WS-1024_30199_CA_LSA_20200707

S&ME, Inc. | 8646 W Market St, Ste 105 | Greensboro, NC 27409 | p 336.288.7180 | www.smeinc.com

July 7, 2020
NCDEQ, DWM, UST Section, Trust Fund Branch
1646 Mail Service Center
Raleigh, NC 27699-1646

Attention: Mr. Herbert Berger Submitted via: [e-mail]
Reference: Letter Report of Limited Groundwater Assessment
Moore’s Exxon/Incident #30199
5891 NC Highway 65, Reidsville, Rockingham County, North Carolina
S&ME Project No. 4305-18-201A
Dear Mr. Berger:
S&ME, Inc., (S&ME) presents this report in accordance with the North Carolina Department of Environmental
Quality/S&ME Contract No. N17002 and S&ME Proposal No. 43-18000711A, dated June 1, 2020, and as
authorized by Task Authorization No. 02, dated June 1, 2020.
The scope of services included the collection of groundwater samples from monitor wells MW-3 and MW-5
(Figure 1), from water supply wells WSW-2 and WSW-4 (Figure 1), for analyses by Method 6200B and 504.1, and a
field blank sample analyzed by Method 6200B; and measure depth to water in monitor wells MW-1, MW-2, and
MW-4; and summarize findings in a Letter Report. The scope of services was completed as proposed.
 Water Supply Well Sampling and Results
Two water supply wells, (WSW-2 and WSW-4), were sampled. The approximate locations of the sampled water
supply wells are shown in Figure 1, Attachment I.
On June 11, 2020, S&ME personnel sampled active potable water supply well WSW-2 and WSW-4. The
groundwater samples and one field blank sample were placed in laboratory-supplied containers, placed in a
cooler on ice, and shipped under standard chain-of-custody procedure to ConTest Analytical for analysis of
volatile organic compounds (VOCs) by EPA Methods 6200B and 504.1. The Water Supply Well Sampling Forms
are provided in Attachment III.
The laboratory analytical results of the groundwater samples collected from WSW-2 and WSW-4, and for the field
blank sample, were each less than the laboratory method reporting limits. A summary of the current and historical
water supply well analytical results are presented in Table 1, Attachment II. A copy of the laboratory analytical
report and chain of custody form is provided in Attachment IV.
On June 22, 2020, upon receipt of the laboratory analytical report for WSW-2 and WSW-4, S&ME informed Mr.
Herbert Berger of the NCDEQ of the water supply well samples via email.
Attachment I – Figure
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MOORE'SCAFE
MOORE'SEXXON
Heating Oil AST
.USTs (Active)
..USTs (Closed-in-place)
N C H IGH W AY 65MW-3 µg/L ACETONE 140N-BUTYLBENZENE 25SEC-BUTYLBENZENE 4.9TERT-BUTYLBENZENE 3.81,2-DIBROMOETHANE 3.5DIISOPROPYL ETHER 6.4ETHYLBENZENE 1802-HEXANONE 35ISOPROPYLBENZENE 9.5P-ISOPROPYLTOLUENE 4.1METHYL ETHYL KETONE 97N-PROPYLBENZENE 13NAPHTHALENE 26TOLUENE 381,2,4-TRIMETHYLBENZENE 551,3,5-TRIMETHYLBENZENE 290TOTAL XYLENES 330
MW-5 µg/L ACETONE 72 JN-BUTYLBENZENE 40TERT-BUTYLBENZENE 7.31,2-DIBROMOETHANE 5.61,2-DICHLOROETHANE 8.0DIISOPROPYL ETHER 120ETHYLBENZENE 5.7ISOPROPYLBENZENE 6.0P-ISOPROPYLTOLUENE 5.3METHYL TERT-BUTYL ETHER 3.3METHYL ETHYL KETONE 19NAPHTHALENE 141,3,5-TRIMETHYLBENZENE 230TOTAL XYLENES 47
WSW-2 BDL
WSW-4 BDL
TW-1
MW-4
MW-3
MW-1
MW-2
MW-6
MW-5
WSW-1
WSW-2
WSW-4
WSW-3
WSW-6
WSW-5
NCCGIA
Groundwater Samples Collected on 6/11/2020Methods 6200B and 504.1Bold Text Indicates > 2L StandardBDL: Below Detection Limitsμg/L: Micrograms per LiterJ: Concentration is an Estimate
!(@A Vertical Extent Monitoring Well
Ð!G Water Supply Well Location
@A Monitoring Well Location
Subject ParcelRockingham Co Parcels
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 75 '
6-24-20Drawing Path: C:\Users\mverbanic\Desktop\Remote GIS\4305-18-201A Moore's Exxon\CONSTITUENT.mxd plotted by mverbanic 06-24-20200 75 150(FEET)
GROUNDWATER CONSTITUENT MAP
³
4305-18-201A
MOORE'S EXXON INCIDENT NO. 301995891 NC HIGHWAY 65REIDSVILLE, ROCKINGHAM COUNTY, NORTH CAROLINA
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2014 NCONEMAP AERIAL ORTHOIMAGERYLAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION,UNLESS STATED OTHERWISE.
Attachment II – Tables
UST Facility ID #: 00-0-0000018409
Well ID Date
BenzeneChloroformChloromethane1,2-Dibromoethane (EDB) by 6200B or 504.11,4-Dichlorobenzene1,2-DichloroethaneDiisopropyl etherToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (total)Lead1 70 3 0.02 6 0.4 70 600 400 400 500 15
5/6/2003 5.1 NA NA <0.50 NA 1.1 12.2 5.9 NA NA 12.4 <0.50
6/2/2003 4.0 NA NA <0.50 NA NA 5.0 4.6 NA NA 11.3 <0.50
7/16/2003 3.9 NA NA NA NA 1.1 8.3 4.3 NA NA 8.8 <0.50
12/3/2004 <1.0 NA NA 0.034 NA <1.0 1.6 <1.0 NA NA 2.0 43
6/2/2003 <0.50 NA NA NA NA NA <0.50 <0.50 NA NA <0.50 <0.50
12/3/2004 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
3/20/2006 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
12/4/2008 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
2/12/2010 <0.5 <0.5 <0.5 <0.5 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
5/26/2011 <0.5 <0.5 <0.5 <0.5 ND <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
4/12/2014 <0.5 <0.5 <0.5 <0.020 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
9/28/2015 <0.50 ------<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 NA
11/19/2018 <0.50 <0.50 <0.50 <0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 NA
6/11/2020 <0.50 <1.0 <2.0 <0.020 <0.50 <0.50 <0.50 <0.50 <1.0 <1.0 <1.5 NA
7/1/2003 <0.50 NA NA NA NA NA <0.50 <0.50 NA NA <0.50 <0.50
3/20/2006 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
12/14/2006 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
2/14/2008 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
2/12/2010 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
7/1/2003 <0.50 NA NA NA NA NA <0.50 <0.50 NA NA <0.50 <0.50
3/20/2006 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
12/14/2006 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
2/14/2008 <1.0 NA NA <0.020 NA <1.0 NA <1.0 NA NA <3.0 <5.0
2/12/2010 <0.5 <0.5 1.1 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
5/26/2011 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
4/12/2014 <0.5 0.51 <0.5 <0.020 0.36J <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
9/28/2015 <0.50 ------<0.020 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 NA
11/17/2018 <0.50 <0.50 <0.50 <0.021 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 NA
6/11/2020 <0.50 <1.0 <2.0 <0.020 <0.50 <0.50 <0.50 <0.50 <1.0 <1.0 <1.5 NA
10/8/2003 <1 NA NA <0.25 NA 1.8 NA <0.50 NA NA <3 NA
12/3/2004 <1.0 <0.25 NA <0.25 NA 1.8 NA <1.0 NA NA <3.0 NA
3/20/2006 NA NA NA NA NA NA NA NA NA NA NA NA
12/14/2006 NA NA NA NA NA NA NA NA NA NA NA NA
2/14/2008 <1.0 <1.0 NA 0.014 NA <1.0 <5.0 <1.0 <1.0 <1.0 <3.0 NA
8/13/2009 <0.5 <0.5 NA 0.12 NA 1.9 9.0 <0.5 0.63 0.51 3.9 <5.0
5/26/2011 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
4/12/2014 <0.5 <0.5 <0.5 <0.020 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
2/12/2010 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
5/26/2011 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
4/12/2014 <0.5 <0.5 <0.5 <0.020 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
2/12/2010 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
5/26/2011 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
WSW-8 2/12/2010 <0.5 <0.5 <0.5 <0.5 NA 1.4 <0.5 <0.5 <0.5 <0.5 <0.5 NA
WSW-10 2/12/2010 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
2/12/2010 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
5/26/2011 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
2/12/2010 <0.5 <0.5 1.3 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA
5/26/2011 <0.5 <0.5 <0.5 <0.5 NA <0.5 <0.5 <0.5 <0.5 <0.5 <1.5 NA
5,000 70,000 3,000 50 6,000 400 70,000 260,000 2,000,000 25,000 85,500 15,000
2L Standard 1 70 3 0.02 6 0.4 70 600 400 400 500 15
Notes:Results reported in micrograms per liter (µg/L)
NA = Not Analyzed Value
--- : Not detected above laboratory reporting limits.
