WA-26944_38117_CA_RPTS_20150218_LSA

Kash & Karry #11 Page 1 February 13, 2015

2315 Kings Road Extension
Shelby, North Carolina 28152
(O) 704.482.2111
(F) 704.482.4335
[e-mail]
A. Site Information

1. Site Identification

Date of Report: February 13, 2015

Facility ID: 00-0-0000002950 UST Incident Number: 38117

Site Name: Kash & Karry #11

Address: 4115 Old Tar Road

City: Winterville State: North Carolina Zip Code: 28590

County: Pitt

Description of Geographical Data Point: UST Basin

Location Method: GPS

Latitude: 35°N 33’ 3.0204” Longitude: 77°W 23’ 2.5686”

2. Information about Contacts Associated with the Leaking UST System:

UST Owner: Kash & Karry, Inc.

Address: PO Box 924, 202 Arlington Blvd., Suite W

City: Greenville State: North Carolina Zip Code: 27835-0924

Telephone: [phone]

UST Operator/Occupant: Kash & Karry #11

Address: 4115 Old Tar Road

City: Greenville State: North Carolina Zip Code: 28590

Telephone: [phone]

Kash & Karry #11 Page 2 February 13, 2015

2315 Kings Road Extension
Shelby, North Carolina 28152
(O) 704.482.2111
(F) 704.482.4335
[e-mail]

Property Owner: Charles R. Hardee & Wayne G. Hardee Etal

Address: 202 E. Arlington Blvd., Suite W.

City: Greenville State: North Carolina Zip Code: 27858

Telephone: N/A

Consultant: Blue Ridge Environmental Services, Inc.

Address: 2315 Kings Road Extension

City: Shelby State: North Carolina Zip Code: 28152

Telephone: [phone]

Analytical Laboratory: Shealy Environmental Services, INC.

State Certification No.: 329

Address: 106 Vantage Point Drive West Columbia, SC 29172

Telephone: [phone]

3. Information about Release:

Date Discovered: August 30, 2010

Estimated Quantity of Release: Unknown

Cause of Release: Leaking UST System

Source of Release: UST System

Size and Contents of UST System (s) from which the release occurred: (Table-1)

Kash & Karry #11 Page 3 February 13, 2015

2315 Kings Road Extension
Shelby, North Carolina 28152
(O) 704.482.2111
(F) 704.482.4335
[e-mail]
B. Site History and Background

The Kash & Karry #11 site is located at 4115 Old Tar Road in Winterville, North
Carolina. The site is currently owned by Wayne G. Hardee and Charles R. Hardee
ETAL of Greenville, North Carolina. A gasoline station/convenience store is located
onsite and currently does not distribute gasoline as the USTs are in temporary closure.
A release occurred at the site on August 30, 2010 and the amount of product released
is unknown. The location of the UST basin is illustrated on Figure 2. For detailed
information about the UST system refer to Table 1 UST/AST System and Other Release
Information and Table - 2 UST/AST Owner/Operator and Other Responsible Party
Information.

C. Receptor Information

A site reconnaissance of the surrounding area was conducted by Blue Ridge personnel
on January 21, 2015. In addition, Blue Ridge passed out water supply well (WSWs)
questionnaires to all property occupants located within 500 feet of the subject site. Two
WSWs (WSW-1 & WSW-2) were identified during the site reconnaissance conducted.
WSW-1 is located approximately 349 feet from the source area at the New Beginnings
Community Church. The well system was found to be empty at the time of the
reconnaissance and appeared to be connected to public water. WSW-2 is located 751
feet from the source area at the Plant and See Nursery. The location of the WSWs is
illustrated on Figure 3. Of the two WSWs identified, WSW-1 was found to be inactive,
while WSW-2 was noted to be currently in-service primarily for irrigation usage.

During the site reconnaissance Blue Ridge observed water meters at almost all
residences. Public water is available to properties located within a 1,500 foot radius of
the site. Underground utilities on or adjacent to the subject property include
underground water, gas, electric, fiber optic and phone lines. Adjacent property owners
are noted on Table-3 Adjacent Property Owners. A Limited Site Assessment Risk
Classification and Land Use Form is included as Appendix B.

D. Site Geology/Hydrogeology

According to soil descriptions from the installation of the LSA monitoring wells MW-1
through MW-4, the soils underlying the subject site consist predominately of grey to
sandy clay to brown clayey sand. Please refer to Appendix C for additional lithological
descriptions. Two unnamed drainage features which flow into Fork Swamp are located
approximately 1,073 feet south/southwest and 1,205 feet northeast of the source area.
The measured depths to groundwater in monitor wells MW-1 through MW-4 on January
22, 2015 ranged between 2.21 feet bgl at MW-2 to 5.03 feet bgl at MW-4. A

Kash & Karry #11 Page 4 February 13, 2015

2315 Kings Road Extension
Shelby, North Carolina 28152
(O) 704.482.2111
(F) 704.482.4335
[e-mail]
groundwater contour map depicting aquifer flow is enclosed as Figure 5. Based on the
groundwater elevations obtained on January 22, 2015 groundwater flow is calculated to
the east.

E. Sampling Results

Limited Site Assessment Activities

On October 28, 2014 Blue Ridge installed monitoring well MW-1 adjacent to the UST
basin. The well was completed to 12 feet below grade level. A soil sample was collected
at 1 foot bgl during the installation of MW-1. The soil sample was laboratory analyzed
according to EPA Method 8260 and MADEP Method VPH. Laboratory results of the soil
sample collected at 1 foot indicated detectable contaminant concentrations of Benzene
(0.29 mg/kg) and MTBE (0.44 mg/kg) above the soil-to-water Maximum Soil
Contaminant Concentration (MSCC). Soil analytical results are summarized in Table-5
Select Summary of Soil Analytical Laboratory Results. Please refer to Figure 5 for soil
analytical results at site specific locations.

On October 28, 2014 Blue Ridge gauged and sampled monitoring well MW-1. A
groundwater sample was obtained and laboratory analyzed according to EPA Method
6200B, EPA Method 3030C and MADEP Method VPH. The laboratory results of the
groundwater sample collected on October 28, 2014 from MW-1 revealed detectable
concentrations of Benzene (20,000 ug/L), Toluene (39,000 ug/L), Ethylbenzene (5,400
ug/L), Xylenes (23,600 ug/L), MTBE (1,600 ug/L), Naphthalene (920 ug/L), n-
Propylbenzene (530 ug/L), 1,3,5-Trimethylbenzene (980 ug/L) and 1,2,4-
Trimethylbenzene (3,700 ug/L) above the North Carolina Groundwater Quality
Standards (GWQS). In addition the reported concentration of Benzene exceeded the
Gross Contamination Level (GCL). Because the groundwater results of MW-1 were
above the North Carolina Gross Contaminate Levels a Phase II LSA was completed.

On January 21, 2015, Blue Ridge mobilized back to the site and installed monitoring
wells MW-2, 3 and 4. On January 22, 2015 Blue Ridge gauged and sampled monitoring
wells MW-2 through MW-4. A groundwater sample was obtained and laboratory
analyzed according to EPA Method 6200B and MADEP Method VPH. The laboratory
results of the groundwater samples collected on January 22, 2015 from MW-2 through
MW-4 revealed concentrations of Benzene, MTBE and Naphthalene that exceeded the
North Carolina GWQS from the groundwater sample collected from MW-4. All other
remaining constituents analyzed were below the GWQS in the groundwater samples
collected on January 22, 2015. Groundwater analytical results are summarized in Table-
6 Summary of Groundwater Sampling Results. Please refer to Figure 7 for groundwater
analytical results at site specific locations. A copy of the laboratory analytical data is

Kash & Karry #11 Page 5 February 13, 2015

2315 Kings Road Extension
Shelby, North Carolina 28152
(O) 704.482.2111
(F) 704.482.4335
[e-mail]
included as Appendix D.

F. Conclusions

• Two WSWs (WSW-1 & WSW-2) were identified during the site reconnaissance
conducted. WSW-1 is inactive and located approximately 349 feet from the
source area. WSW-2 is currently in-service primarily for irrigation usage and is
located 751 feet from the source area. After discussions with the NC DENR
Project Manager, it was decided not to sample the nursery well at this time.
• Public water is available to all occupants located within a 1,500 foot radius of the
subject site.
• Two unnamed drainage features which flow into Fork Swamp are located
approximately 1,073 feet south/southwest and 1,205 feet northeast of the source
area.
• The source area is not located within a designated well head protection area.
• A soil sample collected at 1 ft. indicated a violation of the soil-to-water MSCC for
Benzene (0.29 mg/kg) and MTBE (0.44 mg/kg).
• Laboratory results of the groundwater sample collected from MW-1 revealed
detectable concentrations of Benzene, Toluene, Ethylbenzene, Xylenes, MTBE,
Naphthalene, n-Propylbenzene, 1,3,5-Trimethylbenzene and 1,2,4-
Trimethylbenzene that exceeded the GWQS.
• A reported concentration of Benzene (20,000 ug/L) in MW-1 exceeded the GCL.
• Laboratory results of the groundwater sample collected from MW-4 revealed
detectable concentrations of Benzene, MTBE and Naphthalene that exceeded
the GWQS.
• A reported concentration of Benzene (20,000 ug/L) in MW-1 exceeded the GCL.
• Based on the information presented in this report, it appears additional
assessment may be warranted. Furthermore it is recommended that the site be
ranked “Intermediate Risk” due to the concentration of Benzene reported in MW-
1.

Kash & Karry #11 Page 6 February 13, 2015

2315 Kings Road Extension
Shelby, North Carolina 28152
(O) 704.482.2111
(F) 704.482.4335
[e-mail]

Enclosures
Figures
1. Site Vicinity Map
2. Site Map
3. Tax Map
4. Zoning Map
5. Groundwater Contour Map
6. Soil Contaminant Map
7. Groundwater Contaminant Map

Tables
1. UST/AST System and Other Release Information
2. UST/AST Owner/Operator and Other Responsible Party Information
3. Adjacent Property Owners
4. Monitoring Well and Remediation Well Construction Information
5. Select Summary of Soil Analytical Laboratory Results
6. Select Summary of Groundwater Sampling Results

