.92 0.96 0.96 0.24 13 53 1,3,5-Trimelhylbenzene 0.28 0.21 0.20 0.96 1.4 1.4 0.30 0.34 0.34 0.23 <0.091 0.25 0.25 0.25 <0.091 13 53 Vinyl Acetate <0.66 <0.66 <0.66 7.3 <0.66 7.3 <0.66 5.5 5.5 <0.66 3.4 <0.66 <0.66 3.4 <0.66 42 180 Vinyl Chloride <0.080 <0.080 <0.080 <0.080 <0.080 ND <0.080 <0.080 ND <0.080 <0.080 <0.080 <0.080 ND <0.080 0.17 2.8 m&p-Xylene 13 4.8 5.2 15 12 15 4.4 7.0 7.0 32 0.83 3.0 3.1 3.1 0.87 21 88 o-Xylene 5.0 1.9 2.2 5.2 4.4 5.2 1.4 2.2 2.2 12 0.40 1.3 1.4 1.4 0.29 21 88 Notes: Concentration units: pg/m' NCDEQ DWM = North Carolina Department of Environmental Quality Division of Waste Management J = Estimated Concentration E = Reported result is estimated. Value reported over verified calibration range. HE = Not Established -= Compound was not detected, but had a lab method detection limit (MDL) over the Residential Indoor Air Screening Level. For the purpose of risk evaluation, concentrations of this compound equal to its MDL were assumed. L-05 = Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the high side. V-06 = Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. Z-01 = Calibrations relative standard deviation (RSD) for this compound is>30 % but <40%. Bolded concentrations exceed the Residential Indoor Air Screening Level Shaded concentrations exceed the Non -Residential Indoor Air Screening Level <0.34 = Not detected above the lab method detection limit MDL TABLE 4 CHEMICAL CONSTITUENTS ANALYZED IN SOIL GAS FORMER RALEIGH MGP NO. 2 PHASEIREDEVELOPMENT RALEIGH, NORTH CAROLINA MID -ATLANTIC JOB NO. R3746.00 Sample ID EU 1 EU 2 EU 3 NCDEQ DWM Residential Soil Gas Screening Levels January 2023 (Ng/ms) NCDEQ DWM Non -Residential Soil Gas Screening Levels January 2023 (pg/ms) MP-1 MP-1 DUP MP-2 MP-3 MP-4 MP-5 MP-6 MP-7 MP-8 MP-9 MP-10 MP-11 MP-12 MP-13 MP-13 DUP MP-14 Sampling Date 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 Acetone 25 V-06 33 V-06 21 V-06 44 V-06 23 V-06 35 V-06 13 V-06, J 16 V-06, J <11 32 V-06 <11 19 V-06, J 21 V-06 <11 30 V-06 18 V-06, J NE NE Benzene 0.73 0.74 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 12 160 Benzyl Chloride <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 1.9 25 Bromodichloromethane <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 2.5 33 Bromoform <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 85 1100 Bromomethane <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 35 440 1,3-Butadiene <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 3.1 41 2-Butanone (MEK) <6.3 <6.3 <6.3 8.7 J 9.6 J 7.0 J <6.3 <6.3 <6.3 9.8 J <6.3 7.0 J <6.3 <6.3 <6.3 <6.3 35000 440000 Carbon Disulfide <0.58 <0.58 0.62 J 1.4 J 1.0 J <0.58 1.1 J 0.80 J 1.8 J 1.2 J 0.77 J 0.71 J 0.73 J 1.1 J 1.1 J 0.88 J 4900 61000 Carbon Tetrachloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 16 200 Chlorobenzene <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 350 4400 Chloroethane <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 28000 350000 Chloroform <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 4.1 53 Chloromethane 1.5 1.3 0.45 J 0.33 J 0.37 J 0.40 J <0.33 <0.33 <0.33 1.0 <0.33 0.51 J 1.4 0.76 J 0.80 J 0.45 J 630 7900 Cyclohexane <0.42 <0.42 <0.42 <0.42 <0.42 2.0 <0.42 <0.42 <0.42 <0.42 <0.42 <0.42 <0.42 <0.42 <0.42 <0.42 42000 530000 Dibromochloromethane <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 NE NE 1,2-Dibromoethane (EDB)* <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 0.16 2.0 1,2-Dichlorobenzene <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 1400 18000 1,3-Dichlorobenzene <0.67 <0.67 <0.67 <0.67 <0.67 1.3 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 NE NE 1,4-Dichlorobenzene <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 8.5 110 Dichlorodifluoromethane (Freon 12 1.8 1.6 1.9 1.6 1.9 2.0 1.9 1.8 1.9 1.7 2.0 2.1 2.0 1.7 2.0 1.9 700 8800 1,1-Dichloroethane <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 0.71 J <0.71 <0,71 <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 58 770 1,2-Dichloroethane <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 3.6 47 1,1-Dichloroethylene <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 1400 18000 cis-1,2-Dichloroethylene <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 280 3500 trans-1,2-Dichloroethylene <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 280 3500 1,2-Dichloropropane <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 1.2 1.3 <0.50 25 330 cis-1,3-Dichloropropene <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 NE NE trans-1,3-Dichloropropene <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 NE NE 1,2-Dichloro-1,1,2,2- tetrafluoroethane Freon 114 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 NE NE 1,4-Dioxane <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 19 250 Ethanol 25 37 30 37 31 69 13 J 32 17 31 23 42 55 82 34 55 NE NE Ethyl Acetate <3.F <3.6 <3.6 <3.6 <3.6 3.8 J <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 490 6100 Ethylbenzene 0.96 1.1 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 37 490 4-Ethyltoluene <0 F <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 NE NE Heptane 0.79 J 0.89 0.52 J 0.54 J <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 2800 35000 Hexachlorobutadiene <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 4.3 56 Hexane <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 4900 61000 2-Hexanone (MBK) <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 <0.41 0.46 V-06, J <0.41 <0.41 <0.41 <0.41 0.46 V-06, <0.41 210 2600 Isopropanol <3.4 4.5 J <3.4 13 J 3.9 J <3.4 <3.4 <3.4 <3.4 <3.4 4.2 J 101 11 J <3.4 <3.4 <3.4 1400 18000 Methyl tert-Butyl Ether (MTBE) <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 360 4700 Methylene Chloride <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 3400 53000 4-Methyl-2-pentanone (MIBK) <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 21000 260000 Naphthalene -0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 1.1 2.8 36 Propene <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 21000 260000 Styrene -0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 7000 88000 1,1,2,2-Tetrachloroethane 0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 1.6 21 Tetrachloroethylene <1.0 <1.0 3.7 <1.0 <1.0 1.7 2.1 1.5 5.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 280 3500 Tetrahydrofuran 5.1 J 7.5 9.2 15 9.0 10 4.9 J 5.3 J 5.4 J 7.8 3.1 J 6.0 4.2 J 4.3 J 2.4 J 2.2 J 14000 180000 Toluene 12 15 7.9 11 7.8 7.1 3.5 3.9 7.0 8.0 3.2 8.3 3.6 4.1 3.0 4.5 35000 440000 1,2,4-Trichlorobenzene <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1 <1.4 <1.4 <1.4 <1.4 <1.4 14 180 1, 1, 1 -Trichloroethane -0.86 <0.86 <0.86 <0.86 <0.86 <0.86 1.4 <0.86 <0.86 <0.86 <0.86 <0.86 <0.86 <0.86 <0.86 <0.86 35000 440000 1,1,2-Trichloroethane 0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 1.4 18 Trichloroethylene -0.72 <0.72 1.4 <0.72 <0.72 1.5 1.1 1.1 0.95 J <0.72 <0.72 <0.72 <0.72 <0.72 <0.72 <0.72 14 180 Trichlorofluoromethane (Freon 11 1.5 J 1.5 J 12 6.6 1.4 J 9.1 130 23 45 23 2.2 J 2.0 J 3.3 J 87 66 11 NE NE 1,1,2-Trichloro-1,2,2- trifluoroethane Freon 113 <, <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 <1.7 35000 440000 1,2,4-Trimethylbenzene 0.88 J 1.0 0.85 J 1.2 1.6 1.5 0.55 J 1.1 2.2 1.4 0.57 J 0.71 J 0.69 J 0.75 J 0.73 J 0.67 J 420 5300 1,3,5-Trimethylbenzene <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 420 5300 Vinyl Acetate <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 1400 18000 Vinyl Chloride <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 I <0.46 <0.46 <0.46 <0.46 <0.46 5.6 280 m&p-Xylene 2.8 3.5 2.2 1.8 <0.97 1.1 J <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 <0.97 700 8800 o-Xylene 0.85 J 0.96 0.63 J 0.56 J <0.44 0.50 J <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 I <0.44 <0.44 <0.44 700 8800 Notes: Concentration units: pg/m3 * = Compound was not detected, but had a lab method detection limit over the Residential Sub -Slab Screening Level. For the purpose of risk evaluation, concentrations of this compound equal to its MDL were assumed. J = Estimated Concentration NE = Not Established V-06 = Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. Bolded concentrations exceed the Residential Sub -Slab Soil Gas Level Shaded concentrations exceed the Non -Residential Sub -Slab Soil Gas Screening Level <0.34 = Not detected above the lab method detection limit TABLE 4 CHEMICAL CONSTITUENTS ANALYZED IN SOIL GAS FORMER RALEIGH MGP NO. 2 PHASEIREDEVELOPMENT RALEIGH, NORTH CAROLINA MID -ATLANTIC JOB NO. R3746.00 EU 4 EU 5 EU 6 EU 7 EU 8 NCDEQ DWM Residential Soil Gas Screening Levels January 2023 (pg/m3) NCDEQ DWM Non -Residential Soil Gas Screening Levels January 2023 (pg/m3) Sample ID MP-15 MP-16 MP-17 MP-18 MP-19 MP-20 MP-21 MP-22 MP-23 MP-24 MP-25 Sampling Date 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 6/7/2023 Acetone <11 110 V-06 48 V-06 44 V-06 37 V-06 17 J 23 30 19 <11 <11 NE NE Benzene <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 <0.48 12 160 Benzyl Chloride <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 <0.91 1 <0.91 <0.91 <0.91 1.9 25 Bromodichloromethane <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 <0.94 2.5 33 Bromoform <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 85 1100 Bromomethane <0.52 <0.52 <0.52 0.90 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 35 440 1,3-Butadiene <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 <0.37 3.1 41 2-Butanone (MEK) <6.3 33 7.2 J 7.1 J 7.8 J <6.3 <6.3 <6.3 <6.3 <6.3 <6.3 35000 440000 Carbon Disulfide 1.0 J 0.76 J 1.4 J 4.4 J 4.1 J 0.77 J <0.58 0.62 J 4.4 J 1.2 J 1.0 J 4900 61000 Carbon Tetrachloride <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 16 200 Chlorobenzene <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 <0.61 350 4400 Chloroethane <0.47 0.47 J <0.47 1.8 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 28000 350000 Chloroform <0.93 <0.93 <0.93 1.8 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 4.1 53 Chloromethane <0.33 0.79 J 0.80 J 7.2 0.69 J 0.52 J <0.33 <0.33 0.50 J <0.33 <0.33 630 7900 Cyclohexane <0.42 <0.42 <0.42 1.2 <0.42 <0.42 <0.42 0.51 J <0.42 <0.42 <0.42 42000 530000 Dibromochloromethane <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 <1.1 NE NE 1,2-Dibromoethane (EDB)* <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 <0.93 0.16 2.0 1,2-Dichlorobenzene <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 <0.69 1400 18000 1,3-Dichlorobenzene <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 <0.67 NE NE 1,4-Dichlorobenzene <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 8.5 110 Dichlorodifluoromethane (Freon 12 1.9 1.7 1.8 2.1 1.8 1.6 1.4 1.9 1.9 1.7 2.2 700 8800 1,1-Dichloroethane <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 <0.71 58 770 1,2-Dichloroethane <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 <0.73 3.6 47 1,1-Dichloroethylene <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 1400 18000 cis-1,2-Dichloroethylene <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 <0.58 280 3500 trans-1,2-Dichloroethylene <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 <0.62 280 3500 1,2-Dichloropropane <0.50 0.96 0.83 J <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 0.55 J 25 330 cis-1,3-Dichloropropene <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 <0.47 NE NE trans-1,3-Dichloropropene <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 NE NE 1,2-Dichloro-1,1,2,2- tetrafluoroethane Freon 114 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 NE NE 1,4-Dioxane <0.60 <0.60 <0.60 0.81 J <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 19 250 Ethanol 33 100 50 69 120 86 38 200 36 31 41 NE NE Ethyl Acetate <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 <3.6 490 6100 Ethylbenzene <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 <0.51 0.64 J <0.51 <0.51 <0.51 37 490 4-Ethyltoluene <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 <0.60 NE NE Heptane <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 0.80 J <0.52 <0.52 <0.52 2800 35000 Hexachlorobutadiene <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 <1.8 4.3 56 Hexane <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 <3.7 4900 61000 2-Hexanone (MBK) <0.41 2.5 V-06 0.49 V-06, J 1.2 V-06 0.61 V-06, J <0.41 <0.41 <0.41 0.92 V-06 <0.41 <0.41 210 2600 Isopropanol 21 <3.4 <3.4 <3.4 14 J 14 J 33 35 23 3.7 J 191 1400 18000 Methyl tert-Butyl Ether (MTBE) <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 <0.56 360 4700 Methylene Chloride <3.2 <3.2 <3.2 5.0 J <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 <3.2 3400 53000 4-Methyl-2-pentanone (MIBK) <0.44 0.75 V-06, J <0.44 1.0 V-06 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 <0.44 21000 260000 Naphthalene <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 <0.79 2.8 36 Propene <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 <3.0 21000 260000 Styrene <0.45 <0.45 <0.45 <0.45 1.2 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 7000 88000 1,1,2,2-Tetrachloroethane <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 <0.74 1.6 21 Tetrachloroethylene <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 280 3500 Tetrahydrofuran 4.6 J 29 18 25 29 3.1 J <0.97 2.5 J <0.97 <0.97 <0.97 14000 180000 Toluene 1.3 7.3 4.5 5.6 6.0 4.0 2.9 5.3 0.93 0.54 J 0.57 J 35000 440000 1,2,4-Trichlorobenzene <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 <1.4 14 180 1,1,1-Trichloroethane <0.86 <0.86 1.2 <0.86 <0.86 <0.86 <0.86 <0.86 <0.86 <0.86 <0.86 ism 35000 440000 1,1,2-Trichloroethane <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 <0.77 1.4 18 Trichloroethylene <0.72 <0.72 <0.72 <0.72 <0.72 <0.72 <0.72 <0.72 <0.72 1.6 0.84 J 14 180 Trichlorofluoromethane (Freon 11 14 55 80 10 3.6 J 3.5 J 12 2.7 J 17 2.3 J 9.7 NE NE 1,1,2-Trichloro-1,2,2- trifluoroethane Freon 113 <1.7 <1.7 2.1 J 11 <1.7 <1.7 <1.7 <1.7 2.2 J <1.7 <1.7 35000 440000 1,2,4-Trimethylbenzene 1.2 1.9 1.1 1.2 1.6 1.5 0.71 J 5.3 1.4 1.2 1.4 420 5300 1,3,5-Trimethylbenzene <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 <0.52 420 5300 Vinyl Acetate <3.8 <3.8 4.2 J <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 <3.8 1400 18000 Vinyl Chloride <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 <0.46 5.6 280 m&p-Xylene <0.97 1.5 J <0.97 1.1 J 1.3 J <0.97 <0.97 2.2 V-06 <0.97 <0.97 <0.97 700 8800 o-Xylene <0.44 0.71 J <0.44 <0.44 0.59 J <0.44 <0.44 0.97 V-06 <0.44 <0.44 <0.44 700 8800 Notes: Concentration units: pg/m3 *= Compound was not detected, but had a lab method detection limit over the Residential Sub -Slab Screening Level. For the purpose of risk evaluation, concentrations of this compound equal to its MDL were assumed. J = Estimated Concentration NE = Not Established V-06 = Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. Bolded concentrations exceed the Residential Sub -Slab Soil Gas Level Shaded concentrations exceed the Non -Residential Sub -Slab Soil Gas Screening Level <0.34 = Not detected above the lab method detection limit TABLE 5 PRE -OCCUPANCY INDOOR AIR/SOIL GAS TESTING RISK ASSESSMENT SUMMARY FORMER RALEIGH MGP NO. 2 PHASEIREDEVELOPMENT RALEIGH, NORTH CAROLINA MID -ATLANTIC JOB NO. R3746.00 Assessment Parameters Exposure Unit: EU-1 EU-2 EU-3 EU-4 EU-5 EU-6 EU-7 EU-8 Commercial, Commercial, Commercial, Move -in area, Amenities, leasing Trash room, Building support, Use Description: Lobby, stair, elevators residential above residential above residential above residential above residential above residential above residential above MP-1, 2, 3, 4 MP-10, 11, 12, 13, 14 Sub -slab samples: MP-5, 6, 7, 8, 9 MP-15 MP-16, 17, 18, 19, 20 MP-21, 22 MP-23 MP-24, 25 MP-1 DUP MP-13 DUP IA-5, 6, 7, 8, 9 IA-16, 17, 18, 19 IA-24, 25 Indoor Air Samples: IA-1, 2, 3, 4 IA-10, 11, 12, 13, 14 IA-15 IA-21, 22 IA-23 IA-7 DUP IA-20 cannister failed IA-25 DUP Risk Criterion: Cancer HI Cancer HI Cancer HI Cancer HI Cancer HI Cancer HI Cancer HI Cancer HI Use Scenarios Residential 1.4E-05 6.1E-01 1.8E-05 5.2E-01 1.6E-05 5.1E-01 1.1E-05 3.7E-01 1.4E-05 4.9E-01 3.0E-06 1.9E-01 8.3E-06 5.7E-01 2.9E-06 1.6E-01 Non-residential 3.1E-06 1.4E-01 4.1E-06 1.2E-01 3.6E-06 1.2E-01 2.6E-06 8.8E-02 3.2E-06 1.2E-01 6.9E-07 4.6E-02 1.9E-06 1.4E-01 6.5E-07 3.8E-02 To evaluate risk in each EU: 1. The highest concentration of each compound detected in indoor air above MDLs was entered into the Risk Calculator. 2. If a compound was detected at a greater concentration in the indoor air than in the corresponding paired soil gas sample(s), thus indicating an indoor air source, then the concentration detected in the soil gas was used in the risk calculation in lieu of the concentration detected in the indoor air. 3. For compounds not detected in indoor air but with MDLs above Residential Indoor Air Screening Levels, if the compound was not detected in the corresponding paired soil gas sample(s), then the compound was assumed not to be present in indoor air and was excluded from the risk calculation. If the compound was detected in the corresponding paired soil gas sample(s), then a concentration equal to the MDL from laboratory analysis of the indoor air sample was entered into the risk calculation. APPENDIX A VIMS INSPECTION LOGS U Mid Atlantic Mid Atlantic VIMS Inspection mom Field Tech : Colton Gotshall Date: 3/4/2022 Client: Aptus Project: Cabanas Street Zane : Depressurization Utility Bank? No DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes NIA Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier NA Monitoring points NA Smoke test NIA Vertical risers Yes Seals in concrete slab penetrationsroints NIA Fan installation and operation NIIA NIA Stairwell Elevator pit NIA - - ;,r•, � r�r �y� LL 'f a:A Notes: Gravel layer is not 57 stone but rather a pea gravel size. All gravel needs to be removed and replaced with washed 57 stone. Two vapor pits on -site. Helps were dug wl small shovels throughout Building B and less than E inchesotgrave! was discovered In multiple holes. r � Signature C�w Page 1 of 1 . Atlantic VIMS Inspection 1h Project Field Tech : Nolen Barefoot Info Date : 3/7/2022 Client: Aptus Project : Cabarrus Street Zone : Barrier Only Utility Bank? No DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer Yes Membrane barrier N/A Monitoring points N/A Smoke test N/A Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Photos/Notes Cam', � �• it r _ r. � ,.� r- i 74 ' A- L Pit 5 w/ plywood >6" gravel layer Notes : Piping from Pit 6 removed and has not been replaced at time of site visit. Signature _ r� Page 1 of 1 . Atlantic VIMS Inspection Field Tech : Colton Gotshall Date : 3/16/2022 Client: Aptus Project : Cabarrus Street Zone : Depressurization Utility Bank? No i DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers Yes Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Photos/Notes s Page 1 of2 Notes: Small area in southem portion of Building B has been filled with 57 stone to 6 inch depth. Vapor barrier laid down and passed smoke test. Monitoring points MP-10, MP- 11, MP-12, and MP-13 installed and checked with laser to be flush with concrete slab. Signature Page 2 of2 Atlantic VIMS Inspection Project Field Tech : Colton Gotshall Info Date : 4/13/2022 Client: Aptus Project : Cabarrus Street Zone : Depressurization Utility Bank? No DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier N/A Monitoring points N/A Smoke test N/A Vertical risers Yes Seals in concrete slab penetrations/joints N/A Fan installation and operation WA Stairwell N/A Elevator pit N/A Photos/Notes ...: -�- - _ _ _ .. f •� yam.. � r � � .� � 17 ow .. r IL Page 1 of2 Notes: Inspection of Building A-1. Washed stone is confirmed to be 57 stone to a depth of at least six inches in multiple locations. The correct location has been confirmed of the solid horizontal pipes running from two vapor pits to their respective vertical risers. No monitoring pins have been installed at this point. Vapor barrier has been installed along the wall between the two elevation changes in Building A-1. Signature Page 2 of2 . Atlantic VIMS Inspection Field Tech : Colton Gotshall Date: 4/19/2022 Client: Aptus Project : Cabarrus Street Zone : Depressurization Utility Bank? No i DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers Yes Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Photos/Notes - a M ,. x Page 1 of2 it iAlme ,.. ,q r � AM Al 41 p � d Mk wr T Sign -Off Atlantic VIMS Inspection Form Field Tech: Nolen Barefoot Client: Aptus Zone : Barrier Only Date : 4/25/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell Yes Elevator pit N/A Pagel of4 k n r.u■ ,.1 00, e� (J A Ito N. luil N Notes : Stairwell, commercial trash room, main electrical room and the electrical vault in building A-1 have had a vapor barrier laid down. Smoke test was passed. MP-8 and MP-9 installed. Signature Page 4 of4 Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Depressurization Date : 4/28/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier N/A Monitoring points N/A Smoke test N/A Vertical risers Yes Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell Yes Elevator pit N/A Pagel of2 Notes: Washed gravel layer of 57 stone was placed in Building A-2 and its stairway at depths of at least 6 inches. Mid -Atlantic checked gravel depth various times throughout the entire building area. Solid pipe runs, vertical risers, and vapor pits appear to be in their correct locations. Smoke test set for Monday May 2. Signature C&� Page 2 of2 10 Mid Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client : Aptus Zone : Depressurization Date : 5I2l2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes NIA Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers Yes Seals in concrete slab penetrationsljoints NIA Fan installation and operation NIA Stairwell Yes Elevator pit NIA Page 1 of2 Notes - Smoke test completed on Building A-2 and its associated stairwell. Monitoring points MP-1 thrcugh MPA wea€T" re installed in their mapped locations. Signature (&A Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Barrier Only Date : 05/18/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points N/A Smoke test N/A Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit Yes Pagel of2 Notes : Two elevator pits in Building B have been visually inspected. Vapor barrier and associated tape appears to be correctly installed. Signature Page 2 of Flit! Atlantic Field Tech: Colton Gotshall Client: Aptus Zone : Depressurization Project Checklist VIMS Inspection Form Date : 05/25/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier N/A Monitoring points N/A Smoke test N/A Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit Yes Pagel of 3 dbw � J Page 2 of 3 Notes: Washed gravel layer was verified for 57 stone of a depth of at least 6 inches on the eastern portion of Building B-2. Pit 8 was not fully installed during the site visit; however, Mr. Dennis Strickland stated it would be completed by the end of the day. Signature Page 3 of 3 Flit! Atlantic VIMS Inspection Form Field Tech: Nolen Barefoot Client: Aptus Zone : Depressurization Date : 05/26/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of 3 Photos/Notes I- � F-iei W"w 41 ,O;. it. . m Notes : Meeting/office area, mail room, phone room, and tv lounge have had barrier laid down. MP 18-20 installed. All areas smoke tested and passed. Signature Page 3 of 3 Flit! Atlantic VIMS Inspection Form Field Tech: Gary Fischer Client: Aptus Zone : Barrier Only Date : 06/03/2022 Project : Cabarrus Street Utility Bank? Yes DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer Yes Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of4 Photos/Notes ,i Notes: I got the site and got up with Dennis (Clancy) and Rob Hill. They had put the vapor barrier over the 57 stone in the lobby area. There were 2 stub ups in the lobby. One was a 4a€ white pipe the other was a 3a€ white pipe. Probably for sewer and water. There was one monitoring point to be installed in the lobby (MP-21) Rob performed the smoke test under the barrier. He used one location but blew the smoke in two different directions. No leaks were identified during the test. I filled out the VIMS checklist on XForms. I arrived at the site at 1150 and departed the site at 1320. We had to wait awhile for Donnelly to finish there lunch. Signature Page 4 of Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Depressurization Date : 06/13/2022 Project : Cabarrus Street Utility Bank? Yes DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier N/A Monitoring points N/A Smoke test N/A Vertical risers Yes Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of2 XV J t' 1 '�+ •, f� � � r t r l• t. Notes : The middle section, (including mens and womens restrooms and tv lounge) of Building B-2 was inspected for a washed gravel layer and vapor pit 7. Various sections were dug by shovel to check for 6 inch washed gravel thickness. All areas passed. Signature Page 2 of Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Depressurization Date : 06/15/2022 Project : Cabarrus Street Utility Bank? Yes DESCRIPTION STATUS Vapor pits Yes Perforated horizontal pipes N/A Solid horizontal pipes Yes Washed gravel layer Yes Membrane barrier Yes Monitoring points N/A Smoke test Yes Vertical risers Yes Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of2 Photos/Notes Sign -Off <-- End of Form --> ft Mid Atlantic VINIS Inspection Form =ietd Teel : Colt-n Go shail Zone : ❑epiessurizaton Dam., u6r2-&,2t:2-- Pro, :ct : Cabarrus Street Utility Bank? No DESCRIPT:UN STATUS Vapar pits •es Perforated horizontal pipes NIA Solid horizontal pipes Yes Washed gravel layer Yes Membrane barber NIA Monitoring paints NIA Smoke test NIA Vertical risers NIA Seals in concrete slab penetraibonsljoints NIA Fan installation and operation NIA Stairwell NIA Elevator pit Yes Paw- 1 afy Photos/Notes I I Mom I ■ �4- Skjn-. A. <- End of Form -> L 0 O-i 0 m ti Atlantic Field Notes Field Tech: Colton Gotshall Project Name: JC Penney North Hills Redevelopment Date: 06/28/2022 Notes : Depressurization Influence Testing (-Pascals): Pagel of2 Pit 2: MP-1 = 24.9 MP-2 = 669.7 Pit 1: MP-3 = 150.8 MP-4 = Barrier Only Pit 4: MP-5 = 40.2 MP-6 = 44.6 Pit 3: MP-7 = 67.1 MP-8 = Currently Destroyed MP-9 = Barrier Only Pit 5: MP-10 = 9.9 MP-11 = 9.4 Pit 6: MP-12 = 19.2 MP-13 = 27.5 MP-14 = 7.0 MP-15 = 7.6 Pit 7: MP-16 = 8.2 MP-17 = 12.3 MP-18 = 2.2 (they have open concrete around this point to fix plumbing) Pit 8: MP-19 = hazard zone during testing MP-20 = hazard zone during testing Page 2 of2 Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Barrier Only Date : 06/28/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier N/A Monitoring points N/A Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of2 Notes : Northwest corner portion of Building B passed smoke test. Signature 1�4 Page 2 of2 met Atlantic Field Notes Field Tech: Colton Gotshall Client: Aptus Date: 08/10/2022 Project Name: Cabarrus Street Notes : Depressurization Influence Testing (-Pascals): Page 1 of 2 Pit 8: MP-19 = -23.5 MP-20 = -56.2 Page 2 of 2 Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Barrier Only Date : 08/10/2022 Project : Cabarrus Street Utility Bank? Yes DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of2 Notes: Vapor barrier installed on the northwestern portion of the site (Maintenance office, electrical, and MPF). Monitoring point MP-24 installed. Smoke test was passed after secondary taping was done. Signature X"- Page 2 of2 Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Barrier Only Date : 08/23/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points N/A Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell Yes Elevator pit N/A Pagel of2 , Photos/Notes �4- <-- End of Form --> Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Barrier Only Date : 08/23/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of2 Notes: Vapor barrier was installed in the trash room on the southwest corner of the parking garage area. Successfully passed a smoke test and MP- 23 was installed. Signature height= Page 2 of2 Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Barrier Only Date : 08/29/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points Yes Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell Yes Elevator pit Yes Page 1 of 2 Notes: Vapor barrier was installed on the southeast corner of the parking garage, Building C, in the remainder of the Lobby, storage room, elevator pit, and Stair 3. The elevator pit was visually inspected and appears to be sealed correctly. Smoke test was passed successfully on the remaining areas inspected today. MP-22 was installed inside Stair 3. Darin, Superintendent for Donleys, told Mid -Atlantic this am that a concrete Tooter was poured underneath and there is a couple feet of gravel between the footer and the vapor barrier. Signature Page 2 of 2 Flit! Atlantic VIMS Inspection Form Field Tech: Colton Gotshall Client: Aptus Zone : Barrier Only Date : 09/28/2022 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits N/A Perforated horizontal pipes N/A Solid horizontal pipes N/A Washed gravel layer N/A Membrane barrier Yes Monitoring points N/A Smoke test Yes Vertical risers N/A Seals in concrete slab penetrations/joints N/A Fan installation and operation N/A Stairwell N/A Elevator pit N/A Pagel of2 Notes: Pump room and domestic pump room had a vapor barrier installed upon arrival and was successfully smoke tested. Signature A�4 Page 2 of2 ft Mid Atlantic VIMS Inspection Form Field Tech : Colton Gotshall Client: Aptus Zone : Depressurization Date., 0511812023 Project : Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits NIA Perforated horizontal pipes NIA Solid horizontal pipes NIA Washed gravel layer NIA Membrane barrier NIA Monitoring paints Yes Smoke test NIA Vertical risers NIA Seals in concrete slab penetrationsljoints NIA Fan installation and operation NIA Stairwell NIA Elevator pit NIA Pax 1 nf3 Photos/Notes i� i - r � l -� Notes: Vapor pins associated with monitoring points MP-8 and MP-21 through MP-25 installed. Unable to locate MP-6 and MP-1 S due to obstacles on the floor from ongoing constriction. All other monitoring points were accounted for and checked to be in good condition. Signature Paw 3 of3 ft Mid Atlantic VIMS Inspection Form Field Tech : Colton Gotshall Client: Aptus Zone : Depressurization Date : 05131I2023 Project . Cabarrus Street Utility Bank? No DESCRIPTION STATUS Vapor pits NIA Perforated horizontal pipes NIA Solid horizontal pipes NIA Washed gravel layer NIA Membrane barrier NIA Monitoring paints Yes Smoke test NIA Vertical risers NIA Seals in concrete slab penetrationsljoints NIA Fan installation and operation Yes Stairwell N/A Elevator pit NIA Pax f of? Notes - Influence Testi ng MP-1 = 448.1 MP-2 = -664.3 MP-3 = -685.5 MP-4 = -1.0 MP-5 = -800.6 MP-6 = -803.7 MP-7 = -786.2 MP-8 = 0.0 MP-0 = -23.1 MP-10 = -31.5 MP- 11 =-22.3 MP-12 =-88.7 MP-13 = -129.5 MP-14 =-78.6 MP-15 = -96.6 MP-16 = -203.7 MP-17 = -233.6 MP-18=-217.3 MP-19=-151.2 MP-20 =-211.5 All measurements are in Pascals. VIMS fans were operational upon arrival. Signature Page 2 of2 APPENDIX B INDOOR AIR BUILDING SURVEY AND SAMPLING FORM U Mid Atlantic INDOOR AIR BUILDING SURVEY and SAMPLING FORM Site Name: FVI'MC✓ G IIt MGP NO. 2- ID#: Preparer's name: N ©t.Lh Date: 5-(3'0 /Z 3 Preparer's affiliation: PA Phone #: (zoZ) L8'Sl' ZCQ 4 Part I - Occupants Building Address: 600 C A ba �r! v S S4 PC 2 7&® 3 Property Contact: Dton%iS Owner / Renter / of iv�ci���•„d -- Ckn`y ♦ TLty s Contact's Phone: home ( ) work ( ) cel (IM) 4Z? -03& 3 # of Building occupants: Children under age 13 Children age 13-18 Adults Part II — Building Characteristics ` r- Building type: residential / multi -family residents / office / strip mall / commercial industrial Describe building: S145, `��Z �. �t 2 i• �i Cewc/.e4, Year constructed: Z-02 Z -�7 Sensitive populationAday care / nursing home / hospital / school / other (specify): Number of floors below grade: Al� V (full basement / crawl space / slab on grade) Number of floors at or above grade: _7 Depth of basement below grade / surface: W ft. Basement size: ftz Basement floor constructions 4 rete / dirt / floating / stone / other (specify): Foundation walls: ioured conc e / cinder blocks / stone / other (specify) Basement sump present? Yes (no Sump pump? Yes / No Water in sump? Yes / No Type of heating system (circle all that apply): hot air circulation hot air radiation wood steam radiation eat u hot water radiation kerosene heater electric baseboard other (specify): Type of vents%cle all that apply): mechanical fans athroom ventilation i-- dey air conditioning um ss kitchen range hood fan outside air intake r (specify): Type of fuel util' d (circ 11 that apply): atural jA / 012ectricfuel oil / wood / coal / solar / kerosene Are the basement walls or floor sealed with waterproof paint or epoxy coatings? IJI A Yes / No Part V — Miscellaneous Items Do any occupants of the building smoke? /V/� Yes / No How often? Last time someone smoked in the building? hours / days ago L Does the building have an attached garage directly connected to living space? (Eepl/ No If so, is a car usually parked in the garage? Yes / No Are gas -powered equipment or cans of gasoline/fuels stored in the garage? G / No Do the occupants of the building have their clothes dry cleaned?A✓/A Yes / No If yes, how often? weekly / monthly / 3-4 times a year Do any of the occupants use solvents in work? /1//,. Yes / No If yes, what types of solvents are used? If yes, are their clothes washed at work? Yes / No Have any pesticides/herbicides been applied around the building or in the yard? Yes (20�) If so, when and which chemicals? Has there ever been a fire in the building? Yes /0 If yes, when? Has painting or staining been done in the building CCi..n the last 6 months? Ye / No If yes, when ✓e V 5--,0Ind where? o 4S�. {nP-Q,rotP-a) Part VI —Sampling Information Sample Technician: A/o (cA Phone number: (Zd Z) T rM - 2 (44 7 Sample Source: doDrAi' / Crawlspace Air / Sub-Sla / Near Slab Soil Gas / Exterior Soil Gas Sampler Type: Tedlar bag / Sorbent / winle=Steel-CanisterOther (specify): Analytical Method / TO-17 / other: Cert. Laboratory: ; A c -L Sample locations (floor, room): Field ID # - Field ID # - Field ID # - Field ID # - Were "Instructions for Occupants" followed? Yes No If not, describe modifications: Is there a whole house fan? Septic system? Irrigation/private well? Yes /� Yes / Yes (but not used) Yes / Yes (but not used) Type of ground cover outside of building: grass / concrete / asphalt / other (specify) Pl., dV'I, Existing subsurface depressurization (radon) system in place? Yes No active /passive Sub -slab vapor/moisture barrier in place? es / No Type of barrier: V, Y(ac Part III - Outside Contaminant Sources Other stationary sources nearby (gas stations, emission stacks, etc.): 4,40 5911 f4f jl kj -Jj . Heavy vehicular traffic nearby (or other mobile sources): j;�lf �7 �l,j , h/a - ex�w�w�o� , o'11•a_�T�^� •µ'sac Part IV — Indoor Contaminant Sources Identify all potential indoor sources found in the building (including attached garages) and crawlspace (if present), the location of the source (floor and room), and whether the item was removed from the building 48 hours prior to indoor air sampling event. Any ventilation implemented after removal of the items should be completed at least 24 hours prior to the commencement of the indoor air sampling event. Potential Sources Location(s) Removed (Yes / No / NA) Gasoline storage cans Gas -powered equipment ?,,. 40--4 o-il o,,f t.a- btu NO Kerosene storage cans Paints / thinners / strippers <abb Us-k-s6e, %4f%. tk Ajo Cleaning solvents Oven cleaners Carpet / upholstery cleaners Other house cleaning products Moth balls Polishes / waxes Insecticides Furniture / floor polish Nail polish / polish remover Hairspray Cologne / perfume Air fresheners Fuel tank (inside building) NA Wood stove or fireplace NA New furniture / upholstery New carpeting / flooring 7 l A ; 1% (14 NA Hobbies - glues, paints, etc. •.(..�, ,..x�d•�� Provide Drawing of Sample Location(s) in Building Part VII - Meteorological Conditions Was there significant precipitation within 12 hours prior to (or during) the sampling event? Yes No Describe the general weather conditions: Tv►n;cu wu.'i1.�� �owl•�-i•"f dvr,'�S �,w, p►• �� 6 -75° srN" J%11I �r o-vt.sl s%r®ro. 6�+•z. olsalva •an D" Z ✓l A.& +yfn.'.n of fiv Part VIII — General Observations Provide any information that may be pertinent to the sampling event and may assist in the data interpretation process (e.g., observed that drycleaner operated with door or windows propped open for ventilation). (Adapted from the NJDEP Vapor Intrusion Guidance, October 2005) tAsf 7 5 —2 P-2 T4„F K, IA 23W 1^rJove IA- 1 "5 A.ia Y MP-1 SUB —SLOB MONITORING PAINT MP-14 IA-16 I IA-1 INOO❑R AIR SAMPLE LOCATION ` ® OA-1 OUTDOOR AIR SAMPLE LOCATION MP-13 • IA-13 0 MP-2 r OIA` * IA-22 r r..[++■d,j �.. c•�....� nv --- —12 + ea�o •O + MP-1 W-3 8 V j +I MP-10 MP-21 I _ y^c IL AT I+ i.�v ,w..■.•Y MP-19 -r•.+.rrr•..w � MP-1 I IA-14 fC IA 111 OA— 1 MP-10 IA-20 L., r ar �sP-2❑ �.�..! 1.r .47;L11 J ■ ---- -- ---�-- C. --- ;!. &...f.r MP17 0 AiP-33 a• 1 t+t yMA4. � er.'et J's a 1. A ... uxc*wu. vw. ■ � ■ ■ ` I + r MP-9 • , + J rrti p�Y- M t iJrc�i E hSS MP-4 J-�■� IA -2 MP$ r�tSJ — W `1 1 i NI1� pn,nt � ^ I * MP-8 IA— — SIB $ —5 ■ MP-2 _ ip (ar.� ❑ 64' OS SCALE: 1 I64"=1 '— ❑" a a � � I a r- N CN n CD a CD � 1�7 I z �4k uj C1 0 v a Y Y U U LLI 41 z = Lu U L) � 0 m W z w 7 w z ry �} r z a- m wm ¢m V) Z Z �7_ Q p U 0 Z J LjCD0U rZ :2_ D_ D¢ Li7LLJ�� ��JQp Q Q7 Q 0Li! O— d V W a� Z Q N � � CD MP-25 CD IA-7t1 5 o �s s: :°E.a ► - Z z#= MP-24 L1J (fy IA-24 f �yggl l _ s U U I - u L) a z' z w o I Lo to-23 [] ❑ W w CLt ¢ Ct] j� IA-15 � IA-1 .e MP-18 � Z MP-1 SUB -SLAB MONITORING POINT MP 14 IA-111 � CV .o•e / Z Q 0 IA-1 INDOOR AIR SAMPLE LOCATION QQ ® OA-1 OUTDOOR AIR SAMPLE LOCATION �.,I , LLJ LJ b MP-13■ = I 0 L1C IX IA-13 MP= Z Lq (n Q MP-12 OOIA-12 MP-17 `~r• Z v) L7 tIr OfIA _j8 E _ ME ar < Z d ++ �.■on. MP-18 Ap211 Q MQ N Of L] � } A-19 e^ f! 0 W d w �rli� I fI MP-1 f I 0 � O -i � a < MP- 1 L I IA-10 a g V) A GA-1 MP-10 -20 ate. l 0 a Z LLJ + MP-207 4 Q ca • LJ o � AP77� .1..:f' �I MP-3 G ..... Z 0 • j.J -IA-9 J Y MP-4 i E Q L4-4 I n Z LU Ln • I of LJ V f 0 IMP — 5 ._ ■ MP-2 J ap-1 • ; �+ LLJT_ f O IA- c Z 71 LU (] Iil U — s — — — — — Z LLJ w O 64' W LL_ LLJ SCALE: 1 /64"=1 '-O" or_ APPENDIX C FIELD NOTES U Mid Atlantic Mid-AtlanticAssociates, Field Notes cfit -awe^41 -70" V61 b'-.-7-7 Job Name: r 4w .%lc4 (z: L M6.10 1110. 2 Date: & 13 - 6 r 7-1 Job Number: .`00 Technician: TW13 Task Number: goOOO Weather: Svw �-��J° br s-- I Location: v (, L C, jl.r Sf Arrival 1On ge0 ' Depature: 17,Z.ti'� 12J� Notes: S H ' (4 K Z 14 10Z - 1 IIA - t t Cam ( 11 - 30 F& 102 -R, f-L 3 ''0- IA -Z L4K 1426 10) Z' -T• IZ l` -2-1 L 353 q 14A -7. 29- F�G 35f0 105 -10 G T5 32 -9.ZS 27.s 1 ` L�,.� zz q 175 215 TA - 13 Z OO l q 5-0 - z1.5- � . s - 01 G 3`13 ( `�(g - �tit L 12_T� 1 7 - 9.5 z7.s Sa - -7 ( TVA 1 � g - 2qt-�TAq C-ft� Z q 10©a -30.5 732 11g -ro.FC 6 IOX -� 27 TA- O� 133 2g. S -`/4 - ( Cum f f d� -ZR=S F-C 3-7(2, 133 -10 L 174 NO -7.75 TA - I0 Cam (Wf IM - zi.5- TA- 2ALCk, 0710 1001 - � Ft 3-7qq 17 .2 Equipment / Expendables Used: Page ) of Z Signature T�iw maafieldnotes.xl Mid -Atlantic Associates, Field Notes Date: G 1 /q f t7 Job Name: A4W IJa. 2 Job Number: 3� s00 Technician: TI/r7 Task Number: 0000 Weather: SeL P, ( Location: Arrival: M Depature: fLZ5 f j z!57 Notes: 1a. -Z77 La,,� j`0,90 t015 -30 � -$ Lew 12-2-5- .25_ _ ,.► FL 3010 107-7- -8.57 rIOt X C13 ( 1053 - 25.s- 'C-L �L4U1 1073 - 7 z5 C4,v, 1 IV (o 34 - zq P 3265' I03g - (o •1 � L 34 Sg 103T -115 A'- Z (`4 CAh 10071 (o`tS - 2-1, 1OL(S -9.Z5 of� z e-% I rw f056- -21 14 R 37'&4 1 b5S -7 -14, . F�-2Z tyw tgcl i 1 roq -2B �saq 11`0� - 9 155jp 1104 - z9.S �rC I1 It 1109 -1.2,5 Equipment / Expendables Used: Page Z Of Signature maafieldnotes:xf Associates, Field Notes` Job Name: r l tiSI MG f A16. 2Z Date: & (? z 3 Job Number: A 3 Technician: Twi3 Task Number: 90000 Weather: s..,ot� •� Location: Rot,-: S l Ca b..,. df S - Arrival: 100 Depature: GD 0 Notes: M P= 2�- / CAw Z 927, 7 t% M f - ?,i / E, A t% Z-7975 Tk t ►--k 31io�-L r( 45g3 r= E Oo a I - s 91&�� Zvi % (A41 7-1 (0 Sl� ^✓1 12. Mr- ,h gNs L �. 7,a f�� �� .`l -,_ N.�,��i -za FL T700 Tc IOtGe 0 r-t'., -5 99b t (Q (0 TZIA✓ �l i� \n4 1 1007 Equipment / Expendables Used: C �} t -Q (6 r - 5 10 3� Page of ` Signature maafieldnotes:xl Mid-AtlantIc Associates, Field Notes Notes: Z '1 Sc.,o -d 12.9'ro M{ (9 YZ(aol ( • li 2490 5410/1 Le a✓i 1k.1h,&( (,AP- 1 1( Z2 Z (( Shrev I I -Z -4h I -Z 1 tip- ( /IOU,` zq S J� (l. l% .Iw:�lF � -2 FGT7 0 T4,1161✓ — 5 113 tkp- 13� (z©I C� ` �1q3 St.,.� Io.S°ib,..l�I =Z9 (�-L Li�� t .�1 t F� p��,._ 1�-a 1 z0 0 19 e 4S—00-7 w+Ju✓ too w� �w,,t -5- 12-1-7 M' -Iq a 1 I `( 6A,4 ZGSO SG,:.i� t C•�%` TH:�( `- 21.E Equipment / Expendables Used: T A r j 5010,�. C^C. (- S 1 Z Page Z of Signature maafieldnotesxl Associates, Field Notes Job Name: / ,,,'`RxCa L MG P Na. 2 Date: { -7 23 Job Number: 3 7 , 00 Technician: Task Number: COD Do Weather: Location: Arrival: Depature: Notes: P� (-I, ZC '1-309 Tti���l (o.� d/s 1K®� I -zg- 5' I Z3 1 r (gyp- t ( zS11 24g 3 Sj OJ j I 0. 2°�,� '..,,�,° � - 27 . S t ?01 f - g ' C&V% t 3 Z Loa �hn.J c�' ��� � 'K•�' ( =Z 1. S` 45,1 Z Te-Ji i ou,, - 5 13Wc L4 7b x Ttj(`v Oro Equipment / Expendables Used: ?"315 -2-7) tgoOj 415 SZ �Ld (h� D I V "" ��0. - S t 4 t Page 3 of Signature' maafieldnotes.xl Mid -Atlantic Associates, Field Notes Job Name: „V„rAfu'eik M&V' N. 2 1 Date: G17/-x3 Job Number: 93 7 4 Co. 00 Technician: Task Number: Weather: Location: Arrival: Depature: Notes: 1 5- 1 p"If6,1 014 F-;ka� jq7 0 } qq O t l" ZG2_0 5"A 11. L /b 9 402 IFj_jt" dp w. "5_ I `4`is' ly5 5- 2-1(i3 �ktf, (22��, �,�. ,,� -ZQ F - `f55Ij Ta (^,, Drn,w �w� - 5- (Soa - 15-0f Caw. 21� S �J�� fo.00iO -Z7.5" ('gyp- 15 01 Caw 2 53 f �ro � 1Ci.V/ �'' f = 2 -1 PL)e �L yGpS T41 r mv2t 1 -5 15Z n f - 1 2-520 S6&aj 10.50/,.1 Z?. S 1 5'2_8" 'r-C 4Go(o C- j -5 t Equipment Expendables Used: Page L( of Signature maafieldnotes.xi APPENDIX D LABORATORY ANALYTICAL REPORTS AND CHAIN -OF -CUSTODY RECORDS FOR INDOOR/AMBIENT AIR Mid Atlantic con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 June 19, 2023 Nolen Barefoot Mid -Atlantic Associates, Inc. - Raleigh, NC 409 Rogers View Court Raleigh, NC 27610 Project Location: Raleigh, NC Client Job Number: Project Number: R3746.00 Laboratory Work Order Number: 23F1309 Enclosed are results of analyses for samples as received by the laboratory on June 9, 2023. If you have any questions concerning this report, please feel free to contact me. Sincerely, Rebecca Faust Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 102 con-testo A Pace Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Mid -Atlantic Associates, Inc. - Raleigh, NC REPORT DATE: 6/19/2023 409 Rogers View Court Raleigh, NC 27610 PURCHASE ORDER NUMBER: ATTN: Nolen Barefoot PROJECT NUMBER: R3746.00 ANALYTICAL SUMMARY WORK ORDER NUMBER: 23F1309 The results of analyses performed on the following samples submitted to Con -Test, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: Raleigh, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-1 23F1309-01 Indoor air EPA TO-15 IA-2 23171309-02 Indoor air EPA TO-15 IA-3 23F1309-03 Indoor air EPA TO-15 IA-5 23171309-04 Indoor air EPA TO-15 IA-6 23171309-05 Indoor air EPA TO-15 IA-7 23F1309-06 Indoor air EPA TO-15 IA-7 DUP 23171309-07 Indoor air EPA TO-15 IA-9 23171309-08 Indoor air EPA TO-15 IA-10 23F1309-09 Indoor air EPA TO-15 IA-11 23171309-10 Indoor air EPA TO-15 IA-12 23171309-11 Indoor air EPA TO-15 IA-14 23F1309-12 Indoor air EPA TO-15 IA-13 23171309-13 Indoor air EPA TO-15 IA-16 23171309-14 Indoor air EPA TO-15 IA-17 23F1309-15 Indoor air EPA TO-15 IA-18 23171309-16 Indoor air EPA TO-15 IA-19 23171309-17 Indoor air EPA TO-15 UNUSED 23F1309-18 IA-23 23F1309-19 Indoor air EPA TO-15 IA-15 23F1309-20 Indoor air EPA TO-15 IA-24 23F1309-21 Indoor air EPA TO-15 Page 2 of 102 con-testo A Pace Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Mid -Atlantic Associates, Inc. - Raleigh, NC REPORT DATE: 6/19/2023 409 Rogers View Court Raleigh, NC 27610 PURCHASE ORDER NUMBER: ATTN: Nolen Barefoot PROJECT NUMBER: R3746.00 ANALYTICAL SUMMARY WORK ORDER NUMBER: 23F1309 The results of analyses performed on the following samples submitted to Con -Test, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: Raleigh, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB IA-25 231`1309-22 Indoor air EPA TO-15 IA-25 DUP 23171309-23 Indoor air EPA TO-15 IA-21 23F1309-24 Indoor air EPA TO-15 OA 23171309-25 Indoor air EPA TO-15 IA-22 23171309-26 Indoor air EPA TO-15 IA-4 23F1309-27 Indoor air EPA TO-15 IA-8 23171309-28 Indoor air EPA TO-15 UNUSED 23171309-29 UNUSED 23F1309-30 Page 3 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. Page 4 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 EPA TO-15 Qualifications: B-05 Data is not affected by elevated level in laboratory blank since sample(s) result is 'Not Detected". Analyte & Samples(s) Qualified: Benzyl chloride B343424-BLKI Reported result is estimated. Value reported over verified calibration range. Analyte & Samples(s) Qualified: Acetone, Ethanol 23F1309-04[IA-5], 23F1309-05[IA-6], 23F1309-06[IA-7], 23F1309-07[IA-7 DUP], 23F1309-08[IA-9], 23F1309-09RE1[IA-10], 23F1309-10RE1[IA- 11], 23F1309-11RE1[IA-12], 23F1309-12RE1[IA-14], 23F1309-13RE1[IA-13], 23F1309-28[IA-8], B343439-DUPI, B343523-DUPI, 23F1309-14[IA-16], 23F1309-15[IA-17], 23F 1309-16RE 1 [IA-18], 23F 1309-17RE 1 [IA-19] L-01 Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high side. Analyte & Samples(s) Qualified: Hexachlorobutadiene B343424-BS1, B343439-BSI, B343523-BSI, B343662-BSI L-03 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. Analyte & Samples(s) Qualified: Isopropanol, Methylene Chloride B343523-BLKI, B343523-BSI L-05 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the high side. Analyte & Samples(s) Qualified: 2-Butanone (MEK), Naphthalene 23F1309-12[IA-14], 23F1309-13[IA-13], 23F1309-14[IA-16], 23F1309-15[IA-17], 23F1309-19[IA-23], 23F1309-20[IA-15], 23F1309-21[IA-24], 23F1309-22[IA-25], 23F1309-23[IA-25 DUP], 23F1309-24[IA-21], 23F1309-25[OA], 23F1309-26[IA-22], 23F1309-27[IA-4], 23F1309-28[IA-8], B343439-BSI, 23F1309-16[IA-18], 23F1309-17[IA-19], B343439-DUPI R-01 Duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result. Analyte & Samples(s) Qualified: 2-Butanone (MEK) B343424-DUPI V-06 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. Analyte & Samples(s) Qualified: Naphthalene 23F1309-01[IA-1], 23F1309-02[IA-2], 23F1309-03[IA-3], 23F1309-04[IA-5], 23F1309-05[IA-6], 23F1309-06[IA-7], 23F1309-07[IA-7 DUP], 23F1309-08[IA-9], 23F1309-09[IA-10], 23F1309-10[IA-11], 23F1309-11[IA-12], 23F1309-12[IA-14], 23F1309-13[IA-13], 23F1309-14[IA-16], 23F1309-15[IA-17], 23F1309-16[IA-18], 23F1309-17[IA-19], 23F1309-19[IA-23], 23F1309-20[IA-15], 23F1309-27[IA-4], 23FI309-28[IA-8], B343424-BSI, B343424-DUPI, B343439-BSI, B343439-DUPI, B343523-BS1, B343662-BSI, S089166-CCVI, S089178-CCVI, S089198-CCVI, S089293-CCVI Page 5 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 V-20 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: 1,2,4-Trichlorobenzene, Hexachlorobutadiene B343424-BS1, B343439-BSI, S089166-CCVI, S089178-CCVI, B343523-BSI, B343662-BSI, S089198-CCVI, S089293-CCVI Z-01 Calibrations RSD for this compound is >30% but <40%. Analyte & Samples(s) Qualified: Naphthalene 23171309-01[IA-1], 23F1309-02[IA-2], 23F1309-03[IA-3], 23F1309-04[IA-5], 23F1309-05[IA-6], 231F1309-06[IA-7], 23171309-07[IA-7 DUP], 23F1309-08[IA-9], 23F1309-09[IA-10], 23F1309-10[IA-11], 23F1309-11[IA-12], 23F1309-12[IA-14], 23F1309-13[IA-13], 23F1309-14[IA-16], 23F1309-15[IA-17], 23F1309-16[IA-18], 23F1309-17[IA-19], 23F1309-19[IA-23], 23F1309-20[IA-15], 23F1309-21[IA-24], 23F1309-22[IA-25], 23F1309-23[IA-25 DUP], 23F1309-24[IA-21], 23F1309-25[OA], 23F1309-26[IA-22], 23F1309-27[IA-4], 23F1309-28[IA-8], B343424-BLKI, B343424-BSI, B343424-DUPI, B343439-BLKI, B343439-BSI, B343439-DUPI, B343523-BLKI, B343523-BSI, B343662-BLKI, B343662-BS1, S089166-CCVI, S089178-CCVI, S089198-CCVI, S089293-CCVI The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. d� Lisa A. Worthington Technical Representative Page 6 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-1 Sample ID: 23F1309-01 Sample Matrix: Indoor air Sampled: 6/4/2023 09:02 Sample Description/Location: Sub Description/Location: Canister ID: 2016 Canister Size: 6 liter Flow Controller ID: 3417 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -31 Final Vacuum(in Hg): -9.5 Receipt Vacuum(in Hg): -8.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 55 4.0 2.4 130 9.5 5.7 2 6/15/23 19:25 CMR Benzene 0.23 0.035 0.026 0.74 0.11 0.084 0.698 6/14/23 14:35 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/14/23 14:35 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/14/23 14:35 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/14/23 14:35 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/14/23 14:35 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/14/23 14:35 CMR 2-Butanone (MEK) 20 1.4 0.37 60 4.1 1.1 0.698 6/14/23 14:35 CMR Carbon Disulfide 0.48 0.35 0.032 1.5 1.1 0.10 0.698 6/14/23 14:35 CMR Carbon Tetrachloride 0.078 0.035 0.028 0.49 0.22 0.17 0.698 6/14/23 14:35 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/14/23 14:35 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.082 0.698 6/14/23 14:35 CMR Chloroform 0.035 0.035 0.033 0.17 0.17 0.16 0.698 6/14/23 14:35 CMR Chloromethane 0.57 0.070 0.028 1.2 0.14 0.057 0.698 6/14/23 14:35 CMR Cyclohexane 0.099 0.035 0.021 0.34 0.12 0.073 0.698 6/14/23 14:35 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/14/23 14:35 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/14/23 14:35 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/14/23 14:35 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/14/23 14:35 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/14/23 14:35 CMR Dichlorodifluoromethane (Freon 12) 0.55 0.035 0.034 2.7 0.17 0.17 0.698 6/14/23 14:35 CMR 1, 1 -Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/14/23 14:35 CMR 1,2-Dichloroethane 0.047 0.035 0.032 0.19 0.14 0.13 0.698 6/14/23 14:35 CMR 1, 1 -Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/14/23 14:35 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/14/23 14:35 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/14/23 14:35 CMR 1,2-Dichloropropane 0.021 0.035 0.019 J 0.097 0.16 0.087 0.698 6/14/23 14:35 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/14/23 14:35 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/14/23 14:35 CMR 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/14/23 14:35 CMR 1,4-Dioxane 0.19 0.35 0.029 J 0.69 1.3 0.10 0.698 6/14/23 14:35 CMR Ethanol 32 4.0 1.8 61 7.5 3.3 2 6/15/23 19:25 CMR Ethyl Acetate 0.25 0.35 0.18 J 0.91 1.3 0.64 0.698 6/14/23 14:35 CMR Ethylbenzene 0.56 0.035 0.020 2.4 0.15 0.088 0.698 6/14/23 14:35 CMR 4-Ethyltoluene 0.056 0.035 0.021 0.27 0.17 0.11 0.698 6/14/23 14:35 CMR Heptane 0.60 0.035 0.022 2.4 0.14 0.091 0.698 6/14/23 14:35 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/14/23 14:35 CMR Hexane 0.45 1.4 0.18 J 1.6 4.9 0.64 0.698 6/14/23 14:35 CMR 2-Hexanone (MBK) 0.21 0.14 0.017 0.85 0.57 0.071 0.698 6/14/23 14:35 CMR Isopropanol 3.6 1.4 0.24 8.9 3.4 0.59 0.698 6/14/23 14:35 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/14/23 14:35 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/14/23 14:35 CMR 4-Methyl-2-pentanone (MIBK) 0.19 0.035 0.019 0.76 0.14 0.076 0.698 6/14/23 14:35 CMR Naphthalene 0.068 0.035 0.026 V-06, Z-01 0.36 0.18 0.14 0.698 6/14/23 14:35 CMR Propene ND 1.4 0.31 ND 2.4 0.53 0.698 6/14/23 14:35 CMR Styrene 0.47 0.035 0.018 2.0 0.15 0.078 0.698 6/14/23 14:35 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/14/23 14:35 CMR Page 7 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -31 Field Sample #: IA-1 Canister ID: 2016 Final Vacuum(in Hg): -9.5 Sample ID: 23F1309-01 Canister Size: 6 liter Receipt Vacuum(in Hg): -8.2 Sample Matrix: Indoor air Flow Controller ID: 3417 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:02 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.031 0.035 0.027 J 0.21 0.24 0.18 0.698 6/14/23 14:35 CMR Tetrahydrofuran 33 1.0 0.16 97 2.9 0.48 2 6/15/23 19:25 CMR Toluene 5.3 0.035 0.020 20 0.13 0.075 0.698 6/14/23 14:35 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 14:35 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 14:35 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 14:35 CMR Trichloroethylene 0.054 0.035 0.024 0.29 0.19 0.13 0.698 6/14/23 14:35 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 14:35 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.066 0.14 0.039 J 0.50 1.1 0.30 0.698 6/14/23 14:35 CMR 1,2,4-Trimethylbenzene 0.33 0.035 0.015 1.6 0.17 0.076 0.698 6/14/23 14:35 CMR 1,3,5-Trimethylbenzene 0.082 0.035 0.018 0.40 0.17 0.091 0.698 6/14/23 14:35 CMR Vinyl Acetate 1.7 0.70 0.19 6.0 2.5 0.66 0.698 6/14/23 14:35 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 14:35 CMR m&p-Xylene 2.2 0.070 0.039 9.7 0.30 0.17 0.698 6/14/23 14:35 CMR o-Xylene 0.87 0.035 0.018 3.8 0.15 0.078 0.698 6/14/23 14:35 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 99.1 70-130 6/14/23 14:35 4-Bromofluorobenzene (1) 96.1 70-130 6/15/23 19:25 Page 8 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-2 Sample ID: 23F1309-02 Sample Matrix: Indoor air Sampled: 6/4/2023 09:03 Sample Description/Location: Sub Description/Location: Canister ID: 1626 Canister Size: 6 liter Flow Controller ID: 3508 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -7 Receipt Vacuum(in Hg): -7.