WS-4367_14183_CA_LAB_20100304

March 17, 2010
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 9264720
9264720
Project:
Pace Project No.:
RE:
Ms. Linda Blalock
NCDENR - UST Section
1637 Mail Service Center
Raleigh, NC 276991637
BOWEK'S TRUCKING 1354-09-25-8
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on March 05, 2010. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Charlotte Certification IDsFlorida/NELAP Certification #: E87627Kentucky UST Certification #: 84
9800 Kincey Ave. - Ste 100 Huntersville, NC 28078West Virginia Certification #: 357Virginia Certification #: 00213Tennessee Certification #: 04010South Carolina Drinking Water Cert. #: 990060003
South Carolina Certification #: 990060001
Pennsylvania Certification #: 68-00784North Carolina Wastewater Certification #: 12
North Carolina Field Services Certification #: 5342North Carolina Drinking Water Certification #: 37706New Jersey Certification #: NC012Louisiana/LELAP Certification #: 04034Connecticut Certification #: PH-0104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9264720001 B3-14 MADEP VPH 5 PASI-CDHW
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9264720002 B3-34 MADEP VPH 5 PASI-CDHW
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9264720003 MW-3-4 MADEP VPH 5 PASI-CDHW
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9264720004 MW-3-34 MADEP VPH 5 PASI-CDHW
EPA 8260 71 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
9264720005 MW-3-24 MADEP VPH 5 PASI-CDHW
ASTM D2974-87 1 PASI-CKDF
9264720006 MW-3-14 MADEP VPH 5 PASI-CDHW
ASTM D2974-87 1 PASI-CKDF
9264720007 MW-3-34 MADEP VPH 5 PASI-CDHW
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:B3-14 Lab ID:9264720001 Collected:03/04/10 10:10 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-C08)119 mg/kg 1 03/15/10 20:4803/15/10 16:3210.0
Aliphatic (C09-C12)701 mg/kg 1 03/15/10 20:4803/15/10 16:3210.0
Aromatic (C09-C10)186 mg/kg 1 03/15/10 20:4803/15/10 16:3210.0
2,5-Dibromotoluene (PID)(S)105 %1 03/15/10 20:4803/15/10 16:3270-130
2,5-Dibromotoluene (FID)(S)136 %1 03/15/10 20:48 S503/15/10 16:3270-130
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND mg/kg 250 03/09/10 20:49 67-64-126.4
Benzene ND mg/kg 250 03/09/10 20:49 71-43-21.3
Bromobenzene ND mg/kg 250 03/09/10 20:49 108-86-11.3
Bromochloromethane ND mg/kg 250 03/09/10 20:49 74-97-51.3
Bromodichloromethane ND mg/kg 250 03/09/10 20:49 75-27-41.3
Bromoform ND mg/kg 250 03/09/10 20:49 75-25-21.3
Bromomethane ND mg/kg 250 03/09/10 20:49 74-83-92.6
2-Butanone (MEK)ND mg/kg 250 03/09/10 20:49 78-93-326.4
n-Butylbenzene ND mg/kg 250 03/09/10 20:49 104-51-81.3
sec-Butylbenzene 4.0 mg/kg 250 03/09/10 20:49 135-98-81.3
tert-Butylbenzene ND mg/kg 250 03/09/10 20:49 98-06-61.3
Carbon tetrachloride ND mg/kg 250 03/09/10 20:49 56-23-51.3
Chlorobenzene ND mg/kg 250 03/09/10 20:49 108-90-71.3
Chloroethane ND mg/kg 250 03/09/10 20:49 75-00-32.6
Chloroform ND mg/kg 250 03/09/10 20:49 67-66-31.3
Chloromethane ND mg/kg 250 03/09/10 20:49 74-87-32.6
2-Chlorotoluene ND mg/kg 250 03/09/10 20:49 95-49-81.3
4-Chlorotoluene ND mg/kg 250 03/09/10 20:49 106-43-41.3
1,2-Dibromo-3-chloropropane ND mg/kg 250 03/09/10 20:49 96-12-81.3
Dibromochloromethane ND mg/kg 250 03/09/10 20:49 124-48-11.3
1,2-Dibromoethane (EDB)ND mg/kg 250 03/09/10 20:49 106-93-41.3
Dibromomethane ND mg/kg 250 03/09/10 20:49 74-95-31.3
1,2-Dichlorobenzene ND mg/kg 250 03/09/10 20:49 95-50-11.3
1,3-Dichlorobenzene ND mg/kg 250 03/09/10 20:49 541-73-11.3
1,4-Dichlorobenzene ND mg/kg 250 03/09/10 20:49 106-46-71.3
Dichlorodifluoromethane ND mg/kg 250 03/09/10 20:49 75-71-82.6
1,1-Dichloroethane ND mg/kg 250 03/09/10 20:49 75-34-31.3
1,2-Dichloroethane ND mg/kg 250 03/09/10 20:49 107-06-21.3
1,1-Dichloroethene ND mg/kg 250 03/09/10 20:49 75-35-41.3
cis-1,2-Dichloroethene ND mg/kg 250 03/09/10 20:49 156-59-21.3
trans-1,2-Dichloroethene ND mg/kg 250 03/09/10 20:49 156-60-51.3
1,2-Dichloropropane ND mg/kg 250 03/09/10 20:49 78-87-51.3
1,3-Dichloropropane ND mg/kg 250 03/09/10 20:49 142-28-91.3
2,2-Dichloropropane ND mg/kg 250 03/09/10 20:49 594-20-71.3
1,1-Dichloropropene ND mg/kg 250 03/09/10 20:49 563-58-61.3
cis-1,3-Dichloropropene ND mg/kg 250 03/09/10 20:49 10061-01-51.3
trans-1,3-Dichloropropene ND mg/kg 250 03/09/10 20:49 10061-02-61.3
Diisopropyl ether ND mg/kg 250 03/09/10 20:49 108-20-31.3
Ethylbenzene 20.6 mg/kg 250 03/09/10 20:49 100-41-41.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 4 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:B3-14 Lab ID:9264720001 Collected:03/04/10 10:10 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Hexachloro-1,3-butadiene ND mg/kg 250 03/09/10 20:49 87-68-31.3
2-Hexanone ND mg/kg 250 03/09/10 20:49 591-78-613.2
Isopropylbenzene (Cumene)5.2 mg/kg 250 03/09/10 20:49 98-82-81.3
p-Isopropyltoluene 12.0 mg/kg 250 03/09/10 20:49 99-87-61.3
Methylene Chloride ND mg/kg 250 03/09/10 20:49 75-09-25.3
4-Methyl-2-pentanone (MIBK)ND mg/kg 250 03/09/10 20:49 108-10-113.2
Methyl-tert-butyl ether ND mg/kg 250 03/09/10 20:49 1634-04-41.3
Naphthalene 29.4 mg/kg 250 03/09/10 20:49 91-20-31.3
n-Propylbenzene 13.0 mg/kg 250 03/09/10 20:49 103-65-11.3
Styrene ND mg/kg 250 03/09/10 20:49 100-42-51.3
1,1,1,2-Tetrachloroethane ND mg/kg 250 03/09/10 20:49 630-20-61.3
1,1,2,2-Tetrachloroethane ND mg/kg 250 03/09/10 20:49 79-34-51.3
Tetrachloroethene ND mg/kg 250 03/09/10 20:49 127-18-41.3
Toluene 21.3 mg/kg 250 03/09/10 20:49 108-88-31.3