Appendices
Appendix A: Quality Assurance/Quality Control Procedures Drilling and Field Activities
Protocol
Appendix B: LSA Risk Classification and Land Use Form
Appendix C: Monitoring Well Construction Record
Appendix D: Laboratory Analytical Data and Chain of Custody Records
Figure 1
SITE VICINITY MAP North
Client:
Project:
Location:
Approximate Scale
Date: January 27, 2015
Charles Hardee
Kash & Karry #11
4115 Old Tar Road
Winterville, NC 28590
1’’ = 1,111
Site
0 1,111
0 1122 FT.MW-1Kash & Karry #114115 Old Tar RoadWinterville, North Carolina 28590Pitt CountyUST Incident Number: 38117USTAREA2315 Kings Road Ext.Shelby, North Carolina 28152704-482-2111Fax [phone]Email: [e-mail] & Karry #11Figure 2Site MapCanopyGrassGrassAsphaltFuel DispensersOld Tar RoadConcreteGrassGrass AsphaltMW-2MW-4XXXMW-3Underground Water Line
Underground Water Line AsphaltFence
Figure 4
ZONING MAP North
Client:
Project:
Location:
Approximate Scale
Date: January 27, 2015
Charles Hardee
Kash & Karry #11
4115 Old Tar Road
Winterville, NC 28590
1’’ = 700’
0 700
42344
59518 44165
Figure 3
TAX MAP North
Client:
Project:
Location:
Approximate Scale
Date: January 27, 2015
Charles Hardee
Kash & Karry #11
4115 Old Tar Road
Winterville, NC 28590
1’’ = 700’
42344
0 700
= Inactive Water Supply Well Location
WSW-2
= Active Water Supply Well Location
1,500 Ft.
WSW-1
500 Ft.
0 1122 FT.MW-1Kash & Karry #114115 Old Tar RoadWinterville, North Carolina 28590Pitt CountyUST Incident Number: 38117USTAREA2315 Kings Road Ext.Shelby, North Carolina 28152704-482-2111Fax [phone]Email: [e-mail] & Karry #11Figure 6Soil ContaminantMapCanopyGrassGrassFuel DispensersOld Tar RoadConcreteGrassGrass AsphaltMW-2MW-4XXXMW-3Underground Water Line
Underground Water Line AsphaltFenceMW-1 (1')Benzene: 0.29 Mg/KgToluene: 0.85 Mg/KgEthylbenzene: 0.44 Mg/KgXylenes: 2.1 Mg/KgNaphthalene: 0.029 Mg/KgMTBE: 0.0170 Mg/KgAcetone: 0.070 Mg/Kg2-Butanoe (MEK): 0.021 Mg/KgIsopropylbenzene: 0.019 Mg/Kgn-Propylbenzene: 0.0470 Mg/KgStyrene: 0.0079 Mg/Kg1,2,4-Trimethylbenzene: 1.1 Mg/Kg1,3,5-Trimethylbenzene: 0.085 Mg/KgC5-C8 Aliphatics: 6.5 Mg/KgC9-C12 Aliphatics: 12 Mg/KgC9-C10 Aromatics: 4.1 Mg/Kg
0 1122 FT.MW-1Kash & Karry #114115 Old Tar RoadWinterville, North Carolina 28590Pitt CountyUST Incident Number: 38117USTAREA2315 Kings Road Ext.Shelby, North Carolina 28152704-482-2111Fax [phone]Email: [e-mail] & Karry #11Figure 7Groundwater ContaminantMapCanopyGrassGrassFuel DispensersOld Tar RoadConcreteGrassGrassMW-2MW-4XXXMW-3Underground Water Line
Underground Water LineFence MW-1 Benzene: 20,000 ug/LToluene: 39,000 ug/LEthylbenzene: 5,400 ug/LXylenes: 23,600 ug/LNaphthalene: 920 ug/LMTBE: 1,600 ug/Ln-Propylbenzene: 530 ug/L1,2,4-Trimethylbenzene: 3,700 ug/L1,3,5-Trimethylbenzene: 980 ug/LC5-C8 Aliphatics: 73,000 ug/LC9-C12 Aliphatics: 59,000 ug/LC9-C10 Aromatics: 11,000 ug/LMW-4Benzene: 5.50 ug/LNaphthalene: 14 ug/LMTBE: 38 ug/LIsopropylbenzene: 1.50 ug/Ln-Propylbenzene: 0.83 ug/Lsec-Butylbenzene: 0.54 ug/L Chloroform 1.30 ug/LC5-C8 Aliphatics: 76 ug/LMW-2Not DetectedMW-3MTBE: 1.70 ug/LPlease note only detectable constituents listed.MW-1 Sampled on October 28, 2015.MW-2 through MW-4 Sampled on January 22, 2015.
0 1122 FT.MW-1Kash & Karry #114115 Old Tar RoadWinterville, North Carolina 28590Pitt CountyUST Incident Number: 38117USTAREA2315 Kings Road Ext.Shelby, North Carolina 28152704-482-2111Fax [phone]Email: [e-mail] & Karry #11Figure 5Groundwater Contour MapCanopyGrassGrassAsphaltFuel DispensersOld Tar RoadConcreteGrassGrass AsphaltMW-2MW-4XXXMW-3Underground Water Line
Underground Water Line AsphaltFence97.0997.0796.6696.31Countour Interval Equals 0.20 feetElevations Shown in Feet
UST ID NumberCurrent/Last ContentsPrevious Contents Capacity (in gallons)Construction DetailsTank DimesionsDate Tank InstalledStatus of the USTWas release associated with the UST System?1 Gasoline None 4,000Steel Single Wall5'4" X 24' 1/1/1983Temporarily ClosedYes2 Gasoline None 4,000Steel Single Wall5'4" X 24' 1/1/1983Temporarily ClosedYes3 Gasoline None 4,000Steel Single Wall5'4" X 24' 1/1/1983Temporarily ClosedYes4 Gasoline None 4,000Steel Single Wall5'4" X 24' 1/1/1983Temporarily ClosedYes5 Gasoline None 4,000Steel Single Wall5'4" X 24' 1/1/1983Temporarily ClosedYesAST ID NumberCurrent/Last ContentsPrevious Contents Capacity (in gallons)Construction DetailsTank DimesionsDate Tank InstalledStatus of the USTWas release associated with the UST System?N/A1N/A N/A N/A N/A N/A N/A N/A N/A1N/A: Not ApplicableIncident NumberMaterial ReleasedDate of Release38117 Gasoline 8/30/2010Table 1 Kash & Karry #11UST/AST System and Other Release InformationDescription of ReleaseA release was discovered at the site on August 30, 2010.
UST ID Number WA-26942 Facility ID Number 00-0-0000002950
City State Zip Telephone Number
Greenville NC 27858 N/A1
City State Zip Telephone Number
Winterville NC 28590 [phone]
Incident Number
City State Zip Telephone Number
N/A N/A N/A N/A
1N/A: Not Applicable
N/A
4115 Old Tar Road
Name of Other Responsible Party Date of Release
N/A 8/30/2010
Street Address
38117
Street Address
Table 2
Kash and Karry #11
UST/AST Owner/Operator and Other Responsible Party
Information
Name of Owner Dates of Operation
Charles Hardee 1983 to Present
Street Address
202 E. Arlington Blvd., Suite W
Name of Operator Dates of Operation
Kash & Karry #11 1983 to Present
Parcel ID Property Owner Owner Address
42344 (Site)
Charles Hardee
&
Wayne G. Hardee
ETAL
202 Arlington Blvd., Suite W.
Greenville, NC 27858
49211 Walter Williams
3602 Highway 264 East
Greenville, NC 27834
31595 Andrews Management
Limited Partnership
P.O. Box 443
Battleboro, NC 27809
44165
Branch Banking
and
Trust
P.O. Box 167
Winston Salem, NC 27102
44015 Angela Stewart
4024 Old Tar Road
Winterville, NC 28590
04391 Stallings Investments LLC
1645 E. Arlington Blvd. Suite E
Greenville, NC 27858
49385
Collice
&
Ann Moore
LLC
P.O. Box 7183
Greenville, NC 27835
53096 James Bradley
P.O. Box 8559
Rocky Mount, NC 27804
56259 Wesley Chamberlain
113 C8 Sunshine Lane
Winterville, NC 28590
56258 Judy Nicholson
113 B Sunshine Lane
Winterville, NC 28590
56251 Jami Dickerson
109 C Sunshine Lane
Winterville, NC 28590
56250 Zelma Boyd Savage
109 B Sunshine Lane
Winterville, NC 28590
1: Keyed to Figure 3
Table 31
Adjacent Property Owners
Incident Number and Name: 38117/Kash & Karry #11Facility ID #:00-0-0000002950Well IDDate InstalledDate Water Level MeasuredWell Casing Diameter (in.)Well Casing Depth (ft. BGS) Screened Interval (ft.)Depth of Well (ft. BGS)Top of Casing Elevation (ft.)Depth to Water from top of Casing (ft.)Free Product Thickness (ft.)Groundwater Elevation (ft.)Comments10/28/20143.17N/A296.83 Strong Odor1/22/20152.91 N/A 97.09 Strong OdorMW-2 1/21/2015 1/22/2015 2 2.50 2.50-12.50 12.50 99.28 2.21N/A 97.07 N/AMW-3 1/21/2015 1/22/2015 2 2.50 2.50-12.50 12.50 100.79 4.13 N/A 96.66 N/AMW-4 1/21/2015 1/22/2015 2 2.50 2.50-12.50 12.50 101.34 5.03 N/A 96.31 N/A1: Keyed to Figure 52: N/A: Not ApplicableTable 41 Kash & Karry #11 Monitoring Well and Remediation Well Construction InformationMW-1 10/28/20142 2-12212 100.00
Sample IDDate CollectedSource AreaSample Depth (ft.)Incident PhaseMW-1 (1') 10/28/2014 UST Basin 1Phase 1 LSA0.290.85 0.44 2.1 0.0290.1700.070 0.021 0.019 0.0470 0.0079 1.1 0.085 6.5 12 4.10.0056 4.3 4.9 4.6 0.16 0.091 24 16 1.7 1.7 1.5 8.5 8.3 68 3,300 3418 1,200 1,560 3,129 313 350 14000 9385 1564 626 3128 782 782 939 9,386 469164 32,000 40,000 81,760 8,176 3,100 360,000 245,280 40,88016,350 81,760 20,440 20,440 24,528 245,280 12,2641: Keyed to Figure 6Concentraions in bold exceed soil to groundwater MSCC.Please note that only detectable and common constituents are noted.C9-C12 AliphaticsStyreneC9-C10 AromaticsC5-C8 AliphaticsAnalytical Method EPA METHOD 8260 1,2,4-TrimethylbenzeneNaphthalene MTBETable 51 Kash & Karry #11 Industrial/Commercial MSCC (mg/kg)Soil to groundwater MSCC (mg/kg)Residential MSCC (mg/kg)EthylbenzeneXylenesContaminant of Concern* (mg/kg)BenzeneTolueneSummary of Soil Sampling ResultsMADEP VPH Acetone2-Butanone (MEK)Isopropylbenzenen-propylbenzene1,3,5-Trimethylbenzene

Blue Ridge Environmental Services, Inc.

Quality Assurance/Quality Control Procedures
Drilling and Field Activities Protocol

Pre-Drilling Protocol

Blue Ridge will contact a commercial utilities location service a minimum of 48 hours (per location service
requirements) prior to mobilization of the drill crew to the project site. It will be the responsibility of the utilities
location service to locate and delineate (by marking the ground surface), to the extent possible, buried or
underground utilities which may be encountered during or impeded by drilling activities. This should include,
but may not be limited to: electrical power services, private and/or municipal water and sewer services,
telecommunication services, natural gas services, and/or other public or municipal utilities. Borehole locations
will not be made closer than 36" from surface delineated utilities. If closer proximity to delineated utilities is
required, bore hole advancement will be conducted by hand auger boring protocol.

Prior to commencement of drilling, the augers, down hole equipment and associated tools will be cleaned in a
designated decontamination control area using a steam cleaner or high pressure washer. Bulk soil material
which may remain inside or outside of the augers or tools will be removed. Augers will also be pressure
washed between each successive bore hole to remove any soil material from the preceding boring.

Before raising the drill rig mast, Blue Ridge drilling personnel will observe over-head conditions for the
presence of aerial mounted utilities, tree limbs, canopies, awnings, building overhangs or other structural
impedances to normal drill rig operations.

