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HomeMy WebLinkAbout26002_Commercial Equipment_BF Assessment Report_20230620 Via Email June 20, 2023 NCDEQ – Division of Waste Management Brownfields Redevelopment Section 1646 Mail Service Center Raleigh, North Carolina 27699-1646 Attn: Ms. Carolyn Minnich Re: Brownfields Assessment Report Commercial Equipment Company Charlotte, North Carolina Brownfields Project No. 26002-22-060 H&H Project No. ABS-003 Dear Carolyn: On behalf of Abacus Acquisitions, LLC, please find the enclosed Brownfields Assessment Report prepared for the Commercial Equipment Company Brownfields property. Should you have questions or need additional information, please do not hesitate to contact us. Sincerely, Hart & Hickman, PC Haley Martin, PG Ralph McGee, PG Senior Project Geologist Senior Project Manager Enclosures cc: Mr. Mason Ellerbe, Abacus Capital (via email) Mr. John Grantham, Abacus Capital (via email) Ms. Mary Katherine Stukes, Moore & Van Allen, PLLC (via email) Attachment: i https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Brownfields Assessment Report Commercial Equipment Company N. Graham Street and W. 28th Street Charlotte, North Carolina H&H Job No. ABS-003 Table of Contents 1.0 Introduction .............................................................................................................................1  1.1 Background Information .......................................................................................................2  1.2 Previous Assessment Activities .............................................................................................3  2.0 Brownfields Assessment Activities ......................................................................................10  3.0 Additional Soil Assessment Activities .................................................................................11  3.1 Soil Sampling Activities ......................................................................................................11  3.2 Soil Sampling Analytical Results ........................................................................................13  4.0 Additional Soil Gas Assessment Activities ..........................................................................15  4.1 Soil Gas Sampling Activities ...............................................................................................15  4.2 Soil Gas Sampling Results ..................................................................................................17  4.3 Vapor Intrusion Risk Evaluation .........................................................................................19  5.0 Subsurface Methane Gas and Pressure Measurements ....................................................21  5.1 Methane Gas Sampling Activities .......................................................................................21  5.2 Methane Gas Sampling Results ...........................................................................................22  5.3 Methane Vapor Intrusion Risk Evaluation ..........................................................................23  6.0 Quality Assurance – Quality Control ..................................................................................25  6.1 Field Duplicates ...................................................................................................................25  7.0 Summary and Conclusions ..................................................................................................27  ii https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc List of Tables Table 1 Summary of Soil Analytical Data Table 2 Summary of Soil Gas Analytical Data Table 3 Summary of Subsurface Methane Gas Measurements List of Figures Figure 1 Site Location Map Figure 2 Site Map Figure 3 Sample Location Map List of Appendices Appendix A February 2022 Phase II ESA Data Appendix B Boring Logs Appendix C Laboratory Analytical Reports Appendix D DEQ Risk Calculator (January 2023) Appendix E Vapor Sampling Forms Appendix F Landtec GEM 5000® Portable Gas Analyzer Specifications and Raw Data Set 1 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Brownfields Assessment Report Commercial Equipment Company N. Graham Street and W. 28th Street Charlotte, North Carolina H&H Job No. ABS-003 1.0 Introduction On behalf of Abacus Acquisitions, LLC (Abacus), Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment Report for the Commercial Equipment Company Brownfields property (Brownfields Project No. 26002-22-060) located southeast of the N. Graham Street and W. 28th Street intersection in Charlotte, Mecklenburg County, North Carolina (Site or subject Site). A Site location map is provided as Figure 1. The subject Site is comprised of four contiguous parcels (Mecklenburg County Parcel ID Nos. 07907911, 07907910, 07907909, and 07907908) that collectively total approximately 7.5 acres of land. The northwestern portion of the Site (2402/2426 N. Graham Street) is developed with an approximately 4,500-square foot (sq ft) office building with an approximate 1,800-sq ft basement constructed in 1945, and the southern portion of the Site (609 W. 28th Street) is developed with an approximately 7,350 sq ft service garage constructed in 1969. The parcels located in the southeastern portion of the Site (2409 and 2415 Grimes Street) are developed with single-family residences that were constructed in 1949. The Site and surrounding area are shown in Figure 2. Proposed redevelopment of the Site includes construction of residential for-rent townhome-style buildings and multifamily apartment buildings with associated parking and amenities areas. Note that construction of the for-rent townhome buildings includes ground-level parking garages that are not connected to upper-level occupiable spaces except for a small landing and staircase at the entrance to each unit. An overlay of the preliminary Site redevelopment plan including locations of proposed buildings is provided as Figure 3. A summary of Site background information including previous assessment activities conducted at the Site is provided below. 2 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 1.1 Background Information Prior to the late 1930s, the Site consisted predominately of undeveloped land used for agricultural purposes (e.g., hay fields or pastures) and a rural access road. By the late 1940s, the western portion of the Site was developed with three commercial buildings associated with a motor freight station and auto repair facility. By the late 1950s, the southern portion of the Site was developed with five single-family residences. In the early 1970s, the auto repair shop in the central portion of the Site was razed and a portion of the current 609 W. 28th Street building was constructed in the southern portion of the Site. In the 1980s and 1990s, all but two residences in the southern portion of the Site were razed and additions to the 609 W. 28th Street building were completed. The Site was occupied by Starnes Pallet from the early 2000s to the early 2020s. Starnes Pallet operations included salvage of used wooden and plastic pallets. The pallets were transported to the Site and disassembled prior to transport off-Site for recycling/re-use. In addition, Starnes Pallet allowed customers to stage used totes and drums at the Site prior to transport off-Site for recycling. The totes and drums were reportedly emptied and cleaned prior to arrival at the Site. The office building in the northwestern portion of the Site is currently unoccupied, but is used for storage of personal items by the current property owner (Starnes Commercial Properties LLC). The service garage building is occupied by a tractor trailer truck leasing and rental business. The service garage in the southern portion of the Site is used for routine maintenance and repair of the tractor trailer fleet. Remaining portions of the Site consist of asphalt paved and gravel covered parking and storage areas. Materials stored at the Site include wooden and plastic pallets, empty totes and drums, and construction materials including lumber, steel beams, toilets, sinks, hot water heaters, and other debris. The two single-family residences along Grimes Street are occupied by residential tenants. 3 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 1.2 Previous Assessment Activities H&H recently completed Phase I ESA activities at the Site and identified the following environmental concerns associated with historical on-Site and nearby off-Site operations:  The Site was formerly utilized by Commercial Equipment Co. from the early 1970s until the late 1990s. According to information provided in available environmental documents prepared for the Site, Commercial Equipment Co. utilized one 500-gallon gasoline underground storage tank (UST) as part of Site operations. According to the Site contact and information provided in available environmental documents, the gasoline UST has not been used in over 30 years but remains at the Site. H&H did not observe aboveground evidence (e.g., vent pipes, fill ports, etc.) associated with the 500-gallon tank during Site reconnaissance activities. The potential for an undocumented release associated with the gasoline UST and the potential for additional unidentified USTs at the Site was identified as a Recognized Environmental Condition (REC) in the Phase I ESA.  Review of available environmental documents indicates that a freight depot/motor line company and an auto repair facility with a paint booth operated in the western and central portions of the Site in the 1950s and 1960s. The Site is not listed in the environmental databases as a generator of hazardous wastes and there are no release incidents reported in the environmental databases associated with hazardous wastes or historical automotive repair operations at the Site. However, auto repair operations often include use of various petroleum-related products and solvents for degreasing. Additional information regarding former auto repair and freight operations was not available. Results of the Phase I ESA identified the potential for an undocumented release or releases associated with decades of historical on-Site auto repair and trucking operations as a REC in connection with the Site.  Based on information provided in available environmental documents, the 609 W. 28th Street Site building utilized an oil/water separator (OWS) system and/or waste oil UST until the 1990s. A steel pipe was observed at the ground surface near the southern corner 4 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc of the 609 W. 28th Street Site building and two floor drains were observed in the former wash bay and washdown concrete pad located along the eastern side of the 609 W. 28th Street building. Standing fluids with an oily sheen were observed within the floor drains located in the wash bay and concrete wash pad. The pipe and drains are suspected to be associated with the reported OWS and/or waste oil tank. There are no release incidents associated with the OWS drain system and/or waste oil tank and no available documentation related to routine maintenance and emptying of sub- grade components of the systems. Based on the age of the drains and OWS system/waste oil UST and the observed conditions of the drains, results of the Phase I ESA identified the potential for impact to the Site from an undocumented release associated with the floor drain and OWS system/waste oil UST system as a REC.  Information provided in the environmental databases indicates that approximately 50- gallons of diesel were released to the ground surface and contained using absorbent pads. Additional information pertaining to the surface release (Incident No. 85418) was not available in the database report or in North Carolina Department of Environmental Quality (DEQ) UST Section records. According to information provided by DEQ UST Section personnel, files associated with the release incident are designated as lost and the petroleum release incident remains open. The Site contact was unaware of the reported spill and was therefore unable to provide additional details related to the remedial effort or subsequent sampling confirming the spill was adequately addressed to levels below applicable screening criteria. Based on the lack of details associated with the remedial effort and sampling information, and the open status of the release incident, the reported on-Site surface spill was identified as a REC in the Phase I ESA. A Historical Recognized Environmental Condition (HREC) is defined as a REC which involves a past release of hazardous substances or petroleum products that has been addressed to the satisfaction of the applicable regulatory authority and is not subject to activity and/or use limitations. Results of the Phase I ESA identified the following HREC in connection with the Site: 5 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc  Commercial Equipment Company installed two 12,000-gallon diesel USTs near the southern exterior wall of the 609 W. 28th Street Site building in March 1980. Petroleum impacted soil was discovered during closure of the two diesel USTs in March 1998, and approximately 270 cubic yards of impacted soil was removed from the tank basin and stockpiled on-Site (LUST Incident No. 18731). Soil samples were collected for laboratory analysis beneath the former diesel USTs (T1-E, T2-E, T1-W, and T2-W), along product lines (PL-1, PL-4, and PL-5), and adjacent to dispensers (D-1, D-2, and D- 3). According to information provided in the environmental documents, the product piping and dispensers were not removed during closure activities in March 1998. Laboratory analytical results for soil samples collected from the UST basin indicated that total petroleum hydrocarbons as diesel range organics (TPH-DRO; up to 6,700 milligrams per kilogram {mg/kg}) and as gasoline range organics (TPH-GRO; up to 500 mg/kg) were detected at concentrations above the DEQ UST Section Residential Maximum Soil Contaminant Concentrations (MSCCs) at the time. Note that there are no current MSCCs for TPH and the current DEQ UST Section Action Levels for TPH-DRO and TPH-GRO are 100 mg/kg and 50 mg/kg, respectively. In addition to TPH, UST basin soil sample results identified the presence of several additional petroleum-related compounds including n-butylbenzene, sec-butylbenzene, naphthalene, 1,2,4- trimethylbenzene, 1,3,5-trimethylbenzene, isopropyl benzene, total xylenes, and 2- methylnaphthalene at concentrations above the DEQ UST Section Soil-to-Water MSCCs. Product line soil sample results indicated that naphthalene and 2-methyl naphthalene were detected in one sample at concentrations exceeding the Soil-to-Water MSCC. Laboratory analytical results for soil samples collected in the area near the dispensers did not identify organic compounds at concentrations above the DEQ UST Section MSCCs. In June 1998, one monitoring well (MW-1) was installed and sampled in the area of the former diesel UST basin. Soil samples collected from the monitoring well boring did not indicate the presence of compounds at concentrations above the DEQ UST Section MSCCs with the exception of C9-C10 aromatics hydrocarbon fractions which were 6 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc detected at a concentration slightly above the Soil-to-Water MSCC. Laboratory analytical results for the groundwater sample collected from the monitoring well indicated the presence of benzene, naphthalene, and C9-C22 aromatics at concentrations above the DEQ 2L Groundwater Quality Standards (2L Standards), but below the DEQ UST Section Gross Contamination Levels (GCLs). Information provided in a Limited Site Assessment (LSA) report prepared for the Site on October 23, 1998, by Altura Environmental, indicates that three additional shallow monitoring wells (MW-2, MW-3, MW-4) were installed south of the former diesel UST basin, adjacent to the product piping, and topographically downgradient of the former diesel USTs, respectively. In addition, one deeper monitoring well (MW-1A) was installed near existing well MW-1. Groundwater samples were collected for laboratory analysis from each monitoring well (MW-1 through MW-4 and MW-1A). Groundwater sample laboratory analytical results for groundwater samples collected from monitoring well MW-1 identified benzene, naphthalene, C9-C-22 aromatics, and ethylbenzene at concentrations above the 2L Standards. The compounds naphthalene and 2- methylnaphthalene were detected in deeper well MW-1A at concentrations above the 2L Standards. Petroleum-related compounds were not detected at concentrations above the laboratory reporting limits in samples collected from the remaining monitor wells. Based on results of assessment activities and risk evaluations, the DEQ UST Section assigned a low-risk designation to the incident. On November 6, 1998, the DEQ UST Section issued a No Further Action (NFA) letter providing regulatory closure for the release. Information provided in the NFA letter indicates contaminated groundwater has not been remediated to levels below the 2L Standards and is not a suitable water supply source. However, a Notice of Residual Petroleum (NORP) restricting groundwater use or other activity use limitations was not recorded on the property deed. Based on regulatory closure of the release incident without activity or land use restrictions recorded on the property deed, the release incident associated with the former diesel USTs represents an HREC in connection with the Site. 7 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc To address environmental concerns, the Site was entered into the DEQ Brownfields Redevelopment Section as a part of property transaction due diligence activities. A Brownfields Property Application was submitted to DEQ on January 12, 2022, and a Letter of Eligibility was issued for the Site by DEQ on May 24, 2022. Because the Site was entered into the Brownfields Redevelopment Section, H&H completed Phase II ESA soil, groundwater, and soil gas sampling consistent with assessment activities typically requested by DEQ Brownfields. In addition, H&H completed a receptor survey as part of the Phase II ESA activities, a brief summary of the Phase II ESA soil, groundwater, and soil gas sampling results is provided below. 2022 Phase II ESA In February 2022, H&H performed Phase II ESA activities at the Site to evaluate the potential for impacts and assist in the management of Site media during planned redevelopment activities. Assessment activities included the advancement of seven (7) soil borings near areas of concern (i.e., drains, former and suspect USTs, former dispenser islands, and an OWS/waste oil UST system), and five (5) composite soil samples were collected from shallow soil that will likely be disturbed during future redevelopment. Assessment activities also included groundwater sample collection from five (5) temporary monitoring wells installed in upgradient areas of the Site to evaluate the potential for impact from nearby off-Site properties, areas of potential concern, and in areas downgradient of the existing Site buildings. Additionally, eight (8) exterior soil gas samples and two (2) sub-slab soil gas samples were collected for laboratory analysis within or near the footprint of proposed for-rent apartment buildings to evaluate the potential for structural vapor intrusion. Although there is no known historical landfilling, dumping, waste disposal, or other operations that would result in a subsurface source of methane at the Site, subsurface methane and differential pressure measurements were collected from each exterior soil gas and sub-slab soil gas monitoring point location to minimize the potential for data gaps associated with the redevelopment of a Brownfields property for residential use. Soil, groundwater, and soil gas sample locations from the February 2022 Phase II ESA are depicted in Figure 3, and summaries of the analytical results are provided in Appendix A. 8 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Results of soil sampling activities completed in areas planned for disturbance during future grading and redevelopment on the Site did not identify organic compounds at concentrations above the DEQ Preliminary Soil Remediation Goals (PSRGs). Results of the soil assessment activities completed in the areas near the former USTs, dispenser islands, wash bay, and OWS/waste oil UST system did not identify compounds at concentrations above the DEQ PSRGs or background concentrations in the case of metals. Concentrations of arsenic (COMP-1) and lead (COMP-3) were detected at concentrations above the DEQ Residential PSRGs and regional background concentrations for metals in shallow soil that may be disturbed during redevelopment. Remaining metal concentrations detected in soil samples collected at the Site are consistent with published and established naturally occurring levels. Results of the groundwater sampling identified several organic compounds above 2L Standards and/or DEQ Vapor Intrusion Groundwater Screening Levels (GWSLs), including carbon tetrachloride, chloroform, 1,2-dichloroethane, 1-methylnaphthalene, naphthalene, tetrachloroethene (PCE), and trichloroethene (TCE). Total chromium was detected above the 2L Standard in TMW-3. Results of the soil gas assessment activities identified several compounds at concentrations above the DEQ Vapor Intrusion Sub-slab and Exterior Soil Gas Screening Levels (SGSLs). The chlorinated solvents PCE and TCE were not detected at a concentration above the DEQ Vapor Intrusion SGSLs in soil gas samples collected at the Site. Risk calculator results using compound concentrations detected in the soil gas samples indicate that the Site-wide worst-case calculated cumulative lifetime incremental carcinogenic risk (LICR) is less than the acceptable risk level of 1 x 10-4. However, the cumulative noncarcinogenic hazard index (HI) exceeds the DEQ and Environmental Protection Agency (EPA) acceptable threshold and 1.0. Risk calculator results using the compound concentrations detected in the sub-slab soil gas samples collected within the existing Site buildings did not exceed unacceptable risk thresholds under a residential use scenario. Results of the methane gas measurements identified the presence of methane up to 7.0% by 9 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc volume air (bv) in the southeastern portion of the Site (SG-5/SG-DUP), which is above the lower explosive limit (LEL) of 5% bv for methane. However, the presence of methane in the subsurface is not present at concentrations above the DEQ Brownfields Program 30% bv residential use threshold. Methane concentrations were not detected above the LEL in remaining soil gas sample locations at the Site. Pressure measurements collected at the Site are within the accuracy limits for the instrument and are not present at levels that would allow subsurface methane to migrate vertically to the surface at potentially explosive concentrations. Brownfields Activities As part of the Brownfields process, a kick-off/data gap meeting with the PD, environmental counsel for the PD, DEQ Brownfields personnel, and H&H was held on September 15, 2022, to discuss prior Site history, proposed redevelopment plans, previous sampling data, and the proposed schedule for completing the Brownfields Agreement. Based on results of previous assessment activities and discussions during the data gap/kick-off meeting, in an email dated November 16, 2022, DEQ Brownfields requested collection of additional soil samples and sub- slab soil gas samples. In addition, DEQ Brownfields Redevelopment Section requested collection of subsurface methane readings to further evaluate the extent of potential measurable subsurface methane. H&H prepared a Brownfields Assessment Work Plan (Work Plan) and revisions to the Work Plan based on DEQ Brownfields comments to address the requested additional assessment activities. The Work Plan received DEQ-approval in a letter dated March 30, 2023. This report has been prepared to document the additional soil, soil gas, and methane sampling activities completed at the request of DEQ Brownfields and in accordance with the DEQ-approved Work Plan. A summary of the Brownfields assessment sampling activities and results is provided in the sections below. 10 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 2.0 Brownfields Assessment Activities Brownfields assessment activities included collection of confirmation soil samples in the northern, central, and eastern portions of the Site where organic compounds or metals were detected in February 2022 Phase II ESA samples. Based on the size of the 609 W. 28th Street Site building (approximately 7,350 sq ft) one (1) additional sub-slab soil gas sample was collected as part of Brownfields assessment activities. Based on the proposed redevelopment plan, four (4) additional exterior soil gas samples were collected within the footprint of proposed townhome-style apartment buildings. In addition, subsurface methane and differential pressure measurements were collected from nine (9) soil gas sampling points installed in the southern portion of the Site where measurable levels of methane were identified in February 2022. Prior to conducting field activities, H&H contacted North Carolina 811, the public utility locator, to mark subsurface utilities at the Site. H&H also contracted with a private utility locator, to mark utilities which were not identified by the public locator. The private utility locator also utilized ground penetrating radar (GPR) survey techniques to identify and mark utilities at each sample location. In addition, H&H directed the drilling contractor to hand clear each boring to a depth of approximately 5 feet below the ground surface (ft bgs) to further screen the boring locations for the presence of subsurface utilities. The assessment activities described herein were performed in general accordance with the DEQ Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated Sites (Guidelines) dated September 2022, the DEQ Division of Waste Management (DWM) Vapor Intrusion Guidance (VI Guidance) dated March 2018, DEQ Brownfields Program Methane Assessment Protocol dated September 2020, the most recent versions of the U.S. Environmental Protection Agency (EPA) Region IV Laboratory Services and Applied Science Division (LSASD) guidance, the Los Angeles Department of Building Safety (LADBS) Site Testing Standards for Methane dated January 2014, the DEQ Brownfields Methane Assessment Protocols dated September 2020, and the DEQ-approved Work Plan. Brownfields assessment activities and results are provided in the following sections. 11 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 3.0 Additional Soil Assessment Activities On April 13 and 14, 2023, H&H contracted Mid South Environmental, Inc. (Mid South) to advance soil borings in areas of the Site where field screening identified volatile organic vapors measurements above background levels during Phase II ESA sampling activities and where laboratory analytical results identified lead at concentrations above background levels in a composite soil sample. Soil samples were collected for laboratory analysis at each boring location to further evaluate the potential for impact and assist in managing soil at the Site during planned redevelopment activities. The locations of the soil borings are shown in Figure 3. Soil borings were advanced utilizing a decontaminated stainless-steel hand auger, and a track-mounted direct push technology (DPT) drill rig. During boring advancement, continuous soil samples were collected from the center of the hand auger bucket or from acetate-lined macrocore sleeves. The soil samples were logged for lithologic description, observed for obvious evidence of staining and unusual odors, and field screened for the presence of volatile organic vapors using a calibrated photoionization detector (PID). H&H did not observe obvious evidence of potential impacts in the soil samples based on results of field screening. Boring logs including lithologic descriptions and field screening results for each soil boring are provided in Appendix B. A discussion of the soil sampling activities and results is provided in the following sections. 3.1 Soil Sampling Activities Confirmation Soil Sampling – Northern, Central, and Eastern Deeper Soil Confirmation soil samples were collected for laboratory analysis from previous Phase II ESA borings where field screening results indicated potential impacts as described below.  Two soil borings (BF-SB-01 and BF-SB-02) were advanced in the northern corner of the Site near Phase II ESA borings SG-1 and TMW-1. The soil borings were advanced to approximately 10 ft bgs. Based upon field observations, one soil sample was collected 12 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc from each boring location for laboratory analysis from the 5-7 ft bgs depth interval to evaluate the potential for impact at a depth greater than 2 ft bgs as requested by the DEQ Brownfields Redevelopment Section.  One soil boring (BF-SB-03) was advanced in the central portion of the Site near Phase II ESA soil gas sampling point boring SG-6. The soil boring was advanced to approximately 10 ft bgs. Based upon field observations, a sample was collected from the 4-5 ft bgs depth interval to evaluate the potential for impact at a depth greater than 2 ft bgs as requested by the DEQ Brownfields Redevelopment Section.  Two soil borings (BF-SB-04 and BF-SB-05) were advanced in the eastern portion of the Site near Phase II ESA borings SG-2 and SG-3. Soil borings were advanced to approximately 10 ft bgs. Based upon field observations, one soil sample was collected for laboratory analysis from each boring from the 2-4 ft bgs depth interval to evaluate the potential for impact at a depth greater than 2 ft bgs as requested by the DEQ Brownfields Redevelopment Section. Soil samples selected for laboratory analysis were placed in dedicated laboratory supplied sample containers, labeled with the sample identification, date, and requested analysis, and placed in a laboratory supplied cooler with ice. The samples were delivered to Pace Analytical (Pace), a North Carolina certified laboratory, under standard chain of custody protocols for laboratory analysis of volatile organic compounds (VOCs) by EPA Method 8260, semi-VOCs (SVOCs) by EPA Method 8270, Resource Conservation and Recovery Act (RCRA) metals by EPA Methods 6020/7471, and hexavalent chromium by EPA Method 7199. Composite Soil Sample – Central Shallow Soil In addition to the soil sampling described for the northern, central, and eastern portions of the Site above, six (6) shallow soil borings were advanced for the collection of soil samples in the central portion of the Site to further evaluate soil conditions near the Phase II ESA composite soil sample COMP-3 aliquot soil borings. The shallow soil boring locations (identified as COMP-3A through COMP-3F) are shown in Figure 3. 13 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc The drilling contractor advanced each soil boring with a decontaminated stainless steel hand auger and continuous soil samples were collected from the center of the hand auger bucket. Soil samples for laboratory analysis were collected from the ground surface to approximately 2 ft bgs at each boring location. The soil samples selected for laboratory analysis were collected directly into laboratory-supplied glassware, labeled with the date, time, and sample identification, and placed in a laboratory supplied sample cooler with ice. The samples were submitted to a Pace under standard chain of custody protocols for analysis of lead by EPA Method 6020. Following completion of the confirmation soil sampling activities, the soil borings were properly abandoned, and the ground surface was repaired similar to pre-drilling conditions. In addition, soil boring locations were estimated using a hand-held global positioning system (GPS) unit. 3.2 Soil Sampling Analytical Results A tabular summary of the soil sample analytical results is presented in Table 1, and copies of the laboratory analytical reports and chain of custody records are provided in Appendix C. The laboratory analytical results were compared to the most recent version of the DEQ Residential and Industrial/Commercial PSRGs dated January 2023. Metals results were compared to published concentrations for naturally occurring metals in regional soil (Dragun and Chekiri 2005) and background levels established for a nearby Brownfields property (Cotton Warehouse - Brownfields Project No. 24013-20-060). A discussion of the confirmation soil sample laboratory analytical results is provided below. Confirmation Soil Sampling – Northern, Central, and Eastern Deeper Soil Soil sample analytical results indicate that an estimated level of ethylbenzene (0.0039 J mg/kg) was detected in soil sample BF-SB-01 collected in the northern portion of the Site at a concentration above the laboratory method detection limit, but below the laboratory reporting limit (J-flag), and well below the DEQ PSRGs. Trace levels of methylene chloride (up to 0.147 C9 mg/kg), a laboratory introduced contaminant (C9 Flag), were detected at concentrations above the laboratory method detection limits in each soil confirmation soil sample. No other 14 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc organic compounds were detected at concentrations above the laboratory method detection limits in confirmation soil samples collected in the northern, central, and eastern portion of the Site. Several metals were detected in each confirmation soil sample at concentrations generally consistent with naturally occurring background levels including arsenic (up to 2.9 mg/kg), barium (up to 19.1 mg/kg), trivalent chromium (up to 146 mg/kg), hexavalent chromium (up to 0.921 J mg/kg), lead (up to 10.3 mg/kg), mercury (up to 0.13 mg/kg), and selenium (up to 1.1 mg/kg). Although generally consistent with expected background concentration, levels of concentrations of total chromium detected in the BF-SB-03 (124 mg/kg) soil sample and its duplicate soil sample BF-SB-DUP (139 mg/kg), and soil sample BF-SB-04 (147 mg/kg) exceed the Rule of 20 for toxicity characteristic of 100 mg/kg. Therefore, these samples were submitted for additional chromium analysis using Toxicity Characteristic Leaching Potential (TCLP) methods. Results of the TCLP analysis indicate that chromium was not detected at concentrations above the laboratory method detection limits in the leachate samples. Composite Soil Sampling – Central Shallow Soil Composite soil sample laboratory analytical results indicate that lead (ranging from 12.3 mg/kg to 309 mg/kg) was detected at concentrations above the laboratory method detection limits, but below the DEQ Residential PSRG of 400 mg/kg in each shallow soil sample collected in the central portion of the Site. The lead concentration detected in soil sample COMP-3E (309 mg/kg) exceeds the Rule of 20 for toxicity characteristic of 100 mg/kg. Therefore, this sample was submitted for additional lead analysis using TCLP methods. Results of the TCLP analysis indicate that lead was not detected at concentrations above the laboratory method detection limits in the leachate. 15 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 4.0 Additional Soil Gas Assessment Activities In April 2023, H&H installed and sampled four (4) temporary exterior soil gas monitoring points (SG-9 through SG-12) and one (1) temporary sub-slab soil gas sampling point (SSV-3) within or near the footprint of proposed residential buildings to further evaluate the potential for structural vapor intrusion. The exterior and sub-slab soil gas sampling point locations are shown in Figure 3. The vapor intrusion assessment activities and results are described below. 4.1 Soil Gas Sampling Activities Exterior Soil Gas Sample Point Installation Under the direction of H&H, Mid South advanced four (4) soil borings for installation of temporary exterior soil gas monitoring points (SG-9 through SG-12) within the footprint of the proposed residential buildings (Figure 3). The soil gas monitoring points were installed at depths of 7 ft bgs and above the estimated water table capillary fringe. Each soil boring was advanced using DPT drilling methods. Continuous soil samples were collected from the soil gas monitoring point borings and logged for lithologic description, observed for obvious evidence of staining and unusual odors, and field screened for the presence of volatile organic vapors using a calibrated PID. Field screening results did not indicate obvious evidence of potential impacts in the soil gas monitoring point borings. Once at target depth, a six-inch stainless steel vapor implant screen attached to a length of Teflon® tubing was installed at the base of each borehole. Filter sand was then placed within the annulus of the boring from the base of the boring to a depth of approximately 6-inches above the top of the vapor screen. The sampling points were completed by placing hydrated bentonite from the top of the filter sand to the ground surface. Boring logs including lithologic descriptions, field screening results, and soil gas monitoring point construction details are provided in Appendix B. 16 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Sub-Slab Soil Gas Sample Point Installation H&H installed one (1) sub-slab soil gas sample point (SSV-3) within the vacant office portion of the Site building located at 609 w. 28th Street (Figure 3). The sub-slab soil gas sampling point was installed using a rotary hammer drill and 1½-inch diameter drill bit to advance a pilot hole into the concrete slab to a depth of approximately 1¾ inches below the surface. A drill guide was then placed in the pilot hole and a 5/8-inch diameter drill bit was utilized to advance the boring through the concrete slab and approximately 6-inches into the underlying soil. Following concrete borehole advancement, loose concrete cuttings were removed from each boring using a bottlebrush. A Cox-Colvin Vapor Pin™ (vapor pin) assembly (brass sampling point and silicone sleeve) was then seated in the borehole using an installation/extraction tool and hammer. Upon installation of the vapor pin assembly, dedicated Teflon® sample tubing was connected to the barbed end of the sample point. Soil Gas Sampling Each exterior and sub-slab soil gas sample was collected utilizing a laboratory supplied 1.4-liter Summa® canister connected to an air-flow regulator calibrated by the laboratory to collect the soil gas sample at a rate of no greater than approximately 200 milliliters per minute (mL/min). Prior to collection of the soil gas samples, “shut-in” tests were conducted on the sampling train and helium leak checks were conducted at each sampling point. A description of the shut-in test and helium leak testing procedures is provided below. The shut-in test was conducted by connecting the flow regulator with the vacuum gauge to the Summa® canister and sealing the flow regulator with the laboratory provided brass cap. Once the sampling train was “closed”, the sample valve on the Summa® canister was opened and the reading on the vacuum gauge was recorded. The Summa® canister sample valve was then closed and the vacuum gauge was observed to ensure no vacuum loss occurred. If the vacuum reading remained the same, the shut-in test was considered successful. Shut-in tests were considered successful for each sample canister. Following successful shut-in tests, the Summa® canister was connected to the sample point via Teflon® sample tubing using a brass nut and ferrule assembly to create an air tight seal and a leak 17 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc check was performed. The leak check was performed by constructing a shroud over the sampling point and sampling train, and flooding the shroud with helium gas. Helium concentrations inside the shroud were measured using a calibrated helium gas detector and maintained at concentrations ranging from approximately 5.1% to 6.8%. Once helium concentrations stabilized within the shroud, the sample tubing was purged outside of the shroud using a syringe and a three-way valve to collect purged soil gas into a Tedlar® bag. The purged soil gas was then analyzed using the helium gas detector to ensure that helium concentrations in the soil gas sample were less than 10% of the helium concentrations measured within the shroud. Each soil gas sampling point passed the helium leak check criteria. Following successful leak checks, the soil gas samples were collected by opening the intake valve on the Summa® canister. Vacuum readings on the Summa® canister were recorded prior to and following the sampling period to ensure adequate sample volume was collected. A vacuum of approximately 5 inches of mercury or more was maintained within the canisters at the conclusion of the sampling event in accordance with DEQ DWM VI Guidance. Following sample collection, the Summa® canisters were shipped to Waypoint Analytical under standard chain of custody protocols for analysis of VOCs by EPA Method TO-15. Upon receipt of the samples, the laboratory recorded the final received vacuum pressure for each Summa® canister. After sampling was completed, the sample locations were estimated by measuring from known benchmarks within the Site building for SSV-3 and using a GPS unit for the exterior locations. The sample locations were permanently abandoned, and the surfaces were repaired similar to pre-drilling conditions. 