1,2,3-Trichlorobenzene ND mg/kg 250 03/09/10 20:49 87-61-61.3
1,2,4-Trichlorobenzene ND mg/kg 250 03/09/10 20:49 120-82-11.3
1,1,1-Trichloroethane ND mg/kg 250 03/09/10 20:49 71-55-61.3
1,1,2-Trichloroethane ND mg/kg 250 03/09/10 20:49 79-00-51.3
Trichloroethene ND mg/kg 250 03/09/10 20:49 79-01-61.3
Trichlorofluoromethane ND mg/kg 250 03/09/10 20:49 75-69-41.3
1,2,3-Trichloropropane ND mg/kg 250 03/09/10 20:49 96-18-41.3
1,2,4-Trimethylbenzene 111 mg/kg 1250 03/10/10 17:38 95-63-66.6
1,3,5-Trimethylbenzene 44.5 mg/kg 1250 03/10/10 17:38 108-67-86.6
Vinyl acetate ND mg/kg 250 03/09/10 20:49 108-05-413.2
Vinyl chloride ND mg/kg 250 03/09/10 20:49 75-01-42.6
Xylene (Total)143 mg/kg 250 03/09/10 20:49 1330-20-72.6
m&p-Xylene 93.9 mg/kg 250 03/09/10 20:49 1330-20-72.6
o-Xylene 48.8 mg/kg 250 03/09/10 20:49 95-47-61.3
Dibromofluoromethane (S)116 %250 03/09/10 20:49 1868-53-779-116
Toluene-d8 (S)103 %250 03/09/10 20:49 2037-26-588-110
4-Bromofluorobenzene (S)96 %250 03/09/10 20:49 460-00-474-115
1,2-Dichloroethane-d4 (S)115 %250 03/09/10 20:49 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.0 %1 03/08/10 14:430.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 5 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:B3-34 Lab ID:9264720002 Collected:03/04/10 10:36 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-C08)ND mg/kg 1 03/15/10 21:1303/15/10 16:329.8
Aliphatic (C09-C12)25.8 mg/kg 1 03/15/10 21:1303/15/10 16:329.8
Aromatic (C09-C10)ND mg/kg 1 03/15/10 21:1303/15/10 16:329.8
2,5-Dibromotoluene (PID)(S)120 %1 03/15/10 21:1303/15/10 16:3270-130
2,5-Dibromotoluene (FID)(S)138 %1 03/15/10 21:13 S503/15/10 16:3270-130
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND mg/kg 1 03/09/10 19:54 67-64-10.094
Benzene ND mg/kg 1 03/09/10 19:54 71-43-20.0047
Bromobenzene ND mg/kg 1 03/09/10 19:54 108-86-10.0047
Bromochloromethane ND mg/kg 1 03/09/10 19:54 74-97-50.0047
Bromodichloromethane ND mg/kg 1 03/09/10 19:54 75-27-40.0047
Bromoform ND mg/kg 1 03/09/10 19:54 75-25-20.0047
Bromomethane ND mg/kg 1 03/09/10 19:54 74-83-90.0094
2-Butanone (MEK)ND mg/kg 1 03/09/10 19:54 78-93-30.094
n-Butylbenzene ND mg/kg 1 03/09/10 19:54 104-51-80.0047
sec-Butylbenzene ND mg/kg 1 03/09/10 19:54 135-98-80.0047
tert-Butylbenzene ND mg/kg 1 03/09/10 19:54 98-06-60.0047
Carbon tetrachloride ND mg/kg 1 03/09/10 19:54 56-23-50.0047
Chlorobenzene ND mg/kg 1 03/09/10 19:54 108-90-70.0047
Chloroethane ND mg/kg 1 03/09/10 19:54 75-00-30.0094
Chloroform ND mg/kg 1 03/09/10 19:54 67-66-30.0047
Chloromethane ND mg/kg 1 03/09/10 19:54 74-87-30.0094
2-Chlorotoluene ND mg/kg 1 03/09/10 19:54 95-49-80.0047
4-Chlorotoluene ND mg/kg 1 03/09/10 19:54 106-43-40.0047
1,2-Dibromo-3-chloropropane ND mg/kg 1 03/09/10 19:54 96-12-80.0047
Dibromochloromethane ND mg/kg 1 03/09/10 19:54 124-48-10.0047
1,2-Dibromoethane (EDB)ND mg/kg 1 03/09/10 19:54 106-93-40.0047
Dibromomethane ND mg/kg 1 03/09/10 19:54 74-95-30.0047
1,2-Dichlorobenzene ND mg/kg 1 03/09/10 19:54 95-50-10.0047
1,3-Dichlorobenzene ND mg/kg 1 03/09/10 19:54 541-73-10.0047
1,4-Dichlorobenzene ND mg/kg 1 03/09/10 19:54 106-46-70.0047
Dichlorodifluoromethane ND mg/kg 1 03/09/10 19:54 75-71-80.0094
1,1-Dichloroethane ND mg/kg 1 03/09/10 19:54 75-34-30.0047
1,2-Dichloroethane ND mg/kg 1 03/09/10 19:54 107-06-20.0047
1,1-Dichloroethene ND mg/kg 1 03/09/10 19:54 75-35-40.0047
cis-1,2-Dichloroethene ND mg/kg 1 03/09/10 19:54 156-59-20.0047
trans-1,2-Dichloroethene ND mg/kg 1 03/09/10 19:54 156-60-50.0047
1,2-Dichloropropane ND mg/kg 1 03/09/10 19:54 78-87-50.0047
1,3-Dichloropropane ND mg/kg 1 03/09/10 19:54 142-28-90.0047
2,2-Dichloropropane ND mg/kg 1 03/09/10 19:54 594-20-70.0047
1,1-Dichloropropene ND mg/kg 1 03/09/10 19:54 563-58-60.0047
cis-1,3-Dichloropropene ND mg/kg 1 03/09/10 19:54 10061-01-50.0047
trans-1,3-Dichloropropene ND mg/kg 1 03/09/10 19:54 10061-02-60.0047
Diisopropyl ether ND mg/kg 1 03/09/10 19:54 108-20-30.0047
Ethylbenzene 0.0046 mg/kg 1 03/09/10 19:54 100-41-40.0047
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 6 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:B3-34 Lab ID:9264720002 Collected:03/04/10 10:36 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Hexachloro-1,3-butadiene ND mg/kg 1 03/09/10 19:54 87-68-30.0047
2-Hexanone ND mg/kg 1 03/09/10 19:54 591-78-60.047
Isopropylbenzene (Cumene)ND mg/kg 1 03/09/10 19:54 98-82-80.0047
p-Isopropyltoluene ND mg/kg 1 03/09/10 19:54 99-87-60.0047
Methylene Chloride ND mg/kg 1 03/09/10 19:54 75-09-20.019
4-Methyl-2-pentanone (MIBK)ND mg/kg 1 03/09/10 19:54 108-10-10.047
Methyl-tert-butyl ether 0.16 mg/kg 1 03/09/10 19:54 1634-04-40.0047
Naphthalene ND mg/kg 1 03/09/10 19:54 91-20-30.0047
n-Propylbenzene ND mg/kg 1 03/09/10 19:54 103-65-10.0047
Styrene ND mg/kg 1 03/09/10 19:54 100-42-50.0047
1,1,1,2-Tetrachloroethane ND mg/kg 1 03/09/10 19:54 630-20-60.0047
1,1,2,2-Tetrachloroethane ND mg/kg 1 03/09/10 19:54 79-34-50.0047
Tetrachloroethene ND mg/kg 1 03/09/10 19:54 127-18-40.0047
Toluene 0.013 mg/kg 1 03/09/10 19:54 108-88-30.0047
1,2,3-Trichlorobenzene ND mg/kg 1 03/09/10 19:54 87-61-60.0047
1,2,4-Trichlorobenzene ND mg/kg 1 03/09/10 19:54 120-82-10.0047
1,1,1-Trichloroethane ND mg/kg 1 03/09/10 19:54 71-55-60.0047
1,1,2-Trichloroethane ND mg/kg 1 03/09/10 19:54 79-00-50.0047
Trichloroethene ND mg/kg 1 03/09/10 19:54 79-01-60.0047
Trichlorofluoromethane ND mg/kg 1 03/09/10 19:54 75-69-40.0047
1,2,3-Trichloropropane ND mg/kg 1 03/09/10 19:54 96-18-40.0047
