WA-28646_47885_CA_CLO_20210614

UST Closure Report (UST-12)
Southeastern Freight Lines, Inc. – Kinston, NC

A. Site Information
1. Site Identification: (see Figures 1, 2, 3, 4)
Date of Report: June 3, 2021

Facility I.D.: #00-0-0000021759 UST Incident Number (if known
Site Name: Southeastern Freight Lines, Inc. – Kinston, NC

Site Street Address: 159 Hwy 11 South

City/Town: Kinston Zip Code: 28504 County: Lenoir

Description of Geographical Data Point (e.g., diesel fill port): UST Pit

Location Method (GPS, topographical map, other): Google

Latitude (decimal degrees): 35.22053 N Longitude (decimal degrees): -77.64590 W

2. Information about Contacts Associated with the Leaking UST
UST Owner/operator/property owner: Southeastern Freight Lines, Inc.
Address: 159 Hwy 11 South, Kinston, NC 28504 Tel.: [phone]

Consultant/Analytical Laboratory: Terraquest Environmental Consultants, P.C.
Address: 100 E. Ruffin Street, Mebane, NC 27302 Tel: [phone]
Email: [e-mail]

Analytical Laboratory: Eurofins Test America, Pensacola
Address: 3355 McLemore Drive, Pensacola, FL 32514 Tel: [phone]
Email: [e-mail]

Contractor: Guardian Fueling Technologies Tel: [phone]
Address: 9452 Philips Highway, Suite 2 Jacksonville, FL 32256

2. Information about Release: Groundwater indicates release. No known discrete incident or quantity.

B. Site History and Characterization
1. Provide UST owner and operator information

The USTs were owned and operated by Southeastern Freight Lines, Inc.. See Section A-2.
Southeastern Freight Lines, Inc. – Kinston, NC – UST Closure Report
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2. Provide UST information (inclusive of all USTs, currently and historically in place at facility).

3. Provide non-UST information.

No non-UST release incidents are known.

4. Describe relation of location of current UST system to historical UST releases, non-UST
releases, and off-site releases.

No prior releases are known.

4. Provide a brief description of site characteristics (including status of facility (active or inactive),
land use of site and surrounding area, water supply, topography, vegetation, surface water,
wells, buildings, surface cover, soil type, depth to and nature of bedrock, depth to groundwater,
direction of groundwater flow, etc.)

The site is an active truck transport facility. Land usage in the surrounding vicinity is a mixture of
commercial, agricultural, and residential. A gas station, Lighthouse Food Mart No. 110 (closed -
NCDWM-UST Incident No.: 31302) is located to the north. Farmland surrounds the property in all
other directions. A Piggly Wiggly grocery store is located further to the northeast and a solar farm
is located to the south/southwest.

Prior investigation for the Lighthouse Food Mart No. 110 (Kilcoyne and Grubbs, 2004) release
incident identified a production water supply well operated by the Deep Run Water Corporation.
The Deep Run Well #7 provides water to the majority of residences and commercial properties in
the surrounding area and is located approximately 950 feet northeast of the release area. A
2,000-foot well head protection area (WHPA) has been established for the well in accordance with
42 United States Code (USC) 300h-7(e). The WHPA encompasses the site property. Five other
potable wells were identified within 1,500 feet of the site. Only one of those wells is used as a
sole source of potable water; the other properties are connected to the Deep Run Well #7.

According to the Geologic Map of North Carolina, the site overlies the Peedee Formation of the
Coastal Plain Physiographic Province. The Peedee Formation is primarily composed of sand,
clayey sands, and clays (Brown, et al., 1985). On a regional scale, the Coastal Plain is characterized
by land with little relief and some areas of low relief hills and valleys. The local topography is
characterized by relatively flat topography with little relief. The entire area surrounding 1,000
feet of the site is mapped at 25 five feet above sea level. Local topography is depicted in Figure
1.

While no perennial surface water body was noted within 500 feet of the site, drainage ditches
were noted along Highway 11 and 55. The closest perennial surface water body is the Neuse River
located approximately 6,700 feet north of the site as shown on Figure 1.

Tank Id Product Name Capacity stallation Daerm Close DatCommercial Regulated Tank Constr Name Release Discovered
1 Oil, New/Used/Mix 550 12/31/87 4/26/21 Y Y Single Wall Steel yes
2 Other, Non-Petroleum 550 12/1/87 N N Single Wall FRP no
Southeastern Freight Lines, Inc. – Kinston, NC – UST Closure Report
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Soil within the UST basin was logged as a SAND (SC), mostly gray to brown, loose, medium to fine-
grained sand with little clay. Groundwater was noted in the bottom (7’) of the excavation basin.
Groundwater flow at the site, based on assessment at the neighboring Lighthouse Food Mart No.
110, is directed to the east.

C. Closure Procedure
1. Describe preparations for closure including steps taken to notify authorities, permits obtained,
and steps taken to clean and purge the tanks.

Guardian Fueling Technologies performed tank preparations and removed the tank on April 26,
2021. The removed tank was taken to Foss Recycling of Lagrange, NC as detailed on the attached
receipt included in Appendix A.