Drill Protocol and Techniques

Bore holes utilized in sub-surface intrusive investigations will be advanced using a trailer mounted Simco 2400
SK-1 drill rig equipped with 4.5 inch outside diameter solid stem augers or 3.25 inch hollow stem augers.

Where warranted, shallow boring hole advancement may require utilization of a steel hand auger equipped
with a 3" inside diameter barrel.

Soil Sampling Collection and Analysis

The sample preparation area at each bore hole location will be located as reasonably possible away from
running motors or where discharged vapors, exhaust and/or fumes may come in contact with the sample.
Towels, field meters, sample jars and other equipment will be placed such that they do not come into contact
BLUE RIDGE ENVIRONMENTAL SERVICES, INC.
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DRILLING AND FIELD ACTIVITIES PROTOCOL Page 2

with soil or other materials which may contaminate the sampled soils.

Unless specified by the client or by project requirements, soil samples will be collected at approximately 5 foot
intervals. Soil samples will be retrieved according to one of two sampling protocols (dependent upon project or
client requirements): (1) by split barrel sampling protocol or (2) from bulk soil material retrieved from the solid
stem auger following flight advancement.

In an effort to reduce cross contamination of samples, soil samples which are to be submitted for chemical
analysis will only be handled by the geologist using fresh, manufacturer clean, latex examination gloves.
Following retrieval, the soil sample from each interval will be split into roughly equal portions with one portion
subjected to field examination and classification by Blue Ridge geologic personnel and the remaining portion
placed into a glass sample container to await selection for chemical analysis.

Samples which are to be submitted for volatile constituent analysis will be thermally isolated by being placed
into the plastic ice chest.

After the sample is retrieved from the bore hole and placed into the sample container, the project name,
sampling interval, data and time will be noted on the container.

Soil Screening and Photoionization Detector

Soil samples collected from each sampling interval will be subjected to on site screening by head space
analytical method utilizing a Photovac brand portable photoionization detector (PID). Prior to the soil
screening, the PID will be calibrated in the field to 98.9 parts per million (ppm) using isobutylene calibration gas
per manufacturer's standards.

Soil screening will be conducted by placing a spilt portion of each sample collected from the specified sampling
interval into a resealable plastic bag. The bag is then placed aside to allow the head space air above the
sample to equilibrate. Following the anticipated equilibration interval, the probe of the PID is inserted through
the side of the sample bag and the resulting levels of volatile organic vapors recorded. PID levels are recorded
in parts per million (ppm) and may be an indication of the relative concentration of volatile organic compounds
in the soil.

Monitoring Well Construction Protocol

Monitoring well bore hole advancement will be conducted utilizing 3.25 inch inside diameter hollow stem auger.
For typical monitoring well construction, the bore hole will be advanced through the vadose zone (over burden
soil) into the saturated zone to approximately 10 feet below the water table thereby allowing approximately 10
feet of hydrostatic head within the well. The boring will be converted into a groundwater monitoring well by the
emplacement of 2 inch inside diameter schedule 40 PVC pipe (well screen and riser). The well screen will
have a manufacturer machine cut 0.010 inch slot width and will be emplaced so the top of the well screen will
be located above the anticipated seasonal high water table. The annular space surrounding the well screen
BLUE RIDGE ENVIRONMENTAL SERVICES, INC.
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will be backfilled utilizing an FX-2 filter sand (45 to 55 mm grain size) to approximately 2 feet above the top of
the well screen. The filter pack will be isolated by the emplacement of approximately 2 feet of bentonite pellets
and the bentonite seal will then be hydrated and allowed to seal. Following the bentonite seal hydration, the
remaining annular space will be backfilled to the surface grade utilizing a neat Portland Type II cement or
similar type grout. Typically the wells will be completed at grade level inside a traffic rated steel vault and the
well sealed using a water-tight locking pressure cap. Where it is possible, the well vault will be raised above
the existing surface grade approximately 1 inch to promote surface water run-off and reduce the potential for
standing water above the well head.

Monitoring Well Development

Blue Ridge will allow an anticipated time interval for the well bore to stabilize following construction (typically an
minimum of 72 hours). The monitoring well will then be developed by hand bailing utilizing a fresh manufacturer
clean polyvinyl bailer. Well development will be conducted until: approximately 5 well volumes of water have
been removed, the water is relatively silt and sediment "free", or until essentially dry.

Well development should be performed to accomplish the following:

1) To remove silt and sediment which may have entered the well during construction activities.

2) To remove mud cake and "smeared material@ on the bore hole walls from drilling.

3) To seat and grade the filter pack.

4) To promote hydraulic conductivity into the well bore.

Monitoring Well Gauging

Static water levels within each monitoring well will be measured utilizing a Slope Indicator Company electronic
Water Level Indicator model #51453. Measurements will be made from the top of the casing (riser) and
recorded to the nearest 0.01 foot.

Blue Ridge will electronically measure for the presence of free product in suspect wells utilizing a Keck
Instruments, Inc. electronic oil/water interface probe model #KIR 89. Where free product is indicated to be
present, the depth to the top of the product layer and the depth to the top of the water will be recorded.
Measurement will be made from the top of the well casing (riser) and recorded to the nearest 0.01 foot.

Monitoring wells will be gauged before performing sample collection events at other times that may be required
and warranted.

The water level indicator and the oil/water interface probe will be cleaned with a solution of laboratory grade
soap (Alconox) and distilled water, rinsed with distilled water, rinsed with methanol alcohol and finally rinsed
BLUE RIDGE ENVIRONMENTAL SERVICES, INC.
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with deionized water both before the first well is checked and between successive wells. Bailers used to
inspect the water surface will also be cleaned between successive wells using a solution of 5% tri-sodium
phosphate and water.

Surveying Monitoring Well Casing Elevations

To provide information regarding the elevation of the top of each well casing relative to an established data
point (bench mark), Blue Ridge geologic personnel will survey the top of each well casing if necessary. An on
site bench mark will be established with a given elevation of 100.00' and each well casing elevation will be
measured with respect to the bench mark. Measurements will be made from the lowest point of the well riser
and recorded to the nearest 0.01 foot. All water level measurements will be made from this point to provide
consistency in field measurements.

Groundwater Sampling

Whenever possible, prior to conducting the initial sample collection event for any given monitoring well, Blue
Ridge will allow an anticipated time (a minimum of 72 hours) for the well to stabilize following monitoring well
development.

Before conducting each sampling event, an attempt will be made to purge each well of a minimum of three
volumes of water or until the well becomes essentially dry. All wells will then be allowed to recharge in part or
in whole prior to sampling.

Groundwater samples will be collected by Blue Ridge personnel utilizing disposable manufacturer clean
polyvinyl bailers equipped with a bottom ball check valve. An inert string will be used to lower the bailer to the
water surface. The string will be replaced between successive samples. The sample will be collected by
gently lowering the bailer into the water, thereby reducing degasification and/or volatilization of the sample.
After the bailer is lowered into the water, the sample will be allowed to stabilize for approximately three
seconds, allowing the ball valve to close. Care will be taken not to overfill the bailer, allowing inspection of the
water surface upon removal of the bailer from the well. Once the bailer is removed, water samples will be
transferred to glass vials in such a manner as to reduce volatilization. To reduce the potential of sample cross
contamination, Blue Ridge personnel will don fresh disposable latex examination gloves
between each monitoring well sampling point and whenever contact with groundwater is possible.

Transportation of Samples to Laboratory

Before drilling activities are initiated, a plastic ice chest will be prepared for temporary soil and water sample
storage. Preparation will include placing ice packs into the ice chest for thermal isolation in an attempt to
preserve sample integrity. The cooler will be pre-chilled using blue ice, ice packs or similar items to provide
thermal isolation of the sample materials.

BLUE RIDGE ENVIRONMENTAL SERVICES, INC.
QA/QC PROCEDURES
DRILLING AND FIELD ACTIVITIES PROTOCOL Page 5

The maximum holding time for samples to be tested for volatile organics is 14 days. Therefore, samples will be
delivered to the laboratory and analyzed by the laboratory within this time frame. The laboratory has been
consulted regarding holding times.

If the samples are taken directly to the lab from the drill site, they will be held in the same pre-chilled cooler. If
the samples cannot be taken directly to the lab, they will be taken to Blue Ridge's office, where the sample
containers will be transferred immediately from the cooler to the assigned refrigerator, until such time that they
can be taken to the lab. When the samples are scheduled to be delivered to the lab, they will be transferred
from the refrigerator to a pre-chilled cooler until delivery to the lab has been made.

Blue Ridge Chain of Custody Protocol

For each set of samples collected from the specified project site, Blue Ridge will enter all samples, containers,
and ice chests into standard chain of custody protocol. A chain of custody form will be established for each
sampling event a includes the following information: (1) project name and location, (2) sampling personnel, (3)
project management personnel, (4) sample identification numbers, (5) sample collection date and time, (6)
sample matrix {soil or water}, (7) sample description, (8) preservatives utilized, (9) number of containers, (10)
requested parameters, (11) miscellaneous field or laboratory remarks, (12) and transference records.

The chain of custody form will accompany the samples through each phase of the delivery process.
Kash & Karry #11
Limited Site Assessment Risk Classification and Land Use Form
Part I - Groundwater/Surface water/Vapor Impacts
High Risk
1. Has the discharge or release contaminated any water supply well including any used for
non-drinking purposes? Yes/No
Two water supply wells (WSW-1 & WSW-2) were identified and located 349 and 751
feet from the source area. WSW-1 is inactive and WSW-2 is active for primarley
irrigation purposes.
2. Is a water supply well used for drinking water located within 1,000 feet of the source area
the discharge or release? Yes/No
Two water supply wells (WSW-1 & WSW-2) were identified and located 349 and 751
feet from the source area. WSW-1 is inactive and WSW-2 is active for primarley
irrigation purposes.
3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial
cooling water, filling swimming pools) located within 250 feet of the source area of the
release or discharge? Yes/No
Two water supply wells (WSW-1 & WSW-2) were identified and located 349 and 751
feet from the source area. WSW-1 is inactive and WSW-2 is active for primarley
irrigation purposes.
4. Does groundwater within 500 feet of the source area of the discharge or release have the
potential for future use in that there is no other source of water supply other than the
groundwater? Yes/No
5. Do vapors from the discharge or release pose a threat of explosion because of
accumulation of the vapors in a confined space or pose any other serious threat to public
health, public safety or the environment? Yes/No
If yes, describe.
6. Are there any other factors that would cause the discharge or release to pose an
imminent danger to public health, public safety, or the environment? Yes/No
If yes, describe.
1
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the discharge or
release? Yes/No
No surface water bodies are located within 500 feet of the site. However two unnamed
drainage features which flow into Fork Swamp are located approximately 1,073 feet
south/southwest and 1,205 feet northeast of the source area.
If yes, does the maximum groundwater contaminant concentration exceed the surface
water quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10?
8. Is the source area of the discharge or release located within a designated wellhead
protection area as defined in 42 USC 300h-7(e)? Yes/No
If yes, explain.
9. Is the discharge or release located in the Coastal Plain physiographic region as
designated on a map entitled "Geology of North Carolina" published by the Department in
1985? Yes/No
10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels established (see Table 7) by the Department? Yes/No
A reported concentration of Benzene (20,000 ug/L) in MW-1 exceeded the GCL.
2
Part II- Land Use
Property Containing Source Area of Discharge or Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences permanent or
temporary)? Yes/No
Explain: No, the property is a former gas station/convience store.
2. Does the property contain a school, daycare center, hospital, playground, park,
recreation area, church, nursing home, or other place of public assembly . Yes/No
Explain: No, the property is a former gas station/convience store.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space,
etc.) or industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? Yes/No
Explain: No, the property is a former gas station/convience store.
4. Do children visit the property? Yes/No
Explain: No, the property is an operating gas station/convience store
Is access to the property reliably restricted consistent with its use (e.g., by fences,
security personnel or both)? Yes/No
Explain: All property boundaries surrounding the site are unrestricted.
5. Do pavement, buildings, or other structures cap the contaminated soil? Yes/No
Describe: Soil is capped by asphalt and concrete.
If yes, what mechanisms are in place or can be put into place to ensure that the
contaminated soil will remain capped in the foreseeable future?
The maximum mechanism is in place to ensure the soil remains capped in the future.
6. What is the zoning status of the property?
The property is zoned CG.
3
7. Is the use of the property likely to change in the next 20 years?
Explain: No, the property is a former gas station/convience store.
Property Surrounding Source Area of Discharge or Release
The questions below pertain to the area within 1,500 feet of the source area of the discharge
or release (excludes property containing source area of the release)
8. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?
A residence is located approximately 217 feet to the east.
9. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home or other place
of public assembly?
Childtime Daycare is located approximately 229 feet to the west.
10. What is the zoning status of properties in the surrounding area?
Properties surrounding the site are zoned GB, O, OR, R-6 and RA-20
11. Briefly characterize the use and activities of the land in the surrounding area.
Properties surrounding the site are consistent with a mixture of comercial and
residential usage.
4
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Blue Ridge Environmental Services
2315 Kings Road Ext.
Shelby, NC 28152
Attention: Joe McMurray
PJ28053Lot Number:
K & K #11Project Name:
11/10/2014Date Completed:
Kelly M. Maberry
Project Manager
*PJ28053*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Blue Ridge Environmental Services
Lot Number: PJ28053
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Blue Ridge Environmental Services
Lot Number: PJ28053

