23057_CharlotteVan&Storage_Final Grade Soil Assessment Rpt and Review Letter_20230614

June 14, 2023
Sent via Email
Mr. Patrick Foster Lennar Multifamily Communities, LLC 500 East Morehead Street, Suite 300 Charlotte, North Carolina 28202
[e-mail]
Subject: Review of Final Grade Soil Assessment Report Charlotte Van & Storage Co. Brownfield Property Charlotte, Mecklenburg County
Brownfields Project No. 23057-19-060
Dear Mr. Foster: The North Carolina Department of Environmental Quality’s Brownfields Redevelopment
Section (DEQ Brownfields) received the Final Grade Soil Assessment Report (Report) dated
June 12, 2023, submitted by Hart & Hickman for the above referenced Brownfields Property. The Report summarizes the final grade soil assessment activities conducted in accordance with the approved Final Grade Soil Assessment Work Plan dated January 4, 2023.
DEQ Brownfields reviewed the Report and evaluated the analytical results using the
January 2023 DEQ Risk Calculator. The results are consistent with those provided in the Report
and are below the thresholds for residential use. As such, DEQ Brownfields has determined that the Report complies with Land Use Restrictions 12.g of the Notice of Brownfields Property recorded September 10, 2021.
Be advised that this review from DEQ Brownfields does not waive any applicable
requirement to obtain any necessary permits, licenses or certifications for the above listed
activities nor does it waive any requirement to comply with applicable law for such activities. If you have questions about this correspondence or require additional information, please contact me by phone at [phone], or e-mail at [e-mail].
Sincerely,
Peter L. Doorn
Brownfields Project Manager ec: Haley Martin and John Lopez, Hart & Hickman Tracy Wahl, Jordan Thompson, and Kevin Slaughter, DEQ Brownfields

Via Email
June 12, 2023

NCDEQ – Division of Waste Management
Brownfields Redevelopment Section
1646 Mail Service Center
Raleigh, NC 27699-1646

Attn: Mr. Peter Doorn

Re: Final Grade Soil Assessment Report
Charlotte Van & Storage Co.
Verbena Street and Gilead Street
Charlotte, North Carolina
Brownfields Project No. 23057-19-060
H&H Project No. LEN-008

Dear Mr. Doorn:

On behalf of Lennar Multifamily Communities, LLC, enclosed please find a copy of the Final
Grade Soil Assessment Report prepared for the Charlotte Van & Storage Co. Brownfields
property (Brownfields Project No. 23057-19-060) located in Charlotte, Mecklenburg County.

Should you have questions or need additional information, please do not hesitate to contact us at
[phone].

Sincerely,
Hart & Hickman, PC
Haley Martin, PG John Lopez, PG
Senior Project Geologist Project Manager

Enclosure

cc: Mr. Patrick Foster, Quarterra (via Email)
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Final Grade Soil Assessment Report
Charlotte Van & Storage Co.
Charlotte, North Carolina
Brownfields Project No. 23057-19-060
H&H Job No. LEN-008

Table of Contents

1.0 Introduction and Background .............................................................................................. 1 
2.0 Final Grade Soil Assessment Activities ................................................................................ 3 
2.1 Final Grade Soil Sampling Methodologies .......................................................................... 3 
2.2 Soil Sample Results .............................................................................................................. 5 
2.3 Risk Evaluation..................................................................................................................... 6 
3.0 Summary and Conclusions ................................................................................................... 8 

List of Tables

Table 1 Soil Boring Log Summary
Table 2 Summary of Final Grade Soil Analytical Results

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Final Grade Soil Sample Location Map

List of Appendices

Appendix A Site Plan
Appendix B Laboratory Analytical Reports
Appendix C DEQ Risk Calculator

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Final Grade Soil Assessment Report
Charlotte Van & Storage Co.
Charlotte, North Carolina
Brownfields Project No. 23057-19-060
H&H Job No. LEN-008

1.0 Introduction and Background

On behalf of Lennar Multifamily Communities, LLC (Prospective Developer or PD), Hart &
Hickman, PC (H&H) has prepared this Final Grade Soil Assessment Report for the Charlotte Van
& Storage Co. Brownfields property (Brownfields Project No. 23057-19-060) located east of the
Verbena Street and Gilead Street intersection in Charlotte, Mecklenburg County, North Carolina
(Site). The Site consists of one parcel (Parcel Identification Number 14903412) that totals
approximately 5.4 acres of land located in a mixed residential, commercial, and industrial use area
of lower South End Charlotte. A Site location map is included as Figure 1 and the Site and
surrounding area are shown in Figure 2.

The Site was previously comprised primarily of land used for agricultural purposes with small
structures located in the southwestern portion of the Site as early as the late 1930s. From the late
1940s to the late 1960s, residences were constructed on the southwestern, southern, and
northeastern portions of the Site. In 1969, a storage and distribution warehouse building was
constructed for the Charlotte Van & Storage Company in the northern portion of the former 213
Verbena Street parcel. In 1972, an automotive repair warehouse building was constructed on
former 4615 Gilead Street parcel and has been occupied by multiple tenants for automotive repair,
paint, and body shop operations since construction. In 1974, a service garage was constructed
south of the storage and distribution warehouse building located on the former 213 Verbena Street
parcel for truck maintenance and repairs associated with Charlotte Van & Storage Co. fleet
vehicles.

To assist with managing environmental impacts associated with historical operations at the Site, a
Brownfields Agreement between the North Carolina Department of Environmental Quality (DEQ)
and the PD was recorded on September 10, 2021. As part of the Brownfields process, a review of
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previous environmental assessment at the Site was performed and additional assessment activities
were conducted. A summary of environmental assessment activities conducted at the Site prior to
the recordation of the Brownfields Agreement is provided in the Notice of Brownfields Property
recorded at the Mecklenburg County Register of Deeds.

The Land Use Restriction (LUR) presented in LUR g. of the Brownfields Agreement generally
states that no occupancy of the Brownfields property may occur after redevelopment until
representative final grade soil samples have been collected in areas at the Site that are not covered
by impervious materials (i.e. building foundations, sidewalks, asphalt, concrete, etc.). The
Brownfields Agreement also states that physical redevelopment of the Site will be conducted in
accordance with a DEQ-approved Environmental Management Plan (EMP). An EMP for the Site
was provided to DEQ on November 17, 2020, and was subsequently approved by DEQ on
November 24, 2020.

Redevelopment activities at the Site are complete. The redevelopment activities included the
construction of two multistory high-density residential apartment buildings, a clubhouse building,
a maintenance building, and associated access drives, parking areas, and landscaping. A Site Plan
prepared by BGE, Inc. depicting the redevelopment is included as Appendix A.

As indicated in the DEQ-approved EMP and as required by the executed Brownfields Agreement
for the Site, the PD conducted final grade soil sampling upon completion of redevelopment
activities. To assist with the final grade soil sampling activities, H&H prepared a Final Grade Soil
Assessment Work Plan (Work Plan) for DEQ review and approval. The Work Plan was approved
by DEQ in a letter dated January 12, 2023. A summary of the final grade sampling activities is
provided in the following sections.

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2.0 Final Grade Soil Assessment Activities

Final grade soil sampling activities were conducted at the Site in February 2023 and May 2023 to
evaluate the potential for impacts in shallow soil within landscaped areas of the Site not covered
in building foundations, sidewalks, or asphalt or concrete parking areas and driveways, or other
impervious materials. Due to construction completion dates, final grade soil sampling in February
2023 was conducted in the vicinity of Building 1 and the eastern portion of the Site, and final grade
soil sampling in May 2023 was conducted in the vicinity of Building 2 and the central portion of
the Site.

The final grade soil sampling activities were conducted in general accordance with the DEQ
Inactive Hazardous Sites Branch (IHSB) Guidelines for Assessment and Cleanup of Contaminated
Sites (Guidelines) dated September 2022, the most recent versions of the U.S. Environmental
Protection Agency (EPA) Region IV Laboratory Services and Applied Science Division (LSASD)
Field Branches Quality System and Technical Procedures guidance, and the DEQ-approved Work
Plan.

2.1 Final Grade Soil Sampling Methodologies

As discussed in the Work Plan, results of visual observations conducted by H&H and
conversations with Site personnel indicated that the Site is predominately covered with hardscape
surfaces with the exception of generally isolated or narrow landscaped areas. Locations of
landscaped areas at the Site are shown in Figure 3.

To evaluate for the potential presence of impacts in shallow soil at the Site, landscaped areas were
divided into ten (10) evaluation areas (FG-1 through FG-10) and a representative final grade soil
sample was collected from each area. The ten (10) final grade evaluation areas are shown on
Figure 3 and are described below:

 Final grade areas FG-1 through FG-3 included landscaped areas located near Building 1;
 Final grade areas FG-4 and FG-5 included landscaped areas located near the western and
southwestern portions of Building 2;
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 Final grade area FG-6 included landscaped areas in the central portion of the Site; and
 Final grade areas FG-7 through FG-10 included landscaped areas in the southeastern and
eastern portions of the Site.

Final grade soil samples were collected by advancing a soil boring to approximately 2 feet below
the ground surface (ft bgs) utilizing a decontaminated stainless-steel hand auger and collecting soil
samples from five aliquot locations within in each evaluation area. Continuous soil samples were
collected from the center of the hand auger bucket and observed for the presence of staining or
odors and field screened for elevated volatile organic vapors using a calibrated photoionization
detector (PID). Soil lithology at the aliquot locations generally consisted of moist clayey silt. A
summary of aliquot soil boring lithology and PID readings is provided in Table 1. The aliquot soil
sample locations for each final grade area are shown in Figure 3.

Following boring advancement, the soil sample aliquots from each area were combined and
homogenized to form one composite soil sample per area for a total of ten (10) composite final
grade soil samples (FG-1 through FG-10). Composite soil samples from each area were collected
directly into dedicated laboratory supplied sample containers and submitted to Pace Analytical
(Pace) under standard chain of custody protocols for analysis of semi-volatile organic compounds
(SVOCs) by EPA Method 8270, and Resource Conservation and Recovery Act (RCRA) metals
plus hexavalent chromium by EPA Methods 6020/7471/7199.

In addition to the composite soil samples described above, one representative grab soil sample was
collected from each evaluation area from the aliquot location that exhibited the highest PID
reading. The grab soil samples were collected from undisturbed portions of soil in the hand auger
bucket and placed directly into laboratory supplied glassware for submittal to a Pace under
standard chain of custody protocols for analysis of volatile organic compounds (VOCs) by EPA
Method 8260.

For quality assurance and quality control purposes (QA/QC), H&H collected two duplicate
composite samples (FG-DUP) from FG-1 and (FG-DUP-230509) from FG-7 for SVOCs and
RCRA metals plus hexavalent chromium. H&H also collected a duplicate representative grab
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sample from the aliquot where VOCs were collected in the same sections. A tabular summary of
the duplicate sample results along with the final grade sample analytical results are provided in
Table 2. Review of the duplicate sample laboratory analytical data in comparison to the parent
samples indicate similar results and are within typical laboratory variability. This result suggests
satisfactory laboratory analytical repeatability.

Following sampling activities, the soil borings were abandoned and the surfaces were repaired
similar to pre-drilling conditions. Additionally, the soil boring locations were estimated using a
hand-held global positioning system (GPS) unit.

2.2 Soil Sample Results

A tabular summary of final grade soil sample analytical results is presented in Table 2, and the
laboratory analytical reports and chain of custody records are provided in Appendix B. The
laboratory analytical results were compared to the DEQ Residential PSRGs dated January 2023.
In addition to the PSRGs, metals results were compared to Site-specific and published
concentrations for naturally occurring metals in North Carolina soil.

VOCs
Laboratory analytical results indicate that several VOCs were detected at concentrations above the
laboratory method detection limits, but below the DEQ Residential PSRGs in the final grade soil
samples.

SVOCs
Laboratory analytical results indicate the polynuclear aromatic hydrocarbon (PAH)
benzo(a)pyrene (0.146 J mg/kg) was detected at a concentration above the DEQ Residential PSRG
of 0.11 mg/kg in final grade soil sample FG-5. Note that the “J” flag designation indicates the
concentration was detected above the laboratory method detection limit, but below the laboratory
reporting limit, resulting in a laboratory estimated concentration. No other SVOCs were detected
at concentrations above the DEQ Residential PSRGs in the final grade soil samples.

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Metals
As expected, several metals were detected at concentrations above laboratory method detection
limits in the final grade samples collected at the Site. Hexavalent chromium (up to 1.83 mg/kg)
was detected in several of the final grade soil samples at concentrations slightly above the DEQ
Residential PSRG and Site-specific background concentrations. The remaining concentrations of
metals detected in the final grade soil samples were generally consistent with both published and
Site-specific background concentrations and are considered representative of naturally occurring
levels.

2.3 Risk Evaluation

DEQ PSRGs are very conservative and based upon a Target Cancer Risk (TCR) of 1 x 10-6 for
potential carcinogenic effects and a Hazard Quotient (HQ) of 0.2 for potential non-carcinogenic
effects. Additional assessment or remediation is not typically warranted if the calculated
cumulative lifetime incremental carcinogenic risk (LICR) is 1 x 10-4 or less and the acceptable
level for non-carcinogenic risk is a calculated cumulative hazard index (HI) of 1.0 or less.

H&H utilized the DEQ Risk Calculator (January 2023) assuming a residential land use to further
evaluate potential cumulative risks for the direct exposure pathway for a future occupant. To
model the potential for exposure risk under a hypothetical “worst-case” scenario, H&H
conservatively calculated the cumulative risks using the highest concentration of any compound
detected in any soil sample collected from the Site. Please note that although most of the metal
concentrations are likely naturally occurring, the concentration of metals detected were not omitted
from the risk calculation as a further conservative measure. Risk calculator results are summarized
in the table below and a copy of the completed risk calculator is provided in Appendix C.

Land Use Scenario Calculated
Cumulative LICR
Calculated
Cumulative HI
Calculated LICR or
HI Exceeds
Acceptable Risk
Levels?
Residential 1.2 x 10-5 0.14 No

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The results of the risk calculation indicate that the calculated cumulative risks do not exceed
acceptable carcinogenic or noncarcinogenic risk levels for a residential use exposure scenario. As
such, additional assessment or remediation is not warranted.

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3.0 Summary and Conclusions

H&H has completed final grade soil sampling activities at the Charlotte Van & Storage Co.
Brownfields property located east of the Verbena Street and Gilead Street intersection in Charlotte,
North Carolina. The final grade soil sampling activities were conducted in accordance with the
DEQ Brownfields approved Work Plan dated January 4, 2023. Final grade soil sampling activities
included the collection of soil samples to evaluate the potential for impacts in landscaped areas at
the Site not covered by impervious surfaces following redevelopment.

Laboratory analytical results indicate that several VOCs and SVOCs were detected at
concentrations above the laboratory method detection limits in the soil samples collected at the
Site. The PAH benzo(a)pyrene was detected a concentration above the DEQ Residential PSRG in
the FG-5 evaluation area located in southwestern portion of the Site near Building No. 2. No other
VOCs or SVOCs were detected at concentrations exceeding the DEQ Residential PSRGs.

Hexavalent chromium (up to 1.83 mg/kg) was detected in several samples at concentrations
slightly above the DEQ Residential PSRG and Site-specific background concentrations.
Remaining concentrations of metals detected were generally consistent with published and Site-
specific background concentrations and are considered representative of naturally occurring levels.

Potential cumulative risks for the combined soil pathway for a residential occupant at the Site was
conservatively calculated using the highest concentrations detected in the final grade samples. The
results of the risk calculation indicate that the calculated LICR for final grade soil samples is 1.2
x 10-5 and the HI is 0.14. Thus, the calculated carcinogenic and noncarcinogenic risks do not
exceed acceptable levels for a residential use exposure scenario and additional assessment or
remediation is not warranted.

Tables

Table 1
Soil Boring Log Summary
Charlotte Van & Storage Co.
Charlotte, North Carolina
H&H Job No. LEN-008
Evaluation Area &
Composite Sample ID Aliquot Location Date
Depth
(ft bgs)Lithology PID Reading
(ppm)Notes
0-1 Moist, Soft, Red-Brown Silty Clay 0.8
1-2 Moist, Soft, Yellow-Brown Silty Clay, Trace Fine Sand 0.8
0-1 Moist, Soft, Red-Brown Silty Clay, Trace Fine Gravel 0.7
1-2 Moist, Soft, Red-Brown Silty Clay, Trace Fine Gravel 0.4
0-1 Moist, Soft, Red-Brown Silty Clay, Trace Fine Gravel 1.3
1-2 Moist, Soft, Red-Brown Silty Clay, Trace Fine Gravel 1.2 Grab VOC sample collected for laboratory analysis
0-1 Moist, Soft, Red-Brown Silty Clay, Trace Fine Gravel 1.2
1-2 Moist, Soft, Dark Red-Brown, Silty Clay 0.8
0-1 Moist, Soft, Red-Brown Silty Clay 1.3
1-2 Moist, Soft, Red-Brown Silty Clay 0.6
0-1 Wet, Soft, Red-Brown Silt, Some Clay 0.5
1-2 Soft, Loose, Coarse Gravel, Few Cobbles 0.5
0-1 Moist, Soft, Red-Brown Silt 1.3
1-2 Moist, Soft, Red-Brown Silt 1.5 Grab VOC sample collected for laboratory analysis
0-1 Moist, Soft, Red-Brown/Yellow Silt 0.7
1-2 Moist, Soft, Red-Brown/Yellow Silt, Few Coarse Gravel 0.6
0-1 Moist, Soft, Red-Brown/Yellow Silt, Few Coarse Gravel 1.0
1-2 Moist, Soft, Red-Brown/Yellow Silt, Few Coarse Gravel 1.1
0-1 Moist, Soft, Red-Brown/Yellow Silt, Few Coarse Gravel 2.1
1-2 Moist, Soft, Red-Brown/Yellow Silt, Some Blue/Gray Clay 0.8
0-1 Moist, Soft, Dark Brown Silt 1.8
1-2 Wet, Soft, Brown Sandy Silt 0.8
0-1 Wet, Soft, Blue-Gray Silt 2.5
1-2 Wet, Soft, Blue-Gray Silt 1.0 Grab VOC sample collected for laboratory analysis
0-1 Moist, Soft, Red-Brown Sandy Silt 2.1
1-2 Wet, Soft, Red-Brown Sandy Silt 1.0
0-1 Moist, Soft, Yellow-Brown Sandy Silt 0.9
1-2 Moist, Soft, Yellow-Brown Sandy Silt 0.9
0-1 Moist, Soft, Red-Brown Sandy Silt 2.3
1-2 Moist, Soft, Red-Brown Sandy Silt 0.6
0-1 Moist, Medium Stiff, Brown-Yellow Clay 6.4
1-2 Moist, Medium Stiff, Yellow-Red Clay 6.2
0-1 Moist, Medium Stiff, Yellow-Red Clay 4.9
1-2 Moist, Medium Stiff, Yellow-Red Clay 4.6
0-1 Moist, Medium Stiff, Yellow-Red Clay 6.8
1-2 Moist, Medium Stiff, Yellow-Red Clay 5.1
0-1 Moist, Medium Stiff, Yellow-Red Clay 5.9
1-2 Moist, StiffBrown, Yellow-Red Sandy Clay 7.8 Grab VOC sample collected for laboratory analysis
0-1 Moist, Medium Stiff, Yellow-Red Clay 6.5
1-2 Moist, Medium Stiff, Yellow-Red Clay 4.0
0-1 Dry, Gravely, Medium Sand 2.8
1-2 Dry, Stiff, Yellow-Red Clay 4.0
0-1 Dry, Gravely, Medium Sand 5.4
1-2 Dry, Stiff, Yellow-Red Clay, Some Gravel 5.0
0-1 Dry, Stiff, Yellow-Red Clay, Some Gravel 5.7
1-2 Dry, Stiff, Yellow-Red Clay, Some Gravel 7.6 Grab VOC sample collected for laboratory analysis
0-1 Dry, Stiff, Yellow-Red Clay, Some Gravel 7.0
1-2 Dry, Stiff, Yellow-Red Clay, Some Gravel 6.9
0-1 Dry, Stiff, Yellow-Red Clay, Some Gravel 6.5
1-2 Dry, Stiff, Yellow-Red Clay, Some Gravel 5.9
2/23/2023
2/23/2023
2/23/2023
2/23/2023
2/23/2023
FG-3A
FG-1
FG-2A
FG-2B
FG-2C
FG-2D
FG-2E
FG-1A
FG-1B
FG-1C
FG-1D
FG-1E
2/23/2023
2/23/2023
2/23/2023
2/23/2023
2/23/2023
FG-3B
FG-3C
FG-3D
FG-3E
2/23/2023
2/23/2023
2/23/2023
2/23/2023
2/23/2023
5/9/2023
5/9/2023
FG-4A
FG-4B
FG-4C
FG-4D
FG-4E
5/9/2023
5/9/2023
5/9/2023
5/9/2023
5/9/2023
FG-5
FG-4
FG-3
FG-2
5/9/2023
FG-5A
FG-5B
FG-5C
FG-5D
FG-5E
5/9/2023
5/9/2023
Table 1 (Page 1 of 2)
Hart & Hickman
Table 1
Soil Boring Log Summary
Charlotte Van & Storage Co.
Charlotte, North Carolina
H&H Job No. LEN-008
Evaluation Area &
Composite Sample ID Aliquot Location Date
Depth
(ft bgs)Lithology PID Reading
(ppm)Notes
0-1 Moist, Medium Stiff, Yellow-Red Clay 3.6
1-2 Moist, Medium Stiff, Yellow-Red Clay 5.1
0-1 Moist, Medium Stiff, Yellow-Red Clay 3.3
1-2 Moist, Medium Stiff, Yellow-Red Clay 10.7 Grab VOC sample collected for laboratory analysis
0-1 Moist, Medium Stiff, Yellow-Red Clay 5.3
1-2 Moist, Medium Stiff, Yellow-Red Clay 6.0
0-1 Moist, Medium Stiff, Yellow-Red Clay 5.0
1-2 Moist, Medium Stiff, Yellow-Red Clay 3.1
0-1 Moist, Soft, Brown Silty Sand 5.1
1-2 Moist, Medium Stiff, Yellow-Red Clay 6.0
0-1 Moist, Medium Stiff, Yellow-Red Sandy Clay, Few Gravel 2.9
1-2 Moist, Medium Stiff, Yellow-Red Sandy Clay 4.0
0-1 Moist, Medium Stiff, Yellow-Red Sandy Clay, Few Gravel 3.1
1-2 Moist, Medium Stiff, Yellow-Red Sandy Clay, Few Gravel 2.9
0-1 Moist, Medium Stiff, Yellow-Red Sandy Clay, Few Gravel 3.8
1-2 Moist, Medium Stiff, Yellow-Red Sandy Clay, Few Gravel 4.9
0-1 Moist, Medium Stiff, Yellow-Red Sandy Clay, Some C Gravel 3.6
1-2 Moist, Dense, Dark Brown, Gravely Sand, Few Clays 3.2
0-1 Moist, Medium Stiff, Yellow-Red Sandy Clay, Some C Gravel 3.8
1-2 Moist, Dense, Dark Brown, Gravely Sand, Few Clays 5.0 Grab VOC sample collected for laboratory analysis
0-1 Moist, Soft, Brown-Gray Sandy Silt 0.5
1-2 Moist, Soft, Red-Brown Silt with Clay 0.4
0-1 Moist, Medium Stiff, Red-Brown Silty Clay 1.4 Grab VOC sample collected for laboratory analysis
1-2 Moist, Stiff, Red-Brown Silty Clay 0.7
0-1 Moist, Soft, Red-Brown Silty Clay 0.3
1-2 Moist, Soft, Red-Brown Silty Clay 0.5
0-1 Moist, Soft, Red-Brown Silty Clay 0.6
1-2 Moist, Soft, Red-Brown Silty Clay 0.3
0-1 Dry, Loose, Brown-Gray Silty Sand 0.3
1-2 Dry, Loose, Brown-Gray Silty Sand 0.5
0-1 Wet, Soft, Red-Brown Clay 0.5
1-2 Wet, Soft, Red-Brown Clay 0.9 Grab VOC sample collected for laboratory analysis
0-1 Moist, Soft, Few Sands Than Clay 0.6
1-2 Moist, Soft, Red-Brown Silt, Some Clay 0.6
0-1 Moist, Medium Stiff, Red-Brown Silt, Some Clay 0.8
1-2 Wet, Loose, Brown-Gray Silty Sand 0.5
0-1 Moist, Medium Stiff, Red-Brown Silt, Some Clay 0.5
1-2 Moist, Soft, Red-Brown Silt, Some Clay 0.2
0-1 Moist, Soft, Red-Brown Silt, Some Clay 0.4
1-2 Wet, Loose, Brown-Gray Silty Sand 0.6
0-1 Moist, Stiff, Red-Brown Silty Clay 1.1
1-2 Moist, Stiff, Red-Brown Silty Clay 1.4
0-1 Slight Odor, Moist, Red-Brown Silt 32.5 Grab VOC sample collected for laboratory analysis
1-2 No Odor, Moist, Red-Brown Silt 5.1
0-1 Moist, Soft, Red-Brown, Some Clay, Gray-Green C Sand 1.8
1-2 Moist, Soft, Red-Brown Clay 1.4
0-1 Moist, Soft, Red-Brown C Sand, Brown Silt 4.6
1-2 Moist, Soft, Red-Brown C Sand 10.7
0-1 Moist, Soft Brown-Light Yellow Silt, Few Clays 3.3
1-2 Moist, Dense, Poorly Graded, Light Yellow Brown Sand, Few Silts 3.9
Notes:
1) Composite sample collected for labroatory analysis for labroatory analysisfor laboratory analysis of semi-VOCs, RCRA metals, and hexavalent chromium
PID = photo-ionization detector; VOC = volatile organic compound; ppm = parts per million; ft bgs = feet below ground surface
FG-6
FG-7A
FG-6D
FG-6E
5/9/2023
5/9/2023
5/9/2023
5/9/2023
FG-6A 5/9/2023
FG-6B
FG-6C
FG-7B
FG-7C
FG-7D
FG-7E
FG-7
5/9/2023
5/9/2023
5/9/2023
5/9/2023
5/9/2023
FG-9
FG-9A
FG-9B
FG-9C
FG-9D
FG-8A
FG-8B
FG-8C
FG-8D
FG-8E
FG-8
FG-9E
2/23/23023
2/23/23023
2/23/23023
2/23/23023
2/23/23023
2/23/23023
2/23/23023
2/23/23023
2/23/23023
2/23/23023
2/24/2023
2/24/2023
2/24/2023
2/24/2023
2/24/2023
FG-10
FG-10A
FG-10B
FG-10C
FG-10D
FG-10E
Table 1 (Page 2 of 2)
Hart & Hickman
Table 2Summary of Final Grade Soil Sample Analytical ResultsCharlotte Van & Storage Co. Charlotte, North CarolinaH&H Job No. LEN-008Evaluation AreaScreening CriteriaSample IDDateDepth (ft bgs)1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite UnitsVOCs (8260D)Acetone<0.0501 NA <0.0481 NA <0.0551 NA <0.0491 NA <0.0384 NA <0.0475 NA14,000-- --Chlorobenzene<0.0045 NA <0.0043 NA <0.0049 NA <0.0044 NA0.130NA0.140NA58-- --Ethylbenzene<0.0036 NA <0.0035 NA <0.0040 NA <0.0036 NA <0.0028 NA <0.0035 NA6.1-- --p−Isopropyltoluene<0.0038 NA0.0047 JNA <0.0042 NA <0.0038 NA <0.0029 NA <0.0036 NANE-- --Naphthalene<0.0041 NA <0.0039 NA <0.0045 NA <0.0040 NA <0.0031 NA <0.0039 NA2.1-- --n−Propylbenzene<0.0028 NA <0.0027 NA <0.0031 NA <0.0027 NA <0.0021 NA <0.0026 NA780-- --Styrene<0.0021 NA <0.0020 NA <0.0023 NA <0.0020 NA <0.0016 NA <0.0020 NA1,200-- --1,2,4−Trimethylbenzene<0.0046 NA <0.0045 NA <0.0051 NA <0.0045 NA <0.0036 NA <0.0044 NA63-- --m&p−Xylene<0.0053 NA <0.0051 NA <0.0059 NA <0.0052 NA <0.0041 NA <0.0051 NA120-- --o−Xylene<0.0034 NA <0.0033 NA <0.0038 NA <0.0034 NA <0.0026 NA <0.0033 NA140-- --SVOCs (8270E)Benzo(a)anthraceneNA <0.144 NA <0.140 NA <0.140 NA <0.140 NA <0.146 NA0.173 J1.1-- --Benzo(a)pyreneNA <0.149 NA <0.145 NA <0.145 NA <0.145 NA <0.151 NA0.146 J0.11-- --Benzo(b)fluorantheneNA <0.144 NA <0.140 NA <0.140 NA <0.140 NA <0.146 NA0.168 J1.1-- --ChryseneNA <0.157 NA <0.153 NA <0.153 NA <0.153 NA <0.159 NA0.182 J110-- --FluorantheneNA <0.148 NA <0.144 NA <0.144 NA <0.144 NA <0.150 NA0.242 J480-- --PyreneNA <0.175 NA <0.171 NA <0.171 NA <0.171 NA <0.178 NA0.300 J360-- --Metals (6020B/7471B/7199)ArsenicNA2.4NA2.1NA1.7NA2.4NA2.0NA1.8 0.68 1.28 - 3.03 1.0 - 18BariumNA23.9NA55.6NA73.5NA45.4NA116NA76.6 3,100 38.1 - 94.6 50 - 1,000CadmiumNA <0.038 NA <0.038 NA0.044 JNA <0.037 NA0.071 JNA0.058 J 1.4ND - 0.4341.0 - 10Chromium (total)NA44.2NA41.7NA35.1NA27.2NA66.2NA37.5 NE 47.1 - 59.9 7.0 - 300Hexavalent ChromiumNA <0.329 NA1.07 JNA <0.311 NA1.83NA0.681 JNA0.502 J 0.31 ND - 0.540 NSTrivalent ChromiumNA44.2NA40.6NA35.1NA25.4NA65.5NA37.0 23,000 47.1 - 59.4 NSLeadNA11.5NA13.2NA10.1NA9.2NA18.5NA17.5 400 7.33 - 11.6 ND - 50MercuryNA0.035NA0.048NA0.034NA0.029NA0.032NA0.033 4.70.0365 - 0.05020.03 - 0.52SeleniumNA0.69NA0.55 JNA0.47 JNA0.27 JNA0.47 JNA0.34 J 78 0.586 - 1.04<0.1 - 0.8SilverNA <0.26 NA <0.26 NA <0.26 NA <0.25 NA <0.26 NA <0.2478 ND ND - 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Residential Preliminary Soil Remediation Goals (PSRGs) dated January 2023. 2) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Bold values exceed the Residential PSRs and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface; NS = not specified; NE = not established; -- = not applicable; ND = not detected; NA = not analyzedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. Final GradeResidential PSRGs (1)FG-2 FG-32/23/2023 2/23/2023 5/9/2023 5/9/2023Published Range (2)Site-Specific RangeBackground Metals mg/kgFG-5FG-4FG-1 / FG-DUP2/23/2023https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Lennar (LEN)/LEN‐008 Verbena Assemblage/Final Grade Soil Sampling/Report/Tables/Data Table6/9/2023Table 2 (Page 1 of 2)Hart & Hickman, PC
Table 2Summary of Final Grade Soil Sample Analytical ResultsCharlotte Van & Storage Co. Charlotte, North CarolinaH&H Job No. LEN-008Evaluation AreaScreening CriteriaSample IDDateDepth (ft bgs)1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 1-2 0-2 0-1 0-2Sample Type Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite Grab Composite UnitsVOCs (8260D)Acetone0.0518 JNA <0.0481 NA <0.0336 NA <0.0486 NA <0.0435 NA <0.0441 NA14,000-- --Chlorobenzene<0.0041 NA0.0578NA0.0366NA <0.0043 NA <0.0039 NA <0.0039 NA58-- --Ethylbenzene<0.0034 NA <0.0035 NA <0.0024 NA <0.0035 NA <0.0032 NA0.0230NA6.1-- --p−Isopropyltoluene0.0593NA <0.0037 NA <0.0026 NA <0.0037 NA <0.0033 NA <0.0034 NANE-- --Naphthalene<0.0038 NA <0.0039 NA <0.0027 NA <0.0040 NA <0.0036 NA0.166NA2.1-- --n−Propylbenzene<0.0026 NA <0.0027 NA <0.0019 NA <0.0027 NA <0.0024 NA0.127NA780-- --Styrene<0.0019 NA <0.0020 NA <0.0014 NA0.0244NA <0.0018 NA <0.0018 NA1,200-- --1,2,4−Trimethylbenzene<0.0043 NA <0.0045 NA <0.0031 NA <0.0045 NA0.0053 JNA0.444NA63-- --m&p−Xylene<0.0049 NA <0.0051 NA <0.0036 NA <0.0052 NA <0.0046 NA0.0061 JNA120-- --o−Xylene<0.0032 NA <0.0033 NA <0.0023 NA0.0039 JNA <0.0030 NA <0.0030 NA140-- --SVOCs (8270E)Benzo(a)anthraceneNA <0.146 NA <0.135 NA <0.135 NA <0.145 NA <0.140 NA <0.1421.1-- --Benzo(a)pyreneNA <0.152 NA <0.140 NA <0.139 NA <0.151 NA <0.145 NA <0.1470.11-- --Benzo(b)fluorantheneNA <0.146 NA <0.135 NA <0.135 NA <0.145 NA <0.140 NA <0.1421.1-- --ChryseneNA <0.160 NA <0.147 NA <0.147 NA <0.159 NA <0.152 NA <0.155110-- --FluorantheneNA <0.150 NA <0.138 NA <0.138 NA <0.149 NA <0.144 NA <0.146480-- --PyreneNA <0.178 NA <0.164 NA <0.164 NA <0.177 NA <0.170 NA <0.173360-- --Metals (6020B/7471B/7199)ArsenicNA1.8NA1.6NA2.7NA1.6NA1.3NA1.4 0.68 1.28 - 3.03 1.0 - 18BariumNA75.0NA145NA123NA123NA76.3NA84.6 3,100 38.1 - 94.6 50 - 1,000CadmiumNA <0.039 NA0.24NA0.074 JNA0.045 JNA <0.037 NA0.040 J 1.4ND - 0.4341.0 - 10Chromium (total)NA51.1NA35.2NA41.0NA30.7NA34.9NA35.2 NE 47.1 - 59.9 7.0 - 300Hexavalent ChromiumNA1.13 JNA0.450 JNA0.574 JNA <0.320 NA0.998 JNA0.879 J0.31 ND - 0.540 NSTrivalent ChromiumNA50.0NA34.8NA40.4NA30.7NA33.9NA34.3 23,000 47.1 - 59.4 NSLeadNA11.5NA37.4NA12.5NA12.9NA8.3NA11.5 400 7.33 - 11.6 ND - 50MercuryNA0.046NA0.017 JNA0.025NA0.056NA0.030NA0.034 4.70.0365 - 0.05020.03 - 0.52SeleniumNA0.42 JNA0.42 JNA0.40 JNA0.38 JNA0.44 JNA0.30 J 78 0.586 - 1.04<0.1 - 0.8SilverNA <0.27 NA <0.24 NA <0.23 NA <0.27 NA <0.25 NA <0.2678 ND ND - 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Residential Preliminary Soil Remediation Goals (PSRGs) dated January 2023. 2) Range values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005. Cd and Ag concentrations were taken from Southeastern & Conterminous US soils. Concentrations are reported in milligrams per kilogram (mg/kg).Concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses. Aside from metals, only those compounds detected in at least one sample are shown in the table above. Bold values exceed the Residential PSRG and background levels in the case of metals.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; ft bgs= feet below ground surface; NS = not specified; NE = not established; -- = not applicable; ND = not detected; NA = not analyzedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration. Background Metals Site-Specific RangePublished Range (2)2/23/2023Residential PSRGs (1)FG-65/9/22023Final Grade2/24/2023mg/kgFG-8 FG-102/23/2023FG-7 / FG-DUP-2305095/9/2023FG-9https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Lennar (LEN)/LEN‐008 Verbena Assemblage/Final Grade Soil Sampling/Report/Tables/Data Table6/9/2023Table 2 (Page 2 of 2)Hart & Hickman, PC

Figures

USGS The National Map: National Boundaries Dataset, 3DEP Elevation
Program, Geographic Names Information System, National Hydrography
Dataset, National Land Cover Database, National Structures Dataset, and
National Transportation Dataset; USGS Global Ecosystems; U.S. Census
Bureau TIGER/Line data; USFS Road Data; Natural Earth Data; U.S.
Department of State Humanitarian Information Unit; and NOAA National
Centers for Environmental Information, U.S. Coastal Relief Model. Data
refreshed June, 2022.
SITE LOCATION MAP
CHARLOTTE VAN & STORAGE CO.
VERBENA STREET AND GILEAD STREET
CHARLOTTE, NORTH CAROLINA
DATE: 5-17-23
JOB NO: LEN-008
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100
Charlotte, North Carolina 28203
704-586-0007 (p) 704-586-0373 (f)
License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Lennar (LEN)\LEN-008 Verbena Assemblage\Final Grade Soil Sampling\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE WEST, NORTH CAROLINA 2022
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
PARCEL BOUNDARY
BAKER CONSTRUCTION CO.
(129 VERBENA STREET)
VACANT COMMERCIAL BUILDING
(4516 NATIONS CROSSING ROAD)
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UNDER CONSTRUCTION
RESIDENTIAL
LOWER LEFT BREWING CO.
(4528 NATIONS CROSSING ROAD)
NOTES:
1. AERIAL IMAGERY AND BASE DATA OBTAINED FROM
MECKLENBURG COUNTY GIS (2023).
PIEDMONT NATURAL GAS
(112-338 VERBENA STREET)
REVISION NO. 0
JOB NO. LEN-008
DATE: 5-17-23
FIGURE NO. 2
CHARLOTTE VAN & STORAGE CO.
VERBENA STREET AND GILEAD STREET
CHARLOTTE, NORTH CAROLINA
SITE MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 GeologyGILEAD STREETUNDER CONSTRUCTION
S:\AAA-Master Projects\Lennar (LEN)\LEN-008 Verbena Assemblage\Final Grade Soil Sampling\Figures\LEN.008_20221005.dwg, FIG 2, 5/17/2023 3:08:25 PM, shaynes
POOL
REVISION NO. 0
JOB NO. LEN-008
DATE: 5-17-23
FIGURE NO. 3
CHARLOTTE VAN & STORAGE CO.
VERBENA STREET AND GILEAD STREET
CHARLOTTE, NORTH CAROLINA
FINAL GRADE
SOIL SAMPLE LOCATION MAP
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
BUILDING FOOTPRINT
LANDSCAPED AREA
FINAL GRADE SOIL SAMPLE
ALIQUOT LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
VE
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NOTES:
1. PARCEL DATA OBTAINED FROM MECKLENBURG COUNTY
GIS (2022).
2. SITE PLAN BASED ON REQUIRED PLANTING PLAN
PREPARED BY CLINE DESIGN DATED 10/21/2020.
FG-1A
FG-1E
FG-1D
FG-1B
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FG-10
BUILDING 1
BUILDING 2
FG-3D
FG-3E
S:\AAA-Master Projects\Lennar (LEN)\LEN-008 Verbena Assemblage\Final Grade Soil Sampling\Figures\LEN.008_20221005.dwg, FIG 3 FG, 5/30/2023 2:17:57 PM, shaynes

Appendix A
Site Plan

UBERFOODDELIVERY6
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DUMPSTER/RECYCLE AREA W/GATED SCREENED ENCLOSURE (SEE
ARCHITECTURAL PLANS FOR DETAILS)
STANDARD 2'-6" CONCRETE CURB AND GUTTER (CLDS 10.17A) (SEE SITE DETAIL SHEET)
7'X22' PARALLEL PARKING SPACE (CLDS 50.09C)
STANDARD CONCRETE SIDEWALK (CLDS 10.22) (SEE SITE DETAIL SHEET)
TYPE II MODIFIED DRIVEWAY. (CLDS 10.25E) (SEE SITE DETAIL SHEET)
DIRECTIONAL ACCESSIBLE RAMP WITH DETECTABLE WARNING (CLDS 10.40)
(SEE DETAIL SHEET)
SITE LEGEND
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24" WHITE STOP BAR (SEE SITE DETAIL SHEET)
ACCESSIBLE PARKING SPACE, TYPICAL (CLDS 50.10A)(SEE SITE
DETAIL FOR ACCESSIBLE PARKING SPACE SIZE AND SIGN)
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STANDARD DUTY ASPHALT PAVEMENT (SEE SITE DETAIL SHEET)
STANDARD DUTY 5' WIDE CONCRETE SIDEWALK (SEE SITE DETAIL SHEET)
HEAVY DUTY CONCRETE PAVEMENT (SEE SITE DETAIL SHEET)
PIANO STYLE CROSSWALK (CLDS 50.14) (SEE SITE DETAIL SHEET)
RETAINING WALL (CONTRACTOR TO PROVIDE FULL ENGINEERED PLANS
AND PERMIT THROUGH COUNTY AS REQUIRED)
6' HIGH DECORATIVE FENCE
POOL AND AMENITY AREA (SEE AMENITY PLANS BY OTHERS)
HEAVY DUTY ASPHALT PAVEMENT (SEE SITE DETAIL SHEET)
4' SWING GATE
U DIRECTIONAL PAVEMENT MARKING (SEE SITE DETAIL SHEET)
V BIKE RACK (FOR 4 BIKES) (SEE SITE DETAIL SHEET)
SWSL @ 4" - SINGLE WHITE SOLID LINE/4" WIDE
SWSL @ 24" - SINGLE WHITE SOLID LINE/24" WIDE
STRIPING LEGEND
1
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PROPOSED CURB AND GUTTER
PROPOSED PARKING SPACES
PROPOSED ASPHALT PAVEMENT
PROPOSED STD. CONCRETE SIDEWALK
PROPOSED STRUCTURE
LEGEND FOR PROPOSED IMPROVEMENTS
100
EXISTING LOT LINES
BOUNDARY LIMITS
PROPOSED EASEMENT
EXISTING RIGHT OF WAY
PROPOSED HEAVY DUTY ASPHALT PAVEMENT
PROPOSED HEAVY DUTY CONCRETE PAVEMENT
PROPOSED SITE NOTE11
PROPOSED RIGHT OF WAY
PROPOSED STORM EASEMENT
PROPOSED SPILL CURB AND GUTTER
FOODDELIVERYG:\NCA\Projects\Lennar Multifamily\6874-00 - LoSo Verbena\03 - DWG\PlanSheets\C2-0 SITE PLAN.dwg Layout: SITE Plotted: 3/18/2020 3:07:06 PMDESCRIPTIONREVDESIGNED BY:
REVIEWED BY:
DRAWN BY:DATE121 W. TRADE STREET, SUITE 1030CHARLOTTE, NC 28202www.bgeinc.comNC LICENSE #C-4397Know what's below.
before you dig.Call
R FILE NUMBER:
DATE: 03/18/2020
6874-00 c 2020LENNAR MULTIFAMILY605 LEXINGTON AVENUE, SUITE 200CHARLOTTE, NORTH CAROLINA 28203VERBENAMULTIFAMILY213 VERBENA STCHARLOTTE, NORTH CAROLINA 2821721345SITE DEVELOPMENT DATA
SITE ADDRESS
VERBENA MULTIFAMILY
213 VERBENA STREET, CHARLOTTE, NC 28217
TAX PARCEL ID# 149-034-12, 149-034-15, 149-034-16
ACREAGE 5.91
EXISTING USES INDUSTRIAL
PROPOSED USE RESIDENTIAL MULTIFAMILY APARTMENTS
PROPOSED UNITS 272
BUILDING HEIGHT
MAXIMUM BUILDING HEIGHT 50' (75' WITH BONUS)
MAX. BUILDING HEIGHT PROPOSED 54.65'
OPEN SPACE
OPEN SPACE REQUIRED NOT REQUIRED TO PROVIDE PUBLIC ON-SITE OPEN SPACE
OPEN SPACE PROVIDED N/A ACRES
ZONING CODE SUMMARY
EXISTING ZONING TOD-TR (TRANSIT ORIENTED DEVELOPMENT DISTRICT - TRANSIT
TRANSITION)
JURISDICTION CITY OF CHARLOTTE
SETBACKS AND BUFFERS
REAR YARD 0'
SIDE YARD 0'
FRONT SETBACK 16' MIN. FROM (FUTURE) BACK OF CURB
PARKING
PARKING SPACES REQUIRED0 SPACE(S) IN TOD DISTRICT
PARKING SPACES PROVIDED 292 STANDARD SPACES ( 10 HANDICAP, 8 COMPACT SPACES)
27 OFF-STREET PARKING
321 TOTAL SPACES
SHORT TERM BIKE SPACES REQUIRED 55 SPACES (1 PER 5 UNITS) 272 UNITS / 5 = 54.4
LONG TERM BIKE SPACES REQUIRED 44 SPACES (80% OF REQUIRED SPACES) 54.4 X 80%
= 43.5
SHORT TERM BIKE SPACES PROVIDED 61 SPACES (8 ONSITE SPACES WITH 53 WALL
HANGERS WITHIN UNITS)
LONG TERM BIKE SPACES PROVIDED 44 SPACES (WALL HANGERS WITHIN UNITS)
WASTE MANAGEMENT
SOLID WASTE REQUIRED: (1) X CU.YD. DUMPSTER PER 30 UNITS=
(272 UNITS / 30 UNITS X 8 CU. YDS.)= 72.5 CU. YDS.
32 CU. YD. DUMPSTER (8'X18'X6'HT)
SOLID WASTE PROVIDED:ON-SITE COMPACTOR
RECYCLING REQUIRED:(272 UNITS / 30 UNITS X 8 CU. YDS.)= 72.5 CU. YDS.
RECYCLING PROVIDED: PRIVATE SERVICES
SEE PLAN FOR LOCATION OF POSSIBLE FUTURE RECYCLING
AREA LOCATION
COMPLETION TIME LINE
BEGIN CONSTRUCTION: JULY 1, 2020
COMPLETE CONSTRUCTION:JULY 1, 2021
NATURAL AREA
REQUIRED NATURAL AREA N/A
NOTE
ALL CURB RADII 3' UNLESS OTHERWISE NOTED
SITE PLANC2-0
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(SEE AMENITY PLANS
BY OTHERS)
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INSET C - DRIVEWAY 2
DRIVEWAY 1 (TYPE II MODIFIED) - SEE INSET B
GATED ENTRANCE - SEE INSET A
DRIVEWAY 2 (TYPE II MODIFIED) - SEE INSET C
26.0'
8.0'
12.0'12.0'
R1.0'
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LOADING AREA
DMH
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ECH
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IS ROW (16' FROM
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N
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L
L
L
L
L
L
L
L
L
M
TR
D
D
D
D
D
D
D
D
N
D
D
D
D
EOPEOP
EOP
EOP
EOP
EOP
EOP
R
EOP
NPOOL MAINTENANCE BLDG.
8.00' SIDEWALK
8" - #57 STONE GRAVEL PATH
CONTRACTOR SHALL INSTALL AND SUPPLEMENT EXISTING
TO PROVIDE CONTINUOUS PATH TO YEOMAN ROAD
V
2
2
1
1
1 (TYP.)
1 (TYP.)
1 (TYP.)
1 (TYP.)
1 (TYP.)
R20.00'
R20.00'
R4.00'
R10.00'
R8.00'
R8.00'
R8.00'
R8.00'
8' WIDE STANDARD DUTY ASPHALT PATH