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 55 4.0 2.4 130 9.5 5.7 2 6/15/23 19:51 CMR Benzene 0.24 0.035 0.026 0.76 0.11 0.084 0.698 6/14/23 15:06 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/14/23 15:06 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/14/23 15:06 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/14/23 15:06 CMR Bromomethane 0.027 0.035 0.023 J 0.10 0.14 0.090 0.698 6/14/23 15:06 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/14/23 15:06 CMR 2-Butanone (MEK) 19 1.4 0.37 55 4.1 1.1 0.698 6/14/23 15:06 CMR Carbon Disulfide 0.49 0.35 0.032 1.5 1.1 0.10 0.698 6/14/23 15:06 CMR Carbon Tetrachloride 0.089 0.035 0.028 0.56 0.22 0.17 0.698 6/14/23 15:06 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/14/23 15:06 CMR Chloroethane 0.052 0.035 0.031 0.14 0.092 0.082 0.698 6/14/23 15:06 CMR Chloroform 0.040 0.035 0.033 0.20 0.17 0.16 0.698 6/14/23 15:06 CMR Chloromethane 0.67 0.070 0.028 1.4 0.14 0.057 0.698 6/14/23 15:06 CMR Cyclohexane 0.13 0.035 0.021 0.44 0.12 0.073 0.698 6/14/23 15:06 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/14/23 15:06 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/14/23 15:06 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/14/23 15:06 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/14/23 15:06 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/14/23 15:06 CMR Dichlorodifluoromethane (Freon 12) 0.54 0.035 0.034 2.7 0.17 0.17 0.698 6/14/23 15:06 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/14/23 15:06 CMR 1,2-Dichloroethane 0.048 0.035 0.032 0.19 0.14 0.13 0.698 6/14/23 15:06 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/14/23 15:06 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/14/23 15:06 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/14/23 15:06 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/14/23 15:06 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/14/23 15:06 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/14/23 15:06 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/14/23 15:06 CMR 1,4-Dioxane 0.19 0.35 0.029 J 0.70 1.3 0.10 0.698 6/14/23 15:06 CMR Ethanol 32 4.0 1.8 59 7.5 3.3 2 6/15/23 19:51 CMR Ethyl Acetate 0.47 0.35 0.18 1.7 1.3 0.64 0.698 6/14/23 15:06 CMR Ethylbenzene 0.57 0.035 0.020 2.5 0.15 0.088 0.698 6/14/23 15:06 CMR 4-Ethyltoluene 0.057 0.035 0.021 0.28 0.17 0.11 0.698 6/14/23 15:06 CMR Heptane 0.62 0.035 0.022 2.5 0.14 0.091 0.698 6/14/23 15:06 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/14/23 15:06 CMR Hexane 0.57 1.4 0.18 J 2.0 4.9 0.64 0.698 6/14/23 15:06 CMR 2-Hexanone (MBK) 0.15 0.14 0.017 0.62 0.57 0.071 0.698 6/14/23 15:06 CMR Isopropanol 3.6 1.4 0.24 8.9 3.4 0.59 0.698 6/14/23 15:06 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/14/23 15:06 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/14/23 15:06 CMR 4-Methyl-2-pentanone (MIBK) 0.20 0.035 0.019 0.81 0.14 0.076 0.698 6/14/23 15:06 CMR Naphthalene 0.065 0.035 0.026 V-06, Z-01 0.34 0.18 0.14 0.698 6/14/23 15:06 CMR Propene 0.96 1.4 0.31 J 1.7 2.4 0.53 0.698 6/14/23 15:06 CMR Styrene 0.49 0.035 0.018 2.1 0.15 0.078 0.698 6/14/23 15:06 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/14/23 15:06 CMR Page 9 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: IA-2 Canister ID: 1626 Final Vacuum(in Hg): -7 Sample ID: 23F1309-02 Canister Size: 6 liter Receipt Vacuum(in Hg): -7.3 Sample Matrix: Indoor air Flow Controller ID: 3508 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:03 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.036 0.035 0.027 0.24 0.24 0.18 0.698 6/14/23 15:06 CMR Tetrahydrofuran 31 1.0 0.16 92 2.9 0.48 2 6/15/23 19:51 CMR Toluene 5.1 0.035 0.020 19 0.13 0.075 0.698 6/14/23 15:06 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 15:06 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 15:06 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 15:06 CMR Trichloroethylene 0.028 0.035 0.024 J 0.15 0.19 0.13 0.698 6/14/23 15:06 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 15:06 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.069 0.14 0.039 J 0.53 1.1 0.30 0.698 6/14/23 15:06 CMR 1,2,4-Trimethylbenzene 0.35 0.035 0.015 1.7 0.17 0.076 0.698 6/14/23 15:06 CMR 1,3,5-Trimethylbenzene 0.080 0.035 0.018 0.39 0.17 0.091 0.698 6/14/23 15:06 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 15:06 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 15:06 CMR m&p-Xylene 2.3 0.070 0.039 9.8 0.30 0.17 0.698 6/14/23 15:06 CMR o-Xylene 0.88 0.035 0.018 3.8 0.15 0.078 0.698 6/14/23 15:06 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 98.2 70-130 6/14/23 15:06 4-Bromofluorobenzene (1) 95.8 70-130 6/15/23 19:51 Page 10 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-3 Sample ID: 23F1309-03 Sample Matrix: Indoor air Sampled: 6/4/2023 09:05 Sample Description/Location: Sub Description/Location: Canister ID: 1832 Canister Size: 6 liter Flow Controller ID: 3510 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -10 Receipt Vacuum(in Hg): -8.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 52 4.0 2.4 120 9.5 5.7 2 6/15/23 20:17 CMR Benzene 0.22 0.035 0.026 0.69 0.11 0.084 0.698 6/14/23 15:37 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/14/23 15:37 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/14/23 15:37 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/14/23 15:37 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/14/23 15:37 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/14/23 15:37 CMR 2-Butanone (MEK) 19 1.4 0.37 55 4.1 1.1 0.698 6/14/23 15:37 CMR Carbon Disulfide 0.57 0.35 0.032 1.8 1.1 0.10 0.698 6/14/23 15:37 CMR Carbon Tetrachloride 0.080 0.035 0.028 0.50 0.22 0.17 0.698 6/14/23 15:37 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/14/23 15:37 CMR Chloroethane 0.040 0.035 0.031 0.11 0.092 0.082 0.698 6/14/23 15:37 CMR Chloroform 0.035 0.035 0.033 0.17 0.17 0.16 0.698 6/14/23 15:37 CMR Chloromethane 0.62 0.070 0.028 1.3 0.14 0.057 0.698 6/14/23 15:37 CMR Cyclohexane 0.11 0.035 0.021 0.37 0.12 0.073 0.698 6/14/23 15:37 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/14/23 15:37 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/14/23 15:37 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/14/23 15:37 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/14/23 15:37 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/14/23 15:37 CMR Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.6 0.17 0.17 0.698 6/14/23 15:37 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/14/23 15:37 CMR 1,2-Dichloroethane 0.045 0.035 0.032 0.18 0.14 0.13 0.698 6/14/23 15:37 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/14/23 15:37 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/14/23 15:37 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/14/23 15:37 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/14/23 15:37 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/14/23 15:37 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/14/23 15:37 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/14/23 15:37 CMR 1,4-Dioxane 0.24 0.35 0.029 J 0.86 1.3 0.10 0.698 6/14/23 15:37 CMR Ethanol 31 4.0 1.8 59 7.5 3.3 2 6/15/23 20:17 CMR Ethyl Acetate 0.28 0.35 0.18 J 1.00 1.3 0.64 0.698 6/14/23 15:37 CMR Ethylbenzene 0.57 0.035 0.020 2.5 0.15 0.088 0.698 6/14/23 15:37 CMR 4-Ethyltoluene 0.047 0.035 0.021 0.23 0.17 0.11 0.698 6/14/23 15:37 CMR Heptane 0.56 0.035 0.022 2.3 0.14 0.091 0.698 6/14/23 15:37 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/14/23 15:37 CMR Hexane 0.57 1.4 0.18 J 2.0 4.9 0.64 0.698 6/14/23 15:37 CMR 2-Hexanone (MBK) 0.12 0.14 0.017 J 0.48 0.57 0.071 0.698 6/14/23 15:37 CMR Isopropanol 3.5 1.4 0.24 8.7 3.4 0.59 0.698 6/14/23 15:37 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/14/23 15:37 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/14/23 15:37 CMR 4-Methyl-2-pentanone (MIBK) 0.17 0.035 0.019 0.68 0.14 0.076 0.698 6/14/23 15:37 CMR Naphthalene 0.045 0.035 0.026 V-06, Z-01 0.23 0.18 0.14 0.698 6/14/23 15:37 CMR Propene 0.92 1.4 0.31 J 1.6 2.4 0.53 0.698 6/14/23 15:37 CMR Styrene 0.49 0.035 0.018 2.1 0.15 0.078 0.698 6/14/23 15:37 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/14/23 15:37 CMR Page 11 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-3 Sample ID: 23F1309-03 Sample Matrix: Indoor air Sampled: 6/4/2023 09:05 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1832 Canister Size: 6 liter Flow Controller ID: 3510 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -10 Receipt Vacuum(in Hg): -8.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.033 0.035 0.027 J 0.22 0.24 0.18 0.698 6/14/23 15:37 CMR Tetrahydrofuran 30 1.0 0.16 90 2.9 0.48 2 6/15/23 20:17 CMR Toluene 5.1 0.035 0.020 19 0.13 0.075 0.698 6/14/23 15:37 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 15:37 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 15:37 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 15:37 CMR Trichloroethylene 0.034 0.035 0.024 J 0.18 0.19 0.13 0.698 6/14/23 15:37 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 15:37 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.058 0.14 0.039 J 0.44 1.1 0.30 0.698 6/14/23 15:37 CMR 1,2,4-Trimethylbenzene 0.30 0.035 0.015 1.5 0.17 0.076 0.698 6/14/23 15:37 CMR 1,3,5-Trimethylbenzene 0.071 0.035 0.018 0.35 0.17 0.091 0.698 6/14/23 15:37 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 15:37 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 15:37 CMR m&p-Xylene 2.3 0.070 0.039 10 0.30 0.17 0.698 6/14/23 15:37 CMR o-Xylene 0.90 0.035 0.018 3.9 0.15 0.078 0.698 6/14/23 15:37 CMR Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 99.8 70-130 95.6 70-130 6/14/23 15:37 6/15/23 20:17 Page 12 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-5 Canister ID: 2229 Sample ID: 23F1309-04 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3484 Sampled: 6/4/2023 09:13 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -8 Receipt Vacuum(in Hg): -7.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 120 1.4 0.84 E 290 3.3 Benzene 0.24 0.035 0.026 0.78 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 18 1.4 0.37 53 4.1 Carbon Disulfide 0.90 0.35 0.032 2.8 1.1 Carbon Tetrachloride 0.084 0.035 0.028 0.53 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform 0.10 0.035 0.033 0.51 0.17 Chloromethane 0.60 0.070 0.028 1.2 0.14 Cyclohexane 0.15 0.035 0.021 0.51 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.54 0.035 0.034 2.7 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.071 0.035 0.032 0.29 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane 0.037 0.035 0.019 0.17 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 44 1.4 0.62 E 83 2.6 Ethyl Acetate 0.63 0.35 0.18 2.3 1.3 Ethylbenzene 0.92 0.035 0.020 4.0 0.15 4-Ethyltoluene 0.073 0.035 0.021 0.36 0.17 Heptane 6.3 0.035 0.022 26 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.59 1.4 0.18 J 2.1 4.9 2-Hexanone (MBK) 0.28 0.14 0.017 1.1 0.57 Isopropanol 4.8 1.4 0.24 12 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) ND 0.035 0.019 ND 0.14 Naphthalene 0.083 0.035 0.026 V-06, Z-01 0.44 0.18 Propene 1.3 1.4 0.31 J 2.2 2.4 Styrene 1.3 0.035 0.018 5.4 0.15 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 2.0 0.698 6/14/23 16:08 CMR 0.084 0.698 6/14/23 16:08 CMR 0.16 0.698 6/14/23 16:08 CMR 0.16 0.698 6/14/23 16:08 CMR 0.25 0.698 6/14/23 16:08 CMR 0.090 0.698 6/14/23 16:08 CMR 0.065 0.698 6/14/23 16:08 CMR 1.1 0.698 6/14/23 16:08 CMR 0.10 0.698 6/14/23 16:08 CMR 0.17 0.698 6/14/23 16:08 CMR 0.11 0.698 6/14/23 16:08 CMR 0.082 0.698 6/14/23 16:08 CMR 0.16 0.698 6/14/23 16:08 CMR 0.057 0.698 6/14/23 16:08 CMR 0.073 0.698 6/14/23 16:08 CMR 0.20 0.698 6/14/23 16:08 CMR 0.16 0.698 6/14/23 16:08 CMR 0.12 0.698 6/14/23 16:08 CMR 0.12 0.698 6/14/23 16:08 CMR 0.14 0.698 6/14/23 16:08 CMR 0.17 0.698 6/14/23 16:08 CMR 0.12 0.698 6/14/23 16:08 CMR 0.13 0.698 6/14/23 16:08 CMR 0.11 0.698 6/14/23 16:08 CMR 0.10 0.698 6/14/23 16:08 CMR 0.11 0.698 6/14/23 16:08 CMR 0.087 0.698 6/14/23 16:08 CMR 0.082 0.698 6/14/23 16:08 CMR 0.081 0.698 6/14/23 16:08 CMR 0.24 0.698 6/14/23 16:08 CMR 0.10 0.698 6/14/23 16:08 CMR 1.2 0.698 6/14/23 16:08 CMR 0.64 0.698 6/14/23 16:08 CMR 0.088 0.698 6/14/23 16:08 CMR 0.11 0.698 6/14/23 16:08 CMR 0.091 0.698 6/14/23 16:08 CMR 0.31 0.698 6/14/23 16:08 CMR 0.64 0.698 6/14/23 16:08 CMR 0.071 0.698 6/14/23 16:08 CMR 0.59 0.698 6/14/23 16:08 CMR 0.097 0.698 6/14/23 16:08 CMR 0.56 0.698 6/14/23 16:08 CMR 0.076 0.698 6/14/23 16:08 CMR 0.14 0.698 6/14/23 16:08 CMR 0.53 0.698 6/14/23 16:08 CMR 0.078 0.698 6/14/23 16:08 CMR 0.13 0.698 6/14/23 16:08 CMR Page 13 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29.5 Field Sample #: IA-5 Canister ID: 2229 Final Vacuum(in Hg): -8 Sample ID: 23F1309-04 Canister Size: 6 liter Receipt Vacuum(in Hg): -7.7 Sample Matrix: Indoor air Flow Controller ID: 3484 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:13 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene 0.044 0.035 0.027 0.30 0.24 0.18 0.698 6/14/23 16:08 CMR Tetrahydrofuran 25 0.35 0.057 74 1.0 0.17 0.698 6/14/23 16:08 CMR Toluene 17 0.035 0.020 63 0.13 0.075 0.698 6/14/23 16:08 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 16:08 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 16:08 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 16:08 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 16:08 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 16:08 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.063 0.14 0.039 J 0.48 1.1 0.30 0.698 6/14/23 16:08 CMR 1,2,4-Trimethylbenzene 0.55 0.035 0.015 2.7 0.17 0.076 0.698 6/14/23 16:08 CMR 1,3,5-Trimethylbenzene 0.13 0.035 0.018 0.66 0.17 0.091 0.698 6/14/23 16:08 CMR Vinyl Acetate 2.0 0.70 0.19 7.0 2.5 0.66 0.698 6/14/23 16:08 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 16:08 CMR m&p-Xylene 3.8 0.070 0.039 16 0.30 0.17 0.698 6/14/23 16:08 CMR o-Xylene 1.4 0.035 0.018 6.0 0.15 0.078 0.698 6/14/23 16:08 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 101 70-130 6/14/23 16:08 Page 14 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-6 Canister ID: 1867 Sample ID: 23F1309-05 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3506 Sampled: 6/4/2023 09:14 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -30.5 Final Vacuum(in Hg): -8.5 Receipt Vacuum(in Hg): -7.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 120 1.4 0.84 E 290 3.3 Benzene 0.24 0.035 0.026 0.77 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 16 1.4 0.37 48 4.1 Carbon Disulfide 0.91 0.35 0.032 2.8 1.1 Carbon Tetrachloride 0.084 0.035 0.028 0.53 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform 0.059 0.035 0.033 0.29 0.17 Chloromethane 0.60 0.070 0.028 1.2 0.14 Cyclohexane 0.37 0.035 0.021 1.3 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.54 0.035 0.034 2.7 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.077 0.035 0.032 0.31 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane 0.035 0.035 0.019 0.16 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 44 1.4 0.62 E 82 2.6 Ethyl Acetate 0.62 0.35 0.18 2.2 1.3 Ethylbenzene 0.94 0.035 0.020 4.1 0.15 4-Ethyltoluene 0.089 0.035 0.021 0.44 0.17 Heptane 6.6 0.035 0.022 27 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.47 1.4 0.18 J 1.6 4.9 2-Hexanone (MBK) 0.18 0.14 0.017 0.73 0.57 Isopropanol 4.9 1.4 0.24 12 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) ND 0.035 0.019 ND 0.14 Naphthalene 0.12 0.035 0.026 V-06, Z-01 0.61 0.18 Propene 1.2 1.4 0.31 J 2.1 2.4 Styrene 1.3 0.035 0.018 5.6 0.15 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 2.0 0.698 6/14/23 16:40 CMR 0.084 0.698 6/14/23 16:40 CMR 0.16 0.698 6/14/23 16:40 CMR 0.16 0.698 6/14/23 16:40 CMR 0.25 0.698 6/14/23 16:40 CMR 0.090 0.698 6/14/23 16:40 CMR 0.065 0.698 6/14/23 16:40 CMR 1.1 0.698 6/14/23 16:40 CMR 0.10 0.698 6/14/23 16:40 CMR 0.17 0.698 6/14/23 16:40 CMR 0.11 0.698 6/14/23 16:40 CMR 0.082 0.698 6/14/23 16:40 CMR 0.16 0.698 6/14/23 16:40 CMR 0.057 0.698 6/14/23 16:40 CMR 0.073 0.698 6/14/23 16:40 CMR 0.20 0.698 6/14/23 16:40 CMR 0.16 0.698 6/14/23 16:40 CMR 0.12 0.698 6/14/23 16:40 CMR 0.12 0.698 6/14/23 16:40 CMR 0.14 0.698 6/14/23 16:40 CMR 0.17 0.698 6/14/23 16:40 CMR 0.12 0.698 6/14/23 16:40 CMR 0.13 0.698 6/14/23 16:40 CMR 0.11 0.698 6/14/23 16:40 CMR 0.10 0.698 6/14/23 16:40 CMR 0.11 0.698 6/14/23 16:40 CMR 0.087 0.698 6/14/23 16:40 CMR 0.082 0.698 6/14/23 16:40 CMR 0.081 0.698 6/14/23 16:40 CMR 0.24 0.698 6/14/23 16:40 CMR 0.10 0.698 6/14/23 16:40 CMR 1.2 0.698 6/14/23 16:40 CMR 0.64 0.698 6/14/23 16:40 CMR 0.088 0.698 6/14/23 16:40 CMR 0.11 0.698 6/14/23 16:40 CMR 0.091 0.698 6/14/23 16:40 CMR 0.31 0.698 6/14/23 16:40 CMR 0.64 0.698 6/14/23 16:40 CMR 0.071 0.698 6/14/23 16:40 CMR 0.59 0.698 6/14/23 16:40 CMR 0.097 0.698 6/14/23 16:40 CMR 0.56 0.698 6/14/23 16:40 CMR 0.076 0.698 6/14/23 16:40 CMR 0.14 0.698 6/14/23 16:40 CMR 0.53 0.698 6/14/23 16:40 CMR 0.078 0.698 6/14/23 16:40 CMR 0.13 0.698 6/14/23 16:40 CMR Page 15 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -30.5 Field Sample #: IA-6 Canister ID: 1867 Final Vacuum(in Hg): -8.5 Sample ID: 23F1309-05 Canister Size: 6 liter Receipt Vacuum(in Hg): -7.3 Sample Matrix: Indoor air Flow Controller ID: 3506 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:14 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene 0.045 0.035 0.027 0.30 0.24 0.18 0.698 6/14/23 16:40 CMR Tetrahydrofuran 25 0.35 0.057 74 1.0 0.17 0.698 6/14/23 16:40 CMR Toluene 17 0.035 0.020 64 0.13 0.075 0.698 6/14/23 16:40 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 16:40 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 16:40 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 16:40 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 16:40 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 16:40 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.066 0.14 0.039 J 0.51 1.1 0.30 0.698 6/14/23 16:40 CMR 1,2,4-Trimethylbenzene 0.58 0.035 0.015 2.9 0.17 0.076 0.698 6/14/23 16:40 CMR 1,3,5-Trimethylbenzene 0.14 0.035 0.018 0.69 0.17 0.091 0.698 6/14/23 16:40 CMR Vinyl Acetate 1.9 0.70 0.19 6.7 2.5 0.66 0.698 6/14/23 16:40 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 16:40 CMR m&p-Xylene 3.7 0.070 0.039 16 0.30 0.17 0.698 6/14/23 16:40 CMR o-Xylene 1.4 0.035 0.018 6.0 0.15 0.078 0.698 6/14/23 16:40 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 98.4 70-130 6/14/23 16:40 Page 16 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-7 Canister ID: 1815 Sample ID: 23F1309-06 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3731 Sampled: 6/4/2023 09:18 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -9 Receipt Vacuum(in Hg): -8.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 120 1.4 0.84 E 290 3.3 Benzene 0.24 0.035 0.026 0.76 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane 0.024 0.035 0.023 J 0.092 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 16 1.4 0.37 47 4.1 Carbon Disulfide 0.93 0.35 0.032 2.9 1.1 Carbon Tetrachloride 0.080 0.035 0.028 0.50 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.032 0.035 0.031 J 0.085 0.092 Chloroform 0.065 0.035 0.033 0.32 0.17 Chloromethane 0.64 0.070 0.028 1.3 0.14 Cyclohexane 0.15 0.035 0.021 0.50 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.56 0.035 0.034 2.8 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.071 0.035 0.032 0.29 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene 0.038 0.035 0.019 0.17 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 42 1.4 0.62 E 79 2.6 Ethyl Acetate 0.46 0.35 0.18 1.7 1.3 Ethylbenzene 0.94 0.035 0.020 4.1 0.15 4-Ethyltoluene 0.087 0.035 0.021 0.43 0.17 Heptane 6.3 0.035 0.022 26 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.50 1.4 0.18 J 1.8 4.9 2-Hexanone (MBK) 0.15 0.14 0.017 0.63 0.57 Isopropanol 4.6 1.4 0.24 11 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) ND 0.035 0.019 ND 0.14 Naphthalene 0.091 0.035 0.026 V-06, Z-01 0.48 0.18 Propene ND 1.4 0.31 ND 2.4 Styrene 1.4 0.035 0.018 5.8 0.15 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 2.0 0.698 6/14/23 17:11 CMR 0.084 0.698 6/14/23 17:11 CMR 0.16 0.698 6/14/23 17:11 CMR 0.16 0.698 6/14/23 17:11 CMR 0.25 0.698 6/14/23 17:11 CMR 0.090 0.698 6/14/23 17:11 CMR 0.065 0.698 6/14/23 17:11 CMR 1.1 0.698 6/14/23 17:11 CMR 0.10 0.698 6/14/23 17:11 CMR 0.17 0.698 6/14/23 17:11 CMR 0.11 0.698 6/14/23 17:11 CMR 0.082 0.698 6/14/23 17:11 CMR 0.16 0.698 6/14/23 17:11 CMR 0.057 0.698 6/14/23 17:11 CMR 0.073 0.698 6/14/23 17:11 CMR 0.20 0.698 6/14/23 17:11 CMR 0.16 0.698 6/14/23 17:11 CMR 0.12 0.698 6/14/23 17:11 CMR 0.12 0.698 6/14/23 17:11 CMR 0.14 0.698 6/14/23 17:11 CMR 0.17 0.698 6/14/23 17:11 CMR 0.12 0.698 6/14/23 17:11 CMR 0.13 0.698 6/14/23 17:11 CMR 0.11 0.698 6/14/23 17:11 CMR 0.10 0.698 6/14/23 17:11 CMR 0.11 0.698 6/14/23 17:11 CMR 0.087 0.698 6/14/23 17:11 CMR 0.082 0.698 6/14/23 17:11 CMR 0.081 0.698 6/14/23 17:11 CMR 0.24 0.698 6/14/23 17:11 CMR 0.10 0.698 6/14/23 17:11 CMR 1.2 0.698 6/14/23 17:11 CMR 0.64 0.698 6/14/23 17:11 CMR 0.088 0.698 6/14/23 17:11 CMR 0.11 0.698 6/14/23 17:11 CMR 0.091 0.698 6/14/23 17:11 CMR 0.31 0.698 6/14/23 17:11 CMR 0.64 0.698 6/14/23 17:11 CMR 0.071 0.698 6/14/23 17:11 CMR 0.59 0.698 6/14/23 17:11 CMR 0.097 0.698 6/14/23 17:11 CMR 0.56 0.698 6/14/23 17:11 CMR 0.076 0.698 6/14/23 17:11 CMR 0.14 0.698 6/14/23 17:11 CMR 0.53 0.698 6/14/23 17:11 CMR 0.078 0.698 6/14/23 17:11 CMR 0.13 0.698 6/14/23 17:11 CMR Page 17 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-7 Sample ID: 23F1309-06 Sample Matrix: Indoor air Sampled: 6/4/2023 09:18 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1815 Canister Size: 6 liter Flow Controller ID: 3731 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -9 Receipt Vacuum(in Hg): -8.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.040 0.035 0.027 0.27 0.24 0.18 0.698 6/14/23 17:11 CMR Tetrahydrofuran 27 0.35 0.057 79 1.0 0.17 0.698 6/14/23 17:11 CMR Toluene 16 0.035 0.020 62 0.13 0.075 0.698 6/14/23 17:11 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 17:11 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 17:11 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 17:11 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 17:11 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 17:11 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.066 0.14 0.039 J 0.51 1.1 0.30 0.698 6/14/23 17:11 CMR 1,2,4-Trimethylbenzene 0.57 0.035 0.015 2.8 0.17 0.076 0.698 6/14/23 17:11 CMR 1,3,5-Trimethylbenzene 0.13 0.035 0.018 0.66 0.17 0.091 0.698 6/14/23 17:11 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 17:11 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 17:11 CMR m&p-Xylene 3.7 0.070 0.039 16 0.30 0.17 0.698 6/14/23 17:11 CMR o-Xylene 1.4 0.035 0.018 6.0 0.15 0.078 0.698 6/14/23 17:11 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 101 % REC Limits 70-130 6/14/23 17:11 Page 18 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-7 DUP Sample ID: 23F1309-07 Sample Matrix: Indoor air Sampled: 6/4/2023 09:18 Sample Description/Location: Sub Description/Location: Canister ID: 1809 Canister Size: 6 liter Flow Controller ID: 3732 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -10.5 Receipt Vacuum(in Hg): -10.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 120 1.4 0.84 E 290 3.3 2.0 0.696 6/14/23 17:44 CMR Benzene 0.19 0.035 0.026 0.59 0.11 0.084 0.696 6/14/23 17:44 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.696 6/14/23 17:44 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.696 6/14/23 17:44 CMR Bromoform ND 0.035 0.024 ND 0.36 0.24 0.696 6/14/23 17:44 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.696 6/14/23 17:44 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.696 6/14/23 17:44 CMR 2-Butanone (MEK) 12 1.4 0.37 34 4.1 1.1 0.696 6/14/23 17:44 CMR Carbon Disulfide 0.24 0.35 0.032 J 0.75 1.1 0.10 0.696 6/14/23 17:44 CMR Carbon Tetrachloride 0.091 0.035 0.028 0.57 0.22 0.17 0.696 6/14/23 17:44 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.696 6/14/23 17:44 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.081 0.696 6/14/23 17:44 CMR Chloroform 0.039 0.035 0.033 0.19 0.17 0.16 0.696 6/14/23 17:44 CMR Chloromethane 0.63 0.070 0.028 1.3 0.14 0.057 0.696 6/14/23 17:44 CMR Cyclohexane 0.074 0.035 0.021 0.26 0.12 0.072 0.696 6/14/23 17:44 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.696 6/14/23 17:44 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.696 6/14/23 17:44 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.696 6/14/23 17:44 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.696 6/14/23 17:44 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.696 6/14/23 17:44 CMR Dichlorodifluoromethane (Freon 12) 0.60 0.035 0.034 3.0 0.17 0.17 0.696 6/14/23 17:44 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.696 6/14/23 17:44 CMR 1,2-Dichloroethane 0.040 0.035 0.032 0.16 0.14 0.13 0.696 6/14/23 17:44 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.696 6/14/23 17:44 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.696 6/14/23 17:44 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.696 6/14/23 17:44 CMR 1,2-Dichloropropane 0.023 0.035 0.019 J 0.11 0.16 0.087 0.696 6/14/23 17:44 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.696 6/14/23 17:44 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.696 6/14/23 17:44 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.696 6/14/23 17:44 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.696 6/14/23 17:44 CMR Ethanol 19 1.4 0.61 37 2.6 1.2 0.696 6/14/23 17:44 CMR Ethyl Acetate 0.24 0.35 0.18 J 0.88 1.3 0.63 0.696 6/14/23 17:44 CMR Ethylbenzene 0.55 0.035 0.020 2.4 0.15 0.088 0.696 6/14/23 17:44 CMR 4-Ethyltoluene 0.044 0.035 0.021 0.22 0.17 0.11 0.696 6/14/23 17:44 CMR Heptane 7.3 0.035 0.022 30 0.14 0.091 0.696 6/14/23 17:44 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.696 6/14/23 17:44 CMR Hexane 0.23 1.4 0.18 J 0.80 4.9 0.64 0.696 6/14/23 17:44 CMR 2-Hexanone (MBK) 0.071 0.14 0.017 J 0.29 0.57 0.071 0.696 6/14/23 17:44 CMR Isopropanol 2.1 1.4 0.24 5.3 3.4 0.59 0.696 6/14/23 17:44 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.696 6/14/23 17:44 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.696 6/14/23 17:44 CMR 4-Methyl-2-pentanone (MIBK) ND 0.035 0.019 ND 0.14 0.076 0.696 6/14/23 17:44 CMR Naphthalene 0.045 0.035 0.026 V-06, Z-01 0.23 0.18 0.14 0.696 6/14/23 17:44 CMR Propene ND 1.4 0.31 ND 2.4 0.53 0.696 6/14/23 17:44 CMR Styrene 1.4 0.035 0.018 5.9 0.15 0.078 0.696 6/14/23 17:44 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.696 6/14/23 17:44 CMR Page 19 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: IA-7 DUP Canister ID: 1809 Final Vacuum(in Hg): -10.5 Sample ID: 23F1309-07 Canister Size: 6 liter Receipt Vacuum(in Hg): -10.3 Sample Matrix: Indoor air Flow Controller ID: 3732 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:18 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.696 6/14/23 17:44 CMR Tetrahydrofuran 34 0.35 0.057 100 1.0 0.17 0.696 6/14/23 17:44 CMR Toluene 15 0.035 0.020 56 0.13 0.075 0.696 6/14/23 17:44 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.696 6/14/23 17:44 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.696 6/14/23 17:44 CMR 1,1,2-Trichloroethane ND 0.035 0.024 ND 0.19 0.13 0.696 6/14/23 17:44 CMR Trichloroethylene ND 0.035 0.023 ND 0.19 0.13 0.696 6/14/23 17:44 CMR Trichlorofluoromethane (Freon 11) 0.25 0.14 0.041 1.4 0.78 0.23 0.696 6/14/23 17:44 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.077 0.14 0.039 J 0.59 1.1 0.30 0.696 6/14/23 17:44 CMR 1,2,4-Trimethylbenzene 0.29 0.035 0.015 1.4 0.17 0.076 0.696 6/14/23 17:44 CMR 1,3,5-Trimethylbenzene 0.065 0.035 0.018 0.32 0.17 0.090 0.696 6/14/23 17:44 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.696 6/14/23 17:44 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.696 6/14/23 17:44 CMR m&p-Xylene 2.2 0.070 0.039 9.4 0.30 0.17 0.696 6/14/23 17:44 CMR o-Xylene 0.80 0.035 0.018 3.5 0.15 0.077 0.696 6/14/23 17:44 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 98.6 70-130 6/14/23 17:44 Page 20 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-9 Canister ID: 1449 Sample ID: 23F1309-08 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3712 Sampled: 6/4/2023 09:33 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -10 Receipt Vacuum(in Hg): -9.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 110 1.4 0.84 E 260 3.3 Benzene 0.15 0.035 0.026 0.49 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 9.9 1.4 0.37 29 4.1 Carbon Disulfide 0.21 0.35 0.032 J 0.65 1.1 Carbon Tetrachloride 0.077 0.035 0.028 0.49 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform ND 0.035 0.033 ND 0.17 Chloromethane 0.59 0.070 0.028 1.2 0.14 Cyclohexane 0.065 0.035 0.021 0.22 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.6 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.039 0.035 0.032 0.16 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane 0.022 0.035 0.019 J 0.10 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 17 1.4 0.62 32 2.6 Ethyl Acetate 0.26 0.35 0.18 J 0.94 1.3 Ethylbenzene 0.46 0.035 0.020 2.0 0.15 4-Ethyltoluene 0.036 0.035 0.021 0.17 0.17 Heptane 6.3 0.035 0.022 26 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane ND 1.4 0.18 ND 4.9 2-Hexanone (MBK) 0.050 0.14 0.017 J 0.20 0.57 Isopropanol 1.8 1.4 0.24 4.5 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) ND 0.035 0.019 ND 0.14 Naphthalene 0.034 0.035 0.026 V-06, Z-01, J 0.18 0.18 Propene 0.63 1.4 0.31 J 1.1 2.4 Styrene 1.2 0.035 0.018 5.1 0.15 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 2.0 0.698 6/14/23 18:16 CMR 0.084 0.698 6/14/23 18:16 CMR 0.16 0.698 6/14/23 18:16 CMR 0.16 0.698 6/14/23 18:16 CMR 0.25 0.698 6/14/23 18:16 CMR 0.090 0.698 6/14/23 18:16 CMR 0.065 0.698 6/14/23 18:16 CMR 1.1 0.698 6/14/23 18:16 CMR 0.10 0.698 6/14/23 18:16 CMR 0.17 0.698 6/14/23 18:16 CMR 0.11 0.698 6/14/23 18:16 CMR 0.082 0.698 6/14/23 18:16 CMR 0.16 0.698 6/14/23 18:16 CMR 0.057 0.698 6/14/23 18:16 CMR 0.073 0.698 6/14/23 18:16 CMR 0.20 0.698 6/14/23 18:16 CMR 0.16 0.698 6/14/23 18:16 CMR 0.12 0.698 6/14/23 18:16 CMR 0.12 0.698 6/14/23 18:16 CMR 0.14 0.698 6/14/23 18:16 CMR 0.17 0.698 6/14/23 18:16 CMR 0.12 0.698 6/14/23 18:16 CMR 0.13 0.698 6/14/23 18:16 CMR 0.11 0.698 6/14/23 18:16 CMR 0.10 0.698 6/14/23 18:16 CMR 0.11 0.698 6/14/23 18:16 CMR 0.087 0.698 6/14/23 18:16 CMR 0.082 0.698 6/14/23 18:16 CMR 0.081 0.698 6/14/23 18:16 CMR 0.24 0.698 6/14/23 18:16 CMR 0.10 0.698 6/14/23 18:16 CMR 1.2 0.698 6/14/23 18:16 CMR 0.64 0.698 6/14/23 18:16 CMR 0.088 0.698 6/14/23 18:16 CMR 0.11 0.698 6/14/23 18:16 CMR 0.091 0.698 6/14/23 18:16 CMR 0.31 0.698 6/14/23 18:16 CMR 0.64 0.698 6/14/23 18:16 CMR 0.071 0.698 6/14/23 18:16 CMR 0.59 0.698 6/14/23 18:16 CMR 0.097 0.698 6/14/23 18:16 CMR 0.56 0.698 6/14/23 18:16 CMR 0.076 0.698 6/14/23 18:16 CMR 0.14 0.698 6/14/23 18:16 CMR 0.53 0.698 6/14/23 18:16 CMR 0.078 0.698 6/14/23 18:16 CMR 0.13 0.698 6/14/23 18:16 CMR Page 21 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: IA-9 Canister ID: 1449 Final Vacuum(in Hg): -10 Sample ID: 23F1309-08 Canister Size: 6 liter Receipt Vacuum(in Hg): -9.3 Sample Matrix: Indoor air Flow Controller ID: 3712 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:33 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/14/23 18:16 CMR Tetrahydrofuran 30 0.35 0.057 87 1.0 0.17 0.698 6/14/23 18:16 CMR Toluene 13 0.035 0.020 48 0.13 0.075 0.698 6/14/23 18:16 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 18:16 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 18:16 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 18:16 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 18:16 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 18:16 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.062 0.14 0.039 J 0.48 1.1 0.30 0.698 6/14/23 18:16 CMR 1,2,4-Trimethylbenzene 0.24 0.035 0.015 1.2 0.17 0.076 0.698 6/14/23 18:16 CMR 1,3,5-Trimethylbenzene 0.056 0.035 0.018 0.27 0.17 0.091 0.698 6/14/23 18:16 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 18:16 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 18:16 CMR m&p-Xylene 1.8 0.070 0.039 8.0 0.30 0.17 0.698 6/14/23 18:16 CMR o-Xylene 0.67 0.035 0.018 2.9 0.15 0.078 0.698 6/14/23 18:16 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 98.8 70-130 6/14/23 18:16 Page 22 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-10 Canister ID: 1964 Sample ID: 23F1309-09 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3744 Sampled: 6/4/2023 09:39 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -8.25 Receipt Vacuum(in Hg): -8.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 140 4.0 2.4 E 340 9.5 Benzene 0.24 0.035 0.026 0.75 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 16 1.4 0.37 47 4.1 Carbon Disulfide 0.38 0.35 0.032 1.2 1.1 Carbon Tetrachloride 0.083 0.035 0.028 0.52 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.16 0.035 0.031 0.42 0.092 Chloroform 0.050 0.035 0.033 0.24 0.17 Chloromethane 0.53 0.070 0.028 1.1 0.14 Cyclohexane 0.35 0.035 0.021 1.2 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.57 0.035 0.034 2.8 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.059 0.035 0.032 0.24 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene 0.062 0.035 0.019 0.29 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane 0.35 0.35 0.029 1.3 1.3 Ethanol 35 4.0 1.8 67 7.5 Ethyl Acetate 0.57 0.35 0.18 2.0 1.3 Ethylbenzene 1.2 0.035 0.020 5.4 0.15 4-Ethyltoluene 0.10 0.035 0.021 0.49 0.17 Heptane 1.5 0.035 0.022 6.2 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 2.5 1.4 0.18 8.7 4.9 2-Hexanone (MBK) 0.15 0.14 0.017 0.63 0.57 Isopropanol 2.7 1.4 0.24 6.6 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.31 0.035 0.019 1.3 0.14 Naphthalene 0.080 0.035 0.026 V-06, Z-01 0.42 0.18 Propene 1.3 1.4 0.31 J 2.3 2.4 Styrene 0.93 0.035 0.018 4.0 0.15 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 5.7 2 6/15/23 20:44 CMR 0.084 0.698 6/14/23 18:48 CMR 0.16 0.698 6/14/23 18:48 CMR 0.16 0.698 6/14/23 18:48 CMR 0.25 0.698 6/14/23 18:48 CMR 0.090 0.698 6/14/23 18:48 CMR 0.065 0.698 6/14/23 18:48 CMR 1.1 0.698 6/14/23 18:48 CMR 0.10 0.698 6/14/23 18:48 CMR 0.17 0.698 6/14/23 18:48 CMR 0.11 0.698 6/14/23 18:48 CMR 0.082 0.698 6/14/23 18:48 CMR 0.16 0.698 6/14/23 18:48 CMR 0.057 0.698 6/14/23 18:48 CMR 0.073 0.698 6/14/23 18:48 CMR 0.20 0.698 6/14/23 18:48 CMR 0.16 0.698 6/14/23 18:48 CMR 0.12 0.698 6/14/23 18:48 CMR 0.12 0.698 6/14/23 18:48 CMR 0.14 0.698 6/14/23 18:48 CMR 0.17 0.698 6/14/23 18:48 CMR 0.12 0.698 6/14/23 18:48 CMR 0.13 0.698 6/14/23 18:48 CMR 0.11 0.698 6/14/23 18:48 CMR 0.10 0.698 6/14/23 18:48 CMR 0.11 0.698 6/14/23 18:48 CMR 0.087 0.698 6/14/23 18:48 CMR 0.082 0.698 6/14/23 18:48 CMR 0.081 0.698 6/14/23 18:48 CMR 0.24 0.698 6/14/23 18:48 CMR 0.10 0.698 6/14/23 18:48 CMR 3.3 2 6/15/23 20:44 CMR 0.64 0.698 6/14/23 18:48 CMR 0.088 0.698 6/14/23 18:48 CMR 0.11 0.698 6/14/23 18:48 CMR 0.091 0.698 6/14/23 18:48 CMR 0.31 0.698 6/14/23 18:48 CMR 0.64 0.698 6/14/23 18:48 CMR 0.071 0.698 6/14/23 18:48 CMR 0.59 0.698 6/14/23 18:48 CMR 0.097 0.698 6/14/23 18:48 CMR 0.56 0.698 6/14/23 18:48 CMR 0.076 0.698 6/14/23 18:48 CMR 0.14 0.698 6/14/23 18:48 CMR 0.53 0.698 6/14/23 18:48 CMR 0.078 0.698 6/14/23 18:48 CMR 0.13 0.698 6/14/23 18:48 CMR Page 23 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-10 Sample ID: 23F1309-09 Sample Matrix: Indoor air Sampled: 6/4/2023 09:39 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1964 Canister Size: 6 liter Flow Controller ID: 3744 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -8.25 Receipt Vacuum(in Hg): -8.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/14/23 18:48 CMR Tetrahydrofuran 34 1.0 0.16 100 2.9 0.48 2 6/15/23 20:44 CMR Toluene 32 0.035 0.020 120 0.13 0.075 0.698 6/14/23 18:48 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 18:48 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 18:48 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 18:48 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 18:48 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 18:48 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.064 0.14 0.039 J 0.49 1.1 0.30 0.698 6/14/23 18:48 CMR 1,2,4-Trimethylbenzene 0.64 0.035 0.015 3.2 0.17 0.076 0.698 6/14/23 18:48 CMR 1,3,5-Trimethylbenzene 0.16 0.035 0.018 0.80 0.17 0.091 0.698 6/14/23 18:48 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 18:48 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 18:48 CMR m&p-Xylene 5.0 0.070 0.039 22 0.30 0.17 0.698 6/14/23 18:48 CMR o-Xylene 1.7 0.035 0.018 7.4 0.15 0.078 0.698 6/14/23 18:48 CMR Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 102 70-130 96.0 70-130 6/14/23 18:48 6/15/23 20:44 Page 24 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-11 Sample ID: 23F1309-10 Sample Matrix: Indoor air Sampled: 6/4/2023 09:41 Sample Description/Location: Sub Description/Location: Canister ID: 1878 Canister Size: 6 liter Flow Controller ID: 3743 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -10.25 Receipt Vacuum(in Hg): -9.9 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 140 4.0 2.4 E 330 9.5 5.7 2 6/15/23 21:10 CMR Benzene 0.24 0.035 0.026 0.78 0.11 0.084 0.696 6/14/23 19:21 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.696 6/14/23 19:21 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.696 6/14/23 19:21 CMR Bromoform ND 0.035 0.024 ND 0.36 0.24 0.696 6/14/23 19:21 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.696 6/14/23 19:21 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.696 6/14/23 19:21 CMR 2-Butanone (MEK) 13 1.4 0.37 39 4.1 1.1 0.696 6/14/23 19:21 CMR Carbon Disulfide 0.37 0.35 0.032 1.2 1.1 0.10 0.696 6/14/23 19:21 CMR Carbon Tetrachloride 0.079 0.035 0.028 0.50 0.22 0.17 0.696 6/14/23 19:21 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.696 6/14/23 19:21 CMR Chloroethane 0.17 0.035 0.031 0.45 0.092 0.081 0.696 6/14/23 19:21 CMR Chloroform 0.055 0.035 0.033 0.27 0.17 0.16 0.696 6/14/23 19:21 CMR Chloromethane 0.55 0.070 0.028 1.1 0.14 0.057 0.696 6/14/23 19:21 CMR Cyclohexane 0.35 0.035 0.021 1.2 0.12 0.072 0.696 6/14/23 19:21 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.696 6/14/23 19:21 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.696 6/14/23 19:21 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.696 6/14/23 19:21 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.696 6/14/23 19:21 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.696 6/14/23 19:21 CMR Dichlorodifluoromethane (Freon 12) 0.54 0.035 0.034 2.7 0.17 0.17 0.696 6/14/23 19:21 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.696 6/14/23 19:21 CMR 1,2-Dichloroethane 0.063 0.035 0.032 0.26 0.14 0.13 0.696 6/14/23 19:21 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.696 6/14/23 19:21 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.696 6/14/23 19:21 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.696 6/14/23 19:21 CMR 1,2-Dichloropropane 0.065 0.035 0.019 0.30 0.16 0.087 0.696 6/14/23 19:21 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.696 6/14/23 19:21 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.696 6/14/23 19:21 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.696 6/14/23 19:21 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.696 6/14/23 19:21 CMR Ethanol 36 4.0 1.8 68 7.5 3.3 2 6/15/23 21:10 CMR Ethyl Acetate 0.64 0.35 0.18 2.3 1.3 0.63 0.696 6/14/23 19:21 CMR Ethylbenzene 1.2 0.035 0.020 5.0 0.15 0.088 0.696 6/14/23 19:21 CMR 4-Ethyltoluene 0.094 0.035 0.021 0.46 0.17 0.11 0.696 6/14/23 19:21 CMR Heptane 1.5 0.035 0.022 6.0 0.14 0.091 0.696 6/14/23 19:21 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.696 6/14/23 19:21 CMR Hexane 2.5 1.4 0.18 9.0 4.9 0.64 0.696 6/14/23 19:21 CMR 2-Hexanone (MBK) 0.16 0.14 0.017 0.66 0.57 0.071 0.696 6/14/23 19:21 CMR Isopropanol 2.9 1.4 0.24 7.1 3.4 0.59 0.696 6/14/23 19:21 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.696 6/14/23 19:21 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.696 6/14/23 19:21 CMR 4-Methyl-2-pentanone (MIBK) 0.32 0.035 0.019 1.3 0.14 0.076 0.696 6/14/23 19:21 CMR Naphthalene 0.10 0.035 0.026 V-06, Z-01 0.55 0.18 0.14 0.696 6/14/23 19:21 CMR Propene 1.2 1.4 0.31 J 2.1 2.4 0.53 0.696 6/14/23 19:21 CMR Styrene 0.86 0.035 0.018 3.7 0.15 0.078 0.696 6/14/23 19:21 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.696 6/14/23 19:21 CMR Page 25 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-11 Sample ID: 23F1309-10 Sample Matrix: Indoor air Sampled: 6/4/2023 09:41 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1878 Canister Size: 6 liter Flow Controller ID: 3743 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -10.25 Receipt Vacuum(in Hg): -9.9 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.15 0.035 0.027 1.0 0.24 0.18 0.696 6/14/23 19:21 CMR Tetrahydrofuran 34 1.0 0.16 99 2.9 0.48 2 6/15/23 21:10 CMR Toluene 29 0.035 0.020 110 0.13 0.075 0.696 6/14/23 19:21 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.696 6/14/23 19:21 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.696 6/14/23 19:21 CMR 1,1,2-Trichloroethane ND 0.035 0.024 ND 0.19 0.13 0.696 6/14/23 19:21 CMR Trichloroethylene ND 0.035 0.023 ND 0.19 0.13 0.696 6/14/23 19:21 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.696 6/14/23 19:21 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.062 0.14 0.039 J 0.47 1.1 0.30 0.696 6/14/23 19:21 CMR 1,2,4-Trimethylbenzene 0.61 0.035 0.015 3.0 0.17 0.076 0.696 6/14/23 19:21 CMR 1,3,5-Trimethylbenzene 0.14 0.035 0.018 0.71 0.17 0.090 0.696 6/14/23 19:21 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.696 6/14/23 19:21 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.696 6/14/23 19:21 CMR m&p-Xylene 4.6 0.070 0.039 20 0.30 0.17 0.696 6/14/23 19:21 CMR o-Xylene 1.6 0.035 0.018 6.9 0.15 0.077 0.696 6/14/23 19:21 CMR Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 99.1 70-130 96.0 70-130 6/14/23 19:21 6/15/23 21:10 Page 26 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-12 Canister ID: 2186 Sample ID: 23F1309-11 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3534 Sampled: 6/4/2023 09:44 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -7.25 Receipt Vacuum(in Hg): -7.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 140 4.0 2.4 E 330 9.5 Benzene 0.23 0.035 0.026 0.74 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 14 1.4 0.37 42 4.1 Carbon Disulfide 0.36 0.35 0.032 1.1 1.1 Carbon Tetrachloride 0.075 0.035 0.028 0.47 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.17 0.035 0.031 0.44 0.092 Chloroform 0.052 0.035 0.033 0.25 0.17 Chloromethane 0.59 0.070 0.028 1.2 0.14 Cyclohexane 0.34 0.035 0.021 1.2 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.56 0.035 0.034 2.8 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.059 0.035 0.032 0.24 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene 0.063 0.035 0.019 0.29 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 35 4.0 1.8 66 7.5 Ethyl Acetate 0.56 0.35 0.18 2.0 1.3 Ethylbenzene 1.2 0.035 0.020 5.2 0.15 4-Ethyltoluene 0.10 0.035 0.021 0.50 0.17 Heptane 1.5 0.035 0.022 5.9 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 2.3 1.4 0.18 8.1 4.9 2-Hexanone (MBK) 0.18 0.14 0.017 0.75 0.57 Isopropanol 2.5 1.4 0.24 6.2 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.32 0.035 0.019 1.3 0.14 Naphthalene 0.093 0.035 0.026 V-06, Z-01 0.49 0.18 Propene ND 1.4 0.31 ND 2.4 Styrene 0.88 0.035 0.018 3.7 0.15 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 5.7 2 6/15/23 21:37 CMR 0.084 0.698 6/14/23 19:53 CMR 0.16 0.698 6/14/23 19:53 CMR 0.16 0.698 6/14/23 19:53 CMR 0.25 0.698 6/14/23 19:53 CMR 0.090 0.698 6/14/23 19:53 CMR 0.065 0.698 6/14/23 19:53 CMR 1.1 0.698 6/14/23 19:53 CMR 0.10 0.698 6/14/23 19:53 CMR 0.17 0.698 6/14/23 19:53 CMR 0.11 0.698 6/14/23 19:53 CMR 0.082 0.698 6/14/23 19:53 CMR 0.16 0.698 6/14/23 19:53 CMR 0.057 0.698 6/14/23 19:53 CMR 0.073 0.698 6/14/23 19:53 CMR 0.20 0.698 6/14/23 19:53 CMR 0.16 0.698 6/14/23 19:53 CMR 0.12 0.698 6/14/23 19:53 CMR 0.12 0.698 6/14/23 19:53 CMR 0.14 0.698 6/14/23 19:53 CMR 0.17 0.698 6/14/23 19:53 CMR 0.12 0.698 6/14/23 19:53 CMR 0.13 0.698 6/14/23 19:53 CMR 0.11 0.698 6/14/23 19:53 CMR 0.10 0.698 6/14/23 19:53 CMR 0.11 0.698 6/14/23 19:53 CMR 0.087 0.698 6/14/23 19:53 CMR 0.082 0.698 6/14/23 19:53 CMR 0.081 0.698 6/14/23 19:53 CMR 0.24 0.698 6/14/23 19:53 CMR 0.10 0.698 6/14/23 19:53 CMR 3.3 2 6/15/23 21:37 CMR 0.64 0.698 6/14/23 19:53 CMR 0.088 0.698 6/14/23 19:53 CMR 0.11 0.698 6/14/23 19:53 CMR 0.091 0.698 6/14/23 19:53 CMR 0.31 0.698 6/14/23 19:53 CMR 0.64 0.698 6/14/23 19:53 CMR 0.071 0.698 6/14/23 19:53 CMR 0.59 0.698 6/14/23 19:53 CMR 0.097 0.698 6/14/23 19:53 CMR 0.56 0.698 6/14/23 19:53 CMR 0.076 0.698 6/14/23 19:53 CMR 0.14 0.698 6/14/23 19:53 CMR 0.53 0.698 6/14/23 19:53 CMR 0.078 0.698 6/14/23 19:53 CMR 0.13 0.698 6/14/23 19:53 CMR Page 27 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-12 Sample ID: 23F1309-11 Sample Matrix: Indoor air Sampled: 6/4/2023 09:44 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2186 Canister Size: 6 liter Flow Controller ID: 3534 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -7.25 Receipt Vacuum(in Hg): -7.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/14/23 19:53 CMR Tetrahydrofuran 33 1.0 0.16 97 2.9 0.48 2 6/15/23 21:37 CMR Toluene 30 0.035 0.020 110 0.13 0.075 0.698 6/14/23 19:53 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 19:53 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 19:53 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 19:53 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 19:53 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 19:53 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.064 0.14 0.039 J 0.49 1.1 0.30 0.698 6/14/23 19:53 CMR 1,2,4-Trimethylbenzene 0.60 0.035 0.015 3.0 0.17 0.076 0.698 6/14/23 19:53 CMR 1,3,5-Trimethylbenzene 0.16 0.035 0.018 0.78 0.17 0.091 0.698 6/14/23 19:53 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 19:53 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 19:53 CMR m&p-Xylene 4.7 0.070 0.039 20 0.30 0.17 0.698 6/14/23 19:53 CMR o-Xylene 1.6 0.035 0.018 7.0 0.15 0.078 0.698 6/14/23 19:53 CMR Surrogates 4-Bromofluorobenzene (1) 4-Bromofluorobenzene (1) % Recovery % REC Limits 99.6 70-130 95.0 70-130 6/14/23 19:53 6/15/23 21:37 Page 28 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-14 Canister ID: 1139 Sample ID: 23F1309-12 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3532 Sampled: 6/4/2023 09:46 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29.25 Final Vacuum(in Hg): -8.25 Receipt Vacuum(in Hg): -7.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 140 4.0 2.4 E 330 9.5 Benzene 0.24 0.035 0.026 0.78 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 14 1.4 0.37 L-05 40 4.1 Carbon Disulfide 0.35 0.35 0.032 J 1.1 1.1 Carbon Tetrachloride 0.081 0.035 0.028 0.51 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.16 0.035 0.031 0.42 0.092 Chloroform 0.049 0.035 0.033 0.24 0.17 Chloromethane 0.58 0.070 0.028 1.2 0.14 Cyclohexane 0.35 0.035 0.021 1.2 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.54 0.035 0.034 2.6 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.068 0.035 0.032 0.27 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene 0.059 0.035 0.019 0.27 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 36 4.0 1.8 68 7.5 Ethyl Acetate 0.57 0.35 0.18 2.0 1.3 Ethylbenzene 1.2 0.035 0.020 5.4 0.15 4-Ethyltoluene 0.082 0.035 0.021 0.40 0.17 Heptane 1.5 0.035 0.022 6.0 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 1.5 1.4 0.18 5.2 4.9 2-Hexanone (MBK) 0.18 0.14 0.017 0.75 0.57 Isopropanol 2.7 1.4 0.24 6.6 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.34 0.035 0.019 1.4 0.14 Naphthalene 0.057 0.035 0.026 L-05, V-06, 0.30 0.18 Z-01 Propene ND 1.4 0.31 ND 2.4 Styrene 0.90 0.035 0.018 3.8 0.15 5.7 2 6/15/23 22:30 CMR 0.084 0.698 6/14/23 22:52 CMR 0.16 0.698 6/14/23 22:52 CMR 0.16 0.698 6/14/23 22:52 CMR 0.25 0.698 6/14/23 22:52 CMR 0.090 0.698 6/14/23 22:52 CMR 0.065 0.698 6/14/23 22:52 CMR 1.1 0.698 6/14/23 22:52 CMR 0.10 0.698 6/14/23 22:52 CMR 0.17 0.698 6/14/23 22:52 CMR 0.11 0.698 6/14/23 22:52 CMR 0.082 0.698 6/14/23 22:52 CMR 0.16 0.698 6/14/23 22:52 CMR 0.057 0.698 6/14/23 22:52 CMR 0.073 0.698 6/14/23 22:52 CMR 0.20 0.698 6/14/23 22:52 CMR 0.16 0.698 6/14/23 22:52 CMR 0.12 0.698 6/14/23 22:52 CMR 0.12 0.698 6/14/23 22:52 CMR 0.14 0.698 6/14/23 22:52 CMR 0.17 0.698 6/14/23 22:52 CMR 0.12 0.698 6/14/23 22:52 CMR 0.13 0.698 6/14/23 22:52 CMR 0.11 0.698 6/14/23 22:52 CMR 0.10 0.698 6/14/23 22:52 CMR 0.11 0.698 6/14/23 22:52 CMR 0.087 0.698 6/14/23 22:52 CMR 0.082 0.698 6/14/23 22:52 CMR 0.081 0.698 6/14/23 22:52 CMR 0.24 0.698 6/14/23 22:52 CMR 0.10 0.698 6/14/23 22:52 CMR 3.3 2 6/15/23 22:30 CMR 0.64 0.698 6/14/23 22:52 CMR 0.088 0.698 6/14/23 22:52 CMR 0.11 0.698 6/14/23 22:52 CMR 0.091 0.698 6/14/23 22:52 CMR 0.31 0.698 6/14/23 22:52 CMR 0.64 0.698 6/14/23 22:52 CMR 0.071 0.698 6/14/23 22:52 CMR 0.59 0.698 6/14/23 22:52 CMR 0.097 0.698 6/14/23 22:52 CMR 0.56 0.698 6/14/23 22:52 CMR 0.076 0.698 6/14/23 22:52 CMR 0.14 0.698 6/14/23 22:52 CMR 0.53 0.698 6/14/23 22:52 CMR 0.078 0.698 6/14/23 22:52 CMR Page 29 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29.25 Field Sample #: IA-14 Canister ID: 1139 Final Vacuum(in Hg): -8.25 Sample ID: 23F1309-12 Canister Size: 6 liter Receipt Vacuum(in Hg): -7.8 Sample Matrix: Indoor air Flow Controller ID: 3532 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:46 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/14/23 22:52 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/14/23 22:52 CMR Tetrahydrofuran 35 1.0 0.16 100 2.9 0.48 2 6/15/23 22:30 CMR Toluene 33 0.035 0.020 120 0.13 0.075 0.698 6/14/23 22:52 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 22:52 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 22:52 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 22:52 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 22:52 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 22:52 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.063 0.14 0.039 J 0.49 1.1 0.30 0.698 6/14/23 22:52 CMR 1,2,4-Trimethylbenzene 0.63 0.035 0.015 3.1 0.17 0.076 0.698 6/14/23 22:52 CMR 1,3,5-Trimethylbenzene 0.15 0.035 0.018 0.73 0.17 0.091 0.698 6/14/23 22:52 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 22:52 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 22:52 CMR m&p-Xylene 4.9 0.070 0.039 21 0.30 0.17 0.698 6/14/23 22:52 CMR o-Xylene 1.7 0.035 0.018 7.2 0.15 0.078 0.698 6/14/23 22:52 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 98.4 70-130 6/14/23 22:52 4-Bromofluorobenzene (1) 96.1 70-130 6/15/23 22:30 Page 30 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-13 Canister ID: 2001 Sample ID: 23F1309-13 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3424 Sampled: 6/4/2023 09:50 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -8 Receipt Vacuum(in Hg): -8.0 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 140 4.0 2.4 E 330 9.5 Benzene 0.24 0.035 0.026 0.76 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 11 1.4 0.37 L-05 32 4.1 Carbon Disulfide 0.38 0.35 0.032 1.2 1.1 Carbon Tetrachloride 0.077 0.035 0.028 0.49 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.19 0.035 0.031 0.51 0.092 Chloroform 0.053 0.035 0.033 0.26 0.17 Chloromethane 0.60 0.070 0.028 1.2 0.14 Cyclohexane 0.36 0.035 0.021 1.2 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.56 0.035 0.034 2.8 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.065 0.035 0.032 0.26 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene 0.066 0.035 0.019 0.30 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 36 4.0 1.8 68 7.5 Ethyl Acetate 0.63 0.35 0.18 2.3 1.3 Ethylbenzene 1.2 0.035 0.020 5.3 0.15 4-Ethyltoluene 0.10 0.035 0.021 0.49 0.17 Heptane 1.5 0.035 0.022 6.2 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 1.8 1.4 0.18 6.3 4.9 2-Hexanone (MBK) 0.19 0.14 0.017 0.77 0.57 Isopropanol 2.6 1.4 0.24 6.5 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.34 0.035 0.019 1.4 0.14 Naphthalene 0.077 0.035 0.026 L-05, V-06, 0.40 0.18 Z-01 Propene 1.3 1.4 0.31 J 2.3 2.4 Styrene 0.92 0.035 0.018 3.9 0.15 5.7 2 6/15/23 22:57 CMR 0.084 0.698 6/14/23 23:23 CMR 0.16 0.698 6/14/23 23:23 CMR 0.16 0.698 6/14/23 23:23 CMR 0.25 0.698 6/14/23 23:23 CMR 0.090 0.698 6/14/23 23:23 CMR 0.065 0.698 6/14/23 23:23 CMR 1.1 0.698 6/14/23 23:23 CMR 0.10 0.698 6/14/23 23:23 CMR 0.17 0.698 6/14/23 23:23 CMR 0.11 0.698 6/14/23 23:23 CMR 0.082 0.698 6/14/23 23:23 CMR 0.16 0.698 6/14/23 23:23 CMR 0.057 0.698 6/14/23 23:23 CMR 0.073 0.698 6/14/23 23:23 CMR 0.20 0.698 6/14/23 23:23 CMR 0.16 0.698 6/14/23 23:23 CMR 0.12 0.698 6/14/23 23:23 CMR 0.12 0.698 6/14/23 23:23 CMR 0.14 0.698 6/14/23 23:23 CMR 0.17 0.698 6/14/23 23:23 CMR 0.12 0.698 6/14/23 23:23 CMR 0.13 0.698 6/14/23 23:23 CMR 0.11 0.698 6/14/23 23:23 CMR 0.10 0.698 6/14/23 23:23 CMR 0.11 0.698 6/14/23 23:23 CMR 0.087 0.698 6/14/23 23:23 CMR 0.082 0.698 6/14/23 23:23 CMR 0.081 0.698 6/14/23 23:23 CMR 0.24 0.698 6/14/23 23:23 CMR 0.10 0.698 6/14/23 23:23 CMR 3.3 2 6/15/23 22:57 CMR 0.64 0.698 6/14/23 23:23 CMR 0.088 0.698 6/14/23 23:23 CMR 0.11 0.698 6/14/23 23:23 CMR 0.091 0.698 6/14/23 23:23 CMR 0.31 0.698 6/14/23 23:23 CMR 0.64 0.698 6/14/23 23:23 CMR 0.071 0.698 6/14/23 23:23 CMR 0.59 0.698 6/14/23 23:23 CMR 0.097 0.698 6/14/23 23:23 CMR 0.56 0.698 6/14/23 23:23 CMR 0.076 0.698 6/14/23 23:23 CMR 0.14 0.698 6/14/23 23:23 CMR 0.53 0.698 6/14/23 23:23 CMR 0.078 0.698 6/14/23 23:23 CMR Page 31 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29.5 Field Sample #: IA-13 Canister ID: 2001 Final Vacuum(in Hg): -8 Sample ID: 23F1309-13 Canister Size: 6 liter Receipt Vacuum(in Hg): -8.0 Sample Matrix: Indoor air Flow Controller ID: 3424 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:50 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/14/23 23:23 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/14/23 23:23 CMR Tetrahydrofuran 34 1.0 0.16 100 2.9 0.48 2 6/15/23 22:57 CMR Toluene 32 0.035 0.020 120 0.13 0.075 0.698 6/14/23 23:23 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 23:23 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 23:23 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 23:23 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 23:23 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 23:23 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.063 0.14 0.039 J 0.48 1.1 0.30 0.698 6/14/23 23:23 CMR 1,2,4-Trimethylbenzene 0.64 0.035 0.015 3.1 0.17 0.076 0.698 6/14/23 23:23 CMR 1,3,5-Trimethylbenzene 0.15 0.035 0.018 0.73 0.17 0.091 0.698 6/14/23 23:23 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 23:23 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 23:23 CMR m&p-Xylene 4.8 0.070 0.039 21 0.30 0.17 0.698 6/14/23 23:23 CMR o-Xylene 1.7 0.035 0.018 7.3 0.15 0.078 0.698 6/14/23 23:23 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 99.2 70-130 6/14/23 23:23 4-Bromofluorobenzene (1) 96.3 70-130 6/15/23 22:57 Page 32 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-16 Canister ID: 1232 Sample ID: 23F1309-14 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3425 Sampled: 6/4/2023 09:55 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -6.25 Receipt Vacuum(in Hg): -6.