WA-26757_31939_CA_RPTS_20150821_MMPE

EXECUTIVE SUMMARY

The Miller’s Country Store site (Miller’s) is located at 1706 US Highway 17, North, Merry Hill, Bertie
County, North Carolina. According to available information, a release was discovered during UST
closure activities conducted at the site in September 2008. Three 4,000-gallon gasoline USTs were
removed from the site in September 2008 and one orphan 2,000-gallon UST whose former contents are
unknown was removed from the site in April 2009. Municipal water is available to the site and
surrounding properties. Additional petroleum releases (UST Incident Number 11963 – Todd’s Service
Center and UST Incident Number 13592 – Bowen’s Grocery) are located adjacent to the Miller’s Country
Store site and are considered to be commingled with the Miller’s Country Store contaminant plume.

The current risk classification is high due to the presence of water supply wells within a 250-foot radius
of the source area.

A Mobile Multi-Phase Extraction (MMPE) event was conducted at the site from June 1 through June 5,
2015. The results of the MMPE event indicate that 16,317 gallons of liquid were removed during the
event. Based on mass-removal calculations, an additional 473.03 pounds or 75.68 gallons of vapor phase
hydrocarbons were removed.

A ground water monitoring event was conducted for the Todd’s, Bowen’s and Miller’s sites on July 6,
2015. Concentrations of requested method constituents that exceeded the Maximum Allowable
Concentrations (MACs) were reported in monitoring wells MW-2 through MW-5, MW-11, MW-22,
MW-23A, MW-26, MW-29, MW-34, MW-1M and MW-3M. None of the reported contaminant
concentrations exceeded the Gross Contamination Levels (GCLs).

Pilot testing and New Technology Cleanup Plan (NTCP) activities are tentatively scheduled to be
completed for the Todd’s and Bowen’s sites in September 2015.

Based on this information, semi-annual ground water monitoring should continue at the site until the
NTCP can be completed and implemented. Additional MMPE events should be conducted as needed in
order to continue to reduce the contaminant concentrations at the site. The next semi-annual ground
water monitoring event is tentatively scheduled for January 2016.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ASSESSMENT ............................................................................................ 1
3.0 MMPE EVENT ......................................................................................................................... 2
4.0 GROUND WATER QUALITY ................................................................................................ 2
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 3
6.0 LIMITATIONS ......................................................................................................................... 4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Benzene Isoconcentration Map
Figure 7: Toluene Isoconcentration Map
Figure 8: Ethylbenzene Isoconcentration Map
Figure 9: Xylenes Isoconcentration Map
Figure 10: MTBE Isoconcentration Map
Figure 11: Naphthalene Isoconcentration Map

TABLES

Table 1: Well Construction and Gauging Information
Table 2: Free Product Recovery Results
Table 3: Free Product Recovery Event Information
Table 4: Free Product Recovery Cost Summary
Table 5: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: MMPE Data and Calculations
Appendix B: Laboratory Report - Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
The Miller’s Country Store site is located at 1706 US Highway 17 N in Merry Hill, Bertie County, North
Carolina (Figure 1). The subject site is a former retail petroleum facility. According to available
information, three 4,000-gallon gasoline USTs were removed from the site on September 9, 2008 and one
orphan 2,000-gallon UST, whose former contents are unknown, was removed from the site on April 30,
2009. An additional UST system consisting of three 3,000-gallon gasoline USTs was removed from the
site on September 1, 1988. A release at the site was discovered when petroleum impacted soil was
encountered during the September 2008 UST closure event.

Three Type II monitoring wells (MW-1M, MW-2M and MW-3M) and one Type III monitoring well
(TW-1M) were installed at the site during past assessment activities. A receptor survey was conducted on
October 1, 2009. Eighteen water supply wells were identified within a 1,500-foot radius of the site.
Three out of service water supply wells (WSW-1, WSW-2 and WSW-3) were identified within a 250-foot
radius of the site. Municipal water is available to the site and surrounding properties. A Site Vicinity
Map showing properties and water supply wells within a 1,500-foot radius of the source area is included
as Figure 2. A Site Map is included as Figure 3. This sampling event was conducted in conjunction
with the sampling event at the adjacent Todd’s and Bowen’s sites. The releases from all three sites are
commingled.

Certain information in this report was obtained as a result of assessment activities conducted by past
consultants. Although Geological Resources Inc. (GRI) cannot verify the accuracy of this information,
for the purpose of this report, it is assumed to be correct. Any inferences or interpretations made by GRI
based on data that may be incorrect are not the responsibility of GRI. Please refer to earlier submittals for
additional information regarding past assessment activities.