Appendix B
Laboratory Analytical Reports

#=CL#
May 18, 2023
LIMS USE: FR - HALEY MARTIN
LIMS OBJECT ID: 92667059
92667059
Project:
Pace Project No.:
RE:
Haley Martin
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
LEN.008 FINAL GRADE SAMPLING
Dear Haley Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on May 10, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605
Georgia Certification #: 959
GMP+ Certification #: GMP050884
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 55
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Pace Analytical Services National
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: VT2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 55
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Lab ID Sample ID Matrix Date Collected Date Received
92667059001 FG-4 (0-2)Solid 05/09/23 11:00 05/10/23 06:25
92667059002 FG-5 (0-2)Solid 05/09/23 12:20 05/10/23 06:25
92667059003 FG-6 (0-2)Solid 05/09/23 13:25 05/10/23 06:25
92667059004 FG-7 (0-2)Solid 05/09/23 14:25 05/10/23 06:25
92667059005 FG-DUP-230509 (0-2)Solid 05/09/23 00:00 05/10/23 06:25
92667059006 FG-4 (1-2)Solid 05/09/23 11:00 05/10/23 06:25
92667059007 FG-5 (1-2)Solid 05/09/23 12:20 05/10/23 06:25
92667059008 FG-6 (1-2)Solid 05/09/23 13:25 05/10/23 06:25
92667059009 FG-7 (1-2)Solid 05/09/23 14:25 05/10/23 06:25
92667059010 FG-DUP-230509 (1-2)Solid 05/09/23 00:00 05/10/23 06:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92667059001 FG-4 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667059002 FG-5 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667059003 FG-6 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667059004 FG-7 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667059005 FG-DUP-230509 (0-2)EPA 6020B 7 PASI-MNN2
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667059006 FG-4 (1-2)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667059007 FG-5 (1-2)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667059008 FG-6 (1-2)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92667059009 FG-7 (1-2)EPA 8260D 70 PASI-CLMB
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 55
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
SW-846 1 PASI-CKDF
92667059010 FG-DUP-230509 (1-2)EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-4 (0-2)Lab ID:92667059001 Collected:05/09/23 11:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.0 mg/kg 05/17/23 13:43 7440-38-205/17/23 07:110.64 0.18 1
Barium 116 mg/kg 05/17/23 13:43 7440-39-3 M105/17/23 07:110.39 0.097 1
Cadmium 0.071J mg/kg 05/17/23 13:43 7440-43-905/17/23 07:110.10 0.038 1
Chromium 66.2 mg/kg 05/17/23 13:43 7440-47-3 M105/17/23 07:112.6 0.50 1
Lead 18.5 mg/kg 05/17/23 13:43 7439-92-105/17/23 07:110.64 0.12 1
Selenium 0.47J mg/kg 05/17/23 13:43 7782-49-205/17/23 07:110.64 0.14 1
Silver <0.26 mg/kg 05/17/23 13:43 7440-22-405/17/23 07:110.64 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.032 mg/kg 05/17/23 16:36 7439-97-605/17/23 07:410.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <154 ug/kg 05/15/23 13:24 83-32-905/12/23 14:174381541
Acenaphthylene <154 ug/kg 05/15/23 13:24 208-96-805/12/23 14:174381541
Aniline <171 ug/kg 05/15/23 13:24 62-53-305/12/23 14:174381711
Anthracene <143 ug/kg 05/15/23 13:24 120-12-705/12/23 14:174381431
Benzo(a)anthracene <146 ug/kg 05/15/23 13:24 56-55-305/12/23 14:174381461
Benzo(a)pyrene <151 ug/kg 05/15/23 13:24 50-32-805/12/23 14:174381511
Benzo(b)fluoranthene <146 ug/kg 05/15/23 13:24 205-99-205/12/23 14:174381461
Benzo(g,h,i)perylene <170 ug/kg 05/15/23 13:24 191-24-205/12/23 14:174381701
Benzo(k)fluoranthene <154 ug/kg 05/15/23 13:24 207-08-905/12/23 14:174381541
Benzoic Acid <941 ug/kg 05/15/23 13:24 65-85-005/12/23 14:1721909411
Benzyl alcohol <332 ug/kg 05/15/23 13:24 100-51-605/12/23 14:178763321
4-Bromophenylphenyl ether <168 ug/kg 05/15/23 13:24 101-55-305/12/23 14:174381681
Butylbenzylphthalate <184 ug/kg 05/15/23 13:24 85-68-705/12/23 14:174381841
4-Chloro-3-methylphenol <308 ug/kg 05/15/23 13:24 59-50-705/12/23 14:178763081
4-Chloroaniline <344 ug/kg 05/15/23 13:24 106-47-805/12/23 14:178763441
bis(2-Chloroethoxy)methane <182 ug/kg 05/15/23 13:24 111-91-105/12/23 14:174381821
bis(2-Chloroethyl) ether <165 ug/kg 05/15/23 13:24 111-44-405/12/23 14:174381651
2-Chloronaphthalene <174 ug/kg 05/15/23 13:24 91-58-705/12/23 14:174381741
2-Chlorophenol <165 ug/kg 05/15/23 13:24 95-57-805/12/23 14:174381651
4-Chlorophenylphenyl ether <163 ug/kg 05/15/23 13:24 7005-72-305/12/23 14:174381631
Chrysene <159 ug/kg 05/15/23 13:24 218-01-905/12/23 14:174381591
Dibenz(a,h)anthracene <168 ug/kg 05/15/23 13:24 53-70-305/12/23 14:174381681
Dibenzofuran <158 ug/kg 05/15/23 13:24 132-64-905/12/23 14:174381581
1,2-Dichlorobenzene <158 ug/kg 05/15/23 13:24 95-50-105/12/23 14:174381581
1,3-Dichlorobenzene <155 ug/kg 05/15/23 13:24 541-73-105/12/23 14:174381551
1,4-Dichlorobenzene <167 ug/kg 05/15/23 13:24 106-46-705/12/23 14:174381671
3,3'-Dichlorobenzidine <296 ug/kg 05/15/23 13:24 91-94-105/12/23 14:178762961
2,4-Dichlorophenol <171 ug/kg 05/15/23 13:24 120-83-205/12/23 14:174381711
Diethylphthalate <161 ug/kg 05/15/23 13:24 84-66-205/12/23 14:174381611
2,4-Dimethylphenol <182 ug/kg 05/15/23 13:24 105-67-905/12/23 14:174381821
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-4 (0-2)Lab ID:92667059001 Collected:05/09/23 11:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <159 ug/kg 05/15/23 13:24 131-11-305/12/23 14:174381591
Di-n-butylphthalate <147 ug/kg 05/15/23 13:24 84-74-205/12/23 14:174381471
4,6-Dinitro-2-methylphenol <409 ug/kg 05/15/23 13:24 534-52-105/12/23 14:178764091
2,4-Dinitrophenol <1350 ug/kg 05/15/23 13:24 51-28-505/12/23 14:17219013501
2,4-Dinitrotoluene <168 ug/kg 05/15/23 13:24 121-14-205/12/23 14:174381681
2,6-Dinitrotoluene <161 ug/kg 05/15/23 13:24 606-20-205/12/23 14:174381611
Di-n-octylphthalate <172 ug/kg 05/15/23 13:24 117-84-005/12/23 14:174381721
bis(2-Ethylhexyl)phthalate <170 ug/kg 05/15/23 13:24 117-81-705/12/23 14:174381701
Fluoranthene <150 ug/kg 05/15/23 13:24 206-44-005/12/23 14:174381501
Fluorene <154 ug/kg 05/15/23 13:24 86-73-705/12/23 14:174381541
Hexachloro-1,3-butadiene <190 ug/kg 05/15/23 13:24 87-68-305/12/23 14:174381901
Hexachlorobenzene <171 ug/kg 05/15/23 13:24 118-74-105/12/23 14:174381711
Hexachlorocyclopentadiene <251 ug/kg 05/15/23 13:24 77-47-405/12/23 14:174382511
Hexachloroethane <167 ug/kg 05/15/23 13:24 67-72-105/12/23 14:174381671
Indeno(1,2,3-cd)pyrene <172 ug/kg 05/15/23 13:24 193-39-505/12/23 14:174381721
Isophorone <195 ug/kg 05/15/23 13:24 78-59-105/12/23 14:174381951
1-Methylnaphthalene <154 ug/kg 05/15/23 13:24 90-12-005/12/23 14:174381541
2-Methylnaphthalene <175 ug/kg 05/15/23 13:24 91-57-605/12/23 14:174381751
2-Methylphenol(o-Cresol)<179 ug/kg 05/15/23 13:24 95-48-705/12/23 14:174381791
3&4-Methylphenol(m&p Cresol)<176 ug/kg 05/15/23 13:24 15831-10-405/12/23 14:174381761
Naphthalene <149 ug/kg 05/15/23 13:24 91-20-305/12/23 14:174381491
2-Nitroaniline <358 ug/kg 05/15/23 13:24 88-74-405/12/23 14:1721903581
3-Nitroaniline <344 ug/kg 05/15/23 13:24 99-09-205/12/23 14:1721903441
4-Nitroaniline <333 ug/kg 05/15/23 13:24 100-01-605/12/23 14:178763331
Nitrobenzene <203 ug/kg 05/15/23 13:24 98-95-305/12/23 14:174382031
2-Nitrophenol <190 ug/kg 05/15/23 13:24 88-75-505/12/23 14:174381901
4-Nitrophenol <846 ug/kg 05/15/23 13:24 100-02-705/12/23 14:1721908461
N-Nitrosodimethylamine <147 ug/kg 05/15/23 13:24 62-75-905/12/23 14:174381471
N-Nitroso-di-n-propylamine <165 ug/kg 05/15/23 13:24 621-64-705/12/23 14:174381651
N-Nitrosodiphenylamine <155 ug/kg 05/15/23 13:24 86-30-605/12/23 14:174381551
2,2'-Oxybis(1-chloropropane)<208 ug/kg 05/15/23 13:24 108-60-105/12/23 14:174382081
Pentachlorophenol <429 ug/kg 05/15/23 13:24 87-86-505/12/23 14:178764291
Phenanthrene <143 ug/kg 05/15/23 13:24 85-01-805/12/23 14:174381431
Phenol <195 ug/kg 05/15/23 13:24 108-95-205/12/23 14:174381951
Pyrene <178 ug/kg 05/15/23 13:24 129-00-005/12/23 14:174381781
Pyridine <138 ug/kg 05/15/23 13:24 110-86-105/12/23 14:174381381
1,2,4-Trichlorobenzene <172 ug/kg 05/15/23 13:24 120-82-105/12/23 14:174381721
2,4,5-Trichlorophenol <200 ug/kg 05/15/23 13:24 95-95-405/12/23 14:174382001
2,4,6-Trichlorophenol <180 ug/kg 05/15/23 13:24 88-06-205/12/23 14:174381801
Surrogates
Nitrobenzene-d5 (S)57 %05/15/23 13:24 4165-60-005/12/23 14:1710-130 1
2-Fluorobiphenyl (S)49 %05/15/23 13:24 321-60-805/12/23 14:1710-130 1
Terphenyl-d14 (S)53 %05/15/23 13:24 1718-51-005/12/23 14:1710-130 1
Phenol-d6 (S)45 %05/15/23 13:24 13127-88-305/12/23 14:1710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-4 (0-2)Lab ID:92667059001 Collected:05/09/23 11:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)41 %05/15/23 13:24 367-12-405/12/23 14:1710-130 1
2,4,6-Tribromophenol (S)51 %05/15/23 13:24 118-79-605/12/23 14:1710-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 24.9 %05/11/23 16:26 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 78.3 %05/15/23 14:1605/15/23 14:071
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.681J mg/kg 05/17/23 17:26 18540-29-9 D8,J05/17/23 07:121.28 0.326 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-5 (0-2)Lab ID:92667059002 Collected:05/09/23 12:20 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.8 mg/kg 05/17/23 13:58 7440-38-205/17/23 07:110.58 0.17 1
Barium 76.6 mg/kg 05/17/23 13:58 7440-39-305/17/23 07:110.35 0.087 1
Cadmium 0.058J mg/kg 05/17/23 13:58 7440-43-905/17/23 07:110.093 0.034 1
Chromium 37.5 mg/kg 05/17/23 13:58 7440-47-305/17/23 07:112.3 0.45 1
Lead 17.5 mg/kg 05/17/23 13:58 7439-92-105/17/23 07:110.58 0.11 1
Selenium 0.34J mg/kg 05/17/23 13:58 7782-49-205/17/23 07:110.58 0.12 1
Silver <0.24 mg/kg 05/17/23 13:58 7440-22-405/17/23 07:110.58 0.24 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.033 mg/kg 05/17/23 16:40 7439-97-605/17/23 07:410.023 0.0099 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <137 ug/kg 05/15/23 13:52 83-32-905/12/23 14:173891371
Acenaphthylene <137 ug/kg 05/15/23 13:52 208-96-805/12/23 14:173891371
Aniline <152 ug/kg 05/15/23 13:52 62-53-305/12/23 14:173891521
Anthracene <127 ug/kg 05/15/23 13:52 120-12-705/12/23 14:173891271
Benzo(a)anthracene 173J ug/kg 05/15/23 13:52 56-55-305/12/23 14:173891301
Benzo(a)pyrene 146J ug/kg 05/15/23 13:52 50-32-805/12/23 14:173891351
Benzo(b)fluoranthene 168J ug/kg 05/15/23 13:52 205-99-205/12/23 14:173891301
Benzo(g,h,i)perylene <151 ug/kg 05/15/23 13:52 191-24-205/12/23 14:173891511
Benzo(k)fluoranthene <137 ug/kg 05/15/23 13:52 207-08-905/12/23 14:173891371
Benzoic Acid <837 ug/kg 05/15/23 13:52 65-85-005/12/23 14:1719508371
Benzyl alcohol <295 ug/kg 05/15/23 13:52 100-51-605/12/23 14:177792951
4-Bromophenylphenyl ether <150 ug/kg 05/15/23 13:52 101-55-305/12/23 14:173891501
Butylbenzylphthalate <164 ug/kg 05/15/23 13:52 85-68-705/12/23 14:173891641
4-Chloro-3-methylphenol <274 ug/kg 05/15/23 13:52 59-50-705/12/23 14:177792741
4-Chloroaniline <306 ug/kg 05/15/23 13:52 106-47-805/12/23 14:177793061
bis(2-Chloroethoxy)methane <162 ug/kg 05/15/23 13:52 111-91-105/12/23 14:173891621
bis(2-Chloroethyl) ether <146 ug/kg 05/15/23 13:52 111-44-405/12/23 14:173891461
2-Chloronaphthalene <155 ug/kg 05/15/23 13:52 91-58-705/12/23 14:173891551
2-Chlorophenol <146 ug/kg 05/15/23 13:52 95-57-805/12/23 14:173891461
4-Chlorophenylphenyl ether <145 ug/kg 05/15/23 13:52 7005-72-305/12/23 14:173891451
Chrysene 182J ug/kg 05/15/23 13:52 218-01-905/12/23 14:173891421
Dibenz(a,h)anthracene <150 ug/kg 05/15/23 13:52 53-70-305/12/23 14:173891501
Dibenzofuran <140 ug/kg 05/15/23 13:52 132-64-905/12/23 14:173891401
1,2-Dichlorobenzene <140 ug/kg 05/15/23 13:52 95-50-105/12/23 14:173891401
1,3-Dichlorobenzene <138 ug/kg 05/15/23 13:52 541-73-105/12/23 14:173891381
1,4-Dichlorobenzene <149 ug/kg 05/15/23 13:52 106-46-705/12/23 14:173891491
3,3'-Dichlorobenzidine <263 ug/kg 05/15/23 13:52 91-94-105/12/23 14:177792631
2,4-Dichlorophenol <152 ug/kg 05/15/23 13:52 120-83-205/12/23 14:173891521
Diethylphthalate <143 ug/kg 05/15/23 13:52 84-66-205/12/23 14:173891431
2,4-Dimethylphenol <162 ug/kg 05/15/23 13:52 105-67-905/12/23 14:173891621
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-5 (0-2)Lab ID:92667059002 Collected:05/09/23 12:20 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <142 ug/kg 05/15/23 13:52 131-11-305/12/23 14:173891421
Di-n-butylphthalate <131 ug/kg 05/15/23 13:52 84-74-205/12/23 14:173891311
4,6-Dinitro-2-methylphenol <364 ug/kg 05/15/23 13:52 534-52-105/12/23 14:177793641
2,4-Dinitrophenol <1200 ug/kg 05/15/23 13:52 51-28-505/12/23 14:17195012001
2,4-Dinitrotoluene <150 ug/kg 05/15/23 13:52 121-14-205/12/23 14:173891501
2,6-Dinitrotoluene <143 ug/kg 05/15/23 13:52 606-20-205/12/23 14:173891431
Di-n-octylphthalate <153 ug/kg 05/15/23 13:52 117-84-005/12/23 14:173891531
bis(2-Ethylhexyl)phthalate <151 ug/kg 05/15/23 13:52 117-81-705/12/23 14:173891511
Fluoranthene 242J ug/kg 05/15/23 13:52 206-44-005/12/23 14:173891331
Fluorene <137 ug/kg 05/15/23 13:52 86-73-705/12/23 14:173891371
Hexachloro-1,3-butadiene <169 ug/kg 05/15/23 13:52 87-68-305/12/23 14:173891691
Hexachlorobenzene <152 ug/kg 05/15/23 13:52 118-74-105/12/23 14:173891521
Hexachlorocyclopentadiene <223 ug/kg 05/15/23 13:52 77-47-405/12/23 14:173892231
Hexachloroethane <149 ug/kg 05/15/23 13:52 67-72-105/12/23 14:173891491
Indeno(1,2,3-cd)pyrene <153 ug/kg 05/15/23 13:52 193-39-505/12/23 14:173891531
Isophorone <173 ug/kg 05/15/23 13:52 78-59-105/12/23 14:173891731
1-Methylnaphthalene <137 ug/kg 05/15/23 13:52 90-12-005/12/23 14:173891371
2-Methylnaphthalene <156 ug/kg 05/15/23 13:52 91-57-605/12/23 14:173891561
2-Methylphenol(o-Cresol)<159 ug/kg 05/15/23 13:52 95-48-705/12/23 14:173891591
3&4-Methylphenol(m&p Cresol)<157 ug/kg 05/15/23 13:52 15831-10-405/12/23 14:173891571
Naphthalene <132 ug/kg 05/15/23 13:52 91-20-305/12/23 14:173891321
2-Nitroaniline <319 ug/kg 05/15/23 13:52 88-74-405/12/23 14:1719503191
3-Nitroaniline <306 ug/kg 05/15/23 13:52 99-09-205/12/23 14:1719503061
4-Nitroaniline <296 ug/kg 05/15/23 13:52 100-01-605/12/23 14:177792961
Nitrobenzene <181 ug/kg 05/15/23 13:52 98-95-305/12/23 14:173891811
2-Nitrophenol <169 ug/kg 05/15/23 13:52 88-75-505/12/23 14:173891691
4-Nitrophenol <753 ug/kg 05/15/23 13:52 100-02-705/12/23 14:1719507531
N-Nitrosodimethylamine <131 ug/kg 05/15/23 13:52 62-75-905/12/23 14:173891311
N-Nitroso-di-n-propylamine <146 ug/kg 05/15/23 13:52 621-64-705/12/23 14:173891461
N-Nitrosodiphenylamine <138 ug/kg 05/15/23 13:52 86-30-605/12/23 14:173891381
2,2'-Oxybis(1-chloropropane)<185 ug/kg 05/15/23 13:52 108-60-105/12/23 14:173891851
Pentachlorophenol <381 ug/kg 05/15/23 13:52 87-86-505/12/23 14:177793811
Phenanthrene <127 ug/kg 05/15/23 13:52 85-01-805/12/23 14:173891271
Phenol <173 ug/kg 05/15/23 13:52 108-95-205/12/23 14:173891731
Pyrene 300J ug/kg 05/15/23 13:52 129-00-005/12/23 14:173891581
Pyridine <123 ug/kg 05/15/23 13:52 110-86-105/12/23 14:173891231
1,2,4-Trichlorobenzene <153 ug/kg 05/15/23 13:52 120-82-105/12/23 14:173891531
2,4,5-Trichlorophenol <178 ug/kg 05/15/23 13:52 95-95-405/12/23 14:173891781
2,4,6-Trichlorophenol <161 ug/kg 05/15/23 13:52 88-06-205/12/23 14:173891611
Surrogates
Nitrobenzene-d5 (S)56 %05/15/23 13:52 4165-60-005/12/23 14:1710-130 1
2-Fluorobiphenyl (S)55 %05/15/23 13:52 321-60-805/12/23 14:1710-130 1
Terphenyl-d14 (S)56 %05/15/23 13:52 1718-51-005/12/23 14:1710-130 1
Phenol-d6 (S)46 %05/15/23 13:52 13127-88-305/12/23 14:1710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-5 (0-2)Lab ID:92667059002 Collected:05/09/23 12:20 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)48 %05/15/23 13:52 367-12-405/12/23 14:1710-130 1
2,4,6-Tribromophenol (S)64 %05/15/23 13:52 118-79-605/12/23 14:1710-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.7 %05/11/23 16:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.6 %05/15/23 14:1605/15/23 14:071
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.502J mg/kg 05/17/23 17:36 18540-29-9 J05/17/23 07:121.21 0.309 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-6 (0-2)Lab ID:92667059003 Collected:05/09/23 13:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.8 mg/kg 05/17/23 14:01 7440-38-205/17/23 07:110.66 0.19 1
Barium 75.0 mg/kg 05/17/23 14:01 7440-39-305/17/23 07:110.40 0.099 1
Cadmium <0.039 mg/kg 05/17/23 14:01 7440-43-905/17/23 07:110.11 0.039 1
Chromium 51.1 mg/kg 05/17/23 14:01 7440-47-305/17/23 07:112.7 0.51 1
Lead 11.5 mg/kg 05/17/23 14:01 7439-92-105/17/23 07:110.66 0.12 1
Selenium 0.42J mg/kg 05/17/23 14:01 7782-49-205/17/23 07:110.66 0.14 1
Silver <0.27 mg/kg 05/17/23 14:01 7440-22-405/17/23 07:110.66 0.27 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.046 mg/kg 05/17/23 16:42 7439-97-605/17/23 07:410.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <154 ug/kg 05/15/23 14:20 83-32-905/12/23 14:174391541
Acenaphthylene <154 ug/kg 05/15/23 14:20 208-96-805/12/23 14:174391541
Aniline <172 ug/kg 05/15/23 14:20 62-53-305/12/23 14:174391721
Anthracene <144 ug/kg 05/15/23 14:20 120-12-705/12/23 14:174391441
Benzo(a)anthracene <146 ug/kg 05/15/23 14:20 56-55-305/12/23 14:174391461
Benzo(a)pyrene <152 ug/kg 05/15/23 14:20 50-32-805/12/23 14:174391521
Benzo(b)fluoranthene <146 ug/kg 05/15/23 14:20 205-99-205/12/23 14:174391461
Benzo(g,h,i)perylene <170 ug/kg 05/15/23 14:20 191-24-205/12/23 14:174391701
Benzo(k)fluoranthene <154 ug/kg 05/15/23 14:20 207-08-905/12/23 14:174391541
Benzoic Acid <944 ug/kg 05/15/23 14:20 65-85-005/12/23 14:1722009441
Benzyl alcohol <333 ug/kg 05/15/23 14:20 100-51-605/12/23 14:178793331
4-Bromophenylphenyl ether <169 ug/kg 05/15/23 14:20 101-55-305/12/23 14:174391691
Butylbenzylphthalate <185 ug/kg 05/15/23 14:20 85-68-705/12/23 14:174391851
4-Chloro-3-methylphenol <309 ug/kg 05/15/23 14:20 59-50-705/12/23 14:178793091
4-Chloroaniline <345 ug/kg 05/15/23 14:20 106-47-805/12/23 14:178793451
bis(2-Chloroethoxy)methane <182 ug/kg 05/15/23 14:20 111-91-105/12/23 14:174391821
bis(2-Chloroethyl) ether <165 ug/kg 05/15/23 14:20 111-44-405/12/23 14:174391651
2-Chloronaphthalene <174 ug/kg 05/15/23 14:20 91-58-705/12/23 14:174391741
2-Chlorophenol <165 ug/kg 05/15/23 14:20 95-57-805/12/23 14:174391651
4-Chlorophenylphenyl ether <164 ug/kg 05/15/23 14:20 7005-72-305/12/23 14:174391641
Chrysene <160 ug/kg 05/15/23 14:20 218-01-905/12/23 14:174391601
Dibenz(a,h)anthracene <169 ug/kg 05/15/23 14:20 53-70-305/12/23 14:174391691
Dibenzofuran <158 ug/kg 05/15/23 14:20 132-64-905/12/23 14:174391581
1,2-Dichlorobenzene <158 ug/kg 05/15/23 14:20 95-50-105/12/23 14:174391581
1,3-Dichlorobenzene <156 ug/kg 05/15/23 14:20 541-73-105/12/23 14:174391561
1,4-Dichlorobenzene <168 ug/kg 05/15/23 14:20 106-46-705/12/23 14:174391681
3,3'-Dichlorobenzidine <297 ug/kg 05/15/23 14:20 91-94-105/12/23 14:178792971
2,4-Dichlorophenol <172 ug/kg 05/15/23 14:20 120-83-205/12/23 14:174391721
Diethylphthalate <161 ug/kg 05/15/23 14:20 84-66-205/12/23 14:174391611
2,4-Dimethylphenol <182 ug/kg 05/15/23 14:20 105-67-905/12/23 14:174391821
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-6 (0-2)Lab ID:92667059003 Collected:05/09/23 13:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <160 ug/kg 05/15/23 14:20 131-11-305/12/23 14:174391601
Di-n-butylphthalate <148 ug/kg 05/15/23 14:20 84-74-205/12/23 14:174391481
4,6-Dinitro-2-methylphenol <410 ug/kg 05/15/23 14:20 534-52-105/12/23 14:178794101
2,4-Dinitrophenol <1360 ug/kg 05/15/23 14:20 51-28-505/12/23 14:17220013601
2,4-Dinitrotoluene <169 ug/kg 05/15/23 14:20 121-14-205/12/23 14:174391691
2,6-Dinitrotoluene <161 ug/kg 05/15/23 14:20 606-20-205/12/23 14:174391611
Di-n-octylphthalate <173 ug/kg 05/15/23 14:20 117-84-005/12/23 14:174391731
bis(2-Ethylhexyl)phthalate <170 ug/kg 05/15/23 14:20 117-81-705/12/23 14:174391701
Fluoranthene <150 ug/kg 05/15/23 14:20 206-44-005/12/23 14:174391501
Fluorene <154 ug/kg 05/15/23 14:20 86-73-705/12/23 14:174391541
Hexachloro-1,3-butadiene <190 ug/kg 05/15/23 14:20 87-68-305/12/23 14:174391901
Hexachlorobenzene <172 ug/kg 05/15/23 14:20 118-74-105/12/23 14:174391721
Hexachlorocyclopentadiene <252 ug/kg 05/15/23 14:20 77-47-405/12/23 14:174392521
Hexachloroethane <168 ug/kg 05/15/23 14:20 67-72-105/12/23 14:174391681
Indeno(1,2,3-cd)pyrene <173 ug/kg 05/15/23 14:20 193-39-505/12/23 14:174391731
Isophorone <196 ug/kg 05/15/23 14:20 78-59-105/12/23 14:174391961
1-Methylnaphthalene <154 ug/kg 05/15/23 14:20 90-12-005/12/23 14:174391541
2-Methylnaphthalene <176 ug/kg 05/15/23 14:20 91-57-605/12/23 14:174391761
2-Methylphenol(o-Cresol)<180 ug/kg 05/15/23 14:20 95-48-705/12/23 14:174391801
3&4-Methylphenol(m&p Cresol)<177 ug/kg 05/15/23 14:20 15831-10-405/12/23 14:174391771
Naphthalene <149 ug/kg 05/15/23 14:20 91-20-305/12/23 14:174391491
2-Nitroaniline <360 ug/kg 05/15/23 14:20 88-74-405/12/23 14:1722003601
3-Nitroaniline <345 ug/kg 05/15/23 14:20 99-09-205/12/23 14:1722003451
4-Nitroaniline <334 ug/kg 05/15/23 14:20 100-01-605/12/23 14:178793341
Nitrobenzene <204 ug/kg 05/15/23 14:20 98-95-305/12/23 14:174392041
2-Nitrophenol <190 ug/kg 05/15/23 14:20 88-75-505/12/23 14:174391901
4-Nitrophenol <850 ug/kg 05/15/23 14:20 100-02-705/12/23 14:1722008501
N-Nitrosodimethylamine <148 ug/kg 05/15/23 14:20 62-75-905/12/23 14:174391481
N-Nitroso-di-n-propylamine <165 ug/kg 05/15/23 14:20 621-64-705/12/23 14:174391651
N-Nitrosodiphenylamine <156 ug/kg 05/15/23 14:20 86-30-605/12/23 14:174391561
2,2'-Oxybis(1-chloropropane)<209 ug/kg 05/15/23 14:20 108-60-105/12/23 14:174392091
Pentachlorophenol <430 ug/kg 05/15/23 14:20 87-86-505/12/23 14:178794301
Phenanthrene <144 ug/kg 05/15/23 14:20 85-01-805/12/23 14:174391441
Phenol <196 ug/kg 05/15/23 14:20 108-95-205/12/23 14:174391961
Pyrene <178 ug/kg 05/15/23 14:20 129-00-005/12/23 14:174391781
Pyridine <139 ug/kg 05/15/23 14:20 110-86-105/12/23 14:174391391
1,2,4-Trichlorobenzene <173 ug/kg 05/15/23 14:20 120-82-105/12/23 14:174391731
2,4,5-Trichlorophenol <201 ug/kg 05/15/23 14:20 95-95-405/12/23 14:174392011
2,4,6-Trichlorophenol <181 ug/kg 05/15/23 14:20 88-06-205/12/23 14:174391811
Surrogates
Nitrobenzene-d5 (S)26 %05/15/23 14:20 4165-60-005/12/23 14:1710-130 1
2-Fluorobiphenyl (S)22 %05/15/23 14:20 321-60-805/12/23 14:1710-130 1
Terphenyl-d14 (S)35 %05/15/23 14:20 1718-51-005/12/23 14:1710-130 1
Phenol-d6 (S)21 %05/15/23 14:20 13127-88-305/12/23 14:1710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-6 (0-2)Lab ID:92667059003 Collected:05/09/23 13:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)22 %05/15/23 14:20 367-12-405/12/23 14:1710-130 1
2,4,6-Tribromophenol (S)33 %05/15/23 14:20 118-79-605/12/23 14:1710-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.9 %05/11/23 16:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.9 %05/15/23 14:1605/15/23 14:071
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.13J mg/kg 05/17/23 17:42 18540-29-9 J05/17/23 07:121.37 0.350 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-7 (0-2)Lab ID:92667059004 Collected:05/09/23 14:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.6 mg/kg 05/17/23 14:04 7440-38-205/17/23 07:110.59 0.17 1
Barium 145 mg/kg 05/17/23 14:04 7440-39-305/17/23 07:110.35 0.088 1
Cadmium 0.24 mg/kg 05/17/23 14:04 7440-43-905/17/23 07:110.094 0.034 1
Chromium 35.2 mg/kg 05/17/23 14:04 7440-47-305/17/23 07:112.3 0.46 1
Lead 37.4 mg/kg 05/17/23 14:04 7439-92-105/17/23 07:110.59 0.11 1
Selenium 0.42J mg/kg 05/17/23 14:04 7782-49-205/17/23 07:110.59 0.12 1
Silver <0.24 mg/kg 05/17/23 14:04 7440-22-405/17/23 07:110.59 0.24 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.017J mg/kg 05/17/23 16:44 7439-97-605/17/23 07:410.021 0.0091 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <142 ug/kg 05/15/23 14:48 83-32-905/12/23 14:174041421
Acenaphthylene <142 ug/kg 05/15/23 14:48 208-96-805/12/23 14:174041421
Aniline <158 ug/kg 05/15/23 14:48 62-53-305/12/23 14:174041581
Anthracene <132 ug/kg 05/15/23 14:48 120-12-705/12/23 14:174041321
Benzo(a)anthracene <135 ug/kg 05/15/23 14:48 56-55-305/12/23 14:174041351
Benzo(a)pyrene <140 ug/kg 05/15/23 14:48 50-32-805/12/23 14:174041401
Benzo(b)fluoranthene <135 ug/kg 05/15/23 14:48 205-99-205/12/23 14:174041351
Benzo(g,h,i)perylene <157 ug/kg 05/15/23 14:48 191-24-205/12/23 14:174041571
Benzo(k)fluoranthene <142 ug/kg 05/15/23 14:48 207-08-905/12/23 14:174041421
Benzoic Acid <869 ug/kg 05/15/23 14:48 65-85-005/12/23 14:1720208691
Benzyl alcohol <306 ug/kg 05/15/23 14:48 100-51-605/12/23 14:178083061
4-Bromophenylphenyl ether <156 ug/kg 05/15/23 14:48 101-55-305/12/23 14:174041561
Butylbenzylphthalate <170 ug/kg 05/15/23 14:48 85-68-705/12/23 14:174041701
4-Chloro-3-methylphenol <284 ug/kg 05/15/23 14:48 59-50-705/12/23 14:178082841
4-Chloroaniline <317 ug/kg 05/15/23 14:48 106-47-805/12/23 14:178083171
bis(2-Chloroethoxy)methane <168 ug/kg 05/15/23 14:48 111-91-105/12/23 14:174041681
bis(2-Chloroethyl) ether <152 ug/kg 05/15/23 14:48 111-44-405/12/23 14:174041521
2-Chloronaphthalene <160 ug/kg 05/15/23 14:48 91-58-705/12/23 14:174041601
2-Chlorophenol <152 ug/kg 05/15/23 14:48 95-57-805/12/23 14:174041521
4-Chlorophenylphenyl ether <151 ug/kg 05/15/23 14:48 7005-72-305/12/23 14:174041511
Chrysene <147 ug/kg 05/15/23 14:48 218-01-905/12/23 14:174041471
Dibenz(a,h)anthracene <156 ug/kg 05/15/23 14:48 53-70-305/12/23 14:174041561
Dibenzofuran <146 ug/kg 05/15/23 14:48 132-64-905/12/23 14:174041461
1,2-Dichlorobenzene <146 ug/kg 05/15/23 14:48 95-50-105/12/23 14:174041461
1,3-Dichlorobenzene <143 ug/kg 05/15/23 14:48 541-73-105/12/23 14:174041431
1,4-Dichlorobenzene <154 ug/kg 05/15/23 14:48 106-46-705/12/23 14:174041541
3,3'-Dichlorobenzidine <273 ug/kg 05/15/23 14:48 91-94-105/12/23 14:178082731
2,4-Dichlorophenol <158 ug/kg 05/15/23 14:48 120-83-205/12/23 14:174041581
Diethylphthalate <148 ug/kg 05/15/23 14:48 84-66-205/12/23 14:174041481
2,4-Dimethylphenol <168 ug/kg 05/15/23 14:48 105-67-905/12/23 14:174041681
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-7 (0-2)Lab ID:92667059004 Collected:05/09/23 14:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <147 ug/kg 05/15/23 14:48 131-11-305/12/23 14:174041471
Di-n-butylphthalate <136 ug/kg 05/15/23 14:48 84-74-205/12/23 14:174041361
4,6-Dinitro-2-methylphenol <377 ug/kg 05/15/23 14:48 534-52-105/12/23 14:178083771
2,4-Dinitrophenol <1250 ug/kg 05/15/23 14:48 51-28-505/12/23 14:17202012501
2,4-Dinitrotoluene <156 ug/kg 05/15/23 14:48 121-14-205/12/23 14:174041561
2,6-Dinitrotoluene <148 ug/kg 05/15/23 14:48 606-20-205/12/23 14:174041481
Di-n-octylphthalate <159 ug/kg 05/15/23 14:48 117-84-005/12/23 14:174041591
bis(2-Ethylhexyl)phthalate <157 ug/kg 05/15/23 14:48 117-81-705/12/23 14:174041571
Fluoranthene <138 ug/kg 05/15/23 14:48 206-44-005/12/23 14:174041381
Fluorene <142 ug/kg 05/15/23 14:48 86-73-705/12/23 14:174041421
Hexachloro-1,3-butadiene <175 ug/kg 05/15/23 14:48 87-68-305/12/23 14:174041751
Hexachlorobenzene <158 ug/kg 05/15/23 14:48 118-74-105/12/23 14:174041581
Hexachlorocyclopentadiene <232 ug/kg 05/15/23 14:48 77-47-405/12/23 14:174042321
Hexachloroethane <154 ug/kg 05/15/23 14:48 67-72-105/12/23 14:174041541
Indeno(1,2,3-cd)pyrene <159 ug/kg 05/15/23 14:48 193-39-505/12/23 14:174041591
Isophorone <180 ug/kg 05/15/23 14:48 78-59-105/12/23 14:174041801
1-Methylnaphthalene <142 ug/kg 05/15/23 14:48 90-12-005/12/23 14:174041421
2-Methylnaphthalene <162 ug/kg 05/15/23 14:48 91-57-605/12/23 14:174041621
2-Methylphenol(o-Cresol)<165 ug/kg 05/15/23 14:48 95-48-705/12/23 14:174041651
3&4-Methylphenol(m&p Cresol)<163 ug/kg 05/15/23 14:48 15831-10-405/12/23 14:174041631
Naphthalene <137 ug/kg 05/15/23 14:48 91-20-305/12/23 14:174041371
2-Nitroaniline <331 ug/kg 05/15/23 14:48 88-74-405/12/23 14:1720203311
3-Nitroaniline <317 ug/kg 05/15/23 14:48 99-09-205/12/23 14:1720203171
4-Nitroaniline <307 ug/kg 05/15/23 14:48 100-01-605/12/23 14:178083071
Nitrobenzene <187 ug/kg 05/15/23 14:48 98-95-305/12/23 14:174041871
2-Nitrophenol <175 ug/kg 05/15/23 14:48 88-75-505/12/23 14:174041751
4-Nitrophenol <782 ug/kg 05/15/23 14:48 100-02-705/12/23 14:1720207821
N-Nitrosodimethylamine <136 ug/kg 05/15/23 14:48 62-75-905/12/23 14:174041361
N-Nitroso-di-n-propylamine <152 ug/kg 05/15/23 14:48 621-64-705/12/23 14:174041521
N-Nitrosodiphenylamine <143 ug/kg 05/15/23 14:48 86-30-605/12/23 14:174041431
2,2'-Oxybis(1-chloropropane)<192 ug/kg 05/15/23 14:48 108-60-105/12/23 14:174041921
Pentachlorophenol <396 ug/kg 05/15/23 14:48 87-86-505/12/23 14:178083961
Phenanthrene <132 ug/kg 05/15/23 14:48 85-01-805/12/23 14:174041321
Phenol <180 ug/kg 05/15/23 14:48 108-95-205/12/23 14:174041801
Pyrene <164 ug/kg 05/15/23 14:48 129-00-005/12/23 14:174041641
Pyridine <127 ug/kg 05/15/23 14:48 110-86-105/12/23 14:174041271
1,2,4-Trichlorobenzene <159 ug/kg 05/15/23 14:48 120-82-105/12/23 14:174041591
2,4,5-Trichlorophenol <185 ug/kg 05/15/23 14:48 95-95-405/12/23 14:174041851
2,4,6-Trichlorophenol <167 ug/kg 05/15/23 14:48 88-06-205/12/23 14:174041671
Surrogates
Nitrobenzene-d5 (S)43 %05/15/23 14:48 4165-60-005/12/23 14:1710-130 1
2-Fluorobiphenyl (S)46 %05/15/23 14:48 321-60-805/12/23 14:1710-130 1
Terphenyl-d14 (S)47 %05/15/23 14:48 1718-51-005/12/23 14:1710-130 1
Phenol-d6 (S)36 %05/15/23 14:48 13127-88-305/12/23 14:1710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-7 (0-2)Lab ID:92667059004 Collected:05/09/23 14:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)33 %05/15/23 14:48 367-12-405/12/23 14:1710-130 1
2,4,6-Tribromophenol (S)44 %05/15/23 14:48 118-79-605/12/23 14:1710-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.0 %05/11/23 16:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 83.3 %05/15/23 14:1605/15/23 14:071
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.450J mg/kg 05/17/23 17:47 18540-29-9 J05/17/23 07:121.20 0.306 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-DUP-230509 (0-2)Lab ID:92667059005 Collected:05/09/23 00:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.7 mg/kg 05/17/23 14:13 7440-38-205/17/23 07:110.57 0.16 1
Barium 123 mg/kg 05/17/23 14:13 7440-39-305/17/23 07:110.34 0.085 1
Cadmium 0.074J mg/kg 05/17/23 14:13 7440-43-905/17/23 07:110.091 0.033 1
Chromium 41.0 mg/kg 05/17/23 14:13 7440-47-305/17/23 07:112.3 0.44 1
Lead 12.5 mg/kg 05/17/23 14:13 7439-92-105/17/23 07:110.57 0.11 1
Selenium 0.40J mg/kg 05/17/23 14:13 7782-49-205/17/23 07:110.57 0.12 1
Silver <0.23 mg/kg 05/17/23 14:13 7440-22-405/17/23 07:110.57 0.23 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.025 mg/kg 05/17/23 16:45 7439-97-605/17/23 07:410.022 0.0095 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <142 ug/kg 05/15/23 15:16 83-32-905/12/23 14:174041421
Acenaphthylene <142 ug/kg 05/15/23 15:16 208-96-805/12/23 14:174041421
Aniline <158 ug/kg 05/15/23 15:16 62-53-305/12/23 14:174041581
Anthracene <132 ug/kg 05/15/23 15:16 120-12-705/12/23 14:174041321
Benzo(a)anthracene <135 ug/kg 05/15/23 15:16 56-55-305/12/23 14:174041351
Benzo(a)pyrene <139 ug/kg 05/15/23 15:16 50-32-805/12/23 14:174041391
Benzo(b)fluoranthene <135 ug/kg 05/15/23 15:16 205-99-205/12/23 14:174041351
Benzo(g,h,i)perylene <157 ug/kg 05/15/23 15:16 191-24-205/12/23 14:174041571
Benzo(k)fluoranthene <142 ug/kg 05/15/23 15:16 207-08-905/12/23 14:174041421
Benzoic Acid <867 ug/kg 05/15/23 15:16 65-85-005/12/23 14:1720208671
Benzyl alcohol <306 ug/kg 05/15/23 15:16 100-51-605/12/23 14:178073061
4-Bromophenylphenyl ether <155 ug/kg 05/15/23 15:16 101-55-305/12/23 14:174041551
Butylbenzylphthalate <170 ug/kg 05/15/23 15:16 85-68-705/12/23 14:174041701
4-Chloro-3-methylphenol <284 ug/kg 05/15/23 15:16 59-50-705/12/23 14:178072841
4-Chloroaniline <317 ug/kg 05/15/23 15:16 106-47-805/12/23 14:178073171
bis(2-Chloroethoxy)methane <168 ug/kg 05/15/23 15:16 111-91-105/12/23 14:174041681
bis(2-Chloroethyl) ether <152 ug/kg 05/15/23 15:16 111-44-405/12/23 14:174041521
2-Chloronaphthalene <160 ug/kg 05/15/23 15:16 91-58-705/12/23 14:174041601
2-Chlorophenol <152 ug/kg 05/15/23 15:16 95-57-805/12/23 14:174041521
4-Chlorophenylphenyl ether <150 ug/kg 05/15/23 15:16 7005-72-305/12/23 14:174041501
Chrysene <147 ug/kg 05/15/23 15:16 218-01-905/12/23 14:174041471
Dibenz(a,h)anthracene <155 ug/kg 05/15/23 15:16 53-70-305/12/23 14:174041551
Dibenzofuran <146 ug/kg 05/15/23 15:16 132-64-905/12/23 14:174041461
1,2-Dichlorobenzene <146 ug/kg 05/15/23 15:16 95-50-105/12/23 14:174041461
1,3-Dichlorobenzene <143 ug/kg 05/15/23 15:16 541-73-105/12/23 14:174041431
1,4-Dichlorobenzene <154 ug/kg 05/15/23 15:16 106-46-705/12/23 14:174041541
3,3'-Dichlorobenzidine <273 ug/kg 05/15/23 15:16 91-94-105/12/23 14:178072731
2,4-Dichlorophenol <158 ug/kg 05/15/23 15:16 120-83-205/12/23 14:174041581
Diethylphthalate <148 ug/kg 05/15/23 15:16 84-66-205/12/23 14:174041481
2,4-Dimethylphenol <168 ug/kg 05/15/23 15:16 105-67-905/12/23 14:174041681
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-DUP-230509 (0-2)Lab ID:92667059005 Collected:05/09/23 00:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <147 ug/kg 05/15/23 15:16 131-11-305/12/23 14:174041471
Di-n-butylphthalate <136 ug/kg 05/15/23 15:16 84-74-205/12/23 14:174041361
4,6-Dinitro-2-methylphenol <377 ug/kg 05/15/23 15:16 534-52-105/12/23 14:178073771
2,4-Dinitrophenol <1250 ug/kg 05/15/23 15:16 51-28-505/12/23 14:17202012501
2,4-Dinitrotoluene <155 ug/kg 05/15/23 15:16 121-14-205/12/23 14:174041551
2,6-Dinitrotoluene <148 ug/kg 05/15/23 15:16 606-20-205/12/23 14:174041481
Di-n-octylphthalate <159 ug/kg 05/15/23 15:16 117-84-005/12/23 14:174041591
bis(2-Ethylhexyl)phthalate <157 ug/kg 05/15/23 15:16 117-81-705/12/23 14:174041571
Fluoranthene <138 ug/kg 05/15/23 15:16 206-44-005/12/23 14:174041381
Fluorene <142 ug/kg 05/15/23 15:16 86-73-705/12/23 14:174041421
Hexachloro-1,3-butadiene <175 ug/kg 05/15/23 15:16 87-68-305/12/23 14:174041751
Hexachlorobenzene <158 ug/kg 05/15/23 15:16 118-74-105/12/23 14:174041581
Hexachlorocyclopentadiene <231 ug/kg 05/15/23 15:16 77-47-405/12/23 14:174042311
Hexachloroethane <154 ug/kg 05/15/23 15:16 67-72-105/12/23 14:174041541
Indeno(1,2,3-cd)pyrene <159 ug/kg 05/15/23 15:16 193-39-505/12/23 14:174041591
Isophorone <180 ug/kg 05/15/23 15:16 78-59-105/12/23 14:174041801
1-Methylnaphthalene <142 ug/kg 05/15/23 15:16 90-12-005/12/23 14:174041421
2-Methylnaphthalene <161 ug/kg 05/15/23 15:16 91-57-605/12/23 14:174041611
2-Methylphenol(o-Cresol)<165 ug/kg 05/15/23 15:16 95-48-705/12/23 14:174041651
3&4-Methylphenol(m&p Cresol)<163 ug/kg 05/15/23 15:16 15831-10-405/12/23 14:174041631
Naphthalene <137 ug/kg 05/15/23 15:16 91-20-305/12/23 14:174041371
2-Nitroaniline <330 ug/kg 05/15/23 15:16 88-74-405/12/23 14:1720203301
3-Nitroaniline <317 ug/kg 05/15/23 15:16 99-09-205/12/23 14:1720203171
4-Nitroaniline <307 ug/kg 05/15/23 15:16 100-01-605/12/23 14:178073071
Nitrobenzene <187 ug/kg 05/15/23 15:16 98-95-305/12/23 14:174041871
2-Nitrophenol <175 ug/kg 05/15/23 15:16 88-75-505/12/23 14:174041751
4-Nitrophenol <781 ug/kg 05/15/23 15:16 100-02-705/12/23 14:1720207811
N-Nitrosodimethylamine <136 ug/kg 05/15/23 15:16 62-75-905/12/23 14:174041361
N-Nitroso-di-n-propylamine <152 ug/kg 05/15/23 15:16 621-64-705/12/23 14:174041521
N-Nitrosodiphenylamine <143 ug/kg 05/15/23 15:16 86-30-605/12/23 14:174041431
2,2'-Oxybis(1-chloropropane)<192 ug/kg 05/15/23 15:16 108-60-105/12/23 14:174041921
Pentachlorophenol <395 ug/kg 05/15/23 15:16 87-86-505/12/23 14:178073951
Phenanthrene <132 ug/kg 05/15/23 15:16 85-01-805/12/23 14:174041321
Phenol <180 ug/kg 05/15/23 15:16 108-95-205/12/23 14:174041801
Pyrene <164 ug/kg 05/15/23 15:16 129-00-005/12/23 14:174041641
Pyridine <127 ug/kg 05/15/23 15:16 110-86-105/12/23 14:174041271
1,2,4-Trichlorobenzene <159 ug/kg 05/15/23 15:16 120-82-105/12/23 14:174041591
2,4,5-Trichlorophenol <185 ug/kg 05/15/23 15:16 95-95-405/12/23 14:174041851
2,4,6-Trichlorophenol <166 ug/kg 05/15/23 15:16 88-06-205/12/23 14:174041661
Surrogates
Nitrobenzene-d5 (S)39 %05/15/23 15:16 4165-60-005/12/23 14:1710-130 1
2-Fluorobiphenyl (S)42 %05/15/23 15:16 321-60-805/12/23 14:1710-130 1
Terphenyl-d14 (S)44 %05/15/23 15:16 1718-51-005/12/23 14:1710-130 1
Phenol-d6 (S)34 %05/15/23 15:16 13127-88-305/12/23 14:1710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-DUP-230509 (0-2)Lab ID:92667059005 Collected:05/09/23 00:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)34 %05/15/23 15:16 367-12-405/12/23 14:1710-130 1
2,4,6-Tribromophenol (S)44 %05/15/23 15:16 118-79-605/12/23 14:1710-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.9 %05/11/23 16:27 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 83.1 %05/15/23 14:1605/15/23 14:071
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.574J mg/kg 05/17/23 17:52 18540-29-9 J05/17/23 07:121.20 0.307 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-4 (1-2)Lab ID:92667059006 Collected:05/09/23 11:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <38.4 ug/kg 05/12/23 22:43 67-64-105/11/23 20:2712038.4 1
Benzene <2.4 ug/kg 05/12/23 22:43 71-43-205/11/23 20:276.0 2.4 1
Bromobenzene <1.9 ug/kg 05/12/23 22:43 108-86-105/11/23 20:276.0 1.9 1
Bromochloromethane <1.8 ug/kg 05/12/23 22:43 74-97-505/11/23 20:276.0 1.8 1
Bromodichloromethane <2.3 ug/kg 05/12/23 22:43 75-27-405/11/23 20:276.0 2.3 1
Bromoform <2.1 ug/kg 05/12/23 22:43 75-25-205/11/23 20:276.0 2.1 1
Bromomethane <18.5 ug/kg 05/12/23 22:43 74-83-905/11/23 20:2723.9 18.5 1
2-Butanone (MEK)<28.7 ug/kg 05/12/23 22:43 78-93-305/11/23 20:2712028.7 1
n-Butylbenzene <3.8 ug/kg 05/12/23 22:43 104-51-805/11/23 20:276.0 3.8 1
sec-Butylbenzene <2.6 ug/kg 05/12/23 22:43 135-98-805/11/23 20:276.0 2.6 1
tert-Butylbenzene <2.1 ug/kg 05/12/23 22:43 98-06-605/11/23 20:276.0 2.1 1
Carbon tetrachloride <2.2 ug/kg 05/12/23 22:43 56-23-505/11/23 20:276.0 2.2 1
Chlorobenzene 130 ug/kg 05/12/23 22:43 108-90-705/11/23 20:276.0 3.4 1
Chloroethane <4.6 ug/kg 05/12/23 22:43 75-00-305/11/23 20:2712.0 4.6 1
Chloroform <5.0 ug/kg 05/12/23 22:43 67-66-305/11/23 20:276.0 5.0 1
Chloromethane <5.0 ug/kg 05/12/23 22:43 74-87-305/11/23 20:2712.0 5.0 1
2-Chlorotoluene <2.1 ug/kg 05/12/23 22:43 95-49-805/11/23 20:276.0 2.1 1
4-Chlorotoluene <3.3 ug/kg 05/12/23 22:43 106-43-405/11/23 20:276.0 3.3 1
1,2-Dibromo-3-chloropropane <2.3 ug/kg 05/12/23 22:43 96-12-805/11/23 20:276.0 2.3 1
Dibromochloromethane <3.4 ug/kg 05/12/23 22:43 124-48-105/11/23 20:276.0 3.4 1
1,2-Dibromoethane (EDB)<2.6 ug/kg 05/12/23 22:43 106-93-405/11/23 20:276.0 2.6 1
Dibromomethane <1.3 ug/kg 05/12/23 22:43 74-95-305/11/23 20:276.0 1.3 1
1,2-Dichlorobenzene <2.2 ug/kg 05/12/23 22:43 95-50-105/11/23 20:276.0 2.2 1
1,3-Dichlorobenzene <1.9 ug/kg 05/12/23 22:43 541-73-105/11/23 20:276.0 1.9 1
1,4-Dichlorobenzene <1.6 ug/kg 05/12/23 22:43 106-46-705/11/23 20:276.0 1.6 1
Dichlorodifluoromethane <6.1 ug/kg 05/12/23 22:43 75-71-8 IH05/11/23 20:2712.0 6.1 1
1,1-Dichloroethane <2.5 ug/kg 05/12/23 22:43 75-34-305/11/23 20:276.0 2.5 1
1,2-Dichloroethane <4.0 ug/kg 05/12/23 22:43 107-06-205/11/23 20:276.0 4.0 1
1,1-Dichloroethene <2.5 ug/kg 05/12/23 22:43 75-35-405/11/23 20:276.0 2.5 1
cis-1,2-Dichloroethene <2.0 ug/kg 05/12/23 22:43 156-59-205/11/23 20:276.0 2.0 1
trans-1,2-Dichloroethene <5.1 ug/kg 05/12/23 22:43 156-60-505/11/23 20:276.0 5.1 1
1,2-Dichloropropane <1.8 ug/kg 05/12/23 22:43 78-87-505/11/23 20:276.0 1.8 1
1,3-Dichloropropane <1.9 ug/kg 05/12/23 22:43 142-28-905/11/23 20:276.0 1.9 1
2,2-Dichloropropane <4.5 ug/kg 05/12/23 22:43 594-20-7 v205/11/23 20:276.0 4.5 1
1,1-Dichloropropene <2.9 ug/kg 05/12/23 22:43 563-58-605/11/23 20:276.0 2.9 1
cis-1,3-Dichloropropene <1.6 ug/kg 05/12/23 22:43 10061-01-505/11/23 20:276.0 1.6 1
trans-1,3-Dichloropropene <2.1 ug/kg 05/12/23 22:43 10061-02-605/11/23 20:276.0 2.1 1
Diisopropyl ether <1.6 ug/kg 05/12/23 22:43 108-20-305/11/23 20:276.0 1.6 1
Ethylbenzene <2.8 ug/kg 05/12/23 22:43 100-41-405/11/23 20:276.0 2.8 1