J = Estimated Concentration
2L Standard = 15A NCAC 2L .0202 Groundwater Quality Standard
Concentration exceeds the 2L Standard
WSW-11
WSW-12
Gross Contamination Levels
WSW-6
Revision Date: 6/24/2020
WSW-1
WSW-2
WSW-4
WSW-3
WSW-7
Table 1
SUMMARY OF WATER SUPPLY WELL SAMPLING RESULTS
Moore's Exxon (Incident No.: 30199 WS-1024)
5891 NC Highway 65, Reidsville, Rockingham County, North Carolina
S&ME Project No. 4305-18-201
WSW-5
2L Standard
UST Facility ID #: 00-0-0000018409 Revision Date: 6/24/2020
Well
ID
Date
Installed
Date
Water Level
Measured
Well
Casing
Diameter
(in)
Depth
of Well
(ft-BGS)
Top of
Casing
Elevation*
(ft)
Depth to
Water
from Top
of Casing
(ft)
LNAPL
Thickness
** (ft)
Groundwater
Elevation*
(ft)
Latitude
(decimal)
Longitude
(decimal)
12/03/04 38.78 ND 61.2203/15/06 38.66 ND 61.3412/14/06 39.02 ND 60.9802/14/08 40.33 ND 59.6708/13/09 40.46 ND 59.5402/12/10 40.68 ND 59.3204/12/14 39.80 ND 60.2011/19/18 39.18 ND 60.8212/03/04 35.55 ND 62.0203/15/06 35.55 ND 62.0212/14/06 35.92 ND 61.6502/14/08 37.28 ND 60.2908/13/09 37.41 ND 60.1602/12/10 37.59 ND 59.9804/12/14 Dry ND NM11/19/18 36.15 ND 61.4212/03/04 37.32 ND 61.7503/15/06 37.23 ND NM12/14/06 37.59 ND 61.4802/14/08 38.96 ND 60.1108/13/09 39.08 ND 59.9902/12/10 39.22 ND 59.8504/12/14 45.65 ND 53.4211/19/18 36.80 ND 62.2706/11/20 35.43 ND 63.6412/03/04 41.94 ND 60.5803/15/06 41.82 ND 60.7012/14/06 42.21 ND 60.3102/14/08 43.38 ND 59.1408/13/09 43.55 ND 58.9702/12/10 43.75 ND 58.7704/12/14 43.49 ND 59.0311/19/18 42.31 ND 60.2103/15/06 39.68 ND 61.4212/14/06 40.04 ND 61.0602/14/08 41.03 ND 60.0708/13/09 Dry ND NM02/12/10 Dry ND NM04/12/14 Dry ND NM11/19/18 40.21 ND 60.8906/11/20 37.81 ND 63.2903/15/06 33.17 ND 62.2712/14/06 33.51 ND 61.9302/14/08 35.05 ND 60.3908/13/09 35.09 ND 60.3502/12/10 35.16 ND 60.2812/03/04 38.64 ND 61.6103/15/06 38.09 ND 62.1612/14/06 38.13 ND 62.1202/14/08 39.54 ND 60.7108/13/09 40.43 ND 59.8202/12/10 40.19 ND 60.0611/19/18 39.13 ND 61.12
NOTES:
* : Reference Point for Elevation Measurements:
Benchmark Datum:Benchmark Elevation: 100.00 ft
Assumed or Measured:
** : If LNAPL is present in a well, groundwater elevation should be calculated by: [Top of Casing Elevation - Depth to Water] + [LNAPL thickness x 0.739]
ft-BGS = feet below ground surface NM = Not Measured NA = Not Applicable
ND = Not Detected NG = Not Gauged LNAPL = Light non-aqueous phase liquid
WELL CONSTRUCTION AND LIQUID LEVEL DATA
5891 NC Highway 64, Reidsville, Rockingham County, North Carolina
S&ME Project # 4305-18-201
TABLE 2
NM
Moore's Exxon (Incident No.: 30199 WS-1024)
Screen
Interval
(ft-BGS)
MW-1 08/28/03 2.0 30.0 - 45.0 45.0 100.00 NM
2.012/01/04MW-3 99.0745.045.0-30.0
Top of casing of MW-1
Measured
97.5740.040.0-
50.0
41.0
45.0
58.0
102.52
101.10
95.44
100.25
25.0
2.0
2.0
2.0
MW-2 2.011/30/04
MW-4
MW-5
MW-6
TW-1
11/30/04
03/15/06
03/15/06
12/01/04
2.0 35.0 - 50.0
26.0 - 41.0
30.0 - 45.0
56.0 - 58.0
NM NM
NM NM
NM NM
NM NM
NM NM
NM NM
Page 2 of 2
UST Facility ID #: 00-0-0000028247 Revision Date: 6/24/20
Well ID Date
AcetoneBenzenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChloroform1,2-Dibromoethane (EDB) by 6200B or 504.11,2-DichloroethaneDiisopropyl etherEthylbenzene2-Hexanone (MBK)Isopropylbenzenep-IsopropyltolueneMethyl tert-butyl ether4-Methyl-2-pentanone (MIBK) Methyl ethyl ketone (MEK)n-PropylbenzeneNaphthaleneToluene1,1,2-Trichloroethane1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneXylenes (total)Lead6,000 1 70 70 70 70 0.02 0.4 70 600 40 70 25 20 100 4,000 70 6 600 0.6 400 400 500 15
6,000,000 5,000 6,900 8,500 15,000 70,000 50 400 70,000 84,500 40,000 25,000 11,700 20,000 100,000 4,000,000 30,000 6,000 260,000 600 28,500 25,000 85,500 15,000
8/28/2003 ---<1.0 NA NA NA <1.0 0.16 <1.0 3.2 <1.0 ---NA ---<1.0 ---<5.0 NA NA 1.8 ---NA NA 8.1 7.5
12/3/2004 ---<1.0 NA NA NA <1.0 0.26 1.50 6.5 1.0 ---NA ---<1.0 ---<5.0 NA <2.0 1.8 ---NA NA 4.0 270
3/20/2006 ---<1.0 NA NA NA <1.0 0.25 <1.0 2.0 <1.0 ---NA ---<1.0 ---<5.0 NA <2.0 <1.0 ---NA NA 4.4 NA
12/14/2006 ---<1.0 NA NA NA <1.0 0.20 <1.0 <1.0 <1.0 ---NA ---<1.0 ---<5.0 NA <2.0 <1.0 ---NA NA 5.0 NA
2/14/2008 ---<1.0 NA NA NA <1.0 0.02 <1.0 <0.5 <1.0 ---NA ---<1.0 ---<5.0 NA <1.0 <1.0 ---<1.0 <1.0 <3.0 NA
8/13/2009 ---<0.5 <0.5 <0.5 <0.5 <0.5 0.11 <0.5 <0.5 <0.5 ---<0.5 ---<0.5 ---<5.0 <0.5 <2.0 <0.5 ---<0.5 1.4 1.5 <5.0
2/12/2010 <5 <0.5 <1.0 <0.5 <0.5 <0.5 0.053 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ---<5.0 <0.5 <2 <0.5 ---<0.5 <0.5 <1.5 NA
4/17/2014 <50 <0.50 <2.0 <0.50 <0.5 <0.50 <0.020 <0.50 <0.50 <0.50 <10 <0.50 <0.5 <0.50 <5 <5 <0.5 <5.0 <0.50 <0.50 <0.50 0.94 1.16 J NA
11/19/2018 <50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.020 <0.50 <0.50 <0.50 <5.0 <0.50 <0.50 <0.50 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 0.27 J <0.50 <1.5 NA
12/3/2004 NA <1.0 NA NA NA NA <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA NA NA <2.0 <1.0 NA NA NA <3.0 41
3/20/2006 NA <1.0 NA NA NA NA <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA NA NA <2.0 <1.0 NA NA NA <3.0 NA
12/14/2006 NA <1.0 NA NA NA NA <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA NA NA <2.0 <1.0 NA NA NA <3.0 NA
2/14/2008 NA <1.0 NA NA NA NA <0.020 <1.0 <5.0 <1.0 NA NA NA <1.0 NA NA NA <1.0 <1.0 NA NA NA <3.0 NA
2/12/2010 <5 <0.5 <1.0 <0.5 ---<0.5 <0.5 <0.5 <0.5 <0.5 ---<0.5 ---<0.5 ---<5.0 <0.5 <2 <0.5 ---<0.5 <0.5 <0.5 NA
11/19/2018 <50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.020 <0.50 <0.50 <0.50 <5.0 <0.50 <0.50 <0.50 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 NA
12/3/2004 ---<25 NA NA NA <25 14 <25 47 440 NA NA NA <25 NA <5.0 NA 96 830 NA NA NA 2,400 460
3/20/2006 ---95 NA NA NA <25 19 <25 290 390 NA NA NA <25 NA <5.0 NA 160 780 NA NA NA 2,000 NA
12/14/2006 ---<25 NA NA NA <25 21 <25 130 160 NA NA NA <25 NA <5.0 NA 71 480 NA NA NA 1,500 NA
2/14/2008 ---<10 NA NA NA <10 9.19 <10 66.7 14 NA NA NA <10 NA <5.0 NA 10.4 52.8 NA 87.6 131 619 NA
8/13/2009 ---<0.5 <0.5 <0.5 ---<0.5 1.1 2.1 26.2 7.1 ND 1.1 ---<0.5 ---<5.0 1.8 4.2 19.7 ---12.6 45.1 88.5 <5.0
2/12/2010 21 <1.0 1.5 J 1.2 ---<1.0 10 1.5 7.9 83 ND 5.1 ND <1.0 ---9.3 J 16 4.5 230 E ---110 72 670 E NA
4/12/2014 130 0.13 J 4.9 1.5 0.82 <0.5 6.1 0.92 7.1 73 21 6.0 0.65 0.19 J 10 55 16 9.5 140 0.26 J 77 75 490 NA
11/19/2018 110 <0.50 4.0 2.5 1.4 <0.50 4.8 <0.50 7.3 51 19 6.7 1.2 0.32 J 14 48 18 18 38 <0.50 110 140 370 NA
6/11/2020 140 <1.0 25 4.9 3.8 <2.0 3.5 <1.0 6.4 180 35 9.5 4.1 <1.0 <10 97 13 26 38 <1.0 55 290 330 NA
12/3/2004 ---<1.0 NA NA NA <1.0 0.025 <1.0 <1.0 <1.0 NA NA NA <1.0 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 320
3/20/2006 ---<1.0 NA NA NA <1.0 <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 NA
12/14/2006 ---<1.0 NA NA NA <1.0 <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 NA
2/14/2008 ---<1.0 NA NA NA <1.0 <0.010 <1.0 <5.0 <1.0 NA NA NA <1.0 NA <5.0 NA <1.0 <1.0 NA <1.0 <1.0 <3.0 NA
8/13/2009 ---<0.5 <0.5 <0.5 ---<0.5 <0.019 <0.5 <0.5 <0.5 ND <0.5 ---<0.5 ---<5.0 <0.5 <2.0 <0.5 ---<0.5 <0.5 <1.5 <5.0
2/12/2010 <5 <0.5 <1.0 <0.5 ---<0.5 <0.5 <0.5 <0.5 <0.5 ---<0.5 ---<0.5 ---<5.0 <0.5 <2 <0.5 ---<0.5 <0.5 <1.5 NA
4/12/2014 <50 <0.50 <2.0 <0.50 <0.50 <0.50 <0.020 <0.5 <0.5 <0.5 <10 <0.5 <0.50 <0.5 <5 <5.0 <0.5 <5.0 <0.50 <0.50 <0.5 <0.5 <1.5 NA
3/20/2006 NA <20 NA NA NA NA 34 57 540 140 NA NA NA <20 NA NA NA 140 32 NA NA NA 760 NA
12/14/2006 NA <20 NA NA NA NA 12 32 350 100 NA NA NA <20 NA NA NA <40 38 NA NA NA 650 NA