2.0 CURRENT SITE ASSESSMENT
This report presents the results of the Mobile Multi-Phase Extraction (MMPE) event conducted between
June 1 and 5, 2015 and the ground water sampling activities conducted on July 6, 2015 at the Miller
Country Store site. The subject site is a former petroleum retail facility. A residence is present on the
property. The activities were conducted in accordance with GRI proposal number 14-552, which was
submitted to NCDENR on October 2, 2014 and approved as Task Authorization No. 31939-04 on
February 13, 2015. The purpose of the activities was to reduce contaminant concentrations and to obtain
current ground water quality data for the site.

2
3.0 MMPE EVENT
An MMPE event was conducted at the site by Greenwood Applied Services, LLC under the supervision
of GRI between June 1 and 5, 2015 on MW-1M, MW-3M and MW-22. The MMPE equipment included
a liquid ring pump, 9,500-gallon capacity tanker, flexible vacuum hoses, 1-inch diameter PVC stinger
pipes and associated couplings and pipe fittings to manifold to three monitoring wells simultaneously.
The MMPE system was rated at 24 in. Hg at 280 cfm. Extraction wells, MW-1M, MW-3M and MW-22,
as well as observation wells MW-2M and MW-23A were gauged on June 1, 2015, prior to the event. No
free product was observed in any of the monitoring wells. The stinger pipes were initially set at depths of
18.25, 17.57 and 17.85 feet in MW-1M, MW-3M and MW-22, respectively.

Monitoring wells MW-1M, MW-3M and MW-22 were each vacuumed continuously for the 96 hour
event. During the event, measurements of relative humidity, temperature, vacuum, exhaust velocity and
off-gas concentrations were recorded at the discharge stack a minimum of two times per 24-hour period.
Vacuum at the extraction wells ranged from 10 to 20 in. Hg. System vacuum ranged from 12 to 20 in.
Hg. Exhaust velocities ranged from 1,285 to 2,554 fpm. Temperatures ranged from 86.9 to 100.2o F and
relative humidity ranged from 52.9 to 92.8 percent. Total VOC off-gas concentrations ranged from 48.7
to 885.8 ppm during the event. At the conclusion of the event, no measurable free product was detected
in any of the monitoring wells. A summary of the gauging data obtained before start up and at the
conclusion of the MMPE event is presented in Table 1. A copy of the MMPE data and calculations has
been included as Appendix A.

The results of the MMPE event indicate that 16,317 gallons of liquid were removed during the event.
Based on 96 hours of operation, the average fluid recovery rate was 169.97 gallons per hour. Based on
mass-removal calculations, an additional 102.99 pounds (16.48 gallons) of vapor phase hydrocarbons
were removed during the MMPE event. A summary of free product recovery data has been included as
Table 2. Summaries of MMPE event information and cost analysis are provided in Tables 3 and 4,
respectively. At the conclusion of the MMPE event, all wastewater was transported to a permitted facility
for disposal. Copies of the disposal manifests have been included as Appendix A.

4.0 GROUND WATER QUALITY
Three Type II monitoring wells (MW-1M, MW-2M and MW-3M) and one Type III monitoring well
(TW-1M) were gauged, purged and/or sampled on July 6, 2015. Please note, monitoring wells associated
with the Todd’s Service Center and Bowen’s Grocery sites (MW-2 through MW-5, MW-7, MW-9A,
MW-10A, MW-11, MW-14, MW-17, MW-20, MW-22, MW-23A, MW-25B, MW-26, MW-29, MW-31,

3
MW-34, MW-36, MW-38 and MW-42 through MW-48) as well as WSW-3 were sampled for those
incidents concurrently with the Miller’s Country Store site and are included in data collected for the July
2015 sampling event.