Sample Number Sample ID Matrix Date Sampled Date Received
001 10/23/2014 1200MW-1 Solid 10/28/2014
002 10/23/2014 1310MW-1 Aqueous 10/28/2014
(2 samples)
Page: 3 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Blue Ridge Environmental Services
Lot Number: PJ28053

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 MW-1 Solid Acetone 8260B 70 ug/kg 5
001 MW-1 Solid Benzene 8260B 290 ug/kg 5
001 MW-1 Solid 2-Butanone (MEK)8260B 21 ug/kg 5
001 MW-1 Solid Ethylbenzene 8260B 440 ug/kg 5
001 MW-1 Solid Isopropylbenzene 8260B 19 ug/kg 5
001 MW-1 Solid Methyl tertiary butyl ether (MTBE)8260B 170 ug/kg 5
001 MW-1 Solid Naphthalene 8260B 29 ug/kg 6
001 MW-1 Solid n-Propylbenzene 8260B 47 ug/kg 6
001 MW-1 Solid Styrene 8260B 7.9 ug/kg 6
001 MW-1 Solid Toluene 8260B 850 ug/kg 6
001 MW-1 Solid 1,2,4-Trimethylbenzene 8260B 1100 ug/kg 6
001 MW-1 Solid 1,3,5-Trimethylbenzene 8260B 85 ug/kg 6
001 MW-1 Solid Xylenes (total)8260B 2100 ug/kg 6
001 MW-1 Solid C5 - C8 Aliphatics MADEP-VPH-6.5 mg/kg 7
001 MW-1 Solid C9 - C12 Aliphatics MADEP-VPH-12 mg/kg 7
001 MW-1 Solid C9 - C10 Aromatics MADEP-VPH-4.1 mg/kg 8
002 MW-1 Aqueous Benzene SM 6200B-20000 ug/L 9
002 MW-1 Aqueous Ethylbenzene SM 6200B-5400 ug/L 9
002 MW-1 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-1600 ug/L 9
002 MW-1 Aqueous Naphthalene SM 6200B-920 ug/L 9
002 MW-1 Aqueous n-Propylbenzene SM 6200B-530 ug/L 9
002 MW-1 Aqueous Toluene SM 6200B-39000 ug/L 10
002 MW-1 Aqueous 1,3,5-Trimethylbenzene (Mesitylene)SM 6200B-980 ug/L 10
002 MW-1 Aqueous 1,2,4-Trimethylbenzene SM 6200B-3700 ug/L 10
002 MW-1 Aqueous m+p - Xylenes SM 6200B-16000 ug/L 10
002 MW-1 Aqueous o - Xylenes SM 6200B-7600 ug/L 10
002 MW-1 Aqueous C5 - C8 Aliphatics MADEP-VPH-73000 ug/L 11
002 MW-1 Aqueous C9 - C12 Aliphatics MADEP-VPH-59000 ug/L 11
002 MW-1 Aqueous C9 - C10 Aromatics MADEP-VPH-11000 ug/L 12
002 MW-1 Aqueous Lead 6010C 0.31 mg/L 13
(30 detections)
Page: 4 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-001
10/23/2014 1200
10/28/2014
Solid
% Solids:85.8 10/28/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 11/05/2014 1611 DCS 60084 6.48
2 5035 8260B 50 11/06/2014 1645 DCS 60265 6.70
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Acetone 67-64-1 8260B 70 1ug/kg18
Benzene 71-43-2 8260B 290 2ug/kg220
Bromobenzene 108-86-1 8260B ND 1ug/kg4.5
Bromochloromethane 74-97-5 8260B ND 1ug/kg4.5
Bromodichloromethane 75-27-4 8260B ND 1ug/kg4.5
Bromoform 75-25-2 8260B ND 1ug/kg4.5
Bromomethane (Methyl bromide)74-83-9 8260B ND 1ug/kg4.5
2-Butanone (MEK)78-93-3 8260B 21 1ug/kg9.0
n-Butylbenzene 104-51-8 8260B ND 1ug/kg4.5
sec-Butylbenzene 135-98-8 8260B ND 1ug/kg4.5
tert-Butylbenzene 98-06-6 8260B ND 1ug/kg4.5
Carbon tetrachloride 56-23-5 8260B ND 1ug/kg4.5
Chlorobenzene 108-90-7 8260B ND 1ug/kg4.5
Chloroethane 75-00-3 8260B ND 1ug/kg4.5
Chloroform 67-66-3 8260B ND 1ug/kg4.5
Chloromethane (Methyl chloride)74-87-3 8260B ND 1ug/kg4.5
2-Chlorotoluene 95-49-8 8260B ND 1ug/kg4.5
4-Chlorotoluene 106-43-4 8260B ND 1ug/kg4.5
Dibromochloromethane 124-48-1 8260B ND 1ug/kg4.5
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/kg4.5
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/kg4.5
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/kg4.5
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/kg4.5
Dichlorodifluoromethane 75-71-8 8260B ND 1ug/kg4.5
1,1-Dichloroethane 75-34-3 8260B ND 1ug/kg4.5
1,2-Dichloroethane 107-06-2 8260B ND 1ug/kg4.5
1,1-Dichloroethene 75-35-4 8260B ND 1ug/kg4.5
cis-1,2-Dichloroethene 156-59-2 8260B ND 1ug/kg4.5
trans-1,2-Dichloroethene 156-60-5 8260B ND 1ug/kg4.5
1,2-Dichloropropane 78-87-5 8260B ND 1ug/kg4.5
1,3-Dichloropropane 142-28-9 8260B ND 1ug/kg4.5
2,2-Dichloropropane 594-20-7 8260B ND 1ug/kg4.5
1,1-Dichloropropene 563-58-6 8260B ND 1ug/kg4.5
cis-1,3-Dichloropropene 10061-01-5 8260B ND 1ug/kg4.5
trans-1,3-Dichloropropene 10061-02-6 8260B ND 1ug/kg4.5
Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/kg4.5
Ethylbenzene 100-41-4 8260B 440 2ug/kg220
2-Hexanone 591-78-6 8260B ND 1ug/kg9.0
Isopropylbenzene 98-82-8 8260B 19 1ug/kg4.5
p-Isopropyltoluene 99-87-6 8260B ND 1ug/kg4.5
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B 170 1ug/kg4.5
4-Methyl-2-pentanone 108-10-1 8260B ND 1ug/kg9.0
Methylene chloride 75-09-2 8260B ND 1ug/kg4.5
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-001
10/23/2014 1200
10/28/2014
Solid
% Solids:85.8 10/28/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
1 5035 8260B 1 11/05/2014 1611 DCS 60084 6.48
2 5035 8260B 50 11/06/2014 1645 DCS 60265 6.70
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Naphthalene 91-20-3 8260B 29 1ug/kg4.5
n-Propylbenzene 103-65-1 8260B 47 1ug/kg4.5
Styrene 100-42-5 8260B 7.9 1ug/kg4.5
1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 1ug/kg4.5
Tetrachloroethene 127-18-4 8260B ND 1ug/kg4.5
Toluene 108-88-3 8260B 850 2ug/kg220
1,2,3-Trichlorobenzene 87-61-6 8260B ND 1ug/kg4.5
1,2,4-Trichlorobenzene 120-82-1 8260B ND 1ug/kg4.5
1,1,1-Trichloroethane 71-55-6 8260B ND 1ug/kg4.5
1,1,2-Trichloroethane 79-00-5 8260B ND 1ug/kg4.5
Trichloroethene 79-01-6 8260B ND 1ug/kg4.5
Trichlorofluoromethane 75-69-4 8260B ND 1ug/kg4.5
1,2,3-Trichloropropane 96-18-4 8260B ND 1ug/kg4.5
1,2,4-Trimethylbenzene 95-63-6 8260B 1100 2ug/kg220
1,3,5-Trimethylbenzene 108-67-8 8260B 85 1ug/kg4.5
Vinyl acetate 108-05-4 8260B ND 1ug/kg4.5
Vinyl chloride 75-01-4 8260B ND 1ug/kg4.5
Xylenes (total)1330-20-7 8260B 2100 2ug/kg220
AcceptanceAcceptanceRun 2Run 1
Surrogate Q % Recovery Limits % Recovery LimitsQ
1,2-Dichloroethane-d4 85 53-142 78 53-142
Bromofluorobenzene 91 47-138 80 47-138
Toluene-d8 95 68-124 85 68-124
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-001
10/23/2014 1200
10/28/2014
Solid
% Solids:85.8 10/28/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 11/05/2014 0120 JJG 60008
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-6.5 1mg/kg3.2
C9 - C12 Aliphatics MADEP-VPH-12 1mg/kg3.2
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)87 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-001
10/23/2014 1200
10/28/2014
Solid
% Solids:85.8 10/28/2014 1939
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 11/05/2014 0120 JJG 60009
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-4.1 1mg/kg1.1
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)85 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-002
10/23/2014 1310
10/28/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 500 11/06/2014 0142 JJG 60106
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Benzene 71-43-2 SM 6200B-20 20000 1ug/L250
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L250
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L250
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L250
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L250
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L250
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L250
sec-Butylbenzene 135-98-8 SM 6200B-20 ND 1ug/L250
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L250
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L250
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L250
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L250
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L250
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L250
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L250
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L250
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L250
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L250
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L250
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L250
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L250
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L250
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L250
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L250
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L250
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L250
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L250
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L250
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L250
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L250
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L250
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L250
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L250
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L250
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 ND 1ug/L250
Ethanol 64-17-5 SM 6200B-20 ND 1ug/L50000
Ethylbenzene 100-41-4 SM 6200B-20 5400 1ug/L250
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L250
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 ND 1ug/L250
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L250
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 1600 1ug/L250
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L250
Naphthalene 91-20-3 SM 6200B-20 920 1ug/L250
n-Propylbenzene 103-65-1 SM 6200B-20 530 1ug/L250
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-002
10/23/2014 1310
10/28/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 500 11/06/2014 0142 JJG 60106
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Styrene 100-42-5 SM 6200B-20 ND 1ug/L250
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L250
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L250
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L250
Toluene 108-88-3 SM 6200B-20 39000 1ug/L250
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L250
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L250
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L250
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L250
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L250
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L250
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L250
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L250
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 980 1ug/L250
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 3700 1ug/L250
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L250
m+p - Xylenes 179601-23-1 SM 6200B-20 16000 1ug/L250
o - Xylenes 95-47-6 SM 6200B-20 7600 1ug/L250
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 99 70-130
Bromofluorobenzene 99 70-130
Toluene-d8 99 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-002
10/23/2014 1310
10/28/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 200 11/04/2014 0247 JJG 59878