2. Describe the closure procedure (For guidance, see the Guidelines, Section 5.0.), referencing site
and sampling location maps and cross-sections presented in Section F of this report. Clearly
state how the selection of sample types and locations was influenced by the nature of the
stored substance, any initial alarm or cause for suspicion, the type of backfill, the depth to
groundwater, and other factors appropriate for identifying the presence and source of a
release. Describe the condition of the UST system (pitting, holes, etc.) where it could be
observed. If it was necessary to install and sample monitoring well(s), explain.

Soil beneath the tank was saturated by groundwater and the tank was strapped to a concrete pad
directly beneath it prompting the collection of soil samples from the sidewalls of the excavation
basin at the locations shown on Figure 4. Those samples, CS1-CS4 were collected from each of
the four sidewalls at a depth of 18-24 inches below ground level (BGL).

Picture of the removed tank are attached as Appendix B and show a tank in good condition with
no holes noted. The tank was fiberglass-coated steel and measured four feet in diameter and was
six feet long
3. Note the amount of residual material pumped from the tank and describe the storage,
sampling and disposal of the residual material and the disposal of the tank, pumps and piping
(Refer to appendices with disposal manifests and certificate of tank disposal in Section H.).

Guardian Fueling Technologies performed tank preparations.

4. Document any soil excavation activities.

No soil was excavated as part of the UST closure.

D. Site Investigation
1. Describe field screening:

The samples were retrieved by Terraquest personnel donning a new pair of disposable nitrile
gloves and placed into sealable bags to allow a representative headspace to accrue. Each sample
was screened with a photoionization device (PID). None of the samples registered a value
greater than zero on the PID.

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2. Document soil sampling information:

UST Closure Soil Sampling

Soils were placed into sealable plastic bags and screened with a PID. A representative sample was
then placed into the appropriate laboratory container and labeled. All samples were analyzed by
Terraquest using a SiteLab UVF Trilogy machine for Total Petroleum Hydrocarbons as Gasoline
Range Organics (GRO) and Diesel Range Organics (DRO). Per discussions with the NCDWM-UST
Washington Regional Office, soil samples were also submitted to an NC-certified laboratory for
analysis per 8270E PAH, lead, and chromium.

Sample IDs, depths, dates, and analytical results are listed in Table 1. Sample locations are
depicted on Figure 4.

3. Document groundwater and surface water sampling information (Refer to tables and
appendices provided in Sections G and H.), including:

Groundwater was not sampled during closure.

4. Document quality-control measure information

Soil:
UST closure grab soil samples were collected from the track-hoe bucket. All samples were
collected by Terraquest personnel donning new disposable nitrile gloves. Samples were then
placed into laboratory containers, preserved with acid as required and packed on ice pending
onsite lab analysis. Chain-of-Custody documentation was maintained for each sample.

5. Describe soil and groundwater investigation results:

Soil:
All UST closure soil samples were analyzed utilizing UVF technology targeting TPH GRO and DRO
and for 8270 PAH, chromium, and lead. Those results reported no TPH Action Level exceedances
and no Soil to Groundwater Maximum Soil Contaminant Concentration (STG MSCC) exceedances
in any sample.

Sample IDs, depths, dates, and analytical results are listed in Table 1. Sample locations are
depicted in Figure 4. The analytical report is provided in Appendix C.

Groundwater:
No investigation conducted. Petro odor noted.

Southeastern Freight Lines, Inc. – Kinston, NC – UST Closure Report
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E. Conclusions

Following excavation and offsite disposal of a 550-gallon waste oil UST at the Southeastern
Freight Lines, Inc. facility in Kinston, NC, groundwater was encountered in the excavation basin.
Soil samples were collected around the sidewall of the excavation in the vadose zone. Those
samples did not reveal actionable concentrations of petroleum-type compounds. Groundwater
has not been investigated.

Terraquest Environmental Consultants, P.C. is licensed to practice geology and engineering in North
Carolina. The geology certification number of the corporation is C-291. The engineering certification
number of the corporation is C-4634. Engineering is practiced out of the Cary, NC office.

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C.

Ryan D. Kerins Michael J. Brown, P.G.
Project Manager President

Table of Contents

Tables: Table 1 Summary of Soil Sampling Results

Figures: Figure 1 Site Location Map
Figure 2 Site Vicinity Map
Figure 3 Site Layout Map
Figure 4 UST Closure Soil Sample Map

Appendix: Appendix A Tank Disposal Receipt
Appendix B UST Closure Pictures
Appendix C Analytical Reports

References

Brown, et al, 1985, Geologic Map of North Carolina, North Carolina Department of Natural Resources
and Community Development, 1:500,000 scale.

