WA-28724_47962_CA_RPTS_20210721_CLO

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

July 21, 2021

Mr. Jared Edwards
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: UST Closure Report
May 2021
John E. Ferebee Farming
350 Scotland Road
Camden, Camden County
North Carolina
Facility ID Number: 0-00-0000023546
Incident Number: 7636
GRI Project Number: 5664

Dear Mr. Edwards,

Please find enclosed the referenced report, for the above mentioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Martha Ferebee; John E. Ferebee Farming, Inc. file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
UST Closure Report
May 2021
John E. Ferebee Farming
350 Scotland Road
Camden, Camden County
North Carolina
Facility ID Number: 0-00-0000023546
Incident Number: 7636
GRI Project Number: 5664

Prepared for:

Ms. Martha Ferebee
John E. Ferebee Farming, Inc.
217 Lambs Road
Camden, NC 27921

July 21, 2021

William Regenthal, P.G.
Project Manager
Brett Houghton
Staff Scientist

_____________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
ii

EXECUTIVE SUMMARY
John E. Ferebee Farming is an active potato farm located at 350 Scotland Road in Camden, Camden
County, North Carolina. The adjoining properties are residential and agricultural. Municipal water is
available to the site and surrounding properties. A UST system consisting of one 10,000-gallon diesel UST
was removed from the site in February 1992.

A petroleum release was discovered at the site and was assigned UST Incident Number 7636 for the
release and was closed in April 1992.

One 6,000-gallon gasoline UST was removed from the site in October 2016.

During the May 2021 UST closure activities, ground water was encountered. Therefore, a ground water
sample was collected from an on-site at the direction of the NCDEQ incident manager. UST closure soil
samples were collected along the sidewalls of the UST basin, beneath the product piping and beneath the
diesel dispensers, and were submitted for on-site analyses of gasoline-range and diesel-range total
petroleum hydrocarbons using a mobile ultraviolet fluorescence (UVF) laboratory. Based on the field
observations and UVF field screening results, no new release was observed. A total of 25.49 tons of soil
was removed from the former UST basin and clean fill dirt was brought in to back fill the basin.

Based on the soil and ground water sample results and previous incident low risk classification, the site
should remain low risk. A Notice of Residual Petroleum for soil and ground water should be filed on the
deed of the subject property. No further ground water or soil assessment is necessary.

_____________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
TABLE OF CONTENTS

SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
A. SITE HISTORY AND CHARACTERIZATION ...................................................................................1
B. SITE CHECK ..............................................................................................................................2
C. UST CLOSURE ..........................................................................................................................2
D. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT .........................................................4
E. GROUND WATER INVESTIGATION ............................................................................................4
F. INITIAL RESPONSE AND ABATEMENT ACTION ...........................................................................4
G. EXCAVATION OF CONTAMINATED SOIL ....................................................................................5
H. SOIL AND GROUND WATER RESULTS ........................................................................................5
I. SUMMARY AND CONCLUSIONS ................................................................................................6
J. LIMITATIONS ...........................................................................................................................7
FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Soil Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Summary of Soil Sample Analytical Results
Table 4: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: 24-Hour Release Reporting Form (UST-61)
Appendix B: Notice of Intent form (UST-3)
Appendix C: Site Investigation Report for Permanent Closure or Change-in-Service of UST (UST-2A)
Appendix D: Health and Safety Plan
Appendix E: UST Disposal Manifest
Appendix F: Soil Disposal Manifest and Weight Tickets
Appendix G: Mobile Laboratory Reports – Soil Samples
Appendix H: Laboratory Report – Soil and Ground Water Samples

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
1

A. SITE HISTORY AND CHARACTERIZATION
1. UST Owner and Operator Information:
In accordance with the UST closure guidelines, the underground storage tank (UST) owner and operator
information has been summarized in Table 1.
2. UST System Information:
In accordance with the UST closure guidelines, the UST system information has been summarized in Table
2. A copy of the Registered Tank Report is shown below:

3. Non-UST Information
No aboveground storage tanks (ASTs) were at the site.
4. Comprehensive Description of the Release:
Geological Resources, Inc. (GRI) initiated UST closure activities at the site on May 25, 2021. The UST
system consisted of two 8,000-gallon diesel USTs, associated dispensers and product piping. On May 25,
2021, two 8,000-gallon diesel USTs, associated product piping and dispensers were removed from the
site. During UST closure activities, concentrations of gasoline-range total petroleum hydrocarbons (GRO-
DRO) and diesel-range total petroleum hydrocarbons (TPH-DRO) were reported in soil samples collected
during closure activities. A 24-Hour Notice of Release (UST-61 Form) was submitted to the Washington
regional office of NCDEQ on May 25, 2021. A copy of the UST-61 Form is included as Appendix A.

A prior petroleum release was discovered at the site and was assigned UST Incident Number 7636 for the
release and was closed in April 1992.

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
2

5. Description of the Site Characteristics:
The John E. Ferebee Farming site is an active farm located at 350 Scotland Road in Camden, Camden
County, North Carolina (Figure 1). The site is bordered to the southeast by Scotland Road. A site map has
been included as Figure 2.
6. Summary of Initial Abatement Actions, Assessment Activities, and Corrective Actions:
Prior to closure, the appropriate officials were notified by GRI (i.e., Fire Marshal and NCDEQ). Two 8,000-
gallon diesel USTs, associated dispensers and product piping were removed from the site on May 25, 2021.
Petroleum contamination was noted in the UST basin upon removal of the UST. Ground water was
encountered therefore, a ground water sample was collected from an existing observation well adjacent
to the former UST basin.

B. SITE CHECK
A site check was not part of the UST closure activities.

C. UST CLOSURE
1. Preparation for UST Closure:
Prior to closure, the appropriate officials were notified by GRI (i.e. Fire Marshal and NCDEQ). A copy of
the UST-3 Notice of Intent form is included as Appendix B. A copy of the UST-2A Site Investigation Report
for Permanent Closure or Change-in-Service form was submitted to the compliance branch of NCDEQ on
May 26, 2021, and has been included as Appendix C. A copy of the site-specific health and safety plan
used during UST closure activities site is included as Appendix D.
2. Closure Procedure:
On May 25, 2021, two 8,000-gallon diesel USTs, associated dispensers and product piping were removed
from the site. The USTs were covered with concrete and soil. The USTs were visually inspected and
appeared to be in good condition with no obvious defects. The USTs were constructed of single-wall steel.
The UST was transported off site for proper disposal. A disposal manifest for the USTs removed in May
2021 is included as Appendix E. Photos of the removed 8,000-gallon USTs are shown below:

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
3

3. Residual Material:
The USTs and product piping were emptied of contents prior to site activities.
4. Release information:
According to the available information, a petroleum release was discovered at the site and was assigned
UST Incident Number 7636 for the release and was closed in April 1992. During the May 2021 UST closure
activities, soil and ground water samples were collected in accordance with NCDEQ guidelines.

5. Soil Excavation Activities:
A total of 25.49 tons of soil was removed from the site. All excavated soil was transported to a permitted
disposal facility.
6. Site Investigation:
During excavation activities, GRI personnel collected soil samples for on-site analyses by Rapid
Environmental Diagnostics (REDLab) for total petroleum hydrocarbons gasoline range organics (TPH-GRO)
and diesel range organics (TPH-DRO) using North Carolina accepted QED Environmental Systems
ultraviolet fluorescence (UVF) technology.

During the May 2021 UST closure activities, soil samples (UST-1-1 through UST-1-5 and UST-2-1 through
UST-2-5) were collected along the sidewalls of the UST basin at depths of 7 feet below ground surface
(bgs) and beneath the gasoline dispensers (DI-1 and DI-2) at 5 feet bgs. One stockpile sample (SP-1) and
one overburden sample (OB-1) were collected from the contaminated soil that was transported off-site
for disposal.

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
4

Upon completion of the limited over-excavation activities, confirmation soil samples (CS-1, CS-2 and CS-
3) were collected from the sidewalls of the excavation basin at depths of 8 feet bgs. The collected
confirmation samples were submitted for laboratory analyses of volatile organic compounds (VOCs) using
EPA Method 8260B, semi-VOCs using EPA Method 8270, as well as VPH and EPH using the MADEP
Methods.

Limited over-excavation activities were conducted in the former UST basin. A total of 25.49 tons of soil
was removed from the site and transported for disposal. Soil disposal manifests and weight tickets are
included as Appendix F.

D. FREE PRODUCT INVESTIGATION AND RECOVERY REPORT
During the May 2021 UST closure activities free product was not encountered.

E. GROUND WATER INVESTIGATION
During the May 2021 UST closure activities, ground water was encountered. At the direction of the on-
site NCDEQ personnel, a ground water sample (MW-A) was collected from an existing observation well
located adjacent to the UST basin and was submitted for analyses of VOCs using EPA Method 6200B, semi-
VOCs using EPA Method 625 + 10 highest tentatively identified compounds, as well as MADEP Methods
EPH and VPH.

F. INITIAL RESPONSE AND ABATEMENT ACTION
1. Initial Response Actions:
Two 8,000-gallon diesel USTs, associated dispensers and product piping were removed from the site on
May 25, 2021. Ground water was encountered therefore, a ground water sample was collected. A total
of 25.49 tons of soil was removed from the site and transported for disposal. The UST basin was backfilled
with clean soil.
 Source Control Actions: Two 8,000-gallon diesel USTs, associated dispensers and product piping were
removed from the site on May 25, 2021.
 Contaminant Migration Control Measures: The release was to the subsurface; therefore,
contaminant migration control measures were not necessary.
 Measures Taken to Mitigate Fire/Safety Hazards: Prior to closure, the atmosphere of each UST
compartment was checked with an LEL/02 meter; once each UST compartment atmosphere reached
less than 10% LEL, each tank was removed. There did not appear to be any immediate fire or safety
hazards present because of the release. Free product was not encountered during closure activities.
 Measures Taken to Identify and Mitigate Pollution Hazards: The release was to the subsurface;
therefore, contaminant migration control measures were not necessary.

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
5

G. EXCAVATION OF CONTAMINATED SOIL
1. Extent of Soil Contamination:
Since a past release had been observed at the site, limited over-excavation activities were conducted in
the former UST basin to remove contaminated soil. A total of 25.49 tons of soil was removed from the
site and transported for disposal. The excavation was filled with clean backfill.

2. Excavation Process:
The excavation activities were conducted using a track-mounted excavator.

3. Sampling Description:
All soil samples were collected directly from the bucket of the excavator or using a hand auger by GRI
personnel. Samples were collected with clean, disposable nitrile gloves and immediately transferred
to the onsite mobile UVF laboratory for analysis.

H. SOIL AND GROUND WATER RESULTS
 Soil:
Concentrations of TPH-GRO and/or TPH-DRO that exceeded the RALs were reported in the soil samples
collected from UST-1-1, UST-1-2, UST-1-5, UST-2-3, UST-2-4, UST-2-5, OB-1, SP-1, and DI-2.
Concentrations of benzene, ethylbenzene, xylenes, n-butylbenzene, 1-methylnaphthalene, 2-
methylnaphthalene, C5-C8 aliphatics, C9-C18 aliphatics and/or C9-C22 aromatics that exceeded the soil-
to-water Maximum Contaminant Concentrations (MCCs) were reported in the soil samples collected from
CS-1, CS-2 and CS-3. Concentrations of ethylbenzene and C9-C22 aromatics that exceeded the residential
cleanup levels were reported in the soil sample collected from CS-1. A summary of soil sample analytical
results is presented as Table 3. A Soil Quality Map has been included as Figure 3. Copies of the mobile
laboratory reports are included as Appendix G. A complete laboratory report for the confirmation soil
samples collected in May 2021 is included as Appendix H. A summary of the on-site UVF soil sampling
data from the May UST closure activities is shown below:
Sample ID Sample Depth (ft-BGS) Gasoline-Range TPH Diesel-Range TPH RAL (mg/kg) 50 100
UST-1-1 8 417.2 4,031
UST-1-2 8 28.7 196
UST-1-3 8 <1.1 26.8
UST-1-4 8 <1.1 1.1
UST-1-5 8 9.4 199.8
UST-2-1 8 0.64 1.7
UST-2-2 8 2.7 13.3
UST-2-3 8 18.4 151.4
UST-2-4 8 311 2,908
UST-2-5 8 201.6 1,774
OB-1 --- 1,024 3,074

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
6
Sample ID Sample Depth (ft-BGS) Gasoline-Range TPH Diesel-Range TPH RAL (mg/kg) 50 100
SP-1 --- 2,869 40,892
DI-1 5 2.3 23.4
DI-2 5 777.1 7,425

 Ground Water:
A concentration of C9-C22 Aromatics was reported in the ground water sample collected from MW-A on
May 25, 2021. A summary of ground water sample analytical results is presented as Table 4. A copy of
the laboratory report for the ground water sample collected in May 2021 is included as Appendix H. A
summary of the ground water sampling data from the May UST closure activities is shown below:

Contaminant
of Concern → Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-A <0.13 <0.13 <0.13 <0.25 <0.13 <0.13

I. SUMMARY AND CONCLUSIONS
 On May 25, 2021, two 8,000-gallon diesel USTs, associated dispensers and product piping were
removed from the site.
 A total of 25.49 tons of soil was removed from the site and transported to a permitted disposal facility.
 No free product was noted in the UST basin during closure activities.
 Ground water was encountered during the May 2021 UST closure activities.
 Concentrations of TPH-GRO and/or TPH-DRO that exceeded the RAL were reported in the soil samples
collected from UST-1-1, UST-1-2, UST-1-5, UST-2-3, UST-2-4, UST-2-5, OB-1, SP-1 and DI-2.
 Concentrations of benzene, ethylbenzene, xylenes, n-butylbenzene, 1-methylnaphthalene, 2-
methylnaphthalene, C5-C8 aliphatics, C9-C18 aliphatics and/or C9-C22 aromatics that exceeded the
soil-to-water MCCs were reported in the soil samples collected from CS-1, CS-2 and CS-3.
Concentrations of ethylbenzene and C9-C22 aromatics that exceeded the residential cleanup levels
were reported in the soil sample collected from CS-1.
 A ground water sample was collected from the base of the excavation in lieu of the installation of a
monitoring well at the direction of the on-site NCDEQ personnel. A concentration of C9-C22
Aromatics was reported in the ground water sample collected from MW-A.
 Based on the soil and ground water sample results and previous incident low risk classification, the
site should remain low risk. A Notice of Residual Petroleum for soil and ground water should be filed

____________________________________________________________________________________________
Prepared by: Geological Resources, Inc. UST Closure Report
Prepared on: July 21, 2021 John E. Ferebee Farming
Project Manager: William Regenthal GRI Project No. 5664
7

on the deed of the subject property. No further ground water or soil assessment is necessary.
J. LIMITATIONS
This report has been prepared for the exclusive use of John E. Ferebee Farming, Inc. for specific application
to the referenced site in Camden County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATIONFigure 1 Site Location John E. Ferebee Farming Inc. 250 Scotland RoadCamden, North CarolinaCamden CountyIncident No. 7636GRI Project No. 5664500 M2000 FTDate: 05/27/2021Location: 36.372446° N -76.157001° W Dad

TABLES
UST ID Number 1 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 2 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 3, 4 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
250 Scotland Road, Camden, NC 27921 252-338-6401
00-0-0000023546
Name of Owner or Operator Dates of Ownership / Operation
John E. Ferebee Farming, Inc.03/01/1985 - 05/25/2021
Address Telephone Number
250 Scotland Road, Camden, NC 27921 252-338-6401
00-0-0000023546
Name of Owner or Operator Dates of Ownership / Operation
John E. Ferebee Farming, Inc.03/01/1985 - Current
250 Scotland Road, Camden, NC 27921 252-338-6401
Name of Owner or Operator Dates of Ownership / Operation
John E. Ferebee Farming, Inc.02/24/1976 - 02/12/1992
Address Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
JOHN E. FEREBEE FARMING, INC. (INCIDENT NO. 7636)
00-0-0000023546
Page 1 of 1
Date: 05/26/2021
Was Release
Associated
with UST
System?
(Yes / No)
1 Diesel 10,000 02/24/1976 Single Wall Steel Unknown Single Wall Steel
Removed
(02/12/1992)Yes
(UST Incident No. 7636)
2 Gasoline 6,000 02/21/1985 Single Wall Steel Unknown Single Wall FRP Current Unknown
3 Diesel 8,000 03/31/1993 Single Wall Steel Unknown Single Wall FRP Removed
(05/25/2021)Unknown
4 Diesel 8,000 03/31/1993 Single Wall Steel Unknown Single Wall FRP Removed
(05/25/2021)Unknown
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
JOHN E. FEREBEE FARMING, INC. (INCIDENT NO. 7636)
Facility ID #: 00-0-0000023546
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Date: 06/22/2021 Facility ID #: 00-0-0000023546
Sample ID
Date
Collected
(mm/dd/yy)
Sample
Location
Sample
Depth
(ft-BGS)
50 100 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
NA NA 0.0072 5.4 8.0 6.0 0.085 0.20 2.4 1.3 1.4 0.054 1.5 68 540 NE 31
NA NA 12 1,250 60 3,120 156 6 782 1,560 1,560 23 63 625 1,560 31,200 469
CS-1-8 05/25/21 8 NA NA 1.71 J <1.0 456 7.41 J <0.58 <3.2 201 125 433 22.4 36.0 338 566 142 1,072
CS-2-8 05/25/21 8 NA NA 0.00022 J 0.0020 J 0.00068 J <0.0011 <0.00009 0.00086 J 0.0012 J 0.0010 J 0.0015 J 0.183 J 0.197 J <1.8 33.7 19.3 58.36
CS-3-8 05/25/21 8 NA NA <0.65 <0.59 <0.85 <3.8 <0.34 <1.9 <1.1 <0.93 <1.4 3.29 4.87 2.76 J 328 85.3 525
UST-1-1 05/25/21 7 417.2 4,031 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-1-2 05/25/21 7 28.7 196 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-1-3 05/25/21 7 <1.1 26.8 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-1-4 05/25/21 7 <1.1 1.1 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-1-5 05/25/21 7 9.4 199.8 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-2-1 05/25/21 7 0.64 1.7 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-2-2 05/25/21 7 2.7 13.3 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-2-3 05/25/21 7 18.4 151.4 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-2-4 05/25/21 7 311 2,908 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
UST-2-5 05/25/21 7 201.6 1,774 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
OB-1 05/25/21 Overburden ---1,024 3,073 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
SP-1 05/25/21 Stockpile Area ---2,869 40,892 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
DI-1 05/25/21 5 2.3 23.4 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
DI-2 05/25/21 5 777.1 7,425 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
• NR: Not Requested.
TABLE 3
JOHN E. FEREBEE FARMING, INC. (INCIDENT NO. 7636)
Analytical Method 
• Concentrations in bold face type indicate the RALs were less than the reported concentrations
Notes:
• Results reported in mg/kg; samples analyzed onsite by UVF.
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• < : Less than the UFV method detection limit .
RAL (mg/kg)
Contaminant of Concern Gasoline-Range TPHSUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS - FIELD DATA
Isopropylbenzenen-ButylbenzeneC9-C18 AliphaticsMTBENaphthalene• NA: Not applicable.1-Methylnaphthalene2-MethylnaphthaleneDispenser Island Diesel-Range TPHUVF
C9-C22 AromaticsC19-C36 AliphaticsC5-C8 AliphaticsMADEP VPH
BenzeneSoil to Water MSCC (mg/kg)
Residential Soil Cleanup Levels (mg/kg)
Soil Sample
SW846 8260D
n-PropylbenzeneTolueneEthylbenzeneXylenesPage 1 of 1
Date: 06/22/2021
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 400 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 NE NE NE NE
MW-A 05/25/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <35 <85 <50 419
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Not Established
• Concentrations in bold face type exceeded the 2L standards.
• Concentrations in italics exceeded the gross contamination levels.
• Refer to laboratory report for detected constituents that did not exceed the MACs, or for which no standard has been established.
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
JOHN E. FEREBEE FARMING, INC. (INCIDENT NO. 7636)
Facility ID #: 00-0-0000023546
2L Standard (µg/l)
GCL (µg/l)
MADEP VPH and EPH
C19-C36 AliphaticsC9-C22 AromaticsC5-C8 AliphaticsC9-C18 AliphaticsContaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)NaphthaleneAnalytical Method
SM 6200B
Page 1 of 1