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-73000 1ug/L15000
C9 - C12 Aliphatics MADEP-VPH-59000 1ug/L15000
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)110 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-002
10/23/2014 1310
10/28/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 200 11/04/2014 0247 JJG 59879
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-11000 1ug/L5000
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)110 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
PJ28053-002
10/23/2014 1310
10/28/2014
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3005A 6010C 1 11/03/2014 2053 BNW 10/31/2014 0901 59619
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Lead 7439-92-1 6010C 0.31 1mg/L0.010
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 14 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ60084-001
60084 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Acetone ND 11/05/2014 153320ug/kg1
Bromobenzene ND 11/05/2014 15335.0 ug/kg1
Bromochloromethane ND 11/05/2014 15335.0 ug/kg1
Bromodichloromethane ND 11/05/2014 15335.0 ug/kg1
Bromoform ND 11/05/2014 15335.0 ug/kg1
Bromomethane (Methyl bromide)ND 11/05/2014 15335.0 ug/kg1
2-Butanone (MEK)ND 11/05/2014 153310ug/kg1
sec-Butylbenzene ND 11/05/2014 15335.0 ug/kg1
n-Butylbenzene ND 11/05/2014 15335.0 ug/kg1
tert-Butylbenzene ND 11/05/2014 15335.0 ug/kg1
Carbon tetrachloride ND 11/05/2014 15335.0 ug/kg1
Chlorobenzene ND 11/05/2014 15335.0 ug/kg1
Chloroethane ND 11/05/2014 15335.0 ug/kg1
Chloroform ND 11/05/2014 15335.0 ug/kg1
Chloromethane (Methyl chloride)ND 11/05/2014 15335.0 ug/kg1
2-Chlorotoluene ND 11/05/2014 15335.0 ug/kg1
4-Chlorotoluene ND 11/05/2014 15335.0 ug/kg1
Dibromochloromethane ND 11/05/2014 15335.0 ug/kg1
1,2-Dibromoethane (EDB)ND 11/05/2014 15335.0 ug/kg1
1,3-Dichlorobenzene ND 11/05/2014 15335.0 ug/kg1
1,4-Dichlorobenzene ND 11/05/2014 15335.0 ug/kg1
1,2-Dichlorobenzene ND 11/05/2014 15335.0 ug/kg1
Dichlorodifluoromethane ND 11/05/2014 15335.0 ug/kg1
1,2-Dichloroethane ND 11/05/2014 15335.0 ug/kg1
1,1-Dichloroethane ND 11/05/2014 15335.0 ug/kg1
cis-1,2-Dichloroethene ND 11/05/2014 15335.0 ug/kg1
trans-1,2-Dichloroethene ND 11/05/2014 15335.0 ug/kg1
1,1-Dichloroethene ND 11/05/2014 15335.0 ug/kg1
1,3-Dichloropropane ND 11/05/2014 15335.0 ug/kg1
2,2-Dichloropropane ND 11/05/2014 15335.0 ug/kg1
1,2-Dichloropropane ND 11/05/2014 15335.0 ug/kg1
cis-1,3-Dichloropropene ND 11/05/2014 15335.0 ug/kg1
trans-1,3-Dichloropropene ND 11/05/2014 15335.0 ug/kg1
1,1-Dichloropropene ND 11/05/2014 15335.0 ug/kg1
Diisopropyl ether (IPE)ND 11/05/2014 15335.0 ug/kg1
2-Hexanone ND 11/05/2014 153310ug/kg1
Isopropylbenzene ND 11/05/2014 15335.0 ug/kg1
p-Isopropyltoluene ND 11/05/2014 15335.0 ug/kg1
Methyl tertiary butyl ether (MTBE)ND 11/05/2014 15335.0 ug/kg1
4-Methyl-2-pentanone ND 11/05/2014 153310ug/kg1
Methylene chloride ND 11/05/2014 15335.0 ug/kg1
Naphthalene ND 11/05/2014 15335.0 ug/kg1
n-Propylbenzene ND 11/05/2014 15335.0 ug/kg1
Styrene ND 11/05/2014 15335.0 ug/kg1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 15 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ60084-001
60084 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
1,1,2,2-Tetrachloroethane ND 11/05/2014 15335.0 ug/kg1
Tetrachloroethene ND 11/05/2014 15335.0 ug/kg1
1,2,3-Trichlorobenzene ND 11/05/2014 15335.0 ug/kg1
1,2,4-Trichlorobenzene ND 11/05/2014 15335.0 ug/kg1
1,1,1-Trichloroethane ND 11/05/2014 15335.0 ug/kg1
1,1,2-Trichloroethane ND 11/05/2014 15335.0 ug/kg1
Trichloroethene ND 11/05/2014 15335.0 ug/kg1
Trichlorofluoromethane ND 11/05/2014 15335.0 ug/kg1
1,2,3-Trichloropropane ND 11/05/2014 15335.0 ug/kg1
1,3,5-Trimethylbenzene ND 11/05/2014 15335.0 ug/kg1
Vinyl acetate ND 11/05/2014 15335.0 ug/kg1
Vinyl chloride ND 11/05/2014 15335.0 ug/kg1
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 91 47-138
1,2-Dichloroethane-d4 91 53-142
Toluene-d8 88 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 16 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ60084-002
60084 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Acetone 100 11/05/2014 145710310060-1401
Bromobenzene 49 11/05/2014 1457985053-1371
Bromochloromethane 48 11/05/2014 1457975070-1211
Bromodichloromethane 50 11/05/2014 14571005069-1211
Bromoform 51 11/05/2014 14571025061-1191
Bromomethane (Methyl bromide)59 11/05/2014 14571185010-1681
2-Butanone (MEK)110 11/05/2014 145710810057-1481
sec-Butylbenzene 52 11/05/2014 14571045037-1471
n-Butylbenzene 50 11/05/2014 14571005029-1521
tert-Butylbenzene 47 11/05/2014 1457955038-1491
Carbon tetrachloride 51 11/05/2014 14571035058-1361
Chlorobenzene 49 11/05/2014 1457985059-1291
Chloroethane 59 11/05/2014 14571185042-1631
Chloroform 48 11/05/2014 1457955071-1251
Chloromethane (Methyl chloride)58 11/05/2014 14571155034-1341
2-Chlorotoluene 48 11/05/2014 1457965053-1331
4-Chlorotoluene 48 11/05/2014 1457965053-1351
Dibromochloromethane 51 11/05/2014 14571015066-1191
1,2-Dibromoethane (EDB)52 11/05/2014 14571045074-1241
1,3-Dichlorobenzene 50 11/05/2014 1457995051-1341
1,4-Dichlorobenzene 48 11/05/2014 1457965052-1331
1,2-Dichlorobenzene 49 11/05/2014 1457985057-1311
Dichlorodifluoromethane 58 11/05/2014 14571155010-1571
1,2-Dichloroethane 48 11/05/2014 1457975067-1291
1,1-Dichloroethane 51 11/05/2014 14571025071-1271
cis-1,2-Dichloroethene 50 11/05/2014 14571005070-1221
trans-1,2-Dichloroethene 52 11/05/2014 14571035068-1311
1,1-Dichloroethene 52 11/05/2014 14571045069-1381
1,3-Dichloropropane 49 11/05/2014 1457985070-1301
2,2-Dichloropropane 52 11/05/2014 14571045059-1291
1,2-Dichloropropane 49 11/05/2014 1457995072-1241
cis-1,3-Dichloropropene 50 11/05/2014 14571005070-1261
trans-1,3-Dichloropropene 48 11/05/2014 1457965070-1241
1,1-Dichloropropene 51 11/05/2014 14571025060-1331
Diisopropyl ether (IPE)48 11/05/2014 1457965026-1431
2-Hexanone 110 11/05/2014 145710610054-1371
Isopropylbenzene 51 11/05/2014 14571025050-1361
p-Isopropyltoluene 51 11/05/2014 14571025036-1461
Methyl tertiary butyl ether (MTBE)48 11/05/2014 1457955070-1301
4-Methyl-2-pentanone 100 11/05/2014 145710110060-1341
Methylene chloride 48 11/05/2014 1457965070-1301
Naphthalene 49 11/05/2014 1457975054-1311
n-Propylbenzene 50 11/05/2014 14571005041-1441
Styrene 48 11/05/2014 1457975054-1361
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 17 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ60084-002
60084 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
1,1,2,2-Tetrachloroethane 49 11/05/2014 1457985069-1321
Tetrachloroethene 51 11/05/2014 14571025045-1501
1,2,3-Trichlorobenzene 49 11/05/2014 1457975040-1431
1,2,4-Trichlorobenzene 50 11/05/2014 1457995034-1451
1,1,1-Trichloroethane 49 11/05/2014 1457995063-1281
1,1,2-Trichloroethane 49 11/05/2014 1457995055-1281
Trichloroethene 51 11/05/2014 14571015062-1261
Trichlorofluoromethane 56 11/05/2014 14571135045-1381
1,2,3-Trichloropropane 48 11/05/2014 1457975067-1261
1,3,5-Trimethylbenzene 50 11/05/2014 1457995046-1391
Vinyl acetate 49 11/05/2014 1457985055-1281
Vinyl chloride 56 11/05/2014 14571125042-1321
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 89 47-138
1,2-Dichloroethane-d4 85 53-142
Toluene-d8 91 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 18 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ60106-001
60106 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Benzene ND 11/05/2014 20360.50 ug/L1
Bromobenzene ND 11/05/2014 20360.50 ug/L1
Bromochloromethane ND 11/05/2014 20360.50 ug/L1
Bromodichloromethane ND 11/05/2014 20360.50 ug/L1
Bromoform ND 11/05/2014 20360.50 ug/L1
Bromomethane (Methyl bromide)ND 11/05/2014 20360.50 ug/L1
tert-Butylbenzene ND 11/05/2014 20360.50 ug/L1
sec-Butylbenzene ND 11/05/2014 20360.50 ug/L1
n-Butylbenzene ND 11/05/2014 20360.50 ug/L1
Carbon tetrachloride ND 11/05/2014 20360.50 ug/L1
Chlorobenzene ND 11/05/2014 20360.50 ug/L1
Chloroethane ND 11/05/2014 20360.50 ug/L1
Chloroform ND 11/05/2014 20360.50 ug/L1
Chloromethane (Methyl chloride)ND 11/05/2014 20360.50 ug/L1
4-Chlorotoluene ND 11/05/2014 20360.50 ug/L1
2-Chlorotoluene ND 11/05/2014 20360.50 ug/L1
Dibromochloromethane ND 11/05/2014 20360.50 ug/L1
1,2-Dibromoethane (EDB)ND 11/05/2014 20360.50 ug/L1
Dibromomethane (Methylene bromide)ND 11/05/2014 20360.50 ug/L1
1,4-Dichlorobenzene ND 11/05/2014 20360.50 ug/L1
1,3-Dichlorobenzene ND 11/05/2014 20360.50 ug/L1
1,2-Dichlorobenzene ND 11/05/2014 20360.50 ug/L1
Dichlorodifluoromethane ND 11/05/2014 20360.50 ug/L1
1,2-Dichloroethane ND 11/05/2014 20360.50 ug/L1
1,1-Dichloroethane ND 11/05/2014 20360.50 ug/L1
trans-1,2-Dichloroethene ND 11/05/2014 20360.50 ug/L1
cis-1,2-Dichloroethene ND 11/05/2014 20360.50 ug/L1
1,1-Dichloroethene ND 11/05/2014 20360.50 ug/L1
2,2-Dichloropropane ND 11/05/2014 20360.50 ug/L1
1,3-Dichloropropane ND 11/05/2014 20360.50 ug/L1
1,2-Dichloropropane ND 11/05/2014 20360.50 ug/L1
trans-1,3-Dichloropropene ND 11/05/2014 20360.50 ug/L1
cis-1,3-Dichloropropene ND 11/05/2014 20360.50 ug/L1
1,1-Dichloropropene ND 11/05/2014 20360.50 ug/L1
Diisopropyl ether (IPE)ND 11/05/2014 20360.50 ug/L1
Ethanol ND 11/05/2014 2036100ug/L1
Ethylbenzene ND 11/05/2014 20360.50 ug/L1
Hexachlorobutadiene ND 11/05/2014 20360.50 ug/L1
Isopropylbenzene (Cumene)ND 11/05/2014 20360.50 ug/L1
p-Isopropyltoluene (p-Cymene)ND 11/05/2014 20360.50 ug/L1
Methyl tertiary butyl ether (MTBE)ND 11/05/2014 20360.50 ug/L1
Methylene chloride ND 11/05/2014 20360.50 ug/L1
Naphthalene ND 11/05/2014 20360.50 ug/L1
n-Propylbenzene ND 11/05/2014 20360.50 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 19 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ60106-001
60106 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Styrene ND 11/05/2014 20360.50 ug/L1
1,1,2,2-Tetrachloroethane ND 11/05/2014 20360.50 ug/L1
1,1,1,2-Tetrachloroethane ND 11/05/2014 20360.50 ug/L1
Tetrachloroethene ND 11/05/2014 20360.50 ug/L1
Toluene ND 11/05/2014 20360.50 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 11/05/2014 20360.50 ug/L1
1,2,4-Trichlorobenzene ND 11/05/2014 20360.50 ug/L1
1,2,3-Trichlorobenzene ND 11/05/2014 20360.50 ug/L1
1,1,2-Trichloroethane ND 11/05/2014 20360.50 ug/L1
1,1,1-Trichloroethane ND 11/05/2014 20360.50 ug/L1
Trichloroethene ND 11/05/2014 20360.50 ug/L1
Trichlorofluoromethane ND 11/05/2014 20360.50 ug/L1
1,2,3-Trichloropropane ND 11/05/2014 20360.50 ug/L1
1,2,4-Trimethylbenzene ND 11/05/2014 20360.50 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 11/05/2014 20360.50 ug/L1