Kilcoyne, J. and Grubbs, J., Terraquest Environmental Consultants, P.C. Limited Site Assessment Report
(Phase I & II) LIGHTHOUSE FOOD MART #110, October 26, 2004

TABLES

Table 1Date: 6/3/21
UVF GROUVF DRO6010D6010D8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAH8270 PAHSample ID Date Collected Sample depth (feet)CS1 4/27/2021 1.5-2 <20 <4 4.25 2.75 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344 < 0.0344CS24/27/2021 1.5-2 <20 <4 3.81 2.54 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345 < 0.0345CS34/27/2021 1.5-2 <20 <4 5.04 3.02 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351 < 0.0351CS44/27/2021 1.5-2 <20 <4 4.21 3.35 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349 < 0.0349TPH Action Level 50 100 5.4 270 8.2 11 940 0.35 0.096 1.20 6,400 12 39 0.17 290 47 3.4 0.16 56 270 0.004 3.6Residential MSCC 47 400 940 469 4,600 0.88 0.088 0.88 469 9 88 0.088 620 620 0.88 313 469 469 20 63Notes:1. All results in mg/kg. 2. Bold denotes a compound detection.
3. Shading denotes a TPH Action Level or Soil-to-groundwater MSCC violation. 4. "<" = less than sample detection limit
5. "MSCC" = Maximum Soil Contaminant Concentration
Analytical Method
Contaminant of Concern
AcenaphtheneIncident Name: Southeastern Freight Lines, Inc. Kinston, NC Incident No.: not assignedSUMMARY OF SOIL SAMPLING RESULTS
Gasoline Range OrganicsSoil-to-groundwater MSCC FluoreneIndeno[1,2,3-cd]pyreneBenzo[a]pyreneBenzo[b]fluorantheneBenzo[g,h,i]peryleneBenzo[k]fluorantheneBenzo[a]anthraceneDiesel Range OrganicsChromiumLeadFluorantheneChryseneDibenz(a,h)anthraceneAcenaphthyleneAnthraceneFacility ID No: 00-0-0000021759
1-Methylnaphthalene2-MethylnaphthalenePyreneNaphthalenePhenanthrene

FIGURES

ENVIRONMENTAL CONSULTANTS, P.C.

APPENDIX A

APPENDIX B

Appendix B
Southeastern Freight Lines, Inc. – Kinston, NC – UST Closure Report Pictures
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Access cap on top of UST. Opened for vac truck to remove waste.
Appendix B
Southeastern Freight Lines, Inc. – Kinston, NC – UST Closure Report Pictures
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UST T1, 550-gallon waste oil tank. In-situ. Note straps holding tank down onto
concrete pad.
Appendix B
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Waste oil floor drain in building prior to abandonment. Product line that connects
to subject UST is shown on the right side of the box closest to the shoe.
Appendix B
Southeastern Freight Lines, Inc. – Kinston, NC – UST Closure Report Pictures
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Waste oil floor drain. Product line connecting to subject UST is filled with
concrete.
Appendix B
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Removed subject UST. 6-foot length.
Appendix B
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Removed subject UST. 4-foot diameter.
Appendix B
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Subject UST basin with tank removed. Product line capped off on sidewall
with orange cone overhead. Note groundwater in tank basin.
Appendix B
Southeastern Freight Lines, Inc. – Kinston, NC – UST Closure Report Pictures
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Floor waste drain abandoned by filling with concrete.