6/11/2020 72 J <20 40 <1.0 7.3 <2.0 5.6 8.0 120 5.7 <10 6.0 5.3 3.3 <10 19 <1.0 14 <1.0 <1.0 <2.0 230 47 NA
MW-6 3/20/2006 ---<1.0 NA NA NA <1.0 <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 NA
12/14/2006 ---<1.0 NA NA NA <1.0 <0.020 <1.0 1.1 <1.0 NA NA NA <1.0 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 NA
2/14/2008 ---<1.0 NA NA NA <1.0 <0.010 <1.0 <5.0 <1.0 NA NA NA <1.0 NA <5.0 NA <1.0 <1.0 NA <1.0 <1.0 <3.0 NA
2/12/2010 <5 <0.5 <1.0 <0.5 ---<0.5 <0.5 <0.5 <0.5 <0.5 ---<0.5 ---<0.5 ---<5.0 <0.5 <2 <0.5 ---<0.5 <0.5 <1.5 NA
12/3/2004 ---<1.0 NA NA NA 35 <0.020 <1.0 <1.0 <1.0 NA NA NA 1.8 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 53
3/20/2006 ---<1.0 NA NA NA 35 <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 NA
12/14/2006 ---<1.0 NA NA NA 4 <0.020 <1.0 <1.0 <1.0 NA NA NA <1.0 NA <5.0 NA <2.0 <1.0 NA NA NA <3.0 NA
2/14/2008 ---<1.0 NA NA NA 2.54 <0.010 <1.0 <5.0 <1.0 NA NA NA <1.0 NA <5.0 NA <1.0 <1.0 NA <1.0 <1.0 <3.0 NA
8/13/2009 ---<0.5 <0.5 <0.5 ---1.0 <0.020 <0.5 <0.5 <0.5 ---<0.5 ---<0.5 ---<5.0 <0.5 <2.0 <0.5 ---<0.5 <0.5 <1.0 <5.0
2/12/2010 <5 <0.5 <1.0 <0.5 <0.5 0.7 <0.5 <0.5 <0.5 <0.5 <10 <0.5 <0.5 <0.5 <5 <5.0 <0.5 <2 <0.5 <0.5 <0.5 <0.5 <0.5 NA
11/19/2018 <50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.023 <0.50 <0.50 <0.50 <5.0 <0.50 <0.50 <0.50 <5.0 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5 NA
Notes:Results reported in micrograms per liter (µg/L)GCL = Gross Contamination Level
NA = Not Analyzed 2L Standard = 15A NCAC 2L .0202 Groundwater Quality Standard Value Concentration exceeds the 2L Standard
--- : Not detected above laboratory reporting limits.J = Estimated Concentration Value Concentration exceeds the Gross Contamination Level
Table 3
SUMMARY OF GROUNDWATER SAMPLING RESULTS
Moore's Exxon (Incident No.: 30199 WS-1024)
5891 NC Highway 65, Reidsville, Rockingham County, North Carolina
TW-1
S&ME Project No. 4305-18-201
2L Standard
GCL
MW-1
MW-3
MW-4
MW-2
MW-5
Attachment III – Field Sampling Forms and Field Report
° F
Date Time
6/11/20 12:00 4.0 10.0
6/11/20 12:00 µS/cm
35.43 ft-TOC inch
45.00 ft-TOC gal
9.57 feet gal
15 ft-GRD gal
0 ft-GRD
14:00 End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
14:10 5.6 23.2 136
14:15
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Project Number:4305-18-201A Purge Date: June 11, 2020
Source Well:MW-3 Purge Time (Min.):10
GROUNDWATER SAMPLING FORM
Project Name:Moore's Exxon
Project Location:5891 NC Highway 65, Reidsville, NC
Weather:Overcast Air Temp:84
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date: June 11, 2020
Sampled By:Colby Paine Sample Time:14:15
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 1.6
Height of Water Column:3 * Well Volume 4.7
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:4.7 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 7.8
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:14:10
(Gal)
4.7 Petroleum Odors
Sample Method:Bailer Sample Time:
EDB 504.1
Analytical Data
Method Method Container
6200B
Colby Paine 6/25/2020
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
6/11/20 12:00 4.0 10.0
6/11/20 12:00 µS/cm
37.81 ft-TOC inch
41.00 ft-TOC gal
3.19 feet gal
ft-GRD gal
ft-GRD
13:35 End Time:
gal
Time pH Temp Cond Turbidity
(s.u.)(°C) µS/cm (NTU)
13:40 5.1 22.4 131
13:45
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
3 40mL VOAs NaS2O3
(1)
Notes:
Form Revision Date:
Colby Paine 6/25/2020
9/13/17 8:00 AM
Name Signature Date
EDB 504.1
Analytical Data
Method Method Container
6200B
Sample Method:Bailer Sample Time:
(Gal)
1.6 Petroleum Odors
Total Volume Purged:1.6 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 2.6
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:13:40
Total Well Depth:Well Volume 0.5
Height of Water Column:3 * Well Volume 1.6
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:84
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date: June 11, 2020
Sampled By:Colby Paine Sample Time:13:45
Project Number:4305-18-201A Purge Date: June 11, 2020
Source Well:MW-5 Purge Time (Min.):5
GROUNDWATER SAMPLING FORM
Project Name:Moore’s Exxon
Project Location:5891 NC Highway 65, Reidsville, NC
4.00 7.00 10.00
Units Units
°C μS/cm
Qty Pres.Qty Pres.
3 HCl
3 NaS2O3
Date
(1)
(2)
Revision:
Colby Paine
Well Address:
58.9
Air Temp (°F):
Equipment Calibration Information:
Equipment Time Calibration Solution Calibration Check
pH 6/11/20 12:00
POE Present (Y/N):
Total Volume (Gal)Time pH (s.u.)Temperature
9/1/17 13:30
Well / System Photographs
Date
Site Sketch
Additional Comments (description of location of sample port, water well, filters, etc.)
Sample Date Sample Time
6/11/2020 15:05
1,413
Well Purging Information
Field Parameters and Sampling
Conductivity
15:05 6.7 21.2
SignatureName
6/25/2020
Purge Rate (GPM): 4.0 Purge Start Time:14:50
Volume Purged (Gal):60.0 Purge End Time:15:05
Sample ID
WSW-2
Sample Location
Spigot on Front of House
4.00, 7.00, 10.00
60.00
Method
6200B
EDB 504.1
Method Container
Conductivity 6/11/20 12:00 1413
Container
40mL VOAs
40mL VOAs
WATER SUPPLY WELL SAMPLING FORM
Owner Name:
Owner Phone No.:
Thursday, June 11, 2020
WSW-2
5891 NC-65
Thomas R. Moore
Moore's Exxon
5891 NC-65, Reidsville, NC
4305-18-201A
NCDEQ/Herbert Berger
Sunny
85
No
Client Name/Contact:
Project Name:
Project Location:
Project Number:Sample Date:
Weather:
Water Supply Well ID:
4.00 7.00 10.00
Units Units
°C μS/cm
Qty Pres.Qty Pres.
3 HCl
3 NaS2O3
Date
(1)
(2)
Revision:
Project Number:4305-18-201A Sample Date:Thursday, June 11, 2020
Client Name/Contact:NCDEQ/Herbert Berger Water Supply Well ID:WSW-4
WATER SUPPLY WELL SAMPLING FORM
Project Name:Moore's Exxon
Project Location:5981 NC Highway 65, Reidsville, NC
POE Present (Y/N): No Owner Phone No.:
Equipment Calibration Information:
Weather:Sunny Well Address: 5912 NC Hwy 65
Air Temp (°F):85 Owner Name:Iris J. Sharpe
Well Purging Information
Purge Rate (GPM): 4.0 Purge Start Time:15:30
pH 6/11/20 12:00 4.00, 7.00, 10.00
Conductivity 6/11/20 12:00
Equipment Date Time Calibration Solution Calibration Check
Volume Purged (Gal):60.0 Purge End Time:15:45
Field Parameters and Sampling
Total Volume (Gal)Time pH (s.u.)Temperature Conductivity
60.00 15:45 6.5 20.9 132
Sample ID Sample Location Sample Date Sample Time
6200B 40mL VOAs
EDB 504.1 40mL VOAs
WSW-4 Spigot on Side of House 6/11/2020 15:45
Method Container Method Container
Additional Comments (description of location of sample port, water well, filters, etc.)Well / System Photographs
Site Sketch
9/1/17 13:30
Name Signature
Colby Paine 6/25/2020
Hours Mileage Signature of S&ME Personnel
4.75 40
S&ME, Inc. | www.smeinc.com
Environmental Field Report
Date:
June 11, 2020
Job Number:
4305-18-201A
Project Name:
Moore’s Exxon
Weather/Temperature:
Overcast, 84°F
Project Location
5891 NC Hwy 65, Reidsville, North Carolina
Notes By:
☒
Present at the Site:
Colby Paine
☐
On site to purge and sample two monitor wells and up to two water supply wells.
I opened all wells when I arrived on site at 1245. I let all wells equilibrate for approximately 15 minutes
before taking depth to water measurements.
Depth to water: MW-1 36.87 ft btoc, MW-2 33.81 ft btoc, MW-3 35.43 ft btoc, MW-4 40.07 ft btoc, and
MW-5 37.81 ft btoc.
Set out to start purging and sampling MW-3 and MW-5.
Purge and sample both wells with no issues. Strong petroleum odor in MW-3.
Field blank sample collected at 1420.
Water supply well samples collected afterwards.