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 21 1.4 0.84 50 3.3 Benzene 0.53 0.035 0.026 1.7 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 3.3 1.4 0.37 L-05 9.7 4.1 Carbon Disulfide 0.042 0.35 0.032 J 0.13 1.1 Carbon Tetrachloride 0.076 0.035 0.028 0.48 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform ND 0.035 0.033 ND 0.17 Chloromethane 0.60 0.070 0.028 1.2 0.14 Cyclohexane 0.48 0.035 0.021 1.7 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.53 0.035 0.034 2.6 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.067 0.035 0.032 0.27 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene ND 0.035 0.019 ND 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 55 1.4 0.62 E 100 2.6 Ethyl Acetate 0.52 0.35 0.18 1.9 1.3 Ethylbenzene 0.30 0.035 0.020 1.3 0.15 4-Ethyltoluene 0.029 0.035 0.021 J 0.14 0.17 Heptane 3.4 0.035 0.022 14 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.54 1.4 0.18 J 1.9 4.9 2-Hexanone (MBK) 0.12 0.14 0.017 J 0.51 0.57 Isopropanol 1.6 1.4 0.24 4.0 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.44 0.035 0.019 1.8 0.14 Naphthalene 0.048 0.035 0.026 L-05, V-06, 0.25 0.18 Z-01 Propene 0.97 1.4 0.31 J 1.7 2.4 Styrene 0.42 0.035 0.018 1.8 0.15 2.0 0.698 6/14/23 23:55 CMR 0.084 0.698 6/14/23 23:55 CMR 0.16 0.698 6/14/23 23:55 CMR 0.16 0.698 6/14/23 23:55 CMR 0.25 0.698 6/14/23 23:55 CMR 0.090 0.698 6/14/23 23:55 CMR 0.065 0.698 6/14/23 23:55 CMR 1.1 0.698 6/14/23 23:55 CMR 0.10 0.698 6/14/23 23:55 CMR 0.17 0.698 6/14/23 23:55 CMR 0.11 0.698 6/14/23 23:55 CMR 0.082 0.698 6/14/23 23:55 CMR 0.16 0.698 6/14/23 23:55 CMR 0.057 0.698 6/14/23 23:55 CMR 0.073 0.698 6/14/23 23:55 CMR 0.20 0.698 6/14/23 23:55 CMR 0.16 0.698 6/14/23 23:55 CMR 0.12 0.698 6/14/23 23:55 CMR 0.12 0.698 6/14/23 23:55 CMR 0.14 0.698 6/14/23 23:55 CMR 0.17 0.698 6/14/23 23:55 CMR 0.12 0.698 6/14/23 23:55 CMR 0.13 0.698 6/14/23 23:55 CMR 0.11 0.698 6/14/23 23:55 CMR 0.10 0.698 6/14/23 23:55 CMR 0.11 0.698 6/14/23 23:55 CMR 0.087 0.698 6/14/23 23:55 CMR 0.082 0.698 6/14/23 23:55 CMR 0.081 0.698 6/14/23 23:55 CMR 0.24 0.698 6/14/23 23:55 CMR 0.10 0.698 6/14/23 23:55 CMR 1.2 0.698 6/14/23 23:55 CMR 0.64 0.698 6/14/23 23:55 CMR 0.088 0.698 6/14/23 23:55 CMR 0.11 0.698 6/14/23 23:55 CMR 0.091 0.698 6/14/23 23:55 CMR 0.31 0.698 6/14/23 23:55 CMR 0.64 0.698 6/14/23 23:55 CMR 0.071 0.698 6/14/23 23:55 CMR 0.59 0.698 6/14/23 23:55 CMR 0.097 0.698 6/14/23 23:55 CMR 0.56 0.698 6/14/23 23:55 CMR 0.076 0.698 6/14/23 23:55 CMR 0.14 0.698 6/14/23 23:55 CMR 0.53 0.698 6/14/23 23:55 CMR 0.078 0.698 6/14/23 23:55 CMR Page 33 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: IA-16 Canister ID: 1232 Final Vacuum(in Hg): -6.25 Sample ID: 23F1309-14 Canister Size: 6 liter Receipt Vacuum(in Hg): -6.8 Sample Matrix: Indoor air Flow Controller ID: 3425 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:55 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/14/23 23:55 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/14/23 23:55 CMR Tetrahydrofuran 6.0 0.35 0.057 18 1.0 0.17 0.698 6/14/23 23:55 CMR Toluene 13 0.035 0.020 50 0.13 0.075 0.698 6/14/23 23:55 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/14/23 23:55 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/14/23 23:55 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/14/23 23:55 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/14/23 23:55 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/14/23 23:55 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.062 0.14 0.039 J 0.48 1.1 0.30 0.698 6/14/23 23:55 CMR 1,2,4-Trimethylbenzene 0.17 0.035 0.015 0.83 0.17 0.076 0.698 6/14/23 23:55 CMR 1,3,5-Trimethylbenzene 0.043 0.035 0.018 0.21 0.17 0.091 0.698 6/14/23 23:55 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/14/23 23:55 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/14/23 23:55 CMR m&p-Xylene 1.1 0.070 0.039 4.8 0.30 0.17 0.698 6/14/23 23:55 CMR o-Xylene 0.44 0.035 0.018 1.9 0.15 0.078 0.698 6/14/23 23:55 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 97.0 70-130 6/14/23 23:55 Page 34 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-17 Canister ID: 2455 Sample ID: 23F1309-15 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3257 Sampled: 6/4/2023 09:57 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -31 Final Vacuum(in Hg): -8.5 Receipt Vacuum(in Hg): -6.6 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 20 1.4 0.84 47 3.3 Benzene 0.52 0.035 0.026 1.7 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 3.2 1.4 0.37 L-05 9.6 4.1 Carbon Disulfide 0.051 0.35 0.032 J 0.16 1.1 Carbon Tetrachloride 0.078 0.035 0.028 0.49 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform ND 0.035 0.033 ND 0.17 Chloromethane 0.52 0.070 0.028 1.1 0.14 Cyclohexane 0.62 0.035 0.021 2.1 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.6 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.068 0.035 0.032 0.27 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 70 1.4 0.62 E 130 2.6 Ethyl Acetate 0.56 0.35 0.18 2.0 1.3 Ethylbenzene 0.33 0.035 0.020 1.4 0.15 4-Ethyltoluene 0.031 0.035 0.021 J 0.15 0.17 Heptane 4.9 0.035 0.022 20 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.56 1.4 0.18 J 2.0 4.9 2-Hexanone (MBK) 0.091 0.14 0.017 J 0.37 0.57 Isopropanol 1.6 1.4 0.24 4.0 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.63 0.035 0.019 2.6 0.14 Naphthalene 0.059 0.035 0.026 L-05, V-06, 0.31 0.18 Z-01 Propene 0.90 1.4 0.31 J 1.5 2.4 Styrene 0.44 0.035 0.018 1.9 0.15 2.0 0.698 6/15/23 0:27 CMR 0.084 0.698 6/15/23 0:27 CMR 0.16 0.698 6/15/23 0:27 CMR 0.16 0.698 6/15/23 0:27 CMR 0.25 0.698 6/15/23 0:27 CMR 0.090 0.698 6/15/23 0:27 CMR 0.065 0.698 6/15/23 0:27 CMR 1.1 0.698 6/15/23 0:27 CMR 0.10 0.698 6/15/23 0:27 CMR 0.17 0.698 6/15/23 0:27 CMR 0.11 0.698 6/15/23 0:27 CMR 0.082 0.698 6/15/23 0:27 CMR 0.16 0.698 6/15/23 0:27 CMR 0.057 0.698 6/15/23 0:27 CMR 0.073 0.698 6/15/23 0:27 CMR 0.20 0.698 6/15/23 0:27 CMR 0.16 0.698 6/15/23 0:27 CMR 0.12 0.698 6/15/23 0:27 CMR 0.12 0.698 6/15/23 0:27 CMR 0.14 0.698 6/15/23 0:27 CMR 0.17 0.698 6/15/23 0:27 CMR 0.12 0.698 6/15/23 0:27 CMR 0.13 0.698 6/15/23 0:27 CMR 0.11 0.698 6/15/23 0:27 CMR 0.10 0.698 6/15/23 0:27 CMR 0.11 0.698 6/15/23 0:27 CMR 0.087 0.698 6/15/23 0:27 CMR 0.082 0.698 6/15/23 0:27 CMR 0.081 0.698 6/15/23 0:27 CMR 0.24 0.698 6/15/23 0:27 CMR 0.10 0.698 6/15/23 0:27 CMR 1.2 0.698 6/15/23 0:27 CMR 0.64 0.698 6/15/23 0:27 CMR 0.088 0.698 6/15/23 0:27 CMR 0.11 0.698 6/15/23 0:27 CMR 0.091 0.698 6/15/23 0:27 CMR 0.31 0.698 6/15/23 0:27 CMR 0.64 0.698 6/15/23 0:27 CMR 0.071 0.698 6/15/23 0:27 CMR 0.59 0.698 6/15/23 0:27 CMR 0.097 0.698 6/15/23 0:27 CMR 0.56 0.698 6/15/23 0:27 CMR 0.076 0.698 6/15/23 0:27 CMR 0.14 0.698 6/15/23 0:27 CMR 0.53 0.698 6/15/23 0:27 CMR 0.078 0.698 6/15/23 0:27 CMR Page 35 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -31 Field Sample #: IA-17 Canister ID: 2455 Final Vacuum(in Hg): -8.5 Sample ID: 23F1309-15 Canister Size: 6 liter Receipt Vacuum(in Hg): -6.6 Sample Matrix: Indoor air Flow Controller ID: 3257 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 09:57 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 0:27 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 0:27 CMR Tetrahydrofuran 6.0 0.35 0.057 18 1.0 0.17 0.698 6/15/23 0:27 CMR Toluene 17 0.035 0.020 63 0.13 0.075 0.698 6/15/23 0:27 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 0:27 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 0:27 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 0:27 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 0:27 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 0:27 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.061 0.14 0.039 J 0.47 1.1 0.30 0.698 6/15/23 0:27 CMR 1,2,4-Trimethylbenzene 0.17 0.035 0.015 0.86 0.17 0.076 0.698 6/15/23 0:27 CMR 1,3,5-Trimethylbenzene 0.040 0.035 0.018 0.20 0.17 0.091 0.698 6/15/23 0:27 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 0:27 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 0:27 CMR m&p-Xylene 1.2 0.070 0.039 5.2 0.30 0.17 0.698 6/15/23 0:27 CMR o-Xylene 0.50 0.035 0.018 2.2 0.15 0.078 0.698 6/15/23 0:27 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 97.4 70-130 6/15/23 0:27 Page 36 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-18 Canister ID: 2009 Sample ID: 23F1309-16 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3256 Sampled: 6/4/2023 10:00 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -30.5 Final Vacuum(in Hg): -9 Receipt Vacuum(in Hg): -8.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 37 4.0 2.4 89 9.5 Benzene 0.25 0.035 0.026 0.79 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 56 4.0 1.1 160 12 Carbon Disulfide 0.21 0.35 0.032 J 0.64 1.1 Carbon Tetrachloride 0.077 0.035 0.028 0.48 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.040 0.035 0.031 0.11 0.092 Chloroform 0.036 0.035 0.033 0.17 0.17 Chloromethane 0.61 0.070 0.028 1.3 0.14 Cyclohexane 0.77 0.035 0.021 2.6 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.63 0.035 0.034 3.1 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.078 0.035 0.032 0.32 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene ND 0.035 0.019 ND 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 300 4.0 1.8 E 570 7.5 Ethyl Acetate 0.94 0.35 0.18 3.4 1.3 Ethylbenzene 0.93 0.035 0.020 4.1 0.15 4-Ethyltoluene 0.10 0.035 0.021 0.50 0.17 Heptane 8.5 0.035 0.022 35 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.63 1.4 0.18 J 2.2 4.9 2-Hexanone (MBK) 0.20 0.14 0.017 0.81 0.57 Isopropanol 2.6 1.4 0.24 6.3 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 2.5 0.035 0.019 10 0.14 Naphthalene 0.10 0.035 0.026 L-05, V-06, 0.53 0.18 Z-01 Propene 1.0 1.4 0.31 J 1.8 2.4 Styrene 0.90 0.035 0.018 3.8 0.15 5.7 2 6/15/23 23:23 CMR 0.084 0.698 6/15/23 0:58 CMR 0.16 0.698 6/15/23 0:58 CMR 0.16 0.698 6/15/23 0:58 CMR 0.25 0.698 6/15/23 0:58 CMR 0.090 0.698 6/15/23 0:58 CMR 0.065 0.698 6/15/23 0:58 CMR 3.1 2 6/15/23 23:23 CMR 0.10 0.698 6/15/23 0:58 CMR 0.17 0.698 6/15/23 0:58 CMR 0.11 0.698 6/15/23 0:58 CMR 0.082 0.698 6/15/23 0:58 CMR 0.16 0.698 6/15/23 0:58 CMR 0.057 0.698 6/15/23 0:58 CMR 0.073 0.698 6/15/23 0:58 CMR 0.20 0.698 6/15/23 0:58 CMR 0.16 0.698 6/15/23 0:58 CMR 0.12 0.698 6/15/23 0:58 CMR 0.12 0.698 6/15/23 0:58 CMR 0.14 0.698 6/15/23 0:58 CMR 0.17 0.698 6/15/23 0:58 CMR 0.12 0.698 6/15/23 0:58 CMR 0.13 0.698 6/15/23 0:58 CMR 0.11 0.698 6/15/23 0:58 CMR 0.10 0.698 6/15/23 0:58 CMR 0.11 0.698 6/15/23 0:58 CMR 0.087 0.698 6/15/23 0:58 CMR 0.082 0.698 6/15/23 0:58 CMR 0.081 0.698 6/15/23 0:58 CMR 0.24 0.698 6/15/23 0:58 CMR 0.10 0.698 6/15/23 0:58 CMR 3.3 2 6/15/23 23:23 CMR 0.64 0.698 6/15/23 0:58 CMR 0.088 0.698 6/15/23 0:58 CMR 0.11 0.698 6/15/23 0:58 CMR 0.091 0.698 6/15/23 0:58 CMR 0.31 0.698 6/15/23 0:58 CMR 0.64 0.698 6/15/23 0:58 CMR 0.071 0.698 6/15/23 0:58 CMR 0.59 0.698 6/15/23 0:58 CMR 0.097 0.698 6/15/23 0:58 CMR 0.56 0.698 6/15/23 0:58 CMR 0.076 0.698 6/15/23 0:58 CMR 0.14 0.698 6/15/23 0:58 CMR 0.53 0.698 6/15/23 0:58 CMR 0.078 0.698 6/15/23 0:58 CMR Page 37 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-18 Sample ID: 23F1309-16 Sample Matrix: Indoor air Sampled: 6/4/2023 10:00 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2009 Canister Size: 6 liter Flow Controller ID: 3256 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -30.5 Final Vacuum(in Hg): -9 Receipt Vacuum(in Hg): -8.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 0:58 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 0:58 CMR Tetrahydrofuran 16 0.35 0.057 48 1.0 0.17 0.698 6/15/23 0:58 CMR Toluene 29 0.035 0.020 110 0.13 0.075 0.698 6/15/23 0:58 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 0:58 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 0:58 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 0:58 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 0:58 CMR Trichlorofluoromethane (Freon 11) 0.20 0.14 0.041 1.1 0.78 0.23 0.698 6/15/23 0:58 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.065 0.14 0.039 J 0.50 1.1 0.30 0.698 6/15/23 0:58 CMR 1,2,4-Trimethylbenzene 0.63 0.035 0.015 3.1 0.17 0.076 0.698 6/15/23 0:58 CMR 1,3,5-Trimethylbenzene 0.19 0.035 0.018 0.96 0.17 0.091 0.698 6/15/23 0:58 CMR Vinyl Acetate 2.1 0.70 0.19 7.3 2.5 0.66 0.698 6/15/23 0:58 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 0:58 CMR m&p-Xylene 3.5 0.070 0.039 15 0.30 0.17 0.698 6/15/23 0:58 CMR o-Xylene 1.2 0.035 0.018 5.2 0.15 0.078 0.698 6/15/23 0:58 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 98.6 70-130 6/15/23 0:58 4-Bromofluorobenzene (1) 95.4 70-130 6/15/23 23:23 Page 38 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-19 Canister ID: 1884 Sample ID: 23F1309-17 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3494 Sampled: 6/4/2023 10:07 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -7.75 Receipt Vacuum(in Hg): -7.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 33 4.0 2.4 79 9.5 Benzene 0.22 0.035 0.026 0.70 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 31 4.0 1.1 93 12 Carbon Disulfide 0.21 0.35 0.032 J 0.64 1.1 Carbon Tetrachloride 0.069 0.035 0.028 0.43 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.043 0.035 0.031 0.11 0.092 Chloroform 0.038 0.035 0.033 0.18 0.17 Chloromethane 0.59 0.070 0.028 1.2 0.14 Cyclohexane 0.56 0.035 0.021 1.9 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.51 0.035 0.034 2.5 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.069 0.035 0.032 0.28 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropene ND 0.035 0.019 ND 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 340 4.0 1.8 E 640 7.5 Ethyl Acetate 0.84 0.35 0.18 3.0 1.3 Ethylbenzene 0.74 0.035 0.020 3.2 0.15 4-Ethyltoluene 0.15 0.035 0.021 0.74 0.17 Heptane 5.8 0.035 0.022 24 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.48 1.4 0.18 J 1.7 4.9 2-Hexanone (MBK) 0.19 0.14 0.017 0.79 0.57 Isopropanol 2.4 1.4 0.24 5.8 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 2.4 0.035 0.019 9.9 0.14 Naphthalene 0.11 0.035 0.026 L-05, V-06, 0.57 0.18 Z-01 Propene 0.82 1.4 0.31 J 1.4 2.4 Styrene 0.78 0.035 0.018 3.3 0.15 5.7 2 6/15/23 23:49 CMR 0.084 0.698 6/15/23 1:29 CMR 0.16 0.698 6/15/23 1:29 CMR 0.16 0.698 6/15/23 1:29 CMR 0.25 0.698 6/15/23 1:29 CMR 0.090 0.698 6/15/23 1:29 CMR 0.065 0.698 6/15/23 1:29 CMR 3.1 2 6/15/23 23:49 CMR 0.10 0.698 6/15/23 1:29 CMR 0.17 0.698 6/15/23 1:29 CMR 0.11 0.698 6/15/23 1:29 CMR 0.082 0.698 6/15/23 1:29 CMR 0.16 0.698 6/15/23 1:29 CMR 0.057 0.698 6/15/23 1:29 CMR 0.073 0.698 6/15/23 1:29 CMR 0.20 0.698 6/15/23 1:29 CMR 0.16 0.698 6/15/23 1:29 CMR 0.12 0.698 6/15/23 1:29 CMR 0.12 0.698 6/15/23 1:29 CMR 0.14 0.698 6/15/23 1:29 CMR 0.17 0.698 6/15/23 1:29 CMR 0.12 0.698 6/15/23 1:29 CMR 0.13 0.698 6/15/23 1:29 CMR 0.11 0.698 6/15/23 1:29 CMR 0.10 0.698 6/15/23 1:29 CMR 0.11 0.698 6/15/23 1:29 CMR 0.087 0.698 6/15/23 1:29 CMR 0.082 0.698 6/15/23 1:29 CMR 0.081 0.698 6/15/23 1:29 CMR 0.24 0.698 6/15/23 1:29 CMR 0.10 0.698 6/15/23 1:29 CMR 3.3 2 6/15/23 23:49 CMR 0.64 0.698 6/15/23 1:29 CMR 0.088 0.698 6/15/23 1:29 CMR 0.11 0.698 6/15/23 1:29 CMR 0.091 0.698 6/15/23 1:29 CMR 0.31 0.698 6/15/23 1:29 CMR 0.64 0.698 6/15/23 1:29 CMR 0.071 0.698 6/15/23 1:29 CMR 0.59 0.698 6/15/23 1:29 CMR 0.097 0.698 6/15/23 1:29 CMR 0.56 0.698 6/15/23 1:29 CMR 0.076 0.698 6/15/23 1:29 CMR 0.14 0.698 6/15/23 1:29 CMR 0.53 0.698 6/15/23 1:29 CMR 0.078 0.698 6/15/23 1:29 CMR Page 39 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-19 Sample ID: 23F1309-17 Sample Matrix: Indoor air Sampled: 6/4/2023 10:07 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1884 Canister Size: 6 liter Flow Controller ID: 3494 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -7.75 Receipt Vacuum(in Hg): -7.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 1:29 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 1:29 CMR Tetrahydrofuran 17 0.35 0.057 50 1.0 0.17 0.698 6/15/23 1:29 CMR Toluene 21 0.035 0.020 80 0.13 0.075 0.698 6/15/23 1:29 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 1:29 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 1:29 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 1:29 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 1:29 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 1:29 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.068 0.14 0.039 J 0.52 1.1 0.30 0.698 6/15/23 1:29 CMR 1,2,4-Trimethylbenzene 0.82 0.035 0.015 4.0 0.17 0.076 0.698 6/15/23 1:29 CMR 1,3,5-Trimethylbenzene 0.28 0.035 0.018 1.4 0.17 0.091 0.698 6/15/23 1:29 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 1:29 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 1:29 CMR m&p-Xylene 2.7 0.070 0.039 12 0.30 0.17 0.698 6/15/23 1:29 CMR o-Xylene 1.0 0.035 0.018 4.4 0.15 0.078 0.698 6/15/23 1:29 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 99.7 70-130 6/15/23 1:29 4-Bromofluorobenzene (1) 96.9 70-130 6/15/23 23:49 Page 40 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-23 Canister ID: 1080 Sample ID: 23F1309-19 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3402 Sampled: 6/4/2023 10:15 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -7.75 Receipt Vacuum(in Hg): -7.5 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 91 8.0 4.8 210 19 Benzene 0.15 0.035 0.026 0.47 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane 0.093 0.035 0.023 0.36 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 7.4 1.4 0.37 L-05 22 4.1 Carbon Disulfide 0.033 0.35 0.032 J 0.10 1.1 Carbon Tetrachloride 0.080 0.035 0.028 0.50 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform 0.033 0.035 0.033 J 0.16 0.17 Chloromethane 0.60 0.070 0.028 1.2 0.14 Cyclohexane 1.2 0.035 0.021 4.2 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.5 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane ND 0.035 0.032 ND 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane 0.032 0.035 0.019 J 0.15 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 130 8.0 3.5 240 15 Ethyl Acetate ND 0.35 0.18 ND 1.3 Ethylbenzene 1.6 0.035 0.020 7.1 0.15 4-Ethyltoluene 0.036 0.035 0.021 0.17 0.17 Heptane 3.3 0.035 0.022 13 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 4.1 1.4 0.18 15 4.9 2-Hexanone (MBK) 0.21 0.14 0.017 0.85 0.57 Isopropanol 8.4 1.4 0.24 21 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 1.2 0.035 0.019 5.1 0.14 Naphthalene 0.051 0.035 0.026 L-05, V-06, 0.27 0.18 Z-01 Propene 0.63 1.4 0.31 J 1.1 2.4 Styrene 4.8 0.035 0.018 20 0.15 11 4 6/16/23 12:36 CMR 0.084 0.698 6/15/23 2:01 CMR 0.16 0.698 6/15/23 2:01 CMR 0.16 0.698 6/15/23 2:01 CMR 0.25 0.698 6/15/23 2:01 CMR 0.090 0.698 6/15/23 2:01 CMR 0.065 0.698 6/15/23 2:01 CMR 1.1 0.698 6/15/23 2:01 CMR 0.10 0.698 6/15/23 2:01 CMR 0.17 0.698 6/15/23 2:01 CMR 0.11 0.698 6/15/23 2:01 CMR 0.082 0.698 6/15/23 2:01 CMR 0.16 0.698 6/15/23 2:01 CMR 0.057 0.698 6/15/23 2:01 CMR 0.073 0.698 6/15/23 2:01 CMR 0.20 0.698 6/15/23 2:01 CMR 0.16 0.698 6/15/23 2:01 CMR 0.12 0.698 6/15/23 2:01 CMR 0.12 0.698 6/15/23 2:01 CMR 0.14 0.698 6/15/23 2:01 CMR 0.17 0.698 6/15/23 2:01 CMR 0.12 0.698 6/15/23 2:01 CMR 0.13 0.698 6/15/23 2:01 CMR 0.11 0.698 6/15/23 2:01 CMR 0.10 0.698 6/15/23 2:01 CMR 0.11 0.698 6/15/23 2:01 CMR 0.087 0.698 6/15/23 2:01 CMR 0.082 0.698 6/15/23 2:01 CMR 0.081 0.698 6/15/23 2:01 CMR 0.24 0.698 6/15/23 2:01 CMR 0.10 0.698 6/15/23 2:01 CMR 6.6 4 6/16/23 12:36 CMR 0.64 0.698 6/15/23 2:01 CMR 0.088 0.698 6/15/23 2:01 CMR 0.11 0.698 6/15/23 2:01 CMR 0.091 0.698 6/15/23 2:01 CMR 0.31 0.698 6/15/23 2:01 CMR 0.64 0.698 6/15/23 2:01 CMR 0.071 0.698 6/15/23 2:01 CMR 0.59 0.698 6/15/23 2:01 CMR 0.097 0.698 6/15/23 2:01 CMR 0.56 0.698 6/15/23 2:01 CMR 0.076 0.698 6/15/23 2:01 CMR 0.14 0.698 6/15/23 2:01 CMR 0.53 0.698 6/15/23 2:01 CMR 0.078 0.698 6/15/23 2:01 CMR Page 41 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -30 Field Sample #: IA-23 Canister ID: 1080 Final Vacuum(in Hg): -7.75 Sample ID: 23F1309-19 Canister Size: 6 liter Receipt Vacuum(in Hg): -7.5 Sample Matrix: Indoor air Flow Controller ID: 3402 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 10:15 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 2:01 CMR Tetrachloroethylene 0.031 0.035 0.027 J 0.21 0.24 0.18 0.698 6/15/23 2:01 CMR Tetrahydrofuran 67 2.0 0.33 200 5.9 0.97 4 6/16/23 12:36 CMR Toluene 180 0.20 0.11 690 0.75 0.43 4 6/16/23 12:36 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 2:01 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 2:01 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 2:01 CMR Trichloroethylene 0.064 0.035 0.024 0.34 0.19 0.13 0.698 6/15/23 2:01 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 2:01 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.061 0.14 0.039 J 0.47 1.1 0.30 0.698 6/15/23 2:01 CMR 1,2,4-Trimethylbenzene 0.18 0.035 0.015 0.88 0.17 0.076 0.698 6/15/23 2:01 CMR 1,3,5-Trimethylbenzene 0.046 0.035 0.018 0.23 0.17 0.091 0.698 6/15/23 2:01 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 2:01 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 2:01 CMR m&p-Xylene 7.3 0.070 0.039 32 0.30 0.17 0.698 6/15/23 2:01 CMR o-Xylene 2.7 0.035 0.018 12 0.15 0.078 0.698 6/15/23 2:01 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 99.4 70-130 6/15/23 2:01 4-Bromofluorobenzene (1) 92.7 70-130 6/16/23 12:36 Page 42 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-15 Canister ID: 1730 Sample ID: 23F1309-20 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3090 Sampled: 6/4/2023 10:22 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29.25 Final Vacuum(in Hg): -8.5 Receipt Vacuum(in Hg): -8.6 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone 56 8.0 4.8 130 19 Benzene 0.27 0.035 0.026 0.85 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 9.4 1.4 0.37 L-05 28 4.1 Carbon Disulfide 0.054 0.35 0.032 J 0.17 1.1 Carbon Tetrachloride 0.079 0.035 0.028 0.50 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane 0.035 0.035 0.031 0.092 0.092 Chloroform ND 0.035 0.033 ND 0.17 Chloromethane 0.60 0.070 0.028 1.2 0.14 Cyclohexane 0.44 0.035 0.021 1.5 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.53 0.035 0.034 2.6 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.067 0.035 0.032 0.27 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane 0.023 0.035 0.019 J 0.11 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane 0.19 0.35 0.029 J 0.67 1.3 Ethanol 60 8.0 3.5 110 15 Ethyl Acetate 0.27 0.35 0.18 J 0.97 1.3 Ethylbenzene 0.69 0.035 0.020 3.0 0.15 4-Ethyltoluene 0.040 0.035 0.021 0.20 0.17 Heptane 1.3 0.035 0.022 5.4 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 1.5 1.4 0.18 5.4 4.9 2-Hexanone (MBK) 0.16 0.14 0.017 0.67 0.57 Isopropanol 3.6 1.4 0.24 9.0 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.57 0.035 0.019 2.3 0.14 Naphthalene 0.075 0.035 0.026 L-05, V-06, 0.39 0.18 Z-01 Propene 0.91 1.4 0.31 J 1.6 2.4 Styrene 1.5 0.035 0.018 6.4 0.15 11 4 6/16/23 13:01 CMR 0.084 0.698 6/15/23 2:32 CMR 0.16 0.698 6/15/23 2:32 CMR 0.16 0.698 6/15/23 2:32 CMR 0.25 0.698 6/15/23 2:32 CMR 0.090 0.698 6/15/23 2:32 CMR 0.065 0.698 6/15/23 2:32 CMR 1.1 0.698 6/15/23 2:32 CMR 0.10 0.698 6/15/23 2:32 CMR 0.17 0.698 6/15/23 2:32 CMR 0.11 0.698 6/15/23 2:32 CMR 0.082 0.698 6/15/23 2:32 CMR 0.16 0.698 6/15/23 2:32 CMR 0.057 0.698 6/15/23 2:32 CMR 0.073 0.698 6/15/23 2:32 CMR 0.20 0.698 6/15/23 2:32 CMR 0.16 0.698 6/15/23 2:32 CMR 0.12 0.698 6/15/23 2:32 CMR 0.12 0.698 6/15/23 2:32 CMR 0.14 0.698 6/15/23 2:32 CMR 0.17 0.698 6/15/23 2:32 CMR 0.12 0.698 6/15/23 2:32 CMR 0.13 0.698 6/15/23 2:32 CMR 0.11 0.698 6/15/23 2:32 CMR 0.10 0.698 6/15/23 2:32 CMR 0.11 0.698 6/15/23 2:32 CMR 0.087 0.698 6/15/23 2:32 CMR 0.082 0.698 6/15/23 2:32 CMR 0.081 0.698 6/15/23 2:32 CMR 0.24 0.698 6/15/23 2:32 CMR 0.10 0.698 6/15/23 2:32 CMR 6.6 4 6/16/23 13:01 CMR 0.64 0.698 6/15/23 2:32 CMR 0.088 0.698 6/15/23 2:32 CMR 0.11 0.698 6/15/23 2:32 CMR 0.091 0.698 6/15/23 2:32 CMR 0.31 0.698 6/15/23 2:32 CMR 0.64 0.698 6/15/23 2:32 CMR 0.071 0.698 6/15/23 2:32 CMR 0.59 0.698 6/15/23 2:32 CMR 0.097 0.698 6/15/23 2:32 CMR 0.56 0.698 6/15/23 2:32 CMR 0.076 0.698 6/15/23 2:32 CMR 0.14 0.698 6/15/23 2:32 CMR 0.53 0.698 6/15/23 2:32 CMR 0.078 0.698 6/15/23 2:32 CMR Page 43 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29.25 Field Sample #: IA-15 Canister ID: 1730 Final Vacuum(in Hg): -8.5 Sample ID: 23F1309-20 Canister Size: 6 liter Receipt Vacuum(in Hg): -8.6 Sample Matrix: Indoor air Flow Controller ID: 3090 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 10:22 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 2:32 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 2:32 CMR Tetrahydrofuran 57 2.0 0.33 170 5.9 0.97 4 6/16/23 13:01 CMR Toluene 50 0.20 0.11 190 0.75 0.43 4 6/16/23 13:01 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 2:32 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 2:32 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 2:32 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 2:32 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 2:32 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.065 0.14 0.039 J 0.50 1.1 0.30 0.698 6/15/23 2:32 CMR 1,2,4-Trimethylbenzene 0.27 0.035 0.015 1.3 0.17 0.076 0.698 6/15/23 2:32 CMR 1,3,5-Trimethylbenzene 0.058 0.035 0.018 0.28 0.17 0.091 0.698 6/15/23 2:32 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 2:32 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 2:32 CMR m&p-Xylene 3.0 0.070 0.039 13 0.30 0.17 0.698 6/15/23 2:32 CMR o-Xylene 1.1 0.035 0.018 5.0 0.15 0.078 0.698 6/15/23 2:32 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 92.7 70-130 6/16/23 13:01 4-Bromofluorobenzene (1) 97.6 70-130 6/15/23 2:32 Page 44 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-24 Sample ID: 23F1309-21 Sample Matrix: Indoor air Sampled: 6/4/2023 10:33 Sample Description/Location: Sub Description/Location: Canister ID: 1931 Canister Size: 6 liter Flow Controller ID: 3469 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -7 Receipt Vacuum(in Hg): -8.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 9.3 1.4 0.84 22 3.3 2.0 0.698 6/15/23 3:04 CMR Benzene 0.20 0.035 0.026 0.64 0.11 0.084 0.698 6/15/23 3:04 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/15/23 3:04 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/15/23 3:04 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/15/23 3:04 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/15/23 3:04 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/15/23 3:04 CMR 2-Butanone (MEK) 3.6 1.4 0.37 L-05 11 4.1 1.1 0.698 6/15/23 3:04 CMR Carbon Disulfide ND 0.35 0.032 ND 1.1 0.10 0.698 6/15/23 3:04 CMR Carbon Tetrachloride 0.077 0.035 0.028 0.49 0.22 0.17 0.698 6/15/23 3:04 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/15/23 3:04 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.082 0.698 6/15/23 3:04 CMR Chloroform ND 0.035 0.033 ND 0.17 0.16 0.698 6/15/23 3:04 CMR Chloromethane 0.54 0.070 0.028 1.1 0.14 0.057 0.698 6/15/23 3:04 CMR Cyclohexane 0.029 0.035 0.021 J 0.098 0.12 0.073 0.698 6/15/23 3:04 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/15/23 3:04 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/15/23 3:04 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/15/23 3:04 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/15/23 3:04 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/15/23 3:04 CMR Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.6 0.17 0.17 0.698 6/15/23 3:04 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/15/23 3:04 CMR 1,2-Dichloroethane ND 0.035 0.032 ND 0.14 0.13 0.698 6/15/23 3:04 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 3:04 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/15/23 3:04 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 3:04 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/15/23 3:04 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/15/23 3:04 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/15/23 3:04 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/15/23 3:04 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.698 6/15/23 3:04 CMR Ethanol 9.1 1.4 0.62 17 2.6 1.2 0.698 6/15/23 3:04 CMR Ethyl Acetate 0.27 0.35 0.18 J 0.97 1.3 0.64 0.698 6/15/23 3:04 CMR Ethylbenzene 0.066 0.035 0.020 0.28 0.15 0.088 0.698 6/15/23 3:04 CMR 4-Ethyltoluene ND 0.035 0.021 ND 0.17 0.11 0.698 6/15/23 3:04 CMR Heptane 0.066 0.035 0.022 0.27 0.14 0.091 0.698 6/15/23 3:04 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/15/23 3:04 CMR Hexane ND 1.4 0.18 ND 4.9 0.64 0.698 6/15/23 3:04 CMR 2-Hexanone (MBK) 0.10 0.14 0.017 J 0.41 0.57 0.071 0.698 6/15/23 3:04 CMR Isopropanol 0.47 1.4 0.24 J 1.2 3.4 0.59 0.698 6/15/23 3:04 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/15/23 3:04 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/15/23 3:04 CMR 4-Methyl-2-pentanone (MIBK) 0.055 0.035 0.019 0.23 0.14 0.076 0.698 6/15/23 3:04 CMR Naphthalene ND 0.035 0.026 Z-01 ND 0.18 0.14 0.698 6/15/23 3:04 CMR Propene 0.50 1.4 0.31 J 0.87 2.4 0.53 0.698 6/15/23 3:04 CMR Styrene 0.23 0.035 0.018 0.98 0.15 0.078 0.698 6/15/23 3:04 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 3:04 CMR Page 45 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-24 Sample ID: 23F1309-21 Sample Matrix: Indoor air Sampled: 6/4/2023 10:33 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1931 Canister Size: 6 liter Flow Controller ID: 3469 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -7 Receipt Vacuum(in Hg): -8.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 3:04 CMR Tetrahydrofuran 7.2 0.35 0.057 21 1.0 0.17 0.698 6/15/23 3:04 CMR Toluene 1.2 0.035 0.020 4.7 0.13 0.075 0.698 6/15/23 3:04 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 3:04 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 3:04 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 3:04 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 3:04 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 3:04 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.066 0.14 0.039 J 0.50 1.1 0.30 0.698 6/15/23 3:04 CMR 1,2,4-Trimethylbenzene 0.057 0.035 0.015 0.28 0.17 0.076 0.698 6/15/23 3:04 CMR 1,3,5-Trimethylbenzene ND 0.035 0.018 ND 0.17 0.091 0.698 6/15/23 3:04 CMR Vinyl Acetate 0.98 0.70 0.19 3.4 2.5 0.66 0.698 6/15/23 3:04 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 3:04 CMR m&p-Xylene 0.19 0.070 0.039 0.83 0.30 0.17 0.698 6/15/23 3:04 CMR o-Xylene 0.093 0.035 0.018 0.40 0.15 0.078 0.698 6/15/23 3:04 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 96.2 % REC Limits 70-130 6/15/23 3:04 Page 46 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-25 Sample ID: 23F1309-22 Sample Matrix: Indoor air Sampled: 6/4/2023 10:38 Sample Description/Location: Sub Description/Location: Canister ID: 1987 Canister Size: 6 liter Flow Controller ID: 3265 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -6.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 14 1.4 0.84 33 3.3 2.0 0.698 6/15/23 3:35 CMR Benzene 0.17 0.035 0.026 0.55 0.11 0.084 0.698 6/15/23 3:35 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/15/23 3:35 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/15/23 3:35 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/15/23 3:35 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/15/23 3:35 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/15/23 3:35 CMR 2-Butanone (MEK) 3.8 1.4 0.37 L-05 11 4.1 1.1 0.698 6/15/23 3:35 CMR Carbon Disulfide ND 0.35 0.032 ND 1.1 0.10 0.698 6/15/23 3:35 CMR Carbon Tetrachloride 0.080 0.035 0.028 0.50 0.22 0.17 0.698 6/15/23 3:35 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/15/23 3:35 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.082 0.698 6/15/23 3:35 CMR Chloroform ND 0.035 0.033 ND 0.17 0.16 0.698 6/15/23 3:35 CMR Chloromethane 0.60 0.070 0.028 1.2 0.14 0.057 0.698 6/15/23 3:35 CMR Cyclohexane 0.033 0.035 0.021 J 0.12 0.12 0.073 0.698 6/15/23 3:35 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/15/23 3:35 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/15/23 3:35 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/15/23 3:35 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/15/23 3:35 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/15/23 3:35 CMR Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.6 0.17 0.17 0.698 6/15/23 3:35 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/15/23 3:35 CMR 1,2-Dichloroethane ND 0.035 0.032 ND 0.14 0.13 0.698 6/15/23 3:35 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 3:35 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/15/23 3:35 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 3:35 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/15/23 3:35 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/15/23 3:35 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/15/23 3:35 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/15/23 3:35 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.698 6/15/23 3:35 CMR Ethanol 7.6 1.4 0.62 14 2.6 1.2 0.698 6/15/23 3:35 CMR Ethyl Acetate ND 0.35 0.18 ND 1.3 0.64 0.698 6/15/23 3:35 CMR Ethylbenzene 0.18 0.035 0.020 0.78 0.15 0.088 0.698 6/15/23 3:35 CMR 4-Ethyltoluene 0.031 0.035 0.021 J 0.15 0.17 0.11 0.698 6/15/23 3:35 CMR Heptane 0.057 0.035 0.022 0.23 0.14 0.091 0.698 6/15/23 3:35 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/15/23 3:35 CMR Hexane ND 1.4 0.18 ND 4.9 0.64 0.698 6/15/23 3:35 CMR 2-Hexanone (MBK) 0.084 0.14 0.017 J 0.35 0.57 0.071 0.698 6/15/23 3:35 CMR Isopropanol 0.57 1.4 0.24 J 1.4 3.4 0.59 0.698 6/15/23 3:35 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/15/23 3:35 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/15/23 3:35 CMR 4-Methyl-2-pentanone (MIBK) 0.061 0.035 0.019 0.25 0.14 0.076 0.698 6/15/23 3:35 CMR Naphthalene ND 0.035 0.026 Z-01 ND 0.18 0.14 0.698 6/15/23 3:35 CMR Propene 0.39 1.4 0.31 J 0.67 2.4 0.53 0.698 6/15/23 3:35 CMR Styrene 0.15 0.035 0.018 0.66 0.15 0.078 0.698 6/15/23 3:35 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 3:35 CMR Page 47 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-25 Sample ID: 23F1309-22 Sample Matrix: Indoor air Sampled: 6/4/2023 10:3 8 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1987 Canister Size: 6 liter Flow Controller ID: 3265 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -6 Receipt Vacuum(in Hg): -6.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 3:35 CMR Tetrahydrofuran 14 0.35 0.057 40 1.0 0.17 0.698 6/15/23 3:35 CMR Toluene 7.6 0.035 0.020 29 0.13 0.075 0.698 6/15/23 3:35 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 3:35 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 3:35 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 3:35 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 3:35 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 3:35 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.062 0.14 0.039 J 0.48 1.1 0.30 0.698 6/15/23 3:35 CMR 1,2,4-Trimethylbenzene 0.19 0.035 0.015 0.92 0.17 0.076 0.698 6/15/23 3:35 CMR 1,3,5-Trimethylbenzene 0.050 0.035 0.018 0.25 0.17 0.091 0.698 6/15/23 3:35 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 3:35 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 3:35 CMR m&p-Xylene 0.70 0.070 0.039 3.0 0.30 0.17 0.698 6/15/23 3:35 CMR o-Xylene 0.30 0.035 0.018 1.3 0.15 0.078 0.698 6/15/23 3:35 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 96.2 % REC Limits 70-130 6/15/23 3:35 Page 48 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-25 DUP Sample ID: 23F1309-23 Sample Matrix: Indoor air Sampled: 6/4/2023 10:38 Sample Description/Location: Sub Description/Location: Canister ID: 2041 Canister Size: 6 liter Flow Controller ID: 3458 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -7.75 Receipt Vacuum(in Hg): -7.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 13 1.4 0.84 32 3.3 2.0 0.698 6/15/23 4:06 CMR Benzene 0.15 0.035 0.026 0.47 0.11 0.084 0.698 6/15/23 4:06 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/15/23 4:06 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/15/23 4:06 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/15/23 4:06 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/15/23 4:06 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/15/23 4:06 CMR 2-Butanone (MEK) 3.8 1.4 0.37 L-05 11 4.1 1.1 0.698 6/15/23 4:06 CMR Carbon Disulfide ND 0.35 0.032 ND 1.1 0.10 0.698 6/15/23 4:06 CMR Carbon Tetrachloride 0.080 0.035 0.028 0.50 0.22 0.17 0.698 6/15/23 4:06 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/15/23 4:06 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.082 0.698 6/15/23 4:06 CMR Chloroform ND 0.035 0.033 ND 0.17 0.16 0.698 6/15/23 4:06 CMR Chloromethane 0.59 0.070 0.028 1.2 0.14 0.057 0.698 6/15/23 4:06 CMR Cyclohexane 0.040 0.035 0.021 0.14 0.12 0.073 0.698 6/15/23 4:06 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/15/23 4:06 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/15/23 4:06 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/15/23 4:06 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/15/23 4:06 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/15/23 4:06 CMR Dichlorodifluoromethane (Freon 12) 0.56 0.035 0.034 2.8 0.17 0.17 0.698 6/15/23 4:06 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/15/23 4:06 CMR 1,2-Dichloroethane ND 0.035 0.032 ND 0.14 0.13 0.698 6/15/23 4:06 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 4:06 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/15/23 4:06 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 4:06 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/15/23 4:06 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/15/23 4:06 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/15/23 4:06 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/15/23 4:06 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.698 6/15/23 4:06 CMR Ethanol 7.9 1.4 0.62 15 2.6 1.2 0.698 6/15/23 4:06 CMR Ethyl Acetate 0.18 0.35 0.18 J 0.65 1.3 0.64 0.698 6/15/23 4:06 CMR Ethylbenzene 0.18 0.035 0.020 0.77 0.15 0.088 0.698 6/15/23 4:06 CMR 4-Ethyltoluene 0.033 0.035 0.021 J 0.16 0.17 0.11 0.698 6/15/23 4:06 CMR Heptane 0.052 0.035 0.022 0.21 0.14 0.091 0.698 6/15/23 4:06 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/15/23 4:06 CMR Hexane ND 1.4 0.18 ND 4.9 0.64 0.698 6/15/23 4:06 CMR 2-Hexanone (MBK) 0.084 0.14 0.017 J 0.34 0.57 0.071 0.698 6/15/23 4:06 CMR Isopropanol 0.49 1.4 0.24 J 1.2 3.4 0.59 0.698 6/15/23 4:06 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/15/23 4:06 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/15/23 4:06 CMR 4-Methyl-2-pentanone (MIBK) 0.060 0.035 0.019 0.25 0.14 0.076 0.698 6/15/23 4:06 CMR Naphthalene ND 0.035 0.026 Z-01 ND 0.18 0.14 0.698 6/15/23 4:06 CMR Propene 0.39 1.4 0.31 J 0.67 2.4 0.53 0.698 6/15/23 4:06 CMR Styrene 0.16 0.035 0.018 0.66 0.15 0.078 0.698 6/15/23 4:06 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 4:06 CMR Page 49 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-25 DUP Sample ID: 23F1309-23 Sample Matrix: Indoor air Sampled: 6/4/2023 10:3 8 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2041 Canister Size: 6 liter Flow Controller ID: 3458 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -30 Final Vacuum(in Hg): -7.75 Receipt Vacuum(in Hg): -7.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 4:06 CMR Tetrahydrofuran 14 0.35 0.057 41 1.0 0.17 0.698 6/15/23 4:06 CMR Toluene 7.7 0.035 0.020 29 0.13 0.075 0.698 6/15/23 4:06 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 4:06 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 4:06 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 4:06 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 4:06 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 4:06 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.061 0.14 0.039 J 0.47 1.1 0.30 0.698 6/15/23 4:06 CMR 1,2,4-Trimethylbenzene 0.20 0.035 0.015 0.96 0.17 0.076 0.698 6/15/23 4:06 CMR 1,3,5-Trimethylbenzene 0.052 0.035 0.018 0.25 0.17 0.091 0.698 6/15/23 4:06 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 4:06 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 4:06 CMR m&p-Xylene 0.72 0.070 0.039 3.1 0.30 0.17 0.698 6/15/23 4:06 CMR o-Xylene 0.32 0.035 0.018 1.4 0.15 0.078 0.698 6/15/23 4:06 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 97.4 % REC Limits 70-130 6/15/23 4:06 Page 50 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-21 Sample ID: 23F1309-24 Sample Matrix: Indoor air Sampled: 6/4/2023 10:45 Sample Description/Location: Sub Description/Location: Canister ID: 1002 Canister Size: 6 liter Flow Controller ID: 3454 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29.25 Final Vacuum(in Hg): -8.25 Receipt Vacuum(in Hg): -7.6 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 17 1.4 0.84 41 3.3 2.0 0.698 6/15/23 4:37 CMR Benzene 0.21 0.035 0.026 0.66 0.11 0.084 0.698 6/15/23 4:37 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/15/23 4:37 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/15/23 4:37 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/15/23 4:37 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/15/23 4:37 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/15/23 4:37 CMR 2-Butanone (MEK) 6.5 1.4 0.37 L-05 19 4.1 1.1 0.698 6/15/23 4:37 CMR Carbon Disulfide 0.035 0.35 0.032 J 0.11 1.1 0.10 0.698 6/15/23 4:37 CMR Carbon Tetrachloride 0.077 0.035 0.028 0.48 0.22 0.17 0.698 6/15/23 4:37 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/15/23 4:37 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.082 0.698 6/15/23 4:37 CMR Chloroform ND 0.035 0.033 ND 0.17 0.16 0.698 6/15/23 4:37 CMR Chloromethane 0.56 0.070 0.028 1.1 0.14 0.057 0.698 6/15/23 4:37 CMR Cyclohexane 0.15 0.035 0.021 0.52 0.12 0.073 0.698 6/15/23 4:37 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/15/23 4:37 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/15/23 4:37 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/15/23 4:37 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/15/23 4:37 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/15/23 4:37 CMR Dichlorodifluoromethane (Freon 12) 0.53 0.035 0.034 2.6 0.17 0.17 0.698 6/15/23 4:37 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/15/23 4:37 CMR 1,2-Dichloroethane ND 0.035 0.032 ND 0.14 0.13 0.698 6/15/23 4:37 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 4:37 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/15/23 4:37 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 4:37 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/15/23 4:37 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/15/23 4:37 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/15/23 4:37 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/15/23 4:37 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.698 6/15/23 4:37 CMR Ethanol 11 1.4 0.62 21 2.6 1.2 0.698 6/15/23 4:37 CMR Ethyl Acetate 0.21 0.35 0.18 J 0.76 1.3 0.64 0.698 6/15/23 4:37 CMR Ethylbenzene 0.27 0.035 0.020 1.2 0.15 0.088 0.698 6/15/23 4:37 CMR 4-Ethyltoluene 0.038 0.035 0.021 0.19 0.17 0.11 0.698 6/15/23 4:37 CMR Heptane 0.13 0.035 0.022 0.54 0.14 0.091 0.698 6/15/23 4:37 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/15/23 4:37 CMR Hexane 0.46 1.4 0.18 J 1.6 4.9 0.64 0.698 6/15/23 4:37 CMR 2-Hexanone (MBK) 0.066 0.14 0.017 J 0.27 0.57 0.071 0.698 6/15/23 4:37 CMR Isopropanol 0.51 1.4 0.24 J 1.2 3.4 0.59 0.698 6/15/23 4:37 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/15/23 4:37 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/15/23 4:37 CMR 4-Methyl-2-pentanone (MIBK) 0.069 0.035 0.019 0.28 0.14 0.076 0.698 6/15/23 4:37 CMR Naphthalene ND 0.035 0.026 Z-01 ND 0.18 0.14 0.698 6/15/23 4:37 CMR Propene 0.64 1.4 0.31 J 1.1 2.4 0.53 0.698 6/15/23 4:37 CMR Styrene 0.089 0.035 0.018 0.38 0.15 0.078 0.698 6/15/23 4:37 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 4:37 CMR Page 51 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-21 Sample ID: 23F1309-24 Sample Matrix: Indoor air Sampled: 6/4/2023 10:45 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1002 Canister Size: 6 liter Flow Controller ID: 3454 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29.25 Final Vacuum(in Hg): -8.25 Receipt Vacuum(in Hg): -7.6 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 4:37 CMR Tetrahydrofuran 13 0.35 0.057 39 1.0 0.17 0.698 6/15/23 4:37 CMR Toluene 1.2 0.035 0.020 4.4 0.13 0.075 0.698 6/15/23 4:37 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 4:37 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 4:37 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 4:37 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 4:37 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 4:37 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.058 0.14 0.039 J 0.44 1.1 0.30 0.698 6/15/23 4:37 CMR 1,2,4-Trimethylbenzene 0.24 0.035 0.015 1.2 0.17 0.076 0.698 6/15/23 4:37 CMR 1,3,5-Trimethylbenzene 0.061 0.035 0.018 0.30 0.17 0.091 0.698 6/15/23 4:37 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 4:37 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 4:37 CMR m&p-Xylene 1.0 0.070 0.039 4.4 0.30 0.17 0.698 6/15/23 4:37 CMR o-Xylene 0.33 0.035 0.018 1.4 0.15 0.078 0.698 6/15/23 4:37 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 98.4 % REC Limits 70-130 6/15/23 4:37 Page 52 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: OA Sample ID: 23F1309-25 Sample Matrix: Indoor air Sampled: 6/4/2023 10:55 Sample Description/Location: Sub Description/Location: Canister ID: 1138 Canister Size: 6 liter Flow Controller ID: 3264 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -7 Receipt Vacuum(in Hg): -7.6 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 5.7 1.4 0.84 14 3.3 2.0 0.698 6/15/23 5:08 CMR Benzene 0.16 0.035 0.026 0.52 0.11 0.084 0.698 6/15/23 5:08 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/15/23 5:08 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/15/23 5:08 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/15/23 5:08 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/15/23 5:08 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/15/23 5:08 CMR 2-Butanone (MEK) 0.67 1.4 0.37 L-05, J 2.0 4.1 1.1 0.698 6/15/23 5:08 CMR Carbon Disulfide ND 0.35 0.032 ND 1.1 0.10 0.698 6/15/23 5:08 CMR Carbon Tetrachloride 0.075 0.035 0.028 0.47 0.22 0.17 0.698 6/15/23 5:08 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/15/23 5:08 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.082 0.698 6/15/23 5:08 CMR Chloroform ND 0.035 0.033 ND 0.17 0.16 0.698 6/15/23 5:08 CMR Chloromethane 0.61 0.070 0.028 1.3 0.14 0.057 0.698 6/15/23 5:08 CMR Cyclohexane ND 0.035 0.021 ND 0.12 0.073 0.698 6/15/23 5:08 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/15/23 5:08 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/15/23 5:08 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/15/23 5:08 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/15/23 5:08 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/15/23 5:08 CMR Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.6 0.17 0.17 0.698 6/15/23 5:08 CMR 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/15/23 5:08 CMR 1,2-Dichloroethane ND 0.035 0.032 ND 0.14 0.13 0.698 6/15/23 5:08 CMR 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 5:08 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/15/23 5:08 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 5:08 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/15/23 5:08 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/15/23 5:08 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/15/23 5:08 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/15/23 5:08 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.698 6/15/23 5:08 CMR Ethanol 4.7 1.4 0.62 8.9 2.6 1.2 0.698 6/15/23 5:08 CMR Ethyl Acetate ND 0.35 0.18 ND 1.3 0.64 0.698 6/15/23 5:08 CMR Ethylbenzene 0.057 0.035 0.020 0.25 0.15 0.088 0.698 6/15/23 5:08 CMR 4-Ethyltoluene ND 0.035 0.021 ND 0.17 0.11 0.698 6/15/23 5:08 CMR Heptane 0.085 0.035 0.022 0.35 0.14 0.091 0.698 6/15/23 5:08 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/15/23 5:08 CMR Hexane ND 1.4 0.18 ND 4.9 0.64 0.698 6/15/23 5:08 CMR 2-Hexanone (MBK) 0.031 0.14 0.017 J 0.13 0.57 0.071 0.698 6/15/23 5:08 CMR Isopropanol 0.28 1.4 0.24 J 0.69 3.4 0.59 0.698 6/15/23 5:08 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/15/23 5:08 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/15/23 5:08 CMR 4-Methyl-2-pentanone (MIBK) 0.020 0.035 0.019 J 0.083 0.14 0.076 0.698 6/15/23 5:08 CMR Naphthalene ND 0.035 0.026 Z-01 ND 0.18 0.14 0.698 6/15/23 5:08 CMR Propene 0.33 1.4 0.31 J 0.57 2.4 0.53 0.698 6/15/23 5:08 CMR Styrene 0.029 0.035 0.018 J 0.12 0.15 0.078 0.698 6/15/23 5:08 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 5:08 CMR Page 53 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: OA Sample ID: 23F1309-25 Sample Matrix: Indoor air Sampled: 6/4/2023 10:55 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1138 Canister Size: 6 liter Flow Controller ID: 3264 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -7 Receipt Vacuum(in Hg): -7.6 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 5:08 CMR Tetrahydrofuran 0.25 0.35 0.057 J 0.73 1.0 0.17 0.698 6/15/23 5:08 CMR Toluene 0.35 0.035 0.020 1.3 0.13 0.075 0.698 6/15/23 5:08 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 5:08 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 5:08 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 5:08 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 5:08 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 5:08 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.061 0.14 0.039 J 0.47 1.1 0.30 0.698 6/15/23 5:08 CMR 1,2,4-Trimethylbenzene 0.050 0.035 0.015 0.24 0.17 0.076 0.698 6/15/23 5:08 CMR 1,3,5-Trimethylbenzene ND 0.035 0.018 ND 0.17 0.091 0.698 6/15/23 5:08 CMR Vinyl Acetate ND 0.70 0.19 ND 2.5 0.66 0.698 6/15/23 5:08 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 5:08 CMR m&p-Xylene 0.20 0.070 0.039 0.87 0.30 0.17 0.698 6/15/23 5:08 CMR o-Xylene 0.066 0.035 0.018 0.29 0.15 0.078 0.698 6/15/23 5:08 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 97.1 % REC Limits 70-130 6/15/23 5:08 Page 54 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-22 Sample ID: 23FI309-26 Sample Matrix: Indoor air Sampled: 6/4/2023 11:04 Sample Description/Location: Sub Description/Location: Canister ID: 1991 Canister Size: 6 liter Flow Controller ID: 3504 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -8 Receipt Vacuum(in Hg): -7.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 16 1.4 0.84 39 3.3 2.0 0.698 6/15/23 5:39 CMR Benzene 0.18 0.035 0.026 0.59 0.11 0.084 0.698 6/15/23 5:39 CMR Benzyl chloride ND 0.14 0.031 ND 0.72 0.16 0.698 6/15/23 5:39 CMR Bromodichloromethane ND 0.035 0.024 ND 0.23 0.16 0.698 6/15/23 5:39 CMR Bromoform ND 0.035 0.024 ND 0.36 0.25 0.698 6/15/23 5:39 CMR Bromomethane ND 0.035 0.023 ND 0.14 0.090 0.698 6/15/23 5:39 CMR 1,3-Butadiene ND 0.035 0.029 ND 0.077 0.065 0.698 6/15/23 5:39 CMR 2-Butanone (MEK) 7.9 1.4 0.37 L-05 23 4.1 1.1 0.698 6/15/23 5:39 CMR Carbon Disulfide ND 0.35 0.032 ND 1.1 0.10 0.698 6/15/23 5:39 CMR Carbon Tetrachloride 0.081 0.035 0.028 0.51 0.22 0.17 0.698 6/15/23 5:39 CMR Chlorobenzene ND 0.035 0.023 ND 0.16 0.11 0.698 6/15/23 5:39 CMR Chloroethane ND 0.035 0.031 ND 0.092 0.082 0.698 6/15/23 5:39 CMR Chloroform ND 0.035 0.033 ND 0.17 0.16 0.698 6/15/23 5:39 CMR Chloromethane 0.58 0.070 0.028 1.2 0.14 0.057 0.698 6/15/23 5:39 CMR Cyclohexane 0.23 0.035 0.021 0.79 0.12 0.073 0.698 6/15/23 5:39 CMR Dibromochloromethane ND 0.035 0.023 ND 0.30 0.20 0.698 6/15/23 5:39 CMR 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 0.16 0.698 6/15/23 5:39 CMR 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 0.12 0.698 6/15/23 5:39 CMR 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 0.12 0.698 6/15/23 5:39 CMR 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 0.14 0.698 6/15/23 5:39 CMR Dichlorodifluoromethane (Freon 12) 0.53 0.035 0.034 2.6 0.17 0.17 0.698 6/15/23 5:39 CMR 1,I-Dichloroethane ND 0.035 0.030 ND 0.14 0.12 0.698 6/15/23 5:39 CMR 1,2-Dichloroethane ND 0.035 0.032 ND 0.14 0.13 0.698 6/15/23 5:39 CMR 1,I-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 5:39 CMR cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 0.10 0.698 6/15/23 5:39 CMR trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 0.11 0.698 6/15/23 5:39 CMR 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 0.087 0.698 6/15/23 5:39 CMR cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.082 0.698 6/15/23 5:39 CMR trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 0.081 0.698 6/15/23 5:39 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 0.24 0.698 6/15/23 5:39 CMR 1,4-Dioxane ND 0.35 0.029 ND 1.3 0.10 0.698 6/15/23 5:39 CMR Ethanol 12 1.4 0.62 22 2.6 1.2 0.698 6/15/23 5:39 CMR Ethyl Acetate 0.54 0.35 0.18 2.0 1.3 0.64 0.698 6/15/23 5:39 CMR Ethylbenzene 0.43 0.035 0.020 1.9 0.15 0.088 0.698 6/15/23 5:39 CMR 4-Ethyltoluene 0.041 0.035 0.021 0.20 0.17 0.11 0.698 6/15/23 5:39 CMR Heptane 0.15 0.035 0.022 0.63 0.14 0.091 0.698 6/15/23 5:39 CMR Hexachlorobutadiene ND 0.035 0.029 ND 0.37 0.31 0.698 6/15/23 5:39 CMR Hexane ND 1.4 0.18 ND 4.9 0.64 0.698 6/15/23 5:39 CMR 2-Hexanone (MBK) 0.11 0.14 0.017 J 0.44 0.57 0.071 0.698 6/15/23 5:39 CMR Isopropanol 0.77 1.4 0.24 J 1.9 3.4 0.59 0.698 6/15/23 5:39 CMR Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 0.097 0.698 6/15/23 5:39 CMR Methylene Chloride ND 0.35 0.16 ND 1.2 0.56 0.698 6/15/23 5:39 CMR 4-Methyl-2-pentanone (MIBK) 0.089 0.035 0.019 0.37 0.14 0.076 0.698 6/15/23 5:39 CMR Naphthalene ND 0.035 0.026 Z-01 ND 0.18 0.14 0.698 6/15/23 5:39 CMR Propene 0.96 1.4 0.31 J 1.7 2.4 0.53 0.698 6/15/23 5:39 CMR Styrene 0.091 0.035 0.018 0.39 0.15 0.078 0.698 6/15/23 5:39 CMR 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 5:39 CMR Page 55 of 102 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/9/2023 Field Sample #: IA-22 Sample ID: 23F1309-26 Sample Matrix: Indoor air Sampled: 6/4/2023 11:04 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 1991 Canister Size: 6 liter Flow Controller ID: 3504 Sample Type: 24 hr Work Order: 23171309 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -8 Receipt Vacuum(in Hg): -7.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 5:39 CMR Tetrahydrofuran 11 0.35 0.057 32 1.0 0.17 0.698 6/15/23 5:39 CMR Toluene 1.1 0.035 0.020 4.0 0.13 0.075 0.698 6/15/23 5:39 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 5:39 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 5:39 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 5:39 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 5:39 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 5:39 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.060 0.14 0.039 J 0.46 1.1 0.30 0.698 6/15/23 5:39 CMR 1,2,4-Trimethylbenzene 0.27 0.035 0.015 1.3 0.17 0.076 0.698 6/15/23 5:39 CMR 1,3,5-Trimethylbenzene 0.068 0.035 0.018 0.34 0.17 0.091 0.698 6/15/23 5:39 CMR Vinyl Acetate 1.6 0.70 0.19 5.5 2.5 0.66 0.698 6/15/23 5:39 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 5:39 CMR m&p-Xylene 1.6 0.070 0.039 7.0 0.30 0.17 0.698 6/15/23 5:39 CMR o-Xylene 0.50 0.035 0.018 2.2 0.15 0.078 0.698 6/15/23 5:39 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 96.9 % REC Limits 70-130 6/15/23 5:39 Page 56 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-4 Canister ID: 1856 Sample ID: 23F1309-27 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3711 Sampled: 6/4/2023 11:08 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -9.25 Receipt Vacuum(in Hg): -9.5 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 22 1.4 0.84 51 3.3 Benzene 0.17 0.035 0.026 0.53 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 2.4 1.4 0.37 L-05 7.0 4.1 Carbon Disulfide 0.034 0.35 0.032 J 0.11 1.1 Carbon Tetrachloride 0.075 0.035 0.028 0.47 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform ND 0.035 0.033 ND 0.17 Chloromethane 0.59 0.070 0.028 1.2 0.14 Cyclohexane 0.39 0.035 0.021 1.3 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.53 0.035 0.034 2.6 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.042 0.035 0.032 0.17 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane ND 0.035 0.019 ND 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 23 1.4 0.62 44 2.6 Ethyl Acetate 0.33 0.35 0.18 J 1.2 1.3 Ethylbenzene 0.15 0.035 0.020 0.63 0.15 4-Ethyltoluene ND 0.035 0.021 ND 0.17 Heptane 0.27 0.035 0.022 1.1 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane ND 1.4 0.18 ND 4.9 2-Hexanone (MBK) 0.15 0.14 0.017 0.61 0.57 Isopropanol 1.9 1.4 0.24 4.7 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.24 0.035 0.019 0.98 0.14 Naphthalene 0.029 0.035 0.026 L-05, V-06, 0.15 0.18 Z-01, J Propene 0.50 1.4 0.31 J 0.86 2.4 Styrene 0.13 0.035 0.018 0.55 0.15 2.0 0.698 6/15/23 6:10 CMR 0.084 0.698 6/15/23 6:10 CMR 0.16 0.698 6/15/23 6:10 CMR 0.16 0.698 6/15/23 6:10 CMR 0.25 0.698 6/15/23 6:10 CMR 0.090 0.698 6/15/23 6:10 CMR 0.065 0.698 6/15/23 6:10 CMR 1.1 0.698 6/15/23 6:10 CMR 0.10 0.698 6/15/23 6:10 CMR 0.17 0.698 6/15/23 6:10 CMR 0.11 0.698 6/15/23 6:10 CMR 0.082 0.698 6/15/23 6:10 CMR 0.16 0.698 6/15/23 6:10 CMR 0.057 0.698 6/15/23 6:10 CMR 0.073 0.698 6/15/23 6:10 CMR 0.20 0.698 6/15/23 6:10 CMR 0.16 0.698 6/15/23 6:10 CMR 0.12 0.698 6/15/23 6:10 CMR 0.12 0.698 6/15/23 6:10 CMR 0.14 0.698 6/15/23 6:10 CMR 0.17 0.698 6/15/23 6:10 CMR 0.12 0.698 6/15/23 6:10 CMR 0.13 0.698 6/15/23 6:10 CMR 0.11 0.698 6/15/23 6:10 CMR 0.10 0.698 6/15/23 6:10 CMR 0.11 0.698 6/15/23 6:10 CMR 0.087 0.698 6/15/23 6:10 CMR 0.082 0.698 6/15/23 6:10 CMR 0.081 0.698 6/15/23 6:10 CMR 0.24 0.698 6/15/23 6:10 CMR 0.10 0.698 6/15/23 6:10 CMR 1.2 0.698 6/15/23 6:10 CMR 0.64 0.698 6/15/23 6:10 CMR 0.088 0.698 6/15/23 6:10 CMR 0.11 0.698 6/15/23 6:10 CMR 0.091 0.698 6/15/23 6:10 CMR 0.31 0.698 6/15/23 6:10 CMR 0.64 0.698 6/15/23 6:10 CMR 0.071 0.698 6/15/23 6:10 CMR 0.59 0.698 6/15/23 6:10 CMR 0.097 0.698 6/15/23 6:10 CMR 0.56 0.698 6/15/23 6:10 CMR 0.076 0.698 6/15/23 6:10 CMR 0.14 0.698 6/15/23 6:10 CMR 0.53 0.698 6/15/23 6:10 CMR 0.078 0.698 6/15/23 6:10 CMR Page 57 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: IA-4 Canister ID: 1856 Final Vacuum(in Hg): -9.25 Sample ID: 23F1309-27 Canister Size: 6 liter Receipt Vacuum(in Hg): -9.5 Sample Matrix: Indoor air Flow Controller ID: 3711 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 11:08 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 6:10 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 6:10 CMR Tetrahydrofuran 1.2 0.35 0.057 3.7 1.0 0.17 0.698 6/15/23 6:10 CMR Toluene 1.3 0.035 0.020 4.7 0.13 0.075 0.698 6/15/23 6:10 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 6:10 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 6:10 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 6:10 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 6:10 CMR Trichlorofluoromethane (Freon 11) 0.22 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 6:10 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.063 0.14 0.039 J 0.48 1.1 0.30 0.698 6/15/23 6:10 CMR 1,2,4-Trimethylbenzene 0.093 0.035 0.015 0.46 0.17 0.076 0.698 6/15/23 6:10 CMR 1,3,5-Trimethylbenzene 0.023 0.035 0.018 J 0.11 0.17 0.091 0.698 6/15/23 6:10 CMR Vinyl Acetate 0.73 0.70 0.19 2.6 2.5 0.66 0.698 6/15/23 6:10 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 6:10 CMR m&p-Xylene 0.52 0.070 0.039 2.3 0.30 0.17 0.698 6/15/23 6:10 CMR o-Xylene 0.24 0.035 0.018 1.0 0.15 0.078 0.698 6/15/23 6:10 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 97.5 70-130 6/15/23 6:10 Page 58 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Date Received: 6/9/2023 Sub Description/Location: Field Sample #: IA-8 Canister ID: 1225 Sample ID: 23F1309-28 Canister Size: 6 liter Sample Matrix: Indoor air Flow Controller ID: 3521 Sampled: 6/4/2023 11:12 Sample Type: 24 hr EPA TO-15 Work Order: 23171309 Initial Vacuum(in Hg): -29.25 Final Vacuum(in Hg): -6.5 Receipt Vacuum(in Hg): -7.4 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RI MDL Dilution Analyzed Analyst Acetone 52 1.4 0.84 E 120 3.3 Benzene 0.23 0.035 0.026 0.74 0.11 Benzyl chloride ND 0.14 0.031 ND 0.72 Bromodichloromethane ND 0.035 0.024 ND 0.23 Bromoform ND 0.035 0.024 ND 0.36 Bromomethane ND 0.035 0.023 ND 0.14 1,3-Butadiene ND 0.035 0.029 ND 0.077 2-Butanone (MEK) 4.0 1.4 0.37 L-05 12 4.1 Carbon Disulfide 0.18 0.35 0.032 J 0.57 1.1 Carbon Tetrachloride 0.077 0.035 0.028 0.48 0.22 Chlorobenzene ND 0.035 0.023 ND 0.16 Chloroethane ND 0.035 0.031 ND 0.092 Chloroform 0.034 0.035 0.033 J 0.17 0.17 Chloromethane 0.62 0.070 0.028 1.3 0.14 Cyclohexane 0.31 0.035 0.021 1.1 0.12 Dibromochloromethane ND 0.035 0.023 ND 0.30 1,2-Dibromoethane (EDB) ND 0.035 0.021 ND 0.27 1,2-Dichlorobenzene ND 0.035 0.020 ND 0.21 1,3-Dichlorobenzene ND 0.035 0.019 ND 0.21 1,4-Dichlorobenzene ND 0.035 0.023 ND 0.21 Dichlorodifluoromethane (Freon 12) 0.52 0.035 0.034 2.6 0.17 1,1-Dichloroethane ND 0.035 0.030 ND 0.14 1,2-Dichloroethane 0.059 0.035 0.032 0.24 0.14 1,1-Dichloroethylene ND 0.035 0.027 ND 0.14 cis-1,2-Dichloroethylene ND 0.035 0.025 ND 0.14 trans-1,2-Dichloroethylene ND 0.035 0.027 ND 0.14 1,2-Dichloropropane 0.020 0.035 0.019 J 0.093 0.16 cis- 1,3 -Dichloropropene ND 0.035 0.018 ND 0.16 trans- 1, 3 -Dichloropropene ND 0.035 0.018 ND 0.16 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.035 0.034 ND 0.24 1,4-Dioxane ND 0.35 0.029 ND 1.3 Ethanol 46 1.4 0.62 E 87 2.6 Ethyl Acetate 0.60 0.35 0.18 2.2 1.3 Ethylbenzene 0.44 0.035 0.020 1.9 0.15 4-Ethyltoluene 0.052 0.035 0.021 0.25 0.17 Heptane 1.2 0.035 0.022 4.9 0.14 Hexachlorobutadiene ND 0.035 0.029 ND 0.37 Hexane 0.22 1.4 0.18 J 0.78 4.9 2-Hexanone (MBK) 0.19 0.14 0.017 0.78 0.57 Isopropanol 4.1 1.4 0.24 10.0 3.