Hexachloro-1,3-butadiene <9.8 ug/kg 05/12/23 22:43 87-68-305/11/23 20:2712.0 9.8 1
2-Hexanone <5.8 ug/kg 05/12/23 22:43 591-78-605/11/23 20:2759.8 5.8 1
Isopropylbenzene (Cumene)<2.0 ug/kg 05/12/23 22:43 98-82-805/11/23 20:276.0 2.0 1
p-Isopropyltoluene <2.9 ug/kg 05/12/23 22:43 99-87-605/11/23 20:276.0 2.9 1
Methylene Chloride <16.4 ug/kg 05/12/23 22:43 75-09-205/11/23 20:2723.9 16.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-4 (1-2)Lab ID:92667059006 Collected:05/09/23 11:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<5.8 ug/kg 05/12/23 22:43 108-10-105/11/23 20:2759.8 5.8 1
Methyl-tert-butyl ether <2.2 ug/kg 05/12/23 22:43 1634-04-405/11/23 20:276.0 2.2 1
Naphthalene <3.1 ug/kg 05/12/23 22:43 91-20-305/11/23 20:276.0 3.1 1
n-Propylbenzene <2.1 ug/kg 05/12/23 22:43 103-65-105/11/23 20:276.0 2.1 1
Styrene <1.6 ug/kg 05/12/23 22:43 100-42-505/11/23 20:276.0 1.6 1
1,1,1,2-Tetrachloroethane <2.3 ug/kg 05/12/23 22:43 630-20-605/11/23 20:276.0 2.3 1
1,1,2,2-Tetrachloroethane <1.6 ug/kg 05/12/23 22:43 79-34-505/11/23 20:276.0 1.6 1
Tetrachloroethene <1.9 ug/kg 05/12/23 22:43 127-18-405/11/23 20:276.0 1.9 1
Toluene <4.1 ug/kg 05/12/23 22:43 108-88-305/11/23 20:276.0 4.1 1
1,2,3-Trichlorobenzene <4.8 ug/kg 05/12/23 22:43 87-61-605/11/23 20:276.0 4.8 1
1,2,4-Trichlorobenzene <5.0 ug/kg 05/12/23 22:43 120-82-105/11/23 20:276.0 5.0 1
1,1,1-Trichloroethane <3.1 ug/kg 05/12/23 22:43 71-55-605/11/23 20:276.0 3.1 1
1,1,2-Trichloroethane <2.0 ug/kg 05/12/23 22:43 79-00-505/11/23 20:276.0 2.0 1
Trichloroethene <4.8 ug/kg 05/12/23 22:43 79-01-605/11/23 20:276.0 4.8 1
Trichlorofluoromethane <3.3 ug/kg 05/12/23 22:43 75-69-405/11/23 20:276.0 3.3 1
1,2,3-Trichloropropane <3.0 ug/kg 05/12/23 22:43 96-18-405/11/23 20:276.0 3.0 1
1,2,4-Trimethylbenzene <3.6 ug/kg 05/12/23 22:43 95-63-605/11/23 20:276.0 3.6 1
1,3,5-Trimethylbenzene <2.0 ug/kg 05/12/23 22:43 108-67-805/11/23 20:276.0 2.0 1
Vinyl acetate <12.3 ug/kg 05/12/23 22:43 108-05-405/11/23 20:2759.8 12.3 1
Vinyl chloride <3.0 ug/kg 05/12/23 22:43 75-01-405/11/23 20:2712.0 3.0 1
Xylene (Total)<3.4 ug/kg 05/12/23 22:43 1330-20-705/11/23 20:2712.0 3.4 1
m&p-Xylene <4.1 ug/kg 05/12/23 22:43 179601-23-105/11/23 20:2712.0 4.1 1
o-Xylene <2.6 ug/kg 05/12/23 22:43 95-47-605/11/23 20:276.0 2.6 1
Surrogates
Toluene-d8 (S)101 %05/12/23 22:43 2037-26-505/11/23 20:2770-130 1
4-Bromofluorobenzene (S)101 %05/12/23 22:43 460-00-405/11/23 20:2770-130 1
1,2-Dichloroethane-d4 (S)100 %05/12/23 22:43 17060-07-005/11/23 20:2770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.2 %05/11/23 16:27 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-5 (1-2)Lab ID:92667059007 Collected:05/09/23 12:20 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <47.5 ug/kg 05/12/23 23:02 67-64-105/11/23 20:2714847.5 1
Benzene <2.9 ug/kg 05/12/23 23:02 71-43-205/11/23 20:277.4 2.9 1
Bromobenzene <2.4 ug/kg 05/12/23 23:02 108-86-105/11/23 20:277.4 2.4 1
Bromochloromethane <2.2 ug/kg 05/12/23 23:02 74-97-505/11/23 20:277.4 2.2 1
Bromodichloromethane <2.9 ug/kg 05/12/23 23:02 75-27-405/11/23 20:277.4 2.9 1
Bromoform <2.6 ug/kg 05/12/23 23:02 75-25-205/11/23 20:277.4 2.6 1
Bromomethane <23.0 ug/kg 05/12/23 23:02 74-83-905/11/23 20:2729.6 23.0 1
2-Butanone (MEK)<35.5 ug/kg 05/12/23 23:02 78-93-305/11/23 20:2714835.5 1
n-Butylbenzene <4.7 ug/kg 05/12/23 23:02 104-51-805/11/23 20:277.4 4.7 1
sec-Butylbenzene <3.3 ug/kg 05/12/23 23:02 135-98-805/11/23 20:277.4 3.3 1
tert-Butylbenzene <2.6 ug/kg 05/12/23 23:02 98-06-605/11/23 20:277.4 2.6 1
Carbon tetrachloride <2.8 ug/kg 05/12/23 23:02 56-23-505/11/23 20:277.4 2.8 1
Chlorobenzene 140 ug/kg 05/12/23 23:02 108-90-705/11/23 20:277.4 4.3 1
Chloroethane <5.7 ug/kg 05/12/23 23:02 75-00-305/11/23 20:2714.8 5.7 1
Chloroform <6.2 ug/kg 05/12/23 23:02 67-66-305/11/23 20:277.4 6.2 1
Chloromethane <6.2 ug/kg 05/12/23 23:02 74-87-305/11/23 20:2714.8 6.2 1
2-Chlorotoluene <2.6 ug/kg 05/12/23 23:02 95-49-805/11/23 20:277.4 2.6 1
4-Chlorotoluene <4.1 ug/kg 05/12/23 23:02 106-43-405/11/23 20:277.4 4.1 1
1,2-Dibromo-3-chloropropane <2.9 ug/kg 05/12/23 23:02 96-12-805/11/23 20:277.4 2.9 1
Dibromochloromethane <4.2 ug/kg 05/12/23 23:02 124-48-105/11/23 20:277.4 4.2 1
1,2-Dibromoethane (EDB)<3.3 ug/kg 05/12/23 23:02 106-93-405/11/23 20:277.4 3.3 1
Dibromomethane <1.6 ug/kg 05/12/23 23:02 74-95-305/11/23 20:277.4 1.6 1
1,2-Dichlorobenzene <2.7 ug/kg 05/12/23 23:02 95-50-105/11/23 20:277.4 2.7 1
1,3-Dichlorobenzene <2.3 ug/kg 05/12/23 23:02 541-73-105/11/23 20:277.4 2.3 1
1,4-Dichlorobenzene <1.9 ug/kg 05/12/23 23:02 106-46-705/11/23 20:277.4 1.9 1
Dichlorodifluoromethane <7.5 ug/kg 05/12/23 23:02 75-71-8 IH05/11/23 20:2714.8 7.5 1
1,1-Dichloroethane <3.1 ug/kg 05/12/23 23:02 75-34-305/11/23 20:277.4 3.1 1
1,2-Dichloroethane <4.9 ug/kg 05/12/23 23:02 107-06-205/11/23 20:277.4 4.9 1
1,1-Dichloroethene <3.1 ug/kg 05/12/23 23:02 75-35-405/11/23 20:277.4 3.1 1
cis-1,2-Dichloroethene <2.5 ug/kg 05/12/23 23:02 156-59-205/11/23 20:277.4 2.5 1
trans-1,2-Dichloroethene <6.3 ug/kg 05/12/23 23:02 156-60-505/11/23 20:277.4 6.3 1
1,2-Dichloropropane <2.2 ug/kg 05/12/23 23:02 78-87-505/11/23 20:277.4 2.2 1
1,3-Dichloropropane <2.3 ug/kg 05/12/23 23:02 142-28-905/11/23 20:277.4 2.3 1
2,2-Dichloropropane <5.6 ug/kg 05/12/23 23:02 594-20-7 v2,v305/11/23 20:277.4 5.6 1
1,1-Dichloropropene <3.6 ug/kg 05/12/23 23:02 563-58-605/11/23 20:277.4 3.6 1
cis-1,3-Dichloropropene <2.0 ug/kg 05/12/23 23:02 10061-01-505/11/23 20:277.4 2.0 1
trans-1,3-Dichloropropene <2.5 ug/kg 05/12/23 23:02 10061-02-605/11/23 20:277.4 2.5 1
Diisopropyl ether <2.0 ug/kg 05/12/23 23:02 108-20-305/11/23 20:277.4 2.0 1
Ethylbenzene <3.5 ug/kg 05/12/23 23:02 100-41-405/11/23 20:277.4 3.5 1
Hexachloro-1,3-butadiene <12.1 ug/kg 05/12/23 23:02 87-68-305/11/23 20:2714.8 12.1 1
2-Hexanone <7.1 ug/kg 05/12/23 23:02 591-78-605/11/23 20:2774.0 7.1 1
Isopropylbenzene (Cumene)<2.5 ug/kg 05/12/23 23:02 98-82-805/11/23 20:277.4 2.5 1
p-Isopropyltoluene <3.6 ug/kg 05/12/23 23:02 99-87-605/11/23 20:277.4 3.6 1
Methylene Chloride <20.3 ug/kg 05/12/23 23:02 75-09-205/11/23 20:2729.6 20.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-5 (1-2)Lab ID:92667059007 Collected:05/09/23 12:20 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<7.1 ug/kg 05/12/23 23:02 108-10-105/11/23 20:2774.0 7.1 1
Methyl-tert-butyl ether <2.8 ug/kg 05/12/23 23:02 1634-04-405/11/23 20:277.4 2.8 1
Naphthalene <3.9 ug/kg 05/12/23 23:02 91-20-305/11/23 20:277.4 3.9 1
n-Propylbenzene <2.6 ug/kg 05/12/23 23:02 103-65-105/11/23 20:277.4 2.6 1
Styrene <2.0 ug/kg 05/12/23 23:02 100-42-505/11/23 20:277.4 2.0 1
1,1,1,2-Tetrachloroethane <2.8 ug/kg 05/12/23 23:02 630-20-605/11/23 20:277.4 2.8 1
1,1,2,2-Tetrachloroethane <2.0 ug/kg 05/12/23 23:02 79-34-505/11/23 20:277.4 2.0 1
Tetrachloroethene <2.3 ug/kg 05/12/23 23:02 127-18-405/11/23 20:277.4 2.3 1
Toluene <5.1 ug/kg 05/12/23 23:02 108-88-305/11/23 20:277.4 5.1 1
1,2,3-Trichlorobenzene <6.0 ug/kg 05/12/23 23:02 87-61-605/11/23 20:277.4 6.0 1
1,2,4-Trichlorobenzene <6.2 ug/kg 05/12/23 23:02 120-82-105/11/23 20:277.4 6.2 1
1,1,1-Trichloroethane <3.9 ug/kg 05/12/23 23:02 71-55-605/11/23 20:277.4 3.9 1
1,1,2-Trichloroethane <2.5 ug/kg 05/12/23 23:02 79-00-505/11/23 20:277.4 2.5 1
Trichloroethene <6.0 ug/kg 05/12/23 23:02 79-01-605/11/23 20:277.4 6.0 1
Trichlorofluoromethane <4.1 ug/kg 05/12/23 23:02 75-69-405/11/23 20:277.4 4.1 1
1,2,3-Trichloropropane <3.7 ug/kg 05/12/23 23:02 96-18-405/11/23 20:277.4 3.7 1
1,2,4-Trimethylbenzene <4.4 ug/kg 05/12/23 23:02 95-63-605/11/23 20:277.4 4.4 1
1,3,5-Trimethylbenzene <2.5 ug/kg 05/12/23 23:02 108-67-805/11/23 20:277.4 2.5 1
Vinyl acetate <15.2 ug/kg 05/12/23 23:02 108-05-405/11/23 20:2774.0 15.2 1
Vinyl chloride <3.8 ug/kg 05/12/23 23:02 75-01-405/11/23 20:2714.8 3.8 1
Xylene (Total)<4.2 ug/kg 05/12/23 23:02 1330-20-705/11/23 20:2714.8 4.2 1
m&p-Xylene <5.1 ug/kg 05/12/23 23:02 179601-23-105/11/23 20:2714.8 5.1 1
o-Xylene <3.3 ug/kg 05/12/23 23:02 95-47-605/11/23 20:277.4 3.3 1
Surrogates
Toluene-d8 (S)100 %05/12/23 23:02 2037-26-505/11/23 20:2770-130 1
4-Bromofluorobenzene (S)102 %05/12/23 23:02 460-00-405/11/23 20:2770-130 1
1,2-Dichloroethane-d4 (S)100 %05/12/23 23:02 17060-07-005/11/23 20:2770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.5 %05/11/23 16:27 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-6 (1-2)Lab ID:92667059008 Collected:05/09/23 13:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 51.8J ug/kg 05/12/23 23:20 67-64-105/11/23 20:2714446.3 1
Benzene <2.9 ug/kg 05/12/23 23:20 71-43-205/11/23 20:277.2 2.9 1
Bromobenzene <2.3 ug/kg 05/12/23 23:20 108-86-105/11/23 20:277.2 2.3 1
Bromochloromethane <2.1 ug/kg 05/12/23 23:20 74-97-505/11/23 20:277.2 2.1 1
Bromodichloromethane <2.8 ug/kg 05/12/23 23:20 75-27-405/11/23 20:277.2 2.8 1
Bromoform <2.5 ug/kg 05/12/23 23:20 75-25-205/11/23 20:277.2 2.5 1
Bromomethane <22.3 ug/kg 05/12/23 23:20 74-83-905/11/23 20:2728.8 22.3 1
2-Butanone (MEK)<34.6 ug/kg 05/12/23 23:20 78-93-305/11/23 20:2714434.6 1
n-Butylbenzene <4.5 ug/kg 05/12/23 23:20 104-51-805/11/23 20:277.2 4.5 1
sec-Butylbenzene <3.2 ug/kg 05/12/23 23:20 135-98-805/11/23 20:277.2 3.2 1
tert-Butylbenzene <2.6 ug/kg 05/12/23 23:20 98-06-605/11/23 20:277.2 2.6 1
Carbon tetrachloride <2.7 ug/kg 05/12/23 23:20 56-23-505/11/23 20:277.2 2.7 1
Chlorobenzene <4.1 ug/kg 05/12/23 23:20 108-90-705/11/23 20:277.2 4.1 1
Chloroethane <5.6 ug/kg 05/12/23 23:20 75-00-305/11/23 20:2714.4 5.6 1
Chloroform <6.0 ug/kg 05/12/23 23:20 67-66-305/11/23 20:277.2 6.0 1
Chloromethane <6.1 ug/kg 05/12/23 23:20 74-87-305/11/23 20:2714.4 6.1 1
2-Chlorotoluene <2.6 ug/kg 05/12/23 23:20 95-49-805/11/23 20:277.2 2.6 1
4-Chlorotoluene <4.0 ug/kg 05/12/23 23:20 106-43-405/11/23 20:277.2 4.0 1
1,2-Dibromo-3-chloropropane <2.8 ug/kg 05/12/23 23:20 96-12-805/11/23 20:277.2 2.8 1
Dibromochloromethane <4.0 ug/kg 05/12/23 23:20 124-48-105/11/23 20:277.2 4.0 1
1,2-Dibromoethane (EDB)<3.2 ug/kg 05/12/23 23:20 106-93-405/11/23 20:277.2 3.2 1
Dibromomethane <1.5 ug/kg 05/12/23 23:20 74-95-305/11/23 20:277.2 1.5 1
1,2-Dichlorobenzene <2.6 ug/kg 05/12/23 23:20 95-50-105/11/23 20:277.2 2.6 1
1,3-Dichlorobenzene <2.2 ug/kg 05/12/23 23:20 541-73-105/11/23 20:277.2 2.2 1
1,4-Dichlorobenzene <1.9 ug/kg 05/12/23 23:20 106-46-705/11/23 20:277.2 1.9 1
Dichlorodifluoromethane <7.3 ug/kg 05/12/23 23:20 75-71-8 IH05/11/23 20:2714.4 7.3 1
1,1-Dichloroethane <3.0 ug/kg 05/12/23 23:20 75-34-305/11/23 20:277.2 3.0 1
1,2-Dichloroethane <4.8 ug/kg 05/12/23 23:20 107-06-205/11/23 20:277.2 4.8 1
1,1-Dichloroethene <3.0 ug/kg 05/12/23 23:20 75-35-405/11/23 20:277.2 3.0 1
cis-1,2-Dichloroethene <2.5 ug/kg 05/12/23 23:20 156-59-205/11/23 20:277.2 2.5 1
trans-1,2-Dichloroethene <6.1 ug/kg 05/12/23 23:20 156-60-505/11/23 20:277.2 6.1 1
1,2-Dichloropropane <2.2 ug/kg 05/12/23 23:20 78-87-505/11/23 20:277.2 2.2 1
1,3-Dichloropropane <2.2 ug/kg 05/12/23 23:20 142-28-905/11/23 20:277.2 2.2 1
2,2-Dichloropropane <5.5 ug/kg 05/12/23 23:20 594-20-7 v205/11/23 20:277.2 5.5 1
1,1-Dichloropropene <3.5 ug/kg 05/12/23 23:20 563-58-605/11/23 20:277.2 3.5 1
cis-1,3-Dichloropropene <2.0 ug/kg 05/12/23 23:20 10061-01-505/11/23 20:277.2 2.0 1
trans-1,3-Dichloropropene <2.5 ug/kg 05/12/23 23:20 10061-02-605/11/23 20:277.2 2.5 1
Diisopropyl ether <1.9 ug/kg 05/12/23 23:20 108-20-305/11/23 20:277.2 1.9 1
Ethylbenzene <3.4 ug/kg 05/12/23 23:20 100-41-405/11/23 20:277.2 3.4 1
Hexachloro-1,3-butadiene <11.8 ug/kg 05/12/23 23:20 87-68-305/11/23 20:2714.4 11.8 1
2-Hexanone <6.9 ug/kg 05/12/23 23:20 591-78-605/11/23 20:2772.0 6.9 1
Isopropylbenzene (Cumene)<2.4 ug/kg 05/12/23 23:20 98-82-805/11/23 20:277.2 2.4 1
p-Isopropyltoluene 59.3 ug/kg 05/12/23 23:20 99-87-605/11/23 20:277.2 3.5 1
Methylene Chloride <19.7 ug/kg 05/12/23 23:20 75-09-205/11/23 20:2728.8 19.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-6 (1-2)Lab ID:92667059008 Collected:05/09/23 13:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<6.9 ug/kg 05/12/23 23:20 108-10-105/11/23 20:2772.0 6.9 1
Methyl-tert-butyl ether <2.7 ug/kg 05/12/23 23:20 1634-04-405/11/23 20:277.2 2.7 1
Naphthalene <3.8 ug/kg 05/12/23 23:20 91-20-305/11/23 20:277.2 3.8 1
n-Propylbenzene <2.6 ug/kg 05/12/23 23:20 103-65-105/11/23 20:277.2 2.6 1
Styrene <1.9 ug/kg 05/12/23 23:20 100-42-505/11/23 20:277.2 1.9 1
1,1,1,2-Tetrachloroethane <2.8 ug/kg 05/12/23 23:20 630-20-605/11/23 20:277.2 2.8 1
1,1,2,2-Tetrachloroethane <1.9 ug/kg 05/12/23 23:20 79-34-505/11/23 20:277.2 1.9 1
Tetrachloroethene <2.3 ug/kg 05/12/23 23:20 127-18-405/11/23 20:277.2 2.3 1
Toluene <5.0 ug/kg 05/12/23 23:20 108-88-305/11/23 20:277.2 5.0 1
1,2,3-Trichlorobenzene <5.8 ug/kg 05/12/23 23:20 87-61-605/11/23 20:277.2 5.8 1
1,2,4-Trichlorobenzene <6.1 ug/kg 05/12/23 23:20 120-82-105/11/23 20:277.2 6.1 1
1,1,1-Trichloroethane <3.7 ug/kg 05/12/23 23:20 71-55-605/11/23 20:277.2 3.7 1
1,1,2-Trichloroethane <2.4 ug/kg 05/12/23 23:20 79-00-505/11/23 20:277.2 2.4 1
Trichloroethene <5.8 ug/kg 05/12/23 23:20 79-01-605/11/23 20:277.2 5.8 1
Trichlorofluoromethane <4.0 ug/kg 05/12/23 23:20 75-69-405/11/23 20:277.2 4.0 1
1,2,3-Trichloropropane <3.6 ug/kg 05/12/23 23:20 96-18-405/11/23 20:277.2 3.6 1
1,2,4-Trimethylbenzene <4.3 ug/kg 05/12/23 23:20 95-63-605/11/23 20:277.2 4.3 1
1,3,5-Trimethylbenzene <2.4 ug/kg 05/12/23 23:20 108-67-805/11/23 20:277.2 2.4 1
Vinyl acetate <14.8 ug/kg 05/12/23 23:20 108-05-405/11/23 20:2772.0 14.8 1
Vinyl chloride <3.7 ug/kg 05/12/23 23:20 75-01-405/11/23 20:2714.4 3.7 1
Xylene (Total)<4.1 ug/kg 05/12/23 23:20 1330-20-705/11/23 20:2714.4 4.1 1
m&p-Xylene <4.9 ug/kg 05/12/23 23:20 179601-23-105/11/23 20:2714.4 4.9 1
o-Xylene <3.2 ug/kg 05/12/23 23:20 95-47-605/11/23 20:277.2 3.2 1
Surrogates
Toluene-d8 (S)100 %05/12/23 23:20 2037-26-505/11/23 20:2770-130 1
4-Bromofluorobenzene (S)101 %05/12/23 23:20 460-00-405/11/23 20:2770-130 1
1,2-Dichloroethane-d4 (S)100 %05/12/23 23:20 17060-07-005/11/23 20:2770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.0 %05/11/23 16:27 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-7 (1-2)Lab ID:92667059009 Collected:05/09/23 14:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <48.1 ug/kg 05/12/23 23:57 67-64-105/11/23 20:2715048.1 1
Benzene <3.0 ug/kg 05/12/23 23:57 71-43-205/11/23 20:277.5 3.0 1
Bromobenzene <2.4 ug/kg 05/12/23 23:57 108-86-105/11/23 20:277.5 2.4 1
Bromochloromethane <2.2 ug/kg 05/12/23 23:57 74-97-505/11/23 20:277.5 2.2 1
Bromodichloromethane <2.9 ug/kg 05/12/23 23:57 75-27-405/11/23 20:277.5 2.9 1
Bromoform <2.6 ug/kg 05/12/23 23:57 75-25-205/11/23 20:277.5 2.6 1
Bromomethane <23.2 ug/kg 05/12/23 23:57 74-83-905/11/23 20:2730.0 23.2 1
2-Butanone (MEK)<36.0 ug/kg 05/12/23 23:57 78-93-305/11/23 20:2715036.0 1
n-Butylbenzene <4.7 ug/kg 05/12/23 23:57 104-51-805/11/23 20:277.5 4.7 1
sec-Butylbenzene <3.3 ug/kg 05/12/23 23:57 135-98-805/11/23 20:277.5 3.3 1
tert-Butylbenzene <2.7 ug/kg 05/12/23 23:57 98-06-605/11/23 20:277.5 2.7 1
Carbon tetrachloride <2.8 ug/kg 05/12/23 23:57 56-23-505/11/23 20:277.5 2.8 1
Chlorobenzene 57.8 ug/kg 05/12/23 23:57 108-90-705/11/23 20:277.5 4.3 1
Chloroethane <5.8 ug/kg 05/12/23 23:57 75-00-305/11/23 20:2715.0 5.8 1
Chloroform <6.3 ug/kg 05/12/23 23:57 67-66-305/11/23 20:277.5 6.3 1
Chloromethane <6.3 ug/kg 05/12/23 23:57 74-87-305/11/23 20:2715.0 6.3 1
2-Chlorotoluene <2.7 ug/kg 05/12/23 23:57 95-49-805/11/23 20:277.5 2.7 1
4-Chlorotoluene <4.2 ug/kg 05/12/23 23:57 106-43-405/11/23 20:277.5 4.2 1
1,2-Dibromo-3-chloropropane <2.9 ug/kg 05/12/23 23:57 96-12-805/11/23 20:277.5 2.9 1
Dibromochloromethane <4.2 ug/kg 05/12/23 23:57 124-48-105/11/23 20:277.5 4.2 1
1,2-Dibromoethane (EDB)<3.3 ug/kg 05/12/23 23:57 106-93-405/11/23 20:277.5 3.3 1
Dibromomethane <1.6 ug/kg 05/12/23 23:57 74-95-305/11/23 20:277.5 1.6 1
1,2-Dichlorobenzene <2.7 ug/kg 05/12/23 23:57 95-50-105/11/23 20:277.5 2.7 1
1,3-Dichlorobenzene <2.3 ug/kg 05/12/23 23:57 541-73-105/11/23 20:277.5 2.3 1
1,4-Dichlorobenzene <1.9 ug/kg 05/12/23 23:57 106-46-705/11/23 20:277.5 1.9 1
Dichlorodifluoromethane <7.6 ug/kg 05/12/23 23:57 75-71-8 IH05/11/23 20:2715.0 7.6 1
1,1-Dichloroethane <3.1 ug/kg 05/12/23 23:57 75-34-305/11/23 20:277.5 3.1 1
1,2-Dichloroethane <5.0 ug/kg 05/12/23 23:57 107-06-205/11/23 20:277.5 5.0 1
1,1-Dichloroethene <3.1 ug/kg 05/12/23 23:57 75-35-405/11/23 20:277.5 3.1 1
cis-1,2-Dichloroethene <2.6 ug/kg 05/12/23 23:57 156-59-205/11/23 20:277.5 2.6 1
trans-1,2-Dichloroethene <6.4 ug/kg 05/12/23 23:57 156-60-505/11/23 20:277.5 6.4 1
1,2-Dichloropropane <2.2 ug/kg 05/12/23 23:57 78-87-505/11/23 20:277.5 2.2 1
1,3-Dichloropropane <2.3 ug/kg 05/12/23 23:57 142-28-905/11/23 20:277.5 2.3 1
2,2-Dichloropropane <5.7 ug/kg 05/12/23 23:57 594-20-7 v205/11/23 20:277.5 5.7 1
1,1-Dichloropropene <3.6 ug/kg 05/12/23 23:57 563-58-605/11/23 20:277.5 3.6 1
cis-1,3-Dichloropropene <2.0 ug/kg 05/12/23 23:57 10061-01-505/11/23 20:277.5 2.0 1
trans-1,3-Dichloropropene <2.6 ug/kg 05/12/23 23:57 10061-02-605/11/23 20:277.5 2.6 1
Diisopropyl ether <2.0 ug/kg 05/12/23 23:57 108-20-305/11/23 20:277.5 2.0 1
Ethylbenzene <3.5 ug/kg 05/12/23 23:57 100-41-405/11/23 20:277.5 3.5 1
Hexachloro-1,3-butadiene <12.3 ug/kg 05/12/23 23:57 87-68-305/11/23 20:2715.0 12.3 1
2-Hexanone <7.2 ug/kg 05/12/23 23:57 591-78-605/11/23 20:2774.9 7.2 1
Isopropylbenzene (Cumene)<2.5 ug/kg 05/12/23 23:57 98-82-805/11/23 20:277.5 2.5 1
p-Isopropyltoluene <3.7 ug/kg 05/12/23 23:57 99-87-605/11/23 20:277.5 3.7 1
Methylene Chloride <20.5 ug/kg 05/12/23 23:57 75-09-205/11/23 20:2730.0 20.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-7 (1-2)Lab ID:92667059009 Collected:05/09/23 14:25 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<7.2 ug/kg 05/12/23 23:57 108-10-105/11/23 20:2774.9 7.2 1
Methyl-tert-butyl ether <2.8 ug/kg 05/12/23 23:57 1634-04-405/11/23 20:277.5 2.8 1
Naphthalene <3.9 ug/kg 05/12/23 23:57 91-20-305/11/23 20:277.5 3.9 1
n-Propylbenzene <2.7 ug/kg 05/12/23 23:57 103-65-105/11/23 20:277.5 2.7 1
Styrene <2.0 ug/kg 05/12/23 23:57 100-42-505/11/23 20:277.5 2.0 1
1,1,1,2-Tetrachloroethane <2.9 ug/kg 05/12/23 23:57 630-20-605/11/23 20:277.5 2.9 1
1,1,2,2-Tetrachloroethane <2.0 ug/kg 05/12/23 23:57 79-34-505/11/23 20:277.5 2.0 1
Tetrachloroethene <2.4 ug/kg 05/12/23 23:57 127-18-405/11/23 20:277.5 2.4 1
Toluene <5.2 ug/kg 05/12/23 23:57 108-88-305/11/23 20:277.5 5.2 1
1,2,3-Trichlorobenzene <6.1 ug/kg 05/12/23 23:57 87-61-605/11/23 20:277.5 6.1 1
1,2,4-Trichlorobenzene <6.3 ug/kg 05/12/23 23:57 120-82-105/11/23 20:277.5 6.3 1
1,1,1-Trichloroethane <3.9 ug/kg 05/12/23 23:57 71-55-605/11/23 20:277.5 3.9 1
1,1,2-Trichloroethane <2.5 ug/kg 05/12/23 23:57 79-00-505/11/23 20:277.5 2.5 1
Trichloroethene <6.0 ug/kg 05/12/23 23:57 79-01-605/11/23 20:277.5 6.0 1
Trichlorofluoromethane <4.1 ug/kg 05/12/23 23:57 75-69-405/11/23 20:277.5 4.1 1
1,2,3-Trichloropropane <3.8 ug/kg 05/12/23 23:57 96-18-405/11/23 20:277.5 3.8 1
1,2,4-Trimethylbenzene <4.5 ug/kg 05/12/23 23:57 95-63-605/11/23 20:277.5 4.5 1
1,3,5-Trimethylbenzene <2.5 ug/kg 05/12/23 23:57 108-67-805/11/23 20:277.5 2.5 1
Vinyl acetate <15.4 ug/kg 05/12/23 23:57 108-05-405/11/23 20:2774.9 15.4 1
Vinyl chloride <3.8 ug/kg 05/12/23 23:57 75-01-405/11/23 20:2715.0 3.8 1
Xylene (Total)<4.3 ug/kg 05/12/23 23:57 1330-20-705/11/23 20:2715.0 4.3 1
m&p-Xylene <5.1 ug/kg 05/12/23 23:57 179601-23-105/11/23 20:2715.0 5.1 1
o-Xylene <3.3 ug/kg 05/12/23 23:57 95-47-605/11/23 20:277.5 3.3 1
Surrogates
Toluene-d8 (S)101 %05/12/23 23:57 2037-26-505/11/23 20:2770-130 1
4-Bromofluorobenzene (S)101 %05/12/23 23:57 460-00-405/11/23 20:2770-130 1
1,2-Dichloroethane-d4 (S)100 %05/12/23 23:57 17060-07-005/11/23 20:2770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 7.3 %05/11/23 16:27 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-DUP-230509 (1-2)Lab ID:92667059010 Collected:05/09/23 00:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <33.6 ug/kg 05/13/23 00:15 67-64-105/11/23 20:2710533.6 1
Benzene <2.1 ug/kg 05/13/23 00:15 71-43-205/11/23 20:275.2 2.1 1
Bromobenzene <1.7 ug/kg 05/13/23 00:15 108-86-105/11/23 20:275.2 1.7 1
Bromochloromethane <1.5 ug/kg 05/13/23 00:15 74-97-505/11/23 20:275.2 1.5 1
Bromodichloromethane <2.0 ug/kg 05/13/23 00:15 75-27-405/11/23 20:275.2 2.0 1
Bromoform <1.8 ug/kg 05/13/23 00:15 75-25-205/11/23 20:275.2 1.8 1
Bromomethane <16.2 ug/kg 05/13/23 00:15 74-83-905/11/23 20:2720.9 16.2 1
2-Butanone (MEK)<25.1 ug/kg 05/13/23 00:15 78-93-305/11/23 20:2710525.1 1
n-Butylbenzene <3.3 ug/kg 05/13/23 00:15 104-51-805/11/23 20:275.2 3.3 1
sec-Butylbenzene <2.3 ug/kg 05/13/23 00:15 135-98-805/11/23 20:275.2 2.3 1
tert-Butylbenzene <1.9 ug/kg 05/13/23 00:15 98-06-605/11/23 20:275.2 1.9 1
Carbon tetrachloride <2.0 ug/kg 05/13/23 00:15 56-23-505/11/23 20:275.2 2.0 1
Chlorobenzene 36.6 ug/kg 05/13/23 00:15 108-90-705/11/23 20:275.2 3.0 1
Chloroethane <4.0 ug/kg 05/13/23 00:15 75-00-305/11/23 20:2710.5 4.0 1
Chloroform <4.4 ug/kg 05/13/23 00:15 67-66-305/11/23 20:275.2 4.4 1
Chloromethane <4.4 ug/kg 05/13/23 00:15 74-87-305/11/23 20:2710.5 4.4 1
2-Chlorotoluene <1.9 ug/kg 05/13/23 00:15 95-49-805/11/23 20:275.2 1.9 1
4-Chlorotoluene <2.9 ug/kg 05/13/23 00:15 106-43-405/11/23 20:275.2 2.9 1
1,2-Dibromo-3-chloropropane <2.0 ug/kg 05/13/23 00:15 96-12-805/11/23 20:275.2 2.0 1
Dibromochloromethane <2.9 ug/kg 05/13/23 00:15 124-48-105/11/23 20:275.2 2.9 1
1,2-Dibromoethane (EDB)<2.3 ug/kg 05/13/23 00:15 106-93-405/11/23 20:275.2 2.3 1
Dibromomethane <1.1 ug/kg 05/13/23 00:15 74-95-305/11/23 20:275.2 1.1 1
1,2-Dichlorobenzene <1.9 ug/kg 05/13/23 00:15 95-50-105/11/23 20:275.2 1.9 1
1,3-Dichlorobenzene <1.6 ug/kg 05/13/23 00:15 541-73-105/11/23 20:275.2 1.6 1
1,4-Dichlorobenzene <1.4 ug/kg 05/13/23 00:15 106-46-705/11/23 20:275.2 1.4 1
Dichlorodifluoromethane <5.3 ug/kg 05/13/23 00:15 75-71-8 IH05/11/23 20:2710.5 5.3 1
1,1-Dichloroethane <2.2 ug/kg 05/13/23 00:15 75-34-305/11/23 20:275.2 2.2 1
1,2-Dichloroethane <3.5 ug/kg 05/13/23 00:15 107-06-205/11/23 20:275.2 3.5 1
1,1-Dichloroethene <2.2 ug/kg 05/13/23 00:15 75-35-405/11/23 20:275.2 2.2 1
cis-1,2-Dichloroethene <1.8 ug/kg 05/13/23 00:15 156-59-205/11/23 20:275.2 1.8 1
trans-1,2-Dichloroethene <4.4 ug/kg 05/13/23 00:15 156-60-505/11/23 20:275.2 4.4 1
1,2-Dichloropropane <1.6 ug/kg 05/13/23 00:15 78-87-505/11/23 20:275.2 1.6 1
1,3-Dichloropropane <1.6 ug/kg 05/13/23 00:15 142-28-905/11/23 20:275.2 1.6 1
2,2-Dichloropropane <4.0 ug/kg 05/13/23 00:15 594-20-7 v205/11/23 20:275.2 4.0 1
1,1-Dichloropropene <2.5 ug/kg 05/13/23 00:15 563-58-605/11/23 20:275.2 2.5 1
cis-1,3-Dichloropropene <1.4 ug/kg 05/13/23 00:15 10061-01-505/11/23 20:275.2 1.4 1
trans-1,3-Dichloropropene <1.8 ug/kg 05/13/23 00:15 10061-02-605/11/23 20:275.2 1.8 1
Diisopropyl ether <1.4 ug/kg 05/13/23 00:15 108-20-305/11/23 20:275.2 1.4 1
Ethylbenzene <2.4 ug/kg 05/13/23 00:15 100-41-405/11/23 20:275.2 2.4 1
Hexachloro-1,3-butadiene <8.6 ug/kg 05/13/23 00:15 87-68-305/11/23 20:2710.5 8.6 1
2-Hexanone <5.0 ug/kg 05/13/23 00:15 591-78-605/11/23 20:2752.3 5.0 1
Isopropylbenzene (Cumene)<1.8 ug/kg 05/13/23 00:15 98-82-805/11/23 20:275.2 1.8 1
p-Isopropyltoluene <2.6 ug/kg 05/13/23 00:15 99-87-605/11/23 20:275.2 2.6 1
Methylene Chloride <14.3 ug/kg 05/13/23 00:15 75-09-205/11/23 20:2720.9 14.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 30 of 55
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Sample:FG-DUP-230509 (1-2)Lab ID:92667059010 Collected:05/09/23 00:00 Received:05/10/23 06:25 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<5.0 ug/kg 05/13/23 00:15 108-10-105/11/23 20:2752.3 5.0 1
Methyl-tert-butyl ether <2.0 ug/kg 05/13/23 00:15 1634-04-405/11/23 20:275.2 2.0 1
Naphthalene <2.7 ug/kg 05/13/23 00:15 91-20-305/11/23 20:275.2 2.7 1
n-Propylbenzene <1.9 ug/kg 05/13/23 00:15 103-65-105/11/23 20:275.2 1.9 1
Styrene <1.4 ug/kg 05/13/23 00:15 100-42-505/11/23 20:275.2 1.4 1
1,1,1,2-Tetrachloroethane <2.0 ug/kg 05/13/23 00:15 630-20-605/11/23 20:275.2 2.0 1
1,1,2,2-Tetrachloroethane <1.4 ug/kg 05/13/23 00:15 79-34-505/11/23 20:275.2 1.4 1
Tetrachloroethene <1.7 ug/kg 05/13/23 00:15 127-18-405/11/23 20:275.2 1.7 1
Toluene <3.6 ug/kg 05/13/23 00:15 108-88-305/11/23 20:275.2 3.6 1
1,2,3-Trichlorobenzene <4.2 ug/kg 05/13/23 00:15 87-61-605/11/23 20:275.2 4.2 1
1,2,4-Trichlorobenzene <4.4 ug/kg 05/13/23 00:15 120-82-105/11/23 20:275.2 4.4 1
1,1,1-Trichloroethane <2.7 ug/kg 05/13/23 00:15 71-55-605/11/23 20:275.2 2.7 1
1,1,2-Trichloroethane <1.7 ug/kg 05/13/23 00:15 79-00-505/11/23 20:275.2 1.7 1
Trichloroethene <4.2 ug/kg 05/13/23 00:15 79-01-605/11/23 20:275.2 4.2 1
Trichlorofluoromethane <2.9 ug/kg 05/13/23 00:15 75-69-405/11/23 20:275.2 2.9 1
1,2,3-Trichloropropane <2.6 ug/kg 05/13/23 00:15 96-18-405/11/23 20:275.2 2.6 1
1,2,4-Trimethylbenzene <3.1 ug/kg 05/13/23 00:15 95-63-605/11/23 20:275.2 3.1 1
1,3,5-Trimethylbenzene <1.8 ug/kg 05/13/23 00:15 108-67-805/11/23 20:275.2 1.8 1
Vinyl acetate <10.8 ug/kg 05/13/23 00:15 108-05-405/11/23 20:2752.3 10.8 1
Vinyl chloride <2.7 ug/kg 05/13/23 00:15 75-01-405/11/23 20:2710.5 2.7 1
Xylene (Total)<3.0 ug/kg 05/13/23 00:15 1330-20-705/11/23 20:2710.5 3.0 1
m&p-Xylene <3.6 ug/kg 05/13/23 00:15 179601-23-105/11/23 20:2710.5 3.6 1
o-Xylene <2.3 ug/kg 05/13/23 00:15 95-47-605/11/23 20:275.2 2.3 1
Surrogates
Toluene-d8 (S)101 %05/13/23 00:15 2037-26-505/11/23 20:2770-130 1
4-Bromofluorobenzene (S)101 %05/13/23 00:15 460-00-405/11/23 20:2770-130 1
1,2-Dichloroethane-d4 (S)100 %05/13/23 00:15 17060-07-005/11/23 20:2770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.9 %05/11/23 16:28 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
881325
EPA 7471B
EPA 7471B
7471B Mercury Solids
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4644488
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Matrix:Solid
AnalyzedMDL
Mercury mg/kg <0.0085 0.019 05/17/23 16:320.0085
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4644489LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.440.46 95 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4644490MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667059001
4644491
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.559 91 80-12091 4 200.5860.032 0.55 0.57
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
881324
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4644483
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg <0.14 0.48 05/17/23 13:370.14
Barium mg/kg <0.072 0.29 05/17/23 13:370.072
Cadmium mg/kg <0.028 0.077 05/17/23 13:370.028
Chromium mg/kg <0.37 1.9 05/17/23 13:370.37
Lead mg/kg <0.090 0.48 05/17/23 13:370.090
Selenium mg/kg <0.10 0.48 05/17/23 13:370.10
Silver mg/kg <0.20 0.48 05/17/23 13:370.20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4644484LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 47.147.6 99 80-120
Barium mg/kg 47.447.6 100 80-120
Cadmium mg/kg 46.647.6 98 80-120
Chromium mg/kg 50.747.6 107 80-120
Lead mg/kg 48.847.6 103 80-120
Selenium mg/kg 48.647.6 102 80-120
Silver mg/kg 24.423.8 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4644485MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667059001
4644486
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 63.2 91 75-12592 3 2064.82.0 59.8 61.3
Barium mg/kg M163.2 125 75-12570 19 2064.8116 195 162
Cadmium mg/kg 63.2 98 75-12596 1 2064.80.071J 61.9 62.3
Chromium mg/kg M163.2 66 75-12597 18 2064.866.2 108 129
Lead mg/kg 63.2 89 75-12594 6 2064.818.5 74.9 79.6
Selenium mg/kg 63.2 93 75-12593 3 2064.80.47J 59.0 60.8
Silver mg/kg 31.5 101 75-12599 1 2032.3<0.26 31.9 32.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
774002
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667059006, 92667059007, 92667059008, 92667059009, 92667059010
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4017366
Associated Lab Samples:92667059006, 92667059007, 92667059008, 92667059009, 92667059010
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg <1.9 5.0 05/12/23 17:121.9
1,1,1-Trichloroethane ug/kg <2.6 5.0 05/12/23 17:122.6
1,1,2,2-Tetrachloroethane ug/kg <1.3 5.0 05/12/23 17:121.3
1,1,2-Trichloroethane ug/kg <1.7 5.0 05/12/23 17:121.7
1,1-Dichloroethane ug/kg <2.1 5.0 05/12/23 17:122.1
1,1-Dichloroethene ug/kg <2.1 5.0 05/12/23 17:122.1
1,1-Dichloropropene ug/kg <2.4 5.0 05/12/23 17:122.4
1,2,3-Trichlorobenzene ug/kg <4.0 5.0 05/12/23 17:124.0
1,2,3-Trichloropropane ug/kg <2.5 5.0 05/12/23 17:122.5
1,2,4-Trichlorobenzene ug/kg <4.2 5.0 05/12/23 17:124.2
1,2,4-Trimethylbenzene ug/kg <3.0 5.0 05/12/23 17:123.0
1,2-Dibromo-3-chloropropane ug/kg <1.9 5.0 05/12/23 17:121.9
1,2-Dibromoethane (EDB)ug/kg <2.2 5.0 05/12/23 17:122.2
1,2-Dichlorobenzene ug/kg <1.8 5.0 05/12/23 17:121.8
1,2-Dichloroethane ug/kg <3.3 5.0 05/12/23 17:123.3
1,2-Dichloropropane ug/kg <1.5 5.0 05/12/23 17:121.5
1,3,5-Trimethylbenzene ug/kg <1.7 5.0 05/12/23 17:121.7
1,3-Dichlorobenzene ug/kg <1.6 5.0 05/12/23 17:121.6
1,3-Dichloropropane ug/kg <1.6 5.0 05/12/23 17:121.6
1,4-Dichlorobenzene ug/kg <1.3 5.0 05/12/23 17:121.3
2,2-Dichloropropane ug/kg <3.8 5.0 v205/12/23 17:123.8
2-Butanone (MEK)ug/kg <24.0 100 05/12/23 17:1224.0
2-Chlorotoluene ug/kg <1.8 5.0 05/12/23 17:121.8
2-Hexanone ug/kg <4.8 50.0 05/12/23 17:124.8
4-Chlorotoluene ug/kg <2.8 5.0 05/12/23 17:122.8
4-Methyl-2-pentanone (MIBK)ug/kg <4.8 50.0 05/12/23 17:124.8
Acetone ug/kg <32.1 100 05/12/23 17:1232.1
Benzene ug/kg <2.0 5.0 05/12/23 17:122.0
Bromobenzene ug/kg <1.6 5.0 05/12/23 17:121.6
Bromochloromethane ug/kg <1.5 5.0 05/12/23 17:121.5
Bromodichloromethane ug/kg <1.9 5.0 05/12/23 17:121.9
Bromoform ug/kg <1.8 5.0 05/12/23 17:121.8
Bromomethane ug/kg <15.5 20.0 05/12/23 17:1215.5
Carbon tetrachloride ug/kg <1.9 5.0 05/12/23 17:121.9
Chlorobenzene ug/kg <2.9 5.0 05/12/23 17:122.9
Chloroethane ug/kg <3.9 10.0 05/12/23 17:123.9
Chloroform ug/kg <4.2 5.0 05/12/23 17:124.2
Chloromethane ug/kg <4.2 10.0 05/12/23 17:124.2
cis-1,2-Dichloroethene ug/kg <1.7 5.0 05/12/23 17:121.7
cis-1,3-Dichloropropene ug/kg <1.4 5.0 05/12/23 17:121.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4017366
Associated Lab Samples:92667059006, 92667059007, 92667059008, 92667059009, 92667059010
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg <2.8 5.0 05/12/23 17:122.8
Dibromomethane ug/kg <1.1 5.0 05/12/23 17:121.1
Dichlorodifluoromethane ug/kg <5.1 10.0 IH05/12/23 17:125.1
Diisopropyl ether ug/kg <1.4 5.0 05/12/23 17:121.4
Ethylbenzene ug/kg <2.3 5.0 05/12/23 17:122.3
Hexachloro-1,3-butadiene ug/kg <8.2 10.0 05/12/23 17:128.2
Isopropylbenzene (Cumene)ug/kg <1.7 5.0 05/12/23 17:121.7
m&p-Xylene ug/kg <3.4 10.0 05/12/23 17:123.4
Methyl-tert-butyl ether ug/kg <1.9 5.0 05/12/23 17:121.9
Methylene Chloride ug/kg <13.7 20.0 05/12/23 17:1213.7
n-Butylbenzene ug/kg <3.2 5.0 05/12/23 17:123.2
n-Propylbenzene ug/kg <1.8 5.0 05/12/23 17:121.8
Naphthalene ug/kg <2.6 5.0 05/12/23 17:122.6
o-Xylene ug/kg <2.2 5.0 05/12/23 17:122.2
p-Isopropyltoluene ug/kg <2.5 5.0 05/12/23 17:122.5
sec-Butylbenzene ug/kg <2.2 5.0 05/12/23 17:122.2
Styrene ug/kg <1.3 5.0 05/12/23 17:121.3
tert-Butylbenzene ug/kg <1.8 5.0 05/12/23 17:121.8
Tetrachloroethene ug/kg <1.6 5.0 05/12/23 17:121.6
Toluene ug/kg <3.4 5.0 05/12/23 17:123.4
trans-1,2-Dichloroethene ug/kg <4.2 5.0 05/12/23 17:124.2
trans-1,3-Dichloropropene ug/kg <1.7 5.0 05/12/23 17:121.7
Trichloroethene ug/kg <4.0 5.0 05/12/23 17:124.0
Trichlorofluoromethane ug/kg <2.8 5.0 05/12/23 17:122.8
Vinyl acetate ug/kg <10.3 50.0 05/12/23 17:1210.3
Vinyl chloride ug/kg <2.5 10.0 05/12/23 17:122.5
Xylene (Total)ug/kg <2.8 10.0 05/12/23 17:122.8
1,2-Dichloroethane-d4 (S)%101 70-130 05/12/23 17:12
4-Bromofluorobenzene (S)%101 70-130 05/12/23 17:12
Toluene-d8 (S)%101 70-130 05/12/23 17:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4017367LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 475500 95 70-130
1,1,1-Trichloroethane ug/kg 474500 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 470500 94 70-130
1,1,2-Trichloroethane ug/kg 464500 93 70-130
1,1-Dichloroethane ug/kg 471500 94 70-130
1,1-Dichloroethene ug/kg 499500 100 70-130
1,1-Dichloropropene ug/kg 475500 95 70-130
1,2,3-Trichlorobenzene ug/kg 489500 98 70-130
1,2,3-Trichloropropane ug/kg 454500 91 70-130
1,2,4-Trichlorobenzene ug/kg 470500 94 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4017367LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 479500 96 70-130
1,2-Dibromo-3-chloropropane ug/kg 447500 89 67-130
1,2-Dibromoethane (EDB)ug/kg 475500 95 70-130
1,2-Dichlorobenzene ug/kg 469500 94 70-130
1,2-Dichloroethane ug/kg 469500 94 70-130
1,2-Dichloropropane ug/kg 475500 95 70-130
1,3,5-Trimethylbenzene ug/kg 481500 96 70-130
1,3-Dichlorobenzene ug/kg 465500 93 70-130
1,3-Dichloropropane ug/kg 459500 92 70-130
1,4-Dichlorobenzene ug/kg 430500 86 70-130
2,2-Dichloropropane ug/kg 354 v35007167-130
2-Butanone (MEK)ug/kg 8911000 89 66-130
2-Chlorotoluene ug/kg 465500 93 70-130
2-Hexanone ug/kg 9811000 98 70-130
4-Chlorotoluene ug/kg 474500 95 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9691000 97 70-130
Acetone ug/kg 9121000 91 67-130
Benzene ug/kg 457500 91 70-130
Bromobenzene ug/kg 487500 97 70-130
Bromochloromethane ug/kg 474500 95 70-130
Bromodichloromethane ug/kg 467500 93 70-130
Bromoform ug/kg 466500 93 70-130
Bromomethane ug/kg 433500 87 53-175
Carbon tetrachloride ug/kg 509500 102 70-130
Chlorobenzene ug/kg 487500 97 70-130
Chloroethane ug/kg 464500 93 70-135
Chloroform ug/kg 463500 93 70-130
Chloromethane ug/kg 503500 101 64-130
cis-1,2-Dichloroethene ug/kg 468500 94 70-130
cis-1,3-Dichloropropene ug/kg 417500 83 70-130
Dibromochloromethane ug/kg 477500 95 70-130
Dibromomethane ug/kg 480500 96 70-130
Dichlorodifluoromethane ug/kg 506 IH50010163-145
Diisopropyl ether ug/kg 463500 93 68-130
Ethylbenzene ug/kg 436500 87 70-130
Hexachloro-1,3-butadiene ug/kg 453500 91 70-130
Isopropylbenzene (Cumene)ug/kg 476500 95 70-130
m&p-Xylene ug/kg 9431000 94 70-130
Methyl-tert-butyl ether ug/kg 443500 89 70-130
Methylene Chloride ug/kg 499500 100 67-130
n-Butylbenzene ug/kg 441500 88 70-130
n-Propylbenzene ug/kg 463500 93 70-130
Naphthalene ug/kg 483500 97 70-130
o-Xylene ug/kg 463500 93 70-130
p-Isopropyltoluene ug/kg 471500 94 70-130
sec-Butylbenzene ug/kg 454500 91 70-130
Styrene ug/kg 476500 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4017367LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 575500 115 64-130
Tetrachloroethene ug/kg 490500 98 70-130
Toluene ug/kg 451500 90 70-130
trans-1,2-Dichloroethene ug/kg 487500 97 70-130
trans-1,3-Dichloropropene ug/kg 447500 89 70-130
Trichloroethene ug/kg 479500 96 70-130
Trichlorofluoromethane ug/kg 431500 86 70-130
Vinyl acetate ug/kg 9411000 94 70-134
Vinyl chloride ug/kg 406500 81 68-130
Xylene (Total)ug/kg 14101500 94 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4017368MATRIX SPIKE SAMPLE:
MSSpike
Result
92667059007
1,1,1,2-Tetrachloroethane ug/kg 690740 93 58-140<2.8
1,1,1-Trichloroethane ug/kg 725740 98 58-144<3.9
1,1,2,2-Tetrachloroethane ug/kg 690740 93 52-139<2.0
1,1,2-Trichloroethane ug/kg 691740 93 56-140<2.5
1,1-Dichloroethane ug/kg 701740 95 58-145<3.1
1,1-Dichloroethene ug/kg 753740 102 57-158<3.1
1,1-Dichloropropene ug/kg 725740 98 58-151<3.6
1,2,3-Trichlorobenzene ug/kg 668740 90 48-149<6.0
1,2,3-Trichloropropane ug/kg 638740 86 54-132<3.7
1,2,4-Trichlorobenzene ug/kg 661740 89 51-151<6.2
1,2,4-Trimethylbenzene ug/kg 661740 89 38-170<4.4
1,2-Dibromo-3-chloropropane ug/kg 633740 85 44-134<2.9
1,2-Dibromoethane (EDB)ug/kg 676740 91 60-138<3.3
1,2-Dichlorobenzene ug/kg 673740 91 59-147<2.7
1,2-Dichloroethane ug/kg 673740 91 57-139<4.9
1,2-Dichloropropane ug/kg 707740 96 62-145<2.2
1,3,5-Trimethylbenzene ug/kg 680740 92 47-159<2.5
1,3-Dichlorobenzene ug/kg 641740 87 58-144<2.3
1,3-Dichloropropane ug/kg 675740 91 60-142<2.3
1,4-Dichlorobenzene ug/kg 607740 82 57-143<1.9
2,2-Dichloropropane ug/kg 512 v37406937-144<5.6
2-Butanone (MEK)ug/kg 12801480 87 28-146<35.5
2-Chlorotoluene ug/kg 665740 90 55-158<2.6
2-Hexanone ug/kg 13401480 90 44-141<7.1
4-Chlorotoluene ug/kg 669740 90 55-146<4.1
4-Methyl-2-pentanone (MIBK)ug/kg 13801480 93 50-138<7.1
Acetone ug/kg 12401480 83 20-136<47.5
Benzene ug/kg 682740 92 60-145<2.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4017368MATRIX SPIKE SAMPLE:
MSSpike
Result
92667059007
Bromobenzene ug/kg 674740 91 59-145<2.4
Bromochloromethane ug/kg 675740 91 57-143<2.2
Bromodichloromethane ug/kg 683740 92 53-133<2.9
Bromoform ug/kg 659740 89 48-133<2.6
Bromomethane ug/kg 135740 18 10-167<23.0
Carbon tetrachloride ug/kg 621740 84 57-147<2.8
Chlorobenzene ug/kg 789740 88 61-144140
Chloroethane ug/kg 169740 23 10-153<5.7
Chloroform ug/kg 691740 93 58-141<6.2
Chloromethane ug/kg 802740 108 54-165<6.2
cis-1,2-Dichloroethene ug/kg 688740 93 59-144<2.5
cis-1,3-Dichloropropene ug/kg 589740 80 56-137<2.0
Dibromochloromethane ug/kg 674740 91 53-139<4.2
Dibromomethane ug/kg 671740 91 60-136<1.6
Dichlorodifluoromethane ug/kg 920 IH74012449-177<7.5
Diisopropyl ether ug/kg 688740 93 53-136<2.0
Ethylbenzene ug/kg 640740 86 53-150<3.5
Hexachloro-1,3-butadiene ug/kg 696740 94 42-186<12.1
Isopropylbenzene (Cumene)ug/kg 704740 95 62-154<2.5
m&p-Xylene ug/kg 13501480 91 49-156<5.1
Methyl-tert-butyl ether ug/kg 630740 85 54-133<2.8
Methylene Chloride ug/kg 702740 94 50-153<20.3
n-Butylbenzene ug/kg 643740 87 44-174<4.7
n-Propylbenzene ug/kg 660740 89 52-157<2.6
Naphthalene ug/kg 656740 89 37-150<3.9
o-Xylene ug/kg 674740 91 54-150<3.3
p-Isopropyltoluene ug/kg 682740 92 50-164<3.6
sec-Butylbenzene ug/kg 673740 91 58-161<3.3
Styrene ug/kg 691740 93 60-148<2.0
tert-Butylbenzene ug/kg 638740 86 44-151<2.6
Tetrachloroethene ug/kg 663740 89 53-151<2.3
Toluene ug/kg 673740 91 52-148<5.1
trans-1,2-Dichloroethene ug/kg 683740 92 60-148<6.3
trans-1,3-Dichloropropene ug/kg 648740 88 55-133<2.5
Trichloroethene ug/kg 689740 93 60-148<6.0
Trichlorofluoromethane ug/kg 153740 21 10-154<4.1
Vinyl acetate ug/kg 12501480 85 50-149<15.2
Vinyl chloride ug/kg 636740 86 57-157<3.8
Xylene (Total)ug/kg 20302220 91 52-153<4.2
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 38 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667059008
4017369SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg <2.8 30<2.8
1,1,1-Trichloroethane ug/kg <3.7 30<3.7
1,1,2,2-Tetrachloroethane ug/kg <1.9 30<1.9
1,1,2-Trichloroethane ug/kg <2.4 30<2.4
1,1-Dichloroethane ug/kg <3.0 30<3.0
1,1-Dichloroethene ug/kg <3.0 30<3.0
1,1-Dichloropropene ug/kg <3.5 30<3.5
1,2,3-Trichlorobenzene ug/kg <5.8 30<5.8
1,2,3-Trichloropropane ug/kg <3.6 30<3.6
1,2,4-Trichlorobenzene ug/kg <6.1 30<6.1
1,2,4-Trimethylbenzene ug/kg <4.3 30<4.3
1,2-Dibromo-3-chloropropane ug/kg <2.8 30<2.8
1,2-Dibromoethane (EDB)ug/kg <3.2 30<3.2
1,2-Dichlorobenzene ug/kg <2.6 30<2.6
1,2-Dichloroethane ug/kg <4.8 30<4.8
1,2-Dichloropropane ug/kg <2.2 30<2.2
1,3,5-Trimethylbenzene ug/kg <2.4 30<2.4
1,3-Dichlorobenzene ug/kg <2.2 30<2.2
1,3-Dichloropropane ug/kg <2.2 30<2.2
1,4-Dichlorobenzene ug/kg <1.9 30<1.9
2,2-Dichloropropane ug/kg <5.5 v230<5.5
2-Butanone (MEK)ug/kg <34.6 30<34.6
2-Chlorotoluene ug/kg <2.6 30<2.6
2-Hexanone ug/kg <6.9 30<6.9
4-Chlorotoluene ug/kg <4.0 30<4.0
4-Methyl-2-pentanone (MIBK)ug/kg <6.9 30<6.9
Acetone ug/kg <46.3 3051.8J
Benzene ug/kg <2.9 30<2.9
Bromobenzene ug/kg <2.3 30<2.3
Bromochloromethane ug/kg <2.1 30<2.1
Bromodichloromethane ug/kg <2.8 30<2.8
Bromoform ug/kg <2.5 30<2.5
Bromomethane ug/kg <22.3 30<22.3
Carbon tetrachloride ug/kg <2.7 30<2.7
Chlorobenzene ug/kg <4.1 30<4.1
Chloroethane ug/kg <5.6 30<5.6
Chloroform ug/kg <6.0 30<6.0
Chloromethane ug/kg <6.1 30<6.1
cis-1,2-Dichloroethene ug/kg <2.5 30<2.5
cis-1,3-Dichloropropene ug/kg <2.0 30<2.0
Dibromochloromethane ug/kg <4.0 30<4.0
Dibromomethane ug/kg <1.5 30<1.5
Dichlorodifluoromethane ug/kg <7.3 IH30<7.3
Diisopropyl ether ug/kg <1.9 30<1.9
Ethylbenzene ug/kg <3.4 30<3.4