Vinyl chloride ND 11/05/2014 20360.50 ug/L1
o - Xylenes ND 11/05/2014 20360.50 ug/L1
m+p - Xylenes ND 11/05/2014 20360.50 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 102 70-130
1,2-Dichloroethane-d4 98 70-130
Toluene-d8 99 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 20 of 39
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ60106-002
60106 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 51 11/05/2014 19091035070-1301
Bromobenzene 51 11/05/2014 19091025070-1301
Bromochloromethane 53 11/05/2014 19091075070-1301
Bromodichloromethane 52 11/05/2014 19091045070-1301
Bromoform 57 11/05/2014 19091135070-1301
Bromomethane (Methyl bromide)53 11/05/2014 19091065060-1401
tert-Butylbenzene 51 11/05/2014 19091035070-1301
sec-Butylbenzene 51 11/05/2014 19091025070-1301
n-Butylbenzene 52 11/05/2014 19091035070-1301
Carbon tetrachloride 53 11/05/2014 19091065070-1301
Chlorobenzene 51 11/05/2014 19091035070-1301
Chloroethane 52 11/05/2014 19091045042-1631
Chloroform 51 11/05/2014 19091015070-1301
Chloromethane (Methyl chloride)58 11/05/2014 19091165020-1581
4-Chlorotoluene 50 11/05/2014 19091015070-1301
2-Chlorotoluene 50 11/05/2014 19091005070-1301
Dibromochloromethane 52 11/05/2014 19091055070-1301
1,2-Dibromoethane (EDB)52 11/05/2014 19091035070-1301
Dibromomethane (Methylene bromide)52 11/05/2014 19091035070-1301
1,4-Dichlorobenzene 51 11/05/2014 19091015070-1301
1,3-Dichlorobenzene 51 11/05/2014 19091015070-1301
1,2-Dichlorobenzene 51 11/05/2014 19091025070-1301
Dichlorodifluoromethane 55 11/05/2014 19091095060-1401
1,2-Dichloroethane 52 11/05/2014 19091045070-1301
1,1-Dichloroethane 52 11/05/2014 19091045070-1301
trans-1,2-Dichloroethene 51 11/05/2014 19091015070-1301
cis-1,2-Dichloroethene 50 11/05/2014 19091015070-1301
1,1-Dichloroethene 51 11/05/2014 19091025070-1301
2,2-Dichloropropane 50 11/05/2014 19091005070-1301
1,3-Dichloropropane 52 11/05/2014 19091035070-1301
1,2-Dichloropropane 52 11/05/2014 19091035070-1301
trans-1,3-Dichloropropene 52 11/05/2014 19091035070-1301
cis-1,3-Dichloropropene 52 11/05/2014 19091055070-1301
1,1-Dichloropropene 51 11/05/2014 19091035070-1301
Diisopropyl ether (IPE)53 11/05/2014 19091055070-1301
Ethanol 5400 11/05/2014 1909108500040-1301
Ethylbenzene 52 11/05/2014 19091035070-1301
Hexachlorobutadiene 53 11/05/2014 19091055070-1301
Isopropylbenzene (Cumene)50 11/05/2014 19091015070-1301
p-Isopropyltoluene (p-Cymene)52 11/05/2014 19091035070-1301
Methyl tertiary butyl ether (MTBE)53 11/05/2014 19091055070-1301
Methylene chloride 49 11/05/2014 1909995070-1301
Naphthalene 49 11/05/2014 1909995050-1401
n-Propylbenzene 51 11/05/2014 19091015070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 21 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ60106-002
60106 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Styrene 52 11/05/2014 19091045070-1301
1,1,2,2-Tetrachloroethane 51 11/05/2014 19091025070-1301
1,1,1,2-Tetrachloroethane 52 11/05/2014 19091045070-1301
Tetrachloroethene 51 11/05/2014 19091015070-1301
Toluene 50 11/05/2014 19091015070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 53 11/05/2014 19091075070-1301
1,2,4-Trichlorobenzene 50 11/05/2014 1909995070-1301
1,2,3-Trichlorobenzene 50 11/05/2014 19091005070-1301
1,1,2-Trichloroethane 50 11/05/2014 19091005070-1301
1,1,1-Trichloroethane 52 11/05/2014 19091045070-1301
Trichloroethene 51 11/05/2014 19091035070-1301
Trichlorofluoromethane 56 11/05/2014 19091115060-1401
1,2,3-Trichloropropane 51 11/05/2014 19091025070-1301
1,2,4-Trimethylbenzene 51 11/05/2014 19091015070-1301
1,3,5-Trimethylbenzene (Mesitylene)51 11/05/2014 19091025070-1301
Vinyl chloride 52 11/05/2014 19091055060-1401
o - Xylenes 51 11/05/2014 19091035070-1301
m+p - Xylenes 51 11/05/2014 19091035070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 105 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 22 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:PQ60265-001
60265 5035
Analytical Method:8260B
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
Benzene ND 11/06/2014 1618250ug/kg50
Ethylbenzene ND 11/06/2014 1618250ug/kg50
Toluene ND 11/06/2014 1618250ug/kg50
1,2,4-Trimethylbenzene ND 11/06/2014 1618250ug/kg50
Xylenes (total)ND 11/06/2014 1618250ug/kg50
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 101 47-138
1,2-Dichloroethane-d4 100 53-142
Toluene-d8 107 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 23 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:PQ60265-002
60265 5035
Analytical Method:8260B
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/kg)(ug/kg)
Benzene 2500 11/06/2014 1506101250069-12350
Ethylbenzene 2600 11/06/2014 1506103250059-12850
Toluene 2600 11/06/2014 1506105250061-12950
1,2,4-Trimethylbenzene 2600 11/06/2014 1506104250047-13850
Xylenes (total)5100 11/06/2014 1506102500058-12850
Surrogate Q % Rec
Acceptance
Limit
Bromofluorobenzene 97 47-138
1,2-Dichloroethane-d4 96 53-142
Toluene-d8 105 68-124
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 24 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - MB
Batch:Prep Method:
Sample ID:PQ59878-001
59878 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
C5 - C8 Aliphatics ND 11/04/2014 000275ug/L1
C9 - C12 Aliphatics ND 11/04/2014 000275ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)111 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 25 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - LCS
Batch:Prep Method:
Sample ID:PQ59878-002
59878 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 77 11/03/2014 22451037570-1301
C9 - C12 Aliphatics 71 11/03/2014 2245957570-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 26 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - LCSD
Batch:Prep Method:
Sample ID:PQ59878-003
59878 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 75 11/03/2014 23241007570-1303.0 251
C9 - C12 Aliphatics 70 11/03/2014 2324937570-1301.7 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 27 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - MB
Batch:Prep Method:
Sample ID:PQ59879-001
59879 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
C9 - C10 Aromatics ND 11/04/2014 000225ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)110 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 28 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - LCS
Batch:Prep Method:
Sample ID:PQ59879-002
59879 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 26 11/03/2014 22451022570-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 29 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - LCSD
Batch:Prep Method:
Sample ID:PQ59879-003
59879 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 26 11/03/2014 23241022570-1300.00 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 30 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - MB
Batch:Prep Method:
Sample ID:PQ60008-001
60008 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
C5 - C8 Aliphatics ND 11/04/2014 19053.8 mg/kg1
C9 - C12 Aliphatics ND 11/04/2014 19053.8 mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 31 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - LCS
Batch:Prep Method:
Sample ID:PQ60008-002
60008 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
C5 - C8 Aliphatics 3.4 11/04/2014 1748923.8 70-1301
C9 - C12 Aliphatics 3.5 11/04/2014 1748943.8 70-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)98 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 32 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - LCSD
Batch:Prep Method:
Sample ID:PQ60008-003
60008 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C5 - C8 Aliphatics 3.6 11/04/2014 1826963.8 70-1304.5 251
C9 - C12 Aliphatics 3.7 11/04/2014 18261003.8 70-1305.9 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)104 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 33 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - MB
Batch:Prep Method:
Sample ID:PQ60009-001
60009 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Solid
Parameter Result Q PQL Units Analysis DateDil
C9 - C10 Aromatics ND 11/04/2014 19051.3 mg/kg1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 34 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - LCS
Batch:Prep Method:
Sample ID:PQ60009-002
60009 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/kg)(mg/kg)
C9 - C10 Aromatics 1.1 11/04/2014 1748881.3 70-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)100 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 35 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - LCSD
Batch:Prep Method:
Sample ID:PQ60009-003
60009 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Solid
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/kg)(mg/kg)
C9 - C10 Aromatics 1.2 11/04/2014 1826961.3 70-1308.7 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 36 of 39
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Level 1 Report v2.1
ICP-AES - MB
Batch:Prep Method:
Prep Date:
Sample ID:PQ59619-001
59619 3005A
10/31/2014 901Analytical Method:6010C
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Lead ND 11/03/2014 20410.010 mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 37 of 39
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Level 1 Report v2.1
ICP-AES - LCS
Batch:Prep Method:
Prep Date:
Sample ID:PQ59619-002
59619 3005A
10/31/2014 901Analytical Method:6010C
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Lead 0.42 11/03/2014 20461040.40 80-1201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 38 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
ICP-AES - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:PQ59619-003
59619 3005A
10/31/2014 901Analytical Method:6010C
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(mg/L)(mg/L)
Lead 0.42 11/03/2014 20501050.40 80-1200.94 201
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 39 of 39
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Blue Ridge Environmental Services
2315 Kings Road Ext.
Shelby, NC 28152
Attention: Joe McMurray
QA26023Lot Number:
Kash & Karry #11Project Name:
02/05/2015Date Completed:
Kelly M. Nance
Project Manager
*QA26023*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 27
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Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Blue Ridge Environmental Services
Lot Number: QA26023
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 27
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Blue Ridge Environmental Services
Lot Number: QA26023