Attachments:
Groundwater Sampling Sheet, Water Supply Well Sampling Forms
Equipment Used
Water Level Meter
pH/conductivity meter
Disposable Bailers
Attachment IV- Analytical Report and Chain of Custody Form
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
June 22, 2020
Lyndal Butler
S&ME, Inc - Greensboro, NC
8646 West Market St Suite 105
Greensboro, NC 27409
Project Location: Reidsville, NC
Client Job Number:
Project Number: 4305-18-201A
Laboratory Work Order Number: 20F0590
Enclosed are results of analyses for samples received by the laboratory on June 11, 2020. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 37
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 6
Sample Results 7
20F0590-01 7
20F0590-02 10
20F0590-03 13
20F0590-04 16
20F0590-05 19
Sample Preparation Information 21
QC Data 22
Volatile Organic Compounds by GC/MS 22
B259986 22
Drinking Water Organics EPA 504.1 26
B260377 26
Dual Column RPD Report 27
Flag/Qualifier Summary 32
Certifications 33
Chain of Custody/Sample Receipt 35
Page 2 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
6/22/2020
S&ME, Inc - Greensboro, NC
8646 West Market St Suite 105
Greensboro, NC 27409
ATTN: Lyndal Butler
4305-18-201A
20F0590
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Reidsville, NC
MW-3 20F0590-01 Ground Water EPA 504.1
SM21-22 6200B
MW-5 20F0590-02 Ground Water EPA 504.1
SM21-22 6200B
WSW-2 20F0590-03 Ground Water EPA 504.1
SM21-22 6200B
WSW-4 20F0590-04 Ground Water EPA 504.1
SM21-22 6200B
Field Blank 20F0590-05 Field Blank SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:20F0590-03WSW-2
No Results Detected
Client ID:Lab ID:20F0590-04WSW-4
No Results Detected
Client ID:Lab ID:20F0590-05Field Blank
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
20F0590-01MW-3
DL
1,2,4-Trimethylbenzene 55 2.0 g/L SM21-22 6200B0.36
1,2-Dibromoethane (EDB)3.5 1.0 g/L SM21-22 6200B0.38
1,3,5-Trimethylbenzene 290 2.0 g/L SM21-22 6200B0.28
2-Butanone (MEK)97 10 g/L SM21-22 6200B3.9
2-Hexanone (MBK)35 10 g/L SM21-22 6200B3.0
Acetone 140 100 g/L SM21-22 6200B7.6
Diisopropyl Ether (DIPE)6.4 1.0 g/L SM21-22 6200B0.34
Ethylbenzene 180 1.0 g/L SM21-22 6200B0.26
Isopropylbenzene (Cumene)9.5 4.0 g/L SM21-22 6200B0.34
m+p Xylene 120 2.0 g/L SM21-22 6200B0.60
Naphthalene 26 10 g/L SM21-22 6200B0.62
n-Butylbenzene 25 1.0 g/L SM21-22 6200B0.42
n-Propylbenzene 13 1.0 g/L SM21-22 6200B0.26
o-Xylene 210 1.0 g/L SM21-22 6200B0.34
p-Isopropyltoluene (p-Cymene)4.1 4.0 g/L SM21-22 6200B0.40
sec-Butylbenzene 4.9 1.0 g/L SM21-22 6200B0.32
tert-Butylbenzene 3.8 1.0 g/L SM21-22 6200B0.34
Toluene 38 1.0 g/L SM21-22 6200B0.28
1,2-Dibromoethane (EDB) [2C]4.7 0.80 g/L EPA 504.10.48
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
20F0590-02MW-5
DL
1,2-Dibromoethane (EDB)5.6 1.0 g/L SM21-22 6200B0.38
1,2-Dichloroethane 8.0 1.0 g/L SM21-22 6200B0.82
1,3,5-Trimethylbenzene 230 2.0 g/L SM21-22 6200B0.28
2-Butanone (MEK)19 10 g/L SM21-22 6200B3.9
Acetone 72 100 g/L SM21-22 6200BJ7.6
Diisopropyl Ether (DIPE)120 1.0 g/L SM21-22 6200B0.34
Ethylbenzene 5.7 1.0 g/L SM21-22 6200B0.26
Isopropylbenzene (Cumene)6.0 4.0 g/L SM21-22 6200B0.34
Methyl tert-Butyl Ether (MTBE)3.3 1.0 g/L SM21-22 6200B0.50
Naphthalene 14 10 g/L SM21-22 6200B0.62
n-Butylbenzene 40 1.0 g/L SM21-22 6200B0.42
o-Xylene 47 1.0 g/L SM21-22 6200B0.34
p-Isopropyltoluene (p-Cymene)5.3 4.0 g/L SM21-22 6200B0.40
tert-Butylbenzene 7.3 1.0 g/L SM21-22 6200B0.34
1,2-Dibromoethane (EDB) [2C]5.3 0.83 g/L EPA 504.10.50
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 5 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limts for samples 20F0590-01,02 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
sec-Butylbenzene
B259986-BS1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
20F0590-01[MW-3], 20F0590-02[MW-5]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 6 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-01
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 6/11/2020 14:15
[TOC_2]20F0590-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
140 100 6/15/20 13:19 MFFg/L7.6 6/15/20SM21-22 6200B2Acetone
ND 1.0 6/15/20 13:19 MFFg/L0.36 6/15/20SM21-22 6200B2Benzene
ND 1.0 6/15/20 13:19 MFFg/L0.30 6/15/20SM21-22 6200B2Bromobenzene
ND 1.0 6/15/20 13:19 MFFg/L0.64 6/15/20SM21-22 6200B2Bromochloromethane
ND 1.0 6/15/20 13:19 MFFg/L0.32 6/15/20SM21-22 6200B2Bromodichloromethane
ND 1.0 6/15/20 13:19 MFFg/L0.92 6/15/20SM21-22 6200B2Bromoform
ND 4.0 6/15/20 13:19 MFFg/L2.8 6/15/20SM21-22 6200B2Bromomethane
97 10 6/15/20 13:19 MFFg/L3.9 6/15/20SM21-22 6200B22-Butanone (MEK)
25 1.0 6/15/20 13:19 MFFg/L0.42 6/15/20SM21-22 6200B2n-Butylbenzene
4.9 1.0 6/15/20 13:19 MFFg/L0.32 6/15/20SM21-22 6200B2sec-Butylbenzene
3.8 1.0 6/15/20 13:19 MFFg/L0.34 6/15/20SM21-22 6200B2tert-Butylbenzene
ND 1.0 6/15/20 13:19 MFFg/L0.22 6/15/20SM21-22 6200B2Carbon Tetrachloride
ND 1.0 6/15/20 13:19 MFFg/L0.30 6/15/20SM21-22 6200B2Chlorobenzene
ND 100 6/15/20 13:19 MFFg/L21 6/15/20SM21-22 6200B2Ethanol
ND 1.0 6/15/20 13:19 MFFg/L0.42 6/15/20SM21-22 6200B2Chlorodibromomethane
ND 1.0 6/15/20 13:19 MFFg/L0.72 6/15/20SM21-22 6200B2Chloroethane
ND 2.0 6/15/20 13:19 MFFg/L0.34 6/15/20SM21-22 6200B2Chloroform
ND 4.0 6/15/20 13:19 MFFg/L0.90 6/15/20SM21-22 6200B2Chloromethane
ND 1.0 6/15/20 13:19 MFFg/L0.24 6/15/20SM21-22 6200B22-Chlorotoluene
ND 1.0 6/15/20 13:19 MFFg/L0.28 6/15/20SM21-22 6200B24-Chlorotoluene
3.5 1.0 6/15/20 13:19 MFFg/L0.38 6/15/20SM21-22 6200B21,2-Dibromoethane (EDB)
ND 1.0 6/15/20 13:19 MFFg/L0.32 6/15/20SM21-22 6200B21,2-Dichlorobenzene
ND 1.0 6/15/20 13:19 MFFg/L0.24 6/15/20SM21-22 6200B21,3-Dichlorobenzene
ND 1.0 6/15/20 13:19 MFFg/L0.26 6/15/20SM21-22 6200B21,4-Dichlorobenzene
ND 1.0 6/15/20 13:19 MFFg/L0.52 6/15/20SM21-22 6200B2Dichlorodifluoromethane (Freon 12)
ND 1.0 6/15/20 13:19 MFFg/L0.32 6/15/20SM21-22 6200B21,1-Dichloroethane
ND 1.0 6/15/20 13:19 MFFg/L0.82 6/15/20SM21-22 6200B21,2-Dichloroethane
ND 1.0 6/15/20 13:19 MFFg/L0.64 6/15/20SM21-22 6200B21,1-Dichloroethylene
ND 1.0 6/15/20 13:19 MFFg/L0.26 6/15/20SM21-22 6200B2cis-1,2-Dichloroethylene
ND 1.0 6/15/20 13:19 MFFg/L0.62 6/15/20SM21-22 6200B2trans-1,2-Dichloroethylene
ND 1.0 6/15/20 13:19 MFFg/L0.40 6/15/20SM21-22 6200B21,2-Dichloropropane
ND 1.0 6/15/20 13:19 MFFg/L0.22 6/15/20SM21-22 6200B21,3-Dichloropropane
ND 1.0 6/15/20 13:19 MFFg/L0.40 6/15/20SM21-22 6200B22,2-Dichloropropane
ND 1.0 6/15/20 13:19 MFFg/L0.32 6/15/20SM21-22 6200B21,1-Dichloropropene
ND 1.0 6/15/20 13:19 MFFg/L0.26 6/15/20SM21-22 6200B2cis-1,3-Dichloropropene
ND 1.0 6/15/20 13:19 MFFg/L0.46 6/15/20SM21-22 6200B2trans-1,3-Dichloropropene
6.4 1.0 6/15/20 13:19 MFFg/L0.34 6/15/20SM21-22 6200B2Diisopropyl Ether (DIPE)
180 1.0 6/15/20 13:19 MFFg/L0.26 6/15/20SM21-22 6200B2Ethylbenzene
35 10 6/15/20 13:19 MFFg/L3.0 6/15/20SM21-22 6200B22-Hexanone (MBK)
9.5 4.0 6/15/20 13:19 MFFg/L0.34 6/15/20SM21-22 6200B2Isopropylbenzene (Cumene)
4.1 4.0 6/15/20 13:19 MFFg/L0.40 6/15/20SM21-22 6200B2p-Isopropyltoluene (p-Cymene)
ND 1.0 6/15/20 13:19 MFFg/L0.50 6/15/20SM21-22 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 6/15/20 13:19 MFFg/L0.68 6/15/20SM21-22 6200B2Methylene Chloride
ND 10 6/15/20 13:19 MFFg/L3.3 6/15/20SM21-22 6200B24-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 7 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-01
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 6/11/2020 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
26 10 6/15/20 13:19 MFFg/L0.62 6/15/20SM21-22 6200B2Naphthalene
13 1.0 6/15/20 13:19 MFFg/L0.26 6/15/20SM21-22 6200B2n-Propylbenzene
ND 4.0 6/15/20 13:19 MFFg/L0.22 6/15/20SM21-22 6200B2Styrene
ND 1.0 6/15/20 13:19 MFFg/L0.44 6/15/20SM21-22 6200B21,1,2,2-Tetrachloroethane
ND 1.0 6/15/20 13:19 MFFg/L0.36 6/15/20SM21-22 6200B2Tetrachloroethylene
38 1.0 6/15/20 13:19 MFFg/L0.28 6/15/20SM21-22 6200B2Toluene
ND 2.0 6/15/20 13:19 MFFg/L1.1 6/15/20SM21-22 6200B21,2,3-Trichlorobenzene
ND 2.0 6/15/20 13:19 MFFg/L0.80 6/15/20SM21-22 6200B21,2,4-Trichlorobenzene
ND 1.0 6/15/20 13:19 MFFg/L0.40 6/15/20SM21-22 6200B21,1,1-Trichloroethane
ND 1.0 6/15/20 13:19 MFFg/L0.32 6/15/20SM21-22 6200B21,1,2-Trichloroethane
ND 1.0 6/15/20 13:19 MFFg/L0.48 6/15/20SM21-22 6200B2Trichloroethylene
ND 1.0 6/15/20 13:19 MFFg/L0.66 6/15/20SM21-22 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 6/15/20 13:19 MFFg/L0.50 6/15/20SM21-22 6200B21,2,3-Trichloropropane
55 2.0 6/15/20 13:19 MFFg/L0.36 6/15/20SM21-22 6200B21,2,4-Trimethylbenzene
290 2.0 6/15/20 13:19 MFFg/L0.28 6/15/20SM21-22 6200B21,3,5-Trimethylbenzene
ND 40 6/15/20 13:19 MFFg/L20 6/15/20SM21-22 6200B2Vinyl Acetate