Hexachloro-1,3-butadiene ug/kg <11.8 30<11.8
Isopropylbenzene (Cumene)ug/kg <2.4 30<2.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667059008
4017369SAMPLE DUPLICATE:
m&p-Xylene ug/kg <4.9 30<4.9
Methyl-tert-butyl ether ug/kg <2.7 30<2.7
Methylene Chloride ug/kg <19.7 30<19.7
n-Butylbenzene ug/kg <4.5 30<4.5
n-Propylbenzene ug/kg <2.6 30<2.6
Naphthalene ug/kg <3.8 30<3.8
o-Xylene ug/kg <3.2 30<3.2
p-Isopropyltoluene ug/kg 64.1 8 3059.3
sec-Butylbenzene ug/kg <3.2 30<3.2
Styrene ug/kg <1.9 30<1.9
tert-Butylbenzene ug/kg <2.6 30<2.6
Tetrachloroethene ug/kg <2.3 30<2.3
Toluene ug/kg <5.0 30<5.0
trans-1,2-Dichloroethene ug/kg <6.1 30<6.1
trans-1,3-Dichloropropene ug/kg <2.5 30<2.5
Trichloroethene ug/kg <5.8 30<5.8
Trichlorofluoromethane ug/kg <4.0 30<4.0
Vinyl acetate ug/kg <14.8 30<14.8
Vinyl chloride ug/kg <3.7 30<3.7
Xylene (Total)ug/kg <4.1 30<4.1
1,2-Dichloroethane-d4 (S)%101100
4-Bromofluorobenzene (S)%103101
Toluene-d8 (S)%101100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
774150
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4017930
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg <128 325 05/15/23 10:15128
1,2-Dichlorobenzene ug/kg <117 325 05/15/23 10:15117
1,3-Dichlorobenzene ug/kg <115 325 05/15/23 10:15115
1,4-Dichlorobenzene ug/kg <124 325 05/15/23 10:15124
1-Methylnaphthalene ug/kg <114 325 05/15/23 10:15114
2,2'-Oxybis(1-chloropropane)ug/kg <154 325 05/15/23 10:15154
2,4,5-Trichlorophenol ug/kg <149 325 05/15/23 10:15149
2,4,6-Trichlorophenol ug/kg <134 325 05/15/23 10:15134
2,4-Dichlorophenol ug/kg <127 325 05/15/23 10:15127
2,4-Dimethylphenol ug/kg <135 325 05/15/23 10:15135
2,4-Dinitrophenol ug/kg <1000 1620 v105/15/23 10:151000
2,4-Dinitrotoluene ug/kg <125 325 05/15/23 10:15125
2,6-Dinitrotoluene ug/kg <119 325 05/15/23 10:15119
2-Chloronaphthalene ug/kg <129 325 05/15/23 10:15129
2-Chlorophenol ug/kg <122 325 05/15/23 10:15122
2-Methylnaphthalene ug/kg <130 325 05/15/23 10:15130
2-Methylphenol(o-Cresol)ug/kg <133 325 05/15/23 10:15133
2-Nitroaniline ug/kg <266 1620 05/15/23 10:15266
2-Nitrophenol ug/kg <141 325 05/15/23 10:15141
3&4-Methylphenol(m&p Cresol)ug/kg <131 325 05/15/23 10:15131
3,3'-Dichlorobenzidine ug/kg <219 649 05/15/23 10:15219
3-Nitroaniline ug/kg <255 1620 05/15/23 10:15255
4,6-Dinitro-2-methylphenol ug/kg <303 649 05/15/23 10:15303
4-Bromophenylphenyl ether ug/kg <125 325 05/15/23 10:15125
4-Chloro-3-methylphenol ug/kg <228 649 05/15/23 10:15228
4-Chloroaniline ug/kg <255 649 05/15/23 10:15255
4-Chlorophenylphenyl ether ug/kg <121 325 05/15/23 10:15121
4-Nitroaniline ug/kg <247 649 05/15/23 10:15247
4-Nitrophenol ug/kg <628 1620 05/15/23 10:15628
Acenaphthene ug/kg <114 325 05/15/23 10:15114
Acenaphthylene ug/kg <114 325 05/15/23 10:15114
Aniline ug/kg <127 325 05/15/23 10:15127
Anthracene ug/kg <106 325 05/15/23 10:15106
Benzo(a)anthracene ug/kg <108 325 05/15/23 10:15108
Benzo(a)pyrene ug/kg <112 325 05/15/23 10:15112
Benzo(b)fluoranthene ug/kg <108 325 05/15/23 10:15108
Benzo(g,h,i)perylene ug/kg <126 325 05/15/23 10:15126
Benzo(k)fluoranthene ug/kg <114 325 05/15/23 10:15114
Benzoic Acid ug/kg <697 1620 v105/15/23 10:15697
Benzyl alcohol ug/kg <246 649 05/15/23 10:15246
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4017930
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg <135 325 05/15/23 10:15135
bis(2-Chloroethyl) ether ug/kg <122 325 05/15/23 10:15122
bis(2-Ethylhexyl)phthalate ug/kg <126 325 05/15/23 10:15126
Butylbenzylphthalate ug/kg <137 325 05/15/23 10:15137
Chrysene ug/kg <118 325 05/15/23 10:15118
Di-n-butylphthalate ug/kg <109 325 05/15/23 10:15109
Di-n-octylphthalate ug/kg <128 325 05/15/23 10:15128
Dibenz(a,h)anthracene ug/kg <125 325 05/15/23 10:15125
Dibenzofuran ug/kg <117 325 05/15/23 10:15117
Diethylphthalate ug/kg <119 325 05/15/23 10:15119
Dimethylphthalate ug/kg <118 325 05/15/23 10:15118
Fluoranthene ug/kg <111 325 05/15/23 10:15111
Fluorene ug/kg <114 325 05/15/23 10:15114
Hexachloro-1,3-butadiene ug/kg <141 325 05/15/23 10:15141
Hexachlorobenzene ug/kg <127 325 05/15/23 10:15127
Hexachlorocyclopentadiene ug/kg <186 325 05/15/23 10:15186
Hexachloroethane ug/kg <124 325 05/15/23 10:15124
Indeno(1,2,3-cd)pyrene ug/kg <128 325 05/15/23 10:15128
Isophorone ug/kg <145 325 05/15/23 10:15145
N-Nitroso-di-n-propylamine ug/kg <122 325 05/15/23 10:15122
N-Nitrosodimethylamine ug/kg <109 325 05/15/23 10:15109
N-Nitrosodiphenylamine ug/kg <115 325 05/15/23 10:15115
Naphthalene ug/kg <110 325 05/15/23 10:15110
Nitrobenzene ug/kg <150 325 05/15/23 10:15150
Pentachlorophenol ug/kg <318 649 05/15/23 10:15318
Phenanthrene ug/kg <106 325 05/15/23 10:15106
Phenol ug/kg <145 325 05/15/23 10:15145
Pyrene ug/kg <132 325 05/15/23 10:15132
Pyridine ug/kg <102 325 05/15/23 10:15102
2,4,6-Tribromophenol (S)%43 10-131 05/15/23 10:15
2-Fluorobiphenyl (S)%40 10-130 05/15/23 10:15
2-Fluorophenol (S)%42 10-130 05/15/23 10:15
Nitrobenzene-d5 (S)%44 10-130 05/15/23 10:15
Phenol-d6 (S)%44 10-130 05/15/23 10:15
Terphenyl-d14 (S)%55 10-130 05/15/23 10:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4017931LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 9641640 59 43-130
1,2-Dichlorobenzene ug/kg 9291640 57 43-130
1,3-Dichlorobenzene ug/kg 9141640 56 43-130
1,4-Dichlorobenzene ug/kg 9081640 55 44-130
1-Methylnaphthalene ug/kg 10501640 64 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4017931LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 8961640 55 29-130
2,4,5-Trichlorophenol ug/kg 9981640 61 47-130
2,4,6-Trichlorophenol ug/kg 9991640 61 47-130
2,4-Dichlorophenol ug/kg 10601640 64 45-130
2,4-Dimethylphenol ug/kg 14801640 91 45-130
2,4-Dinitrophenol ug/kg 5240 v182006427-140
2,4-Dinitrotoluene ug/kg 10101640 62 46-130
2,6-Dinitrotoluene ug/kg 10501640 64 48-130
2-Chloronaphthalene ug/kg 9361640 57 46-130
2-Chlorophenol ug/kg 9781640 60 43-130
2-Methylnaphthalene ug/kg 9911640 60 47-130
2-Methylphenol(o-Cresol)ug/kg 9911640 60 42-130
2-Nitroaniline ug/kg 18903280 58 41-130
2-Nitrophenol ug/kg 11101640 68 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 10101640 62 39-130
3,3'-Dichlorobenzidine ug/kg 19503280 59 41-130
3-Nitroaniline ug/kg 18403280 56 37-130
4,6-Dinitro-2-methylphenol ug/kg 23003280 70 38-141
4-Bromophenylphenyl ether ug/kg 9991640 61 47-130
4-Chloro-3-methylphenol ug/kg 20703280 63 44-130
4-Chloroaniline ug/kg 18103280 55 41-130
4-Chlorophenylphenyl ether ug/kg 9701640 59 45-130
4-Nitroaniline ug/kg 19303280 59 42-130
4-Nitrophenol ug/kg 51808200 63 39-131
Acenaphthene ug/kg 10001640 61 49-130
Acenaphthylene ug/kg 9871640 60 50-130
Aniline ug/kg 7721640 47 38-130
Anthracene ug/kg 9651640 59 49-130
Benzo(a)anthracene ug/kg 10401640 64 51-130
Benzo(a)pyrene ug/kg 9791640 60 51-130
Benzo(b)fluoranthene ug/kg 9751640 59 49-130
Benzo(g,h,i)perylene ug/kg 9641640 59 48-140
Benzo(k)fluoranthene ug/kg 10101640 62 51-130
Benzoic Acid ug/kg 2950 v182003622-130
Benzyl alcohol ug/kg 18503280 57 43-130
bis(2-Chloroethoxy)methane ug/kg 9221640 56 43-130
bis(2-Chloroethyl) ether ug/kg 8791640 54 42-130
bis(2-Ethylhexyl)phthalate ug/kg 10601640 65 43-130
Butylbenzylphthalate ug/kg 10501640 64 44-131
Chrysene ug/kg 10801640 66 51-130
Di-n-butylphthalate ug/kg 10201640 62 46-130
Di-n-octylphthalate ug/kg 10801640 66 45-130
Dibenz(a,h)anthracene ug/kg 10701640 65 48-130
Dibenzofuran ug/kg 9831640 60 10-130
Diethylphthalate ug/kg 10101640 62 48-130
Dimethylphthalate ug/kg 10101640 61 48-130
Fluoranthene ug/kg 10401640 63 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4017931LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 9871640 60 48-130
Hexachloro-1,3-butadiene ug/kg 9911640 60 39-130
Hexachlorobenzene ug/kg 9721640 59 47-130
Hexachlorocyclopentadiene ug/kg 8901640 54 17-130
Hexachloroethane ug/kg 9421640 57 40-130
Indeno(1,2,3-cd)pyrene ug/kg 9821640 60 50-130
Isophorone ug/kg 10101640 61 41-130
N-Nitroso-di-n-propylamine ug/kg 9721640 59 36-130
N-Nitrosodimethylamine ug/kg 9081640 55 34-130
N-Nitrosodiphenylamine ug/kg 9841640 60 48-130
Naphthalene ug/kg 10101640 61 46-130
Nitrobenzene ug/kg 9821640 60 39-130
Pentachlorophenol ug/kg 19103280 58 42-130
Phenanthrene ug/kg 10401640 63 50-130
Phenol ug/kg 10301640 63 42-130
Pyrene ug/kg 10201640 62 50-130
Pyridine ug/kg 7931640 48 26-130
2,4,6-Tribromophenol (S)%63 10-131
2-Fluorobiphenyl (S)%57 10-130
2-Fluorophenol (S)%56 10-130
Nitrobenzene-d5 (S)%60 10-130
Phenol-d6 (S)%58 10-130
Terphenyl-d14 (S)%62 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4017932MATRIX SPIKE SAMPLE:
MSSpike
Result
92666610002
1,2,4-Trichlorobenzene ug/kg 9251950 48 16-130ND
1,2-Dichlorobenzene ug/kg 8671950 45 19-130ND
1,3-Dichlorobenzene ug/kg 8561950 44 19-130ND
1,4-Dichlorobenzene ug/kg 8601950 44 20-130ND
1-Methylnaphthalene ug/kg 8751950 45 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 7571950 39 10-130ND
2,4,5-Trichlorophenol ug/kg 10201950 52 19-130ND
2,4,6-Trichlorophenol ug/kg 10001950 52 18-130ND
2,4-Dichlorophenol ug/kg 9741950 50 16-130ND
2,4-Dimethylphenol ug/kg 11001950 57 10-130ND
2,4-Dinitrophenol ug/kg 32109720 33 10-143ND
2,4-Dinitrotoluene ug/kg 9161950 47 19-130ND
2,6-Dinitrotoluene ug/kg 9481950 49 22-130ND
2-Chloronaphthalene ug/kg 9321950 48 18-130ND
2-Chlorophenol ug/kg 8941950 46 20-130ND
2-Methylnaphthalene ug/kg 8541950 44 18-130ND
2-Methylphenol(o-Cresol)ug/kg 8541950 44 13-130ND
2-Nitroaniline ug/kg 1770J3880 46 18-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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[phone]
Page 44 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4017932MATRIX SPIKE SAMPLE:
MSSpike
Result
92666610002
2-Nitrophenol ug/kg 9391950 48 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 8391950 43 13-130ND
3,3'-Dichlorobenzidine ug/kg 16103880 42 10-130ND
3-Nitroaniline ug/kg 1690J3880 44 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 20303880 52 10-144ND
4-Bromophenylphenyl ether ug/kg 9661950 50 18-130ND
4-Chloro-3-methylphenol ug/kg 17703880 46 16-130ND
4-Chloroaniline ug/kg 15903880 41 17-130ND
4-Chlorophenylphenyl ether ug/kg 9021950 46 17-130ND
4-Nitroaniline ug/kg 16503880 42 21-130ND
4-Nitrophenol ug/kg 42709720 44 13-131ND
Acenaphthene ug/kg 9411950 48 20-130ND
Acenaphthylene ug/kg 9341950 48 21-130ND
Aniline ug/kg 6321950 33 10-130ND
Anthracene ug/kg 8851950 46 19-130ND
Benzo(a)anthracene ug/kg 9021950 46 17-130ND
Benzo(a)pyrene ug/kg 8841950 45 14-130ND
Benzo(b)fluoranthene ug/kg 8751950 45 11-134ND
Benzo(g,h,i)perylene ug/kg 10301950 53 12-130ND
Benzo(k)fluoranthene ug/kg 9211950 47 15-130ND
Benzoic Acid ug/kg <827 M19720710-130ND
Benzyl alcohol ug/kg 16003880 41 20-130ND
bis(2-Chloroethoxy)methane ug/kg 8191950 42 16-130ND
bis(2-Chloroethyl) ether ug/kg 8111950 42 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 9381950 48 11-130ND
Butylbenzylphthalate ug/kg 9781950 50 10-130ND
Chrysene ug/kg 9101950 47 17-130ND
Di-n-butylphthalate ug/kg 8771950 45 16-130ND
Di-n-octylphthalate ug/kg 8241950 42 16-130ND
Dibenz(a,h)anthracene ug/kg 9821950 51 13-130ND
Dibenzofuran ug/kg 9301950 48 19-130ND
Diethylphthalate ug/kg 9021950 46 22-130ND
Dimethylphthalate ug/kg 9361950 48 23-130ND
Fluoranthene ug/kg 8101950 42 14-130ND
Fluorene ug/kg 9191950 47 19-130ND
Hexachloro-1,3-butadiene ug/kg 8971950 46 12-130ND
Hexachlorobenzene ug/kg 9741950 50 17-130ND
Hexachlorocyclopentadiene ug/kg 7481950 38 10-130ND
Hexachloroethane ug/kg 8501950 44 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 10301950 53 13-130ND
Isophorone ug/kg 8341950 43 17-130ND
N-Nitroso-di-n-propylamine ug/kg 8351950 43 10-130ND
N-Nitrosodimethylamine ug/kg 8031950 41 16-130ND
N-Nitrosodiphenylamine ug/kg 9871950 51 19-130ND
Naphthalene ug/kg 9101950 47 18-130ND
Nitrobenzene ug/kg 8741950 45 15-130ND
Pentachlorophenol ug/kg 15903880 41 10-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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[phone]
Page 45 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4017932MATRIX SPIKE SAMPLE:
MSSpike
Result
92666610002
Phenanthrene ug/kg 9641950 50 17-130ND
Phenol ug/kg 9161950 47 15-130ND
Pyrene ug/kg 10901950 56 31-130ND
Pyridine ug/kg 7151950 37 10-130ND
2,4,6-Tribromophenol (S)%48 10-131
2-Fluorobiphenyl (S)%45 10-130
2-Fluorophenol (S)%37 10-130
Nitrobenzene-d5 (S)%43 10-130
Phenol-d6 (S)%39 10-130
Terphenyl-d14 (S)%52 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92666610005
4017933SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg <162 30ND
1,2-Dichlorobenzene ug/kg <148 30ND
1,3-Dichlorobenzene ug/kg <145 30ND
1,4-Dichlorobenzene ug/kg <157 30ND
1-Methylnaphthalene ug/kg <144 30ND
2,2'-Oxybis(1-chloropropane)ug/kg <195 30ND
2,4,5-Trichlorophenol ug/kg <188 30ND
2,4,6-Trichlorophenol ug/kg <169 30ND
2,4-Dichlorophenol ug/kg <160 30ND
2,4-Dimethylphenol ug/kg <170 30ND
2,4-Dinitrophenol ug/kg <1270 30ND
2,4-Dinitrotoluene ug/kg <158 30ND
2,6-Dinitrotoluene ug/kg <150 30ND
2-Chloronaphthalene ug/kg <163 30ND
2-Chlorophenol ug/kg <154 30ND
2-Methylnaphthalene ug/kg <164 30ND
2-Methylphenol(o-Cresol)ug/kg <168 30ND
2-Nitroaniline ug/kg <336 30ND
2-Nitrophenol ug/kg <178 30ND
3&4-Methylphenol(m&p Cresol)ug/kg <165 30ND
3,3'-Dichlorobenzidine ug/kg <277 30ND
3-Nitroaniline ug/kg <322 30ND
4,6-Dinitro-2-methylphenol ug/kg <383 30ND
4-Bromophenylphenyl ether ug/kg <158 30ND
4-Chloro-3-methylphenol ug/kg <289 30ND
4-Chloroaniline ug/kg <322 30ND
4-Chlorophenylphenyl ether ug/kg <153 30ND
4-Nitroaniline ug/kg <312 30ND
4-Nitrophenol ug/kg <793 30ND
Acenaphthene ug/kg <144 30ND
Acenaphthylene ug/kg <144 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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[phone]
Page 46 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92666610005
4017933SAMPLE DUPLICATE:
Aniline ug/kg <160 30ND
Anthracene ug/kg <134 30ND
Benzo(a)anthracene ug/kg <137 30ND
Benzo(a)pyrene ug/kg <142 30ND
Benzo(b)fluoranthene ug/kg <137 30ND
Benzo(g,h,i)perylene ug/kg <159 30ND
Benzo(k)fluoranthene ug/kg <144 30ND
Benzoic Acid ug/kg <882 30ND
Benzyl alcohol ug/kg <311 30ND
bis(2-Chloroethoxy)methane ug/kg <170 30ND
bis(2-Chloroethyl) ether ug/kg <154 30ND
bis(2-Ethylhexyl)phthalate ug/kg <159 30ND
Butylbenzylphthalate ug/kg <173 30ND
Chrysene ug/kg <149 30ND
Di-n-butylphthalate ug/kg <138 30ND
Di-n-octylphthalate ug/kg <162 30ND
Dibenz(a,h)anthracene ug/kg <158 30ND
Dibenzofuran ug/kg <148 30ND
Diethylphthalate ug/kg <150 30ND
Dimethylphthalate ug/kg <149 30ND
Fluoranthene ug/kg <141 30ND
Fluorene ug/kg <144 30ND
Hexachloro-1,3-butadiene ug/kg <178 30ND
Hexachlorobenzene ug/kg <160 30ND
Hexachlorocyclopentadiene ug/kg <235 30ND
Hexachloroethane ug/kg <157 30ND
Indeno(1,2,3-cd)pyrene ug/kg <162 30ND
Isophorone ug/kg <183 30ND
N-Nitroso-di-n-propylamine ug/kg <154 30ND
N-Nitrosodimethylamine ug/kg <138 30ND
N-Nitrosodiphenylamine ug/kg <145 30ND
Naphthalene ug/kg <139 30ND
Nitrobenzene ug/kg <190 30ND
Pentachlorophenol ug/kg <402 30ND
Phenanthrene ug/kg <134 30ND
Phenol ug/kg <183 30ND
Pyrene ug/kg <167 30ND
Pyridine ug/kg <129 30ND
2,4,6-Tribromophenol (S)%6669
2-Fluorobiphenyl (S)%5646
2-Fluorophenol (S)%4944
Nitrobenzene-d5 (S)%5549
Phenol-d6 (S)%4944
Terphenyl-d14 (S)%5762
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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[phone]
Page 47 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
773944
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005, 92667059006, 92667059007,
92667059008, 92667059009, 92667059010
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667059001
4017158SAMPLE DUPLICATE:
Percent Moisture %26.3 N262524.9
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92666930006
4017159SAMPLE DUPLICATE:
Percent Moisture %21.8 N252520.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 48 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2059897
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3925200-1
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 05/15/23 14:16
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3925200-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667059001
R3925200-3SAMPLE DUPLICATE:
Total Solids %77.1 1.57 1078.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 55
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2061030
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3926139-1
Associated Lab Samples:92667059001, 92667059002, 92667059003, 92667059004, 92667059005
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg <0.255 1.00 05/17/23 17:130.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3926139-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 8.8010.0 88.0 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3926139-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667059005
R3926139-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 24.1 81.9 75.0-12579.5 2.85 2024.10.574 20.3 19.7
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3926139-6MATRIX SPIKE SAMPLE:
MSSpike
Result
92667059005
Chromium, Hexavalent mg/kg 938771 122 75.0-1250.574
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667059001
R3926139-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.553J D8,J20.8 200.681
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1616119-07
R3926139-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.683J D8,J29.5 200.507
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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[phone]
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The sample and duplicate results for this parameter are less than 5 times the reporting limit, the RPD may not be
statistically valid.D8
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in theassociated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 51 of 55
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92667059
LEN.008 FINAL GRADE SAMPLING
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92667059001 881324 881803FG-4 (0-2)EPA 3050B EPA 6020B
92667059002 881324 881803FG-5 (0-2)EPA 3050B EPA 6020B
92667059003 881324 881803FG-6 (0-2)EPA 3050B EPA 6020B
92667059004 881324 881803FG-7 (0-2)EPA 3050B EPA 6020B
92667059005 881324 881803FG-DUP-230509 (0-2)EPA 3050B EPA 6020B
92667059001 881325 881825FG-4 (0-2)EPA 7471B EPA 7471B
92667059002 881325 881825FG-5 (0-2)EPA 7471B EPA 7471B
92667059003 881325 881825FG-6 (0-2)EPA 7471B EPA 7471B
92667059004 881325 881825FG-7 (0-2)EPA 7471B EPA 7471B
92667059005 881325 881825FG-DUP-230509 (0-2)EPA 7471B EPA 7471B
92667059001 774150 774397FG-4 (0-2)EPA 3546 EPA 8270E
92667059002 774150 774397FG-5 (0-2)EPA 3546 EPA 8270E
92667059003 774150 774397FG-6 (0-2)EPA 3546 EPA 8270E
92667059004 774150 774397FG-7 (0-2)EPA 3546 EPA 8270E
92667059005 774150 774397FG-DUP-230509 (0-2)EPA 3546 EPA 8270E
92667059006 774002 774485FG-4 (1-2)EPA 5035A/5030B EPA 8260D
92667059007 774002 774485FG-5 (1-2)EPA 5035A/5030B EPA 8260D
92667059008 774002 774485FG-6 (1-2)EPA 5035A/5030B EPA 8260D
92667059009 774002 774485FG-7 (1-2)EPA 5035A/5030B EPA 8260D
92667059010 774002 774485FG-DUP-230509 (1-2)EPA 5035A/5030B EPA 8260D
92667059001 773944FG-4 (0-2)SW-846
92667059002 773944FG-5 (0-2)SW-846
92667059003 773944FG-6 (0-2)SW-846
92667059004 773944FG-7 (0-2)SW-846
92667059005 773944FG-DUP-230509 (0-2)SW-846
92667059006 773944FG-4 (1-2)SW-846
92667059007 773944FG-5 (1-2)SW-846
92667059008 773944FG-6 (1-2)SW-846
92667059009 773944FG-7 (1-2)SW-846
92667059010 773944FG-DUP-230509 (1-2)SW-846
92667059001 2059897 2059897FG-4 (0-2)SM 2540 G SM 2540G
92667059002 2059897 2059897FG-5 (0-2)SM 2540 G SM 2540G
92667059003 2059897 2059897FG-6 (0-2)SM 2540 G SM 2540G
92667059004 2059897 2059897FG-7 (0-2)SM 2540 G SM 2540G
92667059005 2059897 2059897FG-DUP-230509 (0-2)SM 2540 G SM 2540G
92667059001 2061030 2061030FG-4 (0-2)3060A EPA 7199
92667059002 2061030 2061030FG-5 (0-2)3060A EPA 7199
92667059003 2061030 2061030FG-6 (0-2)3060A EPA 7199
92667059004 2061030 2061030FG-7 (0-2)3060A EPA 7199
92667059005 2061030 2061030FG-DUP-230509 (0-2)3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/18/2023 03:51 PM
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Page 52 of 55
Page 53 of 55
Page 54 of 55
Page 55 of 55
#=CL#
March 08, 2023
LIMS USE: FR - HALEY MARTIN
LIMS OBJECT ID: 92653934
92653934
Project:
Pace Project No.:
RE:
Haley Martin
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
LEN-008
Dear Haley Martin:
Enclosed are the analytical results for sample(s) received by the laboratory on February 24, 2023. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 75
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92653934
LEN-008
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
1800 Elm Street SE, Minneapolis, MN 55414--Satellite Air
Lab
A2LA Certification #: 2926.01*
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009*
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014*
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605*
Georgia Certification #: 959
GMP+ Certification #: GMP050884
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086*
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064*
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137*
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240*
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081*
New Jersey Certification #: MN002
New York Certification #: 11647*
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Ohio VAP Certification (1800) #: CL110*
Oklahoma Certification #: 9507*
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001*
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192*
Utah Certification #: MN00064*
Vermont Certification #: VT-027053137
Virginia Certification #: 460163*
Washington Certification #: C486*
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
*Please Note: Applicable air certifications are denoted with
an asterisk (*).
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 75
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92653934
LEN-008
Pace Analytical Services National
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 998093910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 75
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92653934
LEN-008
Lab ID Sample ID Matrix Date Collected Date Received
92653934001 FG-1 (0-2)Solid 02/23/23 10:45 02/24/23 12:41
92653934002 FG-2 (0-2)Solid 02/23/23 12:40 02/24/23 12:41
92653934003 FG-3 (0-2)Solid 02/23/23 14:00 02/24/23 12:41
92653934004 FG-8 (0-2)Solid 02/23/23 15:15 02/24/23 12:41
92653934005 FG-9 (0-2)Solid 02/23/23 16:25 02/24/23 12:41
92653934006 FG-10 (0-2)Solid 02/24/23 10:30 02/24/23 12:41
92653934007 FG-DUP (0-2)Solid 02/23/23 00:00 02/24/23 12:41
92653934008 FG-1 (1-2)Solid 02/23/23 10:45 02/24/23 12:41
92653934009 FG-2 (1-2)Solid 02/23/23 12:40 02/24/23 12:41
92653934010 FG-3 (1-2)Solid 02/23/23 14:00 02/24/23 12:41
92653934011 FG-8 (1-2)Solid 02/23/23 15:15 02/24/23 12:41
92653934012 FG-9 (1-2)Solid 02/23/23 16:25 02/24/23 12:41
92653934013 FG-10 (0-1)Solid 02/24/23 10:30 02/24/23 12:41
92653934014 FG-DUP (1-2)Solid 02/23/23 00:00 02/24/23 12:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 75
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92653934
LEN-008
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92653934001 FG-1 (0-2)EPA 6020B 7 PASI-MTJ1
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92653934002 FG-2 (0-2)EPA 6020B 7 PASI-MTJ1
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92653934003 FG-3 (0-2)EPA 6020B 7 PASI-MTJ1
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92653934004 FG-8 (0-2)EPA 6020B 7 PASI-MTJ1
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92653934005 FG-9 (0-2)EPA 6020B 7 PASI-MTJ1
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92653934006 FG-10 (0-2)EPA 6020B 7 PASI-MTJ1
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92653934007 FG-DUP (0-2)EPA 6020B 7 PASI-MTJ1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 75
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92653934
LEN-008
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 7471B 1 PASI-MLMW
EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92653934008 FG-1 (1-2)EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92653934009 FG-2 (1-2)EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92653934010 FG-3 (1-2)EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92653934011 FG-8 (1-2)EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92653934012 FG-9 (1-2)EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92653934013 FG-10 (0-1)EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92653934014 FG-DUP (1-2)EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PAN = Pace National - Mt. Juliet
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-1 (0-2)Lab ID:92653934001 Collected:02/23/23 10:45 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.4 mg/kg 03/01/23 11:15 7440-38-202/28/23 11:260.64 0.18 1
Barium 23.9 mg/kg 03/01/23 11:15 7440-39-302/28/23 11:260.39 0.096 1
Cadmium <0.038 mg/kg 03/01/23 11:15 7440-43-902/28/23 11:260.10 0.038 1
Chromium 44.2 mg/kg 03/01/23 11:15 7440-47-302/28/23 11:262.6 0.50 1
Lead 11.5 mg/kg 03/01/23 11:15 7439-92-102/28/23 11:260.64 0.12 1
Selenium 0.69 mg/kg 03/01/23 11:15 7782-49-202/28/23 11:260.64 0.14 1
Silver <0.26 mg/kg 03/01/23 11:15 7440-22-402/28/23 11:260.64 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.035 mg/kg 03/02/23 15:27 7439-97-602/28/23 11:370.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <152 ug/kg 03/01/23 19:05 83-32-902/28/23 06:444311521
Acenaphthylene <152 ug/kg 03/01/23 19:05 208-96-802/28/23 06:444311521
Aniline <168 ug/kg 03/01/23 19:05 62-53-302/28/23 06:444311681
Anthracene <141 ug/kg 03/01/23 19:05 120-12-702/28/23 06:444311411
Benzo(a)anthracene <144 ug/kg 03/01/23 19:05 56-55-302/28/23 06:444311441
Benzo(a)pyrene <149 ug/kg 03/01/23 19:05 50-32-802/28/23 06:444311491
Benzo(b)fluoranthene <144 ug/kg 03/01/23 19:05 205-99-202/28/23 06:444311441
Benzo(g,h,i)perylene <167 ug/kg 03/01/23 19:05 191-24-202/28/23 06:444311671
Benzo(k)fluoranthene <152 ug/kg 03/01/23 19:05 207-08-902/28/23 06:444311521
Benzoic Acid <926 ug/kg 03/01/23 19:05 65-85-002/28/23 06:4421609261
Benzyl alcohol <327 ug/kg 03/01/23 19:05 100-51-602/28/23 06:448623271
4-Bromophenylphenyl ether <166 ug/kg 03/01/23 19:05 101-55-302/28/23 06:444311661
Butylbenzylphthalate <182 ug/kg 03/01/23 19:05 85-68-702/28/23 06:444311821
4-Chloro-3-methylphenol <303 ug/kg 03/01/23 19:05 59-50-702/28/23 06:448623031
4-Chloroaniline <338 ug/kg 03/01/23 19:05 106-47-802/28/23 06:448623381
bis(2-Chloroethoxy)methane <179 ug/kg 03/01/23 19:05 111-91-102/28/23 06:444311791
bis(2-Chloroethyl) ether <162 ug/kg 03/01/23 19:05 111-44-402/28/23 06:444311621
2-Chloronaphthalene <171 ug/kg 03/01/23 19:05 91-58-702/28/23 06:444311711
2-Chlorophenol <162 ug/kg 03/01/23 19:05 95-57-802/28/23 06:444311621
4-Chlorophenylphenyl ether <161 ug/kg 03/01/23 19:05 7005-72-302/28/23 06:444311611
Chrysene <157 ug/kg 03/01/23 19:05 218-01-902/28/23 06:444311571
Dibenz(a,h)anthracene <166 ug/kg 03/01/23 19:05 53-70-302/28/23 06:444311661
Dibenzofuran <155 ug/kg 03/01/23 19:05 132-64-902/28/23 06:444311551
1,2-Dichlorobenzene <155 ug/kg 03/01/23 19:05 95-50-102/28/23 06:444311551
1,3-Dichlorobenzene <153 ug/kg 03/01/23 19:05 541-73-102/28/23 06:444311531
1,4-Dichlorobenzene <165 ug/kg 03/01/23 19:05 106-46-702/28/23 06:444311651
3,3'-Dichlorobenzidine <291 ug/kg 03/01/23 19:05 91-94-102/28/23 06:448622911
2,4-Dichlorophenol <168 ug/kg 03/01/23 19:05 120-83-202/28/23 06:444311681
Diethylphthalate <158 ug/kg 03/01/23 19:05 84-66-202/28/23 06:444311581
2,4-Dimethylphenol <179 ug/kg 03/01/23 19:05 105-67-902/28/23 06:444311791
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-1 (0-2)Lab ID:92653934001 Collected:02/23/23 10:45 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <157 ug/kg 03/01/23 19:05 131-11-302/28/23 06:444311571
Di-n-butylphthalate <145 ug/kg 03/01/23 19:05 84-74-202/28/23 06:444311451
4,6-Dinitro-2-methylphenol <402 ug/kg 03/01/23 19:05 534-52-102/28/23 06:448624021
2,4-Dinitrophenol <1330 ug/kg 03/01/23 19:05 51-28-502/28/23 06:44216013301
2,4-Dinitrotoluene <166 ug/kg 03/01/23 19:05 121-14-202/28/23 06:444311661
2,6-Dinitrotoluene <158 ug/kg 03/01/23 19:05 606-20-202/28/23 06:444311581
Di-n-octylphthalate <170 ug/kg 03/01/23 19:05 117-84-002/28/23 06:444311701
bis(2-Ethylhexyl)phthalate <167 ug/kg 03/01/23 19:05 117-81-702/28/23 06:444311671
Fluoranthene <148 ug/kg 03/01/23 19:05 206-44-002/28/23 06:444311481
Fluorene <152 ug/kg 03/01/23 19:05 86-73-702/28/23 06:444311521
Hexachloro-1,3-butadiene <187 ug/kg 03/01/23 19:05 87-68-302/28/23 06:444311871
Hexachlorobenzene <168 ug/kg 03/01/23 19:05 118-74-102/28/23 06:444311681
Hexachlorocyclopentadiene <247 ug/kg 03/01/23 19:05 77-47-402/28/23 06:444312471
Hexachloroethane <165 ug/kg 03/01/23 19:05 67-72-102/28/23 06:444311651
Indeno(1,2,3-cd)pyrene <170 ug/kg 03/01/23 19:05 193-39-502/28/23 06:444311701
Isophorone <192 ug/kg 03/01/23 19:05 78-59-102/28/23 06:444311921
1-Methylnaphthalene <152 ug/kg 03/01/23 19:05 90-12-002/28/23 06:444311521
2-Methylnaphthalene <172 ug/kg 03/01/23 19:05 91-57-602/28/23 06:444311721
2-Methylphenol(o-Cresol)<176 ug/kg 03/01/23 19:05 95-48-702/28/23 06:444311761
3&4-Methylphenol(m&p Cresol)<174 ug/kg 03/01/23 19:05 15831-10-402/28/23 06:444311741
Naphthalene <146 ug/kg 03/01/23 19:05 91-20-302/28/23 06:444311461
2-Nitroaniline <353 ug/kg 03/01/23 19:05 88-74-402/28/23 06:4421603531
3-Nitroaniline <338 ug/kg 03/01/23 19:05 99-09-202/28/23 06:4421603381
4-Nitroaniline <328 ug/kg 03/01/23 19:05 100-01-602/28/23 06:448623281
Nitrobenzene <200 ug/kg 03/01/23 19:05 98-95-302/28/23 06:444312001
2-Nitrophenol <187 ug/kg 03/01/23 19:05 88-75-502/28/23 06:444311871
4-Nitrophenol <833 ug/kg 03/01/23 19:05 100-02-702/28/23 06:4421608331
N-Nitrosodimethylamine <145 ug/kg 03/01/23 19:05 62-75-902/28/23 06:444311451
N-Nitroso-di-n-propylamine <162 ug/kg 03/01/23 19:05 621-64-702/28/23 06:444311621
N-Nitrosodiphenylamine <153 ug/kg 03/01/23 19:05 86-30-602/28/23 06:444311531
2,2'-Oxybis(1-chloropropane)<205 ug/kg 03/01/23 19:05 108-60-102/28/23 06:444312051
Pentachlorophenol <422 ug/kg 03/01/23 19:05 87-86-502/28/23 06:448624221
Phenanthrene <141 ug/kg 03/01/23 19:05 85-01-802/28/23 06:444311411
Phenol <192 ug/kg 03/01/23 19:05 108-95-202/28/23 06:444311921
Pyrene <175 ug/kg 03/01/23 19:05 129-00-002/28/23 06:444311751
Pyridine <136 ug/kg 03/01/23 19:05 110-86-102/28/23 06:444311361
1,2,4-Trichlorobenzene <170 ug/kg 03/01/23 19:05 120-82-102/28/23 06:444311701
2,4,5-Trichlorophenol <197 ug/kg 03/01/23 19:05 95-95-402/28/23 06:444311971
2,4,6-Trichlorophenol <178 ug/kg 03/01/23 19:05 88-06-202/28/23 06:444311781
Surrogates
Nitrobenzene-d5 (S)68 %03/01/23 19:05 4165-60-002/28/23 06:4410-130 1
2-Fluorobiphenyl (S)73 %03/01/23 19:05 321-60-802/28/23 06:4410-130 1
Terphenyl-d14 (S)64 %03/01/23 19:05 1718-51-002/28/23 06:4410-130 1
Phenol-d6 (S)69 %03/01/23 19:05 13127-88-302/28/23 06:4410-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-1 (0-2)Lab ID:92653934001 Collected:02/23/23 10:45 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)66 %03/01/23 19:05 367-12-402/28/23 06:4410-130 1
2,4,6-Tribromophenol (S)81 %03/01/23 19:05 118-79-602/28/23 06:4410-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.7 %02/24/23 17:06 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 77.6 %02/27/23 13:4002/27/23 13:321
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent <0.329 mg/kg 02/28/23 12:54 18540-29-902/28/23 03:401.29 0.329 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-2 (0-2)Lab ID:92653934002 Collected:02/23/23 12:40 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.7 mg/kg 02/28/23 18:30 7440-38-202/28/23 11:260.63 0.18 1
Barium 73.5 mg/kg 02/28/23 18:30 7440-39-302/28/23 11:260.38 0.095 1
Cadmium 0.044J mg/kg 02/28/23 18:30 7440-43-902/28/23 11:260.10 0.037 1
Chromium 35.1 mg/kg 02/28/23 18:30 7440-47-302/28/23 11:262.5 0.49 1
Lead 10.1 mg/kg 02/28/23 18:30 7439-92-102/28/23 11:260.63 0.12 1
Selenium 0.47J mg/kg 02/28/23 18:30 7782-49-202/28/23 11:260.63 0.13 1
Silver <0.26 mg/kg 02/28/23 18:30 7440-22-402/28/23 11:260.63 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.034 mg/kg 03/02/23 15:32 7439-97-602/28/23 11:370.024 0.010 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <148 ug/kg 03/01/23 19:33 83-32-902/28/23 06:444211481
Acenaphthylene <148 ug/kg 03/01/23 19:33 208-96-802/28/23 06:444211481
Aniline <164 ug/kg 03/01/23 19:33 62-53-302/28/23 06:444211641
Anthracene <138 ug/kg 03/01/23 19:33 120-12-702/28/23 06:444211381
Benzo(a)anthracene <140 ug/kg 03/01/23 19:33 56-55-302/28/23 06:444211401
Benzo(a)pyrene <145 ug/kg 03/01/23 19:33 50-32-802/28/23 06:444211451
Benzo(b)fluoranthene <140 ug/kg 03/01/23 19:33 205-99-202/28/23 06:444211401
Benzo(g,h,i)perylene <163 ug/kg 03/01/23 19:33 191-24-202/28/23 06:444211631
Benzo(k)fluoranthene <148 ug/kg 03/01/23 19:33 207-08-902/28/23 06:444211481
Benzoic Acid <904 ug/kg 03/01/23 19:33 65-85-002/28/23 06:4421009041
Benzyl alcohol <319 ug/kg 03/01/23 19:33 100-51-602/28/23 06:448413191
4-Bromophenylphenyl ether <162 ug/kg 03/01/23 19:33 101-55-302/28/23 06:444211621
Butylbenzylphthalate <177 ug/kg 03/01/23 19:33 85-68-702/28/23 06:444211771
4-Chloro-3-methylphenol <296 ug/kg 03/01/23 19:33 59-50-702/28/23 06:448412961
4-Chloroaniline <330 ug/kg 03/01/23 19:33 106-47-802/28/23 06:448413301
bis(2-Chloroethoxy)methane <175 ug/kg 03/01/23 19:33 111-91-102/28/23 06:444211751
bis(2-Chloroethyl) ether <158 ug/kg 03/01/23 19:33 111-44-402/28/23 06:444211581
2-Chloronaphthalene <167 ug/kg 03/01/23 19:33 91-58-702/28/23 06:444211671
2-Chlorophenol <158 ug/kg 03/01/23 19:33 95-57-802/28/23 06:444211581
4-Chlorophenylphenyl ether <157 ug/kg 03/01/23 19:33 7005-72-302/28/23 06:444211571
Chrysene <153 ug/kg 03/01/23 19:33 218-01-902/28/23 06:444211531
Dibenz(a,h)anthracene <162 ug/kg 03/01/23 19:33 53-70-302/28/23 06:444211621
Dibenzofuran <152 ug/kg 03/01/23 19:33 132-64-902/28/23 06:444211521
1,2-Dichlorobenzene <152 ug/kg 03/01/23 19:33 95-50-102/28/23 06:444211521
1,3-Dichlorobenzene <149 ug/kg 03/01/23 19:33 541-73-102/28/23 06:444211491
1,4-Dichlorobenzene <161 ug/kg 03/01/23 19:33 106-46-702/28/23 06:444211611
3,3'-Dichlorobenzidine <284 ug/kg 03/01/23 19:33 91-94-102/28/23 06:448412841
2,4-Dichlorophenol <164 ug/kg 03/01/23 19:33 120-83-202/28/23 06:444211641
Diethylphthalate <154 ug/kg 03/01/23 19:33 84-66-202/28/23 06:444211541
2,4-Dimethylphenol <175 ug/kg 03/01/23 19:33 105-67-902/28/23 06:444211751
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-2 (0-2)Lab ID:92653934002 Collected:02/23/23 12:40 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <153 ug/kg 03/01/23 19:33 131-11-302/28/23 06:444211531
Di-n-butylphthalate <141 ug/kg 03/01/23 19:33 84-74-202/28/23 06:444211411
4,6-Dinitro-2-methylphenol <392 ug/kg 03/01/23 19:33 534-52-102/28/23 06:448413921
2,4-Dinitrophenol <1300 ug/kg 03/01/23 19:33 51-28-502/28/23 06:44210013001
2,4-Dinitrotoluene <162 ug/kg 03/01/23 19:33 121-14-202/28/23 06:444211621
2,6-Dinitrotoluene <154 ug/kg 03/01/23 19:33 606-20-202/28/23 06:444211541
Di-n-octylphthalate <166 ug/kg 03/01/23 19:33 117-84-002/28/23 06:444211661
bis(2-Ethylhexyl)phthalate <163 ug/kg 03/01/23 19:33 117-81-702/28/23 06:444211631
Fluoranthene <144 ug/kg 03/01/23 19:33 206-44-002/28/23 06:444211441
Fluorene <148 ug/kg 03/01/23 19:33 86-73-702/28/23 06:444211481
Hexachloro-1,3-butadiene <182 ug/kg 03/01/23 19:33 87-68-302/28/23 06:444211821
Hexachlorobenzene <164 ug/kg 03/01/23 19:33 118-74-102/28/23 06:444211641
Hexachlorocyclopentadiene <241 ug/kg 03/01/23 19:33 77-47-402/28/23 06:444212411
Hexachloroethane <161 ug/kg 03/01/23 19:33 67-72-102/28/23 06:444211611
Indeno(1,2,3-cd)pyrene <166 ug/kg 03/01/23 19:33 193-39-502/28/23 06:444211661
Isophorone <187 ug/kg 03/01/23 19:33 78-59-102/28/23 06:444211871
1-Methylnaphthalene <148 ug/kg 03/01/23 19:33 90-12-002/28/23 06:444211481
2-Methylnaphthalene <168 ug/kg 03/01/23 19:33 91-57-602/28/23 06:444211681
2-Methylphenol(o-Cresol)<172 ug/kg 03/01/23 19:33 95-48-702/28/23 06:444211721
3&4-Methylphenol(m&p Cresol)<169 ug/kg 03/01/23 19:33 15831-10-402/28/23 06:444211691
Naphthalene <143 ug/kg 03/01/23 19:33 91-20-302/28/23 06:444211431
2-Nitroaniline <344 ug/kg 03/01/23 19:33 88-74-402/28/23 06:4421003441
3-Nitroaniline <330 ug/kg 03/01/23 19:33 99-09-202/28/23 06:4421003301
4-Nitroaniline <320 ug/kg 03/01/23 19:33 100-01-602/28/23 06:448413201
Nitrobenzene <195 ug/kg 03/01/23 19:33 98-95-302/28/23 06:444211951
2-Nitrophenol <182 ug/kg 03/01/23 19:33 88-75-502/28/23 06:444211821
4-Nitrophenol <813 ug/kg 03/01/23 19:33 100-02-702/28/23 06:4421008131
N-Nitrosodimethylamine <141 ug/kg 03/01/23 19:33 62-75-902/28/23 06:444211411
N-Nitroso-di-n-propylamine <158 ug/kg 03/01/23 19:33 621-64-702/28/23 06:444211581
N-Nitrosodiphenylamine <149 ug/kg 03/01/23 19:33 86-30-602/28/23 06:444211491
2,2'-Oxybis(1-chloropropane)<200 ug/kg 03/01/23 19:33 108-60-102/28/23 06:444212001
Pentachlorophenol <412 ug/kg 03/01/23 19:33 87-86-502/28/23 06:448414121
Phenanthrene <138 ug/kg 03/01/23 19:33 85-01-802/28/23 06:444211381
Phenol <187 ug/kg 03/01/23 19:33 108-95-202/28/23 06:444211871
Pyrene <171 ug/kg 03/01/23 19:33 129-00-002/28/23 06:444211711
Pyridine <133 ug/kg 03/01/23 19:33 110-86-102/28/23 06:444211331
1,2,4-Trichlorobenzene <166 ug/kg 03/01/23 19:33 120-82-102/28/23 06:444211661
2,4,5-Trichlorophenol <192 ug/kg 03/01/23 19:33 95-95-402/28/23 06:444211921
2,4,6-Trichlorophenol <173 ug/kg 03/01/23 19:33 88-06-202/28/23 06:444211731
Surrogates
Nitrobenzene-d5 (S)68 %03/01/23 19:33 4165-60-002/28/23 06:4410-130 1
2-Fluorobiphenyl (S)69 %03/01/23 19:33 321-60-802/28/23 06:4410-130 1
Terphenyl-d14 (S)63 %03/01/23 19:33 1718-51-002/28/23 06:4410-130 1
Phenol-d6 (S)67 %03/01/23 19:33 13127-88-302/28/23 06:4410-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-2 (0-2)Lab ID:92653934002 Collected:02/23/23 12:40 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)65 %03/01/23 19:33 367-12-402/28/23 06:4410-130 1
2,4,6-Tribromophenol (S)80 %03/01/23 19:33 118-79-602/28/23 06:4410-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.3 %02/24/23 17:06 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 82.1 %02/27/23 13:4002/27/23 13:321
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent <0.311 mg/kg 02/28/23 12:59 18540-29-9 D802/28/23 03:401.22 0.311 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-3 (0-2)Lab ID:92653934003 Collected:02/23/23 14:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.4 mg/kg 02/28/23 18:34 7440-38-202/28/23 11:260.62 0.18 1
Barium 45.4 mg/kg 02/28/23 18:34 7440-39-302/28/23 11:260.37 0.093 1
Cadmium <0.037 mg/kg 02/28/23 18:34 7440-43-902/28/23 11:260.099 0.037 1
Chromium 27.2 mg/kg 02/28/23 18:34 7440-47-302/28/23 11:262.5 0.48 1
Lead 9.2 mg/kg 02/28/23 18:34 7439-92-102/28/23 11:260.62 0.12 1
Selenium 0.27J mg/kg 02/28/23 18:34 7782-49-202/28/23 11:260.62 0.13 1
Silver <0.25 mg/kg 02/28/23 18:34 7440-22-402/28/23 11:260.62 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.029 mg/kg 03/02/23 15:34 7439-97-602/28/23 11:370.024 0.010 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <148 ug/kg 03/01/23 20:01 83-32-902/28/23 06:444211481
Acenaphthylene <148 ug/kg 03/01/23 20:01 208-96-802/28/23 06:444211481
Aniline <164 ug/kg 03/01/23 20:01 62-53-302/28/23 06:444211641
Anthracene <138 ug/kg 03/01/23 20:01 120-12-702/28/23 06:444211381
Benzo(a)anthracene <140 ug/kg 03/01/23 20:01 56-55-302/28/23 06:444211401
Benzo(a)pyrene <145 ug/kg 03/01/23 20:01 50-32-802/28/23 06:444211451
Benzo(b)fluoranthene <140 ug/kg 03/01/23 20:01 205-99-202/28/23 06:444211401
Benzo(g,h,i)perylene <163 ug/kg 03/01/23 20:01 191-24-202/28/23 06:444211631