APPENDICES

APPENDIX A
24-Hour Release Reporting Form (UST-61)

UST-61 24-Hour Release and UST Leak Reporting Form.
For Releases
in NC
This form should be completed and submitted to the UST Section’s regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
suspected release
(DWM USE ONLY) Incident # ________ Risk (H,I,L,U)_______ Received On ________ Received By ________
Reported by (circle one): Phone, Fax or Report Region _______
Suspected Contamination? (Y/N) ________ Confirmed GW Contamination? (Y/N) ______ Confirmed Soil Contamination ?(Y/N) ______
Samples Taken?(Y/N) ______ Free Product? (Y/N) _____ If Yes, State Greatest Thickness ______________
Facility ID Number ______________ Date Leak Discovered ___________ Comm/Non-Commercial? ________
Reg/Non-regulated? _____________
INCIDENT DESCRIPTION
Incident Name:
Address: County:
City/Town: Zip Code: Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): Longitude (decimal degrees) : Obtained by:
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors)  GPS
 Topographic map
 GIS Address matching
 Other
 Unknown
Describe location:

HOW RELEASE WAS DISCOVERED (Release Code)
(Check one)
 Release Detection Equipment or Methods
 During UST Closure/Removal
 Property Transfer
 Visual/Odor
 Water in Tank
 Water Supply Well Contamination
 Groundwater Contamination
 Surface Water Contamination
 Other (specify) _______________

SOURCE OF CONTAMINATION
Source of Release (Check primary source) Cause of Release (Check primary cause) Type of Release (Check one) Product Type Released (Check primary product type released)

 Tank
 Piping
 Dispenser
 Submersible Turbine Pump
 Delivery Problem
 Spill Bucket
 Other
 Unknown
Definitions presented on reverse

 Spill
 Overfill
 Corrosion
 Physical/Mechanical
Damage
 Install Problem
 Other
 Unknown
Definitions presented on reverse

 Petroleum
 Non-Petroleum
 Both
Location
(Check one)
 Facility
 Residence
 Other

 Gasoline/ Diesel/
Kerosene
 Heating Oil
 Other Petroleum
Products
 Metals
 Other Inorganics
 Other Organics

 Diesel/Veg. Oil
Blend
 Vegetable Oil 100%
 E10 – E20
 E21 – E84
 E85 – E99
 Ethanol 100%
 E01 – E09
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining
UST Form 61 (02/19) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected __________________
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) 1. 2. 3.
UST SYSTEM OWNER UST Owner/Company
Point of Contact Address
City State Zip Code Telephone Number
UST SYSTEM OPERATOR
UST Operator/Company Address
City State Zip Code Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner Address
City State Zip Code Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Person Reporting Incident Company Telephone Number
Title Address Date
UST Form 61 (02/19) Page 2 of 2
Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end-use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined

APPENDIX B
Notice of Intent form (UST-3)
UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service
Return completed form to:
The DWM Regional Office located in the area where the facility is located. Also send a copy to the Central Office in Raleigh.
SEE MAP ON THE BACK OF THIS FORM FOR THE CENTRAL AND REGIONAL OFFICE ADDRESSES.
STATE USE ONLY
I.D. #_____________________
Date Received______________
INSTRUCTIONS (READ THIS FIRST)
Complete and return a UST-3 form at least thirty (30) days prior to closure or change-in-service activities.
Completed UST closure or change-in-service site assessment reports, along with a copy of the UST-2A and/or 2B forms, should be submitted
to the appropriate Division of Waste Management (DWM) Regional Office within thirty (30) days following closure activities. The UST-2 form
should also be submitted to the Central Office in Raleigh so that the status of the tanks may be changed to permanently closed and your
tank fee account can be closed out.Note: Tank fees may be due for unregistered tanks.
UST closure and change-in-service site assessments must be completed in accordance with the latest version of the Guidelines for Site
Checks, Tank Closure and Initial Response. The guidelines can be obtained at https://deq.nc.gov/about/divisions/waste-management/ust.
Note: To close tanks in place you must obtain prior approval from the DWM Regional office located in the region where the facility is located.
You must make sure that USTs removed from your property are disposed of properly. When choosing a closure contractor, ask where the
tank(s) will be taken for disposal. Usually, USTs are cleaned and cut up for scrap metal. This is dangerous work and must be performed
by a qualified company. Tanks disposed of illegally in fields or other dumpsites can leak petroleum products and sludge into the environment.
If your tanks are disposed of improperly, you could be held responsible for the cleanup of any environmental damage that occurs.
I. OWNERSHIP OF TANKS II. LOCATION
Owner Name (Corporation, Individual, Public Agency, or Other Entity) Facility Name or Company
Street Address Facility ID # (If known)
City County Street Address
State Zip Code City County Zip Code
Phone Number Email Phone Number
III. CONTACT PERSONNEL
Name:Company Name:Job Title: Phone Number:
IV. TANK REMOVAL, CLOSURE IN PLACE, CHANGE-IN SERVICE
1.Contact local fire marshal.
2.Plan entire closure event.
3.Conduct Site Soil Assessment.
4.If removing tanks or closing in place, refer to
API Publication 2015 Cleaning Petroleum
Storage Tanks and 1604 Removal and
Disposal of Used Underground Petroleum
Storage Tanks.
5.Provide a sketch locating piping, tanks and
soil sampling locations.
6.Submit a closure report in the format of UST-
12 (including the form UST-2) within thirty
(30) days following the site investigation.
7.If a release from the tanks has occurred, the
site assessment portion of the tank closure
must be conducted under the supervision of
a P.E. or L.G., with all closure site assessment
reports bearing the signature and seal of the
P.E. or L.G. If a release has not occurred, the
supervision, signature or seal of a P.E. or L.G.
is not required.
8.Keep closure records for three (3) years.
V. WORK TO BE PERFORMED BY
Contractor Name:Contractor Company Name:
Address:State: Zip Code:Phone No:
Primary Consultant Name:Primary Consultant Company Name:Consultant Phone No:
VI. TANKS SCHEDULED FOR CLOSURE OR CHANGE-IN-SERVICE
Tank ID No.Size in Gallons Last Contents
Proposed Activity
Closure Change-In-Service
Removal Abandonment in Place *New Contents Stored
*Prior written approval to abandon a tank in place must be received from a DWM Regional Office.
VII.OWNEROROWNER’SAUTHORIZEDREPRESENTATIVE
Has a release from a UST system occurred at this location? Yes No Unknown
I understand that I can be held responsible for environmental damage resulting from the improper disposal of my USTs.
Print name and official title:
Signature Date Signed SCHEDULED REMOVAL DATE Notify your DWM Regional Office
48 hours before this date if
scheduled removal date changes
UST-3 Rev 2/2021
NC Camden
NC

APPENDIX C
Site Investigation Report for Permanent Closure or Change-in-Service form (UST-2A)

APPENDIX D
Health and Safety Plan

APPENDIX E
UST Disposal Manifest

UST DISPOSAL MANIFEST

Site Name: John E Ferebee Farming, Inc.
Site Address:350 Scotland Road, Camden, Camden County

The following UST(s) were removed from the above noted site on May 25, 2021, and
transported to John E. Ferebee Farming, Inc., where the UST will be properly disposed of at a
future date.

1. 8,000-gallon diesel UST
2. 8,000-gallon diesel UST
3._____________________
4._____________________

Signature:___________________________
Printed Name: William Regenthal
Date: 05/27/2021

APPENDIX F
Soil Disposal Manifests and Weight Tickets

APPENDIX G
Mobile Laboratory Reports – Soil Samples

Hydrocarbon Analysis Results
Client:Geological Resources, Inc.Samples taken Tuesday, May 25, 2021
Address:Camden, NC Samples extracted Tuesday, May 25, 2021
Samples analysed Tuesday, May 25, 2021
Contact:William Regenthal Operator Caroline Stevens
Project:Ferebee Farming, Inc.
10 F03640
Matrix Sample ID Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s SP-1 (0912)13044.0 <326.1 2869 40892 43761 11237 427 <13 65.4 33.2 1.4 Deg.Diesel 79.1%,(FCM)
s D-1 (0922)21.0 <0.53 2.3 23.4 25.7 6.4 0.23 <0.021 79.3 20 0.6 Deg.Diesel 81.9%,(FCM)
s D-2 (0926)1050.0 <26.3 777.1 7425 8202 1299 47.1 <1.1 84.6 15 0.4 Deg.Diesel 77.3%,(FCM)
s OB-1 (0930)1056.0 <26.4 1024 3073 4097 852.5 31.8 <1.1 91.7 7.8 0.5 Deg.Diesel 80.9%,(FCM)
s UST-1-1 (1021)1413.0 <35.3 417.2 4031 4448 1086 39.7 <1.4 75.9 21.6 2.5 Deg.Diesel 68.5%,(FCM)
s UST-1-2 (1022)34.3 <0.86 28.7 196 224.7 52.5 2 <0.034 80.4 18.7 0.9 Deg.Diesel 79.1%,(FCM)
s UST-1-3 (1023)43.1 <1.1 <1.1 26.8 26.8 5.2 <0.34 <0.043 0 84.8 15.2 Deg.Diesel 77.3%,(FCM)
s UST-1-4 (1024)43.7 <1.1 <1.1 1.1 1.1 1.1 <0.35 <0.044 0 71.5 28.5 V.Deg.PHC 89.4%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 108 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
QED Hydrocarbon Fingerprints
Project:Ferebee Farming, Inc.##################
Hydrocarbon Analysis Results
Client:Geological Resources, Inc.Samples taken Tuesday, May 25, 2021
Address:Camden, NC Samples extracted Tuesday, May 25, 2021
Samples analysed Tuesday, May 25, 2021
Contact:William Regenthal Operator Caroline Stevens
Project:Ferebee Farming, Inc.
16 F03640
Matrix Sample ID Dilution
used
BTEX
(C6 - C9)
GRO
(C5 - C10)
DRO
(C10 - C35)
TPH
(C5 - C35)
Total
Aromatics
(C10-C35)
16 EPA
PAHs BaP HC Fingerprint Match
% light % mid %
heavy
s UST-2-1 (1111)13.8 <0.35 0.64 1.7 2.3 0.8 <0.11 <0.014 63.6 26.3 10.1 Deg.Fuel 86.7%,(FCM),(BO)
s UST-2-2 (1112)20.0 <0.5 2.7 13.3 16 4.7 <0.16 <0.02 67.5 25.8 6.7 Deg.Fuel 84.6%,(FCM)
s UST-2-3 (1115)20.3 <0.51 18.4 151.4 169.8 57.6 2.1 <0.02 72.3 26.1 1.6 Deg.Diesel 73.2%,(FCM)
s UST-2-4 (1118)1033.0 <25.8 311 2908 3219 1169 41.6 <1 79 20.1 0.9 Deg.Diesel 78.1%,(FCM)
s UST-2-5 (1122)1424.0 <35.6 201.6 1774 1976 533.8 19.3 <1.4 81.8 17.8 0.5 Deg.Diesel 81.5%,(FCM)
s UST-1-5 (1126)181.0 <4.5 9.4 199.8 209.2 57.3 2.1 <0.18 63.3 34 2.7 Deg.Diesel 89.9%,(FCM)
Initial Calibrator QC check OK Final FCM QC Check OK 108.8 %
Results generated by a QED HC-1 analyser. Concentration values in mg/kg for soil samples and mg/L for water samples. Soil values are not corrected for moisture or stone content
Fingerprints provide a tentative hydrocarbon identification. The abbreviations are:- FCM = Results calculated using Fundamental Calibration Mode : % = confidence for sample fingerprint match to library
(SBS) or (LBS) = Site Specific or Library Background Subtraction applied to result : (PFM) = Poor Fingerprint Match : (T) = Turbid : (P) = Particulate present
Ratios
QED Hydrocarbon Fingerprints
Project:Ferebee Farming, Inc.##################

APPENDIX H
Laboratory Report – Soil and Ground Water Samples
07/19/21
Technical Report for
GRI (Geological Resources Inc.)
John E Ferebee Farming; 350 S Astland Rd, Camden, NC
5664
SGS Job Number: FA85879
Sampling Date: 05/25/21
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthal
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, UT, VT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 07/19/21
Reissue #1
e-Hardcopy 2.0
Automated Report
81
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 81
FA85879
Florida ♦ 4405 Vineland Road ♦ Suite C-15 ♦ Orlando, FL 32811 ♦ tel: [phone] ♦ fax: [phone]

June 16, 2021 Mr. William Regenthal Geological Resources Inc. 3502 Hayes Road Monroe, NC 28110 RE: SGS North America Inc. - Orlando job FA85879 Reissue Dear Mr. Regenthal, The final report for job number FA85879 has been edited to reflect requested corrections. These edits have been incorporated into the revised report. Additional VOC’s for 8260 analysis have been reported. SGS North America Inc. - Orlando apologies for any inconvenience this may have caused. Please feel free to contact us if we can be of further assistance. Sincerely,