1,2,4-Trimethylbenzene 0.0065 mg/kg 1 03/09/10 19:54 95-63-60.0047
1,3,5-Trimethylbenzene ND mg/kg 1 03/09/10 19:54 108-67-80.0047
Vinyl acetate ND mg/kg 1 03/09/10 19:54 108-05-40.047
Vinyl chloride ND mg/kg 1 03/09/10 19:54 75-01-40.0094
Xylene (Total)0.027 mg/kg 1 03/09/10 19:54 1330-20-70.0094
m&p-Xylene 0.018 mg/kg 1 03/09/10 19:54 1330-20-70.0094
o-Xylene 0.0089 mg/kg 1 03/09/10 19:54 95-47-60.0047
Dibromofluoromethane (S)103 %1 03/09/10 19:54 1868-53-779-116
Toluene-d8 (S)102 %1 03/09/10 19:54 2037-26-588-110
4-Bromofluorobenzene (S)97 %1 03/09/10 19:54 460-00-474-115
1,2-Dichloroethane-d4 (S)114 %1 03/09/10 19:54 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.0 %1 03/08/10 14:430.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 7 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:MW-3-4 Lab ID:9264720003 Collected:03/04/10 10:55 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-C08)450 mg/kg 1 03/15/10 21:3703/15/10 16:329.2
Aliphatic (C09-C12)1580 mg/kg 1 03/15/10 21:3703/15/10 16:329.2
Aromatic (C09-C10)327 mg/kg 1 03/15/10 21:3703/15/10 16:329.2
2,5-Dibromotoluene (PID)(S)119 %1 03/15/10 21:3703/15/10 16:3270-130
2,5-Dibromotoluene (FID)(S)151 %1 03/15/10 21:37 S503/15/10 16:3270-130
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone ND mg/kg 500 03/10/10 08:58 67-64-148.2
Benzene ND mg/kg 500 03/10/10 08:58 71-43-22.4
Bromobenzene ND mg/kg 500 03/10/10 08:58 108-86-12.4
Bromochloromethane ND mg/kg 500 03/10/10 08:58 74-97-52.4
Bromodichloromethane ND mg/kg 500 03/10/10 08:58 75-27-42.4
Bromoform ND mg/kg 500 03/10/10 08:58 75-25-22.4
Bromomethane ND mg/kg 500 03/10/10 08:58 74-83-94.8
2-Butanone (MEK)ND mg/kg 500 03/10/10 08:58 78-93-348.2
n-Butylbenzene 36.7 mg/kg 500 03/10/10 08:58 104-51-82.4
sec-Butylbenzene 11.2 mg/kg 500 03/10/10 08:58 135-98-82.4
tert-Butylbenzene ND mg/kg 500 03/10/10 08:58 98-06-62.4
Carbon tetrachloride ND mg/kg 500 03/10/10 08:58 56-23-52.4
Chlorobenzene ND mg/kg 500 03/10/10 08:58 108-90-72.4
Chloroethane ND mg/kg 500 03/10/10 08:58 75-00-34.8
Chloroform ND mg/kg 500 03/10/10 08:58 67-66-32.4
Chloromethane ND mg/kg 500 03/10/10 08:58 74-87-34.8
2-Chlorotoluene ND mg/kg 500 03/10/10 08:58 95-49-82.4
4-Chlorotoluene ND mg/kg 500 03/10/10 08:58 106-43-42.4
1,2-Dibromo-3-chloropropane ND mg/kg 500 03/10/10 08:58 96-12-82.4
Dibromochloromethane ND mg/kg 500 03/10/10 08:58 124-48-12.4
1,2-Dibromoethane (EDB)ND mg/kg 500 03/10/10 08:58 106-93-42.4
Dibromomethane ND mg/kg 500 03/10/10 08:58 74-95-32.4
1,2-Dichlorobenzene ND mg/kg 500 03/10/10 08:58 95-50-12.4
1,3-Dichlorobenzene ND mg/kg 500 03/10/10 08:58 541-73-12.4
1,4-Dichlorobenzene ND mg/kg 500 03/10/10 08:58 106-46-72.4
Dichlorodifluoromethane ND mg/kg 500 03/10/10 08:58 75-71-84.8
1,1-Dichloroethane ND mg/kg 500 03/10/10 08:58 75-34-32.4
1,2-Dichloroethane ND mg/kg 500 03/10/10 08:58 107-06-22.4
1,1-Dichloroethene ND mg/kg 500 03/10/10 08:58 75-35-42.4
cis-1,2-Dichloroethene ND mg/kg 500 03/10/10 08:58 156-59-22.4
trans-1,2-Dichloroethene ND mg/kg 500 03/10/10 08:58 156-60-52.4
1,2-Dichloropropane ND mg/kg 500 03/10/10 08:58 78-87-52.4
1,3-Dichloropropane ND mg/kg 500 03/10/10 08:58 142-28-92.4
2,2-Dichloropropane ND mg/kg 500 03/10/10 08:58 594-20-72.4
1,1-Dichloropropene ND mg/kg 500 03/10/10 08:58 563-58-62.4
cis-1,3-Dichloropropene ND mg/kg 500 03/10/10 08:58 10061-01-52.4
trans-1,3-Dichloropropene ND mg/kg 500 03/10/10 08:58 10061-02-62.4
Diisopropyl ether ND mg/kg 500 03/10/10 08:58 108-20-32.4
Ethylbenzene 215 mg/kg 5000 03/10/10 19:09 100-41-424.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 8 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:MW-3-4 Lab ID:9264720003 Collected:03/04/10 10:55 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Hexachloro-1,3-butadiene ND mg/kg 500 03/10/10 08:58 87-68-32.4
2-Hexanone ND mg/kg 500 03/10/10 08:58 591-78-624.1
Isopropylbenzene (Cumene)23.9 mg/kg 500 03/10/10 08:58 98-82-82.4
p-Isopropyltoluene 21.0 mg/kg 500 03/10/10 08:58 99-87-62.4
Methylene Chloride ND mg/kg 500 03/10/10 08:58 75-09-29.6
4-Methyl-2-pentanone (MIBK)ND mg/kg 500 03/10/10 08:58 108-10-124.1
Methyl-tert-butyl ether ND mg/kg 500 03/10/10 08:58 1634-04-42.4
Naphthalene 70.8 mg/kg 500 03/10/10 08:58 91-20-32.4
n-Propylbenzene 91.1 mg/kg 500 03/10/10 08:58 103-65-12.4
Styrene 3.3 mg/kg 500 03/10/10 08:58 100-42-52.4
1,1,1,2-Tetrachloroethane ND mg/kg 500 03/10/10 08:58 630-20-62.4
1,1,2,2-Tetrachloroethane ND mg/kg 500 03/10/10 08:58 79-34-52.4
Tetrachloroethene ND mg/kg 500 03/10/10 08:58 127-18-42.4
Toluene 201 mg/kg 5000 03/10/10 19:09 108-88-324.1
1,2,3-Trichlorobenzene ND mg/kg 500 03/10/10 08:58 87-61-62.4
1,2,4-Trichlorobenzene ND mg/kg 500 03/10/10 08:58 120-82-12.4
1,1,1-Trichloroethane ND mg/kg 500 03/10/10 08:58 71-55-62.4
1,1,2-Trichloroethane ND mg/kg 500 03/10/10 08:58 79-00-52.4
Trichloroethene ND mg/kg 500 03/10/10 08:58 79-01-62.4
Trichlorofluoromethane ND mg/kg 500 03/10/10 08:58 75-69-42.4
1,2,3-Trichloropropane ND mg/kg 500 03/10/10 08:58 96-18-42.4
1,2,4-Trimethylbenzene 656 mg/kg 5000 03/10/10 19:09 95-63-624.1
1,3,5-Trimethylbenzene 198 mg/kg 5000 03/10/10 19:09 108-67-824.1
Vinyl acetate ND mg/kg 500 03/10/10 08:58 108-05-424.1
Vinyl chloride ND mg/kg 500 03/10/10 08:58 75-01-44.8
Xylene (Total)1390 mg/kg 5000 03/10/10 19:09 1330-20-748.2
m&p-Xylene 982 mg/kg 5000 03/10/10 19:09 1330-20-748.2
o-Xylene 411 mg/kg 5000 03/10/10 19:09 95-47-624.1