APPENDIX C

ANALYTICAL REPORT
Eurofins TestAmerica, Pensacola
3355 McLemore Drive
Pensacola, FL 32514
Tel: [phone]
Laboratory Job ID: 400-202726-1
Client Project/Site: 159 Hwy 11 Kinston Southeastern Freight
For:
Terraquest Environmental Consultants, PC
100 E. Ruffin Street
Mebane, North Carolina 27302
Attn: Jonathan Grubs
Authorized for release by:
5/12/2021 5:43:17 PM
Chad Bechtold, Project Manager
[phone]
[e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
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Table of Contents
Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Laboratory Job ID: 400-202726-1
Page 2 of 22 Eurofins TestAmerica, Pensacola5/12/2021
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .2
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .11
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .12
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .13
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .21
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
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Case Narrative
Client: Terraquest Environmental Consultants, PC Job ID: 400-202726-1
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Job ID: 400-202726-1
Laboratory: Eurofins TestAmerica, Pensacola
Narrative
Job Narrative
400-202726-1
Comments
No additional comments.
Receipt
The samples were received on 4/29/2021 9:18 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 5.4º C.
GC/MS Semi VOA
Method 8270E: The continuing calibration verification (CCV) associated with batch 400-531130 recovered outside acceptance criteria, low
biased, for Acenaphthene, Pyrene, Benzo[g,h,i]perylene, Acenaphthylene and Fluorene. A reporting limit (RL) standard was analyzed, and
the target analyte was detected. Since the associated samples were non-detect for this analyte, the data have been reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Metals
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Organic Prep
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins TestAmerica, PensacolaPage 3 of 22 5/12/2021
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Detection Summary
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Client Sample ID: CS1 Lab Sample ID: 400-202726-1
☼Chromium
RL
0.997 mg/Kg
MDL
0.309
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA14.25 6010D
☼Lead 0.997 mg/Kg0.219 Total/NA12.75 6010D
Client Sample ID: CS2 Lab Sample ID: 400-202726-2
☼Chromium
RL
1.00 mg/Kg
MDL
0.311
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.81 6010D
☼Lead 1.00 mg/Kg0.221 Total/NA12.54 6010D
Client Sample ID: CS3 Lab Sample ID: 400-202726-3
☼Chromium
RL
1.01 mg/Kg
MDL
0.313
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA15.04 6010D
☼Lead 1.01 mg/Kg0.222 Total/NA13.02 6010D
Client Sample ID: CS4 Lab Sample ID: 400-202726-4
☼Chromium
RL
1.00 mg/Kg
MDL
0.310
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA14.21 6010D
☼Lead 1.00 mg/Kg0.220 Total/NA13.35 6010D
Eurofins TestAmerica, Pensacola
This Detection Summary does not include radiochemical test results.
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Sample Summary
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Lab Sample ID Client Sample ID Matrix Collected Received Asset ID
400-202726-1 CS1 Solid 04/27/21 10:32 04/29/21 09:18
400-202726-2 CS2 Solid 04/27/21 10:30 04/29/21 09:18
400-202726-3 CS3 Solid 04/27/21 10:28 04/29/21 09:18
400-202726-4 CS4 Solid 04/27/21 10:26 04/29/21 09:18
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Lab Sample ID: 400-202726-1Client Sample ID: CS1
Matrix: SolidDate Collected: 04/27/21 10:32
Percent Solids: 93.0Date Received: 04/29/21 09:18
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene 0.0344 U 0.344 0.0344 mg/Kg ☼05/06/21 12:56 05/11/21 15:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Acenaphthylene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Anthracene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Benzo[a]anthracene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Benzo[a]pyrene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Benzo[b]fluoranthene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Benzo[g,h,i]perylene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Benzo[k]fluoranthene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Chrysene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Dibenz(a,h)anthracene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Fluoranthene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Fluorene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Indeno[1,2,3-cd]pyrene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Naphthalene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Phenanthrene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼Pyrene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼1-Methylnaphthalene 0.0344 U
0.344 0.0344 mg/Kg 05/06/21 12:56 05/11/21 15:50 1☼2-Methylnaphthalene 0.0344 U
2-Fluorobiphenyl 74 27-127 05/06/21 12:56 05/11/21 15:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)62 05/06/21 12:56 05/11/21 15:50 115-136
Terphenyl-d14 (Surr)100 05/06/21 12:56 05/11/21 15:50 124-146
Method: 6010D - Metals (ICP)
RL MDL
Chromium 4.25 0.997 0.309 mg/Kg ☼04/30/21 09:53 04/30/21 19:38 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.997 0.219 mg/Kg 04/30/21 09:53 04/30/21 19:38 1☼Lead 2.75
General Chemistry
RL MDL
Percent Solids 93.0 0.01 0.01 %05/01/21 10:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %05/01/21 10:58 1Percent Moisture 7.0
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Lab Sample ID: 400-202726-2Client Sample ID: CS2
Matrix: SolidDate Collected: 04/27/21 10:30
Percent Solids: 93.6Date Received: 04/29/21 09:18
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene 0.0345 U 0.345 0.0345 mg/Kg ☼05/06/21 12:56 05/10/21 16:44 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Acenaphthylene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Anthracene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Benzo[a]anthracene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Benzo[a]pyrene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Benzo[b]fluoranthene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Benzo[g,h,i]perylene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Benzo[k]fluoranthene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Chrysene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Dibenz(a,h)anthracene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Fluoranthene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Fluorene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Indeno[1,2,3-cd]pyrene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Naphthalene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Phenanthrene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼Pyrene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼1-Methylnaphthalene 0.0345 U