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 0.027 ND 0.13 Methylene Chloride ND 0.35 0.16 ND 1.2 4-Methyl-2-pentanone (MIBK) 0.40 0.035 0.019 1.6 0.14 Naphthalene 0.032 0.035 0.026 L-05, V-06, 0.17 0.18 Z-01, J Propene 0.69 1.4 0.31 J 1.2 2.4 Styrene 1.3 0.035 0.018 5.7 0.15 2.0 0.698 6/15/23 6:41 CMR 0.084 0.698 6/15/23 6:41 CMR 0.16 0.698 6/15/23 6:41 CMR 0.16 0.698 6/15/23 6:41 CMR 0.25 0.698 6/15/23 6:41 CMR 0.090 0.698 6/15/23 6:41 CMR 0.065 0.698 6/15/23 6:41 CMR 1.1 0.698 6/15/23 6:41 CMR 0.10 0.698 6/15/23 6:41 CMR 0.17 0.698 6/15/23 6:41 CMR 0.11 0.698 6/15/23 6:41 CMR 0.082 0.698 6/15/23 6:41 CMR 0.16 0.698 6/15/23 6:41 CMR 0.057 0.698 6/15/23 6:41 CMR 0.073 0.698 6/15/23 6:41 CMR 0.20 0.698 6/15/23 6:41 CMR 0.16 0.698 6/15/23 6:41 CMR 0.12 0.698 6/15/23 6:41 CMR 0.12 0.698 6/15/23 6:41 CMR 0.14 0.698 6/15/23 6:41 CMR 0.17 0.698 6/15/23 6:41 CMR 0.12 0.698 6/15/23 6:41 CMR 0.13 0.698 6/15/23 6:41 CMR 0.11 0.698 6/15/23 6:41 CMR 0.10 0.698 6/15/23 6:41 CMR 0.11 0.698 6/15/23 6:41 CMR 0.087 0.698 6/15/23 6:41 CMR 0.082 0.698 6/15/23 6:41 CMR 0.081 0.698 6/15/23 6:41 CMR 0.24 0.698 6/15/23 6:41 CMR 0.10 0.698 6/15/23 6:41 CMR 1.2 0.698 6/15/23 6:41 CMR 0.64 0.698 6/15/23 6:41 CMR 0.088 0.698 6/15/23 6:41 CMR 0.11 0.698 6/15/23 6:41 CMR 0.091 0.698 6/15/23 6:41 CMR 0.31 0.698 6/15/23 6:41 CMR 0.64 0.698 6/15/23 6:41 CMR 0.071 0.698 6/15/23 6:41 CMR 0.59 0.698 6/15/23 6:41 CMR 0.097 0.698 6/15/23 6:41 CMR 0.56 0.698 6/15/23 6:41 CMR 0.076 0.698 6/15/23 6:41 CMR 0.14 0.698 6/15/23 6:41 CMR 0.53 0.698 6/15/23 6:41 CMR 0.078 0.698 6/15/23 6:41 CMR Page 59 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171309 Date Received: 6/9/2023 Sub Description/Location: Initial Vacuum(in Hg): -29.25 Field Sample #: IA-8 Canister ID: 1225 Final Vacuum(in Hg): -6.5 Sample ID: 23F1309-28 Canister Size: 6 liter Receipt Vacuum(in Hg): -7.4 Sample Matrix: Indoor air Flow Controller ID: 3521 Flow Controller Type: Fixed -Orifice Sampled: 6/4/2023 11:12 Sample Type: 24 hr Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst 1,1,2,2-Tetrachloroethane ND 0.035 0.019 ND 0.24 0.13 0.698 6/15/23 6:41 CMR Tetrachloroethylene ND 0.035 0.027 ND 0.24 0.18 0.698 6/15/23 6:41 CMR Tetrahydrofuran 2.7 0.35 0.057 8.0 1.0 0.17 0.698 6/15/23 6:41 CMR Toluene 6.1 0.035 0.020 23 0.13 0.075 0.698 6/15/23 6:41 CMR 1,2,4-Trichlorobenzene ND 0.035 0.032 ND 0.26 0.24 0.698 6/15/23 6:41 CMR 1, 1, 1 -Trichloroethane ND 0.035 0.027 ND 0.19 0.15 0.698 6/15/23 6:41 CMR 1,1,2-Trichloroethane ND 0.035 0.025 ND 0.19 0.13 0.698 6/15/23 6:41 CMR Trichloroethylene ND 0.035 0.024 ND 0.19 0.13 0.698 6/15/23 6:41 CMR Trichlorofluoromethane (Freon 11) 0.21 0.14 0.041 1.2 0.78 0.23 0.698 6/15/23 6:41 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.065 0.14 0.039 J 0.50 1.1 0.30 0.698 6/15/23 6:41 CMR 1,2,4-Trimethylbenzene 0.29 0.035 0.015 1.4 0.17 0.076 0.698 6/15/23 6:41 CMR 1,3,5-Trimethylbenzene 0.075 0.035 0.018 0.37 0.17 0.091 0.698 6/15/23 6:41 CMR Vinyl Acetate 0.89 0.70 0.19 3.1 2.5 0.66 0.698 6/15/23 6:41 CMR Vinyl Chloride ND 0.035 0.031 ND 0.089 0.080 0.698 6/15/23 6:41 CMR m&p-Xylene 1.7 0.070 0.039 7.2 0.30 0.17 0.698 6/15/23 6:41 CMR o-Xylene 0.58 0.035 0.018 2.5 0.15 0.078 0.698 6/15/23 6:41 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 97.8 70-130 6/15/23 6:41 Page 60 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] Batch Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL Date 23F1309-01 [IA-1] B343424 1.5 1 N/A 1000 200 430 06/14/23 23F1309-02 [IA-2] B343424 1.5 1 N/A 1000 200 430 06/14/23 23F1309-03 [IA-3] B343424 1.5 1 N/A 1000 200 430 06/14/23 23F1309-04 [IA-5] B343424 1.5 1 N/A 1000 200 430 06/14/23 23F1309-05 [IA-6] B343424 L5 1 N/A 1000 200 430 06/14/23 23F1309-06 [IA-7] B343424 1.5 1 N/A 1000 200 430 06/14/23 23F1309-07 [IA-7 DUP] B343424 1.74 1 N/A 1000 200 500 06/14/23 23F1309-08 [IA-9] B343424 1.5 1 N/A 1000 200 430 06/14/23 23171309-09 [IA-10] B343424 1.5 1 N/A 1000 200 430 06/14/23 23F1309-10 [IA-11] B343424 1.74 1 N/A 1000 200 500 06/14/23 23F1309-11 [IA-12] B343424 1.5 1 N/A 1000 200 430 06/14/23 Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] Batch Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL Date 23F1309-12 [IA-14] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-13 [IA-13] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-14 [IA-16] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-15 [IA-17] B343439 1.5 1 N/A 1000 200 430 06/14/23 23171309-16 [IA-18] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-17 [IA-19] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-19 [IA-23] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-20 [IA-15] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-21 [IA-24] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-22 [IA-25] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-23 [IA-25 DUP] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-24 [IA-21] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-25 [OA] B343439 1.5 1 N/A 1000 200 430 06/14/23 23171309-26 [IA-22] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-27 [IA-4] B343439 1.5 1 N/A 1000 200 430 06/14/23 23F1309-28 [IA-8] B343439 1.5 1 N/A 1000 200 430 06/14/23 Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] Batch Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL Date 23F1309-OIRE1 [IA-1] B343523 1.5 1 N/A 1000 200 150 06/15/23 23F1309-02RE1 [IA-2] B343523 1.5 1 N/A 1000 200 150 06/15/23 23F1309-03RE1 [IA-3] B343523 1.5 1 N/A 1000 200 150 06/15/23 23F1309-09RE1 [IA-10] B343523 1.5 1 N/A 1000 200 150 06/15/23 23171309-10RE1 [IA-11] B343523 1.74 1 N/A 1000 200 174 06/15/23 23F1309-11RE1 [IA-12] B343523 1.5 1 N/A 1000 200 150 06/15/23 23F1309-12RE1 [IA-14] B343523 1.5 1 N/A 1000 200 150 06/15/23 23F1309-13RE1 [IA-13] B343523 1.5 1 N/A 1000 200 150 06/15/23 23F1309-16RE1 [IA-18] B343523 1.5 1 N/A 1000 200 150 06/15/23 23F1309-17RE1 [IA-19] B343523 1.5 1 N/A 1000 200 150 06/15/23 Page 61 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Pre-Dil Pre-Dil Default Actual Pressure Pre Initial Final Injection Injection Lab Number [Field ID] Batch Dilution Dilution mL mL mL mL Date 23F1309-19RE1 [IA-23] B343662 1.5 1 N/A 1000 200 75 06/16/23 23F1309-20RE1 [IA-15] B343662 1.5 1 N/A 1000 200 75 06/16/23 Page 62 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B343424 - TO-15 Prep Blank (B343424-BLK1) Prepared & Analyzed: 06/14/23 Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride 0.057 0.080 B-05, J Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 1,3-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride ND 0.020 Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 1,4-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1,1-Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis- 1,3 -Dichloropropene ND 0.020 trans- l,3-Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 1,4-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 Ethylbenzene ND 0.020 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Hexachlorobutadiene ND 0.020 Hexane ND 0.80 2-Hexanone (MBK) ND 0.080 Isopropanol ND 0.80 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Z-01 Propene ND 0.80 Styrene ND 0.020 Page 63 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343424 - TO-15 Prep Blank (B343424-BLKI) Prepared & Analyzed: 06/14/23 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene ND 0.020 Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Trichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene ND 0.040 o-Xylene ND 0.020 Surrogate: 4-Bromofluorobenzene (1) LCS (B343424-BS1) 7.68 8.00 96.0 Prepared & Analyzed: 06/14/23 70-130 Acetone 4.32 5.00 86.3 70-130 Benzene 4.97 5.00 99.4 70-130 Benzyl chloride 3.86 5.00 77.2 70-130 Bromodichloromethane 4.95 5.00 99.0 70-130 Bromoform 5.36 5.00 107 70-130 Bromomethane 4.84 5.00 96.8 70-130 1,3-Butadiene 5.48 5.00 110 70-130 2-Butanone (MEK) 6.24 5.00 125 70-130 Carbon Disulfide 4.60 5.00 92.1 70-130 Carbon Tetrachloride 5.19 5.00 104 70-130 Chlorobenzene 4.60 5.00 91.9 70-130 Chloroethane 5.13 5.00 103 70-130 Chloroform 4.80 5.00 96.0 70-130 Chloromethane 5.05 5.00 101 70-130 Cyclohexane 5.39 5.00 108 70-130 Dibromochloromethane 5.38 5.00 108 70-130 1,2-Dibromoethane (EDB) 4.94 5.00 98.8 70-130 1,2-Dichlorobenzene 4.96 5.00 99.1 70-130 1,3-Dichlorobenzene 4.79 5.00 95.9 70-130 1,4-Dichlorobenzene 4.64 5.00 92.8 70-130 Dichlorodifluoromethane (Freon 12) 5.43 5.00 109 70-130 1,1-Dichloroethane 5.07 5.00 101 70-130 1,2-Dichloroethane 4.78 5.00 95.5 70-130 1,1-Dichloroethylene 4.65 5.00 93.0 70-130 cis-1,2-Dichloroethylene 4.99 5.00 99.9 70-130 trans-1,2-Dichloroethylene 5.28 5.00 106 70-130 1,2-Dichloropropane 5.24 5.00 105 70-130 Page 64 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343424 - TO-15 Prep LCS (B343424-BS1) Prepared & Analyzed: 06/14/23 cis-1,3-Dichloropropene 5.48 5.00 110 70-130 trans-1,3-Dichloropropene 6.03 5.00 121 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 4.61 5.00 92.2 70-130 (Freon 114) 1,4-Dioxane 5.12 5.00 102 70-130 Ethanol 5.27 5.00 105 70-130 Ethyl Acetate 4.57 5.00 91.5 70-130 Ethylbenzene 5.08 5.00 102 70-130 4-Ethyltoluene 5.54 5.00 ill 70-130 Heptane 5.87 5.00 117 70-130 Hexachlorobutadiene 6.64 4.25 156 * 70-130 L-01, V-2( Hexane 4.89 5.00 97.8 70-130 2-Hexanone (MBK) 5.04 5.00 101 70-130 Isopropanol 3.90 5.00 78.0 70-130 Methyl tert-Butyl Ether (MTBE) 5.02 5.00 100 70-130 Methylene Chloride 3.91 5.00 78.1 70-130 4-Methyl-2-pentanone (MIBK) 5.96 5.00 119 70-130 Naphthalene 4.67 3.68 127 70-130 V-06, Z-01 Propene 6.50 5.00 130 70-130 Styrene 5.40 5.00 108 70-130 1,1,2,2-Tetrachloroethane 4.88 5.00 97.5 70-130 Tetrachloroethylene 4.72 5.00 94.4 70-130 Tetrahydrofuran 5.35 5.00 107 70-130 Toluene 5.29 5.00 106 70-130 1,2,4-Trichlorobenzene 4.61 3.90 118 70-130 V-2( 1, 1, 1 -Trichloroethane 5.03 5.00 101 70-130 1,1,2-Trichloroethane 5.07 5.00 101 70-130 Trichloroethylene 5.09 5.00 102 70-130 Trichlorofluoromethane (Freon 11) 4.88 5.00 97.6 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 4.41 5.00 88.2 70-130 113) 1,2,4-Trimethylbenzene 5.65 5.00 113 70-130 1,3,5-Trimethylbenzene 5.59 5.00 112 70-130 Vinyl Acetate 5.27 5.00 105 70-130 Vinyl Chloride 5.26 5.00 105 70-130 m&p-Xylene 11.0 10.0 110 70-130 o-Xylene 5.43 5.00 109 70-130 Surrogate: 4-Bromofluorobenzene (1) 8.00 8.00 100 70-130 Page 65 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD knalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B343424 - TO-15 Prep Duplicate (B343424-DUPI) Source: 23171309-11 Prepared & Analyzed: 06/14/23 Benzene 0.23 0.035 0.73 0.11 0.23 1.81 25 Benzyl chloride ND 0.14 ND 0.72 ND 25 Bromodichloromethane ND 0.035 ND 0.23 ND 25 Bromoform ND 0.035 ND 0.36 ND 25 Bromomethane ND 0.035 ND 0.14 ND 25 1,3-Butadiene ND 0.035 ND 0.077 ND 25 2-Butanone (MEK) 11 1.4 31 4.1 14 29.5 25 R-01 Carbon Disulfide 0.36 0.35 1.1 1.1 0.36 1.74 25 Carbon Tetrachloride 0.073 0.035 0.46 0.22 0.075 2.82 25 Chlorobenzene ND 0.035 ND 0.16 ND 25 Chloroethane 0.18 0.035 0.49 0.092 0.17 9.90 25 Chloroform 0.056 0.035 0.27 0.17 0.052 7.79 25 Chloromethane 0.60 0.070 1.2 0.14 0.59 1.87 25 Cyclohexane 0.34 0.035 1.2 0.12 0.34 1.44 25 Dibromochloromethane ND 0.035 ND 0.30 ND 25 1,2-Dibromoethane (EDB) ND 0.035 ND 0.27 ND 25 1,2-Dichlorobenzene ND 0.035 ND 0.21 ND 25 1,3-Dichlorobenzene ND 0.035 ND 0.21 ND 25 1,4-Dichlorobenzene ND 0.035 ND 0.21 ND 25 Dichlorodifluoromethane (Freon 12) 0.56 0.035 2.8 0.17 0.56 0.00 25 1,1-Dichloroethane ND 0.035 ND 0.14 ND 25 1,2-Dichloroethane 0.056 0.035 0.23 0.14 0.059 4.88 25 1,1-Dichloroethylene ND 0.035 ND 0.14 ND 25 cis-1,2-Dichloroethylene ND 0.035 ND 0.14 ND 25 trans-1,2-Dichloroethylene ND 0.035 ND 0.14 ND 25 1,2-Dichloropropane 0.063 0.035 0.29 0.16 0.063 0.00 25 cis- 1,3 -Dichloropropene ND 0.035 ND 0.16 ND 25 trans- l,3-Dichloropropene ND 0.035 ND 0.16 ND 25 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.035 ND 0.24 ND 25 (Freon 114) 1,4-Dioxane ND 0.35 ND 1.3 ND 25 Ethyl Acetate 0.55 0.35 2.0 1.3 0.56 2.38 25 Ethylbenzene 1.2 0.035 5.2 0.15 1.2 0.936 25 4-Ethyltoluene 0.084 0.035 0.41 0.17 0.10 18.0 25 Heptane 1.4 0.035 5.8 0.14 1.5 2.93 25 Hexachlorobutadiene ND 0.035 ND 0.37 ND 25 Hexane 2.5 1.4 8.8 4.9 2.3 8.19 25 2-Hexanone (MBK) 0.19 0.14 0.76 0.57 0.18 1.52 25 Isopropanol 2.6 1.4 6.3 3.4 2.5 2.50 25 Methyl tert-Butyl Ether (MTBE) ND 0.035 ND 0.13 ND 25 Methylene Chloride ND 0.35 ND 1.2 ND 25 4-Methyl-2-pentanone (MIBK) 0.32 0.035 1.3 0.14 0.32 0.00 25 Naphthalene 0.090 0.035 0.47 0.18 0.093 3.05 25 V-06, Z-01 Propene 1.3 1.4 2.3 2.4 ND 25 J Styrene 0.86 0.035 3.7 0.15 0.88 2.01 25 1,1,2,2-Tetrachloroethane ND 0.035 ND 0.24 ND 25 Tetrachloroethylene ND 0.035 ND 0.24 ND 25 Page 66 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B343424 - TO-15 Prep Duplicate (B343424-DUPI) Source: 23171309-11 Prepared & Analyzed: 06/14/23 Toluene 30 0.035 110 0.13 30 0.545 25 1,2,4-Trichlorobenzene ND 0.035 ND 0.26 ND 25 1, 1, 1 -Trichloroethane ND 0.035 ND 0.19 ND 25 1,1,2-Trichloroethane ND 0.035 ND 0.19 ND 25 Trichloroethylene ND 0.035 ND 0.19 ND 25 Trichlorofluoromethane (Freon 11) 0.22 0.14 1.2 0.78 0.22 0.639 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.061 0.14 0.47 1.1 0.064 5.59 25 J 113) 1,2,4-Trimethylbenzene 0.62 0.035 3.0 0.17 0.60 2.17 25 1,3,5-Trimethylbenzene 0.15 0.035 0.75 0.17 0.16 3.15 25 Vinyl Acetate ND 0.70 ND 2.5 ND 25 Vinyl Chloride ND 0.035 ND 0.089 ND 25 m&p-Xylene 4.7 0.070 20 0.30 4.7 1.00 25 o-Xylene 1.6 0.035 6.9 0.15 1.6 0.567 25 Surrogate: 4-BromoJluorobenzene (1) 7.88 8.00 98.4 70-130 Batch B343439 - TO-15 Prep Blank (B343439-BLKI) Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride ND 0.080 Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 1,3-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride ND 0.020 Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 1,4-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1,1-Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis- 1,3 -Dichloropropene ND 0.020 Prepared & Analyzed: 06/14/23 Page 67 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B343439 - TO-15 Prep Blank (B343439-BLKI) Prepared & Analyzed: 06/14/23 trans-1,3-Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 1,4-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 Ethylbenzene ND 0.020 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Hexachlorobutadiene ND 0.020 Hexane ND 0.80 2-Hexanone (MBK) ND 0.080 Isopropanol ND 0.80 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Z-01 Propene ND 0.80 Styrene ND 0.020 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene ND 0.020 Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Trichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene ND 0.040 o-Xylene ND 0.020 Surrogate: 4-BromoJluorobenzene (1) 7.70 8.00 96.3 70-130 Page 68 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343439 - TO-15 Prep LCS (B343439-BSI) Prepared & Analyzed: 06/14/23 Acetone 4.59 5.00 91.8 70-130 Benzene 4.98 5.00 99.6 70-130 Benzyl chloride 3.74 5.00 74.9 70-130 Bromodichloromethane 4.84 5.00 96.9 70-130 Bromoform 5.34 5.00 107 70-130 Bromomethane 4.75 5.00 95.0 70-130 1,3-Butadiene 5.25 5.00 105 70-130 2-Butanone(MEK) 6.59 5.00 132 * 70-130 L-Of Carbon Disulfide 4.68 5.00 93.6 70-130 Carbon Tetrachloride 5.06 5.00 101 70-130 Chlorobenzene 4.73 5.00 94.6 70-130 Chloroethane 4.95 5.00 98.9 70-130 Chloroform 4.89 5.00 97.8 70-130 Chloromethane 4.77 5.00 95.5 70-130 Cyclohexane 5.42 5.00 108 70-130 Dibromochloromethane 5.32 5.00 106 70-130 1,2-Dibromoethane (EDB) 4.87 5.00 97.4 70-130 1,2-Dichlorobenzene 4.88 5.00 97.7 70-130 1,3-Dichlorobenzene 4.52 5.00 90.5 70-130 1,4-Dichlorobenzene 4.39 5.00 87.7 70-130 Dichlorodifluoromethane(Freon 12) 5.42 5.00 108 70-130 1,1-Dichloroethane 5.18 5.00 104 70-130 1,2-Dichloroethane 4.85 5.00 97.0 70-130 1,1-Dichloroethylene 4.62 5.00 92.5 70-130 cis-1,2-Dichloroethylene 5.14 5.00 103 70-130 trans-1,2-Dichloroethylene 5.38 5.00 108 70-130 1,2-Dichloropropane 5.06 5.00 101 70-130 cis- 1,3 -Dichloropropene 5.47 5.00 109 70-130 trans- 1, 3 -Dichloropropene 5.93 5.00 119 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 4.48 5.00 89.7 70-130 (Freon 114) 1,4-Dioxane 5.20 5.00 104 70-130 Ethanol 5.35 5.00 107 70-130 Ethyl Acetate 4.88 5.00 97.6 70-130 Ethylbenzene 5.20 5.00 104 70-130 4-Ethyltoluene 5.52 5.00 110 70-130 Heptane 5.60 5.00 112 70-130 Hexachlorobutadiene 7.01 4.25 165 * 70-130 L-01, V-2( Hexane 5.01 5.00 100 70-130 2-Hexanone (MBK) 5.26 5.00 105 70-130 Isopropanol 3.94 5.00 78.9 70-130 Methyl tert-Butyl Ether (MTBE) 5.67 5.00 113 70-130 Methylene Chloride 3.94 5.00 78.8 70-130 4-Methyl-2-pentanone (MIBK) 6.12 5.00 122 70-130 Naphthalene 5.09 3.68 138 * 70-130 L-05, V-06, Z-01 Propene 6.30 5.00 126 70-130 Page 69 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343439 - TO-15 Prep LCS (B343439-BS1) Prepared & Analyzed: 06/14/23 Styrene 5.64 5.00 113 70-130 1,1,2,2-Tetrachloroethane 4.79 5.00 95.7 70-130 Tetrachloroethylene 4.78 5.00 95.7 70-130 Tetrahydrofuran 5.80 5.00 116 70-130 Toluene 5.30 5.00 106 70-130 1,2,4-Trichlorobenzene 4.66 3.90 120 70-130 V-2( 1, 1, 1 -Trichloroethane 4.93 5.00 98.6 70-130 1,1,2-Trichloroethane 5.05 5.00 101 70-130 Trichloroethylene 5.00 5.00 100 70-130 Trichlorofluoromethane (Freon 11) 4.86 5.00 97.3 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 4.44 5.00 88.7 70-130 113) 1,2,4-Trimethylbenzene 5.80 5.00 116 70-130 1,3,5-Trimethylbenzene 5.67 5.00 113 70-130 Vinyl Acetate 5.85 5.00 117 70-130 Vinyl Chloride 5.09 5.00 102 70-130 m&p-Xylene 11.0 10.0 110 70-130 o-Xylene 5.43 5.00 109 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.91 8.00 98.9 70-130 Duplicate (B343439-DUPI) Source: 23F1309-28 Prepared: 06/14/23 Analyzed: 06/15/23 Acetone 53 1.4 130 3.3 52 1.88 25 E Benzene 0.23 0.035 0.72 0.11 0.23 3.04 25 Benzyl chloride ND 0.14 ND 0.72 ND 25 Bromodichloromethane ND 0.035 ND 0.23 ND 25 Bromoform ND 0.035 ND 0.36 ND 25 Bromomethane ND 0.035 ND 0.14 ND 25 1,3-Butadiene ND 0.035 ND 0.077 ND 25 2-Butanone (MEK) 3.9 1.4 12 4.1 4.0 0.812 25 Carbon Disulfide 0.18 0.35 0.58 1.1 0.18 1.52 25 J Carbon Tetrachloride 0.081 0.035 0.51 0.22 0.077 5.31 25 Chlorobenzene ND 0.035 ND 0.16 ND 25 Chloroethane ND 0.035 ND 0.092 ND 25 Chloroform 0.036 0.035 0.18 0.17 0.034 5.94 25 Chloromethane 0.59 0.070 1.2 0.14 0.62 5.75 25 Cyclohexane 0.30 0.035 1.0 0.12 0.31 0.913 25 Dibromochloromethane ND 0.035 ND 0.30 ND 25 1,2-Dibromoethane (EDB) ND 0.035 ND 0.27 ND 25 1,2-Dichlorobenzene ND 0.035 ND 0.21 ND 25 1,3-Dichlorobenzene ND 0.035 ND 0.21 ND 25 1,4-Dichlorobenzene ND 0.035 ND 0.21 ND 25 Dichlorodifluoromethane (Freon 12) 0.53 0.035 2.6 0.17 0.52 2.14 25 1,1-Dichloroethane ND 0.035 ND 0.14 ND 25 1,2-Dichloroethane 0.052 0.035 0.21 0.14 0.059 12.7 25 1,1-Dichloroethylene ND 0.035 ND 0.14 ND 25 cis-1,2-Dichloroethylene ND 0.035 ND 0.14 ND 25 trans-1,2-Dichloroethylene ND 0.035 ND 0.14 ND 25 Page 70 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B343439 - TO-15 Prep Duplicate (B343439-DUPI) Source: 23F1309-28 Prepared: 06/14/23 Analyzed: 06/15/23 1,2-Dichloropropane 0.023 0.035 0.11 0.16 0.020 12.9 25 J cis-1,3-Dichloropropene ND 0.035 ND 0.16 ND 25 trans-1,3-Dichloropropene ND 0.035 ND 0.16 ND 25 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.035 ND 0.24 ND 25 (Freon 114) 1,4-Dioxane ND 0.35 ND 1.3 ND 25 Ethanol 47 1.4 89 2.6 46 1.77 25 E Ethyl Acetate 0.62 0.35 2.2 1.3 0.60 3.43 25 Ethylbenzene 0.45 0.035 2.0 0.15 0.44 2.19 25 4-Ethyltoluene 0.054 0.035 0.26 0.17 0.052 3.97 25 Heptane 1.2 0.035 5.1 0.14 1.2 3.94 25 Hexachlorobutadiene ND 0.035 ND 0.37 ND 25 Hexane 0.20 1.4 0.71 4.9 0.22 9.52 25 J 2-Hexanone (MBK) 0.19 0.14 0.76 0.57 0.19 2.23 25 Isopropanol 4.1 1.4 10 3.4 4.1 1.08 25 Methyl tert-Butyl Ether (MTBE) ND 0.035 ND 0.13 ND 25 Methylene Chloride ND 0.35 ND 1.2 ND 25 4-Methyl-2-pentanone (MIBK) 0.42 0.035 1.7 0.14 0.40 4.92 25 Naphthalene 0.027 0.035 0.14 0.18 0.032 16.5 25 L-05, V-06, Propene 0.70 1.4 1.2 2.4 0.69 2.51 25 J Styrene 1.4 0.035 6.0 0.15 1.3 3.56 25 1,1,2,2-Tetrachloroethane ND 0.035 ND 0.24 ND 25 Tetrachloroethylene ND 0.035 ND 0.24 ND 25 Tetrahydrofuran 2.8 0.35 8.2 1.0 2.7 2.00 25 Toluene 6.2 0.035 23 0.13 6.1 2.42 25 1,2,4-Trichlorobenzene ND 0.035 ND 0.26 ND 25 1, 1, 1 -Trichloroethane ND 0.035 ND 0.19 ND 25 1,1,2-Trichloroethane ND 0.035 ND 0.19 ND 25 Trichloroethylene ND 0.035 ND 0.19 ND 25 Trichlorofluoromethane (Freon 11) 0.22 0.14 1.3 0.78 0.21 4.78 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 0.063 0.14 0.49 1.1 0.065 2.17 25 1 113) 1,2,4-Trimethylbenzene 0.29 0.035 1.4 0.17 0.29 0.481 25 1,3,5-Trimethylbenzene 0.078 0.035 0.38 0.17 0.075 4.57 25 Vinyl Acetate 0.84 0.70 3.0 2.5 0.89 6.12 25 Vinyl Chloride ND 0.035 ND 0.089 ND 25 m&p-Xylene 1.7 0.070 7.3 0.30 1.7 2.00 25 o-Xylene 0.59 0.035 2.5 0.15 0.58 1.32 25 Surrogate: 4-Bromo/luorobenzene (1) 7.80 8.00 97.6 70-130 Page 71 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD malyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B343523 - TO-15 Prep Blank (B343523-BLKI) Prepared & Analyzed: 06/15/23 Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride ND 0.080 Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 1,3-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride ND 0.020 Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 1,4-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1,1-Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis- 1,3 -Dichloropropene ND 0.020 trans- 1, 3 -Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 1,4-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 Ethylbenzene ND 0.020 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Hexachlorobutadiene ND 0.020 Hexane ND 0.80 2-Hexanone (MBK) ND 0.080 Isopropanol ND 0.80 L-03 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 L-03 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Z-01 Propene ND 0.80 Styrene ND 0.020 Page 72 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343523 - TO-15 Prep Blank (B343523-BLKI) Prepared & Analyzed: 06/15/23 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene ND 0.020 Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Trichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene ND 0.040 o-Xylene ND 0.020 Surrogate: 4-Bromofluorobenzene (1) LCS (B343523-BS1) 7.58 8.00 94.7 Prepared & Analyzed: 06/15/23 70-130 Acetone 3.78 5.00 75.7 70-130 Benzene 4.36 5.00 87.1 70-130 Benzyl chloride 3.54 5.00 70.7 70-130 Bromodichloromethane 4.37 5.00 87.4 70-130 Bromoform 4.70 5.00 94.1 70-130 Bromomethane 3.96 5.00 79.3 70-130 1,3-Butadiene 4.56 5.00 91.1 70-130 2-Butanone (MEK) 5.65 5.00 113 70-130 Carbon Disulfide 3.99 5.00 79.7 70-130 Carbon Tetrachloride 4.48 5.00 89.6 70-130 Chlorobenzene 4.15 5.00 83.0 70-130 Chloroethane 4.25 5.00 85.0 70-130 Chloroform 4.07 5.00 81.4 70-130 Chloromethane 4.24 5.00 84.8 70-130 Cyclohexane 4.86 5.00 97.2 70-130 Dibromochloromethane 4.74 5.00 94.8 70-130 1,2-Dibromoethane (EDB) 4.40 5.00 88.0 70-130 1,2-Dichlorobenzene 4.41 5.00 88.1 70-130 1,3-Dichlorobenzene 4.30 5.00 86.0 70-130 1,4-Dichlorobenzene 4.29 5.00 85.8 70-130 Dichlorodifluoromethane (Freon 12) 4.48 5.00 89.6 70-130 1,1-Dichloroethane 4.36 5.00 87.2 70-130 1,2-Dichloroethane 4.15 5.00 82.9 70-130 1,1-Dichloroethylene 4.07 5.00 81.4 70-130 cis-1,2-Dichloroethylene 4.40 5.00 88.1 70-130 trans-1,2-Dichloroethylene 4.51 5.00 90.2 70-130 1,2-Dichloropropane 4.66 5.00 93.2 70-130 Page 73 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343523 - TO-15 Prep LCS (B343523-BS1) Prepared & Analyzed: 06/15/23 cis-1,3-Dichloropropene 4.94 5.00 98.8 70-130 trans-1,3-Dichloropropene 5.52 5.00 110 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 3.82 5.00 76.4 70-130 (Freon 114) 1,4-Dioxane 4.64 5.00 92.7 70-130 Ethanol 4.51 5.00 90.2 70-130 Ethyl Acetate 4.22 5.00 84.5 70-130 Ethylbenzene 4.64 5.00 92.8 70-130 4-Ethyltoluene 5.02 5.00 100 70-130 Heptane 5.26 5.00 105 70-130 Hexachlorobutadiene 5.95 4.25 140 * 70-130 L-01, V-2( Hexane 4.22 5.00 84.3 70-130 2-Hexanone (MBK) 4.83 5.00 96.6 70-130 Isopropanol 3.40 5.00 67.9 * 70-130 L-03 Methyl tert-Butyl Ether (MTBE) 4.54 5.00 90.7 70-130 Methylene Chloride 3.43 5.00 68.6 * 70-130 L-03 4-Methyl-2-pentanone (MI13K) 5.55 5.00 111 70-130 Naphthalene 4.59 3.68 125 70-130 V-06, Z-01 Propene 5.37 5.00 107 70-130 Styrene 4.94 5.00 98.9 70-130 1,1,2,2-Tetrachloroethane 4.40 5.00 87.9 70-130 Tetrachloroethylene 4.10 5.00 81.9 70-130 Tetrahydrofuran 4.80 5.00 96.0 70-130 Toluene 4.70 5.00 94.1 70-130 1,2,4-Trichlorobenzene 4.26 3.90 109 70-130 1, 1, 1 -Trichloroethane 4.39 5.00 87.7 70-130 1,1,2-Trichloroethane 4.46 5.00 89.2 70-130 Trichloroethylene 4.46 5.00 89.2 70-130 Trichlorofluoromethane (Freon 11) 4.06 5.00 81.3 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 3.73 5.00 74.6 70-130 113) 1,2,4-Trimethylbenzene 5.15 5.00 103 70-130 1,3,5-Trimethylbenzene 4.99 5.00 99.7 70-130 Vinyl Acetate 4.94 5.00 98.8 70-130 Vinyl Chloride 4.40 5.00 88.0 70-130 m&p-Xylene 9.92 10.0 99.2 70-130 o-Xylene 4.90 5.00 98.0 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.82 8.00 97.8 70-130 Page 74 of 1 2 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD Analyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qual Batch B343523 - TO-15 Prep Duplicate (B343523-DUPI) Source: 23171309-11RE1 Prepared & Analyzed: 06/15/23 Acetone 140 4.0 330 9.5 140 0.361 25 E Ethanol 35 4.0 65 7.5 35 1.13 25 Tetrahydrofuran 33 1.0 97 2.9 33 0.158 25 Surrogate: 4-BromoJluorobenzene (1) 7.63 8.00 95.4 70-130 Batch B343662 - TO-15 Prep Blank (B343662-BLKI) Prepared & Analyzed: 06/16/23 Acetone ND 0.80 Benzene ND 0.020 Benzyl chloride ND 0.080 Bromodichloromethane ND 0.020 Bromoform ND 0.020 Bromomethane ND 0.020 1,3-Butadiene ND 0.020 2-Butanone (MEK) ND 0.80 Carbon Disulfide ND 0.20 Carbon Tetrachloride ND 0.020 Chlorobenzene ND 0.020 Chloroethane ND 0.020 Chloroform ND 0.020 Chloromethane ND 0.040 Cyclohexane ND 0.020 Dibromochloromethane ND 0.020 1,2-Dibromoethane (EDB) ND 0.020 1,2-Dichlorobenzene ND 0.020 1,3-Dichlorobenzene ND 0.020 1,4-Dichlorobenzene ND 0.020 Dichlorodifluoromethane (Freon 12) ND 0.020 1,1-Dichloroethane ND 0.020 1,2-Dichloroethane ND 0.020 1,1-Dichloroethylene ND 0.020 cis-1,2-Dichloroethylene ND 0.020 trans-1,2-Dichloroethylene ND 0.020 1,2-Dichloropropane ND 0.020 cis- 1,3 -Dichloropropene ND 0.020 trans- 1, 3 -Dichloropropene ND 0.020 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.020 (Freon 114) 1,4-Dioxane ND 0.20 Ethanol ND 0.80 Ethyl Acetate ND 0.20 Ethylbenzene ND 0.020 4-Ethyltoluene ND 0.020 Heptane ND 0.020 Hexachlorobutadiene ND 0.020 Hexane ND 0.80 Page 75 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343662 - TO-15 Prep Blank (B343662-BLKI) Prepared & Analyzed: 06/16/23 2-Hexanone (MBK) ND 0.080 Isopropanol ND 0.80 Methyl tert-Butyl Ether (MTBE) ND 0.020 Methylene Chloride ND 0.20 4-Methyl-2-pentanone (MIBK) ND 0.020 Naphthalene ND 0.020 Z-01 Propene ND 0.80 Styrene ND 0.020 1,1,2,2-Tetrachloroethane ND 0.020 Tetrachloroethylene ND 0.020 Tetrahydrofuran ND 0.20 Toluene ND 0.020 1,2,4-Trichlorobenzene ND 0.020 1, 1, 1 -Trichloroethane ND 0.020 1,1,2-Trichloroethane ND 0.020 Trichloroethylene ND 0.020 Trichlorofluoromethane (Freon 11) ND 0.080 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.080 113) 1,2,4-Trimethylbenzene ND 0.020 1,3,5-Trimethylbenzene ND 0.020 Vinyl Acetate ND 0.40 Vinyl Chloride ND 0.020 m&p-Xylene ND 0.040 o-Xylene ND 0.020 Surrogate: 4-Bromofluorobenzene (1) LCS (B343662-BS1) 7.38 8.00 92.2 Prepared & Analyzed: 06/16/23 70-130 Acetone 3.94 5.00 78.8 70-130 Benzene 4.64 5.00 92.8 70-130 Benzyl chloride 3.52 5.00 70.4 70-130 Bromodichloromethane 4.58 5.00 91.7 70-130 Bromoform 4.84 5.00 96.7 70-130 Bromomethane 4.17 5.00 83.4 70-130 1,3-Butadiene 4.91 5.00 98.2 70-130 2-Butanone(MEK) 5.79 5.00 116 70-130 Carbon Disulfide 4.24 5.00 84.9 70-130 Carbon Tetrachloride 4.64 5.00 92.7 70-130 Chlorobenzene 4.29 5.00 85.7 70-130 Chloroethane 4.55 5.00 91.1 70-130 Chloroform 4.28 5.00 85.6 70-130 Chloromethane 4.44 5.00 88.8 70-130 Cyclohexane 4.97 5.00 99.4 70-130 Dibromochloromethane 4.98 5.00 99.5 70-130 1,2-Dibromoethane (EDB) 4.61 5.00 92.2 70-130 1,2-Dichlorobenzene 4.53 5.00 90.7 70-130 1,3-Dichlorobenzene 4.76 5.00 95.1 70-130 Page 76 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343662 - TO-15 Prep LCS (B343662-BS1) Prepared & Analyzed: 06/16/23 1,4-Dichlorobenzene 4.48 5.00 89.6 70-130 Dichlorodifluoromethane (Freon 12) 4.71 5.00 94.2 70-130 1,1-Dichloroethane 4.56 5.00 91.3 70-130 1,2-Dichloroethane 4.40 5.00 87.9 70-130 1,1-Dichloroethylene 4.20 5.00 84.1 70-130 cis-1,2-Dichloroethylene 4.49 5.00 89.9 70-130 trans-1,2-Dichloroethylene 4.78 5.00 95.6 70-130 1,2-Dichloropropane 4.82 5.00 96.5 70-130 cis- 1,3 -Dichloropropene 5.08 5.00 102 70-130 trans- l,3-Dichloropropene 5.60 5.00 112 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 3.99 5.00 79.9 70-130 (Freon 114) 1,4-Dioxane 4.63 5.00 92.6 70-130 Ethanol 4.93 5.00 98.6 70-130 Ethyl Acetate 4.33 5.00 86.7 70-130 Ethylbenzene 4.79 5.00 95.8 70-130 4-Ethyltoluene 4.97 5.00 99.5 70-130 Heptane 5.46 5.00 109 70-130 Hexachlorobutadiene 6.08 4.25 143 * 70-130 L-01, V-2( Hexane 4.39 5.00 87.7 70-130 2-Hexanone (MBK) 4.91 5.00 98.2 70-130 Isopropanol 3.56 5.00 71.3 70-130 Methyl tert-Butyl Ether (MTBE) 4.60 5.00 92.1 70-130 Methylene Chloride 3.70 5.00 74.0 70-130 4-Methyl-2-pentanone (MIBK) 5.77 5.00 115 70-130 Naphthalene 4.48 3.68 122 70-130 V-06, Z-01 Propene 5.54 5.00 111 70-130 Styrene 5.04 5.00 101 70-130 1,1,2,2-Tetrachloroethane 4.53 5.00 90.7 70-130 Tetrachloroethylene 4.30 5.00 86.0 70-130 Tetrahydrofuran 4.98 5.00 99.6 70-130 Toluene 4.91 5.00 98.2 70-130 1,2,4-Trichlorobenzene 4.10 3.90 105 70-130 1, 1, 1 -Trichloroethane 4.62 5.00 92.5 70-130 1,1,2-Trichloroethane 4.71 5.00 94.3 70-130 Trichloroethylene 4.58 5.00 91.5 70-130 Trichlorofluoromethane (Freon 11) 4.26 5.00 85.1 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 3.88 5.00 77.6 70-130 113) 1,2,4-Trimethylbenzene 5.27 5.00 105 70-130 1,3,5-Trimethylbenzene 5.23 5.00 105 70-130 Vinyl Acetate 4.66 5.00 93.3 70-130 Vinyl Chloride 4.73 5.00 94.6 70-130 m&p-Xylene 10.3 10.0 103 70-130 o-Xylene 5.12 5.00 102 70-130 Surrogate: 4-BromoJluorobenzene (1) 7.65 8.00 95.7 70-130 Page 77 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. B-05 Data is not affected by elevated level in laboratory blank since sample(s) result is "Not Detected". E Reported result is estimated. Value reported over verified calibration range. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). L-01 Laboratory fortified blank/laboratory control sample recovery outside of control limits. Data validation is not affected since all results are 'hot detected" for all samples in this batch for this compound and bias is on the high side. L-03 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the low side. L-05 Laboratory fortified blank/laboratory control sample recovery is outside of control limits. Reported value for this compound is likely to be biased on the high side. R-01 Duplicate RPD is outside of control limits. Reduced precision is anticipated for reported result. V-06 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. Page 78 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted V-20 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Z-01 Calibrations RSD for this compound is >30% but <40%. ANALYST TPH Thomas P. Hnitecki RLF Rebecca Faust KMC Kristen M Couture CMR Catherine M. Rouleau Page 79 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (5085380-ICV1 Lab File ID: J23A090036.D Analyzed: 04/01/23 05:53 Bromochloromethane (1) 298104 2.788 298104 2.788 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 850179 3.418 850179 3.418 100 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 747035 5.036 747035 5.036 100 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S089166-CCV1) Lab File ID: J23A165004.13 Analyzed: 06/14/23 11:35 Bromochloromethane (1) 243052 2.812 243052 2.812 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 634620 3.435 634620 3.435 100 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 559979 5.039 559979 5.039 100 60-140 0.0000 +/-0.50 LCS (B343424-BS1 ) Lab File ID: J23AI65005.D Analyzed: 06/14/23 12:00 Bromochloromethane (1) 240733 2.812 243052 2.812 99 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 632972 3.434 634620 3.435 100 60-140 -0.0010 +/-0.50 Chlorobenzene-d5(1) 567474 5.038 559979 5.039 101 60-140 -0.0010 +/-0.50 Blank (B343424-BLK1) Lab File ID: J23AI65008.D Analyzed: 06/14/23 13:31 Bromochloromethane (1) 228234 2.791 243052 2.812 94 60 - 140 -0.0210 +/-0.50 1,4-Difluorobenzene(1) 564248 3.422 634620 3.435 89 60-140 -0.0130 +/-0.50 Chlorobenzene-d5(1) 503022 5.036 559979 5.039 90 60-140 -0.0030 +/-0.50 IA-1 (23F1309-01 ) Lab File ID: J23A165010.D Analyzed: 06/14/23 14:35 Bromochloromethane (1) 242501 2.797 243052 2.812 100 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 620196 3.419 634620 3.435 98 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 567575 5.038 559979 5.039 101 60-140 -0.0010 +/-0.50 IA-2 (23F1309-02 ) Lab File ID: J23AI65011.13 Analyzed: 06/14/23 15:06 Bromochloromethane (1) 239563 2.792 243052 2.812 99 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 625272 3.419 634620 3.435 99 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 573268 5.033 559979 5.039 102 60-140 -0.0060 +/-0.50 IA-3 (23F1309-03) Lab File ID: J23A165012.1) Analyzed: 06/14/23 15:37 Bromochloromethane (1) 245625 2.792 243052 2.812 101 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 641829 3.419 634620 3.435 101 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 582239 5.038 559979 5.039 104 60-140 -0.0010 +/-0.50 IA-5 (23F1309-04) Lab File ID: J23A165013.1) Analyzed: 06/14/23 16:08 Bromochloromethane (1) 251352 2.797 243052 2.812 103 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 667089 3.425 634620 3.435 105 60-140 -0.0100 +/-0.50 Chlorobenzene-d5(1) 601370 5.035 559979 5.039 107 60-140 -0.0040 +/-0.50 Page 80 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q IA-6 (23F1309-05) Lab File ID: J23AI65014.D Analyzed: 06/14/23 16:40 Bromochloromethane (1) 251054 2.797 243052 2.812 103 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 672579 3.425 634620 3.435 106 60-140 -0.0100 +/-0.50 Chlorobenzene-d5(1) 615826 5.037 559979 5.039 110 60-140 -0.0020 +/-0.50 IA-7 (23F1309-06) Lab File ID: J23AI65015.D Analyzed: 06/14/23 17:11 Bromochloromethane (1) 258019 2.792 243052 2.812 106 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 688676 3.419 634620 3.435 109 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 626256 5.038 559979 5.039 112 60-140 -0.0010 +/-0.50 IA-7 DUP (23171309-07) Lab File ID: J23A165016.D Analyzed: 06/14/23 17:44 Bromochloromethane (1) 254067 2.796 243052 2.812 105 60 - 140 -0.0160 +/-0.50 1,4-Difluorobenzene(1) 685809 3.424 634620 3.435 108 60-140 -0.0110 +/-0.50 Chlorobenzene-d5(1) 620243 5.038 559979 5.039 111 60-140 -0.0010 +/-0.50 IA-9 (23171309-08) Lab File ID: J23A165017.D Analyzed: 06/14/23 18:16 Bromochloromethane (1) 253456 2.792 243052 2.812 104 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 688098 3.419 634620 3.435 108 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 623592 5.033 559979 5.039 111 60-140 -0.0060 +/-0.50 IA-10 (23F1309-09 ) Lab File ID: J23AI65018.D Analyzed: 06/14/23 18:48 Bromochloromethane (1) 262336 2.792 243052 2.812 108 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 701519 3.419 634620 3.435 ill 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 630233 5.037 559979 5.039 113 60-140 -0.0020 +/-0.50 IA-11 (23171309-10 ) Lab File ID: J23AI65019.D Analyzed: 06/14/23 19:21 Bromochloromethane (1) 263020 2.792 243052 2.812 108 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 710280 3.419 634620 3.435 112 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 648980 5.037 559979 5.039 116 60-140 -0.0020 +/-0.50 IA-12 (23F1309-11 ) Lab File ID: J23A165020.1) Analyzed: 06/14/23 19:53 Bromochloromethane (1) 262162 2.797 243052 2.812 108 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 708308 3.425 634620 3.435 112 60-140 -0.0100 +/-0.50 Chlorobenzene-d5(1) 643209 5.037 559979 5.039 115 60-140 -0.0020 +/-0.50 Duplicate (B343424-DUP1) Lab File ID: J23AI65021.13 Analyzed: 06/14/23 20:24 Bromochloromethane (1) 261069 2.792 243052 2.812 107 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 718804 3.419 634620 3.435 113 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 650330 5.038 559979 5.039 116 60-140 -0.0010 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Reference Reference Area 9 o RT Diff Internal Standard Response RT Response RT Area % Limits 11 RT Diff Limit Q Page 81 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S089178-CCV1) Lab File ID: J23AI65004.D Analyzed: 06/14/23 11:35 Bromochloromethane (1) 243052 2.812 243052 2.812 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 634620 3.435 634620 3.435 100 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 559979 5.039 559979 5.039 100 60-140 0.0000 +/-0.50 LCS (B343439-BS1 ) Lab File ID: J23AI65022.D Analyzed: 06/14/23 20:50 Bromochloromethane (1) 264202 2.812 243052 2.812 109 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 728393 3.43 634620 3.435 115 60-140 -0.0050 +/-0.50 Chlorobenzene-d5(1) 644511 5.039 559979 5.039 115 60-140 0.0000 +/-0.50 Blank (B343439-BLK1) Lab File ID: J23A165025.D Analyzed: 06/14/23 22:20 Bromochloromethane (1) 243900 2.791 243052 2.812 100 60 - 140 -0.0210 +/-0.50 1,4-Difluorobenzene(1) 644004 3.417 634620 3.435 101 60-140 -0.0180 +/-0.50 Chlorobenzene-d5(1) 568973 5.035 559979 5.039 102 60-140 -0.0040 +/-0.50 IA-14 (23F1309-12 ) Lab File ID: J23A165026.D Analyzed: 06/14/23 22:52 Bromochloromethane (1) 256832 2.797 243052 2.812 106 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 683144 3.425 634620 3.435 108 60-140 -0.0100 +/-0.50 Chlorobenzene-d5(1) 617630 5.033 559979 5.039 110 60-140 -0.0060 +/-0.50 IA-13 (231T1309-13 ) Lab File ID: J23AI65027.D Analyzed: 06/14/23 23:23 Bromochloromethane (1) 258526 2.792 243052 2.812 106 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 687716 3.419 634620 3.435 108 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 628316 5.037 559979 5.039 112 60-140 -0.0020 +/-0.50 IA-16 (23F1309-14 ) Lab File ID: J23A165028.D Analyzed: 06/14/23 23:55 Bromochloromethane (1) 253071 2.792 243052 2.812 104 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 689966 3.418 634620 3.435 109 60-140 -0.0170 +/-0.50 Chlorobenzene-d5(1) 629061 5.033 559979 5.039 112 60-140 -0.0060 +/-0.50 IA-17 (231T1309-15 ) Lab File ID: J23A165029.1) Analyzed: 06/15/23 00:27 Bromochloromethane (1) 256102 2.792 243052 2.812 105 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 691576 3.418 634620 3.435 109 60-140 -0.0170 +/-0.50 Chlorobenzene-d5(1) 626810 5.033 559979 5.039 112 60-140 -0.0060 +/-0.50 IA-18 (23171309-16) Lab File ID: J23AI65030.13 Analyzed: 06/15/23 00:58 Bromochloromethane (1) 254088 2.792 243052 2.812 105 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 699056 3.419 634620 3.435 110 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 637318 5.034 559979 5.039 114 60-140 -0.0050 +/-0.50 IA-19 (23F1309-17) Lab File ID: J23AI6503 LD Analyzed: 06/15/23 01:29 Bromochloromethane (1) 260663 2.792 243052 2.812 107 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 717163 3.419 634620 3.435 113 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 649021 5.038 559979 5.039 116 60-140 -0.0010 +/-0.50 Page 82 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q IA-23 (23F1309-19) Lab File ID: J23AI65032.1) Analyzed: 06/15/23 02:01 Bromochloromethane (1) 265490 2.792 243052 2.812 109 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 741705 3.419 634620 3.435 117 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 670153 5.037 559979 5.039 120 60-140 -0.0020 +/-0.50 IA-15 (23F1309-20 ) Lab File ID: J23AI65033.D Analyzed: 06/15/23 02:32 Bromochloromethane (1) 261348 2.792 243052 2.812 108 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 736046 3.419 634620 3.435 116 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 661437 5.033 559979 5.039 118 60-140 -0.0060 +/-0.50 IA-24 (23F1309-21 ) Lab File ID: J23AI65034.D Analyzed: 06/15/23 03:04 Bromochloromethane (1) 265906 2.797 243052 2.812 109 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 737415 3.423 634620 3.435 116 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 673265 5.037 559979 5.039 120 60-140 -0.0020 +/-0.50 IA-25 (23F1309-22 ) Lab File ID: J23A165035.D Analyzed: 06/15/23 03:35 Bromochloromethane (1) 266433 2.792 243052 2.812 110 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 729490 3.423 634620 3.435 115 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 670338 5.037 559979 5.039 120 60-140 -0.0020 +/-0.50 IA-25 DUP (23F1309-23) Lab File ID: J23A165036.D Analyzed: 06/15/23 04:06 Bromochloromethane (1) 259419 2.792 243052 2.812 107 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 704956 3.423 634620 3.435 111 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 643932 5.037 559979 5.039 115 60-140 -0.0020 +/-0.50 IA-21 (23F1309-24 ) Lab File ID: J23A165037.D Analyzed: 06/15/23 04:37 Bromochloromethane (1) 262112 2.792 243052 2.812 108 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 718279 3.423 634620 3.435 113 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 640527 5.037 559979 5.039 114 60-140 -0.0020 +/-0.50 OA (23F1309-25) Lab File ID: J23A165038.1) Analyzed: 06/15/23 05:08 Bromochloromethane (1) 257195 2.791 243052 2.812 106 60 - 140 -0.0210 +/-0.50 1,4-Difluorobenzene(1) 685303 3.418 634620 3.435 108 60-140 -0.0170 +/-0.50 Chlorobenzene-d5(1) 628137 5.037 559979 5.039 112 60-140 -0.0020 +/-0.50 IA-22 (23F1309-26) Lab File ID: J23AI65039.13 Analyzed: 06/15/23 05:39 Bromochloromethane (1) 256695 2.792 243052 2.812 106 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 683647 3.419 634620 3.435 108 60-140 -0.0160 +/-0.50 Chlorobenzene-d5(1) 627110 5.037 559979 5.039 112 60-140 -0.0020 +/-0.50 IA-4 (23F1309-27) Lab File ID: J23A165040.13 Analyzed: 06/15/23 06:10 Bromochloromethane (1) 254495 2.792 243052 2.812 105 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 682963 3.423 634620 3.435 108 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 625130 5.033 559979 5.039 112 60-140 -0.0060 +/-0.50 Page 83 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q IA-8 (23F1309-28) Lab File ID: J23A165041.D Analyzed: 06/15/23 06:41 Bromochloromethane (1) 257399 2.792 243052 2.812 106 60 - 140 -0.0200 +/-0.50 1,4-Difluorobenzene(1) 691394 3.423 634620 3.435 109 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 634567 5.038 559979 5.039 113 60-140 -0.0010 +/-0.50 Duplicate (B343439-DUP1) Lab File ID: J23AI65042.D Analyzed: 06/15/23 07:12 Bromochloromethane (1) 255936 2.797 243052 2.812 105 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 682206 3.423 634620 3.435 107 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 628121 5.038 559979 5.039 112 60-140 -0.0010 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q Calibration Check (S089198-CCV1) Lab File ID: J23AI66014.D Analyzed: 06/15/23 15:13 Bromochloromethane (1) 294149 2.812 294149 2.812 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 764052 3.435 764052 3.435 100 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 678403 5.038 678403 5.038 100 60-140 0.0000 +/-0.50 LCS (B343523-BS1 ) Lab File ID: J23AI66015.D Analyzed: 06/15/23 15:38 Bromochloromethane (1) 302331 2.812 294149 2.812 103 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 772023 3.434 764052 3.435 101 60-140 -0.0010 +/-0.50 Chlorobenzene-d5(1) 677605 5.038 678403 5.038 100 60-140 0.0000 +/-0.50 Blank (B343523-BLK1) Lab File ID: J23AI66018.D Analyzed: 06/15/23 17:11 Bromochloromethane (1) 280250 2.796 294149 2.812 95 60 - 140 -0.0160 +/-0.50 1,4-Difluorobenzene(1) 701403 3.422 764052 3.435 92 60-140 -0.0130 +/-0.50 Chlorobenzene-d5(1) 617604 5.035 678403 5.038 91 60-140 -0.0030 +/-0.50 IA-1 (23171309-01RE1) Lab File ID: J23AI66023.D Analyzed: 06/15/23 19:25 Bromochloromethane (1) 294735 2.797 294149 2.812 100 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 732673 3.423 764052 3.435 96 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 668261 5.038 678403 5.038 99 60-140 0.0000 +/-0.50 IA-2 (23171309-02RE1) Lab File ID: J23A166024.D Analyzed: 06/15/23 19:51 Bromochloromethane (1) 292597 2.796 294149 2.812 99 60 - 140 -0.0160 +/-0.50 1,4-Difluorobenzene(1) 728673 3.423 764052 3.435 95 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 655135 5.037 678403 5.038 97 60-140 -0.0010 +/-0.50 IA-3 (23171309-03RE1) Lab File ID: J23A166025.D Analyzed: 06/15/23 20:17 Bromochloromethane (1) 292375 2.796 294149 2.812 99 60 - 140 -0.0160 +/-0.50 1,4-Difluorobenzene(1) 736398 3.424 764052 3.435 96 60-140 -0.0110 +/-0.50 Chlorobenzene-d5(1) 658660 5.037 678403 5.038 97 60-140 -0.0010 +/-0.50 Page 84 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q IA-10 (23F1309-09RE1) Lab File ID: J23AI66026.D Analyzed: 06/15/23 20:44 Bromochloromethane (1) 291663 2.797 294149 2.812 99 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 745485 3.423 764052 3.435 98 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 661349 5.038 678403 5.038 97 60-140 0.0000 +/-0.50 IA-11 (23F1309-10RE1 Lab File ID: J23AI66027.D Analyzed: 06/15/23 21:10 Bromochloromethane (1) 294727 2.797 294149 2.812 100 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 747449 3.423 764052 3.435 98 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 666054 5.038 678403 5.038 98 60-140 0.0000 +/-0.50 IA-12 (23F1309-11RE1) Lab File ID: J23AI66028.D Analyzed: 06/15/23 21:37 Bromochloromethane (1) 290370 2.797 294149 2.812 99 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 737160 3.423 764052 3.435 96 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 669890 5.038 678403 5.038 99 60-140 0.0000 +/-0.50 Duplicate (B343523-DUP1) Lab File ID: J23AI66029.D Analyzed: 06/15/23 22:04 Bromochloromethane (1) 289209 2.797 294149 2.812 98 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 734652 3.423 764052 3.435 96 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 661912 5.037 678403 5.038 98 60-140 -0.0010 +/-0.50 IA-14 (23F1309-12RE1) Lab File ID: J23AI66030.D Analyzed: 06/15/23 22:30 Bromochloromethane (1) 289450 2.797 294149 2.812 98 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 740608 3.423 764052 3.435 97 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 659481 5.038 678403 5.038 97 60-140 0.0000 +/-0.50 IA-13 (23F1309-13RE1) Lab File ID: J23AI6603 LD Analyzed: 06/15/23 22:57 Bromochloromethane (1) 295457 2.797 294149 2.812 100 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 743200 3.424 764052 3.435 97 60-140 -0.0110 +/-0.50 Chlorobenzene-d5(1) 670101 5.038 678403 5.038 99 60-140 0.0000 +/-0.50 IA-18 (23F1309-16RE1) Lab File ID: J23A166032.D Analyzed: 06/15/23 23:23 Bromochloromethane (1) 286914 2.797 294149 2.812 98 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 741515 3.424 764052 3.435 97 60-140 -0.0110 +/-0.50 Chlorobenzene-d5(1) 668976 5.033 678403 5.038 99 60-140 -0.0050 +/-0.50 IA-19 (23F1309-17RE1) Lab File ID: J23AI66033.13 Analyzed: 06/15/23 23:49 Bromochloromethane (1) 298212 2.797 294149 2.812 101 60 - 140 -0.0150 +/-0.50 1,4-Difluorobenzene(1) 756874 3.423 764052 3.435 99 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 683279 5.038 678403 5.038 101 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREA AND RT SUMMARY EPA TO-15 Reference Reference Area 9 o RT Diff Internal Standard Response RT Response RT Area % Limits 11 RT Diff Limit Q Page 85 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S089293-CCV1) Lab File ID: J23AI67004.D Analyzed: 06/16/23 10:06 Bromochloromethane (1) 289197 2.812 289197 2.812 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 725179 3.434 725179 3.434 100 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 640163 5.039 640163 5.039 100 60-140 0.0000 +/-0.50 LCS (B343662-BS1 ) Lab File ID: J23AI67005.D Analyzed: 06/16/23 10:31 Bromochloromethane (1) 287884 2.812 289197 2.812 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 736213 3.435 725179 3.434 102 60-140 0.0010 +/-0.50 Chlorobenzene-d5(1) 646258 5.038 640163 5.039 101 60-140 -0.0010 +/-0.50 Blank (B343662-BLK1) Lab File ID: J23A167008.D Analyzed: 06/16/23 12:11 Bromochloromethane (1) 277891 2.796 289197 2.812 96 60 - 140 -0.0160 +/-0.50 1,4-Difluorobenzene(1) 667865 3.422 725179 3.434 92 60-140 -0.0120 +/-0.50 Chlorobenzene-d5(1) 592858 5.035 640163 5.039 93 60-140 -0.0040 +/-0.50 IA-23 (23F1309-19RE1) Lab File ID: J23A167009.D Analyzed: 06/16/23 12:36 Bromochloromethane (1) 278496 2.796 289197 2.812 96 60 - 140 -0.0160 +/-0.50 1,4-Difluorobenzene(1) 682401 3.423 725179 3.434 94 60-140 -0.0110 +/-0.50 Chlorobenzene-d5(1) 621470 5.037 640163 5.039 97 60-140 -0.0020 +/-0.50 IA-15 (23F1309-20RE1) Lab File ID: J23A167010.D Analyzed: 06/16/23 13:01 Bromochloromethane (1) 279480 2.796 289197 2.812 97 60 - 140 -0.0160 +/-0.50 1,4-Difluorobenzene(1) 683473 3.423 725179 3.434 94 60-140 -0.0110 +/-0.50 Chlorobenzene-d5(1) 624397 5.037 640163 5.039 98 60-140 -0.0020 +/-0.50 Page 86 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089166-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 4.21 1.034114 0.8713592 -15.7 30 Benzene A 5.00 5.11 0.8123645 0.8299341 2.2 30 Benzyl chloride L 5.00 4.36 0.5056852 0.6616191 -12.8 30 Bromodichloromethane A 5.00 5.14 0.6094342 0.6265999 2.8 30 Bromoform A 5.00 5.58 0.4573839 0.5104991 11.6 30 Bromomethane A 5.00 4.79 0.6761959 0.6481444 -4.1 30 1,3-Butadiene A 5.00 5.47 0.5092257 0.5567335 9.3 30 2-Butanone (MEK) A 5.00 6.00 1.148647 1.377272 19.9 30 Carbon Disulfide A 5.00 4.31 2.001154 1.723588 -13.9 30 Carbon Tetrachloride A 5.00 5.42 0.5037067 0.5456821 8.3 30 Chlorobenzene A 5.00 4.81 0.7622773 0.7338418 -3.7 30 Chloroethane A 5.00 4.95 0.4202137 0.4162072 -1.0 30 Chloroform A 5.00 4.77 1.577837 1.506009 -4.6 30 Chloromethane A 5.00 5.22 0.5966374 0.6233728 4.5 30 Cyclohexane A 5.00 5.34 0.3246406 0.3464801 6.7 30 Dibromochloromethane A 5.00 5.57 0.5189836 0.5780245 11.4 30 1,2-Dibromoethane (EDB) A 5.00 5.18 0.4960864 0.5141993 3.7 30 1,2-Dichlorobenzene A 5.00 5.68 0.4911951 0.5576666 13.5 30 1,3-Dichlorobenzene A 5.00 5.31 0.5456808 0.5791446 6.1 30 1,4-Dichlorobenzene A 5.00 5.30 0.5309926 0.562824 6.0 30 Dichlorodifluoromethane (Freon 12) A 5.00 5.48 1.809285 1.981936 9.5 30 1,1-Dichloroethane A 5.00 5.01 1.317427 1.319632 0.2 30 1,2-Dichloroethane A 5.00 4.82 0.9730911 0.9371098 -3.7 30 1,1-Dichloroethylene A 5.00 4.66 1.146845 1.068479 -6.8 30 cis-1,2-Dichloroethylene A 5.00 5.06 0.9524103 0.9634482 1.2 30 trans-1,2-Dichloroethylene A 5.00 5.13 1.02979 1.057295 2.7 30 1,2-Dichloropropane A 5.00 5.24 0.3033695 0.3177788 4.7 30 cis-1,3-Dichloropropene A 5.00 5.65 0.4042769 0.4570773 13.1 30 trans- l,3-Dichloropropene A 5.00 5.89 0.3279415 0.3864965 17.9 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 4.90 1.964888 1.924408 -2.1 30 1,4-Dioxane A 5.00 5.02 0.1624784 0.1632826 0.5 30 Ethanol A 5.00 4.64 0.1724202 0.1601764 -7.1 30 Ethyl Acetate A 5.00 5.19 0.2040016 0.2118065 3.8 30 Ethylbenzene A 5.00 5.39 1.293794 1.394149 7.8 30 4-Ethyltoluene A 5.00 5.72 1.173601 1.341865 14.3 30 Heptane A 5.00 5.73 0.2390228 0.2739832 14.6 30 Hexachlorobutadiene A 5.00 8.66 0.2261563 0.3916633 73.2 30 Hexane L 5.00 4.59 0.6738496 0.6217797 -8.3 30 Page 87 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089166-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 5.20 0.4320676 0.4489083 3.9 30 Isopropanol A 5.00 4.52 1.163166 1.050824 -9.7 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.92 1.752887 1.724168 -1.6 30 Methylene Chloride A 5.00 3.95 0.8161184 0.6440498 -21.1 30 4-Methyl-2-pentanone (MI13K) A 5.00 5.99 0.1991676 0.2384999 19.7 30 Naphthalene A 5.00 7.45 0.4140914 0.6167946 49.0 30 Propene A 5.00 6.28 0.3783566 0.4751444 25.6 30 Styrene A 5.00 5.88 0.6193387 0.7285559 17.6 30 1,1,2,2-Tetrachloroethane A 5.00 5.43 0.7875453 0.8546435 8.5 30 Tetrachloroethylene A 5.00 4.90 0.4061033 0.3980121 -2.0 30 Tetrahydroforan A 5.00 5.01 0.5602263 0.5612824 0.2 30 Toluene A 5.00 5.34 0.9952737 1.062371 6.7 30 1,2,4-Trichlorobenzene A 5.00 6.56 0.1951236 0.2559753 31.2 30 1, 1, 1 -Trichloroethane A 5.00 5.27 0.5148362 0.5426416 5.4 30 1,1,2-Trichloroethane A 5.00 5.22 0.3494055 0.364988 4.5 30 Trichloroethylene A 5.00 5.07 0.3469588 0.3520192 1.5 30 Trichlorofluoromethane(Freon 11) A 5.00 4.94 1.832227 1.810694 -1.2 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 4.43 1.363757 1.207807 -11.4 30 1,2,4-Trimethylbenzene A 5.00 6.33 