Dibromofluoromethane (S)101 %500 03/10/10 08:58 1868-53-779-116
Toluene-d8 (S)97 %500 03/10/10 08:58 2037-26-588-110
4-Bromofluorobenzene (S)93 %500 03/10/10 08:58 460-00-474-115
1,2-Dichloroethane-d4 (S)121 %500 03/10/10 08:58 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.5 %1 03/08/10 14:430.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 9 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:MW-3-34 Lab ID:9264720004 Collected:03/04/10 11:16 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-C08)ND mg/kg 1 03/15/10 22:0203/15/10 16:328.4
Aliphatic (C09-C12)31.9 mg/kg 1 03/15/10 22:0203/15/10 16:328.4
Aromatic (C09-C10)ND mg/kg 1 03/15/10 22:0203/15/10 16:328.4
2,5-Dibromotoluene (PID)(S)91 %1 03/15/10 22:0203/15/10 16:3270-130
2,5-Dibromotoluene (FID)(S)107 %1 03/15/10 22:0203/15/10 16:3270-130
8260/5035A Volatile Organics Analytical Method: EPA 8260
Acetone 0.23 mg/kg 1 03/09/10 20:12 67-64-10.083
Benzene 0.14 mg/kg 1 03/09/10 20:12 71-43-20.0042
Bromobenzene ND mg/kg 1 03/09/10 20:12 108-86-10.0042
Bromochloromethane ND mg/kg 1 03/09/10 20:12 74-97-50.0042
Bromodichloromethane ND mg/kg 1 03/09/10 20:12 75-27-40.0042
Bromoform ND mg/kg 1 03/09/10 20:12 75-25-20.0042
Bromomethane ND mg/kg 1 03/09/10 20:12 74-83-90.0083
2-Butanone (MEK)0.098 mg/kg 1 03/09/10 20:12 78-93-30.083
n-Butylbenzene ND mg/kg 1 03/09/10 20:12 104-51-80.0042
sec-Butylbenzene ND mg/kg 1 03/09/10 20:12 135-98-80.0042
tert-Butylbenzene ND mg/kg 1 03/09/10 20:12 98-06-60.0042
Carbon tetrachloride ND mg/kg 1 03/09/10 20:12 56-23-50.0042
Chlorobenzene ND mg/kg 1 03/09/10 20:12 108-90-70.0042
Chloroethane ND mg/kg 1 03/09/10 20:12 75-00-30.0083
Chloroform ND mg/kg 1 03/09/10 20:12 67-66-30.0042
Chloromethane ND mg/kg 1 03/09/10 20:12 74-87-30.0083
2-Chlorotoluene ND mg/kg 1 03/09/10 20:12 95-49-80.0042
4-Chlorotoluene ND mg/kg 1 03/09/10 20:12 106-43-40.0042
1,2-Dibromo-3-chloropropane ND mg/kg 1 03/09/10 20:12 96-12-80.0042
Dibromochloromethane ND mg/kg 1 03/09/10 20:12 124-48-10.0042
1,2-Dibromoethane (EDB)0.0045 mg/kg 1 03/09/10 20:12 106-93-40.0042
Dibromomethane ND mg/kg 1 03/09/10 20:12 74-95-30.0042
1,2-Dichlorobenzene ND mg/kg 1 03/09/10 20:12 95-50-10.0042
1,3-Dichlorobenzene ND mg/kg 1 03/09/10 20:12 541-73-10.0042
1,4-Dichlorobenzene ND mg/kg 1 03/09/10 20:12 106-46-70.0042
Dichlorodifluoromethane ND mg/kg 1 03/09/10 20:12 75-71-80.0083
1,1-Dichloroethane ND mg/kg 1 03/09/10 20:12 75-34-30.0042
1,2-Dichloroethane ND mg/kg 1 03/09/10 20:12 107-06-20.0042
1,1-Dichloroethene ND mg/kg 1 03/09/10 20:12 75-35-40.0042
cis-1,2-Dichloroethene ND mg/kg 1 03/09/10 20:12 156-59-20.0042
trans-1,2-Dichloroethene ND mg/kg 1 03/09/10 20:12 156-60-50.0042
1,2-Dichloropropane ND mg/kg 1 03/09/10 20:12 78-87-50.0042
1,3-Dichloropropane ND mg/kg 1 03/09/10 20:12 142-28-90.0042
2,2-Dichloropropane ND mg/kg 1 03/09/10 20:12 594-20-70.0042
1,1-Dichloropropene ND mg/kg 1 03/09/10 20:12 563-58-60.0042
cis-1,3-Dichloropropene ND mg/kg 1 03/09/10 20:12 10061-01-50.0042
trans-1,3-Dichloropropene ND mg/kg 1 03/09/10 20:12 10061-02-60.0042
Diisopropyl ether 0.018 mg/kg 1 03/09/10 20:12 108-20-30.0042
Ethylbenzene 0.10 mg/kg 1 03/09/10 20:12 100-41-40.0042
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 10 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:MW-3-34 Lab ID:9264720004 Collected:03/04/10 11:16 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8260/5035A Volatile Organics Analytical Method: EPA 8260
Hexachloro-1,3-butadiene ND mg/kg 1 03/09/10 20:12 87-68-30.0042
2-Hexanone ND mg/kg 1 03/09/10 20:12 591-78-60.042
Isopropylbenzene (Cumene)0.0067 mg/kg 1 03/09/10 20:12 98-82-80.0042
p-Isopropyltoluene 0.0045 mg/kg 1 03/09/10 20:12 99-87-60.0042
Methylene Chloride ND mg/kg 1 03/09/10 20:12 75-09-20.017
4-Methyl-2-pentanone (MIBK)ND mg/kg 1 03/09/10 20:12 108-10-10.042
Methyl-tert-butyl ether ND mg/kg 1 03/09/10 20:12 1634-04-40.0042
Naphthalene 0.019 mg/kg 1 03/09/10 20:12 91-20-30.0042
n-Propylbenzene 0.011 mg/kg 1 03/09/10 20:12 103-65-10.0042
Styrene ND mg/kg 1 03/09/10 20:12 100-42-50.0042
1,1,1,2-Tetrachloroethane ND mg/kg 1 03/09/10 20:12 630-20-60.0042
1,1,2,2-Tetrachloroethane ND mg/kg 1 03/09/10 20:12 79-34-50.0042
Tetrachloroethene ND mg/kg 1 03/09/10 20:12 127-18-40.0042
Toluene 0.023 mg/kg 1 03/09/10 20:12 108-88-30.0042
1,2,3-Trichlorobenzene ND mg/kg 1 03/09/10 20:12 87-61-60.0042
1,2,4-Trichlorobenzene ND mg/kg 1 03/09/10 20:12 120-82-10.0042
1,1,1-Trichloroethane ND mg/kg 1 03/09/10 20:12 71-55-60.0042
1,1,2-Trichloroethane ND mg/kg 1 03/09/10 20:12 79-00-50.0042
Trichloroethene ND mg/kg 1 03/09/10 20:12 79-01-60.0042
Trichlorofluoromethane ND mg/kg 1 03/09/10 20:12 75-69-40.0042
1,2,3-Trichloropropane ND mg/kg 1 03/09/10 20:12 96-18-40.0042
1,2,4-Trimethylbenzene 0.10 mg/kg 1 03/09/10 20:12 95-63-60.0042
1,3,5-Trimethylbenzene 0.037 mg/kg 1 03/09/10 20:12 108-67-80.0042
Vinyl acetate ND mg/kg 1 03/09/10 20:12 108-05-40.042
Vinyl chloride ND mg/kg 1 03/09/10 20:12 75-01-40.0083
Xylene (Total)0.37 mg/kg 1 03/09/10 20:12 1330-20-70.0083
m&p-Xylene 0.29 mg/kg 1 03/09/10 20:12 1330-20-70.0083
o-Xylene 0.076 mg/kg 1 03/09/10 20:12 95-47-60.0042
Dibromofluoromethane (S)113 %1 03/09/10 20:12 1868-53-779-116
Toluene-d8 (S)102 %1 03/09/10 20:12 2037-26-588-110
4-Bromofluorobenzene (S)96 %1 03/09/10 20:12 460-00-474-115
1,2-Dichloroethane-d4 (S)113 %1 03/09/10 20:12 17060-07-069-121