The depths to ground water in the Type II monitoring wells during the July 2015 sampling event ranged
from 6.47 to 19.13 feet below the top of casings. Ground water elevations in the Type II monitoring
wells relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from 75.77 to
81.84 feet. Based on this information, the direction of ground water flow was generally toward the
southeast. The average horizontal hydraulic gradient across the site was less than 0.01 feet per foot. The
vertical gradient calculated for paired wells MW-1M and TW-1M was approximately 0.02 feet per foot
upward. A Water Table Surface Map for the July 2015 sampling event has been included as Figure 4.
Well construction and gauging information is presented in Table 1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the July 2105 sampling event for volatile organic compounds (VOCs) using EPA Method 6200B.
Concentrations of one or more BTEX constituents, MTBE, naphthalene, isopropylbenzene, n-
propylbenzene 1,3,5-trimethylbenzene, 1,2,4-trimethylbenzene, 1,2-dichloroethane, n-butylbenzene, p-
isopropyltoluene and/or styrene that exceeded the maximum allowable concentrations (MACs) specified
in T15A NCAC 2L.0202 were reported in the ground water samples collected from monitoring wells
MW-2 through MW-5, MW-11, MW-22, MW-23A, MW-26, MW-29, MW-34, MW-1M and MW-3M.
None of the reported contaminant concentrations exceeded the gross contamination levels (GCLs). No
detectable contaminant concentrations were reported in the ground water sample collected from WSW-3.
A Ground Water Quality Map based on data from the July 6, 2015 sampling event has been included as
Figure 5. Contaminant specific isoconcentration maps for benzene, toluene, ethylbenzene, xylenes,
MTBE and naphthalene are included as Figures 6 through 11, respectively. A summary of ground water
sample analytical results is presented in Table 5. A complete laboratory report has been included as
Appendix B.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 An MMPE event was conducted on monitoring wells MW-1M, MW-3M and MW-22 between
June 1 and 5, 2015. According to the disposal manifests and off-gas calculations, the MMPE
recovered 16,317 gallons of liquid and removed 75.68 gallons of free product in the vapor phase.
 The average depth to ground water in the Type II monitoring wells in July 2015 was 17.79 feet
below the tops of well casings. Ground water flow was generally toward the southeast with an

4
average horizontal hydraulic gradient of less than 0.01 feet per foot. The average vertical
gradient between paired wells MW-1M and TW-1M was approximately 0.02 feet per foot
upward.
 Concentrations of one or more BTEX constituents, MTBE, naphthalene, isopropylbenzene, n-
propylbenzene 1,3,5-trimethylbenzene, 1,2,4-trimethylbenzene, 1,2-dichloroethane, n-
butylbenzene, p-isopropyltoluene and/or styrene that exceeded the MACs were reported in the
ground water samples collected from monitoring wells MW-2 through MW-5, MW-11, MW-22,
MW-23A, MW-26, MW-29, MW-34, MW-1M and MW-3M. None of the reported contaminant
concentrations exceeded the GCLs. No detectable contaminant concentrations were reported in
the ground water sample collected from WSW-3.
 Based on this information, the site should remain high risk. New Technology Cleanup Plan
(NTCP) and pilot testing activities are tentatively scheduled to be performed at the site in
September 2015. Semi-annual ground water monitoring should continue at the site until the
NTCP can be completed and implemented. Additional MMPE and/or AFVR events should be
conducted as needed in order to continue to reduce the contaminant concentrations at the site.
The next semi-annual ground water monitoring event is tentatively scheduled for January 2016.

6.0 LIMITATIONS
This report has been prepared for the exclusive use of Ms. Shirley Miller for the specific application to
the reference site in Bertie County, North Carolina. The assessment was conducted based on the scope of
work and level of effort desired by NCDENR and with resources adequate only for that scope of work.
Our findings have been developed in accordance with generally accepted standards of environmental
practices in the State of North Carolina, available information, and our professional judgment. No other
warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the times the samples were collected. In addition, the data obtained from the samples
would be interpreted as being meaningful with respect to parameters indicated in the laboratory report.
No additional information can logically be inferred from these data.

FIGURES
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SITE
U S 1 7 H W Y
NC 45 HWYU S 1 7 H W Y
NC
4
5 HWYWSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
WSW-18
WSW-17
WSW-16 WSW-15
WSW-14
WSW-13
WSW-12
WSW-11
WSW-10
6853575623
6853588050
6853482256
6853487344
6853386041
6853592031
6853590189
6853487515
6853489091
6853497974
6853482637
6853586821
6853484771
6853487891
6853486737
6853489601
6853489510 6853582419
6853582338
6853496178
6853484413
³
0 300150Feet
FIGURE 2: SITE VICINITY MAPMILLER'S COUNTRY STORE1706 US HWY 17 NORTHMERRY HILL,BERTIE COUNTYNORTH CAROLINAINCIDENT NO. 31939
PREPARED BYGEOLOGICAL RESOURCES, INC.SEPTEMBER 16, 2009
1 inch equals 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
Legend
"J Water Supply Well
River_Line
Centerline
Parcel_Polygon
Pond_Lake_Polygon
6853575623
6853487515 PIN Number