0.9035781 1.143574 26.6 30 1,3,5-Trimethylbenzene A 5.00 6.21 0.9651619 1.197971 24.1 30 Vinyl Acetate A 5.00 4.29 1.160867 0.9964551 -14.2 30 Vinyl Chloride A 5.00 5.27 0.7330867 0.7720619 5.3 30 m&p-Xylene A 10.0 11.6 1.010218 1.176028 16.4 30 o-Xylene A 5.00 5.79 0.9862305 1.141943 15.8 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 88 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089178-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 4.21 1.034114 0.8713592 -15.7 30 Benzene A 5.00 5.11 0.8123645 0.8299341 2.2 30 Benzyl chloride L 5.00 4.36 0.5056852 0.6616191 -12.8 30 Bromodichloromethane A 5.00 5.14 0.6094342 0.6265999 2.8 30 Bromoform A 5.00 5.58 0.4573839 0.5104991 11.6 30 Bromomethane A 5.00 4.79 0.6761959 0.6481444 -4.1 30 1,3-Butadiene A 5.00 5.47 0.5092257 0.5567335 9.3 30 2-Butanone (MEK) A 5.00 6.00 1.148647 1.377272 19.9 30 Carbon Disulfide A 5.00 4.31 2.001154 1.723588 -13.9 30 Carbon Tetrachloride A 5.00 5.42 0.5037067 0.5456821 8.3 30 Chlorobenzene A 5.00 4.81 0.7622773 0.7338418 -3.7 30 Chloroethane A 5.00 4.95 0.4202137 0.4162072 -1.0 30 Chloroform A 5.00 4.77 1.577837 1.506009 -4.6 30 Chloromethane A 5.00 5.22 0.5966374 0.6233728 4.5 30 Cyclohexane A 5.00 5.34 0.3246406 0.3464801 6.7 30 Dibromochloromethane A 5.00 5.57 0.5189836 0.5780245 11.4 30 1,2-Dibromoethane (EDB) A 5.00 5.18 0.4960864 0.5141993 3.7 30 1,2-Dichlorobenzene A 5.00 5.68 0.4911951 0.5576666 13.5 30 1,3-Dichlorobenzene A 5.00 5.31 0.5456808 0.5791446 6.1 30 1,4-Dichlorobenzene A 5.00 5.30 0.5309926 0.562824 6.0 30 Dichlorodifluoromethane (Freon 12) A 5.00 5.48 1.809285 1.981936 9.5 30 1,1-Dichloroethane A 5.00 5.01 1.317427 1.319632 0.2 30 1,2-Dichloroethane A 5.00 4.82 0.9730911 0.9371098 -3.7 30 1,1-Dichloroethylene A 5.00 4.66 1.146845 1.068479 -6.8 30 cis-1,2-Dichloroethylene A 5.00 5.06 0.9524103 0.9634482 1.2 30 trans-1,2-Dichloroethylene A 5.00 5.13 1.02979 1.057295 2.7 30 1,2-Dichloropropane A 5.00 5.24 0.3033695 0.3177788 4.7 30 cis-1,3-Dichloropropene A 5.00 5.65 0.4042769 0.4570773 13.1 30 trans- l,3-Dichloropropene A 5.00 5.89 0.3279415 0.3864965 17.9 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 4.90 1.964888 1.924408 -2.1 30 1,4-Dioxane A 5.00 5.02 0.1624784 0.1632826 0.5 30 Ethanol A 5.00 4.64 0.1724202 0.1601764 -7.1 30 Ethyl Acetate A 5.00 5.19 0.2040016 0.2118065 3.8 30 Ethylbenzene A 5.00 5.39 1.293794 1.394149 7.8 30 4-Ethyltoluene A 5.00 5.72 1.173601 1.341865 14.3 30 Heptane A 5.00 5.73 0.2390228 0.2739832 14.6 30 Hexachlorobutadiene A 5.00 8.66 0.2261563 0.3916633 73.2 30 Hexane L 5.00 4.59 0.6738496 0.6217797 -8.3 30 Page 89 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089178-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 5.20 0.4320676 0.4489083 3.9 30 Isopropanol A 5.00 4.52 1.163166 1.050824 -9.7 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.92 1.752887 1.724168 -1.6 30 Methylene Chloride A 5.00 3.95 0.8161184 0.6440498 -21.1 30 4-Methyl-2-pentanone (MI13K) A 5.00 5.99 0.1991676 0.2384999 19.7 30 Naphthalene A 5.00 7.45 0.4140914 0.6167946 49.0 30 Propene A 5.00 6.28 0.3783566 0.4751444 25.6 30 Styrene A 5.00 5.88 0.6193387 0.7285559 17.6 30 1,1,2,2-Tetrachloroethane A 5.00 5.43 0.7875453 0.8546435 8.5 30 Tetrachloroethylene A 5.00 4.90 0.4061033 0.3980121 -2.0 30 Tetrahydroforan A 5.00 5.01 0.5602263 0.5612824 0.2 30 Toluene A 5.00 5.34 0.9952737 1.062371 6.7 30 1,2,4-Trichlorobenzene A 5.00 6.56 0.1951236 0.2559753 31.2 30 1, 1, 1 -Trichloroethane A 5.00 5.27 0.5148362 0.5426416 5.4 30 1,1,2-Trichloroethane A 5.00 5.22 0.3494055 0.364988 4.5 30 Trichloroethylene A 5.00 5.07 0.3469588 0.3520192 1.5 30 Trichlorofluoromethane(Freon 11) A 5.00 4.94 1.832227 1.810694 -1.2 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 4.43 1.363757 1.207807 -11.4 30 1,2,4-Trimethylbenzene A 5.00 6.33 0.9035781 1.143574 26.6 30 1,3,5-Trimethylbenzene A 5.00 6.21 0.9651619 1.197971 24.1 30 Vinyl Acetate A 5.00 4.29 1.160867 0.9964551 -14.2 30 Vinyl Chloride A 5.00 5.27 0.7330867 0.7720619 5.3 30 m&p-Xylene A 10.0 11.6 1.010218 1.176028 16.4 30 o-Xylene A 5.00 5.79 0.9862305 1.141943 15.8 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 90 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089198-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 3.75 1.034114 0.7754546 -25.0 30 Benzene A 5.00 4.57 0.8123645 0.7423118 -8.6 30 Benzyl chloride L 5.00 4.02 0.5056852 0.6073275 -19.7 30 Bromodichloromethane A 5.00 4.60 0.6094342 0.56121 -7.9 30 Bromoform A 5.00 4.82 0.4573839 0.4407221 -3.6 30 Bromomethane A 5.00 4.14 0.6761959 0.5596239 -17.2 30 1,3-Butadiene A 5.00 4.89 0.5092257 0.4978919 -2.2 30 2-Butanone (MEK) A 5.00 5.60 1.148647 1.285786 11.9 30 Carbon Disulfide A 5.00 3.88 2.001154 1.554423 -22.3 30 Carbon Tetrachloride A 5.00 4.81 0.5037067 0.4848885 -3.7 30 Chlorobenzene A 5.00 4.30 0.7622773 0.6547613 -14.1 30 Chloroethane A 5.00 4.38 0.4202137 0.3678245 -12.5 30 Chloroform A 5.00 4.24 1.577837 1.338946 -15.1 30 Chloromethane A 5.00 4.30 0.5966374 0.5131549 -14.0 30 Cyclohexane A 5.00 4.84 0.3246406 0.313897 -3.3 30 Dibromochloromethane A 5.00 4.91 0.5189836 0.50971 -1.8 30 1,2-Dibromoethane (EDB) A 5.00 4.68 0.4960864 0.4642739 -6.4 30 1,2-Dichlorobenzene A 5.00 4.92 0.4911951 0.4834837 -1.6 30 1,3-Dichlorobenzene A 5.00 4.71 0.5456808 0.5143421 -5.7 30 1,4-Dichlorobenzene A 5.00 4.67 0.5309926 0.4957572 -6.6 30 Dichlorodifluoromethane (Freon 12) A 5.00 4.71 1.809285 1.704002 -5.8 30 1,1-Dichloroethane A 5.00 4.44 1.317427 1.17096 -11.1 30 1,2-Dichloroethane A 5.00 4.30 0.9730911 0.8372464 -14.0 30 1,1-Dichloroethylene A 5.00 4.15 1.146845 0.9511479 -17.1 30 cis-1,2-Dichloroethylene A 5.00 4.57 0.9524103 0.871319 -8.5 30 trans-1,2-Dichloroethylene A 5.00 4.53 1.02979 0.9332032 -9.4 30 1,2-Dichloropropane A 5.00 4.76 0.3033695 0.288839 -4.8 30 cis-1,3-Dichloropropene A 5.00 5.21 0.4042769 0.4213682 4.2 30 trans- l,3-Dichloropropene A 5.00 5.50 0.3279415 0.3604781 9.9 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 4.24 1.964888 1.666339 -15.2 30 1,4-Dioxane A 5.00 4.56 0.1624784 0.1482726 -8.7 30 Ethanol A 5.00 4.06 0.1724202 0.1399672 -18.8 30 Ethyl Acetate A 5.00 4.87 0.2040016 0.1985388 -2.7 30 Ethylbenzene A 5.00 4.81 1.293794 1.243756 -3.9 30 4-Ethyltoluene A 5.00 5.21 1.173601 1.223247 4.2 30 Heptane A 5.00 5.26 0.2390228 0.2514865 5.2 30 Hexachlorobutadiene 4 5.00 7.60 0.2261563 0.3435622 51.9 30 Hexane L 5.00 4.26 0.6738496 0.5790154 -14.7 30 Page 91 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089198-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 5.05 0.4320676 0.4365877 1.0 30 Isopropanol A 5.00 3.95 1.163166 0.9192566 -21.0 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.60 1.752887 1.611771 -8.1 30 Methylene Chloride A 5.00 3.62 0.8161184 0.5913085 -27.5 30 4-Methyl-2-pentanone (MI13K) A 5.00 5.66 0.1991676 0.2256747 13.3 30 Naphthalene A 5.00 6.96 0.4140914 0.5767663 39.3 30 Propene A 5.00 5.42 0.3783566 0.4104804 8.5 30 Styrene A 5.00 5.31 0.6193387 0.6572094 6.1 30 1,1,2,2-Tetrachloroethane A 5.00 4.86 0.7875453 0.7651594 -2.8 30 Tetrachloroethylene A 5.00 4.27 0.4061033 0.3465857 -14.7 30 Tetrahydroforan A 5.00 4.74 0.5602263 0.5312192 -5.2 30 Toluene A 5.00 4.82 0.9952737 0.9591656 -3.6 30 1,2,4-Trichlorobenzene A 5.00 6.15 0.1951236 0.2398598 22.9 30 1, 1, 1 -Trichloroethane A 5.00 4.69 0.5148362 0.4829347 -6.2 30 1,1,2-Trichloroethane A 5.00 4.59 0.3494055 0.3209538 -8.1 30 Trichloroethylene A 5.00 4.59 0.3469588 0.3183511 8.2 30 Trichlorofluoromethane(Freon 11) A 5.00 4.25 1.832227 1.558677 -14.9 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 3.93 1.363757 1.071245 -21.4 30 1,2,4-Trimethylbenzene A 5.00 5.72 0.9035781 1.033217 14.3 30 1,3,5-Trimethylbenzene A 5.00 5.45 0.9651619 1.051627 9.0 30 Vinyl Acetate A 5.00 4.34 1.160867 1.007571 -13.2 30 Vinyl Chloride A 5.00 4.64 0.7330867 0.6807543 -7.1 30 m&p-Xylene A 1 10.0 10.3 1.010218 1.04046 3.0 30 o-Xylene A 1 5.00 5.13 0.9862305 1.012144 2.6 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 92 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089293-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 3.86 1.034114 0.7994274 -22.7 30 Benzene A 5.00 4.64 0.8123645 0.7535883 -7.2 30 Benzyl chloride L 5.00 4.04 0.5056852 0.6113018 -19.2 30 Bromodichloromethane A 5.00 4.90 0.6094342 0.5968866 -2.1 30 Bromoform A 5.00 5.06 0.4573839 0.4627396 1.2 30 Bromomethane A 5.00 4.22 0.6761959 0.5710709 -15.5 30 1,3-Butadiene A 5.00 4.97 0.5092257 0.5064285 -0.5 30 2-Butanone (MEK) A 5.00 5.62 1.148647 1.291715 12.5 30 Carbon Disulfide A 5.00 3.99 2.001154 1.598285 -20.1 30 Carbon Tetrachloride A 5.00 5.04 0.5037067 0.507964 0.8 30 Chlorobenzene A 5.00 4.56 0.7622773 0.6946131 -8.9 30 Chloroethane A 5.00 4.54 0.4202137 0.3818297 -9.1 30 Chloroform A 5.00 4.31 1.577837 1.359173 -13.9 30 Chloromethane A 5.00 4.58 0.5966374 0.5465174 -8.4 30 Cyclohexane A 5.00 5.01 0.3246406 0.3254567 0.3 30 Dibromochloromethane A 5.00 5.18 0.5189836 0.5372957 3.5 30 1,2-Dibromoethane(EDB) A 5.00 4.85 0.4960864 0.4813624 -3.0 30 1,2-Dichlorobenzene A 5.00 5.28 0.4911951 0.5186854 5.6 30 1,3-Dichlorobenzene A 5.00 5.37 0.5456808 0.5856059 7.3 30 1,4-Dichlorobenzene A 5.00 5.17 0.5309926 0.5492876 3.4 30 Dichlorodifluoromethane (Freon 12) A 5.00 4.86 1.809285 1.758563 -2.8 30 1,1-Dichloroethane A 5.00 4.55 1.317427 1.199609 -8.9 30 1,2-Dichloroethane A 5.00 4.33 0.9730911 0.8425703 -13.4 30 1,1-Dichloroethylene A 5.00 4.24 1.146845 0.9728344 -15.2 30 cis-1,2-Dichloroethylene A 5.00 4.62 0.9524103 0.8809165 -7.5 30 trans-1,2-Dichloroethylene A 5.00 4.69 1.02979 0.96614 -6.2 30 1,2-Dichloropropane A 5.00 5.01 0.3033695 0.3040706 0.2 30 cis-1,3-Dichloropropene A 5.00 5.34 0.4042769 0.4315977 6.8 30 trans- l,3-Dichloropropene A 5.00 5.67 0.3279415 0.3717659 13.4 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 4.34 1.964888 1.705274 -13.2 30 1,4-Dioxane A 5.00 4.87 0.1624784 0.1582087 -2.6 30 Ethanol A 5.00 4.47 0.1724202 0.1539988 -10.7 30 Ethyl Acetate A 5.00 4.81 0.2040016 0.1962731 -3.8 30 Ethylbenzene A 5.00 5.07 1.293794 1.312476 1.4 30 4-Ethyltoluene A 5.00 5.26 1.173601 1.235388 5.3 30 Heptane A 5.00 5.51 0.2390228 0.2634825 10.2 30 Hexachlorobutadiene 4 5.00 7.85 0.2261563 0.3550471 57.0 30 Hexane L 5.00 4.34 0.6738496 0.5891237 -13.2 30 Page 93 of 102 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 S089293-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 5.22 0.4320676 0.4515325 4.5 30 Isopropanol A 5.00 4.06 1.163166 0.9457083 -18.7 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.49 1.752887 1.57387 -10.2 30 Methylene Chloride A 5.00 3.78 0.8161184 0.6167146 -24.4 30 4-Methyl-2-pentanone (MI13K) A 5.00 5.85 0.1991676 0.2331628 17.1 30 Naphthalene A 5.00 6.68 0.4140914 0.5536515 33.7 30 Propene A 5.00 5.62 0.3783566 0.4250224 12.3 30 Styrene A 5.00 5.52 0.6193387 0.6839183 10.4 30 1,1,2,2-Tetrachloroethane A 5.00 5.12 0.7875453 0.8064221 2.4 30 Tetrachloroethylene A 5.00 4.52 0.4061033 0.366929 -9.6 30 Tetrahydroforan A 5.00 4.71 0.5602263 0.5281549 -5.7 30 Toluene A 5.00 5.02 0.9952737 0.9990106 0.4 30 1,2,4-Trichlorobenzene A 5.00 5.94 0.1951236 0.231766 18.8 30 1, 1, 1 -Trichloroethane A 5.00 4.94 0.5148362 0.5084119 -1.2 30 1,1,2-Trichloroethane A 5.00 4.86 0.3494055 0.339696 -2.8 30 Trichloroethylene A 5.00 4.79 0.3469588 0.3321663 -4.3 30 Trichlorofluoromethane(Freon 11) A 5.00 4.34 1.832227 1.590169 -13.2 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 3.97 1.363757 1.083613 -20.5 30 1,2,4-Trimethylbenzene A 5.00 5.98 0.9035781 1.080532 19.6 30 1,3,5-Trimethylbenzene A 5.00 5.85 0.9651619 1.12903 17.0 30 Vinyl Acetate A 5.00 4.10 1.160867 0.9514511 -18.0 30 Vinyl Chloride A 5.00 4.74 0.7330867 0.6951607 -5.2 30 m&p-Xylene A 10.0 11.0 1.010218 1.106877 9.6 30 o-Xylene A 5.00 5.46 0.9862305 1.075963 9.1 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 94 of 102 con-testo A Face Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Acetone Benzene Benzyl chloride Bromodichloromethane Bromoform Bromomethane 1,3-Butadiene 2-Butanone (MEK) Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Cyclohexane Dibromochloromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane (Freon 12) 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans- l,2-Dichloro ethylene 1,2-Dichloropropane cis- 1,3 -Dichloropropene trans- 1, 3 -Dichloropropene 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 1,4-Dioxane Ethanol Ethyl Acetate Ethylbenzene 4-Ethyltoluene Heptane Hexachlorobutadiene Hexane 2-Hexanone (MBK) Isopropanol Methyl tart -Butyl Ether (MTBE) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Naphthalene Propene Styrene 1,1,2,2-Tetrachloroethane Certifications AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA, FL,NJ,NY,ME,NH, VA AIHA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH NY,ME,NH AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA Page 95 of 102 con-testo A Face Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Tetrachloroethylene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichlorofluoromethane (Freon 11) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl Chloride m&p-Xylene o-Xylene Certifications AIHA,FL,NJ,NY,ME,NH, VA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation: Code Description Number Expires AHIA AIHA-LAP, LLC - ISO 17025:2017 100033 03/l/2024 NY New York State Department of Health 10899 NELAP 04/1/2024 NH New Hampshire Environmental Lab 2516 NELAP 02/5/2024 NJ New Jersey DEP MA007 NELAP 06/30/2023 FL Florida Department of Health E871027 NELAP 06/30/2024 ME State of Maine MA00100 06/9/2025 VA Commonwealth of Virginia 460217 12/14/2023 Page 96 of 102 I V o.: D ;R m m d N C) O V � � a�3 o W Cr. N V7 r �I J m a M u 0 0 Lab Receipt Pressure Final Pressure Initial Pressure 451-7 v V w M2iN.-- a T T J fO fO W o n � r V w L ❑ q a n or w L: ° c.1 Cze Z v ovn E Z E C � N O '._' 2 O 2 Ua a s a a a Do � M !"'1 tin 1+1 M e•►► fir► r++ N Lr► 9s � ,y/v ,,[� /� rym [T Ta 171, fr M !+► h� s++. !'� t+ y�. T a' J E_ %% � ~ ~ Act. o,& La f� H H H% N H,- 414 1 J � o Q — m ■■ E E E v , N a G O lz� v y a ( C a Page 97 of 102 a' w U• O" a '0 � a CD Q un a z 0 (U Ew V i v UJ CL C, w LLJ Nn uh r � TE J n �t u 0 0 AY N qC �. ` Ir T O d 19, ,9 IA V+ .1 d' i � � r m m a�wQ � U.... C'm r.+l M M M M 111 r� �� �[ a C U o Dm d�.0 ?� LO Cr en 0 Lab Receipt Pressure �E e C� $ Final Pressure t Initial Pressure M � „� N N Q C m a a v � c � A 7 C o V Y W )-0 5 1 g� �C x �[ x %C K 7� rL a o R 3 (U u 7t U U1 J u ❑ L� U C K 3v ❑❑ ec � C 0 fJ 6"YUC O1 _t li. 7 U d_7 a x u; Z O x O u y Via; s az'N E J F r 1+ L 0. X C 3 a: -511 MQq+p�flP�n a s�a a a s'a 4 N n E p p v+ N u J d o v a 4 Vt LAlp ..`" r4 N 4 N tJ z 49E 1z -Cr Q Q%r Q `- fNNHHH H H Cr 47 Jr � vv— U rot3l m y V a o zZA "a „ C W "o a> Uj E E ¢ a a a a a v°i ... , _ v Q ElU C 30 C r6 7 0 0 C t, C W x ❑ ❑ ❑ 0 z L v C an C on a T - T d j 0 ff CK cc: ne Page 99 of 102 Lab Receipt Pressure Final Pressure Initial Pressure �s"7 d�rw s�-ol, x m b N > „Y'3 W o o u a W O r %j, O" a O z rx✓ d 0 G O Y 11w LL. u Q U W 1L 0 �Vy F'1 2 N � + Ln LA � � m � s ci v 0 aX# a # u s aU �v It a' Ir 3 �U. E C V C �G d' E z a c m u Z u :F u 0 d v [ C� V ' L 1 Q Q O . Oj E U H 95 Q Q W W Q U l7 0 m NC U O d Coa J L x N Z E€ :) e m u NI[ to J it r{ V] Q N O m i m v A a rn N T � � n � n -V 4 72 > a > Cr w U Z au Of Ix Page 100 of 102 6/ 12/23, 9:27 AM Detailed Tracking FedEx® Tracking TRACKING ID Mufti -piece shipment 772371658582 (master) Multi -piece shipment 772371659762 MUlti-piece shipment 772371659887 Multi -piece shipment 772371659144 Multi -piece shipment 772371659648 Multi -piece shipment 772371659442 Multi -piece shipment 772371659876 Summary Tracking Results SHIPPER SHIP CITY RECIPIENT CITY, STATUS DATE STATE STATE DELIVERY DATE 6/07/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/09/2023 1,29 pm 6/07/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/09/2023 1:29 pm 6/07/2023 RALEIGH, INC EAST LONGMEADOW, MA Delivered 6/09/2023 1 29 pm 6/07/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/09/2023 1:29 pm 6/07/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/09/2023 1:79 pm 610712023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/09/2023 1:29 pm 6/07/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/09/2023 1 29 pm Mufti -piece shipment 772371659773 6/07/2023 RALEIGH, NC LAST LONGMEADOW, MA Delivered 6/U9/2023 4:34 pm OUR COMPANY About FedEx(https://www.fedex.com/en-us/about.html) Cur Portfolio(hops://www.fedex.cam/en-us/about/company-structure htrnl) Investor Relations(https://investors.fedex.com/home/default.aspx) Careers(https://careers.fedex.ccm/fedex/) FedEx BIog(https1/www.fedex.com/en-us/blog.him]) Corporate Responsibility(httpS://WWWLfedex.com/en-us/about/corporate-social-respons€bility.htrnl) Newsroom(https://newsroom.fedex.com/) Contact Us(https://www.fedex.com/en-us/customer-support/contact-us.htmi) SCHEDULED DELIVERY DATE OBTAIN PROOF OF DELIVER) https://www.fedex.com/fedextrack/summary?trknbr=772371658582,772371659762,772371659887,772371659144,772371659648,7723 Page 101 of 102 39 Spruce St. East Longmeadow, MA. 01028 P: 413-525-2332 F:413-525-6405 www.pacelabs.com ENV-FRM-ELON-0009V02_Air Sample Receiving Checklist 1-12-2023 Log In Back -Sheet Login Sample Receipt Checklist —(Rejection Criteria Listing — Using Acceptance Policy) Any False statement will be Peav-Le AOYANC1NG SCIMCe brought to the attention of the Client —True or False True False Client._iQt�C�_ `G�t�t�C ��SCCiC� r lfrC. Project_ LOML( (Mf�q ) Mt�, 3) MCP/RCP Required Deliverable Package Requirement Location 14 PWSID# (When Applicable) Arrival Method°C CX 1-123 '1W5 SE,'�7- Received By / Date / Time V-MC, CaIq IL `t33 Ca Back -Sheet By / Date / Time (L I t Z IZ.3 QA C Temperature Method Temp < 6o C ❑ Actual Temperature Rush Samples: Yes / Notify Short Hold: Yes / Notify Notes regarding Samples/COC Outside Of SOP: Ccky\ e (�—t io cell tiv eci y'v'�Y� ❑ Received on Ice ❑ Received in Cooler ❑ Custody Seal: DATE TIME ® ❑ COC Relinquished ® ❑ COC/Samples Labels Agree © ❑ All Samples in Good Condition ® ❑ Samples Received within Holdin Time © ❑ Is there enough Volume ® ❑ Proper Media/Container Used Individually Certified Cans C'� ® ❑ ❑ Trip Blanks IZI ❑ COC Legible COC Included: (Check all included) Client © Analysis© Sampler Name El ProjectEl ID5 ® Collection Date/Time El Ili #'S 8 tit { i 16 2 24 8 7 t 2 16 3 Z cjL. 24 1 9 LciUq 17 1� `J 25 113 1 2sL�I j 9 7j'L41-$ 17 4.JC1H 25 q 2 Ats3�� 10 s61 18 26 icictl 2 `7C)� 10 114 3 18 2r' 3 t 11 \' 4J 19 1l)s5� 27 �% ac Q 3 F?Iu 11 ' ) —1 19 3(A 27 h 1tt 4 i �l i2 \\,J CI 20 i-1i 28 i1 T � 4 .3H-6q 12 �� � L 20 IL:q 28 �1 � 5 � 13 21 4C .f 29 5 35C P 13 y`tI L4 21 Ct 29 6`r\ 14 t�3 22 �(��� 30 613) 14 �2_r 22 3GS 30 7 l�SiiQ 15 Zv5�3�J 23 2Ci4 31 7 3�� 15 'l 23 3L{tj�$ 31 nuset�Me i 8 16 24 �uf'(fl i +�, 8 16 24 1 \ 9 17 25 1 9 17 25 2 3 G 10 18 26 2 10 18 26 3 t Ci 11 19 27 3 11 19 27 4 1J��\� 12 20 28 4 12 20 28 5i-� 13 21 29 5 13 21 29 6 14 22 30 6 14 22 30 7 15 23 31 7 15 23 Page 102 Of 102 APPENDIX E LABORATORY ANALYTICAL REPORTS AND CHAIN -OF -CUSTODY RECORDS FOR SUB -SLAB SOIL GAS SAMPLES U Mid Atlantic con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 June 19, 2023 Nolen Barefoot Mid -Atlantic Associates, Inc. - Raleigh, NC 409 Rogers View Court Raleigh, NC 27610 Project Location: Raleigh, NC Client Job Number: Project Number: R3746.00 Laboratory Work Order Number: 23F1634 Enclosed are results of analyses for samples as received by the laboratory on June 13, 2023. If you have any questions concerning this report, please feel free to contact me. Sincerely, Rebecca Faust Project Manager QA Officer Katherine Allen Laboratory Manager Daren Damboragian Page 1 of 84 con-testo A Pace Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Mid -Atlantic Associates, Inc. - Raleigh, NC REPORT DATE: 6/19/2023 409 Rogers View Court Raleigh, NC 27610 PURCHASE ORDER NUMBER: ATTN: Nolen Barefoot PROJECT NUMBER: R3746.00 ANALYTICAL SUMMARY WORK ORDER NUMBER: 23F1634 The results of analyses performed on the following samples submitted to Con -Test, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: Raleigh, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB MP-25 23F1634-01 Sub Slab EPA TO-15 MP-24 23171634-02 Sub Slab EPA TO-15 MP-23 23F1634-03 Sub Slab EPA TO-15 MP-15 23171634-04 Sub Slab EPA TO-15 MP-21 23171634-05 Sub Slab EPA TO-15 MP-22 23F1634-06 Sub Slab EPA TO-15 MP-20 23171634-07 Sub Slab EPA TO-15 MP-19 23171634-08 Sub Slab EPA TO-15 MP-18 23F1634-09 Sub Slab EPA TO-15 MP-17 23171634-10 Sub Slab EPA TO-15 MP-16 23171634-11 Sub Slab EPA TO-15 MP-13 23F1634-12 Sub Slab EPA TO-15 MP-13 DUP 23171634-13 Sub Slab EPA TO-15 MP-14 23171634-14 Sub Slab EPA TO-15 MP-12 23F1634-15 Sub Slab EPA TO-15 MP-10 23171634-16 Sub Slab EPA TO-15 MP-11 23171634-17 Sub Slab EPA TO-15 MP-8 23F1634-18 Sub Slab EPA TO-15 MP-9 23171634-19 Sub Slab EPA TO-15 MP-7 23171634-20 Sub Slab EPA TO-15 Page 2 of 84 con-testo A Pace Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Mid -Atlantic Associates, Inc. - Raleigh, NC REPORT DATE: 6/19/2023 409 Rogers View Court Raleigh, NC 27610 PURCHASE ORDER NUMBER: ATTN: Nolen Barefoot PROJECT NUMBER: R3746.00 ANALYTICAL SUMMARY WORK ORDER NUMBER: 23F1634 The results of analyses performed on the following samples submitted to Con -Test, a Pace Analytical Laboratory, are found in this report. PROJECT LOCATION: Raleigh, NC FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB MP-6 231`1634-21 Sub Slab EPA TO-15 MP-5 23171634-22 Sub Slab EPA TO-15 MP-4 23FI634-23 Sub Slab EPA TO-15 MP-3 23171634-24 Sub Slab EPA TO-15 MP-2 23171634-25 Sub Slab EPA TO-15 MP -I 23FI634-26 Sub Slab EPA TO-15 MP-1 DUP 23171634-27 Sub Slab EPA TO-15 UNUSED 23171634-28 UNUSED 23FI634-29 UNUSED 23FI634-30 Page 3 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CASE NARRATIVE SUMMARY All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report. EPA TO-15 Qualifications: V-06 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. Analyte & Samples(s) Qualified: 2-Hexanone (MBK), 4-Methyl-2-pentanone (MIBK), Acetone, m&p-Xylene, o-Xylene 23F1634-03[MP-23], 23F1634-08[MP-19], 23F1634-09[MP-18], 23F1634-10[MP-17], 23F 1634- 11 [MP- 16], 23F1634-13[MP-13 DUP], 23F1634-19[MP-9], B343675-BS1, B343702-BS1, 5089310-CCVI, 5089326-CCVI, 23F1634-14[MP-14], 23F1634-15[MP-12], 23F1634-17[MP-11], 23F1634-20[MP-7], 23F1634-21[MP-6], 23F1634-22[MP-5], 23F1634-23[MP-4], 23F1634-24[MP-3], 23F1634-25[MP-2], 231`1634-26[MP-1], 23F1634-27[MP-1 DUP], B343702-DUPI, 23F1634-06[MP-22] V-20 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. Analyte & Samples(s) Qualified: 4-Methyl-2-pentanone (MIBK), Benzyl chloride B343675-BS1, 5089310-CCVI The results of analyses reported only relate to samples submitted to Con -Test, a Pace Analytical Laboratory, for testing. I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the best of my knowledge and belief, accurate and complete. d� Lisa A. Worthington Technical Representative Page 4 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-25 Sample ID: 23F1634-01 Sample Matrix: Sub Slab Sampled: 6/7/2023 07:53 Sample Description/Location: Sub Description/Location: Canister ID: 2822 Canister Size: 1 liter Flow Controller ID: 4584 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -27.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -4.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Acetone ND 8.0 4.8 ND 19 11 4 6/17/23 3:29 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 3:29 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 3:29 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 3:29 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 3:29 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 3:29 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 3:29 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 3:29 CMR Carbon Disulfide 0.34 2.0 0.18 J 1.0 6.2 0.58 4 6/17/23 3:29 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 3:29 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 3:29 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 3:29 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 3:29 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/17/23 3:29 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 3:29 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 3:29 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 3:29 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 3:29 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 3:29 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 3:29 CMR Dichlorodifluoromethane (Freon 12) 0.45 0.20 0.20 2.2 0.99 0.97 4 6/17/23 3:29 CMR 1, 1 -Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 3:29 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 3:29 CMR 1, 1 -Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 3:29 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 3:29 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 3:29 CMR 1,2-Dichloropropane 0.12 0.20 0.11 J 0.55 0.92 0.50 4 6/17/23 3:29 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 3:29 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 3:29 CMR 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 3:29 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 3:29 CMR Ethanol 22 8.0 3.5 41 15 6.6 4 6/17/23 3:29 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 3:29 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 3:29 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 3:29 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 3:29 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 3:29 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 3:29 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 3:29 CMR Isopropanol 7.5 8.0 1.4 J 19 20 3.4 4 6/17/23 3:29 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 3:29 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 3:29 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 3:29 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 3:29 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 3:29 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 3:29 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 3:29 CMR Page 5 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-25 Canister ID: 2822 Final Vacuum(in Hg): -5 Sample ID: 23F1634-01 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.7 Sample Matrix: Sub Slab Flow Controller ID: 4584 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 07:53 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 3:29 CMR Tetrahydrofuran ND 2.0 0.33 ND 5.9 0.97 4 6/17/23 3:29 CMR Toluene 0.15 0.20 0.11 J 0.57 0.75 0.43 4 6/17/23 3:29 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 3:29 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 3:29 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 3:29 CMR Trichloroethylene 0.16 0.20 0.13 J 0.84 1.1 0.72 4 6/17/23 3:29 CMR Trichlorofluoromethane (Freon 11) 1.7 0.80 0.24 9.7 4.5 1.3 4 6/17/23 3:29 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 3:29 CMR 1,2,4-Trimethylbenzene 0.29 0.20 0.088 1.4 0.98 0.43 4 6/17/23 3:29 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 3:29 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 3:29 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 3:29 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 3:29 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 3:29 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 94.0 70-130 6/17/23 3:29 Page 6 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-24 Canister ID: 2785 Final Vacuum(in Hg): -5 Sample ID: 23F1634-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4583 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 08:16 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone ND 8.0 4.8 ND 19 11 4 6/17/23 4:11 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 4:11 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 4:11 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 4:11 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 4:11 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 4:11 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 4:11 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 4:11 CMR Carbon Disulfide 0.39 2.0 0.18 J 1.2 6.2 0.58 4 6/17/23 4:11 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 4:11 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 4:11 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 4:11 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 4:11 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/17/23 4:11 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 4:11 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 4:11 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 4:11 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 4:11 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 4:11 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 4:11 CMR Dichlorodifluoromethane (Freon 12) 0.35 0.20 0.20 1.7 0.99 0.97 4 6/17/23 4:11 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 4:11 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 4:11 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 4:11 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 4:11 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 4:11 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 4:11 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 4:11 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 4:11 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 4:11 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 4:11 CMR Ethanol 16 8.0 3.5 31 15 6.6 4 6/17/23 4:11 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 4:11 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 4:11 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 4:11 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 4:11 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 4:11 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 4:11 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 4:11 CMR Isopropanol 1.5 8.0 1.4 J 3.7 20 3.4 4 6/17/23 4:11 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 4:11 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 4:11 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 4:11 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 4:11 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 4:11 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 4:11 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 4:11 CMR Page 7 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-24 Canister ID: 2785 Final Vacuum(in Hg): -5 Sample ID: 23F1634-02 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4583 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 08:16 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 4:11 CMR Tetrahydrofuran ND 2.0 0.33 ND 5.9 0.97 4 6/17/23 4:11 CMR Toluene 0.14 0.20 0.11 J 0.54 0.75 0.43 4 6/17/23 4:11 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 4:11 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 4:11 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 4:11 CMR Trichloroethylene 0.29 0.20 0.13 1.6 1.1 0.72 4 6/17/23 4:11 CMR Trichlorofluoromethane (Freon 11) 0.42 0.80 0.24 J 2.3 4.5 1.3 4 6/17/23 4:11 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 4:11 CMR 1,2,4-Trimethylbenzene 0.24 0.20 0.088 1.2 0.98 0.43 4 6/17/23 4:11 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 4:11 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 4:11 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 4:11 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 4:11 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 4:11 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 93.0 70-130 6/17/23 4:11 Page 8 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-23 Canister ID: 2110 Final Vacuum(in Hg): -5 Sample ID: 23F1634-03 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.8 Sample Matrix: Sub Slab Flow Controller ID: 4575 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 08:34 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 8.1 8.0 4.8 19 19 11 4 6/17/23 4:53 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 4:53 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 4:53 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 4:53 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 4:53 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 4:53 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 4:53 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 4:53 CMR Carbon Disulfide 1.4 2.0 0.18 J 4.4 6.2 0.58 4 6/17/23 4:53 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 4:53 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 4:53 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 4:53 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 4:53 CMR Chloromethane 0.24 0.40 0.16 J 0.50 0.83 0.33 4 6/17/23 4:53 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 4:53 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 4:53 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 4:53 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 4:53 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 4:53 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 4:53 CMR Dichlorodifluoromethane (Freon 12) 0.39 0.20 0.20 1.9 0.99 0.97 4 6/17/23 4:53 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 4:53 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 4:53 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 4:53 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 4:53 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 4:53 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 4:53 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 4:53 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 4:53 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 4:53 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 4:53 CMR Ethanol 19 8.0 3.5 36 15 6.6 4 6/17/23 4:53 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 4:53 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 4:53 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 4:53 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 4:53 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 4:53 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 4:53 CMR 2-Hexanone (MBK) 0.22 0.20 0.10 V-06 0.92 0.82 0.41 4 6/17/23 4:53 CMR Isopropanol 9.4 8.0 1.4 23 20 3.4 4 6/17/23 4:53 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 4:53 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 4:53 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 4:53 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 4:53 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 4:53 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 4:53 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 4:53 CMR Page 9 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-23 Canister ID: 2110 Final Vacuum(in Hg): -5 Sample ID: 23F1634-03 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.8 Sample Matrix: Sub Slab Flow Controller ID: 4575 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 08:34 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 4:53 CMR Tetrahydrofuran ND 2.0 0.33 ND 5.9 0.97 4 6/17/23 4:53 CMR Toluene 0.25 0.20 0.11 0.93 0.75 0.43 4 6/17/23 4:53 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 4:53 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 4:53 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 4:53 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 4:53 CMR Trichlorofluoromethane (Freon 11) 3.0 0.80 0.24 17 4.5 1.3 4 6/17/23 4:53 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.28 0.80 0.22 J 2.2 6.1 1.7 4 6/17/23 4:53 CMR 1,2,4-Trimethylbenzene 0.28 0.20 0.088 1.4 0.98 0.43 4 6/17/23 4:53 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 4:53 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 4:53 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 4:53 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 4:53 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 4:53 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 93.2 70-130 6/17/23 4:53 Page 10 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-15 Canister ID: 2794 Final Vacuum(in Hg): -5 Sample ID: 23F1634-04 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Sub Slab Flow Controller ID: 4700 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 08:50 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone ND 8.0 4.8 ND 19 11 4 6/17/23 5:35 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 5:35 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 5:35 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 5:35 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 5:35 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 5:35 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 5:35 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 5:35 CMR Carbon Disulfide 0.32 2.0 0.18 J 1.00 6.2 0.58 4 6/17/23 5:35 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 5:35 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 5:35 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 5:35 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 5:35 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/17/23 5:35 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 5:35 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 5:35 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 5:35 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 5:35 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 5:35 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 5:35 CMR Dichlorodifluoromethane (Freon 12) 0.38 0.20 0.20 1.9 0.99 0.97 4 6/17/23 5:35 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 5:35 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 5:35 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 5:35 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 5:35 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 5:35 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 5:35 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 5:35 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 5:35 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 5:35 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 5:35 CMR Ethanol 18 8.0 3.5 33 15 6.6 4 6/17/23 5:35 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 5:35 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 5:35 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 5:35 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 5:35 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 5:35 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 5:35 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 5:35 CMR Isopropanol 8.6 8.0 1.4 21 20 3.4 4 6/17/23 5:35 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 5:35 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 5:35 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 5:35 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 5:35 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 5:35 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 5:35 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 5:35 CMR Page 11 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-15 Sample ID: 23F1634-04 Sample Matrix: Sub Slab Sampled: 6/7/2023 08:50 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2794 Canister Size: 1 liter Flow Controller ID: 4700 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 5:35 CMR Tetrahydrofuran 1.5 2.0 0.33 J 4.6 5.9 0.97 4 6/17/23 5:35 CMR Toluene 0.34 0.20 0.11 1.3 0.75 0.43 4 6/17/23 5:35 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 5:35 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 5:35 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 5:35 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 5:35 CMR Trichlorofluoromethane (Freon 11) 2.5 0.80 0.24 14 4.5 1.3 4 6/17/23 5:35 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 5:35 CMR 1,2,4-Trimethylbenzene 0.25 0.20 0.088 1.2 0.98 0.43 4 6/17/23 5:35 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 5:35 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 5:35 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 5:35 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 5:35 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 5:35 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 93.5 % REC Limits 70-130 6/17/23 5:35 Page 12 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-21 Canister ID: 2892 Final Vacuum(in Hg): -5 Sample ID: 23F1634-05 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.7 Sample Matrix: Sub Slab Flow Controller ID: 4668 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 10:03 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 9.6 8.0 4.8 23 19 11 4 6/17/23 9:07 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 9:07 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 9:07 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 9:07 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 9:07 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 9:07 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 9:07 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 9:07 CMR Carbon Disulfide ND 2.0 0.18 ND 6.2 0.58 4 6/17/23 9:07 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 9:07 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 9:07 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 9:07 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 9:07 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/17/23 9:07 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 9:07 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 9:07 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 9:07 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 9:07 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 9:07 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 9:07 CMR Dichlorodifluoromethane (Freon 12) 0.29 0.20 0.20 1.4 0.99 0.97 4 6/17/23 9:07 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 9:07 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 9:07 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 9:07 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 9:07 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 9:07 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 9:07 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 9:07 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 9:07 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 9:07 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 9:07 CMR Ethanol 20 8.0 3.5 38 15 6.6 4 6/17/23 9:07 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 9:07 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 9:07 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 9:07 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 9:07 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 9:07 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 9:07 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 9:07 CMR Isopropanol 14 8.0 1.4 33 20 3.4 4 6/17/23 9:07 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 9:07 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 9:07 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 9:07 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 9:07 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 9:07 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 9:07 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 9:07 CMR Page 13 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-21 Sample ID: 23F1634-05 Sample Matrix: Sub Slab Sampled: 6/7/2023 10:03 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2892 Canister Size: 1 liter Flow Controller ID: 4668 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -27.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 9:07 CMR Tetrahydrofuran ND 2.0 0.33 ND 5.9 0.97 4 6/17/23 9:07 CMR Toluene 0.78 0.20 0.11 2.9 0.75 0.43 4 6/17/23 9:07 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 9:07 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 9:07 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 9:07 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 9:07 CMR Trichlorofluoromethane (Freon 11) 2.1 0.80 0.24 12 4.5 1.3 4 6/17/23 9:07 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 9:07 CMR 1,2,4-Trimethylbenzene 0.14 0.20 0.088 J 0.71 0.98 0.43 4 6/17/23 9:07 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 9:07 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 9:07 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 9:07 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 9:07 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 9:07 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 90.0 % REC Limits 70-130 6/17/23 9:07 Page 14 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: MP-22 Canister ID: 2833 Final Vacuum(in Hg): -5 Sample ID: 23F1634-06 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.5 Sample Matrix: Sub Slab Flow Controller ID: 4587 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 10:15 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 13 8.0 4.8 30 19 11 4 6/17/23 9:48 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 9:48 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 9:48 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 9:48 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 9:48 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 9:48 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 9:48 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 9:48 CMR Carbon Disulfide 0.20 2.0 0.18 J 0.62 6.2 0.58 4 6/17/23 9:48 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 9:48 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 9:48 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 9:48 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 9:48 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/17/23 9:48 CMR Cyclohexane 0.15 0.20 0.12 J 0.51 0.69 0.42 4 6/17/23 9:48 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 9:48 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 9:48 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 9:48 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 9:48 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 9:48 CMR Dichlorodifluoromethane (Freon 12) 0.38 0.20 0.20 1.9 0.99 0.97 4 6/17/23 9:48 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 9:48 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 9:48 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 9:48 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 9:48 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 9:48 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 9:48 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 9:48 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 9:48 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 9:48 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 9:48 CMR Ethanol 110 8.0 3.5 200 15 6.6 4 6/17/23 9:48 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 9:48 CMR Ethylbenzene 0.15 0.20 0.12 J 0.64 0.87 0.51 4 6/17/23 9:48 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 9:48 CMR Heptane 0.20 0.20 0.13 J 0.80 0.82 0.52 4 6/17/23 9:48 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 9:48 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 9:48 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 9:48 CMR Isopropanol 14 8.0 1.4 35 20 3.4 4 6/17/23 9:48 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 9:48 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 9:48 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 9:48 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 9:48 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 9:48 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 9:48 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 9:48 CMR Page 15 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: MP-22 Canister ID: 2833 Final Vacuum(in Hg): -5 Sample ID: 23F1634-06 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.5 Sample Matrix: Sub Slab Flow Controller ID: 4587 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 10:15 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 9:48 CMR Tetrahydrofuran 0.86 2.0 0.33 J 2.5 5.9 0.97 4 6/17/23 9:48 CMR Toluene 1.4 0.20 0.11 5.3 0.75 0.43 4 6/17/23 9:48 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 9:48 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 9:48 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 9:48 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 9:48 CMR Trichlorofluoromethane (Freon 11) 0.49 0.80 0.24 J 2.7 4.5 1.3 4 6/17/23 9:48 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 9:48 CMR 1,2,4-Trimethylbenzene 1.1 0.20 0.088 5.3 0.98 0.43 4 6/17/23 9:48 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 9:48 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 9:48 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 9:48 CMR m&p-Xylene 0.50 0.40 0.22 V-06 2.2 1.7 0.97 4 6/17/23 9:48 CMR o-Xylene 0.22 0.20 0.10 V-06 0.97 0.87 0.44 4 6/17/23 9:48 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 90.8 70-130 6/17/23 9:48 Page 16 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: MP-20 Canister ID: 2647 Final Vacuum(in Hg): -5 Sample ID: 23F1634-07 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4688 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 10:36 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 7.0 8.0 4.8 J 17 19 11 4 6/17/23 10:29 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 10:29 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 10:29 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 10:29 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 10:29 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 10:29 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 10:29 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 10:29 CMR Carbon Disulfide 0.25 2.0 0.18 J 0.77 6.2 0.58 4 6/17/23 10:29 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 10:29 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 10:29 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 10:29 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 10:29 CMR Chloromethane 0.25 0.40 0.16 J 0.52 0.83 0.33 4 6/17/23 10:29 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 10:29 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 10:29 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 10:29 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 10:29 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 10:29 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 10:29 CMR Dichlorodifluoromethane (Freon 12) 0.32 0.20 0.20 1.6 0.99 0.97 4 6/17/23 10:29 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 10:29 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 10:29 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 10:29 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 10:29 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 10:29 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 10:29 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 10:29 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 10:29 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 10:29 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 10:29 CMR Ethanol 46 8.0 3.5 86 15 6.6 4 6/17/23 10:29 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 10:29 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 10:29 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 10:29 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 10:29 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 10:29 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 10:29 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 10:29 CMR Isopropanol 5.5 8.0 1.4 J 14 20 3.4 4 6/17/23 10:29 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 10:29 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 10:29 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 10:29 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 10:29 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 10:29 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 10:29 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 10:29 CMR Page 17 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-20 Sample ID: 23F1634-07 Sample Matrix: Sub Slab Sampled: 6/7/2023 10:36 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2647 Canister Size: 1 liter Flow Controller ID: 4688 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.0 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 10:29 CMR Tetrahydrofuran 1.1 2.0 0.33 J 3.1 5.9 0.97 4 6/17/23 10:29 CMR Toluene 1.1 0.20 0.11 4.0 0.75 0.43 4 6/17/23 10:29 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 10:29 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 10:29 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 10:29 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 10:29 CMR Trichlorofluoromethane (Freon 11) 0.63 0.80 0.24 J 3.5 4.5 1.3 4 6/17/23 10:29 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 10:29 CMR 1,2,4-Trimethylbenzene 0.30 0.20 0.088 1.5 0.98 0.43 4 6/17/23 10:29 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 10:29 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 10:29 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 10:29 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 10:29 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 10:29 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 93.1 % REC Limits 70-130 6/17/23 10:29 Page 18 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: MP-19 Canister ID: 2293 Final Vacuum(in Hg): -5 Sample ID: 23F1634-08 Canister Size: 1 liter Receipt Vacuum(in Hg): -3.7 Sample Matrix: Sub Slab Flow Controller ID: 4594 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 10:58 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 16 8.0 4.8 V-06 37 19 11 4 6/17/23 17:29 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 17:29 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 17:29 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 17:29 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 17:29 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 17:29 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 17:29 CMR 2-Butanone (MEK) 2.6 8.0 2.1 J 7.8 24 6.3 4 6/17/23 17:29 CMR Carbon Disulfide 1.3 2.0 0.18 J 4.1 6.2 0.58 4 6/17/23 17:29 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 17:29 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 17:29 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 17:29 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 17:29 CMR Chloromethane 0.34 0.40 0.16 J 0.69 0.83 0.33 4 6/17/23 17:29 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 17:29 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 17:29 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 17:29 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 17:29 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 17:29 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 17:29 CMR Dichlorodifluoromethane (Freon 12) 0.37 0.20 0.20 1.8 0.99 0.97 4 6/17/23 17:29 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 17:29 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 17:29 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 17:29 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 17:29 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 17:29 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 17:29 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 17:29 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 17:29 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 17:29 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 17:29 CMR Ethanol 63 8.0 3.5 120 15 6.6 4 6/17/23 17:29 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 17:29 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 17:29 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 17:29 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 17:29 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 17:29 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 17:29 CMR 2-Hexanone (MBK) 0.15 0.20 0.10 V-06, J 0.61 0.82 0.41 4 6/17/23 17:29 CMR Isopropanol 5.7 8.0 1.4 J 14 20 3.4 4 6/17/23 17:29 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 17:29 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 17:29 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 17:29 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 17:29 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 17:29 CMR Styrene 0.28 0.20 0.11 1.2 0.85 0.45 4 6/17/23 17:29 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 17:29 CMR Page 19 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: MP-19 Canister ID: 2293 Final Vacuum(in Hg): -5 Sample ID: 23F1634-08 Canister Size: 1 liter Receipt Vacuum(in Hg): -3.7 Sample Matrix: Sub Slab Flow Controller ID: 4594 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 10:58 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 17:29 CMR Tetrahydrofuran 9.9 2.0 0.33 29 5.9 0.97 4 6/17/23 17:29 CMR Toluene 1.6 0.20 0.11 6.0 0.75 0.43 4 6/17/23 17:29 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 17:29 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 17:29 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 17:29 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 17:29 CMR Trichlorofluoromethane (Freon 11) 0.64 0.80 0.24 J 3.6 4.5 1.3 4 6/17/23 17:29 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 17:29 CMR 1,2,4-Trimethylbenzene 0.33 0.20 0.088 1.6 0.98 0.43 4 6/17/23 17:29 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 17:29 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 17:29 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 17:29 CMR m&p-Xylene 0.29 0.40 0.22 J 1.3 1.7 0.97 4 6/17/23 17:29 CMR o-Xylene 0.14 0.20 0.10 J 0.59 0.87 0.44 4 6/17/23 17:29 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 93.7 70-130 6/17/23 17:29 Page 20 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-18 Canister ID: 2680 Final Vacuum(in Hg): -5 Sample ID: 23F1634-09 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4593 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 11:14 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 18 8.0 4.8 V-06 44 19 11 4 6/17/23 18:10 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 18:10 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 18:10 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 18:10 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 18:10 CMR Bromomethane 0.23 0.20 0.13 0.90 0.78 0.52 4 6/17/23 18:10 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 18:10 CMR 2-Butanone (MEK) 2.4 8.0 2.1 J 7.1 24 6.3 4 6/17/23 18:10 CMR Carbon Disulfide 1.4 2.0 0.18 J 4.4 6.2 0.58 4 6/17/23 18:10 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 18:10 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 18:10 CMR Chloroethane 0.69 0.20 0.18 1.8 0.53 0.47 4 6/17/23 18:10 CMR Chloroform 0.37 0.20 0.19 1.8 0.98 0.93 4 6/17/23 18:10 CMR Chloromethane 3.5 0.40 0.16 7.2 0.83 0.33 4 6/17/23 18:10 CMR Cyclohexane 0.35 0.20 0.12 1.2 0.69 0.42 4 6/17/23 18:10 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 18:10 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 18:10 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 18:10 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 18:10 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 18:10 CMR Dichlorodifluoromethane (Freon 12) 0.42 0.20 0.20 2.1 0.99 0.97 4 6/17/23 18:10 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 18:10 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 18:10 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 18:10 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 18:10 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 18:10 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 18:10 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 18:10 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 18:10 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 18:10 CMR 1,4-Dioxane 0.22 2.0 0.17 J 0.81 7.2 0.60 4 6/17/23 18:10 CMR Ethanol 37 8.0 3.5 69 15 6.6 4 6/17/23 18:10 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 18:10 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 18:10 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 18:10 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 18:10 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 18:10 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 18:10 CMR 2-Hexanone (MBK) 0.29 0.20 0.10 V-06 1.2 0.82 0.41 4 6/17/23 18:10 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/17/23 18:10 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 18:10 CMR Methylene Chloride 1.4 2.0 0.93 J 5.0 6.9 3.2 4 6/17/23 18:10 CMR 4-Methyl-2-pentanone (MIBK) 0.25 0.20 0.11 V-06 1.0 0.82 0.44 4 6/17/23 18:10 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 18:10 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 18:10 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 18:10 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 18:10 CMR Page 21 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-18 Sample ID: 23F1634-09 Sample Matrix: Sub Slab Sampled: 6/7/2023 11:14 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2680 Canister Size: 1 liter Flow Controller ID: 4593 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -27.