4.2 Soil Gas Sampling Results A tabular summary of the soil gas sample analytical results is provided as Table 2, and a copy of the laboratory analytical report and chain of custody record is provided in Appendix C. The soil gas sample results were compared to DEQ Residential and Non-Residential Vapor Intrusion Sub- Slab and Exterior Soil Gas Screening Levels (SGSLs) dated January 2023. A brief summary of the exterior and sub-slab soil gas sampling results is provided below. 18 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Exterior Soil Gas Sample Results The following petroleum-related compounds were detected at concentrations above the DEQ Vapor Intrusion SGSLs in the April 2023 exterior soil gas samples collected at the Site:  Benzene (up to 148 µg/m3) was detected in soil gas samples SG-9, SG-10, and SG-12 at concentrations above the DEQ Residential SGSL of 12 µg/m3.  1,3-butadiene (up to 45.7 µg/m3) was detected in soil gas samples SG-9, SG-10, and SG- 12 at concentrations above the DEQ Residential SGSL of 3.1 µg/m3. The detected concentration in SG-10 (45.7 µg/m3) also exceeds the Non-Residential SGSL of 41 µg/m3. Note that 1,3-butadiene is commonly attributed to off gassing of rubber seals associated with DPT drilling equipment used to install the sampling points and its presence in the soil gas samples is not likely associated with soil gas conditions at the Site.  Chloroform (5.52 µg/m3) was detected in soil gas sample SG-10 at a concentration above the DEQ Residential SGSL of 4.1 µg/m3.  Ethylbenzene (up to 388 µg/m3) was detected in SG-9 through SG-12 at concentrations above the DEQ Residential SGSL of 37 µg/m3.  Naphthalene (6.26 µg/m3) was detected in soil gas sample SG-9 at a concentration above the DEQ Residential SGSL of 2.8 µg/m3.  Xylenes (up to 1,720 µg/m3) were detected in soil gas samples SG-9, SG-10, and SG-12 at concentrations above the DEQ Residential SGSL of 700 µg/m3. No other compounds, including chlorinated solvents, were detected at concentrations above the DEQ Vapor Intrusion SGSLs in the exterior soil gas samples. This is consistent with the results of Phase II ESA soil gas sampling activities completed at the Site in February 2022. Sub-Slab Soil Gas Sampling Points Laboratory analytical results indicate that several compounds were detected at concentrations above the laboratory method detection limits in the sub-slab soil gas sample collected within the 609 W. 28th Street Site building. No compounds, including chlorinated solvents, were detected at concentrations above the DEQ Vapor Intrusion SGSLs in the SSV-3 sub-slab soil gas sample. 19 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc collected from the office building. This is consistent with the results of Phase II ESA sub-slab soil gas sampling activities completed at the Site in February 2022. 4.3 Vapor Intrusion Risk Evaluation The DEQ Vapor Intrusion SGSLs are very conservative and based upon a target cancer risk (TCR) of 1 x 10-6 for potential carcinogenic effects and a target hazard quotient (THQ) of 0.2 for potential non-carcinogenic effects. Vapor intrusion mitigation or additional assessment is not typically warranted if the calculated cumulative lifetime incremental carcinogenic risk (LICR) is 1 x 10-4 or less and the acceptable level for non-carcinogenic risk is a calculated cumulative hazard index (HI) of 1.0 or less. H&H utilized the DEQ Risk Calculator (January 2023) assuming residential land use to further evaluate potential cumulative risks for the soil gas to indoor air vapor intrusion pathway. To model the potential for vapor intrusion risks under a hypothetical “worst-case” scenario, H&H conservatively calculated the cumulative risks using the highest concentration of any compound detected in any soil gas sample collected from the Site for both the February 2022 Phase II ESA and the April 2023 Brownfields assessment. Risk calculator results are summarized in the table below. A copy of the completed risk calculators is provided in Appendix D. Risk calculator results indicate that under a hypothetical worst-case scenario for the soil gas to indoor air vapor intrusion pathway for residential use, the cumulative LICR is less than the acceptable risk level of 1 x 10-4. However, the cumulative HI for residential use is greater than the acceptable risk level of 1.0. Results of assessments completed at the Site indicate that TCE has not been detected in soil or soil gas at concentrations above the laboratory method detection limit. However, a trace level of Land Use Scenario Calculated Cumulative LICR Calculated Cumulative HI Exceedance of Acceptable Levels? Residential 4.2 x 10-5 2.5 Yes 20 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc TCE (1.6 µg/L) was detected at a concentration above the laboratory method detection limit in one groundwater sample (TMW-6) collected at the Site in February 2022. Based on review of the DEQ DWM draft Minimum Mitigation and Sampling Requirements for Reuse dated February 2023 and results of assessments completed at the Site, potential vapor intrusion risks at can easily be managed through the installation of DEQ-approved passive vapor intrusion mitigation systems designed with the capability to be converted to active sub-slab depressurization systems if warranted. 21 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 5.0 Subsurface Methane Gas and Pressure Measurements Results of the February 2022 Phase II ESA identified subsurface methane gas in soil gas monitoring point SG-5 collected in southern portion of the Site near the Franklin Avenue right of way (Figure 3). Although there is no indication or reports of historical landfilling, dumping, or subsurface waste disposal at the Site, subsurface methane gas was measured in SG-5 at concentrations up to 7.0% bv, which exceeds the atmospheric LEL for methane. To confirm the presence of subsurface methane gas in the southern portion of the Site, H&H re- installed soil gas monitoring point SG-5 and collected additional subsurface methane and pressure measurements. In addition, H&H installed eight (8) additional “step-out” soil gas monitoring points (MP-A through MP-H) in each cardinal direction away from the SG-5 replacement sampling point to evaluate the extent and potential source of subsurface methane gas. The approximate locations of the monitoring points are shown on Figure 3. 5.1 Methane Gas Sampling Activities On April 16, 2023, the methane monitoring points were installed to a depth of 7 ft bgs, which is above the estimated water table capillary fringe. Monitoring point borings were advanced at each proposed location using a stainless-steel decontaminated hand auger and DPT drilling techniques. An approximate 6-inch stainless steel vapor implant screen attached to Teflon® sample tubing was then placed at the base of the borehole. The annular space around the vapor implant screen was filled with filter sand to a depth of approximately 6-inches above the vapor screen. Following installation of the sand, hydrated bentonite was installed in the boring from the top of the sand to near the ground surface. The sample tubing for each exterior monitoring point was capped using an airtight petcock valve immediately following installation to allow subsurface conditions to equilibrate. Each point was allowed to equilibrate for a minimum of 24-hours after installation and prior to the collection of field measurements in accordance with DEQ VI Guidance and the DEQ Brownfields Program Methane Assessment Protocol. After allowing for subsurface equilibration, H&H collected both 22 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc static and differential pressure readings from each monitoring point on April 17, 2023. The pressure readings were collected using a Landtec Gem 5000® and were collected prior to performing helium leak checks (described in Section 5.1 above). Note that the static pressure measurement collected from a soil gas point using the Landtec Gem 5000® instrument represents the differential pressure between the subsurface and the atmosphere. Following collection of the pressure readings, helium leaks checks were completed at each sampling point. After subsurface equilibration and successful leak checks, a Landtec Gem 5000® was connected to the sample tubing and field measurements of oxygen, carbon dioxide, carbon monoxide, hydrogen sulfide, and methane (percent by volume and percent lower explosive limit) were collected and recorded by sampling personnel. After completion of the first round of measurements, H&H capped the points with an airtight valve for a minimum of 24- hours prior to collection of a second round of subsurface landfill gas measurements on April 18, 2023. Following the second round of subsurface landfill gas measurements, the sample tubing at each sampling point was secured with an airtight valve and allowed to equilibrate for approximately two weeks. H&H returned to the Site on May 1 and 2, 2023, and collected a third and fourth round of subsurface landfill gas measurements at each sample location using the same methods described above. Following completion of the fourth round of measurements, the soil gas points were permanently abandoned, and the surfaces were repaired similar to pre-drilling conditions. In addition, the location of each sampling point was estimated using a handheld GPS unit. 5.2 Methane Gas Sampling Results The landfill gas and pressure measurements are summarized in Table 3 and copies of raw data output obtained from the Landtec Gem 5000® meter are provided in Appendix F. Methane gas poses a potential risk of explosion when present in the atmosphere or in enclosed 23 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc spaces between a LEL of 5% bv and an upper explosive limit (UEL) of 15% bv. There is no LEL for soil gas as a typical soil matrix stops propagation of flame in the subsurface preventing methane in soil gas from exploding. Therefore, the LEL at 1 atmosphere of 5% by volume air was used as a conservative comparison to detectable levels of methane in Site soil gas. In addition, the NCDEQ Brownfields Program Threshold Criteria for Methane Site Development dated December 2020 identifies 30% methane by volume air in soil gas and measurable static pressure within 200 feet of a building as residential use thresholds. Based on the proposed redevelopment, H&H used the DEQ Brownfields Program 30% methane bv in soil gas and pressure thresholds for further comparison to measurements collected at the Site. As shown in Table 3, methane was identified at measurable concentrations in each MP up to 0.6% bv. Methane was not measured at concentrations above the LEL, or the DEQ Brownfields Program 30% bv residential use screening criteria during the April or May 2023 evaluations. 5.3 Methane Vapor Intrusion Risk Evaluation As discussed above, methane gas may pose a potential risk of explosion when present in the atmosphere or enclosed spaces at levels between 5% and 15% by volume air. Soil is a flame arrestor which prevents the propagation of flame in the subsurface rendering methane in soil gas non-explosive at any concentration. Therefore, a driving mechanism (such as a pressure gradient) is needed to move methane in soil gas to the surface for there to be a potential risk of explosion. To evaluate potential risks associated with methane in soil gas, methane levels, static pressure measurements are collected concurrently at each sample interval at each sample location to evaluate subsurface to atmospheric differential pressure. Methane gas in the atmosphere has a very rapid diffusivity rate (approximately 0.22 square centimeters per second [cm2/s] at 70°F)1 as compared to a common petroleum-related compound such as benzene (approximately 0.09 cm2/s at 70°F)2. It is generally accepted that without pressure-driven advective flow created by greater than 2 inches of water differential pressure in 1 Diffusion of Methane and Chloromethanes in Air; Canadian Journal of Chemistry; M. Cowie and Harry Watts; 1971 2 https://www3.epa.gov/ceampubl/learn2model/part-two/onsite/estdiffusion.html 24 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc the subsurface, the rate of methane gas diffusion is too rapid for large volumes of methane in soil gas to reach the surface at potentially explosive levels (Proposed Regulatory Framework for Evaluating the Methane Hazard due to Vapor Intrusion; Bart Eklund; 2011). As noted above, the static pressure as measured by the Landtec Gem 5000® is the pressure reading at the screened interval relative to ambient air at the instrument station. A positive static pressure reading indicates that subsurface pressure is higher than the ambient pressure at the instrument and is the differential pressure measurement used to evaluate the presence of increased subsurface pressure. Based on information provided by the manufacturer, which is provided as a supporting document in Appendix F, the accuracy of the GEM meter is +/- 2 in H2O for static pressure which is consistent with the generally accepted differential pressure needed to drive methane in the subsurface to the surface at potentially explosive levels. Results of differential pressure measurements did not identify pressure in the subsurface above the accuracy limits of the instrument. Based on the results of the methane screening activities, methane gas in the subsurface is not present at levels that may pose a potential explosion risk and Site-wide static pressure is not present at levels above the accuracy threshold of the instrument and do not pose a significant concern for the Site as a whole. In accordance with the NCDEQ Brownfields Program Threshold Criteria for Methane Site Development, the negligible static pressure levels measured at the Site within 200 feet of the proposed building are acceptable for residential use. In addition, methane in soil gas is not present at levels above the DEQ Brownfields 30% methane by volume air in soil gas residential use threshold. Therefore, results of the assessment activities confirm that subsurface methane gas does not pose a potential risk at the Site and methane mitigation of the proposed Site buildings is not warranted. 25 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 6.0 Quality Assurance – Quality Control For quality assurance and quality control purposes (QA/QC), non-dedicated equipment and tools were decontaminated prior to use at each boring or sampling location or following exposure to soil and groundwater. Field QA/QC samples were analyzed along with the investigative samples to determine potential variability introduced in sampling, handling, shipping, and analysis. H&H collected duplicate soil and soil gas samples to evaluate the ability of the laboratory to reproduce sample results. Duplicate samples were submitted to the laboratory for the same analysis as the corresponding parent sample. 6.1 Field Duplicates Duplicate samples were collected to evaluate the precision of the field sampling procedures, sample matrix variability, and analytical reproducibility. Duplicate soil and groundwater samples were collected directly into individual laboratory supplied sample containers using sampling methodologies described in previous sections. The duplicate soil gas sample was collected concurrently with the parent sample using a laboratory supplied T-fitting which allows for collection of two soil gas samples from one soil gas sampling point simultaneously. The samples were analyzed for the same parameters as the parent samples, and the analytical results were compared with those of the parent sample. The analytical results of the parent sample and the duplicate sample were used to evaluate the cumulative precision of the analytical method, sample matrix, and sample collection techniques. H&H also collected confirmation methane and pressure measurements at sample location MP-B as part of each round of sampling. The confirmation gas and pressure measurements were collected approximately 10 minutes after collection of the parent measurements. Without an extensive sub-surface investigation to monitor sub-surface pressure changes over time, H&H cannot definitively calculate or model decreases in soil gas concentrations and pressure over a 10-minute time interval following collection of the parent measurement. The measurement collection process does not include removal of significant volumes of air. Therefore, the confirmation sample results were used to validate the parent sample results. 26 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Duplicate sample laboratory analytical results for each sample media are presented in the summary tables (Table 1 for soil, Table 2 for soil gas, and Table 3 for methane and pressure measurements). Review of the duplicate sample results in comparison to the parent sample results indicate that the duplicate samples had acceptable reproducibility. 27 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc 7.0 Summary and Conclusions H&H completed Brownfields assessment activities at Commercial Equipment Company Brownfields property located at N. Graham Street and W. 28th Street in Charlotte, Mecklenburg County, North Carolina. The Site is located in a rapidly densifying area surrounding Camp North End and in close proximity to uptown Charlotte. Brownfields assessment activities included the collection of soil and soil gas samples for laboratory analysis to evaluate the potential for impacts at the Site associated with historical on-Site and nearby off-Site operations and to evaluate risks associated with proposed redevelopment of the Site. H&H also collected subsurface methane gas and pressure measurements at the Site to evaluate the potential presence of a subsurface methane source. A brief summary of the assessment activities is provided below. Soil Soil sample analytical results indicate that no organic compounds were detected at concentrations above the DEQ Residential PSRGs in soil samples collected in areas where volatile organic vapors were identified at levels above background in select February 2022 Phase II ESA soil borings. Several metals were detected at concentrations generally consistent with background levels in soil samples collected at the Site. Total chromium concentrations exceeded the Rule of 20 for toxicity characteristic in two soil sample locations. However, the results of TCLP analysis indicate that chromium was not detected in the leachate at concentrations above the laboratory method detection limits. Lead was detected at concentrations consistent with background levels in five of the six shallow soil samples collected at February 2022 Phase II ESA composite soil sample COMP-3 aliquot boring locations. The lead concentration detected in the COMP-3E soil sample is below the DEQ Residential PSRG but exceeds the Rule of 20 for toxicity characteristics. Results of TCLP analysis indicate that lead was not detected at concentrations above the laboratory method detection limit in the COMP-3E leachate. 28 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Soil Gas Results of the exterior soil gas sampling activities identified several petroleum-related compounds at concentrations above the DEQ Vapor Intrusion SGSLs. No compounds were detected at concentration above the DEQ Vapor Intrusion SGSLs in the sub-slab soil gas samples collected within the 609 W. 28th Street Site building. Please note that the chlorinated solvents PCE and TCE were not detected at a concentration above the DEQ Vapor Intrusion SGSLs in soil gas samples collected at the Site. This is consistent with the results of Phase II ESA soil gas sampling activities completed at the Site in February 2022. To further evaluate potential vapor intrusion risks for the proposed Site buildings, H&H utilized the DEQ Risk Calculator (January 2023) assuming residential land use scenario for the soil gas to indoor air vapor intrusion pathway. Hypothetical worst-case risk calculations included the highest concentration of any compound detected in any soil gas sample collected at the Site during any sampling event (both February 2022 and April 2023). Risk calculator results indicate that under a hypothetical worst-case scenario for the soil gas to indoor air vapor intrusion pathway for residential use, the cumulative LICR is less than the acceptable risk level of 1 x 10-4. However, the cumulative HI (2.5) for residential use is greater than the acceptable risk level (1.0). Methane Gas Sampling H&H installed and collected subsurface landfill gas measurement from a cluster of ten soil gas points installed in the southern portion of the Site where low levels of subsurface methane gas were detected slightly above the atmospheric LEL near the Franklin Avenue right of way. Subsurface landfill gas measurements were collected from each sampling point on April 17 and 18 and again on May 1 and 2. Results of the methane gas measurements identified trace levels (up to 0.6% bv) of methane at concentrations well below the atmospheric LEL and the DEQ Brownfields thresholds for residential use and methane mitigation. Pressure measurements collected at the Site are within the accuracy limits for the instrument and are not present at levels that would allow for subsurface methane to migrate vertically to the surface at potentially explosive concentrations. 29 https://harthick.sharepoint.com/sites/masterfiles-1/shared documents/aaa-master projects/abacus capital (abs)/w. 28th and n.graham assembly/brownfields/bf assessment/final/26002 - brownfields assessment report_commercial equipment company.doc Based on results of the supplemental subsurface landfill gas evaluation, the presence of methane in Phase II ESA sampling point SG-5 is considered to be anomalous and it likely attributable to intermittent off gassing of utilities located in the nearby Franklin Avenue right of way Summary Results of soil sampling activities indicate that soil disturbed during planned redevelopment can easily be managed in accordance with a DEQ-approved Environmental Management Plan. In addition, potential vapor intrusion risks posed by petroleum related compounds detected in soil gas at the Site can easily be managed through the installation of DEQ-approved passive vapor intrusion mitigation systems designed to have the capability to be converted to active sub-slab depressurization systems if warranted. Subsurface methane gas measurements collected in April and May 2023 confirm that there is not an on-Site source generating methane at concentrations that would pose a risk for the proposed residential redevelopment and methane mitigation is not warranted. Table 1 Summary of Soil Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation AreaSample IDBF-SB-01 BF-SB-02 BF-SB-04 BF-SB-05Date4/14/2023 4/14/2023 4/14/2023 4/14/2023Depth (ft bgs)5-7 5-7 2-4 2-4Sample Type Grab Grab Grab Grab UnitsVOCs (8260D)Ethylbenzene0.0039 J<0.0046<0.0043<0.0040<0.0041<0.00296.127------Methylene chloride0.112 C90.119 C90.145 C90.147 C90.137 C90.140 C958650------SVOCs (8270E)ALL BDLALL BDLALL BDLALL BDLALL BDLALL BDL----------Metals (6020B/7471B/7199)Arsenic2.22.12.42.92.42.10.683.0--1.0 - 181.1 - 3.0Barium19.113.211.513.611.812.03,10047,000--50 - 1,000 38 - 110Cadmium <0.039<0.037<0.039<0.038<0.038<0.0351.420--1.0 - 10 ND - 0.36 JChromium (total)45.247.712413914715.2NENE--7.0 - 30014 - 45Chromium (VI)0.819 J 0.921 J0.726 J0.733 J0.734 J<0.3140.316.5--NS0.34 J - 0.98 JChromium (III)44.446.812313814615.223,000350,000--NS13.7 - 44.0Lead7.84.99.110.37.37.1400800--ND - 5011 - 36Mercury0.0390.021 J0.0840.110.130.022 J4.770--0.03 - 0.52 0.024 J - 0.097 Selenium0.981.10.700.820.650.54 J781,200--<0.1 - 0.8NDSilver<0.27<0.26<0.27<0.27<0.26<0.24781,200--ND - 5.0 0.033 J - 0.60Metals (6010D TCLP)ChromiumNA NA <0.0043 mg/L <0.0043 mg/L <0.0043NA----5 mg/L----LeadNANANANANANA----5 mg/L----Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.2) Environmental Protection Agency (EPA) Maximum Concentrations of Contaminants for Toxicity Characteristics Leaching Procedure (TCLP) dated November 2004. 3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005; Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils.4) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060). Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface; mg/L= milligrams per liter; NA = not analyzedNS = not specified; NE = not established; -- = not applicable; BDL = below laboratory method detection limitC9 = Common laboratory introduced contaminant.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. BF-SB-03/BF-SB-DUP4/14/20234-5Screening Criteria Background MetalsPublished Range (3)Local Range (4)Northern Corner Eastern Portion Central Portion Residential PSRGs (1)Industrial/ Commercial PSRGs (1)Maximum Concentration for TCLP (2)Grab mg/kghttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Brownfields/BF Assessment/Tables/Data TablesTable 1 (Page 1 of 2)Hart & Hickman, PC Table 1 Summary of Soil Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation AreaSample IDCOMP-3A COMP-3B COMP-3C COMP-3D COMP-3E COMP-3FDate4/13/2023 4/13/2023 4/13/2023 4/13/2023 4/13/2023 4/13/2023Depth (ft bgs)0.5-2 0.5-2 0.5-2 0.5-2 0.5-2 0.5-2Sample Type Grab Grab Grab Grab Grab GrabUnitsVOCs (8260D)EthylbenzeneNA NA NA NA NA NA6.1 27-- -- --Methylene chlorideNANANANANANA58650------SVOCs (8270E)ALL BDLALL BDLALL BDLALL BDLALL BDLALL BDL----------Metals (6020B/7471B/7199)ArsenicNA NA NA NA NA NA0.68 3.0--1.0 - 181.1 - 3.0BariumNANANANANANA3,10047,000--50 - 1,000 38 - 110Cadmium NANANANANANA1.420--1.0 - 10 ND - 0.36 JChromium (total)NANANANANANANENE--7.0 - 30014 - 45Chromium (VI)NANANANANANA0.316.5--NS0.34 J - 0.98 JChromium (III)NANANANANANA23,000350,000--NS13.7 - 44.0Lead23.644.920.253.530912.3400800--ND - 5011 - 36MercuryNANANANANANA4.770--0.03 - 0.52 0.024 J - 0.097 SeleniumNANANANANANA781,200--<0.1 - 0.8NDSilverNANANANANANA781,200--ND - 5.0 0.033 J - 0.60Metals (6010D TCLP)ChromiumNA NA NA NA NA NA-- --5 mg/L-- --LeadNANANANA<0.0010NA----5 mg/L----Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated January 2023.2) Environmental Protection Agency (EPA) Maximum Concentrations of Contaminants for Toxicity Characteristics Leaching Procedure (TCLP) dated November 2004. 3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005; Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils.4) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060). Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface; mg/L= milligrams per liter; NA = not analyzedNS = not specified; NE = not established; -- = not applicable; BDL = below laboratory method detection limitC9 = Common laboratory introduced contaminant.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. Screening Criteria Background MetalsPublished Range (3)Local Range (4)Maximum Concentration for TCLP (2)Residential PSRGs (1)Industrial/ Commercial PSRGs (1)Western Portion of the Site mg/kghttps://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Brownfields/BF Assessment/Tables/Data TablesTable 1 (Page 2 of 2)Hart & Hickman, PC Table 2Summary of Soil Gas Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation AreaSample IDSG-9 SG-10 SG-11 SG-12Sample Date4/17/2023 4/17/2023 4/17/2023 4/17/2023Sample Type UnitsVOCs (TO-15)Acetone8.35 2.66 J24.120.617.58.67NENEBenzene3.193.321481466.24118121601,3-Butadiene<0.328<0.32836.945.71.256.193.1 41Carbon Disulfide1.30 J1.00 J11026219.01404,90061,000Chlorobenzene<0.107<0.1071.70 J<0.107<0.107<0.1073504,400Chloroethane<0.164<0.1642.973.30<0.164<0.16470,000880,000Chloroform<0.086<0.086<0.0865.52<0.0861.07 J4.153Chloromethane<0.067<0.067<0.0674.44<0.067<0.0676307,900Cyclohexane<0.161<0.16115.718.14.6116.142,000530,000Dichlorodifluoromethane2.921.61 J2.613.393.631.53 J7008,800Ethylbenzene0.694 J0.616 J38824938.4336374904-Ethyltoluene<0.128<0.12878.659.313.257.0NENE1,1,2-Trichlorotrifluoroethane19.717.61.26 J10.20.574 J<0.56135,000440,000n-Heptane0.745 J0.590 J93.61097.3562.52,80035,000n-Hexane1.57 J1.44 J33029732.224.64,90061,000Isopropyl Alcohol0.609 J<0.1393.21 JB0.916 J1.79 J<0.1391,40018,0002-Butanone (MEK)1.08 J<0.2246.045.051.581.7835,000440,0004-Methyl-2-pentanone (MIBK)<0.121<0.12116.39.321.90 J7.1121,000260,000Methylene Chloride<0.488<0.4883.41<0.488<0.488<0.4883,40053,000Naphthalene1.42 J<0.1836.261.44 J1.12 J<0.1832.836Propylene<0.242<0.2422731,25036.258.521,000260,000Styrene3.133.1340.2314.2315.3700088,000Tetrachloroethene20.919.72.22 J5.1115.72.56 J2803,500Tetrahydrofuran0.345 J0.297 J<0.1075.390.451 J<0.10714,000180,000Toluene6.216.012,7001,8201181,82035,000440,000Trichloroethene1.47 J1.77 J<0.199<0.199<0.199<0.19914180Trichlorofluoromethane<0.130<0.1302.53 J<0.130<0.1303.10NENE1,2,4-Trimethylbenzene3.963.8015894.421.71184205,3001,3,5-Trimethylbenzene<0.236<0.23686.262.86.4982.94205,300Vinyl chloride<0.127<0.1274.184.58<0.1270.784 J5.6280Xylene (total)4.18 J3.97 J1,7201,0101661,7107008,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated January 2023.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses. Only compounds detected in at least one sample are shown in the above table.Bold values exceed the Residential Vapor Intrusion SGSL. Underlined values indicate an exceedance of Non-Residential SGSL. VOCs = volatile organic compounds; NE = not establishedB = Analyte detected in laboratory blank.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. µg/m3SSV-3/SSV-DUP609 W. 28th Street Proposed Residential Building 4/17/2023Exterior Soil Gas Sub-Slab Soil GasScreening CriteriaResidential SGSLs (1)Non-Residential SGSLs (1)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Brownfields/BF Assessment/Tables/Data Tables6/2/2023Table 2 (Page 1 of 1)Hart & Hickman, PC Table 3Summary of Subsurface Methane Gas MeasurementsCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003% % LELBarometric (in. Hg)Static (in. H₂O)4/17/2023 11:32 21.20.10.00.00.12.029.06 -17.934/18/2023 15:16 20.90.0 0.0001 0.00.612.0 29.20 -17.615/1/2023 9:5720.00.40.00.00.12.028.77 -0.255/2/2023 13:02 18.61.00.00.00.12.028.77 -1.264/17/2023 9:2813.10.1 0.0049 0.00.510.0 29.01 0.014/18/2023 13:41 19.10.00.00.00.24.029.20 -0.035/1/2023 10:15 20.50.10.00.00.12.028.78 0.025/2/2023 13:27 19.50.00.00.00.00.028.79 -2.434/17/2023 9:3813.10.1 0.0045 0.00.510.0 29.02 0.014/18/2023 13:54 20.00.00.00.00.36.029.22 -8.115/1/2023 10:40 20.50.10.00.00.12.028.78 -0.635/2/2023 13:52 19.90.10.00.00.00.028.82 -0.164/17/2023 11:06 21.50.10.00.00.12.029.05 0.374/18/2023 14:58 21.10.2 0.0001 0.00.510.0 29.20 -1.015/1/2023 10:29 19.31.20.00.00.00.028.80 -0.095/2/2023 13:39 18.01.70.00.00.00.028.82 -1.084/17/2023 11:25 16.30.3 0.0001 0.00.24.029.01 0.154/18/2023 14:40 12.20.1 0.0004 0.00.612.0 29.23 -2.495/1/2023 10:54 17.90.90.00.00.00.028.80 0.135/2/2023 14:04 17.81.80.00.00.00.028.83 -2.154/17/2023 9:5919.20.3 0.0001 0.00.00.029.04 -0.024/18/2023 13:51 17.10.2 0.0009 0.00.24.029.21 0.015/1/2023 11:26 19.50.90.00.00.00.028.82 -15.305/2/2023 14:46 19.51.50.00.00.12.028.72 -1.984/17/2023 13:07 21.20.10.00.00.12.029.03 0.044/18/2023 14:06 19.40.3 0.0001 0.00.36.029.23 -8.645/1/2023 11:45 15.82.10.00.00.00.028.85 0.255/2/2023 15:04 19.62.10.00.00.00.028.81 -4.564/17/2023 10:441.30.00.00.00.00.029.03 -0.024/18/2023 14:151.20.00.00.00.612.0 29.23 0.195/1/2023 11:56 14.50.10.00.00.00.028.85 -0.085/2/2023 15:20 19.50.10.00.00.00.028.80 -0.134/17/2023 10:592.40.90.00.00.00.029.03 -0.124/18/2023 14:241.61.50.00.00.48.029.23 0.035/1/2023 12:093.47.50.00.00.00.028.85 0.005/2/2023 15:293.65.70.00.00.00.028.81 0.034/17/2023 11:18 18.40.20.00.00.24.029.05 0.034/18/2023 14:33 19.40.1 0.0001 0.00.510.0 29.23 -34.665/1/2023 11:07 17.60.10.00.00.00.028.84 0.025/2/2023 14:20 19.20.10.00.00.00.028.57 -2.95Notes:Measurements were collected by H&H using a calibrated Landtec GEM 5000. * MP-DUP collected at monitoring point MP-B. MP-DUP is identified as DUP10000 in the raw data set. Positive static pressure values indicate that subsurface pressure is greater than ambient air pressure. LEL = lower explosive limit; O2= oxygen; CO2 = carbon dioxide; CO = carbon monoxideH2S = hydrogen sulfide; in H₂O = inches of water; % = percent by volume of air; in. Hg = inches of mercury H2S (%)CO2 (%)MP-AMP-HMP-GMP-FMP-EMP-DMP-CMP-DUP* MP-BSG-5Methane PressureSample ID Sample DateCO (%)O2 (%)Sample Timehttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Brownfields/BF Assessment/Methane/Methane_Tables6/2/2023Table 3 (Page 1 of 1)Hart & Hickman, PC USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S. Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed August, 2021. SITE LOCATION MAP COMMERCIAL EQUIPMENT COMPANY N.GRAHAM STREET AND W. 28TH STREETCHARLOTTE, NORTH CAROLINA DATE: 5-23-2023 JOB NO: ABS-003 REVISION NO: 0 FIGURE. 1 2923 South Tryon Street - Suite 100 Charlotte, North Carolina 28203 704-586-0007 (p) 704-586-0373 (f) License # C-1269 / # C-245 Geology TITLE PROJECT 0 2,000 4,000 SCALE IN FEET Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\ABS-003\Figure 1.mxdN U.S.G.S. QUADRANGLE MAP CHARLOTTE EAST, NORTH CAROLINA 2013 DERITA, NORTH CAROLINA 2013 QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC) SITE REVISION NO. 0 JOB NO. ABS-003 DATE: 5-23-23 FIGURE NO. 2 COMMERCIAL EQUIPMENT COMPANY N. GRAHAM STREET AND W. 28TH STREET CHARLOTTE, NORTH CAROLINA SITE MAP LEGEND BROWNFIELDS PROPERTY BOUNDARY PARCEL BOUNDARY ELEVATOR POTENTIAL GASOLINE UST POTENTIAL OIL/WATER SEPARATOR/WASTE OIL UST FORMER DIESEL UST VENT PIPE FLOOR DRAIN 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology NOTES: 1. PARCEL DATA AND AERIAL IMAGERY OBTAINED FROMMECKLENBURG COUNTY GIS, 2023. 2. UST = UNDERGROUND STORAGE TANK PEP BOYS DISTRIBUTION CENTER(700 W. 28TH STREET) FIRE STATION NO. 11 & FIRE DEPARTMENT MAINTENANCE SHOP(620 W. 28TH STREET) EASY BUILDING SUPPLIES(600 W. 28TH STREET) ASHLEY SLING, INC.(2401 N. GRAHAM STREET) MCGRANT TAX & BOOKING(2336 N. GRAHAM STREET) FRA N K L I N A V E N U E W. 2 8 T H S T R E E TN. GRAHAM STREETGRIMES STREETBANCROFT STREETBANCROFT STREETSTORAGE(2402/2426 N. GRAHAM STREET) RESIDENCE(2415 GRIMES STREET) OFFICES(609 W. 28TH STREET) EQUIPMENTSTORAGE PALLET AND CONSTRUCTION MATERIALSSTORAGE PALLET AND PLASTIC TOTE STORAGE TRUCK/TRAILERPARKING TRUCK/TRAILERPARKING FORMERDISPENSER ISLAND TRUCK REPAIR RESIDENTIAL FORMERWASH BAY RESIDENCE(2409 GRIMES STREET)S:\AAA-Master Projects\Abacus Capital (ABS)\W. 28th and N.Graham Assembly\Brownfields\EMP\Figures\Site Map_23523.dwg, FIG 2, 5/23/2023 1:05:53 PM, kmckinney SSV-2 SG-8 SG-7 SG-1 SG-2 SG-3 SG-4SG-5 SB-1 SB-2 SB-3 SB-5SB-6 COMP-2 COMP-1 COMP-5 COMP-4 SB-4 TMW-1 TMW-2 TMW-3 TMW-5 TMW-4 TMW-6/SB-7 SSV-1 A B C D E A A A A B B B B C C C C D D D E E E E F SG-5 BF-SB-5 BF-SB-4 BF-SB-2 BF-SB-1 SSV-3 COMP-3A COMP-3B COMP-3C COMP-3E COMP-3F SG-12 SG-10 SG-9 SG-11 MP-C MP-H MP-E MP-B MP-A MP-D MP-G MP-F SG-6 COMP-3 D BF-SB-3 COMP-3D SB-5 SG-5B SG-5 MP-C MP-B MP-A MP-D MP-E MP-H MP-G MP-F COMP-4 TMW-5 TMW-6/SB-7 B C D REVISION NO. 0 JOB NO. ABS-003 DATE: 5-23-23 FIGURE NO. 3 SAMPLE LOCATION MAP LEGEND FROWNFIELDS PROPERTY BOUNDARY PARCEL BOUNDARY POTENTIAL GASOLINE UST POTENTIAL OIL/WATER SEPARATOR/ WASTE OIL UST FORMER DIESEL UST VENT PIPE FLOOR DRAIN EXISTING BUILDING PROPOSED RESIDENTIAL BUILDING PROPOSED TOWNHOME STYLEAPARTMENT PREVIOUS TEMPORARY MONITORINGWELL PREVIOUS SOIL BORING PREVIOUS CO-LOCATED TEMPORARYMONITORING WELL/SOIL BORING PREVIOUS ALIQUOT SOIL BORING PREVIOUS SOIL GAS POINT PREVIOUS SUB-SLAB SOIL GAS POINT SOIL BORING LOCATION SUB-SLAB SOIL GAS POINT SOIL GAS POINT SUBSURFACE METHANE MONITORINGPOINT 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology NOTES: 1. PARCEL DATA OBTAINED FROM MECKLENBURG COUNTYGIS, 2023. 2. UST = UNDERGROUND STORAGE TANK EASY BUILDING SUPPLIES(600 W. 28TH STREET) FRA N K L I N A V E N U E W. 2 8 T H S T R E E TN. GRAHAM STREETGRIMES STREETBANCROFT STREETBANCROFT STREETSTORAGE(2402/2426 N. GRAHAM STREET) RESIDENCE(2415 GRIMES STREET) OFFICES(609 W. 28TH STREET) FORMERDISPENSER ISLAND TRUCK REPAIR FORMERWASH BAY RESIDENCE(2409 GRIMES STREET) COMMERCIAL EQUIPMENT COMPANY N.GRAHAM STREET AND W. 28TH STREET CHARLOTTE, NORTH CAROLINA PROPOSED AMENITY AREA S:\AAA-Master Projects\Abacus Capital (ABS)\W. 28th and N.Graham Assembly\Brownfields\EMP\Figures\Site Map_23523.dwg, FIG 3, 5/23/2023 1:06:15 PM, kmckinney Appendix A February 2022 Phase II ESA Data Table 1 Summary of Soil Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation AreaPotential USTSample IDCOMP-1 COMP-2 COMP-3 COMP-5 SB-1 SB-2 SB-3Date2/7/20222/9/2022Depth (ft bgs)0-2 0-2 0-2 0-2 0-2 0-2 0-2 10-12 8-10Sample Type Range Mean Range Mean UnitsVOCs (8260D)Acetone<0.0510 <0.0423 <0.0555 <0.0970 <0.0796 <0.0503 <0.0401 <0.0561 <0.049914,000 210,000-- -- -- -- --n-Butylbenzene<0.0038 <0.0031 <0.0041 <0.0071 <0.0059 <0.0037 <0.0029 <0.0041 <0.0037780 12,000-- -- -- -- --sec-Butylbenzene<0.0035 <0.0029 <0.0038 <0.0066 <0.0055 <0.0034 <0.0027 <0.0038 <0.00341600 23,000-- -- -- -- --2-Chlorotoluene<0.0028 <0.0023 <0.0031 <0.0053 <0.0044 <0.0028 <0.0022 <0.0031 <0.0028310 4,700-- -- -- -- --Ethylbenzene 0.0111 0.0041 J 0.0053 J<0.0070 <0.00580.0043 J<0.0029 <0.0041 <0.00366.1 27-- -- -- -- --Isopropylbenzene (cumene)<0.0027 <0.0022 <0.0029 <0.0051 <0.0042 <0.0027 <0.0021 <0.0030 <0.0026410 2,100-- -- -- -- --Methylene chloride 0.0528<0.0181 <0.0237 <0.0414 <0.0340 <0.0214 <0.0171 <0.0239 <0.021358 650-- -- -- -- --Naphthalene<0.0042 <0.0035 <0.0045 <0.0079 <0.0065 <0.0041 <0.0033 <0.0046 <0.00412.1 8.8-- -- -- -- --n-Propylbenzene<0.0028 <0.0023 <0.0031 <0.0054 <0.0044 <0.0028 <0.0022 <0.0031 <0.0028780 5,100-- -- -- -- --Tetrachloroethene<0.0025 <0.0021 <0.0027 <0.0048 <0.0039 <0.00285 <0.0020 <0.0028 <0.002517 82-- -- -- -- --Toluene 0.0087<0.0019 <0.0025 <0.0043 <0.0035 <0.0022 <0.0018 <0.0025 <0.0022990 9,700-- -- -- -- --1,2,4-Trimethylbenzene 0.0095<0.0018 <0.0024 <0.0041 <0.0034 <0.0021 <0.0017 <0.0024 <0.002163 370-- -- -- -- --m&p-Xylene 0.0423 0.0088 J<0.0059 <0.0103 <0.0085 <0.0054 <0.0043 <0.0060 <0.0053120 520-- -- -- -- --o-Xylene 0.0108<0.0029 <0.0038 <0.0067 <0.0055 <0.0035 <0.0028 <0.0039 <0.0034140 590-- -- -- -- --Xylene (Total)0.05300.0088 J<0.0049<0.0086<0.0071<0.0045<0.0036<0.0050<0.0044120530SVOCs (8270E)Benzo(b)fluoranthene<0.147<0.128<0.1440.216 J<0.151 <0.140 <0.128 <0.151 <0.1461.1 21-- -- -- -- --Chrysene<0.160<0.140<0.1580.174 J<0.165 <0.152 <0.140 <0.165 <0.159110 2,100-- -- -- -- --bis(2-Ethylhexyl)phthalate<0.171<0.149<0.168 <0.179 <0.176 <0.163 <0.149 <0.176 <0.17039160----------Fluoranthene<0.151<0.132<01480.245 J<0.155<0.144<0.132<0.155<0.1504806,000----------1-Methylnaphthalene<0.155<0.135<0.152<0.162<0.159<0.147<0.135<0.159<0.1541873----------2-Methylnaphthalene<0.176<0.157<0.173<0.184<0.181<0.168<0.154<0.181<0.17548600----------Phenanthrene<0.144<0.126<0.142<0.151<0.148<0.137<0.126<0.148<0.143NENE----------Pyrene<0.179<0.156<0.1760.245 J<0.184<0.170<0.156<0.184<0.1783604,500----------Metals (6020B/7471B/7199)Arsenic242.92.6 3.4 4.2 1.9 2.6 1.2 1.60.68 3.0--1.0 - 184.81.1 - 3.02.3Barium18070 MS-1159064541410014283,10047,000--50 - 1,00035638 - 11074Cadmium 0.16 J0.15 J1.8<0.062<0.0610.22 J0.13 J<0.0630.14 J1.420--1.0 - 10 4.3ND - 0.36 J0.13Chromium (total)7737 MS-1140536755561333NENE--7.0 - 3006514 - 4531.3Chromium (VI)0.42 J0.09 J0.24 J0.36 J0.35 J0.17 J0.29 J0.35 J0.660.316.5--NSNS0.34 J - 0.98 J 0.62Chromium (III)76.5836.9139.7152.6466.6554.8355.7112.6532.3423,000350,000--NSNS13.7 - 44.030.7Lead682599025196.916129.1400800--ND - 501611 - 3620.7Mercury0.0340.0340.0820.0510.0370.130.034 J0.019 J0.029 J4.770--0.03 - 0.520.121 0.024 J - 0.097 0.074Selenium0.49 J0.53 J0.60 J0.45 J0.440.55 J0.60 J<0.350.62 J781,200--<0.1 - 0.80.42NDNDSilver0.13 0.045 R-04, J 0.500.098 J0.11<0.0180.045 J<0.018<0.018781,200--ND - 5.0NS0.033 J - 0.60 0.60Metals (6010D TCLP)ChromiumNA NA NA NA NA NA NA NA NA-- --5 mg/L-- -- -- --LeadNA NA <0.19 mg/L NA NA NA NA NA NA-- --5 mg/L-- -- -- --Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.2) Environmental Protection Agency (EPA) Maximum Concentrations of Contaminants for Toxicity Characteristics Leaching Procedure (TCLP) regulatory level dated November 2004. 