TABLES
Date: 07/06/15
11/01/07
09/16/09
09/20/10
10/27/11
01/07/13
11/01/07 99.34 21.00 0.00 78.34
07/20/09 22.00 0.01 78.01 Pre-MMPE
07/24/09 21.25 0.00 78.75 Post-MMPE
09/16/09 21.57 0.00 78.43
09/20/10 19.92 0.00 80.08
10/27/11 19.90 0.00 80.10
12/03/12 21.45 0.00 78.55 Pre-MMPE
12/07/12 20.50 0.00 79.50 Post-MMPE
01/07/13 21.47 0.00 78.53
06/24/13 21.09 0.00 78.91 Pre-MMPE
06/28/13 21.19 0.00 78.81 Post-MMPE
07/29/13 NM NM NM Not Found
05/19/14 19.54 0.00 80.46 Pre-MMPE
05/23/14 19.45 0.00 80.55 Post-MMPE
06/23/14 19.68 0.00 80.32
07/06/15 NM NM NM Not Found
11/01/07 99.51 20.92 0.00 78.59
07/20/09 21.07 0.00 78.79 Pre-MMPE
07/24/09 21.34 0.00 78.52 Post-MMPE
09/16/09 21.48 0.00 78.38
09/20/10 19.83 0.00 80.03
10/27/11 19.86 0.00 80.00
12/03/12 21.37 0.00 78.49 Pre-MMPE
12/07/12 21.42 0.00 78.44 Post-MMPE
01/07/13 21.40 0.00 78.46
06/24/13 20.91 0.00 78.95 Pre-MMPE
06/28/13 21.06 0.00 78.80 Post-MMPE
07/29/13 20.43 0.00 79.43
05/19/14 19.49 0.00 80.37 Pre-MMPE
05/23/14 19.44 0.00 80.42 Post-MMPE
06/23/14 19.62 0.00 80.24
06/01/15 18.39 0.00 81.47 Pre-MMPE
06/05/15 18.51 0.00 81.35 Post-MMPE
07/06/15 19.13 0.00 80.73
11/01/07 99.59 20.86 0.00 78.73
09/16/09 21.40 0.00 78.56
09/20/10 19.74 0.00 80.22
10/27/11 19.70 0.00 80.26
01/07/13 21.27 0.00 78.69
07/29/13 20.31 0.00 79.65
05/19/14 19.40 0.00 80.56 Pre-MMPE
05/23/14 19.29 0.00 80.67 Post-MMPE
06/03/14 19.47 0.00 80.49
06/01/15 18.22 0.00 81.74 Pre-MMPE
06/05/15 18.34 0.00 81.62 Post-MMPE
07/06/15 18.98 0.00 80.98
11/01/07 99.57 20.60 0.00 78.99
09/16/09 NM NM NM
09/20/10 19.47 0.00 80.10
10/27/11 19.40 0.00 80.17
12/03/12 21.00 0.00 78.57 Pre-MMPE
12/07/12 21.06 0.00 78.51 Post-MMPE
01/07/13 21.03 0.00 78.54
06/24/13 20.55 0.00 79.02 Pre-MMPE
06/28/13 20.67 0.00 78.90 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 19.19 0.00 80.38
07/06/15 18.73 0.00 80.84
11/01/07 99.19 20.29 0.00 78.90
09/16/09 20.85 0.00 78.72
09/20/10 19.17 0.00 80.40
10/27/11 19.10 0.00 80.47
01/07/13 20.70 0.00 78.87
07/29/13 19.76 0.00 79.81
05/19/14 18.69 0.00 80.88 Pre-MMPE
05/23/14 18.58 0.00 80.99 Post-MMPE
06/23/14 18.83 0.00 80.74
07/06/15 18.38 0.00 81.19
MW-5 04/27/94 15 15-25 25 99.57
MW-4 04/27/94 15 15-25 25 99.57
MW-3 04/27/94 15 15-25 25 99.96
100.00
MW-2 04/27/94 15 15-25 25 99.86
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
Casing
Collapsed
MW-1A 11/16/01 20 20-30 30
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
MW-1 04/27/94 15 15-25 25
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Page 1 of 6
Date: 07/06/15
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/01/07 99.27 21.20 0.00 78.07
09/16/09 21.06 0.00 78.60
09/20/10 19.74 0.00 79.92
10/27/11 19.48 0.00 80.18
01/07/13 21.04 0.00 78.62