SGS North America, Inc. - Orlando
2 of 81
FA85879
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................8
3.1: FA85879-1: MW-A .......................................................................................................9
3.2: FA85879-2: CS-1 8' ......................................................................................................16
3.3: FA85879-3: CS-2 8' ......................................................................................................22
3.4: FA85879-4: CS-3 8' ......................................................................................................28
Section 4: Misc. Forms ............................................................................................................34
4.1: Chain of Custody ...........................................................................................................35
Section 5: MS Volatiles - QC Data Summaries .....................................................................37
5.1: Method Blank Summary ................................................................................................38
5.2: Blank Spike Summary ...................................................................................................39
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................40
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................41
6.1: Method Blank Summary ................................................................................................42
6.2: Blank Spike Summary ...................................................................................................46
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................50
Section 7: GC Volatiles - QC Data Summaries .....................................................................52
7.1: Method Blank Summary ................................................................................................53
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................56
7.3: Duplicate Summary .......................................................................................................59
Section 8: GC/LC Semi-volatiles - QC Data Summaries .....................................................61
8.1: Method Blank Summary ................................................................................................62
8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................64
8.3: Duplicate Summary .......................................................................................................66
Section 9: Misc. Forms (SGS Scott, LA) ................................................................................67
9.1: Chain of Custody ...........................................................................................................68
Section 10: MS Volatiles - QC Data (SGS Scott, LA) ...........................................................71
10.1: Method Blank Summary ..............................................................................................72
10.2: Blank Spike/Blank Spike Duplicate Summary ............................................................76
10.3: Matrix Spike/Matrix Spike Duplicate Summary .........................................................80 123456789103 of 81
FA85879
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA85879
John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Project No: 5664
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA85879-1 05/25/21 10:31 WR 05/26/21 AQ Ground Water MW-A
FA85879-2 05/25/21 12:12 WR 05/26/21 SO Soil CS-1 8'
FA85879-3 05/25/21 12:15 WR 05/26/21 SO Soil CS-2 8'
FA85879-4 05/25/21 12:19 WR 05/26/21 SO Soil CS-3 8'
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
4 of 81
FA858791
Summary of Hits Page 1 of 3
Job Number:FA85879
Account:GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Collected:05/25/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA85879-1 MW-A
Total TIC, Semi-Volatile 304.8 J ug/l
C11-C22 Aromatics (Unadj.) a 419 200 80 ug/l MADEP EPH REV 2.1
C11-C22 Aromatics a 419 200 80 ug/l MADEP EPH REV 2.1
FA85879-2 CS-1 8'
Benzene b 1.71 J 2.8 1.1 mg/kg SW846 8260D
n-Butylbenzene b 201 28 1.8 mg/kg SW846 8260D
Ethylbenzene b 456 5.5 1.4 mg/kg SW846 8260D
Isopropylbenzene b 125 28 1.6 mg/kg SW846 8260D
Methylcyclohexane b 283 28 7.2 mg/kg SW846 8260D
n-Propylbenzene b 433 28 2.4 mg/kg SW846 8260D
Xylene (total) b 7.41 J 11 6.4 mg/kg SW846 8260D
Acenaphthene 1.88 1.0 0.11 mg/kg SW846 8270E
Anthracene 0.686 J 1.0 0.11 mg/kg SW846 8270E
Dibenzofuran 1.00 1.0 0.10 mg/kg SW846 8270E
bis(2-Ethylhexyl)phthalate 0.283 J 2.0 0.20 mg/kg SW846 8270E
Fluorene 2.99 1.0 0.11 mg/kg SW846 8270E
1-Methylnaphthalene 22.4 5.1 0.51 mg/kg SW846 8270E
2-Methylnaphthalene 36.0 5.1 0.51 mg/kg SW846 8270E
Phenanthrene 5.22 1.0 0.10 mg/kg SW846 8270E
Pyrene 0.485 J 1.0 0.12 mg/kg SW846 8270E
Benzene 1.44 0.63 0.63 mg/kg MADEP VPH REV 2.1
Ethylbenzene 16.1 1.3 0.63 mg/kg MADEP VPH REV 2.1
Naphthalene 3.83 3.1 1.9 mg/kg MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.)339 63 22 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)488 250 88 mg/kg MADEP VPH REV 2.1
C5- C8 Aliphatics 338 63 22 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics 488 250 88 mg/kg MADEP VPH REV 2.1
Acenaphthene 4.05 1.2 0.61 mg/kg MADEP EPH REV 2.1
2-Methylnaphthalene 17.4 1.2 0.61 mg/kg MADEP EPH REV 2.1
Naphthalene 7.48 1.2 0.61 mg/kg MADEP EPH REV 2.1
Phenanthrene 2.49 1.2 0.61 mg/kg MADEP EPH REV 2.1
C11-C22 Aromatics (Unadj.)615 61 24 mg/kg MADEP EPH REV 2.1
C11-C22 Aromatics 584 61 24 mg/kg MADEP EPH REV 2.1
C9-C18 Aliphatics 566 61 15 mg/kg MADEP EPH REV 2.1
C19-C36 Aliphatics 142 61 15 mg/kg MADEP EPH REV 2.1
FA85879-3 CS-2 8'
Acetone b 0.0272 J 0.045 0.0020 mg/kg SW846 8260D
Benzene b 0.00022 J 0.00045 0.00018 mg/kg SW846 8260D
n-Butylbenzene b 0.0012 J 0.0045 0.00029 mg/kg SW846 8260D
5 of 81
FA858792
Summary of Hits Page 2 of 3
Job Number:FA85879
Account:GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Collected:05/25/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Carbon Disulfide b 0.0011 0.00091 0.00038 mg/kg SW846 8260D
Cyclohexane b 0.0019 0.00091 0.00032 mg/kg SW846 8260D
Ethylbenzene b 0.00068 J 0.00091 0.00024 mg/kg SW846 8260D
Isopropylbenzene b 0.0010 J 0.0045 0.00026 mg/kg SW846 8260D
Naphthalene b 0.00086 J 0.0045 0.00052 mg/kg SW846 8260D
n-Propylbenzene b 0.0015 J 0.0045 0.00039 mg/kg SW846 8260D
Toluene b 0.0020 J 0.0045 0.00016 mg/kg SW846 8260D
1,2,4-Trimethylbenzene b 0.00081 J 0.0045 0.00035 mg/kg SW846 8260D
1,3,5-Trimethylbenzene b 0.00031 J 0.0045 0.00023 mg/kg SW846 8260D
1-Methylnaphthalene 0.183 J 1.0 0.10 mg/kg SW846 8270E
2-Methylnaphthalene 0.197 J 1.0 0.10 mg/kg SW846 8270E
Phenanthrene 0.123 J 1.0 0.10 mg/kg SW846 8270E
C9- C10 Aromatics (Unadj.)8.76 5.3 1.8 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics 8.76 5.3 1.8 mg/kg MADEP VPH REV 2.1
2-Methylnaphthalene 0.489 0.24 0.12 mg/kg MADEP EPH REV 2.1
C11-C22 Aromatics (Unadj.)50.0 12 4.8 mg/kg MADEP EPH REV 2.1
C11-C22 Aromatics 49.6 12 4.8 mg/kg MADEP EPH REV 2.1
C9-C18 Aliphatics 33.7 12 3.0 mg/kg MADEP EPH REV 2.1
C19-C36 Aliphatics 19.3 12 3.0 mg/kg MADEP EPH REV 2.1
FA85879-4 CS-3 8'
Methylene Chloride b 6.08 J 16 1.8 mg/kg SW846 8260D
Acenaphthene 0.765 J 1.1 0.11 mg/kg SW846 8270E
Dibenzofuran 0.444 J 1.1 0.11 mg/kg SW846 8270E
Fluorene 1.28 1.1 0.11 mg/kg SW846 8270E
1-Methylnaphthalene 3.29 1.1 0.11 mg/kg SW846 8270E
2-Methylnaphthalene 4.87 1.1 0.11 mg/kg SW846 8270E
Phenanthrene 2.56 1.1 0.11 mg/kg SW846 8270E
Pyrene 0.178 J 1.1 0.12 mg/kg SW846 8270E
Naphthalene 2.09 0.34 0.20 mg/kg MADEP VPH REV 2.1
C5- C8 Aliphatics (Unadj.)2.76 J 6.8 2.4 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics (Unadj.)191 68 24 mg/kg MADEP VPH REV 2.1
C5- C8 Aliphatics 2.76 J 6.8 2.4 mg/kg MADEP VPH REV 2.1
C9- C10 Aromatics 191 68 24 mg/kg MADEP VPH REV 2.1
Acenaphthene 2.41 0.26 0.13 mg/kg MADEP EPH REV 2.1
2-Methylnaphthalene 7.23 0.26 0.13 mg/kg MADEP EPH REV 2.1
Naphthalene 2.82 0.26 0.13 mg/kg MADEP EPH REV 2.1
Phenanthrene 2.53 0.26 0.13 mg/kg MADEP EPH REV 2.1
C11-C22 Aromatics (Unadj.)348 64 26 mg/kg MADEP EPH REV 2.1
C11-C22 Aromatics 334 64 26 mg/kg MADEP EPH REV 2.1
C9-C18 Aliphatics 328 64 16 mg/kg MADEP EPH REV 2.1
C19-C36 Aliphatics 85.3 13 3.2 mg/kg MADEP EPH REV 2.1
(a) Confirmed by reanalysis. Insufficient sample to re-extract.
6 of 81
FA858792
Summary of Hits Page 3 of 3
Job Number:FA85879
Account:GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Collected:05/25/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
(b) Analysis performed at SGS Scott, LA.
7 of 81
FA858792
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
8 of 81
FA858793
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-A
Lab Sample ID:FA85879-1 Date Sampled:05/25/21
Matrix:AQ - Ground Water Date Received:05/26/21
Method:SM 6200B Percent Solids:n/a
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E107087.D 1 05/28/21 12:15 LR n/a n/a VE2475
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
Purgeable Aromatics, Full List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 81
FA8587933.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-A
Lab Sample ID:FA85879-1 Date Sampled:05/25/21
Matrix:AQ - Ground Water Date Received:05/26/21
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F09187.D 1 06/01/21 21:20 WH 06/01/21 07:59 OP85647 S6F346
Run #2
Initial Volume Final Volume
Run #1 1000 ml 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol a ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene a ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene a ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 81
FA8587933.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-A
Lab Sample ID:FA85879-1 Date Sampled:05/25/21
Matrix:AQ - Ground Water Date Received:05/26/21
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate a ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate a ND 5.0 1.0 ug/l
84-74-2 Di-n-butyl Phthalate a ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.0 0.81 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.0 0.71 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 23%14-67%
4165-62-2 Phenol-d5 22%10-50%
118-79-6 2,4,6-Tribromophenol 61%33-118%
4165-60-0 Nitrobenzene-d5 58%42-108%
321-60-8 2-Fluorobiphenyl 50%40-106%
1718-51-0 Terphenyl-d14 70%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
23230-86-6 Propene, 3-tert-butoxy-2-(methoxymethyl)7.40 32 ug/l JN
34256-82-1 Acetamide, 2-chloro-N-(ethoxymethyl)-N-(10.22 20 ug/l JN
54365-78-5 3(2H)-Benzofuranone, 2,6-dimethyl-10.45 11 ug/l JN
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 81
FA8587933.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-A
Lab Sample ID:FA85879-1 Date Sampled:05/25/21
Matrix:AQ - Ground Water Date Received:05/26/21
Method:EPA 625.1 SW846 3510C Percent Solids:n/a
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
ABN Special List
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
51218-45-2 Metolachlor 10.69 200 ug/l JN
12215-40-6 Iron, dicarbonyl(.eta.5-2,4-cyclopentadi 11.10 6.2 ug/l JN
504-20-1 2,5-Heptadien-4-one, 2,6-dimethyl-11.49 26 ug/l JN
21366-63-2 1H-4-Oxabenzo(f)cyclobut(cd)inden-8-ol,12.95 9.6 ug/l JN
Total TIC, Semi-Volatile 304.8 ug/l J
(a) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 81
FA8587933.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:MW-A
Lab Sample ID:FA85879-1 Date Sampled:05/25/21
Matrix:AQ - Ground Water Date Received:05/26/21
Method:MADEP VPH REV 2.1 Percent Solids:n/a
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S6781.D 1 05/30/21 19:11 CG n/a n/a G1S244
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 102%70-130%
460-00-4 BFB 111%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 81
FA8587933.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-A
Lab Sample ID:FA85879-1 Date Sampled:05/25/21
Matrix:AQ - Ground Water Date Received:05/26/21
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a NN033358.D 1 06/02/21 02:37 AF 05/28/21 06:30 OP85606 GNN1613
Run #2 b NN033379.D 1 06/03/21 19:45 AF 06/03/21 10:00 OP85606 GNN1614
Initial Volume Final Volume
Run #1 1000 ml 2.0 ml
Run #2 1000 ml 2.0 ml
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)419 200 80 ug/l
C11-C22 Aromatics 419 200 80 ug/l
C9-C18 Aliphatics c ND 200 50 ug/l
C19-C36 Aliphatics ND 200 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 30% d 14%40-140%
580-13-2 2-Bromonaphthalene 97%51%40-140%
84-15-1 o-Terphenyl 64%33%40-140%
321-60-8 2-Fluorobiphenyl 124%74%40-140%
(a) Confirmed by reanalysis. Insufficient sample to re-extract.
(b) Confirmation run for surrogate recoveries.
(c) Associated BSD recovery outside control limits.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 81
FA8587933.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-A
Lab Sample ID:FA85879-1 Date Sampled:05/25/21
Matrix:AQ - Ground Water Date Received:05/26/21
Method:MADEP EPH REV 2.1 SW846 3510C Percent Solids:n/a
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
MAEPH List
CAS No.Compound Result RL MDL Units Q
(d) Outside control limits. Confirmed by refractionation and reanalysis. Insufficient sample for re-extraction.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 81
FA8587933.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:CS-1 8'
Lab Sample ID:FA85879-2 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8260D Percent Solids:81.8
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2I083764.D 51 06/01/21 18:23 ALA n/a n/a L:V2I2995
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.1 g 5.0 ml 50.0 ul
Run #2
8260 special list
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 280 12 mg/kg
71-43-2 Benzene 1.71 2.8 1.1 mg/kg J
75-27-4 Bromodichloromethane ND 5.5 1.8 mg/kg
75-25-2 Bromoform ND 5.5 4.4 mg/kg
104-51-8 n-Butylbenzene 201 28 1.8 mg/kg
75-15-0 Carbon Disulfide ND 5.5 2.3 mg/kg
56-23-5 Carbon Tetrachloride ND 5.5 2.2 mg/kg
108-90-7 Chlorobenzene ND 5.5 1.4 mg/kg
75-00-3 Chloroethane ND 5.5 1.9 mg/kg
67-66-3 Chloroform ND 5.5 1.5 mg/kg
110-82-7 Cyclohexane ND 5.5 1.9 mg/kg
124-48-1 Dibromochloromethane ND 5.5 1.6 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 28 4.9 mg/kg
106-93-4 1,2-Dibromoethane ND 5.5 3.2 mg/kg
75-71-8 Dichlorodifluoromethane ND 5.5 3.6 mg/kg
541-73-1 m-Dichlorobenzene ND 5.5 1.8 mg/kg
95-50-1 o-Dichlorobenzene ND 5.5 1.1 mg/kg
106-46-7 p-Dichlorobenzene ND 5.5 1.4 mg/kg
75-34-3 1,1-Dichloroethane ND 5.5 1.3 mg/kg
107-06-2 1,2-Dichloroethane ND 5.5 1.2 mg/kg
75-35-4 1,1-Dichloroethylene ND 5.5 2.2 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.5 1.7 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.5 1.1 mg/kg
78-87-5 1,2-Dichloropropane ND 5.5 0.70 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.5 1.3 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.5 1.4 mg/kg
100-41-4 Ethylbenzene 456 5.5 1.4 mg/kg
591-78-6 2-Hexanone ND 69 3.6 mg/kg
98-82-8 Isopropylbenzene 125 28 1.6 mg/kg
79-20-9 Methyl Acetate ND 55 1.8 mg/kg
74-83-9 Methyl Bromide ND 55 8.6 mg/kg
74-87-3 Methyl Chloride ND 28 1.7 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 81
FA8587933.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:CS-1 8'
Lab Sample ID:FA85879-2 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8260D Percent Solids:81.8
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
8260 special list
CAS No.Compound Result RL MDL Units Q
108-87-2 Methylcyclohexane 283 28 7.2 mg/kg
75-09-2 Methylene Chloride ND 28 3.1 mg/kg
78-93-3 Methyl Ethyl Ketone ND 69 4.2 mg/kg
108-10-1 4-Methyl-2-pentanone ND 69 2.8 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.5 0.58 mg/kg
91-20-3 Naphthalene ND 28 3.2 mg/kg
103-65-1 n-Propylbenzene 433 28 2.4 mg/kg