Benzo(k)fluoranthene <148 ug/kg 03/01/23 20:01 207-08-902/28/23 06:444211481
Benzoic Acid <903 ug/kg 03/01/23 20:01 65-85-002/28/23 06:4421009031
Benzyl alcohol <319 ug/kg 03/01/23 20:01 100-51-602/28/23 06:448413191
4-Bromophenylphenyl ether <162 ug/kg 03/01/23 20:01 101-55-302/28/23 06:444211621
Butylbenzylphthalate <177 ug/kg 03/01/23 20:01 85-68-702/28/23 06:444211771
4-Chloro-3-methylphenol <296 ug/kg 03/01/23 20:01 59-50-702/28/23 06:448412961
4-Chloroaniline <330 ug/kg 03/01/23 20:01 106-47-802/28/23 06:448413301
bis(2-Chloroethoxy)methane <175 ug/kg 03/01/23 20:01 111-91-102/28/23 06:444211751
bis(2-Chloroethyl) ether <158 ug/kg 03/01/23 20:01 111-44-402/28/23 06:444211581
2-Chloronaphthalene <167 ug/kg 03/01/23 20:01 91-58-702/28/23 06:444211671
2-Chlorophenol <158 ug/kg 03/01/23 20:01 95-57-802/28/23 06:444211581
4-Chlorophenylphenyl ether <157 ug/kg 03/01/23 20:01 7005-72-302/28/23 06:444211571
Chrysene <153 ug/kg 03/01/23 20:01 218-01-902/28/23 06:444211531
Dibenz(a,h)anthracene <162 ug/kg 03/01/23 20:01 53-70-302/28/23 06:444211621
Dibenzofuran <152 ug/kg 03/01/23 20:01 132-64-902/28/23 06:444211521
1,2-Dichlorobenzene <152 ug/kg 03/01/23 20:01 95-50-102/28/23 06:444211521
1,3-Dichlorobenzene <149 ug/kg 03/01/23 20:01 541-73-102/28/23 06:444211491
1,4-Dichlorobenzene <161 ug/kg 03/01/23 20:01 106-46-702/28/23 06:444211611
3,3'-Dichlorobenzidine <284 ug/kg 03/01/23 20:01 91-94-102/28/23 06:448412841
2,4-Dichlorophenol <164 ug/kg 03/01/23 20:01 120-83-202/28/23 06:444211641
Diethylphthalate <154 ug/kg 03/01/23 20:01 84-66-202/28/23 06:444211541
2,4-Dimethylphenol <175 ug/kg 03/01/23 20:01 105-67-902/28/23 06:444211751
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-3 (0-2)Lab ID:92653934003 Collected:02/23/23 14:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <153 ug/kg 03/01/23 20:01 131-11-302/28/23 06:444211531
Di-n-butylphthalate <141 ug/kg 03/01/23 20:01 84-74-202/28/23 06:444211411
4,6-Dinitro-2-methylphenol <392 ug/kg 03/01/23 20:01 534-52-102/28/23 06:448413921
2,4-Dinitrophenol <1300 ug/kg 03/01/23 20:01 51-28-502/28/23 06:44210013001
2,4-Dinitrotoluene <162 ug/kg 03/01/23 20:01 121-14-202/28/23 06:444211621
2,6-Dinitrotoluene <154 ug/kg 03/01/23 20:01 606-20-202/28/23 06:444211541
Di-n-octylphthalate <166 ug/kg 03/01/23 20:01 117-84-002/28/23 06:444211661
bis(2-Ethylhexyl)phthalate <163 ug/kg 03/01/23 20:01 117-81-702/28/23 06:444211631
Fluoranthene <144 ug/kg 03/01/23 20:01 206-44-002/28/23 06:444211441
Fluorene <148 ug/kg 03/01/23 20:01 86-73-702/28/23 06:444211481
Hexachloro-1,3-butadiene <182 ug/kg 03/01/23 20:01 87-68-302/28/23 06:444211821
Hexachlorobenzene <164 ug/kg 03/01/23 20:01 118-74-102/28/23 06:444211641
Hexachlorocyclopentadiene <241 ug/kg 03/01/23 20:01 77-47-402/28/23 06:444212411
Hexachloroethane <161 ug/kg 03/01/23 20:01 67-72-102/28/23 06:444211611
Indeno(1,2,3-cd)pyrene <166 ug/kg 03/01/23 20:01 193-39-502/28/23 06:444211661
Isophorone <187 ug/kg 03/01/23 20:01 78-59-102/28/23 06:444211871
1-Methylnaphthalene <148 ug/kg 03/01/23 20:01 90-12-002/28/23 06:444211481
2-Methylnaphthalene <168 ug/kg 03/01/23 20:01 91-57-602/28/23 06:444211681
2-Methylphenol(o-Cresol)<172 ug/kg 03/01/23 20:01 95-48-702/28/23 06:444211721
3&4-Methylphenol(m&p Cresol)<169 ug/kg 03/01/23 20:01 15831-10-402/28/23 06:444211691
Naphthalene <143 ug/kg 03/01/23 20:01 91-20-302/28/23 06:444211431
2-Nitroaniline <344 ug/kg 03/01/23 20:01 88-74-402/28/23 06:4421003441
3-Nitroaniline <330 ug/kg 03/01/23 20:01 99-09-202/28/23 06:4421003301
4-Nitroaniline <320 ug/kg 03/01/23 20:01 100-01-602/28/23 06:448413201
Nitrobenzene <195 ug/kg 03/01/23 20:01 98-95-302/28/23 06:444211951
2-Nitrophenol <182 ug/kg 03/01/23 20:01 88-75-502/28/23 06:444211821
4-Nitrophenol <813 ug/kg 03/01/23 20:01 100-02-702/28/23 06:4421008131
N-Nitrosodimethylamine <141 ug/kg 03/01/23 20:01 62-75-902/28/23 06:444211411
N-Nitroso-di-n-propylamine <158 ug/kg 03/01/23 20:01 621-64-702/28/23 06:444211581
N-Nitrosodiphenylamine <149 ug/kg 03/01/23 20:01 86-30-602/28/23 06:444211491
2,2'-Oxybis(1-chloropropane)<200 ug/kg 03/01/23 20:01 108-60-102/28/23 06:444212001
Pentachlorophenol <412 ug/kg 03/01/23 20:01 87-86-502/28/23 06:448414121
Phenanthrene <138 ug/kg 03/01/23 20:01 85-01-802/28/23 06:444211381
Phenol <187 ug/kg 03/01/23 20:01 108-95-202/28/23 06:444211871
Pyrene <171 ug/kg 03/01/23 20:01 129-00-002/28/23 06:444211711
Pyridine <133 ug/kg 03/01/23 20:01 110-86-102/28/23 06:444211331
1,2,4-Trichlorobenzene <166 ug/kg 03/01/23 20:01 120-82-102/28/23 06:444211661
2,4,5-Trichlorophenol <192 ug/kg 03/01/23 20:01 95-95-402/28/23 06:444211921
2,4,6-Trichlorophenol <173 ug/kg 03/01/23 20:01 88-06-202/28/23 06:444211731
Surrogates
Nitrobenzene-d5 (S)61 %03/01/23 20:01 4165-60-002/28/23 06:4410-130 1
2-Fluorobiphenyl (S)69 %03/01/23 20:01 321-60-802/28/23 06:4410-130 1
Terphenyl-d14 (S)57 %03/01/23 20:01 1718-51-002/28/23 06:4410-130 1
Phenol-d6 (S)59 %03/01/23 20:01 13127-88-302/28/23 06:4410-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-3 (0-2)Lab ID:92653934003 Collected:02/23/23 14:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)53 %03/01/23 20:01 367-12-402/28/23 06:4410-130 1
2,4,6-Tribromophenol (S)66 %03/01/23 20:01 118-79-602/28/23 06:4410-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.5 %02/24/23 17:06 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 79.4 %02/27/23 13:4002/27/23 13:321
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.83 mg/kg 02/28/23 13:20 18540-29-902/28/23 03:401.26 0.321 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-8 (0-2)Lab ID:92653934004 Collected:02/23/23 15:15 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.6 mg/kg 02/28/23 18:37 7440-38-202/28/23 11:260.67 0.19 1
Barium 123 mg/kg 02/28/23 18:37 7440-39-302/28/23 11:260.40 0.10 1
Cadmium 0.045J mg/kg 02/28/23 18:37 7440-43-902/28/23 11:260.11 0.039 1
Chromium 30.7 mg/kg 02/28/23 18:37 7440-47-302/28/23 11:262.7 0.52 1
Lead 12.9 mg/kg 02/28/23 18:37 7439-92-102/28/23 11:260.67 0.12 1
Selenium 0.38J mg/kg 02/28/23 18:37 7782-49-202/28/23 11:260.67 0.14 1
Silver <0.27 mg/kg 02/28/23 18:37 7440-22-402/28/23 11:260.67 0.27 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.056 mg/kg 03/02/23 15:35 7439-97-602/28/23 11:370.024 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <153 ug/kg 03/01/23 20:29 83-32-902/28/23 06:444361531
Acenaphthylene <153 ug/kg 03/01/23 20:29 208-96-802/28/23 06:444361531
Aniline <170 ug/kg 03/01/23 20:29 62-53-302/28/23 06:444361701
Anthracene <143 ug/kg 03/01/23 20:29 120-12-702/28/23 06:444361431
Benzo(a)anthracene <145 ug/kg 03/01/23 20:29 56-55-302/28/23 06:444361451
Benzo(a)pyrene <151 ug/kg 03/01/23 20:29 50-32-802/28/23 06:444361511
Benzo(b)fluoranthene <145 ug/kg 03/01/23 20:29 205-99-202/28/23 06:444361451
Benzo(g,h,i)perylene <169 ug/kg 03/01/23 20:29 191-24-202/28/23 06:444361691
Benzo(k)fluoranthene <153 ug/kg 03/01/23 20:29 207-08-902/28/23 06:444361531
Benzoic Acid <937 ug/kg 03/01/23 20:29 65-85-002/28/23 06:4421809371
Benzyl alcohol <330 ug/kg 03/01/23 20:29 100-51-602/28/23 06:448723301
4-Bromophenylphenyl ether <168 ug/kg 03/01/23 20:29 101-55-302/28/23 06:444361681
Butylbenzylphthalate <184 ug/kg 03/01/23 20:29 85-68-702/28/23 06:444361841
4-Chloro-3-methylphenol <307 ug/kg 03/01/23 20:29 59-50-702/28/23 06:448723071
4-Chloroaniline <342 ug/kg 03/01/23 20:29 106-47-802/28/23 06:448723421
bis(2-Chloroethoxy)methane <181 ug/kg 03/01/23 20:29 111-91-102/28/23 06:444361811
bis(2-Chloroethyl) ether <164 ug/kg 03/01/23 20:29 111-44-402/28/23 06:444361641
2-Chloronaphthalene <173 ug/kg 03/01/23 20:29 91-58-702/28/23 06:444361731
2-Chlorophenol <164 ug/kg 03/01/23 20:29 95-57-802/28/23 06:444361641
4-Chlorophenylphenyl ether <163 ug/kg 03/01/23 20:29 7005-72-302/28/23 06:444361631
Chrysene <159 ug/kg 03/01/23 20:29 218-01-902/28/23 06:444361591
Dibenz(a,h)anthracene <168 ug/kg 03/01/23 20:29 53-70-302/28/23 06:444361681
Dibenzofuran <157 ug/kg 03/01/23 20:29 132-64-902/28/23 06:444361571
1,2-Dichlorobenzene <157 ug/kg 03/01/23 20:29 95-50-102/28/23 06:444361571
1,3-Dichlorobenzene <155 ug/kg 03/01/23 20:29 541-73-102/28/23 06:444361551
1,4-Dichlorobenzene <166 ug/kg 03/01/23 20:29 106-46-702/28/23 06:444361661
3,3'-Dichlorobenzidine <295 ug/kg 03/01/23 20:29 91-94-102/28/23 06:448722951
2,4-Dichlorophenol <170 ug/kg 03/01/23 20:29 120-83-202/28/23 06:444361701
Diethylphthalate <160 ug/kg 03/01/23 20:29 84-66-202/28/23 06:444361601
2,4-Dimethylphenol <181 ug/kg 03/01/23 20:29 105-67-902/28/23 06:444361811
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-8 (0-2)Lab ID:92653934004 Collected:02/23/23 15:15 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <159 ug/kg 03/01/23 20:29 131-11-302/28/23 06:444361591
Di-n-butylphthalate <147 ug/kg 03/01/23 20:29 84-74-202/28/23 06:444361471
4,6-Dinitro-2-methylphenol <407 ug/kg 03/01/23 20:29 534-52-102/28/23 06:448724071
2,4-Dinitrophenol <1350 ug/kg 03/01/23 20:29 51-28-502/28/23 06:44218013501
2,4-Dinitrotoluene <168 ug/kg 03/01/23 20:29 121-14-202/28/23 06:444361681
2,6-Dinitrotoluene <160 ug/kg 03/01/23 20:29 606-20-202/28/23 06:444361601
Di-n-octylphthalate <172 ug/kg 03/01/23 20:29 117-84-002/28/23 06:444361721
bis(2-Ethylhexyl)phthalate <169 ug/kg 03/01/23 20:29 117-81-702/28/23 06:444361691
Fluoranthene <149 ug/kg 03/01/23 20:29 206-44-002/28/23 06:444361491
Fluorene <153 ug/kg 03/01/23 20:29 86-73-702/28/23 06:444361531
Hexachloro-1,3-butadiene <189 ug/kg 03/01/23 20:29 87-68-302/28/23 06:444361891
Hexachlorobenzene <170 ug/kg 03/01/23 20:29 118-74-102/28/23 06:444361701
Hexachlorocyclopentadiene <250 ug/kg 03/01/23 20:29 77-47-402/28/23 06:444362501
Hexachloroethane <166 ug/kg 03/01/23 20:29 67-72-102/28/23 06:444361661
Indeno(1,2,3-cd)pyrene <172 ug/kg 03/01/23 20:29 193-39-502/28/23 06:444361721
Isophorone <194 ug/kg 03/01/23 20:29 78-59-102/28/23 06:444361941
1-Methylnaphthalene <153 ug/kg 03/01/23 20:29 90-12-002/28/23 06:444361531
2-Methylnaphthalene <174 ug/kg 03/01/23 20:29 91-57-602/28/23 06:444361741
2-Methylphenol(o-Cresol)<178 ug/kg 03/01/23 20:29 95-48-702/28/23 06:444361781
3&4-Methylphenol(m&p Cresol)<176 ug/kg 03/01/23 20:29 15831-10-402/28/23 06:444361761
Naphthalene <148 ug/kg 03/01/23 20:29 91-20-302/28/23 06:444361481
2-Nitroaniline <357 ug/kg 03/01/23 20:29 88-74-402/28/23 06:4421803571
3-Nitroaniline <342 ug/kg 03/01/23 20:29 99-09-202/28/23 06:4421803421
4-Nitroaniline <332 ug/kg 03/01/23 20:29 100-01-602/28/23 06:448723321
Nitrobenzene <202 ug/kg 03/01/23 20:29 98-95-302/28/23 06:444362021
2-Nitrophenol <189 ug/kg 03/01/23 20:29 88-75-502/28/23 06:444361891
4-Nitrophenol <843 ug/kg 03/01/23 20:29 100-02-702/28/23 06:4421808431
N-Nitrosodimethylamine <147 ug/kg 03/01/23 20:29 62-75-902/28/23 06:444361471
N-Nitroso-di-n-propylamine <164 ug/kg 03/01/23 20:29 621-64-702/28/23 06:444361641
N-Nitrosodiphenylamine <155 ug/kg 03/01/23 20:29 86-30-602/28/23 06:444361551
2,2'-Oxybis(1-chloropropane)<207 ug/kg 03/01/23 20:29 108-60-102/28/23 06:444362071
Pentachlorophenol <427 ug/kg 03/01/23 20:29 87-86-502/28/23 06:448724271
Phenanthrene <143 ug/kg 03/01/23 20:29 85-01-802/28/23 06:444361431
Phenol <194 ug/kg 03/01/23 20:29 108-95-202/28/23 06:444361941
Pyrene <177 ug/kg 03/01/23 20:29 129-00-002/28/23 06:444361771
Pyridine <137 ug/kg 03/01/23 20:29 110-86-102/28/23 06:444361371
1,2,4-Trichlorobenzene <172 ug/kg 03/01/23 20:29 120-82-102/28/23 06:444361721
2,4,5-Trichlorophenol <200 ug/kg 03/01/23 20:29 95-95-402/28/23 06:444362001
2,4,6-Trichlorophenol <180 ug/kg 03/01/23 20:29 88-06-202/28/23 06:444361801
Surrogates
Nitrobenzene-d5 (S)66 %03/01/23 20:29 4165-60-002/28/23 06:4410-130 1
2-Fluorobiphenyl (S)69 %03/01/23 20:29 321-60-802/28/23 06:4410-130 1
Terphenyl-d14 (S)63 %03/01/23 20:29 1718-51-002/28/23 06:4410-130 1
Phenol-d6 (S)62 %03/01/23 20:29 13127-88-302/28/23 06:4410-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-8 (0-2)Lab ID:92653934004 Collected:02/23/23 15:15 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)58 %03/01/23 20:29 367-12-402/28/23 06:4410-130 1
2,4,6-Tribromophenol (S)78 %03/01/23 20:29 118-79-602/28/23 06:4410-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 25.3 %02/24/23 17:06 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 79.7 %02/27/23 13:4002/27/23 13:321
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent <0.320 mg/kg 02/28/23 13:25 18540-29-902/28/23 03:401.25 0.320 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-9 (0-2)Lab ID:92653934005 Collected:02/23/23 16:25 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.3 mg/kg 02/28/23 18:49 7440-38-202/28/23 11:260.62 0.18 1
Barium 76.3 mg/kg 02/28/23 18:49 7440-39-302/28/23 11:260.37 0.093 1
Cadmium <0.037 mg/kg 02/28/23 18:49 7440-43-902/28/23 11:260.099 0.037 1
Chromium 34.9 mg/kg 02/28/23 18:49 7440-47-302/28/23 11:262.5 0.48 1
Lead 8.3 mg/kg 02/28/23 18:49 7439-92-102/28/23 11:260.62 0.12 1
Selenium 0.44J mg/kg 02/28/23 18:49 7782-49-202/28/23 11:260.62 0.13 1
Silver <0.25 mg/kg 02/28/23 18:49 7440-22-402/28/23 11:260.62 0.25 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.030 mg/kg 03/02/23 15:40 7439-97-602/28/23 11:370.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <147 ug/kg 03/01/23 20:57 83-32-902/28/23 06:444191471
Acenaphthylene <147 ug/kg 03/01/23 20:57 208-96-802/28/23 06:444191471
Aniline <164 ug/kg 03/01/23 20:57 62-53-302/28/23 06:444191641
Anthracene <137 ug/kg 03/01/23 20:57 120-12-702/28/23 06:444191371
Benzo(a)anthracene <140 ug/kg 03/01/23 20:57 56-55-302/28/23 06:444191401
Benzo(a)pyrene <145 ug/kg 03/01/23 20:57 50-32-802/28/23 06:444191451
Benzo(b)fluoranthene <140 ug/kg 03/01/23 20:57 205-99-202/28/23 06:444191401
Benzo(g,h,i)perylene <163 ug/kg 03/01/23 20:57 191-24-202/28/23 06:444191631
Benzo(k)fluoranthene <147 ug/kg 03/01/23 20:57 207-08-902/28/23 06:444191471
Benzoic Acid <901 ug/kg 03/01/23 20:57 65-85-002/28/23 06:4421009011
Benzyl alcohol <318 ug/kg 03/01/23 20:57 100-51-602/28/23 06:448393181
4-Bromophenylphenyl ether <161 ug/kg 03/01/23 20:57 101-55-302/28/23 06:444191611
Butylbenzylphthalate <177 ug/kg 03/01/23 20:57 85-68-702/28/23 06:444191771
4-Chloro-3-methylphenol <295 ug/kg 03/01/23 20:57 59-50-702/28/23 06:448392951
4-Chloroaniline <329 ug/kg 03/01/23 20:57 106-47-802/28/23 06:448393291
bis(2-Chloroethoxy)methane <174 ug/kg 03/01/23 20:57 111-91-102/28/23 06:444191741
bis(2-Chloroethyl) ether <158 ug/kg 03/01/23 20:57 111-44-402/28/23 06:444191581
2-Chloronaphthalene <166 ug/kg 03/01/23 20:57 91-58-702/28/23 06:444191661
2-Chlorophenol <158 ug/kg 03/01/23 20:57 95-57-802/28/23 06:444191581
4-Chlorophenylphenyl ether <156 ug/kg 03/01/23 20:57 7005-72-302/28/23 06:444191561
Chrysene <152 ug/kg 03/01/23 20:57 218-01-902/28/23 06:444191521
Dibenz(a,h)anthracene <161 ug/kg 03/01/23 20:57 53-70-302/28/23 06:444191611
Dibenzofuran <151 ug/kg 03/01/23 20:57 132-64-902/28/23 06:444191511
1,2-Dichlorobenzene <151 ug/kg 03/01/23 20:57 95-50-102/28/23 06:444191511
1,3-Dichlorobenzene <149 ug/kg 03/01/23 20:57 541-73-102/28/23 06:444191491
1,4-Dichlorobenzene <160 ug/kg 03/01/23 20:57 106-46-702/28/23 06:444191601
3,3'-Dichlorobenzidine <283 ug/kg 03/01/23 20:57 91-94-102/28/23 06:448392831
2,4-Dichlorophenol <164 ug/kg 03/01/23 20:57 120-83-202/28/23 06:444191641
Diethylphthalate <154 ug/kg 03/01/23 20:57 84-66-202/28/23 06:444191541
2,4-Dimethylphenol <174 ug/kg 03/01/23 20:57 105-67-902/28/23 06:444191741
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-9 (0-2)Lab ID:92653934005 Collected:02/23/23 16:25 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <152 ug/kg 03/01/23 20:57 131-11-302/28/23 06:444191521
Di-n-butylphthalate <141 ug/kg 03/01/23 20:57 84-74-202/28/23 06:444191411
4,6-Dinitro-2-methylphenol <391 ug/kg 03/01/23 20:57 534-52-102/28/23 06:448393911
2,4-Dinitrophenol <1300 ug/kg 03/01/23 20:57 51-28-502/28/23 06:44210013001
2,4-Dinitrotoluene <161 ug/kg 03/01/23 20:57 121-14-202/28/23 06:444191611
2,6-Dinitrotoluene <154 ug/kg 03/01/23 20:57 606-20-202/28/23 06:444191541
Di-n-octylphthalate <165 ug/kg 03/01/23 20:57 117-84-002/28/23 06:444191651
bis(2-Ethylhexyl)phthalate <163 ug/kg 03/01/23 20:57 117-81-702/28/23 06:444191631
Fluoranthene <144 ug/kg 03/01/23 20:57 206-44-002/28/23 06:444191441
Fluorene <147 ug/kg 03/01/23 20:57 86-73-702/28/23 06:444191471
Hexachloro-1,3-butadiene <182 ug/kg 03/01/23 20:57 87-68-302/28/23 06:444191821
Hexachlorobenzene <164 ug/kg 03/01/23 20:57 118-74-102/28/23 06:444191641
Hexachlorocyclopentadiene <240 ug/kg 03/01/23 20:57 77-47-402/28/23 06:444192401
Hexachloroethane <160 ug/kg 03/01/23 20:57 67-72-102/28/23 06:444191601
Indeno(1,2,3-cd)pyrene <165 ug/kg 03/01/23 20:57 193-39-502/28/23 06:444191651
Isophorone <187 ug/kg 03/01/23 20:57 78-59-102/28/23 06:444191871
1-Methylnaphthalene <147 ug/kg 03/01/23 20:57 90-12-002/28/23 06:444191471
2-Methylnaphthalene <168 ug/kg 03/01/23 20:57 91-57-602/28/23 06:444191681
2-Methylphenol(o-Cresol)<172 ug/kg 03/01/23 20:57 95-48-702/28/23 06:444191721
3&4-Methylphenol(m&p Cresol)<169 ug/kg 03/01/23 20:57 15831-10-402/28/23 06:444191691
Naphthalene <142 ug/kg 03/01/23 20:57 91-20-302/28/23 06:444191421
2-Nitroaniline <343 ug/kg 03/01/23 20:57 88-74-402/28/23 06:4421003431
3-Nitroaniline <329 ug/kg 03/01/23 20:57 99-09-202/28/23 06:4421003291
4-Nitroaniline <319 ug/kg 03/01/23 20:57 100-01-602/28/23 06:448393191
Nitrobenzene <194 ug/kg 03/01/23 20:57 98-95-302/28/23 06:444191941
2-Nitrophenol <182 ug/kg 03/01/23 20:57 88-75-502/28/23 06:444191821
4-Nitrophenol <811 ug/kg 03/01/23 20:57 100-02-702/28/23 06:4421008111
N-Nitrosodimethylamine <141 ug/kg 03/01/23 20:57 62-75-902/28/23 06:444191411
N-Nitroso-di-n-propylamine <158 ug/kg 03/01/23 20:57 621-64-702/28/23 06:444191581
N-Nitrosodiphenylamine <149 ug/kg 03/01/23 20:57 86-30-602/28/23 06:444191491
2,2'-Oxybis(1-chloropropane)<199 ug/kg 03/01/23 20:57 108-60-102/28/23 06:444191991
Pentachlorophenol <410 ug/kg 03/01/23 20:57 87-86-502/28/23 06:448394101
Phenanthrene <137 ug/kg 03/01/23 20:57 85-01-802/28/23 06:444191371
Phenol <187 ug/kg 03/01/23 20:57 108-95-202/28/23 06:444191871
Pyrene <170 ug/kg 03/01/23 20:57 129-00-002/28/23 06:444191701
Pyridine <132 ug/kg 03/01/23 20:57 110-86-102/28/23 06:444191321
1,2,4-Trichlorobenzene <165 ug/kg 03/01/23 20:57 120-82-102/28/23 06:444191651
2,4,5-Trichlorophenol <192 ug/kg 03/01/23 20:57 95-95-402/28/23 06:444191921
2,4,6-Trichlorophenol <173 ug/kg 03/01/23 20:57 88-06-202/28/23 06:444191731
Surrogates
Nitrobenzene-d5 (S)63 %03/01/23 20:57 4165-60-002/28/23 06:4410-130 1
2-Fluorobiphenyl (S)65 %03/01/23 20:57 321-60-802/28/23 06:4410-130 1
Terphenyl-d14 (S)61 %03/01/23 20:57 1718-51-002/28/23 06:4410-130 1
Phenol-d6 (S)61 %03/01/23 20:57 13127-88-302/28/23 06:4410-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-9 (0-2)Lab ID:92653934005 Collected:02/23/23 16:25 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)58 %03/01/23 20:57 367-12-402/28/23 06:4410-130 1
2,4,6-Tribromophenol (S)79 %03/01/23 20:57 118-79-602/28/23 06:4410-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.1 %02/24/23 17:06 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 80.5 %02/27/23 13:4002/27/23 13:321
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.998J mg/kg 02/28/23 13:30 18540-29-9 J02/28/23 03:401.24 0.317 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-10 (0-2)Lab ID:92653934006 Collected:02/24/23 10:30 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 1.4 mg/kg 02/28/23 18:53 7440-38-202/28/23 11:260.64 0.18 1
Barium 84.6 mg/kg 02/28/23 18:53 7440-39-302/28/23 11:260.39 0.096 1
Cadmium 0.040J mg/kg 02/28/23 18:53 7440-43-902/28/23 11:260.10 0.038 1
Chromium 35.2 mg/kg 02/28/23 18:53 7440-47-302/28/23 11:262.6 0.50 1
Lead 11.5 mg/kg 02/28/23 18:53 7439-92-102/28/23 11:260.64 0.12 1
Selenium 0.30J mg/kg 02/28/23 18:53 7782-49-202/28/23 11:260.64 0.13 1
Silver <0.26 mg/kg 02/28/23 18:53 7440-22-402/28/23 11:260.64 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.034 mg/kg 03/02/23 15:42 7439-97-602/28/23 11:370.024 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <150 ug/kg 03/07/23 17:05 83-32-903/03/23 09:234271501
Acenaphthylene <150 ug/kg 03/07/23 17:05 208-96-803/03/23 09:234271501
Aniline <167 ug/kg 03/07/23 17:05 62-53-303/03/23 09:234271671
Anthracene <140 ug/kg 03/07/23 17:05 120-12-703/03/23 09:234271401
Benzo(a)anthracene <142 ug/kg 03/07/23 17:05 56-55-303/03/23 09:234271421
Benzo(a)pyrene <147 ug/kg 03/07/23 17:05 50-32-803/03/23 09:234271471
Benzo(b)fluoranthene <142 ug/kg 03/07/23 17:05 205-99-203/03/23 09:234271421
Benzo(g,h,i)perylene <166 ug/kg 03/07/23 17:05 191-24-203/03/23 09:234271661
Benzo(k)fluoranthene <150 ug/kg 03/07/23 17:05 207-08-903/03/23 09:234271501
Benzoic Acid <917 ug/kg 03/07/23 17:05 65-85-003/03/23 09:2321309171
Benzyl alcohol <323 ug/kg 03/07/23 17:05 100-51-603/03/23 09:238533231
4-Bromophenylphenyl ether <164 ug/kg 03/07/23 17:05 101-55-303/03/23 09:234271641
Butylbenzylphthalate <180 ug/kg 03/07/23 17:05 85-68-703/03/23 09:234271801
4-Chloro-3-methylphenol <300 ug/kg 03/07/23 17:05 59-50-703/03/23 09:238533001
4-Chloroaniline <335 ug/kg 03/07/23 17:05 106-47-803/03/23 09:238533351
bis(2-Chloroethoxy)methane <177 ug/kg 03/07/23 17:05 111-91-103/03/23 09:234271771
bis(2-Chloroethyl) ether <160 ug/kg 03/07/23 17:05 111-44-403/03/23 09:234271601
2-Chloronaphthalene <169 ug/kg 03/07/23 17:05 91-58-703/03/23 09:234271691
2-Chlorophenol <160 ug/kg 03/07/23 17:05 95-57-803/03/23 09:234271601
4-Chlorophenylphenyl ether <159 ug/kg 03/07/23 17:05 7005-72-303/03/23 09:234271591
Chrysene <155 ug/kg 03/07/23 17:05 218-01-903/03/23 09:234271551
Dibenz(a,h)anthracene <164 ug/kg 03/07/23 17:05 53-70-303/03/23 09:234271641
Dibenzofuran <154 ug/kg 03/07/23 17:05 132-64-903/03/23 09:234271541
1,2-Dichlorobenzene <154 ug/kg 03/07/23 17:05 95-50-103/03/23 09:234271541
1,3-Dichlorobenzene <151 ug/kg 03/07/23 17:05 541-73-103/03/23 09:234271511
1,4-Dichlorobenzene <163 ug/kg 03/07/23 17:05 106-46-703/03/23 09:234271631
3,3'-Dichlorobenzidine <288 ug/kg 03/07/23 17:05 91-94-103/03/23 09:238532881
2,4-Dichlorophenol <167 ug/kg 03/07/23 17:05 120-83-203/03/23 09:234271671
Diethylphthalate <156 ug/kg 03/07/23 17:05 84-66-203/03/23 09:234271561
2,4-Dimethylphenol <177 ug/kg 03/07/23 17:05 105-67-903/03/23 09:234271771
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-10 (0-2)Lab ID:92653934006 Collected:02/24/23 10:30 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <155 ug/kg 03/07/23 17:05 131-11-303/03/23 09:234271551
Di-n-butylphthalate <144 ug/kg 03/07/23 17:05 84-74-203/03/23 09:234271441
4,6-Dinitro-2-methylphenol <398 ug/kg 03/07/23 17:05 534-52-103/03/23 09:238533981
2,4-Dinitrophenol <1320 ug/kg 03/07/23 17:05 51-28-5 v103/03/23 09:23213013201
2,4-Dinitrotoluene <164 ug/kg 03/07/23 17:05 121-14-203/03/23 09:234271641
2,6-Dinitrotoluene <156 ug/kg 03/07/23 17:05 606-20-203/03/23 09:234271561
Di-n-octylphthalate <168 ug/kg 03/07/23 17:05 117-84-003/03/23 09:234271681
bis(2-Ethylhexyl)phthalate <166 ug/kg 03/07/23 17:05 117-81-703/03/23 09:234271661
Fluoranthene <146 ug/kg 03/07/23 17:05 206-44-003/03/23 09:234271461
Fluorene <150 ug/kg 03/07/23 17:05 86-73-703/03/23 09:234271501
Hexachloro-1,3-butadiene <185 ug/kg 03/07/23 17:05 87-68-303/03/23 09:234271851
Hexachlorobenzene <167 ug/kg 03/07/23 17:05 118-74-103/03/23 09:234271671
Hexachlorocyclopentadiene <244 ug/kg 03/07/23 17:05 77-47-403/03/23 09:234272441
Hexachloroethane <163 ug/kg 03/07/23 17:05 67-72-103/03/23 09:234271631
Indeno(1,2,3-cd)pyrene <168 ug/kg 03/07/23 17:05 193-39-503/03/23 09:234271681
Isophorone <190 ug/kg 03/07/23 17:05 78-59-103/03/23 09:234271901
1-Methylnaphthalene <150 ug/kg 03/07/23 17:05 90-12-003/03/23 09:234271501
2-Methylnaphthalene <171 ug/kg 03/07/23 17:05 91-57-603/03/23 09:234271711
2-Methylphenol(o-Cresol)<175 ug/kg 03/07/23 17:05 95-48-703/03/23 09:234271751
3&4-Methylphenol(m&p Cresol)<172 ug/kg 03/07/23 17:05 15831-10-403/03/23 09:234271721
Naphthalene <145 ug/kg 03/07/23 17:05 91-20-303/03/23 09:234271451
2-Nitroaniline <349 ug/kg 03/07/23 17:05 88-74-403/03/23 09:2321303491
3-Nitroaniline <335 ug/kg 03/07/23 17:05 99-09-203/03/23 09:2321303351
4-Nitroaniline <325 ug/kg 03/07/23 17:05 100-01-603/03/23 09:238533251
Nitrobenzene <198 ug/kg 03/07/23 17:05 98-95-303/03/23 09:234271981
2-Nitrophenol <185 ug/kg 03/07/23 17:05 88-75-503/03/23 09:234271851
4-Nitrophenol <825 ug/kg 03/07/23 17:05 100-02-703/03/23 09:2321308251
N-Nitrosodimethylamine <144 ug/kg 03/07/23 17:05 62-75-903/03/23 09:234271441
N-Nitroso-di-n-propylamine <160 ug/kg 03/07/23 17:05 621-64-703/03/23 09:234271601
N-Nitrosodiphenylamine <151 ug/kg 03/07/23 17:05 86-30-603/03/23 09:234271511
2,2'-Oxybis(1-chloropropane)<203 ug/kg 03/07/23 17:05 108-60-103/03/23 09:234272031
Pentachlorophenol <418 ug/kg 03/07/23 17:05 87-86-503/03/23 09:238534181
Phenanthrene <140 ug/kg 03/07/23 17:05 85-01-803/03/23 09:234271401
Phenol <190 ug/kg 03/07/23 17:05 108-95-203/03/23 09:234271901
Pyrene <173 ug/kg 03/07/23 17:05 129-00-003/03/23 09:234271731
Pyridine <134 ug/kg 03/07/23 17:05 110-86-103/03/23 09:234271341
1,2,4-Trichlorobenzene <168 ug/kg 03/07/23 17:05 120-82-103/03/23 09:234271681
2,4,5-Trichlorophenol <195 ug/kg 03/07/23 17:05 95-95-403/03/23 09:234271951
2,4,6-Trichlorophenol <176 ug/kg 03/07/23 17:05 88-06-203/03/23 09:234271761
Surrogates
Nitrobenzene-d5 (S)61 %03/07/23 17:05 4165-60-003/03/23 09:2310-130 1
2-Fluorobiphenyl (S)55 %03/07/23 17:05 321-60-803/03/23 09:2310-130 1
Terphenyl-d14 (S)52 %03/07/23 17:05 1718-51-003/03/23 09:2310-130 1
Phenol-d6 (S)40 %03/07/23 17:05 13127-88-303/03/23 09:2310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-10 (0-2)Lab ID:92653934006 Collected:02/24/23 10:30 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)18 %03/07/23 17:05 367-12-403/03/23 09:2310-130 1
2,4,6-Tribromophenol (S)15 %03/07/23 17:05 118-79-603/03/23 09:2310-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.9 %02/24/23 17:07 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 75.4 %02/27/23 13:4002/27/23 13:321
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 0.879J mg/kg 02/28/23 13:36 18540-29-9 J02/28/23 03:401.33 0.338 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-DUP (0-2)Lab ID:92653934007 Collected:02/23/23 00:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Arsenic 2.1 mg/kg 02/28/23 18:56 7440-38-202/28/23 11:260.64 0.18 1
Barium 55.6 mg/kg 02/28/23 18:56 7440-39-302/28/23 11:260.39 0.096 1
Cadmium <0.038 mg/kg 02/28/23 18:56 7440-43-902/28/23 11:260.10 0.038 1
Chromium 41.7 mg/kg 02/28/23 18:56 7440-47-302/28/23 11:262.6 0.50 1
Lead 13.2 mg/kg 02/28/23 18:56 7439-92-102/28/23 11:260.64 0.12 1
Selenium 0.55J mg/kg 02/28/23 18:56 7782-49-202/28/23 11:260.64 0.13 1
Silver <0.26 mg/kg 02/28/23 18:56 7440-22-402/28/23 11:260.64 0.26 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Minneapolis
7471B Mercury
Mercury 0.048 mg/kg 03/02/23 15:44 7439-97-602/28/23 11:370.025 0.011 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene <148 ug/kg 03/07/23 17:33 83-32-903/03/23 09:234211481
Acenaphthylene <148 ug/kg 03/07/23 17:33 208-96-803/03/23 09:234211481
Aniline <165 ug/kg 03/07/23 17:33 62-53-303/03/23 09:234211651
Anthracene <138 ug/kg 03/07/23 17:33 120-12-703/03/23 09:234211381
Benzo(a)anthracene <140 ug/kg 03/07/23 17:33 56-55-303/03/23 09:234211401
Benzo(a)pyrene <145 ug/kg 03/07/23 17:33 50-32-803/03/23 09:234211451
Benzo(b)fluoranthene <140 ug/kg 03/07/23 17:33 205-99-203/03/23 09:234211401
Benzo(g,h,i)perylene <163 ug/kg 03/07/23 17:33 191-24-203/03/23 09:234211631
Benzo(k)fluoranthene <148 ug/kg 03/07/23 17:33 207-08-903/03/23 09:234211481
Benzoic Acid <905 ug/kg 03/07/23 17:33 65-85-003/03/23 09:2321109051
Benzyl alcohol <319 ug/kg 03/07/23 17:33 100-51-603/03/23 09:238423191
4-Bromophenylphenyl ether <162 ug/kg 03/07/23 17:33 101-55-303/03/23 09:234211621
Butylbenzylphthalate <177 ug/kg 03/07/23 17:33 85-68-703/03/23 09:234211771
4-Chloro-3-methylphenol <296 ug/kg 03/07/23 17:33 59-50-703/03/23 09:238422961
4-Chloroaniline <331 ug/kg 03/07/23 17:33 106-47-803/03/23 09:238423311
bis(2-Chloroethoxy)methane <175 ug/kg 03/07/23 17:33 111-91-103/03/23 09:234211751
bis(2-Chloroethyl) ether <158 ug/kg 03/07/23 17:33 111-44-403/03/23 09:234211581
2-Chloronaphthalene <167 ug/kg 03/07/23 17:33 91-58-703/03/23 09:234211671
2-Chlorophenol <158 ug/kg 03/07/23 17:33 95-57-803/03/23 09:234211581
4-Chlorophenylphenyl ether <157 ug/kg 03/07/23 17:33 7005-72-303/03/23 09:234211571
Chrysene <153 ug/kg 03/07/23 17:33 218-01-903/03/23 09:234211531
Dibenz(a,h)anthracene <162 ug/kg 03/07/23 17:33 53-70-303/03/23 09:234211621
Dibenzofuran <152 ug/kg 03/07/23 17:33 132-64-903/03/23 09:234211521
1,2-Dichlorobenzene <152 ug/kg 03/07/23 17:33 95-50-103/03/23 09:234211521
1,3-Dichlorobenzene <149 ug/kg 03/07/23 17:33 541-73-103/03/23 09:234211491
1,4-Dichlorobenzene <161 ug/kg 03/07/23 17:33 106-46-703/03/23 09:234211611
3,3'-Dichlorobenzidine <285 ug/kg 03/07/23 17:33 91-94-103/03/23 09:238422851
2,4-Dichlorophenol <165 ug/kg 03/07/23 17:33 120-83-203/03/23 09:234211651
Diethylphthalate <154 ug/kg 03/07/23 17:33 84-66-203/03/23 09:234211541
2,4-Dimethylphenol <175 ug/kg 03/07/23 17:33 105-67-903/03/23 09:234211751
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-DUP (0-2)Lab ID:92653934007 Collected:02/23/23 00:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate <153 ug/kg 03/07/23 17:33 131-11-303/03/23 09:234211531
Di-n-butylphthalate <142 ug/kg 03/07/23 17:33 84-74-203/03/23 09:234211421
4,6-Dinitro-2-methylphenol <393 ug/kg 03/07/23 17:33 534-52-103/03/23 09:238423931
2,4-Dinitrophenol <1300 ug/kg 03/07/23 17:33 51-28-5 v103/03/23 09:23211013001
2,4-Dinitrotoluene <162 ug/kg 03/07/23 17:33 121-14-203/03/23 09:234211621
2,6-Dinitrotoluene <154 ug/kg 03/07/23 17:33 606-20-203/03/23 09:234211541
Di-n-octylphthalate <166 ug/kg 03/07/23 17:33 117-84-003/03/23 09:234211661
bis(2-Ethylhexyl)phthalate <163 ug/kg 03/07/23 17:33 117-81-703/03/23 09:234211631
Fluoranthene <144 ug/kg 03/07/23 17:33 206-44-003/03/23 09:234211441
Fluorene <148 ug/kg 03/07/23 17:33 86-73-703/03/23 09:234211481
Hexachloro-1,3-butadiene <182 ug/kg 03/07/23 17:33 87-68-303/03/23 09:234211821
Hexachlorobenzene <165 ug/kg 03/07/23 17:33 118-74-103/03/23 09:234211651
Hexachlorocyclopentadiene <241 ug/kg 03/07/23 17:33 77-47-403/03/23 09:234212411
Hexachloroethane <161 ug/kg 03/07/23 17:33 67-72-103/03/23 09:234211611
Indeno(1,2,3-cd)pyrene <166 ug/kg 03/07/23 17:33 193-39-503/03/23 09:234211661
Isophorone <188 ug/kg 03/07/23 17:33 78-59-103/03/23 09:234211881
1-Methylnaphthalene <148 ug/kg 03/07/23 17:33 90-12-003/03/23 09:234211481
2-Methylnaphthalene <168 ug/kg 03/07/23 17:33 91-57-603/03/23 09:234211681
2-Methylphenol(o-Cresol)<172 ug/kg 03/07/23 17:33 95-48-703/03/23 09:234211721
3&4-Methylphenol(m&p Cresol)<170 ug/kg 03/07/23 17:33 15831-10-403/03/23 09:234211701
Naphthalene <143 ug/kg 03/07/23 17:33 91-20-303/03/23 09:234211431
2-Nitroaniline <345 ug/kg 03/07/23 17:33 88-74-403/03/23 09:2321103451
3-Nitroaniline <331 ug/kg 03/07/23 17:33 99-09-203/03/23 09:2321103311
4-Nitroaniline <320 ug/kg 03/07/23 17:33 100-01-603/03/23 09:238423201
Nitrobenzene <195 ug/kg 03/07/23 17:33 98-95-303/03/23 09:234211951
2-Nitrophenol <182 ug/kg 03/07/23 17:33 88-75-503/03/23 09:234211821
4-Nitrophenol <814 ug/kg 03/07/23 17:33 100-02-703/03/23 09:2321108141
N-Nitrosodimethylamine <142 ug/kg 03/07/23 17:33 62-75-903/03/23 09:234211421
N-Nitroso-di-n-propylamine <158 ug/kg 03/07/23 17:33 621-64-703/03/23 09:234211581
N-Nitrosodiphenylamine <149 ug/kg 03/07/23 17:33 86-30-603/03/23 09:234211491
2,2'-Oxybis(1-chloropropane)<200 ug/kg 03/07/23 17:33 108-60-103/03/23 09:234212001
Pentachlorophenol <412 ug/kg 03/07/23 17:33 87-86-503/03/23 09:238424121
Phenanthrene <138 ug/kg 03/07/23 17:33 85-01-803/03/23 09:234211381
Phenol <188 ug/kg 03/07/23 17:33 108-95-203/03/23 09:234211881
Pyrene <171 ug/kg 03/07/23 17:33 129-00-003/03/23 09:234211711
Pyridine <133 ug/kg 03/07/23 17:33 110-86-103/03/23 09:234211331
1,2,4-Trichlorobenzene <166 ug/kg 03/07/23 17:33 120-82-103/03/23 09:234211661
2,4,5-Trichlorophenol <193 ug/kg 03/07/23 17:33 95-95-403/03/23 09:234211931
2,4,6-Trichlorophenol <174 ug/kg 03/07/23 17:33 88-06-203/03/23 09:234211741
Surrogates
Nitrobenzene-d5 (S)70 %03/07/23 17:33 4165-60-003/03/23 09:2310-130 1
2-Fluorobiphenyl (S)63 %03/07/23 17:33 321-60-803/03/23 09:2310-130 1
Terphenyl-d14 (S)65 %03/07/23 17:33 1718-51-003/03/23 09:2310-130 1
Phenol-d6 (S)66 %03/07/23 17:33 13127-88-303/03/23 09:2310-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-DUP (0-2)Lab ID:92653934007 Collected:02/23/23 00:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)64 %03/07/23 17:33 367-12-403/03/23 09:2310-130 1
2,4,6-Tribromophenol (S)78 %03/07/23 17:33 118-79-603/03/23 09:2310-131 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.7 %02/24/23 17:07 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 72.0 %02/27/23 13:4002/27/23 13:321
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent 1.07J mg/kg 02/28/23 13:41 18540-29-9 J02/28/23 03:401.39 0.354 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-1 (1-2)Lab ID:92653934008 Collected:02/23/23 10:45 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <50.1 ug/kg 02/24/23 21:40 67-64-102/24/23 20:2515650.1 1
Benzene <3.1 ug/kg 02/24/23 21:40 71-43-202/24/23 20:257.8 3.1 1
Bromobenzene <2.5 ug/kg 02/24/23 21:40 108-86-102/24/23 20:257.8 2.5 1
Bromochloromethane <2.3 ug/kg 02/24/23 21:40 74-97-502/24/23 20:257.8 2.3 1
Bromodichloromethane <3.0 ug/kg 02/24/23 21:40 75-27-402/24/23 20:257.8 3.0 1
Bromoform <2.7 ug/kg 02/24/23 21:40 75-25-202/24/23 20:257.8 2.7 1
Bromomethane <24.2 ug/kg 02/24/23 21:40 74-83-902/24/23 20:2531.2 24.2 1
2-Butanone (MEK)<37.4 ug/kg 02/24/23 21:40 78-93-302/24/23 20:2515637.4 1
n-Butylbenzene <4.9 ug/kg 02/24/23 21:40 104-51-802/24/23 20:257.8 4.9 1
sec-Butylbenzene <3.4 ug/kg 02/24/23 21:40 135-98-802/24/23 20:257.8 3.4 1
tert-Butylbenzene <2.8 ug/kg 02/24/23 21:40 98-06-602/24/23 20:257.8 2.8 1
Carbon tetrachloride <2.9 ug/kg 02/24/23 21:40 56-23-5 IK02/24/23 20:257.8 2.9 1
Chlorobenzene <4.5 ug/kg 02/24/23 21:40 108-90-702/24/23 20:257.8 4.5 1
Chloroethane <6.0 ug/kg 02/24/23 21:40 75-00-302/24/23 20:2515.6 6.0 1
Chloroform <6.5 ug/kg 02/24/23 21:40 67-66-302/24/23 20:257.8 6.5 1
Chloromethane <6.5 ug/kg 02/24/23 21:40 74-87-302/24/23 20:2515.6 6.5 1
2-Chlorotoluene <2.8 ug/kg 02/24/23 21:40 95-49-802/24/23 20:257.8 2.8 1
4-Chlorotoluene <4.3 ug/kg 02/24/23 21:40 106-43-402/24/23 20:257.8 4.3 1
1,2-Dibromo-3-chloropropane <3.0 ug/kg 02/24/23 21:40 96-12-802/24/23 20:257.8 3.0 1
Dibromochloromethane <4.4 ug/kg 02/24/23 21:40 124-48-1 IK02/24/23 20:257.8 4.4 1
1,2-Dibromoethane (EDB)<3.4 ug/kg 02/24/23 21:40 106-93-402/24/23 20:257.8 3.4 1
Dibromomethane <1.7 ug/kg 02/24/23 21:40 74-95-302/24/23 20:257.8 1.7 1
1,2-Dichlorobenzene <2.8 ug/kg 02/24/23 21:40 95-50-102/24/23 20:257.8 2.8 1
1,3-Dichlorobenzene <2.4 ug/kg 02/24/23 21:40 541-73-102/24/23 20:257.8 2.4 1
1,4-Dichlorobenzene <2.0 ug/kg 02/24/23 21:40 106-46-702/24/23 20:257.8 2.0 1
Dichlorodifluoromethane <7.9 ug/kg 02/24/23 21:40 75-71-802/24/23 20:2515.6 7.9 1
1,1-Dichloroethane <3.2 ug/kg 02/24/23 21:40 75-34-302/24/23 20:257.8 3.2 1
1,2-Dichloroethane <5.2 ug/kg 02/24/23 21:40 107-06-202/24/23 20:257.8 5.2 1
1,1-Dichloroethene <3.2 ug/kg 02/24/23 21:40 75-35-402/24/23 20:257.8 3.2 1
cis-1,2-Dichloroethene <2.7 ug/kg 02/24/23 21:40 156-59-2 M102/24/23 20:257.8 2.7 1
trans-1,2-Dichloroethene <6.6 ug/kg 02/24/23 21:40 156-60-502/24/23 20:257.8 6.6 1
1,2-Dichloropropane <2.3 ug/kg 02/24/23 21:40 78-87-502/24/23 20:257.8 2.3 1
1,3-Dichloropropane <2.4 ug/kg 02/24/23 21:40 142-28-902/24/23 20:257.8 2.4 1
2,2-Dichloropropane <5.9 ug/kg 02/24/23 21:40 594-20-7 v202/24/23 20:257.8 5.9 1
1,1-Dichloropropene <3.7 ug/kg 02/24/23 21:40 563-58-602/24/23 20:257.8 3.7 1
cis-1,3-Dichloropropene <2.1 ug/kg 02/24/23 21:40 10061-01-502/24/23 20:257.8 2.1 1
trans-1,3-Dichloropropene <2.7 ug/kg 02/24/23 21:40 10061-02-602/24/23 20:257.8 2.7 1
Diisopropyl ether <2.1 ug/kg 02/24/23 21:40 108-20-302/24/23 20:257.8 2.1 1
Ethylbenzene <3.6 ug/kg 02/24/23 21:40 100-41-402/24/23 20:257.8 3.6 1
Hexachloro-1,3-butadiene <12.8 ug/kg 02/24/23 21:40 87-68-302/24/23 20:2515.6 12.8 1
2-Hexanone <7.5 ug/kg 02/24/23 21:40 591-78-602/24/23 20:2578.0 7.5 1
Isopropylbenzene (Cumene)<2.7 ug/kg 02/24/23 21:40 98-82-802/24/23 20:257.8 2.7 1
p-Isopropyltoluene <3.8 ug/kg 02/24/23 21:40 99-87-602/24/23 20:257.8 3.8 1
Methylene Chloride <21.4 ug/kg 02/24/23 21:40 75-09-202/24/23 20:2531.2 21.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-1 (1-2)Lab ID:92653934008 Collected:02/23/23 10:45 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<7.5 ug/kg 02/24/23 21:40 108-10-102/24/23 20:2578.0 7.5 1
Methyl-tert-butyl ether <2.9 ug/kg 02/24/23 21:40 1634-04-402/24/23 20:257.8 2.9 1
Naphthalene <4.1 ug/kg 02/24/23 21:40 91-20-302/24/23 20:257.8 4.1 1
n-Propylbenzene <2.8 ug/kg 02/24/23 21:40 103-65-102/24/23 20:257.8 2.8 1
Styrene <2.1 ug/kg 02/24/23 21:40 100-42-5 IK02/24/23 20:257.8 2.1 1
1,1,1,2-Tetrachloroethane <3.0 ug/kg 02/24/23 21:40 630-20-602/24/23 20:257.8 3.0 1
1,1,2,2-Tetrachloroethane <2.1 ug/kg 02/24/23 21:40 79-34-502/24/23 20:257.8 2.1 1
Tetrachloroethene <2.5 ug/kg 02/24/23 21:40 127-18-402/24/23 20:257.8 2.5 1
Toluene <5.4 ug/kg 02/24/23 21:40 108-88-302/24/23 20:257.8 5.4 1
1,2,3-Trichlorobenzene <6.3 ug/kg 02/24/23 21:40 87-61-6 M102/24/23 20:257.8 6.3 1
1,2,4-Trichlorobenzene <6.5 ug/kg 02/24/23 21:40 120-82-102/24/23 20:257.8 6.5 1
1,1,1-Trichloroethane <4.1 ug/kg 02/24/23 21:40 71-55-602/24/23 20:257.8 4.1 1
1,1,2-Trichloroethane <2.6 ug/kg 02/24/23 21:40 79-00-502/24/23 20:257.8 2.6 1
Trichloroethene <6.3 ug/kg 02/24/23 21:40 79-01-602/24/23 20:257.8 6.3 1
Trichlorofluoromethane <4.3 ug/kg 02/24/23 21:40 75-69-402/24/23 20:257.8 4.3 1
1,2,3-Trichloropropane <3.9 ug/kg 02/24/23 21:40 96-18-402/24/23 20:257.8 3.9 1
1,2,4-Trimethylbenzene <4.6 ug/kg 02/24/23 21:40 95-63-602/24/23 20:257.8 4.6 1
1,3,5-Trimethylbenzene <2.6 ug/kg 02/24/23 21:40 108-67-802/24/23 20:257.8 2.6 1
Vinyl acetate <16.0 ug/kg 02/24/23 21:40 108-05-402/24/23 20:2578.0 16.0 1
Vinyl chloride <4.0 ug/kg 02/24/23 21:40 75-01-402/24/23 20:2515.6 4.0 1
Xylene (Total)<4.4 ug/kg 02/24/23 21:40 1330-20-702/24/23 20:2515.6 4.4 1
m&p-Xylene <5.3 ug/kg 02/24/23 21:40 179601-23-102/24/23 20:2515.6 5.3 1
o-Xylene <3.4 ug/kg 02/24/23 21:40 95-47-602/24/23 20:257.8 3.4 1
Surrogates
Toluene-d8 (S)100 %02/24/23 21:40 2037-26-502/24/23 20:2570-130 1
4-Bromofluorobenzene (S)106 %02/24/23 21:40 460-00-402/24/23 20:2570-130 1
1,2-Dichloroethane-d4 (S)112 %02/24/23 21:40 17060-07-002/24/23 20:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.4 %02/24/23 16:43 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-2 (1-2)Lab ID:92653934009 Collected:02/23/23 12:40 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <55.1 ug/kg 02/24/23 23:32 67-64-102/24/23 20:2517255.1 1
Benzene <3.4 ug/kg 02/24/23 23:32 71-43-202/24/23 20:258.6 3.4 1
Bromobenzene <2.8 ug/kg 02/24/23 23:32 108-86-102/24/23 20:258.6 2.8 1
Bromochloromethane <2.5 ug/kg 02/24/23 23:32 74-97-502/24/23 20:258.6 2.5 1
Bromodichloromethane <3.3 ug/kg 02/24/23 23:32 75-27-402/24/23 20:258.6 3.3 1
Bromoform <3.0 ug/kg 02/24/23 23:32 75-25-202/24/23 20:258.6 3.0 1
Bromomethane <26.6 ug/kg 02/24/23 23:32 74-83-902/24/23 20:2534.3 26.6 1
2-Butanone (MEK)<41.2 ug/kg 02/24/23 23:32 78-93-302/24/23 20:2517241.2 1
n-Butylbenzene <5.4 ug/kg 02/24/23 23:32 104-51-802/24/23 20:258.6 5.4 1
sec-Butylbenzene <3.8 ug/kg 02/24/23 23:32 135-98-802/24/23 20:258.6 3.8 1