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 7.8 %1 03/08/10 14:440.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 11 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:MW-3-24 Lab ID:9264720005 Collected:03/04/10 11:22 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-C08)ND mg/kg 1 03/15/10 22:2603/15/10 16:328.7
Aliphatic (C09-C12)ND mg/kg 1 03/15/10 22:2603/15/10 16:328.7
Aromatic (C09-C10)ND mg/kg 1 03/15/10 22:2603/15/10 16:328.7
2,5-Dibromotoluene (PID)(S)119 %1 03/15/10 22:2603/15/10 16:3270-130
2,5-Dibromotoluene (FID)(S)124 %1 03/15/10 22:2603/15/10 16:3270-130
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.9 %1 03/08/10 14:440.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 12 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:MW-3-14 Lab ID:9264720006 Collected:03/04/10 11:05 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-C08)285 mg/kg 1 03/15/10 22:5103/15/10 16:3210.3
Aliphatic (C09-C12)770 mg/kg 1 03/15/10 22:5103/15/10 16:3210.3
Aromatic (C09-C10)183 mg/kg 1 03/15/10 22:5103/15/10 16:3210.3
2,5-Dibromotoluene (PID)(S)91 %1 03/15/10 22:5103/15/10 16:3270-130
2,5-Dibromotoluene (FID)(S)119 %1 03/15/10 22:5103/15/10 16:3270-130
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.3 %1 03/08/10 14:440.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 13 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Sample:MW-3-34 Lab ID:9264720007 Collected:03/04/10 11:09 Received:03/05/10 14:52 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-C08)11.6 mg/kg 1 03/15/10 23:1603/15/10 16:3210.6
Aliphatic (C09-C12)48.1 mg/kg 1 03/15/10 23:1603/15/10 16:3210.6
Aromatic (C09-C10)12.2 mg/kg 1 03/15/10 23:1603/15/10 16:3210.6
2,5-Dibromotoluene (PID)(S)102 %1 03/15/10 23:1603/15/10 16:3270-130
2,5-Dibromotoluene (FID)(S)119 %1 03/15/10 23:1603/15/10 16:3270-130
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.9 %1 03/08/10 14:440.10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 14 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/3901
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:9264720001, 9264720002, 9264720003, 9264720004, 9264720005, 9264720006, 9264720007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:415272
Associated Lab Samples:9264720001, 9264720002, 9264720003, 9264720004, 9264720005, 9264720006, 9264720007
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 10.0 03/15/10 16:17
Aliphatic (C09-C12)mg/kg ND 10.0 03/15/10 16:17
Aromatic (C09-C10)mg/kg ND 10.0 03/15/10 16:17
2,5-Dibromotoluene (FID)(S)%126 70-130 03/15/10 16:17
2,5-Dibromotoluene (PID)(S)%122 70-130 03/15/10 16:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
415273LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
415274
Aliphatic (C05-C08)mg/kg 15.515 103 70-13010015.0 3 25
Aliphatic (C09-C12)mg/kg 17.815 118 30-13011617.4 2 25
Aromatic (C09-C10)mg/kg ND5 103 70-130102ND 25
2,5-Dibromotoluene (FID)(S)%115 70-130113
2,5-Dibromotoluene (PID)(S)%103 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 15 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/10205
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9264720001, 9264720002, 9264720004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:411981
Associated Lab Samples:9264720001, 9264720002, 9264720004
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 03/09/10 10:18
1,1,1-Trichloroethane mg/kg ND 0.0050 03/09/10 10:18
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 03/09/10 10:18
1,1,2-Trichloroethane mg/kg ND 0.0050 03/09/10 10:18
1,1-Dichloroethane mg/kg ND 0.0050 03/09/10 10:18
1,1-Dichloroethene mg/kg ND 0.0050 03/09/10 10:18
1,1-Dichloropropene mg/kg ND 0.0050 03/09/10 10:18
1,2,3-Trichlorobenzene mg/kg ND 0.0050 03/09/10 10:18
1,2,3-Trichloropropane mg/kg ND 0.0050 03/09/10 10:18
1,2,4-Trichlorobenzene mg/kg ND 0.0050 03/09/10 10:18
1,2,4-Trimethylbenzene mg/kg ND 0.0050 03/09/10 10:18
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 03/09/10 10:18
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 03/09/10 10:18
1,2-Dichlorobenzene mg/kg ND 0.0050 03/09/10 10:18
1,2-Dichloroethane mg/kg ND 0.0050 03/09/10 10:18
1,2-Dichloropropane mg/kg ND 0.0050 03/09/10 10:18
1,3,5-Trimethylbenzene mg/kg ND 0.0050 03/09/10 10:18
1,3-Dichlorobenzene mg/kg ND 0.0050 03/09/10 10:18
1,3-Dichloropropane mg/kg ND 0.0050 03/09/10 10:18
1,4-Dichlorobenzene mg/kg ND 0.0050 03/09/10 10:18
2,2-Dichloropropane mg/kg ND 0.0050 03/09/10 10:18
2-Butanone (MEK)mg/kg ND 0.10 03/09/10 10:18
2-Chlorotoluene mg/kg ND 0.0050 03/09/10 10:18
2-Hexanone mg/kg ND 0.050 03/09/10 10:18
4-Chlorotoluene mg/kg ND 0.0050 03/09/10 10:18
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 03/09/10 10:18
Acetone mg/kg ND 0.10 03/09/10 10:18
Benzene mg/kg ND 0.0050 03/09/10 10:18
Bromobenzene mg/kg ND 0.0050 03/09/10 10:18
Bromochloromethane mg/kg ND 0.0050 03/09/10 10:18
Bromodichloromethane mg/kg ND 0.0050 03/09/10 10:18
Bromoform mg/kg ND 0.0050 03/09/10 10:18
Bromomethane mg/kg ND 0.010 03/09/10 10:18
Carbon tetrachloride mg/kg ND 0.0050 03/09/10 10:18
Chlorobenzene mg/kg ND 0.0050 03/09/10 10:18
Chloroethane mg/kg ND 0.010 03/09/10 10:18
Chloroform mg/kg ND 0.0050 03/09/10 10:18
Chloromethane mg/kg ND 0.010 03/09/10 10:18
cis-1,2-Dichloroethene mg/kg ND 0.0050 03/09/10 10:18
cis-1,3-Dichloropropene mg/kg ND 0.0050 03/09/10 10:18
Dibromochloromethane mg/kg ND 0.0050 03/09/10 10:18
Dibromomethane mg/kg ND 0.0050 03/09/10 10:18