ND 1.0 6/15/20 13:19 MFFg/L0.90 6/15/20SM21-22 6200B2Vinyl Chloride
120 2.0 6/15/20 13:19 MFFg/L0.60 6/15/20SM21-22 6200B2m+p Xylene
210 1.0 6/15/20 13:19 MFFg/L0.34 6/15/20SM21-22 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 115 6/15/20 13:1970-130
Toluene-d8 94.9 6/15/20 13:1970-130
4-Bromofluorobenzene 104 6/15/20 13:1970-130
Page 8 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-01
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 6/11/2020 14:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Drinking Water Organics EPA 504.1
4.7 0.80 6/19/20 20:19 JMBg/L0.48 6/19/20EPA 504.1401,2-Dibromoethane (EDB) (2)
Surrogates % Recovery Recovery Limits Flag/Qual
1,3-Dibromopropane (2)103 6/19/20 16:2670-130
Page 9 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-02
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 6/11/2020 13:45
[TOC_2]20F0590-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
72 100 6/15/20 13:44 MFFg/L7.6 6/15/20SM21-22 6200B2JAcetone
ND 1.0 6/15/20 13:44 MFFg/L0.36 6/15/20SM21-22 6200B2Benzene
ND 1.0 6/15/20 13:44 MFFg/L0.30 6/15/20SM21-22 6200B2Bromobenzene
ND 1.0 6/15/20 13:44 MFFg/L0.64 6/15/20SM21-22 6200B2Bromochloromethane
ND 1.0 6/15/20 13:44 MFFg/L0.32 6/15/20SM21-22 6200B2Bromodichloromethane
ND 1.0 6/15/20 13:44 MFFg/L0.92 6/15/20SM21-22 6200B2Bromoform
ND 4.0 6/15/20 13:44 MFFg/L2.8 6/15/20SM21-22 6200B2Bromomethane
19 10 6/15/20 13:44 MFFg/L3.9 6/15/20SM21-22 6200B22-Butanone (MEK)
40 1.0 6/15/20 13:44 MFFg/L0.42 6/15/20SM21-22 6200B2n-Butylbenzene
ND 1.0 6/15/20 13:44 MFFg/L0.32 6/15/20SM21-22 6200B2sec-Butylbenzene
7.3 1.0 6/15/20 13:44 MFFg/L0.34 6/15/20SM21-22 6200B2tert-Butylbenzene
ND 1.0 6/15/20 13:44 MFFg/L0.22 6/15/20SM21-22 6200B2Carbon Tetrachloride
ND 1.0 6/15/20 13:44 MFFg/L0.30 6/15/20SM21-22 6200B2Chlorobenzene
ND 100 6/15/20 13:44 MFFg/L21 6/15/20SM21-22 6200B2Ethanol
ND 1.0 6/15/20 13:44 MFFg/L0.42 6/15/20SM21-22 6200B2Chlorodibromomethane
ND 1.0 6/15/20 13:44 MFFg/L0.72 6/15/20SM21-22 6200B2Chloroethane
ND 2.0 6/15/20 13:44 MFFg/L0.34 6/15/20SM21-22 6200B2Chloroform
ND 4.0 6/15/20 13:44 MFFg/L0.90 6/15/20SM21-22 6200B2Chloromethane
ND 1.0 6/15/20 13:44 MFFg/L0.24 6/15/20SM21-22 6200B22-Chlorotoluene
ND 1.0 6/15/20 13:44 MFFg/L0.28 6/15/20SM21-22 6200B24-Chlorotoluene
5.6 1.0 6/15/20 13:44 MFFg/L0.38 6/15/20SM21-22 6200B21,2-Dibromoethane (EDB)
ND 1.0 6/15/20 13:44 MFFg/L0.32 6/15/20SM21-22 6200B21,2-Dichlorobenzene
ND 1.0 6/15/20 13:44 MFFg/L0.24 6/15/20SM21-22 6200B21,3-Dichlorobenzene
ND 1.0 6/15/20 13:44 MFFg/L0.26 6/15/20SM21-22 6200B21,4-Dichlorobenzene
ND 1.0 6/15/20 13:44 MFFg/L0.52 6/15/20SM21-22 6200B2Dichlorodifluoromethane (Freon 12)
ND 1.0 6/15/20 13:44 MFFg/L0.32 6/15/20SM21-22 6200B21,1-Dichloroethane
8.0 1.0 6/15/20 13:44 MFFg/L0.82 6/15/20SM21-22 6200B21,2-Dichloroethane
ND 1.0 6/15/20 13:44 MFFg/L0.64 6/15/20SM21-22 6200B21,1-Dichloroethylene
ND 1.0 6/15/20 13:44 MFFg/L0.26 6/15/20SM21-22 6200B2cis-1,2-Dichloroethylene
ND 1.0 6/15/20 13:44 MFFg/L0.62 6/15/20SM21-22 6200B2trans-1,2-Dichloroethylene
ND 1.0 6/15/20 13:44 MFFg/L0.40 6/15/20SM21-22 6200B21,2-Dichloropropane
ND 1.0 6/15/20 13:44 MFFg/L0.22 6/15/20SM21-22 6200B21,3-Dichloropropane
ND 1.0 6/15/20 13:44 MFFg/L0.40 6/15/20SM21-22 6200B22,2-Dichloropropane
ND 1.0 6/15/20 13:44 MFFg/L0.32 6/15/20SM21-22 6200B21,1-Dichloropropene
ND 1.0 6/15/20 13:44 MFFg/L0.26 6/15/20SM21-22 6200B2cis-1,3-Dichloropropene
ND 1.0 6/15/20 13:44 MFFg/L0.46 6/15/20SM21-22 6200B2trans-1,3-Dichloropropene
120 1.0 6/15/20 13:44 MFFg/L0.34 6/15/20SM21-22 6200B2Diisopropyl Ether (DIPE)
5.7 1.0 6/15/20 13:44 MFFg/L0.26 6/15/20SM21-22 6200B2Ethylbenzene
ND 10 6/15/20 13:44 MFFg/L3.0 6/15/20SM21-22 6200B22-Hexanone (MBK)
6.0 4.0 6/15/20 13:44 MFFg/L0.34 6/15/20SM21-22 6200B2Isopropylbenzene (Cumene)
5.3 4.0 6/15/20 13:44 MFFg/L0.40 6/15/20SM21-22 6200B2p-Isopropyltoluene (p-Cymene)
3.3 1.0 6/15/20 13:44 MFFg/L0.50 6/15/20SM21-22 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 6/15/20 13:44 MFFg/L0.68 6/15/20SM21-22 6200B2Methylene Chloride
ND 10 6/15/20 13:44 MFFg/L3.3 6/15/20SM21-22 6200B24-Methyl-2-pentanone (MIBK)
Page 10 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-02
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 6/11/2020 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
14 10 6/15/20 13:44 MFFg/L0.62 6/15/20SM21-22 6200B2Naphthalene
ND 1.0 6/15/20 13:44 MFFg/L0.26 6/15/20SM21-22 6200B2n-Propylbenzene
ND 4.0 6/15/20 13:44 MFFg/L0.22 6/15/20SM21-22 6200B2Styrene
ND 1.0 6/15/20 13:44 MFFg/L0.44 6/15/20SM21-22 6200B21,1,2,2-Tetrachloroethane
ND 1.0 6/15/20 13:44 MFFg/L0.36 6/15/20SM21-22 6200B2Tetrachloroethylene
ND 1.0 6/15/20 13:44 MFFg/L0.28 6/15/20SM21-22 6200B2Toluene
ND 2.0 6/15/20 13:44 MFFg/L1.1 6/15/20SM21-22 6200B21,2,3-Trichlorobenzene
ND 2.0 6/15/20 13:44 MFFg/L0.80 6/15/20SM21-22 6200B21,2,4-Trichlorobenzene
ND 1.0 6/15/20 13:44 MFFg/L0.40 6/15/20SM21-22 6200B21,1,1-Trichloroethane
ND 1.0 6/15/20 13:44 MFFg/L0.32 6/15/20SM21-22 6200B21,1,2-Trichloroethane
ND 1.0 6/15/20 13:44 MFFg/L0.48 6/15/20SM21-22 6200B2Trichloroethylene
ND 1.0 6/15/20 13:44 MFFg/L0.66 6/15/20SM21-22 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 6/15/20 13:44 MFFg/L0.50 6/15/20SM21-22 6200B21,2,3-Trichloropropane
ND 2.0 6/15/20 13:44 MFFg/L0.36 6/15/20SM21-22 6200B21,2,4-Trimethylbenzene
230 2.0 6/15/20 13:44 MFFg/L0.28 6/15/20SM21-22 6200B21,3,5-Trimethylbenzene
ND 40 6/15/20 13:44 MFFg/L20 6/15/20SM21-22 6200B2Vinyl Acetate
ND 1.0 6/15/20 13:44 MFFg/L0.90 6/15/20SM21-22 6200B2Vinyl Chloride
ND 2.0 6/15/20 13:44 MFFg/L0.60 6/15/20SM21-22 6200B2m+p Xylene
47 1.0 6/15/20 13:44 MFFg/L0.34 6/15/20SM21-22 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 115 6/15/20 13:4470-130
Toluene-d8 96.5 6/15/20 13:4470-130
4-Bromofluorobenzene 108 6/15/20 13:4470-130
Page 11 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-02
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 6/11/2020 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Drinking Water Organics EPA 504.1
5.3 0.83 6/19/20 20:51 JMBg/L0.50 6/19/20EPA 504.1401,2-Dibromoethane (EDB) (2)
Surrogates % Recovery Recovery Limits Flag/Qual
1,3-Dibromopropane (2)94.4 6/19/20 17:0070-130
Page 12 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-03
Field Sample #: WSW-2
Sample Matrix: Ground Water
Sampled: 6/11/2020 15:05
[TOC_2]20F0590-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 6/15/20 11:21 MFFg/L3.8 6/15/20SM21-22 6200B1Acetone
ND 0.50 6/15/20 11:21 MFFg/L0.18 6/15/20SM21-22 6200B1Benzene
ND 0.50 6/15/20 11:21 MFFg/L0.15 6/15/20SM21-22 6200B1Bromobenzene
ND 0.50 6/15/20 11:21 MFFg/L0.32 6/15/20SM21-22 6200B1Bromochloromethane
ND 0.50 6/15/20 11:21 MFFg/L0.16 6/15/20SM21-22 6200B1Bromodichloromethane
ND 0.50 6/15/20 11:21 MFFg/L0.46 6/15/20SM21-22 6200B1Bromoform
ND 2.0 6/15/20 11:21 MFFg/L1.4 6/15/20SM21-22 6200B1Bromomethane
ND 5.0 6/15/20 11:21 MFFg/L1.9 6/15/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 6/15/20 11:21 MFFg/L0.21 6/15/20SM21-22 6200B1n-Butylbenzene
ND 0.50 6/15/20 11:21 MFFg/L0.16 6/15/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 6/15/20 11:21 MFFg/L0.17 6/15/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 6/15/20 11:21 MFFg/L0.11 6/15/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 6/15/20 11:21 MFFg/L0.15 6/15/20SM21-22 6200B1Chlorobenzene
ND 50 6/15/20 11:21 MFFg/L11 6/15/20SM21-22 6200B1Ethanol
ND 0.50 6/15/20 11:21 MFFg/L0.21 6/15/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 6/15/20 11:21 MFFg/L0.36 6/15/20SM21-22 6200B1Chloroethane
ND 1.0 6/15/20 11:21 MFFg/L0.17 6/15/20SM21-22 6200B1Chloroform
ND 2.0 6/15/20 11:21 MFFg/L0.45 6/15/20SM21-22 6200B1Chloromethane
ND 0.50 6/15/20 11:21 MFFg/L0.12 6/15/20SM21-22 6200B12-Chlorotoluene
ND 0.50 6/15/20 11:21 MFFg/L0.14 6/15/20SM21-22 6200B14-Chlorotoluene
ND 0.50 6/15/20 11:21 MFFg/L0.19 6/15/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 6/15/20 11:21 MFFg/L0.16 6/15/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 6/15/20 11:21 MFFg/L0.12 6/15/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 6/15/20 11:21 MFFg/L0.13 6/15/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 6/15/20 11:21 MFFg/L0.26 6/15/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 6/15/20 11:21 MFFg/L0.16 6/15/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 6/15/20 11:21 MFFg/L0.41 6/15/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 6/15/20 11:21 MFFg/L0.32 6/15/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 6/15/20 11:21 MFFg/L0.13 6/15/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 6/15/20 11:21 MFFg/L0.31 6/15/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 6/15/20 11:21 MFFg/L0.20 6/15/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 6/15/20 11:21 MFFg/L0.11 6/15/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 6/15/20 11:21 MFFg/L0.20 6/15/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 6/15/20 11:21 MFFg/L0.16 6/15/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 6/15/20 11:21 MFFg/L0.13 6/15/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 6/15/20 11:21 MFFg/L0.23 6/15/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 6/15/20 11:21 MFFg/L0.17 6/15/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 6/15/20 11:21 MFFg/L0.13 6/15/20SM21-22 6200B1Ethylbenzene