tert-Butylbenzene <3.1 ug/kg 02/24/23 23:32 98-06-602/24/23 20:258.6 3.1 1
Carbon tetrachloride <3.2 ug/kg 02/24/23 23:32 56-23-5 IK02/24/23 20:258.6 3.2 1
Chlorobenzene <4.9 ug/kg 02/24/23 23:32 108-90-702/24/23 20:258.6 4.9 1
Chloroethane <6.6 ug/kg 02/24/23 23:32 75-00-302/24/23 20:2517.2 6.6 1
Chloroform <7.2 ug/kg 02/24/23 23:32 67-66-302/24/23 20:258.6 7.2 1
Chloromethane <7.2 ug/kg 02/24/23 23:32 74-87-302/24/23 20:2517.2 7.2 1
2-Chlorotoluene <3.0 ug/kg 02/24/23 23:32 95-49-802/24/23 20:258.6 3.0 1
4-Chlorotoluene <4.8 ug/kg 02/24/23 23:32 106-43-402/24/23 20:258.6 4.8 1
1,2-Dibromo-3-chloropropane <3.3 ug/kg 02/24/23 23:32 96-12-802/24/23 20:258.6 3.3 1
Dibromochloromethane <4.8 ug/kg 02/24/23 23:32 124-48-1 IK02/24/23 20:258.6 4.8 1
1,2-Dibromoethane (EDB)<3.8 ug/kg 02/24/23 23:32 106-93-402/24/23 20:258.6 3.8 1
Dibromomethane <1.8 ug/kg 02/24/23 23:32 74-95-302/24/23 20:258.6 1.8 1
1,2-Dichlorobenzene <3.1 ug/kg 02/24/23 23:32 95-50-102/24/23 20:258.6 3.1 1
1,3-Dichlorobenzene <2.7 ug/kg 02/24/23 23:32 541-73-102/24/23 20:258.6 2.7 1
1,4-Dichlorobenzene <2.2 ug/kg 02/24/23 23:32 106-46-702/24/23 20:258.6 2.2 1
Dichlorodifluoromethane <8.7 ug/kg 02/24/23 23:32 75-71-802/24/23 20:2517.2 8.7 1
1,1-Dichloroethane <3.5 ug/kg 02/24/23 23:32 75-34-302/24/23 20:258.6 3.5 1
1,2-Dichloroethane <5.7 ug/kg 02/24/23 23:32 107-06-202/24/23 20:258.6 5.7 1
1,1-Dichloroethene <3.5 ug/kg 02/24/23 23:32 75-35-402/24/23 20:258.6 3.5 1
cis-1,2-Dichloroethene <2.9 ug/kg 02/24/23 23:32 156-59-202/24/23 20:258.6 2.9 1
trans-1,2-Dichloroethene <7.3 ug/kg 02/24/23 23:32 156-60-502/24/23 20:258.6 7.3 1
1,2-Dichloropropane <2.6 ug/kg 02/24/23 23:32 78-87-502/24/23 20:258.6 2.6 1
1,3-Dichloropropane <2.7 ug/kg 02/24/23 23:32 142-28-902/24/23 20:258.6 2.7 1
2,2-Dichloropropane <6.5 ug/kg 02/24/23 23:32 594-20-7 v202/24/23 20:258.6 6.5 1
1,1-Dichloropropene <4.1 ug/kg 02/24/23 23:32 563-58-602/24/23 20:258.6 4.1 1
cis-1,3-Dichloropropene <2.3 ug/kg 02/24/23 23:32 10061-01-502/24/23 20:258.6 2.3 1
trans-1,3-Dichloropropene <3.0 ug/kg 02/24/23 23:32 10061-02-602/24/23 20:258.6 3.0 1
Diisopropyl ether <2.3 ug/kg 02/24/23 23:32 108-20-302/24/23 20:258.6 2.3 1
Ethylbenzene <4.0 ug/kg 02/24/23 23:32 100-41-402/24/23 20:258.6 4.0 1
Hexachloro-1,3-butadiene <14.0 ug/kg 02/24/23 23:32 87-68-302/24/23 20:2517.2 14.0 1
2-Hexanone <8.3 ug/kg 02/24/23 23:32 591-78-602/24/23 20:2585.9 8.3 1
Isopropylbenzene (Cumene)<2.9 ug/kg 02/24/23 23:32 98-82-802/24/23 20:258.6 2.9 1
p-Isopropyltoluene <4.2 ug/kg 02/24/23 23:32 99-87-602/24/23 20:258.6 4.2 1
Methylene Chloride <23.5 ug/kg 02/24/23 23:32 75-09-202/24/23 20:2534.3 23.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-2 (1-2)Lab ID:92653934009 Collected:02/23/23 12:40 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<8.3 ug/kg 02/24/23 23:32 108-10-102/24/23 20:2585.9 8.3 1
Methyl-tert-butyl ether <3.2 ug/kg 02/24/23 23:32 1634-04-402/24/23 20:258.6 3.2 1
Naphthalene <4.5 ug/kg 02/24/23 23:32 91-20-302/24/23 20:258.6 4.5 1
n-Propylbenzene <3.1 ug/kg 02/24/23 23:32 103-65-102/24/23 20:258.6 3.1 1
Styrene <2.3 ug/kg 02/24/23 23:32 100-42-5 IK02/24/23 20:258.6 2.3 1
1,1,1,2-Tetrachloroethane <3.3 ug/kg 02/24/23 23:32 630-20-602/24/23 20:258.6 3.3 1
1,1,2,2-Tetrachloroethane <2.3 ug/kg 02/24/23 23:32 79-34-502/24/23 20:258.6 2.3 1
Tetrachloroethene <2.7 ug/kg 02/24/23 23:32 127-18-402/24/23 20:258.6 2.7 1
Toluene <5.9 ug/kg 02/24/23 23:32 108-88-302/24/23 20:258.6 5.9 1
1,2,3-Trichlorobenzene <6.9 ug/kg 02/24/23 23:32 87-61-602/24/23 20:258.6 6.9 1
1,2,4-Trichlorobenzene <7.2 ug/kg 02/24/23 23:32 120-82-102/24/23 20:258.6 7.2 1
1,1,1-Trichloroethane <4.5 ug/kg 02/24/23 23:32 71-55-602/24/23 20:258.6 4.5 1
1,1,2-Trichloroethane <2.9 ug/kg 02/24/23 23:32 79-00-502/24/23 20:258.6 2.9 1
Trichloroethene <6.9 ug/kg 02/24/23 23:32 79-01-602/24/23 20:258.6 6.9 1
Trichlorofluoromethane <4.7 ug/kg 02/24/23 23:32 75-69-402/24/23 20:258.6 4.7 1
1,2,3-Trichloropropane <4.3 ug/kg 02/24/23 23:32 96-18-402/24/23 20:258.6 4.3 1
1,2,4-Trimethylbenzene <5.1 ug/kg 02/24/23 23:32 95-63-602/24/23 20:258.6 5.1 1
1,3,5-Trimethylbenzene <2.9 ug/kg 02/24/23 23:32 108-67-802/24/23 20:258.6 2.9 1
Vinyl acetate <17.7 ug/kg 02/24/23 23:32 108-05-402/24/23 20:2585.9 17.7 1
Vinyl chloride <4.4 ug/kg 02/24/23 23:32 75-01-402/24/23 20:2517.2 4.4 1
Xylene (Total)<4.9 ug/kg 02/24/23 23:32 1330-20-702/24/23 20:2517.2 4.9 1
m&p-Xylene <5.9 ug/kg 02/24/23 23:32 179601-23-102/24/23 20:2517.2 5.9 1
o-Xylene <3.8 ug/kg 02/24/23 23:32 95-47-602/24/23 20:258.6 3.8 1
Surrogates
Toluene-d8 (S)100 %02/24/23 23:32 2037-26-502/24/23 20:2570-130 1
4-Bromofluorobenzene (S)107 %02/24/23 23:32 460-00-402/24/23 20:2570-130 1
1,2-Dichloroethane-d4 (S)110 %02/24/23 23:32 17060-07-002/24/23 20:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %02/24/23 17:07 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-3 (1-2)Lab ID:92653934010 Collected:02/23/23 14:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <49.1 ug/kg 02/24/23 21:59 67-64-102/24/23 20:2515349.1 1
Benzene <3.0 ug/kg 02/24/23 21:59 71-43-202/24/23 20:257.6 3.0 1
Bromobenzene <2.5 ug/kg 02/24/23 21:59 108-86-102/24/23 20:257.6 2.5 1
Bromochloromethane <2.3 ug/kg 02/24/23 21:59 74-97-502/24/23 20:257.6 2.3 1
Bromodichloromethane <2.9 ug/kg 02/24/23 21:59 75-27-402/24/23 20:257.6 2.9 1
Bromoform <2.7 ug/kg 02/24/23 21:59 75-25-202/24/23 20:257.6 2.7 1
Bromomethane <23.7 ug/kg 02/24/23 21:59 74-83-902/24/23 20:2530.6 23.7 1
2-Butanone (MEK)<36.7 ug/kg 02/24/23 21:59 78-93-302/24/23 20:2515336.7 1
n-Butylbenzene <4.8 ug/kg 02/24/23 21:59 104-51-802/24/23 20:257.6 4.8 1
sec-Butylbenzene <3.4 ug/kg 02/24/23 21:59 135-98-802/24/23 20:257.6 3.4 1
tert-Butylbenzene <2.7 ug/kg 02/24/23 21:59 98-06-602/24/23 20:257.6 2.7 1
Carbon tetrachloride <2.9 ug/kg 02/24/23 21:59 56-23-5 IK02/24/23 20:257.6 2.9 1
Chlorobenzene <4.4 ug/kg 02/24/23 21:59 108-90-702/24/23 20:257.6 4.4 1
Chloroethane <5.9 ug/kg 02/24/23 21:59 75-00-302/24/23 20:2515.3 5.9 1
Chloroform <6.4 ug/kg 02/24/23 21:59 67-66-302/24/23 20:257.6 6.4 1
Chloromethane <6.4 ug/kg 02/24/23 21:59 74-87-302/24/23 20:2515.3 6.4 1
2-Chlorotoluene <2.7 ug/kg 02/24/23 21:59 95-49-802/24/23 20:257.6 2.7 1
4-Chlorotoluene <4.2 ug/kg 02/24/23 21:59 106-43-402/24/23 20:257.6 4.2 1
1,2-Dibromo-3-chloropropane <3.0 ug/kg 02/24/23 21:59 96-12-802/24/23 20:257.6 3.0 1
Dibromochloromethane <4.3 ug/kg 02/24/23 21:59 124-48-1 IK02/24/23 20:257.6 4.3 1
1,2-Dibromoethane (EDB)<3.4 ug/kg 02/24/23 21:59 106-93-402/24/23 20:257.6 3.4 1
Dibromomethane <1.6 ug/kg 02/24/23 21:59 74-95-302/24/23 20:257.6 1.6 1
1,2-Dichlorobenzene <2.8 ug/kg 02/24/23 21:59 95-50-102/24/23 20:257.6 2.8 1
1,3-Dichlorobenzene <2.4 ug/kg 02/24/23 21:59 541-73-102/24/23 20:257.6 2.4 1
1,4-Dichlorobenzene <2.0 ug/kg 02/24/23 21:59 106-46-702/24/23 20:257.6 2.0 1
Dichlorodifluoromethane <7.8 ug/kg 02/24/23 21:59 75-71-802/24/23 20:2515.3 7.8 1
1,1-Dichloroethane <3.1 ug/kg 02/24/23 21:59 75-34-302/24/23 20:257.6 3.1 1
1,2-Dichloroethane <5.1 ug/kg 02/24/23 21:59 107-06-202/24/23 20:257.6 5.1 1
1,1-Dichloroethene <3.1 ug/kg 02/24/23 21:59 75-35-402/24/23 20:257.6 3.1 1
cis-1,2-Dichloroethene <2.6 ug/kg 02/24/23 21:59 156-59-202/24/23 20:257.6 2.6 1
trans-1,2-Dichloroethene <6.5 ug/kg 02/24/23 21:59 156-60-502/24/23 20:257.6 6.5 1
1,2-Dichloropropane <2.3 ug/kg 02/24/23 21:59 78-87-502/24/23 20:257.6 2.3 1
1,3-Dichloropropane <2.4 ug/kg 02/24/23 21:59 142-28-902/24/23 20:257.6 2.4 1
2,2-Dichloropropane <5.8 ug/kg 02/24/23 21:59 594-20-7 v202/24/23 20:257.6 5.8 1
1,1-Dichloropropene <3.7 ug/kg 02/24/23 21:59 563-58-602/24/23 20:257.6 3.7 1
cis-1,3-Dichloropropene <2.1 ug/kg 02/24/23 21:59 10061-01-502/24/23 20:257.6 2.1 1
trans-1,3-Dichloropropene <2.6 ug/kg 02/24/23 21:59 10061-02-602/24/23 20:257.6 2.6 1
Diisopropyl ether <2.1 ug/kg 02/24/23 21:59 108-20-302/24/23 20:257.6 2.1 1
Ethylbenzene <3.6 ug/kg 02/24/23 21:59 100-41-402/24/23 20:257.6 3.6 1
Hexachloro-1,3-butadiene <12.5 ug/kg 02/24/23 21:59 87-68-302/24/23 20:2515.3 12.5 1
2-Hexanone <7.4 ug/kg 02/24/23 21:59 591-78-602/24/23 20:2576.4 7.4 1
Isopropylbenzene (Cumene)<2.6 ug/kg 02/24/23 21:59 98-82-802/24/23 20:257.6 2.6 1
p-Isopropyltoluene <3.8 ug/kg 02/24/23 21:59 99-87-602/24/23 20:257.6 3.8 1
Methylene Chloride <20.9 ug/kg 02/24/23 21:59 75-09-202/24/23 20:2530.6 20.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-3 (1-2)Lab ID:92653934010 Collected:02/23/23 14:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<7.4 ug/kg 02/24/23 21:59 108-10-102/24/23 20:2576.4 7.4 1
Methyl-tert-butyl ether <2.9 ug/kg 02/24/23 21:59 1634-04-402/24/23 20:257.6 2.9 1
Naphthalene <4.0 ug/kg 02/24/23 21:59 91-20-302/24/23 20:257.6 4.0 1
n-Propylbenzene <2.7 ug/kg 02/24/23 21:59 103-65-102/24/23 20:257.6 2.7 1
Styrene <2.0 ug/kg 02/24/23 21:59 100-42-5 IK02/24/23 20:257.6 2.0 1
1,1,1,2-Tetrachloroethane <2.9 ug/kg 02/24/23 21:59 630-20-602/24/23 20:257.6 2.9 1
1,1,2,2-Tetrachloroethane <2.0 ug/kg 02/24/23 21:59 79-34-502/24/23 20:257.6 2.0 1
Tetrachloroethene <2.4 ug/kg 02/24/23 21:59 127-18-402/24/23 20:257.6 2.4 1
Toluene <5.3 ug/kg 02/24/23 21:59 108-88-302/24/23 20:257.6 5.3 1
1,2,3-Trichlorobenzene <6.2 ug/kg 02/24/23 21:59 87-61-602/24/23 20:257.6 6.2 1
1,2,4-Trichlorobenzene <6.4 ug/kg 02/24/23 21:59 120-82-102/24/23 20:257.6 6.4 1
1,1,1-Trichloroethane <4.0 ug/kg 02/24/23 21:59 71-55-602/24/23 20:257.6 4.0 1
1,1,2-Trichloroethane <2.5 ug/kg 02/24/23 21:59 79-00-502/24/23 20:257.6 2.5 1
Trichloroethene <6.2 ug/kg 02/24/23 21:59 79-01-602/24/23 20:257.6 6.2 1
Trichlorofluoromethane <4.2 ug/kg 02/24/23 21:59 75-69-402/24/23 20:257.6 4.2 1
1,2,3-Trichloropropane <3.9 ug/kg 02/24/23 21:59 96-18-402/24/23 20:257.6 3.9 1
1,2,4-Trimethylbenzene <4.5 ug/kg 02/24/23 21:59 95-63-602/24/23 20:257.6 4.5 1
1,3,5-Trimethylbenzene <2.6 ug/kg 02/24/23 21:59 108-67-802/24/23 20:257.6 2.6 1
Vinyl acetate <15.7 ug/kg 02/24/23 21:59 108-05-402/24/23 20:2576.4 15.7 1
Vinyl chloride <3.9 ug/kg 02/24/23 21:59 75-01-402/24/23 20:2515.3 3.9 1
Xylene (Total)<4.4 ug/kg 02/24/23 21:59 1330-20-702/24/23 20:2515.3 4.4 1
m&p-Xylene <5.2 ug/kg 02/24/23 21:59 179601-23-102/24/23 20:2515.3 5.2 1
o-Xylene <3.4 ug/kg 02/24/23 21:59 95-47-602/24/23 20:257.6 3.4 1
Surrogates
Toluene-d8 (S)101 %02/24/23 21:59 2037-26-502/24/23 20:2570-130 1
4-Bromofluorobenzene (S)106 %02/24/23 21:59 460-00-402/24/23 20:2570-130 1
1,2-Dichloroethane-d4 (S)111 %02/24/23 21:59 17060-07-002/24/23 20:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.3 %02/24/23 17:07 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-8 (1-2)Lab ID:92653934011 Collected:02/23/23 15:15 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <48.6 ug/kg 02/24/23 23:51 67-64-102/24/23 20:2515148.6 1
Benzene <3.0 ug/kg 02/24/23 23:51 71-43-202/24/23 20:257.6 3.0 1
Bromobenzene <2.5 ug/kg 02/24/23 23:51 108-86-102/24/23 20:257.6 2.5 1
Bromochloromethane <2.2 ug/kg 02/24/23 23:51 74-97-502/24/23 20:257.6 2.2 1
Bromodichloromethane <2.9 ug/kg 02/24/23 23:51 75-27-402/24/23 20:257.6 2.9 1
Bromoform <2.7 ug/kg 02/24/23 23:51 75-25-202/24/23 20:257.6 2.7 1
Bromomethane <23.4 ug/kg 02/24/23 23:51 74-83-902/24/23 20:2530.3 23.4 1
2-Butanone (MEK)<36.3 ug/kg 02/24/23 23:51 78-93-302/24/23 20:2515136.3 1
n-Butylbenzene <4.8 ug/kg 02/24/23 23:51 104-51-802/24/23 20:257.6 4.8 1
sec-Butylbenzene <3.3 ug/kg 02/24/23 23:51 135-98-802/24/23 20:257.6 3.3 1
tert-Butylbenzene <2.7 ug/kg 02/24/23 23:51 98-06-602/24/23 20:257.6 2.7 1
Carbon tetrachloride <2.8 ug/kg 02/24/23 23:51 56-23-5 IK02/24/23 20:257.6 2.8 1
Chlorobenzene <4.3 ug/kg 02/24/23 23:51 108-90-702/24/23 20:257.6 4.3 1
Chloroethane <5.8 ug/kg 02/24/23 23:51 75-00-302/24/23 20:2515.1 5.8 1
Chloroform <6.3 ug/kg 02/24/23 23:51 67-66-302/24/23 20:257.6 6.3 1
Chloromethane <6.4 ug/kg 02/24/23 23:51 74-87-302/24/23 20:2515.1 6.4 1
2-Chlorotoluene <2.7 ug/kg 02/24/23 23:51 95-49-802/24/23 20:257.6 2.7 1
4-Chlorotoluene <4.2 ug/kg 02/24/23 23:51 106-43-402/24/23 20:257.6 4.2 1
1,2-Dibromo-3-chloropropane <2.9 ug/kg 02/24/23 23:51 96-12-802/24/23 20:257.6 2.9 1
Dibromochloromethane <4.3 ug/kg 02/24/23 23:51 124-48-1 IK02/24/23 20:257.6 4.3 1
1,2-Dibromoethane (EDB)<3.3 ug/kg 02/24/23 23:51 106-93-402/24/23 20:257.6 3.3 1
Dibromomethane <1.6 ug/kg 02/24/23 23:51 74-95-302/24/23 20:257.6 1.6 1
1,2-Dichlorobenzene <2.7 ug/kg 02/24/23 23:51 95-50-102/24/23 20:257.6 2.7 1
1,3-Dichlorobenzene <2.3 ug/kg 02/24/23 23:51 541-73-102/24/23 20:257.6 2.3 1
1,4-Dichlorobenzene <2.0 ug/kg 02/24/23 23:51 106-46-702/24/23 20:257.6 2.0 1
Dichlorodifluoromethane <7.7 ug/kg 02/24/23 23:51 75-71-802/24/23 20:2515.1 7.7 1
1,1-Dichloroethane <3.1 ug/kg 02/24/23 23:51 75-34-302/24/23 20:257.6 3.1 1
1,2-Dichloroethane <5.0 ug/kg 02/24/23 23:51 107-06-202/24/23 20:257.6 5.0 1
1,1-Dichloroethene <3.1 ug/kg 02/24/23 23:51 75-35-402/24/23 20:257.6 3.1 1
cis-1,2-Dichloroethene <2.6 ug/kg 02/24/23 23:51 156-59-202/24/23 20:257.6 2.6 1
trans-1,2-Dichloroethene <6.4 ug/kg 02/24/23 23:51 156-60-502/24/23 20:257.6 6.4 1
1,2-Dichloropropane <2.3 ug/kg 02/24/23 23:51 78-87-502/24/23 20:257.6 2.3 1
1,3-Dichloropropane <2.4 ug/kg 02/24/23 23:51 142-28-902/24/23 20:257.6 2.4 1
2,2-Dichloropropane <5.7 ug/kg 02/24/23 23:51 594-20-7 v202/24/23 20:257.6 5.7 1
1,1-Dichloropropene <3.6 ug/kg 02/24/23 23:51 563-58-602/24/23 20:257.6 3.6 1
cis-1,3-Dichloropropene <2.1 ug/kg 02/24/23 23:51 10061-01-502/24/23 20:257.6 2.1 1
trans-1,3-Dichloropropene <2.6 ug/kg 02/24/23 23:51 10061-02-602/24/23 20:257.6 2.6 1
Diisopropyl ether <2.0 ug/kg 02/24/23 23:51 108-20-302/24/23 20:257.6 2.0 1
Ethylbenzene <3.5 ug/kg 02/24/23 23:51 100-41-402/24/23 20:257.6 3.5 1
Hexachloro-1,3-butadiene <12.4 ug/kg 02/24/23 23:51 87-68-302/24/23 20:2515.1 12.4 1
2-Hexanone <7.3 ug/kg 02/24/23 23:51 591-78-602/24/23 20:2575.6 7.3 1
Isopropylbenzene (Cumene)<2.6 ug/kg 02/24/23 23:51 98-82-802/24/23 20:257.6 2.6 1
p-Isopropyltoluene <3.7 ug/kg 02/24/23 23:51 99-87-602/24/23 20:257.6 3.7 1
Methylene Chloride <20.7 ug/kg 02/24/23 23:51 75-09-202/24/23 20:2530.3 20.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-8 (1-2)Lab ID:92653934011 Collected:02/23/23 15:15 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<7.3 ug/kg 02/24/23 23:51 108-10-102/24/23 20:2575.6 7.3 1
Methyl-tert-butyl ether <2.8 ug/kg 02/24/23 23:51 1634-04-402/24/23 20:257.6 2.8 1
Naphthalene <4.0 ug/kg 02/24/23 23:51 91-20-302/24/23 20:257.6 4.0 1
n-Propylbenzene <2.7 ug/kg 02/24/23 23:51 103-65-102/24/23 20:257.6 2.7 1
Styrene 24.4 ug/kg 02/24/23 23:51 100-42-5 IK02/24/23 20:257.6 2.0 1
1,1,1,2-Tetrachloroethane <2.9 ug/kg 02/24/23 23:51 630-20-602/24/23 20:257.6 2.9 1
1,1,2,2-Tetrachloroethane <2.0 ug/kg 02/24/23 23:51 79-34-502/24/23 20:257.6 2.0 1
Tetrachloroethene <2.4 ug/kg 02/24/23 23:51 127-18-402/24/23 20:257.6 2.4 1
Toluene <5.2 ug/kg 02/24/23 23:51 108-88-302/24/23 20:257.6 5.2 1
1,2,3-Trichlorobenzene <6.1 ug/kg 02/24/23 23:51 87-61-602/24/23 20:257.6 6.1 1
1,2,4-Trichlorobenzene <6.4 ug/kg 02/24/23 23:51 120-82-102/24/23 20:257.6 6.4 1
1,1,1-Trichloroethane <3.9 ug/kg 02/24/23 23:51 71-55-602/24/23 20:257.6 3.9 1
1,1,2-Trichloroethane <2.5 ug/kg 02/24/23 23:51 79-00-502/24/23 20:257.6 2.5 1
Trichloroethene <6.1 ug/kg 02/24/23 23:51 79-01-602/24/23 20:257.6 6.1 1
Trichlorofluoromethane <4.2 ug/kg 02/24/23 23:51 75-69-402/24/23 20:257.6 4.2 1
1,2,3-Trichloropropane <3.8 ug/kg 02/24/23 23:51 96-18-402/24/23 20:257.6 3.8 1
1,2,4-Trimethylbenzene <4.5 ug/kg 02/24/23 23:51 95-63-602/24/23 20:257.6 4.5 1
1,3,5-Trimethylbenzene <2.5 ug/kg 02/24/23 23:51 108-67-802/24/23 20:257.6 2.5 1
Vinyl acetate <15.6 ug/kg 02/24/23 23:51 108-05-402/24/23 20:2575.6 15.6 1
Vinyl chloride <3.8 ug/kg 02/24/23 23:51 75-01-402/24/23 20:2515.1 3.8 1
Xylene (Total)<4.3 ug/kg 02/24/23 23:51 1330-20-702/24/23 20:2515.1 4.3 1
m&p-Xylene <5.2 ug/kg 02/24/23 23:51 179601-23-102/24/23 20:2515.1 5.2 1
o-Xylene 3.9J ug/kg 02/24/23 23:51 95-47-602/24/23 20:257.6 3.3 1
Surrogates
Toluene-d8 (S)101 %02/24/23 23:51 2037-26-502/24/23 20:2570-130 1
4-Bromofluorobenzene (S)104 %02/24/23 23:51 460-00-402/24/23 20:2570-130 1
1,2-Dichloroethane-d4 (S)111 %02/24/23 23:51 17060-07-002/24/23 20:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.1 %02/24/23 17:07 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-9 (1-2)Lab ID:92653934012 Collected:02/23/23 16:25 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <43.5 ug/kg 02/24/23 23:13 67-64-102/24/23 20:2513543.5 1
Benzene <2.7 ug/kg 02/24/23 23:13 71-43-202/24/23 20:256.8 2.7 1
Bromobenzene <2.2 ug/kg 02/24/23 23:13 108-86-102/24/23 20:256.8 2.2 1
Bromochloromethane <2.0 ug/kg 02/24/23 23:13 74-97-502/24/23 20:256.8 2.0 1
Bromodichloromethane <2.6 ug/kg 02/24/23 23:13 75-27-402/24/23 20:256.8 2.6 1
Bromoform <2.4 ug/kg 02/24/23 23:13 75-25-202/24/23 20:256.8 2.4 1
Bromomethane <21.0 ug/kg 02/24/23 23:13 74-83-902/24/23 20:2527.1 21.0 1
2-Butanone (MEK)<32.5 ug/kg 02/24/23 23:13 78-93-302/24/23 20:2513532.5 1
n-Butylbenzene <4.3 ug/kg 02/24/23 23:13 104-51-802/24/23 20:256.8 4.3 1
sec-Butylbenzene <3.0 ug/kg 02/24/23 23:13 135-98-802/24/23 20:256.8 3.0 1
tert-Butylbenzene <2.4 ug/kg 02/24/23 23:13 98-06-602/24/23 20:256.8 2.4 1
Carbon tetrachloride <2.5 ug/kg 02/24/23 23:13 56-23-5 IK02/24/23 20:256.8 2.5 1
Chlorobenzene <3.9 ug/kg 02/24/23 23:13 108-90-702/24/23 20:256.8 3.9 1
Chloroethane <5.2 ug/kg 02/24/23 23:13 75-00-302/24/23 20:2513.5 5.2 1
Chloroform <5.7 ug/kg 02/24/23 23:13 67-66-302/24/23 20:256.8 5.7 1
Chloromethane <5.7 ug/kg 02/24/23 23:13 74-87-302/24/23 20:2513.5 5.7 1
2-Chlorotoluene <2.4 ug/kg 02/24/23 23:13 95-49-802/24/23 20:256.8 2.4 1
4-Chlorotoluene <3.8 ug/kg 02/24/23 23:13 106-43-402/24/23 20:256.8 3.8 1
1,2-Dibromo-3-chloropropane <2.6 ug/kg 02/24/23 23:13 96-12-802/24/23 20:256.8 2.6 1
Dibromochloromethane <3.8 ug/kg 02/24/23 23:13 124-48-1 IK02/24/23 20:256.8 3.8 1
1,2-Dibromoethane (EDB)<3.0 ug/kg 02/24/23 23:13 106-93-402/24/23 20:256.8 3.0 1
Dibromomethane <1.4 ug/kg 02/24/23 23:13 74-95-302/24/23 20:256.8 1.4 1
1,2-Dichlorobenzene <2.4 ug/kg 02/24/23 23:13 95-50-102/24/23 20:256.8 2.4 1
1,3-Dichlorobenzene <2.1 ug/kg 02/24/23 23:13 541-73-102/24/23 20:256.8 2.1 1
1,4-Dichlorobenzene <1.8 ug/kg 02/24/23 23:13 106-46-702/24/23 20:256.8 1.8 1
Dichlorodifluoromethane <6.9 ug/kg 02/24/23 23:13 75-71-802/24/23 20:2513.5 6.9 1
1,1-Dichloroethane <2.8 ug/kg 02/24/23 23:13 75-34-302/24/23 20:256.8 2.8 1
1,2-Dichloroethane <4.5 ug/kg 02/24/23 23:13 107-06-202/24/23 20:256.8 4.5 1
1,1-Dichloroethene <2.8 ug/kg 02/24/23 23:13 75-35-402/24/23 20:256.8 2.8 1
cis-1,2-Dichloroethene <2.3 ug/kg 02/24/23 23:13 156-59-202/24/23 20:256.8 2.3 1
trans-1,2-Dichloroethene <5.8 ug/kg 02/24/23 23:13 156-60-502/24/23 20:256.8 5.8 1
1,2-Dichloropropane <2.0 ug/kg 02/24/23 23:13 78-87-502/24/23 20:256.8 2.0 1
1,3-Dichloropropane <2.1 ug/kg 02/24/23 23:13 142-28-902/24/23 20:256.8 2.1 1
2,2-Dichloropropane <5.1 ug/kg 02/24/23 23:13 594-20-7 v202/24/23 20:256.8 5.1 1
1,1-Dichloropropene <3.3 ug/kg 02/24/23 23:13 563-58-602/24/23 20:256.8 3.3 1
cis-1,3-Dichloropropene <1.8 ug/kg 02/24/23 23:13 10061-01-502/24/23 20:256.8 1.8 1
trans-1,3-Dichloropropene <2.3 ug/kg 02/24/23 23:13 10061-02-602/24/23 20:256.8 2.3 1
Diisopropyl ether <1.8 ug/kg 02/24/23 23:13 108-20-302/24/23 20:256.8 1.8 1
Ethylbenzene <3.2 ug/kg 02/24/23 23:13 100-41-402/24/23 20:256.8 3.2 1
Hexachloro-1,3-butadiene <11.1 ug/kg 02/24/23 23:13 87-68-302/24/23 20:2513.5 11.1 1
2-Hexanone <6.5 ug/kg 02/24/23 23:13 591-78-602/24/23 20:2567.7 6.5 1
Isopropylbenzene (Cumene)<2.3 ug/kg 02/24/23 23:13 98-82-802/24/23 20:256.8 2.3 1
p-Isopropyltoluene <3.3 ug/kg 02/24/23 23:13 99-87-602/24/23 20:256.8 3.3 1
Methylene Chloride <18.6 ug/kg 02/24/23 23:13 75-09-202/24/23 20:2527.1 18.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-9 (1-2)Lab ID:92653934012 Collected:02/23/23 16:25 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<6.5 ug/kg 02/24/23 23:13 108-10-102/24/23 20:2567.7 6.5 1
Methyl-tert-butyl ether <2.5 ug/kg 02/24/23 23:13 1634-04-402/24/23 20:256.8 2.5 1
Naphthalene <3.6 ug/kg 02/24/23 23:13 91-20-302/24/23 20:256.8 3.6 1
n-Propylbenzene <2.4 ug/kg 02/24/23 23:13 103-65-102/24/23 20:256.8 2.4 1
Styrene <1.8 ug/kg 02/24/23 23:13 100-42-5 IK02/24/23 20:256.8 1.8 1
1,1,1,2-Tetrachloroethane <2.6 ug/kg 02/24/23 23:13 630-20-602/24/23 20:256.8 2.6 1
1,1,2,2-Tetrachloroethane <1.8 ug/kg 02/24/23 23:13 79-34-502/24/23 20:256.8 1.8 1
Tetrachloroethene <2.1 ug/kg 02/24/23 23:13 127-18-402/24/23 20:256.8 2.1 1
Toluene <4.7 ug/kg 02/24/23 23:13 108-88-302/24/23 20:256.8 4.7 1
1,2,3-Trichlorobenzene <5.5 ug/kg 02/24/23 23:13 87-61-602/24/23 20:256.8 5.5 1
1,2,4-Trichlorobenzene <5.7 ug/kg 02/24/23 23:13 120-82-102/24/23 20:256.8 5.7 1
1,1,1-Trichloroethane <3.5 ug/kg 02/24/23 23:13 71-55-602/24/23 20:256.8 3.5 1
1,1,2-Trichloroethane <2.2 ug/kg 02/24/23 23:13 79-00-502/24/23 20:256.8 2.2 1
Trichloroethene <5.5 ug/kg 02/24/23 23:13 79-01-602/24/23 20:256.8 5.5 1
Trichlorofluoromethane <3.7 ug/kg 02/24/23 23:13 75-69-402/24/23 20:256.8 3.7 1
1,2,3-Trichloropropane <3.4 ug/kg 02/24/23 23:13 96-18-402/24/23 20:256.8 3.4 1
1,2,4-Trimethylbenzene 5.3J ug/kg 02/24/23 23:13 95-63-602/24/23 20:256.8 4.0 1
1,3,5-Trimethylbenzene <2.3 ug/kg 02/24/23 23:13 108-67-802/24/23 20:256.8 2.3 1
Vinyl acetate <13.9 ug/kg 02/24/23 23:13 108-05-402/24/23 20:2567.7 13.9 1
Vinyl chloride <3.4 ug/kg 02/24/23 23:13 75-01-402/24/23 20:2513.5 3.4 1
Xylene (Total)<3.9 ug/kg 02/24/23 23:13 1330-20-702/24/23 20:2513.5 3.9 1
m&p-Xylene <4.6 ug/kg 02/24/23 23:13 179601-23-102/24/23 20:2513.5 4.6 1
o-Xylene <3.0 ug/kg 02/24/23 23:13 95-47-602/24/23 20:256.8 3.0 1
Surrogates
Toluene-d8 (S)100 %02/24/23 23:13 2037-26-502/24/23 20:2570-130 1
4-Bromofluorobenzene (S)110 %02/24/23 23:13 460-00-402/24/23 20:2570-130 1
1,2-Dichloroethane-d4 (S)108 %02/24/23 23:13 17060-07-002/24/23 20:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.9 %02/24/23 17:07 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-10 (0-1)Lab ID:92653934013 Collected:02/24/23 10:30 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <44.1 ug/kg 02/24/23 22:36 67-64-102/24/23 20:2513744.1 1
Benzene <2.7 ug/kg 02/24/23 22:36 71-43-202/24/23 20:256.9 2.7 1
Bromobenzene <2.2 ug/kg 02/24/23 22:36 108-86-102/24/23 20:256.9 2.2 1
Bromochloromethane <2.0 ug/kg 02/24/23 22:36 74-97-502/24/23 20:256.9 2.0 1
Bromodichloromethane <2.6 ug/kg 02/24/23 22:36 75-27-402/24/23 20:256.9 2.6 1
Bromoform <2.4 ug/kg 02/24/23 22:36 75-25-202/24/23 20:256.9 2.4 1
Bromomethane <21.3 ug/kg 02/24/23 22:36 74-83-902/24/23 20:2527.4 21.3 1
2-Butanone (MEK)<32.9 ug/kg 02/24/23 22:36 78-93-302/24/23 20:2513732.9 1
n-Butylbenzene <4.3 ug/kg 02/24/23 22:36 104-51-802/24/23 20:256.9 4.3 1
sec-Butylbenzene <3.0 ug/kg 02/24/23 22:36 135-98-802/24/23 20:256.9 3.0 1
tert-Butylbenzene <2.4 ug/kg 02/24/23 22:36 98-06-602/24/23 20:256.9 2.4 1
Carbon tetrachloride <2.6 ug/kg 02/24/23 22:36 56-23-5 IK02/24/23 20:256.9 2.6 1
Chlorobenzene <3.9 ug/kg 02/24/23 22:36 108-90-702/24/23 20:256.9 3.9 1
Chloroethane <5.3 ug/kg 02/24/23 22:36 75-00-302/24/23 20:2513.7 5.3 1
Chloroform <5.7 ug/kg 02/24/23 22:36 67-66-302/24/23 20:256.9 5.7 1
Chloromethane <5.8 ug/kg 02/24/23 22:36 74-87-302/24/23 20:2513.7 5.8 1
2-Chlorotoluene <2.4 ug/kg 02/24/23 22:36 95-49-802/24/23 20:256.9 2.4 1
4-Chlorotoluene <3.8 ug/kg 02/24/23 22:36 106-43-402/24/23 20:256.9 3.8 1
1,2-Dibromo-3-chloropropane <2.7 ug/kg 02/24/23 22:36 96-12-802/24/23 20:256.9 2.7 1
Dibromochloromethane <3.9 ug/kg 02/24/23 22:36 124-48-1 IK02/24/23 20:256.9 3.9 1
1,2-Dibromoethane (EDB)<3.0 ug/kg 02/24/23 22:36 106-93-402/24/23 20:256.9 3.0 1
Dibromomethane <1.5 ug/kg 02/24/23 22:36 74-95-302/24/23 20:256.9 1.5 1
1,2-Dichlorobenzene <2.5 ug/kg 02/24/23 22:36 95-50-102/24/23 20:256.9 2.5 1
1,3-Dichlorobenzene <2.1 ug/kg 02/24/23 22:36 541-73-102/24/23 20:256.9 2.1 1
1,4-Dichlorobenzene <1.8 ug/kg 02/24/23 22:36 106-46-702/24/23 20:256.9 1.8 1
Dichlorodifluoromethane <7.0 ug/kg 02/24/23 22:36 75-71-802/24/23 20:2513.7 7.0 1
1,1-Dichloroethane <2.8 ug/kg 02/24/23 22:36 75-34-302/24/23 20:256.9 2.8 1
1,2-Dichloroethane <4.5 ug/kg 02/24/23 22:36 107-06-202/24/23 20:256.9 4.5 1
1,1-Dichloroethene <2.8 ug/kg 02/24/23 22:36 75-35-402/24/23 20:256.9 2.8 1
cis-1,2-Dichloroethene <2.3 ug/kg 02/24/23 22:36 156-59-202/24/23 20:256.9 2.3 1
trans-1,2-Dichloroethene <5.8 ug/kg 02/24/23 22:36 156-60-502/24/23 20:256.9 5.8 1
1,2-Dichloropropane <2.1 ug/kg 02/24/23 22:36 78-87-502/24/23 20:256.9 2.1 1
1,3-Dichloropropane <2.1 ug/kg 02/24/23 22:36 142-28-902/24/23 20:256.9 2.1 1
2,2-Dichloropropane <5.2 ug/kg 02/24/23 22:36 594-20-7 v202/24/23 20:256.9 5.2 1
1,1-Dichloropropene <3.3 ug/kg 02/24/23 22:36 563-58-602/24/23 20:256.9 3.3 1
cis-1,3-Dichloropropene <1.9 ug/kg 02/24/23 22:36 10061-01-502/24/23 20:256.9 1.9 1
trans-1,3-Dichloropropene <2.4 ug/kg 02/24/23 22:36 10061-02-602/24/23 20:256.9 2.4 1
Diisopropyl ether <1.9 ug/kg 02/24/23 22:36 108-20-302/24/23 20:256.9 1.9 1
Ethylbenzene 23.0 ug/kg 02/24/23 22:36 100-41-402/24/23 20:256.9 3.2 1
Hexachloro-1,3-butadiene <11.2 ug/kg 02/24/23 22:36 87-68-302/24/23 20:2513.7 11.2 1
2-Hexanone <6.6 ug/kg 02/24/23 22:36 591-78-602/24/23 20:2568.6 6.6 1
Isopropylbenzene (Cumene)<2.3 ug/kg 02/24/23 22:36 98-82-802/24/23 20:256.9 2.3 1
p-Isopropyltoluene <3.4 ug/kg 02/24/23 22:36 99-87-602/24/23 20:256.9 3.4 1
Methylene Chloride <18.8 ug/kg 02/24/23 22:36 75-09-202/24/23 20:2527.4 18.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-10 (0-1)Lab ID:92653934013 Collected:02/24/23 10:30 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<6.6 ug/kg 02/24/23 22:36 108-10-102/24/23 20:2568.6 6.6 1
Methyl-tert-butyl ether <2.6 ug/kg 02/24/23 22:36 1634-04-402/24/23 20:256.9 2.6 1
Naphthalene 166 ug/kg 02/24/23 22:36 91-20-302/24/23 20:256.9 3.6 1
n-Propylbenzene 127 ug/kg 02/24/23 22:36 103-65-102/24/23 20:256.9 2.4 1
Styrene <1.8 ug/kg 02/24/23 22:36 100-42-5 IK02/24/23 20:256.9 1.8 1
1,1,1,2-Tetrachloroethane <2.6 ug/kg 02/24/23 22:36 630-20-602/24/23 20:256.9 2.6 1
1,1,2,2-Tetrachloroethane <1.8 ug/kg 02/24/23 22:36 79-34-502/24/23 20:256.9 1.8 1
Tetrachloroethene <2.2 ug/kg 02/24/23 22:36 127-18-402/24/23 20:256.9 2.2 1
Toluene <4.7 ug/kg 02/24/23 22:36 108-88-302/24/23 20:256.9 4.7 1
1,2,3-Trichlorobenzene <5.5 ug/kg 02/24/23 22:36 87-61-602/24/23 20:256.9 5.5 1
1,2,4-Trichlorobenzene <5.8 ug/kg 02/24/23 22:36 120-82-102/24/23 20:256.9 5.8 1
1,1,1-Trichloroethane <3.6 ug/kg 02/24/23 22:36 71-55-602/24/23 20:256.9 3.6 1
1,1,2-Trichloroethane <2.3 ug/kg 02/24/23 22:36 79-00-502/24/23 20:256.9 2.3 1
Trichloroethene <5.5 ug/kg 02/24/23 22:36 79-01-602/24/23 20:256.9 5.5 1
Trichlorofluoromethane <3.8 ug/kg 02/24/23 22:36 75-69-402/24/23 20:256.9 3.8 1
1,2,3-Trichloropropane <3.5 ug/kg 02/24/23 22:36 96-18-402/24/23 20:256.9 3.5 1
1,2,4-Trimethylbenzene 444 ug/kg 02/24/23 22:36 95-63-602/24/23 20:256.9 4.1 1
1,3,5-Trimethylbenzene <2.3 ug/kg 02/24/23 22:36 108-67-802/24/23 20:256.9 2.3 1
Vinyl acetate <14.1 ug/kg 02/24/23 22:36 108-05-402/24/23 20:2568.6 14.1 1
Vinyl chloride <3.5 ug/kg 02/24/23 22:36 75-01-402/24/23 20:2513.7 3.5 1
Xylene (Total)6.1J ug/kg 02/24/23 22:36 1330-20-702/24/23 20:2513.7 3.9 1
m&p-Xylene 6.1J ug/kg 02/24/23 22:36 179601-23-102/24/23 20:2513.7 4.7 1
o-Xylene <3.0 ug/kg 02/24/23 22:36 95-47-602/24/23 20:256.9 3.0 1
Surrogates
Toluene-d8 (S)101 %02/24/23 22:36 2037-26-502/24/23 20:2570-130 1
4-Bromofluorobenzene (S)110 %02/24/23 22:36 460-00-402/24/23 20:2570-130 1
1,2-Dichloroethane-d4 (S)108 %02/24/23 22:36 17060-07-002/24/23 20:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.5 %02/24/23 17:07 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-DUP (1-2)Lab ID:92653934014 Collected:02/23/23 00:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone <48.1 ug/kg 02/24/23 22:55 67-64-102/24/23 20:2515048.1 1
Benzene <3.0 ug/kg 02/24/23 22:55 71-43-202/24/23 20:257.5 3.0 1
Bromobenzene <2.4 ug/kg 02/24/23 22:55 108-86-102/24/23 20:257.5 2.4 1
Bromochloromethane <2.2 ug/kg 02/24/23 22:55 74-97-502/24/23 20:257.5 2.2 1
Bromodichloromethane <2.9 ug/kg 02/24/23 22:55 75-27-402/24/23 20:257.5 2.9 1
Bromoform <2.6 ug/kg 02/24/23 22:55 75-25-202/24/23 20:257.5 2.6 1
Bromomethane <23.2 ug/kg 02/24/23 22:55 74-83-902/24/23 20:2530.0 23.2 1
2-Butanone (MEK)<36.0 ug/kg 02/24/23 22:55 78-93-302/24/23 20:2515036.0 1
n-Butylbenzene <4.7 ug/kg 02/24/23 22:55 104-51-802/24/23 20:257.5 4.7 1
sec-Butylbenzene <3.3 ug/kg 02/24/23 22:55 135-98-802/24/23 20:257.5 3.3 1
tert-Butylbenzene <2.7 ug/kg 02/24/23 22:55 98-06-602/24/23 20:257.5 2.7 1
Carbon tetrachloride <2.8 ug/kg 02/24/23 22:55 56-23-5 IK02/24/23 20:257.5 2.8 1
Chlorobenzene <4.3 ug/kg 02/24/23 22:55 108-90-702/24/23 20:257.5 4.3 1
Chloroethane <5.8 ug/kg 02/24/23 22:55 75-00-302/24/23 20:2515.0 5.8 1
Chloroform <6.3 ug/kg 02/24/23 22:55 67-66-302/24/23 20:257.5 6.3 1
Chloromethane <6.3 ug/kg 02/24/23 22:55 74-87-302/24/23 20:2515.0 6.3 1
2-Chlorotoluene <2.7 ug/kg 02/24/23 22:55 95-49-802/24/23 20:257.5 2.7 1
4-Chlorotoluene <4.2 ug/kg 02/24/23 22:55 106-43-402/24/23 20:257.5 4.2 1
1,2-Dibromo-3-chloropropane <2.9 ug/kg 02/24/23 22:55 96-12-802/24/23 20:257.5 2.9 1
Dibromochloromethane <4.2 ug/kg 02/24/23 22:55 124-48-1 IK02/24/23 20:257.5 4.2 1
1,2-Dibromoethane (EDB)<3.3 ug/kg 02/24/23 22:55 106-93-402/24/23 20:257.5 3.3 1
Dibromomethane <1.6 ug/kg 02/24/23 22:55 74-95-302/24/23 20:257.5 1.6 1
1,2-Dichlorobenzene <2.7 ug/kg 02/24/23 22:55 95-50-102/24/23 20:257.5 2.7 1
1,3-Dichlorobenzene <2.3 ug/kg 02/24/23 22:55 541-73-102/24/23 20:257.5 2.3 1
1,4-Dichlorobenzene <1.9 ug/kg 02/24/23 22:55 106-46-702/24/23 20:257.5 1.9 1
Dichlorodifluoromethane <7.6 ug/kg 02/24/23 22:55 75-71-802/24/23 20:2515.0 7.6 1
1,1-Dichloroethane <3.1 ug/kg 02/24/23 22:55 75-34-302/24/23 20:257.5 3.1 1
1,2-Dichloroethane <5.0 ug/kg 02/24/23 22:55 107-06-202/24/23 20:257.5 5.0 1
1,1-Dichloroethene <3.1 ug/kg 02/24/23 22:55 75-35-402/24/23 20:257.5 3.1 1
cis-1,2-Dichloroethene <2.6 ug/kg 02/24/23 22:55 156-59-202/24/23 20:257.5 2.6 1
trans-1,2-Dichloroethene <6.4 ug/kg 02/24/23 22:55 156-60-502/24/23 20:257.5 6.4 1
1,2-Dichloropropane <2.2 ug/kg 02/24/23 22:55 78-87-502/24/23 20:257.5 2.2 1
1,3-Dichloropropane <2.3 ug/kg 02/24/23 22:55 142-28-902/24/23 20:257.5 2.3 1
2,2-Dichloropropane <5.7 ug/kg 02/24/23 22:55 594-20-7 v202/24/23 20:257.5 5.7 1
1,1-Dichloropropene <3.6 ug/kg 02/24/23 22:55 563-58-602/24/23 20:257.5 3.6 1
cis-1,3-Dichloropropene <2.0 ug/kg 02/24/23 22:55 10061-01-502/24/23 20:257.5 2.0 1
trans-1,3-Dichloropropene <2.6 ug/kg 02/24/23 22:55 10061-02-602/24/23 20:257.5 2.6 1
Diisopropyl ether <2.0 ug/kg 02/24/23 22:55 108-20-302/24/23 20:257.5 2.0 1
Ethylbenzene <3.5 ug/kg 02/24/23 22:55 100-41-402/24/23 20:257.5 3.5 1
Hexachloro-1,3-butadiene <12.3 ug/kg 02/24/23 22:55 87-68-302/24/23 20:2515.0 12.3 1
2-Hexanone <7.2 ug/kg 02/24/23 22:55 591-78-602/24/23 20:2575.0 7.2 1
Isopropylbenzene (Cumene)<2.5 ug/kg 02/24/23 22:55 98-82-802/24/23 20:257.5 2.5 1
p-Isopropyltoluene 4.7J ug/kg 02/24/23 22:55 99-87-602/24/23 20:257.5 3.7 1
Methylene Chloride <20.5 ug/kg 02/24/23 22:55 75-09-202/24/23 20:2530.0 20.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 75
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92653934
LEN-008
Sample:FG-DUP (1-2)Lab ID:92653934014 Collected:02/23/23 00:00 Received:02/24/23 12:41 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)<7.2 ug/kg 02/24/23 22:55 108-10-102/24/23 20:2575.0 7.2 1
Methyl-tert-butyl ether <2.8 ug/kg 02/24/23 22:55 1634-04-402/24/23 20:257.5 2.8 1
Naphthalene <3.9 ug/kg 02/24/23 22:55 91-20-302/24/23 20:257.5 3.9 1
n-Propylbenzene <2.7 ug/kg 02/24/23 22:55 103-65-102/24/23 20:257.5 2.7 1
Styrene <2.0 ug/kg 02/24/23 22:55 100-42-5 IK02/24/23 20:257.5 2.0 1
1,1,1,2-Tetrachloroethane <2.9 ug/kg 02/24/23 22:55 630-20-602/24/23 20:257.5 2.9 1
1,1,2,2-Tetrachloroethane <2.0 ug/kg 02/24/23 22:55 79-34-502/24/23 20:257.5 2.0 1
Tetrachloroethene <2.4 ug/kg 02/24/23 22:55 127-18-402/24/23 20:257.5 2.4 1
Toluene <5.2 ug/kg 02/24/23 22:55 108-88-302/24/23 20:257.5 5.2 1
1,2,3-Trichlorobenzene <6.1 ug/kg 02/24/23 22:55 87-61-602/24/23 20:257.5 6.1 1
1,2,4-Trichlorobenzene <6.3 ug/kg 02/24/23 22:55 120-82-102/24/23 20:257.5 6.3 1
1,1,1-Trichloroethane <3.9 ug/kg 02/24/23 22:55 71-55-602/24/23 20:257.5 3.9 1
1,1,2-Trichloroethane <2.5 ug/kg 02/24/23 22:55 79-00-502/24/23 20:257.5 2.5 1
Trichloroethene <6.0 ug/kg 02/24/23 22:55 79-01-602/24/23 20:257.5 6.0 1
Trichlorofluoromethane <4.1 ug/kg 02/24/23 22:55 75-69-402/24/23 20:257.5 4.1 1
1,2,3-Trichloropropane <3.8 ug/kg 02/24/23 22:55 96-18-402/24/23 20:257.5 3.8 1
1,2,4-Trimethylbenzene <4.5 ug/kg 02/24/23 22:55 95-63-602/24/23 20:257.5 4.5 1
1,3,5-Trimethylbenzene <2.5 ug/kg 02/24/23 22:55 108-67-802/24/23 20:257.5 2.5 1
Vinyl acetate <15.4 ug/kg 02/24/23 22:55 108-05-402/24/23 20:2575.0 15.4 1
Vinyl chloride <3.8 ug/kg 02/24/23 22:55 75-01-402/24/23 20:2515.0 3.8 1
Xylene (Total)<4.3 ug/kg 02/24/23 22:55 1330-20-702/24/23 20:2515.0 4.3 1
m&p-Xylene <5.1 ug/kg 02/24/23 22:55 179601-23-102/24/23 20:2515.0 5.1 1
o-Xylene <3.3 ug/kg 02/24/23 22:55 95-47-602/24/23 20:257.5 3.3 1
Surrogates
Toluene-d8 (S)100 %02/24/23 22:55 2037-26-502/24/23 20:2570-130 1
4-Bromofluorobenzene (S)108 %02/24/23 22:55 460-00-402/24/23 20:2570-130 1
1,2-Dichloroethane-d4 (S)112 %02/24/23 22:55 17060-07-002/24/23 20:2570-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.5 %02/24/23 17:07 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
869233
EPA 7471B
EPA 7471B
7471B Mercury Solids
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4585032
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Matrix:Solid
AnalyzedMDL
Mercury mg/kg <0.0083 0.019 03/02/23 15:240.0083
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4585033LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.500.47 106 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4585034MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653934001
4585035
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.608 108 80-120101 6 200.5950.035 0.69 0.64
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
869234
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4585036
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg <0.14 0.49 02/28/23 18:040.14
Barium mg/kg <0.074 0.30 02/28/23 18:040.074
Cadmium mg/kg <0.029 0.079 02/28/23 18:040.029
Chromium mg/kg <0.38 2.0 02/28/23 18:040.38
Lead mg/kg <0.092 0.49 02/28/23 18:040.092
Selenium mg/kg <0.10 0.49 02/28/23 18:040.10
Silver mg/kg <0.20 0.49 02/28/23 18:040.20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4585037LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 44.549.4 90 80-120
Barium mg/kg 43.549.4 88 80-120
Cadmium mg/kg 44.449.4 90 80-120
Chromium mg/kg 45.849.4 93 80-120
Lead mg/kg 45.749.4 93 80-120
Selenium mg/kg 46.849.4 95 80-120
Silver mg/kg 22.424.7 91 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4585038MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92653934001
4585039
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 63.6 87 75-12589 3 2064.32.4 57.7 59.6
Barium mg/kg 63.6 121 75-12598 15 2064.323.9 101 86.9
Cadmium mg/kg 63.6 91 75-12594 4 2064.3<0.038 57.8 60.1
Chromium mg/kg 63.6 84 75-12586 2 2064.344.2 97.6 99.7
Lead mg/kg 63.6 93 75-12597 4 2064.311.5 70.5 73.6
Selenium mg/kg 63.6 91 75-12593 4 2064.30.69 58.5 60.7
Silver mg/kg 31.8 90 75-12593 5 2032.2<0.26 28.6 30.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758074
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653934008, 92653934009, 92653934010, 92653934011, 92653934012, 92653934013, 92653934014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3937977
Associated Lab Samples:92653934008, 92653934009, 92653934010, 92653934011, 92653934012, 92653934013, 92653934014
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg <1.9 5.0 02/24/23 16:041.9
1,1,1-Trichloroethane ug/kg <2.6 5.0 02/24/23 16:042.6
1,1,2,2-Tetrachloroethane ug/kg <1.3 5.0 02/24/23 16:041.3
1,1,2-Trichloroethane ug/kg <1.7 5.0 02/24/23 16:041.7
1,1-Dichloroethane ug/kg <2.1 5.0 02/24/23 16:042.1
1,1-Dichloroethene ug/kg <2.1 5.0 02/24/23 16:042.1
1,1-Dichloropropene ug/kg <2.4 5.0 02/24/23 16:042.4
1,2,3-Trichlorobenzene ug/kg <4.0 5.0 02/24/23 16:044.0
1,2,3-Trichloropropane ug/kg <2.5 5.0 02/24/23 16:042.5
1,2,4-Trichlorobenzene ug/kg <4.2 5.0 02/24/23 16:044.2
1,2,4-Trimethylbenzene ug/kg <3.0 5.0 02/24/23 16:043.0
1,2-Dibromo-3-chloropropane ug/kg <1.9 5.0 02/24/23 16:041.9
1,2-Dibromoethane (EDB)ug/kg <2.2 5.0 02/24/23 16:042.2
1,2-Dichlorobenzene ug/kg <1.8 5.0 02/24/23 16:041.8
1,2-Dichloroethane ug/kg <3.3 5.0 02/24/23 16:043.3
1,2-Dichloropropane ug/kg <1.5 5.0 02/24/23 16:041.5
1,3,5-Trimethylbenzene ug/kg <1.7 5.0 02/24/23 16:041.7
1,3-Dichlorobenzene ug/kg <1.6 5.0 02/24/23 16:041.6
1,3-Dichloropropane ug/kg <1.6 5.0 02/24/23 16:041.6
1,4-Dichlorobenzene ug/kg <1.3 5.0 02/24/23 16:041.3
2,2-Dichloropropane ug/kg <3.8 5.0 v202/24/23 16:043.8
2-Butanone (MEK)ug/kg <24.0 100 02/24/23 16:0424.0
2-Chlorotoluene ug/kg <1.8 5.0 02/24/23 16:041.8
2-Hexanone ug/kg <4.8 50.0 02/24/23 16:044.8
4-Chlorotoluene ug/kg <2.8 5.0 02/24/23 16:042.8
4-Methyl-2-pentanone (MIBK)ug/kg <4.8 50.0 02/24/23 16:044.8
Acetone ug/kg <32.1 100 02/24/23 16:0432.1
Benzene ug/kg <2.0 5.0 02/24/23 16:042.0
Bromobenzene ug/kg <1.6 5.0 02/24/23 16:041.6
Bromochloromethane ug/kg <1.5 5.0 02/24/23 16:041.5
Bromodichloromethane ug/kg <1.9 5.0 02/24/23 16:041.9
Bromoform ug/kg <1.8 5.0 02/24/23 16:041.8
Bromomethane ug/kg <15.5 20.0 02/24/23 16:0415.5
Carbon tetrachloride ug/kg <1.9 5.0 IK02/24/23 16:041.9
Chlorobenzene ug/kg <2.9 5.0 02/24/23 16:042.9
Chloroethane ug/kg <3.9 10.0 02/24/23 16:043.9
Chloroform ug/kg <4.2 5.0 02/24/23 16:044.2
Chloromethane ug/kg <4.2 10.0 02/24/23 16:044.2
cis-1,2-Dichloroethene ug/kg <1.7 5.0 02/24/23 16:041.7
cis-1,3-Dichloropropene ug/kg <1.4 5.0 02/24/23 16:041.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3937977
Associated Lab Samples:92653934008, 92653934009, 92653934010, 92653934011, 92653934012, 92653934013, 92653934014
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg <2.8 5.0 IK02/24/23 16:042.8
Dibromomethane ug/kg <1.1 5.0 02/24/23 16:041.1
Dichlorodifluoromethane ug/kg <5.1 10.0 02/24/23 16:045.1
Diisopropyl ether ug/kg <1.4 5.0 02/24/23 16:041.4
Ethylbenzene ug/kg <2.3 5.0 02/24/23 16:042.3
Hexachloro-1,3-butadiene ug/kg <8.2 10.0 02/24/23 16:048.2
Isopropylbenzene (Cumene)ug/kg <1.7 5.0 02/24/23 16:041.7
m&p-Xylene ug/kg <3.4 10.0 02/24/23 16:043.4
Methyl-tert-butyl ether ug/kg <1.9 5.0 02/24/23 16:041.9
Methylene Chloride ug/kg <13.7 20.0 02/24/23 16:0413.7
n-Butylbenzene ug/kg <3.2 5.0 02/24/23 16:043.2
n-Propylbenzene ug/kg <1.8 5.0 02/24/23 16:041.8
Naphthalene ug/kg <2.6 5.0 02/24/23 16:042.6
o-Xylene ug/kg <2.2 5.0 02/24/23 16:042.2
p-Isopropyltoluene ug/kg <2.5 5.0 02/24/23 16:042.5
sec-Butylbenzene ug/kg <2.2 5.0 02/24/23 16:042.2
Styrene ug/kg <1.3 5.0 IK02/24/23 16:041.3
tert-Butylbenzene ug/kg <1.8 5.0 02/24/23 16:041.8
Tetrachloroethene ug/kg <1.6 5.0 02/24/23 16:041.6
Toluene ug/kg <3.4 5.0 02/24/23 16:043.4
trans-1,2-Dichloroethene ug/kg <4.2 5.0 02/24/23 16:044.2
trans-1,3-Dichloropropene ug/kg <1.7 5.0 02/24/23 16:041.7
Trichloroethene ug/kg <4.0 5.0 02/24/23 16:044.0
Trichlorofluoromethane ug/kg <2.8 5.0 02/24/23 16:042.8
Vinyl acetate ug/kg <10.3 50.0 02/24/23 16:0410.3
Vinyl chloride ug/kg <2.5 10.0 02/24/23 16:042.5
Xylene (Total)ug/kg <2.8 10.0 02/24/23 16:042.8
1,2-Dichloroethane-d4 (S)%105 70-130 02/24/23 16:04
4-Bromofluorobenzene (S)%98 70-130 02/24/23 16:04
Toluene-d8 (S)%99 70-130 02/24/23 16:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3937978LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 455500 91 70-130
1,1,1-Trichloroethane ug/kg 475500 95 70-130