100-42-5 Styrene ND 5.5 0.80 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.5 0.82 mg/kg
127-18-4 Tetrachloroethylene ND 5.5 1.9 mg/kg
108-88-3 Toluene ND 28 1.0 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 28 1.1 mg/kg
71-55-6 1,1,1-Trichloroethane ND 5.5 1.9 mg/kg
79-00-5 1,1,2-Trichloroethane ND 5.5 0.83 mg/kg
79-01-6 Trichloroethylene ND 5.5 2.8 mg/kg
75-69-4 Trichlorofluoromethane ND 5.5 2.0 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 28 2.1 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 28 1.4 mg/kg
75-01-4 Vinyl Chloride ND 5.5 1.5 mg/kg
1330-20-7 Xylene (total)7.41 11 6.4 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 98%59-143%
2037-26-5 Toluene-D8 98%52-159%
460-00-4 4-Bromofluorobenzene 97%38-183%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 81
FA8587933.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:CS-1 8'
Lab Sample ID:FA85879-2 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8270E SW846 3550C Percent Solids:81.8
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F09179.D 5 06/01/21 17:52 WH 06/01/21 08:45 OP85652 S6F346
Run #2 6F09195.D 25 06/02/21 12:09 WH 06/01/21 08:45 OP85652 S6F347
Initial Weight Final Volume
Run #1 29.9 g 1.0 ml
Run #2 29.9 g 1.0 ml
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 5.1 1.0 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 1.0 0.12 mg/kg
95-57-8 2-Chlorophenol ND 1.0 0.13 mg/kg
120-83-2 2,4-Dichlorophenol ND 1.0 0.12 mg/kg
105-67-9 2,4-Dimethylphenol ND 1.0 0.27 mg/kg
51-28-5 2,4-Dinitrophenol ND 5.1 1.0 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 2.0 0.41 mg/kg
95-48-7 2-Methylphenol ND 1.0 0.12 mg/kg
3&4-Methylphenol ND 1.0 0.17 mg/kg
88-75-5 2-Nitrophenol ND 1.0 0.11 mg/kg
100-02-7 4-Nitrophenol ND 5.1 1.0 mg/kg
87-86-5 Pentachlorophenol ND 5.1 1.0 mg/kg
108-95-2 Phenol ND 1.0 0.10 mg/kg
88-06-2 2,4,6-Trichlorophenol b ND 1.0 0.12 mg/kg
83-32-9 Acenaphthene 1.88 1.0 0.11 mg/kg
208-96-8 Acenaphthylene b ND 1.0 0.10 mg/kg
120-12-7 Anthracene 0.686 1.0 0.11 mg/kg J
56-55-3 Benzo(a)anthracene ND 1.0 0.10 mg/kg
50-32-8 Benzo(a)pyrene ND 1.0 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 1.0 0.11 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 1.0 0.11 mg/kg
207-08-9 Benzo(k)fluoranthene ND 1.0 0.13 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 1.0 0.11 mg/kg
85-68-7 Butyl benzyl phthalate ND 1.0 0.20 mg/kg
106-47-8 4-Chloroaniline ND 1.0 0.26 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 1.0 0.10 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 1.0 0.12 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1.0 0.13 mg/kg
91-58-7 2-Chloronaphthalene b ND 1.0 0.10 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 1.0 0.10 mg/kg
218-01-9 Chrysene ND 1.0 0.10 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 1.0 0.13 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 81
FA8587933.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:CS-1 8'
Lab Sample ID:FA85879-2 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8270E SW846 3550C Percent Solids:81.8
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran 1.00 1.0 0.10 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 1.0 0.24 mg/kg
84-66-2 Diethyl Phthalate b ND 2.0 0.20 mg/kg
131-11-3 Dimethyl Phthalate b ND 1.0 0.20 mg/kg
117-84-0 Di-n-octyl Phthalate ND 1.0 0.20 mg/kg
84-74-2 Di-n-butyl Phthalate b ND 2.0 0.41 mg/kg
121-14-2 2,4-Dinitrotoluene ND 1.0 0.10 mg/kg
606-20-2 2,6-Dinitrotoluene ND 1.0 0.13 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate 0.283 2.0 0.20 mg/kg J
206-44-0 Fluoranthene ND 1.0 0.10 mg/kg
86-73-7 Fluorene 2.99 1.0 0.11 mg/kg
118-74-1 Hexachlorobenzene ND 1.0 0.10 mg/kg
87-68-3 Hexachlorobutadiene ND 1.0 0.10 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 1.0 0.20 mg/kg
67-72-1 Hexachloroethane ND 1.0 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 1.0 0.12 mg/kg
78-59-1 Isophorone ND 1.0 0.10 mg/kg
90-12-0 1-Methylnaphthalene 22.4 c 5.1 0.51 mg/kg
91-57-6 2-Methylnaphthalene 36.0 c 5.1 0.51 mg/kg
91-20-3 Naphthalene ND 1.0 0.10 mg/kg
98-95-3 Nitrobenzene ND 1.0 0.10 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 1.0 0.10 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 1.0 0.11 mg/kg
85-01-8 Phenanthrene 5.22 1.0 0.10 mg/kg
129-00-0 Pyrene 0.485 1.0 0.12 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 53%48%40-102%
4165-62-2 Phenol-d5 61%58%41-100%
118-79-6 2,4,6-Tribromophenol 60%54%42-108%
4165-60-0 Nitrobenzene-d5 73%65%40-105%
321-60-8 2-Fluorobiphenyl 60%56%43-107%
1718-51-0 Terphenyl-d14 70%67%45-119%
(a) Associated BS recovery outside control limits.
(b) Associated CCV outside of control limits low.
(c) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 81
FA8587933.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:CS-1 8'
Lab Sample ID:FA85879-2 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:MADEP VPH REV 2.1 Percent Solids:81.8
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S6879.D 1 06/08/21 10:46 CG n/a n/a G1S250
Run #2 1S6901.D 1 06/09/21 11:02 CG n/a n/a G1S251
Initial Weight Final Volume Methanol Aliquot
Run #1 5.94 g 5.0 ml 10.0 ul
Run #2 5.94 g 5.0 ml 2.5 ul
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 1.44 0.63 0.63 mg/kg
100-41-4 Ethylbenzene 16.1 1.3 0.63 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 1.3 0.63 mg/kg
91-20-3 Naphthalene 3.83 3.1 1.9 mg/kg
108-88-3 Toluene ND 1.3 0.63 mg/kg
m,p-Xylene ND 2.5 1.3 mg/kg
95-47-6 o-Xylene ND 1.3 0.63 mg/kg
C5- C8 Aliphatics (Unadj.)339 63 22 mg/kg
C9- C12 Aliphatics (Unadj.)ND 63 22 mg/kg
C9- C10 Aromatics (Unadj.)488 a 250 88 mg/kg
C5- C8 Aliphatics 338 63 22 mg/kg
C9- C12 Aliphatics ND 63 22 mg/kg
C9- C10 Aromatics 488 a 250 88 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 107%0% b 70-130%
460-00-4 BFB 103%0% b 70-130%
(a) Result is from Run# 2
(b) Outside control limits due to dilution.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 81
FA8587933.2
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:CS-1 8'
Lab Sample ID:FA85879-2 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:81.8
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN033416.D 5 06/04/21 14:46 AF 06/01/21 14:05 OP85654 GNN1614
Run #2
Initial Weight Final Volume
Run #1 20.0 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene 4.05 1.2 0.61 mg/kg
208-96-8 Acenaphthylene ND 1.2 0.61 mg/kg
120-12-7 Anthracene ND 1.2 0.61 mg/kg
56-55-3 Benzo(a)anthracene ND 1.2 0.61 mg/kg
50-32-8 Benzo(a)pyrene ND 1.2 0.61 mg/kg
205-99-2 Benzo(b)fluoranthene ND 1.2 0.61 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 1.2 0.61 mg/kg
207-08-9 Benzo(k)fluoranthene ND 1.2 0.61 mg/kg
218-01-9 Chrysene ND 1.2 0.61 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 1.2 0.61 mg/kg
206-44-0 Fluoranthene ND 1.2 0.61 mg/kg
86-73-7 Fluorene ND 1.2 0.61 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 1.2 0.61 mg/kg
91-57-6 2-Methylnaphthalene 17.4 1.2 0.61 mg/kg
91-20-3 Naphthalene 7.48 1.2 0.61 mg/kg
85-01-8 Phenanthrene 2.49 1.2 0.61 mg/kg
129-00-0 Pyrene ND 1.2 0.61 mg/kg
C11-C22 Aromatics (Unadj.)615 61 24 mg/kg
C11-C22 Aromatics 584 61 24 mg/kg
C9-C18 Aliphatics 566 61 15 mg/kg
C19-C36 Aliphatics 142 61 15 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 79%40-140%
580-13-2 2-Bromonaphthalene 108%40-140%
84-15-1 o-Terphenyl 70%40-140%
321-60-8 2-Fluorobiphenyl 106%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 81
FA8587933.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:CS-2 8'
Lab Sample ID:FA85879-3 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8260D Percent Solids:83.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2H0072819.D 1 06/02/21 02:28 ALA n/a n/a L:V2H2825
Run #2
Initial Weight
Run #1 6.6 g
Run #2
8260 special list
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone 0.0272 0.045 0.0020 mg/kg J
71-43-2 Benzene 0.00022 0.00045 0.00018 mg/kg J
75-27-4 Bromodichloromethane ND 0.00091 0.00029 mg/kg
75-25-2 Bromoform ND 0.00091 0.00073 mg/kg
104-51-8 n-Butylbenzene 0.0012 0.0045 0.00029 mg/kg J
75-15-0 Carbon Disulfide 0.0011 0.00091 0.00038 mg/kg
56-23-5 Carbon Tetrachloride ND 0.00091 0.00036 mg/kg
108-90-7 Chlorobenzene ND 0.00091 0.00022 mg/kg
75-00-3 Chloroethane ND 0.00091 0.00031 mg/kg
67-66-3 Chloroform ND 0.00091 0.00024 mg/kg
110-82-7 Cyclohexane 0.0019 0.00091 0.00032 mg/kg
124-48-1 Dibromochloromethane ND 0.00091 0.00026 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 0.0045 0.00081 mg/kg
106-93-4 1,2-Dibromoethane ND 0.00091 0.00052 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.00091 0.00059 mg/kg
541-73-1 m-Dichlorobenzene ND 0.00091 0.00029 mg/kg
95-50-1 o-Dichlorobenzene ND 0.00091 0.00018 mg/kg
106-46-7 p-Dichlorobenzene ND 0.00091 0.00024 mg/kg
75-34-3 1,1-Dichloroethane ND 0.00091 0.00021 mg/kg
107-06-2 1,2-Dichloroethane ND 0.00091 0.00020 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.00091 0.00037 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.00091 0.00029 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.00091 0.00019 mg/kg
78-87-5 1,2-Dichloropropane ND 0.00091 0.00012 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.00091 0.00022 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 0.00091 0.00024 mg/kg
100-41-4 Ethylbenzene 0.00068 0.00091 0.00024 mg/kg J
591-78-6 2-Hexanone ND 0.011 0.00060 mg/kg
98-82-8 Isopropylbenzene 0.0010 0.0045 0.00026 mg/kg J
79-20-9 Methyl Acetate ND 0.0091 0.00030 mg/kg
74-83-9 Methyl Bromide ND 0.0091 0.0014 mg/kg
74-87-3 Methyl Chloride ND 0.0045 0.00027 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 81
FA8587933.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:CS-2 8'
Lab Sample ID:FA85879-3 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8260D Percent Solids:83.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
8260 special list
CAS No.Compound Result RL MDL Units Q
108-87-2 Methylcyclohexane ND 0.0045 0.0012 mg/kg
75-09-2 Methylene Chloride ND 0.0045 0.00051 mg/kg
78-93-3 Methyl Ethyl Ketone ND 0.011 0.00070 mg/kg
108-10-1 4-Methyl-2-pentanone ND 0.011 0.00047 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.00091 0.000095mg/kg
91-20-3 Naphthalene 0.00086 0.0045 0.00052 mg/kg J
103-65-1 n-Propylbenzene 0.0015 0.0045 0.00039 mg/kg J
100-42-5 Styrene ND 0.00091 0.00013 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.00091 0.00014 mg/kg
127-18-4 Tetrachloroethylene ND 0.00091 0.00031 mg/kg
108-88-3 Toluene 0.0020 0.0045 0.00016 mg/kg J
120-82-1 1,2,4-Trichlorobenzene ND 0.0045 0.00019 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.00091 0.00032 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.00091 0.00014 mg/kg
79-01-6 Trichloroethylene ND 0.00091 0.00045 mg/kg
75-69-4 Trichlorofluoromethane ND 0.00091 0.00033 mg/kg
95-63-6 1,2,4-Trimethylbenzene 0.00081 0.0045 0.00035 mg/kg J
108-67-8 1,3,5-Trimethylbenzene 0.00031 0.0045 0.00023 mg/kg J
75-01-4 Vinyl Chloride ND 0.00091 0.00024 mg/kg
1330-20-7 Xylene (total)ND 0.0018 0.0011 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 105%59-143%
2037-26-5 Toluene-D8 103%52-159%
460-00-4 4-Bromofluorobenzene 106%38-183%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 81
FA8587933.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:CS-2 8'
Lab Sample ID:FA85879-3 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8270E SW846 3550C Percent Solids:83.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F09180.D 5 06/01/21 18:18 WH 06/01/21 08:45 OP85652 S6F346
Run #2 a 6F09196.D 5 06/02/21 12:34 WH 06/01/21 08:45 OP85652 S6F347
Initial Weight Final Volume
Run #1 29.9 g 1.0 ml
Run #2 29.9 g 1.0 ml
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid b ND 5.0 1.0 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 1.0 0.11 mg/kg
95-57-8 2-Chlorophenol ND 1.0 0.12 mg/kg
120-83-2 2,4-Dichlorophenol ND 1.0 0.12 mg/kg
105-67-9 2,4-Dimethylphenol ND 1.0 0.27 mg/kg
51-28-5 2,4-Dinitrophenol ND 5.0 1.0 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 2.0 0.40 mg/kg
95-48-7 2-Methylphenol ND 1.0 0.12 mg/kg
3&4-Methylphenol ND 1.0 0.17 mg/kg
88-75-5 2-Nitrophenol ND 1.0 0.11 mg/kg
100-02-7 4-Nitrophenol ND 5.0 1.0 mg/kg
87-86-5 Pentachlorophenol ND 5.0 1.0 mg/kg
108-95-2 Phenol ND 1.0 0.10 mg/kg
88-06-2 2,4,6-Trichlorophenol c ND 1.0 0.12 mg/kg
83-32-9 Acenaphthene ND 1.0 0.11 mg/kg
208-96-8 Acenaphthylene c ND 1.0 0.10 mg/kg
120-12-7 Anthracene ND 1.0 0.11 mg/kg
56-55-3 Benzo(a)anthracene ND 1.0 0.10 mg/kg
50-32-8 Benzo(a)pyrene ND 1.0 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 1.0 0.11 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 1.0 0.10 mg/kg
207-08-9 Benzo(k)fluoranthene ND 1.0 0.13 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 1.0 0.10 mg/kg
85-68-7 Butyl benzyl phthalate ND 1.0 0.20 mg/kg
106-47-8 4-Chloroaniline ND 1.0 0.25 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 1.0 0.10 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 1.0 0.12 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1.0 0.13 mg/kg
91-58-7 2-Chloronaphthalene c ND 1.0 0.10 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 1.0 0.10 mg/kg
218-01-9 Chrysene ND 1.0 0.10 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 1.0 0.13 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 81
FA8587933.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:CS-2 8'
Lab Sample ID:FA85879-3 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8270E SW846 3550C Percent Solids:83.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran ND 1.0 0.10 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 1.0 0.24 mg/kg
84-66-2 Diethyl Phthalate c ND 2.0 0.20 mg/kg
131-11-3 Dimethyl Phthalate c ND 1.0 0.20 mg/kg
117-84-0 Di-n-octyl Phthalate ND 1.0 0.20 mg/kg
84-74-2 Di-n-butyl Phthalate c ND 2.0 0.40 mg/kg
121-14-2 2,4-Dinitrotoluene ND 1.0 0.10 mg/kg
606-20-2 2,6-Dinitrotoluene ND 1.0 0.13 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 2.0 0.20 mg/kg
206-44-0 Fluoranthene ND 1.0 0.10 mg/kg
86-73-7 Fluorene ND 1.0 0.11 mg/kg
118-74-1 Hexachlorobenzene ND 1.0 0.10 mg/kg
87-68-3 Hexachlorobutadiene ND 1.0 0.10 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 1.0 0.20 mg/kg
67-72-1 Hexachloroethane ND 1.0 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 1.0 0.12 mg/kg
78-59-1 Isophorone ND 1.0 0.10 mg/kg
90-12-0 1-Methylnaphthalene 0.183 1.0 0.10 mg/kg J
91-57-6 2-Methylnaphthalene 0.197 1.0 0.10 mg/kg J
91-20-3 Naphthalene ND 1.0 0.10 mg/kg
98-95-3 Nitrobenzene ND 1.0 0.10 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 1.0 0.10 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 1.0 0.11 mg/kg
85-01-8 Phenanthrene 0.123 1.0 0.10 mg/kg J
129-00-0 Pyrene ND 1.0 0.12 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%63%40-102%
4165-62-2 Phenol-d5 67%72%41-100%
118-79-6 2,4,6-Tribromophenol 55%61%42-108%
4165-60-0 Nitrobenzene-d5 62%60%40-105%
321-60-8 2-Fluorobiphenyl 55%55%43-107%
1718-51-0 Terphenyl-d14 67%68%45-119%
(a) Confirmation run.
(b) Associated BS recovery outside control limits.
(c) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 81
FA8587933.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:CS-2 8'
Lab Sample ID:FA85879-3 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:MADEP VPH REV 2.1 Percent Solids:83.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S6884.D 1 06/08/21 13:07 CG n/a n/a G1S250
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 7.03 g 5.0 ml 100 ul
Run #2
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.053 0.053 mg/kg
100-41-4 Ethylbenzene ND 0.11 0.053 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.11 0.053 mg/kg
91-20-3 Naphthalene ND 0.26 0.16 mg/kg
108-88-3 Toluene ND 0.11 0.053 mg/kg
m,p-Xylene ND 0.21 0.11 mg/kg
95-47-6 o-Xylene ND 0.11 0.053 mg/kg
C5- C8 Aliphatics (Unadj.)ND 5.3 1.8 mg/kg
C9- C12 Aliphatics (Unadj.)ND 5.3 1.8 mg/kg