ND 5.0 6/15/20 11:21 MFFg/L1.5 6/15/20SM21-22 6200B12-Hexanone (MBK)
ND 2.0 6/15/20 11:21 MFFg/L0.17 6/15/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 2.0 6/15/20 11:21 MFFg/L0.20 6/15/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 6/15/20 11:21 MFFg/L0.25 6/15/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 6/15/20 11:21 MFFg/L0.34 6/15/20SM21-22 6200B1Methylene Chloride
ND 5.0 6/15/20 11:21 MFFg/L1.7 6/15/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 13 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-03
Field Sample #: WSW-2
Sample Matrix: Ground Water
Sampled: 6/11/2020 15:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 6/15/20 11:21 MFFg/L0.31 6/15/20SM21-22 6200B1Naphthalene
ND 0.50 6/15/20 11:21 MFFg/L0.13 6/15/20SM21-22 6200B1n-Propylbenzene
ND 2.0 6/15/20 11:21 MFFg/L0.11 6/15/20SM21-22 6200B1Styrene
ND 0.50 6/15/20 11:21 MFFg/L0.22 6/15/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 6/15/20 11:21 MFFg/L0.18 6/15/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 6/15/20 11:21 MFFg/L0.14 6/15/20SM21-22 6200B1Toluene
ND 1.0 6/15/20 11:21 MFFg/L0.57 6/15/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 1.0 6/15/20 11:21 MFFg/L0.40 6/15/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 6/15/20 11:21 MFFg/L0.20 6/15/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 6/15/20 11:21 MFFg/L0.16 6/15/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 6/15/20 11:21 MFFg/L0.24 6/15/20SM21-22 6200B1Trichloroethylene
ND 0.50 6/15/20 11:21 MFFg/L0.33 6/15/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 6/15/20 11:21 MFFg/L0.25 6/15/20SM21-22 6200B11,2,3-Trichloropropane
ND 1.0 6/15/20 11:21 MFFg/L0.18 6/15/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 1.0 6/15/20 11:21 MFFg/L0.14 6/15/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 6/15/20 11:21 MFFg/L10 6/15/20SM21-22 6200B1Vinyl Acetate
ND 0.50 6/15/20 11:21 MFFg/L0.45 6/15/20SM21-22 6200B1Vinyl Chloride
ND 1.0 6/15/20 11:21 MFFg/L0.30 6/15/20SM21-22 6200B1m+p Xylene
ND 0.50 6/15/20 11:21 MFFg/L0.17 6/15/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 6/15/20 11:2170-130
Toluene-d8 95.0 6/15/20 11:2170-130
4-Bromofluorobenzene 94.2 6/15/20 11:2170-130
Page 14 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-03
Field Sample #: WSW-2
Sample Matrix: Ground Water
Sampled: 6/11/2020 15:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Drinking Water Organics EPA 504.1
ND 0.020 6/19/20 17:33 JMBg/L0.012 6/19/20EPA 504.111,2-Dibromoethane (EDB) (2)
Surrogates % Recovery Recovery Limits Flag/Qual
1,3-Dibromopropane (2)105 6/19/20 17:3370-130
Page 15 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-04
Field Sample #: WSW-4
Sample Matrix: Ground Water
Sampled: 6/11/2020 15:45
[TOC_2]20F0590-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 6/15/20 11:45 MFFg/L3.8 6/15/20SM21-22 6200B1Acetone
ND 0.50 6/15/20 11:45 MFFg/L0.18 6/15/20SM21-22 6200B1Benzene
ND 0.50 6/15/20 11:45 MFFg/L0.15 6/15/20SM21-22 6200B1Bromobenzene
ND 0.50 6/15/20 11:45 MFFg/L0.32 6/15/20SM21-22 6200B1Bromochloromethane
ND 0.50 6/15/20 11:45 MFFg/L0.16 6/15/20SM21-22 6200B1Bromodichloromethane
ND 0.50 6/15/20 11:45 MFFg/L0.46 6/15/20SM21-22 6200B1Bromoform
ND 2.0 6/15/20 11:45 MFFg/L1.4 6/15/20SM21-22 6200B1Bromomethane
ND 5.0 6/15/20 11:45 MFFg/L1.9 6/15/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 6/15/20 11:45 MFFg/L0.21 6/15/20SM21-22 6200B1n-Butylbenzene
ND 0.50 6/15/20 11:45 MFFg/L0.16 6/15/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 6/15/20 11:45 MFFg/L0.17 6/15/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 6/15/20 11:45 MFFg/L0.11 6/15/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 6/15/20 11:45 MFFg/L0.15 6/15/20SM21-22 6200B1Chlorobenzene
ND 50 6/15/20 11:45 MFFg/L11 6/15/20SM21-22 6200B1Ethanol
ND 0.50 6/15/20 11:45 MFFg/L0.21 6/15/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 6/15/20 11:45 MFFg/L0.36 6/15/20SM21-22 6200B1Chloroethane
ND 1.0 6/15/20 11:45 MFFg/L0.17 6/15/20SM21-22 6200B1Chloroform
ND 2.0 6/15/20 11:45 MFFg/L0.45 6/15/20SM21-22 6200B1Chloromethane
ND 0.50 6/15/20 11:45 MFFg/L0.12 6/15/20SM21-22 6200B12-Chlorotoluene
ND 0.50 6/15/20 11:45 MFFg/L0.14 6/15/20SM21-22 6200B14-Chlorotoluene
ND 0.50 6/15/20 11:45 MFFg/L0.19 6/15/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 6/15/20 11:45 MFFg/L0.16 6/15/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 6/15/20 11:45 MFFg/L0.12 6/15/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 6/15/20 11:45 MFFg/L0.13 6/15/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 6/15/20 11:45 MFFg/L0.26 6/15/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 6/15/20 11:45 MFFg/L0.16 6/15/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 6/15/20 11:45 MFFg/L0.41 6/15/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 6/15/20 11:45 MFFg/L0.32 6/15/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 6/15/20 11:45 MFFg/L0.13 6/15/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 6/15/20 11:45 MFFg/L0.31 6/15/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 6/15/20 11:45 MFFg/L0.20 6/15/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 6/15/20 11:45 MFFg/L0.11 6/15/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 6/15/20 11:45 MFFg/L0.20 6/15/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 6/15/20 11:45 MFFg/L0.16 6/15/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 6/15/20 11:45 MFFg/L0.13 6/15/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 6/15/20 11:45 MFFg/L0.23 6/15/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 6/15/20 11:45 MFFg/L0.17 6/15/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 6/15/20 11:45 MFFg/L0.13 6/15/20SM21-22 6200B1Ethylbenzene
ND 5.0 6/15/20 11:45 MFFg/L1.5 6/15/20SM21-22 6200B12-Hexanone (MBK)
ND 2.0 6/15/20 11:45 MFFg/L0.17 6/15/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 2.0 6/15/20 11:45 MFFg/L0.20 6/15/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 6/15/20 11:45 MFFg/L0.25 6/15/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 6/15/20 11:45 MFFg/L0.34 6/15/20SM21-22 6200B1Methylene Chloride
ND 5.0 6/15/20 11:45 MFFg/L1.7 6/15/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 16 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-04
Field Sample #: WSW-4
Sample Matrix: Ground Water
Sampled: 6/11/2020 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 6/15/20 11:45 MFFg/L0.31 6/15/20SM21-22 6200B1Naphthalene
ND 0.50 6/15/20 11:45 MFFg/L0.13 6/15/20SM21-22 6200B1n-Propylbenzene
ND 2.0 6/15/20 11:45 MFFg/L0.11 6/15/20SM21-22 6200B1Styrene
ND 0.50 6/15/20 11:45 MFFg/L0.22 6/15/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 6/15/20 11:45 MFFg/L0.18 6/15/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 6/15/20 11:45 MFFg/L0.14 6/15/20SM21-22 6200B1Toluene
ND 1.0 6/15/20 11:45 MFFg/L0.57 6/15/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 1.0 6/15/20 11:45 MFFg/L0.40 6/15/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 6/15/20 11:45 MFFg/L0.20 6/15/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 6/15/20 11:45 MFFg/L0.16 6/15/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 6/15/20 11:45 MFFg/L0.24 6/15/20SM21-22 6200B1Trichloroethylene
ND 0.50 6/15/20 11:45 MFFg/L0.33 6/15/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 6/15/20 11:45 MFFg/L0.25 6/15/20SM21-22 6200B11,2,3-Trichloropropane
ND 1.0 6/15/20 11:45 MFFg/L0.18 6/15/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 1.0 6/15/20 11:45 MFFg/L0.14 6/15/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 6/15/20 11:45 MFFg/L10 6/15/20SM21-22 6200B1Vinyl Acetate
ND 0.50 6/15/20 11:45 MFFg/L0.45 6/15/20SM21-22 6200B1Vinyl Chloride
ND 1.0 6/15/20 11:45 MFFg/L0.30 6/15/20SM21-22 6200B1m+p Xylene
ND 0.50 6/15/20 11:45 MFFg/L0.17 6/15/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 112 6/15/20 11:4570-130
Toluene-d8 93.6 6/15/20 11:4570-130
4-Bromofluorobenzene 93.2 6/15/20 11:4570-130