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.0 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 18:10 CMR Tetrahydrofuran 8.6 2.0 0.33 25 5.9 0.97 4 6/17/23 18:10 CMR Toluene 1.5 0.20 0.11 5.6 0.75 0.43 4 6/17/23 18:10 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 18:10 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 18:10 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 18:10 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 18:10 CMR Trichlorofluoromethane (Freon 11) 1.9 0.80 0.24 10 4.5 1.3 4 6/17/23 18:10 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1.4 0.80 0.22 11 6.1 1.7 4 6/17/23 18:10 CMR 1,2,4-Trimethylbenzene 0.24 0.20 0.088 1.2 0.98 0.43 4 6/17/23 18:10 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 18:10 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 18:10 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 18:10 CMR m&p-Xylene 0.25 0.40 0.22 J 1.1 1.7 0.97 4 6/17/23 18:10 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 18:10 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 93.1 % REC Limits 70-130 6/17/23 18:10 Page 22 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -29 Field Sample #: MP-17 Canister ID: 2311 Final Vacuum(in Hg): -5 Sample ID: 23F1634-10 Canister Size: 1 liter Receipt Vacuum(in Hg): -3.5 Sample Matrix: Sub Slab Flow Controller ID: 4703 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 11:27 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 20 8.0 4.8 V-06 48 19 11 4 6/17/23 18:50 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 18:50 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 18:50 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 18:50 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 18:50 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 18:50 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 18:50 CMR 2-Butanone (MEK) 2.4 8.0 2.1 J 7.2 24 6.3 4 6/17/23 18:50 CMR Carbon Disulfide 0.44 2.0 0.18 J 1.4 6.2 0.58 4 6/17/23 18:50 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 18:50 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 18:50 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 18:50 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 18:50 CMR Chloromethane 0.39 0.40 0.16 J 0.80 0.83 0.33 4 6/17/23 18:50 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 18:50 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 18:50 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 18:50 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 18:50 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 18:50 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 18:50 CMR Dichlorodifluoromethane (Freon 12) 0.37 0.20 0.20 1.8 0.99 0.97 4 6/17/23 18:50 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 18:50 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 18:50 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 18:50 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 18:50 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 18:50 CMR 1,2-Dichloropropene 0.18 0.20 0.11 J 0.83 0.92 0.50 4 6/17/23 18:50 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 18:50 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 18:50 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 18:50 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 18:50 CMR Ethanol 26 8.0 3.5 50 15 6.6 4 6/17/23 18:50 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 18:50 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 18:50 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 18:50 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 18:50 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 18:50 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 18:50 CMR 2-Hexanone (MBK) 0.12 0.20 0.10 V-06, J 0.49 0.82 0.41 4 6/17/23 18:50 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/17/23 18:50 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 18:50 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 18:50 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 18:50 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 18:50 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 18:50 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 18:50 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 18:50 CMR Page 23 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-17 Sample ID: 23F1634-10 Sample Matrix: Sub Slab Sampled: 6/7/2023 11:27 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2311 Canister Size: 1 liter Flow Controller ID: 4703 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -29 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -3.5 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 18:50 CMR Tetrahydrofuran 6.2 2.0 0.33 18 5.9 0.97 4 6/17/23 18:50 CMR Toluene 1.2 0.20 0.11 4.5 0.75 0.43 4 6/17/23 18:50 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 18:50 CMR 1, 1, 1 -Trichloroethane 0.22 0.20 0.16 1.2 1.1 0.86 4 6/17/23 18:50 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 18:50 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 18:50 CMR Trichlorofluoromethane (Freon 11) 14 0.80 0.24 80 4.5 1.3 4 6/17/23 18:50 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 0.27 0.80 0.22 J 2.1 6.1 1.7 4 6/17/23 18:50 CMR 1,2,4-Trimethylbenzene 0.22 0.20 0.088 1.1 0.98 0.43 4 6/17/23 18:50 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 18:50 CMR Vinyl Acetate 1.2 4.0 1.1 J 4.2 14 3.8 4 6/17/23 18:50 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 18:50 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 18:50 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 18:50 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 93.9 % REC Limits 70-130 6/17/23 18:50 Page 24 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-16 Canister ID: 2298 Final Vacuum(in Hg): -5 Sample ID: 23F1634-11 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.9 Sample Matrix: Sub Slab Flow Controller ID: 4704 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 11:33 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 44 8.0 4.8 V-06 110 19 11 4 6/17/23 19:30 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 19:30 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 19:30 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 19:30 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 19:30 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 19:30 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 19:30 CMR 2-Butanone (MEK) 11 8.0 2.1 33 24 6.3 4 6/17/23 19:30 CMR Carbon Disulfide 0.24 2.0 0.18 J 0.76 6.2 0.58 4 6/17/23 19:30 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 19:30 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 19:30 CMR Chloroethane 0.18 0.20 0.18 J 0.47 0.53 0.47 4 6/17/23 19:30 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 19:30 CMR Chloromethane 0.38 0.40 0.16 J 0.79 0.83 0.33 4 6/17/23 19:30 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 19:30 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 19:30 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 19:30 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 19:30 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 19:30 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 19:30 CMR Dichlorodifluoromethane (Freon 12) 0.34 0.20 0.20 1.7 0.99 0.97 4 6/17/23 19:30 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 19:30 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 19:30 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 19:30 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 19:30 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 19:30 CMR 1,2-Dichloropropane 0.21 0.20 0.11 0.96 0.92 0.50 4 6/17/23 19:30 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 19:30 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 19:30 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 19:30 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 19:30 CMR Ethanol 53 8.0 3.5 100 15 6.6 4 6/17/23 19:30 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 19:30 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 19:30 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 19:30 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 19:30 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 19:30 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 19:30 CMR 2-Hexanone (MBK) 0.61 0.20 0.10 V-06 2.5 0.82 0.41 4 6/17/23 19:30 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/17/23 19:30 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 19:30 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 19:30 CMR 4-Methyl-2-pentanone (MIBK) 0.18 0.20 0.11 V-06, J 0.75 0.82 0.44 4 6/17/23 19:30 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 19:30 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 19:30 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 19:30 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 19:30 CMR Page 25 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-16 Canister ID: 2298 Final Vacuum(in Hg): -5 Sample ID: 23F1634-11 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.9 Sample Matrix: Sub Slab Flow Controller ID: 4704 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 11:33 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 19:30 CMR Tetrahydrofuran 9.8 2.0 0.33 29 5.9 0.97 4 6/17/23 19:30 CMR Toluene 1.9 0.20 0.11 7.3 0.75 0.43 4 6/17/23 19:30 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 19:30 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 19:30 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 19:30 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 19:30 CMR Trichlorofluoromethane (Freon 11) 9.7 0.80 0.24 55 4.5 1.3 4 6/17/23 19:30 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 19:30 CMR 1,2,4-Trimethylbenzene 0.39 0.20 0.088 1.9 0.98 0.43 4 6/17/23 19:30 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 19:30 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 19:30 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 19:30 CMR m&p-Xylene 0.34 0.40 0.22 J 1.5 1.7 0.97 4 6/17/23 19:30 CMR o-Xylene 0.16 0.20 0.10 J 0.71 0.87 0.44 4 6/17/23 19:30 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 93.6 70-130 6/17/23 19:30 Page 26 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-13 Canister ID: 2793 Final Vacuum(in Hg): -5 Sample ID: 23F1634-12 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.8 Sample Matrix: Sub Slab Flow Controller ID: 4590 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 12:06 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone ND 8.0 4.8 ND 19 11 4 6/17/23 20:11 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 20:11 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 20:11 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 20:11 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 20:11 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 20:11 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 20:11 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 20:11 CMR Carbon Disulfide 0.35 2.0 0.18 J 1.1 6.2 0.58 4 6/17/23 20:11 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 20:11 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 20:11 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 20:11 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 20:11 CMR Chloromethane 0.37 0.40 0.16 J 0.76 0.83 0.33 4 6/17/23 20:11 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 20:11 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 20:11 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 20:11 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 20:11 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 20:11 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 20:11 CMR Dichlorodifluoromethane (Freon 12) 0.34 0.20 0.20 1.7 0.99 0.97 4 6/17/23 20:11 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 20:11 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 20:11 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 20:11 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 20:11 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 20:11 CMR 1,2-Dichloropropane 0.25 0.20 0.11 1.2 0.92 0.50 4 6/17/23 20:11 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 20:11 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 20:11 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 20:11 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 20:11 CMR Ethanol 43 8.0 3.5 82 15 6.6 4 6/17/23 20:11 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 20:11 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 20:11 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 20:11 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 20:11 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 20:11 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 20:11 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 20:11 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/17/23 20:11 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 20:11 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 20:11 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 20:11 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 20:11 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 20:11 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 20:11 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 20:11 CMR Page 27 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-13 Sample ID: 23F1634-12 Sample Matrix: Sub Slab Sampled: 6/7/2023 12:06 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2793 Canister Size: 1 liter Flow Controller ID: 4590 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.8 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 20:11 CMR Tetrahydrofuran 1.5 2.0 0.33 J 4.3 5.9 0.97 4 6/17/23 20:11 CMR Toluene 1.1 0.20 0.11 4.1 0.75 0.43 4 6/17/23 20:11 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 20:11 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 20:11 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 20:11 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 20:11 CMR Trichlorofluoromethane (Freon 11) 16 0.80 0.24 87 4.5 1.3 4 6/17/23 20:11 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 20:11 CMR 1,2,4-Trimethylbenzene 0.15 0.20 0.088 J 0.75 0.98 0.43 4 6/17/23 20:11 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 20:11 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 20:11 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 20:11 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 20:11 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 20:11 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 94.5 % REC Limits 70-130 6/17/23 20:11 Page 28 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: MP-13 DUP Canister ID: 2245 Final Vacuum(in Hg): -5 Sample ID: 23F1634-13 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.9 Sample Matrix: Sub Slab Flow Controller ID: 4567 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 12:17 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 13 8.0 4.8 V-06 30 19 11 4 6/17/23 20:51 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 20:51 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 20:51 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 20:51 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 20:51 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 20:51 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 20:51 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 20:51 CMR Carbon Disulfide 0.36 2.0 0.18 J 1.1 6.2 0.58 4 6/17/23 20:51 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 20:51 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 20:51 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 20:51 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 20:51 CMR Chloromethane 0.39 0.40 0.16 J 0.80 0.83 0.33 4 6/17/23 20:51 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 20:51 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 20:51 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 20:51 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 20:51 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 20:51 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 20:51 CMR Dichlorodifluoromethane (Freon 12) 0.40 0.20 0.20 2.0 0.99 0.97 4 6/17/23 20:51 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 20:51 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 20:51 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 20:51 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 20:51 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 20:51 CMR 1,2-Dichloropropane 0.27 0.20 0.11 1.3 0.92 0.50 4 6/17/23 20:51 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 20:51 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 20:51 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 20:51 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 20:51 CMR Ethanol 18 8.0 3.5 34 15 6.6 4 6/17/23 20:51 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 20:51 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 20:51 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 20:51 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 20:51 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 20:51 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 20:51 CMR 2-Hexanone (MBK) 0.11 0.20 0.10 V-06, J 0.46 0.82 0.41 4 6/17/23 20:51 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/17/23 20:51 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 20:51 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 20:51 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 20:51 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 20:51 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 20:51 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 20:51 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 20:51 CMR Page 29 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-13 DUP Sample ID: 23F1634-13 Sample Matrix: Sub Slab Sampled: 6/7/2023 12:17 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2245 Canister Size: 1 liter Flow Controller ID: 4567 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -4.9 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 20:51 CMR Tetrahydrofuran 0.80 2.0 0.33 J 2.4 5.9 0.97 4 6/17/23 20:51 CMR Toluene 0.81 0.20 0.11 3.0 0.75 0.43 4 6/17/23 20:51 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 20:51 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 20:51 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 20:51 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 20:51 CMR Trichlorofluoromethane (Freon 11) 12 0.80 0.24 66 4.5 1.3 4 6/17/23 20:51 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 20:51 CMR 1,2,4-Trimethylbenzene 0.15 0.20 0.088 J 0.73 0.98 0.43 4 6/17/23 20:51 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 20:51 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 20:51 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 20:51 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 20:51 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 20:51 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 93.2 % REC Limits 70-130 6/17/23 20:51 Page 30 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-14 Canister ID: 2650 Final Vacuum(in Hg): -5 Sample ID: 23F1634-14 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.9 Sample Matrix: Sub Slab Flow Controller ID: 4589 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 12:24 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 7.5 8.0 4.8 V-06, J 18 19 11 4 6/17/23 21:31 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 21:31 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 21:31 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 21:31 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 21:31 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 21:31 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 21:31 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 21:31 CMR Carbon Disulfide 0.28 2.0 0.18 J 0.88 6.2 0.58 4 6/17/23 21:31 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 21:31 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 21:31 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 21:31 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 21:31 CMR Chloromethane 0.22 0.40 0.16 J 0.45 0.83 0.33 4 6/17/23 21:31 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 21:31 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 21:31 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 21:31 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 21:31 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 21:31 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 21:31 CMR Dichlorodifluoromethane (Freon 12) 0.38 0.20 0.20 1.9 0.99 0.97 4 6/17/23 21:31 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 21:31 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 21:31 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 21:31 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 21:31 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 21:31 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 21:31 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 21:31 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 21:31 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 21:31 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 21:31 CMR Ethanol 29 8.0 3.5 55 15 6.6 4 6/17/23 21:31 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 21:31 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 21:31 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 21:31 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 21:31 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 21:31 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 21:31 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 21:31 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/17/23 21:31 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 21:31 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 21:31 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 21:31 CMR Naphthalene 0.21 0.20 0.15 1.1 1.0 0.79 4 6/17/23 21:31 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 21:31 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 21:31 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 21:31 CMR Page 31 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-14 Sample ID: 23F1634-14 Sample Matrix: Sub Slab Sampled: 6/7/2023 12:24 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2650 Canister Size: 1 liter Flow Controller ID: 4589 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -27.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -4.9 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 21:31 CMR Tetrahydrofuran 0.76 2.0 0.33 J 2.2 5.9 0.97 4 6/17/23 21:31 CMR Toluene 1.2 0.20 0.11 4.5 0.75 0.43 4 6/17/23 21:31 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 21:31 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 21:31 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 21:31 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 21:31 CMR Trichlorofluoromethane (Freon 11) 2.0 0.80 0.24 11 4.5 1.3 4 6/17/23 21:31 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 21:31 CMR 1,2,4-Trimethylbenzene 0.14 0.20 0.088 J 0.67 0.98 0.43 4 6/17/23 21:31 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 21:31 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 21:31 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 21:31 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 21:31 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 21:31 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 93.8 % REC Limits 70-130 6/17/23 21:31 Page 32 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: MP-12 Canister ID: 2308 Final Vacuum(in Hg): -5 Sample ID: 23F1634-15 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4568 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 12:36 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RI MDL Dilution Date/Time Analyzed Analyst Acetone 9.0 8.0 4.8 V-06 21 19 11 4 6/17/23 22:12 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 22:12 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 22:12 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 22:12 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 22:12 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 22:12 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 22:12 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 22:12 CMR Carbon Disulfide 0.24 2.0 0.18 J 0.73 6.2 0.58 4 6/17/23 22:12 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 22:12 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 22:12 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 22:12 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 22:12 CMR Chloromethane 0.68 0.40 0.16 1.4 0.83 0.33 4 6/17/23 22:12 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 22:12 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 22:12 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 22:12 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 22:12 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 22:12 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 22:12 CMR Dichlorodifluoromethane (Freon 12) 0.40 0.20 0.20 2.0 0.99 0.97 4 6/17/23 22:12 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 22:12 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 22:12 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 22:12 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 22:12 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 22:12 CMR 1,2-Dichloropropene ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 22:12 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 22:12 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 22:12 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 22:12 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 22:12 CMR Ethanol 29 8.0 3.5 55 15 6.6 4 6/17/23 22:12 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 22:12 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 22:12 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 22:12 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 22:12 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 22:12 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 22:12 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 22:12 CMR Isopropanol 4.4 8.0 1.4 J 11 20 3.4 4 6/17/23 22:12 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 22:12 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 22:12 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 22:12 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 22:12 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 22:12 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 22:12 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 22:12 CMR Page 33 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-12 Sample ID: 23F1634-15 Sample Matrix: Sub Slab Sampled: 6/7/2023 12:36 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2308 Canister Size: 1 liter Flow Controller ID: 4568 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.0 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 22:12 CMR Tetrahydrofuran 1.4 2.0 0.33 J 4.2 5.9 0.97 4 6/17/23 22:12 CMR Toluene 0.96 0.20 0.11 3.6 0.75 0.43 4 6/17/23 22:12 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 22:12 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 22:12 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 22:12 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 22:12 CMR Trichlorofluoromethane (Freon 11) 0.59 0.80 0.24 J 3.3 4.5 1.3 4 6/17/23 22:12 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 22:12 CMR 1,2,4-Trimethylbenzene 0.14 0.20 0.088 J 0.69 0.98 0.43 4 6/17/23 22:12 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 22:12 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 22:12 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 22:12 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 22:12 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 22:12 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 92.7 % REC Limits 70-130 6/17/23 22:12 Page 34 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-10 Canister ID: 2854 Final Vacuum(in Hg): -5 Sample ID: 23F1634-16 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Sub Slab Flow Controller ID: 4591 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 13:11 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone ND 8.0 4.8 ND 19 11 4 6/17/23 22:52 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 22:52 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 22:52 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 22:52 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 22:52 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 22:52 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 22:52 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/17/23 22:52 CMR Carbon Disulfide 0.25 2.0 0.18 J 0.77 6.2 0.58 4 6/17/23 22:52 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 22:52 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 22:52 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 22:52 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 22:52 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/17/23 22:52 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 22:52 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 22:52 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 22:52 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 22:52 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 22:52 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 22:52 CMR Dichlorodifluoromethane (Freon 12) 0.40 0.20 0.20 2.0 0.99 0.97 4 6/17/23 22:52 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 22:52 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 22:52 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 22:52 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 22:52 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 22:52 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 22:52 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 22:52 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 22:52 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 22:52 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 22:52 CMR Ethanol 12 8.0 3.5 23 15 6.6 4 6/17/23 22:52 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 22:52 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 22:52 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 22:52 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 22:52 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 22:52 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 22:52 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 22:52 CMR Isopropanol 1.7 8.0 1.4 J 4.2 20 3.4 4 6/17/23 22:52 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 22:52 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 22:52 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 22:52 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 22:52 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 22:52 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 22:52 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 22:52 CMR Page 35 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-10 Sample ID: 23F1634-16 Sample Matrix: Sub Slab Sampled: 6/7/2023 13:11 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2854 Canister Size: 1 liter Flow Controller ID: 4591 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 22:52 CMR Tetrahydrofuran 1.0 2.0 0.33 J 3.1 5.9 0.97 4 6/17/23 22:52 CMR Toluene 0.84 0.20 0.11 3.2 0.75 0.43 4 6/17/23 22:52 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 22:52 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 22:52 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 22:52 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 22:52 CMR Trichlorofluoromethane (Freon 11) 0.39 0.80 0.24 J 2.2 4.5 1.3 4 6/17/23 22:52 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 22:52 CMR 1,2,4-Trimethylbenzene 0.12 0.20 0.088 J 0.57 0.98 0.43 4 6/17/23 22:52 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 22:52 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 22:52 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 22:52 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 22:52 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 22:52 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 92.9 % REC Limits 70-130 6/17/23 22:52 Page 36 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-11 Canister ID: 2883 Final Vacuum(in Hg): -5 Sample ID: 23F1634-17 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4571 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 13:04 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 7.9 8.0 4.8 V-06, J 19 19 11 4 6/17/23 23:33 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/17/23 23:33 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/17/23 23:33 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/17/23 23:33 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/17/23 23:33 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/17/23 23:33 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/17/23 23:33 CMR 2-Butanone (MEK) 2.4 8.0 2.1 J 7.0 24 6.3 4 6/17/23 23:33 CMR Carbon Disulfide 0.23 2.0 0.18 J 0.71 6.2 0.58 4 6/17/23 23:33 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/17/23 23:33 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/17/23 23:33 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/17/23 23:33 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/17/23 23:33 CMR Chloromethane 0.25 0.40 0.16 J 0.51 0.83 0.33 4 6/17/23 23:33 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/17/23 23:33 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/17/23 23:33 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/17/23 23:33 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/17/23 23:33 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/17/23 23:33 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/17/23 23:33 CMR Dichlorodifluoromethane (Freon 12) 0.43 0.20 0.20 2.1 0.99 0.97 4 6/17/23 23:33 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/17/23 23:33 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/17/23 23:33 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/17/23 23:33 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/17/23 23:33 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/17/23 23:33 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/17/23 23:33 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/17/23 23:33 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/17/23 23:33 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/17/23 23:33 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/17/23 23:33 CMR Ethanol 22 8.0 3.5 42 15 6.6 4 6/17/23 23:33 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/17/23 23:33 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/17/23 23:33 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/17/23 23:33 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/17/23 23:33 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/17/23 23:33 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/17/23 23:33 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/17/23 23:33 CMR Isopropanol 4.1 8.0 1.4 J 10 20 3.4 4 6/17/23 23:33 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/17/23 23:33 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/17/23 23:33 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/17/23 23:33 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/17/23 23:33 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/17/23 23:33 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/17/23 23:33 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/17/23 23:33 CMR Page 37 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-11 Sample ID: 23F1634-17 Sample Matrix: Sub Slab Sampled: 6/7/2023 13:04 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2883 Canister Size: 1 liter Flow Controller ID: 4571 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -27.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.0 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/17/23 23:33 CMR Tetrahydrofuran 2.0 2.0 0.33 6.0 5.9 0.97 4 6/17/23 23:33 CMR Toluene 2.2 0.20 0.11 8.3 0.75 0.43 4 6/17/23 23:33 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/17/23 23:33 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/17/23 23:33 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/17/23 23:33 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/17/23 23:33 CMR Trichlorofluoromethane (Freon 11) 0.36 0.80 0.24 J 2.0 4.5 1.3 4 6/17/23 23:33 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/17/23 23:33 CMR 1,2,4-Trimethylbenzene 0.14 0.20 0.088 J 0.71 0.98 0.43 4 6/17/23 23:33 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/17/23 23:33 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/17/23 23:33 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/17/23 23:33 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/17/23 23:33 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/17/23 23:33 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 94.5 % REC Limits 70-130 6/17/23 23:33 Page 38 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -29.5 Field Sample #: MP-8 Canister ID: 2831 Final Vacuum(in Hg): -5 Sample ID: 23F1634-18 Canister Size: 1 liter Receipt Vacuum(in Hg): -3.3 Sample Matrix: Sub Slab Flow Controller ID: 4592 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 13:30 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone ND 8.0 4.8 ND 19 11 4 6/18/23 0:52 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 0:52 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 0:52 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 0:52 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 0:52 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 0:52 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 0:52 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/18/23 0:52 CMR Carbon Disulfide 0.58 2.0 0.18 J 1.8 6.2 0.58 4 6/18/23 0:52 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 0:52 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 0:52 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 0:52 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 0:52 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/18/23 0:52 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 0:52 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 0:52 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 0:52 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 0:52 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 0:52 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 0:52 CMR Dichlorodifluoromethane (Freon 12) 0.38 0.20 0.20 1.9 0.99 0.97 4 6/18/23 0:52 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 0:52 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 0:52 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 0:52 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 0:52 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 0:52 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 0:52 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 0:52 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 0:52 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 0:52 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 0:52 CMR Ethanol 9.2 8.0 3.5 17 15 6.6 4 6/18/23 0:52 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 0:52 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 0:52 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 0:52 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/18/23 0:52 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 0:52 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 0:52 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 0:52 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/18/23 0:52 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 0:52 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 0:52 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 0:52 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 0:52 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 0:52 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 0:52 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 0:52 CMR Page 39 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-8 Sample ID: 23F1634-18 Sample Matrix: Sub Slab Sampled: 6/7/2023 13:30 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2831 Canister Size: 1 liter Flow Controller ID: 4592 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -29.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -3.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.75 0.20 0.15 5.1 1.4 1.0 4 6/18/23 0:52 CMR Tetrahydrofuran 1.8 2.0 0.33 J 5.4 5.9 0.97 4 6/18/23 0:52 CMR Toluene 1.9 0.20 0.11 7.0 0.75 0.43 4 6/18/23 0:52 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 0:52 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 0:52 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 0:52 CMR Trichloroethylene 0.18 0.20 0.13 J 0.95 1.1 0.72 4 6/18/23 0:52 CMR Trichlorofluoromethane (Freon 11) 8.0 0.80 0.24 45 4.5 1.3 4 6/18/23 0:52 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 0:52 CMR 1,2,4-Trimethylbenzene 0.44 0.20 0.088 2.2 0.98 0.43 4 6/18/23 0:52 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 0:52 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 0:52 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 0:52 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/18/23 0:52 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/18/23 0:52 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 93.8 % REC Limits 70-130 6/18/23 0:52 Page 40 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-9 Canister ID: 2312 Final Vacuum(in Hg): -5 Sample ID: 23F1634-19 Canister Size: 1 liter Receipt Vacuum(in Hg): -3.9 Sample Matrix: Sub Slab Flow Controller ID: 4669 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 13:47 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 13 8.0 4.8 V-06 32 19 11 4 6/18/23 1:33 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 1:33 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 1:33 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 1:33 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 1:33 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 1:33 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 1:33 CMR 2-Butanone (MEK) 3.3 8.0 2.1 J 9.8 24 6.3 4 6/18/23 1:33 CMR Carbon Disulfide 0.38 2.0 0.18 J 1.2 6.2 0.58 4 6/18/23 1:33 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 1:33 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 1:33 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 1:33 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 1:33 CMR Chloromethane 0.48 0.40 0.16 1.00 0.83 0.33 4 6/18/23 1:33 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 1:33 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 1:33 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 1:33 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 1:33 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 1:33 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 1:33 CMR Dichlorodifluoromethane (Freon 12) 0.35 0.20 0.20 1.7 0.99 0.97 4 6/18/23 1:33 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 1:33 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 1:33 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 1:33 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 1:33 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 1:33 CMR 1,2-Dichloropropene ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 1:33 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 1:33 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 1:33 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 1:33 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 1:33 CMR Ethanol 17 8.0 3.5 31 15 6.6 4 6/18/23 1:33 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 1:33 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 1:33 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 1:33 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/18/23 1:33 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 1:33 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 1:33 CMR 2-Hexanone (MBK) 0.11 0.20 0.10 V-06, J 0.46 0.82 0.41 4 6/18/23 1:33 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/18/23 1:33 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 1:33 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 1:33 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 1:33 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 1:33 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 1:33 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 1:33 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 1:33 CMR Page 41 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-9 Sample ID: 23F1634-19 Sample Matrix: Sub Slab Sampled: 6/7/2023 13:47 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2312 Canister Size: 1 liter Flow Controller ID: 4669 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -3.9 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/18/23 1:33 CMR Tetrahydrofuran 2.7 2.0 0.33 7.8 5.9 0.97 4 6/18/23 1:33 CMR Toluene 2.1 0.20 0.11 8.0 0.75 0.43 4 6/18/23 1:33 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 1:33 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 1:33 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 1:33 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/18/23 1:33 CMR Trichlorofluoromethane (Freon 11) 4.0 0.80 0.24 23 4.5 1.3 4 6/18/23 1:33 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 1:33 CMR 1,2,4-Trimethylbenzene 0.29 0.20 0.088 1.4 0.98 0.43 4 6/18/23 1:33 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 1:33 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 1:33 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 1:33 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/18/23 1:33 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/18/23 1:33 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 94.3 % REC Limits 70-130 6/18/23 1:33 Page 42 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28.5 Field Sample #: MP-7 Canister ID: 2834 Final Vacuum(in Hg): -5 Sample ID: 23F1634-20 Canister Size: 1 liter Receipt Vacuum(in Hg): -6.7 Sample Matrix: Sub Slab Flow Controller ID: 4670 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 14:06 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 6.5 8.0 4.8 V-06, J 16 19 11 4 6/18/23 2:13 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 2:13 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 2:13 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 2:13 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 2:13 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 2:13 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 2:13 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/18/23 2:13 CMR Carbon Disulfide 0.26 2.0 0.18 J 0.80 6.2 0.58 4 6/18/23 2:13 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 2:13 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 2:13 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 2:13 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 2:13 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/18/23 2:13 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 2:13 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 2:13 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 2:13 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 2:13 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 2:13 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 2:13 CMR Dichlorodifluoromethane (Freon 12) 0.36 0.20 0.20 1.8 0.99 0.97 4 6/18/23 2:13 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 2:13 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 2:13 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 2:13 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 2:13 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 2:13 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 2:13 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 2:13 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 2:13 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 2:13 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 2:13 CMR Ethanol 17 8.0 3.5 32 15 6.6 4 6/18/23 2:13 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 2:13 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 2:13 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 2:13 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/18/23 2:13 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 2:13 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 2:13 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 2:13 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/18/23 2:13 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 2:13 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 2:13 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 2:13 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 2:13 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 2:13 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 2:13 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 2:13 CMR Page 43 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-7 Sample ID: 23F1634-20 Sample Matrix: Sub Slab Sampled: 6/7/2023 14:06 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2834 