3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005; Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils.4) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060). Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Composite soil samples that were analyzed for VOCs were collected from undisturbed portions of soil and placed directly into laboratory supplied glassware.Bold values exceed the Residential PSRGs and background levels in the case of metals. Underlined values exceed the Industrial/Commercial PSRGs and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; UST = underground storage tank; ft bgs= feet below ground surface; mg/L= milligrams per liter; NS = not specified; NE = not established; -- = not applicable MS-11 = Matrix spike recovery outside of control limits. Possibility of sample matrix effects that lead to a high bias for reported result or non-homogeneous sample aliquots cannot be eliminated.R-04 = Duplicate relative percent difference is less useful indicator of sample precision for sample results that are <5 times the reporting limit.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. mg/kgCOMP-4/COMP-DUPResidential PSRGs (1)Industrial/ Commercial PSRGs (1)Maximum Concentration for TCLP (2)Background Metals in Nearby Brownfield Properties (4)CompositeGrab2/10/2022Western Portion of the Site Eastern Portion of the Site Former Dispenser IslandScreening Criteria2/7/2022 2/10/2022Regional Background Metals in Soil (3)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Phase II ESA/Tables/Data Tables.xlsxTable 1 (Page 1 of 2)Hart & Hickman, PC Table 1 Summary of Soil Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation AreaOWSSample IDSB-5 SB-6DateDepth (ft bgs)12-14 12-14Sample Type Range Mean Range Mean UnitsVOCs (8260D)Acetone<0.504 <0.0581 <0.0560 <0.06340.0676 J 0.0714 J14,000210,000----------n-Butylbenzene<0.0037<0.0043<0.0041<0.00470.01660.072878012,000----------sec-Butylbenzene<0.0035<0.0040<0.0038<0.00430.01180.0555160023,000----------2-Chlorotoluene<0.0028<0.0032<0.00310.0056 J<0.00360.0071 J3104,700----------Ethylbenzene<0.0037<0.0042<0.0041<0.00460.01590.03246.127----------Isopropylbenzene (cumene)<0.0027<0.0031<0.0030<0.00340.0059 J0.02174102,100----------Methylene chloride<0.0215<0.0248<0.0239<0.02710.0452<0.029658650----------Naphthalene<0.0041<0.0048<0.0046<0.00520.1110.3902.18.8----------n-Propylbenzene<0.0028<0.0032<0.0031<0.00350.0110.04627805,100----------Tetrachloroethene<0.0025<0.00290.0177<0.00310.01790.08351782----------Toluene<0.0022<0.0026<0.0025<0.00280.0082 J<0.00319909,700----------1,2,4-Trimethylbenzene<0.0021<0.0025<0.0024<0.00270.02310.11663370----------m&p-Xylene<0.0054<0.0062<0.0060<0.0068<0.0070<0.0074120520----------o-Xylene<0.0035<0.0040<0.0039<0.0044<0.0045<0.0048140590----------Xylene (Total)<0.0045<0.0052<0.0050<0.0056<0.0059<0.0062120530------SVOCs (8270E)Benzo(b)fluoranthene<0.144 <0.143 <0.155 <0.167 <0.161 <0.1711.1 21-- -- -- -- --Chrysene<0.157 <0.156 <0.169 <0.182 <0.175 <0.187110 2,100-- -- -- -- --bis(2-Ethylhexyl)phthalate<0.167 <0.166 <0.1810.243 J<0.1870.314 J39 160-- -- -- -- --Fluoranthene<0.148 <0.147 <0.159 <0.172 <0.165 <0.176480 6,000-- -- -- -- --1-Methylnaphthalene<0.152 <0.151 <0.164 <0.176 <0.1700.230 J18 73-- -- -- -- --2-Methylnaphthalene<0.173 <0.171 <0.186 <0.2010.220 J 0.370 J48 600-- -- -- -- --Phenanthrene<0.141 <0.140 <0.1520.173 J<0.158 <0.168NE NE-- -- -- -- --Pyrene<0.175 <0.174 <0.189 <0.204 <0.196 <0.208360 4,500-- -- -- -- --Metals (6020B/7471B/7199)Arsenic2.4 2.8 1.6 1.6 1.7 2.20.68 3.0--1.0 - 184.81.1 - 3.02.3Barium1111562767483,10047,000--50 - 1,00035638 - 11074Cadmium 0.15 J0.14 J0.10 J0.20 J1.40.811.420--1.0 - 10 4.3ND - 0.36 J0.13Chromium (total)14015046387491NENE--7.0 - 3006514 - 4531.3Chromium (VI)0.38 J0.38 J0.860.18 J0.57 J0.17 J0.316.5--NSNS0.34 J - 0.98 J 0.62Chromium (III)139.62149.6245.1437.8273.4390.8323,000350,000--NSNS13.7 - 44.030.7Lead8.38.7386.61016400800--ND - 501611 - 3620.7Mercury0.0530.0550.019 J0.031 J0.0620.030 J4.770--0.03 - 0.520.121 0.024 J - 0.097 0.074Selenium0.83 J1.1 J0.48 J0.66 J0.51 J1.1 J781,200--<0.1 - 0.80.42NDNDSilver0.026 J0.028 J0.024 J0.020 J0.028 J0.034 J781,200--ND - 5.0NS0.033 J - 0.60 0.60Metals (6010D TCLP)Chromium<0.036 mg/L <0.036 mg/LNANANANA----5 mg/L--------LeadNANANANANANA----5 mg/L--------Notes:1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) dated July 2022.2) Environmental Protection Agency (EPA) Maximum Concentrations of Contaminants for Toxicity Characteristics Leaching Procedure (TCLP) regulatory level dated November 2004. 3) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005; Cd and Ag concentrations were taken from Southeastern and Conterminous U.S. Soils.4) Background metals data collected from Cotton Warehouse Brownfields property (Brownfields Project No. 24013-20-060). Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Composite soil samples that were analyzed for VOCs were collected from undisturbed portions of soil and placed directly into laboratory supplied glassware.Bold values exceed the Residential PSRGs and background levels in the case of metals. Underlined values exceed the Industrial/Commercial PSRGs and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; UST = underground storage tank; ft bgs= feet below ground surface; mg/L= milligrams per liter; NS = not specified; NE = not established; -- = not applicable MS-11 = Matrix spike recovery outside of control limits. Possibility of sample matrix effects that lead to a high bias for reported result or non-homogeneous sample aliquots cannot be eliminated.R-04 = Duplicate relative percent difference is less useful indicator of sample precision for sample results that are <5 times the reporting limit.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. Maximum Concentration for TCLP (2)Screening Criteriamg/kgGrabRegional Background Metals in Soil (3)Background Metals in Nearby Brownfield Properties (4)SB-4/SB-DUP-3Floor Drains Former USTSB-7/SB-DUP-2Residential PSRGs (1)Industrial/ Commercial PSRGs (1)2/10/20222/9/20222-414-16https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Phase II ESA/Tables/Data Tables.xlsxTable 1 (Page 2 of 2)Hart & Hickman, PC Table 2Summary of Well Construction and Groundwater Depth DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Well IDTotal Depth (ft bgs)Screen Length (ft)Screen Interval (ft bgs)Depth to Groundwater (ft bgs)TOC Elevation (ft above msl)Groundwater Elevation (ft above msl)TMW-122157-2213.68749.05 735.37TMW-2251510-2519.70748.58 728.88TMW-3301515-3018.72746.45 727.73TMW-4251510-2513.56748.56 735.00TMW-5251510-2514.99744.54 729.55TMW-6251510-2517.81747.45 729.64 Notes:Depth to groundwater measurements were collected by H&H on February 10, 2022. Temporary monitoring wells TMW-1 through TMW-6 were surveyed by H&H relative to known benchmarks on February 14, 2022. Benchmark elevations estalished by McAdams on October 14, 2021. TOC = top of casing; ft bgs = feet below ground surface; msl = mean sea levelhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Phase II ESA/Tables/Data Tables.xlsx9/12/2022Table 2 (Page 1 of 1)Hart & Hickman, PC Table 3 Summary of Groundwater Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation AreaUpgradient Upgradient Sample IDTMW-1 TMW-2 TMW-3 TMW-4DateUnitsVOCs (8260D)Benzene <0.34 <0.34 <0.34 <0.34 <0.34 <0.340.89 J0.90 J11.66.9Carbon tetrachloride<0.330.86 J<0.33<0.33<0.33<0.33<0.33<0.330.30.411.8Chloroform <0.431.1<0.43<0.43<0.43<0.43<0.43<0.43700.813.62-Chlorotoluene<0.32<0.32<0.32<0.32<0.32<0.327.07.2100NENEDi-Isopropyl Ether <0.310.96 J<0.31<0.31<0.31<0.31<0.31<0.31701,4005,9001,2-Dichloroethane <0.322.8<0.32<0.32<0.32<0.32<0.32<0.320.42.29.8cis-1,2-Dichloroethene<0.38<0.38<0.38<0.38<0.38<0.388.78.470NENEEthylbenzene <0.30<0.30<0.30<0.30<0.30<0.301.61.66003.5152-Hexanone<0.48<0.48<0.48<0.48<0.480.50 J<0.48<0.48NE1,6006,900Naphthalene <0.64<0.64<0.64<0.64<0.64<0.6423.624.064.620Tetrachloroethene <0.29<0.29<0.29<0.29<0.29<0.295.35.10.71248Trichloroethene<0.38<0.38<0.38<0.38<0.38<0.381.61.531.04.4Trichlorofluoromethane0.39 J<0.30<0.30<0.30<0.30<0.30<0.30<0.302,000NENEo-Xylene<0.34<0.34<0.34<0.34<0.34<0.340.91 J0.99 J50098410Xylenes (total) <0.34<0.34<0.34<0.34<0.34<0.340.91 J0.99 J50077320SVOCs (8270E)1-Methylnaphthalene<1.7 <1.7 <1.8 <1.8 <1.7 <1.810.9 16.51NENE2-Methylnaphthalene<1.6<1.6<1.7<1.7<1.6<1.714.322.230NENENaphthalene<1.7<1.7<1.9<1.9<1.7<1.911.115.664.620Metals (6020B/7470A)Arsenic<0.31 <0.31 <0.31 <0.31 <0.31 <0.31 <0.31 <0.3110 NE NEBarium5789603536353231700NENECadmium<0.0300.061 J 0.041 R-04, J<0.0300.067 J0.067 J0.063 J0.066 J2NENEChromium (Total)2.21.7112.53.12.61.81.510NENELead<0.13<0.130.21 J0.30 J<0.13<0.13<0.13<0.1315NENEMercury<0.000040 <0.000040 <0.000040 <0.000040 <0.000040 <0.000040 <0.000040 <0.00004010.180.75Selenium<0.95<0.95<0.95<0.95<0.95<0.95<0.95<0.9520NENESilver<0.027<0.027<0.027<0.027<0.027<0.027<0.027<0.02720NENENotes:1) North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 2022.2) DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening Levels (GWSLs) dated July 2022. Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the 2L Standard.Underlined values exceed the DWM Residential Vapor Intrusion GWSLs. Shaded values exceed the DWM Non-Residential Vapor Intrusion GWSLs. VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; UST = underground storage tank; NE = not establishedR-04 = Duplicate relative percent difference is a less useful indicator of sample precision for sample results that are <5 times the reporting limit.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. µg/LScreening Criteria 2L Standards (1) Residential GWSLs (2)Non-Residential GWSLs (2)TMW-5/TMW-DUP-2TMW-6/TMW-DUP-12/10/20222/11/2022Former USTsDowngradient Downgradient https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Phase II ESA/Tables/Data Tables.xlsx9/12/2022Table 3 (Page 1 of 1)Hart & Hickman, PC Table 4Summary of Soil Gas Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation Area2426 N. Graham Street609 W. 28th StreetSample IDSSV-1 SSV-2 SG-1 SG-2 SG-3 SG-4Sample Date2/11/2022 2/14/2022 2/11/2022 2/14/2022Sample Type UnitsVOCs (TO-15)Acetone59.48.5224.29.3738.919.3NENEBenzene0.626 J0.367 J25.221.826.04.7312160Benzyl chloride<0.148<0.148<0.148<0.1484.83 J<0.1481.925Bromodichloromethane<0.150<0.150<0.150<0.1500.570 J<0.1502.5331,3-Butadiene<0.328<0.32834.51.89<0.328<0.3283.141Carbon Disulfide13.3 B0.514 JB45.577.211.9 B4.12 JB4,90061,000Carbon Tetrachloride<0.155<0.155<0.1551.11 J0.705 J<0.15516200Chlorobenzene<0.107<0.107<0.1072.860.663 J<0.1073504,400Chloroform<0.0864<0.0864<0.08646.891.70 J11.14.153Chloromethane<0.0673<0.0673<0.0673<0.0673<0.0673<0.06736307,900Cyclohexane<0.161<0.16166.813.54.367.2242,000530,000Dichlorodifluoromethane3.093.33<0.1343.853.543.287008,8001,2-Dichloropropane<0.205<0.2051.21 J<0.205<0.205<0.20525330Ethylbenzene0.812 J0.404 J56.433.055.14.05374904-Ethyltoluene<0.128<0.12822.64.3812.50.600 JNENE1,1,2-Trichlorotrifluoroethane0.667 J33.19.672.41 J<0.5610.713 J35,000440,000n-Heptane0.443 J0.451 J1661911072.522,80035,000n-Hexane0.518 J0.430 J49.728.85.921.06 J4,90061,0002-Hexanone4.154.06<0.285<0.2858.27<0.2852102,600Isopropyl Alcohol6.87 B<0.1393.65 JB<0.1394.20 JB<0.1391,40018,0002-Butanone (MEK)1.891.12 J8.094.855.572.1535,000440,0004-Methyl-2-pentanone (MIBK)0.705 J<0.1214.36<0.1214.350.594 J21,000260,000Methylene Chloride1.21 J1.04 J<0.4891.36 J1.32 J0.952 J3,40054,000Naphthalene4.51<0.18310.24.225.294.192.836Propylene<0.242<0.242319<0.2423.10<0.24221,000260,000Styrene<0.124<0.124<0.124<0.1244.47<0.124700088,0001,1,2,2-Tetrachloroethane<0.104<0.104<0.104<0.1041.78 J<0.1041321Tetrachloroethene14.159.13.832.07 J2.31 J0.590 J2803,500Tetrahydrofuran0.478 J<0.1071.06 J0.596 J0.855 J<0.10714,000180,000Toluene3.771.60 J31227239058.535,000440,000Trichlorofluoromethane1.83 J1.87 J1,8702.44 J2.25 J3.55NENE1,2,4-Trimethylbenzene1.45 J1.03 J1328.2436.52.08 J4205,3001,3,5-Trimethylbenzene0.590 J<0.23667.62.37 J11.70.693 J4205,300o-Xylene1.31 J0.638 J98.227.062.65.707008,800m&p-Xylene3.24 J1.54 J20190.018712.07008,800Xylene (total)4.55 J2.18 J29911725017.77008,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated July 2022.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses. Only compounds detected in at least one sample are shown in the above table.Bold values exceed the DWM Residential Vapor Intrusion SGSL. VOCs = volatile organic compounds; NE = not establishedB = Analyte detected in blank.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.µg/m3Proposed Residential Building2/14/2022Exterior Soil Gas Sub-Slab Soil GasScreening CriteriaResidential SGSLs (1)Non-Residential SGSLs (1)https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Phase II ESA/Tables/Data Tables.xlsx9/12/2022Table 4 (Page 1 of 2)Hart & Hickman, PC Table 4Summary of Soil Gas Analytical DataCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003Evaluation AreaSample IDSG-6 SG-7 SG-8Sample DateSample Type UnitsVOCs (TO-15)Acetone29.224.952.281.9101NENEBenzene25.227.087.815.33.0212160Benzyl chloride<0.148<0.148<0.148<0.148<0.1481.925Bromodichloromethane<0.150<0.150<0.150<0.150<0.1502.5331,3-Butadiene5.906.278.21<0.328<0.3283.141Carbon disulfide22.323.666.78.82 B1.98 JB4,90061,000Carbon tetrachloride1.07 J1.20 J<0.155<0.155<0.15516200Chlorobenzene<0.107<0.107<0.107<0.107<0.1073504,400Chloroform<0.0864<0.0864<0.08642.40 J<0.08644.153Chloromethane<0.0673<0.06732.57<0.0673<0.06736307,900Cyclohexane7.868.2225.311.9<0.16142,000530,000Dichlorodifluoromethane4.31<0.1343.683.183.327008,8001,2-Dichloropropane<0.205<0.205<0.205<0.205<0.20525330Ethylbenzene51.354.313.726.63.10374904-Ethyltoluene9.239.603.797.270.909 JNENE1,1,2-Trichlorotrifluoroethane1.14 J1.71 J1.13 J0.874 J<0.56135,000440,000n-Heptane14315211788.411.02,80035,000n-Hexane49.050.874.39.552.604,90061,0002-Hexanone<0.285<0.285<0.285<0.285<0.2852102,600Isopropyl Alcohol3.93 JB3.59 JB<0.1394.05 JB4.05 JB1,40018,0002-Butanone (MEK)5.005.429.115.905.0435,000440,0004-Methyl-2-pentanone (MIBK)2.272.616.905.805.5521,000260,000Methylene Chloride<0.489<0.489<0.4891.58 J0.674 J3,40054,000Naphthalene5.265.467.854.855.692.836Propylene168156329<0.242<0.24221,000260,000Styrene<0.124<0.124<0.124<0.1244.47700088,0001,1,2,2-Tetrachloroethane<0.104<0.104<0.104<0.104<0.1041321Tetrachloroethene1.63 J1.81 J0.705 J2.74 J1.07 J2803,500Tetrahydrofuran0.805 J<0.1071.510.876 J0.696 J14,000180,000Toluene44241018618835.235,000440,000Trichlorofluoromethane83.286.3<0.1303.961.83 JNENE1,2,4-Trimethylbenzene25.927.133.721.84.844205,3001,3,5-Trimethylbenzene8.769.4819.66.320.988 J4205,300o-Xylene57.561.024.230.24.097008,800m&p-Xylene17418241.988.610.47008,800Xylene (total)23224366.111914.57008,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated July 2022.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses. Only compounds detected in at least one sample are shown in the above table.Bold values exceed the DWM Residential Vapor Intrusion SGSL. VOCs = volatile organic compounds; NE = not establishedB = Analyte detected in blank.J = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.µg/m3Exterior Soil GasProposed Residential BuildingSG-5/SG-DUPResidential SGSLs (1)Non-Residential SGSLs (1)Screening Criteria2/11/2022https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Phase II ESA/Tables/Data Tables.xlsx9/12/2022Table 4 (Page 2 of 2)Hart & Hickman, PC Table 5Summary of Subsurface Methane Gas MeasurementsCommercial Equipment CompanyCharlotte, North CarolinaH&H Job No. ABS-003% % LELBarometric (in. Hg)Static (in. H₂O)2/14/2022 9:32 0.3 0.7 0.0001 0.0 0.1 2.0 29.39 0.062/15/2022 13:59 0.4 0.9 0.0 0.0 0.0 0.0 29.76 -0.072/14/2022 8:37 20.0 1.3 0.0 0.0 0.0 0.0 29.39 -0.062/15/2022 12:48 19.0 1.2 0.0 0.0 0.0 0.0 29.78 0.042/14/2022 10:30 20.0 1.3 0.0 0.0 0.0 0.0 29.40 -0.092/15/2022 12:55 19.2 1.3 0.0 0.0 0.0 0.0 29.77 -0.012/14/2022 7:57 14.3 3.6 0.0 0.0 0.1 2.0 29.42 -0.042/15/2022 12:39 14.0 1.5 0.0 0.0 0.0 0.0 29.72 0.072/14/2022 10:371.00.3 0.0002 0.07.0>100 29.48 0.022/15/2022 13:030.90.3 0.0001 0.06.7>100 29.79 0.092/14/2022 10:470.90.3 0.0001 0.06.8>100 29.46 0.062/15/2022 13:150.90.30.00.06.5>100 29.79 0.102/14/2022 9:5415.00.8 0.0013 0.00.00.029.40 0.062/15/2022 13:23 13.50.8 0.0014 0.00.00.029.78 -0.042/14/2022 9:4818.62.10.00.00.00.029.42 0.042/15/2022 13:45 18.22.00.00.00.00.029.77 0.002/14/2022 9:4011.33.30.00.00.00.029.39 -0.092/15/2022 13:52 11.12.6 0.0001 0.00.00.029.76 0.012/14/2022 9:1018.31.50.00.00.00.029.40 0.002/15/2022 14:06 17.81.30.00.00.00.029.76 -0.032/14/2022 10:07 18.12.2 0.0001 0.00.00.029.42 -0.052/15/2022 13:34 17.52.10.00.00.00.029.76 0.11Notes:Measurements were collected by H&H using a calibrated Landtec GEM 5000. Positive static pressure values indicate that subsurface pressure is greater than ambient air pressure. Bold values indicates methane concentration exceeds Atmospheric Lower Explosive Limit (LEL) of 5.0 % by volume of air. O2= Oxygen; CO2 = Carbon Dioxide; CO = Carbon Monoxide; H2S = Hydrogen Sulfide; in H₂O = Inches of Water; % = Percent By Volume of AirSG-1H2S (%)SG-DUPSG-6CO2 (%)SG-7SG-8SSV-1SSV-2SG-2SG-4SG-5SG-3Methane PressureSample ID Sample Date CO (%)O2 (%)Sample Timehttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Abacus Capital (ABS)/W. 28th and N.Graham Assembly/Phase II ESA/Tables/Methane_Tables.xlsx9/12/2022Table 5 (Page 1 of 1)Hart & Hickman, PC USGS The National Map: National Boundaries Dataset, 3DEP ElevationProgram, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset,and National Transportation Dataset; USGS Global Ecosystems; U.S. Census Bureau TIGER/Line data; USFS Road Data; Natural Earth Data;U.S. Department of State Humanitarian Information Unit; and NOAANational Centers for Environmental Information, U.S. Coastal ReliefModel. Data refreshed August, 2021. SITE LOCATION MAP COMMERCIAL EQUIPMENT COMPANY N. GRAHAM STREET AND W. 28TH STREETCHARLOTTE, NORTH CAROLINA DATE: 1-24-22 JOB NO: ABS-003 REVISION NO: 0 FIGURE. 1 2923 South Tryon Street - Suite 100 Charlotte, North Carolina 28203 704-586-0007 (p) 704-586-0373 (f) License # C-1269 / # C-245 Geology TITLE PROJECT 0 2,000 4,000 SCALE IN FEET Path: \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\ABS-003\Figure 1.mxdN U.S.G.S. QUADRANGLE MAP CHARLOTTE EAST, NORTH CAROLINA 2013 DERITA, NORTH CAROLINA 2013 QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC) SITE REVISION NO. 0 JOB NO. ABS-003 DATE: 1-24-22 FIGURE NO. 2 COMMERCIAL EQUIPMENT COMPANY N. GRAHAM STREET AND W. 28TH STREET CHARLOTTE, NORTH CAROLINA SITE MAP LEGEND SITE PROPERTY BOUNDARY PARCEL BOUNDARY POLE-MOUNTED TRANSFORMER PAD-MOUNTED TRANSFORMER ELEVATOR DUMPSTER POTENTIAL GASOLINE UST POTENTIAL OIL/WATER SEPARATOR/WASTE OIL UST FORMER DIESEL UST AIR COMPRESSOR VENT PIPE FLOOR DRAIN 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology NOTES: 1. PARCEL DATA AND AERIAL IMAGERY OBTAINED FROMMECKLENBURG COUNTY GIS, 2021. 2. UST = UNDERGROUND STORAGE TANK PEP BOYS DISTRIBUTION CENTER(700 W. 28TH STREET) FIRE STATION NO. 11 & FIRE DEPARTMENT MAINTENANCE SHOP(620 W. 28TH STREET) EASY BUILDING SUPPLIES(600 W. 28TH STREET) ASHLEY SLING, INC.(2401 N. GRAHAM STREET) MCGRANT TAX & BOOKING (2336 N. GRAHAM STREET) FRA N K L I N A V E N U E W. 2 8 T H S T R E E TN. GRAHAM STREETGRIMES STREETBANCROFT STREETBANCROFT STREETSTORAGE(2402/2426 N. GRAHAM STREET) RESIDENCE(2415 GRIMES STREET) OFFICES(609 W. 28TH STREET) EQUIPMENTSTORAGE PALLET AND CONSTRUCTION MATERIALSSTORAGE PALLET AND PLASTIC TOTE STORAGE TRUCK/TRAILERPARKING TRUCK/TRAILERPARKING FORMERDISPENSER ISLAND TRUCK REPAIR RESIDENTIAL FORMERWASH BAY RESIDENCE(2409 GRIMES STREET)S:\AAA-Master Projects\Abacus Capital (ABS)\ABS-003 - W. 28th and N.Graham Assembly\Phase II ESA\Figures\Site Map.dwg, FIG 2, 1/25/2022 3:03:23 PM, sperry SSV-2 SG-8 SG-7 SG-1 SG-2 SG-3 SG-4SG-5 SG-6 SB-1 SB-2 SB-3 SB-5SB-6 COMP-2 COMP-1 COMP-5 COMP-4 COMP-3 SB-4 TMW-1 TMW-2 TMW-3 TMW-5 TMW-4 TMW-6/SB-7 SSV-1 REVISION NO. 0 JOB NO. ABS-003 DATE: 3-18-22 FIGURE NO. 3 SAMPLE LOCATION MAP LEGEND SITE PROPERTY BOUNDARY PARCEL BOUNDARY POTENTIAL GASOLINE UST POTENTIAL OIL/WATER SEPARATOR/ WASTE OIL UST FORMER DIESEL UST VENT PIPE FLOOR DRAIN TEMPORARY MONITORING WELL SOIL BORING CO-LOCATED TEMPORARY MONITORINGWELL/SOIL BORING ALIQUOT SOIL BORING SOIL GAS POINT SUB-SLAB SOIL GAS POINT EXISTING BUILDING PROPOSED BUILDING 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology NOTES: 1. PARCEL DATA AND AERIAL IMAGERY OBTAINED FROMMECKLENBURG COUNTY GIS, 2021. 2. UST = UNDERGROUND STORAGE TANK PEP BOYS DISTRIBUTION CENTER(700 W. 28TH STREET) FIRE STATION NO. 11 & FIRE DEPARTMENT MAINTENANCE SHOP(620 W. 28TH STREET) EASY BUILDING SUPPLIES(600 W. 28TH STREET) ASHLEY SLING, INC.(2401 N. GRAHAM STREET) MCGRANT TAX & BOOKING(2336 N. GRAHAM STREET) FRA N K L I N A V E N U E W. 2 8 T H S T R E E TN. GRAHAM STREETGRIMES STREETBANCROFT STREETBANCROFT STREETSTORAGE(2402/2426 N. GRAHAM STREET) RESIDENCE(2415 GRIMES STREET) OFFICES(609 W. 28TH STREET) FORMERDISPENSER ISLAND TRUCK REPAIR RESIDENTIAL FORMERWASH BAY RESIDENCE(2409 GRIMES STREET) COMMERCIAL EQUIPMENT COMPANY N. GRAHAM STREET AND W. 28TH STREET CHARLOTTE, NORTH CAROLINA PROPOSED AMENITY AREA S:\AAA-Master Projects\Abacus Capital (ABS)\ABS-003 - W. 28th and N.Graham Assembly\Phase II ESA\Figures\Site Map.dwg, FIG 3, 4/4/2022 2:30:58 PM, shaynes N GRAHAM STN CHURCH STROFT STWO L FBE R R Y S T N TRYON STWI C K RDEN ST OHLER AV W24THSTRACHEL STWOODWARDAV W 3 2 N D S T CATAL INA AVNC H URCHSTW 3 1 S T S T W 2 7 T H S TGRIMES STE 2 6 T H S T M A T H E S O N A V CARTER AV EDISON STDOGWOOD AVJEFFERSONDAVISSTN PINE STBANCROFT STLUCENA STVANDERBI LT RD B ELLEFONTEDRNO RRI S A V FR A N K LIN A V N PO PLAR ST W28THSTMORETZ A V CO N C O R D I A A V W 30THST COLORADOAV W 26 T H STGRIMES STCOL O R A D O A V FRA NKL I N A V W 2 5T H S T N POPLAR STEN N I S A V OLANDO STHOBBS STBANCROFT STE 27 TH S T W 2 9 T H ST CA M P R D E 2 8 T H S TOLANDOSTDRUID CRWIN ST O N S T BANCROFT STENTERPRISE DRRECEPTOR SURVEY MAP COMMERCIAL EQUIPMENT COMPANYN. GRAHAM STREET AND W. 28TH STREET CHARLOTTE, NORTH CAROLINA REVISION NO: 0 FIGURE NO: 4 2923 South Tryon Street - Suite 100 Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f) License # C-1269 / # C-245 Geology 0400800 SCALE IN FEET N DATE: 3-22-22 JOB NO. ABS-003 NOTES: 1. AERIAL IMAGERY OBTAINED FROM MECKLENBURGCOUNTY GIS, 2021.2. BASE DATA OBTAINED FROM MECKLENBURG COUNTYGIS, 2022. SEE INSET \\HHFS01\Redirectedfolders\sperry\My Documents\ArcGIS\PROJECTS\ABS-003\RECEPTOR_SURVEY.mxdLEGEND SITE PROPERTY BOUNDARY PARCEL LINE BUSINESS ZONING INDUSTRIAL MIXED USE RESIDENTIAL UPTOWN MIXED USE O/H OVERHEAD ELECTRIC LINE GAS NATURAL GAS LINE SS SEWER LINE W WATER LINE 1,500 FT W 2 8 TH ST R E E TN GRAHAM STREETINSET O/H O/H O/H O/H O/H O/H O/H O/H O/H O/H O/HO/HO/HO/HO/HO/H O/H O/H O/H O/H O/H O/H O/HO/HO/HO/HO/HO/HO/HWWGASGASGAS GAS W WSS SS TMW-1 TMW-2 TMW-3 TMW-5 TMW-4 TMW-6/SB-7 REVISION NO. 0 JOB NO. ABS-003 DATE: 3-18-22 FIGURE NO. 5 POTENTIOMETRIC SURFACE MAP LEGEND SITE PROPERTY BOUNDARY PARCEL BOUNDARY POTENTIAL GASOLINE UST POTENTIAL OIL/WATER SEPARATOR/ WASTE OIL UST FORMER DIESEL UST VENT PIPE FLOOR DRAIN TEMPORARY MONITORING WELL CO-LOCATED SOIL BORING/TEMPORARYMONITORING WELL EXISTING BUILDING PROPOSED BUILDING GROUNDWATER ELEVATION (FT MSL) INFERRED GROUNDWATER ELEVATIONCONTOUR (FT MSL) INFERRED GROUNDWATER FLOWDIRECTION COMMERCIAL EQUIPMENT COMPANY N. GRAHAM STREET AND W. 28TH STREET CHARLOTTE, NORTH CAROLINA 2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology NOTES: 1. PARCEL DATA AND AERIAL IMAGERY OBTAINED FROMMECKLENBURG COUNTY GIS, 2021. 2. UST = UNDERGROUND STORAGE TANK 3. GROUNDWATER ELEVATIONS MEASURED FEBRUARY 10,2022. PEP BOYS DISTRIBUTION CENTER(700 W. 28TH STREET) FIRE STATION NO. 11 & FIRE DEPARTMENT MAINTENANCE SHOP(620 W. 28TH STREET) EASY BUILDING SUPPLIES(600 W. 28TH STREET) ASHLEY SLING, INC.(2401 N. GRAHAM STREET) MCGRANT TAX & BOOKING(2336 N. GRAHAM STREET) FR A N K L I N A V E N U E W. 2 8 T H S T R E E TN. GRAHAM STREETGRIMES STREETBANCROFT STREETBANCROFT STREETSTORAGE(2402/2426 N. GRAHAM STREET) RESIDENCE(2415 GRIMES STREET) OFFICES(609 W. 28TH STREET) FORMERDISPENSER ISLAND TRUCK REPAIR RESIDENTIAL FORMERWASH BAY RESIDENCE(2409 GRIMES STREET) 730 (727.73) (729.55) (727.73) (728.88) (735.37) (735.00) (729.64)734732730728728730732734PROPOSED AMENITY AREA S:\AAA-Master Projects\Abacus Capital (ABS)\W. 28th and N.Graham Assembly\Phase II ESA\Figures\Site Map.dwg, FIG 5, 5/3/2022 6:46:30 AM, shaynes Appendix B Boring Logs NOTES: Soil boring advanced adjacent to former building foundations. Hand cleared to 5 ft bgs. Soil sample collected for analysis of VOCs, SVOCs, and metals. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: BF-SB-1 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/14/23 4/14/23 MidSouth Direct Push GeoProbe54 DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 10.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 (0') Well-graded GRAVEL (GW) (0.5') SILT (ML); trace medium sand, some clay, medium stiff, wet, red-brown (2') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling (9') SILT (ML); some clay, medium stiff, moist, red-brown w/ white veins (10') Boring terminated 3.5 3.6 3.0 1.0 1.1 BF-SB-1(5-7) 0 5 10 15 DPT GA 5.00 5.00GP NOTES: Hand cleared to 5 ft bgs. Soil sample collected for analysis of VOCs, SVOCs, and metals. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: BF-SB-2 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/14/23 4/14/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 10.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 (0') Asphalt (0.25') Well-graded GRAVEL (GW) (4') SILT (ML); little clay, stiff, moist, red-brown w/ some tan mottling (10') Boring terminated 4.4 5.3 5.0 4.5 BF-SB-2(5-7) 0 5 10 15 DPT (0.5') SILT (ML); little clay, medium stiff, moist, red-brown w/ some tan-mottling GP GA 5.00 5.00 NOTES: Hand cleared to 5 ft bgs. Soil sample collected for analysis of VOCs, SVOCs, and metals. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: BF-SB-3 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/14/23 4/14/23 MidSouth Direct Push GeoProbe 54 DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 10.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 (0') Well-graded GRAVEL (GW) (0.5') SILT (ML); some clay, stiff, moist, red-brown (10') Boring terminated 11.8 11.0 6.5 4.2 3.6 BF-SB-3(4-5) 0 5 10 15 DPT 5.00 5.00 GA GP NOTES: Hand cleared to 5 ft bgs. Soil sample collected for analysis of VOCs, SVOCs, and metals. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: BF-SB-4 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/14/23 4/14/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 10.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 (0') Asphalt (0.25') Well-graded GRAVEL (GW) (0.5') SILT (ML); some clay, stiff, moist, red-brown w/ few tan mottling (10') Boring terminated 3.6 3.6 5.7 4.7 BF-SB-4(2-4) 0 5 10 15 DPT 3.6 5.00GA 5.00GP NOTES: Hand cleared to 5 ft bgs. Soil sample collected for analysis of VOCs, SVOCs, and metals. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: BF-SB-5 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/14/23 4/14/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 10.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 15 (0') Well-graded GRAVEL (GW) (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling (4') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling & few pink and white (10') Boring terminated 6.3 7.1 5.9 6.1 5.5 BF-SB-5 0 5 10 15 DPT (2-4) 5.00GA 5.00GP NOTES: Hole advanced to 2.0' using hand auger. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: COMP-3A 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Other Hand Auger CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 2.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 1 2 3 4 5 (0') Gravel (0.5') Silty CLAY (CL); medium stiff, moist, reddish-brown (2') Boring terminated 9.1 COMP-3A (0.5-2) 0 1 2 3 4 5 Don Warren GA 2.00 NOTES: Hole advanced to 2.0' using hand auger. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: COMP-3B 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 2.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 1 2 3 4 5 (0') Gravel (0.5') Silty CLAY (CL); medium stiff, moist, red with tan mottling (2') Boring terminated 8.4 COMP-3B (0.5-2) 0 1 2 3 4 5 4/13/23 4/13/23 MidSouth Other Hand Auger CMB Don Warren 2.00GA NOTES: Hole advanced to 2.0' using hand auger. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: COMP-3C 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 2.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 1 2 3 4 5 (0') Asphalt (0.5') Silty CLAY (CL); medium stiff, moist, red (2') Boring terminated 7.4 COMP-3C (0.5-2) 0 1 2 3 4 5 4/13/23 4/13/23 MidSouth Other Hand Auger CMB (0.25') Gravel Don Warren 2.00GA NOTES: Hole advanced to 2.0' using hand auger. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: COMP-3D 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 2.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 1 2 3 4 5 (0.5') Silty CLAY (CL); medium stiff, moist, reddish-brown (2') Boring terminated 7.6 COMP-3D (0.5-2) 0 1 2 3 4 5 4/13/23 4/13/23 MidSouth Other Hand Auger CMB (0') Asphalt (0.25') Gravel Don Warren 2.00GA NOTES: Hole advanced to 2.0' using hand auger. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: COMP-3E 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 2.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 1 2 3 4 5 (0.5') Silty CLAY (CL); medium stiff, moist, red (2') Boring terminated 5.3 COMP-3E (0.5-2) 0 1 2 3 4 5 4/13/23 4/13/23 MidSouth Other Hand Auger CMB (0') Asphalt (0.25') Gravel Don Warren 2.00GA NOTES: Hole advanced to 2.0' using hand auger. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC BORING LOG Boring No. Page: COMP-3F 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 2.0 3.25 Grab DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 1 2 3 4 5 (0.5') Silty CLAY (CL); medium stiff, moist, reddish-brown (2') Boring terminated 7.9 COMP-3F (0.5-2) 0 1 2 3 4 5 4/13/23 4/13/23 MidSouth Other Hand Auger CMB (0') Asphalt (0.25') Gravel Don Warren 2.00GA NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 7' bgs. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC MP CONSTRUCTION LOG Boring No. Page: MP-A 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELMPCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (6') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan and pink minerals, relict structure (7') Boring terminated 4.4 7.2 7.2 6.1 6.3 7.0 7.3 0 5 10 (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling None 5.00 2.00 generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: MP-B 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (6') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan and pink minerals, relict structure (7') Boring terminated 3.0 3.1 3.5 3.3 3.1 0 5 10 (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling None MP CONSTRUCTION LOG MP5.00 2.00 NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 7' bgs. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: MP-C 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (6') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan and pink minerals, relict structure (7') Boring terminated 2.4 2.2 2.3 2.4 1.5 0 5 10 (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling None MP CONSTRUCTION LOG MP2.00 5.00 NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 7' bgs. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: MP-D 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (6') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan and pink minerals, relict structure (7') Boring terminated 1.5 3.8 4.2 5.1 5.2 4.5 4.1 0 5 10 (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling None NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 7' bgs. 2.00 5.00MP MP CONSTRUCTION LOG generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: MP-E 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling (5') SILT (ML); some clay, medium stiff, moist, orange-brown w/ tan mottling (7') Boring terminated 2.1 2.8 1.7 3.2 3.3 0 5 10 None NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 7' bgs. MP CONSTRUCTION LOG MP5.00 2.00 NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 6' bgs and not 7' due to cave in. generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: MP-F 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (6') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan and pink minerals, relict structure (7') Boring terminated 2.7 3.5 3.3 3.1 2.6 2.7 2.5 0 5 10 (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling None MP CONSTRUCTION LOG MP5.00 2.00 generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: MP-G 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (6') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan and pink minerals, relict structure (7') Boring terminated 5.3 5.6 6.6 4.3 4.1 0 5 10 (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling None NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 7' bgs. MP CONSTRUCTION LOG MP5.00 2.00 generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: MP-H 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling (4') SILT (ML); trace fine gravel, trace clay, soft, moist, brown, few quartz (7') Boring terminated 2.4 4.1 5.1 4.5 5.3 0 5 10 None MP CONSTRUCTION LOG NOTES: Hand cleared to 5 ft bgs. Monitoring point (MP) installed at 7' bgs. 5.00 2.00MP generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: SG-5 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (6') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan and pink minerals, relict structure (7') Boring terminated 2.9 2.1 2.8 1.9 2.6 0 5 10 (0.5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan mottling None SG CONSTRUCTION LOG SGNOTES: Hand cleared to 5 ft bgs. Monitoring point installed at 7' bgs. 2.00 5.00 generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: SG-9 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (0.25') SILT (ML); some clay, medium stiff, moist, red-brown w/ yellow-tan (3') SILT (ML); trace medium sand, trace clay, medium stiff, moist, brown w/ dark red (4') SILT (ML); little clay, medium stiff, moist, red-brown (7') Boring terminated 1.1 2.7 3.3 2.8 2.6 3.0 3.4 0 5 10 None SG CONSTRUCTION LOG NOTES: Hand cleared to 5 ft bgs. Soil gas point (SG) installed at 7' bgs.SG5.00 2.00 generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: SG-10 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Asphalt (0.25') SILT (ML); trace medium sand, some clay, medium stiff, moist, red-brown, some mica (5') SILT (ML); little clay, medium stiff, moist, red-brown w/ trace tan veins, some mica (7') Boring terminated 2.0 2.6 2.2 1.9 1.7 2.0 1.9 0 5 10 None SG CONSTRUCTION LOG NOTES: Hand cleared to 5 ft bgs. Soil gas point (SG) installed at 7' bgs. 5.00 2.00SG generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: SG-11 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: 4/13/23 4/13/23 MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (0.5') SILT (ML); some clay, medium stiff, moist, red-brown (2') SILT (ML); few clay, medium stiff, moist, red-brown w/ tan mottling (7') Boring terminated 2.9 4.3 5.6 6.2 5.7 0 5 10 None NOTES: Hand cleared to 5 ft bgs. Soil gas point (SG) installed at 7' bgs. SG CONSTRUCTION LOG 5.00 2.00SG generated using GroundLogs.online Client: Project: Address: Abacus Capital ABS-003 N. Graham and W. 28th St.,Charlotte, NC Boring No. Page: SG-12 1 of 1 Drilling Start Date: Drilling End Date: Drilling Company: Drilling Method: Drilling Equipment: Driller: Logged By: MidSouth Direct Push GeoProbe 54DT Don Warren CMB Boring Depth (ft): Boring Diameter (in): Sampling Method(s): DTW During Drilling (ft): DTW After Drilling (ft): Ground Surface Elev. (ft): Location (X,Y): 7.0 3.25 DEPTH (ft)LITHOLOGYWATER LEVELCOMPLETIONCOLLECT Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION MEASURE PID (ppm)Lab SampleDEPTH (ft)0 5 10 (0') Well-graded GRAVEL (GW) (1') SILT (ML); some clay, medium stiff, moist, red-brown (3') SILT (ML); some clay, medium stiff, moist, red-brown w/ trace tan veins and mottling (5') SILT (ML); some clay, medium stiff, moist, red-brown w/ tan & yellow-brown layers, relict structure (7') Boring terminated 2.0 2.6 2.9 2.5 2.3 2.3 1.9 0 5 10 None 4/13/23 4/13/23 SG CONSTRUCTION LOG 5.00 2.00 NOTES: Hand cleared to 5 ft bgs. Soil gas point (SG) installed at 7' bgs.SG Appendix C Laboratory Analytical Reports #=CL# May 12, 2023 LIMS USE: FR - HALEY MARTIN LIMS OBJECT ID: 92662335 92662335 Project: Pace Project No.: RE: Haley Martin Hart & Hickman 2923 S. Tryon St Suite 100 Charlotte, NC 28203 ABS.003 Commercial Equipment Dear Haley Martin: Enclosed are the analytical results for sample(s) received by the laboratory on April 14, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Charlotte • Pace Analytical Services - Minneapolis This report was revised on April 28, 2023, to add 6010D TCLP lead to Pace sample 92662335010; and 6010D TCLP chromium to Pace samples 92662335003, 004, and 012. If you have any questions concerning this report, please feel free to contact me. Sincerely, Taylor M Cannon taylor.cannon@pacelabs.com Project Manager (704)875-9092 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 69 #=CP# CERTIFICATIONS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Pace Analytical Services, LLC - Minneapolis MN 1700 Elm Street SE, Minneapolis, MN 55414 A2LA Certification #: 2926.01 Alabama Certification #: 40770 Alaska Contaminated Sites Certification #: 17-009 Alaska DW Certification #: MN00064 Arizona Certification #: AZ0014 Arkansas DW Certification #: MN00064 Arkansas WW Certification #: 88-0680 California Certification #: 2929 Colorado Certification #: MN00064 Connecticut Certification #: PH-0256 EPA Region 8 Tribal Water Systems+Wyoming DW Certification #: via MN 027-053-137 Florida Certification #: E87605 Georgia Certification #: 959 GMP+ Certification #: GMP050884 Hawaii