C9- C10 Aromatics (Unadj.)8.76 5.3 1.8 mg/kg
C5- C8 Aliphatics ND 5.3 1.8 mg/kg
C9- C12 Aliphatics ND 5.3 1.8 mg/kg
C9- C10 Aromatics 8.76 5.3 1.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 76%70-130%
460-00-4 BFB 74%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 81
FA8587933.3
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:CS-2 8'
Lab Sample ID:FA85879-3 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:83.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN033410.D 1 06/04/21 11:02 AF 06/01/21 14:05 OP85654 GNN1614
Run #2
Initial Weight Final Volume
Run #1 20.2 g 2.0 ml
Run #2
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 0.24 0.12 mg/kg
208-96-8 Acenaphthylene ND 0.24 0.12 mg/kg
120-12-7 Anthracene ND 0.24 0.12 mg/kg
56-55-3 Benzo(a)anthracene ND 0.24 0.12 mg/kg
50-32-8 Benzo(a)pyrene ND 0.24 0.12 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.24 0.12 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.24 0.12 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.24 0.12 mg/kg
218-01-9 Chrysene ND 0.24 0.12 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.24 0.12 mg/kg
206-44-0 Fluoranthene ND 0.24 0.12 mg/kg
86-73-7 Fluorene ND 0.24 0.12 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.24 0.12 mg/kg
91-57-6 2-Methylnaphthalene 0.489 0.24 0.12 mg/kg
91-20-3 Naphthalene ND 0.24 0.12 mg/kg
85-01-8 Phenanthrene ND 0.24 0.12 mg/kg
129-00-0 Pyrene ND 0.24 0.12 mg/kg
C11-C22 Aromatics (Unadj.)50.0 12 4.8 mg/kg
C11-C22 Aromatics 49.6 12 4.8 mg/kg
C9-C18 Aliphatics 33.7 12 3.0 mg/kg
C19-C36 Aliphatics 19.3 12 3.0 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 75%40-140%
580-13-2 2-Bromonaphthalene 101%40-140%
84-15-1 o-Terphenyl 91%40-140%
321-60-8 2-Fluorobiphenyl 125%40-140%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 81
FA8587933.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:CS-3 8'
Lab Sample ID:FA85879-4 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8260D Percent Solids:77.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 2I083762.D 51 06/01/21 17:57 ALA n/a n/a L:V2I2995
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 6.5 g 5.0 ml 100 ul
Run #2
8260 special list
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 160 7.3 mg/kg
71-43-2 Benzene ND 1.6 0.65 mg/kg
75-27-4 Bromodichloromethane ND 3.3 1.0 mg/kg
75-25-2 Bromoform ND 3.3 2.6 mg/kg
104-51-8 n-Butylbenzene ND 16 1.1 mg/kg
75-15-0 Carbon Disulfide ND 3.3 1.4 mg/kg
56-23-5 Carbon Tetrachloride ND 3.3 1.3 mg/kg
108-90-7 Chlorobenzene ND 3.3 0.81 mg/kg
75-00-3 Chloroethane ND 3.3 1.1 mg/kg
67-66-3 Chloroform ND 3.3 0.86 mg/kg
110-82-7 Cyclohexane ND 3.3 1.1 mg/kg
124-48-1 Dibromochloromethane ND 3.3 0.95 mg/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 16 2.9 mg/kg
106-93-4 1,2-Dibromoethane ND 3.3 1.9 mg/kg
75-71-8 Dichlorodifluoromethane ND 3.3 2.1 mg/kg
541-73-1 m-Dichlorobenzene ND 3.3 1.0 mg/kg
95-50-1 o-Dichlorobenzene ND 3.3 0.64 mg/kg
106-46-7 p-Dichlorobenzene ND 3.3 0.85 mg/kg
75-34-3 1,1-Dichloroethane ND 3.3 0.75 mg/kg
107-06-2 1,2-Dichloroethane ND 3.3 0.71 mg/kg
75-35-4 1,1-Dichloroethylene ND 3.3 1.3 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 3.3 1.0 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 3.3 0.67 mg/kg
78-87-5 1,2-Dichloropropane ND 3.3 0.42 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 3.3 0.78 mg/kg
10061-02-6 trans-1,3-Dichloropropene ND 3.3 0.86 mg/kg
100-41-4 Ethylbenzene ND 3.3 0.85 mg/kg
591-78-6 2-Hexanone ND 41 2.2 mg/kg
98-82-8 Isopropylbenzene ND 16 0.93 mg/kg
79-20-9 Methyl Acetate ND 33 1.1 mg/kg
74-83-9 Methyl Bromide ND 33 5.1 mg/kg
74-87-3 Methyl Chloride ND 16 0.98 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 81
FA8587933.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:CS-3 8'
Lab Sample ID:FA85879-4 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8260D Percent Solids:77.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
8260 special list
CAS No.Compound Result RL MDL Units Q
108-87-2 Methylcyclohexane ND 16 4.3 mg/kg
75-09-2 Methylene Chloride 6.08 16 1.8 mg/kg J
78-93-3 Methyl Ethyl Ketone ND 41 2.5 mg/kg
108-10-1 4-Methyl-2-pentanone ND 41 1.7 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 3.3 0.34 mg/kg
91-20-3 Naphthalene ND 16 1.9 mg/kg
103-65-1 n-Propylbenzene ND 16 1.4 mg/kg
100-42-5 Styrene ND 3.3 0.48 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 3.3 0.49 mg/kg
127-18-4 Tetrachloroethylene ND 3.3 1.1 mg/kg
108-88-3 Toluene ND 16 0.59 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 16 0.68 mg/kg
71-55-6 1,1,1-Trichloroethane ND 3.3 1.2 mg/kg
79-00-5 1,1,2-Trichloroethane ND 3.3 0.50 mg/kg
79-01-6 Trichloroethylene ND 3.3 1.6 mg/kg
75-69-4 Trichlorofluoromethane ND 3.3 1.2 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 16 1.2 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 16 0.83 mg/kg
75-01-4 Vinyl Chloride ND 3.3 0.86 mg/kg
1330-20-7 Xylene (total)ND 6.6 3.8 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 100%59-143%
2037-26-5 Toluene-D8 100%52-159%
460-00-4 4-Bromofluorobenzene 103%38-183%
(a) Analysis performed at SGS Scott, LA.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 81
FA8587933.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:CS-3 8'
Lab Sample ID:FA85879-4 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8270E SW846 3550C Percent Solids:77.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 6F09181.D 5 06/01/21 18:44 WH 06/01/21 08:45 OP85652 S6F346
Run #2
Initial Weight Final Volume
Run #1 30.4 g 1.0 ml
Run #2
ABN Special List
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 5.3 1.1 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 1.1 0.12 mg/kg
95-57-8 2-Chlorophenol ND 1.1 0.13 mg/kg
120-83-2 2,4-Dichlorophenol ND 1.1 0.12 mg/kg
105-67-9 2,4-Dimethylphenol ND 1.1 0.28 mg/kg
51-28-5 2,4-Dinitrophenol ND 5.3 1.1 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 2.1 0.43 mg/kg
95-48-7 2-Methylphenol ND 1.1 0.13 mg/kg
3&4-Methylphenol ND 1.1 0.18 mg/kg
88-75-5 2-Nitrophenol ND 1.1 0.12 mg/kg
100-02-7 4-Nitrophenol ND 5.3 1.1 mg/kg
87-86-5 Pentachlorophenol ND 5.3 1.1 mg/kg
108-95-2 Phenol ND 1.1 0.11 mg/kg
88-06-2 2,4,6-Trichlorophenol b ND 1.1 0.12 mg/kg
83-32-9 Acenaphthene 0.765 1.1 0.11 mg/kg J
208-96-8 Acenaphthylene b ND 1.1 0.11 mg/kg
120-12-7 Anthracene ND 1.1 0.12 mg/kg
56-55-3 Benzo(a)anthracene ND 1.1 0.11 mg/kg
50-32-8 Benzo(a)pyrene ND 1.1 0.13 mg/kg
205-99-2 Benzo(b)fluoranthene ND 1.1 0.12 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 1.1 0.11 mg/kg
207-08-9 Benzo(k)fluoranthene ND 1.1 0.14 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 1.1 0.11 mg/kg
85-68-7 Butyl benzyl phthalate ND 1.1 0.21 mg/kg
106-47-8 4-Chloroaniline ND 1.1 0.27 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 1.1 0.11 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 1.1 0.12 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1.1 0.13 mg/kg
91-58-7 2-Chloronaphthalene b ND 1.1 0.11 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 1.1 0.11 mg/kg
218-01-9 Chrysene ND 1.1 0.11 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 1.1 0.13 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 81
FA8587933.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:CS-3 8'
Lab Sample ID:FA85879-4 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:SW846 8270E SW846 3550C Percent Solids:77.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
ABN Special List
CAS No.Compound Result RL MDL Units Q
132-64-9 Dibenzofuran 0.444 1.1 0.11 mg/kg J
91-94-1 3,3'-Dichlorobenzidine ND 1.1 0.25 mg/kg
84-66-2 Diethyl Phthalate b ND 2.1 0.21 mg/kg
131-11-3 Dimethyl Phthalate b ND 1.1 0.21 mg/kg
117-84-0 Di-n-octyl Phthalate ND 1.1 0.21 mg/kg
84-74-2 Di-n-butyl Phthalate b ND 2.1 0.43 mg/kg
121-14-2 2,4-Dinitrotoluene ND 1.1 0.11 mg/kg
606-20-2 2,6-Dinitrotoluene ND 1.1 0.14 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 2.1 0.21 mg/kg
206-44-0 Fluoranthene ND 1.1 0.11 mg/kg
86-73-7 Fluorene 1.28 1.1 0.11 mg/kg
118-74-1 Hexachlorobenzene ND 1.1 0.11 mg/kg
87-68-3 Hexachlorobutadiene ND 1.1 0.11 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 1.1 0.21 mg/kg
67-72-1 Hexachloroethane ND 1.1 0.13 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 1.1 0.13 mg/kg
78-59-1 Isophorone ND 1.1 0.11 mg/kg
90-12-0 1-Methylnaphthalene 3.29 1.1 0.11 mg/kg
91-57-6 2-Methylnaphthalene 4.87 1.1 0.11 mg/kg
91-20-3 Naphthalene ND 1.1 0.11 mg/kg
98-95-3 Nitrobenzene ND 1.1 0.11 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 1.1 0.11 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 1.1 0.11 mg/kg
85-01-8 Phenanthrene 2.56 1.1 0.11 mg/kg
129-00-0 Pyrene 0.178 1.1 0.12 mg/kg J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 56%40-102%
4165-62-2 Phenol-d5 60%41-100%
118-79-6 2,4,6-Tribromophenol 55%42-108%
4165-60-0 Nitrobenzene-d5 66%40-105%
321-60-8 2-Fluorobiphenyl 57%43-107%
1718-51-0 Terphenyl-d14 65%45-119%
(a) Associated BS recovery outside control limits.
(b) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 81
FA8587933.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:CS-3 8'
Lab Sample ID:FA85879-4 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:MADEP VPH REV 2.1 Percent Solids:77.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 1S6890.D 1 06/08/21 15:59 CG n/a n/a G1S250
Run #2 1S6881.D 1 06/08/21 11:43 CG n/a n/a G1S250
Initial Weight Final Volume Methanol Aliquot
Run #1 6.03 g 5.0 ml 100 ul
Run #2 6.03 g 5.0 ml 10.0 ul
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.068 0.068 mg/kg
100-41-4 Ethylbenzene ND 0.14 0.068 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.14 0.068 mg/kg
91-20-3 Naphthalene 2.09 0.34 0.20 mg/kg
108-88-3 Toluene ND 0.14 0.068 mg/kg
m,p-Xylene ND 0.27 0.14 mg/kg
95-47-6 o-Xylene ND 0.14 0.068 mg/kg
C5- C8 Aliphatics (Unadj.)2.76 6.8 2.4 mg/kg J
C9- C12 Aliphatics (Unadj.)ND 6.8 2.4 mg/kg
C9- C10 Aromatics (Unadj.)191 a 68 24 mg/kg
C5- C8 Aliphatics 2.76 6.8 2.4 mg/kg J
C9- C12 Aliphatics ND 6.8 2.4 mg/kg
C9- C10 Aromatics 191 a 68 24 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 BFB 101%127%70-130%
460-00-4 BFB 87%95%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 81
FA8587933.4
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:CS-3 8'
Lab Sample ID:FA85879-4 Date Sampled:05/25/21
Matrix:SO - Soil Date Received:05/26/21
Method:MADEP EPH REV 2.1 SW846 3546 Percent Solids:77.3
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN033411.D 1 06/04/21 11:32 AF 06/01/21 14:05 OP85654 GNN1614
Run #2 NN033417.D 5 06/04/21 15:16 AF 06/01/21 14:05 OP85654 GNN1614
Initial Weight Final Volume
Run #1 20.1 g 2.0 ml
Run #2 20.1 g 2.0 ml
MAEPH List
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene 2.41 0.26 0.13 mg/kg
208-96-8 Acenaphthylene ND 0.26 0.13 mg/kg
120-12-7 Anthracene ND 0.26 0.13 mg/kg
56-55-3 Benzo(a)anthracene ND 0.26 0.13 mg/kg
50-32-8 Benzo(a)pyrene ND 0.26 0.13 mg/kg
205-99-2 Benzo(b)fluoranthene ND 0.26 0.13 mg/kg
191-24-2 Benzo(g,h,i)perylene ND 0.26 0.13 mg/kg
207-08-9 Benzo(k)fluoranthene ND 0.26 0.13 mg/kg
218-01-9 Chrysene ND 0.26 0.13 mg/kg
53-70-3 Dibenzo(a,h)anthracene ND 0.26 0.13 mg/kg
206-44-0 Fluoranthene ND 0.26 0.13 mg/kg
86-73-7 Fluorene ND 0.26 0.13 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 0.26 0.13 mg/kg
91-57-6 2-Methylnaphthalene 7.23 0.26 0.13 mg/kg
91-20-3 Naphthalene 2.82 0.26 0.13 mg/kg
85-01-8 Phenanthrene 2.53 0.26 0.13 mg/kg
129-00-0 Pyrene ND 0.26 0.13 mg/kg
C11-C22 Aromatics (Unadj.)348 a 64 26 mg/kg
C11-C22 Aromatics 334 a 64 26 mg/kg
C9-C18 Aliphatics 328 a 64 16 mg/kg
C19-C36 Aliphatics 85.3 13 3.2 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
3386-33-2 1-Chlorooctadecane 79%75%40-140%
580-13-2 2-Bromonaphthalene 116%129%40-140%
84-15-1 o-Terphenyl 84%80%40-140%
321-60-8 2-Fluorobiphenyl 200% b 114%40-140%
(a) Result is from Run# 2
(b) Outside control limits due to matrix interference.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 81
FA8587933.4
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
34 of 81
FA858794
FA85879: Chain of Custody
Page 1 of 2
35 of 81
FA8587944.1
Job Number:FA85879 Client:GRI
Date / Time Received:5/26/2021 10:30:00 AM Delivery Method:FX
Project:FEREBEE FARMING INC.
Airbill #'s:8033 2260 1636
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments FROZEN @1200
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.6);
Cooler 1: (1.8);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:-1.8; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH Date:Date:5/26/2021 10:30:00 A
FA85879: Chain of Custody
Page 2 of 2
36 of 81
FA8587944.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
37 of 81
FA858795
Method Blank Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2475-MB E107085.D 1 05/28/21 LR n/a n/a VE2475
The QC reported here applies to the following samples:Method: SM 6200B
FA85879-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 104%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
38 of 81
FA8587955.1.1
Blank Spike Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2475-BS E107083.D 1 05/28/21 LR n/a n/a VE2475
The QC reported here applies to the following samples:Method: SM 6200B
FA85879-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.0 100 70-130
108-90-7 Chlorobenzene 10 9.1 91 70-130
95-50-1 1,2-Dichlorobenzene 10 9.3 93 70-130
541-73-1 1,3-Dichlorobenzene 10 9.2 92 70-130
106-46-7 1,4-Dichlorobenzene 10 8.8 88 70-130
108-20-3 Di-Isopropyl Ether 10 8.3 83 70-130
100-41-4 Ethylbenzene 10 9.0 90 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.4 94 70-130
91-20-3 Naphthalene 10 8.0 80 70-130
108-88-3 Toluene 10 9.1 91 70-130
1330-20-7 Xylene (total)30 25.1 84 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
* = Outside of Control Limits.
39 of 81
FA8587955.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA85836-3MS E107095.D 10 05/28/21 LR n/a n/a VE2475
FA85836-3MSD E107096.D 10 05/28/21 LR n/a n/a VE2475
FA85836-3 E107094.D 10 05/28/21 LR n/a n/a VE2475
The QC reported here applies to the following samples:Method: SM 6200B
FA85879-1
FA85836-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 100 99.5 100 100 97.4 97 2 70-130/20
108-90-7 Chlorobenzene ND 100 90.8 91 100 89.3 89 2 70-130/20
95-50-1 1,2-Dichlorobenzene ND 100 94.4 94 100 94.3 94 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 93.3 93 100 91.6 92 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 88.3 88 100 86.6 87 2 70-130/20
108-20-3 Di-Isopropyl Ether ND 100 81.6 82 100 80.2 80 2 70-130/20
100-41-4 Ethylbenzene 45.6 100 141 95 100 138 92 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 100 92.2 92 100 92.3 92 0 70-130/20
91-20-3 Naphthalene 401 100 485 84 100 473 72 3 70-130/20
108-88-3 Toluene 5.6 100 95.8 90 100 93.4 88 3 70-130/20
1330-20-7 Xylene (total)1110 300 1380 90 300 1330 73 4 70-130/20
CAS No.Surrogate Recoveries MS MSD FA85836-3 Limits
1868-53-7 Dibromofluoromethane 102%102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%102%102%70-130%
2037-26-5 Toluene-D8 95%96%95%70-130%
460-00-4 4-Bromofluorobenzene 100%98%96%70-130%
* = Outside of Control Limits.
40 of 81
FA8587955.3.1
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
41 of 81
FA858796
Method Blank Summary Page 1 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85647-MB 6F09186.D 1 06/01/21 WH 06/01/21 OP85647 S6F346
The QC reported here applies to the following samples:Method: EPA 625.1
FA85879-1
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
42 of 81
FA8587966.1.1
Method Blank Summary Page 2 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85647-MB 6F09186.D 1 06/01/21 WH 06/01/21 OP85647 S6F346
The QC reported here applies to the following samples:Method: EPA 625.1
FA85879-1
CAS No.Compound Result RL MDL Units Q
84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