0.345 0.0345 mg/Kg 05/06/21 12:56 05/10/21 16:44 1☼2-Methylnaphthalene 0.0345 U
2-Fluorobiphenyl 43 27-127 05/06/21 12:56 05/10/21 16:44 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)50 05/06/21 12:56 05/10/21 16:44 115-136
Terphenyl-d14 (Surr)60 05/06/21 12:56 05/10/21 16:44 124-146
Method: 6010D - Metals (ICP)
RL MDL
Chromium 3.81 1.00 0.311 mg/Kg ☼04/30/21 09:53 04/30/21 19:53 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 0.221 mg/Kg 04/30/21 09:53 04/30/21 19:53 1☼Lead 2.54
General Chemistry
RL MDL
Percent Solids 93.6 0.01 0.01 %05/01/21 10:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %05/01/21 10:58 1Percent Moisture 6.4
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Lab Sample ID: 400-202726-3Client Sample ID: CS3
Matrix: SolidDate Collected: 04/27/21 10:28
Percent Solids: 92.3Date Received: 04/29/21 09:18
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene 0.0351 U 0.351 0.0351 mg/Kg ☼05/06/21 12:56 05/10/21 17:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Acenaphthylene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Anthracene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Benzo[a]anthracene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Benzo[a]pyrene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Benzo[b]fluoranthene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Benzo[g,h,i]perylene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Benzo[k]fluoranthene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Chrysene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Dibenz(a,h)anthracene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Fluoranthene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Fluorene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Indeno[1,2,3-cd]pyrene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Naphthalene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Phenanthrene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼Pyrene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼1-Methylnaphthalene 0.0351 U
0.351 0.0351 mg/Kg 05/06/21 12:56 05/10/21 17:08 1☼2-Methylnaphthalene 0.0351 U
2-Fluorobiphenyl 48 27-127 05/06/21 12:56 05/10/21 17:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)57 05/06/21 12:56 05/10/21 17:08 115-136
Terphenyl-d14 (Surr)69 05/06/21 12:56 05/10/21 17:08 124-146
Method: 6010D - Metals (ICP)
RL MDL
Chromium 5.04 1.01 0.313 mg/Kg ☼04/30/21 09:53 04/30/21 19:57 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.01 0.222 mg/Kg 04/30/21 09:53 04/30/21 19:57 1☼Lead 3.02
General Chemistry
RL MDL
Percent Solids 92.3 0.01 0.01 %05/01/21 10:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %05/01/21 10:58 1Percent Moisture 7.7
Eurofins TestAmerica, Pensacola
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Client Sample Results
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Lab Sample ID: 400-202726-4Client Sample ID: CS4
Matrix: SolidDate Collected: 04/27/21 10:26
Percent Solids: 93.1Date Received: 04/29/21 09:18
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
RL MDL
Acenaphthene 0.0349 U 0.349 0.0349 mg/Kg ☼05/06/21 12:56 05/10/21 17:33 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Acenaphthylene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Anthracene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Benzo[a]anthracene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Benzo[a]pyrene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Benzo[b]fluoranthene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Benzo[g,h,i]perylene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Benzo[k]fluoranthene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Chrysene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Dibenz(a,h)anthracene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Fluoranthene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Fluorene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Indeno[1,2,3-cd]pyrene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Naphthalene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Phenanthrene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼Pyrene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼1-Methylnaphthalene 0.0349 U
0.349 0.0349 mg/Kg 05/06/21 12:56 05/10/21 17:33 1☼2-Methylnaphthalene 0.0349 U
2-Fluorobiphenyl 44 27-127 05/06/21 12:56 05/10/21 17:33 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Nitrobenzene-d5 (Surr)54 05/06/21 12:56 05/10/21 17:33 115-136
Terphenyl-d14 (Surr)60 05/06/21 12:56 05/10/21 17:33 124-146
Method: 6010D - Metals (ICP)
RL MDL
Chromium 4.21 1.00 0.310 mg/Kg ☼04/30/21 09:53 04/30/21 20:01 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1.00 0.220 mg/Kg 04/30/21 09:53 04/30/21 20:01 1☼Lead 3.35
General Chemistry
RL MDL
Percent Solids 93.1 0.01 0.01 %05/01/21 10:58 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
0.01 0.01 %05/01/21 10:58 1Percent Moisture 6.9
Eurofins TestAmerica, Pensacola
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Definitions/Glossary
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Qualifiers
GC/MS Semi VOA
Qualifier Description
U Indicates the analyte was analyzed for but not detected.
Qualifier
Metals
Qualifier Description
U Indicates the analyte was analyzed for but not detected.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins TestAmerica, Pensacola
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Surrogate Summary
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Prep Type: Total/NAMatrix: Solid
Lab Sample ID Client Sample ID (27-127)(15-136)(24-146)
FBP NBZ TPHL
74 62 100400-202726-1
Percent Surrogate Recovery (Acceptance Limits)
CS1
43 50 60400-202726-2 CS2
48 57 69400-202726-3 CS3
44 54 60400-202726-4 CS4
67 67 86LCS 400-530668/2-A Lab Control Sample
73 72 94LCSD 400-530668/3-A Lab Control Sample Dup
71 58 97MB 400-530668/1-A Method Blank
Surrogate Legend
FBP = 2-Fluorobiphenyl
NBZ = Nitrobenzene-d5 (Surr)
TPHL = Terphenyl-d14 (Surr)
Eurofins TestAmerica, Pensacola
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QC Association Summary
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
GC/MS Semi VOA
Prep Batch: 530668