Page 17 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-04
Field Sample #: WSW-4
Sample Matrix: Ground Water
Sampled: 6/11/2020 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Drinking Water Organics EPA 504.1
ND 0.020 6/19/20 18:07 JMBg/L0.012 6/19/20EPA 504.111,2-Dibromoethane (EDB) (2)
Surrogates % Recovery Recovery Limits Flag/Qual
1,3-Dibromopropane (2)121 6/19/20 18:0770-130
Page 18 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-05
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 6/11/2020 14:20
[TOC_2]20F0590-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 6/15/20 10:10 MFFg/L3.8 6/15/20SM21-22 6200B1Acetone
ND 0.50 6/15/20 10:10 MFFg/L0.18 6/15/20SM21-22 6200B1Benzene
ND 0.50 6/15/20 10:10 MFFg/L0.15 6/15/20SM21-22 6200B1Bromobenzene
ND 0.50 6/15/20 10:10 MFFg/L0.32 6/15/20SM21-22 6200B1Bromochloromethane
ND 0.50 6/15/20 10:10 MFFg/L0.16 6/15/20SM21-22 6200B1Bromodichloromethane
ND 0.50 6/15/20 10:10 MFFg/L0.46 6/15/20SM21-22 6200B1Bromoform
ND 2.0 6/15/20 10:10 MFFg/L1.4 6/15/20SM21-22 6200B1Bromomethane
ND 5.0 6/15/20 10:10 MFFg/L1.9 6/15/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 6/15/20 10:10 MFFg/L0.21 6/15/20SM21-22 6200B1n-Butylbenzene
ND 0.50 6/15/20 10:10 MFFg/L0.16 6/15/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 6/15/20 10:10 MFFg/L0.17 6/15/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 6/15/20 10:10 MFFg/L0.11 6/15/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 6/15/20 10:10 MFFg/L0.15 6/15/20SM21-22 6200B1Chlorobenzene
ND 50 6/15/20 10:10 MFFg/L11 6/15/20SM21-22 6200B1Ethanol
ND 0.50 6/15/20 10:10 MFFg/L0.21 6/15/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 6/15/20 10:10 MFFg/L0.36 6/15/20SM21-22 6200B1Chloroethane
ND 1.0 6/15/20 10:10 MFFg/L0.17 6/15/20SM21-22 6200B1Chloroform
ND 2.0 6/15/20 10:10 MFFg/L0.45 6/15/20SM21-22 6200B1Chloromethane
ND 0.50 6/15/20 10:10 MFFg/L0.12 6/15/20SM21-22 6200B12-Chlorotoluene
ND 0.50 6/15/20 10:10 MFFg/L0.14 6/15/20SM21-22 6200B14-Chlorotoluene
ND 0.50 6/15/20 10:10 MFFg/L0.19 6/15/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 6/15/20 10:10 MFFg/L0.16 6/15/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 6/15/20 10:10 MFFg/L0.12 6/15/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 6/15/20 10:10 MFFg/L0.13 6/15/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 6/15/20 10:10 MFFg/L0.26 6/15/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 6/15/20 10:10 MFFg/L0.16 6/15/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 6/15/20 10:10 MFFg/L0.41 6/15/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 6/15/20 10:10 MFFg/L0.32 6/15/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 6/15/20 10:10 MFFg/L0.13 6/15/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 6/15/20 10:10 MFFg/L0.31 6/15/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 6/15/20 10:10 MFFg/L0.20 6/15/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 6/15/20 10:10 MFFg/L0.11 6/15/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 6/15/20 10:10 MFFg/L0.20 6/15/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 6/15/20 10:10 MFFg/L0.16 6/15/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 6/15/20 10:10 MFFg/L0.13 6/15/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 6/15/20 10:10 MFFg/L0.23 6/15/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 6/15/20 10:10 MFFg/L0.17 6/15/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 6/15/20 10:10 MFFg/L0.13 6/15/20SM21-22 6200B1Ethylbenzene
ND 5.0 6/15/20 10:10 MFFg/L1.5 6/15/20SM21-22 6200B12-Hexanone (MBK)
ND 2.0 6/15/20 10:10 MFFg/L0.17 6/15/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 2.0 6/15/20 10:10 MFFg/L0.20 6/15/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 6/15/20 10:10 MFFg/L0.25 6/15/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 6/15/20 10:10 MFFg/L0.34 6/15/20SM21-22 6200B1Methylene Chloride
ND 5.0 6/15/20 10:10 MFFg/L1.7 6/15/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 19 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 6/11/2020
Work Order: 20F0590Sample Description:Project Location: Reidsville, NC
Sample ID: 20F0590-05
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 6/11/2020 14:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 6/15/20 10:10 MFFg/L0.31 6/15/20SM21-22 6200B1Naphthalene
ND 0.50 6/15/20 10:10 MFFg/L0.13 6/15/20SM21-22 6200B1n-Propylbenzene
ND 2.0 6/15/20 10:10 MFFg/L0.11 6/15/20SM21-22 6200B1Styrene
ND 0.50 6/15/20 10:10 MFFg/L0.22 6/15/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 6/15/20 10:10 MFFg/L0.18 6/15/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 6/15/20 10:10 MFFg/L0.14 6/15/20SM21-22 6200B1Toluene
ND 1.0 6/15/20 10:10 MFFg/L0.57 6/15/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 1.0 6/15/20 10:10 MFFg/L0.40 6/15/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 6/15/20 10:10 MFFg/L0.20 6/15/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 6/15/20 10:10 MFFg/L0.16 6/15/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 6/15/20 10:10 MFFg/L0.24 6/15/20SM21-22 6200B1Trichloroethylene
ND 0.50 6/15/20 10:10 MFFg/L0.33 6/15/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 6/15/20 10:10 MFFg/L0.25 6/15/20SM21-22 6200B11,2,3-Trichloropropane
ND 1.0 6/15/20 10:10 MFFg/L0.18 6/15/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 1.0 6/15/20 10:10 MFFg/L0.14 6/15/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 6/15/20 10:10 MFFg/L10 6/15/20SM21-22 6200B1Vinyl Acetate
ND 0.50 6/15/20 10:10 MFFg/L0.45 6/15/20SM21-22 6200B1Vinyl Chloride
ND 1.0 6/15/20 10:10 MFFg/L0.30 6/15/20SM21-22 6200B1m+p Xylene
ND 0.50 6/15/20 10:10 MFFg/L0.17 6/15/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 6/15/20 10:1070-130
Toluene-d8 91.8 6/15/20 10:1070-130
4-Bromofluorobenzene 96.7 6/15/20 10:1070-130
Page 20 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: EPA 504 water-EPA 504.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B260377 06/19/2035.2 35.020F0590-01 [MW-3]
B260377 06/19/2033.9 35.020F0590-02 [MW-5]
B260377 06/19/2035.3 35.020F0590-03 [WSW-2]
B260377 06/19/2035.6 35.020F0590-04 [WSW-4]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B259986 06/15/202.5 5.0020F0590-01 [MW-3]
B259986 06/15/202.5 5.0020F0590-02 [MW-5]
B259986 06/15/205 5.0020F0590-03 [WSW-2]
B259986 06/15/205 5.0020F0590-04 [WSW-4]
B259986 06/15/205 5.0020F0590-05 [Field Blank]
[TOC_1]Sample Preparation Information[TOC]
Page 21 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B259986 - SW-846 5030B
[TOC_3]B259986[TOC]
Blank (B259986-BLK1) Prepared & Analyzed: 06/15/20
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 22 of 37
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B259986 - SW-846 5030B
Blank (B259986-BLK1) Prepared & Analyzed: 06/15/20
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.4
g/L 25.0 70-130Surrogate: Toluene-d8 93.323.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.524.4
LCS (B259986-BS1) Prepared & Analyzed: 06/15/20
Acetone g/L50 100 70-130122122
Benzene g/L0.50 10.0 70-13011711.7
Bromobenzene g/L0.50 10.0 70-13010910.9
Bromochloromethane g/L0.50 10.0 70-13012112.1
Bromodichloromethane g/L0.50 10.0 70-13094.59.45
Bromoform g/L0.50 10.0 70-13097.79.77
Bromomethane g/L2.0 10.0 60-14082.68.26
2-Butanone (MEK)g/L5.0 100 70-130125125
n-Butylbenzene g/L0.50 10.0 70-13012712.7
sec-Butylbenzene g/L0.50 10.0 L-0770-130132*13.2
tert-Butylbenzene g/L0.50 10.0 70-13012412.4
Carbon Tetrachloride g/L0.50 10.0 70-13093.19.31
Chlorobenzene g/L0.50 10.0 70-13010810.8
Ethanol g/L50 100 70-13084.884.8
Chlorodibromomethane g/L0.50 10.0 70-13086.18.61
Chloroethane g/L0.50 10.0 60-14098.99.89
Chloroform g/L0.50 10.0 70-13011411.4
Chloromethane g/L0.60 10.0 60-14078.77.87
2-Chlorotoluene g/L0.50 10.0 70-13011211.2
4-Chlorotoluene g/L0.50 10.0 70-13011311.3
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13098.69.86
1,2-Dichlorobenzene g/L0.50 10.0 70-13010710.7
1,3-Dichlorobenzene g/L0.50 10.0 70-13011511.5
1,4-Dichlorobenzene g/L0.50 10.0 70-13010810.8
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14073.47.34
1,1-Dichloroethane g/L0.50 10.0 70-13012112.1
1,2-Dichloroethane g/L0.50 10.0 70-13091.29.12
1,1-Dichloroethylene g/L0.50 10.0 70-13011011.0
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13012612.6
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010310.3
1,2-Dichloropropane g/L0.50 10.0 70-13010910.9
1,3-Dichloropropane g/L0.50 10.0 70-13010010.0
2,2-Dichloropropane g/L0.50 10.0 70-13010810.8
1,1-Dichloropropene g/L0.50 10.0 70-13010610.6
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010310.3