Canister Size: 1 liter Flow Controller ID: 4670 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -6.7 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qua] Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.22 0.20 0.15 1.5 1.4 1.0 4 6/18/23 2:13 CMR Tetrahydrofuran 1.8 2.0 0.33 J 5.3 5.9 0.97 4 6/18/23 2:13 CMR Toluene 1.0 0.20 0.11 3.9 0.75 0.43 4 6/18/23 2:13 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 2:13 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 2:13 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 2:13 CMR Trichloroethylene 0.21 0.20 0.13 1.1 1.1 0.72 4 6/18/23 2:13 CMR Trichlorofluoromethane (Freon 11) 4.0 0.80 0.24 23 4.5 1.3 4 6/18/23 2:13 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 2:13 CMR 1,2,4-Trimethylbenzene 0.23 0.20 0.088 1.1 0.98 0.43 4 6/18/23 2:13 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 2:13 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 2:13 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 2:13 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/18/23 2:13 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/18/23 2:13 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 94.5 % REC Limits 70-130 6/18/23 2:13 Page 44 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: MP-6 Canister ID: 2835 Final Vacuum(in Hg): -5 Sample ID: 23F1634-21 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Sub Slab Flow Controller ID: 4582 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 14:14 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 5.5 8.0 4.8 V-06, J 13 19 11 4 6/18/23 2:53 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 2:53 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 2:53 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 2:53 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 2:53 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 2:53 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 2:53 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/18/23 2:53 CMR Carbon Disulfide 0.37 2.0 0.18 J 1.1 6.2 0.58 4 6/18/23 2:53 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 2:53 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 2:53 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 2:53 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 2:53 CMR Chloromethane ND 0.40 0.16 ND 0.83 0.33 4 6/18/23 2:53 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 2:53 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 2:53 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 2:53 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 2:53 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 2:53 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 2:53 CMR Dichlorodifluoromethane (Freon 12) 0.39 0.20 0.20 1.9 0.99 0.97 4 6/18/23 2:53 CMR 1,1-Dichloroethane 0.18 0.20 0.17 J 0.71 0.81 0.71 4 6/18/23 2:53 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 2:53 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 2:53 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 2:53 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 2:53 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 2:53 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 2:53 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 2:53 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 2:53 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 2:53 CMR Ethanol 7.0 8.0 3.5 J 13 15 6.6 4 6/18/23 2:53 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 2:53 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 2:53 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 2:53 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/18/23 2:53 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 2:53 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 2:53 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 2:53 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/18/23 2:53 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 2:53 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 2:53 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 2:53 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 2:53 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 2:53 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 2:53 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 2:53 CMR Page 45 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-6 Sample ID: 23F1634-21 Sample Matrix: Sub Slab Sampled: 6/7/2023 14:14 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2835 Canister Size: 1 liter Flow Controller ID: 4582 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -27 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.2 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene 0.32 0.20 0.15 2.1 1.4 1.0 4 6/18/23 2:53 CMR Tetrahydrofuran 1.7 2.0 0.33 J 4.9 5.9 0.97 4 6/18/23 2:53 CMR Toluene 0.92 0.20 0.11 3.5 0.75 0.43 4 6/18/23 2:53 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 2:53 CMR 1, 1, 1 -Trichloroethane 0.26 0.20 0.16 1.4 1.1 0.86 4 6/18/23 2:53 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 2:53 CMR Trichloroethylene 0.21 0.20 0.13 1.1 1.1 0.72 4 6/18/23 2:53 CMR Trichlorofluoromethane (Freon 11) 22 0.80 0.24 130 4.5 1.3 4 6/18/23 2:53 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 2:53 CMR 1,2,4-Trimethylbenzene 0.11 0.20 0.088 J 0.55 0.98 0.43 4 6/18/23 2:53 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 2:53 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 2:53 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 2:53 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/18/23 2:53 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/18/23 2:53 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 94.0 % REC Limits 70-130 6/18/23 2:53 Page 46 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: MP-5 Canister ID: 2768 Final Vacuum(in Hg): -5 Sample ID: 23F1634-22 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.8 Sample Matrix: Sub Slab Flow Controller ID: 4581 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 14:20 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 15 8.0 4.8 V-06 35 19 11 4 6/18/23 3:34 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 3:34 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 3:34 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 3:34 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 3:34 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 3:34 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 3:34 CMR 2-Butanone (MEK) 2.4 8.0 2.1 J 7.0 24 6.3 4 6/18/23 3:34 CMR Carbon Disulfide ND 2.0 0.18 ND 6.2 0.58 4 6/18/23 3:34 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 3:34 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 3:34 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 3:34 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 3:34 CMR Chloromethane 0.19 0.40 0.16 J 0.40 0.83 0.33 4 6/18/23 3:34 CMR Cyclohexane 0.58 0.20 0.12 2.0 0.69 0.42 4 6/18/23 3:34 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 3:34 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 3:34 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 3:34 CMR 1,3-Dichlorobenzene 0.22 0.20 0.11 1.3 1.2 0.67 4 6/18/23 3:34 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 3:34 CMR Dichlorodifluoromethane (Freon 12) 0.40 0.20 0.20 2.0 0.99 0.97 4 6/18/23 3:34 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 3:34 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 3:34 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 3:34 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 3:34 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 3:34 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 3:34 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 3:34 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 3:34 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 3:34 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 3:34 CMR Ethanol 37 8.0 3.5 69 15 6.6 4 6/18/23 3:34 CMR Ethyl Acetate 1.1 2.0 1.0 J 3.8 7.2 3.6 4 6/18/23 3:34 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 3:34 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 3:34 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/18/23 3:34 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 3:34 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 3:34 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 3:34 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/18/23 3:34 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 3:34 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 3:34 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 3:34 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 3:34 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 3:34 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 3:34 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 3:34 CMR Page 47 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: MP-5 Canister ID: 2768 Final Vacuum(in Hg): -5 Sample ID: 23F1634-22 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.8 Sample Matrix: Sub Slab Flow Controller ID: 4581 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 14:20 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene 0.25 0.20 0.15 1.7 1.4 1.0 4 6/18/23 3:34 CMR Tetrahydrofuran 3.4 2.0 0.33 10 5.9 0.97 4 6/18/23 3:34 CMR Toluene 1.9 0.20 0.11 7.1 0.75 0.43 4 6/18/23 3:34 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 3:34 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 3:34 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 3:34 CMR Trichloroethylene 0.28 0.20 0.13 1.5 1.1 0.72 4 6/18/23 3:34 CMR Trichlorofluoromethane (Freon 11) 1.6 0.80 0.24 9.1 4.5 1.3 4 6/18/23 3:34 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 3:34 CMR 1,2,4-Trimethylbenzene 0.30 0.20 0.088 1.5 0.98 0.43 4 6/18/23 3:34 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 3:34 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 3:34 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 3:34 CMR m&p-Xylene 0.24 0.40 0.22 J 1.1 1.7 0.97 4 6/18/23 3:34 CMR o-Xylene 0.12 0.20 0.10 J 0.50 0.87 0.44 4 6/18/23 3:34 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 94.1 70-130 6/18/23 3:34 Page 48 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-4 Canister ID: 2620 Final Vacuum(in Hg): -5 Sample ID: 23F1634-23 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4602 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 14:45 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 9.5 8.0 4.8 V-06 23 19 11 4 6/18/23 4:14 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 4:14 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 4:14 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 4:14 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 4:14 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 4:14 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 4:14 CMR 2-Butanone (MEK) 3.3 8.0 2.1 J 9.6 24 6.3 4 6/18/23 4:14 CMR Carbon Disulfide 0.34 2.0 0.18 J 1.0 6.2 0.58 4 6/18/23 4:14 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 4:14 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 4:14 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 4:14 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 4:14 CMR Chloromethane 0.18 0.40 0.16 J 0.37 0.83 0.33 4 6/18/23 4:14 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 4:14 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 4:14 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 4:14 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 4:14 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 4:14 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 4:14 CMR Dichlorodifluoromethane (Freon 12) 0.39 0.20 0.20 1.9 0.99 0.97 4 6/18/23 4:14 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 4:14 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 4:14 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 4:14 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 4:14 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 4:14 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 4:14 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 4:14 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 4:14 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 4:14 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 4:14 CMR Ethanol 16 8.0 3.5 31 15 6.6 4 6/18/23 4:14 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 4:14 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 4:14 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 4:14 CMR Heptane ND 0.20 0.13 ND 0.82 0.52 4 6/18/23 4:14 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 4:14 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 4:14 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 4:14 CMR Isopropanol 1.6 8.0 1.4 J 3.9 20 3.4 4 6/18/23 4:14 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 4:14 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 4:14 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 4:14 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 4:14 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 4:14 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 4:14 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 4:14 CMR Page 49 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-4 Sample ID: 23F1634-23 Sample Matrix: Sub Slab Sampled: 6/7/2023 14:45 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2620 Canister Size: 1 liter Flow Controller ID: 4602 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -28 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.0 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/18/23 4:14 CMR Tetrahydrofuran 3.1 2.0 0.33 9.0 5.9 0.97 4 6/18/23 4:14 CMR Toluene 2.1 0.20 0.11 7.8 0.75 0.43 4 6/18/23 4:14 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 4:14 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 4:14 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 4:14 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/18/23 4:14 CMR Trichlorofluoromethane (Freon 11) 0.25 0.80 0.24 J 1.4 4.5 1.3 4 6/18/23 4:14 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 4:14 CMR 1,2,4-Trimethylbenzene 0.32 0.20 0.088 1.6 0.98 0.43 4 6/18/23 4:14 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 4:14 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 4:14 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 4:14 CMR m&p-Xylene ND 0.40 0.22 ND 1.7 0.97 4 6/18/23 4:14 CMR o-Xylene ND 0.20 0.10 ND 0.87 0.44 4 6/18/23 4:14 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 96.6 % REC Limits 70-130 6/18/23 4:14 Page 50 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-3 Canister ID: 2913 Final Vacuum(in Hg): -5 Sample ID: 23F1634-24 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4559 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 15:00 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 18 8.0 4.8 V-06 44 19 11 4 6/18/23 4:56 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 4:56 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 4:56 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 4:56 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 4:56 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 4:56 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 4:56 CMR 2-Butanone (MEK) 2.9 8.0 2.1 J 8.7 24 6.3 4 6/18/23 4:56 CMR Carbon Disulfide 0.45 2.0 0.18 J 1.4 6.2 0.58 4 6/18/23 4:56 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 4:56 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 4:56 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 4:56 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 4:56 CMR Chloromethane 0.16 0.40 0.16 J 0.33 0.83 0.33 4 6/18/23 4:56 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 4:56 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 4:56 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 4:56 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 4:56 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 4:56 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 4:56 CMR Dichlorodifluoromethane (Freon 12) 0.33 0.20 0.20 1.6 0.99 0.97 4 6/18/23 4:56 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 4:56 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 4:56 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 4:56 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 4:56 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 4:56 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 4:56 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 4:56 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 4:56 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 4:56 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 4:56 CMR Ethanol 20 8.0 3.5 37 15 6.6 4 6/18/23 4:56 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 4:56 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 4:56 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 4:56 CMR Heptane 0.13 0.20 0.13 J 0.54 0.82 0.52 4 6/18/23 4:56 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 4:56 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 4:56 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 4:56 CMR Isopropanol 5.4 8.0 1.4 J 13 20 3.4 4 6/18/23 4:56 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 4:56 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 4:56 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 4:56 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 4:56 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 4:56 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 4:56 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 4:56 CMR Page 51 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -28 Field Sample #: MP-3 Canister ID: 2913 Final Vacuum(in Hg): -5 Sample ID: 23F1634-24 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.0 Sample Matrix: Sub Slab Flow Controller ID: 4559 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 15:00 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/18/23 4:56 CMR Tetrahydrofuran 4.9 2.0 0.33 15 5.9 0.97 4 6/18/23 4:56 CMR Toluene 2.8 0.20 0.11 11 0.75 0.43 4 6/18/23 4:56 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 4:56 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 4:56 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 4:56 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/18/23 4:56 CMR Trichlorofluoromethane (Freon 11) 1.2 0.80 0.24 6.6 4.5 1.3 4 6/18/23 4:56 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 4:56 CMR 1,2,4-Trimethylbenzene 0.24 0.20 0.088 1.2 0.98 0.43 4 6/18/23 4:56 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 4:56 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 4:56 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 4:56 CMR m&p-Xylene 0.42 0.40 0.22 1.8 1.7 0.97 4 6/18/23 4:56 CMR o-Xylene 0.13 0.20 0.10 J 0.56 0.87 0.44 4 6/18/23 4:56 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 95.9 70-130 6/18/23 4:56 Page 52 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-2 Canister ID: 2619 Final Vacuum(in Hg): -5 Sample ID: 23F1634-25 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.7 Sample Matrix: Sub Slab Flow Controller ID: 4560 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 15:11 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RI MDL Dilution Date/Time Analyzed Analyst Acetone 9.0 8.0 4.8 V-06 21 19 11 4 6/18/23 6:20 CMR Benzene ND 0.20 0.15 ND 0.64 0.48 4 6/18/23 6:20 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 6:20 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 6:20 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 6:20 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 6:20 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 6:20 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/18/23 6:20 CMR Carbon Disulfide 0.20 2.0 0.18 J 0.62 6.2 0.58 4 6/18/23 6:20 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 6:20 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 6:20 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 6:20 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 6:20 CMR Chloromethane 0.22 0.40 0.16 J 0.45 0.83 0.33 4 6/18/23 6:20 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 6:20 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 6:20 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 6:20 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 6:20 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 6:20 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 6:20 CMR Dichlorodifluoromethane (Freon 12) 0.39 0.20 0.20 1.9 0.99 0.97 4 6/18/23 6:20 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 6:20 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 6:20 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 6:20 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 6:20 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 6:20 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 6:20 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 6:20 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 6:20 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 6:20 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 6:20 CMR Ethanol 16 8.0 3.5 30 15 6.6 4 6/18/23 6:20 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 6:20 CMR Ethylbenzene ND 0.20 0.12 ND 0.87 0.51 4 6/18/23 6:20 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 6:20 CMR Heptane 0.13 0.20 0.13 J 0.52 0.82 0.52 4 6/18/23 6:20 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 6:20 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 6:20 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 6:20 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/18/23 6:20 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 6:20 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 6:20 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 6:20 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 6:20 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 6:20 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 6:20 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 6:20 CMR Page 53 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-2 Canister ID: 2619 Final Vacuum(in Hg): -5 Sample ID: 23F1634-25 Canister Size: 1 liter Receipt Vacuum(in Hg): -4.7 Sample Matrix: Sub Slab Flow Controller ID: 4560 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 15:11 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene 0.54 0.20 0.15 3.7 1.4 1.0 4 6/18/23 6:20 CMR Tetrahydrofuran 3.1 2.0 0.33 9.2 5.9 0.97 4 6/18/23 6:20 CMR Toluene 2.1 0.20 0.11 7.9 0.75 0.43 4 6/18/23 6:20 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 6:20 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 6:20 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 6:20 CMR Trichloroethylene 0.26 0.20 0.13 1.4 1.1 0.72 4 6/18/23 6:20 CMR Trichlorofluoromethane (Freon 11) 2.2 0.80 0.24 12 4.5 1.3 4 6/18/23 6:20 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 6:20 CMR 1,2,4-Trimethylbenzene 0.17 0.20 0.088 J 0.85 0.98 0.43 4 6/18/23 6:20 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 6:20 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 6:20 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 6:20 CMR m&p-Xylene 0.51 0.40 0.22 2.2 1.7 0.97 4 6/18/23 6:20 CMR o-Xylene 0.14 0.20 0.10 J 0.63 0.87 0.44 4 6/18/23 6:20 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 94.8 70-130 6/18/23 6:20 Page 54 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27.5 Field Sample #: MP-1 Canister ID: 2520 Final Vacuum(in Hg): -5 Sample ID: 23F1634-26 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.3 Sample Matrix: Sub Slab Flow Controller ID: 4606 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 15:33 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 10 8.0 4.8 V-06 25 19 11 4 6/18/23 7:02 CMR Benzene 0.23 0.20 0.15 0.73 0.64 0.48 4 6/18/23 7:02 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 7:02 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 7:02 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 7:02 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 7:02 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 7:02 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/18/23 7:02 CMR Carbon Disulfide ND 2.0 0.18 ND 6.2 0.58 4 6/18/23 7:02 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 7:02 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 7:02 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 7:02 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 7:02 CMR Chloromethane 0.72 0.40 0.16 1.5 0.83 0.33 4 6/18/23 7:02 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 7:02 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 7:02 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 7:02 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 7:02 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 7:02 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 7:02 CMR Dichlorodifluoromethane (Freon 12) 0.37 0.20 0.20 1.8 0.99 0.97 4 6/18/23 7:02 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 7:02 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 7:02 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 7:02 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 7:02 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 7:02 CMR 1,2-Dichloropropene ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 7:02 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 7:02 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 7:02 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 7:02 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 7:02 CMR Ethanol 13 8.0 3.5 25 15 6.6 4 6/18/23 7:02 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 7:02 CMR Ethylbenzene 0.22 0.20 0.12 0.96 0.87 0.51 4 6/18/23 7:02 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 7:02 CMR Heptane 0.19 0.20 0.13 J 0.79 0.82 0.52 4 6/18/23 7:02 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 7:02 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 7:02 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 7:02 CMR Isopropanol ND 8.0 1.4 ND 20 3.4 4 6/18/23 7:02 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 7:02 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 7:02 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 7:02 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 7:02 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 7:02 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 7:02 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 7:02 CMR Page 55 of 84 con-testo A Face Analy6call Laboratory Project Location: Raleigh, NC Date Received: 6/13/2023 Field Sample #: MP-1 Sample ID: 23F1634-26 Sample Matrix: Sub Slab Sampled: 6/7/2023 15:33 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Sample Description/Location: Sub Description/Location: Canister ID: 2520 Canister Size: 1 liter Flow Controller ID: 4606 Sample Type: 10 min Work Order: 23171634 Initial Vacuum(in Hg): -27.5 Final Vacuum(in Hg): -5 Receipt Vacuum(in Hg): -5.3 Flow Controller Type: Fixed -Orifice Flow Controller Calibration RPD Pre and Post -Sampling: EPA TO-15 ppbv ug/m3 Date/Time Analyte Results RL MDL Flag/Qual Results RL MDL Dilution Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/18/23 7:02 CMR Tetrahydrofuran 1.7 2.0 0.33 J 5.1 5.9 0.97 4 6/18/23 7:02 CMR Toluene 3.2 0.20 0.11 12 0.75 0.43 4 6/18/23 7:02 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 7:02 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 7:02 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 7:02 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/18/23 7:02 CMR Trichlorofluoromethane (Freon 11) 0.27 0.80 0.24 J 1.5 4.5 1.3 4 6/18/23 7:02 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 7:02 CMR 1,2,4-Trimethylbenzene 0.18 0.20 0.088 J 0.88 0.98 0.43 4 6/18/23 7:02 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 7:02 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 7:02 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 7:02 CMR m&p-Xylene 0.65 0.40 0.22 2.8 1.7 0.97 4 6/18/23 7:02 CMR o-Xylene 0.20 0.20 0.10 J 0.85 0.87 0.44 4 6/18/23 7:02 CMR Surrogates 4-Bromofluorobenzene (1) % Recovery 94.6 % REC Limits 70-130 6/18/23 7:02 Page 56 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: MP-1 DUP Canister ID: 2531 Final Vacuum(in Hg): -5 Sample ID: 23F1634-27 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Sub Slab Flow Controller ID: 4605 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 15:24 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Acetone 14 8.0 4.8 V-06 33 19 11 4 6/18/23 7:44 CMR Benzene 0.23 0.20 0.15 0.74 0.64 0.48 4 6/18/23 7:44 CMR Benzyl chloride ND 0.20 0.18 ND 1.0 0.91 4 6/18/23 7:44 CMR Bromodichloromethane ND 0.20 0.14 ND 1.3 0.94 4 6/18/23 7:44 CMR Bromoform ND 0.20 0.14 ND 2.1 1.4 4 6/18/23 7:44 CMR Bromomethane ND 0.20 0.13 ND 0.78 0.52 4 6/18/23 7:44 CMR 1,3-Butadiene ND 0.20 0.17 ND 0.44 0.37 4 6/18/23 7:44 CMR 2-Butanone (MEK) ND 8.0 2.1 ND 24 6.3 4 6/18/23 7:44 CMR Carbon Disulfide ND 2.0 0.18 ND 6.2 0.58 4 6/18/23 7:44 CMR Carbon Tetrachloride ND 0.20 0.16 ND 1.3 1.0 4 6/18/23 7:44 CMR Chlorobenzene ND 0.20 0.13 ND 0.92 0.61 4 6/18/23 7:44 CMR Chloroethane ND 0.20 0.18 ND 0.53 0.47 4 6/18/23 7:44 CMR Chloroform ND 0.20 0.19 ND 0.98 0.93 4 6/18/23 7:44 CMR Chloromethane 0.63 0.40 0.16 1.3 0.83 0.33 4 6/18/23 7:44 CMR Cyclohexane ND 0.20 0.12 ND 0.69 0.42 4 6/18/23 7:44 CMR Dibromochloromethane ND 0.20 0.13 ND 1.7 1.1 4 6/18/23 7:44 CMR 1,2-Dibromoethane (EDB) ND 0.20 0.12 ND 1.5 0.93 4 6/18/23 7:44 CMR 1,2-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.69 4 6/18/23 7:44 CMR 1,3-Dichlorobenzene ND 0.20 0.11 ND 1.2 0.67 4 6/18/23 7:44 CMR 1,4-Dichlorobenzene ND 0.20 0.13 ND 1.2 0.79 4 6/18/23 7:44 CMR Dichlorodifluoromethane (Freon 12) 0.32 0.20 0.20 1.6 0.99 0.97 4 6/18/23 7:44 CMR 1,1-Dichloroethane ND 0.20 0.17 ND 0.81 0.71 4 6/18/23 7:44 CMR 1,2-Dichloroethane ND 0.20 0.18 ND 0.81 0.73 4 6/18/23 7:44 CMR 1,1-Dichloroethylene ND 0.20 0.15 ND 0.79 0.60 4 6/18/23 7:44 CMR cis-1,2-Dichloroethylene ND 0.20 0.15 ND 0.79 0.58 4 6/18/23 7:44 CMR trans-1,2-Dichloroethylene ND 0.20 0.16 ND 0.79 0.62 4 6/18/23 7:44 CMR 1,2-Dichloropropane ND 0.20 0.11 ND 0.92 0.50 4 6/18/23 7:44 CMR cis- 1,3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.47 4 6/18/23 7:44 CMR trans- 1, 3 -Dichloropropene ND 0.20 0.10 ND 0.91 0.46 4 6/18/23 7:44 CMR 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) ND 0.20 0.20 ND 1.4 1.4 4 6/18/23 7:44 CMR 1,4-Dioxane ND 2.0 0.17 ND 7.2 0.60 4 6/18/23 7:44 CMR Ethanol 19 8.0 3.5 37 15 6.6 4 6/18/23 7:44 CMR Ethyl Acetate ND 2.0 1.0 ND 7.2 3.6 4 6/18/23 7:44 CMR Ethylbenzene 0.24 0.20 0.12 1.1 0.87 0.51 4 6/18/23 7:44 CMR 4-Ethyltoluene ND 0.20 0.12 ND 0.98 0.60 4 6/18/23 7:44 CMR Heptane 0.22 0.20 0.13 0.89 0.82 0.52 4 6/18/23 7:44 CMR Hexachlorobutadiene ND 0.20 0.16 ND 2.1 1.8 4 6/18/23 7:44 CMR Hexane ND 8.0 1.0 ND 28 3.7 4 6/18/23 7:44 CMR 2-Hexanone (MBK) ND 0.20 0.10 ND 0.82 0.41 4 6/18/23 7:44 CMR Isopropanol 1.8 8.0 1.4 J 4.5 20 3.4 4 6/18/23 7:44 CMR Methyl tert-Butyl Ether (MTBE) ND 0.20 0.15 ND 0.72 0.56 4 6/18/23 7:44 CMR Methylene Chloride ND 2.0 0.93 ND 6.9 3.2 4 6/18/23 7:44 CMR 4-Methyl-2-pentanone (MIBK) ND 0.20 0.11 ND 0.82 0.44 4 6/18/23 7:44 CMR Naphthalene ND 0.20 0.15 ND 1.0 0.79 4 6/18/23 7:44 CMR Propene ND 8.0 1.8 ND 14 3.0 4 6/18/23 7:44 CMR Styrene ND 0.20 0.11 ND 0.85 0.45 4 6/18/23 7:44 CMR 1,1,2,2-Tetrachloroethane ND 0.20 0.11 ND 1.4 0.74 4 6/18/23 7:44 CMR Page 57 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 ANALYTICAL RESULTS Project Location: Raleigh, NC Sample Description/Location: Work Order: 23171634 Date Received: 6/13/2023 Sub Description/Location: Initial Vacuum(in Hg): -27 Field Sample #: MP-1 DUP Canister ID: 2531 Final Vacuum(in Hg): -5 Sample ID: 23F1634-27 Canister Size: 1 liter Receipt Vacuum(in Hg): -5.2 Sample Matrix: Sub Slab Flow Controller ID: 4605 Flow Controller Type: Fixed -Orifice Sampled: 6/7/2023 15:24 Sample Type: 10 min Flow Controller Calibration RPD Pre and Post -Sampling: Analyte Results ppbv RL EPA TO-15 MDL Flag/Qual Results ug/m3 RL MDL Dilution Date/Time Analyzed Analyst Tetrachloroethylene ND 0.20 0.15 ND 1.4 1.0 4 6/18/23 7:44 CMR Tetrahydrofuran 2.6 2.0 0.33 7.5 5.9 0.97 4 6/18/23 7:44 CMR Toluene 3.9 0.20 0.11 15 0.75 0.43 4 6/18/23 7:44 CMR 1,2,4-Trichlorobenzene ND 0.20 0.19 ND 1.5 1.4 4 6/18/23 7:44 CMR 1, 1, 1 -Trichloroethane ND 0.20 0.16 ND 1.1 0.86 4 6/18/23 7:44 CMR 1,1,2-Trichloroethane ND 0.20 0.14 ND 1.1 0.77 4 6/18/23 7:44 CMR Trichloroethylene ND 0.20 0.13 ND 1.1 0.72 4 6/18/23 7:44 CMR Trichlorofluoromethane (Freon 11) 0.27 0.80 0.24 J 1.5 4.5 1.3 4 6/18/23 7:44 CMR 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) ND 0.80 0.22 ND 6.1 1.7 4 6/18/23 7:44 CMR 1,2,4-Trimethylbenzene 0.20 0.20 0.088 1.0 0.98 0.43 4 6/18/23 7:44 CMR 1,3,5-Trimethylbenzene ND 0.20 0.11 ND 0.98 0.52 4 6/18/23 7:44 CMR Vinyl Acetate ND 4.0 1.1 ND 14 3.8 4 6/18/23 7:44 CMR Vinyl Chloride ND 0.20 0.18 ND 0.51 0.46 4 6/18/23 7:44 CMR m&p-Xylene 0.81 0.40 0.22 3.5 1.7 0.97 4 6/18/23 7:44 CMR o-Xylene 0.22 0.20 0.10 0.96 0.87 0.44 4 6/18/23 7:44 CMR Surrogates % Recovery % REC Limits 4-Bromofluorobenzene (1) 95.3 70-130 6/18/23 7:44 Page 58 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 Sample Extraction Data Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] Batch Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL Date 23F1634-01 [MP-25] B343675 1.5 1 N/A 1000 400 150 06/16/23 23F1634-02 [MP-24] B343675 1.5 1 N/A 1000 400 150 06/16/23 23F1634-03 [MP-23] B343675 1.5 1 N/A 1000 400 150 06/16/23 23F1634-04 [MP-15] B343675 1.5 1 N/A 1000 400 150 06/16/23 23171634-05 [MP-21] B343675 1.5 1 N/A 1000 400 150 06/16/23 23F1634-06 [MP-22] B343675 1.5 1 N/A 1000 400 150 06/16/23 23F1634-07 [MP-20] B343675 1.5 1 N/A 1000 400 150 06/16/23 Prep Method: TO-15 Prep -EPA TO-15 Lab Number [Field ID] Batch Pressure Dilution Pre Dilution Pre-Dil Initial mL Pre-Dil Final mL Default Injection mL Actual Injection mL Date 23F1634-08 [MP-19] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-09 [MP-18] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-10 [MP-17] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-11 [MP-16] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-12 [MP-13] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-13 [MP-13 DUP] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-14 [MP-14] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-15 [MP-12] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-16 [MP-10] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-17 [MP-11] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-18 [MP-8] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-19 [MP-9] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-20 [MP-7] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-21 [MP-6] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-22 [MP-5] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-23 [MP-4] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-24 [MP-3] B343702 1.5 1 N/A 1000 400 150 06/17/23 23171634-25 [MP-2] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-26 [MP-1] B343702 1.5 1 N/A 1000 400 150 06/17/23 23F1634-27 [MP-1 DUP] B343702 1.5 1 N/A 1000 400 150 06/17/23 Page 59 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B343675 - TO-15 Prep Blank (B343675-BLK1) Prepared & Analyzed: 06/16/23 Acetone ND 1.4 Benzene ND 0.035 Benzyl chloride ND 0.035 Bromodichloromethane ND 0.035 Bromoform ND 0.035 Bromomethane ND 0.035 1,3-Butadiene ND 0.035 2-Butanone (MEK) ND 1.4 Carbon Disulfide ND 0.35 Carbon Tetrachloride ND 0.035 Chlorobenzene ND 0.035 Chloroethane ND 0.035 Chloroform ND 0.035 Chloromethane ND 0.070 Cyclohexane ND 0.035 Dibromochloromethane ND 0.035 1,2-Dibromoethane (EDB) ND 0.035 1,2-Dichlorobenzene ND 0.035 1,3-Dichlorobenzene ND 0.035 114-Dichlorobenzene ND 0.035 Dichlorodifluoromethane (Freon 12) ND 0.035 1,1-Dichloroethane ND 0.035 1,2-Dichloroethane ND 0.035 1,1-Dichloroethylene ND 0.035 cis-1,2-Dichloroethylene ND 0.035 trans-1,2-Dichloroethylene ND 0.035 1,2-Dichloropropane ND 0.035 cis- 1,3 -Dichloropropene ND 0.035 trans- l,3-Dichloropropene ND 0.035 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.035 (Freon 114) 1,4-Dioxane ND 0.35 Ethanol ND 1.4 Ethyl Acetate ND 0.35 Ethylbenzene ND 0.035 4-Ethyltoluene ND 0.035 Heptane ND 0.035 Hexachlorobutadiene ND 0.035 Hexane ND 1.4 2-Hexanone (MBK) ND 0.035 Isopropanol ND 1.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 Methylene Chloride ND 0.35 4-Methyl-2-pentanone (MIBK) ND 0.035 Naphthalene ND 0.035 Propene ND 1.4 Styrene ND 0.035 Page 60 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343675 - TO-15 Prep Blank (B343675-BLKI) Prepared & Analyzed: 06/16/23 1,1,2,2-Tetrachloroethane ND 0.035 Tetrachloroethylene ND 0.035 Tetrahydrofuran ND 0.35 Toluene ND 0.035 1,2,4-Trichlorobenzene ND 0.035 1, 1, 1 -Trichloroethane ND 0.035 1,1,2-Trichloroethane ND 0.035 Trichloroethylene ND 0.035 Trichlorofluoromethane (Freon 11) ND 0.14 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.14 113) 1,2,4-Trimethylbenzene ND 0.035 1,3,5-Trimethylbenzene ND 0.035 Vinyl Acetate ND 0.70 Vinyl Chloride ND 0.035 m&p-Xylene ND 0.070 o-Xylene ND 0.035 Surrogate: 4-Bromofluorobenzene (1) LCS (B343675-BS1) 7.27 8.00 90.9 Prepared & Analyzed: 06/16/23 70-130 Acetone 5.99 5.00 120 70-130 Benzene 5.01 5.00 100 70-130 Benzyl chloride 5.21 5.00 104 70-130 V-20 Bromodichloromethane 4.98 5.00 99.6 70-130 Bromoform 4.89 5.00 97.9 70-130 Bromomethane 5.15 5.00 103 70-130 1,3-Butadiene 5.55 5.00 ill 70-130 2-Butanone (MEK) 4.83 5.00 96.6 70-130 Carbon Disulfide 4.79 5.00 95.9 70-130 Carbon Tetrachloride 5.12 5.00 102 70-130 Chlorobenzene 4.76 5.00 95.1 70-130 Chloroethane 5.66 5.00 113 70-130 Chloroform 4.63 5.00 92.6 70-130 Chloromethane 5.40 5.00 108 70-130 Cyclohexane 5.28 5.00 106 70-130 Dibromochloromethane 4.98 5.00 99.7 70-130 1,2-Dibromoethane (EDB) 4.76 5.00 95.2 70-130 1,2-Dichlorobenzene 4.01 5.00 80.2 70-130 1,3-Dichlorobenzene 4.47 5.00 89.5 70-130 1,4-Dichlorobenzene 4.29 5.00 85.9 70-130 Dichlorodifluoromethane (Freon 12) 5.39 5.00 108 70-130 1,1-Dichloroethane 4.64 5.00 92.8 70-130 1,2-Dichloroethane 4.77 5.00 95.4 70-130 1,1-Dichloroethylene 4.96 5.00 99.3 70-130 cis-1,2-Dichloroethylene 4.56 5.00 91.2 70-130 trans-1,2-Dichloroethylene 4.71 5.00 94.3 70-130 1,2-Dichloropropane 5.02 5.00 100 70-130 Page 61 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343675 - TO-15 Prep LCS (B343675-BS1) Prepared & Analyzed: 06/16/23 cis-1,3-Dichloropropene 4.90 5.00 98.0 70-130 trans-1,3-Dichloropropene 5.20 5.00 104 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 4.78 5.00 95.5 70-130 (Freon 114) 1,4-Dioxane 4.92 5.00 98.4 70-130 Ethanol 5.23 5.00 105 70-130 Ethyl Acetate 4.41 5.00 88.1 70-130 Ethylbenzene 5.47 5.00 109 70-130 4-Ethyltoluene 5.46 5.00 109 70-130 Heptane 5.85 5.00 117 70-130 Hexachlorobutadiene 3.33 4.25 78.4 70-130 Hexane 4.97 5.00 99.3 70-130 2-Hexanone (MBK) 5.72 5.00 114 70-130 V-O( Isopropanol 4.61 5.00 92.1 70-130 Methyl tert-Butyl Ether (MTBE) 4.71 5.00 94.3 70-130 Methylene Chloride 4.88 5.00 97.7 70-130 4-Methyl-2-pentanone (MIBK) 5.78 5.00 116 70-130 V-2( Naphthalene 2.76 3.68 75.1 70-130 Propene 4.58 5.00 91.6 70-130 Styrene 5.33 5.00 107 70-130 1,1,2,2-Tetrachloroethane 4.87 5.00 97.5 70-130 Tetrachloroethylene 4.50 5.00 90.1 70-130 Tetrahydrofuran 4.78 5.00 95.7 70-130 Toluene 5.38 5.00 108 70-130 1,2,4-Trichlorobenzene 2.79 3.90 71.6 70-130 1, 1, 1 -Trichloroethane 4.92 5.00 98.4 70-130 1,1,2-Trichloroethane 5.23 5.00 105 70-130 Trichloroethylene 5.09 5.00 102 70-130 Trichlorofluoromethane (Freon 11) 5.38 5.00 108 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 4.37 5.00 87.4 70-130 113) 1,2,4-Trimethylbenzene 5.15 5.00 103 70-130 1,3,5-Trimethylbenzene 5.33 5.00 107 70-130 Vinyl Acetate 5.47 5.00 109 70-130 Vinyl Chloride 5.32 5.00 106 70-130 m&p-Xylene 11.7 10.0 117 70-130 V-O( o-Xylene 5.80 5.00 116 70-130 V-0( Surrogate: 4-Bromofluorobenzene (1) 7.71 8.00 96.4 70-130 Page 62 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B343702 - TO-15 Prep Blank (B343702-BLKI) Prepared & Analyzed: 06/17/23 Acetone ND 1.4 Benzene ND 0.035 Benzyl chloride ND 0.035 Bromodichloromethane ND 0.035 Bromoform ND 0.035 Bromomethane ND 0.035 1,3-Butadiene ND 0.035 2-Butanone (MEK) ND 1.4 Carbon Disulfide ND 0.35 Carbon Tetrachloride ND 0.035 Chlorobenzene ND 0.035 Chloroethane ND 0.035 Chloroform ND 0.035 Chloromethane ND 0.070 Cyclohexane ND 0.035 Dibromochloromethane ND 0.035 1,2-Dibromoethane (EDB) ND 0.035 1,2-Dichlorobenzene ND 0.035 1,3-Dichlorobenzene ND 0.035 1,4-Dichlorobenzene ND 0.035 Dichlorodifluoromethane (Freon 12) ND 0.035 1,1-Dichloroethane ND 0.035 1,2-Dichloroethane ND 0.035 1,1-Dichloroethylene ND 0.035 cis-1,2-Dichloroethylene ND 0.035 trans-1,2-Dichloroethylene ND 0.035 1,2-Dichloropropane ND 0.035 cis- 1,3 -Dichloropropene ND 0.035 trans- 1, 3 -Dichloropropene ND 0.035 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.035 (Freon 114) 1,4-Dioxane ND 0.35 Ethanol ND 1.4 Ethyl Acetate ND 0.35 Ethylbenzene ND 0.035 4-Ethyltoluene ND 0.035 Heptane ND 0.035 Hexachlorobutadiene ND 0.035 Hexane ND 1.4 2-Hexanone (MBK) ND 0.035 Isopropanol ND 1.4 Methyl tert-Butyl Ether (MTBE) ND 0.035 Methylene Chloride ND 0.35 4-Methyl-2-pentanone (MIBK) ND 0.035 Naphthalene ND 0.035 Propene ND 1.4 Styrene ND 0.035 Page 63 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343702 - TO-15 Prep Blank (B343702-BLKI) Prepared & Analyzed: 06/17/23 1,1,2,2-Tetrachloroethane ND 0.035 Tetrachloroethylene ND 0.035 Tetrahydrofuran ND 0.35 Toluene ND 0.035 1,2,4-Trichlorobenzene ND 0.035 1, 1, 1 -Trichloroethane ND 0.035 1,1,2-Trichloroethane ND 0.035 Trichloroethylene ND 0.035 Trichlorofluoromethane (Freon 11) ND 0.14 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.14 113) 1,2,4-Trimethylbenzene ND 0.035 1,3,5-Trimethylbenzene ND 0.035 Vinyl Acetate ND 0.70 Vinyl Chloride ND 0.035 m&p-Xylene ND 0.070 o-Xylene ND 0.035 Surrogate: 4-Bromofluorobenzene (1) LCS (B343702-BS1) 7.31 8.00 91.4 Prepared & Analyzed: 06/17/23 70-130 Acetone 6.20 5.00 124 70-130 V-06 Benzene 4.94 5.00 98.7 70-130 Benzyl chloride 4.85 5.00 97.0 70-130 Bromodichloromethane 4.96 5.00 99.2 70-130 Bromoform 4.81 5.00 96.2 70-130 Bromomethane 5.02 5.00 100 70-130 1,3-Butadiene 5.39 5.00 108 70-130 2-Butanone (MEK) 4.86 5.00 97.3 70-130 Carbon Disulfide 4.61 5.00 92.2 70-130 Carbon Tetrachloride 5.22 5.00 104 70-130 Chlorobenzene 4.62 5.00 92.4 70-130 Chloroethane 5.45 5.00 109 70-130 Chloroform 4.60 5.00 91.9 70-130 Chloromethane 5.33 5.00 107 70-130 Cyclohexane 5.28 5.00 106 70-130 Dibromochloromethane 4.86 5.00 97.3 70-130 1,2-Dibromoethane (EDB) 4.62 5.00 92.4 70-130 1,2-Dichlorobenzene 3.93 5.00 78.5 70-130 1,3-Dichlorobenzene 4.37 5.00 87.3 70-130 1,4-Dichlorobenzene 4.18 5.00 83.5 70-130 Dichlorodifluoromethane (Freon 12) 5.21 5.00 104 70-130 1,1-Dichloroethane 4.55 5.00 91.0 70-130 1,2-Dichloroethane 4.85 5.00 96.9 70-130 1,1-Dichloroethylene 4.92 5.00 98.4 70-130 cis-1,2-Dichloroethylene 4.57 5.00 91.3 70-130 trans-1,2-Dichloroethylene 4.68 5.00 93.5 70-130 1,2-Dichloropropane 4.95 5.00 99.0 70-130 Page 64 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343702 - TO-15 Prep LCS (B343702-BS1) Prepared & Analyzed: 06/17/23 cis-1,3-Dichloropropene 4.94 5.00 98.8 70-130 trans-1,3-Dichloropropene 5.14 5.00 103 70-130 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane 4.67 5.00 93.5 70-130 (Freon 114) 1,4-Dioxane 4.85 5.00 97.0 70-130 Ethanol 5.46 5.00 109 70-130 Ethyl Acetate 4.35 5.00 86.9 70-130 Ethylbenzene 5.33 5.00 107 70-130 4-Ethyltoluene 5.46 5.00 109 70-130 Heptane 5.88 5.00 118 70-130 Hexachlorobutadiene 3.28 4.25 77.2 70-130 Hexane 4.98 5.00 99.5 70-130 2-Hexanone (MBK) 5.60 5.00 112 70-130 V-0( Isopropanol 4.73 5.00 94.6 70-130 Methyl tert-Butyl Ether (MTBE) 4.64 5.00 92.7 70-130 Methylene Chloride 4.90 5.00 98.0 70-130 4-Methyl-2-pentanone (MIBK) 5.86 5.00 117 70-130 V-0( Naphthalene 2.68 3.68 72.9 70-130 Propene 4.56 5.00 91.2 70-130 Styrene 5.22 5.00 104 70-130 1,1,2,2-Tetrachloroethane 4.52 5.00 90.4 70-130 Tetrachloroethylene 4.45 5.00 89.0 70-130 Tetrahydrofuran 4.76 5.00 95.2 70-130 Toluene 5.17 5.00 103 70-130 1,2,4-Trichlorobenzene 2.80 3.90 71.8 70-130 1, 1, 1 -Trichloroethane 4.94 5.00 98.7 70-130 1,1,2-Trichloroethane 4.97 5.00 99.3 70-130 Trichloroethylene 5.00 5.00 100 70-130 Trichlorofluoromethane (Freon 11) 5.44 5.00 109 70-130 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 4.31 5.00 86.2 70-130 113) 1,2,4-Trimethylbenzene 5.07 5.00 101 70-130 1,3,5-Trimethylbenzene 5.21 5.00 104 70-130 Vinyl Acetate 5.51 5.00 110 70-130 Vinyl Chloride 5.11 5.00 102 70-130 m&p-Xylene 11.2 10.0 112 70-130 o-Xylene 5.56 5.00 ill 70-130 Surrogate: 4-Bromofluorobenzene (1) 7.64 8.00 95.4 70-130 Page 65 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD \nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua] Batch B343702 - TO-15 Prep Duplicate (B343702-DUPI) Source: 23171634-24 Prepared: 06/17/23 Analyzed: 06/18/23 Acetone 18 8.0 42 19 18 2.50 25 V-06 Benzene ND 0.20 ND 0.64 ND 25 Benzyl chloride ND 0.20 ND 1.0 ND 25 Bromodichloromethane ND 0.20 ND 1.3 ND 25 Bromoform ND 0.20 ND 2.1 ND 25 Bromomethane ND 0.20 ND 0.78 ND 25 1,3-Butadiene ND 0.20 ND 0.44 ND 25 2-Butanone (MEK) 2.9 8.0 8.6 24 2.9 0.136 25 J Carbon Disulfide 0.43 2.0 1.3 6.2 0.45 4.52 25 J Carbon Tetrachloride ND 0.20 ND 1.3 ND 25 Chlorobenzene ND 0.20 ND 0.92 ND 25 Chloroethane ND 0.20 ND 0.53 ND 25 Chloroform ND 0.20 ND 0.98 ND 25 Chloromethane 0.20 0.40 0.40 0.83 0.16 20.2 25 J Cyclohexane ND 0.20 ND 0.69 ND 25 Dibromochloromethane ND 0.20 ND 1.7 ND 25 1,2-Dibromoethane (EDB) ND 0.20 ND 1.5 ND 25 1,2-Dichlorobenzene ND 0.20 ND 1.2 ND 25 1,3-Dichlorobenzene ND 0.20 ND 1.2 ND 25 1,4-Dichlorobenzene ND 0.20 ND 1.2 ND 25 Dichlorodifluoromethane (Freon 12) 0.32 0.20 1.6 0.99 0.33 3.68 25 1,1-Dichloroethane ND 0.20 ND 0.81 ND 25 1,2-Dichloroethane ND 0.20 ND 0.81 ND 25 1,1-Dichloroethylene ND 0.20 ND 0.79 ND 25 cis-1,2-Dichloroethylene ND 0.20 ND 0.79 ND 25 trans-1,2-Dichloroethylene ND 0.20 ND 0.79 ND 25 1,2-Dichloropropane ND 0.20 ND 0.92 ND 25 cis- 1,3 -Dichloropropene ND 0.20 ND 0.91 ND 25 trans- 1, 3 -Dichloropropene ND 0.20 ND 0.91 ND 25 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane ND 0.20 ND 1.4 ND 25 (Freon 114) 1,4-Dioxane ND 2.0 ND 7.2 ND 25 Ethanol 19 8.0 37 15 20 1.69 25 Ethyl Acetate ND 2.0 ND 7.2 ND 25 Ethylbenzene 0.12 0.20 0.52 0.87 ND 25 J 4-Ethyltoluene ND 0.20 ND 0.98 ND 25 Heptane ND 0.20 ND 0.82 0.13 25 Hexachlorobutadiene ND 0.20 ND 2.1 ND 25 Hexane ND 8.0 ND 28 ND 25 2-Hexanone (MBK) ND 0.20 ND 0.82 ND 25 Isopropanol 5.2 8.0 13 20 5.4 4.32 25 J Methyl tert-Butyl Ether (MTBE) ND 0.20 ND 0.72 ND 25 Methylene Chloride ND 2.0 ND 6.9 ND 25 4-Methyl-2-pentanone (MIBK) ND 0.20 ND 0.82 ND 25 Naphthalene ND 0.20 ND 1.0 ND 25 Propene ND 8.0 ND 14 ND 25 Styrene ND 0.20 ND 0.85 ND 25 Page 66 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 QUALITY CONTROL Air Toxics by EPA Compendium Methods - Quality Control ppbv ug/m3 Spike Level Source %REC RPD .nalyte Results RL Results RL ppbv Result %REC Limits RPD Limit Flag/Qua Batch B343702 - TO-15 Prep Duplicate (B343702-DUP1) Source: 23F1634-24 Prepared: 06/17/23 Analyzed: 06/18/23 1,1,2,2-Tetrachloroethane ND 0.20 ND 1.4 ND 25 Tetrachloroethylene ND 0.20 ND 1.4 ND 25 Tetrahydrofuran 4.6 2.0 14 5.9 4.9 6.20 25 Toluene 2.8 0.20 11 0.75 2.8 0.707 25 1,2,4-Trichlorobenzene ND 0.20 ND 1.5 ND 25 1, 1, 1 -Trichloroethane ND 0.20 ND 1.1 ND 25 1,1,2-Trichloroethane ND 0.20 ND 1.1 ND 25 Trichloroethylene ND 0.20 ND 1.1 ND 25 Trichlorofluoromethane (Freon 11) 1.1 0.80 6.3 4.5 1.2 4.90 25 1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon ND 0.80 ND 6.1 ND 25 113) 1,2,4-Trimethylbenzene 0.24 0.20 1.2 0.98 0.24 0.00 25 1,3,5-Trimethylbenzene ND 0.20 ND 0.98 ND 25 Vinyl Acetate ND 4.0 ND 14 ND 25 Vinyl Chloride ND 0.20 ND 0.51 ND 25 m&p-Xylene 0.43 0.40 1.9 1.7 0.42 2.84 25 o-Xylene 0.13 0.20 0.57 0.87 0.13 3.08 25 J Surrogate: 4-BromoJluorobenzene (1) 7.48 8.00 93.4 70-130 Page 67 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 ` TEL. 413/525-2332 Note: Blank Subtraction is not performed unless otherwise noted FLAG/QUALIFIER SUMMARY * QC result is outside of established limits. t Wide recovery limits established for difficult compound. $ Wide RPD limits established for difficult compound. # Data exceeded client recommended or regulatory level RL Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference LCS Laboratory Control Sample LCS Dup Duplicate Laboratory Control Sample MS Matrix Spike Sample MS Dup Duplicate Matrix Spike Sample REC Recovery QC Quality Control ppbv Parts per billion volume EPA United States Environmental Protection Agency % REC Percent Recovery ND Not Detected N/A Not Applicable DL Detection Limit NC Not Calculated LFB/LCS Lab Fortified Blank/Lab Control Sample ORP Oxidation -Reduction Potential wet Not dry weight corrected % wt Percent weight Kg Kilogram g Gram mg Milligram µg Microgram ng Nanogram L Liter mL Milliliter µL Microliter m3 Cubic Meter EPH Extractable Petroleum Hydrocarbons VPH Volatile Petroleum Hydrocarbons APH Air Petroleum Hydrocarbons FID Flame Ionization Detector PID Photo Ionization Detector Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the calculation which have not been rounded. J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated concentration (CLP J-Flag). V-06 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound. V-20 Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected since sample result was "not detected" for this compound. ANALYST RLF Rebecca Faust MEM Marc E. Mahoney KMC Kristen M Couture CMR Catherine M. Rouleau Page 68 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Initial Cal Check (5087880-ICV1 Lab File ID: G23A142005.D Analyzed: 05/22/23 12:35 Bromochloromethane (1) 1177814 8.294 1177814 8.294 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 2526889 10.069 2526889 10.069 100 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2419599 14.434 2419599 14.434 100 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q Calibration Check (S089310-CCV1) Lab File ID: G23A167005.13 Analyzed: 06/16/23 11:55 Bromochloromethane (1) 1561526 8.288 1561526 8.288 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 2871931 10.062 2871931 10.062 100 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2565252 14.427 2565252 14.427 100 60-140 0.0000 +/-0.50 LCS (B343675-BS1 ) Lab File ID: G23AI67007.13 Analyzed: 06/16/23 13:14 Bromochloromethane (1) 1617615 8.294 1561526 8.288 104 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene (1) 2980402 10.068 2871931 10.062 104 60 - 140 0.0060 +/-0.50 Chlorobenzene-d5(1) 2672135 14.427 2565252 14.427 104 60-140 0.0000 +/-0.50 Blank (B343675-BLK1) Lab File ID: G23AI67012.13 Analyzed: 06/16/23 16:45 Bromochloromethane (1) 1563212 8.295 1561526 8.288 100 60 - 140 0.0070 +/-0.50 1,4-Difluorobenzene(1) 2723760 10.062 2871931 10.062 95 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2418763 14.427 2565252 14.427 94 60-140 0.0000 +/-0.50 MP-25 (23F1634-01 ) Lab File ID: G23AI67028.13 Analyzed: 06/17/23 03:29 Bromochloromethane (1) 1507830 8.295 1561526 8.288 97 60 - 140 0.0070 +/-0.50 1,4-Difluorobenzene(1) 2771903 10.063 2871931 10.062 97 60-140 0.0010 +/-0.50 Chlorobenzene-d5(1) 2675020 14.428 2565252 14.427 104 60-140 0.0010 +/-0.50 MP-24 (23F1634-02 ) Lab File ID: G23A167029.13 Analyzed: 06/17/23 04:11 Bromochloromethane (1) 1488556 8.294 1561526 8.288 95 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene(1) 2739326 10.062 2871931 10.062 95 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2603614 14.433 2565252 14.427 101 60-140 0.0060 +/-0.50 MP-23 (23F1634-03) Lab File ID: G23A167030.D Analyzed: 06/17/23 04:53 Bromochloromethane (1) 1526013 8.294 1561526 8.288 98 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene(1) 2765548 10.062 2871931 10.062 96 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2693593 14.427 2565252 14.427 105 60-140 0.0000 +/-0.50 MP-15 (23F1634-04 ) Lab File ID: G23AI67031.1) Analyzed: 06/17/23 05:35 Bromochloromethane (1) 1501867 8.294 1561526 8.288 96 60 - 140 0.0060 +/-0.50 1,4-Difluorobenzene(1) 2759593 10.062 2871931 10.062 96 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2630395 14.433 2565252 14.427 103 60-140 0.0060 +/-0.50 Page 69 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q MP-21 (23F1634-05) Lab File ID: G23A167032.D Analyzed: 06/17/23 09:07 Bromochloromethane (1) 1513128 8.288 1561526 8.288 97 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 2347877 10.056 2871931 10.062 82 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2259207 14.427 2565252 14.427 88 60-140 0.0000 +/-0.50 MP-22 (23F1634-06 ) Lab File ID: G23AI67033.D Analyzed: 06/17/23 09:48 Bromochloromethane (1) 1468783 8.295 1561526 8.288 94 60 - 140 0.0070 +/-0.50 1,4-Difluorobenzene (1) 2428268 10.062 2871931 10.062 85 60 - 140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2345717 14.427 2565252 14.427 91 60-140 0.0000 +/-0.50 MP-20 (23171634-07) Lab File ID: G23AI67034.D Analyzed: 06/17/23 10:29 Bromochloromethane (1) 1520075 8.288 1561526 8.288 97 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2567248 10.062 2871931 10.062 89 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2448941 14.427 2565252 14.427 95 60-140 0.0000 +/-0.50 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area % Limits RT Diff RT Diff Limit Q Calibration Check (S089326-CCV1) Lab File ID: G23AI68004.D Analyzed: 06/17/23 13:55 Bromochloromethane (1) 1538701 8.294 1538701 8.294 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2832465 10.068 2832465 10.068 100 60-140 0.0000 +/-0.50 Chlorobenzene-d5(1) 2633080 14.433 2633080 14.433 100 60-140 0.0000 +/-0.50 LCS (B343702-BS1) Lab File ID: G23AI68005.D Analyzed: 06/17/23 14:35 Bromochloromethane (1) 1544327 8.295 1538701 8.294 100 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene(1) 2831127 10.069 2832465 10.068 100 60-140 0.0010 +/-0.50 Chlorobenzene-d5(1) 2634214 14.428 2633080 14.433 100 60-140 -0.0050 +/-0.50 Blank (B343702-BLK1) Lab File ID: G23AI68008.D Analyzed: 06/17/23 16:49 Bromochloromethane (1) 1445847 8.295 1538701 8.294 94 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene(1) 2530603 10.063 2832465 10.068 89 60-140 -0.0050 +/-0.50 Chlorobenzene-d5(1) 2292887 14.428 2633080 14.433 87 60-140 -0.0050 +/-0.50 MP-19 (23171634-08 ) Lab File ID: G23A168009.D Analyzed: 06/17/23 17:29 Bromochloromethane (1) 1488165 8.295 1538701 8.294 97 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene(1) 2646454 10.062 2832465 10.068 93 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2583074 14.427 2633080 14.433 98 60-140 -0.0060 +/-0.50 MP-18 (23F1634-09) Lab File ID: G23A168010.1) Analyzed: 06/17/23 18:10 Bromochloromethane (1) 1531807 8.294 1538701 8.294 100 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2750174 10.062 2832465 10.068 97 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2667077 14.427 2633080 14.433 101 60-140 -0.0060 +/-0.50 Page 70 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q MP-17 (23F1634-10) Lab File ID: G23A168011.D Analyzed: 06/17/23 18:50 Bromochloromethane (1) 1509303 8.295 1538701 8.294 98 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene (1) 2695465 10.062 2832465 10.068 95 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2610556 14.427 2633080 14.433 99 60-140 -0.0060 +/-0.50 MP-16 (23F1634-11 ) Lab File ID: G23AI68012.D Analyzed: 06/17/23 19:30 Bromochloromethane (1) 1486462 8.294 1538701 8.294 97 