Certification #: MN00064 Idaho Certification #: MN00064 Illinois Certification #: 200011 Indiana Certification #: C-MN-01 Iowa Certification #: 368 Kansas Certification #: E-10167 Kentucky DW Certification #: 90062 Kentucky WW Certification #: 90062 Louisiana DEQ Certification #: AI-03086 Louisiana DW Certification #: MN00064 Maine Certification #: MN00064 Maryland Certification #: 322 Michigan Certification #: 9909 Minnesota Certification #: 027-053-137 Minnesota Dept of Ag Approval: via MN 027-053-137 Minnesota Petrofund Registration #: 1240 Mississippi Certification #: MN00064 Missouri Certification #: 10100 Montana Certification #: CERT0092 Nebraska Certification #: NE-OS-18-06 Nevada Certification #: MN00064 New Hampshire Certification #: 2081 New Jersey Certification #: MN002 New York Certification #: 11647 North Carolina DW Certification #: 27700 North Carolina WW Certification #: 530 North Dakota Certification (A2LA) #: R-036 North Dakota Certification (MN) #: R-036 Ohio DW Certification #: 41244 Ohio VAP Certification (1700) #: CL101 Oklahoma Certification #: 9507 Oregon Primary Certification #: MN300001 Oregon Secondary Certification #: MN200001 Pennsylvania Certification #: 68-00563 Puerto Rico Certification #: MN00064 South Carolina Certification #:74003001 Tennessee Certification #: TN02818 Texas Certification #: T104704192 Utah Certification #: MN00064 Vermont Certification #: VT-027053137 Virginia Certification #: 460163 Washington Certification #: C486 West Virginia DEP Certification #: 382 West Virginia DW Certification #: 9952 C Wisconsin Certification #: 999407970 Wyoming UST Certification #: via A2LA 2926.01 USDA Permit #: P330-19-00208 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: AI30792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TN003 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification #: CERT0086 Nebraska Certification #: NE-OS-15-05 Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 69 #=CP# CERTIFICATIONS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Pace Analytical Services National New Jersey Certification #: TN002 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LAO00356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Certification #: T 104704245-17-14 Texas Mold Certification #: LAB0152 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: VT2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 998093910 Wyoming UST Certification #: via A2LA 2926.01 A2LA-ISO 17025 Certification #: 1461.01 A2LA-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 69 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Lab ID Sample ID Matrix Date Collected Date Received 92662335001 BF-SB-01 (5-7)Solid 04/14/23 09:30 04/14/23 13:10 92662335002 BF-SB-02 (5-7)Solid 04/14/23 09:20 04/14/23 13:10 92662335003 BF-SB-03 (4-5)Solid 04/14/23 11:00 04/14/23 13:10 92662335004 BF-SB-04 (2-4)Solid 04/14/23 11:45 04/14/23 13:10 92662335005 BF-SB-05 (2-4)Solid 04/14/23 11:55 04/14/23 13:10 92662335006 COMP-3A (0.5-2)Solid 04/13/23 15:30 04/14/23 13:10 92662335007 COMP-3B (0.5-2)Solid 04/13/23 15:35 04/14/23 13:10 92662335008 COMP-3C (0.5-2)Solid 04/13/23 15:45 04/14/23 13:10 92662335009 COMP-3D (0.5-2)Solid 04/13/23 15:50 04/14/23 13:10 92662335010 COMP-3E (0.5-2)Solid 04/13/23 16:00 04/14/23 13:10 92662335011 COMP-3F (0.5-2)Solid 04/13/23 16:05 04/14/23 13:10 92662335012 BF-SB-DUP Solid 04/13/23 00:00 04/14/23 13:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 69 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92662335001 BF-SB-01 (5-7)EPA 6020B 7 PASI-MNN2 EPA 7471B 1 PASI-MDJM EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CCL SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92662335002 BF-SB-02 (5-7)EPA 6020B 7 PASI-MNN2 EPA 7471B 1 PASI-MDJM EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CCL SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92662335003 BF-SB-03 (4-5)EPA 6010D 1 PASI-MIP EPA 6020B 7 PASI-MNN2 EPA 7471B 1 PASI-MDJM EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CCL SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92662335004 BF-SB-04 (2-4)EPA 6010D 1 PASI-MIP EPA 6020B 7 PASI-MNN2 EPA 7471B 1 PASI-MDJM EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CCL SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS 92662335005 BF-SB-05 (2-4)EPA 6020B 7 PASI-MNN2 EPA 7471B 1 PASI-MDJM EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CCL SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 69 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92662335006 COMP-3A (0.5-2)EPA 6020B 1 PASI-MNN2 SW-846 1 PASI-CKDF 92662335007 COMP-3B (0.5-2)EPA 6020B 1 PASI-MNN2 SW-846 1 PASI-CKDF 92662335008 COMP-3C (0.5-2)EPA 6020B 1 PASI-MNN2 SW-846 1 PASI-CKDF 92662335009 COMP-3D (0.5-2)EPA 6020B 1 PASI-MNN2 SW-846 1 PASI-CKDF 92662335010 COMP-3E (0.5-2)EPA 6010D 1 PASI-MIP EPA 6020B 1 PASI-MNN2 SW-846 1 PASI-CKDF 92662335011 COMP-3F (0.5-2)EPA 6020B 1 PASI-MNN2 SW-846 1 PASI-CKDF 92662335012 BF-SB-DUP EPA 6010D 1 PASI-MIP EPA 6020B 7 PASI-MNN2 EPA 7471B 1 PASI-MDJM EPA 8270E 75 PASI-CBPJ EPA 8260D 70 PASI-CCL SW-846 1 PASI-CKDF SM 2540G 1 PANCMK EPA 7199 1 PANVSS PAN = Pace National - Mt. Juliet PASI-C = Pace Analytical Services - Charlotte PASI-M = Pace Analytical Services - Minneapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-01 (5-7)Lab ID: 92662335001 Collected: 04/14/23 09:30 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 2.2 mg/kg 04/20/23 14:20 7440-38-204/20/23 10:030.67 0.19 1 Barium 19.1 mg/kg 04/20/23 14:20 7440-39-3 M104/20/23 10:030.40 0.10 1 Cadmium ND mg/kg 04/20/23 14:20 7440-43-9 R104/20/23 10:030.11 0.039 1 Chromium 45.2 mg/kg 04/20/23 14:20 7440-47-304/20/23 10:032.7 0.52 1 Lead 7.8 mg/kg 04/20/23 14:20 7439-92-1 M1,R104/20/23 10:030.67 0.12 1 Selenium 0.98 mg/kg 04/20/23 14:20 7782-49-204/20/23 10:030.67 0.14 1 Silver ND mg/kg 04/20/23 14:20 7440-22-4 R104/20/23 10:030.67 0.27 1 Analytical Method: EPA 7471B Preparation Method: EPA 7471B Pace Analytical Services - Minneapolis 7471B Mercury Mercury 0.039 mg/kg 04/21/23 11:07 7439-97-604/20/23 10:060.026 0.011 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 04/16/23 14:18 83-32-904/15/23 15:46447 157 1 Acenaphthylene ND ug/kg 04/16/23 14:18 208-96-804/15/23 15:46447 157 1 Aniline ND ug/kg 04/16/23 14:18 62-53-304/15/23 15:46447 175 1 Anthracene ND ug/kg 04/16/23 14:18 120-12-704/15/23 15:46447 146 1 Benzo(a)anthracene ND ug/kg 04/16/23 14:18 56-55-304/15/23 15:46447 149 1 Benzo(a)pyrene ND ug/kg 04/16/23 14:18 50-32-804/15/23 15:46447 154 1 Benzo(b)fluoranthene ND ug/kg 04/16/23 14:18 205-99-204/15/23 15:46447 149 1 Benzo(g,h,i)perylene ND ug/kg 04/16/23 14:18 191-24-204/15/23 15:46447 173 1 Benzo(k)fluoranthene ND ug/kg 04/16/23 14:18 207-08-904/15/23 15:46447 157 1 Benzoic Acid ND ug/kg 04/16/23 14:18 65-85-0 L204/15/23 15:462240 961 1 Benzyl alcohol ND ug/kg 04/16/23 14:18 100-51-604/15/23 15:46894 339 1 4-Bromophenylphenyl ether ND ug/kg 04/16/23 14:18 101-55-304/15/23 15:46447 172 1 Butylbenzylphthalate ND ug/kg 04/16/23 14:18 85-68-704/15/23 15:46447 188 1 4-Chloro-3-methylphenol ND ug/kg 04/16/23 14:18 59-50-704/15/23 15:46894 314 1 4-Chloroaniline ND ug/kg 04/16/23 14:18 106-47-804/15/23 15:46894 351 1 bis(2-Chloroethoxy)methane ND ug/kg 04/16/23 14:18 111-91-104/15/23 15:46447 186 1 bis(2-Chloroethyl) ether ND ug/kg 04/16/23 14:18 111-44-404/15/23 15:46447 168 1 2-Chloronaphthalene ND ug/kg 04/16/23 14:18 91-58-704/15/23 15:46447 178 1 2-Chlorophenol ND ug/kg 04/16/23 14:18 95-57-804/15/23 15:46447 168 1 4-Chlorophenylphenyl ether ND ug/kg 04/16/23 14:18 7005-72-304/15/23 15:46447 167 1 Chrysene ND ug/kg 04/16/23 14:18 218-01-904/15/23 15:46447 163 1 Dibenz(a,h)anthracene ND ug/kg 04/16/23 14:18 53-70-304/15/23 15:46447 172 1 Dibenzofuran ND ug/kg 04/16/23 14:18 132-64-904/15/23 15:46447 161 1 1,2-Dichlorobenzene ND ug/kg 04/16/23 14:18 95-50-104/15/23 15:46447 161 1 1,3-Dichlorobenzene ND ug/kg 04/16/23 14:18 541-73-104/15/23 15:46447 159 1 1,4-Dichlorobenzene ND ug/kg 04/16/23 14:18 106-46-704/15/23 15:46447 171 1 3,3'-Dichlorobenzidine ND ug/kg 04/16/23 14:18 91-94-104/15/23 15:46894 302 1 2,4-Dichlorophenol ND ug/kg 04/16/23 14:18 120-83-204/15/23 15:46447 175 1 Diethylphthalate ND ug/kg 04/16/23 14:18 84-66-204/15/23 15:46447 164 1 2,4-Dimethylphenol ND ug/kg 04/16/23 14:18 105-67-904/15/23 15:46447 186 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-01 (5-7)Lab ID: 92662335001 Collected: 04/14/23 09:30 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 04/16/23 14:18 131-11-304/15/23 15:46447 163 1 Di-n-butylphthalate ND ug/kg 04/16/23 14:18 84-74-204/15/23 15:46447 150 1 4,6-Dinitro-2-methylphenol ND ug/kg 04/16/23 14:18 534-52-104/15/23 15:46894 417 1 2,4-Dinitrophenol ND ug/kg 04/16/23 14:18 51-28-504/15/23 15:462240 1380 1 2,4-Dinitrotoluene ND ug/kg 04/16/23 14:18 121-14-204/15/23 15:46447 172 1 2,6-Dinitrotoluene ND ug/kg 04/16/23 14:18 606-20-204/15/23 15:46447 164 1 Di-n-octylphthalate ND ug/kg 04/16/23 14:18 117-84-004/15/23 15:46447 176 1 bis(2-Ethylhexyl)phthalate ND ug/kg 04/16/23 14:18 117-81-704/15/23 15:46447 173 1 Fluoranthene ND ug/kg 04/16/23 14:18 206-44-004/15/23 15:46447 153 1 Fluorene ND ug/kg 04/16/23 14:18 86-73-704/15/23 15:46447 157 1 Hexachloro-1,3-butadiene ND ug/kg 04/16/23 14:18 87-68-304/15/23 15:46447 194 1 Hexachlorobenzene ND ug/kg 04/16/23 14:18 118-74-104/15/23 15:46447 175 1 Hexachlorocyclopentadiene ND ug/kg 04/16/23 14:18 77-47-404/15/23 15:46447 256 1 Hexachloroethane ND ug/kg 04/16/23 14:18 67-72-104/15/23 15:46447 171 1 Indeno(1,2,3-cd)pyrene ND ug/kg 04/16/23 14:18 193-39-504/15/23 15:46447 176 1 Isophorone ND ug/kg 04/16/23 14:18 78-59-104/15/23 15:46447 199 1 1-Methylnaphthalene ND ug/kg 04/16/23 14:18 90-12-004/15/23 15:46447 157 1 2-Methylnaphthalene ND ug/kg 04/16/23 14:18 91-57-604/15/23 15:46447 179 1 2-Methylphenol(o-Cresol)ND ug/kg 04/16/23 14:18 95-48-704/15/23 15:46447 183 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 04/16/23 14:18 15831-10-404/15/23 15:46447 180 1 Naphthalene ND ug/kg 04/16/23 14:18 91-20-304/15/23 15:46447 152 1 2-Nitroaniline ND ug/kg 04/16/23 14:18 88-74-404/15/23 15:462240 366 1 3-Nitroaniline ND ug/kg 04/16/23 14:18 99-09-204/15/23 15:462240 351 1 4-Nitroaniline ND ug/kg 04/16/23 14:18 100-01-604/15/23 15:46894 340 1 Nitrobenzene ND ug/kg 04/16/23 14:18 98-95-304/15/23 15:46447 207 1 2-Nitrophenol ND ug/kg 04/16/23 14:18 88-75-504/15/23 15:46447 194 1 4-Nitrophenol ND ug/kg 04/16/23 14:18 100-02-704/15/23 15:462240 865 1 N-Nitrosodimethylamine ND ug/kg 04/16/23 14:18 62-75-904/15/23 15:46447 150 1 N-Nitroso-di-n-propylamine ND ug/kg 04/16/23 14:18 621-64-704/15/23 15:46447 168 1 N-Nitrosodiphenylamine ND ug/kg 04/16/23 14:18 86-30-604/15/23 15:46447 159 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 04/16/23 14:18 108-60-104/15/23 15:46447 213 1 Pentachlorophenol ND ug/kg 04/16/23 14:18 87-86-504/15/23 15:46894 438 1 Phenanthrene ND ug/kg 04/16/23 14:18 85-01-804/15/23 15:46447 146 1 Phenol ND ug/kg 04/16/23 14:18 108-95-204/15/23 15:46447 199 1 Pyrene ND ug/kg 04/16/23 14:18 129-00-004/15/23 15:46447 182 1 Pyridine ND ug/kg 04/16/23 14:18 110-86-104/15/23 15:46447 141 1 1,2,4-Trichlorobenzene ND ug/kg 04/16/23 14:18 120-82-104/15/23 15:46447 176 1 2,4,5-Trichlorophenol ND ug/kg 04/16/23 14:18 95-95-404/15/23 15:46447 205 1 2,4,6-Trichlorophenol ND ug/kg 04/16/23 14:18 88-06-204/15/23 15:46447 184 1 Surrogates Nitrobenzene-d5 (S)41 %04/16/23 14:18 4165-60-004/15/23 15:4610-130 1 2-Fluorobiphenyl (S)29 %04/16/23 14:18 321-60-804/15/23 15:4610-130 1 Terphenyl-d14 (S)58 %04/16/23 14:18 1718-51-004/15/23 15:4610-130 1 Phenol-d6 (S)45 %04/16/23 14:18 13127-88-304/15/23 15:4610-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-01 (5-7)Lab ID: 92662335001 Collected: 04/14/23 09:30 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)43 %04/16/23 14:18 367-12-404/15/23 15:4610-130 1 2,4,6-Tribromophenol (S)52 %04/16/23 14:18 118-79-604/15/23 15:4610-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 04/19/23 03:40 67-64-104/17/23 20:30152 48.7 1 Benzene ND ug/kg 04/19/23 03:40 71-43-204/17/23 20:307.6 3.0 1 Bromobenzene ND ug/kg 04/19/23 03:40 108-86-104/17/23 20:307.6 2.5 1 Bromochloromethane ND ug/kg 04/19/23 03:40 74-97-504/17/23 20:307.6 2.2 1 Bromodichloromethane ND ug/kg 04/19/23 03:40 75-27-404/17/23 20:307.6 2.9 1 Bromoform ND ug/kg 04/19/23 03:40 75-25-204/17/23 20:307.6 2.7 1 Bromomethane ND ug/kg 04/19/23 03:40 74-83-904/17/23 20:3030.3 23.5 1 2-Butanone (MEK)ND ug/kg 04/19/23 03:40 78-93-304/17/23 20:30152 36.4 1 n-Butylbenzene ND ug/kg 04/19/23 03:40 104-51-804/17/23 20:307.6 4.8 1 sec-Butylbenzene ND ug/kg 04/19/23 03:40 135-98-804/17/23 20:307.6 3.3 1 tert-Butylbenzene ND ug/kg 04/19/23 03:40 98-06-604/17/23 20:307.6 2.7 1 Carbon tetrachloride ND ug/kg 04/19/23 03:40 56-23-504/17/23 20:307.6 2.8 1 Chlorobenzene ND ug/kg 04/19/23 03:40 108-90-704/17/23 20:307.6 4.4 1 Chloroethane ND ug/kg 04/19/23 03:40 75-00-3 IH04/17/23 20:3015.2 5.9 1 Chloroform ND ug/kg 04/19/23 03:40 67-66-304/17/23 20:307.6 6.3 1 Chloromethane ND ug/kg 04/19/23 03:40 74-87-3 IH,L1,v104/17/23 20:3015.2 6.4 1 2-Chlorotoluene ND ug/kg 04/19/23 03:40 95-49-804/17/23 20:307.6 2.7 1 4-Chlorotoluene ND ug/kg 04/19/23 03:40 106-43-404/17/23 20:307.6 4.2 1 1,2-Dibromo-3-chloropropane ND ug/kg 04/19/23 03:40 96-12-804/17/23 20:307.6 2.9 1 Dibromochloromethane ND ug/kg 04/19/23 03:40 124-48-104/17/23 20:307.6 4.3 1 1,2-Dibromoethane (EDB)ND ug/kg 04/19/23 03:40 106-93-404/17/23 20:307.6 3.3 1 Dibromomethane ND ug/kg 04/19/23 03:40 74-95-304/17/23 20:307.6 1.6 1 1,2-Dichlorobenzene ND ug/kg 04/19/23 03:40 95-50-104/17/23 20:307.6 2.7 1 1,3-Dichlorobenzene ND ug/kg 04/19/23 03:40 541-73-104/17/23 20:307.6 2.3 1 1,4-Dichlorobenzene ND ug/kg 04/19/23 03:40 106-46-704/17/23 20:307.6 2.0 1 Dichlorodifluoromethane ND ug/kg 04/19/23 03:40 75-71-8 IH,v104/17/23 20:3015.2 7.7 1 1,1-Dichloroethane ND ug/kg 04/19/23 03:40 75-34-304/17/23 20:307.6 3.1 1 1,2-Dichloroethane ND ug/kg 04/19/23 03:40 107-06-204/17/23 20:307.6 5.0 1 1,1-Dichloroethene ND ug/kg 04/19/23 03:40 75-35-404/17/23 20:307.6 3.1 1 cis-1,2-Dichloroethene ND ug/kg 04/19/23 03:40 156-59-204/17/23 20:307.6 2.6 1 trans-1,2-Dichloroethene ND ug/kg 04/19/23 03:40 156-60-504/17/23 20:307.6 6.4 1 1,2-Dichloropropane ND ug/kg 04/19/23 03:40 78-87-504/17/23 20:307.6 2.3 1 1,3-Dichloropropane ND ug/kg 04/19/23 03:40 142-28-904/17/23 20:307.6 2.4 1 2,2-Dichloropropane ND ug/kg 04/19/23 03:40 594-20-704/17/23 20:307.6 5.7 1 1,1-Dichloropropene ND ug/kg 04/19/23 03:40 563-58-604/17/23 20:307.6 3.6 1 cis-1,3-Dichloropropene ND ug/kg 04/19/23 03:40 10061-01-504/17/23 20:307.6 2.1 1 trans-1,3-Dichloropropene ND ug/kg 04/19/23 03:40 10061-02-604/17/23 20:307.6 2.6 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-01 (5-7)Lab ID: 92662335001 Collected: 04/14/23 09:30 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Diisopropyl ether ND ug/kg 04/19/23 03:40 108-20-304/17/23 20:307.6 2.0 1 Ethylbenzene 3.9J ug/kg 04/19/23 03:40 100-41-404/17/23 20:307.6 3.5 1 Hexachloro-1,3-butadiene ND ug/kg 04/19/23 03:40 87-68-304/17/23 20:3015.2 12.4 1 2-Hexanone ND ug/kg 04/19/23 03:40 591-78-604/17/23 20:3075.8 7.3 1 Isopropylbenzene (Cumene)ND ug/kg 04/19/23 03:40 98-82-804/17/23 20:307.6 2.6 1 p-Isopropyltoluene ND ug/kg 04/19/23 03:40 99-87-604/17/23 20:307.6 3.7 1 Methylene Chloride 112 ug/kg 04/19/23 03:40 75-09-2 C904/17/23 20:3030.3 20.8 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/23 03:40 108-10-104/17/23 20:3075.8 7.3 1 Methyl-tert-butyl ether ND ug/kg 04/19/23 03:40 1634-04-404/17/23 20:307.6 2.8 1 Naphthalene ND ug/kg 04/19/23 03:40 91-20-304/17/23 20:307.6 4.0 1 n-Propylbenzene ND ug/kg 04/19/23 03:40 103-65-104/17/23 20:307.6 2.7 1 Styrene ND ug/kg 04/19/23 03:40 100-42-504/17/23 20:307.6 2.0 1 1,1,1,2-Tetrachloroethane ND ug/kg 04/19/23 03:40 630-20-604/17/23 20:307.6 2.9 1 1,1,2,2-Tetrachloroethane ND ug/kg 04/19/23 03:40 79-34-504/17/23 20:307.6 2.0 1 Tetrachloroethene ND ug/kg 04/19/23 03:40 127-18-404/17/23 20:307.6 2.4 1 Toluene ND ug/kg 04/19/23 03:40 108-88-304/17/23 20:307.6 5.2 1 1,2,3-Trichlorobenzene ND ug/kg 04/19/23 03:40 87-61-604/17/23 20:307.6 6.1 1 1,2,4-Trichlorobenzene ND ug/kg 04/19/23 03:40 120-82-104/17/23 20:307.6 6.4 1 1,1,1-Trichloroethane ND ug/kg 04/19/23 03:40 71-55-604/17/23 20:307.6 3.9 1 1,1,2-Trichloroethane ND ug/kg 04/19/23 03:40 79-00-504/17/23 20:307.6 2.5 1 Trichloroethene ND ug/kg 04/19/23 03:40 79-01-604/17/23 20:307.6 6.1 1 Trichlorofluoromethane ND ug/kg 04/19/23 03:40 75-69-404/17/23 20:307.6 4.2 1 1,2,3-Trichloropropane ND ug/kg 04/19/23 03:40 96-18-404/17/23 20:307.6 3.8 1 1,2,4-Trimethylbenzene ND ug/kg 04/19/23 03:40 95-63-604/17/23 20:307.6 4.5 1 1,3,5-Trimethylbenzene ND ug/kg 04/19/23 03:40 108-67-804/17/23 20:307.6 2.5 1 Vinyl acetate ND ug/kg 04/19/23 03:40 108-05-404/17/23 20:3075.8 15.6 1 Vinyl chloride ND ug/kg 04/19/23 03:40 75-01-4 IH04/17/23 20:3015.2 3.9 1 Xylene (Total)ND ug/kg 04/19/23 03:40 1330-20-704/17/23 20:3015.2 4.3 1 m&p-Xylene ND ug/kg 04/19/23 03:40 179601-23-104/17/23 20:3015.2 5.2 1 o-Xylene ND ug/kg 04/19/23 03:40 95-47-604/17/23 20:307.6 3.3 1 Surrogates Toluene-d8 (S)101 %04/19/23 03:40 2037-26-504/17/23 20:3070-130 1 4-Bromofluorobenzene (S)105 %04/19/23 03:40 460-00-404/17/23 20:3070-130 1 1,2-Dichloroethane-d4 (S)103 %04/19/23 03:40 17060-07-004/17/23 20:3070-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 26.9 %04/14/23 15:27 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 72.5 %04/20/23 11:1404/20/23 10:571 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-01 (5-7)Lab ID: 92662335001 Collected: 04/14/23 09:30 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.819J mg/kg 04/24/23 03:38 18540-29-9 J04/21/23 11:531.38 0.351 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-02 (5-7)Lab ID: 92662335002 Collected: 04/14/23 09:20 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 2.1 mg/kg 04/20/23 14:34 7440-38-204/20/23 10:030.63 0.18 1 Barium 13.2 mg/kg 04/20/23 14:34 7440-39-304/20/23 10:030.38 0.095 1 Cadmium ND mg/kg 04/20/23 14:34 7440-43-904/20/23 10:030.10 0.037 1 Chromium 47.7 mg/kg 04/20/23 14:34 7440-47-304/20/23 10:032.5 0.49 1 Lead 4.9 mg/kg 04/20/23 14:34 7439-92-104/20/23 10:030.63 0.12 1 Selenium 1.1 mg/kg 04/20/23 14:34 7782-49-204/20/23 10:030.63 0.13 1 Silver ND mg/kg 04/20/23 14:34 7440-22-404/20/23 10:030.63 0.26 1 Analytical Method: EPA 7471B Preparation Method: EPA 7471B Pace Analytical Services - Minneapolis 7471B Mercury Mercury 0.021J mg/kg 04/21/23 11:11 7439-97-604/20/23 10:060.025 0.011 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 04/17/23 10:52 83-32-904/15/23 15:46429 151 1 Acenaphthylene ND ug/kg 04/17/23 10:52 208-96-804/15/23 15:46429 151 1 Aniline ND ug/kg 04/17/23 10:52 62-53-304/15/23 15:46429 168 1 Anthracene ND ug/kg 04/17/23 10:52 120-12-704/15/23 15:46429 141 1 Benzo(a)anthracene ND ug/kg 04/17/23 10:52 56-55-304/15/23 15:46429 143 1 Benzo(a)pyrene ND ug/kg 04/17/23 10:52 50-32-804/15/23 15:46429 148 1 Benzo(b)fluoranthene ND ug/kg 04/17/23 10:52 205-99-204/15/23 15:46429 143 1 Benzo(g,h,i)perylene ND ug/kg 04/17/23 10:52 191-24-204/15/23 15:46429 167 1 Benzo(k)fluoranthene ND ug/kg 04/17/23 10:52 207-08-904/15/23 15:46429 151 1 Benzoic Acid ND ug/kg 04/17/23 10:52 65-85-0 L204/15/23 15:462150 923 1 Benzyl alcohol ND ug/kg 04/17/23 10:52 100-51-604/15/23 15:46859 325 1 4-Bromophenylphenyl ether ND ug/kg 04/17/23 10:52 101-55-304/15/23 15:46429 165 1 Butylbenzylphthalate ND ug/kg 04/17/23 10:52 85-68-704/15/23 15:46429 181 1 4-Chloro-3-methylphenol ND ug/kg 04/17/23 10:52 59-50-704/15/23 15:46859 302 1 4-Chloroaniline ND ug/kg 04/17/23 10:52 106-47-804/15/23 15:46859 337 1 bis(2-Chloroethoxy)methane ND ug/kg 04/17/23 10:52 111-91-104/15/23 15:46429 178 1 bis(2-Chloroethyl) ether ND ug/kg 04/17/23 10:52 111-44-404/15/23 15:46429 161 1 2-Chloronaphthalene ND ug/kg 04/17/23 10:52 91-58-704/15/23 15:46429 170 1 2-Chlorophenol ND ug/kg 04/17/23 10:52 95-57-804/15/23 15:46429 161 1 4-Chlorophenylphenyl ether ND ug/kg 04/17/23 10:52 7005-72-304/15/23 15:46429 160 1 Chrysene ND ug/kg 04/17/23 10:52 218-01-904/15/23 15:46429 156 1 Dibenz(a,h)anthracene ND ug/kg 04/17/23 10:52 53-70-304/15/23 15:46429 165 1 Dibenzofuran ND ug/kg 04/17/23 10:52 132-64-904/15/23 15:46429 155 1 1,2-Dichlorobenzene ND ug/kg 04/17/23 10:52 95-50-104/15/23 15:46429 155 1 1,3-Dichlorobenzene ND ug/kg 04/17/23 10:52 541-73-104/15/23 15:46429 152 1 1,4-Dichlorobenzene ND ug/kg 04/17/23 10:52 106-46-704/15/23 15:46429 164 1 3,3'-Dichlorobenzidine ND ug/kg 04/17/23 10:52 91-94-104/15/23 15:46859 290 1 2,4-Dichlorophenol ND ug/kg 04/17/23 10:52 120-83-204/15/23 15:46429 168 1 Diethylphthalate ND ug/kg 04/17/23 10:52 84-66-204/15/23 15:46429 157 1 2,4-Dimethylphenol ND ug/kg 04/17/23 10:52 105-67-904/15/23 15:46429 178 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-02 (5-7)Lab ID: 92662335002 Collected: 04/14/23 09:20 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 04/17/23 10:52 131-11-304/15/23 15:46429 156 1 Di-n-butylphthalate ND ug/kg 04/17/23 10:52 84-74-204/15/23 15:46429 144 1 4,6-Dinitro-2-methylphenol ND ug/kg 04/17/23 10:52 534-52-104/15/23 15:46859 401 1 2,4-Dinitrophenol ND ug/kg 04/17/23 10:52 51-28-504/15/23 15:462150 1330 1 2,4-Dinitrotoluene ND ug/kg 04/17/23 10:52 121-14-204/15/23 15:46429 165 1 2,6-Dinitrotoluene ND ug/kg 04/17/23 10:52 606-20-204/15/23 15:46429 157 1 Di-n-octylphthalate ND ug/kg 04/17/23 10:52 117-84-004/15/23 15:46429 169 1 bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/23 10:52 117-81-704/15/23 15:46429 167 1 Fluoranthene ND ug/kg 04/17/23 10:52 206-44-004/15/23 15:46429 147 1 Fluorene ND ug/kg 04/17/23 10:52 86-73-704/15/23 15:46429 151 1 Hexachloro-1,3-butadiene ND ug/kg 04/17/23 10:52 87-68-304/15/23 15:46429 186 1 Hexachlorobenzene ND ug/kg 04/17/23 10:52 118-74-104/15/23 15:46429 168 1 Hexachlorocyclopentadiene ND ug/kg 04/17/23 10:52 77-47-404/15/23 15:46429 246 1 Hexachloroethane ND ug/kg 04/17/23 10:52 67-72-104/15/23 15:46429 164 1 Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/23 10:52 193-39-504/15/23 15:46429 169 1 Isophorone ND ug/kg 04/17/23 10:52 78-59-104/15/23 15:46429 191 1 1-Methylnaphthalene ND ug/kg 04/17/23 10:52 90-12-004/15/23 15:46429 151 1 2-Methylnaphthalene ND ug/kg 04/17/23 10:52 91-57-604/15/23 15:46429 172 1 2-Methylphenol(o-Cresol)ND ug/kg 04/17/23 10:52 95-48-704/15/23 15:46429 176 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/23 10:52 15831-10-404/15/23 15:46429 173 1 Naphthalene ND ug/kg 04/17/23 10:52 91-20-304/15/23 15:46429 146 1 2-Nitroaniline ND ug/kg 04/17/23 10:52 88-74-404/15/23 15:462150 351 1 3-Nitroaniline ND ug/kg 04/17/23 10:52 99-09-204/15/23 15:462150 337 1 4-Nitroaniline ND ug/kg 04/17/23 10:52 100-01-604/15/23 15:46859 327 1 Nitrobenzene ND ug/kg 04/17/23 10:52 98-95-304/15/23 15:46429 199 1 2-Nitrophenol ND ug/kg 04/17/23 10:52 88-75-504/15/23 15:46429 186 1 4-Nitrophenol ND ug/kg 04/17/23 10:52 100-02-704/15/23 15:462150 830 1 N-Nitrosodimethylamine ND ug/kg 04/17/23 10:52 62-75-904/15/23 15:46429 144 1 N-Nitroso-di-n-propylamine ND ug/kg 04/17/23 10:52 621-64-704/15/23 15:46429 161 1 N-Nitrosodiphenylamine ND ug/kg 04/17/23 10:52 86-30-604/15/23 15:46429 152 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/23 10:52 108-60-104/15/23 15:46429 204 1 Pentachlorophenol ND ug/kg 04/17/23 10:52 87-86-504/15/23 15:46859 420 1 Phenanthrene ND ug/kg 04/17/23 10:52 85-01-804/15/23 15:46429 141 1 Phenol ND ug/kg 04/17/23 10:52 108-95-204/15/23 15:46429 191 1 Pyrene ND ug/kg 04/17/23 10:52 129-00-004/15/23 15:46429 174 1 Pyridine ND ug/kg 04/17/23 10:52 110-86-104/15/23 15:46429 135 1 1,2,4-Trichlorobenzene ND ug/kg 04/17/23 10:52 120-82-104/15/23 15:46429 169 1 2,4,5-Trichlorophenol ND ug/kg 04/17/23 10:52 95-95-404/15/23 15:46429 197 1 2,4,6-Trichlorophenol ND ug/kg 04/17/23 10:52 88-06-204/15/23 15:46429 177 1 Surrogates Nitrobenzene-d5 (S)35 %04/17/23 10:52 4165-60-004/15/23 15:4610-130 1 2-Fluorobiphenyl (S)44 %04/17/23 10:52 321-60-804/15/23 15:4610-130 1 Terphenyl-d14 (S)61 %04/17/23 10:52 1718-51-004/15/23 15:4610-130 1 Phenol-d6 (S)35 %04/17/23 10:52 13127-88-304/15/23 15:4610-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-02 (5-7)Lab ID: 92662335002 Collected: 04/14/23 09:20 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)34 %04/17/23 10:52 367-12-404/15/23 15:4610-130 1 2,4,6-Tribromophenol (S)52 %04/17/23 10:52 118-79-604/15/23 15:4610-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 04/19/23 03:58 67-64-104/17/23 20:30198 63.5 1 Benzene ND ug/kg 04/19/23 03:58 71-43-204/17/23 20:309.9 3.9 1 Bromobenzene ND ug/kg 04/19/23 03:58 108-86-104/17/23 20:309.9 3.2 1 Bromochloromethane ND ug/kg 04/19/23 03:58 74-97-504/17/23 20:309.9 2.9 1 Bromodichloromethane ND ug/kg 04/19/23 03:58 75-27-404/17/23 20:309.9 3.8 1 Bromoform ND ug/kg 04/19/23 03:58 75-25-204/17/23 20:309.9 3.5 1 Bromomethane ND ug/kg 04/19/23 03:58 74-83-904/17/23 20:3039.6 30.7 1 2-Butanone (MEK)ND ug/kg 04/19/23 03:58 78-93-304/17/23 20:30198 47.5 1 n-Butylbenzene ND ug/kg 04/19/23 03:58 104-51-804/17/23 20:309.9 6.2 1 sec-Butylbenzene ND ug/kg 04/19/23 03:58 135-98-804/17/23 20:309.9 4.4 1 tert-Butylbenzene ND ug/kg 04/19/23 03:58 98-06-604/17/23 20:309.9 3.5 1 Carbon tetrachloride ND ug/kg 04/19/23 03:58 56-23-504/17/23 20:309.9 3.7 1 Chlorobenzene ND ug/kg 04/19/23 03:58 108-90-704/17/23 20:309.9 5.7 1 Chloroethane ND ug/kg 04/19/23 03:58 75-00-3 IH04/17/23 20:3019.8 7.6 1 Chloroform ND ug/kg 04/19/23 03:58 67-66-304/17/23 20:309.9 8.3 1 Chloromethane ND ug/kg 04/19/23 03:58 74-87-3 IH,L1,v104/17/23 20:3019.8 8.3 1 2-Chlorotoluene ND ug/kg 04/19/23 03:58 95-49-804/17/23 20:309.9 3.5 1 4-Chlorotoluene ND ug/kg 04/19/23 03:58 106-43-404/17/23 20:309.9 5.5 1 1,2-Dibromo-3-chloropropane ND ug/kg 04/19/23 03:58 96-12-804/17/23 20:309.9 3.8 1 Dibromochloromethane ND ug/kg 04/19/23 03:58 124-48-104/17/23 20:309.9 5.6 1 1,2-Dibromoethane (EDB)ND ug/kg 04/19/23 03:58 106-93-404/17/23 20:309.9 4.4 1 Dibromomethane ND ug/kg 04/19/23 03:58 74-95-304/17/23 20:309.9 2.1 1 1,2-Dichlorobenzene ND ug/kg 04/19/23 03:58 95-50-104/17/23 20:309.9 3.6 1 1,3-Dichlorobenzene ND ug/kg 04/19/23 03:58 541-73-104/17/23 20:309.9 3.1 1 1,4-Dichlorobenzene ND ug/kg 04/19/23 03:58 106-46-704/17/23 20:309.9 2.6 1 Dichlorodifluoromethane ND ug/kg 04/19/23 03:58 75-71-8 IH,v104/17/23 20:3019.8 10.1 1 1,1-Dichloroethane ND ug/kg 04/19/23 03:58 75-34-304/17/23 20:309.9 4.1 1 1,2-Dichloroethane ND ug/kg 04/19/23 03:58 107-06-204/17/23 20:309.9 6.6 1 1,1-Dichloroethene ND ug/kg 04/19/23 03:58 75-35-404/17/23 20:309.9 4.1 1 cis-1,2-Dichloroethene ND ug/kg 04/19/23 03:58 156-59-204/17/23 20:309.9 3.4 1 trans-1,2-Dichloroethene ND ug/kg 04/19/23 03:58 156-60-504/17/23 20:309.9 8.4 1 1,2-Dichloropropane ND ug/kg 04/19/23 03:58 78-87-504/17/23 20:309.9 3.0 1 1,3-Dichloropropane ND ug/kg 04/19/23 03:58 142-28-904/17/23 20:309.9 3.1 1 2,2-Dichloropropane ND ug/kg 04/19/23 03:58 594-20-704/17/23 20:309.9 7.5 1 1,1-Dichloropropene ND ug/kg 04/19/23 03:58 563-58-604/17/23 20:309.9 4.7 1 cis-1,3-Dichloropropene ND ug/kg 04/19/23 03:58 10061-01-504/17/23 20:309.9 2.7 1 trans-1,3-Dichloropropene ND ug/kg 04/19/23 03:58 10061-02-604/17/23 20:309.9 3.4 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-02 (5-7)Lab ID: 92662335002 Collected: 04/14/23 09:20 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Diisopropyl ether ND ug/kg 04/19/23 03:58 108-20-304/17/23 20:309.9 2.7 1 Ethylbenzene ND ug/kg 04/19/23 03:58 100-41-404/17/23 20:309.9 4.6 1 Hexachloro-1,3-butadiene ND ug/kg 04/19/23 03:58 87-68-304/17/23 20:3019.8 16.2 1 2-Hexanone ND ug/kg 04/19/23 03:58 591-78-604/17/23 20:3099.0 9.5 1 Isopropylbenzene (Cumene)ND ug/kg 04/19/23 03:58 98-82-804/17/23 20:309.9 3.4 1 p-Isopropyltoluene ND ug/kg 04/19/23 03:58 99-87-604/17/23 20:309.9 4.9 1 Methylene Chloride 119 ug/kg 04/19/23 03:58 75-09-2 C904/17/23 20:3039.6 27.1 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/23 03:58 108-10-104/17/23 20:3099.0 9.5 1 Methyl-tert-butyl ether ND ug/kg 04/19/23 03:58 1634-04-404/17/23 20:309.9 3.7 1 Naphthalene ND ug/kg 04/19/23 03:58 91-20-304/17/23 20:309.9 5.2 1 n-Propylbenzene ND ug/kg 04/19/23 03:58 103-65-104/17/23 20:309.9 3.5 1 Styrene ND ug/kg 04/19/23 03:58 100-42-504/17/23 20:309.9 2.6 1 1,1,1,2-Tetrachloroethane ND ug/kg 04/19/23 03:58 630-20-604/17/23 20:309.9 3.8 1 1,1,2,2-Tetrachloroethane ND ug/kg 04/19/23 03:58 79-34-504/17/23 20:309.9 2.6 1 Tetrachloroethene ND ug/kg 04/19/23 03:58 127-18-404/17/23 20:309.9 3.1 1 Toluene ND ug/kg 04/19/23 03:58 108-88-304/17/23 20:309.9 6.8 1 1,2,3-Trichlorobenzene ND ug/kg 04/19/23 03:58 87-61-604/17/23 20:309.9 8.0 1 1,2,4-Trichlorobenzene ND ug/kg 04/19/23 03:58 120-82-104/17/23 20:309.9 8.3 1 1,1,1-Trichloroethane ND ug/kg 04/19/23 03:58 71-55-604/17/23 20:309.9 5.1 1 1,1,2-Trichloroethane ND ug/kg 04/19/23 03:58 79-00-504/17/23 20:309.9 3.3 1 Trichloroethene ND ug/kg 04/19/23 03:58 79-01-604/17/23 20:309.9 8.0 1 Trichlorofluoromethane ND ug/kg 04/19/23 03:58 75-69-404/17/23 20:309.9 5.4 1 1,2,3-Trichloropropane ND ug/kg 04/19/23 03:58 96-18-404/17/23 20:309.9 5.0 1 1,2,4-Trimethylbenzene ND ug/kg 04/19/23 03:58 95-63-604/17/23 20:309.9 5.9 1 1,3,5-Trimethylbenzene ND ug/kg 04/19/23 03:58 108-67-804/17/23 20:309.9 3.3 1 Vinyl acetate ND ug/kg 04/19/23 03:58 108-05-404/17/23 20:3099.0 20.4 1 Vinyl chloride ND ug/kg 04/19/23 03:58 75-01-4 IH04/17/23 20:3019.8 5.0 1 Xylene (Total)ND ug/kg 04/19/23 03:58 1330-20-704/17/23 20:3019.8 5.6 1 m&p-Xylene ND ug/kg 04/19/23 03:58 179601-23-104/17/23 20:3019.8 6.8 1 o-Xylene ND ug/kg 04/19/23 03:58 95-47-604/17/23 20:309.9 4.4 1 Surrogates Toluene-d8 (S)102 %04/19/23 03:58 2037-26-504/17/23 20:3070-130 1 4-Bromofluorobenzene (S)104 %04/19/23 03:58 460-00-404/17/23 20:3070-130 1 1,2-Dichloroethane-d4 (S)102 %04/19/23 03:58 17060-07-004/17/23 20:3070-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 24.4 %04/14/23 15:27 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 75.6 %04/20/23 11:1404/20/23 10:571 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-02 (5-7)Lab ID: 92662335002 Collected: 04/14/23 09:20 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.921J mg/kg 04/24/23 03:43 18540-29-9 J04/21/23 11:531.32 0.337 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-03 (4-5)Lab ID: 92662335003 Collected: 04/14/23 11:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010D Preparation Method: EPA 3015A Leachate Method/Date: EPA 1311; 04/26/23 14:12 Pace Analytical Services - Minneapolis 6010D MET ICP, TCLP MICRO Chromium ND mg/L 04/27/23 13:35 7440-47-304/27/23 10:550.10 0.0043 1 Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 2.4 mg/kg 04/20/23 14:37 7440-38-204/20/23 10:030.66 0.19 1 Barium 11.5 mg/kg 04/20/23 14:37 7440-39-304/20/23 10:030.40 0.099 1 Cadmium ND mg/kg 04/20/23 14:37 7440-43-904/20/23 10:030.11 0.039 1 Chromium 124 mg/kg 04/20/23 14:37 7440-47-304/20/23 10:032.6 0.51 1 Lead 9.1 mg/kg 04/20/23 14:37 7439-92-104/20/23 10:030.66 0.12 1 Selenium 0.70 mg/kg 04/20/23 14:37 7782-49-204/20/23 10:030.66 0.14 1 Silver ND mg/kg 04/20/23 14:37 7440-22-404/20/23 10:030.66 0.27 1 Analytical Method: EPA 7471B Preparation Method: EPA 7471B Pace Analytical Services - Minneapolis 7471B Mercury Mercury 0.084 mg/kg 04/21/23 11:13 7439-97-604/20/23 10:060.025 0.011 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 04/17/23 11:20 83-32-904/15/23 15:46438 154 1 Acenaphthylene ND ug/kg 04/17/23 11:20 208-96-804/15/23 15:46438 154 1 Aniline ND ug/kg 04/17/23 11:20 62-53-304/15/23 15:46438 171 1 Anthracene ND ug/kg 04/17/23 11:20 120-12-704/15/23 15:46438 143 1 Benzo(a)anthracene ND ug/kg 04/17/23 11:20 56-55-304/15/23 15:46438 146 1 Benzo(a)pyrene ND ug/kg 04/17/23 11:20 50-32-804/15/23 15:46438 151 1 Benzo(b)fluoranthene ND ug/kg 04/17/23 11:20 205-99-204/15/23 15:46438 146 1 Benzo(g,h,i)perylene ND ug/kg 04/17/23 11:20 191-24-204/15/23 15:46438 170 1 Benzo(k)fluoranthene ND ug/kg 04/17/23 11:20 207-08-904/15/23 15:46438 154 1 Benzoic Acid ND ug/kg 04/17/23 11:20 65-85-0 L204/15/23 15:462190 942 1 Benzyl alcohol ND ug/kg 04/17/23 11:20 100-51-604/15/23 15:46876 332 1 4-Bromophenylphenyl ether ND ug/kg 04/17/23 11:20 101-55-304/15/23 15:46438 169 1 Butylbenzylphthalate ND ug/kg 04/17/23 11:20 85-68-704/15/23 15:46438 185 1 4-Chloro-3-methylphenol ND ug/kg 04/17/23 11:20 59-50-704/15/23 15:46876 308 1 4-Chloroaniline ND ug/kg 04/17/23 11:20 106-47-804/15/23 15:46876 344 1 bis(2-Chloroethoxy)methane ND ug/kg 04/17/23 11:20 111-91-104/15/23 15:46438 182 1 bis(2-Chloroethyl) ether ND ug/kg 04/17/23 11:20 111-44-404/15/23 15:46438 165 1 2-Chloronaphthalene ND ug/kg 04/17/23 11:20 91-58-704/15/23 15:46438 174 1 2-Chlorophenol ND ug/kg 04/17/23 11:20 95-57-804/15/23 15:46438 165 1 4-Chlorophenylphenyl ether ND ug/kg 04/17/23 11:20 7005-72-304/15/23 15:46438 163 1 Chrysene ND ug/kg 04/17/23 11:20 218-01-904/15/23 15:46438 159 1 Dibenz(a,h)anthracene ND ug/kg 04/17/23 11:20 53-70-304/15/23 15:46438 169 1 Dibenzofuran ND ug/kg 04/17/23 11:20 132-64-904/15/23 15:46438 158 1 1,2-Dichlorobenzene ND ug/kg 04/17/23 11:20 95-50-104/15/23 15:46438 158 1 1,3-Dichlorobenzene ND ug/kg 04/17/23 11:20 541-73-104/15/23 15:46438 155 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-03 (4-5)Lab ID: 92662335003 Collected: 04/14/23 11:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave 1,4-Dichlorobenzene ND ug/kg 04/17/23 11:20 106-46-704/15/23 15:46438 167 1 3,3'-Dichlorobenzidine ND ug/kg 04/17/23 11:20 91-94-104/15/23 15:46876 296 1 2,4-Dichlorophenol ND ug/kg 04/17/23 11:20 120-83-204/15/23 15:46438 171 1 Diethylphthalate ND ug/kg 04/17/23 11:20 84-66-204/15/23 15:46438 161 1 2,4-Dimethylphenol ND ug/kg 04/17/23 11:20 105-67-904/15/23 15:46438 182 1 Dimethylphthalate ND ug/kg 04/17/23 11:20 131-11-304/15/23 15:46438 159 1 Di-n-butylphthalate ND ug/kg 04/17/23 11:20 84-74-204/15/23 15:46438 147 1 4,6-Dinitro-2-methylphenol ND ug/kg 04/17/23 11:20 534-52-104/15/23 15:46876 409 1 2,4-Dinitrophenol ND ug/kg 04/17/23 11:20 51-28-504/15/23 15:462190 1350 1 2,4-Dinitrotoluene ND ug/kg 04/17/23 11:20 121-14-204/15/23 15:46438 169 1 2,6-Dinitrotoluene ND ug/kg 04/17/23 11:20 606-20-204/15/23 15:46438 161 1 Di-n-octylphthalate ND ug/kg 04/17/23 11:20 117-84-004/15/23 15:46438 173 1 bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/23 11:20 117-81-704/15/23 15:46438 170 1 Fluoranthene ND ug/kg 04/17/23 11:20 206-44-004/15/23 15:46438 150 1 Fluorene ND ug/kg 04/17/23 11:20 86-73-704/15/23 15:46438 154 1 Hexachloro-1,3-butadiene ND ug/kg 04/17/23 11:20 87-68-304/15/23 15:46438 190 1 Hexachlorobenzene ND ug/kg 04/17/23 11:20 118-74-104/15/23 15:46438 171 1 Hexachlorocyclopentadiene ND ug/kg 04/17/23 11:20 77-47-404/15/23 15:46438 251 1 Hexachloroethane ND ug/kg 04/17/23 11:20 67-72-104/15/23 15:46438 167 1 Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/23 11:20 193-39-504/15/23 15:46438 173 1 Isophorone ND ug/kg 04/17/23 11:20 78-59-104/15/23 15:46438 195 1 1-Methylnaphthalene ND ug/kg 04/17/23 11:20 90-12-004/15/23 15:46438 154 1 2-Methylnaphthalene ND ug/kg 04/17/23 11:20 91-57-604/15/23 15:46438 175 1 2-Methylphenol(o-Cresol)ND ug/kg 04/17/23 11:20 95-48-704/15/23 15:46438 179 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/23 11:20 15831-10-404/15/23 15:46438 177 1 Naphthalene ND ug/kg 04/17/23 11:20 91-20-304/15/23 15:46438 149 1 2-Nitroaniline ND ug/kg 04/17/23 11:20 88-74-404/15/23 15:462190 359 1 3-Nitroaniline ND ug/kg 04/17/23 11:20 99-09-204/15/23 15:462190 344 1 4-Nitroaniline ND ug/kg 04/17/23 11:20 100-01-604/15/23 15:46876 333 1 Nitrobenzene ND ug/kg 04/17/23 11:20 98-95-304/15/23 15:46438 203 1 2-Nitrophenol ND ug/kg 04/17/23 11:20 88-75-504/15/23 15:46438 190 1 4-Nitrophenol ND ug/kg 04/17/23 11:20 100-02-704/15/23 15:462190 847 1 N-Nitrosodimethylamine ND ug/kg 04/17/23 11:20 62-75-904/15/23 15:46438 147 1 N-Nitroso-di-n-propylamine ND ug/kg 04/17/23 11:20 621-64-704/15/23 15:46438 165 1 N-Nitrosodiphenylamine ND ug/kg 04/17/23 11:20 86-30-604/15/23 15:46438 155 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/23 11:20 108-60-104/15/23 15:46438 208 1 Pentachlorophenol ND ug/kg 04/17/23 11:20 87-86-504/15/23 15:46876 429 1 Phenanthrene ND ug/kg 04/17/23 11:20 85-01-804/15/23 15:46438 143 1 Phenol ND ug/kg 04/17/23 11:20 108-95-204/15/23 15:46438 195 1 Pyrene ND ug/kg 04/17/23 11:20 129-00-004/15/23 15:46438 178 1 Pyridine ND ug/kg 04/17/23 11:20 110-86-104/15/23 15:46438 138 1 1,2,4-Trichlorobenzene ND ug/kg 04/17/23 11:20 120-82-104/15/23 15:46438 173 1 2,4,5-Trichlorophenol ND ug/kg 04/17/23 11:20 95-95-404/15/23 15:46438 201 1 2,4,6-Trichlorophenol ND ug/kg 04/17/23 11:20 88-06-204/15/23 15:46438 181 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-03 (4-5)Lab ID: 92662335003 Collected: 04/14/23 11:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates Nitrobenzene-d5 (S)52 %04/17/23 11:20 4165-60-004/15/23 15:4610-130 1 2-Fluorobiphenyl (S)35 %04/17/23 11:20 321-60-804/15/23 15:4610-130 1 Terphenyl-d14 (S)81 %04/17/23 11:20 1718-51-004/15/23 15:4610-130 1 Phenol-d6 (S)54 %04/17/23 11:20 13127-88-304/15/23 15:4610-130 1 2-Fluorophenol (S)52 %04/17/23 11:20 367-12-404/15/23 15:4610-130 1 2,4,6-Tribromophenol (S)64 %04/17/23 11:20 118-79-604/15/23 15:4610-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 04/19/23 04:33 67-64-104/17/23 20:30183 58.6 1 Benzene ND ug/kg 04/19/23 04:33 71-43-204/17/23 20:309.1 3.6 1 Bromobenzene ND ug/kg 04/19/23 04:33 108-86-104/17/23 20:309.1 3.0 1 Bromochloromethane ND ug/kg 04/19/23 04:33 74-97-504/17/23 20:309.1 2.7 1 Bromodichloromethane ND ug/kg 04/19/23 04:33 75-27-404/17/23 20:309.1 3.5 1 Bromoform ND ug/kg 04/19/23 04:33 75-25-204/17/23 20:309.1 3.2 1 Bromomethane ND ug/kg 04/19/23 04:33 74-83-904/17/23 20:3036.5 28.3 1 2-Butanone (MEK)ND ug/kg 04/19/23 04:33 78-93-304/17/23 20:30183 43.8 1 n-Butylbenzene ND ug/kg 04/19/23 04:33 104-51-804/17/23 20:309.1 5.8 1 sec-Butylbenzene ND ug/kg 04/19/23 04:33 135-98-804/17/23 20:309.1 4.0 1 tert-Butylbenzene ND ug/kg 04/19/23 04:33 98-06-604/17/23 20:309.1 3.2 1 Carbon tetrachloride ND ug/kg 04/19/23 04:33 56-23-504/17/23 20:309.1 3.4 1 Chlorobenzene ND ug/kg 04/19/23 04:33 108-90-704/17/23 20:309.1 5.2 1 Chloroethane ND ug/kg 04/19/23 04:33 75-00-3 IH04/17/23 20:3018.3 7.0 1 Chloroform ND ug/kg 04/19/23 04:33 67-66-304/17/23 20:309.1 7.6 1 Chloromethane ND ug/kg 04/19/23 04:33 74-87-3 IH,L1, v104/17/23 20:3018.3 7.7 1 2-Chlorotoluene ND ug/kg 04/19/23 04:33 95-49-804/17/23 20:309.1 3.2 1 4-Chlorotoluene ND ug/kg 04/19/23 04:33 106-43-404/17/23 20:309.1 5.1 1 1,2-Dibromo-3-chloropropane ND ug/kg 04/19/23 04:33 96-12-804/17/23 20:309.1 3.5 1 Dibromochloromethane ND ug/kg 04/19/23 04:33 124-48-104/17/23 20:309.1 5.1 1 1,2-Dibromoethane (EDB)ND ug/kg 04/19/23 04:33 106-93-404/17/23 20:309.1 4.0 1 Dibromomethane ND ug/kg 04/19/23 04:33 74-95-304/17/23 20:309.1 2.0 1 1,2-Dichlorobenzene ND ug/kg 04/19/23 04:33 95-50-104/17/23 20:309.1 3.3 1 1,3-Dichlorobenzene ND ug/kg 04/19/23 04:33 541-73-104/17/23 20:309.1 2.8 1 1,4-Dichlorobenzene ND ug/kg 04/19/23 04:33 106-46-704/17/23 20:309.1 2.4 1 Dichlorodifluoromethane ND ug/kg 04/19/23 04:33 75-71-8 IH,v104/17/23 20:3018.3 9.3 1 1,1-Dichloroethane ND ug/kg 04/19/23 04:33 75-34-304/17/23 20:309.1 3.8 1 1,2-Dichloroethane ND ug/kg 04/19/23 04:33 107-06-204/17/23 20:309.1 6.0 1 1,1-Dichloroethene ND ug/kg 04/19/23 04:33 75-35-404/17/23 20:309.1 3.8 1 cis-1,2-Dichloroethene ND ug/kg 04/19/23 04:33 156-59-204/17/23 20:309.1 3.1 1 trans-1,2-Dichloroethene ND ug/kg 04/19/23 04:33 156-60-504/17/23 20:309.1 7.8 1 1,2-Dichloropropane ND ug/kg 04/19/23 04:33 78-87-504/17/23 20:309.1 2.7 1 1,3-Dichloropropane ND ug/kg 04/19/23 04:33 142-28-904/17/23 20:309.1 2.8 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-03 (4-5)Lab ID: 92662335003 Collected: 04/14/23 11:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles 2,2-Dichloropropane ND ug/kg 04/19/23 04:33 594-20-704/17/23 20:309.1 6.9 1 1,1-Dichloropropene ND ug/kg 04/19/23 04:33 563-58-604/17/23 20:309.1 4.4 1 cis-1,3-Dichloropropene ND