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 99.00 20.41 0.00 78.59
09/16/09 20.96 0.00 78.44
09/20/10 19.31 0.00 80.09
10/27/11 19.32 0.00 80.08
01/07/13 20.84 0.00 78.56
07/29/13 20.40 0.00 79.00
06/23/14 19.07 0.00 80.33
07/06/15 18.59 0.00 80.81
11/01/07 99.28 20.63 0.00 78.65
09/16/09 21.20 0.00 78.47
09/20/10 19.55 0.00 80.12
10/27/11 19.48 0.00 80.19
01/07/13 21.07 0.00 78.60
07/29/13 NM NM NM Not Found
06/23/14 19.25 0.00 80.42
07/06/15 18.78 0.00 80.89
11/01/07 99.11 20.45 0.00 78.66
09/16/09 21.22 0.00 78.31
09/20/10 19.58 0.00 79.95
10/27/11 19.55 0.00 79.98
01/07/13 21.10 0.00 78.43
07/29/13 20.12 0.00 79.41
06/23/14 19.30 0.00 80.23
07/06/15 18.82 0.00 80.71
11/01/07 98.11 19.73 0.00 78.38
09/16/09 20.29 0.00 78.07
09/20/10 18.65 0.00 79.71
10/27/11 18.68 0.00 79.68
01/07/13 20.20 0.00 78.16
07/29/13 19.23 0.00 79.13
06/23/14 18.36 0.00 80.00
07/06/15 18.00 0.00 80.36
11/01/07 98.28 19.92 0.00 78.36
07/20/09 20.03 0.00 78.63 Pre-MMPE
07/24/09 20.21 0.00 78.45 Post-MMPE
09/16/09 20.48 0.00 78.18
09/20/10 18.75 0.00 79.91
10/27/11 18.87 0.00 79.79
12/03/12 20.39 0.00 78.27 Pre-MMPE
12/07/12 20.45 0.00 78.21 Post-MMPE
01/07/13 20.40 0.00 78.26
06/24/13 19.83 0.00 78.83 Pre-MMPE
06/28/13 19.95 0.00 78.71 Post-MMPE
07/29/13 19.46 0.00 79.20
05/19/14 18.51 0.00 80.15 Pre-MMPE
05/23/14 18.43 0.00 80.23 Post-MMPE
06/23/14 NM NM NM Not Found
11/01/07 98.23 19.85 0.00 78.38
09/16/09 20.40 0.00 78.20
09/20/10 18.77 0.00 79.83
10/27/11 18.81 0.00 79.79
01/07/13 20.30 0.00 78.30
07/29/13 19.40 0.00 79.20
06/23/14 NM NM NM Not Found
11/01/07 98.90 20.17 0.00 78.73
09/16/09 20.71 0.00 78.61
09/20/10 19.07 0.00 80.25
10/27/11 19.01 0.00 80.31
12/03/12 20.59 0.00 78.73 Pre-MMPE
12/07/12 20.66 0.00 78.66 Post-MMPE
01/07/13 20.60 0.00 78.72
06/24/13 20.11 0.00 79.21 Pre-MMPE
06/28/13 20.23 0.00 79.09 Post-MMPE
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
07/06/15 18.30 0.00 81.02
MW-15 12/08/95 06/23/14 18 18-28 28 NM 18.94 0.00 NM
MW-14 11/28/95 15 15-25 25 99.32
MW-13 11/30/95 15 15-25 25 98.60
MW-12 12/01/95 18 18-28 28 98.66
MW-11 12/01/95 18 18-28 28 98.36
MW-10A 10/31/07 15 15-25 25 99.53
MW-9A 10/31/07 15 15-25 25 99.67
MW-7 11/24/95 18 18-28 28 99.40
MWD-6 11/22/95 39 39-44 44 99.66
Page 2 of 6
Date: 07/06/15
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/01/07 99.34 20.42 0.00 78.92
09/16/09 20.97 0.00 78.76
09/20/10 19.23 0.00 80.50
10/27/11 19.20 0.00 80.53
01/07/13 20.51 0.00 79.22
07/29/13 NM NM NM Not Found
05/19/14 18.80 0.00 80.93 Pre-MMPE
05/23/14 18.78 0.00 80.95 Post-MMPE
06/23/14 NM NM NM Not Found
11/01/07 98.66 20.26 0.00 78.40
09/16/09 20.89 0.00 78.06
09/20/10 19.22 0.00 79.73
10/27/11 19.22 0.00 79.73
01/07/13 20.78 0.00 78.17