Dichlorodifluoromethane mg/kg ND 0.010 03/09/10 10:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 16 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:411981
Associated Lab Samples:9264720001, 9264720002, 9264720004
Matrix:Solid
Analyzed
Diisopropyl ether mg/kg ND 0.0050 03/09/10 10:18
Ethylbenzene mg/kg ND 0.0050 03/09/10 10:18
Hexachloro-1,3-butadiene mg/kg ND 0.0050 03/09/10 10:18
Isopropylbenzene (Cumene)mg/kg ND 0.0050 03/09/10 10:18
m&p-Xylene mg/kg ND 0.010 03/09/10 10:18
Methyl-tert-butyl ether mg/kg ND 0.0050 03/09/10 10:18
Methylene Chloride mg/kg ND 0.020 03/09/10 10:18
n-Butylbenzene mg/kg ND 0.0050 03/09/10 10:18
n-Propylbenzene mg/kg ND 0.0050 03/09/10 10:18
Naphthalene mg/kg ND 0.0050 03/09/10 10:18
o-Xylene mg/kg ND 0.0050 03/09/10 10:18
p-Isopropyltoluene mg/kg ND 0.0050 03/09/10 10:18
sec-Butylbenzene mg/kg ND 0.0050 03/09/10 10:18
Styrene mg/kg ND 0.0050 03/09/10 10:18
tert-Butylbenzene mg/kg ND 0.0050 03/09/10 10:18
Tetrachloroethene mg/kg ND 0.0050 03/09/10 10:18
Toluene mg/kg ND 0.0050 03/09/10 10:18
trans-1,2-Dichloroethene mg/kg ND 0.0050 03/09/10 10:18
trans-1,3-Dichloropropene mg/kg ND 0.0050 03/09/10 10:18
Trichloroethene mg/kg ND 0.0050 03/09/10 10:18
Trichlorofluoromethane mg/kg ND 0.0050 03/09/10 10:18
Vinyl acetate mg/kg ND 0.050 03/09/10 10:18
Vinyl chloride mg/kg ND 0.010 03/09/10 10:18
Xylene (Total)mg/kg ND 0.010 03/09/10 10:18
1,2-Dichloroethane-d4 (S)%114 69-121 03/09/10 10:18
4-Bromofluorobenzene (S)%95 74-115 03/09/10 10:18
Dibromofluoromethane (S)%101 79-116 03/09/10 10:18
Toluene-d8 (S)%102 88-110 03/09/10 10:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
411982LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.049.05 98 75-137
1,1,1-Trichloroethane mg/kg 0.053.05 107 70-140
1,1,2,2-Tetrachloroethane mg/kg 0.047.05 94 74-133
1,1,2-Trichloroethane mg/kg 0.052.05 103 79-129
1,1-Dichloroethane mg/kg 0.052.05 105 72-139
1,1-Dichloroethene mg/kg 0.051.05 101 69-154
1,1-Dichloropropene mg/kg 0.051.05 101 74-138
1,2,3-Trichlorobenzene mg/kg 0.053.05 106 71-150
1,2,3-Trichloropropane mg/kg 0.049.05 99 74-135
1,2,4-Trichlorobenzene mg/kg 0.053.05 107 68-150
1,2,4-Trimethylbenzene mg/kg 0.053.05 107 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.049.05 98 65-146
1,2-Dibromoethane (EDB)mg/kg 0.049.05 98 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 17 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
411982LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene mg/kg 0.052.05 103 75-141
1,2-Dichloroethane mg/kg 0.054.05 108 74-134
1,2-Dichloropropane mg/kg 0.050.05 101 77-138
1,3,5-Trimethylbenzene mg/kg 0.053.05 105 65-128
1,3-Dichlorobenzene mg/kg 0.052.05 103 76-133
1,3-Dichloropropane mg/kg 0.050.05 99 79-132
1,4-Dichlorobenzene mg/kg 0.050.05 101 75-137
2,2-Dichloropropane mg/kg 0.053.05 107 73-137
2-Butanone (MEK)mg/kg 0.11.1 106 61-138
2-Chlorotoluene mg/kg 0.051.05 102 73-138
2-Hexanone mg/kg 0.10.1 104 58-159
4-Chlorotoluene mg/kg 0.054.05 108 75-136
4-Methyl-2-pentanone (MIBK)mg/kg 0.11.1 106 74-139
Acetone mg/kg 0.12.1 117 58-150
Benzene mg/kg 0.050.05 101 71-140
Bromobenzene mg/kg 0.052.05 105 72-144
Bromochloromethane mg/kg 0.050.05 100 78-133
Bromodichloromethane mg/kg 0.050.05 99 78-133
Bromoform mg/kg 0.049.05 98 74-132
Bromomethane mg/kg 0.036.05 72 63-184
Carbon tetrachloride mg/kg 0.063.05 127 73-143
Chlorobenzene mg/kg 0.051.05 102 77-137
Chloroethane mg/kg 0.050.05 99 68-146
Chloroform mg/kg 0.050.05 101 75-137
Chloromethane mg/kg 0.045.05 90 54-143
cis-1,2-Dichloroethene mg/kg 0.052.05 103 71-143
cis-1,3-Dichloropropene mg/kg 0.050.05 101 76-133
Dibromochloromethane mg/kg 0.049.05 98 77-131
Dibromomethane mg/kg 0.052.05 103 63-184
Dichlorodifluoromethane mg/kg 0.035.05 70 36-173
Diisopropyl ether mg/kg 0.052.05 105 68-144
Ethylbenzene mg/kg 0.051.05 102 69-141
Hexachloro-1,3-butadiene mg/kg 0.049.05 99 70-152
Isopropylbenzene (Cumene)mg/kg 0.053.05 105 77-143
m&p-Xylene mg/kg 0.10.1 103 72-138
Methyl-tert-butyl ether mg/kg 0.055.05 111 2-138
Methylene Chloride mg/kg 0.046.05 93 69-136
n-Butylbenzene mg/kg 0.054.05 108 65-128
n-Propylbenzene mg/kg 0.054.05 108 72-139
Naphthalene mg/kg 0.052.05 103 61-138
o-Xylene mg/kg 0.053.05 105 74-137
p-Isopropyltoluene mg/kg 0.052.05 105 66-128
sec-Butylbenzene mg/kg 0.053.05 105 72-140
Styrene mg/kg 0.050.05 101 76-137
tert-Butylbenzene mg/kg 0.053.05 106 68-141
Tetrachloroethene mg/kg 0.051.05 101 72-136
Toluene mg/kg 0.051.05 102 69-139
trans-1,2-Dichloroethene mg/kg 0.050.05 101 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 18 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
411982LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene mg/kg 0.052.05 104 73-135
Trichloroethene mg/kg 0.052.05 105 75-136
Trichlorofluoromethane mg/kg 0.047.05 95 69-144
Vinyl acetate mg/kg 0.12.1 115 50-150
Vinyl chloride mg/kg 0.042.05 83 61-145
Xylene (Total)mg/kg 0.16.15 104 73-138
1,2-Dichloroethane-d4 (S)%101 69-121
4-Bromofluorobenzene (S)%98 74-115
Dibromofluoromethane (S)%100 79-116
Toluene-d8 (S)%101 88-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
412855MATRIX SPIKE SAMPLE:
MSSpike
Result
9264731008
1,1-Dichloroethene mg/kg 0.062.053 118 33-158ND
Benzene mg/kg 0.056.053 107 46-143ND
Chlorobenzene mg/kg 0.053.053 100 29-159ND
Toluene mg/kg 0.057.053 109 38-145ND
Trichloroethene mg/kg 0.057.053 108 70-130ND
1,2-Dichloroethane-d4 (S)%S012269-121
4-Bromofluorobenzene (S)%95 74-115
Dibromofluoromethane (S)%110 79-116
Toluene-d8 (S)%102 88-110