ug/kg 04/19/23 04:33 10061-01-504/17/23 20:309.1 2.5 1 trans-1,3-Dichloropropene ND ug/kg 04/19/23 04:33 10061-02-604/17/23 20:309.1 3.1 1 Diisopropyl ether ND ug/kg 04/19/23 04:33 108-20-304/17/23 20:309.1 2.5 1 Ethylbenzene ND ug/kg 04/19/23 04:33 100-41-404/17/23 20:309.1 4.3 1 Hexachloro-1,3-butadiene ND ug/kg 04/19/23 04:33 87-68-304/17/23 20:3018.3 14.9 1 2-Hexanone ND ug/kg 04/19/23 04:33 591-78-604/17/23 20:3091.3 8.8 1 Isopropylbenzene (Cumene)ND ug/kg 04/19/23 04:33 98-82-804/17/23 20:309.1 3.1 1 p-Isopropyltoluene ND ug/kg 04/19/23 04:33 99-87-604/17/23 20:309.1 4.5 1 Methylene Chloride 145 ug/kg 04/19/23 04:33 75-09-2 C904/17/23 20:3036.5 25.0 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/23 04:33 108-10-104/17/23 20:3091.3 8.8 1 Methyl-tert-butyl ether ND ug/kg 04/19/23 04:33 1634-04-404/17/23 20:309.1 3.4 1 Naphthalene ND ug/kg 04/19/23 04:33 91-20-304/17/23 20:309.1 4.8 1 n-Propylbenzene ND ug/kg 04/19/23 04:33 103-65-104/17/23 20:309.1 3.2 1 Styrene ND ug/kg 04/19/23 04:33 100-42-504/17/23 20:309.1 2.4 1 1,1,1,2-Tetrachloroethane ND ug/kg 04/19/23 04:33 630-20-604/17/23 20:309.1 3.5 1 1,1,2,2-Tetrachloroethane ND ug/kg 04/19/23 04:33 79-34-504/17/23 20:309.1 2.4 1 Tetrachloroethene ND ug/kg 04/19/23 04:33 127-18-404/17/23 20:309.1 2.9 1 Toluene ND ug/kg 04/19/23 04:33 108-88-304/17/23 20:309.1 6.3 1 1,2,3-Trichlorobenzene ND ug/kg 04/19/23 04:33 87-61-604/17/23 20:309.1 7.4 1 1,2,4-Trichlorobenzene ND ug/kg 04/19/23 04:33 120-82-104/17/23 20:309.1 7.7 1 1,1,1-Trichloroethane ND ug/kg 04/19/23 04:33 71-55-604/17/23 20:309.1 4.7 1 1,1,2-Trichloroethane ND ug/kg 04/19/23 04:33 79-00-504/17/23 20:309.1 3.0 1 Trichloroethene ND ug/kg 04/19/23 04:33 79-01-604/17/23 20:309.1 7.4 1 Trichlorofluoromethane ND ug/kg 04/19/23 04:33 75-69-404/17/23 20:309.1 5.0 1 1,2,3-Trichloropropane ND ug/kg 04/19/23 04:33 96-18-404/17/23 20:309.1 4.6 1 1,2,4-Trimethylbenzene ND ug/kg 04/19/23 04:33 95-63-604/17/23 20:309.1 5.4 1 1,3,5-Trimethylbenzene ND ug/kg 04/19/23 04:33 108-67-804/17/23 20:309.1 3.1 1 Vinyl acetate ND ug/kg 04/19/23 04:33 108-05-404/17/23 20:3091.3 18.8 1 Vinyl chloride ND ug/kg 04/19/23 04:33 75-01-4 IH04/17/23 20:3018.3 4.6 1 Xylene (Total)ND ug/kg 04/19/23 04:33 1330-20-704/17/23 20:3018.3 5.2 1 m&p-Xylene ND ug/kg 04/19/23 04:33 179601-23-104/17/23 20:3018.3 6.2 1 o-Xylene ND ug/kg 04/19/23 04:33 95-47-604/17/23 20:309.1 4.0 1 Surrogates Toluene-d8 (S)101 %04/19/23 04:33 2037-26-504/17/23 20:3070-130 1 4-Bromofluorobenzene (S)105 %04/19/23 04:33 460-00-404/17/23 20:3070-130 1 1,2-Dichloroethane-d4 (S)99 %04/19/23 04:33 17060-07-004/17/23 20:3070-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 25.2 %04/14/23 15:28 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-03 (4-5)Lab ID: 92662335003 Collected: 04/14/23 11:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 74.5 %04/20/23 11:1404/20/23 10:571 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.726J mg/kg 04/24/23 03:48 18540-29-9 J04/21/23 11:531.34 0.342 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-04 (2-4)Lab ID: 92662335004 Collected: 04/14/23 11:45 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010D Preparation Method: EPA 3015A Leachate Method/Date: EPA 1311; 04/26/23 14:12 Pace Analytical Services - Minneapolis 6010D MET ICP, TCLP MICRO Chromium ND mg/L 04/27/23 13:50 7440-47-304/27/23 10:550.10 0.0043 1 Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 2.4 mg/kg 04/20/23 14:40 7440-38-204/20/23 10:030.64 0.18 1 Barium 11.8 mg/kg 04/20/23 14:40 7440-39-304/20/23 10:030.38 0.096 1 Cadmium ND mg/kg 04/20/23 14:40 7440-43-904/20/23 10:030.10 0.038 1 Chromium 147 mg/kg 04/20/23 14:40 7440-47-304/20/23 10:032.6 0.50 1 Lead 7.3 mg/kg 04/20/23 14:40 7439-92-104/20/23 10:030.64 0.12 1 Selenium 0.65 mg/kg 04/20/23 14:40 7782-49-204/20/23 10:030.64 0.13 1 Silver ND mg/kg 04/20/23 14:40 7440-22-404/20/23 10:030.64 0.26 1 Analytical Method: EPA 7471B Preparation Method: EPA 7471B Pace Analytical Services - Minneapolis 7471B Mercury Mercury 0.13 mg/kg 04/21/23 11:15 7439-97-604/20/23 10:060.025 0.011 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 04/17/23 07:39 83-32-904/15/23 15:46438 154 1 Acenaphthylene ND ug/kg 04/17/23 07:39 208-96-804/15/23 15:46438 154 1 Aniline ND ug/kg 04/17/23 07:39 62-53-304/15/23 15:46438 171 1 Anthracene ND ug/kg 04/17/23 07:39 120-12-704/15/23 15:46438 143 1 Benzo(a)anthracene ND ug/kg 04/17/23 07:39 56-55-304/15/23 15:46438 146 1 Benzo(a)pyrene ND ug/kg 04/17/23 07:39 50-32-804/15/23 15:46438 151 1 Benzo(b)fluoranthene ND ug/kg 04/17/23 07:39 205-99-204/15/23 15:46438 146 1 Benzo(g,h,i)perylene ND ug/kg 04/17/23 07:39 191-24-204/15/23 15:46438 170 1 Benzo(k)fluoranthene ND ug/kg 04/17/23 07:39 207-08-904/15/23 15:46438 154 1 Benzoic Acid ND ug/kg 04/17/23 07:39 65-85-0 L204/15/23 15:462190 942 1 Benzyl alcohol ND ug/kg 04/17/23 07:39 100-51-604/15/23 15:46877 332 1 4-Bromophenylphenyl ether ND ug/kg 04/17/23 07:39 101-55-304/15/23 15:46438 169 1 Butylbenzylphthalate ND ug/kg 04/17/23 07:39 85-68-704/15/23 15:46438 185 1 4-Chloro-3-methylphenol ND ug/kg 04/17/23 07:39 59-50-704/15/23 15:46877 308 1 4-Chloroaniline ND ug/kg 04/17/23 07:39 106-47-804/15/23 15:46877 344 1 bis(2-Chloroethoxy)methane ND ug/kg 04/17/23 07:39 111-91-104/15/23 15:46438 182 1 bis(2-Chloroethyl) ether ND ug/kg 04/17/23 07:39 111-44-404/15/23 15:46438 165 1 2-Chloronaphthalene ND ug/kg 04/17/23 07:39 91-58-704/15/23 15:46438 174 1 2-Chlorophenol ND ug/kg 04/17/23 07:39 95-57-804/15/23 15:46438 165 1 4-Chlorophenylphenyl ether ND ug/kg 04/17/23 07:39 7005-72-304/15/23 15:46438 163 1 Chrysene ND ug/kg 04/17/23 07:39 218-01-904/15/23 15:46438 159 1 Dibenz(a,h)anthracene ND ug/kg 04/17/23 07:39 53-70-304/15/23 15:46438 169 1 Dibenzofuran ND ug/kg 04/17/23 07:39 132-64-904/15/23 15:46438 158 1 1,2-Dichlorobenzene ND ug/kg 04/17/23 07:39 95-50-104/15/23 15:46438 158 1 1,3-Dichlorobenzene ND ug/kg 04/17/23 07:39 541-73-104/15/23 15:46438 155 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-04 (2-4)Lab ID: 92662335004 Collected: 04/14/23 11:45 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave 1,4-Dichlorobenzene ND ug/kg 04/17/23 07:39 106-46-704/15/23 15:46438 167 1 3,3'-Dichlorobenzidine ND ug/kg 04/17/23 07:39 91-94-104/15/23 15:46877 296 1 2,4-Dichlorophenol ND ug/kg 04/17/23 07:39 120-83-204/15/23 15:46438 171 1 Diethylphthalate ND ug/kg 04/17/23 07:39 84-66-204/15/23 15:46438 161 1 2,4-Dimethylphenol ND ug/kg 04/17/23 07:39 105-67-904/15/23 15:46438 182 1 Dimethylphthalate ND ug/kg 04/17/23 07:39 131-11-304/15/23 15:46438 159 1 Di-n-butylphthalate ND ug/kg 04/17/23 07:39 84-74-204/15/23 15:46438 147 1 4,6-Dinitro-2-methylphenol ND ug/kg 04/17/23 07:39 534-52-104/15/23 15:46877 409 1 2,4-Dinitrophenol ND ug/kg 04/17/23 07:39 51-28-504/15/23 15:462190 1350 1 2,4-Dinitrotoluene ND ug/kg 04/17/23 07:39 121-14-204/15/23 15:46438 169 1 2,6-Dinitrotoluene ND ug/kg 04/17/23 07:39 606-20-204/15/23 15:46438 161 1 Di-n-octylphthalate ND ug/kg 04/17/23 07:39 117-84-004/15/23 15:46438 173 1 bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/23 07:39 117-81-704/15/23 15:46438 170 1 Fluoranthene ND ug/kg 04/17/23 07:39 206-44-004/15/23 15:46438 150 1 Fluorene ND ug/kg 04/17/23 07:39 86-73-704/15/23 15:46438 154 1 Hexachloro-1,3-butadiene ND ug/kg 04/17/23 07:39 87-68-304/15/23 15:46438 190 1 Hexachlorobenzene ND ug/kg 04/17/23 07:39 118-74-104/15/23 15:46438 171 1 Hexachlorocyclopentadiene ND ug/kg 04/17/23 07:39 77-47-404/15/23 15:46438 251 1 Hexachloroethane ND ug/kg 04/17/23 07:39 67-72-104/15/23 15:46438 167 1 Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/23 07:39 193-39-504/15/23 15:46438 173 1 Isophorone ND ug/kg 04/17/23 07:39 78-59-104/15/23 15:46438 195 1 1-Methylnaphthalene ND ug/kg 04/17/23 07:39 90-12-004/15/23 15:46438 154 1 2-Methylnaphthalene ND ug/kg 04/17/23 07:39 91-57-604/15/23 15:46438 175 1 2-Methylphenol(o-Cresol)ND ug/kg 04/17/23 07:39 95-48-704/15/23 15:46438 179 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/23 07:39 15831-10-404/15/23 15:46438 177 1 Naphthalene ND ug/kg 04/17/23 07:39 91-20-304/15/23 15:46438 149 1 2-Nitroaniline ND ug/kg 04/17/23 07:39 88-74-404/15/23 15:462190 359 1 3-Nitroaniline ND ug/kg 04/17/23 07:39 99-09-204/15/23 15:462190 344 1 4-Nitroaniline ND ug/kg 04/17/23 07:39 100-01-604/15/23 15:46877 333 1 Nitrobenzene ND ug/kg 04/17/23 07:39 98-95-304/15/23 15:46438 203 1 2-Nitrophenol ND ug/kg 04/17/23 07:39 88-75-504/15/23 15:46438 190 1 4-Nitrophenol ND ug/kg 04/17/23 07:39 100-02-704/15/23 15:462190 847 1 N-Nitrosodimethylamine ND ug/kg 04/17/23 07:39 62-75-904/15/23 15:46438 147 1 N-Nitroso-di-n-propylamine ND ug/kg 04/17/23 07:39 621-64-704/15/23 15:46438 165 1 N-Nitrosodiphenylamine ND ug/kg 04/17/23 07:39 86-30-604/15/23 15:46438 155 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/23 07:39 108-60-104/15/23 15:46438 209 1 Pentachlorophenol ND ug/kg 04/17/23 07:39 87-86-504/15/23 15:46877 429 1 Phenanthrene ND ug/kg 04/17/23 07:39 85-01-804/15/23 15:46438 143 1 Phenol ND ug/kg 04/17/23 07:39 108-95-204/15/23 15:46438 195 1 Pyrene ND ug/kg 04/17/23 07:39 129-00-004/15/23 15:46438 178 1 Pyridine ND ug/kg 04/17/23 07:39 110-86-104/15/23 15:46438 138 1 1,2,4-Trichlorobenzene ND ug/kg 04/17/23 07:39 120-82-104/15/23 15:46438 173 1 2,4,5-Trichlorophenol ND ug/kg 04/17/23 07:39 95-95-404/15/23 15:46438 201 1 2,4,6-Trichlorophenol ND ug/kg 04/17/23 07:39 88-06-204/15/23 15:46438 181 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-04 (2-4)Lab ID: 92662335004 Collected: 04/14/23 11:45 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates Nitrobenzene-d5 (S)38 %04/17/23 07:39 4165-60-004/15/23 15:4610-130 1 2-Fluorobiphenyl (S)35 %04/17/23 07:39 321-60-804/15/23 15:4610-130 1 Terphenyl-d14 (S)64 %04/17/23 07:39 1718-51-004/15/23 15:4610-130 1 Phenol-d6 (S)35 %04/17/23 07:39 13127-88-304/15/23 15:4610-130 1 2-Fluorophenol (S)35 %04/17/23 07:39 367-12-404/15/23 15:4610-130 1 2,4,6-Tribromophenol (S)37 %04/17/23 07:39 118-79-604/15/23 15:4610-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 04/19/23 04:51 67-64-104/17/23 20:30175 56.3 1 Benzene ND ug/kg 04/19/23 04:51 71-43-204/17/23 20:308.8 3.5 1 Bromobenzene ND ug/kg 04/19/23 04:51 108-86-104/17/23 20:308.8 2.9 1 Bromochloromethane ND ug/kg 04/19/23 04:51 74-97-504/17/23 20:308.8 2.6 1 Bromodichloromethane ND ug/kg 04/19/23 04:51 75-27-404/17/23 20:308.8 3.4 1 Bromoform ND ug/kg 04/19/23 04:51 75-25-204/17/23 20:308.8 3.1 1 Bromomethane ND ug/kg 04/19/23 04:51 74-83-904/17/23 20:3035.1 27.2 1 2-Butanone (MEK)ND ug/kg 04/19/23 04:51 78-93-304/17/23 20:30175 42.1 1 n-Butylbenzene ND ug/kg 04/19/23 04:51 104-51-804/17/23 20:308.8 5.5 1 sec-Butylbenzene ND ug/kg 04/19/23 04:51 135-98-804/17/23 20:308.8 3.9 1 tert-Butylbenzene ND ug/kg 04/19/23 04:51 98-06-604/17/23 20:308.8 3.1 1 Carbon tetrachloride ND ug/kg 04/19/23 04:51 56-23-504/17/23 20:308.8 3.3 1 Chlorobenzene ND ug/kg 04/19/23 04:51 108-90-704/17/23 20:308.8 5.0 1 Chloroethane ND ug/kg 04/19/23 04:51 75-00-3 IH04/17/23 20:3017.5 6.8 1 Chloroform ND ug/kg 04/19/23 04:51 67-66-304/17/23 20:308.8 7.3 1 Chloromethane ND ug/kg 04/19/23 04:51 74-87-3 IH,L1, v104/17/23 20:3017.5 7.4 1 2-Chlorotoluene ND ug/kg 04/19/23 04:51 95-49-804/17/23 20:308.8 3.1 1 4-Chlorotoluene ND ug/kg 04/19/23 04:51 106-43-404/17/23 20:308.8 4.9 1 1,2-Dibromo-3-chloropropane ND ug/kg 04/19/23 04:51 96-12-804/17/23 20:308.8 3.4 1 Dibromochloromethane ND ug/kg 04/19/23 04:51 124-48-104/17/23 20:308.8 4.9 1 1,2-Dibromoethane (EDB)ND ug/kg 04/19/23 04:51 106-93-404/17/23 20:308.8 3.9 1 Dibromomethane ND ug/kg 04/19/23 04:51 74-95-304/17/23 20:308.8 1.9 1 1,2-Dichlorobenzene ND ug/kg 04/19/23 04:51 95-50-104/17/23 20:308.8 3.2 1 1,3-Dichlorobenzene ND ug/kg 04/19/23 04:51 541-73-104/17/23 20:308.8 2.7 1 1,4-Dichlorobenzene ND ug/kg 04/19/23 04:51 106-46-704/17/23 20:308.8 2.3 1 Dichlorodifluoromethane ND ug/kg 04/19/23 04:51 75-71-8 IH,v104/17/23 20:3017.5 8.9 1 1,1-Dichloroethane ND ug/kg 04/19/23 04:51 75-34-304/17/23 20:308.8 3.6 1 1,2-Dichloroethane ND ug/kg 04/19/23 04:51 107-06-204/17/23 20:308.8 5.8 1 1,1-Dichloroethene ND ug/kg 04/19/23 04:51 75-35-404/17/23 20:308.8 3.6 1 cis-1,2-Dichloroethene ND ug/kg 04/19/23 04:51 156-59-204/17/23 20:308.8 3.0 1 trans-1,2-Dichloroethene ND ug/kg 04/19/23 04:51 156-60-504/17/23 20:308.8 7.5 1 1,2-Dichloropropane ND ug/kg 04/19/23 04:51 78-87-504/17/23 20:308.8 2.6 1 1,3-Dichloropropane ND ug/kg 04/19/23 04:51 142-28-904/17/23 20:308.8 2.7 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-04 (2-4)Lab ID: 92662335004 Collected: 04/14/23 11:45 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles 2,2-Dichloropropane ND ug/kg 04/19/23 04:51 594-20-704/17/23 20:308.8 6.6 1 1,1-Dichloropropene ND ug/kg 04/19/23 04:51 563-58-604/17/23 20:308.8 4.2 1 cis-1,3-Dichloropropene ND ug/kg 04/19/23 04:51 10061-01-504/17/23 20:308.8 2.4 1 trans-1,3-Dichloropropene ND ug/kg 04/19/23 04:51 10061-02-604/17/23 20:308.8 3.0 1 Diisopropyl ether ND ug/kg 04/19/23 04:51 108-20-304/17/23 20:308.8 2.4 1 Ethylbenzene ND ug/kg 04/19/23 04:51 100-41-404/17/23 20:308.8 4.1 1 Hexachloro-1,3-butadiene ND ug/kg 04/19/23 04:51 87-68-304/17/23 20:3017.5 14.3 1 2-Hexanone ND ug/kg 04/19/23 04:51 591-78-604/17/23 20:3087.7 8.5 1 Isopropylbenzene (Cumene)ND ug/kg 04/19/23 04:51 98-82-804/17/23 20:308.8 3.0 1 p-Isopropyltoluene ND ug/kg 04/19/23 04:51 99-87-604/17/23 20:308.8 4.3 1 Methylene Chloride 137 ug/kg 04/19/23 04:51 75-09-2 C904/17/23 20:3035.1 24.0 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/23 04:51 108-10-104/17/23 20:3087.7 8.5 1 Methyl-tert-butyl ether ND ug/kg 04/19/23 04:51 1634-04-404/17/23 20:308.8 3.3 1 Naphthalene ND ug/kg 04/19/23 04:51 91-20-304/17/23 20:308.8 4.6 1 n-Propylbenzene ND ug/kg 04/19/23 04:51 103-65-104/17/23 20:308.8 3.1 1 Styrene ND ug/kg 04/19/23 04:51 100-42-504/17/23 20:308.8 2.3 1 1,1,1,2-Tetrachloroethane ND ug/kg 04/19/23 04:51 630-20-604/17/23 20:308.8 3.4 1 1,1,2,2-Tetrachloroethane ND ug/kg 04/19/23 04:51 79-34-504/17/23 20:308.8 2.3 1 Tetrachloroethene ND ug/kg 04/19/23 04:51 127-18-404/17/23 20:308.8 2.8 1 Toluene ND ug/kg 04/19/23 04:51 108-88-304/17/23 20:308.8 6.0 1 1,2,3-Trichlorobenzene ND ug/kg 04/19/23 04:51 87-61-604/17/23 20:308.8 7.1 1 1,2,4-Trichlorobenzene ND ug/kg 04/19/23 04:51 120-82-104/17/23 20:308.8 7.4 1 1,1,1-Trichloroethane ND ug/kg 04/19/23 04:51 71-55-604/17/23 20:308.8 4.6 1 1,1,2-Trichloroethane ND ug/kg 04/19/23 04:51 79-00-504/17/23 20:308.8 2.9 1 Trichloroethene ND ug/kg 04/19/23 04:51 79-01-604/17/23 20:308.8 7.1 1 Trichlorofluoromethane ND ug/kg 04/19/23 04:51 75-69-404/17/23 20:308.8 4.8 1 1,2,3-Trichloropropane ND ug/kg 04/19/23 04:51 96-18-404/17/23 20:308.8 4.4 1 1,2,4-Trimethylbenzene ND ug/kg 04/19/23 04:51 95-63-604/17/23 20:308.8 5.2 1 1,3,5-Trimethylbenzene ND ug/kg 04/19/23 04:51 108-67-804/17/23 20:308.8 2.9 1 Vinyl acetate ND ug/kg 04/19/23 04:51 108-05-404/17/23 20:3087.7 18.0 1 Vinyl chloride ND ug/kg 04/19/23 04:51 75-01-4 IH04/17/23 20:3017.5 4.5 1 Xylene (Total)ND ug/kg 04/19/23 04:51 1330-20-704/17/23 20:3017.5 5.0 1 m&p-Xylene ND ug/kg 04/19/23 04:51 179601-23-104/17/23 20:3017.5 6.0 1 o-Xylene ND ug/kg 04/19/23 04:51 95-47-604/17/23 20:308.8 3.9 1 Surrogates Toluene-d8 (S)103 %04/19/23 04:51 2037-26-504/17/23 20:3070-130 1 4-Bromofluorobenzene (S)106 %04/19/23 04:51 460-00-404/17/23 20:3070-130 1 1,2-Dichloroethane-d4 (S)101 %04/19/23 04:51 17060-07-004/17/23 20:3070-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 24.5 %04/14/23 15:28 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-04 (2-4)Lab ID: 92662335004 Collected: 04/14/23 11:45 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 75.8 %04/21/23 17:4804/21/23 17:351 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.734J mg/kg 04/24/23 03:53 18540-29-9 J04/21/23 11:531.32 0.336 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-05 (2-4)Lab ID: 92662335005 Collected: 04/14/23 11:55 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 2.1 mg/kg 04/20/23 14:49 7440-38-204/20/23 10:030.60 0.17 1 Barium 12.0 mg/kg 04/20/23 14:49 7440-39-304/20/23 10:030.36 0.089 1 Cadmium ND mg/kg 04/20/23 14:49 7440-43-904/20/23 10:030.095 0.035 1 Chromium 15.2 mg/kg 04/20/23 14:49 7440-47-304/20/23 10:032.4 0.46 1 Lead 7.1 mg/kg 04/20/23 14:49 7439-92-104/20/23 10:030.60 0.11 1 Selenium 0.54J mg/kg 04/20/23 14:49 7782-49-204/20/23 10:030.60 0.13 1 Silver ND mg/kg 04/20/23 14:49 7440-22-404/20/23 10:030.60 0.24 1 Analytical Method: EPA 7471B Preparation Method: EPA 7471B Pace Analytical Services - Minneapolis 7471B Mercury Mercury 0.022J mg/kg 04/21/23 11:20 7439-97-604/20/23 10:060.024 0.010 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 04/17/23 08:06 83-32-904/15/23 15:46409 144 1 Acenaphthylene ND ug/kg 04/17/23 08:06 208-96-804/15/23 15:46409 144 1 Aniline ND ug/kg 04/17/23 08:06 62-53-304/15/23 15:46409 160 1 Anthracene ND ug/kg 04/17/23 08:06 120-12-704/15/23 15:46409 134 1 Benzo(a)anthracene ND ug/kg 04/17/23 08:06 56-55-304/15/23 15:46409 136 1 Benzo(a)pyrene ND ug/kg 04/17/23 08:06 50-32-804/15/23 15:46409 141 1 Benzo(b)fluoranthene ND ug/kg 04/17/23 08:06 205-99-204/15/23 15:46409 136 1 Benzo(g,h,i)perylene ND ug/kg 04/17/23 08:06 191-24-204/15/23 15:46409 159 1 Benzo(k)fluoranthene ND ug/kg 04/17/23 08:06 207-08-904/15/23 15:46409 144 1 Benzoic Acid ND ug/kg 04/17/23 08:06 65-85-0 L204/15/23 15:462040 878 1 Benzyl alcohol ND ug/kg 04/17/23 08:06 100-51-604/15/23 15:46817 310 1 4-Bromophenylphenyl ether ND ug/kg 04/17/23 08:06 101-55-304/15/23 15:46409 157 1 Butylbenzylphthalate ND ug/kg 04/17/23 08:06 85-68-704/15/23 15:46409 172 1 4-Chloro-3-methylphenol ND ug/kg 04/17/23 08:06 59-50-704/15/23 15:46817 287 1 4-Chloroaniline ND ug/kg 04/17/23 08:06 106-47-804/15/23 15:46817 321 1 bis(2-Chloroethoxy)methane ND ug/kg 04/17/23 08:06 111-91-104/15/23 15:46409 170 1 bis(2-Chloroethyl) ether ND ug/kg 04/17/23 08:06 111-44-404/15/23 15:46409 154 1 2-Chloronaphthalene ND ug/kg 04/17/23 08:06 91-58-704/15/23 15:46409 162 1 2-Chlorophenol ND ug/kg 04/17/23 08:06 95-57-804/15/23 15:46409 154 1 4-Chlorophenylphenyl ether ND ug/kg 04/17/23 08:06 7005-72-304/15/23 15:46409 152 1 Chrysene ND ug/kg 04/17/23 08:06 218-01-904/15/23 15:46409 149 1 Dibenz(a,h)anthracene ND ug/kg 04/17/23 08:06 53-70-304/15/23 15:46409 157 1 Dibenzofuran ND ug/kg 04/17/23 08:06 132-64-904/15/23 15:46409 147 1 1,2-Dichlorobenzene ND ug/kg 04/17/23 08:06 95-50-104/15/23 15:46409 147 1 1,3-Dichlorobenzene ND ug/kg 04/17/23 08:06 541-73-104/15/23 15:46409 145 1 1,4-Dichlorobenzene ND ug/kg 04/17/23 08:06 106-46-704/15/23 15:46409 156 1 3,3'-Dichlorobenzidine ND ug/kg 04/17/23 08:06 91-94-104/15/23 15:46817 276 1 2,4-Dichlorophenol ND ug/kg 04/17/23 08:06 120-83-204/15/23 15:46409 160 1 Diethylphthalate ND ug/kg 04/17/23 08:06 84-66-204/15/23 15:46409 150 1 2,4-Dimethylphenol ND ug/kg 04/17/23 08:06 105-67-904/15/23 15:46409 170 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-05 (2-4)Lab ID: 92662335005 Collected: 04/14/23 11:55 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Dimethylphthalate ND ug/kg 04/17/23 08:06 131-11-304/15/23 15:46409 149 1 Di-n-butylphthalate ND ug/kg 04/17/23 08:06 84-74-204/15/23 15:46409 137 1 4,6-Dinitro-2-methylphenol ND ug/kg 04/17/23 08:06 534-52-104/15/23 15:46817 381 1 2,4-Dinitrophenol ND ug/kg 04/17/23 08:06 51-28-504/15/23 15:462040 1260 1 2,4-Dinitrotoluene ND ug/kg 04/17/23 08:06 121-14-204/15/23 15:46409 157 1 2,6-Dinitrotoluene ND ug/kg 04/17/23 08:06 606-20-204/15/23 15:46409 150 1 Di-n-octylphthalate ND ug/kg 04/17/23 08:06 117-84-004/15/23 15:46409 161 1 bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/23 08:06 117-81-704/15/23 15:46409 159 1 Fluoranthene ND ug/kg 04/17/23 08:06 206-44-004/15/23 15:46409 140 1 Fluorene ND ug/kg 04/17/23 08:06 86-73-704/15/23 15:46409 144 1 Hexachloro-1,3-butadiene ND ug/kg 04/17/23 08:06 87-68-304/15/23 15:46409 177 1 Hexachlorobenzene ND ug/kg 04/17/23 08:06 118-74-104/15/23 15:46409 160 1 Hexachlorocyclopentadiene ND ug/kg 04/17/23 08:06 77-47-404/15/23 15:46409 234 1 Hexachloroethane ND ug/kg 04/17/23 08:06 67-72-104/15/23 15:46409 156 1 Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/23 08:06 193-39-504/15/23 15:46409 161 1 Isophorone ND ug/kg 04/17/23 08:06 78-59-104/15/23 15:46409 182 1 1-Methylnaphthalene ND ug/kg 04/17/23 08:06 90-12-004/15/23 15:46409 144 1 2-Methylnaphthalene ND ug/kg 04/17/23 08:06 91-57-604/15/23 15:46409 163 1 2-Methylphenol(o-Cresol)ND ug/kg 04/17/23 08:06 95-48-704/15/23 15:46409 167 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/23 08:06 15831-10-404/15/23 15:46409 165 1 Naphthalene ND ug/kg 04/17/23 08:06 91-20-304/15/23 15:46409 139 1 2-Nitroaniline ND ug/kg 04/17/23 08:06 88-74-404/15/23 15:462040 334 1 3-Nitroaniline ND ug/kg 04/17/23 08:06 99-09-204/15/23 15:462040 321 1 4-Nitroaniline ND ug/kg 04/17/23 08:06 100-01-604/15/23 15:46817 311 1 Nitrobenzene ND ug/kg 04/17/23 08:06 98-95-304/15/23 15:46409 190 1 2-Nitrophenol ND ug/kg 04/17/23 08:06 88-75-504/15/23 15:46409 177 1 4-Nitrophenol ND ug/kg 04/17/23 08:06 100-02-704/15/23 15:462040 790 1 N-Nitrosodimethylamine ND ug/kg 04/17/23 08:06 62-75-904/15/23 15:46409 137 1 N-Nitroso-di-n-propylamine ND ug/kg 04/17/23 08:06 621-64-704/15/23 15:46409 154 1 N-Nitrosodiphenylamine ND ug/kg 04/17/23 08:06 86-30-604/15/23 15:46409 145 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/23 08:06 108-60-104/15/23 15:46409 194 1 Pentachlorophenol ND ug/kg 04/17/23 08:06 87-86-504/15/23 15:46817 400 1 Phenanthrene ND ug/kg 04/17/23 08:06 85-01-804/15/23 15:46409 134 1 Phenol ND ug/kg 04/17/23 08:06 108-95-204/15/23 15:46409 182 1 Pyrene ND ug/kg 04/17/23 08:06 129-00-004/15/23 15:46409 166 1 Pyridine ND ug/kg 04/17/23 08:06 110-86-104/15/23 15:46409 129 1 1,2,4-Trichlorobenzene ND ug/kg 04/17/23 08:06 120-82-104/15/23 15:46409 161 1 2,4,5-Trichlorophenol ND ug/kg 04/17/23 08:06 95-95-404/15/23 15:46409 187 1 2,4,6-Trichlorophenol ND ug/kg 04/17/23 08:06 88-06-204/15/23 15:46409 168 1 Surrogates Nitrobenzene-d5 (S)48 %04/17/23 08:06 4165-60-004/15/23 15:4610-130 1 2-Fluorobiphenyl (S)44 %04/17/23 08:06 321-60-804/15/23 15:4610-130 1 Terphenyl-d14 (S)69 %04/17/23 08:06 1718-51-004/15/23 15:4610-130 1 Phenol-d6 (S)53 %04/17/23 08:06 13127-88-304/15/23 15:4610-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-05 (2-4)Lab ID: 92662335005 Collected: 04/14/23 11:55 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates 2-Fluorophenol (S)51 %04/17/23 08:06 367-12-404/15/23 15:4610-130 1 2,4,6-Tribromophenol (S)58 %04/17/23 08:06 118-79-604/15/23 15:4610-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 04/19/23 05:09 67-64-104/17/23 20:30126 40.5 1 Benzene ND ug/kg 04/19/23 05:09 71-43-204/17/23 20:306.3 2.5 1 Bromobenzene ND ug/kg 04/19/23 05:09 108-86-104/17/23 20:306.3 2.1 1 Bromochloromethane ND ug/kg 04/19/23 05:09 74-97-504/17/23 20:306.3 1.9 1 Bromodichloromethane ND ug/kg 04/19/23 05:09 75-27-404/17/23 20:306.3 2.4 1 Bromoform ND ug/kg 04/19/23 05:09 75-25-204/17/23 20:306.3 2.2 1 Bromomethane ND ug/kg 04/19/23 05:09 74-83-904/17/23 20:3025.2 19.6 1 2-Butanone (MEK)ND ug/kg 04/19/23 05:09 78-93-304/17/23 20:30126 30.3 1 n-Butylbenzene ND ug/kg 04/19/23 05:09 104-51-804/17/23 20:306.3 4.0 1 sec-Butylbenzene ND ug/kg 04/19/23 05:09 135-98-804/17/23 20:306.3 2.8 1 tert-Butylbenzene ND ug/kg 04/19/23 05:09 98-06-604/17/23 20:306.3 2.2 1 Carbon tetrachloride ND ug/kg 04/19/23 05:09 56-23-504/17/23 20:306.3 2.4 1 Chlorobenzene ND ug/kg 04/19/23 05:09 108-90-704/17/23 20:306.3 3.6 1 Chloroethane ND ug/kg 04/19/23 05:09 75-00-3 IH04/17/23 20:3012.6 4.9 1 Chloroform ND ug/kg 04/19/23 05:09 67-66-304/17/23 20:306.3 5.3 1 Chloromethane ND ug/kg 04/19/23 05:09 74-87-3 IH,L1,v104/17/23 20:3012.6 5.3 1 2-Chlorotoluene ND ug/kg 04/19/23 05:09 95-49-804/17/23 20:306.3 2.2 1 4-Chlorotoluene ND ug/kg 04/19/23 05:09 106-43-404/17/23 20:306.3 3.5 1 1,2-Dibromo-3-chloropropane ND ug/kg 04/19/23 05:09 96-12-804/17/23 20:306.3 2.4 1 Dibromochloromethane ND ug/kg 04/19/23 05:09 124-48-104/17/23 20:306.3 3.5 1 1,2-Dibromoethane (EDB)ND ug/kg 04/19/23 05:09 106-93-404/17/23 20:306.3 2.8 1 Dibromomethane ND ug/kg 04/19/23 05:09 74-95-304/17/23 20:306.3 1.4 1 1,2-Dichlorobenzene ND ug/kg 04/19/23 05:09 95-50-104/17/23 20:306.3 2.3 1 1,3-Dichlorobenzene ND ug/kg 04/19/23 05:09 541-73-104/17/23 20:306.3 2.0 1 1,4-Dichlorobenzene ND ug/kg 04/19/23 05:09 106-46-704/17/23 20:306.3 1.6 1 Dichlorodifluoromethane ND ug/kg 04/19/23 05:09 75-71-8 IH,v104/17/23 20:3012.6 6.4 1 1,1-Dichloroethane ND ug/kg 04/19/23 05:09 75-34-304/17/23 20:306.3 2.6 1 1,2-Dichloroethane ND ug/kg 04/19/23 05:09 107-06-204/17/23 20:306.3 4.2 1 1,1-Dichloroethene ND ug/kg 04/19/23 05:09 75-35-404/17/23 20:306.3 2.6 1 cis-1,2-Dichloroethene ND ug/kg 04/19/23 05:09 156-59-204/17/23 20:306.3 2.2 1 trans-1,2-Dichloroethene ND ug/kg 04/19/23 05:09 156-60-504/17/23 20:306.3 5.4 1 1,2-Dichloropropane ND ug/kg 04/19/23 05:09 78-87-504/17/23 20:306.3 1.9 1 1,3-Dichloropropane ND ug/kg 04/19/23 05:09 142-28-904/17/23 20:306.3 2.0 1 2,2-Dichloropropane ND ug/kg 04/19/23 05:09 594-20-704/17/23 20:306.3 4.8 1 1,1-Dichloropropene ND ug/kg 04/19/23 05:09 563-58-604/17/23 20:306.3 3.0 1 cis-1,3-Dichloropropene ND ug/kg 04/19/23 05:09 10061-01-504/17/23 20:306.3 1.7 1 trans-1,3-Dichloropropene ND ug/kg 04/19/23 05:09 10061-02-604/17/23 20:306.3 2.2 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-05 (2-4)Lab ID: 92662335005 Collected: 04/14/23 11:55 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Diisopropyl ether ND ug/kg 04/19/23 05:09 108-20-304/17/23 20:306.3 1.7 1 Ethylbenzene ND ug/kg 04/19/23 05:09 100-41-404/17/23 20:306.3 2.9 1 Hexachloro-1,3-butadiene ND ug/kg 04/19/23 05:09 87-68-304/17/23 20:3012.6 10.3 1 2-Hexanone ND ug/kg 04/19/23 05:09 591-78-604/17/23 20:3063.1 6.1 1 Isopropylbenzene (Cumene)ND ug/kg 04/19/23 05:09 98-82-804/17/23 20:306.3 2.1 1 p-Isopropyltoluene ND ug/kg 04/19/23 05:09 99-87-604/17/23 20:306.3 3.1 1 Methylene Chloride 140 ug/kg 04/19/23 05:09 75-09-2 C904/17/23 20:3025.2 17.3 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/23 05:09 108-10-104/17/23 20:3063.1 6.1 1 Methyl-tert-butyl ether ND ug/kg 04/19/23 05:09 1634-04-404/17/23 20:306.3 2.4 1 Naphthalene ND ug/kg 04/19/23 05:09 91-20-304/17/23 20:306.3 3.3 1 n-Propylbenzene ND ug/kg 04/19/23 05:09 103-65-104/17/23 20:306.3 2.2 1 Styrene ND ug/kg 04/19/23 05:09 100-42-504/17/23 20:306.3 1.7 1 1,1,1,2-Tetrachloroethane ND ug/kg 04/19/23 05:09 630-20-604/17/23 20:306.3 2.4 1 1,1,2,2-Tetrachloroethane ND ug/kg 04/19/23 05:09 79-34-504/17/23 20:306.3 1.7 1 Tetrachloroethene ND ug/kg 04/19/23 05:09 127-18-404/17/23 20:306.3 2.0 1 Toluene ND ug/kg 04/19/23 05:09 108-88-304/17/23 20:306.3 4.4 1 1,2,3-Trichlorobenzene ND ug/kg 04/19/23 05:09 87-61-604/17/23 20:306.3 5.1 1 1,2,4-Trichlorobenzene ND ug/kg 04/19/23 05:09 120-82-104/17/23 20:306.3 5.3 1 1,1,1-Trichloroethane ND ug/kg 04/19/23 05:09 71-55-604/17/23 20:306.3 3.3 1 1,1,2-Trichloroethane ND ug/kg 04/19/23 05:09 79-00-504/17/23 20:306.3 2.1 1 Trichloroethene ND ug/kg 04/19/23 05:09 79-01-604/17/23 20:306.3 5.1 1 Trichlorofluoromethane ND ug/kg 04/19/23 05:09 75-69-404/17/23 20:306.3 3.5 1 1,2,3-Trichloropropane ND ug/kg 04/19/23 05:09 96-18-404/17/23 20:306.3 3.2 1 1,2,4-Trimethylbenzene ND ug/kg 04/19/23 05:09 95-63-604/17/23 20:306.3 3.7 1 1,3,5-Trimethylbenzene ND ug/kg 04/19/23 05:09 108-67-804/17/23 20:306.3 2.1 1 Vinyl acetate ND ug/kg 04/19/23 05:09 108-05-404/17/23 20:3063.1 13.0 1 Vinyl chloride ND ug/kg 04/19/23 05:09 75-01-4 IH04/17/23 20:3012.6 3.2 1 Xylene (Total)ND ug/kg 04/19/23 05:09 1330-20-704/17/23 20:3012.6 3.6 1 m&p-Xylene ND ug/kg 04/19/23 05:09 179601-23-104/17/23 20:3012.6 4.3 1 o-Xylene ND ug/kg 04/19/23 05:09 95-47-604/17/23 20:306.3 2.8 1 Surrogates Toluene-d8 (S)102 %04/19/23 05:09 2037-26-504/17/23 20:3070-130 1 4-Bromofluorobenzene (S)102 %04/19/23 05:09 460-00-404/17/23 20:3070-130 1 1,2-Dichloroethane-d4 (S)99 %04/19/23 05:09 17060-07-004/17/23 20:3070-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 19.0 %04/14/23 15:28 N20.10 0.10 1 Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 81.3 %04/21/23 17:4804/21/23 17:351 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-05 (2-4)Lab ID: 92662335005 Collected: 04/14/23 11:55 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent ND mg/kg 04/24/23 03:58 18540-29-904/21/23 11:531.23 0.314 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: COMP-3A (0.5-2)Lab ID: 92662335006 Collected: 04/13/23 15:30 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Lead 23.6 mg/kg 04/20/23 14:52 7439-92-104/20/23 10:030.58 0.11 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 15.8 %04/14/23 15:28 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: COMP-3B (0.5-2)Lab ID: 92662335007 Collected: 04/13/23 15:35 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Lead 44.9 mg/kg 04/20/23 14:55 7439-92-104/20/23 10:030.60 0.11 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 18.1 %04/14/23 15:28 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: COMP-3C (0.5-2)Lab ID: 92662335008 Collected: 04/13/23 15:45 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Lead 20.2 mg/kg 04/20/23 14:58 7439-92-104/20/23 10:030.61 0.11 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 19.0 %04/14/23 15:29 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: COMP-3D (0.5-2)Lab ID: 92662335009 Collected: 04/13/23 15:50 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Lead 53.5 mg/kg 04/20/23 15:01 7439-92-104/20/23 10:030.59 0.11 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 17.0 %04/14/23 15:29 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: COMP-3E (0.5-2)Lab ID: 92662335010 Collected: 04/13/23 16:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010D Preparation Method: EPA 3015A Leachate Method/Date: EPA 1311; 04/26/23 14:12 Pace Analytical Services - Minneapolis 6010D MET ICP, TCLP MICRO Lead ND mg/L 04/27/23 13:51 7439-92-104/27/23 10:550.10 0.010 1 Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Lead 309 mg/kg 04/20/23 15:04 7439-92-104/20/23 10:030.58 0.11 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 16.2 %04/14/23 15:29 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: COMP-3F (0.5-2)Lab ID: 92662335011 Collected: 04/13/23 16:05 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Lead 12.3 mg/kg 04/20/23 15:07 7439-92-104/20/23 10:030.56 0.10 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 14.3 %04/14/23 15:29 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-DUP Lab ID: 92662335012 Collected: 04/13/23 00:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 6010D Preparation Method: EPA 3015A Leachate Method/Date: EPA 1311; 04/26/23 14:12 Pace Analytical Services - Minneapolis 6010D MET ICP, TCLP MICRO Chromium ND mg/L 04/27/23 13:53 7440-47-304/27/23 10:550.10 0.0043 1 Analytical Method: EPA 6020B Preparation Method: EPA 3050B Pace Analytical Services - Minneapolis 6020B MET ICPMS Arsenic 2.9 mg/kg 04/20/23 15:10 7440-38-204/20/23 10:030.65 0.19 1 Barium 13.6 mg/kg 04/20/23 15:10 7440-39-304/20/23 10:030.39 0.098 1 Cadmium ND mg/kg 04/20/23 15:10 7440-43-904/20/23 10:030.10 0.038 1 Chromium 139 mg/kg 04/20/23 15:10 7440-47-304/20/23 10:032.6 0.51 1 Lead 10.3 mg/kg 04/20/23 15:10 7439-92-104/20/23 10:030.65 0.12 1 Selenium 0.82 mg/kg 04/20/23 15:10 7782-49-204/20/23 10:030.65 0.14 1 Silver ND mg/kg 04/20/23 15:10 7440-22-404/20/23 10:030.65 0.27 1 Analytical Method: EPA 7471B Preparation Method: EPA 7471B Pace Analytical Services - Minneapolis 7471B Mercury Mercury 0.11 mg/kg 04/21/23 11:21 7439-97-604/20/23 10:060.025 0.011 1 Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Acenaphthene ND ug/kg 04/17/23 08:34 83-32-904/15/23 15:46435 153 1 Acenaphthylene ND ug/kg 04/17/23 08:34 208-96-804/15/23 15:46435 153 1 Aniline ND ug/kg 04/17/23 08:34 62-53-304/15/23 15:46435 170 1 Anthracene ND ug/kg 04/17/23 08:34 120-12-704/15/23 15:46435 142 1 Benzo(a)anthracene ND ug/kg 04/17/23 08:34 56-55-304/15/23 15:46435 145 1 Benzo(a)pyrene ND ug/kg 04/17/23 08:34 50-32-804/15/23 15:46435 150 1 Benzo(b)fluoranthene ND ug/kg 04/17/23 08:34 205-99-204/15/23 15:46435 145 1 Benzo(g,h,i)perylene ND ug/kg 04/17/23 08:34 191-24-204/15/23 15:46435 169 1 Benzo(k)fluoranthene ND ug/kg 04/17/23 08:34 207-08-904/15/23 15:46435 153 1 Benzoic Acid ND ug/kg 04/17/23 08:34 65-85-0 L204/15/23 15:462170 934 1 Benzyl alcohol ND ug/kg 04/17/23 08:34 100-51-604/15/23 15:46870 330 1 4-Bromophenylphenyl ether ND ug/kg 04/17/23 08:34 101-55-304/15/23 15:46435 167 1 Butylbenzylphthalate ND ug/kg 04/17/23 08:34 85-68-704/15/23 15:46435 183 1 4-Chloro-3-methylphenol ND ug/kg 04/17/23 08:34 59-50-704/15/23 15:46870 306 1 4-Chloroaniline ND ug/kg 04/17/23 08:34 106-47-804/15/23 15:46870 341 1 bis(2-Chloroethoxy)methane ND ug/kg 04/17/23 08:34 111-91-104/15/23 15:46435 181 1 bis(2-Chloroethyl) ether ND ug/kg 04/17/23 08:34 111-44-404/15/23 15:46435 163 1 2-Chloronaphthalene ND ug/kg 04/17/23 08:34 91-58-704/15/23 15:46435 173 1 2-Chlorophenol ND ug/kg 04/17/23 08:34 95-57-804/15/23 15:46435 163 1 4-Chlorophenylphenyl ether ND ug/kg 04/17/23 08:34 7005-72-304/15/23 15:46435 162 1 Chrysene ND ug/kg 04/17/23 08:34 218-01-904/15/23 15:46435 158 1 Dibenz(a,h)anthracene ND ug/kg 04/17/23 08:34 53-70-304/15/23 15:46435 167 1 Dibenzofuran ND ug/kg 04/17/23 08:34 132-64-904/15/23 15:46435 157 1 1,2-Dichlorobenzene ND ug/kg 04/17/23 08:34 95-50-104/15/23 15:46435 157 1 1,3-Dichlorobenzene ND ug/kg 04/17/23 08:34 541-73-104/15/23 15:46435 154 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-DUP Lab ID: 92662335012 Collected: 04/13/23 00:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave 1,4-Dichlorobenzene ND ug/kg 04/17/23 08:34 106-46-704/15/23 15:46435 166 1 3,3'-Dichlorobenzidine ND ug/kg 04/17/23 08:34 91-94-104/15/23 15:46870 294 1 2,4-Dichlorophenol ND ug/kg 04/17/23 08:34 120-83-204/15/23 15:46435 170 1 Diethylphthalate ND ug/kg 04/17/23 08:34 84-66-204/15/23 15:46435 159 1 2,4-Dimethylphenol ND ug/kg 04/17/23 08:34 105-67-904/15/23 15:46435 181 1 Dimethylphthalate ND ug/kg 04/17/23 08:34 131-11-304/15/23 15:46435 158 1 Di-n-butylphthalate ND ug/kg 04/17/23 08:34 84-74-204/15/23 15:46435 146 1 4,6-Dinitro-2-methylphenol ND ug/kg 04/17/23 08:34 534-52-104/15/23 15:46870 406 1 2,4-Dinitrophenol ND ug/kg 04/17/23 08:34 51-28-504/15/23 15:462170 1340 1 2,4-Dinitrotoluene ND ug/kg 04/17/23 08:34 121-14-204/15/23 15:46435 167 1 2,6-Dinitrotoluene ND ug/kg 04/17/23 08:34 606-20-204/15/23 15:46435 159 1 Di-n-octylphthalate ND ug/kg 04/17/23 08:34 117-84-004/15/23 15:46435 171 1 bis(2-Ethylhexyl)phthalate ND ug/kg 04/17/23 08:34 117-81-704/15/23 15:46435 169 1 Fluoranthene ND ug/kg 04/17/23 08:34 206-44-004/15/23 15:46435 149 1 Fluorene ND ug/kg 04/17/23 08:34 86-73-704/15/23 15:46435 153 1 Hexachloro-1,3-butadiene ND ug/kg 04/17/23 08:34 87-68-304/15/23 15:46435 188 1 Hexachlorobenzene ND ug/kg 04/17/23 08:34 118-74-104/15/23 15:46435 170 1 Hexachlorocyclopentadiene ND ug/kg 04/17/23 08:34 77-47-404/15/23 15:46435 249 1 Hexachloroethane ND ug/kg 04/17/23 08:34 67-72-104/15/23 15:46435 166 1 Indeno(1,2,3-cd)pyrene ND ug/kg 04/17/23 08:34 193-39-504/15/23 15:46435 171 1 Isophorone ND ug/kg 04/17/23 08:34 78-59-104/15/23 15:46435 194 1 1-Methylnaphthalene ND ug/kg 04/17/23 08:34 90-12-004/15/23 15:46435 153 1 2-Methylnaphthalene ND ug/kg 04/17/23 08:34 91-57-604/15/23 15:46435 174 1 2-Methylphenol(o-Cresol)ND ug/kg 04/17/23 08:34 95-48-704/15/23 15:46435 178 1 3&4-Methylphenol(m&p Cresol)ND ug/kg 04/17/23 08:34 15831-10-404/15/23 15:46435 175 1 Naphthalene ND ug/kg 04/17/23 08:34 91-20-304/15/23 15:46435 148 1 2-Nitroaniline ND ug/kg 04/17/23 08:34 88-74-404/15/23 15:462170 356 1 3-Nitroaniline ND ug/kg 04/17/23 08:34 99-09-204/15/23 15:462170 341 1 4-Nitroaniline ND ug/kg 04/17/23 08:34 100-01-604/15/23 15:46870 331 1 Nitrobenzene ND ug/kg 04/17/23 08:34 98-95-304/15/23 15:46435 202 1 2-Nitrophenol ND ug/kg 04/17/23 08:34 88-75-504/15/23 15:46435 188 1 4-Nitrophenol ND ug/kg 04/17/23 08:34 100-02-704/15/23 15:462170 841 1 N-Nitrosodimethylamine ND ug/kg 04/17/23 08:34 62-75-904/15/23 15:46435 146 1 N-Nitroso-di-n-propylamine ND ug/kg 04/17/23 08:34 621-64-704/15/23 15:46435 163 1 N-Nitrosodiphenylamine ND ug/kg 04/17/23 08:34 86-30-604/15/23 15:46435 154 1 2,2'-Oxybis(1-chloropropane)ND ug/kg 04/17/23 08:34 108-60-104/15/23 15:46435 207 1 Pentachlorophenol ND ug/kg 04/17/23 08:34 87-86-504/15/23 15:46870 426 1 Phenanthrene ND ug/kg 04/17/23 08:34 85-01-804/15/23 15:46435 142 1 Phenol ND ug/kg 04/17/23 08:34 108-95-204/15/23 15:46435 194 1 Pyrene ND ug/kg 04/17/23 08:34 129-00-004/15/23 15:46435 177 1 Pyridine ND ug/kg 04/17/23 08:34 110-86-104/15/23 15:46435 137 1 1,2,4-Trichlorobenzene ND ug/kg 04/17/23 08:34 120-82-104/15/23 15:46435 171 1 2,4,5-Trichlorophenol ND ug/kg 04/17/23 08:34 95-95-404/15/23 15:46435 199 1 2,4,6-Trichlorophenol ND ug/kg 04/17/23 08:34 88-06-204/15/23 15:46435 179 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-DUP Lab ID: 92662335012 Collected: 04/13/23 00:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8270E Preparation Method: EPA 3546 Pace Analytical Services - Charlotte 8270E MSSV Microwave Surrogates Nitrobenzene-d5 (S)53 %04/17/23 08:34 4165-60-004/15/23 15:4610-130 1 2-Fluorobiphenyl (S)34 %04/17/23 08:34 321-60-804/15/23 15:4610-130 1 Terphenyl-d14 (S)71 %04/17/23 08:34 1718-51-004/15/23 15:4610-130 1 Phenol-d6 (S)55 %04/17/23 08:34 13127-88-304/15/23 15:4610-130 1 2-Fluorophenol (S)54 %04/17/23 08:34 367-12-404/15/23 15:4610-130 1 2,4,6-Tribromophenol (S)60 %04/17/23 08:34 118-79-604/15/23 15:4610-131 1 Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles Acetone ND ug/kg 04/19/23 05:26 67-64-104/17/23 20:30173 55.6 1 Benzene ND ug/kg 04/19/23 05:26 71-43-204/17/23 20:308.7 3.4 1 Bromobenzene ND ug/kg 04/19/23 05:26 108-86-104/17/23 20:308.7 2.8 1 Bromochloromethane ND ug/kg 04/19/23 05:26 74-97-504/17/23 20:308.7 2.6 1 Bromodichloromethane ND ug/kg 04/19/23 05:26 75-27-404/17/23 20:308.7 3.3 1 Bromoform ND ug/kg 04/19/23 05:26 75-25-204/17/23 20:308.7 3.0 1 Bromomethane ND ug/kg 04/19/23 05:26 74-83-904/17/23 20:3034.7 26.9 1 2-Butanone (MEK)ND ug/kg 04/19/23 05:26 78-93-304/17/23 20:30173 41.6 1 n-Butylbenzene ND ug/kg 04/19/23 05:26 104-51-804/17/23 20:308.7 5.5 1 sec-Butylbenzene ND ug/kg 04/19/23 05:26 135-98-804/17/23 20:308.7 3.8 1 tert-Butylbenzene ND ug/kg 04/19/23 05:26 98-06-604/17/23 20:308.7 3.1 1 Carbon tetrachloride ND ug/kg 04/19/23 05:26 56-23-504/17/23 20:308.7 3.2 1 Chlorobenzene ND ug/kg 04/19/23 05:26 108-90-704/17/23 20:308.7 5.0 1 Chloroethane ND ug/kg 04/19/23 05:26 75-00-3 IH04/17/23 20:3017.3 6.7 1 Chloroform ND ug/kg 04/19/23 05:26 67-66-304/17/23 20:308.7 7.2 1 Chloromethane ND ug/kg 04/19/23 05:26 74-87-3 IH,L1, v104/17/23 20:3017.3 7.3 1 2-Chlorotoluene ND ug/kg 04/19/23 05:26 95-49-804/17/23 20:308.7 3.1 1 4-Chlorotoluene ND ug/kg 04/19/23 05:26 106-43-404/17/23 20:308.7 4.8 1 1,2-Dibromo-3-chloropropane ND ug/kg 04/19/23 05:26 96-12-804/17/23 20:308.7 3.4 1 Dibromochloromethane ND ug/kg 04/19/23 05:26 124-48-104/17/23 20:308.7 4.9 1 1,2-Dibromoethane (EDB)ND ug/kg 04/19/23 05:26 106-93-404/17/23 20:308.7 3.8 1 Dibromomethane ND ug/kg 04/19/23 05:26 74-95-304/17/23 20:308.7 1.9 1 1,2-Dichlorobenzene ND ug/kg 04/19/23 05:26 95-50-104/17/23 20:308.7 3.1 1 1,3-Dichlorobenzene ND ug/kg 04/19/23 05:26 541-73-104/17/23 20:308.7 2.7 1 1,4-Dichlorobenzene ND ug/kg 04/19/23 05:26 106-46-704/17/23 20:308.7 2.3 1 Dichlorodifluoromethane ND ug/kg 04/19/23 05:26 75-71-8 IH,v104/17/23 20:3017.3 8.8 1 1,1-Dichloroethane ND ug/kg 04/19/23 05:26 75-34-304/17/23 20:308.7 3.6 1 1,2-Dichloroethane ND ug/kg 04/19/23 05:26 107-06-204/17/23 20:308.7 5.7 1 1,1-Dichloroethene ND ug/kg 04/19/23 05:26 75-35-404/17/23 20:308.7 3.6 1 cis-1,2-Dichloroethene ND ug/kg 04/19/23 05:26 156-59-204/17/23 20:308.7 3.0 1 trans-1,2-Dichloroethene ND ug/kg 04/19/23 05:26 156-60-504/17/23 20:308.7 7.4 1 1,2-Dichloropropane ND ug/kg 04/19/23 05:26 78-87-504/17/23 20:308.7 2.6 1 1,3-Dichloropropane ND ug/kg 04/19/23 05:26 142-28-904/17/23 20:308.7 2.7 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-DUP Lab ID: 92662335012 Collected: 04/13/23 00:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B Pace Analytical Services - Charlotte 8260D/5035A/5030B Volatiles 2,2-Dichloropropane ND ug/kg 04/19/23 05:26 594-20-704/17/23 20:308.7 6.6 1 1,1-Dichloropropene ND ug/kg 04/19/23 05:26 563-58-604/17/23 20:308.7 4.2 1 cis-1,3-Dichloropropene ND ug/kg 04/19/23 05:26 10061-01-504/17/23 20:308.7 2.4 1 trans-1,3-Dichloropropene ND ug/kg 04/19/23 05:26 10061-02-604/17/23 20:308.7 3.0 1 Diisopropyl ether ND ug/kg 04/19/23 05:26 108-20-304/17/23 20:308.7 2.3 1 Ethylbenzene ND ug/kg 04/19/23 05:26 100-41-404/17/23 20:308.7 4.0 1 Hexachloro-1,3-butadiene ND ug/kg 04/19/23 05:26 87-68-304/17/23 20:3017.3 14.2 1 2-Hexanone ND ug/kg 04/19/23 05:26 591-78-604/17/23 20:3086.6 8.4 1 Isopropylbenzene (Cumene)ND ug/kg 04/19/23 05:26 98-82-804/17/23 20:308.7 2.9 1 p-Isopropyltoluene ND ug/kg 04/19/23 05:26 99-87-604/17/23 20:308.7 4.3 1 Methylene Chloride 147 ug/kg 04/19/23 05:26 75-09-2 C904/17/23 20:3034.7 23.7 1 4-Methyl-2-pentanone (MIBK)ND ug/kg 04/19/23 05:26 108-10-104/17/23 20:3086.6 8.4 1 Methyl-tert-butyl ether ND ug/kg 04/19/23 05:26 1634-04-404/17/23 20:308.7 3.2 1 Naphthalene ND ug/kg 04/19/23 05:26 91-20-304/17/23 20:308.7 4.6 1 n-Propylbenzene ND ug/kg 04/19/23 05:26 103-65-104/17/23 20:308.7 3.1 1 Styrene ND ug/kg 04/19/23 05:26 100-42-504/17/23 20:308.7 2.3 1 1,1,1,2-Tetrachloroethane ND ug/kg 04/19/23 05:26 630-20-604/17/23 20:308.7 3.3 1 1,1,2,2-Tetrachloroethane ND ug/kg 04/19/23 05:26 79-34-504/17/23 20:308.7 2.3 1 Tetrachloroethene ND ug/kg 04/19/23 05:26 127-18-404/17/23 20:308.7 2.7 1 Toluene ND ug/kg 04/19/23 05:26 108-88-304/17/23 20:308.7 6.0 1 1,2,3-Trichlorobenzene ND ug/kg 04/19/23 05:26 87-61-604/17/23 20:308.7 7.0 1 1,2,4-Trichlorobenzene ND ug/kg 04/19/23 05:26 120-82-104/17/23 20:308.7 7.3 1 1,1,1-Trichloroethane ND ug/kg 04/19/23 05:26 71-55-604/17/23 20:308.7 4.5 1 1,1,2-Trichloroethane ND ug/kg 04/19/23 05:26 79-00-504/17/23 20:308.7 2.9 1 Trichloroethene ND ug/kg 04/19/23 05:26 79-01-604/17/23 20:308.7 7.0 1 Trichlorofluoromethane ND ug/kg 04/19/23 05:26 75-69-404/17/23 20:308.7 4.8 1 1,2,3-Trichloropropane ND ug/kg 04/19/23 05:26 96-18-404/17/23 20:308.7 4.4 1 1,2,4-Trimethylbenzene ND ug/kg 04/19/23 05:26 95-63-604/17/23 20:308.7 5.1 1 1,3,5-Trimethylbenzene ND ug/kg 04/19/23 05:26 108-67-804/17/23 20:308.7 2.9 1 Vinyl acetate ND ug/kg 04/19/23 05:26 108-05-404/17/23 20:3086.6 17.8 1 Vinyl chloride ND ug/kg 04/19/23 05:26 75-01-4 IH04/17/23 20:3017.3 4.4 1 Xylene (Total)ND ug/kg 04/19/23 05:26 1330-20-704/17/23 20:3017.3 4.9 1 m&p-Xylene ND ug/kg 04/19/23 05:26 179601-23-104/17/23 20:3017.3 5.9 1 o-Xylene ND ug/kg 04/19/23 05:26 95-47-604/17/23 20:308.7 3.8 1 Surrogates Toluene-d8 (S)103 %04/19/23 05:26 2037-26-504/17/23 20:3070-130 1 4-Bromofluorobenzene (S)100 %04/19/23 05:26 460-00-404/17/23 20:3070-130 1 1,2-Dichloroethane-d4 (S)101 %04/19/23 05:26 17060-07-004/17/23 20:3070-130 1 Analytical Method: SW-846 Pace Analytical Services - Charlotte Percent Moisture Percent Moisture 25.4 %04/14/23 15:29 N20.10 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 69 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Sample: BF-SB-DUP Lab ID: 92662335012 Collected: 04/13/23 00:00 Received: 04/14/23 13:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit Report Analytical Method: SM 2540G Preparation Method: SM 2540 G Pace National - Mt. Juliet Total Solids 2540 G-2011 Total Solids 74.0 %04/21/23 17:4804/21/23 17:351 Analytical Method: EPA 7199 Preparation Method: 3060A Pace National - Mt. Juliet Wet Chemistry 7199 Chromium, Hexavalent 0.733J mg/kg 04/24/23 04:04 18540-29-9 J04/21/23 11:531.35 0.344 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 876585 EPA 7471B EPA 7471B 7471B Mercury Solids Laboratory:Pace Analytical Services - Minneapolis Associated Lab Samples: 92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4622409 Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Matrix: Solid AnalyzedMDL Mercury mg/kg ND 0.019 04/21/23 11:030.0083 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4622410LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.470.47 100 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 4622411MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92662335001 4622412 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/kg 0.657 106 80-120107 1 200.6430.039 0.73 0.73 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 43 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 877876 EPA 3015A EPA 6010D 6010D MET ICP, TCLP MICRO Laboratory:Pace Analytical Services - Minneapolis Associated Lab Samples: 92662335003, 92662335004, 92662335010, 92662335012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4628570 Associated Lab Samples:92662335003, 92662335004, 92662335010, 92662335012 Matrix: Water AnalyzedMDL Chromium mg/L ND 0.10 04/27/23 13:070.0043 Lead mg/L ND 0.10 04/27/23 13:070.010 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4628571LABORATORY CONTROL SAMPLE: LCSSpike Chromium mg/L 4.95 99 80-120 Lead mg/L 5.05 99 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 4628572MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 10649608001 4628573 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Chromium mg/L 5 98 75-12598 1 205ND4.9 4.9 Lead mg/L 5 97 75-12597 0 205ND4.9 4.