07/29/13 19.84 0.00 79.11
06/23/14 19.00 0.00 79.95
07/06/15 18.56 0.00 80.39
11/01/07 98.08 19.57 0.00 78.51
09/16/09 20.13 0.00 78.41
09/20/10 18.50 0.00 80.04
10/27/11 18.51 0.00 80.03
01/07/13 20.00 0.00 78.54
07/29/13 NM NM NM Not Found
06/23/14 NM NM NM Not Found
11/01/07 98.23 20.12 0.00 78.11
09/16/09 20.73 0.00 77.90
09/20/10 19.10 0.00 79.53
10/27/11 19.14 0.00 79.49
01/07/13 20.65 0.00 77.98
07/29/13 19.76 0.00 78.87
06/23/14 18.98 0.00 79.25
07/06/15 18.50 0.00 80.13
11/01/07 100.03 20.57 0.00 79.46
09/16/09 21.18 0.00 79.21
09/20/10 19.41 0.00 80.98
10/27/11 19.25 0.00 81.14
01/07/13 20.95 0.00 79.44
07/29/13 20.84 0.00 79.55
06/23/14 18.99 0.00 81.40
11/01/07 99.07 20.10 0.00 78.97
09/16/09 20.62 0.00 78.90
09/20/10 18.94 0.00 80.58
10/27/11 18.91 0.00 80.61
01/07/13 20.49 0.00 79.03
07/29/13 19.44 0.00 80.08
05/19/14 18.41 0.00 81.11 Pre-MMPE
05/23/14 18.62 0.00 80.90 Post-MMPE
06/23/14 18.61 0.00 80.91
06/01/15 17.35 0.00 82.17 Pre-MMPE
06/05/15 17.65 0.00 81.87 Post-MMPE
07/06/15 18.14 0.00 81.38
11/01/07 98.90 20.14 0.00 78.76
09/16/09 20.69 0.00 78.80
09/20/10 18.95 0.00 80.54
10/27/11 18.92 0.00 80.57
01/07/13 20.54 0.00 78.95
07/29/13 19.46 0.00 80.03
06/23/14 18.66 0.00 80.83
07/06/15 18.19 0.00 81.30
11/01/07 99.41 20.10 0.00 79.31
09/16/09 20.69 0.00 79.12
09/20/10 NM NM NM
11/01/07 98.43 20.42 0.00 78.01
09/16/09 21.01 0.00 77.88
09/20/10 19.38 0.00 79.51
10/27/11 19.50 0.00 79.39
01/07/13 20.92 0.00 77.97
07/29/13 20.07 0.00 78.82
06/23/14 19.31 0.00 79.58
07/06/15 18.80 0.00 80.09
MW-25B 11/01/07 15 15-25 25 98.89
MW-24 09/25/96 18 18-28 28 99.81
MW-23A 11/01/07 20 20-30 30 99.49
MW-22 09/24/96 18 18-28 28 99.52
MW-21 09/24/96 18 18-28 28 100.39
MW-20 04/22/96 18 18-28 28 98.63
MW-19 04/22/96 18 18-28 28 98.54
MW-17 04/19/96 18 18-28 28 98.95
MW-15A 11/01/07 15 15-25 25 99.73
Page 3 of 6
Date: 07/06/15
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
11/01/07 97.29 19.57 0.00 77.72
09/16/09 20.13 0.00 77.57
09/20/10 18.58 0.00 79.12
10/27/11 18.65 0.00 79.05
01/07/13 20.07 0.00 77.63
07/29/13 19.30 0.00 78.40
18.24 0.00 79.46 Pre-AFVR
18.30 0.00 79.40 Post-AFVR
06/23/14 18.52 0.00 79.18
06/01/15 17.40 0.00 80.30 Pre-AFVR
06/01/15 17.44 0.00 80.26 Post-AFVR
07/06/15 18.05 0.00 79.65
11/01/07 98.36 NM NM NM Well Dry
09/16/09 NM NM NM Well Dry
09/20/10 NM NM NM Well Dry
10/27/11 NM NM NM Well Dry
01/07/13 17.25 0.00 81.53
07/29/13 NM NM NM Well Dry
06/23/14 NM NM NM Well Dry
07/06/15 NM NM NM Well Dry
11/01/07 95.54 18.14 0.00 77.40
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
10/04/12 20.92 0.00 74.62 Pre-AFVR
10/04/12 20.93 0.00 74.61 Post-AFVR
01/07/13 NM NM NM
06/23/14 NM NM NM
11/01/07 97.70 20.25 0.00 77.45
09/16/09 20.85 0.00 77.30