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 2642618 10.062 2832465 10.068 93 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2572357 14.433 2633080 14.433 98 60-140 0.0000 +/-0.50 MP-13 (23F1634-12) Lab File ID: G23AI68013.D Analyzed: 06/17/23 20:11 Bromochloromethane (1) 1488428 8.295 1538701 8.294 97 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene (1) 2662324 10.062 2832465 10.068 94 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5 (1) 2521149 14.427 2633080 14.433 96 60 - 140 -0.0060 +/-0.50 MP-13 DUP (23F1634-13) Lab File ID: G23AI68014.D Analyzed: 06/17/23 20:51 Bromochloromethane (1) 1494843 8.294 1538701 8.294 97 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2703231 10.062 2832465 10.068 95 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2631893 14.427 2633080 14.433 100 60-140 -0.0060 +/-0.50 MP-14 (23F1634-14) Lab File ID: G23AI68015.D Analyzed: 06/17/23 21:31 Bromochloromethane (1) 1478223 8.288 1538701 8.294 96 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene(1) 2647887 10.062 2832465 10.068 93 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2576232 14.427 2633080 14.433 98 60-140 -0.0060 +/-0.50 MP-12 (23F1634-15) Lab File ID: G23A168016.D Analyzed: 06/17/23 22:12 Bromochloromethane (1) 1482312 8.294 1538701 8.294 96 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2631763 10.062 2832465 10.068 93 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2564118 14.427 2633080 14.433 97 60-140 -0.0060 +/-0.50 MP-10 (23F1634-16) Lab File ID: G23A168017.D Analyzed: 06/17/23 22:52 Bromochloromethane (1) 1475821 8.295 1538701 8.294 96 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene(1) 2652406 10.069 2832465 10.068 94 60-140 0.0010 +/-0.50 Chlorobenzene-d5(1) 2550899 14.434 2633080 14.433 97 60-140 0.0010 +/-0.50 MP-11 (23F1634-17) Lab File ID: G23AI68018.D Analyzed: 06/17/23 23:33 Bromochloromethane (1) 1469985 8.294 1538701 8.294 96 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2660676 10.062 2832465 10.068 94 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2552937 14.433 2633080 14.433 97 60-140 0.0000 +/-0.50 MP-8 (23F1634-18) Lab File ID: G23AI68020.D Analyzed: 06/18/23 00:52 Bromochloromethane (1) 1449347 8.295 1538701 8.294 94 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene (1) 2634390 10.063 2832465 10.068 93 60 - 140 -0.0050 +/-0.50 Chlorobenzene-d5(1) 2544320 14.428 2633080 14.433 97 60-140 -0.0050 +/-0.50 Page 71 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q MP-9 (23F1634-19) Lab File ID: G23A168021.D Analyzed: 06/18/23 01:33 Bromochloromethane (1) 1451458 8.294 1538701 8.294 94 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 2656124 10.062 2832465 10.068 94 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2567183 14.427 2633080 14.433 97 60-140 -0.0060 +/-0.50 MP-7 (23F1634-20) Lab File ID: G23AI68022.D Analyzed: 06/18/23 02:13 Bromochloromethane (1) 1510407 8.294 1538701 8.294 98 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 2697445 10.062 2832465 10.068 95 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2595152 14.433 2633080 14.433 99 60-140 0.0000 +/-0.50 MP-6 (23171634-21 ) Lab File ID: G23AI68023.D Analyzed: 06/19/23 02:53 Bromochloromethane (1) 1483896 8.295 1538701 8.294 96 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene (1) 2685567 10.063 2832465 10.068 95 60 - 140 -0.0050 +/-0.50 Chlorobenzene-d5 (1) 2591508 14.428 2633080 14.433 98 60 - 140 -0.0050 +/-0.50 MP-5 (23171634-22) Lab File ID: G23AI68024.D Analyzed: 06/18/23 03:34 Bromochloromethane (1) 1486778 8.294 1538701 8.294 97 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2723857 10.062 2832465 10.068 96 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2627405 14.427 2633080 14.433 100 60-140 -0.0060 +/-0.50 MP-4 (23171634-23 ) Lab File ID: G23AI68025.D Analyzed: 06/18/23 04:14 Bromochloromethane (1) 1516012 8.289 1538701 8.294 99 60 - 140 -0.0050 +/-0.50 1,4-Difluorobenzene(1) 2818073 10.063 2832465 10.068 99 60-140 -0.0050 +/-0.50 Chlorobenzene-d5(1) 2790061 14.428 2633080 14.433 106 60-140 -0.0050 +/-0.50 MP-3 (23171634-24) Lab File ID: G23A168026.D Analyzed: 06/18/23 04:56 Bromochloromethane (1) 1454640 8.294 1538701 8.294 95 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2689120 10.062 2832465 10.068 95 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2592447 14.427 2633080 14.433 98 60-140 -0.0060 +/-0.50 Duplicate (B343702-DUP1) Lab File ID: G23A168027.D Analyzed: 06/18/23 05:39 Bromochloromethane (1) 1454232 8.294 1538701 8.294 95 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene(1) 2602844 10.062 2832465 10.068 92 60-140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2511616 14.427 2633080 14.433 95 60-140 -0.0060 +/-0.50 MP-2 (23F1634-25) Lab File ID: G23AI68028.D Analyzed: 06/18/23 06:20 Bromochloromethane (1) 1478967 8.295 1538701 8.294 96 60 - 140 0.0010 +/-0.50 1,4-Difluorobenzene(1) 2642660 10.063 2832465 10.068 93 60-140 -0.0050 +/-0.50 Chlorobenzene-d5(1) 2541181 14.428 2633080 14.433 97 60-140 -0.0050 +/-0.50 MP-1 (23F1634-26) Lab File ID: G23AI68029.D Analyzed: 06/18/23 07:02 Bromochloromethane (1) 1438759 8.294 1538701 8.294 94 60 - 140 0.0000 +/-0.50 1,4-Difluorobenzene (1) 2595375 10.062 2832465 10.068 92 60 - 140 -0.0060 +/-0.50 Chlorobenzene-d5(1) 2502533 14.427 2633080 14.433 95 60-140 -0.0060 +/-0.50 Page 72 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 INTERNAL STANDARD AREAAND RT SUMMARY EPA TO-15 Internal Standard Response RT Reference Response Reference RT Area % Area o/ Limits RT Diff RT Diff Limit Q MP-1 DUP (23F1634-27) Lab File ID: G23A168030.D Analyzed: 06/18/23 07:44 Bromochloromethane (1) 1436445 8.288 1538701 8.294 93 60 - 140 -0.0060 +/-0.50 1,4-Difluorobenzene (1) 2608233 10.063 2832465 10.068 92 60 - 140 -0.0050 +/-0.50 Chlorobenzene-d5(1) 2504671 14.428 2633080 14.433 95 60-140 -0.0050 +/-0.50 Page 73 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 5089310-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 6.37 0.842918 1.073387 27.3 30 Benzene A 5.00 5.33 0.7637592 0.8143444 6.6 30 Benzyl chloride A 5.00 6.65 0.8073339 1.073187 32.9 30 Bromodichloromethane A 5.00 5.59 0.6340264 0.7086688 11.8 30 Bromoform A 5.00 5.48 0.5011309 0.5492282 9.6 30 Bromomethane A 5.00 5.47 0.4077907 0.4462968 9.4 30 1,3-Butadiene A 5.00 5.82 0.3749869 0.4367543 16.5 30 2-Butanone (MEK) A 5.00 5.19 1.356654 1.407894 3.8 30 Carbon Disulfide A 5.00 4.93 1.498765 1.478648 -1.3 30 Carbon Tetrachloride A 5.00 5.14 0.539535 0.5544022 2.8 30 Chlorobenzene A 5.00 5.42 0.7621755 0.8260777 8.4 30 Chloroethane A 5.00 5.85 0.2218197 0.2596025 17.0 30 Chloroform A 5.00 4.96 1.217612 1.208112 -0.8 30 Chloromethane A 5.00 6.04 0.4957722 0.5987384 20.8 30 Cyclohexane A 5.00 5.49 0.2931361 0.3216451 9.7 30 Dibromochloromethane A 5.00 5.46 0.6090453 0.6650862 9.2 30 1,2-Dibromoethane (EDB) A 5.00 5.52 0.5427769 0.5992612 10.4 30 1,2-Dichlorobenzene A 5.00 5.16 0.5821018 0.600692 3.2 30 1,3-Dichlorobenzene A 5.00 5.49 0.6255462 0.6873255 9.9 30 1,4-Dichlorobenzene A 5.00 5.38 0.6180168 0.6648566 7.6 30 Dichlorodifluoromethane (Freon 12) A 5.00 5.78 1.160248 1.341923 15.7 30 1,1-Dichloroethane A 5.00 4.91 1.08368 1.064464 -1.8 30 1,2-Dichloroethane A 5.00 5.23 0.8141384 0.8522084 4.7 30 1,1-Dichloroethylene A 5.00 5.24 0.9011757 0.9453307 4.9 30 cis-1,2-Dichloroethylene A 5.00 4.88 0.7729613 0.7544804 -2.4 30 trans-1,2-Dichloroethylene A 5.00 4.84 0.8219112 0.7959209 -3.2 30 1,2-Dichloropropane A 5.00 5.44 0.3298189 0.3585958 8.7 30 cis-1,3-Dichloropropene A 5.00 5.50 0.4150927 0.4567051 10.0 30 trans- l,3-Dichloropropene A 5.00 5.62 0.3654657 0.4104505 12.3 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 5.51 1.209903 1.332243 10.1 30 1,4-Dioxane A 5.00 5.84 0.1479759 0.1727512 16.7 30 Ethanol A 5.00 6.04 0.1349814 0.1630262 20.8 30 Ethyl Acetate A 5.00 5.26 0.2012452 0.211923 5.3 30 Ethylbenzene A 5.00 6.15 1.135348 1.395828 22.9 30 4-Ethyltoluene A 5.00 6.30 1.109241 1.397036 25.9 30 Heptane A 5.00 6.24 0.2586753 0.3226328 24.7 30 Hexachlorobutadiene A 5.00 4.90 0.387821 0.3797971 -2.1 30 Hexane A 5.00 5.15 0.8920789 0.9181613 2.9 30 Page 74 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 5089310-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 7.42 0.7281651 1.080929 48.4 30 Isopropanol A 5.00 5.75 1.000317 1.149684 14.9 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.85 1.287691 1.248881 -3.0 30 Methylene Chloride A 5.00 5.34 0.7800979 0.8338582 6.9 30 4-Methyl-2-pentanone (MI13K) A 5.00 6.76 0.7770459 1.050367 35.2 30 Naphthalene A 5.00 5.54 0.8550023 0.9476009 10.8 30 Propene A 5.00 4.70 0.5584422 0.5246499 -6.1 30 Styrene A 5.00 6.36 0.6029259 0.7664389 27.1 30 1,1,2,2-Tetrachloroethane A 5.00 6.00 0.8096179 0.9712568 20.0 30 Tetrachloroethylene A 5.00 4.97 0.4009165 0.3984669 -0.6 30 Tetrahydroforan A 5.00 5.01 0.1920565 0.192422 0.2 30 Toluene A 5.00 5.90 0.9093073 1.07351 18.1 30 1,2,4-Trichlorobenzene A 5.00 5.03 0.3643446 0.366485 0.6 30 1, 1, 1 -Trichloroethane A 5.00 5.49 0.5599026 0.6145323 9.8 30 1,1,2-Trichloroethane A 5.00 5.68 0.3528872 0.401119 13.7 30 Trichloroethylene A 5.00 5.59 0.3564595 0.398619 11.8 30 Trichlorofluoromethane(Freon 11) A 5.00 5.64 1.116203 1.258081 12.7 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 4.81 1.151585 1.107158 -3.9 30 1,2,4-Trimethylbenzene A 5.00 6.41 0.8946339 1.147531 28.3 30 1,3,5-Trimethylbenzene A 5.00 6.46 0.9396313 1.213394 29.1 30 Vinyl Acetate A 5.00 5.27 1.381 1.454866 5.3 30 Vinyl Chloride A 5.00 5.66 0.4775782 0.540457 13.2 30 m&p-Xylene A 10.0 13.2 0.8677866 1.144744 31.9 30 o-Xylene A 5.00 6.61 0.8787838 1.161751 32.2 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 75 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 5089326-CCV 1 COMPOUND TYPE. CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) Acetone A 5.00 6.79 0.842918 1.143984 35.7 30 Benzene A 5.00 5.22 0.7637592 0.7965347 4.3 30 Benzyl chloride A 5.00 6.20 0.8073339 1.000474 23.9 30 Bromodichloromethane A 5.00 5.52 0.6340264 0.7006477 10.5 30 Bromoform A 5.00 5.24 0.5011309 0.5253127 4.8 30 Bromomethane A 5.00 5.38 0.4077907 0.4387171 7.6 30 1,3-Butadiene A 5.00 5.90 0.3749869 0.4426841 18.1 30 2-Butanone (MEK) A 5.00 5.32 1.356654 1.443283 6.4 30 Carbon Disulfide A 5.00 4.71 1.498765 1.410902 -5.9 30 Carbon Tetrachloride A 5.00 5.00 0.539535 0.5400283 0.09 30 Chlorobenzene A 5.00 5.16 0.7621755 0.786456 3.2 30 Chloroethane A 5.00 5.76 0.2218197 0.255456 15.2 30 Chloroform A 5.00 4.85 1.217612 1.180996 -3.0 30 Chloromethane A 5.00 5.94 0.4957722 0.5893803 18.9 30 Cyclohexane A 5.00 5.37 0.2931361 0.3150511 7.5 30 Dibromochloromethane A 5.00 5.18 0.6090453 0.6315214 3.7 30 1,2-Dibromoethane (EDB) A 5.00 5.27 0.5427769 0.5722697 5.4 30 1,2-Dichlorobenzene A 5.00 4.98 0.5821018 0.5803321 -0.3 30 1,3-Dichlorobenzene A 5.00 5.32 0.6255462 0.6653021 6.4 30 1,4-Dichlorobenzene A 5.00 5.20 0.6180168 0.6428511 4.0 30 Dichlorodifluoromethane (Freon 12) A 5.00 5.52 1.160248 1.280612 10.4 30 1,1-Dichloroethane A 5.00 4.82 1.08368 1.043557 -3.7 30 1,2-Dichloroethane A 5.00 5.19 0.8141384 0.8444474 3.7 30 1,1-Dichloroethylene A 5.00 5.22 0.9011757 0.9414143 4.5 30 cis-1,2-Dichloroethylene A 5.00 4.90 0.7729613 0.7569699 -2.1 30 trans-1,2-Dichloroethylene A 5.00 4.80 0.8219112 0.7898278 -3.9 30 1,2-Dichloropropane A 5.00 5.34 0.3298189 0.3524834 6.9 30 cis-1,3-Dichloropropene A 5.00 5.47 0.4150927 0.4544231 9.5 30 trans- l,3-Dichloropropene A 5.00 5.62 0.3654657 0.410954 12.4 30 1,2-Dichloro- 1, 1,2,2-tetrafluoroethane (Freon 1 A 5.00 5.32 1.209903 1.286726 6.3 30 1,4-Dioxane A 5.00 5.62 0.1479759 0.1663879 12.4 30 Ethanol A 5.00 6.31 0.1349814 0.1704139 26.2 30 Ethyl Acetate A 5.00 5.24 0.2012452 0.2109988 4.8 30 Ethylbenzene A 5.00 5.85 1.135348 1.329259 17.1 30 4-Ethyltoluene A 5.00 6.08 1.109241 1.349695 21.7 30 Heptane A 5.00 6.04 0.2586753 0.3123075 20.7 30 Hexachlorobutadiene A 5.00 4.81 0.387821 0.3728124 -3.9 30 Hexane A 5.00 5.18 0.8920789 0.9233212 3.5 30 Page 76 of 84 con-testo A Face Analy6call Laboratory 39 Spruce Street' East Longmeadow, MA 01028 ` FAX 413/525-6405 " TEL. 413/525-2332 CONTINUING CALIBRATION CHECK EPA TO-15 5089326-CCV 1 COMPOUND TYPE CONC. (ppbv) RESPONSE FACTOR % DIFF / DRIFT STD CCV ICAL CCV MIN (#) CCV LIMIT (#) 2-Hexanone (MBK) A 5.00 7.12 0.7281651 1.036597 42.4 30 Isopropanol A 5.00 6.22 1.000317 1.245443 24.5 30 Methyl tert-Butyl Ether (MTBE) A 5.00 4.86 1.287691 1.250408 -2.9 30 Methylene Chloride A 5.00 5.26 0.7800979 0.8199311 5.1 30 4-Methyl-2-pentanone (MI13K) A 5.00 6.80 0.7770459 1.056324 35.9 30 Naphthalene A 5.00 5.18 0.8550023 0.886491 3.7 30 Propene A 5.00 4.96 0.5584422 0.5540798 -0.8 30 Styrene A 5.00 6.25 0.6029259 0.7534416 25.0 30 1,1,2,2-Tetrachloroethane A 5.00 5.50 0.8096179 0.8898944 9.9 30 Tetrachloroethylene A 5.00 4.84 0.4009165 0.3878056 -3.3 30 Tetrahydroforan A 5.00 4.92 0.1920565 0.1891507 -1.5 30 Toluene A 5.00 5.60 0.9093073 1.018868 12.0 30 1,2,4-Trichlorobenzene A 5.00 4.87 0.3643446 0.3548805 -2.6 30 1, 1, 1 -Trichloroethane A 5.00 5.54 0.5599026 0.6205766 10.8 30 1,1,2-Trichloroethane A 5.00 5.35 0.3528872 0.3776286 7.0 30 Trichloroethylene A 5.00 5.42 0.3564595 0.3867088 8.5 30 Trichlorofluoromethane(Freon 11) A 5.00 5.87 1.116203 1.310596 17.4 30 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 11 A 5.00 4.67 1.151585 1.076152 -6.6 30 1,2,4-Trimethylbenzene A 5.00 6.18 0.8946339 1.10607 23.6 30 1,3,5-Trimethylbenzene A 5.00 6.18 0.9396313 1.160511 23.5 30 Vinyl Acetate A 5.00 5.33 1.381 1.471563 6.6 30 Vinyl Chloride A 5.00 5.53 0.4775782 0.5278801 10.5 30 m&p-Xylene A 10.0 12.5 0.8677866 1.088249 25.4 30 o-Xylene A 5.00 6.29 0.8787838 1.105027 25.7 30 # Column to be used to flag Response Factor and %Diff/Drift values with an asterisk * Values outside of QC limits Page 77 of 84 con-testo A Face Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Acetone Benzene Benzyl chloride Bromodichloromethane Bromoform Bromomethane 1,3-Butadiene 2-Butanone (MEK) Carbon Disulfide Carbon Tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane Cyclohexane Dibromochloromethane 1,2-Dibromoethane (EDB) 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Dichlorodifluoromethane (Freon 12) 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethylene cis-1,2-Dichloroethylene trans- l,2-Dichloro ethylene 1,2-Dichloropropane cis- 1,3 -Dichloropropene trans- 1, 3 -Dichloropropene 1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114) 1,4-Dioxane Ethanol Ethyl Acetate Ethylbenzene 4-Ethyltoluene Heptane Hexachlorobutadiene Hexane 2-Hexanone (MBK) Isopropanol Methyl tart -Butyl Ether (MTBE) Methylene Chloride 4-Methyl-2-pentanone (MIBK) Naphthalene Propene Styrene 1,1,2,2-Tetrachloroethane Certifications AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH,VA AIHA, FL,NJ,NY,ME,NH, VA AIHA AIHA,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH NY,ME,NH AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA Page 78 of 84 con-testo A Face Analytical' Laboratory 39 Spruce Street ` East Longmeadow, MA 01028 ' FAX 413/525-6405 " TEL. 413/525-2332 CERTIFICATIONS Certified Analyses included in this Report Analyte EPA TO-15 in Air Tetrachloroethylene Tetrahydrofuran Toluene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethylene Trichlorofluoromethane (Freon 11) 1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113) 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl Acetate Vinyl Chloride m&p-Xylene o-Xylene Certifications AIHA,FL,NJ,NY,ME,NH, VA AIHA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NJ,NY,ME,NH,VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA,NY,ME,NH AIHA,NJ,NY,ME,NH,VA AIHA,NJ,NY,ME,NH AIHA,NJ,NY,ME,NH AIHA,FL,NJ,NY,ME,NH, VA AIHA,FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA AIHA, FL,NJ,NY,ME,NH, VA Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditation: Code Description Number Expires AHIA AIHA-LAP, LLC - ISO 17025:2017 100033 03/l/2024 NY New York State Department of Health 10899 NELAP 04/1/2024 NH New Hampshire Environmental Lab 2516 NELAP 02/5/2024 NJ New Jersey DEP MA007 NELAP 06/30/2023 FL Florida Department of Health E871027 NELAP 06/30/2024 ME State of Maine MA00100 06/9/2025 VA Commonwealth of Virginia 460217 12/14/2023 Page 79 of 84 M : u ai Fj m '0 a N EL: n ;ro £' :; tL 0 a Lab Receipt Pressure 3 2 Final Pressure m � UO Initial Pressure V C VI � O LI l a�� a q% NUJ C/ M W Nh Vi N � Y W z z M 3t U EJ o u f �i C X �► 3". L ❑❑ R ?. Q T. ?, Y F iry m E � q ;� .y a <° .e (� rN r-i 0 N p Eo vi !n a 4 Q � m isi v a y a LL 3 l • v y N U Oqro on m m 0 a ° ° V Ql 61 U a 00 V* M '00 1n �n i• Ln O �` X a 'alp �g �9 7` U it x r lwlr an * en 1r x NLA Do a,cr Q' M T- M Cb N N C4 e�J N r` rl ,S 44� ` `y` R!1 1P7 i.Rt 7 (�_r a i i! 1 1 ► 1 N UN N 00ir �'_� N N a a c N c° Y a d C a w � C Si-o1.�Cx� xxx a_ $ c E A u a m v V a v O C O '^ l] O O J k - •per A O V J 3 a � c rS A 0 QI L 7 V ml C U 40' M + i QM O V) r� r �0 80 w MM 0a W 0 �' ... r' 4o N 00 T 00 a" 4 F. — J. � � O �L 00 • 4-. V% O Q Q LA oo J q e on � i- ". V N N { ❑ ❑ ❑ ❑ ❑ v M aes m on a LY (Y tY Page 80 of 84 3 � � C � N n � n w V V d � v Page 82 of 84 6113/23, 2:51 PM Detailed Tracking Fed Ex* Tracking Summary Tracking Results SHIP SHIPPER RECIPIENT CITY, TRACKING ID DATE CITY, STATE STATUS STATE DELIVERY DATE Multi -piece shipment 772393042673 (master) 6/09/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/13/2023 2.35 pm Multi -piece shipment 772393043051 6/09/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/13/2023 2:35 pm Multi -piece shipment 772393043989 6/09/2023 RALEIGH, NC EAST LONGMEADpW, MA Delivered 6/13/2023 2:35 pm Multi -piece shipment 7722930441 72 6/09/2023 RALEIGH, NC EAST LONGMEADOW. MA Delivered 6/13/2023 2:35 pm Multi -piece shipment 772393043831 6/09/2023 RALEIGH, NC EAST LONGMEADOW, MA Delivered 6/13/2023 2:35 pm Multi -piece shipment 772393043636 6/C9/2023 RALEIGH. NC EAST LONGMEADOW, MA Delivered 6/13/2023 2:35 pm Multi -piece shipment 772393044003 6/D9/2023 RALEIGH, NC EAST LONCMEADOW, MA Delivered 6/13/2023 2:35 pm Multi -piece shipment 772393044919 6/09/2023 RALEIGH, NC EAST LONG MEADOW, MA Delivered 6/13/2023 2:35 pm OUR COMPANY About FedEx(https://www fedex.com/en-us/abcut.html) Our Portfolio(https://www,fedex.com/en-us/about/company-structure.htmn ) Investor Relations(https://investors.fedex.com/home/defauft.aspx) Careers(https://careers.fedex.com/fedex/) FedEx BIog(https://www.fedex.ccm/en-us/blog.html) Corporate Responsibility(https://www.fedex.coru/en-us/about/corporate-social-responsibiIity,htm1) Newsroom(ht'Lps://newsroom.fedex.com/) Contact Us(https://www.fedex.com/en-us/customer-support/contact-is.html) SCHEDULED DELIVERY DATE 08TAIN PROOF OF DELIVERti ASKFEDEX Page 83 of 84 https://www.fedex.com/fedextracklsummary?trknbr=772393042673,772393043051,772393043989,772393044172,772393043831,77239 39 Spruce St. East Longmeadow, MA, 01028 P: 413-525-2332 F:413-525-6405 www.pacelabs.com ENV-FRM-ELON-0009V02_Air Sample Receiving Checklist 1-12-2023 Log In Back -Sheet Login Sample Receipt Checklist— (Rejection Criteria Listing — Using Acceptance Policy) Any False statement will be brought to the attention of the Client —True or False Client A C+Cn T-nc, Project 7- MCP/RCP Required Deliverable Package Requiremen Location ,2C1tei Cln,. PWSID# (When Applicable) Arrival Method it e 6K -1-)2-3 q3()q 20 1 Received By / Date / Time IL ''t%4gQi Back -Sheet By / Date / Time KhRC t.1 t 3 I %.3 Eire QO Temperature Method Temp < 60 C ❑ Actual Temperature Rush Samples: Yes /a Notify Short Hold: Yes /(IV`o) Notify Notes regarding Samples/COC outside of SOP: TE ADVANCING SCIENCE True False Received on Ice ❑El Received in Cooler ❑IZI Custody Seal: DATE TIME ❑ COC Relinquished ® ❑ COC/Samples Labels Agree ® ❑ AI! Samples in Good Condition ® ❑ Samples Received within Holding Time ® ❑ Is there enough Volume © ❑ Proper Media/Container Used ® ❑ Individually Certified Cans ❑ Trip Blanks ❑ COC Legible ® ❑ COC Included: (Check all included) Client ® Analysis® Sampler Name El 117171 Project © IDS ® Collection Date/Time �i i 24 ReSj�5 8 L4517i�r 16 �d�� f 24 1 �2-2 9 % &9 O 1 2 25 2iDt CJ 1 i7 � 9 q 593 17 L4 5-1 t 25 L45{iZ 2 ��(j�y 10 "G3r�S 18 IS�1 26 2 � 26 2 t-I15�3 10 L. -7t 18 �`Jet2- 26 ��Qu 3 1�� 11 2�"I s 19 2 27 fir, 3 L4S-15 11 (4-10"4 19 LJ(.L,U 27 �L3� 4 2'1G14 12 I_J[$ 3 20 'L C; 28 4 k41UO 12 t{5 b 20 28 5 Cu, 13 t i 5 21 1%3 J 29 5 13 C4C, '1 21 � jIS Z 29 6 Z �3 14 �� 5 22 2-7 � 30 6 5 et 14 Ll 15 22 S ( 30 7 Z �A -1 15 2 d 23 ) u 26 31 7 14�%t`s 15 a g(OFk 23 gUol 31 �ipU58iI IVI8t118 8 16 24L1S�TQ'S 8 16 24 9 17 25 1 9 17 25 2 { y��� 10 18 26 2 10 18 26 3 11 19 27 3 11 19 27 4 q 5 -JZ 12 20 28 4 12 20 28 5� 13 21 29 5 13 21 29 6%t 14 22 30 6 14 22 30 7 is 23 31 7 15 23 Page 84 Of 84 APPENDIX F INDOOR AIR AND SUB -SLAB SOIL GAS VAPOR INTRUSION RISK CALCULATIONS Mid Atlantic Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in u¢/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 44 V 71-43-2 Benzene 0.76 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 2.1E-06 2.4E-02 74-83-9 Bromomethane 0.1 V 5.00E-03 1.0E+00 1.9E-02 75-15-0 Carbon Disulfide 1.4 V 7.00E-01 1.5E+02 1.9E-03 56-23-5 Carbon Tetrachloride 0.56 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.2E-06 5.4E-03 67-66-3 Chloroform 0.2 0.000023 V 1.2E-01 9.80E-02 2.0E+01 1.6E-06 2.0E-03 74-87-3 Chloromethane 1.4 V 9.00E-02 1.9E+01 1.5E-02 110-82-7 C clohexane 0.42 V 6.00E+00 1.3E+03 6.7E-05 75-71-8 Dichlorodifluoromethane 1.9 V 1.00E-01 2.1E+01 1.8E-02 107-06-2 Dichloroethane, 1,2- 0.19 0.000026 V 1.1E-01 7.00E-03 1.5E+40 1.5E-06 2.6E-02 78-87-5 Dichloro ro ane, 1,2- 0.097 0.0000037 1 V 7.6E-01 4.00E-03 8.3E-01 1.3E-07 2.3E-02 123-91-1 Dioxane, 1,4- 0.6 0.000005 V 5.6E-01 3.00E-02 6.3E+40 1.1E-06 1.9E-02 141-78-6 Ethyl Acetate 1.7 V 7.00E-02 1.5E+01 2.3E-02 75-00-3 Ethyl Chloride Chloroethane 0.14 V 4.00E+00 8.3E+02 3.4E-05 100-41-4 Eth lbenzene 1.1 0.0000025 V 1.1E+00 LOOE+00 2.1E+42 9.8E-07 1.1E-03 109-99-9 -Tetrah drofitran 15 V 2.00E+00 4.2E+02 7.2E-03 142-82-5 Heptane,N- 0.89 V 4.00E-01 8.3E+01 2.1E-03 110-54-3 Hexane, N- 2 V 7.00E-01 1.5E+02 2.7E-03 591-78-6 Hexanone, 2- 0.41 V 3.00E-02 6.3E+00 1.3E-02 67-63-0 Iso ro anol 8.9 V 2.00E-01 4.2E+O1 4.3E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 9.6 V - 5.00E+00 1.0E+03 1.8E-03 108-10-1 Methyl lsobutyl Ketone 4-meth 1-2- entanone 0.44 V 3.00E+00 6.3E+02 1.4E-04 91-20-3 -Naphthalene 0.36 0.000034 V 8.3E-02 3.00E-03 6.3E-01 4.4E-06 1.2E-01 115-07-1 Propylene 1.7 V 3.00E+00 6.3E+02 5.4E-04 100-42-5 Styrene 0.45 V 1.00E+00 2.1E+02 4.3E-04 127-18-4 Tetrachloroethylene 0.24 0.00000026 V 1.1E+41 4.00E-02 8.3E+00 2.2E-08 5.8E-03 108-88-3 Toluene 15 V 5.00E+00 1.0E+03 2.9E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.53 V 5.00E+00 1.0E+03 1.0E-04 79-01-6 Trichloroeth lene 0.29 0.0000041 M V 4.8E-01 2.00E-03 4.2E-01 6.1E-07 1.4E-01 75-69-4 Trichlorofluoromethane 1.2 V 95-63-6 Trimetitlbenzene, 1,2,4- 1.6 V 6.00E-02 1.3E+01 2.6E-02 108-67-8 1 Trimeth lbenzene, 1,3,5- 4 V 6 .00E-0 1.E+010 3 61..48EE--002108- Vinyl V0-O E41 Xylene, 3.5 100E-01 2.1E+41 34E-0234 95-47-6 1 X lene, o- 0.96 V 1.00E-01 2.1E+41 9.2E-03 Cumulative: I 1.4E-OS 6.1E-Ol North Cerdiea DED Risk Calculata IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 1 (IA-1 to IA-4)Adiusted ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in uo/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 44 71-43-2 Benzene 0.76 1.6E+00 2.6E+01 4.8E-07 5.8E-03 74-83-9 Bromomethane 0.1 4.4E+00 4.6E-03 75-15-0 Carbon Disulfide 1.4 6.1E+02 4.6E-04 56-23-5 Carbon Tetrachloride 0.56 2.0E+00 8.8E+01 2.7E-07 1.3E-03 67-66-3 Chloroform 0.2 5.3E-01 8.6E+01 3.8E-07 4.7E-04 74-87-3 Chloromethane 1.4 7.9E+01 3.6E-03 110-82-7 C clohexane 0.42 5.3E+03 1.6E-05 75-71-8 Dichlorodifluoromethane 1.9 8.8E+01 4.3E-03 107-06-2 Dichloroethane, 1,2- 0.19 4.7E-01 6.1E+00 4.0E-07 6.2E-03 78-87-5 Dichloro ro ane, 1,2- 0.097 3.3E+00 3.5E+00 2.9E-08 5.5E-03 123-91-1 Dioxane, 1,4- 0.6 2.5E+00 2.6E+01 2.4E-07 4.6E-03 141-78-6 Ethyl Acetate 1.7 6.1E+01 5.5E-03 75-00-3 Ethyl Chloride Chloroethane 0.14 3.5E+03 8.0E-06 100-41-4 Eth lbenzene 1.1 4.9E+00 8.8E+02 2.2E-07 2.5E-04 109-99-9 -Tetrah drofuran 15 1.8E+03 1.7E-03 142-82-5 Heptane, N- 0.89 3.5E+02 5.1E-04 110-54-3 Hexane, N- 2 6.1E+02 6.5E-04 591-78-6 Hexanone, 2- 0.41 2.6E+01 3.1E-03 67-63-0 Iso ro anol 8.9 1.8E+02 1.0E-02 78-93-3 Methyl Ethyl Ketone 2-Butanone 9.6 4.4E+03 4.4E-04 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 0.44 2.6E+03 3.3E-05 91-20-3 -Naphthalene 0.36 3.6E-01 2.6E+00 1.0E-06 2.7E-02 115-07-1 Propylene 1.7 2.6E+03 1.3E-04 100-42-5 Styrene 0.45 8.8E+02 1.0E-04 127-184 Tetrachloroethylene 0.24 4.7E+01 3.5E+01 5.1E-09 1.4E-03 108-88-3 Toluene 15 4.4E+03 6.8E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.53 4.4E+03 2.4E-05 79-01-6 Trichloroeth lene 0.29 3.0E+00 1.8E+00 9.7E-08 3.3E-02 75-694 Trichlorofluoromethane 1.2 95-63-6 Trimeth lbenzene, 1,2,4- 1.6 5.3E+01 6.1E-03 108-67-8 Trimeth lbenzene, 1,3,5- 0.4 5.3E+01 1.5E-03 108-054 Vinyl Acetate 3.8 1.8E+02 4.3E-03 108-38-3 X lene, m- 3.5 8.8E+01 8.0E-03 9547-6 X lene, o- 0.96 8.8E+01 2.2E-03 Cumulative: I 3.1E-06 1.4E-01 North Carolina DEQ Risk Calculator Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in u¢/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 35 V 71-43-2 Benzene 0.48 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 1.3E-06 1.5E-02 74-83-9 Bromomethane 0.092 V 5.00E-03 1.0E+00 1.8E-02 75-15-0 Carbon Disulfide 1.8 V 7.00E-01 1.5E+02 2.5E-03 56-23-5 Carbon Tetrachloride 0.57 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.2E-06 5.5E-03 67-66-3 Chloroform 0.51 0.000023 V 1.2E-01 9.80E-02 2.0E+01 4.2E-06 5.0E-03 74-87-3 Chloromethane 1 V 9.00E-02 1.9E+01 1.1E-02 110-82-7 C clohexane 1.3 V 6.00E+00 1.3E+03 2.1E-04 75-71-8 Dichlorodifluoromethane 2 V 1.00E-01 2.1E+01 1.9E-02 107-06-2 Dichloroethane, 1,2- 0.31 0.000026 V 1.1E-01 7.00E-03 1.5E+00 2.9E-06 4.2E-02 78-87-5 Dichloro ro ane, 1,2- 0.17 0.0000037 V 7.6E-01 4.00E-03 8.3E-01 2.2E-07 4.1E-02 141-78-6 Ethyl Acetate 2.3 V 7.00E-02 1.5E+01 3.2E-02 75-00-3 Ethyl Chloride Chloroethane 0.085 V 4.00E+00 8.3E+02 2.0E-05 100-41-4 Eth lbenzene 0.51 0.0000025 V 1.1E+00 1.00E+00 2.1E+42 4.5E-07 4.9E-04 109-99-9 -Tetrah drofuran 10 V 2.00E+00 4.2E+02 4.8E-03 142-82-5 Heptane, N- 0.52 V 4.00E-01 8.3E+01 1.2E-03 110-54-3 Hexane, N- 2.1 V 7.00E-01 1.5E+02 2.9E-03 591-78-6 Hexanone, 2- 0.46 V 3.00E-02 6.3E+00 1.5E-02 67-63-0 Iso ro anol 3.4 V 2.00E-01 4.2E+O1 1.6E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 9.8 V - 5.00E+00 1.0E+03 1.9E-03 108-10-1 Methyl lsobut ( Ketone 4-meth 1-2- entanone 0.44 V 3.00E+00 6.3E+02 1.4E-04 91-20-3 -Naphthalene 0.61 0.000034 V 8.3E-02 3.00E-03 6.3E-01 7.4E-06 1.9E-01 115-07-1 Propylene 2.2 V 3.00E+00 6.3E+02 7.0E-04 100-42-5 Styrene 0.45 V 1.00E+00 2.1E+02 4.3E-04 127-18-4 Tetrachloroethylene 0.3 0.00000026 V 1.1E+01 4.00E-02 8.3E+00 2.8E-08 7.2E-03 108-88-3 Toluene 8 V 5.00E+00 1.0E+03 1.5E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.59 V 5.00E+00 1.0E+03 1.1E-04 75-69-4 Trichlorofluoromethane 1.4 V 95-63-6 Trimeth lbenzene, 1,2,4- 2.2 V 6.00E-02 1.3E+01 3.5E-02 108-67-8 Trimeth lbenzene, 1,3,5- 0.52 V 6.00E-02 1.3E+01 8.3E-03 108-05-4 Vinyl Acetate 3.8 V 2.00E-01 4.2E+01 1.8E-02 108-38-3 X lene, in- 1.1 I 1.00E-01 2.1E+01 1.1E-02 95-47-6 1 X lene, o- 0.5 1 1.00E-01 2.1E+01 4.8E-03 Cumulative: I 1.8E-OS 5.2E-Ol North Cerdha DED Risk Calculata IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 2 (IA-5 to IA-9)Adiusted ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in no/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/ru) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 35 71-43-2 Benzene 0.48 1.6E+00 2.6E+01 3.1E-07 3.7E-03 74-83-9 Bromomethane 0.092 4.4E+00 4.2E-03 75-15-0 Carbon Disulfide 1.8 6.1E+02 5.9E-04 56-23-5 Carbon Tetrachloride 0.57 2.0E+00 8.8E+01 2.8E-07 1.3E-03 67-66-3 Chloroform 0.51 5.3E-01 8.6E+01 9.6E-07 1.2E-03 74-87-3 Chloromethane 1 7.9E+01 2.5E-03 110-82-7 C clohexane 1.3 5.3E+03 4.9E-05 75-71-8 Dichlorodifluoromethane 2 8.8E+01 4.6E-03 107-06-2 Dichloroethane, 1,2- 0.31 4.7E-01 6.1E+00 6.6E-07 1.0E-02 78-87-5 Dichloro ro ane, 1,2- 0.17 3.3E+00 3.5E+00 5.1E-08 9.7E-03 141-78-6 Ethyl Acetate 2.3 6.1E+01 7.5E-03 75-00-3 Ethyl Chloride Chloroethane 0.085 3.5E+03 4.9E-06 100-41-4 Eth lbenzene 0.51 4.9E+00 8.8E+02 1.0E-07 1.2E-04 109-99-9 -Tetrah drofuran 10 1.8E+03 1.1E-03 142-82-5 Heptane, N- 0.52 3.5E+02 3.0E-04 110-54-3 Hexane, N- 2.1 6.1E+02 6.8E-04 591-78-6 Hexanone, 2- 0.46 2.6E+01 3.5E-03 67-63-0 Iso ro anol 3.4 1.8E+02 3.9E-03 78-93-3 Methyl Ethyl Ketone 2-Butanone 9.8 4.4E+03 4.5E-04 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 0.44 2.6E+03 3.3E-05 91-20-3 -Naphthalene 0.61 3.6E-01 2.6E+00 1.7E-06 4.6E-02 115-07-1 Propylene 2.2 2.6E+03 1.7E-04 100-42-5 Styrene 0.45 8.8E+02 1.0E-04 127-184 Tetrachloroethylene 0.3 4.7E+01 3.5E+01 6.4E-09 1.7E-03 108-88-3 Toluene 8 4.4E+03 3.7E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.59 4.4E+03 2.7E-05 75-694 Trichlorofluoromethane 1.4 95-63-6 Trimeth lbenzene, 1,2,4- 2.2 5.3E+01 8.4E-03 108-67-8 Trimeth lbenzene, 1,3,5- 0.52 5.3E+01 2.0E-03 108-054 Vinyl Acetate 3.8 1.8E+02 4.3E-03 108-38-3 1 X lene, m- 1.1 8.8E+01 2.5E-03 9547-6 1 X lene, o- 0.5 8.8E+01 1.1E-03 Cumulative: I 4.1E-06 1.2E-0 l North Carolina DEQ Risk Calculator Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in u¢/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 30 V 71-43-2 Benzene 0.48 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 1.3E-06 1.5E-02 75-15-0 Carbon Disulfide 1.1 V 7.00E-01 1.5E+02 1.5E-03 56-23-5 Carbon Tetrachloride 0.52 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.1E-06 5.0E-03 67-66-3 Chloroform 0.27 0.000023 V 1.2E-01 9.80E-02 2.0E+01 2.2E-06 2.6E-03 74-87-3 Chloromethane 1.2 V 9.00E-02 1.9E+01 1.3E-02 110-82-7 C clohexane 0.42 V 6.00E+00 1.3E+03 6.7E-05 75-71-8 Dichlorodifluoromethane 2.1 V 1.00E-01 2.1E+01 2.0E-02 107-06-2 Dichloroethane, 1,2- 0.27 0.000026 V 1.1E-01 7.00E-03 1.5E+40 2.5E-06 3.7E-02 78-87-5 Dichloro ro ane, 1,2- 0.3 0.0000037 V 7.6E-01 4.00E-03 8.3E-01 4.0E-07 7.2E-02 123-91-1 Dioxane, 1,4- 0.6 0.000005 V 5.6E-01 3.00E-02 6.3E+40 1.1E-06 1.9E-02 141-78-6 Ethyl Acetate 2.3 V 7.00E-02 1.5E+01 3.2E-02 75-00-3 Ethyl Chloride Chloroethane 0.47 V 4.00E+00 8.3E+02 1.1E-04 100-41-4 Eth lbenzene 0.51 0.0000025 V 1.1E+00 LOOE+00 2.1E+02 4.5E-07 4.9E-04 109-99-9 -Tetrah drofitran 6 V 2.00E+00 4.2E+02 2.9E-03 142-82-5 Heptane, N- 0.52 V 4.00E-01 8.3E+01 1.2E-03 110-54-3 Hexane, N- 3.7 V 7.00E-01 1.5E+02 5.1E-03 591-78-6 Hexanone, 2- 0.46 V 3.00E-02 6.3E+00 1.5E-02 67-63-0 Iso ro anol 7.1 V 2.00E-01 4.2E+O1 3.4E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 7 V - 5.00E+00 1.0E+03 1.3E-03 108-10-1 Methyl lsobutyl Ketone 4-meth 1-2- entanone 0.44 V 3.00E+00 6.3E+02 1.4E-04 91-20-3 -Naphthalene 0.55 0.000034 V 8.3E-02 3.00E-03 6.3E-01 6.7E-06 1.8E-01 115-07-1 Propylene 2.3 V 3.00E+00 6.3E+02 7.4E-04 100-42-5 Styrene 0.45 V 1.00E+00 2.1E+02 4.3E-04 127-18-4 Tetrachloroethylene 1 0.00000026 V 1.1E+01 4.00E-02 8.3E+40 9.3E-08 2.4E-02 108-88-3 Toluene 8.3 V 5.00E+00 1.0E+03 1.6E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.49 V 5.00E+00 1.0E+03 9.4E-05 75-69-4 Trichlorofluoromethane 1.2 V 95-63-6 Trimeth lbenzene, 1,2,4- 0.75 V 6.00E-02 1.3E+01 1.2E-02 -6-8 Trimeth lbeene, 1,3,5- 0 V . 1.3E+1 8.3E-03 Xlene, 9 9.3E-03]O37- 95-47-6 1 X lene, o- 1 0.44 1 1 1 V I 1.00E-01 I 2.1E+01 I 4.2E-03 Cumulative: I 1.6E-OS 5.1E-Ol North Cerdiea DED Risk Calculata IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 3 (IA-10 to IA-14) Adiusted ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in uo/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 30 71-43-2 Benzene 0.48 1.6E+00 2.6E+01 3.1E-07 3.7E-03 75-15-0 Carbon Disulfide 1.1 6.1E+02 3.6E-04 56-23-5 Carbon Tetrachloride 0.52 2.0E+00 8.8E+01 2.5E-07 1.2E-03 67-66-3 Chloroform 0.27 5.3E-01 8.6E+01 5.1E-07 6.3E-04 74-87-3 Chloromethane 1.2 7.9E+01 3.0E-03 110-82-7 C clohexane 0.42 5.3E+03 1.6E-05 75-71-8 Dichlorodifluoromethane 2.1 8.8E+01 4.8E-03 107-06-2 Dichloroethane, 1,2- 0.27 4.7E-01 6.1E+00 5.7E-07 8.8E-03 78-87-5 Dichloro ro ane, 1,2- 0.3 3.3E+00 3.5E+00 9.1E-08 1.7E-02 123-91-1 Dioxane, 1,4- 0.6 2.5E+00 2.6E+01 2.4E-07 4.6E-03 141-78-6 Ethyl Acetate 2.3 6.1E+01 7.5E-03 75-00-3 Ethyl Chloride Chloroethane 0.47 3.5E+03 2.7E-05 100-41-4 Eth lbenzene 0.51 4.9E+00 8.8E+02 1.0E-07 1.2E-04 109-99-9 -Tetrah drofuran 6 1.8E+03 6.8E-04 142-82-5 He tane, N- 0.52 3.5E+02 3.0E-04 110-54-3 Hexane, N- 3.7 6.1 E+02 1.2E-03 591-78-6 Hexanone, 2- 0.46 2.6E+01 3.5E-03 67-63-0 Iso ro anol 7.1 1.8E+02 8.1E-03 78-93-3 Methyl Ethyl Ketone 2-Butanone 7 4.4E+03 3.2E-04 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 0.44 2.6E+03 3.3E-05 91-20-3 -Naphthalene 0.55 3.6E-01 2.6E+00 1.5E-06 4.2E-02 115-07-1 Propylene 2.3 2.6E+03 1.8E-04 10042-5 Styrene 0.45 8.8E+02 1.0E-04 127-184 Tetrachloroethylene 1 4.7E+01 3.5E+01 2.1E-08 5.7E-03 108-88-3 Toluene 8.3 4.4E+03 3.8E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.49 4.4E+03 2.2E-05 75-694 Trichlorofluoromethane 1.2 95-63-6 Trimeth lbenzene, 1,2,4- 0.75 5.3E+01 2.9E-03 108-67-8 Trimeth lbenzene, 1,3,5- 0.52 5.3E+01 2.0E-03 108-38-3 X lene, m- 0.97 8.8E+01 2.2E-03 9547-6 X lene, o- 0.44 8.8E+01 1.0E-03 Cumulative: I 3.6E-06 1.2E-0 l North Carolina DEQ Risk Calculator Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in u¢/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 11 V 71-43-2 Benzene 0.48 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 1.3E-06 1.5E-02 75-15-0 Carbon Disulfide 0.17 V 7.00E-01 1.5E+02 2.3E-04 56-23-5 Carbon Tetrachloride 0.5 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.1E-06 4.8E-03 74-87-3 Chloromethane 0.33 V 9.00E-02 1.9E+01 3.5E-03 110-82-7 C clohexane 0.42 V 6.00E+00 1.3E+03 6.7E-05 75-71-8 Dichlorodifluoromethane 1.9 V 1.00E-01 2.1E+01 1.8E-02 107-06-2 Dichloroethane, 1,2- 0.27 0.000026 V 1.1E-01 7.00E-03 1.5E+40 2.5E-06 3.7E-02 78-87-5 Dichloro ro ane, 1,2- 0.11 0.0000037 V 7.6E-01 4.00E-03 8.3E-01 1.4E-07 2.6E-02 123-91-1 Dioxane, 1,4- 0.6 0.000005 V 5.6E-01 3.00E-02 6.3E+40 1.1E-06 1.9E-02 141-78-6 Ethyl Acetate 0.97 V 7.00E-02 1.5E+01 1.3E-02 75-00-3 Ethyl Chloride Chloroethane 0.092 V 4.00E+00 8.3E+02 2.2E-05 100-41-4 Eth lbenzene 0.51 0.0000025 V 1.1E+00 1.00E+00 2.1E+42 4.5E-07 4.9E-04 109-99-9 -Tetrah drofitran 4.6 V 2.00E+00 4.2E+02 2.2E-03 142-82-5 Heptane, N- 0.52 V 4.00E-01 8.3E+01 1.2E-03 110-54-3 Hexane, N- 3.7 V 7.00E-01 1.5E+02 5.1E-03 591-78-6 Hexanone, 2- 0.41 V 3.00E-02 6.3E+00 1.3E-02 67-63-0 Iso ro anol 9 V 2.00E-01 4.2E+O1 4.3E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 6.3 V - 5.00E+00 1.0E+03 1.2E-03 108-10-1 Methyl Isobutyl Ketone 4-meth I-2- entanone 0.44 V 3.00E+00 6.3E+02 1.4E-04 91-20-3 -Naphthalene 0.39 0.000034 V 8.3E-02 3.00E-03 6.3E-01 4.7E-06 1.2E-01 115-07-1 Propylene 1.6 V 3.00E+00 6.3E+02 5.1E-04 100-42-5 Styrene 0.45 V 1.00E+00 2.1E+02 4.3E-04 108-88-3 Toluene 1.3 V 5.00E+00 1.0E+03 2.5E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.5 V 5.00E+00 1.0E+03 9.6E-05 75-69-4 Trichlorofluoromethane 1.2 V 95-63-6 Trhneth lbenzene, 1,2,4- 1.2 V 6.00E-02 1.3E+01 1.9E-02 108-67-8 Trimeth lbenzene, 1,3,5- 0.28 V 6.00E-02 1.3E+01 4.5E-03 108-38-3 X lene, m- 0.97 V 1.00E-01 2.1E+01 9.3E-03 95-47-6 X lene, o- 0.44 V 1.00E-01 2.1E+01 4.2E-03 Cumulative: I l.lE-OS 3.7E-Ol North Cerdiea DED Risk Calculata IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 4 ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentratinnc are in no/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 11 71-43-2 Benzene 0.48 1.6E+00 2.6E+01 3.1E-07 3.7E-03 75-15-0 Carbon Disulfide 0.17 6.1E+02 5.5E-05 56-23-5 Carbon Tetrachloride 0.5 2.0E+00 8.8E+01 2.4E-07 1.1E-03 74-87-3 Chloromethane 0.33 7.9E+01 8.4E-04 110-82-7 C clohexane 0.42 5.3E+03 1.6E-05 75-71-8 Dichlorodifluoromethane 1.9 8.8E+01 4.3E-03 107-06-2 Dichloroethane, 1,2- 0.27 4.7E-01 6.1E+00 5.7E-07 8.8E-03 78-87-5 Dichloro ro ane, 1,2- 0.11 3.3E+00 3.5E+00 3.3E-08 6.3E-03 123-91-1 Dioxane, 1,4- 0.6 2.5E+00 2.6E+01 2.4E-07 4.6E-03 141-78-6 Ethyl Acetate 0.97 6.1E+01 3.2E-03 75-00-3 Ethyl Chloride Chloroethane 0.092 3.5E+03 5.3E-06 100414 Eth lbenzene 0.51 4.9E+00 8.8E+02 1.0E-07 1.2E-04 109-99-9 -Tetrah drofivan 4.6 1.8E+03 5.3E-04 142-82-5 He tane, N- 0.52 3.5E+02 3.0E-04 110-54-3 Hexane, N- 3.7 6.1 E+02 1.2E-03 591-78-6 Hexanone, 2- 0.41 2.6E+01 3.1E-03 67-63-0 Iso ro anol 9 1.8E+02 1.0E-02 78-93-3 Methyl Ethyl Ketone 2-Butanone 6.3 4.4E+03 2.9E-04 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 0.44 2.6E+03 3.3E-05 91-20-3 -Naphthalene 0.39 3.6E-01 2.6E+00 11E-06 3.0E-02 115-07-1 Propylene 1.6 2.6E+03 1.2E-04 10042-5 Styrene 0.45 8.8E+02 1.0E-04 108-88-3 Toluene 1.3 4.4E+03 5.9E-05 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.5 4.4E+03 2.3E-05 75-69 4 Trichlorofluoromethane 1.2 95-63-6 Trimeth lbenzene, 1,2,4- 1.2 5.3E+01 4.6E-03 108-67-8 Trimeth lbenzene, 1,3,5- 0.28 5.3E+01 1.1E-03 108-38-3 X lene, m- 0.97 8.8E+01 2.2E-03 9547-6 X lene, o- 0.44 8.8E+01 1.0E-03 Cumulative: I 2.6E-06 8.8E-02 North Carolina DEQ Risk Calculator Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in u¢/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 89 V 71-43-2 Benzene 0.48 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 1.3E-06 1.5E-02 75-15-0 Carbon Disulfide 0.64 V 7.00E-01 1.5E+02 8.8E-04 56-23-5 Carbon Tetrachloride 0.49 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.0E-06 4.7E-03 67-66-3 Chloroform 0.18 0.000023 V 1.2E-01 9.80E-02 2.0E+01 1.5E-06 1.8E-03 74-87-3 Chloromethane 1.3 V 9.00E-02 1.9E+01 1.4E-02 110-82-7 C clohexane 1.2 V 6.00E+00 1.3E+03 1.9E-04 75-71-8 Dichlorodifluoromethane 2.1 V 1.00E-01 2.1E+01 2.0E-02 107-06-2 Dichloroethane, 1,2- 0.32 0.000026 V 1.1E-01 7.00E-03 1.5E+40 3.0E-06 4.4E-02 141-78-6 Ethyl Acetate 3.4 V 7.00E-02 1.5E+01 4.7E-02 75-00-3 Ethyl Chloride Chloroethane 0.11 V 4.00E+00 8.3E+02 2.6E-05 100-41-4 Eth lbenzene 0.51 0.0000025 V 1.1E+00 1.00E+00 2.1E+42 4.5E-07 4.9E-04 109-99-9 -Tetrah drofitran 29 V 2.00E+00 4.2E+02 1.4E-02 142-82-5 Heptane, N- 0.52 V 4.00E-01 8.3E+01 1.2E-03 110-54-3 Hexane, N- 2.2 V 7.00E-01 1.5E+02 3.0E-03 591-78-6 Hexanone, 2- 0.81 V 3.00E-02 6.3E+00 2.6E-02 67-63-0 Iso ro anol 6.3 V 2.00E-01 4.2E+O1 3.0E-02 78-93-3 Methyl Ethyl Ketone (2-Butanone) 33 V - 5.00E+00 1.0E+03 6.3E-03 108-10-1 Methyl lsol ut ( Ketone 4-meth 1-2- entanone 1 V 3.00E+00 6.3E+02 3.2E-04 91-20-3 -Naphthalene 0.57 0.000034 V 8.3E-02 3.00E-03 6.3E-01 6.9E-06 1.8E-01 115-07-1 Propylene 1.8 V 3.00E+00 6.3E+02 5.8E-04 100-42-5 Styrene 1.2 V 1.00E+00 2.1E+02 1.2E-03 108-88-3 Toluene 7.3 V 5.00E+00 1.0E+03 1.4E-03 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.52 V 5.00E+00 1.0E+03 1.0E-04 75-69-4 Trichlorofluoromethane 1.2 V 95-63-6 Trhneth lbenzene, 1,2,4- 1.9 V 6.00E-02 1.3E+01 3.0E-02 108-67-8 Trimeth lbenzene, 1,3,5- 0.52 V 6.00E-02 1.3E+O1 8.3E-03 108-05-4 Vinyl Acetate 4.2 V 2.00E-01 4.2E+01 2.0E-02 108-38-3 X lene, m- 1.5 V 1.00E-01 2.1E+01 1.4E-02 95-47-6 X lene, o- 0.71 V 1.00E-01 2.1E+01 6.8E-03 Cumulative: I 1.4E-OS 4.9E-Ol North Cerdiea DED Risk Calculata IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 5 QA-16 to IA-191 Adiusted ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All cnncentratinnc are in uv/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 89 71-43-2 Benzene 0.48 1.6E+00 2.6E+01 3.1E-07 3.7E-03 75-15-0 Carbon Disulfide 0.64 6.1E+02 2.1E-04 56-23-5 Carbon Tetrachloride 0.49 2.0E+00 8.8E+01 2.4E-07 1.1E-03 67-66-3 Chloroform 0.18 5.3E-01 8.6E+01 3.4E-07 4.2E-04 74-87-3 Chloromethane 1.3 7.9E+01 3.3E-03 110-82-7 C clohexane 1.2 5.3E+03 4.6E-05 75-71-8 Dichlorodifluoromethane 2.1 8.8E+01 4.8E-03 107-06-2 Dichloroethane, 1,2- 0.32 4.7E-01 6.1E+00 6.8E-07 1.0E-02 141-78-6 Ethyl Acetate 3.4 6.1E+01 1.1E-02 75-00-3 Ethyl Chloride Chloroethane 0.11 3.5E+03 6.3E-06 100-41-4 Eth lbenzene 0.51 4.9E+00 8.8E+02 1.0E-07 1.2E-04 109-99-9 -Tetrah drofuran 29 1.8E+03 3.3E-03 142-82-5 Heptane, N- 0.52 3.5E+02 3.0E-04 110-54-3 Hexane, N- 2.2 6.1E+02 7.2E-04 591-78-6 Hexanone, 2- 0.81 2.6E+01 6.2E-03 67-63-0 Iso ro anol 6.3 1.8E+02 7.2E-03 78-93-3 Methyl Ethyl Ketone 2-Butanone 33 4.4E+03 1.5E-03 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 1 2.6E+03 7.6E-05 91-20-3 -Naphthalene 0.57 3.6E-01 2.6E+00 1.6E-06 4.3E-02 115-07-1 Propylene 1.8 2.6E+03 1.4E-04 100-42-5 Styrene 1.2 8.8E+02 2.7E-04 108-88-3 Toluene 7.3 4.4E+03 3.3E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.52 4.4E+03 2.4E-05 75-69-4 Trichlorofluoromethane 1.2 95-63-6 Trimeth lbenzene, 1,2,4- 1.9 5.3E+01 7.2E-03 108-67-8 1 Trimeth lbenzene, 1,3,5- 0.52 5.3E+01 2.0E-03 108-05-4 Vinyl Acetate 4.2 1.8E+02 4.8E-03 108-38-3 X lene, m- 1.5 8.8E+01 3.4E-03 9547-6 X lene, o- 0.71 8.8E+01 1.6E-03 Cumulative: I 3.2E-06 1.2E-01 North Carolina DEQ Risk Calculator Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in ue/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 30 V 71-43-2 Benzene 0.48 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 1.3E-06 1.5E-02 75-15-0 Carbon Disulfide 0.11 V 7.00E-01 1.5E+02 1.5E-04 56-23-5 Carbon Tetrachloride 0.51 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.1E-06 4.9E-03 74-87-3 Chloromethane 0.33 V 9.00E-02 1.9E+01 3.5E-03 110-82-7 C clohexane 0.51 V 6.00E+00 1.3E+03 8.2E-05 75-71-8 Dichlorodifluoromethane 1.9 V 1.00E-01 2.1E+01 1.8E-02 141-78-6 Ethyl Acetate 2 V 7.00E-02 1.5E+01 2.7E-02 100-41-4 Eth lbenzene 0.64 0.0000025 V 1.1E+00 1.00E+00 2.1E+42 5.7E-07 6.1E-04 109-99-9 -Tetrah drofitran 39 V 2.00E+00 4.2E+02 1.9E-02 142-82-5 Heptane, N- 0.63 V 4.00E-01 8.3E+01 1.5E-03 110-54-3 J Hexane, N- 1.6 V 7.00E-01 1.5E+02 2.2E-03 591-78-6 Hexanone, 2- 0.41 V 3.00E-02 6.3E+00 1.3E-02 67-63-0 Iso ro anol 1.9 V 2.00E-01 4.2E+O1 9.1E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone) 6.3 V - 5.00E+00 1.0E+03 1.2E-03 108-10-1 Methyl lsobut ( Ketone 4-meth 1-2- entanone 0.37 V 3.00E+00 6.3E+02 1.2E-04 115-07-1 Propylene 1.7 V 3.00E+00 6.3E+02 5.4E-04 100-42-5 Styrene 0.39 V 1.00E+00 2.1E+02 3.7E-04 108-88-3 Toluene 4.4 V 5.00E+00 1.0E+03 8.4E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.46 V 5.00E+00 1.0E+03 8.8E-05 75-69-4 Trichlorofluoromethane 1.2 V 95-63-6 Trimeth lbenzene, 1,2,4- 1.3 V 6.00E-02 1.3E+01 2.1E-02 108-67-8 Trimetitlbenzene, 1,3,5- 0.34 V 6.00E-02 1.3E+01 5.4E-03 108-05-4 Vinyl Acetate 3.8 V 2.00E-01 4.2E+O1 1.8E-02 108-38-3 X lene, m- 2.2 V 1.00E-01 2.1E+01 2.1E-02 95-47-6 X lene, o- 0.97 V 1.00E-01 2.1E+01 9.3E-03 Cumulative: 1 3.0E-06 1.9E-0l NOMh Cardin. DED Risk CWWaW IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 6 (IA-21 and ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in uo/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/ru) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 30 71-43-2 Benzene 0.48 1.6E+00 2.6E+01 3.1E-07 3.7E-03 75-15-0 Carbon Disulfide 0.11 6.1E+02 3.6E-05 56-23-5 Carbon Tetrachloride 0.51 2.0E+00 8.8E+01 2.5E-07 1.2E-03 74-87-3 Chloromethane 0.33 7.9E+01 8.4E-04 110-82-7 C clohexane 0.51 5.3E+03 1.9E-05 75-71-8 Dichlorodifluoromethane 1.9 8.8E+01 4.3E-03 141-78-6 Ethyl Acetate 2 6.1E+01 6.5E-03 100414 Eth lbenzene 0.64 4.9E+00 8.8E+02 1.3E-07 1.5E-04 109-99-9 -Tetrah drofivan 39 1.8E+03 4.5E-03 142-82-5 He tane, N- 0.63 3.5E+02 3.6E-04 110-54-3 Hexane, N- 1.6 6.1 E+02 5.2E-04 591-78-6 Hexanone, 2- 0.41 2.6E+01 3.1E-03 67-63-0 Iso ro anol 1.9 1.8E+02 2.2E-03 78-93-3 Methyl Ethyl Ketone 2-Butanone 6.3 4.4E+03 2.9E-04 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 0.37 2.6E+03 2.8E-05 115-07-1 Propylene 1.7 2.6E+03 1.3E-04 10042-5 Styrene 0.39 8.8E+02 8.9E-05 108-88-3 Toluene 4.4 4.4E+03 2.0E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.46 4.4E+03 2.1E-05 75-694 Trichlorofluoromethane 1.2 95-63-6 Trimeth lbenzene, 1,2,4- 1.3 5.3E+01 4.9E-03 108-67-8 Trimeth lbenzene, 1,3,5- 0.34 5.3E+01 1.3E-03 108-054 Vinyl Acetate 3.8 1.8E+02 4.3E-03 108-38-3 X lene, m- 2.2 8.8E+01 5.0E-03 9547-6 X lene, o- 0.97 8.8E+01 2.2E-03 Cumulative: I 6.9E-07 4.6E-02 North Carolina DEQ Risk Calculator Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in u¢/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 19 V 71-43-2 Benzene 0.47 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 1.3E-06 1.5E-02 74-83-9 Bromomethane 0.36 V 5.00E-03 1.0E+00 6.9E-02 75-15-0 Carbon Disulfide 0.1 V 7.00E-01 1.5E+02 1.4E-04 56-23-5 Carbon Tetrachloride 0.5 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.1E-06 4.8E-03 67-66-3 Chloroform 0.16 0.000023 V 1.2E-01 9.80E-02 2.0E+01 1.3E-06 1.6E-03 74-87-3 Chloromethane 0.5 V 9.00E-02 1.9E+01 5.3E-03 110-82-7 C clohexane 0.42 V 6.00E+00 1.3E+03 6.7E-05 75-71-8 Dichlorodifluoromethane 1.9 V 1.00E-01 2.1E+01 1.8E-02 78-87-5 Dichloro ro ane, 1,2- 0.15 0.0000037 V 7.6E-01 4.00E-03 8.3E-01 2.0E-07 3.6E-02 100-41-4 Eth lbenzene 0.51 0.0000025 V 1.1E+00 1.00E+00 2.1E+42 4.5E-07 4.9E-04 109-99-9 -Tetrah drofuran 0.97 V 2.00E+00 4.2E+02 4.7E-04 142-82-5 Heptane, N- 0.52 V 4.00E-01 8.3E+01 1.2E-03 110-54-3 J Hexane, N- 3.7 V 7.00E-01 1.5E+02 5.1E-03 591-78-6 Hexanone, 2- 0.85 V 3.00E-02 6.3E+00 2.7E-02 67-63-0 Iso ro anol 21 V 2.00E-01 4.2E+O1 1.0E-01 78-93-3 Methyl Ethyl Ketone (2-Butanone) 6.3 V - 5.00E+00 1.0E+03 1.2E-03 108-10-1 Methyl Isobut ( Ketone 4-meth 1-2- entanone 0.44 V 3.00E+00 6.3E+02 1.4E-04 91-20-3 -Naphthalene 0.27 0.000034 V 8.3E-02 3.00E-03 6.3E-01 3.3E-06 8.6E-02 115-07-1 Propylene 1.1 V 3.00E+00 6.3E+02 3.5E-04 100-42-5 Styrene 0.45 V 1.00E+00 2.1E+02 4.3E-04 127-18-4 Tetrachloroethylene 0.21 0.00000026 V 1.1E+01 4.00E-02 8.3E+00 1.9E-08 5.0E-03 108-88-3 Toluene 0.93 V 5.00E+00 1.0E+03 1.8E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.47 V 5.00E+00 1.0E+03 9.0E-05 79-01-6 Trichloroeth lene 0.34 0.0000041 M V 4.8E-01 2.00E-03 4.2E-01 7.1E-07 1.6E-01 75-69-4 Trichlorofluoromethane 1.2 V 95-63-6 Trimeth lbenzene, 1,2,4- 0.88 V 6.00E-02 1.3E+01 1.4E-02 -8 Trimeth lbenzene, 11315- 027 V .E0 1.3 3.7E-031067 Xylene, . - 2E+1 9.3E-03 95-47-6 1 X lene, o- 1 0.44 1 1 1 V I 1.00E-01 I 2.1E+01 I 4.2E-03 Cumulative: 1 8.3E-06 5.7E-Ol North Cerdiea DED Risk Calculata IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 7 ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in no/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 19 71-43-2 Benzene 0.47 1.6E+00 2.6E+01 3.0E-07 3.6E-03 74-83-9 Bromomethane 0.36 4.4E+00 1.6E-02 75-15-0 Carbon Disulfide 0.1 6.1E+02 3.3E-05 56-23-5 Carbon Tetrachloride 0.5 2.0E+00 8.8E+01 2.4E-07 1.1E-03 67-66-3 Chloroform 0.16 5.3E-01 8.6E+01 3.0E-07 3.7E-04 74-87-3 Chloromethane 0.5 7.9E+01 1.3E-03 110-82-7 C clohexane 0.42 5.3E+03 1.6E-05 75-71-8 Dichlorodifluoromethane 1.9 8.8E+01 4.3E-03 78-87-5 Dichloro ro ane, 1,2- 0.15 3.3E+00 3.5E+00 4.5E-08 8.6E-03 100-41-4 Eth lbenzene 0.51 4.9E+00 8.8E+02 1.0E-07 1.2E-04 109-99-9 -Tetrah drofuran 0.97 1.8E+03 1.1E-04 142-82-5 He tane, N- 0.52 3.5E+02 3.0E-04 110-54-3 Hexane, N- 3.7 6.1 E+02 1.2E-03 591-78-6 Hexanone, 2- 0.85 2.6E+01 6.5E-03 67-63-0 Iso ro anol 21 1.8E+02 2.4E-02 78-93-3 Methyl Ethyl Ketone 2-Butanone 6.3 4.4E+03 2.9E-04 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 0.44 2.6E+03 3.3E-05 91-20-3 -Naphthalene 0.27 3.6E-01 2.6E+00 7.5E-07 2.1E-02 115-07-1 Propylene 1.1 2.6E+03 8.4E-05 10042-5 Styrene 0.45 8.8E+02 1.0E-04 127-184 Tetrachloroethylene 0.21 4.7E+01 3.5E+01 4.5E-09 1.2E-03 108-88-3 Toluene 0.93 4.4E+03 4.2E-05 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.47 4.4E+03 2.1E-05 79-01-6 Trichloroeth lene 0.34 3.0E+00 1.8E+00 1.1E-07 3.9E-02 75-694 Trichlorofluoromethane 1.2 95-63-6 Trimeth lbenzene, 1,2,4- 0.88 5.3E+01 3.3E-03 108-67-8 Trimeth lbenzene, 1,3,5- 0.23 5.3E+01 8.8E-04 108-38-3 X lene, m- 0.97 8.8E+01 2.2E-03 9547-6 X lene, o- 0.44 8.8E+01 1.0E-03 Cumulative: I 1.9E-06 1.4E-01 North Carolina DEQ Risk Calculator Date: January 2023 November 2022 EPA ID: ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrations are in u¢/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) IUR (ug/m3)-1 muta- gen V Target Indoor Air Cone. for Carcinogens @ TCR = 1 E-06 RIC 3 (mg/m) Target Indoor Air Cone. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 11 V 71-43-2 Benzene 0.48 0.0000078 V 3.6E-01 3.00E-02 6.3E+00 1.3E-06 1.5E-02 56-23-5 Carbon Tetrachloride 0.5 0.000006 V 4.7E-01 1.00E-01 2.1E+01 1.1E-06 4.8E-03 74-87-3 Chloromethane 0.33 V 9.00E-02 1.9E+01 3.5E-03 110-82-7 C clohexane 0.14 V 6.00E+00 1.3E+03 2.2E-05 75-71-8 Dichlorodifluoromethane 2.2 V 1.00E-01 2.1E+01 2.1E-02 141-78-6 Ethyl Acetate 0.97 V 7.00E-02 1.5E+01 1.3E-02 100-41-4 Eth lbenzene 0.51 0.0000025 V 1.1E+00 1.00E+00 2.1E+02 4.5E-07 4.9E-04 109-99-9 -Tetrah drofuran 0.97 V 2.00E+00 4.2E+02 4.7E-04 142-82-5 Heptane, N- 0.27 V 4.00E-01 8.3E+01 6.5E-04 591-78-6 Hexanone, 2- 0.41 V 3.00E-02 6.3E+00 1.3E-02 67-63-0 Iso ro anol 1.4 V 2.00E-01 4.2E+O1 6.7E-03 78-93-3 Methyl Ethyl Ketone (2-Butanone) 6.3 V - 5.00E+40 1.0E+03 1.2E-03 108-10-1 Methyl Isobut ( Ketone 4-meth I-2- entanone 0.25 V 3.00E+00 6.3E+02 8.0E-05 115-07-1 Propylene 0.87 V 3.00E+00 6.3E+02 2.8E-04 100-42-5 Styrene 0.45 V 1.00E+00 2.1E+02 4.3E-04 108-88-3 Toluene 0.57 V 5.00E+00 1.0E+03 1.1E-04 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.5 V 5.00E+00 1.0E+03 9.6E-05 75-69-4 Trichlorofluoromethane 1.2 V 95-63-6 Truneth lbenzene, 1,2,4- 0.96 V 6.00E-02 1.3E+01 1.5E-02 108-67-8 Truneth lbenzene, 1,3,5- 0.25 V 6.00E-02 1.3E+01 4.0E-03 108-OS-4 Vinyl Acetate 3.4 V 2.00E-01 4.2E+01 1.6E-02 108-38-3 X lene, m- 3.1 V 1.00E-01 2.1E+01 3.0E-02 95-47-6 1 X lene, o- 1.4 V 1.00E-01 2.1E+01 1.3E-02 Cumulative: 1 2.9E-06 1.6E-0 l North Cerdha DED Risk Calculata IDEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Indoor Air r Version Date: January 2023 Basis: November 2022 EPA RSL Table ID: Unit ID: EU 8 (IA-24. IA-25. IA-25 ** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 µg/m3. Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion. All concentrntions are in nv/m3 CAS # Chemical Name: Indoor Air Concentration 3 (ug/m) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 67-64-1 Acetone 11 71-43-2 Benzene 0.48 1.6E+00 2.6E+01 3.1E-07 3.7E-03 56-23-5 Carbon Tetrachloride 0.5 2.0E+00 8.8E+01 2.4E-07 1.1E-03 74-87-3 Chloromethane 0.33 7.9E+01 8.4E-04 110-82-7 C clohexane 0.14 5.3E+03 5.3E-06 75-71-8 Dichlorodifluoromethane 2.2 8.8E+01 5.0E-03 141-78-6 Ethyl Acetate 0.97 6.1E+01 3.2E-03 100414 Eth lbenzene 0.51 4.9E+00 8.8E+02 1.0E-07 1.2E-04 109-99-9 --Tetrah drofuran 0.97 1.8E+03 1.1E-04 142-82-5 He tane, N- 0.27 3.5E+02 1.5E-04 591-78-6 Hexanone, 2- 0.41 2.6E+01 3.1E-03 67-63-0 Iso ro anol 1.4 1.8E+02 1.6E-03 78-93-3 Methyl Ethyl Ketone 2-Butanone 6.3 4.4E+03 2.9E-04 108-10-1 Methyl Isobutyl Ketone 4-meth 1-2- entanone 0.25 2.6E+03 1.9E-05 115-07-1 Propylene 0.87 2.6E+03 6.6E-05 100-42-5 Styrene 0.45 8.8E+02 1.0E-04 108-88-3 Toluene 0.57 4.4E+03 2.6E-05 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 0.5 4.4E+03 2.3E-05 75-694 Trichlorofluoromethane 1.2 95-63-6 Trimeth lbenzene, 1,2,4- 0.96 5.3E+01 3.7E-03 108-67-8 Trimeth lbenzene, 1,3,5- 0.25 5.3E+01 9.5E-04 108-05-4 Vinyl Acetate 3.4 1.8E+02 3.9E-03 108-38-3 X lene, m- 3.1 8.8E+01 7.1E-03 9547-6 X lene, o- 1.4 8.8E+01 3.2E-03 Cumulative: I 6.5E-07 3.8E-02 North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 23076-19-092 Exposure Unit ID: Site -wide Sub -Slab Soil Gas Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in u /m3 Calculated Target Indoor Target CAS # Chemical Name: Soil Gas Concentration 3 (ug/m) Indoor Air Concentration Concentration (ug/m3) Air Conc. for Carcinogens @ TCR = 1E-06 Indoor Air Conc. for Non - Carcinogens @ THQ = 0.2 Calculated Risk Calculated Non - Carcinogenic Hazard Quotient 71-43-2 Benzene 0.74 0.0222 3.6E-01 6.3E+00 6.2E-08 7.1E-04 74-83-9 Bromomethane 0.9 0.027 - 1.0E+00 5.2E-03 75-15-0 Carbon Disulfide 4.4 0.132 - 1.5E+02 1.8E-04 67-66-3 Chloroform 1.8 0.054 1.2E-01 2.0E+01 4.4E-07 5.3E-04 74-87-3 Chloromethane 7.2 0.216 - 1.9E+01 2.3E-03 110-82-7 C clohexane 2 0.06 - 1.3E+03 9.6E-06 106-93-4 Dibromoethane, 1,2- 0.93 0.0279 4.7E-03 1.9E+00 6.0E-06 3.0E-03 75-71-8 Dichlorodifluoromethane 2.2 0.066 - 2.1E+01 6.3E-04 75-34-3 Dichloroethane, 1,1- 0.71 0.0213 1.8E+00 - 1.2E-08 78-87-5 Dichloro ro one, 1,2- 1.3 0.039 7.6E-01 8.3E-01 5.1E-08 9.3E-03 123-91-1 Dioxane, 1,4- 0.81 0.0243 5.6E-01 6.3E+00 4.3E-08 7.8E-04 141-78-6 Ethyl Acetate 3.8 0.114 - 1.5E+01 1.6E-03 75-00-3 Ethyl Chloride Chloroethane 1.8 0.054 - 8.3E+02 1.3E-05 100-41-4 Eth lbenzene 1.1 0.033 1.1E+00 2.1E+02 2.9E-08 3.2E-05 109-99-9 -Tetrah drofuran 29 0.87 - 4.2E+02 4.2E-04 142-82-5 He tare, N- 0.89 0.0267 - 8.3E+01 6.4E-05 591-78-6 Hexanone, 2- 2.5 0.075 - 6.3E+00 2.4E-03 67-63-0 Iso ro anol 35 1.05 - 4.2E+01 5.0E-03 78-93-3 Methyl Ethyl Ketone 2-Butanone 33 0.99 - 1.0E+03 1.9E-04 108-10-1 Methyl Isobu 1 Ketone 4-meth 1-2- entanone) 1 0.03 - 6.3E+02 9.6E-06 75-09-2 Methylene Chloride 5 0.15 1.0E+02 1.3E+02 1.5E-09 2.4E-04 91-20-3 -Naphthalene 1.1 0.033 8.3E-02 6.3E-01 4.0E-07 1.1E-02 100-42-5 Styrene 1.2 0.036 - 2.1E+02 3.5E-05 127-18-4 Tetrachloroeth lene 5.1 0.153 1.1E+01 8.3E+00 1.4E-08 3.7E-03 108-88-3 Toluene 15 0.45 - 1.0E+03 8.6E-05 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 11 0.33 - 1.0E+03 6.3E-05 71-55-6 Trichloroethane, 1,1,1- 1.4 0.042 - 1.0E+03 8.1E-06 79-01-6 Trichloroeth lene 1.6 0.048 4.8E-01 4.2E-01 1.0E-07 2.3E-02 95-63-6 Trimeth lbenzene, 1,2,4- 5.3 0.159 - 1.3E+01 2.5E-03 108-05-4 Vinyl Acetate 4.2 0.126 - 4.2E+01 6.0E-04 108-38-3 X lene, m- 3.5 0.105 - 2.1E+01 1.0E-03 9547-6 X lene, o- 0.97 0.0291 - 2.1E+01 2.8E-04 North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Non -Residential Worker Soil Gas to Indoor Air 1 Version Date: July 2023 Basis: May 2023 EPA RSL Table Site ID: 23076-19-092 jmmi& Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. All concentrations are in ue/m3 CAS # Chemical Name: Soil Gas Concentration 3 (ug/m) Calculated Indoor Air Concentration (ug/ms) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non - Carcinogens @ T'HQ = 0.2 Calculated Carcinogenic Risk Calculated Non - Carcinogenic Hazard Quotient 71-43-2 Benzene 0.74 0.0074 1.6E+00 2.6E+01 4.7E-09 5.6E-05 74-83-9 Bromomethane 0.9 0.009 4.4E+00 4.1E-04 75-15-0 Carbon Disulfide 4.4 0.044 6.1E+02 1.4E-05 67-66-3 Chloroform 1.8 0.018 5.3E-01 8.6E+01 3.4E-08 4.2E-05 74-87-3 Chloromethane 7.2 0.072 7.9E+01 1.8E-04 110-82-7 C clohexane 2 0.02 5.3E+03 7.6E-07 106-93-4 Dibromoethane, 1,2- 0.93 0.0093 2.0E-02 7.9E+00 4.5E-07 2.4E-04 75-71-8 Dichlorodifluoromethane 2.2 0.022 8.8E+01 5.0E-05 75-34-3 Dichloroethane, 1,1- 0.71 0.0071 7.7E+00 9.3E-10 78-87-5 Dichloro ro ane, 1,2- 1.3 0.013 3.3E+00 3.5E+00 3.9E-09 7.4E-04 123-91-1 Dioxane, 1,4- 0.81 0.0081 2.5E+00 2.6E+01 3.3E-09 6.2E-05 141-78-6 Ethyl Acetate 3.8 0.038 6.1E+01 1.2E-04 75-00-3 Ethyl Chloride (Chloroethane) 1.8 0.018 3.5E+03 1.0E-06 100-41-4 Eth lbenzene 1.1 0.011 4.9E+00 8.8E+02 2.2E-09 2.5E-06 109-99-9 -Tetrah drofuran 29 0.29 1.8E+03 3.3E-05 142-82-5 Heptane, N- 0.89 0.0089 3.5E+02 5.1E-06 591-78-6 Hexanone, 2- 2.5 0.025 2.6E+01 1.9E-04 67-63-0 Iso ro anol 35 0.35 1.8E+02 4.0E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone) 33 0.33 4.4E+03 1.5E-05 108-10-1 Methyl Isobutyl Ketone (4-meth 1-2- entanone) 1 0.01 2.6E+03 7.6E-07 75-09-2 Methylene Chloride 5 0.05 1.2E+03 5.3E+02 4.1E-11 1.9E-05 91-20-3 -Naphthalene 1.1 0.011 3.6E-01 2.6E+00 3.0E-08 8.4E-04 100-42-5 Styrene 1.2 0.012 8.8E+02 2.7E-06 127-18-4 Tetrachloroethylene 5.1 0.051 4.7E+01 3.5E+01 1.1E-09 2.9E-04 108-88-3 Toluene 15 0.15 4.4E+03 6.8E-06 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 11 0.11 4.4E+03 5.0E-06 71-55-6 Trichloroethane, 1,1,1- 1.4 0.014 4.4E+03 6.4E-07 79-01-6 Trichloroethylene 1.6 0.016 3.0E+00 1.8E+00 5.3E-09 1.8E-03 95-63-6 Trimeth lbenzene, 1,2,4- 5.3 0.053 5.3E+01 2.0E-04 108-05-4 Vinyl Acetate 4.2 0.042 1.8E+02 4.8E-05 108-39-3 X lene, m- 3.5 0.035 8.8E+01 8.0E-05 95-47-6 X lene, o- 0.97 0.0097 8.8E+01 2.2E-05 Cumulative: I 5.4E-07 I 5.9E-03 North Carolina DEQ Risk Calculator