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 44 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 876553 EPA 3050B EPA 6020B 6020B Solids UPD5 Laboratory:Pace Analytical Services - Minneapolis Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335006, 92662335007, 92662335008, 92662335009, 92662335010, 92662335011, 92662335012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 4622328 Associated Lab Samples: 92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335006, 92662335007, 92662335008, 92662335009, 92662335010, 92662335011, 92662335012 Matrix: Solid AnalyzedMDL Arsenic mg/kg ND 0.49 04/20/23 14:130.14 Barium mg/kg ND 0.29 04/20/23 14:130.073 Cadmium mg/kg ND 0.078 04/20/23 14:130.029 Chromium mg/kg ND 2.0 04/20/23 14:130.38 Lead mg/kg ND 0.49 04/20/23 14:130.091 Selenium mg/kg ND 0.49 04/20/23 14:130.10 Silver mg/kg ND 0.49 04/20/23 14:130.20 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 4622329LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/kg 48.848.8 100 80-120 Barium mg/kg 50.048.8 103 80-120 Cadmium mg/kg 47.348.8 97 80-120 Chromium mg/kg 52.148.8 107 80-120 Lead mg/kg 50.748.8 104 80-120 Selenium mg/kg 48.448.8 99 80-120 Silver mg/kg 24.524.4 100 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 4622330MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92662335001 4622331 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Arsenic mg/kg 66.8 89 75-125110 20 2066.72.2 61.5 75.4 Barium mg/kg M166.8 113 75-125139 16 2066.719.1 94.4 111 Cadmium mg/kg R166.8 94 75-125117 22 2066.7ND 62.5 77.8 Chromium mg/kg 66.8 91 75-125121 17 2066.745.2 106 126 Lead mg/kg M1,R166.8 98 75-125126 23 2066.77.8 73.0 91.8 Selenium mg/kg 66.8 90 75-12594 4 2066.70.98 61.2 63.7 Silver mg/kg R133.4 96 75-125120 22 2033.3ND 32.3 40.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 45 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 768545 EPA 5035A/5030B EPA 8260D 8260D 5035A 5030B Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 3990257 Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Matrix: Solid AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/19/23 03:221.9 1,1,1-Trichloroethane ug/kg ND 5.0 04/19/23 03:222.6 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/19/23 03:221.3 1,1,2-Trichloroethane ug/kg ND 5.0 04/19/23 03:221.7 1,1-Dichloroethane ug/kg ND 5.0 04/19/23 03:222.1 1,1-Dichloroethene ug/kg ND 5.0 04/19/23 03:222.1 1,1-Dichloropropene ug/kg ND 5.0 04/19/23 03:222.4 1,2,3-Trichlorobenzene ug/kg ND 5.0 04/19/23 03:224.0 1,2,3-Trichloropropane ug/kg ND 5.0 04/19/23 03:222.5 1,2,4-Trichlorobenzene ug/kg ND 5.0 04/19/23 03:224.2 1,2,4-Trimethylbenzene ug/kg ND 5.0 04/19/23 03:223.0 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/19/23 03:221.9 1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/19/23 03:222.2 1,2-Dichlorobenzene ug/kg ND 5.0 04/19/23 03:221.8 1,2-Dichloroethane ug/kg ND 5.0 04/19/23 03:223.3 1,2-Dichloropropane ug/kg ND 5.0 04/19/23 03:221.5 1,3,5-Trimethylbenzene ug/kg ND 5.0 04/19/23 03:221.7 1,3-Dichlorobenzene ug/kg ND 5.0 04/19/23 03:221.6 1,3-Dichloropropane ug/kg ND 5.0 04/19/23 03:221.6 1,4-Dichlorobenzene ug/kg ND 5.0 04/19/23 03:221.3 2,2-Dichloropropane ug/kg ND 5.0 04/19/23 03:223.8 2-Butanone (MEK)ug/kg ND 100 04/19/23 03:2224.0 2-Chlorotoluene ug/kg ND 5.0 04/19/23 03:221.8 2-Hexanone ug/kg ND 50.0 04/19/23 03:224.8 4-Chlorotoluene ug/kg ND 5.0 04/19/23 03:222.8 4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/19/23 03:224.8 Acetone ug/kg ND 100 04/19/23 03:2232.1 Benzene ug/kg ND 5.0 04/19/23 03:222.0 Bromobenzene ug/kg ND 5.0 04/19/23 03:221.6 Bromochloromethane ug/kg ND 5.0 04/19/23 03:221.5 Bromodichloromethane ug/kg ND 5.0 04/19/23 03:221.9 Bromoform ug/kg ND 5.0 04/19/23 03:221.8 Bromomethane ug/kg ND 20.0 04/19/23 03:2215.5 Carbon tetrachloride ug/kg ND 5.0 04/19/23 03:221.9 Chlorobenzene ug/kg ND 5.0 04/19/23 03:222.9 Chloroethane ug/kg ND 10.0 IH04/19/23 03:223.9 Chloroform ug/kg ND 5.0 04/19/23 03:224.2 Chloromethane ug/kg ND 10.0 IH,v104/19/23 03:224.2 cis-1,2-Dichloroethene ug/kg ND 5.0 04/19/23 03:221.7 cis-1,3-Dichloropropene ug/kg ND 5.0 04/19/23 03:221.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 46 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 3990257 Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Matrix: Solid AnalyzedMDL Dibromochloromethane ug/kg ND 5.0 04/19/23 03:222.8 Dibromomethane ug/kg ND 5.0 04/19/23 03:221.1 Dichlorodifluoromethane ug/kg ND 10.0 IH,v104/19/23 03:225.1 Diisopropyl ether ug/kg ND 5.0 04/19/23 03:221.4 Ethylbenzene ug/kg ND 5.0 04/19/23 03:222.3 Hexachloro-1,3-butadiene ug/kg ND 10.0 04/19/23 03:228.2 Isopropylbenzene (Cumene)ug/kg ND 5.0 04/19/23 03:221.7 m&p-Xylene ug/kg ND 10.0 04/19/23 03:223.4 Methyl-tert-butyl ether ug/kg ND 5.0 04/19/23 03:221.9 Methylene Chloride ug/kg ND 20.0 04/19/23 03:2213.7 n-Butylbenzene ug/kg ND 5.0 04/19/23 03:223.2 n-Propylbenzene ug/kg ND 5.0 04/19/23 03:221.8 Naphthalene ug/kg ND 5.0 04/19/23 03:222.6 o-Xylene ug/kg ND 5.0 04/19/23 03:222.2 p-Isopropyltoluene ug/kg ND 5.0 04/19/23 03:222.5 sec-Butylbenzene ug/kg ND 5.0 04/19/23 03:222.2 Styrene ug/kg ND 5.0 04/19/23 03:221.3 tert-Butylbenzene ug/kg ND 5.0 04/19/23 03:221.8 Tetrachloroethene ug/kg ND 5.0 04/19/23 03:221.6 Toluene ug/kg ND 5.0 04/19/23 03:223.4 trans-1,2-Dichloroethene ug/kg ND 5.0 04/19/23 03:224.2 trans-1,3-Dichloropropene ug/kg ND 5.0 04/19/23 03:221.7 Trichloroethene ug/kg ND 5.0 04/19/23 03:224.0 Trichlorofluoromethane ug/kg ND 5.0 04/19/23 03:222.8 Vinyl acetate ug/kg ND 50.0 04/19/23 03:2210.3 Vinyl chloride ug/kg ND 10.0 IH04/19/23 03:222.5 Xylene (Total)ug/kg ND 10.0 04/19/23 03:222.8 1,2-Dichloroethane-d4 (S)%100 70-130 04/19/23 03:22 4-Bromofluorobenzene (S)%101 70-130 04/19/23 03:22 Toluene-d8 (S)%100 70-130 04/19/23 03:22 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3990258LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/kg 500500 100 70-130 1,1,1-Trichloroethane ug/kg 480500 96 70-130 1,1,2,2-Tetrachloroethane ug/kg 491500 98 70-130 1,1,2-Trichloroethane ug/kg 486500 97 70-130 1,1-Dichloroethane ug/kg 476500 95 70-130 1,1-Dichloroethene ug/kg 513500 103 70-130 1,1-Dichloropropene ug/kg 486500 97 70-130 1,2,3-Trichlorobenzene ug/kg 545500 109 70-130 1,2,3-Trichloropropane ug/kg 491500 98 70-130 1,2,4-Trichlorobenzene ug/kg 524500 105 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 47 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3990258LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trimethylbenzene ug/kg 515500 103 70-130 1,2-Dibromo-3-chloropropane ug/kg 454500 91 67-130 1,2-Dibromoethane (EDB)ug/kg 465500 93 70-130 1,2-Dichlorobenzene ug/kg 500500 100 70-130 1,2-Dichloroethane ug/kg 464500 93 70-130 1,2-Dichloropropane ug/kg 429500 86 70-130 1,3,5-Trimethylbenzene ug/kg 501500 100 70-130 1,3-Dichlorobenzene ug/kg 476500 95 70-130 1,3-Dichloropropane ug/kg 501500 100 70-130 1,4-Dichlorobenzene ug/kg 463500 93 70-130 2,2-Dichloropropane ug/kg 411500 82 67-130 2-Butanone (MEK)ug/kg 9691000 97 66-130 2-Chlorotoluene ug/kg 513500 103 70-130 2-Hexanone ug/kg 10401000 104 70-130 4-Chlorotoluene ug/kg 511500 102 70-130 4-Methyl-2-pentanone (MIBK)ug/kg 10101000 101 70-130 Acetone ug/kg 9791000 98 67-130 Benzene ug/kg 447500 89 70-130 Bromobenzene ug/kg 474500 95 70-130 Bromochloromethane ug/kg 455500 91 70-130 Bromodichloromethane ug/kg 484500 97 70-130 Bromoform ug/kg 474500 95 70-130 Bromomethane ug/kg 449500 90 53-175 Carbon tetrachloride ug/kg 494500 99 70-130 Chlorobenzene ug/kg 495500 99 70-130 Chloroethane ug/kg 567 IH500113 70-135 Chloroform ug/kg 482500 96 70-130 Chloromethane ug/kg 679 IH,L1,v1500136 64-130 cis-1,2-Dichloroethene ug/kg 487500 97 70-130 cis-1,3-Dichloropropene ug/kg 490500 98 70-130 Dibromochloromethane ug/kg 477500 95 70-130 Dibromomethane ug/kg 472500 94 70-130 Dichlorodifluoromethane ug/kg 673 IH,v1500135 63-145 Diisopropyl ether ug/kg 471500 94 68-130 Ethylbenzene ug/kg 470500 94 70-130 Hexachloro-1,3-butadiene ug/kg 493500 99 70-130 Isopropylbenzene (Cumene)ug/kg 512500 102 70-130 m&p-Xylene ug/kg 10301000 103 70-130 Methyl-tert-butyl ether ug/kg 453500 91 70-130 Methylene Chloride ug/kg 433500 87 67-130 n-Butylbenzene ug/kg 487500 97 70-130 n-Propylbenzene ug/kg 496500 99 70-130 Naphthalene ug/kg 490500 98 70-130 o-Xylene ug/kg 525500 105 70-130 p-Isopropyltoluene ug/kg 494500 99 70-130 sec-Butylbenzene ug/kg 506500 101 70-130 Styrene ug/kg 491500 98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 48 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3990258LABORATORY CONTROL SAMPLE: LCSSpike tert-Butylbenzene ug/kg 454500 91 64-130 Tetrachloroethene ug/kg 495500 99 70-130 Toluene ug/kg 487500 97 70-130 trans-1,2-Dichloroethene ug/kg 472500 94 70-130 trans-1,3-Dichloropropene ug/kg 500500 100 70-130 Trichloroethene ug/kg 485500 97 70-130 Trichlorofluoromethane ug/kg 463500 93 70-130 Vinyl acetate ug/kg 9541000 95 70-134 Vinyl chloride ug/kg 592 IH500118 68-130 Xylene (Total)ug/kg 15601500 104 70-130 1,2-Dichloroethane-d4 (S)%93 70-130 4-Bromofluorobenzene (S)%104 70-130 Toluene-d8 (S)%100 70-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 3990259MATRIX SPIKE SAMPLE: MSSpike Result 92662335001 1,1,1,2-Tetrachloroethane ug/kg 868758 114 58-140ND 1,1,1-Trichloroethane ug/kg 824758 109 58-144ND 1,1,2,2-Tetrachloroethane ug/kg 822758 108 52-139ND 1,1,2-Trichloroethane ug/kg 813758 107 56-140ND 1,1-Dichloroethane ug/kg 833758 110 58-145ND 1,1-Dichloroethene ug/kg 873758 115 57-158ND 1,1-Dichloropropene ug/kg 787758 104 58-151ND 1,2,3-Trichlorobenzene ug/kg 560758 74 48-149ND 1,2,3-Trichloropropane ug/kg 796758 105 54-132ND 1,2,4-Trichlorobenzene ug/kg 645758 85 51-151ND 1,2,4-Trimethylbenzene ug/kg 805758 106 38-170ND 1,2-Dibromo-3-chloropropane ug/kg 593758 78 44-134ND 1,2-Dibromoethane (EDB)ug/kg 765758 101 60-138ND 1,2-Dichlorobenzene ug/kg 824758 109 59-147ND 1,2-Dichloroethane ug/kg 756758 100 57-139ND 1,2-Dichloropropane ug/kg 783758 103 62-145ND 1,3,5-Trimethylbenzene ug/kg 778758 103 47-159ND 1,3-Dichlorobenzene ug/kg 763758 101 58-144ND 1,3-Dichloropropane ug/kg 837758 110 60-142ND 1,4-Dichlorobenzene ug/kg 720758 95 57-143ND 2,2-Dichloropropane ug/kg 481758 63 37-144ND 2-Butanone (MEK)ug/kg 15301520 101 28-146ND 2-Chlorotoluene ug/kg 798758 105 55-158ND 2-Hexanone ug/kg 15501520 102 44-141ND 4-Chlorotoluene ug/kg 776758 102 55-146ND 4-Methyl-2-pentanone (MIBK)ug/kg 16001520 105 50-138ND Acetone ug/kg 15901520 105 20-136ND Benzene ug/kg 777758 103 60-145ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 49 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 3990259MATRIX SPIKE SAMPLE: MSSpike Result 92662335001 Bromobenzene ug/kg 737758 97 59-145ND Bromochloromethane ug/kg 738758 97 57-143ND Bromodichloromethane ug/kg 803758 106 53-133ND Bromoform ug/kg 730758 96 48-133ND Bromomethane ug/kg 568758 75 10-167ND Carbon tetrachloride ug/kg 811758 107 57-147ND Chlorobenzene ug/kg 800758 106 61-144ND Chloroethane ug/kg 716 IH75894 10-153ND Chloroform ug/kg 797758 105 58-141ND Chloromethane ug/kg 1180 IH,v1758156 54-165ND cis-1,2-Dichloroethene ug/kg 804758 106 59-144ND cis-1,3-Dichloropropene ug/kg 785758 104 56-137ND Dibromochloromethane ug/kg 779758 103 53-139ND Dibromomethane ug/kg 790758 104 60-136ND Dichlorodifluoromethane ug/kg 1210 IH,v1758160 49-177ND Diisopropyl ether ug/kg 802758 106 53-136ND Ethylbenzene ug/kg 775758 102 53-1503.9J Hexachloro-1,3-butadiene ug/kg 657758 87 42-186ND Isopropylbenzene (Cumene)ug/kg 845758 111 62-154ND m&p-Xylene ug/kg 16401520 108 49-156ND Methyl-tert-butyl ether ug/kg 756758 100 54-133ND Methylene Chloride ug/kg 951758 111 50-153112 n-Butylbenzene ug/kg 719758 95 44-174ND n-Propylbenzene ug/kg 765758 101 52-157ND Naphthalene ug/kg 522758 69 37-150ND o-Xylene ug/kg 833758 110 54-150ND p-Isopropyltoluene ug/kg 758758 100 50-164ND sec-Butylbenzene ug/kg 799758 105 58-161ND Styrene ug/kg 791758 104 60-148ND tert-Butylbenzene ug/kg 769758 102 44-151ND Tetrachloroethene ug/kg 718758 95 53-151ND Toluene ug/kg 809758 107 52-148ND trans-1,2-Dichloroethene ug/kg 762758 101 60-148ND trans-1,3-Dichloropropene ug/kg 782758 103 55-133ND Trichloroethene ug/kg 802758 106 60-148ND Trichlorofluoromethane ug/kg 520758 69 10-154ND Vinyl acetate ug/kg 13001520 86 50-149ND Vinyl chloride ug/kg 995 IH758131 57-157ND Xylene (Total)ug/kg 24802270 109 52-153ND 1,2-Dichloroethane-d4 (S)%91 70-130 4-Bromofluorobenzene (S)%106 70-130 Toluene-d8 (S)%101 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 50 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92662335002 3990260SAMPLE DUPLICATE: 1,1,1,2-Tetrachloroethane ug/kg ND 30ND 1,1,1-Trichloroethane ug/kg ND 30ND 1,1,2,2-Tetrachloroethane ug/kg ND 30ND 1,1,2-Trichloroethane ug/kg ND 30ND 1,1-Dichloroethane ug/kg ND 30ND 1,1-Dichloroethene ug/kg ND 30ND 1,1-Dichloropropene ug/kg ND 30ND 1,2,3-Trichlorobenzene ug/kg ND 30ND 1,2,3-Trichloropropane ug/kg ND 30ND 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2,4-Trimethylbenzene ug/kg ND 30ND 1,2-Dibromo-3-chloropropane ug/kg ND 30ND 1,2-Dibromoethane (EDB)ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,2-Dichloroethane ug/kg ND 30ND 1,2-Dichloropropane ug/kg ND 30ND 1,3,5-Trimethylbenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,3-Dichloropropane ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 2,2-Dichloropropane ug/kg ND 30ND 2-Butanone (MEK)ug/kg ND 30ND 2-Chlorotoluene ug/kg ND 30ND 2-Hexanone ug/kg ND 30ND 4-Chlorotoluene ug/kg ND 30ND 4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND Acetone ug/kg ND 30ND Benzene ug/kg ND 30ND Bromobenzene ug/kg ND 30ND Bromochloromethane ug/kg ND 30ND Bromodichloromethane ug/kg ND 30ND Bromoform ug/kg ND 30ND Bromomethane ug/kg ND 30ND Carbon tetrachloride ug/kg ND 30ND Chlorobenzene ug/kg ND 30ND Chloroethane ug/kg ND IH30ND Chloroform ug/kg ND 30ND Chloromethane ug/kg ND IH,v130ND cis-1,2-Dichloroethene ug/kg ND 30ND cis-1,3-Dichloropropene ug/kg ND 30ND Dibromochloromethane ug/kg ND 30ND Dibromomethane ug/kg ND 30ND Dichlorodifluoromethane ug/kg ND IH,v130ND Diisopropyl ether ug/kg ND 30ND Ethylbenzene ug/kg ND 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Isopropylbenzene (Cumene)ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 51 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92662335002 3990260SAMPLE DUPLICATE: m&p-Xylene ug/kg ND 30ND Methyl-tert-butyl ether ug/kg ND 30ND Methylene Chloride ug/kg 153 C92530119 n-Butylbenzene ug/kg ND 30ND n-Propylbenzene ug/kg ND 30ND Naphthalene ug/kg ND 30ND o-Xylene ug/kg ND 30ND p-Isopropyltoluene ug/kg ND 30ND sec-Butylbenzene ug/kg ND 30ND Styrene ug/kg ND 30ND tert-Butylbenzene ug/kg ND 30ND Tetrachloroethene ug/kg ND 30ND Toluene ug/kg ND 30ND trans-1,2-Dichloroethene ug/kg ND 30ND trans-1,3-Dichloropropene ug/kg ND 30ND Trichloroethene ug/kg ND 30ND Trichlorofluoromethane ug/kg ND 30ND Vinyl acetate ug/kg ND 30ND Vinyl chloride ug/kg ND IH30ND Xylene (Total)ug/kg ND 30ND 1,2-Dichloroethane-d4 (S)%102102 4-Bromofluorobenzene (S)%103104 Toluene-d8 (S)%100102 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 52 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 768315 EPA 3546 EPA 8270E 8270E Solid MSSV Microwave Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples: 92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 3989138 Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Matrix: Solid AnalyzedMDL 1,2,4-Trichlorobenzene ug/kg ND 331 04/16/23 09:11130 1,2-Dichlorobenzene ug/kg ND 331 04/16/23 09:11119 1,3-Dichlorobenzene ug/kg ND 331 04/16/23 09:11117 1,4-Dichlorobenzene ug/kg ND 331 04/16/23 09:11126 1-Methylnaphthalene ug/kg ND 331 04/16/23 09:11116 2,2'-Oxybis(1-chloropropane)ug/kg ND 331 04/16/23 09:11158 2,4,5-Trichlorophenol ug/kg ND 331 04/16/23 09:11152 2,4,6-Trichlorophenol ug/kg ND 331 04/16/23 09:11136 2,4-Dichlorophenol ug/kg ND 331 04/16/23 09:11129 2,4-Dimethylphenol ug/kg ND 331 04/16/23 09:11137 2,4-Dinitrophenol ug/kg ND 1660 04/16/23 09:111020 2,4-Dinitrotoluene ug/kg ND 331 04/16/23 09:11127 2,6-Dinitrotoluene ug/kg ND 331 04/16/23 09:11121 2-Chloronaphthalene ug/kg ND 331 04/16/23 09:11131 2-Chlorophenol ug/kg ND 331 04/16/23 09:11124 2-Methylnaphthalene ug/kg ND 331 04/16/23 09:11132 2-Methylphenol(o-Cresol)ug/kg ND 331 04/16/23 09:11135 2-Nitroaniline ug/kg ND 1660 04/16/23 09:11271 2-Nitrophenol ug/kg ND 331 04/16/23 09:11143 3&4-Methylphenol(m&p Cresol)ug/kg ND 331 04/16/23 09:11133 3,3'-Dichlorobenzidine ug/kg ND 662 04/16/23 09:11224 3-Nitroaniline ug/kg ND 1660 04/16/23 09:11260 4,6-Dinitro-2-methylphenol ug/kg ND 662 04/16/23 09:11309 4-Bromophenylphenyl ether ug/kg ND 331 04/16/23 09:11127 4-Chloro-3-methylphenol ug/kg ND 662 04/16/23 09:11233 4-Chloroaniline ug/kg ND 662 04/16/23 09:11260 4-Chlorophenylphenyl ether ug/kg ND 331 04/16/23 09:11123 4-Nitroaniline ug/kg ND 662 04/16/23 09:11252 4-Nitrophenol ug/kg ND 1660 04/16/23 09:11640 Acenaphthene ug/kg ND 331 04/16/23 09:11116 Acenaphthylene ug/kg ND 331 04/16/23 09:11116 Aniline ug/kg ND 331 04/16/23 09:11129 Anthracene ug/kg ND 331 04/16/23 09:11108 Benzo(a)anthracene ug/kg ND 331 04/16/23 09:11110 Benzo(a)pyrene ug/kg ND 331 04/16/23 09:11114 Benzo(b)fluoranthene ug/kg ND 331 04/16/23 09:11110 Benzo(g,h,i)perylene ug/kg ND 331 04/16/23 09:11128 Benzo(k)fluoranthene ug/kg ND 331 04/16/23 09:11116 Benzoic Acid ug/kg ND 1660 04/16/23 09:11711 Benzyl alcohol ug/kg ND 662 04/16/23 09:11251 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 53 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: 3989138 Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Matrix: Solid AnalyzedMDL bis(2-Chloroethoxy)methane ug/kg ND 331 04/16/23 09:11137 bis(2-Chloroethyl) ether ug/kg ND 331 04/16/23 09:11124 bis(2-Ethylhexyl)phthalate ug/kg ND 331 04/16/23 09:11128 Butylbenzylphthalate ug/kg ND 331 04/16/23 09:11139 Chrysene ug/kg ND 331 04/16/23 09:11120 Di-n-butylphthalate ug/kg ND 331 04/16/23 09:11111 Di-n-octylphthalate ug/kg ND 331 04/16/23 09:11130 Dibenz(a,h)anthracene ug/kg ND 331 04/16/23 09:11127 Dibenzofuran ug/kg ND 331 04/16/23 09:11119 Diethylphthalate ug/kg ND 331 04/16/23 09:11121 Dimethylphthalate ug/kg ND 331 04/16/23 09:11120 Fluoranthene ug/kg ND 331 04/16/23 09:11113 Fluorene ug/kg ND 331 04/16/23 09:11116 Hexachloro-1,3-butadiene ug/kg ND 331 04/16/23 09:11143 Hexachlorobenzene ug/kg ND 331 04/16/23 09:11129 Hexachlorocyclopentadiene ug/kg ND 331 04/16/23 09:11190 Hexachloroethane ug/kg ND 331 04/16/23 09:11126 Indeno(1,2,3-cd)pyrene ug/kg ND 331 04/16/23 09:11130 Isophorone ug/kg ND 331 04/16/23 09:11147 N-Nitroso-di-n-propylamine ug/kg ND 331 04/16/23 09:11124 N-Nitrosodimethylamine ug/kg ND 331 04/16/23 09:11111 N-Nitrosodiphenylamine ug/kg ND 331 04/16/23 09:11117 Naphthalene ug/kg ND 331 04/16/23 09:11112 Nitrobenzene ug/kg ND 331 04/16/23 09:11154 Pentachlorophenol ug/kg ND 662 04/16/23 09:11324 Phenanthrene ug/kg ND 331 04/16/23 09:11108 Phenol ug/kg ND 331 04/16/23 09:11147 Pyrene ug/kg ND 331 04/16/23 09:11134 Pyridine ug/kg ND 331 04/16/23 09:11104 2,4,6-Tribromophenol (S)%59 10-131 04/16/23 09:11 2-Fluorobiphenyl (S)%60 10-130 04/16/23 09:11 2-Fluorophenol (S)%54 10-130 04/16/23 09:11 Nitrobenzene-d5 (S)%57 10-130 04/16/23 09:11 Phenol-d6 (S)%54 10-130 04/16/23 09:11 Terphenyl-d14 (S)%70 10-130 04/16/23 09:11 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3989137LABORATORY CONTROL SAMPLE: LCSSpike 1,2,4-Trichlorobenzene ug/kg 11301670 68 43-130 1,2-Dichlorobenzene ug/kg 11101670 66 43-130 1,3-Dichlorobenzene ug/kg 10901670 65 43-130 1,4-Dichlorobenzene ug/kg 10901670 65 44-130 1-Methylnaphthalene ug/kg 12001670 72 47-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 54 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3989137LABORATORY CONTROL SAMPLE: LCSSpike 2,2'-Oxybis(1-chloropropane)ug/kg 9851670 59 29-130 2,4,5-Trichlorophenol ug/kg 12301670 73 47-130 2,4,6-Trichlorophenol ug/kg 12401670 74 47-130 2,4-Dichlorophenol ug/kg 12701670 76 45-130 2,4-Dimethylphenol ug/kg 17201670 103 45-130 2,4-Dinitrophenol ug/kg 38608360 46 27-140 2,4-Dinitrotoluene ug/kg 12101670 72 46-130 2,6-Dinitrotoluene ug/kg 12301670 73 48-130 2-Chloronaphthalene ug/kg 11401670 68 46-130 2-Chlorophenol ug/kg 11801670 71 43-130 2-Methylnaphthalene ug/kg 11301670 68 47-130 2-Methylphenol(o-Cresol)ug/kg 12201670 73 42-130 2-Nitroaniline ug/kg 22403340 67 41-130 2-Nitrophenol ug/kg 11601670 69 48-130 3&4-Methylphenol(m&p Cresol)ug/kg 11801670 71 39-130 3,3'-Dichlorobenzidine ug/kg 20303340 61 41-130 3-Nitroaniline ug/kg 20003340 60 37-130 4,6-Dinitro-2-methylphenol ug/kg 22203340 66 38-141 4-Bromophenylphenyl ether ug/kg 11701670 70 47-130 4-Chloro-3-methylphenol ug/kg 24303340 73 44-130 4-Chloroaniline ug/kg 22003340 66 41-130 4-Chlorophenylphenyl ether ug/kg 11601670 69 45-130 4-Nitroaniline ug/kg 21703340 65 42-130 4-Nitrophenol ug/kg 59808360 72 39-131 Acenaphthene ug/kg 11701670 70 49-130 Acenaphthylene ug/kg 12001670 72 50-130 Aniline ug/kg 9761670 58 38-130 Anthracene ug/kg 11301670 67 49-130 Benzo(a)anthracene ug/kg 12201670 73 51-130 Benzo(a)pyrene ug/kg 13001670 78 51-130 Benzo(b)fluoranthene ug/kg 12901670 77 49-130 Benzo(g,h,i)perylene ug/kg 14001670 84 48-140 Benzo(k)fluoranthene ug/kg 13601670 81 51-130 Benzoic Acid ug/kg 834J L2836010 22-130 Benzyl alcohol ug/kg 21803340 65 43-130 bis(2-Chloroethoxy)methane ug/kg 10601670 64 43-130 bis(2-Chloroethyl) ether ug/kg 10501670 63 42-130 bis(2-Ethylhexyl)phthalate ug/kg 12001670 72 43-130 Butylbenzylphthalate ug/kg 12201670 73 44-131 Chrysene ug/kg 12401670 74 51-130 Di-n-butylphthalate ug/kg 11501670 69 46-130 Di-n-octylphthalate ug/kg 11701670 70 45-130 Dibenz(a,h)anthracene ug/kg 13801670 82 48-130 Dibenzofuran ug/kg 11701670 70 10-130 Diethylphthalate ug/kg 11901670 71 48-130 Dimethylphthalate ug/kg 11801670 70 48-130 Fluoranthene ug/kg 11801670 71 48-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 55 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3989137LABORATORY CONTROL SAMPLE: LCSSpike Fluorene ug/kg 12001670 72 48-130 Hexachloro-1,3-butadiene ug/kg 11001670 66 39-130 Hexachlorobenzene ug/kg 11501670 69 47-130 Hexachlorocyclopentadiene ug/kg 12301670 74 17-130 Hexachloroethane ug/kg 11001670 66 40-130 Indeno(1,2,3-cd)pyrene ug/kg 14301670 85 50-130 Isophorone ug/kg 11301670 68 41-130 N-Nitroso-di-n-propylamine ug/kg 10801670 64 36-130 N-Nitrosodimethylamine ug/kg 10901670 65 34-130 N-Nitrosodiphenylamine ug/kg 11801670 70 48-130 Naphthalene ug/kg 11301670 68 46-130 Nitrobenzene ug/kg 10801670 65 39-130 Pentachlorophenol ug/kg 21803340 65 42-130 Phenanthrene ug/kg 12001670 72 50-130 Phenol ug/kg 12601670 76 42-130 Pyrene ug/kg 12701670 76 50-130 Pyridine ug/kg 8671670 52 26-130 2,4,6-Tribromophenol (S)%72 10-131 2-Fluorobiphenyl (S)%68 10-130 2-Fluorophenol (S)%68 10-130 Nitrobenzene-d5 (S)%65 10-130 Phenol-d6 (S)%67 10-130 Terphenyl-d14 (S)%75 10-130 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 3989139MATRIX SPIKE SAMPLE: MSSpike Result 92661774001 1,2,4-Trichlorobenzene ug/kg 10801830 59 16-130ND 1,2-Dichlorobenzene ug/kg 10001830 55 19-130ND 1,3-Dichlorobenzene ug/kg 9821830 53 19-130ND 1,4-Dichlorobenzene ug/kg 9951830 54 20-130ND 1-Methylnaphthalene ug/kg 10401830 57 19-130ND 2,2'-Oxybis(1-chloropropane)ug/kg 8941830 49 10-130ND 2,4,5-Trichlorophenol ug/kg 10701830 58 19-130ND 2,4,6-Trichlorophenol ug/kg 11501830 63 18-130ND 2,4-Dichlorophenol ug/kg 11901830 65 16-130ND 2,4-Dimethylphenol ug/kg 17401830 95 10-130ND 2,4-Dinitrophenol ug/kg 52709190 57 10-143ND 2,4-Dinitrotoluene ug/kg 8131830 44 19-130ND 2,6-Dinitrotoluene ug/kg 11701830 64 22-130ND 2-Chloronaphthalene ug/kg 9271830 50 18-130ND 2-Chlorophenol ug/kg 10601830 58 20-130ND 2-Methylnaphthalene ug/kg 9751830 53 18-130ND 2-Methylphenol(o-Cresol)ug/kg 10601830 58 13-130ND 2-Nitroaniline ug/kg 19203670 52 18-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 56 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 3989139MATRIX SPIKE SAMPLE: MSSpike Result 92661774001 2-Nitrophenol ug/kg 12001830 65 19-130ND 3&4-Methylphenol(m&p Cresol)ug/kg 10401830 57 13-130ND 3,3'-Dichlorobenzidine ug/kg 17003670 46 10-130ND 3-Nitroaniline ug/kg 1590J3670 43 22-130ND 4,6-Dinitro-2-methylphenol ug/kg 22703670 62 10-144ND 4-Bromophenylphenyl ether ug/kg 11601830 63 18-130ND 4-Chloro-3-methylphenol ug/kg 20103670 55 16-130ND 4-Chloroaniline ug/kg 18503670 50 17-130ND 4-Chlorophenylphenyl ether ug/kg 10601830 58 17-130ND 4-Nitroaniline ug/kg 16903670 46 21-130ND 4-Nitrophenol ug/kg 50309190 55 13-131ND Acenaphthene ug/kg 9621830 52 20-130ND Acenaphthylene ug/kg 10101830 55 21-130ND Aniline ug/kg 7721830 42 10-130ND Anthracene ug/kg 9921830 54 19-130ND Benzo(a)anthracene ug/kg 10801830 59 17-130ND Benzo(a)pyrene ug/kg 11501830 63 14-130ND Benzo(b)fluoranthene ug/kg 12101830 66 11-134ND Benzo(g,h,i)perylene ug/kg 10001830 55 12-130ND Benzo(k)fluoranthene ug/kg 12701830 69 15-130ND Benzoic Acid ug/kg 48109190 52 10-130ND Benzyl alcohol ug/kg 18603670 51 20-130ND bis(2-Chloroethoxy)methane ug/kg 9801830 53 16-130ND bis(2-Chloroethyl) ether ug/kg 9611830 52 18-130ND bis(2-Ethylhexyl)phthalate ug/kg 10801830 59 11-130ND Butylbenzylphthalate ug/kg 10201830 56 10-130ND Chrysene ug/kg 11101830 61 17-130ND Di-n-butylphthalate ug/kg 10101830 55 16-130ND Di-n-octylphthalate ug/kg 10101830 55 16-130ND Dibenz(a,h)anthracene ug/kg 10301830 56 13-130ND Dibenzofuran ug/kg 10401830 57 19-130ND Diethylphthalate ug/kg 9531830 52 22-130ND Dimethylphthalate ug/kg 8161830 44 23-130ND Fluoranthene ug/kg 11701830 64 14-130ND Fluorene ug/kg 9611830 52 19-130ND Hexachloro-1,3-butadiene ug/kg 11101830 61 12-130ND Hexachlorobenzene ug/kg 12601830 68 17-130ND Hexachlorocyclopentadiene ug/kg 11901830 65 10-130ND Hexachloroethane ug/kg 10201830 55 14-130ND Indeno(1,2,3-cd)pyrene ug/kg 10701830 58 13-130ND Isophorone ug/kg 9761830 53 17-130ND N-Nitroso-di-n-propylamine ug/kg 10001830 55 10-130ND N-Nitrosodimethylamine ug/kg 9201830 50 16-130ND N-Nitrosodiphenylamine ug/kg 15101830 82 19-130ND Naphthalene ug/kg 10301830 56 18-130ND Nitrobenzene ug/kg 10301830 56 15-130ND Pentachlorophenol ug/kg 21903670 60 10-130ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 57 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 3989139MATRIX SPIKE SAMPLE: MSSpike Result 92661774001 Phenanthrene ug/kg 10501830 57 17-130ND Phenol ug/kg 11001830 60 15-130ND Pyrene ug/kg 11101830 60 31-130ND Pyridine ug/kg 6361830 35 10-130ND 2,4,6-Tribromophenol (S)%66 10-131 2-Fluorobiphenyl (S)%53 10-130 2-Fluorophenol (S)%52 10-130 Nitrobenzene-d5 (S)%56 10-130 Phenol-d6 (S)%51 10-130 Terphenyl-d14 (S)%63 10-130 Parameter Units Dup Result Max RPD QualifiersRPDResult 92661946008 3989140SAMPLE DUPLICATE: 1,2,4-Trichlorobenzene ug/kg ND 30ND 1,2-Dichlorobenzene ug/kg ND 30ND 1,3-Dichlorobenzene ug/kg ND 30ND 1,4-Dichlorobenzene ug/kg ND 30ND 1-Methylnaphthalene ug/kg ND 30ND 2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND 2,4,5-Trichlorophenol ug/kg ND 30ND 2,4,6-Trichlorophenol ug/kg ND 30ND 2,4-Dichlorophenol ug/kg ND 30ND 2,4-Dimethylphenol ug/kg ND 30ND 2,4-Dinitrophenol ug/kg ND 30ND 2,4-Dinitrotoluene ug/kg ND 30ND 2,6-Dinitrotoluene ug/kg ND 30ND 2-Chloronaphthalene ug/kg ND 30ND 2-Chlorophenol ug/kg ND 30ND 2-Methylnaphthalene ug/kg ND 30ND 2-Methylphenol(o-Cresol)ug/kg ND 30ND 2-Nitroaniline ug/kg ND 30ND 2-Nitrophenol ug/kg ND 30ND 3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND 3,3'-Dichlorobenzidine ug/kg ND 30ND 3-Nitroaniline ug/kg ND 30ND 4,6-Dinitro-2-methylphenol ug/kg ND 30ND 4-Bromophenylphenyl ether ug/kg ND 30ND 4-Chloro-3-methylphenol ug/kg ND 30ND 4-Chloroaniline ug/kg ND 30ND 4-Chlorophenylphenyl ether ug/kg ND 30ND 4-Nitroaniline ug/kg ND 30ND 4-Nitrophenol ug/kg ND 30ND Acenaphthene ug/kg 1290J 30ND Acenaphthylene ug/kg ND 30ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 58 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Dup Result Max RPD QualifiersRPDResult 92661946008 3989140SAMPLE DUPLICATE: Aniline ug/kg ND 30ND Anthracene ug/kg 2680 0 302.7 mg/kg Benzo(a)anthracene ug/kg 8890 11 307.9 mg/kg Benzo(a)pyrene ug/kg 7650 14 306.6 mg/kg Benzo(b)fluoranthene ug/kg 11600 10 3010.5 mg/kg Benzo(g,h,i)perylene ug/kg 5510 14 304.8 mg/kg Benzo(k)fluoranthene ug/kg 4830 13 304.2 mg/kg Benzoic Acid ug/kg ND 30ND Benzyl alcohol ug/kg ND 30ND bis(2-Chloroethoxy)methane ug/kg ND 30ND bis(2-Chloroethyl) ether ug/kg ND 30ND bis(2-Ethylhexyl)phthalate ug/kg ND 30ND Butylbenzylphthalate ug/kg ND 30ND Chrysene ug/kg 9290 6 308.8 mg/kg Di-n-butylphthalate ug/kg ND 30ND Di-n-octylphthalate ug/kg ND 30ND Dibenz(a,h)anthracene ug/kg 1800J 30ND Dibenzofuran ug/kg ND 30ND Diethylphthalate ug/kg ND 30ND Dimethylphthalate ug/kg ND 30ND Fluoranthene ug/kg 14900 4 3014.3 mg/kg Fluorene ug/kg 1160J 30ND Hexachloro-1,3-butadiene ug/kg ND 30ND Hexachlorobenzene ug/kg ND 30ND Hexachlorocyclopentadiene ug/kg ND 30ND Hexachloroethane ug/kg ND 30ND Indeno(1,2,3-cd)pyrene ug/kg 5180 16 304.4 mg/kg Isophorone ug/kg ND 30ND N-Nitroso-di-n-propylamine ug/kg ND 30ND N-Nitrosodimethylamine ug/kg ND 30ND N-Nitrosodiphenylamine ug/kg ND 30ND Naphthalene ug/kg ND 30ND Nitrobenzene ug/kg ND 30ND Pentachlorophenol ug/kg ND 30ND Phenanthrene ug/kg 12600 6 3013.3 mg/kg Phenol ug/kg ND 30ND Pyrene ug/kg 16200 8 3015.0 mg/kg Pyridine ug/kg ND 30ND 2,4,6-Tribromophenol (S)%3937 2-Fluorobiphenyl (S)%3834 2-Fluorophenol (S)%3729 Nitrobenzene-d5 (S)%49 D347 Phenol-d6 (S)%4840 Terphenyl-d14 (S)%6361 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 59 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 768218 SW-846 SW-846 Dry Weight/Percent Moisture Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335006, 92662335007, 92662335008, 92662335009, 92662335010, 92662335011, 92662335012 Parameter Units Dup Result Max RPD QualifiersRPDResult 92662312006 3988581SAMPLE DUPLICATE: Percent Moisture %25.3 N262526.9 Parameter Units Dup Result Max RPD QualifiersRPDResult 92662335012 3988642SAMPLE DUPLICATE: Percent Moisture %24.9 N222525.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 60 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2045390 SM 2540 G SM 2540G Total Solids 2540 G-2011 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92662335001, 92662335002, 92662335003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3915770-1 Associated Lab Samples:92662335001, 92662335002, 92662335003 Matrix: Solid AnalyzedMDL Total Solids %0.00200 04/20/23 11:14 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3915770-2LABORATORY CONTROL SAMPLE: LCSSpike Total Solids %50.050.0 100 85.0-115 Parameter Units Dup Result Max RPD QualifiersRPDResult L1606384-18 R3915770-3SAMPLE DUPLICATE: Total Solids %72.4 0.987 1071.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 61 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2045415 SM 2540 G SM 2540G Total Solids 2540 G-2011 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92662335004, 92662335005, 92662335012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3916181-1 Associated Lab Samples:92662335004, 92662335005, 92662335012 Matrix: Solid AnalyzedMDL Total Solids %0.00400 04/21/23 17:48 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3916181-2LABORATORY CONTROL SAMPLE: LCSSpike Total Solids %50.050.0 100 85.0-115 Parameter Units Dup Result Max RPD QualifiersRPDResult 92662335004 R3916181-3SAMPLE DUPLICATE: Total Solids %76.8 1.23 1075.8 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 62 of 69 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 2045352 3060A EPA 7199 Wet Chemistry 7199 Laboratory:Pace National - Mt. Juliet Associated Lab Samples: 92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK: R3916419-1 Associated Lab Samples:92662335001, 92662335002, 92662335003, 92662335004, 92662335005, 92662335012 Matrix: Solid AnalyzedMDL Chromium, Hexavalent mg/kg ND 1.00 04/24/23 01:200.255 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. R3916419-2LABORATORY CONTROL SAMPLE: LCSSpike Chromium, Hexavalent mg/kg 10.510.0 105 80.0-120 Parameter Units MS Result % Rec Limits Qual% RecConc. R3916419-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result L1606850-05 R3916419-6 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Chromium, Hexavalent mg/kg 23.7 75.8 75.0-12578.3 3.23 2023.7ND 17.9 18.5 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. R3916419-7MATRIX SPIKE SAMPLE: MSSpike Result L1606850-05 Chromium, Hexavalent mg/kg 693761 91.1 75.0-125ND Parameter Units Dup Result Max RPD QualifiersRPDResult L1606425-09 R3916419-3SAMPLE DUPLICATE: Chromium, Hexavalent mg/kg ND 0.00 20ND Parameter Units Dup Result Max RPD QualifiersRPDResult L1606853-05 R3916419-8SAMPLE DUPLICATE: Chromium, Hexavalent mg/kg ND 0.00 20ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 63 of 69 #=QL# QUALIFIERS Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Common Laboratory Contaminant.C9 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should beconsidered an estimated value.IH Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high.L1 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples may be biased low.L2 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request.N2 RPD value was outside control limits.R1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias.v1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 64 of 69 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92662335003 877876 877975BF-SB-03 (4-5)EPA 3015A EPA 6010D 92662335004 877876 877975BF-SB-04 (2-4)EPA 3015A EPA 6010D 92662335010 877876 877975COMP-3E (0.5-2)EPA 3015A EPA 6010D 92662335012 877876 877975BF-SB-DUP EPA 3015A EPA 6010D 92662335001 876553 876687BF-SB-01 (5-7)EPA 3050B EPA 6020B 92662335002 876553 876687BF-SB-02 (5-7)EPA 3050B EPA 6020B 92662335003 876553 876687BF-SB-03 (4-5)EPA 3050B EPA 6020B 92662335004 876553 876687BF-SB-04 (2-4)EPA 3050B EPA 6020B 92662335005 876553 876687BF-SB-05 (2-4)EPA 3050B EPA 6020B 92662335006 876553 876687COMP-3A (0.5-2)EPA 3050B EPA 6020B 92662335007 876553 876687COMP-3B (0.5-2)EPA 3050B EPA 6020B 92662335008 876553 876687COMP-3C (0.5-2)EPA 3050B EPA 6020B 92662335009 876553 876687COMP-3D (0.5-2)EPA 3050B EPA 6020B 92662335010 876553 876687COMP-3E (0.5-2)EPA 3050B EPA 6020B 92662335011 876553 876687COMP-3F (0.5-2)EPA 3050B EPA 6020B 92662335012 876553 876687BF-SB-DUP EPA 3050B EPA 6020B 92662335001 876585 876671BF-SB-01 (5-7)EPA 7471B EPA 7471B 92662335002 876585 876671BF-SB-02 (5-7)EPA 7471B EPA 7471B 92662335003 876585 876671BF-SB-03 (4-5)EPA 7471B EPA 7471B 92662335004 876585 876671BF-SB-04 (2-4)EPA 7471B EPA 7471B 92662335005 876585 876671BF-SB-05 (2-4)EPA 7471B EPA 7471B 92662335012 876585 876671BF-SB-DUP EPA 7471B EPA 7471B 92662335001 768315 768346BF-SB-01 (5-7)EPA 3546 EPA 8270E 92662335002 768315 768346BF-SB-02 (5-7)EPA 3546 EPA 8270E 92662335003 768315 768346BF-SB-03 (4-5)EPA 3546 EPA 8270E 92662335004 768315 768346BF-SB-04 (2-4)EPA 3546 EPA 8270E 92662335005 768315 768346BF-SB-05 (2-4)EPA 3546 EPA 8270E 92662335012 768315 768346BF-SB-DUP EPA 3546 EPA 8270E 92662335001 768545 768908BF-SB-01 (5-7)EPA 5035A/5030B EPA 8260D 92662335002 768545 768908BF-SB-02 (5-7)EPA 5035A/5030B EPA 8260D 92662335003 768545 768908BF-SB-03 (4-5)EPA 5035A/5030B EPA 8260D 92662335004 768545 768908BF-SB-04 (2-4)EPA 5035A/5030B EPA 8260D 92662335005 768545 768908BF-SB-05 (2-4)EPA 5035A/5030B EPA 8260D 92662335012 768545 768908BF-SB-DUP EPA 5035A/5030B EPA 8260D 92662335001 768218BF-SB-01 (5-7)SW-846 92662335002 768218BF-SB-02 (5-7)SW-846 92662335003 768218BF-SB-03 (4-5)SW-846 92662335004 768218BF-SB-04 (2-4)SW-846 92662335005 768218BF-SB-05 (2-4)SW-846 92662335006 768218COMP-3A (0.5-2)SW-846 92662335007 768218COMP-3B (0.5-2)SW-846 92662335008 768218COMP-3C (0.5-2)SW-846 92662335009 768218COMP-3D (0.5-2)SW-846 92662335010 768218COMP-3E (0.5-2)SW-846 92662335011 768218COMP-3F (0.5-2)SW-846 92662335012 768218BF-SB-DUP SW-846 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 65 of 69 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92662335 ABS.003 Commercial Equipment Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92662335001 2045390 2045390BF-SB-01 (5-7)SM 2540 G SM 2540G 92662335002 2045390 2045390BF-SB-02 (5-7)SM 2540 G SM 2540G 92662335003 2045390 2045390BF-SB-03 (4-5)SM 2540 G SM 2540G 92662335004 2045415 2045415BF-SB-04 (2-4)SM 2540 G SM 2540G 92662335005 2045415 2045415BF-SB-05 (2-4)SM 2540 G SM 2540G 92662335012 2045415 2045415BF-SB-DUP SM 2540 G SM 2540G 92662335001 2045352 2045352BF-SB-01 (5-7)3060A EPA 7199 92662335002 2045352 2045352BF-SB-02 (5-7)3060A EPA 7199 92662335003 2045352 2045352BF-SB-03 (4-5)3060A EPA 7199 92662335004 2045352 2045352BF-SB-04 (2-4)3060A EPA 7199 92662335005 2045352 2045352BF-SB-05 (2-4)3060A EPA 7199 92662335012 2045352 2045352BF-SB-DUP 3060A EPA 7199 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 05/12/2023 01:52 PM Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 66 of 69 Page 67 of 69 Page 68 of 69 Page 69 of 69   Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.   