09/20/10 19.31 0.00 78.84
10/27/11 19.47 0.00 78.68
20.81 0.00 77.34 Pre-AFVR
20.82 0.00 77.33 Post-AFVR
01/07/13 20.77 0.00 77.38
20.52 0.00 77.63 Pre-AFVR
20.52 0.00 77.63 Post-AFVR
07/29/13 20.05 0.00 78.10
18.88 0.00 79.27 Pre-AFVR
19.05 0.00 79.10 Post-AFVR
06/23/14 19.32 0.00 78.83
06/01/15 18.23 0.00 79.92 Pre-AFVR
06/01/15 18.23 0.00 79.92 Post-AFVR
07/06/15 19.32 0.00 78.83
11/01/07 96.32 19.34 0.00 76.98
09/16/09 19.88 0.00 76.85
09/20/10 NM NM NM
11/01/07 97.86 20.37 0.00 77.49
09/16/09 20.96 0.00 77.28
09/20/10 19.42 0.00 78.82
10/27/11 19.51 0.00 78.73
01/07/13 20.83 0.00 77.41
07/29/13 19.14 0.00 79.10
06/23/14 19.39 0.00 78.85
07/06/15 18.97 0.00 79.27
11/01/07 97.64 19.30 0.00 78.34
09/16/09 19.87 0.00 78.47
09/20/10 NM NM NM
11/01/07 94.72 18.32 0.00 76.40
09/16/09 18.81 0.00 76.38
09/20/10 17.51 0.00 77.68
10/27/11 17.68 0.00 77.51
01/07/13 18.78 0.00 76.41
07/29/13 18.31 0.00 76.88
06/23/14 17.68 0.00 77.51
07/06/15 17.30 0.00 77.89
11/01/07 NA 6.53 0.00 ---
09/16/09 7.03 0.00 75.21
09/20/10 6.40 0.00 75.84
10/27/11 6.47 0.00 75.77
01/07/13 7.23 0.00 75.01
07/29/13 6.95 0.00 75.29
06/23/14 6.69 0.00 75.55
07/06/15 6.47 0.00 75.77
09/16/09 20.36 0.00 79.16
09/20/10 NM NM NMMW-37 09/01/09 10 10-25 25 99.52
MW-36 03/10/03 10 10-25 25 82.24
MW-34 11/07/01 20 20-30 30 95.19
MW-33 11/07/01 20 20-30 30 98.34
MW-31 02/28/01 20 20-30 30 98.24
MW-30A 03/19/01 19 19-29 29 96.73
MW-29 10/15/98 25 25-35 35 98.15
12/04/12
06/26/13
05/22/14
MW-28 10/15/98 22 22-32 32 95.54
MW-27 10/03/96 8 8-18 18 98.78
MW-26 09/25/96 18 18-28 28 97.7005/22/14
Page 4 of 6
Date: 07/06/15
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
09/16/09 17.58 0.00 75.75
09/20/10 16.50 0.00 76.83
10/27/11 16.64 0.00 76.69
01/07/13 17.67 0.00 75.66
07/29/13 17.17 0.00 76.16
06/23/14 16.68 0.00 76.65
07/06/15 16.35 0.00 76.98
09/16/09 19.54 0.00 78.77
09/20/10 NM NM NM
09/16/09 24.24 0.00 77.82
09/20/10 NM NM NM
09/20/10 19.42 0.00 81.20
10/27/11 19.19 0.00 81.43
01/07/13 20.99 0.00 79.63
06/23/14 18.94 0.00 81.68
09/20/10 19.74 0.00 81.01
10/27/11 19.60 0.00 81.15
01/07/13 21.27 0.00 79.48
07/29/13 20.13 0.00 80.62
06/23/14 19.30 0.00 81.45
07/06/15 18.91 0.00 81.84
09/20/10 19.15 0.00 79.47
10/27/11 19.27 0.00 79.35
01/07/13 20.55 0.00 78.07
07/29/13 19.85 0.00 78.77
06/23/14 19.09 0.00 79.53
07/06/15 18.58 0.00 80.04
09/20/10 18.81 0.00 78.38
10/27/11 18.92 0.00 78.27
01/07/13 20.19 0.00 77.00
07/29/13 19.55 0.00 77.64
06/23/14 18.86 0.00 78.33
07/06/15 18.42 0.00 78.77
09/20/10 18.10 0.00 78.15
10/27/11 18.31 0.00 77.94
01/07/13 19.52 0.00 76.73
07/29/13 14.48 0.00 81.77
06/23/14 18.22 0.00 78.03
07/06/15 17.76 0.00 78.49
09/20/10 17.59 0.00 77.88
10/27/11 17.77 0.00 77.70
01/07/13 18.94 0.00 76.53