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3546400-202726-1 CS1 Total/NA
Solid 3546400-202726-2 CS2 Total/NA
Solid 3546400-202726-3 CS3 Total/NA
Solid 3546400-202726-4 CS4 Total/NA
Solid 3546MB 400-530668/1-A Method Blank Total/NA
Solid 3546LCS 400-530668/2-A Lab Control Sample Total/NA
Solid 3546LCSD 400-530668/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 531130
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 530668400-202726-2 CS2 Total/NA
Solid 8270E 530668400-202726-3 CS3 Total/NA
Solid 8270E 530668400-202726-4 CS4 Total/NA
Analysis Batch: 531271
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 8270E 530668400-202726-1 CS1 Total/NA
Solid 8270E 530668MB 400-530668/1-A Method Blank Total/NA
Solid 8270E 530668LCS 400-530668/2-A Lab Control Sample Total/NA
Solid 8270E 530668LCSD 400-530668/3-A Lab Control Sample Dup Total/NA
Metals
Prep Batch: 529815
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 3050B400-202726-1 CS1 Total/NA
Solid 3050B400-202726-2 CS2 Total/NA
Solid 3050B400-202726-3 CS3 Total/NA
Solid 3050B400-202726-4 CS4 Total/NA
Solid 3050BMB 400-529815/1-A Method Blank Total/NA
Solid 3050BLCS 400-529815/2-A Lab Control Sample Total/NA
Analysis Batch: 530032
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid 6010D 529815400-202726-1 CS1 Total/NA
Solid 6010D 529815400-202726-2 CS2 Total/NA
Solid 6010D 529815400-202726-3 CS3 Total/NA
Solid 6010D 529815400-202726-4 CS4 Total/NA
Solid 6010D 529815MB 400-529815/1-A Method Blank Total/NA
Solid 6010D 529815LCS 400-529815/2-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 529967
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Solid Moisture400-202726-1 CS1 Total/NA
Solid Moisture400-202726-2 CS2 Total/NA
Solid Moisture400-202726-3 CS3 Total/NA
Solid Moisture400-202726-4 CS4 Total/NA
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Method: 8270E - Semivolatile Organic Compounds (GC/MS)
Client Sample ID: Method BlankLab Sample ID: MB 400-530668/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 531271 Prep Batch: 530668
RL MDL
Acenaphthene 0.0330 U 0.330 0.0330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Acenaphthylene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Anthracene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Benzo[a]anthracene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Benzo[a]pyrene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Benzo[b]fluoranthene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Benzo[g,h,i]perylene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Benzo[k]fluoranthene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Chrysene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Dibenz(a,h)anthracene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Fluoranthene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Fluorene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Indeno[1,2,3-cd]pyrene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Naphthalene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Phenanthrene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 1Pyrene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 11-Methylnaphthalene
0.0330 U 0.03300.330 mg/Kg 05/06/21 12:55 05/11/21 14:46 12-Methylnaphthalene
2-Fluorobiphenyl 71 27-127 05/11/21 14:46 1
MB MB
Surrogate
05/06/21 12:55
Dil FacPreparedAnalyzedQualifierLimits%Recovery
58 05/06/21 12:55 05/11/21 14:46 1Nitrobenzene-d5 (Surr)15-136
97 05/06/21 12:55 05/11/21 14:46 1Terphenyl-d14 (Surr)24-146
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-530668/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 531271 Prep Batch: 530668
Acenaphthene 2.00 1.326 mg/Kg 66 50 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Acenaphthylene 2.00 1.338 mg/Kg 67 50 -120
Anthracene 2.00 1.605 mg/Kg 80 52 -120
Benzo[a]anthracene 2.00 1.574 mg/Kg 79 55 -120
Benzo[a]pyrene 2.00 1.696 mg/Kg 85 54 -120
Benzo[b]fluoranthene 2.00 1.648 mg/Kg 82 55 -120
Benzo[g,h,i]perylene 2.00 1.639 mg/Kg 82 45 -120
Benzo[k]fluoranthene 2.00 1.751 mg/Kg 88 52 -120
Chrysene 2.00 1.664 mg/Kg 83 54 -120
Dibenz(a,h)anthracene 2.00 1.443 mg/Kg 72 49 -120
Fluoranthene 2.00 1.557 mg/Kg 78 49 -120
Fluorene 2.00 1.487 mg/Kg 74 47 -120
Indeno[1,2,3-cd]pyrene 2.00 1.475 mg/Kg 74 47 -120
Naphthalene 2.00 1.301 mg/Kg 65 41 -120
Phenanthrene 2.00 1.587 mg/Kg 79 50 -120
Pyrene 2.00 1.514 mg/Kg 76 54 -120
1-Methylnaphthalene 2.00 1.313 mg/Kg 66 40 -120
2-Methylnaphthalene 2.00 1.311 mg/Kg 66 40 -120
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Method: 8270E - Semivolatile Organic Compounds (GC/MS) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-530668/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 531271 Prep Batch: 530668
2-Fluorobiphenyl 27 -127
Surrogate
67
LCS LCS
Qualifier Limits%Recovery
67Nitrobenzene-d5 (Surr)15 -136
86Terphenyl-d14 (Surr)24 -146
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-530668/3-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 531271 Prep Batch: 530668
Acenaphthene 2.00 1.529 mg/Kg 76 50 -120 14 30
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits LimitRPD
RPD
Acenaphthylene 2.00 1.504 mg/Kg 75 50 -120 12 30
Anthracene 2.00 1.800 mg/Kg 90 52 -120 11 30
Benzo[a]anthracene 2.00 1.780 mg/Kg 89 55 -120 12 30
Benzo[a]pyrene 2.00 1.928 mg/Kg 96 54 -120 13 30
Benzo[b]fluoranthene 2.00 1.884 mg/Kg 94 55 -120 13 30
Benzo[g,h,i]perylene 2.00 1.811 mg/Kg 91 45 -120 10 30
Benzo[k]fluoranthene 2.00 1.999 mg/Kg 100 52 -120 13 30
Chrysene 2.00 1.881 mg/Kg 94 54 -120 12 30
Dibenz(a,h)anthracene 2.00 1.582 mg/Kg 79 49 -120 9 30
Fluoranthene 2.00 1.728 mg/Kg 86 49 -120 10 30
Fluorene 2.00 1.689 mg/Kg 84 47 -120 13 30
Indeno[1,2,3-cd]pyrene 2.00 1.621 mg/Kg 81 47 -120 9 30
Naphthalene 2.00 1.488 mg/Kg 74 41 -120 13 30
Phenanthrene 2.00 1.777 mg/Kg 89 50 -120 11 30
Pyrene 2.00 1.761 mg/Kg 88 54 -120 15 30
1-Methylnaphthalene 2.00 1.498 mg/Kg 75 40 -120 13 30
2-Methylnaphthalene 2.00 1.484 mg/Kg 74 40 -120 12 30
2-Fluorobiphenyl 27 -127
Surrogate
73
LCSD LCSD
Qualifier Limits%Recovery
72Nitrobenzene-d5 (Surr)15 -136
94Terphenyl-d14 (Surr)24 -146
Method: 6010D - Metals (ICP)
Client Sample ID: Method BlankLab Sample ID: MB 400-529815/1-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 530032 Prep Batch: 529815
RL MDL
Chromium 0.308 U 0.994 0.308 mg/Kg 04/30/21 09:53 04/30/21 18:25 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.219 U 0.2190.994 mg/Kg 04/30/21 09:53 04/30/21 18:25 1Lead
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-529815/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 530032 Prep Batch: 529815