121-14-2 2,4-Dinitrotoluene ND 5.0 0.81 ug/l
606-20-2 2,6-Dinitrotoluene ND 5.0 0.71 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 36%14-67%
4165-62-2 Phenol-d5 28%10-50%
118-79-6 2,4,6-Tribromophenol 67%33-118%
4165-60-0 Nitrobenzene-d5 72%42-108%
321-60-8 2-Fluorobiphenyl 59%40-106%
1718-51-0 Terphenyl-d14 90%39-121%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Semi-Volatile 0 ug/l
43 of 81
FA8587966.1.1
Method Blank Summary Page 1 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85652-MB 6F09178.D 1 06/01/21 WH 06/01/21 OP85652 S6F346
The QC reported here applies to the following samples:Method: SW846 8270E
FA85879-2, FA85879-3, FA85879-4
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg
95-57-8 2-Chlorophenol ND 170 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 20 ug/kg
3&4-Methylphenol ND 170 27 ug/kg
88-75-5 2-Nitrophenol ND 170 18 ug/kg
100-02-7 4-Nitrophenol ND 830 170 ug/kg
87-86-5 Pentachlorophenol ND 830 170 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg
83-32-9 Acenaphthene ND 170 18 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
120-12-7 Anthracene ND 170 19 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 42 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 21 ug/kg
91-58-7 2-Chloronaphthalene ND 170 17 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
44 of 81
FA8587966.1.2
Method Blank Summary Page 2 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85652-MB 6F09178.D 1 06/01/21 WH 06/01/21 OP85652 S6F346
The QC reported here applies to the following samples:Method: SW846 8270E
FA85879-2, FA85879-3, FA85879-4
CAS No.Compound Result RL MDL Units Q
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
121-14-2 2,4-Dinitrotoluene ND 170 17 ug/kg
606-20-2 2,6-Dinitrotoluene ND 170 21 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 18 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 20 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 19 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 59%40-102%
4165-62-2 Phenol-d5 65%41-100%
118-79-6 2,4,6-Tribromophenol 54%42-108%
4165-60-0 Nitrobenzene-d5 62%40-105%
321-60-8 2-Fluorobiphenyl 53%43-107%
1718-51-0 Terphenyl-d14 64%45-119%
45 of 81
FA8587966.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85647-BS 6F09185.D 1 06/01/21 WH 06/01/21 OP85647 S6F346
The QC reported here applies to the following samples:Method: EPA 625.1
FA85879-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
65-85-0 Benzoic Acid 100 28.5 29 10-69
59-50-7 4-Chloro-3-methyl Phenol 50 35.5 71 54-103
95-57-8 2-Chlorophenol 50 36.7 73 52-98
120-83-2 2,4-Dichlorophenol 50 36.5 73 53-103
105-67-9 2,4-Dimethylphenol 50 36.8 74 43-90
51-28-5 2,4-Dinitrophenol 100 60.0 60 44-112
534-52-1 4,6-Dinitro-o-cresol 100 82.4 82 66-121
95-48-7 2-Methylphenol 50 32.2 64 43-90
3&4-Methylphenol 100 59.5 60 36-88
88-75-5 2-Nitrophenol 50 38.4 77 53-102
100-02-7 4-Nitrophenol 100 28.8 29 18-62
87-86-5 Pentachlorophenol 100 78.5 79 61-115
108-95-2 Phenol 50 17.6 35 19-56
88-06-2 2,4,6-Trichlorophenol 50 37.0 74 59-107
83-32-9 Acenaphthene 50 38.0 76 61-107
208-96-8 Acenaphthylene 50 35.6 71 60-104
120-12-7 Anthracene 50 39.8 80 65-108
56-55-3 Benzo(a)anthracene 50 42.5 85 66-111
50-32-8 Benzo(a)pyrene 50 44.9 90 62-107
205-99-2 Benzo(b)fluoranthene 50 42.6 85 65-114
191-24-2 Benzo(g,h,i)perylene 50 42.5 85 66-116
207-08-9 Benzo(k)fluoranthene 50 44.3 89 65-114
101-55-3 4-Bromophenyl Phenyl Ether 50 42.9 86 65-109
85-68-7 Butyl Benzyl Phthalate 50 43.7 87 65-112
106-47-8 4-Chloroaniline 50 64.7 129*49-105
111-91-1 bis(2-Chloroethoxy)methane 50 37.3 75 51-102
111-44-4 bis(2-Chloroethyl)ether 50 35.4 71 53-100
108-60-1 2,2'-Oxybis(1-chloropropane)50 37.5 75 45-106
91-58-7 2-Chloronaphthalene 50 34.6 69 57-103
7005-72-3 4-Chlorophenyl Phenyl Ether 50 38.9 78 62-105
218-01-9 Chrysene 50 42.5 85 66-111
53-70-3 Dibenzo(a,h)anthracene 50 43.1 86 66-119
132-64-9 Dibenzofuran 50 79.7 159*61-106
91-94-1 3,3'-Dichlorobenzidine 50 89.6 179*46-117
84-66-2 Diethyl Phthalate 50 38.2 76 64-108
131-11-3 Dimethyl Phthalate 50 36.9 74 63-106
* = Outside of Control Limits.
46 of 81
FA8587966.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85647-BS 6F09185.D 1 06/01/21 WH 06/01/21 OP85647 S6F346
The QC reported here applies to the following samples:Method: EPA 625.1
FA85879-1
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
84-74-2 Di-n-butyl Phthalate 50 39.9 80 65-107
117-84-0 Di-n-octyl Phthalate 50 44.0 88 62-118
121-14-2 2,4-Dinitrotoluene 50 43.4 87 61-110
606-20-2 2,6-Dinitrotoluene 50 38.0 76 63-108
117-81-7 bis(2-Ethylhexyl)phthalate 50 42.8 86 61-117
206-44-0 Fluoranthene 50 40.5 81 63-106
86-73-7 Fluorene 50 41.1 82 62-108
118-74-1 Hexachlorobenzene 50 40.5 81 63-108
87-68-3 Hexachlorobutadiene 50 41.0 82 42-102
77-47-4 Hexachlorocyclopentadiene 50 32.0 64 39-102
67-72-1 Hexachloroethane 50 34.1 68 42-100
193-39-5 Indeno(1,2,3-cd)pyrene 50 44.5 89 64-119
78-59-1 Isophorone 50 39.6 79 43-87
90-12-0 1-Methylnaphthalene 50 40.6 81 53-102
91-57-6 2-Methylnaphthalene 50 76.4 153*51-102
91-20-3 Naphthalene 50 37.0 74 47-100
98-95-3 Nitrobenzene 50 38.3 77 50-104
621-64-7 N-Nitrosodi-n-propylamine 50 38.8 78 52-104
86-30-6 N-Nitrosodiphenylamine 50 35.4 71 64-108
85-01-8 Phenanthrene 50 40.4 81 66-110
129-00-0 Pyrene 50 44.7 89 64-113
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 46%14-67%
4165-62-2 Phenol-d5 34%10-50%
118-79-6 2,4,6-Tribromophenol 71%33-118%
4165-60-0 Nitrobenzene-d5 83%42-108%
321-60-8 2-Fluorobiphenyl 69%40-106%
1718-51-0 Terphenyl-d14 83%39-121%
* = Outside of Control Limits.
47 of 81
FA8587966.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85652-BS 6F09201.D 1 06/02/21 WH 06/01/21 OP85652 S6F347
The QC reported here applies to the following samples:Method: SW846 8270E
FA85879-2, FA85879-3, FA85879-4
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 783 23*36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1140 68 52-108
95-57-8 2-Chlorophenol 1670 1110 67 48-104
120-83-2 2,4-Dichlorophenol 1670 1070 64 51-105
105-67-9 2,4-Dimethylphenol 1670 986 59 43-96
51-28-5 2,4-Dinitrophenol 3330 2250 68 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 2800 84 64-121
95-48-7 2-Methylphenol 1670 1110 67 46-107
3&4-Methylphenol 3330 2200 66 44-111
88-75-5 2-Nitrophenol 1670 1030 62 49-104
100-02-7 4-Nitrophenol 3330 2240 67 56-116
87-86-5 Pentachlorophenol 3330 2320 70 61-114
108-95-2 Phenol 1670 1080 65 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1030 62 56-109
83-32-9 Acenaphthene 1670 1030 62 56-109
208-96-8 Acenaphthylene 1670 934 56 56-106
120-12-7 Anthracene 1670 1130 68 61-110
56-55-3 Benzo(a)anthracene 1670 1260 76 66-111
50-32-8 Benzo(a)pyrene 1670 1260 76 59-104
205-99-2 Benzo(b)fluoranthene 1670 1240 74 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1210 73 67-113
207-08-9 Benzo(k)fluoranthene 1670 1220 73 67-114
101-55-3 4-Bromophenyl phenyl ether 1670 1210 73 62-110
85-68-7 Butyl benzyl phthalate 1670 1210 73 65-113
106-47-8 4-Chloroaniline 1670 918 55 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1020 61 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 915 55 46-103
108-60-1 2,2'-Oxybis(1-chloropropane)1670 936 56 40-110
91-58-7 2-Chloronaphthalene 1670 949 57 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1080 65 58-106
218-01-9 Chrysene 1670 1200 72 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1170 70 68-115
132-64-9 Dibenzofuran 1670 1070 64 57-108
91-94-1 3,3'-Dichlorobenzidine 1670 1230 74 36-114
84-66-2 Diethyl Phthalate 1670 1060 64 61-109
131-11-3 Dimethyl Phthalate 1670 1030 62 59-108
* = Outside of Control Limits.
48 of 81
FA8587966.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85652-BS 6F09201.D 1 06/02/21 WH 06/01/21 OP85652 S6F347
The QC reported here applies to the following samples:Method: SW846 8270E
FA85879-2, FA85879-3, FA85879-4
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
117-84-0 Di-n-octyl Phthalate 1670 1200 72 64-119
84-74-2 Di-n-butyl Phthalate 1670 1140 68 63-108
121-14-2 2,4-Dinitrotoluene 1670 1190 71 59-109
606-20-2 2,6-Dinitrotoluene 1670 1090 65 61-107
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1180 71 64-115
206-44-0 Fluoranthene 1670 1190 71 60-108
86-73-7 Fluorene 1670 1110 67 58-109
118-74-1 Hexachlorobenzene 1670 1150 69 59-111
87-68-3 Hexachlorobutadiene 1670 1070 64 41-108
77-47-4 Hexachlorocyclopentadiene 1670 917 55 49-110
67-72-1 Hexachloroethane 1670 872 52 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1250 75 66-116
78-59-1 Isophorone 1670 1050 63 42-89
90-12-0 1-Methylnaphthalene 1670 1060 64 49-106
91-57-6 2-Methylnaphthalene 1670 1010 61 47-106
91-20-3 Naphthalene 1670 963 58 44-104
98-95-3 Nitrobenzene 1670 992 60 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1010 61 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1030 62 62-110
85-01-8 Phenanthrene 1670 1170 70 63-111
129-00-0 Pyrene 1670 1200 72 65-115
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 64%40-102%
4165-62-2 Phenol-d5 73%41-100%
118-79-6 2,4,6-Tribromophenol 63%42-108%
4165-60-0 Nitrobenzene-d5 64%40-105%
321-60-8 2-Fluorobiphenyl 56%43-107%
1718-51-0 Terphenyl-d14 69%45-119%
* = Outside of Control Limits.
49 of 81
FA8587966.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85652-MS 6F09183.D 5 06/01/21 WH 06/01/21 OP85652 S6F346
OP85652-MSD 6F09184.D 5 06/01/21 WH 06/01/21 OP85652 S6F346
FA85889-1 a 6F09197.D 5 06/02/21 WH 06/01/21 OP85652 S6F347
The QC reported here applies to the following samples:Method: SW846 8270E
FA85879-2, FA85879-3, FA85879-4
FA85889-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid ND 3950 1810 46 4000 2000 50 10 36-118/41
59-50-7 4-Chloro-3-methyl Phenol ND 1970 1100 56 2000 1080 54 2 52-108/21
95-57-8 2-Chlorophenol ND 1970 1100 56 2000 1110 55 1 48-104/26
120-83-2 2,4-Dichlorophenol ND 1970 1070 54 2000 1060 53 1 51-105/27
105-67-9 2,4-Dimethylphenol ND 1970 865 44 2000 842 42*3 43-96/23
534-52-1 4,6-Dinitro-o-cresol ND 3950 1660 42*4000 1860 46*11 64-121/29
95-48-7 2-Methylphenol ND 1970 1060 54 2000 948 47 11 46-107/24
3&4-Methylphenol ND 3950 2100 53 4000 2130 53 1 44-111/24
88-75-5 2-Nitrophenol ND 1970 1020 52 2000 1050 52 3 49-104/27
100-02-7 4-Nitrophenol ND 3950 1800 46*4000 1650 41*9 56-116/23
87-86-5 Pentachlorophenol ND 3950 1790 45*4000 1940 48*8 61-114/23
108-95-2 Phenol ND 1970 1020 52 2000 1080 54 6 45-110/24
88-06-2 2,4,6-Trichlorophenol ND 1970 966 49*2000 1010 50*4 56-109/25
83-32-9 Acenaphthene ND 1970 1050 53*2000 1060 53*1 56-109/23
208-96-8 Acenaphthylene ND 1970 999 51*2000 966 48*3 56-106/23
120-12-7 Anthracene ND 1970 1100 56*2000 1190 59*8 61-110/21
56-55-3 Benzo(a)anthracene ND 1970 1290 65*2000 2220 111 53*66-111/23
50-32-8 Benzo(a)pyrene ND 1970 1230 62 2000 2000 100 48*59-104/23
205-99-2 Benzo(b)fluoranthene ND 1970 1180 60*2000 2260 113 63*67-113/24
191-24-2 Benzo(g,h,i)perylene ND 1970 1150 58*2000 1510 75 27*67-113/21
207-08-9 Benzo(k)fluoranthene ND 1970 1200 61*2000 1590 79 28*67-114/22
101-55-3 4-Bromophenyl phenyl ether ND 1970 1230 62 2000 1200 60*2 62-110/21
85-68-7 Butyl benzyl phthalate ND 1970 ND 0*2000 1270 63*200*65-113/20
106-47-8 4-Chloroaniline ND 1970 767 39 2000 803 40 5 30-115/30
111-91-1 bis(2-Chloroethoxy)methane ND 1970 1290 65 2000 1220 61 6 48-105/24
111-44-4 bis(2-Chloroethyl)ether ND 1970 942 48 2000 961 48 2 46-103/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1970 1030 52 2000 1030 51 0 40-110/25
91-58-7 2-Chloronaphthalene ND 1970 949 48*2000 968 48*2 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether ND 1970 1080 55*2000 1110 55*3 58-106/21
218-01-9 Chrysene ND 1970 1140 58*2000 1910 95 50*65-112/25
53-70-3 Dibenzo(a,h)anthracene ND 1970 1210 61*2000 1230 61*2 68-115/23
132-64-9 Dibenzofuran ND 1970 1090 55*2000 1110 55*2 57-108/22
91-94-1 3,3'-Dichlorobenzidine ND 1970 280 14*2000 279 14*0 36-114/28
84-66-2 Diethyl Phthalate ND 1970 1070 54*2000 1080 54*1 61-109/20
131-11-3 Dimethyl Phthalate ND 1970 1020 52*2000 1030 51*1 59-108/20
117-84-0 Di-n-octyl Phthalate ND 1970 1190 60*2000 1270 63*7 64-119/21
* = Outside of Control Limits.
50 of 81
FA8587966.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85652-MS 6F09183.D 5 06/01/21 WH 06/01/21 OP85652 S6F346
OP85652-MSD 6F09184.D 5 06/01/21 WH 06/01/21 OP85652 S6F346
FA85889-1 a 6F09197.D 5 06/02/21 WH 06/01/21 OP85652 S6F347
The QC reported here applies to the following samples:Method: SW846 8270E
FA85879-2, FA85879-3, FA85879-4
FA85889-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
84-74-2 Di-n-butyl Phthalate ND 1970 1100 56*2000 1130 56*3 63-108/19
121-14-2 2,4-Dinitrotoluene ND 1970 1070 54*2000 1130 56*5 59-109/20
606-20-2 2,6-Dinitrotoluene ND 1970 1090 55*2000 1020 51*7 61-107/22
117-81-7 bis(2-Ethylhexyl)phthalate ND 1970 1340 68 2000 1260 63*6 64-115/23
206-44-0 Fluoranthene ND 1970 1140 58*2000 2310 115*68*60-108/25
86-73-7 Fluorene ND 1970 1100 56*2000 1140 57*4 58-109/21
118-74-1 Hexachlorobenzene ND 1970 1130 57*2000 1150 57*2 59-111/21
87-68-3 Hexachlorobutadiene ND 1970 1090 55 2000 1110 55 2 41-108/27
77-47-4 Hexachlorocyclopentadiene ND 1970 619 31*2000 596 30*4 49-110/31
67-72-1 Hexachloroethane ND 1970 935 47 2000 885 44 5 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene ND 1970 1190 60*2000 1600 80 29*66-116/22
78-59-1 Isophorone ND 1970 1070 54 2000 1090 54 2 42-89/22
90-12-0 1-Methylnaphthalene ND 1970 1150 58 2000 1140 57 1 49-106/26
91-57-6 2-Methylnaphthalene ND 1970 1080 55 2000 1060 53 2 47-106/27
91-20-3 Naphthalene ND 1970 1040 53 2000 1020 51 2 44-104/27
98-95-3 Nitrobenzene ND 1970 1060 54 2000 1070 53 1 43-108/25
621-64-7 N-Nitrosodi-n-propylamine ND 1970 1020 52 2000 1050 52 3 48-108/27
86-30-6 N-Nitrosodiphenylamine ND 1970 947 48*2000 965 48*2 62-110/21
85-01-8 Phenanthrene ND 1970 1110 56*2000 1510 75 31*63-111/22
129-00-0 Pyrene ND 1970 1270 64*2000 2450 122*63*65-115/25
CAS No.Surrogate Recoveries MS MSD FA85889-1 Limits
367-12-4 2-Fluorophenol 53%54%45%40-102%
4165-62-2 Phenol-d5 60%60%48%41-100%
118-79-6 2,4,6-Tribromophenol 44%49%43%42-108%
4165-60-0 Nitrobenzene-d5 55%56%40%40-105%
321-60-8 2-Fluorobiphenyl 48%50%40%*43-107%
1718-51-0 Terphenyl-d14 58%57%51%45-119%
(a) Dilution required due to matrix interference.
* = Outside of Control Limits.
51 of 81
FA8587966.3.1
SGS North America Inc.
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 7
52 of 81
FA858797
Method Blank Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S244-MB 1S6773.D 1 05/30/21 CG n/a n/a G1S244
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-1
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 1.0 1.0 ug/l
100-41-4 Ethylbenzene ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.0 1.0 ug/l
91-20-3 Naphthalene ND 5.0 3.0 ug/l
108-88-3 Toluene ND 2.0 1.0 ug/l
m,p-Xylene ND 4.0 2.0 ug/l
95-47-6 o-Xylene ND 2.0 1.0 ug/l
C5- C8 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C12 Aliphatics (Unadj.)ND 100 35 ug/l
C9- C10 Aromatics (Unadj.)ND 100 35 ug/l
C5- C8 Aliphatics ND 100 35 ug/l
C9- C12 Aliphatics ND 100 35 ug/l
C9- C10 Aromatics ND 100 35 ug/l
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 101%70-130%
460-00-4 BFB 108%70-130%
53 of 81
FA8587977.1.1
Method Blank Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S250-MB 1S6878.D 1 06/08/21 CG n/a n/a G1S250
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-2, FA85879-3, FA85879-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 50 50 ug/kg
100-41-4 Ethylbenzene ND 100 50 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 100 50 ug/kg
91-20-3 Naphthalene ND 250 150 ug/kg
108-88-3 Toluene ND 100 50 ug/kg
m,p-Xylene ND 200 100 ug/kg
95-47-6 o-Xylene ND 100 50 ug/kg
C5- C8 Aliphatics (Unadj.)ND 5000 1800 ug/kg
C9- C12 Aliphatics (Unadj.)ND 5000 1800 ug/kg
C9- C10 Aromatics (Unadj.)ND 5000 1800 ug/kg
C5- C8 Aliphatics ND 5000 1800 ug/kg