trans-1,3-Dichloropropene g/L0.50 10.0 70-13097.39.73
Page 23 of 37
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B259986 - SW-846 5030B
LCS (B259986-BS1) Prepared & Analyzed: 06/15/20
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13011711.7
Ethylbenzene g/L0.50 10.0 70-13011511.5
2-Hexanone (MBK)g/L5.0 100 70-130106106
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010910.9
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011611.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13092.89.28
Methylene Chloride g/L5.0 10.0 70-13012412.4
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130111111
Naphthalene g/L0.50 10.0 70-13011111.1
n-Propylbenzene g/L0.50 10.0 70-13011011.0
Styrene g/L0.50 10.0 70-13010910.9
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13097.59.75
Tetrachloroethylene g/L0.50 10.0 70-13098.79.87
Toluene g/L0.50 10.0 70-13010410.4
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13098.49.84
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13010710.7
1,1,1-Trichloroethane g/L0.50 10.0 70-13099.99.99
1,1,2-Trichloroethane g/L0.50 10.0 70-13096.99.69
Trichloroethylene g/L0.50 10.0 70-13099.79.97
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13086.08.60
1,2,3-Trichloropropane g/L0.50 10.0 70-13010510.5
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011611.6
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010210.2
Vinyl Acetate g/L20 100 70-130111111
Vinyl Chloride g/L0.50 10.0 60-14079.07.90
m+p Xylene g/L1.0 20.0 70-13011623.2
o-Xylene g/L0.50 10.0 70-13011411.4
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.124.3
g/L 25.0 70-130Surrogate: Toluene-d8 96.024.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.2
LCS Dup (B259986-BSD1) Prepared & Analyzed: 06/15/20
Acetone g/L50 100 2570-130119 2.70119
Benzene g/L0.50 10.0 2570-130111 5.0011.1
Bromobenzene g/L0.50 10.0 2570-130106 2.4110.6
Bromochloromethane g/L0.50 10.0 2570-130117 4.0311.7
Bromodichloromethane g/L0.50 10.0 2570-13093.2 1.399.32
Bromoform g/L0.50 10.0 2570-13092.7 5.259.27
Bromomethane g/L2.0 10.0 2560-14086.2 4.278.62
2-Butanone (MEK)g/L5.0 100 2570-130123 1.65123
n-Butylbenzene g/L0.50 10.0 2570-130128 1.1012.8
sec-Butylbenzene g/L0.50 10.0 2570-130127 4.2412.7
tert-Butylbenzene g/L0.50 10.0 2570-130125 0.80512.5
Carbon Tetrachloride g/L0.50 10.0 2570-13089.5 3.948.95
Chlorobenzene g/L0.50 10.0 2570-130105 2.2510.5
Ethanol g/L50 100 2570-13082.1 3.2282.1
Chlorodibromomethane g/L0.50 10.0 2570-13086.2 0.1168.62
Chloroethane g/L0.50 10.0 2560-14093.3 5.839.33
Chloroform g/L0.50 10.0 2570-130110 3.4811.0
Chloromethane g/L0.60 10.0 2560-14081.2 3.138.12
2-Chlorotoluene g/L0.50 10.0 2570-130111 1.4311.1
4-Chlorotoluene g/L0.50 10.0 2570-130111 1.2511.1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B259986 - SW-846 5030B
LCS Dup (B259986-BSD1) Prepared & Analyzed: 06/15/20
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13099.5 0.9099.95
1,2-Dichlorobenzene g/L0.50 10.0 2570-130109 1.8510.9
1,3-Dichlorobenzene g/L0.50 10.0 2570-130115 0.0011.5
1,4-Dichlorobenzene g/L0.50 10.0 2570-130106 2.1510.6
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14067.8 7.936.78
1,1-Dichloroethane g/L0.50 10.0 2570-130117 3.9511.7
1,2-Dichloroethane g/L0.50 10.0 2570-13088.2 3.348.82
1,1-Dichloroethylene g/L0.50 10.0 2570-130105 4.4610.5
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130114 10.111.4
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130109 5.9410.9
1,2-Dichloropropane g/L0.50 10.0 2570-130103 6.2310.3
1,3-Dichloropropane g/L0.50 10.0 2570-13099.5 1.009.95
2,2-Dichloropropane g/L0.50 10.0 2570-130100 7.0310.0
1,1-Dichloropropene g/L0.50 10.0 2570-13098.7 7.239.87
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13098.8 3.879.88
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13097.7 0.4109.77
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130117 0.17111.7
Ethylbenzene g/L0.50 10.0 2570-130113 2.0111.3
2-Hexanone (MBK)g/L5.0 100 2570-130109 1.99109
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130107 1.8610.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130115 1.2111.5
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130102 9.8410.2
Methylene Chloride g/L5.0 10.0 2570-130115 7.6811.5
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130112 0.779112
Naphthalene g/L0.50 10.0 2570-130110 0.63111.0
n-Propylbenzene g/L0.50 10.0 2570-130106 3.8110.6
Styrene g/L0.50 10.0 2570-130106 3.1610.6
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13097.5 0.009.75
Tetrachloroethylene g/L0.50 10.0 2570-13096.8 1.949.68
Toluene g/L0.50 10.0 2570-130101 2.0510.1
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13095.9 2.579.59
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130106 0.93810.6
1,1,1-Trichloroethane g/L0.50 10.0 2570-13097.3 2.649.73
1,1,2-Trichloroethane g/L0.50 10.0 2570-13096.4 0.5179.64
Trichloroethylene g/L0.50 10.0 2570-13097.7 2.039.77
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13080.5 6.618.05
1,2,3-Trichloropropane g/L0.50 10.0 2570-130101 3.4010.1
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130114 2.4311.4
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130102 0.19710.2
Vinyl Acetate g/L20 100 2570-130108 2.98108
Vinyl Chloride g/L0.50 10.0 2560-14077.4 2.057.74
m+p Xylene g/L1.0 20.0 2570-130112 3.7722.4
o-Xylene g/L0.50 10.0 2570-130111 3.0111.1
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.524.4
g/L 25.0 70-130Surrogate: Toluene-d8 95.523.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10426.0
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Drinking Water Organics EPA 504.1 - Quality Control
QUALITY CONTROL
[TOC_2]Drinking Water Organics EPA 504.1[TOC]
Batch B260377 - EPA 504 water
[TOC_3]B260377[TOC]
Blank (B260377-BLK1) Prepared & Analyzed: 06/19/20
1,2-Dibromoethane (EDB) [2C]g/L0.021ND
g/L 1.05 70-130Surrogate: 1,3-Dibromopropane [2C]97.81.03
LCS (B260377-BS1) Prepared & Analyzed: 06/19/20
1,2-Dibromoethane (EDB) [2C]g/L0.021 0.257 70-13084.40.217
g/L 1.03 70-130Surrogate: 1,3-Dibromopropane [2C]1141.17
LCS Dup (B260377-BSD1) Prepared & Analyzed: 06/19/20
1,2-Dibromoethane (EDB) [2C]g/L0.021 0.262 70-13072.8 12.70.191
g/L 1.05 70-130Surrogate: 1,3-Dibromopropane [2C]1101.15
Matrix Spike (B260377-MS1) Prepared & Analyzed: 06/19/20 Source: 20F0590-04
1,2-Dibromoethane (EDB) [2C]g/L0.020 0.246 65-13580.40.197 ND
g/L 0.982 70-130Surrogate: 1,3-Dibromopropane [2C]1051.03
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
IDENTIFICATION SUMMARY
FOR SINGLE COMPONENT ANALYTES MW-3
EPA 504.1
Lab Sample ID:Date(s) Analyzed:20F0590-01
Instrument ID (1):
GC Column (1):ID:(mm)(mm)ID:GC Column (2):
A Instrument ID (2):B
06/19/2020 06/19/2020
ANALYTE CONCENTRATION %DCOLRTRT WINDOW
FROM TO
4.70.0000.0003.3182 11.2
[TOC_1]Dual Column RPD Report[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
IDENTIFICATION SUMMARY
FOR SINGLE COMPONENT ANALYTES MW-5
EPA 504.1
Lab Sample ID:Date(s) Analyzed:20F0590-02
Instrument ID (1):
GC Column (1):ID:(mm)(mm)ID:GC Column (2):
A Instrument ID (2):B
06/19/2020 06/19/2020
ANALYTE CONCENTRATION %DCOLRTRT WINDOW
FROM TO
5.30.0000.0003.3192 5.8
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
IDENTIFICATION SUMMARY
FOR SINGLE COMPONENT ANALYTES LCS
EPA 504.1
Lab Sample ID:Date(s) Analyzed:B260377-BS1
Instrument ID (1):
GC Column (1):ID:(mm)(mm)ID:GC Column (2):
Instrument ID (2):
06/19/2020 06/19/2020
ANALYTE CONCENTRATION %DCOLRTRT WINDOW
FROM TO
0.2170.0000.0003.3142 13.3
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
IDENTIFICATION SUMMARY
FOR SINGLE COMPONENT ANALYTES LCS Dup
EPA 504.1
Lab Sample ID:Date(s) Analyzed:B260377-BSD1
Instrument ID (1):
GC Column (1):ID:(mm)(mm)ID:GC Column (2):
Instrument ID (2):
06/19/2020 06/19/2020
ANALYTE CONCENTRATION %DCOLRTRT WINDOW
FROM TO
0.1910.0000.0003.3152 5.9
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
IDENTIFICATION SUMMARY
FOR SINGLE COMPONENT ANALYTES Matrix Spike
EPA 504.1
Lab Sample ID:Date(s) Analyzed:B260377-MS1
Instrument ID (1):
GC Column (1):ID:(mm)(mm)ID:GC Column (2):
Instrument ID (2):
06/19/2020 06/19/2020
ANALYTE CONCENTRATION %DCOLRTRT WINDOW
FROM TO
0.1970.0000.0003.3202 9.0
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
Page 33 of 37
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2021
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2021
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2021
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2021
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2021
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