5/8/2023 Hart & Hickman (Charlotte) Haley Martin 2923 South Tryon St. Ste 100 Charlotte, NC, 28203 Ref: Analytical Testing Lab Report Number: 23-108-0008 Client Project Description: ABS.003 Dear Haley Martin: Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/18/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Angela D Overcash Senior Project Manager Page 1 of 41 Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date 07/31/202337735State ProgramNorth Carolina 12/31/2023402State ProgramNorth Carolina 07/31/202399012State ProgramSouth Carolina 12/31/202299012State ProgramSouth Carolina Page 1 of 1 00016/23-108-0008 Page 2 of 41 Report Number: Sample Summary Table Client Project Description: 23-108-0008 ABS.003 Lab No Client Sample ID Matrix Date Collected Date Received 04/17/2023Air 94126 SSV-DUP 04/18/2023 12:21 04/17/2023 14:46Air 94127 SSV-3 04/18/2023 12:21 04/17/2023 12:12Air 94128 SG-12 04/18/2023 12:21 04/17/2023 15:28Air 94129 SG-11 04/18/2023 12:21 04/17/2023 13:36Air 94130 SG-10 04/18/2023 12:21 04/17/2023 14:15Air 94131 SG-9 04/18/2023 12:21 Page 3 of 41 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-108-0008 Report Limit Project:ABS.003 V 94126SSV-DUP J2.66 04/28/2023 04:00TO-15 Acetone µg/m3 0.202 3.32 04/28/2023 04:00TO-15 Benzene µg/m3 0.073 J1.00 04/28/2023 04:00TO-15 Carbon Disulfide µg/m3 0.060 J1.61 04/28/2023 04:00TO-15 Dichlorodifluoromethane µg/m3 0.134 J0.616 04/28/2023 04:00TO-15 Ethylbenzene µg/m3 0.106 17.6 04/28/2023 04:00TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561 J0.590 04/28/2023 04:00TO-15 Heptane µg/m3 0.143 J1.44 04/28/2023 04:00TO-15 n-Hexane µg/m3 0.047 3.13 04/28/2023 04:00TO-15 Styrene µg/m3 0.124 19.7 04/28/2023 04:00TO-15 Tetrachloroethene µg/m3 0.181 J0.297 04/28/2023 04:00TO-15 Tetrahydrofuran µg/m3 0.107 6.01 04/28/2023 04:00TO-15 Toluene µg/m3 0.090 J1.77 04/28/2023 04:00TO-15 Trichloroethene µg/m3 0.199 3.80 04/28/2023 04:00TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 J0.581 04/28/2023 04:00TO-15 o-Xylene µg/m3 0.157 J3.39 04/28/2023 04:00TO-15 m,p-Xylene µg/m3 0.217 J3.97 04/28/2023 04:00TO-15 Xylene (Total)µg/m3 0.157 V 94127SSV-3 8.35 04/28/2023 04:52TO-15 Acetone µg/m3 0.202 3.19 04/28/2023 04:52TO-15 Benzene µg/m3 0.073 J1.30 04/28/2023 04:52TO-15 Carbon Disulfide µg/m3 0.060 2.92 04/28/2023 04:52TO-15 Dichlorodifluoromethane µg/m3 0.134 J0.694 04/28/2023 04:52TO-15 Ethylbenzene µg/m3 0.106 19.7 04/28/2023 04:52TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561 J0.745 04/28/2023 04:52TO-15 Heptane µg/m3 0.143 J1.57 04/28/2023 04:52TO-15 n-Hexane µg/m3 0.047 J0.609 04/28/2023 04:52TO-15 Isopropyl Alcohol µg/m3 0.139 J1.08 04/28/2023 04:52TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J1.42 04/28/2023 04:52TO-15 Naphthalene µg/m3 0.183 3.13 04/28/2023 04:52TO-15 Styrene µg/m3 0.124 20.9 04/28/2023 04:52TO-15 Tetrachloroethene µg/m3 0.181 J0.345 04/28/2023 04:52TO-15 Tetrahydrofuran µg/m3 0.107 6.21 04/28/2023 04:52TO-15 Toluene µg/m3 0.090 J1.47 04/28/2023 04:52TO-15 Trichloroethene µg/m3 0.199 3.96 04/28/2023 04:52TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 J0.716 04/28/2023 04:52TO-15 o-Xylene µg/m3 0.157 Page 4 of 41 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-108-0008 Report Limit Project:ABS.003 V 94127SSV-3 J3.46 04/28/2023 04:52TO-15 m,p-Xylene µg/m3 0.217 J4.18 04/28/2023 04:52TO-15 Xylene (Total)µg/m3 0.157 V 94128SG-12 8.67 04/28/2023 05:47TO-15 Acetone µg/m3 0.202 118 04/28/2023 05:47TO-15 Benzene µg/m3 0.073 6.19 04/28/2023 05:47TO-15 1,3-Butadiene µg/m3 0.328 140 04/28/2023 05:47TO-15 Carbon Disulfide µg/m3 0.060 J1.07 04/28/2023 05:47TO-15 Chloroform µg/m3 0.086 16.1 04/28/2023 05:47TO-15 Cyclohexane µg/m3 0.161 J1.53 04/28/2023 05:47TO-15 Dichlorodifluoromethane µg/m3 0.134 336 04/27/2023 13:31TO-15 Ethylbenzene µg/m3 2.12 57.0 04/28/2023 05:47TO-15 4-Ethyltoluene µg/m3 0.128 62.5 04/28/2023 05:47TO-15 Heptane µg/m3 0.143 24.6 04/28/2023 05:47TO-15 n-Hexane µg/m3 0.047 1.78 04/28/2023 05:47TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 7.11 04/28/2023 05:47TO-15 4-Methyl-2-Pentanone µg/m3 0.121 58.5 04/28/2023 05:47TO-15 Propene µg/m3 0.242 15.3 04/28/2023 05:47TO-15 Styrene µg/m3 0.124 J2.56 04/28/2023 05:47TO-15 Tetrachloroethene µg/m3 0.181 1820 04/27/2023 13:31TO-15 Toluene µg/m3 1.80 3.10 04/28/2023 05:47TO-15 Trichlorofluoromethane µg/m3 0.130 118 04/28/2023 05:47TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 82.9 04/28/2023 05:47TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 J0.784 04/28/2023 05:47TO-15 Vinyl Chloride µg/m3 0.127 264 04/27/2023 13:31TO-15 o-Xylene µg/m3 3.14 1450 04/27/2023 13:31TO-15 m,p-Xylene µg/m3 4.34 1710 04/27/2023 13:31TO-15 Xylene (Total)µg/m3 3.14 V 94129SG-11 17.5 04/28/2023 06:39TO-15 Acetone µg/m3 0.202 6.24 04/28/2023 06:39TO-15 Benzene µg/m3 0.073 1.25 04/28/2023 06:39TO-15 1,3-Butadiene µg/m3 0.328 19.0 04/28/2023 06:39TO-15 Carbon Disulfide µg/m3 0.060 4.61 04/28/2023 06:39TO-15 Cyclohexane µg/m3 0.161 3.63 04/28/2023 06:39TO-15 Dichlorodifluoromethane µg/m3 0.134 38.4 04/28/2023 06:39TO-15 Ethylbenzene µg/m3 0.106 13.2 04/28/2023 06:39TO-15 4-Ethyltoluene µg/m3 0.128 Page 5 of 41 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-108-0008 Report Limit Project:ABS.003 V 94129SG-11 J0.574 04/28/2023 06:39TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561 7.35 04/28/2023 06:39TO-15 Heptane µg/m3 0.143 32.2 04/28/2023 06:39TO-15 n-Hexane µg/m3 0.047 J1.79 04/28/2023 06:39TO-15 Isopropyl Alcohol µg/m3 0.139 1.58 04/28/2023 06:39TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 J1.90 04/28/2023 06:39TO-15 4-Methyl-2-Pentanone µg/m3 0.121 J1.12 04/28/2023 06:39TO-15 Naphthalene µg/m3 0.183 36.2 04/28/2023 06:39TO-15 Propene µg/m3 0.242 4.23 04/28/2023 06:39TO-15 Styrene µg/m3 0.124 15.7 04/28/2023 06:39TO-15 Tetrachloroethene µg/m3 0.181 J0.451 04/28/2023 06:39TO-15 Tetrahydrofuran µg/m3 0.107 118 04/28/2023 06:39TO-15 Toluene µg/m3 0.090 21.7 04/28/2023 06:39TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 6.49 04/28/2023 06:39TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 38.8 04/28/2023 06:39TO-15 o-Xylene µg/m3 0.157 127 04/28/2023 06:39TO-15 m,p-Xylene µg/m3 0.217 166 04/28/2023 06:39TO-15 Xylene (Total)µg/m3 0.157 V 94130SG-10 20.6 04/28/2023 07:36TO-15 Acetone µg/m3 0.202 146 04/28/2023 07:36TO-15 Benzene µg/m3 0.073 45.7 04/28/2023 07:36TO-15 1,3-Butadiene µg/m3 0.328 262 04/27/2023 14:45TO-15 Carbon Disulfide µg/m3 1.22 3.30 04/28/2023 07:36TO-15 Chloroethane µg/m3 0.164 5.52 04/28/2023 07:36TO-15 Chloroform µg/m3 0.086 4.44 04/28/2023 07:36TO-15 Chloromethane µg/m3 0.067 18.1 04/28/2023 07:36TO-15 Cyclohexane µg/m3 0.161 3.39 04/28/2023 07:36TO-15 Dichlorodifluoromethane µg/m3 0.134 249 04/27/2023 14:45TO-15 Ethylbenzene µg/m3 2.12 59.3 04/28/2023 07:36TO-15 4-Ethyltoluene µg/m3 0.128 10.2 04/28/2023 07:36TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561 109 04/28/2023 07:36TO-15 Heptane µg/m3 0.143 297 04/27/2023 14:45TO-15 n-Hexane µg/m3 0.942 J0.916 04/28/2023 07:36TO-15 Isopropyl Alcohol µg/m3 0.139 5.05 04/28/2023 07:36TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 9.32 04/28/2023 07:36TO-15 4-Methyl-2-Pentanone µg/m3 0.121 J1.44 04/28/2023 07:36TO-15 Naphthalene µg/m3 0.183 Page 6 of 41 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-108-0008 Report Limit Project:ABS.003 V 94130SG-10 1250 04/27/2023 14:45TO-15 Propene µg/m3 4.84 31.0 04/28/2023 07:36TO-15 Styrene µg/m3 0.124 5.11 04/28/2023 07:36TO-15 Tetrachloroethene µg/m3 0.181 5.39 04/28/2023 07:36TO-15 Tetrahydrofuran µg/m3 0.107 1820 04/27/2023 14:45TO-15 Toluene µg/m3 1.80 94.4 04/28/2023 07:36TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 62.8 04/28/2023 07:36TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 4.58 04/28/2023 07:36TO-15 Vinyl Chloride µg/m3 0.127 164 04/27/2023 14:45TO-15 o-Xylene µg/m3 3.14 846 04/27/2023 14:45TO-15 m,p-Xylene µg/m3 4.34 1010 04/27/2023 14:45TO-15 Xylene (Total)µg/m3 3.14 V 94131SG-9 24.1 05/04/2023 17:03TO-15 Acetone µg/m3 0.202 148 05/04/2023 17:03TO-15 Benzene µg/m3 0.073 36.9 05/04/2023 17:03TO-15 1,3-Butadiene µg/m3 0.328 110 05/04/2023 17:03TO-15 Carbon Disulfide µg/m3 0.060 J1.70 05/04/2023 17:03TO-15 Chlorobenzene µg/m3 0.107 2.97 05/04/2023 17:03TO-15 Chloroethane µg/m3 0.164 15.7 05/04/2023 17:03TO-15 Cyclohexane µg/m3 0.161 2.61 05/04/2023 17:03TO-15 Dichlorodifluoromethane µg/m3 0.134 388 04/27/2023 15:22TO-15 Ethylbenzene µg/m3 2.12 78.6 05/04/2023 17:03TO-15 4-Ethyltoluene µg/m3 0.128 J1.26 05/04/2023 17:03TO-15 1,1,2-Trichloro-1,2,2-trifluoroethane µg/m3 0.561 93.6 05/04/2023 17:03TO-15 Heptane µg/m3 0.143 330 04/27/2023 15:22TO-15 n-Hexane µg/m3 0.942 JB3.21 05/04/2023 17:03TO-15 Isopropyl Alcohol µg/m3 0.139 6.04 05/04/2023 17:03TO-15 Methyl Ethyl Ketone (MEK)µg/m3 0.224 16.3 05/04/2023 17:03TO-15 4-Methyl-2-Pentanone µg/m3 0.121 3.41 05/04/2023 17:03TO-15 Methylene Chloride µg/m3 0.488 6.26 05/04/2023 17:03TO-15 Naphthalene µg/m3 0.183 273 04/27/2023 15:22TO-15 Propene µg/m3 4.84 40.2 05/04/2023 17:03TO-15 Styrene µg/m3 0.124 J2.22 05/04/2023 17:03TO-15 Tetrachloroethene µg/m3 0.181 2700 04/27/2023 15:22TO-15 Toluene µg/m3 1.80 J2.53 05/04/2023 17:03TO-15 Trichlorofluoromethane µg/m3 0.130 158 05/04/2023 17:03TO-15 1,2,4-Trimethylbenzene µg/m3 0.110 Page 7 of 41 Summary of Detected Analytes QualifiersAnalyzedUnitsResult Report Number: Client Sample ID Method Parameters Lab Sample ID 23-108-0008 Report Limit Project:ABS.003 V 94131SG-9 86.2 05/04/2023 17:03TO-15 1,3,5-Trimethylbenzene µg/m3 0.236 4.18 05/04/2023 17:03TO-15 Vinyl Chloride µg/m3 0.127 307 04/27/2023 15:22TO-15 o-Xylene µg/m3 3.14 1410 04/27/2023 15:22TO-15 m,p-Xylene µg/m3 4.34 1720 04/27/2023 15:22TO-15 Xylene (Total)µg/m3 3.14 Page 8 of 41   Client: Hart & Hickman (Charlotte) CASE NARRATIVE Project: ABS.003 Lab Report Number: 23-108-0008 Date: 5/8/2023 Report Comments Revised Report: Revision 1 A sample ID has been corrected to match the COC. Page 9 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SSV-DUP 94126 Matrix: 4/17/2023 0:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 2.66 J µg/m3 0.202 4.75Acetone 1 04/28/23 04:00 V32621ENM 3.32 µg/m3 0.073 1.60 Benzene 1 04/28/23 04:00 V32621ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 04/28/23 04:00 V32621ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 04/28/23 04:00 V32621ENM <0.153 µg/m3 0.153 5.17Bromoform 1 04/28/23 04:00 V32621ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 04/28/23 04:00 V32621ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 04/28/23 04:00 V32621ENM 1.00 J µg/m3 0.060 6.23Carbon Disulfide 1 04/28/23 04:00 V32621ENM <0.155 µg/m3 0.155 3.15 Carbon Tetrachloride 1 04/28/23 04:00 V32621ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 04/28/23 04:00 V32621ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 04/28/23 04:00 V32621ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 04/28/23 04:00 V32621ENM <0.086 µg/m3 0.086 2.44Chloroform 1 04/28/23 04:00 V32621ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 04/28/23 04:00 V32621ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 04/28/23 04:00 V32621ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 04/28/23 04:00 V32621ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 04/28/23 04:00 V32621ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 04/28/23 04:00 V32621ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 04/28/23 04:00 V32621ENM 1.61 J µg/m3 0.134 2.47Dichlorodifluoromethane 1 04/28/23 04:00 V32621ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 04/28/23 04:00 V32621ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 04/28/23 04:00 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 10 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SSV-DUP 94126 Matrix: 4/17/2023 0:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 04/28/23 04:00 V32621ENM <0.095 µg/m3 0.095 1.98 cis-1,2-Dichloroethene 1 04/28/23 04:00 V32621ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 04/28/23 04:00 V32621ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 04/28/23 04:00 V32621ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 04/28/23 04:00 V32621ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 04/28/23 04:00 V32621ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 04/28/23 04:00 V32621ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 04/28/23 04:00 V32621ENM <0.136 µg/m3 0.136 1.80 Ethyl Acetate 1 04/28/23 04:00 V32621ENM 0.616 J µg/m3 0.106 2.17Ethylbenzene 1 04/28/23 04:00 V32621ENM <0.128 µg/m3 0.128 2.464-Ethyltoluene 1 04/28/23 04:00 V32621ENM 17.6 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 04/28/23 04:00 V32621ENM 0.590 J µg/m3 0.143 2.05Heptane 1 04/28/23 04:00 V32621ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 04/28/23 04:00 V32621ENM 1.44 J µg/m3 0.047 1.76n-Hexane 1 04/28/23 04:00 V32621ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 04/28/23 04:00 V32621ENM <0.139 µg/m3 0.139 4.92Isopropyl Alcohol 1 04/28/23 04:00 V32621ENM <0.224 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 04/28/23 04:00 V32621ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 04/28/23 04:00 V32621ENM <0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 04/28/23 04:00 V32621ENM <0.488 µg/m3 0.488 1.74Methylene Chloride 1 04/28/23 04:00 V32621ENM <0.183 µg/m3 0.183 2.62Naphthalene 1 04/28/23 04:00 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 11 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SSV-DUP 94126 Matrix: 4/17/2023 0:00 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 <0.242 µg/m3 0.242 0.860Propene 1 04/28/23 04:00 V32621ENM 3.13 µg/m3 0.124 2.13 Styrene 1 04/28/23 04:00 V32621ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 04/28/23 04:00 V32621ENM 19.7 µg/m3 0.181 3.39Tetrachloroethene 1 04/28/23 04:00 V32621ENM 0.297 J µg/m3 0.107 1.47Tetrahydrofuran 1 04/28/23 04:00 V32621ENM 6.01 µg/m3 0.090 1.88Toluene 1 04/28/23 04:00 V32621ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 04/28/23 04:00 V32621ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 04/28/23 04:00 V32621ENM <0.087 µg/m3 0.087 2.73 1,1,2-Trichloroethane 1 04/28/23 04:00 V32621ENM 1.77 J µg/m3 0.199 2.15Trichloroethene 1 04/28/23 04:00 V32621ENM <0.130 µg/m3 0.130 2.81Trichlorofluoromethane 1 04/28/23 04:00 V32621ENM 3.80 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 04/28/23 04:00 V32621ENM <0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 04/28/23 04:00 V32621ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 04/28/23 04:00 V32621ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 04/28/23 04:00 V32621ENM 0.581 J µg/m3 0.157 2.17o-Xylene 1 04/28/23 04:00 V32621ENM 3.39 J µg/m3 0.217 5.65m,p-Xylene 1 04/28/23 04:00 V32621ENM 3.97 J µg/m3 0.157 2.17Xylene (Total)1 04/28/23 04:00 V32621 Surrogate: 4-Bromofluorobenzene 74.6 Limits: 70-130%04/28/23 04:001 ENM V32621 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 12 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SSV-3 94127 Matrix: 4/17/2023 14:46 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 8.35 µg/m3 0.202 4.75Acetone 1 04/28/23 04:52 V32621ENM 3.19 µg/m3 0.073 1.60 Benzene 1 04/28/23 04:52 V32621ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 04/28/23 04:52 V32621ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 04/28/23 04:52 V32621ENM <0.153 µg/m3 0.153 5.17Bromoform 1 04/28/23 04:52 V32621ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 04/28/23 04:52 V32621ENM <0.328 µg/m3 0.328 1.111,3-Butadiene 1 04/28/23 04:52 V32621ENM 1.30 J µg/m3 0.060 6.23Carbon Disulfide 1 04/28/23 04:52 V32621ENM <0.155 µg/m3 0.155 3.15 Carbon Tetrachloride 1 04/28/23 04:52 V32621ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 04/28/23 04:52 V32621ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 04/28/23 04:52 V32621ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 04/28/23 04:52 V32621ENM <0.086 µg/m3 0.086 2.44Chloroform 1 04/28/23 04:52 V32621ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 04/28/23 04:52 V32621ENM <0.161 µg/m3 0.161 3.44Cyclohexane 1 04/28/23 04:52 V32621ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 04/28/23 04:52 V32621ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 04/28/23 04:52 V32621ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 04/28/23 04:52 V32621ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 04/28/23 04:52 V32621ENM 2.92 µg/m3 0.134 2.47Dichlorodifluoromethane 1 04/28/23 04:52 V32621ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 04/28/23 04:52 V32621ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 04/28/23 04:52 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 13 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SSV-3 94127 Matrix: 4/17/2023 14:46 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 04/28/23 04:52 V32621ENM <0.095 µg/m3 0.095 1.98 cis-1,2-Dichloroethene 1 04/28/23 04:52 V32621ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 04/28/23 04:52 V32621ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 04/28/23 04:52 V32621ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 04/28/23 04:52 V32621ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 04/28/23 04:52 V32621ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 04/28/23 04:52 V32621ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 04/28/23 04:52 V32621ENM <0.136 µg/m3 0.136 1.80 Ethyl Acetate 1 04/28/23 04:52 V32621ENM 0.694 J µg/m3 0.106 2.17Ethylbenzene 1 04/28/23 04:52 V32621ENM <0.128 µg/m3 0.128 2.464-Ethyltoluene 1 04/28/23 04:52 V32621ENM 19.7 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 04/28/23 04:52 V32621ENM 0.745 J µg/m3 0.143 2.05Heptane 1 04/28/23 04:52 V32621ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 04/28/23 04:52 V32621ENM 1.57 J µg/m3 0.047 1.76n-Hexane 1 04/28/23 04:52 V32621ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 04/28/23 04:52 V32621ENM 0.609 J µg/m3 0.139 4.92Isopropyl Alcohol 1 04/28/23 04:52 V32621ENM 1.08 J µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 04/28/23 04:52 V32621ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 04/28/23 04:52 V32621ENM <0.121 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 04/28/23 04:52 V32621ENM <0.488 µg/m3 0.488 1.74Methylene Chloride 1 04/28/23 04:52 V32621ENM 1.42 J µg/m3 0.183 2.62Naphthalene 1 04/28/23 04:52 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 14 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SSV-3 94127 Matrix: 4/17/2023 14:46 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 <0.242 µg/m3 0.242 0.860Propene 1 04/28/23 04:52 V32621ENM 3.13 µg/m3 0.124 2.13 Styrene 1 04/28/23 04:52 V32621ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 04/28/23 04:52 V32621ENM 20.9 µg/m3 0.181 3.39Tetrachloroethene 1 04/28/23 04:52 V32621ENM 0.345 J µg/m3 0.107 1.47Tetrahydrofuran 1 04/28/23 04:52 V32621ENM 6.21 µg/m3 0.090 1.88Toluene 1 04/28/23 04:52 V32621ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 04/28/23 04:52 V32621ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 04/28/23 04:52 V32621ENM <0.087 µg/m3 0.087 2.73 1,1,2-Trichloroethane 1 04/28/23 04:52 V32621ENM 1.47 J µg/m3 0.199 2.15Trichloroethene 1 04/28/23 04:52 V32621ENM <0.130 µg/m3 0.130 2.81Trichlorofluoromethane 1 04/28/23 04:52 V32621ENM 3.96 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 04/28/23 04:52 V32621ENM <0.236 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 04/28/23 04:52 V32621ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 04/28/23 04:52 V32621ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 04/28/23 04:52 V32621ENM 0.716 J µg/m3 0.157 2.17o-Xylene 1 04/28/23 04:52 V32621ENM 3.46 J µg/m3 0.217 5.65m,p-Xylene 1 04/28/23 04:52 V32621ENM 4.18 J µg/m3 0.157 2.17Xylene (Total)1 04/28/23 04:52 V32621 Surrogate: 4-Bromofluorobenzene 88.0 Limits: 70-130%04/28/23 04:521 ENM V32621 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 15 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-12 94128 Matrix: 4/17/2023 12:12 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 8.67 µg/m3 0.202 4.75Acetone 1 04/28/23 05:47 V32621ENM 118 µg/m3 0.073 1.60 Benzene 1 04/28/23 05:47 V32621ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 04/28/23 05:47 V32621ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 04/28/23 05:47 V32621ENM <0.153 µg/m3 0.153 5.17Bromoform 1 04/28/23 05:47 V32621ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 04/28/23 05:47 V32621ENM 6.19 µg/m3 0.328 1.111,3-Butadiene 1 04/28/23 05:47 V32621ENM 140 µg/m3 0.060 6.23Carbon Disulfide 1 04/28/23 05:47 V32621ENM <0.155 µg/m3 0.155 3.15 Carbon Tetrachloride 1 04/28/23 05:47 V32621ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 04/28/23 05:47 V32621ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 04/28/23 05:47 V32621ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 04/28/23 05:47 V32621ENM 1.07 J µg/m3 0.086 2.44Chloroform 1 04/28/23 05:47 V32621ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 04/28/23 05:47 V32621ENM 16.1 µg/m3 0.161 3.44Cyclohexane 1 04/28/23 05:47 V32621ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 04/28/23 05:47 V32621ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 04/28/23 05:47 V32621ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 04/28/23 05:47 V32621ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 04/28/23 05:47 V32621ENM 1.53 J µg/m3 0.134 2.47Dichlorodifluoromethane 1 04/28/23 05:47 V32621ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 04/28/23 05:47 V32621ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 04/28/23 05:47 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 16 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-12 94128 Matrix: 4/17/2023 12:12 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 04/28/23 05:47 V32621ENM <0.095 µg/m3 0.095 1.98 cis-1,2-Dichloroethene 1 04/28/23 05:47 V32621ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 04/28/23 05:47 V32621ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 04/28/23 05:47 V32621ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 04/28/23 05:47 V32621ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 04/28/23 05:47 V32621ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 04/28/23 05:47 V32621ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 04/28/23 05:47 V32621ENM <0.136 µg/m3 0.136 1.80 Ethyl Acetate 1 04/28/23 05:47 V32621ENM 336 µg/m3 2.12 43.4Ethylbenzene 20 04/27/23 13:31 V32621ENM 57.0 µg/m3 0.128 2.464-Ethyltoluene 1 04/28/23 05:47 V32621ENM <0.561 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 04/28/23 05:47 V32621ENM 62.5 µg/m3 0.143 2.05Heptane 1 04/28/23 05:47 V32621ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 04/28/23 05:47 V32621ENM 24.6 µg/m3 0.047 1.76n-Hexane 1 04/28/23 05:47 V32621ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 04/28/23 05:47 V32621ENM <0.139 µg/m3 0.139 4.92Isopropyl Alcohol 1 04/28/23 05:47 V32621ENM 1.78 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 04/28/23 05:47 V32621ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 04/28/23 05:47 V32621ENM 7.11 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 04/28/23 05:47 V32621ENM <0.488 µg/m3 0.488 1.74Methylene Chloride 1 04/28/23 05:47 V32621ENM <0.183 µg/m3 0.183 2.62Naphthalene 1 04/28/23 05:47 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 17 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-12 94128 Matrix: 4/17/2023 12:12 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 58.5 µg/m3 0.242 0.860Propene 1 04/28/23 05:47 V32621ENM 15.3 µg/m3 0.124 2.13 Styrene 1 04/28/23 05:47 V32621ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 04/28/23 05:47 V32621ENM 2.56 J µg/m3 0.181 3.39Tetrachloroethene 1 04/28/23 05:47 V32621ENM <0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 04/28/23 05:47 V32621ENM 1820 µg/m3 1.80 37.7Toluene 20 04/27/23 13:31 V32621ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 04/28/23 05:47 V32621ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 04/28/23 05:47 V32621ENM <0.087 µg/m3 0.087 2.73 1,1,2-Trichloroethane 1 04/28/23 05:47 V32621ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 04/28/23 05:47 V32621ENM 3.10 µg/m3 0.130 2.81Trichlorofluoromethane 1 04/28/23 05:47 V32621ENM 118 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 04/28/23 05:47 V32621ENM 82.9 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 04/28/23 05:47 V32621ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 04/28/23 05:47 V32621ENM 0.784 J µg/m3 0.127 1.28Vinyl Chloride 1 04/28/23 05:47 V32621ENM 264 µg/m3 3.14 43.4o-Xylene 20 04/27/23 13:31 V32621ENM 1450 µg/m3 4.34 113m,p-Xylene 20 04/27/23 13:31 V32621ENM 1710 µg/m3 3.14 43.4Xylene (Total)20 04/27/23 13:31 V32621 Surrogate: 4-Bromofluorobenzene 109 Limits: 70-130%04/28/23 05:471 ENM V32621 Surrogate: 4-Bromofluorobenzene 125 Limits: 70-130%04/27/23 13:3120 ENM V32621 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 18 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-11 94129 Matrix: 4/17/2023 15:28 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 17.5 µg/m3 0.202 4.75Acetone 1 04/28/23 06:39 V32621ENM 6.24 µg/m3 0.073 1.60 Benzene 1 04/28/23 06:39 V32621ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 04/28/23 06:39 V32621ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 04/28/23 06:39 V32621ENM <0.153 µg/m3 0.153 5.17Bromoform 1 04/28/23 06:39 V32621ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 04/28/23 06:39 V32621ENM 1.25 µg/m3 0.328 1.111,3-Butadiene 1 04/28/23 06:39 V32621ENM 19.0 µg/m3 0.060 6.23Carbon Disulfide 1 04/28/23 06:39 V32621ENM <0.155 µg/m3 0.155 3.15 Carbon Tetrachloride 1 04/28/23 06:39 V32621ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 04/28/23 06:39 V32621ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 04/28/23 06:39 V32621ENM <0.164 µg/m3 0.164 1.32Chloroethane 1 04/28/23 06:39 V32621ENM <0.086 µg/m3 0.086 2.44Chloroform 1 04/28/23 06:39 V32621ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 04/28/23 06:39 V32621ENM 4.61 µg/m3 0.161 3.44Cyclohexane 1 04/28/23 06:39 V32621ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 04/28/23 06:39 V32621ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 04/28/23 06:39 V32621ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 04/28/23 06:39 V32621ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 04/28/23 06:39 V32621ENM 3.63 µg/m3 0.134 2.47Dichlorodifluoromethane 1 04/28/23 06:39 V32621ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 04/28/23 06:39 V32621ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 04/28/23 06:39 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 19 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-11 94129 Matrix: 4/17/2023 15:28 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 04/28/23 06:39 V32621ENM <0.095 µg/m3 0.095 1.98 cis-1,2-Dichloroethene 1 04/28/23 06:39 V32621ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 04/28/23 06:39 V32621ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 04/28/23 06:39 V32621ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 04/28/23 06:39 V32621ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 04/28/23 06:39 V32621ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 04/28/23 06:39 V32621ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 04/28/23 06:39 V32621ENM <0.136 µg/m3 0.136 1.80 Ethyl Acetate 1 04/28/23 06:39 V32621ENM 38.4 µg/m3 0.106 2.17Ethylbenzene 1 04/28/23 06:39 V32621ENM 13.2 µg/m3 0.128 2.464-Ethyltoluene 1 04/28/23 06:39 V32621ENM 0.574 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 04/28/23 06:39 V32621ENM 7.35 µg/m3 0.143 2.05Heptane 1 04/28/23 06:39 V32621ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 04/28/23 06:39 V32621ENM 32.2 µg/m3 0.047 1.76n-Hexane 1 04/28/23 06:39 V32621ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 04/28/23 06:39 V32621ENM 1.79 J µg/m3 0.139 4.92Isopropyl Alcohol 1 04/28/23 06:39 V32621ENM 1.58 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 04/28/23 06:39 V32621ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 04/28/23 06:39 V32621ENM 1.90 J µg/m3 0.121 2.054-Methyl-2-Pentanone 1 04/28/23 06:39 V32621ENM <0.488 µg/m3 0.488 1.74Methylene Chloride 1 04/28/23 06:39 V32621ENM 1.12 J µg/m3 0.183 2.62Naphthalene 1 04/28/23 06:39 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 20 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-11 94129 Matrix: 4/17/2023 15:28 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 36.2 µg/m3 0.242 0.860Propene 1 04/28/23 06:39 V32621ENM 4.23 µg/m3 0.124 2.13 Styrene 1 04/28/23 06:39 V32621ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 04/28/23 06:39 V32621ENM 15.7 µg/m3 0.181 3.39Tetrachloroethene 1 04/28/23 06:39 V32621ENM 0.451 J µg/m3 0.107 1.47Tetrahydrofuran 1 04/28/23 06:39 V32621ENM 118 µg/m3 0.090 1.88Toluene 1 04/28/23 06:39 V32621ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 04/28/23 06:39 V32621ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 04/28/23 06:39 V32621ENM <0.087 µg/m3 0.087 2.73 1,1,2-Trichloroethane 1 04/28/23 06:39 V32621ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 04/28/23 06:39 V32621ENM <0.130 µg/m3 0.130 2.81Trichlorofluoromethane 1 04/28/23 06:39 V32621ENM 21.7 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 04/28/23 06:39 V32621ENM 6.49 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 04/28/23 06:39 V32621ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 04/28/23 06:39 V32621ENM <0.127 µg/m3 0.127 1.28Vinyl Chloride 1 04/28/23 06:39 V32621ENM 38.8 µg/m3 0.157 2.17o-Xylene 1 04/28/23 06:39 V32621ENM 127 µg/m3 0.217 5.65m,p-Xylene 1 04/28/23 06:39 V32621ENM 166 µg/m3 0.157 2.17Xylene (Total)1 04/28/23 06:39 V32621 Surrogate: 4-Bromofluorobenzene 123 Limits: 70-130%04/28/23 06:391 ENM V32621 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 21 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-10 94130 Matrix: 4/17/2023 13:36 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 20.6 µg/m3 0.202 4.75Acetone 1 04/28/23 07:36 V32621ENM 146 µg/m3 0.073 1.60 Benzene 1 04/28/23 07:36 V32621ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 04/28/23 07:36 V32621ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 04/28/23 07:36 V32621ENM <0.153 µg/m3 0.153 5.17Bromoform 1 04/28/23 07:36 V32621ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 04/28/23 07:36 V32621ENM 45.7 µg/m3 0.328 1.111,3-Butadiene 1 04/28/23 07:36 V32621ENM 262 µg/m3 1.22 125Carbon Disulfide 20 04/27/23 14:45 V32621ENM <0.155 µg/m3 0.155 3.15 Carbon Tetrachloride 1 04/28/23 07:36 V32621ENM <0.107 µg/m3 0.107 2.30Chlorobenzene 1 04/28/23 07:36 V32621ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 04/28/23 07:36 V32621ENM 3.30 µg/m3 0.164 1.32Chloroethane 1 04/28/23 07:36 V32621ENM 5.52 µg/m3 0.086 2.44Chloroform 1 04/28/23 07:36 V32621ENM 4.44 µg/m3 0.067 1.03Chloromethane 1 04/28/23 07:36 V32621ENM 18.1 µg/m3 0.161 3.44Cyclohexane 1 04/28/23 07:36 V32621ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 04/28/23 07:36 V32621ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 04/28/23 07:36 V32621ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 04/28/23 07:36 V32621ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 04/28/23 07:36 V32621ENM 3.39 µg/m3 0.134 2.47Dichlorodifluoromethane 1 04/28/23 07:36 V32621ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 04/28/23 07:36 V32621ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 04/28/23 07:36 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 22 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-10 94130 Matrix: 4/17/2023 13:36 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 04/28/23 07:36 V32621ENM <0.095 µg/m3 0.095 1.98 cis-1,2-Dichloroethene 1 04/28/23 07:36 V32621ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 04/28/23 07:36 V32621ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 04/28/23 07:36 V32621ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 04/28/23 07:36 V32621ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 04/28/23 07:36 V32621ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 04/28/23 07:36 V32621ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 04/28/23 07:36 V32621ENM <0.136 µg/m3 0.136 1.80 Ethyl Acetate 1 04/28/23 07:36 V32621ENM 249 µg/m3 2.12 43.4Ethylbenzene 20 04/27/23 14:45 V32621ENM 59.3 µg/m3 0.128 2.464-Ethyltoluene 1 04/28/23 07:36 V32621ENM 10.2 µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 04/28/23 07:36 V32621ENM 109 µg/m3 0.143 2.05Heptane 1 04/28/23 07:36 V32621ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 04/28/23 07:36 V32621ENM 297 µg/m3 0.942 35.2n-Hexane 20 04/27/23 14:45 V32621ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 04/28/23 07:36 V32621ENM 0.916 J µg/m3 0.139 4.92Isopropyl Alcohol 1 04/28/23 07:36 V32621ENM 5.05 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 04/28/23 07:36 V32621ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 04/28/23 07:36 V32621ENM 9.32 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 04/28/23 07:36 V32621ENM <0.488 µg/m3 0.488 1.74Methylene Chloride 1 04/28/23 07:36 V32621ENM 1.44 J µg/m3 0.183 2.62Naphthalene 1 04/28/23 07:36 V32621ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 23 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-10 94130 Matrix: 4/17/2023 13:36 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32597 04/27/23 09:00 1250 µg/m3 4.84 17.2Propene 20 04/27/23 14:45 V32621ENM 31.0 µg/m3 0.124 2.13 Styrene 1 04/28/23 07:36 V32621ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 04/28/23 07:36 V32621ENM 5.11 µg/m3 0.181 3.39Tetrachloroethene 1 04/28/23 07:36 V32621ENM 5.39 µg/m3 0.107 1.47Tetrahydrofuran 1 04/28/23 07:36 V32621ENM 1820 µg/m3 1.80 37.7Toluene 20 04/27/23 14:45 V32621ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 04/28/23 07:36 V32621ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 04/28/23 07:36 V32621ENM <0.087 µg/m3 0.087 2.73 1,1,2-Trichloroethane 1 04/28/23 07:36 V32621ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 04/28/23 07:36 V32621ENM <0.130 µg/m3 0.130 2.81Trichlorofluoromethane 1 04/28/23 07:36 V32621ENM 94.4 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 04/28/23 07:36 V32621ENM 62.8 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 04/28/23 07:36 V32621ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 04/28/23 07:36 V32621ENM 4.58 µg/m3 0.127 1.28Vinyl Chloride 1 04/28/23 07:36 V32621ENM 164 µg/m3 3.14 43.4o-Xylene 20 04/27/23 14:45 V32621ENM 846 µg/m3 4.34 113m,p-Xylene 20 04/27/23 14:45 V32621ENM 1010 µg/m3 3.14 43.4Xylene (Total)20 04/27/23 14:45 V32621 Surrogate: 4-Bromofluorobenzene 128 Limits: 70-130%04/28/23 07:361 ENM V32621 Surrogate: 4-Bromofluorobenzene 93.9 Limits: 70-130%04/27/23 14:4520 ENM V32621 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 24 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-9 94131 Matrix: 4/17/2023 14:15 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32828 05/04/23 09:00 V32834 04/27/23 09:00 24.1 µg/m3 0.202 4.75Acetone 1 05/04/23 17:03 V32829ENM 148 µg/m3 0.073 1.60 Benzene 1 05/04/23 17:03 V32829ENM <0.147 µg/m3 0.147 10.4Benzyl Chloride 1 05/04/23 17:03 V32829ENM <0.150 µg/m3 0.150 3.35Bromodichloromethane 1 05/04/23 17:03 V32829ENM <0.153 µg/m3 0.153 5.17Bromoform 1 05/04/23 17:03 V32829ENM <0.115 µg/m3 0.115 1.94Bromomethane 1 05/04/23 17:03 V32829ENM 36.9 µg/m3 0.328 1.111,3-Butadiene 1 05/04/23 17:03 V32829ENM 110 µg/m3 0.060 6.23Carbon Disulfide 1 05/04/23 17:03 V32829ENM <0.155 µg/m3 0.155 3.15 Carbon Tetrachloride 1 05/04/23 17:03 V32829ENM 1.70 J µg/m3 0.107 2.30Chlorobenzene 1 05/04/23 17:03 V32829ENM <0.208 µg/m3 0.208 4.26Chlorodibromomethane 1 05/04/23 17:03 V32829ENM 2.97 µg/m3 0.164 1.32Chloroethane 1 05/04/23 17:03 V32829ENM <0.086 µg/m3 0.086 2.44Chloroform 1 05/04/23 17:03 V32829ENM <0.067 µg/m3 0.067 1.03Chloromethane 1 05/04/23 17:03 V32829ENM 15.7 µg/m3 0.161 3.44Cyclohexane 1 05/04/23 17:03 V32829ENM <0.151 µg/m3 0.151 3.841,2-Dibromoethane 1 05/04/23 17:03 V32829ENM <0.096 µg/m3 0.096 3.011,2-Dichlorobenzene 1 05/04/23 17:03 V32829ENM <0.174 µg/m3 0.174 12.01,3-Dichlorobenzene 1 05/04/23 17:03 V32829ENM <0.186 µg/m3 0.186 3.011,4-Dichlorobenzene 1 05/04/23 17:03 V32829ENM 2.61 µg/m3 0.134 2.47Dichlorodifluoromethane 1 05/04/23 17:03 V32829ENM <0.101 µg/m3 0.101 2.021,1-Dichloroethane 1 05/04/23 17:03 V32829ENM <0.129 µg/m3 0.129 2.021,2-Dichloroethane 1 05/04/23 17:03 V32829ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 25 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-9 94131 Matrix: 4/17/2023 14:15 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32828 05/04/23 09:00 V32834 04/27/23 09:00 <0.107 µg/m3 0.107 1.981,1-Dichloroethene 1 05/04/23 17:03 V32829ENM <0.095 µg/m3 0.095 1.98 cis-1,2-Dichloroethene 1 05/04/23 17:03 V32829ENM <0.108 µg/m3 0.108 1.98trans-1,2-Dichloroethene 1 05/04/23 17:03 V32829ENM <0.205 µg/m3 0.205 2.311,2-Dichloropropane 1 05/04/23 17:03 V32829ENM <0.622 µg/m3 0.622 3.501,2-Dichlorotetrafluoroethane 1 05/04/23 17:03 V32829ENM <0.178 µg/m3 0.178 2.27cis-1,3-Dichloropropene 1 05/04/23 17:03 V32829ENM <0.178 µg/m3 0.178 2.27trans-1,3-Dichloropropene 1 05/04/23 17:03 V32829ENM <0.435 µg/m3 0.435 1.801,4-Dioxane 1 05/04/23 17:03 V32829ENM <0.136 µg/m3 0.136 1.80 Ethyl Acetate 1 05/04/23 17:03 V32829ENM 388 µg/m3 2.12 43.4Ethylbenzene 20 04/27/23 15:22 V32835ENM 78.6 µg/m3 0.128 2.464-Ethyltoluene 1 05/04/23 17:03 V32829ENM 1.26 J µg/m3 0.561 3.831,1,2-Trichloro-1,2,2-trifluoroethane 1 05/04/23 17:03 V32829ENM 93.6 µg/m3 0.143 2.05Heptane 1 05/04/23 17:03 V32829ENM <0.330 µg/m3 0.330 5.33Hexachlorobutadiene 1 05/04/23 17:03 V32829ENM 330 µg/m3 0.942 35.2n-Hexane 20 04/27/23 15:22 V32835ENM <0.285 µg/m3 0.285 2.052-Hexanone 1 05/04/23 17:03 V32829ENM 3.21 JB µg/m3 0.139 4.92Isopropyl Alcohol 1 05/04/23 17:03 V32829ENM 6.04 µg/m3 0.224 1.47Methyl Ethyl Ketone (MEK)1 05/04/23 17:03 V32829ENM <0.033 µg/m3 0.033 1.80Methyl tert-butyl ether (MTBE)1 05/04/23 17:03 V32829ENM 16.3 µg/m3 0.121 2.054-Methyl-2-Pentanone 1 05/04/23 17:03 V32829ENM 3.41 µg/m3 0.488 1.74Methylene Chloride 1 05/04/23 17:03 V32829ENM 6.26 µg/m3 0.183 2.62Naphthalene 1 05/04/23 17:03 V32829ENM Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 26 of 41 , REPORT OF ANALYSISReport Number : Project Information : NC 28203 23-108-0008 01102 Hart & Hickman (Charlotte) 2923 South Tryon St. Ste 100 Haley Martin Charlotte Received : 04/18/2023 ABS.003 Report Date : 05/08/2023 Sample ID : Lab No : Sampled:SG-9 94131 Matrix: 4/17/2023 14:15 Air Analytical Method: Prep Method: Test Results Units MDL MQL By Analytical Batch Date / Time Analyzed DF TO-15 Prep TO-15 Prep Batch(es):V32828 05/04/23 09:00 V32834 04/27/23 09:00 273 µg/m3 4.84 17.2Propene 20 04/27/23 15:22 V32835ENM 40.2 µg/m3 0.124 2.13 Styrene 1 05/04/23 17:03 V32829ENM <0.104 µg/m3 0.104 3.431,1,2,2-Tetrachloroethane 1 05/04/23 17:03 V32829ENM 2.22 J µg/m3 0.181 3.39Tetrachloroethene 1 05/04/23 17:03 V32829ENM <0.107 µg/m3 0.107 1.47Tetrahydrofuran 1 05/04/23 17:03 V32829ENM 2700 µg/m3 1.80 37.7Toluene 20 04/27/23 15:22 V32835ENM <0.209 µg/m3 0.209 3.711,2,4-Trichlorobenzene 1 05/04/23 17:03 V32829ENM <0.144 µg/m3 0.144 2.731,1,1-Trichloroethane 1 05/04/23 17:03 V32829ENM <0.087 µg/m3 0.087 2.73 1,1,2-Trichloroethane 1 05/04/23 17:03 V32829ENM <0.199 µg/m3 0.199 2.15Trichloroethene 1 05/04/23 17:03 V32829ENM 2.53 J µg/m3 0.130 2.81Trichlorofluoromethane 1 05/04/23 17:03 V32829ENM 158 µg/m3 0.110 2.461,2,4-Trimethylbenzene 1 05/04/23 17:03 V32829ENM 86.2 µg/m3 0.236 2.461,3,5-Trimethylbenzene 1 05/04/23 17:03 V32829ENM <0.224 µg/m3 0.224 1.76Vinyl Acetate 1 05/04/23 17:03 V32829ENM 4.18 µg/m3 0.127 1.28Vinyl Chloride 1 05/04/23 17:03 V32829ENM 307 µg/m3 3.14 43.4o-Xylene 20 04/27/23 15:22 V32835ENM 1410 µg/m3 4.34 113m,p-Xylene 20 04/27/23 15:22 V32835ENM 1720 µg/m3 3.14 43.4Xylene (Total)20 04/27/23 15:22 V32835 Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%05/04/23 17:031 ENM V32829 Surrogate: 4-Bromofluorobenzene 95.8 Limits: 70-130%04/27/23 15:2220 ENM V32835 Qualifiers/ Definitions Dilution FactorDFAnalyte detected in blankB Method Quantitation LimitMQLEstimated valueJ Page 27 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32621QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32597 Associated Lab Samples: 94126, 94127, 94128, 94129, 94130 LRB-V32597 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 04/27/23 11:294.750.202<0.202µg/m3Acetone 04/27/23 11:291.600.073<0.073µg/m3Benzene 04/27/23 11:2910.40.147<0.147µg/m3Benzyl Chloride 04/27/23 11:293.350.150<0.150µg/m3Bromodichloromethane 04/27/23 11:295.170.153<0.153µg/m3Bromoform 04/27/23 11:291.940.115<0.115µg/m3Bromomethane 04/27/23 11:291.110.328<0.328µg/m31,3-Butadiene 04/27/23 11:296.230.060<0.060µg/m3Carbon Disulfide 04/27/23 11:293.150.155<0.155µg/m3Carbon Tetrachloride 04/27/23 11:292.300.107<0.107µg/m3Chlorobenzene 04/27/23 11:294.260.208<0.208µg/m3Chlorodibromomethane 04/27/23 11:291.320.164<0.164µg/m3Chloroethane 04/27/23 11:292.440.086<0.086µg/m3Chloroform 04/27/23 11:291.030.067<0.067µg/m3Chloromethane 04/27/23 11:293.440.161<0.161µg/m3Cyclohexane 04/27/23 11:293.840.151<0.151µg/m31,2-Dibromoethane 04/27/23 11:293.010.096<0.096µg/m31,2-Dichlorobenzene 04/27/23 11:2912.00.174<0.174µg/m31,3-Dichlorobenzene 04/27/23 11:293.010.186<0.186µg/m31,4-Dichlorobenzene 04/27/23 11:292.470.134<0.134µg/m3Dichlorodifluoromethane 04/27/23 11:292.020.101<0.101µg/m31,1-Dichloroethane 04/27/23 11:292.020.129<0.129µg/m31,2-Dichloroethane 04/27/23 11:291.980.107<0.107µg/m31,1-Dichloroethene 04/27/23 11:291.980.095<0.095µg/m3cis-1,2-Dichloroethene 04/27/23 11:291.980.108<0.108µg/m3trans-1,2-Dichloroethene 04/27/23 11:292.310.205<0.205µg/m31,2-Dichloropropane 04/27/23 11:293.