Sample Number Sample ID Matrix Date Sampled Date Received
001 01/22/2015 0845MW-2 Aqueous 01/26/2015
002 01/22/2015 0848MW-3 Aqueous 01/26/2015
003 01/22/2015 0851MW-4 Aqueous 01/26/2015
(3 samples)
Page: 3 of 27
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Blue Ridge Environmental Services
Lot Number: QA26023

Sample Sample ID Matrix Parameter Method Result Q Units Page
002 MW-3 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-1.7 ug/L 9
003 MW-4 Aqueous Benzene SM 6200B-5.5 ug/L 13
003 MW-4 Aqueous sec-Butylbenzene SM 6200B-0.54 ug/L 13
003 MW-4 Aqueous Chloroform SM 6200B-1.3 ug/L 13
003 MW-4 Aqueous Isopropylbenzene (Cumene)SM 6200B-1.5 ug/L 13
003 MW-4 Aqueous Methyl tertiary butyl ether (MTBE)SM 6200B-38 ug/L 13
003 MW-4 Aqueous Naphthalene SM 6200B-14 ug/L 13
003 MW-4 Aqueous n-Propylbenzene SM 6200B-0.83 ug/L 13
003 MW-4 Aqueous C5 - C8 Aliphatics MADEP-VPH-76 ug/L 15
(9 detections)
Page: 4 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-2
QA26023-001
01/22/2015 0845
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 02/03/2015 1610 EH1 66778
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Benzene 71-43-2 SM 6200B-20 ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-20 ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-20 ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 ND 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-20 ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-20 ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-2
QA26023-001
01/22/2015 0845
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 02/03/2015 1610 EH1 66778
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-20 ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-20 ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-20 ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 70-130
Bromofluorobenzene 108 70-130
Toluene-d8 107 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-2
QA26023-001
01/22/2015 0845
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/28/2015 2052 JJG 66395
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 1ug/L75
C9 - C12 Aliphatics MADEP-VPH-0 ND 1ug/L75
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)108 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-2
QA26023-001
01/22/2015 0845
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/28/2015 2052 JJG 66396
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 1ug/L25
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)110 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-3
QA26023-002
01/22/2015 0848
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 02/03/2015 1637 EH1 66778
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Benzene 71-43-2 SM 6200B-20 ND 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-20 ND 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-20 ND 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-20 ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 ND 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 1.7 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-20 ND 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-20 ND 1ug/L0.50
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-3
QA26023-002
01/22/2015 0848
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 02/03/2015 1637 EH1 66778
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-20 ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-20 ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-20 ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 104 70-130
Bromofluorobenzene 103 70-130
Toluene-d8 107 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-3
QA26023-002
01/22/2015 0848
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/28/2015 2131 JJG 66395
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-0 ND 1ug/L75
C9 - C12 Aliphatics MADEP-VPH-0 ND 1ug/L75
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)102 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-3
QA26023-002
01/22/2015 0848
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/28/2015 2131 JJG 66396
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 1ug/L25
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)101 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-4
QA26023-003
01/22/2015 0851
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 02/03/2015 1704 EH1 66778
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Benzene 71-43-2 SM 6200B-20 5.5 1ug/L0.50
Bromobenzene 108-86-1 SM 6200B-20 ND 1ug/L0.50
Bromochloromethane 74-97-5 SM 6200B-20 ND 1ug/L0.50
Bromodichloromethane 75-27-4 SM 6200B-20 ND 1ug/L0.50
Bromoform 75-25-2 SM 6200B-20 ND 1ug/L0.50
Bromomethane (Methyl bromide)74-83-9 SM 6200B-20 ND 1ug/L0.50
n-Butylbenzene 104-51-8 SM 6200B-20 ND 1ug/L0.50
sec-Butylbenzene 135-98-8 SM 6200B-20 0.54 1ug/L0.50
tert-Butylbenzene 98-06-6 SM 6200B-20 ND 1ug/L0.50
Carbon tetrachloride 56-23-5 SM 6200B-20 ND 1ug/L0.50
Chlorobenzene 108-90-7 SM 6200B-20 ND 1ug/L0.50
Chloroethane 75-00-3 SM 6200B-20 ND 1ug/L0.50
Chloroform 67-66-3 SM 6200B-20 1.3 1ug/L0.50
Chloromethane (Methyl chloride)74-87-3 SM 6200B-20 ND 1ug/L0.50
2-Chlorotoluene 95-49-8 SM 6200B-20 ND 1ug/L0.50
4-Chlorotoluene 106-43-4 SM 6200B-20 ND 1ug/L0.50
Dibromochloromethane 124-48-1 SM 6200B-20 ND 1ug/L0.50
1,2-Dibromoethane (EDB)106-93-4 SM 6200B-20 ND 1ug/L0.50
Dibromomethane (Methylene bromide)74-95-3 SM 6200B-20 ND 1ug/L0.50
1,2-Dichlorobenzene 95-50-1 SM 6200B-20 ND 1ug/L0.50
1,3-Dichlorobenzene 541-73-1 SM 6200B-20 ND 1ug/L0.50
1,4-Dichlorobenzene 106-46-7 SM 6200B-20 ND 1ug/L0.50
Dichlorodifluoromethane 75-71-8 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloroethane 75-34-3 SM 6200B-20 ND 1ug/L0.50
1,2-Dichloroethane 107-06-2 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloroethene 75-35-4 SM 6200B-20 ND 1ug/L0.50
cis-1,2-Dichloroethene 156-59-2 SM 6200B-20 ND 1ug/L0.50
trans-1,2-Dichloroethene 156-60-5 SM 6200B-20 ND 1ug/L0.50
1,2-Dichloropropane 78-87-5 SM 6200B-20 ND 1ug/L0.50
1,3-Dichloropropane 142-28-9 SM 6200B-20 ND 1ug/L0.50
2,2-Dichloropropane 594-20-7 SM 6200B-20 ND 1ug/L0.50
1,1-Dichloropropene 563-58-6 SM 6200B-20 ND 1ug/L0.50
cis-1,3-Dichloropropene 10061-01-5 SM 6200B-20 ND 1ug/L0.50
trans-1,3-Dichloropropene 10061-02-6 SM 6200B-20 ND 1ug/L0.50
Diisopropyl ether (IPE)108-20-3 SM 6200B-20 ND 1ug/L0.50
Ethylbenzene 100-41-4 SM 6200B-20 ND 1ug/L0.50
Hexachlorobutadiene 87-68-3 SM 6200B-20 ND 1ug/L0.50
Isopropylbenzene (Cumene)98-82-8 SM 6200B-20 1.5 1ug/L0.50
p-Isopropyltoluene (p-Cymene)99-87-6 SM 6200B-20 ND 1ug/L0.50
Methyl tertiary butyl ether (MTBE)1634-04-4 SM 6200B-20 38 1ug/L0.50
Methylene chloride 75-09-2 SM 6200B-20 ND 1ug/L0.50
Naphthalene 91-20-3 SM 6200B-20 14 1ug/L0.50
n-Propylbenzene 103-65-1 SM 6200B-20 0.83 1ug/L0.50
Styrene 100-42-5 SM 6200B-20 ND 1ug/L0.50
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-4
QA26023-003
01/22/2015 0851
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 SM 6200B-SM 6200B-2011 1 02/03/2015 1704 EH1 66778
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
1,1,1,2-Tetrachloroethane 630-20-6 SM 6200B-20 ND 1ug/L0.50
1,1,2,2-Tetrachloroethane 79-34-5 SM 6200B-20 ND 1ug/L0.50
Tetrachloroethene 127-18-4 SM 6200B-20 ND 1ug/L0.50
Toluene 108-88-3 SM 6200B-20 ND 1ug/L0.50
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 SM 6200B-20 ND 1ug/L0.50
1,2,3-Trichlorobenzene 87-61-6 SM 6200B-20 ND 1ug/L0.50
1,2,4-Trichlorobenzene 120-82-1 SM 6200B-20 ND 1ug/L0.50
1,1,1-Trichloroethane 71-55-6 SM 6200B-20 ND 1ug/L0.50
1,1,2-Trichloroethane 79-00-5 SM 6200B-20 ND 1ug/L0.50
Trichloroethene 79-01-6 SM 6200B-20 ND 1ug/L0.50
Trichlorofluoromethane 75-69-4 SM 6200B-20 ND 1ug/L0.50
1,2,3-Trichloropropane 96-18-4 SM 6200B-20 ND 1ug/L0.50
1,3,5-Trimethylbenzene (Mesitylene)108-67-8 SM 6200B-20 ND 1ug/L0.50
1,2,4-Trimethylbenzene 95-63-6 SM 6200B-20 ND 1ug/L0.50
Vinyl chloride 75-01-4 SM 6200B-20 ND 1ug/L0.50
m+p - Xylenes 179601-23-1 SM 6200B-20 ND 1ug/L0.50
o - Xylenes 95-47-6 SM 6200B-20 ND 1ug/L0.50
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 104 70-130
Bromofluorobenzene 105 70-130
Toluene-d8 105 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 27
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-4
QA26023-003
01/22/2015 0851
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/28/2015 2210 JJG 66395
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C5 - C8 Aliphatics MADEP-VPH-76 1ug/L75
C9 - C12 Aliphatics MADEP-VPH-0 ND 1ug/L75
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)105 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-4
QA26023-003
01/22/2015 0851
01/26/2015
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 01/28/2015 2210 JJG 66396
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
C9 - C10 Aromatics MADEP-VPH-0 ND 1ug/L25
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)106 70-130
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 27
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
Page: 17 of 27