C9- C12 Aliphatics ND 5000 1800 ug/kg
C9- C10 Aromatics ND 5000 1800 ug/kg
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 77%70-130%
460-00-4 BFB 78%70-130%
54 of 81
FA8587977.1.2
Method Blank Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S251-MB 1S6900.D 1 06/09/21 CG n/a n/a G1S251
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-2
CAS No.Compound Result RL MDL Units Q
C9- C10 Aromatics (Unadj.)ND 5000 1800 ug/kg
C9- C10 Aromatics ND 5000 1800 ug/kg
CAS No.Surrogate Recoveries Limits
460-00-4 BFB 92%70-130%
460-00-4 BFB 93%70-130%
55 of 81
FA8587977.1.3
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S244-BS 1S6762.D 1 05/30/21 CG n/a n/a G1S244
G1S244-BSD 1S6763.D 1 05/30/21 CG n/a n/a G1S244
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-1
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 80 74.1 93 76.1 95 3 70-130/25
100-41-4 Ethylbenzene 80 74.4 93 75.9 95 2 70-130/25
1634-04-4 Methyl Tert Butyl Ether 80 76.4 96 81.1 101 6 70-130/25
91-20-3 Naphthalene 80 76.2 95 80.4 101 5 70-130/25
108-88-3 Toluene 80 71.9 90 73.8 92 3 70-130/25
m,p-Xylene 160 149 93 152 95 2 70-130/25
95-47-6 o-Xylene 80 74.7 93 76.3 95 2 70-130/25
C5- C8 Aliphatics (Unadj.)240 219 91 220 92 0 70-130/25
C9- C12 Aliphatics (Unadj.)160 134 84 139 87 4 70-130/25
C9- C10 Aromatics (Unadj.)80 83.3 104 81.9 102 2 70-130/25
C5- C8 Aliphatics ND ND nc 70-130/25
C9- C12 Aliphatics ND ND nc 70-130/25
C9- C10 Aromatics 80 83.3 104 81.9 102 2 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 117%118%70-130%
460-00-4 BFB 125%126%70-130%
* = Outside of Control Limits.
56 of 81
FA8587977.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S250-BS 1S6887.D 1 06/08/21 CG n/a n/a G1S250
G1S250-BSD 1S6888.D 1 06/08/21 CG n/a n/a G1S250
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-2, FA85879-3, FA85879-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
71-43-2 Benzene 4080 4020 99 3980 98 1 70-130/25
100-41-4 Ethylbenzene 4080 3910 96 3860 95 1 70-130/25
1634-04-4 Methyl Tert Butyl Ether 4080 4220 103 4190 103 1 70-130/25
91-20-3 Naphthalene 4080 3740 92 3730 91 0 70-130/25
108-88-3 Toluene 4080 3880 95 3840 94 1 70-130/25
m,p-Xylene 8160 7870 96 7730 95 2 70-130/25
95-47-6 o-Xylene 4080 3950 97 3880 95 2 70-130/25
C5- C8 Aliphatics (Unadj.)12200 10600 87 10500 86 1 70-130/25
C9- C12 Aliphatics (Unadj.)8160 6820 84 6630 81 3 70-130/25
C9- C10 Aromatics (Unadj.)4080 4250 104 4330 106 2 70-130/25
C9- C10 Aromatics 4080 4250 104 4330 106 2 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 98%97%70-130%
460-00-4 BFB 100%99%70-130%
* = Outside of Control Limits.
57 of 81
FA8587977.2.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
G1S251-BS 1S6898.D 1 06/09/21 CG n/a n/a G1S251
G1S251-BSD 1S6899.D 1 06/09/21 CG n/a n/a G1S251
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-2
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
C9- C10 Aromatics (Unadj.)4080 3380 83 3890 95 14 70-130/25
C9- C10 Aromatics 4080 3380 83 3890 95 14 70-130/25
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 BFB 93%92%70-130%
460-00-4 BFB 94%93%70-130%
* = Outside of Control Limits.
58 of 81
FA8587977.2.3
Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA85758-1DUP 1S6766.D 1 05/30/21 CG n/a n/a G1S244
FA85758-1 1S6765.D 1 05/30/21 CG n/a n/a G1S244
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-1
FA85758-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
71-43-2 Benzene ND ND nc 50
100-41-4 Ethylbenzene ND ND nc 50
1634-04-4 Methyl Tert Butyl Ether ND ND nc 50
91-20-3 Naphthalene ND ND nc 50
108-88-3 Toluene ND ND nc 50
m,p-Xylene ND ND nc 50
95-47-6 o-Xylene ND ND nc 50
C5- C8 Aliphatics (Unadj.)ND ND nc 50
C9- C12 Aliphatics (Unadj.)ND ND nc 50
C9- C10 Aromatics (Unadj.)ND ND nc 50
C5- C8 Aliphatics ND ND nc 50
C9- C12 Aliphatics ND ND nc 50
C9- C10 Aromatics ND ND nc 50
CAS No.Surrogate Recoveries DUP FA85758-1 Limits
460-00-4 BFB 101%99%70-130%
460-00-4 BFB 107%106%70-130%
* = Outside of Control Limits.
59 of 81
FA8587977.3.1
Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA85879-2DUP 1S6902.D 1 06/09/21 CG n/a n/a G1S251
FA85879-2 1S6901.D 1 06/09/21 CG n/a n/a G1S251
The QC reported here applies to the following samples:Method: MADEP VPH REV 2.1
FA85879-2
FA85879-2 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
C9- C10 Aromatics (Unadj.)488000 678000 33 50
C9- C10 Aromatics 488000 678000 33 50
CAS No.Surrogate Recoveries DUP FA85879-2 Limits
460-00-4 BFB 0%* a 0%* a 70-130%
460-00-4 BFB 0%* a 0%* a 70-130%
(a) Outside control limits due to dilution.
* = Outside of Control Limits.
60 of 81
FA8587977.3.2
SGS North America Inc.
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 8
61 of 81
FA858798
Method Blank Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85606-MB NN033341.D 1 06/01/21 AF 05/28/21 OP85606 GNN1613
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA85879-1
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 4.0 2.0 ug/l
208-96-8 Acenaphthylene ND 4.0 2.0 ug/l
120-12-7 Anthracene ND 4.0 2.0 ug/l
56-55-3 Benzo(a)anthracene ND 4.0 2.0 ug/l
50-32-8 Benzo(a)pyrene ND 4.0 2.0 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.0 2.0 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.0 2.0 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.0 2.0 ug/l
218-01-9 Chrysene ND 4.0 2.0 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 4.0 2.0 ug/l
206-44-0 Fluoranthene ND 4.0 2.0 ug/l
86-73-7 Fluorene ND 4.0 2.0 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.0 2.0 ug/l
91-57-6 2-Methylnaphthalene ND 4.0 2.0 ug/l
91-20-3 Naphthalene ND 4.0 2.0 ug/l
85-01-8 Phenanthrene ND 4.0 2.0 ug/l
129-00-0 Pyrene ND 4.0 2.0 ug/l
C11-C22 Aromatics (Unadj.)ND 200 80 ug/l
C11-C22 Aromatics ND 200 80 ug/l
C9-C18 Aliphatics ND 200 50 ug/l
C19-C36 Aliphatics ND 200 50 ug/l
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 87%40-140%
580-13-2 2-Bromonaphthalene 123%40-140%
84-15-1 o-Terphenyl 99%40-140%
321-60-8 2-Fluorobiphenyl 122%40-140%
62 of 81
FA8587988.1.1
Method Blank Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85654-MB NN033402.D 1 06/04/21 AF 06/01/21 OP85654 GNN1614
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA85879-2, FA85879-3, FA85879-4
CAS No.Compound Result RL MDL Units Q
83-32-9 Acenaphthene ND 200 100 ug/kg
208-96-8 Acenaphthylene ND 200 100 ug/kg
120-12-7 Anthracene ND 200 100 ug/kg
56-55-3 Benzo(a)anthracene ND 200 100 ug/kg
50-32-8 Benzo(a)pyrene ND 200 100 ug/kg
205-99-2 Benzo(b)fluoranthene ND 200 100 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 200 100 ug/kg
207-08-9 Benzo(k)fluoranthene ND 200 100 ug/kg
218-01-9 Chrysene ND 200 100 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 200 100 ug/kg
206-44-0 Fluoranthene ND 200 100 ug/kg
86-73-7 Fluorene ND 200 100 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 200 100 ug/kg
91-57-6 2-Methylnaphthalene ND 200 100 ug/kg
91-20-3 Naphthalene ND 200 100 ug/kg
85-01-8 Phenanthrene ND 200 100 ug/kg
129-00-0 Pyrene ND 200 100 ug/kg
C11-C22 Aromatics (Unadj.)ND 10000 4000 ug/kg
C11-C22 Aromatics ND 10000 4000 ug/kg
C9-C18 Aliphatics ND 10000 2500 ug/kg
C19-C36 Aliphatics ND 10000 2500 ug/kg
CAS No.Surrogate Recoveries Limits
3386-33-2 1-Chlorooctadecane 79%40-140%
580-13-2 2-Bromonaphthalene 116%40-140%
84-15-1 o-Terphenyl 95%40-140%
321-60-8 2-Fluorobiphenyl 113%40-140%
63 of 81
FA8587988.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85606-BS NN033342.D 1 06/01/21 AF 05/28/21 OP85606 GNN1613
OP85606-BSD NN033343.D 1 06/01/21 AF 05/28/21 OP85606 GNN1613
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA85879-1
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
83-32-9 Acenaphthene 100 90.9 91 93.2 93 2 40-140/30
208-96-8 Acenaphthylene 100 89.9 90 92.7 93 3 40-140/30
120-12-7 Anthracene 100 100 100 103 103 3 40-140/30
56-55-3 Benzo(a)anthracene 100 115 115 119 119 3 40-140/30
50-32-8 Benzo(a)pyrene 100 115 115 118 118 3 40-140/30
205-99-2 Benzo(b)fluoranthene 100 118 118 122 122 3 40-140/30
191-24-2 Benzo(g,h,i)perylene 100 101 101 104 104 3 40-140/30
207-08-9 Benzo(k)fluoranthene 100 94.5 95 97.3 97 3 40-140/30
218-01-9 Chrysene 100 109 109 112 112 3 40-140/30
53-70-3 Dibenzo(a,h)anthracene 100 108 108 111 111 3 40-140/30
206-44-0 Fluoranthene 100 105 105 109 109 4 40-140/30
86-73-7 Fluorene 100 93.6 94 95.6 96 2 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 100 104 104 107 107 3 40-140/30
91-57-6 2-Methylnaphthalene 100 77.9 78 80.9 81 4 40-140/30
91-20-3 Naphthalene 100 72.3 72 75.9 76 5 40-140/30
85-01-8 Phenanthrene 100 99.0 99 101 101 2 40-140/30
129-00-0 Pyrene 100 109 109 112 112 3 40-140/30
C11-C22 Aromatics (Unadj.)1700 1750 103 1790 105 2 40-140/30
C9-C18 Aliphatics 600 237 40 226 38*5 40-140/30
C19-C36 Aliphatics 800 546 68 536 67 2 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 80%77%40-140%
580-13-2 2-Bromonaphthalene 112%113%40-140%
84-15-1 o-Terphenyl 97%99%40-140%
321-60-8 2-Fluorobiphenyl 110%112%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP85606-BS 2-Methylnaphthalene 77.9 ND 0.0%5.0
OP85606-BS Naphthalene 72.3 ND 0.0%5.0
OP85606-BSD 2-Methylnaphthalene 80.9 ND 0.0%5.0
OP85606-BSD Naphthalene 75.9 ND 0.0%5.0
* = Outside of Control Limits.
64 of 81
FA8587988.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85654-BS NN033403.D 1 06/04/21 AF 06/01/21 OP85654 GNN1614
OP85654-BSD NN033404.D 1 06/04/21 AF 06/01/21 OP85654 GNN1614
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA85879-2, FA85879-3, FA85879-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
83-32-9 Acenaphthene 5000 4390 88 4460 89 2 40-140/30
208-96-8 Acenaphthylene 5000 4370 87 4450 89 2 40-140/30
120-12-7 Anthracene 5000 4830 97 4790 96 1 40-140/30
56-55-3 Benzo(a)anthracene 5000 5430 109 5290 106 3 40-140/30
50-32-8 Benzo(a)pyrene 5000 5400 108 5250 105 3 40-140/30
205-99-2 Benzo(b)fluoranthene 5000 5560 111 5420 108 3 40-140/30
191-24-2 Benzo(g,h,i)perylene 5000 4690 94 4590 92 2 40-140/30
207-08-9 Benzo(k)fluoranthene 5000 4460 89 4330 87 3 40-140/30
218-01-9 Chrysene 5000 5130 103 5000 100 3 40-140/30
53-70-3 Dibenzo(a,h)anthracene 5000 5080 102 4920 98 3 40-140/30
206-44-0 Fluoranthene 5000 4980 100 4880 98 2 40-140/30
86-73-7 Fluorene 5000 4490 90 4560 91 2 40-140/30
193-39-5 Indeno(1,2,3-cd)pyrene 5000 4910 98 4670 93 5 40-140/30
91-57-6 2-Methylnaphthalene 5000 3880 78 3940 79 2 40-140/30
91-20-3 Naphthalene 5000 3620 72 3700 74 2 40-140/30
85-01-8 Phenanthrene 5000 4710 94 4710 94 0 40-140/30
129-00-0 Pyrene 5000 5140 103 5050 101 2 40-140/30
C11-C22 Aromatics (Unadj.)85000 83700 98 82600 97 1 40-140/30
C9-C18 Aliphatics 30000 12300 41 12300 41 0 40-140/30
C19-C36 Aliphatics 40000 23200 58 23400 59 1 40-140/30
CAS No.Surrogate Recoveries BSP BSD Limits
3386-33-2 1-Chlorooctadecane 73%73%40-140%
580-13-2 2-Bromonaphthalene 106%104%40-140%
84-15-1 o-Terphenyl 93%92%40-140%
321-60-8 2-Fluorobiphenyl 102%101%40-140%
Sample Compound Col #1 Col #2 Breakthrough Limit
OP85654-BS 2-Methylnaphthalene 3880 ND 0.0%5.0
OP85654-BS Naphthalene 3620 ND 0.0%5.0
OP85654-BSD 2-Methylnaphthalene 3940 ND 0.0%5.0
OP85654-BSD Naphthalene 3700 ND 0.0%5.0
* = Outside of Control Limits.
65 of 81
FA8587988.2.2
Duplicate Summary Page 1 of 1
Job Number:FA85879
Account:GRINCC GRI (Geological Resources Inc.)
Project:John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP85654-DUP NN033415.D 5 06/04/21 AF 06/01/21 OP85654 GNN1614
FA85879-2 NN033416.D 5 06/04/21 AF 06/01/21 OP85654 GNN1614
The QC reported here applies to the following samples:Method: MADEP EPH REV 2.1
FA85879-2, FA85879-3, FA85879-4
FA85879-2 DUP
CAS No.Compound ug/kg Q ug/kg Q RPD Limits
83-32-9 Acenaphthene 4050 2250 57*30 a
208-96-8 Acenaphthylene ND ND nc 30 a
120-12-7 Anthracene ND ND nc 30 a
56-55-3 Benzo(a)anthracene ND ND nc 30 a
50-32-8 Benzo(a)pyrene ND ND nc 30 a
205-99-2 Benzo(b)fluoranthene ND ND nc 30 a
191-24-2 Benzo(g,h,i)perylene ND ND nc 30 a
207-08-9 Benzo(k)fluoranthene ND ND nc 30 a
218-01-9 Chrysene ND ND nc 30 a
53-70-3 Dibenzo(a,h)anthracene ND ND nc 30 a
206-44-0 Fluoranthene ND ND nc 30 a
86-73-7 Fluorene ND ND nc 30 a
193-39-5 Indeno(1,2,3-cd)pyrene ND ND nc 30 a
91-57-6 2-Methylnaphthalene 17400 11100 44*30 a
91-20-3 Naphthalene 7480 4070 59*30 a
85-01-8 Phenanthrene 2490 3210 25 30 a
129-00-0 Pyrene ND ND nc 30 a
C11-C22 Aromatics (Unadj.)615000 411000 40*30 a
C11-C22 Aromatics 584000 390000 40*30 a
C9-C18 Aliphatics 566000 323000 55*30 a
C19-C36 Aliphatics 142000 85200 50*30 a
CAS No.Surrogate Recoveries DUP FA85879-2 Limits
3386-33-2 1-Chlorooctadecane 79%79%40-140%
580-13-2 2-Bromonaphthalene 103%108%40-140%
84-15-1 o-Terphenyl 85%70%40-140%
321-60-8 2-Fluorobiphenyl 100%106%40-140%
(a) Advisory control limits.
* = Outside of Control Limits.
66 of 81
FA8587988.3.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
(SGS Scott, LA)
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 9
67 of 81
FA858799
FA85879: Chain of Custody
Page 1 of 3
SGS Scott, LA
68 of 81
FA8587999.1
FA85879: Chain of Custody
Page 2 of 3
69 of 81
FA8587999.1
FA85879: Chain of Custody
Page 3 of 3
70 of 81
FA8587999.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
(SGS Scott, LA)
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 10
71 of 81
FA8587910
Method Blank Summary Page 1 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I2995-MB1 2I083740.D 1 06/01/21 CP n/a n/a V2I2995
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-2, FA85879-4
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 2500 110 ug/kg
71-43-2 Benzene ND 25 9.9 ug/kg
75-27-4 Bromodichloromethane ND 50 16 ug/kg
75-25-2 Bromoform ND 50 40 ug/kg
104-51-8 n-Butylbenzene ND 250 16 ug/kg
75-15-0 Carbon Disulfide ND 50 21 ug/kg
56-23-5 Carbon Tetrachloride ND 50 20 ug/kg
108-90-7 Chlorobenzene ND 50 12 ug/kg
75-00-3 Chloroethane ND 50 17 ug/kg
67-66-3 Chloroform ND 50 13 ug/kg
110-82-7 Cyclohexane ND 50 17 ug/kg
124-48-1 Dibromochloromethane ND 50 14 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 250 45 ug/kg
106-93-4 1,2-Dibromoethane ND 50 29 ug/kg
75-71-8 Dichlorodifluoromethane ND 50 33 ug/kg
541-73-1 m-Dichlorobenzene ND 50 16 ug/kg
95-50-1 o-Dichlorobenzene ND 50 9.7 ug/kg
106-46-7 p-Dichlorobenzene ND 50 13 ug/kg
75-34-3 1,1-Dichloroethane ND 50 11 ug/kg
107-06-2 1,2-Dichloroethane ND 50 11 ug/kg
75-35-4 1,1-Dichloroethylene ND 50 20 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 50 16 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 50 10 ug/kg
78-87-5 1,2-Dichloropropane ND 50 6.3 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 50 12 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 50 13 ug/kg
100-41-4 Ethylbenzene ND 50 13 ug/kg
591-78-6 2-Hexanone ND 630 33 ug/kg
98-82-8 Isopropylbenzene ND 250 14 ug/kg
79-20-9 Methyl Acetate ND 500 16 ug/kg
74-83-9 Methyl Bromide ND 500 78 ug/kg
74-87-3 Methyl Chloride ND 250 15 ug/kg
108-87-2 Methylcyclohexane ND 250 65 ug/kg
75-09-2 Methylene Chloride ND 250 28 ug/kg
78-93-3 Methyl Ethyl Ketone ND 630 38 ug/kg
108-10-1 4-Methyl-2-pentanone ND 630 26 ug/kg
72 of 81
FA858791010.1.1
Method Blank Summary Page 2 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I2995-MB1 2I083740.D 1 06/01/21 CP n/a n/a V2I2995
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-2, FA85879-4
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 50 5.2 ug/kg
91-20-3 Naphthalene ND 250 29 ug/kg
103-65-1 n-Propylbenzene ND 250 21 ug/kg
100-42-5 Styrene ND 50 7.3 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 50 7.4 ug/kg
127-18-4 Tetrachloroethylene ND 50 17 ug/kg
108-88-3 Toluene ND 250 9.0 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 250 10 ug/kg
71-55-6 1,1,1-Trichloroethane ND 50 18 ug/kg
79-00-5 1,1,2-Trichloroethane ND 50 7.5 ug/kg
79-01-6 Trichloroethylene ND 50 25 ug/kg