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane Page 1 of 11Date:05/08/2023 09:21 AM Page 28 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32621QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32597 Associated Lab Samples: 94126, 94127, 94128, 94129, 94130 LRB-V32597 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 04/27/23 11:292.270.178<0.178µg/m3cis-1,3-Dichloropropene 04/27/23 11:292.270.178<0.178µg/m3trans-1,3-Dichloropropene 04/27/23 11:291.800.435<0.435µg/m31,4-Dioxane 04/27/23 11:291.800.136<0.136µg/m3Ethyl Acetate 04/27/23 11:292.170.106<0.106µg/m3Ethylbenzene 04/27/23 11:292.460.128<0.128µg/m34-Ethyltoluene 04/27/23 11:293.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 04/27/23 11:292.050.143<0.143µg/m3Heptane 04/27/23 11:295.330.330<0.330µg/m3Hexachlorobutadiene 04/27/23 11:291.760.047<0.047µg/m3n-Hexane 04/27/23 11:292.050.285<0.285µg/m32-Hexanone 04/27/23 11:294.920.139<0.139µg/m3Isopropyl Alcohol 04/27/23 11:291.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK) 04/27/23 11:291.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE) 04/27/23 11:292.050.121<0.121µg/m34-Methyl-2-Pentanone 04/27/23 11:291.740.488<0.488µg/m3Methylene Chloride 04/27/23 11:292.620.183<0.183µg/m3Naphthalene 04/27/23 11:290.8600.242<0.242µg/m3Propene 04/27/23 11:292.130.124<0.124µg/m3Styrene 04/27/23 11:293.430.104<0.104µg/m31,1,2,2-Tetrachloroethane 04/27/23 11:293.390.181<0.181µg/m3Tetrachloroethene 04/27/23 11:291.470.107<0.107µg/m3Tetrahydrofuran 04/27/23 11:291.880.090<0.090µg/m3Toluene 04/27/23 11:293.710.209<0.209µg/m31,2,4-Trichlorobenzene 04/27/23 11:292.730.144<0.144µg/m31,1,1-Trichloroethane 04/27/23 11:292.730.087<0.087µg/m31,1,2-Trichloroethane 04/27/23 11:292.150.199<0.199µg/m3Trichloroethene Page 2 of 11Date:05/08/2023 09:21 AM Page 29 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32621QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32597 Associated Lab Samples: 94126, 94127, 94128, 94129, 94130 LRB-V32597 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 04/27/23 11:292.810.130<0.130µg/m3Trichlorofluoromethane 04/27/23 11:292.460.110<0.110µg/m31,2,4-Trimethylbenzene 04/27/23 11:292.460.236<0.236µg/m31,3,5-Trimethylbenzene 04/27/23 11:291.760.224<0.224µg/m3Vinyl Acetate 04/27/23 11:291.280.127<0.127µg/m3Vinyl Chloride 04/27/23 11:292.170.157<0.157µg/m3o-Xylene 04/27/23 11:295.650.217<0.217µg/m3m,p-Xylene 04/27/23 11:294-Bromofluorobenzene (S)84.3 70-130 LCS-V32597Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 12915.311.9µg/m3Acetone 70-130 10316.516.0µg/m3Benzene 70-130 99.625.825.9µg/m3Benzyl Chloride 70-130 95.231.933.5µg/m3Bromodichloromethane 70-130 10353.551.7µg/m3Bromoform 70-130 12524.219.4µg/m3Bromomethane 70-130 11813.111.1µg/m31,3-Butadiene 70-130 11918.615.6µg/m3Carbon Disulfide 70-130 10131.831.5µg/m3Carbon Tetrachloride 70-130 10925.123.0µg/m3Chlorobenzene 70-130 10745.642.6µg/m3Chlorodibromomethane 70-130 12516.513.2µg/m3Chloroethane 70-130 10224.924.4µg/m3Chloroform 70-130 12813.210.3µg/m3Chloromethane 70-130 10117.317.2µg/m3Cyclohexane 70-130 Page 3 of 11Date:05/08/2023 09:21 AM Page 30 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32621QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32597 LCS-V32597Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 11042.438.4µg/m31,2-Dibromoethane 70-130 11334.030.1µg/m31,2-Dichlorobenzene 70-130 11233.830.1µg/m31,3-Dichlorobenzene 70-130 11434.430.1µg/m31,4-Dichlorobenzene 70-130 12731.324.7µg/m3Dichlorodifluoromethane 70-130 11523.220.2µg/m31,1-Dichloroethane 70-130 99.520.120.2µg/m31,2-Dichloroethane 70-130 12825.419.8µg/m31,1-Dichloroethene 70-130 11122.019.8µg/m3cis-1,2-Dichloroethene 70-130 11622.919.8µg/m3trans-1,2-Dichloroethene 70-130 96.122.223.1µg/m31,2-Dichloropropane 70-130 12543.835.0µg/m31,2-Dichlorotetrafluoroethane 70-130 12628.522.7µg/m3cis-1,3-Dichloropropene 70-130 12628.522.7µg/m3trans-1,3-Dichloropropene 70-130 94.417.018.0µg/m31,4-Dioxane 70-130 10619.118.0µg/m3Ethyl Acetate 70-130 10623.021.7µg/m3Ethylbenzene 70-130 10024.624.6µg/m34-Ethyltoluene 70-130 12748.838.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130 95.119.520.5µg/m3Heptane 70-130 10556.253.3µg/m3Hexachlorobutadiene 70-130 11119.617.6µg/m3n-Hexane 70-130 13026.620.5µg/m32-Hexanone 70-130 12815.812.3µg/m3Isopropyl Alcohol 70-130 10816.014.8µg/m3Methyl Ethyl Ketone (MEK)70-130 10919.618.0µg/m3Methyl tert-butyl ether (MTBE)70-130 11924.320.5µg/m34-Methyl-2-Pentanone 70-130 Page 4 of 11Date:05/08/2023 09:21 AM Page 31 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32621QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32597 LCS-V32597Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 12922.417.4µg/m3Methylene Chloride 70-130 11530.026.2µg/m3Naphthalene 70-130 12811.08.61µg/m3Propene 70-130 98.521.021.3µg/m3Styrene 70-130 10937.334.3µg/m31,1,2,2-Tetrachloroethane 70-130 95.232.333.9µg/m3Tetrachloroethene 70-130 10014.714.7µg/m3Tetrahydrofuran 70-130 12723.818.8µg/m3Toluene 70-130 11141.037.1µg/m31,2,4-Trichlorobenzene 70-130 97.826.727.3µg/m31,1,1-Trichloroethane 70-130 12634.327.3µg/m31,1,2-Trichloroethane 70-130 97.326.226.9µg/m3Trichloroethene 70-130 12234.328.1µg/m3Trichlorofluoromethane 70-130 10124.824.6µg/m31,2,4-Trimethylbenzene 70-130 11127.224.6µg/m31,3,5-Trimethylbenzene 70-130 11420.117.6µg/m3Vinyl Acetate 70-130 12015.312.8µg/m3Vinyl Chloride 70-130 10823.521.7µg/m3o-Xylene 70-130 97.242.243.4µg/m3m,p-Xylene 70-130 95.84-Bromofluorobenzene (S)70-130 Page 5 of 11Date:05/08/2023 09:21 AM Page 32 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32829QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32828 Associated Lab Samples: 94131 LRB-V32828 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/04/23 11:304.750.2020.992µg/m3Acetone 05/04/23 11:301.600.073<0.073µg/m3Benzene 05/04/23 11:3010.40.147<0.147µg/m3Benzyl Chloride 05/04/23 11:303.350.150<0.150µg/m3Bromodichloromethane 05/04/23 11:305.170.153<0.153µg/m3Bromoform 05/04/23 11:301.940.115<0.115µg/m3Bromomethane 05/04/23 11:301.110.328<0.328µg/m31,3-Butadiene 05/04/23 11:306.230.060<0.060µg/m3Carbon Disulfide 05/04/23 11:303.150.155<0.155µg/m3Carbon Tetrachloride 05/04/23 11:302.300.107<0.107µg/m3Chlorobenzene 05/04/23 11:304.260.208<0.208µg/m3Chlorodibromomethane 05/04/23 11:301.320.164<0.164µg/m3Chloroethane 05/04/23 11:302.440.086<0.086µg/m3Chloroform 05/04/23 11:301.030.067<0.067µg/m3Chloromethane 05/04/23 11:303.440.161<0.161µg/m3Cyclohexane 05/04/23 11:303.840.151<0.151µg/m31,2-Dibromoethane 05/04/23 11:303.010.096<0.096µg/m31,2-Dichlorobenzene 05/04/23 11:3012.00.174<0.174µg/m31,3-Dichlorobenzene 05/04/23 11:303.010.186<0.186µg/m31,4-Dichlorobenzene 05/04/23 11:302.470.134<0.134µg/m3Dichlorodifluoromethane 05/04/23 11:302.020.101<0.101µg/m31,1-Dichloroethane 05/04/23 11:302.020.129<0.129µg/m31,2-Dichloroethane 05/04/23 11:301.980.107<0.107µg/m31,1-Dichloroethene 05/04/23 11:301.980.095<0.095µg/m3cis-1,2-Dichloroethene 05/04/23 11:301.980.108<0.108µg/m3trans-1,2-Dichloroethene 05/04/23 11:302.310.205<0.205µg/m31,2-Dichloropropane 05/04/23 11:303.500.622<0.622µg/m31,2-Dichlorotetrafluoroethane Page 6 of 11Date:05/08/2023 09:21 AM Page 33 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32829QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32828 Associated Lab Samples: 94131 LRB-V32828 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/04/23 11:302.270.178<0.178µg/m3cis-1,3-Dichloropropene 05/04/23 11:302.270.178<0.178µg/m3trans-1,3-Dichloropropene 05/04/23 11:301.800.435<0.435µg/m31,4-Dioxane 05/04/23 11:301.800.136<0.136µg/m3Ethyl Acetate 05/04/23 11:302.460.128<0.128µg/m34-Ethyltoluene 05/04/23 11:303.830.561<0.561µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 05/04/23 11:302.050.143<0.143µg/m3Heptane 05/04/23 11:305.330.330<0.330µg/m3Hexachlorobutadiene 05/04/23 11:302.050.285<0.285µg/m32-Hexanone 05/04/23 11:304.920.1392.37µg/m3Isopropyl Alcohol 05/04/23 11:301.470.224<0.224µg/m3Methyl Ethyl Ketone (MEK) 05/04/23 11:301.800.033<0.033µg/m3Methyl tert-butyl ether (MTBE) 05/04/23 11:302.050.121<0.121µg/m34-Methyl-2-Pentanone 05/04/23 11:301.740.488<0.488µg/m3Methylene Chloride 05/04/23 11:302.620.183<0.183µg/m3Naphthalene 05/04/23 11:302.130.124<0.124µg/m3Styrene 05/04/23 11:303.430.104<0.104µg/m31,1,2,2-Tetrachloroethane 05/04/23 11:303.390.181<0.181µg/m3Tetrachloroethene 05/04/23 11:301.470.107<0.107µg/m3Tetrahydrofuran 05/04/23 11:303.710.209<0.209µg/m31,2,4-Trichlorobenzene 05/04/23 11:302.730.144<0.144µg/m31,1,1-Trichloroethane 05/04/23 11:302.730.087<0.087µg/m31,1,2-Trichloroethane 05/04/23 11:302.150.199<0.199µg/m3Trichloroethene 05/04/23 11:302.810.130<0.130µg/m3Trichlorofluoromethane 05/04/23 11:302.460.110<0.110µg/m31,2,4-Trimethylbenzene 05/04/23 11:302.460.236<0.236µg/m31,3,5-Trimethylbenzene 05/04/23 11:301.760.224<0.224µg/m3Vinyl Acetate Page 7 of 11Date:05/08/2023 09:21 AM Page 34 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32829QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32828 Associated Lab Samples: 94131 LRB-V32828 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 05/04/23 11:301.280.127<0.127µg/m3Vinyl Chloride 05/04/23 11:304-Bromofluorobenzene (S)91.0 70-130 LCS-V32828Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 89.010.611.9µg/m3Acetone 70-130 81.813.116.0µg/m3Benzene 70-130 90.723.525.9µg/m3Benzyl Chloride 70-130 79.726.733.5µg/m3Bromodichloromethane 70-130 84.943.951.7µg/m3Bromoform 70-130 83.516.219.4µg/m3Bromomethane 70-130 81.09.0011.1µg/m31,3-Butadiene 70-130 87.813.715.6µg/m3Carbon Disulfide 70-130 82.526.031.5µg/m3Carbon Tetrachloride 70-130 88.220.323.0µg/m3Chlorobenzene 70-130 87.037.142.6µg/m3Chlorodibromomethane 70-130 81.010.713.2µg/m3Chloroethane 70-130 82.720.224.4µg/m3Chloroform 70-130 86.38.8910.3µg/m3Chloromethane 70-130 77.313.317.2µg/m3Cyclohexane 70-130 86.433.238.4µg/m31,2-Dibromoethane 70-130 93.328.130.1µg/m31,2-Dichlorobenzene 70-130 89.326.930.1µg/m31,3-Dichlorobenzene 70-130 91.027.430.1µg/m31,4-Dichlorobenzene 70-130 85.821.224.7µg/m3Dichlorodifluoromethane 70-130 85.617.320.2µg/m31,1-Dichloroethane 70-130 Page 8 of 11Date:05/08/2023 09:21 AM Page 35 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32829QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32828 LCS-V32828Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 81.616.520.2µg/m31,2-Dichloroethane 70-130 85.316.919.8µg/m31,1-Dichloroethene 70-130 87.317.319.8µg/m3cis-1,2-Dichloroethene 70-130 87.317.319.8µg/m3trans-1,2-Dichloroethene 70-130 80.918.723.1µg/m31,2-Dichloropropane 70-130 86.030.135.0µg/m31,2-Dichlorotetrafluoroethane 70-130 83.218.922.7µg/m3cis-1,3-Dichloropropene 70-130 83.218.922.7µg/m3trans-1,3-Dichloropropene 70-130 80.514.518.0µg/m31,4-Dioxane 70-130 81.614.718.0µg/m3Ethyl Acetate 70-130 86.521.324.6µg/m34-Ethyltoluene 70-130 85.932.938.3µg/m31,1,2-Trichloro-1,2,2-trifluoroethane 70-130 82.917.020.5µg/m3Heptane 70-130 91.348.753.3µg/m3Hexachlorobutadiene 70-130 85.317.520.5µg/m32-Hexanone 70-130 93.411.512.3µg/m3Isopropyl Alcohol 70-130 83.712.414.8µg/m3Methyl Ethyl Ketone (MEK)70-130 84.415.218.0µg/m3Methyl tert-butyl ether (MTBE)70-130 82.416.920.5µg/m34-Methyl-2-Pentanone 70-130 82.714.417.4µg/m3Methylene Chloride 70-130 90.023.626.2µg/m3Naphthalene 70-130 89.219.021.3µg/m3Styrene 70-130 89.530.734.3µg/m31,1,2,2-Tetrachloroethane 70-130 84.628.733.9µg/m3Tetrachloroethene 70-130 82.912.214.7µg/m3Tetrahydrofuran 70-130 92.734.437.1µg/m31,2,4-Trichlorobenzene 70-130 81.622.327.3µg/m31,1,1-Trichloroethane 70-130 Page 9 of 11Date:05/08/2023 09:21 AM Page 36 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32829QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32828 LCS-V32828Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 87.123.827.3µg/m31,1,2-Trichloroethane 70-130 83.222.426.9µg/m3Trichloroethene 70-130 86.424.328.1µg/m3Trichlorofluoromethane 70-130 90.622.324.6µg/m31,2,4-Trimethylbenzene 70-130 89.822.124.6µg/m31,3,5-Trimethylbenzene 70-130 88.015.517.6µg/m3Vinyl Acetate 70-130 85.110.912.8µg/m3Vinyl Chloride 70-130 1024-Bromofluorobenzene (S)70-130 Page 10 of 11Date:05/08/2023 09:21 AM Page 37 of 41 Quality Control Data 23-108-0008Report No: Project Description: Client ID:Hart & Hickman (Charlotte) ABS.003 QC Prep Batch Method: Volatile Organic Compounds in Air- GC/MS TO-15 V32835QC Analytical Batch(es): Analysis Method: Analysis Description: TO-15 Prep QC Prep:V32834 Associated Lab Samples: 94131 LRB-V32834 Matrix: AIRLab Reagent Blank Parameter AnalyzedMQLMDLBlank ResultUnits % Recovery % Rec Limits 04/27/23 11:292.170.106<0.106µg/m3Ethylbenzene 04/27/23 11:291.760.047<0.047µg/m3n-Hexane 04/27/23 11:290.8600.242<0.242µg/m3Propene 04/27/23 11:291.880.090<0.090µg/m3Toluene 04/27/23 11:292.170.157<0.157µg/m3o-Xylene 04/27/23 11:295.650.217<0.217µg/m3m,p-Xylene 04/27/23 11:294-Bromofluorobenzene (S)84.3 70-130 LCS-V32834Laboratory Control Sample Parameter LCS %RecLCS Result Spike Conc.Units % Rec Limits 10623.021.7µg/m3Ethylbenzene 70-130 11119.617.6µg/m3n-Hexane 70-130 12811.08.61µg/m3Propene 70-130 12723.818.8µg/m3Toluene 70-130 10823.521.7µg/m3o-Xylene 70-130 97.242.243.4µg/m3m,p-Xylene 70-130 95.84-Bromofluorobenzene (S)70-130 Page 11 of 11Date:05/08/2023 09:21 AM Page 38 of 41 Fed Ex UPS US Postal Client Lab Courier Other : Shipment Receipt Form Customer Number: Customer Name: Report Number:23-108-0008 Hart & Hickman (Charlotte) 01102 Shipping Method Shipping container/cooler uncompromised? Thermometer ID:N/A Chain of Custody (COC) present?Yes No Yes No Not Present Yes No Not Present Yes No COC agrees with sample label(s)?Yes No COC properly completed Samples in proper containers? Sample containers intact? Sufficient sample volume for indicated test(s)? All samples received within holding time? Cooler temperature in compliance? Yes No Yes No Yes No Yes No Yes No Yes NoCooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes No Yes No N/A Yes No N/A Yes No N/ASoil VOA method 5035 – compliance criteria met Water - Sample containers properly preserved Water - VOA vials free of headspace Yes No N/A Trip Blanks received with VOAs Low concentration EnCore samplers (48 hr) High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d) High concentration container (48 hr) Custody seals intact on shipping container/cooler? Custody seals intact on sample bottles? Number of coolers/boxes received Yes No 1 Signature:Angelo Norvell Date & Time:04/18/2023 12:46:51 Special precautions or instructions included? Comments: Page 39 of 41 Page 40 of 41 Page 41 of 41 Appendix D DEQ Risk Calculator (January 2023) Version Date: Basis: Site Name: Site Address: DEQ Section: Site ID: Exposure Unit ID: Submittal Date: Reviewed By: Hypothetical Worst Case - Soil Gas North Carolina Department of Environmental Quality Risk Calculator Commercial Equipment Company N. Graham Street and W. 28th Street Brownfields Redevelopment Section 26002-22-060 January 2023 November 2022 EPA RSL Table Prepared By:Hart & Hickman, PC 2923 S. Tryon Street, Ste 100, Charlotte, NC North Carolina DEQ Risk Calculator Complete Exposure Pathways Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 26002-22-060 Exposure Unit ID: Hypothetical Worst Case - Soil Gas Note: Risk output will only be calculated for complete exposure pathways. Receptor Pathway Check box if pathway complete Soil Groundwater Use Soil Groundwater Use Construction Worker Soil Soil Surface Water Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Groundwater to Indoor Air Soil Gas to Indoor Air Indoor Air Source Soil Source Groundwater Source Soil Source Groundwater Resident Non-Residential Worker CONTAMINANT MIGRATION PATHWAYS Groundwater Surface Water Input Form 1A VAPOR INTRUSION PATHWAYS DIRECT CONTACT SOIL AND WATER PATHWAYS Resident Non-Residential Worker Recreator/Trespasser North Carolina DEQ Risk Calculator Exposure Point ConcentrationsVersion Date: January 2023Basis: November 2022 EPA RSL TableSite ID: 26002-22-060Exposure Unit ID: Hypothetical Worst Case - Soil GasDescription of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion101 67-64-1 Acetoneug/m314871-43-2Benzeneug/m34.83100-44-7Benzyl Chlorideug/m30.5775-27-4Bromodichloromethaneug/m345.7106-99-0Butadiene, 1,3-ug/m326275-15-0Carbon Disulfideug/m31.256-23-5Carbon Tetrachlorideug/m32.86108-90-7Chlorobenzeneug/m311.167-66-3Chloroformug/m34.4474-87-3Chloromethaneug/m366.8110-83-8Cyclohexeneug/m34.3175-71-8Dichlorodifluoromethaneug/m31.278-87-5Dichloropropane, 1,2-ug/m33.375-00-3Ethyl Chloride (Chloroethane)ug/m3388100-41-4Ethylbenzeneug/m3191109-99-9~Tetrahydrofuranug/m3109142-82-5Heptane, N-ug/m3330110-54-3Hexane, N-ug/m38.27591-78-6Hexanone, 2-ug/m36.8767-63-0Isopropanolug/m39.1178-93-3Methyl Ethyl Ketone (2-Butanone)ug/m316.3108-10-1Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m33.4175-09-2Methylene Chlorideug/m310.291-20-3~Naphthaleneug/m31250115-07-1Propyleneug/m340.2100-42-5Styreneug/m31.7879-34-5Tetrachloroethane, 1,1,2,2-ug/m359.1127-18-4Tetrachloroethyleneug/m32700108-88-3Tolueneug/m333.176-13-1Trichloro-1,2,2-trifluoroethane, 1,1,2-ug/m31.7779-01-6Trichloroethyleneug/m3187075-69-4Trichlorofluoromethaneug/m315895-63-6Trimethylbenzene, 1,2,4-ug/m386.2108-67-8Trimethylbenzene, 1,3,5-ug/m34.5875-01-4Vinyl Chlorideug/m317201330-20-7Xylenesug/m3Input Form 2DSoil Gas Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator Risk for Individual Pathways Output Form 1A Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 26002-22-060 Exposure Unit ID: Hypothetical Worst Case - Soil Gas Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Soil NC NC NC Groundwater Use*NC NC NC Soil NC NC NC Groundwater Use*NC NC NC Construction Worker Soil NC NC NC Soil NC NC NC Surface Water*NC NC NC Receptor Pathway Carcinogenic Risk Hazard Index Risk exceeded? Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air 4.9E-05 1.8E+00 YES Indoor Air NC NC NC Groundwater to Indoor Air NC NC NC Soil Gas to Indoor Air NC NC NC Indoor Air NC NC NC Pathway Source Source Soil NC Source Groundwater NC Source Soil NC Source Groundwater NC Groundwater Exceedence of 2L at Receptor? Exceedence of 2L at Receptor? 1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations. Notes: 3. NM = Not modeled, user did not check this pathway as complete. 4. NC = Pathway not calculated, required contaminant migration parameters were not entered. DIRECT CONTACT SOIL AND WATER CALCULATORS Resident Non-Residential Worker Recreator/Trespasser 2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure. Surface Water Exceedence of 2B at Receptor? Exceedence of 2B at Receptor? VAPOR INTRUSION CALCULATORS Resident Non-Residential Worker CONTAMINANT MIGRATION CALCULATORS Target Receptor Concentrations Exceeded? North Carolina DEQ Risk Calculator DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air Version Date: January 2023 Basis: November 2022 EPA RSL Table Site ID: 26002-22-060 Exposure Unit ID: Hypothetical Worst Case - Soil Gas CAS # Chemical Name: Soil Gas Concentration (ug/m3) Calculated Indoor Air Concentration (ug/m3) Target Indoor Air Conc. for Carcinogens @ TCR = 1E-06 Target Indoor Air Conc. for Non- Carcinogens @ THQ = 0.2 Calculated Carcinogenic Risk Calculated Non- Carcinogenic Hazard Quotient 67-64-1 Acetone 101 3.03 -- 71-43-2 Benzene 148 4.44 3.6E-01 6.3E+00 1.2E-05 1.4E-01 100-44-7 Benzyl Chloride 4.83 0.1449 5.7E-02 2.1E-01 2.5E-06 1.4E-01 75-27-4 Bromodichloromethane 0.57 0.0171 7.6E-02 - 2.3E-07 106-99-0 Butadiene, 1,3-45.7 1.371 9.4E-02 4.2E-01 1.5E-05 6.6E-01 75-15-0 Carbon Disulfide 262 7.86 -1.5E+02 1.1E-02 56-23-5 Carbon Tetrachloride 1.2 0.036 4.7E-01 2.1E+01 7.7E-08 3.5E-04 108-90-7 Chlorobenzene 2.86 0.0858 -1.0E+01 1.6E-03 67-66-3 Chloroform 11.1 0.333 1.2E-01 2.0E+01 2.7E-06 3.3E-03 74-87-3 Chloromethane 4.44 0.1332 -1.9E+01 1.4E-03 110-83-8 Cyclohexene 66.8 2.004 -2.1E+02 1.9E-03 75-71-8 Dichlorodifluoromethane 4.31 0.1293 -2.1E+01 1.2E-03 78-87-5 Dichloropropane, 1,2-1.2 0.036 7.6E-01 8.3E-01 4.7E-08 8.6E-03 75-00-3 Ethyl Chloride (Chloroethane)3.3 0.099 -8.3E+02 2.4E-05 100-41-4 Ethylbenzene 388 11.64 1.1E+00 2.1E+02 1.0E-05 1.1E-02 109-99-9 ~Tetrahydrofuran 191 5.73 -4.2E+02 2.7E-03 142-82-5 Heptane, N-109 3.27 -8.3E+01 7.8E-03 110-54-3 Hexane, N-330 9.9 -1.5E+02 1.4E-02 591-78-6 Hexanone, 2-8.27 0.2481 -6.3E+00 7.9E-03 67-63-0 Isopropanol 6.87 0.2061 -4.2E+01 9.9E-04 78-93-3 Methyl Ethyl Ketone (2-Butanone)9.11 0.2733 -1.0E+03 5.2E-05 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 16.3 0.489 -6.3E+02 1.6E-04 75-09-2 Methylene Chloride 3.41 0.1023 1.0E+02 1.3E+02 1.0E-09 1.6E-04 91-20-3 ~Naphthalene 10.2 0.306 8.3E-02 6.3E-01 3.7E-06 9.8E-02 115-07-1 Propylene 1250 37.5 -6.3E+02 1.2E-02 100-42-5 Styrene 40.2 1.206 -2.1E+02 1.2E-03 79-34-5 Tetrachloroethane, 1,1,2,2-1.78 0.0534 4.8E-02 -1.1E-06 127-18-4 Tetrachloroethylene 59.1 1.773 1.1E+01 8.3E+00 1.6E-07 4.3E-02 108-88-3 Toluene 2700 81 -1.0E+03 1.6E-02 76-13-1 Trichloro-1,2,2-trifluoroethane, 1,1,2- 33.1 0.993 -1.0E+03 1.9E-04 79-01-6 Trichloroethylene 1.77 0.0531 4.8E-01 4.2E-01 1.1E-07 2.5E-02 75-69-4 Trichlorofluoromethane 1870 56.1 -- 95-63-6 Trimethylbenzene, 1,2,4-158 4.74 -1.3E+01 7.6E-02 108-67-8 Trimethylbenzene, 1,3,5-86.2 2.586 -1.3E+01 4.1E-02 75-01-4 Vinyl Chloride 4.58 0.1374 1.7E-01 1.7E+01 8.2E-07 1.6E-03 1330-20-7 Xylenes 1720 51.6 -2.1E+01 4.9E-01 Cumulative: 4.9E-05 1.8E+00 All concentrations are in ug/m3 Output Form 3B Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals. North Carolina DEQ Risk Calculator Appendix E Vapor Sampling Forms &Žƌŵ^sͲϭ6XE6ODE6RLO*DV9DSRU,QVWDOODWLRQ)LHOG)RUP3URMHFW1RBBBBBBBBBBBBBBBBBB6DPSOHUBBBBBBBBBBBBBBBBBBBBBB:HDWKHUBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBSurface MaterialSlab Thickness (if appl.) Material Below Slab (if appl.)Depth of Screen (if appl.)Type Date & TimeAmbient Temp.Purge MethodVolume PurgedShroud Helium Conc.Purge Helium Conc.Leak Test Pass? (see note)SS, SGPerm., Temp.Concrete, soil, gravel, asphaltInchesGravel, sand, clay, etc.ft bgsFull sample train or point-onlymm/dd/yy 24-hroFSyringe, pumpLiters (see notes for calc.)%% or ppm(indicate units below)Yes / No^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗^͗͗Z͗S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporary; Volume Purged = x3 purge volumes = 3*L*aLast updated: 8/16/2022" Hg = inches of mercury; ppm = parts per million1RWHV________________________________________________________________________________________________________________________________________________________________________________________________________________6DPSOH,'Type9DSRU0RQLWRULQJ3RLQW&RQVWUXFWLRQ +HOLXP/HDN7HVWEŽƚĞ͗>ĞĂŬdĞƐƚZĞƋƵŝƌĞŵĞŶƚƐWĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ůĞĂŬƚĞƐƚƉĂƐƐĞƐŝĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƉƵƌŐĞĂŝƌŝƐůĞƐƐƚŚĂŶϭϬйŽĨŚĞůŝƵŵĐŽŶĐĞŶƚƌĂƚŝŽŶŝŶƐŚƌŽƵĚ͘L = length of tubing/pipe (ft)a = 0.163 for 2" diameter (L/ft)a = 0.010 for 0.25" diameter (L/ft)^͗ͰDĂƐƚĞƌdĞŵƉůĂƚĞƐͰ&ŽƌŵƐͲϮϬϮϮ&ŽƌŵƐͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϯ͘ƉĚĨ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ/ŶƐƚĂůůĂƚŝŽŶ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WABS.003CMBLow 51F, high 71F, sunnySG-125769SG Temp. Gravel NA Clay/Silt 7Full120563 Syringe 0.6 L 5.1 0.0 Yes16221SG-106010SG Temp. Asphalt NA Clay/Silt 7Full133564 Syringe 0.6 L 5.6 0.0 Yes6557SG-95977SG Temp. Asphalt NA Clay/Silt 7Full140467 Syringe 0.6 L 6.8 0.0 Yes16241SG-115935SG Temp. Asphalt NA Clay/Silt 7Full152067 Syringe 0.6 L 6.3 0.0Yes6553SSV-3/DUP6003/5552SS Temp. Conc. 6" Clay/Silt NAFull144065 Syringe 0.3 L 5.4 0.0 Yes13114 &Žƌŵ^sͲϮ6XE6ODE6RLO*DV9DSRU6DPSOLQJ)LHOG)RUP3URMHFW1RBBBBBBBBBBBBBBBBBBB 6DPSOHUBBBBBBBBBBBBBBBBBBBBBB :HDWKHUBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBDate Proposed Sampling Duration Time Canister PressureOutdoor TemperatureOutdoor HumidityIndoor TemperatureIndoor Humiditymm/dd/yy Minutes24-hr" HgoF%oF%^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End ^͗Beginning͗Middle Z͗End S = sample ID; C = canister ID; R = regulator ID; SS = sub-slab; SG = soil gas; Perm = permanent; Temp = temporaryLast updated: 8/16/2022" Hg = inches of mercury1RWHV_____________________________________________________________________________________________________________________________________________________________________________________________________________________________________________________^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗6DPSOH,'^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗6DPSOLQJ,QIRUPDWLRQ ,QGRRU3DUDPHWHUV2XWGRRU3DUDPHWHUVSampling PeriodEŽƚĞ͗WĞƌEYtDsĂƉŽƌ/ŶƚƌƵƐŝŽŶ'ƵŝĚĂŶĐĞ͕ƐŚƵƚͲŝŶƚĞƐƚĂŶĚŚĞůŝƵŵůĞĂŬĐŚĞĐŬŵƵƐƚďĞƉĂƐƐĞĚďĞĨŽƌĞƐĂŵƉůŝŶŐ͘^͗ͰDĂƐƚĞƌdĞŵƉůĂƚĞƐͰ&ŽƌŵƐͲϮϬϮϮ&ŽƌŵƐͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϯ͘ƉĚĨ^ƵďͲ^ůĂďͬ^Žŝů'ĂƐ^ĂŵƉůŝŶŐsĂƉŽƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WABS.003CMBLow 51F, high 71F, sunnySG-121.4 L57694/17/2310100mL/min1217 -1863 35 NA162211222 -51212 -28NASG-101.4 L1336 -2860104/17/23101341 -1964 31 NA NA100mL/min65571350 -5SG-91415 -281.4 L59774/17/23 1065 32 NA NA16241100mL/min1420 -171427 -5SG-111528 -281.4 L59354/17/23101533 -1867 28 NA NA6553100mL/min1540 -5SSV-3/SSV-DUP1446 -281.4 L6003/55524/17/23101451 -2265 29 65 29100mL/min131141503 -5 Appendix F Landtec GEM 5000® Portable Gas Analyzer Specifications and Raw Data Set Appendix FLandtec GEM 5000® Portable Gas Analyzer Specifications and Raw Data SetCommercial Equipment Company Charlotte, North CarolinaH&H Job No. ABS-003Device IDDate/Time CH4 CO2 O2 Balance %LEL Init. Static Press. Adj. Static Press. Init. Diff. Press. Adj. Diff. Press. Init. Gas Temp. Adj. Gas Temp. Init. Flow Adj. Flow Init. Power Adj. Power Baro. Press. Sys. Press. CO H2S H2 FLD‐Tech DL‐Tech Serial Number Rel. Press.GEM™5000; G5 V1_15_12; LSGAM:6_0_20160627; {92158346888}% % % % % inches H2O inches H2O inches H2O inches H2O DegFDegFSCFM SCFM e3BTU/h e3BTU/h inches Hg inches H2O ppm ppm LMHinches H2O0000SG‐54/17/2023 11:18 0.1 0 20.7 79.2 200.03‐0.116‐0.0976262 0 0 0 0 29.05‐0.01 0 0 10 CMB CMB G504637 N/A0000SG‐54/17/2023 11:22 0.2 0.2 18.4 81.2 4 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.05 N/A0 0 9 CMB CMB G5046370DUP100004/17/2023 9:38 0 0.1 21.6 78.3 000.01‐0.005‐0.0055858 0 0 0 0 29.020 0 0 0 CMB CMB G504637 N/ADUP100004/17/2023 9:40 0.5 0.1 13.1 86.3 10 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.02 N/A45 0 0 CMB CMB G504637‐0.01MP‐A00004/17/2023 11:320.1021.2 78.7 2‐18.01‐17.93 >>>>>>>>6262 0 0 0 0 29.060 0 0 9 CMB CMB G504637 N/AMP‐A00004/17/2023 13:04 0.1 0.1 21.3 78.5 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.99 N/A0 0 0 CMB CMB G5046370.01MP‐B00004/17/2023 9:28 0 0.1 21.6 78.3 000.01‐0.005‐0.0055858 0 0 0 0 29.010 0 0 0 CMB CMB G504637 N/AMP‐B00004/17/2023 9:30 0.5 0.1 13.1 86.3 10 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.01 N/A49 0 0 CMB CMB G504637‐0.01MP‐C00004/17/2023 11:06 0 0.1 21 78.9 00.360.37‐0.35‐0.3566161 0 0 0 0 29.05‐0.01 0 0 2 CMB CMB G504637 N/AMP‐C00004/17/2023 12:52 0.1 0.1 21.5 78.3 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.98 N/A0 0 0 CMB CMB G5046370.02MP‐D00004/17/2023 11:25 0 0.1 22 77.9 00.180.15‐0.176‐0.1525858 0 0 0 0 29.010 0 0 0 CMB CMB G504637 N/AMP‐D00004/17/2023 11:28 0.2 0.3 16.3 83.2 4 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.06 N/A1 0 12 CMB CMB G5046370.01MP‐E00004/17/2023 9:59 0 0 20.7 79.3 0‐0.04‐0.02‐0.005‐0.0045858 0 0 0 0 29.04 0.01 0 0 6 CMB CMB G504637 N/AMP‐E00004/17/2023 10:01 0 0.3 19.2 80.5 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.04 N/A1 0 6 CMB CMB G504637‐0.01MP‐F00004/17/2023 13:07 0 0.1 21.4 78.5 0‐0.010.04‐0.272‐0.1726060 0 0 0 0 29.03‐0.01 0 0 0 CMB CMB G504637 N/AMP‐F00004/17/2023 13:10 0.1 0.1 21.2 78.6 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29 N/A0 0 0 CMB CMB G504637‐0.13MP‐G00004/17/2023 10:440 0.1 19.4 80.5 0‐0.05‐0.020.0210.0126060 0 0 0 0 29.030 0 0 0 CMB CMB G504637 N/AMP‐G00004/17/2023 10:45 0 0 1.3 98.7 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.03 N/A0 0 0 CMB CMB G5046370.01MP‐H00004/17/2023 10:59 0 0 21.5 78.5 0‐0.2‐0.120.0270.0076060 0 0 0 0 29.03 0.05 0 0 0 CMB CMB G504637 N/AMP‐H00004/17/2023 11:01 0 0.9 2.4 96.7 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.03 N/A0 0 7 CMB CMB G504637‐0.01 Appendix FLandtec GEM 5000® Portable Gas Analyzer Specifications and Raw Data SetCommercial Equipment Company Charlotte, North CarolinaH&H Job No. ABS-003Device IDDate/Time CH4 CO2 O2 Balance %LEL Init. Static Press. Adj. Static Press. Init. Diff. Press. Adj. Diff. Press. Init. Gas Temp. Adj. Gas Temp. Init. Flow Adj. Flow Init. Power Adj. Power Baro. Press. Sys. Press. CO H2S H2 FLD‐Tech DL‐Tech Serial Number Rel. Press.GEM™5000; G5 V1_15_12; LSGAM:6_0_20160627; {112327583518}% % % % % inches H2O inches H2O inches H2O inches H2O DegFDegFSCFM SCFM e3BTU/h e3BTU/h inches Hg inches H2O ppm ppm LMHinches H2O0000SG‐54/18/2023 14:33 0.4 0 19.7 79.9 8‐33.44‐34.66 >>>>>>>>7676 0 0 0 0 29.23 N/A0 0 70 CMB CMB G504637 N/A0000SG‐54/18/2023 14:35 0.5 0.1 19.4 80 10 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.23 N/A1 0 65 CMB CMB G5046370DUP100004/18/2023 13:54 0.2 0 20 79.8 4‐8.22‐8.118.1658.1277474 0 0 0 0 29.220 0 0 73 CMB CMB G504637 N/ADUP100004/18/2023 13:56 0.3 0 20 79.7 6 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.22 N/A0 0 68 CMB CMB G5046370.01MP‐A00004/18/2023 15:16 0.5 0 20.5 79 10‐16.97‐17.61>>>>>>>>77.777.700 0 0 29.2 0.01 0 0 74 CMB CMB G504637 N/AMP‐A00004/18/2023 15:19 0.6 0 20.9 78.5 12 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.2 N/A1 0 78 CMB CMB G5046370MP‐B00004/18/2023 13:41 0.2 0 19.3 80.5 40‐0.03‐0.0470.0447373 0 0 0 0 29.20 0 0 55 CMB CMB G504637 N/AMP‐B00004/18/2023 13:42 0.2 0 19.1 80.7 4 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.2 N/A0 0 69 CMB CMB G5046370MP‐C00004/18/2023 14:58 0.5 0 21.4 78.1 10‐0.44‐1.010.5521.1737676 0 0 0 0 29.2 N/A0 0 65 CMB CMB G504637 N/AMP‐C00004/18/2023 15:01 0.5 0.2 21.1 78.2 10 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.2 N/A1 0 79 CMB CMB G5046370.02MP‐D00004/18/2023 14:40 0.5 0 20.8 78.7 10‐4.33‐2.494.3462.4747676 0 0 0 0 29.23 N/A0 0 70 CMB CMB G504637 N/AMP‐D00004/18/2023 14:43 0.6 0.1 12.2 87.1 12 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.23 N/A4 0 65 CMB CMB G5046370.03MP‐E00004/18/2023 13:51 0.2 0 19.7 80.1 40.010.01‐0.0010.0137474 0 0 0 0 29.210 0 0 73 CMB CMB G504637 N/AMP‐E00004/18/2023 13:52 0.2 0.2 17.1 82.5 4 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.21 N/A9 0 71 CMB CMB G5046370.01MP‐F00004/18/2023 14:06 0.3 0 20.6 79.1 6‐10.9‐8.64 >>>>8.7027575 0 0 0 0 29.23 0.02 0 0 65 CMB CMB G504637 N/AMP‐F00004/18/2023 14:08 0.3 0.3 19.4 80 6 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.23 N/A1 0 63 CMB CMB G5046370.01MP‐G00004/18/2023 14:15 0.6 0 21.4 78 120.420.19‐0.203‐0.0227575 0 0 0 0 29.230 0 0 62 CMB CMB G504637 N/AMP‐G00004/18/2023 14:18 0.6 0 1.2 98.2 12 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.23 N/A0 0 66 CMB CMB G5046370.01MP‐H00004/18/2023 14:24 0.5 0 20 79.5 10‐0.040.03‐0.033‐0.017575 0 0 0 0 29.23 0.01 0 0 62 CMB CMB G504637 N/AMP‐H00004/18/2023 14:260.4 1.5 1.6 96.5 8 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A29.23 N/A0 0 64 CMB CMB G5046370 Appendix FLandtec GEM 5000® Portable Gas Analyzer Specifications and Raw Data SetCommercial Equipment Company Charlotte, North CarolinaH&H Job No. ABS-003Device IDDate/Time CH4 CO2 O2 Balance %LEL Init. Static Press. Adj. Static Press. Init. Diff. Press. Adj. Diff. Press. Init. Gas Temp. Adj. Gas Temp. Init. Flow Adj. Flow Init. Power Adj. Power Baro. Press. Sys. Press. CO H2SGEM™5000; G5 V1_15_12; LSGAM:6_0_20160627; {67549614609}% % % % % inches H2O inches H2O inches H2O inches H2O DegFDegFSCFM SCFM e3BTU/h e3BTU/h inches Hg inches H2O ppm ppmMP‐A00005/1/2023 9:55 0.1 0.1 21.6 78.2 2‐0.15‐0.250.1380.3065555 0 0 0 0 28.77 0.02 0 0MP‐A00005/1/2023 9:57 0.1 0.4 20 79.5 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.77 N/A0 0MP‐B00005/1/2023 10:06 0.1 0.1 21.6 78.2 2‐0.030.02‐0.074‐0.0535555 0 0 0 0 28.780 0 0MP‐B00005/1/2023 10:15 0.1 0.1 20.5 79.3 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.8 N/A0 0DUP100005/1/2023 10:38 0 0.1 21.2 78.7 0‐0.09‐0.630.3330.6555656 0 0 0 0 28.780 0 0DUP100005/1/2023 10:40 0.1 0.1 20.5 79.3 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.78 N/A0 0MP‐C00005/1/2023 10:260.1 0.1 21.3 78.5 2‐0.06‐0.090.0330.0615555 0 0 0 0 28.80 0 0MP‐C00005/1/2023 10:29 0 1.2 19.3 79.5 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.8 N/A0 0MP‐D00005/1/2023 10:48 0 0.1 20.7 79.2 00.10.13‐0.089‐0.0995757 0 0 0 0 28.80 0 0MP‐D00005/1/2023 10:54 0 0.9 17.9 81.2 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.8 N/A0 00000SG‐55/1/2023 11:02 0 0.1 19.7 80.2 00.030.02‐0.022‐0.0145757 0 0 0 0 28.840 0 00000SG‐55/1/2023 11:07 0 0.1 17.6 82.3 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.83 N/A0 0MP‐E00005/1/2023 11:23 0 0.1 20.7 79.2 0‐15.29‐15.3 >>>>>>>>5858 0 0 0 0 28.820 0 0MP‐E00005/1/2023 11:26 0 0.9 19.5 79.6 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.82 N/A0 0MP‐F00005/1/2023 11:43 0 0 20.2 79.8 00.140.25‐0.067‐0.0955959 0 0 <<>>0 28.850 0 0MP‐F00005/1/2023 11:45 0 2.1 15.8 82.1 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.85 N/A0 0MP‐G00005/1/2023 11:53 0 0 20.6 79.4 0‐0.09‐0.080.0340.0525959 0 0 0 0 28.850 0 0MP‐G00005/1/2023 11:56 0 0.1 14.5 85.4 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.83 N/A0 0MP‐H00005/1/2023 12:07 0 0 20.4 79.6 00.0200.0040.0045959 0 0 0 0 28.850 0 0MP‐H00005/1/2023 12:09 0 7.5 3.4 89.1 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.85 N/A0 0 Appendix FLandtec GEM 5000® Portable Gas Analyzer Specifications and Raw Data SetCommercial Equipment Company Charlotte, North CarolinaH&H Job No. ABS-003Device IDDate/Time CH4 CO2 O2 Balance %LEL Init. Static Press. Adj. Static Press. Init. Diff. Press. Adj. Diff. Press. Init. Gas Temp. Adj. Gas Temp. Init. Flow Adj. Flow Init. Power Adj. Power Baro. Press. Sys. Press. CO H2SGEM™5000; G5 V1_15_12; LSGAM:6_0_20160627; {151510745133}% % % % % inches H2O inches H2O inches H2O inches H2O DegFDegFSCFM SCFM e3BTU/h e3BTU/h inches Hg inches H2OMP‐A00005/2/2023 13:00 0 0.1 20.9 79 0‐0.74‐1.260.8261.2466565 0 0 0 0 28.770 0 0MP‐A00005/2/2023 13:02 0.1 1 18.6 80.3 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.77 N/A 0 0MP‐B00005/2/2023 13:25 0 0 19.8 80.2 0‐1.92‐2.431.8912.4156464 0 0 0 0 28.790 0 0MP‐B00005/2/2023 13:27 0 0 19.5 80.5 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.79 N/A 0 0MP‐C00005/2/2023 13:37 0 0 19.7 80.3 0‐0.98‐1.080.9921.3036565 0 0 0 0 28.82 0.01 0 0MP‐C00005/2/2023 13:390 1.7 18 80.3 0 N/AN/AN/AN/AN/AN/AN/AN/AN/A N/A28.82 N/A 0 0DUP100005/2/2023 13:51 0 0 19.9 80.1 0‐0.04‐0.160.1320.4176565 0 0 0 0 28.820 0 0DUP100005/2/2023 13:52 0 0.1 19.9 80 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.82 N/A 0 0MP‐D00005/2/2023 14:02 0 0 20.2 79.8 0‐1.24‐2.151.6052.336666 0 0 0 0 28.830 0 0MP‐D00005/2/2023 14:04 0 1.8 17.8 80.4 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.83 N/A 0 00000SG‐55/2/2023 14:18 0 0 21.2 78.8 0‐2.42‐2.952.5433.1856666 0 0 0 0 28.57 0.01 0 00000SG‐55/2/2023 14:20 0 0.1 19.2 80.7 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.57 N/A 0 0MP‐E00005/2/2023 14:45 0.1 0 20.2 79.7 2‐1.46‐1.981.3041.9586666 0 0 0 0 28.720 0 0MP‐E00005/2/2023 14:46 0.1 1.5 19.5 78.9 2 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.72 N/A 0 0MP‐F00005/2/2023 15:02 0 0 21.3 78.7 0‐3.45‐4.563.3814.5316666 0 0 0 0 28.810 0 0MP‐F00005/2/2023 15:04 0 2.1 19.6 78.3 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.81 N/A 0 0MP‐G00005/2/2023 15:18‐‐ ‐‐ ‐‐ ‐‐ ‐‐‐0.11‐0.130.0290.036‐‐‐‐‐‐ ‐‐ ‐‐ ‐‐28.80 N/A‐‐ ‐‐MP‐G00005/2/2023 15:20 0 0.1 19.5 80.4 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.80 N/A 0 0MP‐H00005/2/2023 15:27 0 0 22.3 77.7 00.040.03‐0.005‐0.0076666 0 0 0 0 28.81 0.01 0 0MP‐H00005/2/2023 15:29 0 5.7 3.6 90.7 0 N/AN/AN/AN/AN/AN/AN/A N/A N/A N/A28.81 N/A 0 0