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ66778-001
66778 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Benzene ND 02/03/2015 10460.50 ug/L1
Bromobenzene ND 02/03/2015 10460.50 ug/L1
Bromochloromethane ND 02/03/2015 10460.50 ug/L1
Bromodichloromethane ND 02/03/2015 10460.50 ug/L1
Bromoform ND 02/03/2015 10460.50 ug/L1
Bromomethane (Methyl bromide)ND 02/03/2015 10460.50 ug/L1
tert-Butylbenzene ND 02/03/2015 10460.50 ug/L1
sec-Butylbenzene ND 02/03/2015 10460.50 ug/L1
n-Butylbenzene ND 02/03/2015 10460.50 ug/L1
Carbon tetrachloride ND 02/03/2015 10460.50 ug/L1
Chlorobenzene ND 02/03/2015 10460.50 ug/L1
Chloroethane ND 02/03/2015 10460.50 ug/L1
Chloroform ND 02/03/2015 10460.50 ug/L1
Chloromethane (Methyl chloride)ND 02/03/2015 10460.50 ug/L1
4-Chlorotoluene ND 02/03/2015 10460.50 ug/L1
2-Chlorotoluene ND 02/03/2015 10460.50 ug/L1
Dibromochloromethane ND 02/03/2015 10460.50 ug/L1
1,2-Dibromoethane (EDB)ND 02/03/2015 10460.50 ug/L1
Dibromomethane (Methylene bromide)ND 02/03/2015 10460.50 ug/L1
1,4-Dichlorobenzene ND 02/03/2015 10460.50 ug/L1
1,3-Dichlorobenzene ND 02/03/2015 10460.50 ug/L1
1,2-Dichlorobenzene ND 02/03/2015 10460.50 ug/L1
Dichlorodifluoromethane ND 02/03/2015 10460.50 ug/L1
1,2-Dichloroethane ND 02/03/2015 10460.50 ug/L1
1,1-Dichloroethane ND 02/03/2015 10460.50 ug/L1
trans-1,2-Dichloroethene ND 02/03/2015 10460.50 ug/L1
cis-1,2-Dichloroethene ND 02/03/2015 10460.50 ug/L1
1,1-Dichloroethene ND 02/03/2015 10460.50 ug/L1
2,2-Dichloropropane ND 02/03/2015 10460.50 ug/L1
1,3-Dichloropropane ND 02/03/2015 10460.50 ug/L1
1,2-Dichloropropane ND 02/03/2015 10460.50 ug/L1
trans-1,3-Dichloropropene ND 02/03/2015 10460.50 ug/L1
cis-1,3-Dichloropropene ND 02/03/2015 10460.50 ug/L1
1,1-Dichloropropene ND 02/03/2015 10460.50 ug/L1
Diisopropyl ether (IPE)ND 02/03/2015 10460.50 ug/L1
Ethylbenzene ND 02/03/2015 10460.50 ug/L1
Hexachlorobutadiene ND 02/03/2015 10460.50 ug/L1
Isopropylbenzene (Cumene)ND 02/03/2015 10460.50 ug/L1
p-Isopropyltoluene (p-Cymene)ND 02/03/2015 10460.50 ug/L1
Methyl tertiary butyl ether (MTBE)ND 02/03/2015 10460.50 ug/L1
Methylene chloride ND 02/03/2015 10460.50 ug/L1
Naphthalene ND 02/03/2015 10460.50 ug/L1
n-Propylbenzene ND 02/03/2015 10460.50 ug/L1
Styrene ND 02/03/2015 10460.50 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 18 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:QQ66778-001
66778 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
1,1,2,2-Tetrachloroethane ND 02/03/2015 10460.50 ug/L1
1,1,1,2-Tetrachloroethane ND 02/03/2015 10460.50 ug/L1
Tetrachloroethene ND 02/03/2015 10460.50 ug/L1
Toluene ND 02/03/2015 10460.50 ug/L1
1,1,2-Trichloro-1,2,2-Trifluoroethane ND 02/03/2015 10460.50 ug/L1
1,2,4-Trichlorobenzene ND 02/03/2015 10460.50 ug/L1
1,2,3-Trichlorobenzene ND 02/03/2015 10460.50 ug/L1
1,1,2-Trichloroethane ND 02/03/2015 10460.50 ug/L1
1,1,1-Trichloroethane ND 02/03/2015 10460.50 ug/L1
Trichloroethene ND 02/03/2015 10460.50 ug/L1
Trichlorofluoromethane ND 02/03/2015 10460.50 ug/L1
1,2,3-Trichloropropane ND 02/03/2015 10460.50 ug/L1
1,2,4-Trimethylbenzene ND 02/03/2015 10460.50 ug/L1
1,3,5-Trimethylbenzene (Mesitylene)ND 02/03/2015 10460.50 ug/L1
Vinyl chloride ND 02/03/2015 10460.50 ug/L1
o - Xylenes ND 02/03/2015 10460.50 ug/L1
m+p - Xylenes ND 02/03/2015 10460.50 ug/L1
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 107 70-130
1,2-Dichloroethane-d4 101 70-130
Toluene-d8 109 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 19 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ66778-002
66778 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 51 02/03/2015 09431035070-1301
Bromobenzene 50 02/03/2015 09431005070-1301
Bromochloromethane 56 02/03/2015 09431115070-1301
Bromodichloromethane 53 02/03/2015 09431065070-1301
Bromoform 53 02/03/2015 09431075070-1301
Bromomethane (Methyl bromide)56 02/03/2015 09431135060-1401
tert-Butylbenzene 49 02/03/2015 0943995070-1301
sec-Butylbenzene 50 02/03/2015 09431005070-1301
n-Butylbenzene 50 02/03/2015 09431015070-1301
Carbon tetrachloride 57 02/03/2015 09431145070-1301
Chlorobenzene 50 02/03/2015 09431005070-1301
Chloroethane 56 02/03/2015 09431115042-1631
Chloroform 54 02/03/2015 09431075070-1301
Chloromethane (Methyl chloride)57 02/03/2015 09431135020-1581
4-Chlorotoluene 50 02/03/2015 09431005070-1301
2-Chlorotoluene 50 02/03/2015 0943995070-1301
Dibromochloromethane 51 02/03/2015 09431035070-1301
1,2-Dibromoethane (EDB)51 02/03/2015 09431025070-1301
Dibromomethane (Methylene bromide)54 02/03/2015 09431095070-1301
1,4-Dichlorobenzene 49 02/03/2015 0943995070-1301
1,3-Dichlorobenzene 49 02/03/2015 0943985070-1301
1,2-Dichlorobenzene 49 02/03/2015 0943985070-1301
Dichlorodifluoromethane 61 02/03/2015 09431225060-1401
1,2-Dichloroethane 56 02/03/2015 09431135070-1301
1,1-Dichloroethane 53 02/03/2015 09431055070-1301
trans-1,2-Dichloroethene 53 02/03/2015 09431065070-1301
cis-1,2-Dichloroethene 53 02/03/2015 09431065070-1301
1,1-Dichloroethene 50 02/03/2015 09431015070-1301
2,2-Dichloropropane 55 02/03/2015 09431115070-1301
1,3-Dichloropropane 50 02/03/2015 09431005070-1301
1,2-Dichloropropane 52 02/03/2015 09431035070-1301
trans-1,3-Dichloropropene 51 02/03/2015 09431025070-1301
cis-1,3-Dichloropropene 53 02/03/2015 09431065070-1301
1,1-Dichloropropene 52 02/03/2015 09431045070-1301
Diisopropyl ether (IPE)55 02/03/2015 09431115070-1301
Ethylbenzene 48 02/03/2015 0943965070-1301
Hexachlorobutadiene 54 02/03/2015 09431085070-1301
Isopropylbenzene (Cumene)51 02/03/2015 09431035070-1301
p-Isopropyltoluene (p-Cymene)51 02/03/2015 09431025070-1301
Methyl tertiary butyl ether (MTBE)56 02/03/2015 09431115070-1301
Methylene chloride 52 02/03/2015 09431045070-1301
Naphthalene 51 02/03/2015 09431015050-1401
n-Propylbenzene 49 02/03/2015 0943995070-1301
Styrene 50 02/03/2015 09431005070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 20 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:QQ66778-002
66778 SM 6200B-2011
Analytical Method:SM 6200B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
1,1,2,2-Tetrachloroethane 50 02/03/2015 09431005070-1301
1,1,1,2-Tetrachloroethane 53 02/03/2015 09431065070-1301
Tetrachloroethene 50 02/03/2015 09431015070-1301
Toluene 51 02/03/2015 09431025070-1301
1,1,2-Trichloro-1,2,2-Trifluoroethane 56 02/03/2015 09431135070-1301
1,2,4-Trichlorobenzene 50 02/03/2015 09431015070-1301
1,2,3-Trichlorobenzene 49 02/03/2015 0943995070-1301
1,1,2-Trichloroethane 51 02/03/2015 09431025070-1301
1,1,1-Trichloroethane 54 02/03/2015 09431095070-1301
Trichloroethene 50 02/03/2015 09431005070-1301
Trichlorofluoromethane 64 02/03/2015 09431275060-1401
1,2,3-Trichloropropane 52 02/03/2015 09431035070-1301
1,2,4-Trimethylbenzene 50 02/03/2015 09431005070-1301
1,3,5-Trimethylbenzene (Mesitylene)51 02/03/2015 09431025070-1301
Vinyl chloride 59 02/03/2015 09431185060-1401
o - Xylenes 50 02/03/2015 0943995070-1301
m+p - Xylenes 48 02/03/2015 0943965070-1301
Surrogate Q % Rec Acceptance
Limit
Bromofluorobenzene 100 70-130
1,2-Dichloroethane-d4 108 70-130
Toluene-d8 106 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 21 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - MB
Batch:Prep Method:
Sample ID:QQ66395-001
66395 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
C5 - C8 Aliphatics ND 01/28/2015 193775ug/L1
C9 - C12 Aliphatics ND 01/28/2015 193775ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 22 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - LCS
Batch:Prep Method:
Sample ID:QQ66395-002
66395 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 75 01/28/2015 18191017570-1301
C9 - C12 Aliphatics 66 01/28/2015 1819877570-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)88 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 23 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aliphatics) - LCSD
Batch:Prep Method:
Sample ID:QQ66395-003
66395 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 69 01/28/2015 1858917570-1309.4 251
C9 - C12 Aliphatics 62 01/28/2015 1858827570-1306.1 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)88 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 24 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - MB
Batch:Prep Method:
Sample ID:QQ66396-001
66396 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
C9 - C10 Aromatics ND 01/28/2015 193725ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 25 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - LCS
Batch:Prep Method:
Sample ID:QQ66396-002
66396 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 25 01/28/2015 18191002570-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)90 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 26 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
MADEP VPH (aromatics) - LCSD
Batch:Prep Method:
Sample ID:QQ66396-003
66396 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 24 01/28/2015 1858962570-1304.1 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)88 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
Page: 27 of 27
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1