Parameter Units
Dup
Result QualifiersRPDResult
9264748003
412854SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 19 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
Dup
Result QualifiersRPDResult
9264748003
412854SAMPLE DUPLICATE:
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 20 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
Dup
Result QualifiersRPDResult
9264748003
412854SAMPLE DUPLICATE:
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%128 S228114
4-Bromofluorobenzene (S)%92 1197
Dibromofluoromethane (S)%106 8115
Toluene-d8 (S)%102 16103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 21 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/10233
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:9264720003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:412474
Associated Lab Samples:9264720003
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 03/09/10 22:57
1,1,1-Trichloroethane mg/kg ND 0.0050 03/09/10 22:57
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 03/09/10 22:57
1,1,2-Trichloroethane mg/kg ND 0.0050 03/09/10 22:57
1,1-Dichloroethane mg/kg ND 0.0050 03/09/10 22:57
1,1-Dichloroethene mg/kg ND 0.0050 03/09/10 22:57
1,1-Dichloropropene mg/kg ND 0.0050 03/09/10 22:57
1,2,3-Trichlorobenzene mg/kg ND 0.0050 03/09/10 22:57
1,2,3-Trichloropropane mg/kg ND 0.0050 03/09/10 22:57
1,2,4-Trichlorobenzene mg/kg ND 0.0050 03/09/10 22:57
1,2,4-Trimethylbenzene mg/kg ND 0.0050 03/09/10 22:57
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 03/09/10 22:57
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 03/09/10 22:57
1,2-Dichlorobenzene mg/kg ND 0.0050 03/09/10 22:57
1,2-Dichloroethane mg/kg ND 0.0050 03/09/10 22:57
1,2-Dichloropropane mg/kg ND 0.0050 03/09/10 22:57
1,3,5-Trimethylbenzene mg/kg ND 0.0050 03/09/10 22:57
1,3-Dichlorobenzene mg/kg ND 0.0050 03/09/10 22:57
1,3-Dichloropropane mg/kg ND 0.0050 03/09/10 22:57
1,4-Dichlorobenzene mg/kg ND 0.0050 03/09/10 22:57
2,2-Dichloropropane mg/kg ND 0.0050 03/09/10 22:57
2-Butanone (MEK)mg/kg ND 0.10 03/09/10 22:57
2-Chlorotoluene mg/kg ND 0.0050 03/09/10 22:57
2-Hexanone mg/kg ND 0.050 03/09/10 22:57
4-Chlorotoluene mg/kg ND 0.0050 03/09/10 22:57
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 03/09/10 22:57
Acetone mg/kg ND 0.10 03/09/10 22:57
Benzene mg/kg ND 0.0050 03/09/10 22:57
Bromobenzene mg/kg ND 0.0050 03/09/10 22:57
Bromochloromethane mg/kg ND 0.0050 03/09/10 22:57
Bromodichloromethane mg/kg ND 0.0050 03/09/10 22:57
Bromoform mg/kg ND 0.0050 03/09/10 22:57
Bromomethane mg/kg ND 0.010 03/09/10 22:57
Carbon tetrachloride mg/kg ND 0.0050 03/09/10 22:57
Chlorobenzene mg/kg ND 0.0050 03/09/10 22:57
Chloroethane mg/kg ND 0.010 03/09/10 22:57
Chloroform mg/kg ND 0.0050 03/09/10 22:57
Chloromethane mg/kg ND 0.010 03/09/10 22:57
cis-1,2-Dichloroethene mg/kg ND 0.0050 03/09/10 22:57
cis-1,3-Dichloropropene mg/kg ND 0.0050 03/09/10 22:57
Dibromochloromethane mg/kg ND 0.0050 03/09/10 22:57
Dibromomethane mg/kg ND 0.0050 03/09/10 22:57
Dichlorodifluoromethane mg/kg ND 0.010 03/09/10 22:57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 22 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:412474
Associated Lab Samples:9264720003
Matrix:Solid
Analyzed
Diisopropyl ether mg/kg ND 0.0050 03/09/10 22:57
Ethylbenzene mg/kg ND 0.0050 03/09/10 22:57
Hexachloro-1,3-butadiene mg/kg ND 0.0050 03/09/10 22:57
Isopropylbenzene (Cumene)mg/kg ND 0.0050 03/09/10 22:57
m&p-Xylene mg/kg ND 0.010 03/09/10 22:57
Methyl-tert-butyl ether mg/kg ND 0.0050 03/09/10 22:57
Methylene Chloride mg/kg ND 0.020 03/09/10 22:57
n-Butylbenzene mg/kg ND 0.0050 03/09/10 22:57
n-Propylbenzene mg/kg ND 0.0050 03/09/10 22:57
Naphthalene mg/kg ND 0.0050 03/09/10 22:57
o-Xylene mg/kg ND 0.0050 03/09/10 22:57
p-Isopropyltoluene mg/kg ND 0.0050 03/09/10 22:57
sec-Butylbenzene mg/kg ND 0.0050 03/09/10 22:57
Styrene mg/kg ND 0.0050 03/09/10 22:57
tert-Butylbenzene mg/kg ND 0.0050 03/09/10 22:57
Tetrachloroethene mg/kg ND 0.0050 03/09/10 22:57
Toluene mg/kg ND 0.0050 03/09/10 22:57
trans-1,2-Dichloroethene mg/kg ND 0.0050 03/09/10 22:57
trans-1,3-Dichloropropene mg/kg ND 0.0050 03/09/10 22:57
Trichloroethene mg/kg ND 0.0050 03/09/10 22:57
Trichlorofluoromethane mg/kg ND 0.0050 03/09/10 22:57
Vinyl acetate mg/kg ND 0.050 03/09/10 22:57
Vinyl chloride mg/kg ND 0.010 03/09/10 22:57
Xylene (Total)mg/kg ND 0.010 03/09/10 22:57
1,2-Dichloroethane-d4 (S)%106 69-121 03/09/10 22:57
4-Bromofluorobenzene (S)%97 74-115 03/09/10 22:57
Dibromofluoromethane (S)%109 79-116 03/09/10 22:57
Toluene-d8 (S)%103 88-110 03/09/10 22:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
412475LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.054.05 107 75-137
1,1,1-Trichloroethane mg/kg 0.059.05 119 70-140
1,1,2,2-Tetrachloroethane mg/kg 0.050.05 100 74-133
1,1,2-Trichloroethane mg/kg 0.056.05 113 79-129
1,1-Dichloroethane mg/kg 0.057.05 115 72-139
1,1-Dichloroethene mg/kg 0.055.05 111 69-154
1,1-Dichloropropene mg/kg 0.053.05 107 74-138
1,2,3-Trichlorobenzene mg/kg 0.049.05 97 71-150
1,2,3-Trichloropropane mg/kg 0.054.05 107 74-135
1,2,4-Trichlorobenzene mg/kg 0.046.05 92 68-150
1,2,4-Trimethylbenzene mg/kg 0.053.05 107 70-130
1,2-Dibromo-3-chloropropane mg/kg 0.053.05 105 65-146
1,2-Dibromoethane (EDB)mg/kg 0.052.05 104 77-136
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 23 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