75-69-4 Trichlorofluoromethane ND 50 18 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 250 19 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 250 13 ug/kg
75-01-4 Vinyl Chloride ND 50 13 ug/kg
1330-20-7 Xylene (total)ND 100 58 ug/kg
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 100%59-143%
2037-26-5 Toluene-D8 97%52-159%
460-00-4 4-Bromofluorobenzene 94%38-183%
73 of 81
FA858791010.1.1
Method Blank Summary Page 1 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H2825-MB1 2H0072807.D 1 06/01/21 CP n/a n/a V2H2825
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-3
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 50 2.2 ug/kg
71-43-2 Benzene ND 0.50 0.20 ug/kg
75-27-4 Bromodichloromethane ND 1.0 0.32 ug/kg
75-25-2 Bromoform ND 1.0 0.80 ug/kg
104-51-8 n-Butylbenzene ND 5.0 0.32 ug/kg
75-15-0 Carbon Disulfide 0.52 1.0 0.41 ug/kg J
56-23-5 Carbon Tetrachloride ND 1.0 0.39 ug/kg
108-90-7 Chlorobenzene ND 1.0 0.25 ug/kg
75-00-3 Chloroethane ND 1.0 0.34 ug/kg
67-66-3 Chloroform ND 1.0 0.26 ug/kg
110-82-7 Cyclohexane ND 1.0 0.35 ug/kg
124-48-1 Dibromochloromethane ND 1.0 0.29 ug/kg
96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 0.89 ug/kg
106-93-4 1,2-Dibromoethane ND 1.0 0.57 ug/kg
75-71-8 Dichlorodifluoromethane ND 1.0 0.65 ug/kg
541-73-1 m-Dichlorobenzene ND 1.0 0.32 ug/kg
95-50-1 o-Dichlorobenzene ND 1.0 0.19 ug/kg
106-46-7 p-Dichlorobenzene ND 1.0 0.26 ug/kg
75-34-3 1,1-Dichloroethane ND 1.0 0.23 ug/kg
107-06-2 1,2-Dichloroethane ND 1.0 0.22 ug/kg
75-35-4 1,1-Dichloroethylene ND 1.0 0.41 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.31 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.20 ug/kg
78-87-5 1,2-Dichloropropane ND 1.0 0.13 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.24 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.26 ug/kg
100-41-4 Ethylbenzene ND 1.0 0.26 ug/kg
591-78-6 2-Hexanone ND 13 0.66 ug/kg
98-82-8 Isopropylbenzene ND 5.0 0.28 ug/kg
79-20-9 Methyl Acetate ND 10 0.33 ug/kg
74-83-9 Methyl Bromide ND 10 1.6 ug/kg
74-87-3 Methyl Chloride ND 5.0 0.30 ug/kg
108-87-2 Methylcyclohexane ND 5.0 1.3 ug/kg
75-09-2 Methylene Chloride ND 5.0 0.56 ug/kg
78-93-3 Methyl Ethyl Ketone ND 13 0.77 ug/kg
108-10-1 4-Methyl-2-pentanone ND 13 0.52 ug/kg
74 of 81
FA858791010.1.2
Method Blank Summary Page 2 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H2825-MB1 2H0072807.D 1 06/01/21 CP n/a n/a V2H2825
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-3
CAS No.Compound Result RL MDL Units Q
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.10 ug/kg
91-20-3 Naphthalene ND 5.0 0.57 ug/kg
103-65-1 n-Propylbenzene ND 5.0 0.43 ug/kg
100-42-5 Styrene ND 1.0 0.15 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.15 ug/kg
127-18-4 Tetrachloroethylene ND 1.0 0.34 ug/kg
108-88-3 Toluene ND 5.0 0.18 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 0.21 ug/kg
71-55-6 1,1,1-Trichloroethane ND 1.0 0.35 ug/kg
79-00-5 1,1,2-Trichloroethane ND 1.0 0.15 ug/kg
79-01-6 Trichloroethylene ND 1.0 0.50 ug/kg
75-69-4 Trichlorofluoromethane ND 1.0 0.36 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 0.38 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 0.25 ug/kg
75-01-4 Vinyl Chloride ND 1.0 0.26 ug/kg
1330-20-7 Xylene (total)ND 2.0 1.2 ug/kg
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 109%59-143%
2037-26-5 Toluene-D8 105%52-159%
460-00-4 4-Bromofluorobenzene 105%38-183%
75 of 81
FA858791010.1.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I2995-BS1 2I083734.D 1 06/01/21 CP n/a n/a V2I2995
V2I2995-BSD1 2I083736.D 1 06/01/21 CP n/a n/a V2I2995
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-2, FA85879-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
67-64-1 Acetone 50 59.5 119 67.0 134 12 40-153/30
71-43-2 Benzene 20 20.0 100 21.9 110 9 67-135/30
75-27-4 Bromodichloromethane 20 20.2 101 21.9 110 8 54-146/30
75-25-2 Bromoform 20 20.3 102 22.5 113 10 49-145/30
104-51-8 n-Butylbenzene 20 20.9 105 22.8 114 9 47-160/30
75-15-0 Carbon Disulfide 20 20.4 102 22.1 111 8 48-153/30
56-23-5 Carbon Tetrachloride 20 19.5 98 21.0 105 7 50-152/30
108-90-7 Chlorobenzene 20 20.8 104 22.3 112 7 57-144/30
75-00-3 Chloroethane 20 20.5 103 22.0 110 7 38-176/30
67-66-3 Chloroform 20 19.5 98 21.8 109 11 53-147/30
110-82-7 Cyclohexane 20 21.8 109 23.3 117 7 46-159/30
124-48-1 Dibromochloromethane 20 20.7 104 22.3 112 7 54-146/30
96-12-8 1,2-Dibromo-3-chloropropane 20 19.2 96 20.6 103 7 51-145/30
106-93-4 1,2-Dibromoethane 20 23.1 116 23.9 120 3 55-145/30
75-71-8 Dichlorodifluoromethane 20 21.7 109 22.4 112 3 24-179/30
541-73-1 m-Dichlorobenzene 20 22.0 110 23.8 119 8 54-147/30
95-50-1 o-Dichlorobenzene 20 21.9 110 23.6 118 7 55-144/30
106-46-7 p-Dichlorobenzene 20 21.2 106 22.7 114 7 54-147/30
75-34-3 1,1-Dichloroethane 20 20.7 104 22.5 113 8 53-148/30
107-06-2 1,2-Dichloroethane 20 19.7 99 21.4 107 8 55-144/30
75-35-4 1,1-Dichloroethylene 20 20.0 100 21.7 109 8 49-153/30
156-59-2 cis-1,2-Dichloroethylene 20 20.9 105 22.5 113 7 52-147/30
156-60-5 trans-1,2-Dichloroethylene 20 20.1 101 22.5 113 11 51-152/30
78-87-5 1,2-Dichloropropane 20 20.3 102 21.7 109 7 56-145/30
10061-01-5 cis-1,3-Dichloropropene 20 19.6 98 21.0 105 7 54-148/30
10061-02-6 trans-1,3-Dichloropropene 20 20.7 104 22.4 112 8 53-151/30
100-41-4 Ethylbenzene 20 21.5 108 23.4 117 8 69-136/30
591-78-6 2-Hexanone 50 73.9 148 82.2 164* a 11 45-148/30
98-82-8 Isopropylbenzene 20 22.9 115 24.6 123 7 52-151/30
79-20-9 Methyl Acetate 20 17.6 88 19.5 98 10 36-171/30
74-83-9 Methyl Bromide 20 24.1 121 25.4 127 5 40-170/30
74-87-3 Methyl Chloride 20 20.8 104 22.0 110 6 39-152/30
108-87-2 Methylcyclohexane 20 20.3 102 22.2 111 9 47-160/30
75-09-2 Methylene Chloride 20 21.6 108 23.4 117 8 51-142/30
78-93-3 Methyl Ethyl Ketone 50 55.0 110 58.7 117 7 48-150/30
108-10-1 4-Methyl-2-pentanone 50 57.8 116 63.8 128 10 50-151/30
* = Outside of Control Limits.
76 of 81
FA858791010.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I2995-BS1 2I083734.D 1 06/01/21 CP n/a n/a V2I2995
V2I2995-BSD1 2I083736.D 1 06/01/21 CP n/a n/a V2I2995
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-2, FA85879-4
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether 20 19.3 97 21.4 107 10 61-142/30
91-20-3 Naphthalene 20 20.4 102 22.7 114 11 58-147/30
103-65-1 n-Propylbenzene 20 22.8 114 24.1 121 6 50-154/30
100-42-5 Styrene 20 21.4 107 23.3 117 9 56-145/30
79-34-5 1,1,2,2-Tetrachloroethane 20 23.0 115 24.1 121 5 55-141/30
127-18-4 Tetrachloroethylene 20 21.2 106 22.5 113 6 54-156/30
108-88-3 Toluene 20 20.8 104 22.2 111 7 71-135/30
120-82-1 1,2,4-Trichlorobenzene 20 21.8 109 23.8 119 9 48-163/30
71-55-6 1,1,1-Trichloroethane 20 19.9 100 21.6 108 8 52-153/30
79-00-5 1,1,2-Trichloroethane 20 22.8 114 24.3 122 6 55-144/30
79-01-6 Trichloroethylene 20 20.0 100 21.7 109 8 56-151/30
75-69-4 Trichlorofluoromethane 20 21.4 107 21.9 110 2 36-171/30
95-63-6 1,2,4-Trimethylbenzene 20 21.9 110 23.7 119 8 50-153/30
108-67-8 1,3,5-Trimethylbenzene 20 23.4 117 25.5 128 9 51-153/30
75-01-4 Vinyl Chloride 20 21.2 106 22.7 114 7 42-155/30
1330-20-7 Xylene (total)60 67.0 112 72.9 122 8 69-138/30
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 97%98%59-143%
2037-26-5 Toluene-D8 99%99%52-159%
460-00-4 4-Bromofluorobenzene 98%98%38-183%
(a) Outside control limits biased high. Analyte not detected in associated samples.
* = Outside of Control Limits.
77 of 81
FA858791010.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H2825-BS1 2H0072804.D 1 06/01/21 CP n/a n/a V2H2825
V2H2825-BSD1 2H0072805.D 1 06/01/21 CP n/a n/a V2H2825
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
67-64-1 Acetone 50 51.2 102 54.9 110 7 40-153/30
71-43-2 Benzene 20 20.7 104 20.6 103 0 67-135/30
75-27-4 Bromodichloromethane 20 19.1 96 20.1 101 5 54-146/30
75-25-2 Bromoform 20 19.1 96 20.3 102 6 49-145/30
104-51-8 n-Butylbenzene 20 15.2 76 15.8 79 4 47-160/30
75-15-0 Carbon Disulfide 20 19.0 95 19.6 98 3 48-153/30
56-23-5 Carbon Tetrachloride 20 19.9 100 20.0 100 1 50-152/30
108-90-7 Chlorobenzene 20 19.2 96 20.1 101 5 57-144/30
75-00-3 Chloroethane 20 18.3 92 18.5 93 1 38-176/30
67-66-3 Chloroform 20 19.2 96 20.5 103 7 53-147/30
110-82-7 Cyclohexane 20 18.6 93 18.9 95 2 46-159/30
124-48-1 Dibromochloromethane 20 20.2 101 21.4 107 6 54-146/30
96-12-8 1,2-Dibromo-3-chloropropane 20 20.6 103 23.0 115 11 51-145/30
106-93-4 1,2-Dibromoethane 20 20.6 103 22.2 111 7 55-145/30
75-71-8 Dichlorodifluoromethane 20 21.4 107 21.0 105 2 24-179/30
541-73-1 m-Dichlorobenzene 20 16.1 81 17.3 87 7 54-147/30
95-50-1 o-Dichlorobenzene 20 20.3 102 21.2 106 4 55-144/30
106-46-7 p-Dichlorobenzene 20 19.9 100 20.7 104 4 54-147/30
75-34-3 1,1-Dichloroethane 20 20.3 102 20.5 103 1 53-148/30
107-06-2 1,2-Dichloroethane 20 21.8 109 23.6 118 8 55-144/30
75-35-4 1,1-Dichloroethylene 20 20.2 101 21.1 106 4 49-153/30
156-59-2 cis-1,2-Dichloroethylene 20 19.9 100 21.3 107 7 52-147/30
156-60-5 trans-1,2-Dichloroethylene 20 17.6 88 17.4 87 1 51-152/30
78-87-5 1,2-Dichloropropane 20 18.7 94 19.2 96 3 56-145/30
10061-01-5 cis-1,3-Dichloropropene 20 19.9 100 20.1 101 1 54-148/30
10061-02-6 trans-1,3-Dichloropropene 20 19.6 98 20.6 103 5 53-151/30
100-41-4 Ethylbenzene 20 15.0 75 15.7 79 5 69-136/30
591-78-6 2-Hexanone 50 51.2 102 58.0 116 12 45-148/30
98-82-8 Isopropylbenzene 20 17.3 87 17.9 90 3 52-151/30
79-20-9 Methyl Acetate 20 16.6 83 18.3 92 10 36-171/30
74-83-9 Methyl Bromide 20 22.6 113 24.0 120 6 40-170/30
74-87-3 Methyl Chloride 20 20.0 100 20.0 100 0 39-152/30
108-87-2 Methylcyclohexane 20 16.8 84 17.3 87 3 47-160/30
75-09-2 Methylene Chloride 20 19.2 96 20.2 101 5 51-142/30
78-93-3 Methyl Ethyl Ketone 50 46.2 92 51.0 102 10 48-150/30
108-10-1 4-Methyl-2-pentanone 50 51.4 103 53.7 107 4 50-151/30
* = Outside of Control Limits.
78 of 81
FA858791010.2.2
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2H2825-BS1 2H0072804.D 1 06/01/21 CP n/a n/a V2H2825
V2H2825-BSD1 2H0072805.D 1 06/01/21 CP n/a n/a V2H2825
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether 20 20.8 104 22.1 111 6 61-142/30
91-20-3 Naphthalene 20 20.3 102 21.8 109 7 58-147/30
103-65-1 n-Propylbenzene 20 15.0 75 15.6 78 4 50-154/30
100-42-5 Styrene 20 18.1 91 18.9 95 4 56-145/30
79-34-5 1,1,2,2-Tetrachloroethane 20 19.0 95 21.1 106 10 55-141/30
127-18-4 Tetrachloroethylene 20 15.9 80 16.3 82 2 54-156/30
108-88-3 Toluene 20 18.5 93 18.7 94 1 71-135/30
120-82-1 1,2,4-Trichlorobenzene 20 16.3 82 18.0 90 10 48-163/30
71-55-6 1,1,1-Trichloroethane 20 18.0 90 18.7 94 4 52-153/30
79-00-5 1,1,2-Trichloroethane 20 18.5 93 21.0 105 13 55-144/30
79-01-6 Trichloroethylene 20 17.8 89 18.8 94 5 56-151/30
75-69-4 Trichlorofluoromethane 20 21.6 108 21.9 110 1 36-171/30
95-63-6 1,2,4-Trimethylbenzene 20 16.9 85 17.1 86 1 50-153/30
108-67-8 1,3,5-Trimethylbenzene 20 16.5 83 17.6 88 6 51-153/30
75-01-4 Vinyl Chloride 20 19.0 95 19.3 97 2 42-155/30
1330-20-7 Xylene (total)60 53.8 90 54.9 92 2 69-138/30
CAS No.Surrogate Recoveries BSP BSD Limits
17060-07-0 1,2-Dichloroethane-D4 101%101%59-143%
2037-26-5 Toluene-D8 102%99%52-159%
460-00-4 4-Bromofluorobenzene 102%104%38-183%
* = Outside of Control Limits.
79 of 81
FA858791010.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA71578-26MS 2I083768.D 1 06/01/21 CP n/a n/a V2I2995
LA71578-26MSD 2I083770.D 1 06/01/21 CP n/a n/a V2I2995
LA71578-26 a 2I083758.D 1 06/01/21 CP n/a n/a V2I2995
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-2, FA85879-4
LA71578-26 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 4630 4770 103 4630 4520 98 5 19-170/34
71-43-2 Benzene ND 1850 2010 109 1850 1940 105 4 15-162/33
75-27-4 Bromodichloromethane ND 1850 1870 101 1850 1780 96 5 48-124/14
75-25-2 Bromoform ND 1850 1670 90 1850 1620 87 3 20-128/16
104-51-8 n-Butylbenzene ND 1850 2000 108 1850 1880 102 6 1-199/21
75-15-0 Carbon Disulfide ND 1850 1800 97 1850 1790 97 1 4-140/31
56-23-5 Carbon Tetrachloride ND 1850 1700 92 1850 1700 92 0 25-136/17
108-90-7 Chlorobenzene ND 1850 2040 110 1850 1970 106 3 31-153/12
75-00-3 Chloroethane ND 1850 1020 55 1850 1030 56 1 1-171/64
67-66-3 Chloroform ND 1850 1950 105 1850 1900 103 3 26-153/42
110-82-7 Cyclohexane ND 1850 2170 117 1850 2180 118 0 1-180/17
124-48-1 Dibromochloromethane ND 1850 1780 96 1850 1720 93 3 26-131/14
96-12-8 1,2-Dibromo-3-chloropropane ND 1850 1790 97 1850 1750 94 2 18-141/68
106-93-4 1,2-Dibromoethane ND 1850 2210 119 1850 2110 114 5 39-143/14
75-71-8 Dichlorodifluoromethane ND 1850 1850 100 1850 1880 102 2 1-149/18
541-73-1 m-Dichlorobenzene ND 1850 2110 114 1850 1990 107 6 22-152/15
95-50-1 o-Dichlorobenzene ND 1850 2120 114 1850 2040 110 4 27-150/12
106-46-7 p-Dichlorobenzene ND 1850 2020 109 1850 1880 102 7 19-154/12
75-34-3 1,1-Dichloroethane ND 1850 2040 110 1850 2010 109 1 31-147/13
107-06-2 1,2-Dichloroethane ND 1850 2080 112 1850 1920 104 8 31-147/13
75-35-4 1,1-Dichloroethylene ND 1850 1960 106 1850 1910 103 3 22-148/19
156-59-2 cis-1,2-Dichloroethylene ND 1850 2170 117 1850 2150 116 1 25-145/15
156-60-5 trans-1,2-Dichloroethylene ND 1850 2150 116 1850 2080 112 3 24-145/17
78-87-5 1,2-Dichloropropane ND 1850 2060 111 1850 2000 108 3 36-141/13
10061-01-5 cis-1,3-Dichloropropene ND 1850 1930 104 1850 1840 99 5 27-143/12
10061-02-6 trans-1,3-Dichloropropene ND 1850 2000 108 1850 1890 102 6 46-130/14
100-41-4 Ethylbenzene ND 1850 2140 116 1850 2090 113 2 14-168/13
591-78-6 2-Hexanone ND 4630 6480 140 4630 6010 130 8 16-169/26
98-82-8 Isopropylbenzene ND 1850 2280 123 1850 2210 119 3 12-186/18
79-20-9 Methyl Acetate ND 1850 2020 109 1850 1920 104 5 66-172/51
74-83-9 Methyl Bromide ND 1850 1730 93 1850 1760 95 2 1-178/40
74-87-3 Methyl Chloride ND 1850 1900 103 1850 1990 107 5 1-151/37
108-87-2 Methylcyclohexane ND 1850 2040 110 1850 1990 107 2 2-179/18
75-09-2 Methylene Chloride ND 1850 2130 115 1850 2100 113 1 27-147/18
78-93-3 Methyl Ethyl Ketone ND 4630 4720 102 4630 4210 91 11 29-156/32
108-10-1 4-Methyl-2-pentanone ND 4630 5480 118 4630 5080 110 8 33-160/23
* = Outside of Control Limits.
80 of 81
FA858791010.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA85879
Account:ALSE SGS Orlando, FL
Project:GRINCC: John E Ferebee Farming; 350 S Astland Rd, Camden, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA71578-26MS 2I083768.D 1 06/01/21 CP n/a n/a V2I2995
LA71578-26MSD 2I083770.D 1 06/01/21 CP n/a n/a V2I2995
LA71578-26 a 2I083758.D 1 06/01/21 CP n/a n/a V2I2995
The QC reported here applies to the following samples:Method: SW846 8260D
FA85879-2, FA85879-4
LA71578-26 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
1634-04-4 Methyl Tert Butyl Ether ND 1850 2150 116 1850 2040 110 5 37-145/14
91-20-3 Naphthalene ND 1850 2370 128 1850 2230 120 6 1-192/73
103-65-1 n-Propylbenzene ND 1850 2210 119 1850 2130 115 4 8-170/17
100-42-5 Styrene ND 1850 2120 114 1850 2080 112 2 24-165/13
79-34-5 1,1,2,2-Tetrachloroethane ND 1850 2290 124 1850 2170 117 5 33-146/48
127-18-4 Tetrachloroethylene ND 1850 2100 113 1850 2030 110 3 21-149/18
108-88-3 Toluene ND 1850 2040 110 1850 1990 107 2 11-173/43
120-82-1 1,2,4-Trichlorobenzene ND 1850 2140 116 1850 2050 111 4 15-155/65
71-55-6 1,1,1-Trichloroethane ND 1850 1920 104 1850 1900 103 1 31-142/16
79-00-5 1,1,2-Trichloroethane ND 1850 2270 123 1850 2180 118 4 11-185/16
79-01-6 Trichloroethylene ND 1850 2000 108 1850 1980 107 1 21-154/15
75-69-4 Trichlorofluoromethane ND 1850 1640 89 1850 1590 86 3 1-163/27
95-63-6 1,2,4-Trimethylbenzene ND 1850 2100 113 1850 2010 109 4 90-183/15
108-67-8 1,3,5-Trimethylbenzene ND 1850 2250 121 1850 2180 118 3 10-179/14
75-01-4 Vinyl Chloride ND 1850 1940 105 1850 1940 105 0 32-153/15
1330-20-7 Xylene (total)ND 5560 6600 119 5560 6410 115 3 14-172/12
CAS No.Surrogate Recoveries MS MSD LA71578-26 Limits
17060-07-0 1,2-Dichloroethane-D4 100%100%103%59-143%
2037-26-5 Toluene-D8 100%101%99%52-159%
460-00-4 4-Bromofluorobenzene 99%99%95%38-183%
(a) Confirmation run.
* = Outside of Control Limits.
81 of 81
FA858791010.3.1