1,1,2,2-Tetrachloroethane ug/kg 511500 102 70-130
1,1,2-Trichloroethane ug/kg 447500 89 70-130
1,1-Dichloroethane ug/kg 486500 97 70-130
1,1-Dichloroethene ug/kg 490500 98 70-130
1,1-Dichloropropene ug/kg 534500 107 70-130
1,2,3-Trichlorobenzene ug/kg 521500 104 70-130
1,2,3-Trichloropropane ug/kg 503500 101 70-130
1,2,4-Trichlorobenzene ug/kg 500500 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3937978LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 490500 98 70-130
1,2-Dibromo-3-chloropropane ug/kg 453500 91 67-130
1,2-Dibromoethane (EDB)ug/kg 520500 104 70-130
1,2-Dichlorobenzene ug/kg 500500 100 70-130
1,2-Dichloroethane ug/kg 475500 95 70-130
1,2-Dichloropropane ug/kg 463500 93 70-130
1,3,5-Trimethylbenzene ug/kg 499500 100 70-130
1,3-Dichlorobenzene ug/kg 482500 96 70-130
1,3-Dichloropropane ug/kg 511500 102 70-130
1,4-Dichlorobenzene ug/kg 461500 92 70-130
2,2-Dichloropropane ug/kg 377 v35007567-130
2-Butanone (MEK)ug/kg 10301000 103 66-130
2-Chlorotoluene ug/kg 486500 97 70-130
2-Hexanone ug/kg 10101000 101 70-130
4-Chlorotoluene ug/kg 490500 98 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 9731000 97 70-130
Acetone ug/kg 10501000 105 67-130
Benzene ug/kg 463500 93 70-130
Bromobenzene ug/kg 484500 97 70-130
Bromochloromethane ug/kg 507500 101 70-130
Bromodichloromethane ug/kg 478500 96 70-130
Bromoform ug/kg 487500 97 70-130
Bromomethane ug/kg 492500 98 53-175
Carbon tetrachloride ug/kg 447 IK5008970-130
Chlorobenzene ug/kg 473500 95 70-130
Chloroethane ug/kg 449500 90 70-135
Chloroform ug/kg 450500 90 70-130
Chloromethane ug/kg 492500 98 64-130
cis-1,2-Dichloroethene ug/kg 508500 102 70-130
cis-1,3-Dichloropropene ug/kg 474500 95 70-130
Dibromochloromethane ug/kg 466 IK5009370-130
Dibromomethane ug/kg 478500 96 70-130
Dichlorodifluoromethane ug/kg 568500 114 63-145
Diisopropyl ether ug/kg 486500 97 68-130
Ethylbenzene ug/kg 462500 92 70-130
Hexachloro-1,3-butadiene ug/kg 482500 96 70-130
Isopropylbenzene (Cumene)ug/kg 509500 102 70-130
m&p-Xylene ug/kg 9431000 94 70-130
Methyl-tert-butyl ether ug/kg 472500 94 70-130
Methylene Chloride ug/kg 526500 105 67-130
n-Butylbenzene ug/kg 477500 95 70-130
n-Propylbenzene ug/kg 469500 94 70-130
Naphthalene ug/kg 540500 108 70-130
o-Xylene ug/kg 494500 99 70-130
p-Isopropyltoluene ug/kg 502500 100 70-130
sec-Butylbenzene ug/kg 484500 97 70-130
Styrene ug/kg 514 IK50010370-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3937978LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 504500 101 64-130
Tetrachloroethene ug/kg 490500 98 70-130
Toluene ug/kg 453500 91 70-130
trans-1,2-Dichloroethene ug/kg 478500 96 70-130
trans-1,3-Dichloropropene ug/kg 470500 94 70-130
Trichloroethene ug/kg 476500 95 70-130
Trichlorofluoromethane ug/kg 516500 103 70-130
Vinyl acetate ug/kg 10601000 106 70-134
Vinyl chloride ug/kg 439500 88 68-130
Xylene (Total)ug/kg 14401500 96 70-130
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%105 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3937979MATRIX SPIKE SAMPLE:
MSSpike
Result
92653934008
1,1,1,2-Tetrachloroethane ug/kg 835779 107 58-140<3.0
1,1,1-Trichloroethane ug/kg 1030779 133 58-144<4.1
1,1,2,2-Tetrachloroethane ug/kg 1010779 130 52-139<2.1
1,1,2-Trichloroethane ug/kg 943779 121 56-140<2.6
1,1-Dichloroethane ug/kg 1050779 135 58-145<3.2
1,1-Dichloroethene ug/kg 1080779 138 57-158<3.2
1,1-Dichloropropene ug/kg 1150779 147 58-151<3.7
1,2,3-Trichlorobenzene ug/kg 314 M17794048-149<6.3
1,2,3-Trichloropropane ug/kg 928779 119 54-132<3.9
1,2,4-Trichlorobenzene ug/kg 643779 83 51-151<6.5
1,2,4-Trimethylbenzene ug/kg 872779 112 38-170<4.6
1,2-Dibromo-3-chloropropane ug/kg 714779 92 44-134<3.0
1,2-Dibromoethane (EDB)ug/kg 949779 122 60-138<3.4
1,2-Dichlorobenzene ug/kg 915779 117 59-147<2.8
1,2-Dichloroethane ug/kg 999779 128 57-139<5.2
1,2-Dichloropropane ug/kg 967779 124 62-145<2.3
1,3,5-Trimethylbenzene ug/kg 902779 116 47-159<2.6
1,3-Dichlorobenzene ug/kg 862779 111 58-144<2.4
1,3-Dichloropropane ug/kg 961779 123 60-142<2.4
1,4-Dichlorobenzene ug/kg 832779 107 57-143<2.0
2,2-Dichloropropane ug/kg 960 v377912337-144<5.9
2-Butanone (MEK)ug/kg 17401560 112 28-146<37.4
2-Chlorotoluene ug/kg 892779 114 55-158<2.8
2-Hexanone ug/kg 15601560 100 44-141<7.5
4-Chlorotoluene ug/kg 884779 113 55-146<4.3
4-Methyl-2-pentanone (MIBK)ug/kg 18101560 116 50-138<7.5
Acetone ug/kg 16201560 104 20-136<50.1
Benzene ug/kg 975779 125 60-145<3.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3937979MATRIX SPIKE SAMPLE:
MSSpike
Result
92653934008
Bromobenzene ug/kg 870779 112 59-145<2.5
Bromochloromethane ug/kg 1080779 138 57-143<2.3
Bromodichloromethane ug/kg 971779 125 53-133<3.0
Bromoform ug/kg 899779 115 48-133<2.7
Bromomethane ug/kg 575779 74 10-167<24.2
Carbon tetrachloride ug/kg 705 IK7799057-147<2.9
Chlorobenzene ug/kg 899779 115 61-144<4.5
Chloroethane ug/kg 536779 69 10-153<6.0
Chloroform ug/kg 1030779 132 58-141<6.5
Chloromethane ug/kg 1090779 140 54-165<6.5
cis-1,2-Dichloroethene ug/kg 1130 M177914559-144<2.7
cis-1,3-Dichloropropene ug/kg 1020779 131 56-137<2.1
Dibromochloromethane ug/kg 833 IK77910753-139<4.4
Dibromomethane ug/kg 938779 120 60-136<1.7
Dichlorodifluoromethane ug/kg 1370779 176 49-177<7.9
Diisopropyl ether ug/kg 1050779 135 53-136<2.1
Ethylbenzene ug/kg 868779 111 53-150<3.6
Hexachloro-1,3-butadiene ug/kg 933779 120 42-186<12.8
Isopropylbenzene (Cumene)ug/kg 965779 124 62-154<2.7
m&p-Xylene ug/kg 17601560 113 49-156<5.3
Methyl-tert-butyl ether ug/kg 1040779 133 54-133<2.9
Methylene Chloride ug/kg 1070779 137 50-153<21.4
n-Butylbenzene ug/kg 893779 115 44-174<4.9
n-Propylbenzene ug/kg 823779 106 52-157<2.8
Naphthalene ug/kg 397779 51 37-150<4.1
o-Xylene ug/kg 941779 121 54-150<3.4
p-Isopropyltoluene ug/kg 902779 116 50-164<3.8
sec-Butylbenzene ug/kg 895779 115 58-161<3.4
Styrene ug/kg 999 IK77912860-148<2.1
tert-Butylbenzene ug/kg 878779 113 44-151<2.8
Tetrachloroethene ug/kg 833779 107 53-151<2.5
Toluene ug/kg 934779 120 52-148<5.4
trans-1,2-Dichloroethene ug/kg 1070779 137 60-148<6.6
trans-1,3-Dichloropropene ug/kg 945779 121 55-133<2.7
Trichloroethene ug/kg 928779 119 60-148<6.3
Trichlorofluoromethane ug/kg 901779 116 10-154<4.3
Vinyl acetate ug/kg 20101560 129 50-149<16.0
Vinyl chloride ug/kg 815779 105 57-157<4.0
Xylene (Total)ug/kg 27002340 115 52-153<4.4
1,2-Dichloroethane-d4 (S)%112 70-130
4-Bromofluorobenzene (S)%109 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
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Page 48 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653934010
3937980SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg <2.9 30<2.9
1,1,1-Trichloroethane ug/kg <4.0 30<4.0
1,1,2,2-Tetrachloroethane ug/kg <2.0 30<2.0
1,1,2-Trichloroethane ug/kg <2.5 30<2.5
1,1-Dichloroethane ug/kg <3.1 30<3.1
1,1-Dichloroethene ug/kg <3.1 30<3.1
1,1-Dichloropropene ug/kg <3.7 30<3.7
1,2,3-Trichlorobenzene ug/kg <6.2 30<6.2
1,2,3-Trichloropropane ug/kg <3.9 30<3.9
1,2,4-Trichlorobenzene ug/kg <6.4 30<6.4
1,2,4-Trimethylbenzene ug/kg <4.5 30<4.5
1,2-Dibromo-3-chloropropane ug/kg <3.0 30<3.0
1,2-Dibromoethane (EDB)ug/kg <3.4 30<3.4
1,2-Dichlorobenzene ug/kg <2.8 30<2.8
1,2-Dichloroethane ug/kg <5.1 30<5.1
1,2-Dichloropropane ug/kg <2.3 30<2.3
1,3,5-Trimethylbenzene ug/kg <2.6 30<2.6
1,3-Dichlorobenzene ug/kg <2.4 30<2.4
1,3-Dichloropropane ug/kg <2.4 30<2.4
1,4-Dichlorobenzene ug/kg <2.0 30<2.0
2,2-Dichloropropane ug/kg <5.8 v230<5.8
2-Butanone (MEK)ug/kg <36.7 30<36.7
2-Chlorotoluene ug/kg <2.7 30<2.7
2-Hexanone ug/kg <7.4 30<7.4
4-Chlorotoluene ug/kg <4.2 30<4.2
4-Methyl-2-pentanone (MIBK)ug/kg <7.4 30<7.4
Acetone ug/kg <49.1 30<49.1
Benzene ug/kg <3.0 30<3.0
Bromobenzene ug/kg <2.5 30<2.5
Bromochloromethane ug/kg <2.3 30<2.3
Bromodichloromethane ug/kg <2.9 30<2.9
Bromoform ug/kg <2.7 30<2.7
Bromomethane ug/kg <23.7 30<23.7
Carbon tetrachloride ug/kg <2.9 IK30<2.9
Chlorobenzene ug/kg <4.4 30<4.4
Chloroethane ug/kg <5.9 30<5.9
Chloroform ug/kg <6.4 30<6.4
Chloromethane ug/kg <6.4 30<6.4
cis-1,2-Dichloroethene ug/kg <2.6 30<2.6
cis-1,3-Dichloropropene ug/kg <2.1 30<2.1
Dibromochloromethane ug/kg <4.3 IK30<4.3
Dibromomethane ug/kg <1.6 30<1.6
Dichlorodifluoromethane ug/kg <7.8 30<7.8
Diisopropyl ether ug/kg <2.1 30<2.1
Ethylbenzene ug/kg <3.6 30<3.6
Hexachloro-1,3-butadiene ug/kg <12.5 30<12.5
Isopropylbenzene (Cumene)ug/kg <2.6 30<2.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653934010
3937980SAMPLE DUPLICATE:
m&p-Xylene ug/kg <5.2 30<5.2
Methyl-tert-butyl ether ug/kg <2.9 30<2.9
Methylene Chloride ug/kg <20.9 30<20.9
n-Butylbenzene ug/kg <4.8 30<4.8
n-Propylbenzene ug/kg <2.7 30<2.7
Naphthalene ug/kg <4.0 30<4.0
o-Xylene ug/kg <3.4 30<3.4
p-Isopropyltoluene ug/kg <3.8 30<3.8
sec-Butylbenzene ug/kg <3.4 30<3.4
Styrene ug/kg <2.0 IK30<2.0
tert-Butylbenzene ug/kg <2.7 30<2.7
Tetrachloroethene ug/kg <2.4 30<2.4
Toluene ug/kg <5.3 30<5.3
trans-1,2-Dichloroethene ug/kg <6.5 30<6.5
trans-1,3-Dichloropropene ug/kg <2.6 30<2.6
Trichloroethene ug/kg <6.2 30<6.2
Trichlorofluoromethane ug/kg <4.2 30<4.2
Vinyl acetate ug/kg <15.7 30<15.7
Vinyl chloride ug/kg <3.9 30<3.9
Xylene (Total)ug/kg <4.4 30<4.4
1,2-Dichloroethane-d4 (S)%113111
4-Bromofluorobenzene (S)%108106
Toluene-d8 (S)%103101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758553
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3940128
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg <131 332 03/01/23 10:18131
1,2-Dichlorobenzene ug/kg <120 332 03/01/23 10:18120
1,3-Dichlorobenzene ug/kg <118 332 03/01/23 10:18118
1,4-Dichlorobenzene ug/kg <127 332 03/01/23 10:18127
1-Methylnaphthalene ug/kg <117 332 03/01/23 10:18117
2,2'-Oxybis(1-chloropropane)ug/kg <158 332 03/01/23 10:18158
2,4,5-Trichlorophenol ug/kg <152 332 03/01/23 10:18152
2,4,6-Trichlorophenol ug/kg <137 332 03/01/23 10:18137
2,4-Dichlorophenol ug/kg <130 332 03/01/23 10:18130
2,4-Dimethylphenol ug/kg <138 332 03/01/23 10:18138
2,4-Dinitrophenol ug/kg <1030 1660 03/01/23 10:181030
2,4-Dinitrotoluene ug/kg <128 332 03/01/23 10:18128
2,6-Dinitrotoluene ug/kg <122 332 03/01/23 10:18122
2-Chloronaphthalene ug/kg <132 332 03/01/23 10:18132
2-Chlorophenol ug/kg <125 332 03/01/23 10:18125
2-Methylnaphthalene ug/kg <133 332 03/01/23 10:18133
2-Methylphenol(o-Cresol)ug/kg <136 332 03/01/23 10:18136
2-Nitroaniline ug/kg <272 1660 03/01/23 10:18272
2-Nitrophenol ug/kg <144 332 03/01/23 10:18144
3&4-Methylphenol(m&p Cresol)ug/kg <134 332 03/01/23 10:18134
3,3'-Dichlorobenzidine ug/kg <224 664 03/01/23 10:18224
3-Nitroaniline ug/kg <261 1660 03/01/23 10:18261
4,6-Dinitro-2-methylphenol ug/kg <310 664 03/01/23 10:18310
4-Bromophenylphenyl ether ug/kg <128 332 03/01/23 10:18128
4-Chloro-3-methylphenol ug/kg <234 664 03/01/23 10:18234
4-Chloroaniline ug/kg <261 664 03/01/23 10:18261
4-Chlorophenylphenyl ether ug/kg <124 332 03/01/23 10:18124
4-Nitroaniline ug/kg <253 664 03/01/23 10:18253
4-Nitrophenol ug/kg <642 1660 03/01/23 10:18642
Acenaphthene ug/kg <117 332 03/01/23 10:18117
Acenaphthylene ug/kg <117 332 03/01/23 10:18117
Aniline ug/kg <130 332 03/01/23 10:18130
Anthracene ug/kg <109 332 03/01/23 10:18109
Benzo(a)anthracene ug/kg <111 332 03/01/23 10:18111
Benzo(a)pyrene ug/kg <115 332 03/01/23 10:18115
Benzo(b)fluoranthene ug/kg <111 332 03/01/23 10:18111
Benzo(g,h,i)perylene ug/kg <129 332 03/01/23 10:18129
Benzo(k)fluoranthene ug/kg <117 332 03/01/23 10:18117
Benzoic Acid ug/kg <714 1660 03/01/23 10:18714
Benzyl alcohol ug/kg <252 664 03/01/23 10:18252
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3940128
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg <138 332 03/01/23 10:18138
bis(2-Chloroethyl) ether ug/kg <125 332 03/01/23 10:18125
bis(2-Ethylhexyl)phthalate ug/kg <129 332 03/01/23 10:18129
Butylbenzylphthalate ug/kg <140 332 03/01/23 10:18140
Chrysene ug/kg <121 332 03/01/23 10:18121
Di-n-butylphthalate ug/kg <112 332 03/01/23 10:18112
Di-n-octylphthalate ug/kg <131 332 03/01/23 10:18131
Dibenz(a,h)anthracene ug/kg <128 332 03/01/23 10:18128
Dibenzofuran ug/kg <120 332 03/01/23 10:18120
Diethylphthalate ug/kg <122 332 03/01/23 10:18122
Dimethylphthalate ug/kg <121 332 03/01/23 10:18121
Fluoranthene ug/kg <114 332 03/01/23 10:18114
Fluorene ug/kg <117 332 03/01/23 10:18117
Hexachloro-1,3-butadiene ug/kg <144 332 03/01/23 10:18144
Hexachlorobenzene ug/kg <130 332 03/01/23 10:18130
Hexachlorocyclopentadiene ug/kg <190 332 03/01/23 10:18190
Hexachloroethane ug/kg <127 332 03/01/23 10:18127
Indeno(1,2,3-cd)pyrene ug/kg <131 332 03/01/23 10:18131
Isophorone ug/kg <148 332 03/01/23 10:18148
N-Nitroso-di-n-propylamine ug/kg <125 332 03/01/23 10:18125
N-Nitrosodimethylamine ug/kg <112 332 03/01/23 10:18112
N-Nitrosodiphenylamine ug/kg <118 332 03/01/23 10:18118
Naphthalene ug/kg <113 332 03/01/23 10:18113
Nitrobenzene ug/kg <154 332 03/01/23 10:18154
Pentachlorophenol ug/kg <325 664 03/01/23 10:18325
Phenanthrene ug/kg <109 332 03/01/23 10:18109
Phenol ug/kg <148 332 03/01/23 10:18148
Pyrene ug/kg <135 332 03/01/23 10:18135
Pyridine ug/kg <105 332 03/01/23 10:18105
2,4,6-Tribromophenol (S)%77 10-131 03/01/23 10:18
2-Fluorobiphenyl (S)%72 10-130 03/01/23 10:18
2-Fluorophenol (S)%72 10-130 03/01/23 10:18
Nitrobenzene-d5 (S)%73 10-130 03/01/23 10:18
Phenol-d6 (S)%69 10-130 03/01/23 10:18
Terphenyl-d14 (S)%66 10-130 03/01/23 10:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940129LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 533825 65 43-130
1,2-Dichlorobenzene ug/kg 583825 71 43-130
1,3-Dichlorobenzene ug/kg 548825 66 43-130
1,4-Dichlorobenzene ug/kg 562825 68 44-130
1-Methylnaphthalene ug/kg 565825 68 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940129LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 584825 71 29-130
2,4,5-Trichlorophenol ug/kg 564825 68 47-130
2,4,6-Trichlorophenol ug/kg 594825 72 47-130
2,4-Dichlorophenol ug/kg 517825 63 45-130
2,4-Dimethylphenol ug/kg 703825 85 45-130
2,4-Dinitrophenol ug/kg 27904130 68 27-140
2,4-Dinitrotoluene ug/kg 645825 78 46-130
2,6-Dinitrotoluene ug/kg 592825 72 48-130
2-Chloronaphthalene ug/kg 563825 68 46-130
2-Chlorophenol ug/kg 521825 63 43-130
2-Methylnaphthalene ug/kg 543825 66 47-130
2-Methylphenol(o-Cresol)ug/kg 568825 69 42-130
2-Nitroaniline ug/kg 1290J1650 78 41-130
2-Nitrophenol ug/kg 500825 61 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 572825 69 39-130
3,3'-Dichlorobenzidine ug/kg 11301650 69 41-130
3-Nitroaniline ug/kg 1130J1650 69 37-130
4,6-Dinitro-2-methylphenol ug/kg 12701650 77 38-141
4-Bromophenylphenyl ether ug/kg 604825 73 47-130
4-Chloro-3-methylphenol ug/kg 11101650 67 44-130
4-Chloroaniline ug/kg 10801650 66 41-130
4-Chlorophenylphenyl ether ug/kg 569825 69 45-130
4-Nitroaniline ug/kg 11601650 70 42-130
4-Nitrophenol ug/kg 28004130 68 39-131
Acenaphthene ug/kg 592825 72 49-130
Acenaphthylene ug/kg 585825 71 50-130
Aniline ug/kg 486825 59 38-130
Anthracene ug/kg 564825 68 49-130
Benzo(a)anthracene ug/kg 614825 74 51-130
Benzo(a)pyrene ug/kg 603825 73 51-130
Benzo(b)fluoranthene ug/kg 571825 69 49-130
Benzo(g,h,i)perylene ug/kg 696825 84 48-140
Benzo(k)fluoranthene ug/kg 580825 70 51-130
Benzoic Acid ug/kg 23404130 57 22-130
Benzyl alcohol ug/kg 11201650 68 43-130
bis(2-Chloroethoxy)methane ug/kg 530825 64 43-130
bis(2-Chloroethyl) ether ug/kg 542825 66 42-130
bis(2-Ethylhexyl)phthalate ug/kg 571825 69 43-130
Butylbenzylphthalate ug/kg 540825 66 44-131
Chrysene ug/kg 616825 75 51-130
Di-n-butylphthalate ug/kg 603825 73 46-130
Di-n-octylphthalate ug/kg 613825 74 45-130
Dibenz(a,h)anthracene ug/kg 656825 79 48-130
Dibenzofuran ug/kg 617825 75 10-130
Diethylphthalate ug/kg 588825 71 48-130
Dimethylphthalate ug/kg 589825 71 48-130
Fluoranthene ug/kg 612825 74 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3940129LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 593825 72 48-130
Hexachloro-1,3-butadiene ug/kg 525825 64 39-130
Hexachlorobenzene ug/kg 586825 71 47-130
Hexachlorocyclopentadiene ug/kg 360825 44 17-130
Hexachloroethane ug/kg 549825 67 40-130
Indeno(1,2,3-cd)pyrene ug/kg 706825 86 50-130
Isophorone ug/kg 554825 67 41-130
N-Nitroso-di-n-propylamine ug/kg 593825 72 36-130
N-Nitrosodimethylamine ug/kg 524825 63 34-130
N-Nitrosodiphenylamine ug/kg 625825 76 48-130
Naphthalene ug/kg 551825 67 46-130
Nitrobenzene ug/kg 541825 66 39-130
Pentachlorophenol ug/kg 10801650 65 42-130
Phenanthrene ug/kg 624825 76 50-130
Phenol ug/kg 550825 67 42-130
Pyrene ug/kg 554825 67 50-130
Pyridine ug/kg 476825 58 26-130
2,4,6-Tribromophenol (S)%73 10-131
2-Fluorobiphenyl (S)%63 10-130
2-Fluorophenol (S)%61 10-130
Nitrobenzene-d5 (S)%60 10-130
Phenol-d6 (S)%64 10-130
Terphenyl-d14 (S)%60 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3940130MATRIX SPIKE SAMPLE:
MSSpike
Result
92653946008
1,2,4-Trichlorobenzene ug/kg 5841640 36 16-130ND
1,2-Dichlorobenzene ug/kg 5921640 36 19-130ND
1,3-Dichlorobenzene ug/kg 5561640 34 19-130ND
1,4-Dichlorobenzene ug/kg 5681640 35 20-130ND
1-Methylnaphthalene ug/kg 6271640 38 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 6131640 37 10-130ND
2,4,5-Trichlorophenol ug/kg 6401640 39 19-130ND
2,4,6-Trichlorophenol ug/kg 6271640 38 18-130ND
2,4-Dichlorophenol ug/kg 5931640 36 16-130ND
2,4-Dimethylphenol ug/kg 8251640 50 10-130ND
2,4-Dinitrophenol ug/kg 29508220 36 10-143ND
2,4-Dinitrotoluene ug/kg 6781640 41 19-130ND
2,6-Dinitrotoluene ug/kg 6771640 41 22-130ND
2-Chloronaphthalene ug/kg 6541640 40 18-130ND
2-Chlorophenol ug/kg 5601640 34 20-130ND
2-Methylnaphthalene ug/kg 6071640 37 18-130ND
2-Methylphenol(o-Cresol)ug/kg 5971640 36 13-130ND
2-Nitroaniline ug/kg 1370J3290 42 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3940130MATRIX SPIKE SAMPLE:
MSSpike
Result
92653946008
2-Nitrophenol ug/kg 5731640 35 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 6081640 37 13-130ND
3,3'-Dichlorobenzidine ug/kg 12703290 39 10-130ND
3-Nitroaniline ug/kg 1270J3290 39 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 13003290 40 10-144ND
4-Bromophenylphenyl ether ug/kg 6321640 38 18-130ND
4-Chloro-3-methylphenol ug/kg 12803290 39 16-130ND
4-Chloroaniline ug/kg 11903290 36 17-130ND
4-Chlorophenylphenyl ether ug/kg 6021640 37 17-130ND
4-Nitroaniline ug/kg 12103290 37 21-130ND
4-Nitrophenol ug/kg 31308220 38 13-131ND
Acenaphthene ug/kg 6521640 40 20-130ND
Acenaphthylene ug/kg 6501640 40 21-130ND
Aniline ug/kg 5421640 33 10-130ND
Anthracene ug/kg 6311640 38 19-130ND
Benzo(a)anthracene ug/kg 6821640 41 17-130ND
Benzo(a)pyrene ug/kg 6351640 39 14-130ND
Benzo(b)fluoranthene ug/kg 6431640 39 11-134ND
Benzo(g,h,i)perylene ug/kg 7281640 44 12-130ND
Benzo(k)fluoranthene ug/kg 6411640 39 15-130ND
Benzoic Acid ug/kg 30508220 37 10-130ND
Benzyl alcohol ug/kg 11703290 36 20-130ND
bis(2-Chloroethoxy)methane ug/kg 5831640 35 16-130ND
bis(2-Chloroethyl) ether ug/kg 5451640 33 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 6081640 37 11-130ND
Butylbenzylphthalate ug/kg 5661640 34 10-130ND
Chrysene ug/kg 6791640 41 17-130ND
Di-n-butylphthalate ug/kg 6671640 41 16-130ND
Di-n-octylphthalate ug/kg 6731640 41 16-130ND
Dibenz(a,h)anthracene ug/kg 6641640 40 13-130ND
Dibenzofuran ug/kg 6701640 41 19-130ND
Diethylphthalate ug/kg 6401640 39 22-130ND
Dimethylphthalate ug/kg 6451640 39 23-130ND
Fluoranthene ug/kg 6951640 42 14-130ND
Fluorene ug/kg 6411640 39 19-130ND
Hexachloro-1,3-butadiene ug/kg 5621640 34 12-130ND
Hexachlorobenzene ug/kg 6621640 40 17-130ND
Hexachlorocyclopentadiene ug/kg 3671640 22 10-130ND
Hexachloroethane ug/kg 5791640 35 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 7331640 45 13-130ND
Isophorone ug/kg 6241640 38 17-130ND
N-Nitroso-di-n-propylamine ug/kg 6201640 38 10-130ND
N-Nitrosodimethylamine ug/kg 5371640 33 16-130ND
N-Nitrosodiphenylamine ug/kg 6681640 41 19-130ND
Naphthalene ug/kg 6251640 38 18-130ND
Nitrobenzene ug/kg 5831640 35 15-130ND
Pentachlorophenol ug/kg 12403290 38 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3940130MATRIX SPIKE SAMPLE:
MSSpike
Result
92653946008
Phenanthrene ug/kg 6861640 42 17-130ND
Phenol ug/kg 5841640 36 15-130ND
Pyrene ug/kg 5701640 35 31-130ND
Pyridine ug/kg 5021640 31 10-130ND
2,4,6-Tribromophenol (S)%79 10-131
2-Fluorobiphenyl (S)%69 10-130
2-Fluorophenol (S)%63 10-130
Nitrobenzene-d5 (S)%69 10-130
Phenol-d6 (S)%68 10-130
Terphenyl-d14 (S)%61 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653946014
3940131SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg <132 30ND
1,2-Dichlorobenzene ug/kg <121 30ND
1,3-Dichlorobenzene ug/kg <119 30ND
1,4-Dichlorobenzene ug/kg <128 30ND
1-Methylnaphthalene ug/kg <118 30ND
2,2'-Oxybis(1-chloropropane)ug/kg <160 30ND
2,4,5-Trichlorophenol ug/kg <154 30ND
2,4,6-Trichlorophenol ug/kg <138 30ND
2,4-Dichlorophenol ug/kg <131 30ND
2,4-Dimethylphenol ug/kg <139 30ND
2,4-Dinitrophenol ug/kg <1040 30ND
2,4-Dinitrotoluene ug/kg <129 30ND
2,6-Dinitrotoluene ug/kg <123 30ND
2-Chloronaphthalene ug/kg <133 30ND
2-Chlorophenol ug/kg <126 30ND
2-Methylnaphthalene ug/kg <134 30ND
2-Methylphenol(o-Cresol)ug/kg <137 30ND
2-Nitroaniline ug/kg <275 30ND
2-Nitrophenol ug/kg <145 30ND
3&4-Methylphenol(m&p Cresol)ug/kg <135 30ND
3,3'-Dichlorobenzidine ug/kg <227 30ND
3-Nitroaniline ug/kg <263 30ND
4,6-Dinitro-2-methylphenol ug/kg <313 30ND
4-Bromophenylphenyl ether ug/kg <129 30ND
4-Chloro-3-methylphenol ug/kg <236 30ND
4-Chloroaniline ug/kg <263 30ND
4-Chlorophenylphenyl ether ug/kg <125 30ND
4-Nitroaniline ug/kg <255 30ND
4-Nitrophenol ug/kg <649 30ND
Acenaphthene ug/kg <118 30ND
Acenaphthylene ug/kg <118 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653946014
3940131SAMPLE DUPLICATE:
Aniline ug/kg <131 30ND
Anthracene ug/kg <110 30ND
Benzo(a)anthracene ug/kg <112 30ND
Benzo(a)pyrene ug/kg <116 30ND
Benzo(b)fluoranthene ug/kg <112 30ND
Benzo(g,h,i)perylene ug/kg <130 30ND
Benzo(k)fluoranthene ug/kg <118 30ND
Benzoic Acid ug/kg <721 30ND
Benzyl alcohol ug/kg <254 30ND
bis(2-Chloroethoxy)methane ug/kg <139 30ND
bis(2-Chloroethyl) ether ug/kg <126 30ND
bis(2-Ethylhexyl)phthalate ug/kg <130 30ND
Butylbenzylphthalate ug/kg <141 30ND
Chrysene ug/kg <122 30ND
Di-n-butylphthalate ug/kg <113 30ND
Di-n-octylphthalate ug/kg <132 30ND
Dibenz(a,h)anthracene ug/kg <129 30ND
Dibenzofuran ug/kg <121 30ND
Diethylphthalate ug/kg <123 30ND
Dimethylphthalate ug/kg <122 30ND
Fluoranthene ug/kg <115 30ND
Fluorene ug/kg <118 30ND
Hexachloro-1,3-butadiene ug/kg <145 30ND
Hexachlorobenzene ug/kg <131 30ND
Hexachlorocyclopentadiene ug/kg <192 30ND
Hexachloroethane ug/kg <128 30ND
Indeno(1,2,3-cd)pyrene ug/kg <132 30ND
Isophorone ug/kg <149 30ND
N-Nitroso-di-n-propylamine ug/kg <126 30ND
N-Nitrosodimethylamine ug/kg <113 30ND
N-Nitrosodiphenylamine ug/kg <119 30ND
Naphthalene ug/kg <114 30ND
Nitrobenzene ug/kg <156 30ND
Pentachlorophenol ug/kg <328 30ND
Phenanthrene ug/kg <110 30ND
Phenol ug/kg <149 30ND
Pyrene ug/kg <136 30ND
Pyridine ug/kg <106 30ND
2,4,6-Tribromophenol (S)%7876
2-Fluorobiphenyl (S)%7372
2-Fluorophenol (S)%7066
Nitrobenzene-d5 (S)%7269
Phenol-d6 (S)%7368
Terphenyl-d14 (S)%6566
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
759260
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653934006, 92653934007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3943934
Associated Lab Samples:92653934006, 92653934007
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg <130 329 03/06/23 08:42130
1,2-Dichlorobenzene ug/kg <119 329 03/06/23 08:42119
1,3-Dichlorobenzene ug/kg <117 329 03/06/23 08:42117
1,4-Dichlorobenzene ug/kg <126 329 03/06/23 08:42126
1-Methylnaphthalene ug/kg <116 329 03/06/23 08:42116
2,2'-Oxybis(1-chloropropane)ug/kg <156 329 03/06/23 08:42156
2,4,5-Trichlorophenol ug/kg <150 329 03/06/23 08:42150
2,4,6-Trichlorophenol ug/kg <136 329 03/06/23 08:42136
2,4-Dichlorophenol ug/kg <129 329 03/06/23 08:42129
2,4-Dimethylphenol ug/kg <137 329 03/06/23 08:42137
2,4-Dinitrophenol ug/kg <1020 1640 03/06/23 08:421020
2,4-Dinitrotoluene ug/kg <127 329 03/06/23 08:42127
2,6-Dinitrotoluene ug/kg <121 329 03/06/23 08:42121
2-Chloronaphthalene ug/kg <131 329 03/06/23 08:42131
2-Chlorophenol ug/kg <124 329 03/06/23 08:42124
2-Methylnaphthalene ug/kg <132 329 03/06/23 08:42132
2-Methylphenol(o-Cresol)ug/kg <135 329 03/06/23 08:42135
2-Nitroaniline ug/kg <269 1640 03/06/23 08:42269
2-Nitrophenol ug/kg <143 329 03/06/23 08:42143
3&4-Methylphenol(m&p Cresol)ug/kg <133 329 03/06/23 08:42133
3,3'-Dichlorobenzidine ug/kg <222 658 03/06/23 08:42222
3-Nitroaniline ug/kg <258 1640 03/06/23 08:42258
4,6-Dinitro-2-methylphenol ug/kg <307 658 03/06/23 08:42307
4-Bromophenylphenyl ether ug/kg <127 329 03/06/23 08:42127
4-Chloro-3-methylphenol ug/kg <231 658 03/06/23 08:42231
4-Chloroaniline ug/kg <258 658 03/06/23 08:42258
4-Chlorophenylphenyl ether ug/kg <123 329 03/06/23 08:42123
4-Nitroaniline ug/kg <250 658 03/06/23 08:42250
4-Nitrophenol ug/kg <636 1640 03/06/23 08:42636
Acenaphthene ug/kg <116 329 03/06/23 08:42116
Acenaphthylene ug/kg <116 329 03/06/23 08:42116
Aniline ug/kg <129 329 03/06/23 08:42129
Anthracene ug/kg <108 329 03/06/23 08:42108
Benzo(a)anthracene ug/kg <110 329 03/06/23 08:42110
Benzo(a)pyrene ug/kg <114 329 03/06/23 08:42114
Benzo(b)fluoranthene ug/kg <110 329 03/06/23 08:42110
Benzo(g,h,i)perylene ug/kg <128 329 03/06/23 08:42128
Benzo(k)fluoranthene ug/kg <116 329 03/06/23 08:42116
Benzoic Acid ug/kg <707 1640 03/06/23 08:42707
Benzyl alcohol ug/kg <249 658 03/06/23 08:42249
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3943934
Associated Lab Samples:92653934006, 92653934007
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg <137 329 03/06/23 08:42137
bis(2-Chloroethyl) ether ug/kg <124 329 03/06/23 08:42124
bis(2-Ethylhexyl)phthalate ug/kg <128 329 03/06/23 08:42128
Butylbenzylphthalate ug/kg <139 329 03/06/23 08:42139
Chrysene ug/kg <120 329 03/06/23 08:42120
Di-n-butylphthalate ug/kg <111 329 03/06/23 08:42111
Di-n-octylphthalate ug/kg <130 329 03/06/23 08:42130
Dibenz(a,h)anthracene ug/kg <127 329 03/06/23 08:42127
Dibenzofuran ug/kg <119 329 03/06/23 08:42119
Diethylphthalate ug/kg <121 329 03/06/23 08:42121
Dimethylphthalate ug/kg <120 329 03/06/23 08:42120
Fluoranthene ug/kg <113 329 03/06/23 08:42113
Fluorene ug/kg <116 329 03/06/23 08:42116
Hexachloro-1,3-butadiene ug/kg <143 329 03/06/23 08:42143
Hexachlorobenzene ug/kg <129 329 03/06/23 08:42129
Hexachlorocyclopentadiene ug/kg <188 329 v203/06/23 08:42188
Hexachloroethane ug/kg <126 329 03/06/23 08:42126
Indeno(1,2,3-cd)pyrene ug/kg <130 329 03/06/23 08:42130
Isophorone ug/kg <147 329 03/06/23 08:42147
N-Nitroso-di-n-propylamine ug/kg <124 329 03/06/23 08:42124
N-Nitrosodimethylamine ug/kg <111 329 03/06/23 08:42111
N-Nitrosodiphenylamine ug/kg <117 329 03/06/23 08:42117
Naphthalene ug/kg <112 329 03/06/23 08:42112
Nitrobenzene ug/kg <152 329 03/06/23 08:42152
Pentachlorophenol ug/kg <322 658 03/06/23 08:42322
Phenanthrene ug/kg <108 329 03/06/23 08:42108
Phenol ug/kg <147 329 03/06/23 08:42147
Pyrene ug/kg <134 329 03/06/23 08:42134
Pyridine ug/kg <104 329 03/06/23 08:42104
2,4,6-Tribromophenol (S)%60 10-131 03/06/23 08:42
2-Fluorobiphenyl (S)%58 10-130 03/06/23 08:42
2-Fluorophenol (S)%57 10-130 03/06/23 08:42
Nitrobenzene-d5 (S)%63 10-130 03/06/23 08:42
Phenol-d6 (S)%59 10-130 03/06/23 08:42
Terphenyl-d14 (S)%61 10-130 03/06/23 08:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3943935LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10301680 61 43-130
1,2-Dichlorobenzene ug/kg 9641680 57 43-130
1,3-Dichlorobenzene ug/kg 9601680 57 43-130
1,4-Dichlorobenzene ug/kg 9591680 57 44-130
1-Methylnaphthalene ug/kg 11701680 70 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3943935LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 10001680 59 29-130
2,4,5-Trichlorophenol ug/kg 12601680 75 47-130
2,4,6-Trichlorophenol ug/kg 12001680 71 47-130
2,4-Dichlorophenol ug/kg 11101680 66 45-130
2,4-Dimethylphenol ug/kg 14501680 86 45-130
2,4-Dinitrophenol ug/kg 57008420 68 27-140
2,4-Dinitrotoluene ug/kg 13601680 81 46-130
2,6-Dinitrotoluene ug/kg 14101680 84 48-130
2-Chloronaphthalene ug/kg 12101680 72 46-130
2-Chlorophenol ug/kg 9691680 58 43-130
2-Methylnaphthalene ug/kg 11601680 69 47-130
2-Methylphenol(o-Cresol)ug/kg 10601680 63 42-130
2-Nitroaniline ug/kg 24503370 73 41-130
2-Nitrophenol ug/kg 11201680 67 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 10501680 62 39-130
3,3'-Dichlorobenzidine ug/kg 24703370 74 41-130
3-Nitroaniline ug/kg 24703370 73 37-130
4,6-Dinitro-2-methylphenol ug/kg 25903370 77 38-141
4-Bromophenylphenyl ether ug/kg 12701680 76 47-130
4-Chloro-3-methylphenol ug/kg 25503370 76 44-130
4-Chloroaniline ug/kg 22203370 66 41-130
4-Chlorophenylphenyl ether ug/kg 11701680 70 45-130
4-Nitroaniline ug/kg 25603370 76 42-130
4-Nitrophenol ug/kg 58008420 69 39-131
Acenaphthene ug/kg 12101680 72 49-130
Acenaphthylene ug/kg 12301680 73 50-130
Aniline ug/kg 9021680 54 38-130
Anthracene ug/kg 11601680 69 49-130
Benzo(a)anthracene ug/kg 12801680 76 51-130
Benzo(a)pyrene ug/kg 13201680 79 51-130
Benzo(b)fluoranthene ug/kg 13101680 78 49-130
Benzo(g,h,i)perylene ug/kg 14501680 86 48-140
Benzo(k)fluoranthene ug/kg 13301680 79 51-130
Benzoic Acid ug/kg 46608420 55 22-130
Benzyl alcohol ug/kg 20803370 62 43-130
bis(2-Chloroethoxy)methane ug/kg 11401680 67 43-130
bis(2-Chloroethyl) ether ug/kg 9981680 59 42-130
bis(2-Ethylhexyl)phthalate ug/kg 12801680 76 43-130
Butylbenzylphthalate ug/kg 14001680 83 44-131
Chrysene ug/kg 12701680 75 51-130
Di-n-butylphthalate ug/kg 13101680 78 46-130
Di-n-octylphthalate ug/kg 14101680 84 45-130
Dibenz(a,h)anthracene ug/kg 14101680 83 48-130
Dibenzofuran ug/kg 12601680 75 10-130
Diethylphthalate ug/kg 13501680 80 48-130
Dimethylphthalate ug/kg 13201680 78 48-130
Fluoranthene ug/kg 12901680 77 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3943935LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 12101680 72 48-130
Hexachloro-1,3-butadiene ug/kg 10101680 60 39-130
Hexachlorobenzene ug/kg 12301680 73 47-130
Hexachlorocyclopentadiene ug/kg 704 v316804217-130
Hexachloroethane ug/kg 9561680 57 40-130
Indeno(1,2,3-cd)pyrene ug/kg 14701680 88 50-130
Isophorone ug/kg 12901680 77 41-130
N-Nitroso-di-n-propylamine ug/kg 11101680 66 36-130
N-Nitrosodimethylamine ug/kg 9181680 55 34-130
N-Nitrosodiphenylamine ug/kg 12601680 75 48-130
Naphthalene ug/kg 10601680 63 46-130
Nitrobenzene ug/kg 11501680 68 39-130
Pentachlorophenol ug/kg 21603370 64 42-130
Phenanthrene ug/kg 12901680 76 50-130
Phenol ug/kg 10901680 64 42-130
Pyrene ug/kg 13101680 78 50-130
Pyridine ug/kg 7751680 46 26-130
2,4,6-Tribromophenol (S)%79 10-131
2-Fluorobiphenyl (S)%68 10-130
2-Fluorophenol (S)%55 10-130
Nitrobenzene-d5 (S)%64 10-130
Phenol-d6 (S)%60 10-130
Terphenyl-d14 (S)%73 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92654879001
3943937SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg <156 30ND
1,2-Dichlorobenzene ug/kg <143 30ND
1,3-Dichlorobenzene ug/kg <140 30ND
1,4-Dichlorobenzene ug/kg <151 30ND
1-Methylnaphthalene ug/kg <139 30ND
2,2'-Oxybis(1-chloropropane)ug/kg <188 30ND
2,4,5-Trichlorophenol ug/kg <181 30ND
2,4,6-Trichlorophenol ug/kg <163 30ND
2,4-Dichlorophenol ug/kg <155 30ND
2,4-Dimethylphenol ug/kg <164 30ND
2,4-Dinitrophenol ug/kg <1220 30ND
2,4-Dinitrotoluene ug/kg <152 30ND
2,6-Dinitrotoluene ug/kg <145 30ND
2-Chloronaphthalene ug/kg <157 30ND
2-Chlorophenol ug/kg <149 30ND
2-Methylnaphthalene ug/kg <158 30ND
2-Methylphenol(o-Cresol)ug/kg <162 30ND
2-Nitroaniline ug/kg <324 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92654879001
3943937SAMPLE DUPLICATE:
2-Nitrophenol ug/kg <172 30ND
3&4-Methylphenol(m&p Cresol)ug/kg <160 30ND
3,3'-Dichlorobenzidine ug/kg <268 30ND
3-Nitroaniline ug/kg <311 30ND
4,6-Dinitro-2-methylphenol ug/kg <370 30ND
4-Bromophenylphenyl ether ug/kg <152 30ND
4-Chloro-3-methylphenol ug/kg <278 30ND
4-Chloroaniline ug/kg <311 30ND
4-Chlorophenylphenyl ether ug/kg <148 30ND
4-Nitroaniline ug/kg <301 30ND
4-Nitrophenol ug/kg <766 30ND
Acenaphthene ug/kg <139 30ND
Acenaphthylene ug/kg <139 30ND
Aniline ug/kg <155 30ND
Anthracene ug/kg <130 30ND
Benzo(a)anthracene ug/kg <132 30ND
Benzo(a)pyrene ug/kg <137 30ND
Benzo(b)fluoranthene ug/kg <132 30ND
Benzo(g,h,i)perylene ug/kg <154 30ND
Benzo(k)fluoranthene ug/kg <139 30ND
Benzoic Acid ug/kg <851 30ND
Benzyl alcohol ug/kg <300 30ND
bis(2-Chloroethoxy)methane ug/kg <164 30ND
bis(2-Chloroethyl) ether ug/kg <149 30ND
bis(2-Ethylhexyl)phthalate ug/kg <154 30ND
Butylbenzylphthalate ug/kg <167 30ND
Chrysene ug/kg <144 30ND
Di-n-butylphthalate ug/kg <133 30ND
Di-n-octylphthalate ug/kg <156 30ND
Dibenz(a,h)anthracene ug/kg <152 30ND
Dibenzofuran ug/kg <143 30ND
Diethylphthalate ug/kg <145 30ND
Dimethylphthalate ug/kg <144 30ND
Fluoranthene ug/kg <136 30ND
Fluorene ug/kg <139 30ND
Hexachloro-1,3-butadiene ug/kg <172 30ND
Hexachlorobenzene ug/kg <155 30ND
Hexachlorocyclopentadiene ug/kg <227 v230ND
Hexachloroethane ug/kg <151 30ND
Indeno(1,2,3-cd)pyrene ug/kg <156 30ND
Isophorone ug/kg <176 30ND
N-Nitroso-di-n-propylamine ug/kg <149 30ND
N-Nitrosodimethylamine ug/kg <133 30ND
N-Nitrosodiphenylamine ug/kg <140 30ND
Naphthalene ug/kg <134 30ND
Nitrobenzene ug/kg <184 30ND
Pentachlorophenol ug/kg <388 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92654879001
3943937SAMPLE DUPLICATE:
Phenanthrene ug/kg <130 30ND
Phenol ug/kg <176 30ND
Pyrene ug/kg <161 30ND
Pyridine ug/kg <125 30ND
2,4,6-Tribromophenol (S)%7373
2-Fluorobiphenyl (S)%6263
2-Fluorophenol (S)%5154
Nitrobenzene-d5 (S)%6468
Phenol-d6 (S)%5557
Terphenyl-d14 (S)%6265
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758075
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653934008
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653762001
3937981SAMPLE DUPLICATE:
Percent Moisture %12.7 D6,N226259.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653963003
3937982SAMPLE DUPLICATE:
Percent Moisture %15.6 N262514.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
758079
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007,
92653934009, 92653934010, 92653934011, 92653934012, 92653934013, 92653934014
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653934001
3938038SAMPLE DUPLICATE:
Percent Moisture %22.2 N222522.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653967001
3938041SAMPLE DUPLICATE:
Percent Moisture %19.9 N242519.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2013298
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3895478-1
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 02/27/23 13:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3895478-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653934006
R3895478-3SAMPLE DUPLICATE:
Total Solids %75.2 0.339 1075.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 75
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92653934
LEN-008
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2013835
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3895939-1
Associated Lab Samples:92653934001, 92653934002, 92653934003, 92653934004, 92653934005, 92653934006, 92653934007
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg <0.255 1.00 02/28/23 12:100.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3895939-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 11.410.0 114 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3895939-3MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1589348-08
R3895939-4
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg ML,R120.0 40.7 75.0-12559.6 37.7 2020.0ND 8.14 11.9
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3895939-5MATRIX SPIKE SAMPLE:
MSSpike
Result
L1589348-08
Chromium, Hexavalent mg/kg 753656 115 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92653934002
R3895939-7SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg 0.366J D8,J20020ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1589539-06
R3895939-8SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg <0.255 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 75
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92653934
LEN-008
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The sample and duplicate results for this parameter are less than 5 times the reporting limit, the RPD may not be
statistically valid.D8
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 75
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92653934
LEN-008
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92653934001 869234 869341FG-1 (0-2)EPA 3050B EPA 6020B
92653934002 869234 869341FG-2 (0-2)EPA 3050B EPA 6020B
92653934003 869234 869341FG-3 (0-2)EPA 3050B EPA 6020B
92653934004 869234 869341FG-8 (0-2)EPA 3050B EPA 6020B
92653934005 869234 869341FG-9 (0-2)EPA 3050B EPA 6020B
92653934006 869234 869341FG-10 (0-2)EPA 3050B EPA 6020B
92653934007 869234 869341FG-DUP (0-2)EPA 3050B EPA 6020B
92653934001 869233 869360FG-1 (0-2)EPA 7471B EPA 7471B
92653934002 869233 869360FG-2 (0-2)EPA 7471B EPA 7471B
92653934003 869233 869360FG-3 (0-2)EPA 7471B EPA 7471B
92653934004 869233 869360FG-8 (0-2)EPA 7471B EPA 7471B
92653934005 869233 869360FG-9 (0-2)EPA 7471B EPA 7471B
92653934006 869233 869360FG-10 (0-2)EPA 7471B EPA 7471B
92653934007 869233 869360FG-DUP (0-2)EPA 7471B EPA 7471B
92653934001 758553 758698FG-1 (0-2)EPA 3546 EPA 8270E
92653934002 758553 758698FG-2 (0-2)EPA 3546 EPA 8270E
92653934003 758553 758698FG-3 (0-2)EPA 3546 EPA 8270E
92653934004 758553 758698FG-8 (0-2)EPA 3546 EPA 8270E
92653934005 758553 758698FG-9 (0-2)EPA 3546 EPA 8270E
92653934006 759260 759573FG-10 (0-2)EPA 3546 EPA 8270E
92653934007 759260 759573FG-DUP (0-2)EPA 3546 EPA 8270E
92653934008 758074 758238FG-1 (1-2)EPA 5035A/5030B EPA 8260D
92653934009 758074 758238FG-2 (1-2)EPA 5035A/5030B EPA 8260D
92653934010 758074 758238FG-3 (1-2)EPA 5035A/5030B EPA 8260D
92653934011 758074 758238FG-8 (1-2)EPA 5035A/5030B EPA 8260D
92653934012 758074 758238FG-9 (1-2)EPA 5035A/5030B EPA 8260D
92653934013 758074 758238FG-10 (0-1)EPA 5035A/5030B EPA 8260D
92653934014 758074 758238FG-DUP (1-2)EPA 5035A/5030B EPA 8260D
92653934001 758079FG-1 (0-2)SW-846
92653934002 758079FG-2 (0-2)SW-846
92653934003 758079FG-3 (0-2)SW-846
92653934004 758079FG-8 (0-2)SW-846
92653934005 758079FG-9 (0-2)SW-846
92653934006 758079FG-10 (0-2)SW-846
92653934007 758079FG-DUP (0-2)SW-846
92653934008 758075FG-1 (1-2)SW-846
92653934009 758079FG-2 (1-2)SW-846
92653934010 758079FG-3 (1-2)SW-846
92653934011 758079FG-8 (1-2)SW-846
92653934012 758079FG-9 (1-2)SW-846
92653934013 758079FG-10 (0-1)SW-846
92653934014 758079FG-DUP (1-2)SW-846
92653934001 2013298 2013298FG-1 (0-2)SM 2540 G SM 2540G
92653934002 2013298 2013298FG-2 (0-2)SM 2540 G SM 2540G
92653934003 2013298 2013298FG-3 (0-2)SM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
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9800 Kincey Ave. Suite 100
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[phone]
Page 69 of 75
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92653934
LEN-008
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92653934004 2013298 2013298FG-8 (0-2)SM 2540 G SM 2540G
92653934005 2013298 2013298FG-9 (0-2)SM 2540 G SM 2540G
92653934006 2013298 2013298FG-10 (0-2)SM 2540 G SM 2540G
92653934007 2013298 2013298FG-DUP (0-2)SM 2540 G SM 2540G
92653934001 2013835 2013835FG-1 (0-2)3060A EPA 7199
92653934002 2013835 2013835FG-2 (0-2)3060A EPA 7199
92653934003 2013835 2013835FG-3 (0-2)3060A EPA 7199
92653934004 2013835 2013835FG-8 (0-2)3060A EPA 7199
92653934005 2013835 2013835FG-9 (0-2)3060A EPA 7199
92653934006 2013835 2013835FG-10 (0-2)3060A EPA 7199
92653934007 2013835 2013835FG-DUP (0-2)3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/08/2023 10:02 AM
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[phone]
Page 70 of 75
Page 71 of 75
Page 72 of 75
Page 73 of 75
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Page 75 of 75