Chromium 100 93.85 mg/Kg 94 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Eurofins TestAmerica, Pensacola
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QC Sample Results
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Method: 6010D - Metals (ICP) (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-529815/2-A
Matrix: Solid Prep Type: Total/NA
Analysis Batch: 530032 Prep Batch: 529815
Lead 100 96.03 mg/Kg 96 80 -120
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec.
Limits
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-202726-1
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Client Sample ID: CS1 Lab Sample ID: 400-202726-1
Matrix: SolidDate Collected: 04/27/21 10:32
Date Received: 04/29/21 09:18
Analysis Moisture TMP05/01/21 10:581 TAL PEN529967
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: CS1 Lab Sample ID: 400-202726-1
Matrix: SolidDate Collected: 04/27/21 10:32
Percent Solids: 93.0Date Received: 04/29/21 09:18
Prep 3546 BKL05/06/21 12:56 TAL PEN530668
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.48 g 1 mL
Analysis 8270E 1 531271 05/11/21 15:50 S1B TAL PENTotal/NA
Prep 3050B 529815 04/30/21 09:53 NET TAL PENTotal/NA .5392 g 50 mL
Analysis 6010D 1 530032 04/30/21 19:38 JTW TAL PENTotal/NA
Client Sample ID: CS2 Lab Sample ID: 400-202726-2
Matrix: SolidDate Collected: 04/27/21 10:30
Date Received: 04/29/21 09:18
Analysis Moisture TMP05/01/21 10:581 TAL PEN529967
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: CS2 Lab Sample ID: 400-202726-2
Matrix: SolidDate Collected: 04/27/21 10:30
Percent Solids: 93.6Date Received: 04/29/21 09:18
Prep 3546 BKL05/06/21 12:56 TAL PEN530668
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.35 g 1 mL
Analysis 8270E 1 531130 05/10/21 16:44 S1B TAL PENTotal/NA
Prep 3050B 529815 04/30/21 09:53 NET TAL PENTotal/NA .5330 g 50 mL
Analysis 6010D 1 530032 04/30/21 19:53 JTW TAL PENTotal/NA
Client Sample ID: CS3 Lab Sample ID: 400-202726-3
Matrix: SolidDate Collected: 04/27/21 10:28
Date Received: 04/29/21 09:18
Analysis Moisture TMP05/01/21 10:581 TAL PEN529967
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: CS3 Lab Sample ID: 400-202726-3
Matrix: SolidDate Collected: 04/27/21 10:28
Percent Solids: 92.3Date Received: 04/29/21 09:18
Prep 3546 BKL05/06/21 12:56 TAL PEN530668
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.27 g 1 mL
Analysis 8270E 1 531130 05/10/21 17:08 S1B TAL PENTotal/NA
Prep 3050B 529815 04/30/21 09:53 NET TAL PENTotal/NA .5366 g 50 mL
Analysis 6010D 1 530032 04/30/21 19:57 JTW TAL PENTotal/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-202726-1
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Client Sample ID: CS4 Lab Sample ID: 400-202726-4
Matrix: SolidDate Collected: 04/27/21 10:26
Date Received: 04/29/21 09:18
Analysis Moisture TMP05/01/21 10:581 TAL PEN529967
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA
Client Sample ID: CS4 Lab Sample ID: 400-202726-4
Matrix: SolidDate Collected: 04/27/21 10:26
Percent Solids: 93.1Date Received: 04/29/21 09:18
Prep 3546 BKL05/06/21 12:56 TAL PEN530668
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15.22 g 1 mL
Analysis 8270E 1 531130 05/10/21 17:33 S1B TAL PENTotal/NA
Prep 3050B 529815 04/30/21 09:53 NET TAL PENTotal/NA .5368 g 50 mL
Analysis 6010D 1 530032 04/30/21 20:01 JTW TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-529815/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3050B NET04/30/21 09:53 TAL PEN529815
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA .5030 g 50 mL
Analysis 6010D 1 530032 04/30/21 18:25 JTW TAL PENTotal/NA
Client Sample ID: Method Blank Lab Sample ID: MB 400-530668/1-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL05/06/21 12:55 TAL PEN530668
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E 1 531271 05/11/21 14:46 S1B TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-529815/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3050B NET04/30/21 09:53 TAL PEN529815
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA .5002 g 50 mL
Analysis 6010D 1 530032 04/30/21 18:29 JTW TAL PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-530668/2-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL05/06/21 12:55 TAL PEN530668
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E 1 531271 05/11/21 15:07 S1B TAL PENTotal/NA
Eurofins TestAmerica, Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-202726-1
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-530668/3-A
Matrix: SolidDate Collected: N/A
Date Received: N/A
Prep 3546 BKL05/06/21 12:55 TAL PEN530668
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 15 g 1 mL
Analysis 8270E 1 531271 05/11/21 15:29 S1B TAL PENTotal/NA
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
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Method Summary
Job ID: 400-202726-1Client: Terraquest Environmental Consultants, PC
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Method Method Description LaboratoryProtocol
SW8468270ESemivolatile Organic Compounds (GC/MS)TAL PEN
SW8466010DMetals (ICP)TAL PEN
EPAMoisturePercent Moisture TAL PEN
SW8463050BPreparation, Metals TAL PEN
SW8463546Microwave Extraction TAL PEN
Protocol References:
EPA = US Environmental Protection Agency
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
TAL PEN = Eurofins TestAmerica, Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins TestAmerica, Pensacola
Page 19 of 22 5/12/2021
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Accreditation/Certification Summary
Client: Terraquest Environmental Consultants, PC Job ID: 400-202726-1
Project/Site: 159 Hwy 11 Kinston Southeastern Freight
Laboratory: Eurofins TestAmerica, Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)314State 12-31-21
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
Moisture Solid Percent Moisture
Moisture Solid Percent Solids
Eurofins TestAmerica, Pensacola
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1234567
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Login Sample Receipt Checklist
Client: Terraquest Environmental Consultants, PC Job Number: 400-202726-1
Login Number: 202726
Question Answer Comment
Creator: Conrady, Hank W
List Source: Eurofins TestAmerica, Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.5.4°C IR-9
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
N/AContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins TestAmerica, Pensacola
Page 22 of 22 5/12/2021
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0