412475LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene mg/kg 0.052.05 103 75-141
1,2-Dichloroethane mg/kg 0.060.05 121 74-134
1,2-Dichloropropane mg/kg 0.056.05 113 77-138
1,3,5-Trimethylbenzene mg/kg 0.053.05 106 65-128
1,3-Dichlorobenzene mg/kg 0.050.05 100 76-133
1,3-Dichloropropane mg/kg 0.054.05 108 79-132
1,4-Dichlorobenzene mg/kg 0.049.05 97 75-137
2,2-Dichloropropane mg/kg 0.054.05 108 73-137
2-Butanone (MEK)mg/kg 0.11.1 114 61-138
2-Chlorotoluene mg/kg 0.052.05 103 73-138
2-Hexanone mg/kg 0.11.1 113 58-159
4-Chlorotoluene mg/kg 0.053.05 106 75-136
4-Methyl-2-pentanone (MIBK)mg/kg 0.12.1 117 74-139
Acetone mg/kg 0.13.1 135 58-150
Benzene mg/kg 0.054.05 109 71-140
Bromobenzene mg/kg 0.055.05 109 72-144
Bromochloromethane mg/kg 0.069 L3.05 137 78-133
Bromodichloromethane mg/kg 0.054.05 108 78-133
Bromoform mg/kg 0.051.05 102 74-132
Bromomethane mg/kg 0.055.05 110 63-184
Carbon tetrachloride mg/kg 0.062.05 124 73-143
Chlorobenzene mg/kg 0.053.05 107 77-137
Chloroethane mg/kg 0.055.05 110 68-146
Chloroform mg/kg 0.058.05 116 75-137
Chloromethane mg/kg 0.052.05 104 54-143
cis-1,2-Dichloroethene mg/kg 0.057.05 113 71-143
cis-1,3-Dichloropropene mg/kg 0.054.05 108 76-133
Dibromochloromethane mg/kg 0.052.05 105 77-131
Dibromomethane mg/kg 0.056.05 113 63-184
Dichlorodifluoromethane mg/kg 0.048.05 95 36-173
Diisopropyl ether mg/kg 0.057.05 115 68-144
Ethylbenzene mg/kg 0.053.05 105 69-141
Hexachloro-1,3-butadiene mg/kg 0.049.05 98 70-152
Isopropylbenzene (Cumene)mg/kg 0.054.05 107 77-143
m&p-Xylene mg/kg 0.11.1 106 72-138
Methyl-tert-butyl ether mg/kg 0.063.05 127 2-138
Methylene Chloride mg/kg 0.050.05 101 69-136
n-Butylbenzene mg/kg 0.050.05 101 65-128
n-Propylbenzene mg/kg 0.054.05 107 72-139
Naphthalene mg/kg 0.052.05 105 61-138
o-Xylene mg/kg 0.054.05 109 74-137
p-Isopropyltoluene mg/kg 0.051.05 103 66-128
sec-Butylbenzene mg/kg 0.052.05 105 72-140
Styrene mg/kg 0.052.05 104 76-137
tert-Butylbenzene mg/kg 0.055.05 111 68-141
Tetrachloroethene mg/kg 0.051.05 101 72-136
Toluene mg/kg 0.054.05 109 69-139
trans-1,2-Dichloroethene mg/kg 0.054.05 108 72-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 24 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
412475LABORATORY CONTROL SAMPLE:
LCSSpike
trans-1,3-Dichloropropene mg/kg 0.055.05 110 73-135
Trichloroethene mg/kg 0.055.05 109 75-136
Trichlorofluoromethane mg/kg 0.052.05 104 69-144
Vinyl acetate mg/kg .036J L0.1 36 50-150
Vinyl chloride mg/kg 0.048.05 97 61-145
Xylene (Total)mg/kg 0.16.15 107 73-138
1,2-Dichloroethane-d4 (S)%110 69-121
4-Bromofluorobenzene (S)%98 74-115
Dibromofluoromethane (S)%102 79-116
Toluene-d8 (S)%101 88-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
412903MATRIX SPIKE SAMPLE:
MSSpike
Result
9264750001
1,1-Dichloroethene mg/kg 0.069.052 132 33-158ND
Benzene mg/kg 0.063.052 120 46-143ND
Chlorobenzene mg/kg 0.059.052 113 29-159ND
Toluene mg/kg 0.062.052 120 38-145ND
Trichloroethene mg/kg 0.064.052 124 70-130ND
1,2-Dichloroethane-d4 (S)%113 69-121
4-Bromofluorobenzene (S)%91 74-115
Dibromofluoromethane (S)%102 79-116
Toluene-d8 (S)%101 88-110
Parameter Units
Dup
Result QualifiersRPDResult
9264745003
412904SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 25 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
Dup
Result QualifiersRPDResult
9264745003
412904SAMPLE DUPLICATE:
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 26 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Parameter Units
Dup
Result QualifiersRPDResult
9264745003
412904SAMPLE DUPLICATE:
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%117 0116
4-Bromofluorobenzene (S)%95 195
Dibromofluoromethane (S)%104 12117
Toluene-d8 (S)%102 0101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 27 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/3059
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:9264720001, 9264720002, 9264720003, 9264720004, 9264720005, 9264720006, 9264720007
Parameter Units
Dup
Result QualifiersRPDResult
9264672001
411971SAMPLE DUPLICATE:
Percent Moisture %17.1 2121.2
Parameter Units
Dup
Result QualifiersRPDResult
9264750001
411972SAMPLE DUPLICATE:
Percent Moisture %17.3 1319.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 28 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
U - Indicates the compound was analyzed for, but not detected.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 29 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9264720
BOWEK'S TRUCKING 1354-09-25-8
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9264720001 GCV/3901 GCV/3902B3-14 MADEP VPH MADEP VPH
9264720002 GCV/3901 GCV/3902B3-34 MADEP VPH MADEP VPH
9264720003 GCV/3901 GCV/3902MW-3-4 MADEP VPH MADEP VPH
9264720004 GCV/3901 GCV/3902MW-3-34 MADEP VPH MADEP VPH
9264720005 GCV/3901 GCV/3902MW-3-24 MADEP VPH MADEP VPH
9264720006 GCV/3901 GCV/3902MW-3-14 MADEP VPH MADEP VPH
9264720007 GCV/3901 GCV/3902MW-3-34 MADEP VPH MADEP VPH
9264720001 MSV/10205B3-14 EPA 8260
9264720002 MSV/10205B3-34 EPA 8260
9264720003 MSV/10233MW-3-4 EPA 8260
9264720004 MSV/10205MW-3-34 EPA 8260
9264720001 PMST/3059B3-14 ASTM D2974-87
9264720002 PMST/3059B3-34 ASTM D2974-87
9264720003 PMST/3059MW-3-4 ASTM D2974-87
9264720004 PMST/3059MW-3-34 ASTM D2974-87
9264720005 PMST/3059MW-3-24 ASTM D2974-87
9264720006 PMST/3059MW-3-14 ASTM D2974-87
9264720007 PMST/3059MW-3-34 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 03/17/2010 12:31 PM Page 30 of 30
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]