Appendix C
DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Final Grade Site Wide - Worst Case
North Carolina Department of Environmental Quality
Risk Calculator
Charlotte Van & Storage Co.
Verbena Street & Gilead Street
Brownfields Redevelopment Section
23057-19-060
January 2023
November 2022 EPA RSL Table
Prepared By:Hart & Hickman, PC
2923 S. Tryon Street, Suite 100, Charlotte, NC
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 23057-19-060
Exposure Unit ID: Final Grade Site Wide - Worst Case
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2023Basis: November 2022 EPA RSL TableSite ID: 23057-19-060Exposure Unit ID: Final Grade Site Wide - Worst CaseNOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsExposure Point Concentration (mg/kg)Notes: CAS NumberChemicalFor the chemicals highlighted in blue, data entry notes are provided in the PSRG Table link on the Main MenuMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion0.0518 67-64-1Acetonemg/kg2.7 7440-38-2Arsenic, Inorganicmg/kg145 7440-39-3Bariummg/kg0.24 7440-43-9Cadmium (Diet)mg/kg0.14 108-90-7Chlorobenzenemg/kg65.5 16065-83-1Chromium(III), Insoluble Saltsmg/kg1.83 18540-29-9Chromium(VI)mg/kg0.023 100-41-4Ethylbenzenemg/kg37.4 7439-92-1~Lead and Compoundsmg/kg0.056 7487-94-7~Mercuric Chloride (and other Mercury salts)mg/kg0.173 56-55-3~Benz[a]anthracenemg/kg0.146 50-32-8~Benzo[a]pyrenemg/kg0.168 205-99-2~Benzo[b]fluoranthenemg/kg0.182 218-01-9~Chrysenemg/kg0.242 206-44-0~Fluoranthenemg/kg0.166 91-20-3~Naphthalenemg/kg0.3 129-00-0~Pyrenemg/kg0.127 103-65-1Propyl benzenemg/kg0.69 7782-49-2Seleniummg/kg0.0244 100-42-5Styrenemg/kg0.444 95-63-6Trimethylbenzene, 1,2,4-mg/kg0.01 1330-20-7 Xylenesmg/kgInput Form 2ASoil Exposure Point Concentration TableDescription of Exposure Point Concentration Selection:North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 23057-19-060
Exposure Unit ID: Final Grade Site Wide - Worst Case
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil 1.2E-05 1.4E-01 NO
Groundwater Use* NC NC NC
Soil NC NC NC
Groundwater Use* NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water* NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Direct Contact - Resident Soil
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 23057-19-060
Exposure Unit ID: Final Grade Site Wide - Worst Case
* - Note that inhalation on this calculator refers to outdoor inhalation of volatiles and particulates, not indoor inhalation associated with vapor intrusion.
CAS # Chemical Name:
Ingestion
Concentration
(mg/kg)
Dermal
Concentration
(mg/kg)
Inhalation
Concentration
(mg/kg)*
Ingestion
Carcinogenic
Risk
Dermal
Carcinogenic
Risk
Inhalation
Carcinogenic
Risk*
Calculated
Carcinogenic
Risk
Ingestion
Hazard
Quotient
Dermal
Hazard
Quotient
Inhalation
Hazard
Quotient*
Calculated Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 0.0518 0.0518 0.0518 7.4E-07 7.4E-07
7440-38-2 Arsenic, Inorganic 2.7 2.7 2.7 3.5E-06 4.9E-07 7.0E-11 4.0E-06 6.9E-02 8.2E-03 2.9E-06 7.7E-02
7440-39-3 Barium 145 145 145 9.3E-03 4.7E-06 9.3E-03
7440-43-9 Cadmium (Diet) 0.24 0.24 0.24 2.6E-12 2.6E-12 3.1E-02 2.9E-03 3.9E-07 3.4E-02
108-90-7 Chlorobenzene 0.14 0.14 0.14 8.9E-05 3.9E-04 4.8E-04
16065-83-1 Chromium(III), Insoluble Salts 65.5 65.5 65.5 5.6E-04 5.6E-04
18540-29-9 Chromium(VI) 1.83 1.83 1.83 6.0E-06 2.6E-09 6.0E-06 7.8E-03 3.0E-07 7.8E-03
100-41-4 Ethylbenzene 0.023 0.023 0.023 3.6E-10 3.4E-09 3.8E-09 5.9E-06 3.7E-06 9.5E-06
7439-92-1 ~Lead and Compounds 37.4 37.4 37.4 <SL** <SL** <SL**
7487-94-7 ~Mercuric Chloride (and other Mercury salts) 0.056 0.056 0.056 2.4E-03 3.0E-09 2.4E-03
56-55-3 ~Benz[a]anthracene 0.173 0.173 0.173 1.1E-07 3.8E-08 2.2E-09 1.5E-07
50-32-8 ~Benzo[a]pyrene 0.146 0.146 0.146 9.5E-07 3.2E-07 1.5E-12 1.3E-06 6.2E-03 1.9E-03 1.2E-06 8.1E-03
205-99-2 ~Benzo[b]fluoranthene 0.168 0.168 0.168 1.1E-07 3.7E-08 1.7E-13 1.5E-07
218-01-9 ~Chrysene 0.182 0.182 0.182 1.2E-09 4.0E-10 1.8E-15 1.6E-09
206-44-0 ~Fluoranthene 0.242 0.242 0.242 7.7E-05 2.4E-05 1.0E-04
91-20-3 ~Naphthalene 0.166 0.166 0.166 2.9E-08 1.0E-08 4.1E-08 8.0E-08 1.1E-04 3.3E-05 1.1E-03 1.2E-03
129-00-0 ~Pyrene 0.3 0.3 0.3 1.3E-04 3.9E-05 1.7E-04
103-65-1 Propyl benzene 0.127 0.127 0.127 1.6E-05 1.6E-05 3.3E-05
7782-49-2 Selenium 0.69 0.69 0.69 1.8E-03 5.6E-10 1.8E-03
100-42-5 Styrene 0.0244 0.0244 0.0244 1.6E-06 2.4E-06 3.9E-06
95-63-6 Trimethylbenzene, 1,2,4- 0.444 0.444 0.444 5.7E-04 8.4E-04 1.4E-03
1330-20-7 Xylenes 0.01 0.01 0.01 6.4E-07 1.6E-05 1.6E-05
Cumulative: 1.2E-05 1.4E-01
Output Form 2A
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate cancer risk or hazard quotient. Lead concentrations are compared to the EPA screening level
of 400 mg/kg for residential soil.
North Carolina DEQ Risk Calculator