UVF TRILOGY ANALYTICAL REPORT
Project Name: 159 Hwy 11 Kinston, NC
Project Number: 06821

Standard Technical Procedures

The UVF TRILOGY instrument is a fixed-wavelength fluorometer but uses deep UV LEDS to detect
monoaromatic and polyaromatic hydrocarbons.
SITELAB’s CAL-025 GRO Module is used to detect volatile petroleum hydrocarbons in the C6 to C10
range. This test matches well to EPA Methods for GRO, BTEX, BPH or VOC’s using GC/FID
instrumentation.
SITELAB’s CAL-042 EDRO Module is used to detect petroleum hydrocarbons in the C10 to C36 diesel and
oil range. This test matches well to EPA methods for TPH, EPH, DRO, and others using GC-FID
instrumentation.
Prior to field usage, the UVF TRILOGY is calibrated with five calibration standard solutions per targeted
analyte.
Soil samples are weighed to the nearest gram (i.e. 5.0 g) and added to a 1-ounce HDPE Nalgene bottle
with a measured amount of laboratory grade methanol to the nearest mL (i.e. 10 mL) to create a sample
extract. After addition of both the soil and methanol, the bottle is agitated for several minutes. Next,
the sample rests for several minutes allowing for the soil and methanol extract to separate.
After ample resting time, the methanol extract is collected with a syringe. A filter is connected to the
end of the syringe and dispensed into a clean sample test tube. The test tube is labeled with sample ID
and extract dilution factor (i.e. 2X).
Known amounts of extract are pipetted into a second test tube and diluted with methanol. The sample
ID and dilution factor are labeled on the test tube (i.e. 100X).
Samples are placed into a clean cuvette and carefully inserted into the selected UV Module. Prior to
analyzing the sample, the stored calibration that matches the UV Module being used, is selected. The
UVF TRILOGY produces a result that when multiplied to the dilution factor equals the true TPH value.
Quenching occurs when the detector is swamped by too many or certain type of hydrocarbons,
producing low or negative concentrations. The sample is tested at multiple dilutions to confirm the
results are linear and accurate.
Solvent blank samples are periodically analyzed to confirm the solvent is clean and the calibration of the
machine is maintained.

UVF Analytical Report
Project Name 159 Hwy 11 Kinston, NC
Project Number 06821
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
CS1 1.5-2 4/27/2021 DRO 40 <4 4 mg/kg
CS1 1.5-2 4/27/2021 GRO 40 <20 20 mg/kg
Wednesday, April 28, 2021 Page 1 of 4
Project Name 159 Hwy 11 Kinston, NC
Project Number 06821
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
CS2 1.5-2 4/27/2021 DRO 40 <4 4 mg/kg
CS2 1.5-2 4/27/2021 GRO 40 <20 20 mg/kg
Wednesday, April 28, 2021 Page 2 of 4
Project Name 159 Hwy 11 Kinston, NC
Project Number 06821
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
CS3 1.5-2 4/27/2021 DRO 40 <4 4 mg/kg
CS3 1.5-2 4/27/2021 GRO 40 <20 20 mg/kg
Wednesday, April 28, 2021 Page 3 of 4
Project Name 159 Hwy 11 Kinston, NC
Project Number 06821
Method UVF Trilogy
Sample Name Sample Depth Sample Date Analyte Name Dilution Result MDL Units
CS4 1.5-2 4/27/2021 DRO 40 <4 4 mg/kg
CS4 1.5-2 4/27/2021 GRO 40 <20 20 mg/kg
Wednesday, April 28, 2021 Page 4 of 4