07/29/13 18.41 0.00 77.06
06/23/14 17.71 0.00 77.76
07/06/15 17.29 0.00 78.18
09/20/10 17.62 0.00 77.47
10/27/11 17.79 0.00 77.30
01/07/13 18.91 0.00 76.18
07/29/13 18.38 0.00 76.71
06/23/14 17.79 0.00 77.30
07/06/15 17.44 0.00 77.65
09/20/10 14.57 0.00 76.59
10/27/11 14.70 0.00 76.46
01/07/13 15.61 0.00 75.55
07/29/13 15.24 0.00 75.92
06/23/14 14.80 0.00 76.36
07/06/15 14.48 0.00 76.68
09/20/10 19.38 0.00 80.81
10/27/11 19.19 0.00 81.00
01/07/13 20.76 0.00 79.43
07/29/13 19.85 0.00 80.34
06/23/14 18.92 0.00 81.27
07/06/15 18.28 0.00 81.91
09/17/09 21.10 0.00 79.01
09/20/10 19.38 0.00 80.73
10/27/11 19.34 0.00 80.77
01/07/13 20.93 0.00 79.18
07/29/13 19.66 0.00 80.45
05/19/14 18.88 0.00 81.23 Pre-MMPE
05/23/14 19.21 0.00 80.90 Post-MMPE
06/23/14 19.06 0.00 81.05
06/01/15 17.75 0.00 82.36 Pre-MMPE
06/05/15 18.09 0.00 82.02 Post-MMPE
07/06/15 18.58 0.00 81.53
MW-1M 09/17/09 10 10-25 25 100.11
TW-1M 09/15/10 40 40-45 45 100.19
MW-48 09/15/10 10 10-25 25 91.16
MW-47 09/15/10 10 10-25 25 95.09
MW-46 09/15/10 10 10-25 25 95.47
MW-45 09/15/10 10 10-25 25 96.25
MW-44 09/15/10 10 10-25 25 97.19
MW-43 09/15/10 10 10-25 25 98.62
MW-42 09/16/10 10 10-25 25 100.75
MW-41 09/16/10 10 10-25 25 100.62
MW-40 09/16/09 10 10-25 25 102.06
MW-39 09/16/09 10 10-25 25 98.31
MW-38 09/16/09 10 10-25 25 93.33
Page 5 of 6
Date: 07/06/15
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID #: 0-022895
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
09/20/10 18.73 0.00 80.49
10/27/11 18.73 0.00 80.49
01/07/13 NM NM NM
07/29/13 19.35 0.00 79.87
05/19/14 18.26 0.00 80.96 Pre-MMPE
05/23/14 18.45 0.00 80.77 Post-MMPE
06/23/14 18.43 0.00 80.79
07/06/15 17.93 0.00 81.29
09/20/10 18.60 0.00 80.40
10/27/11 18.59 0.00 80.41
01/07/13 20.17 0.00 78.83
07/29/13 20.17 0.00 78.83
05/19/14 18.15 0.00 80.85 Pre-MMPE
05/23/14 18.26 0.00 80.74 Post-MMPE
06/23/14 18.31 0.00 80.69
06/01/15 17.07 0.00 81.93 Pre-MMPE
06/05/15 17.47 0.00 81.53 Post-MMPE
07/06/15 17.84 0.00 81.16
11/01/07 NA 20.89 0.00 ---
09/16/09 NM NM NM
09/20/10 NM NM NM
10/27/11 NM NM NM
01/07/13 NM NM NM
07/29/13 NM NM NM
06/23/14 NM NM NM
Notes:
• Reference point for elevation measurements: assumed elevation 100.00 ft.
• If free product is present in a well, groundwater elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness
x 0.8581].
• ft BGS: feet below ground surface.
• NA: Data not available.
• Top-of-casing elevations and well construction information for monitoring wells installed prior to 2007 reproduced from previous assessment
reports prepared by CES Engineering, P. C.
• Monitoring wells MW-9A, MW-10A, MW-15A and MW-25B were resurveyed on August 12, 2008 by GRI personnel.
• Monitoring wells MW-41 through MW-48, TW-1M, MW-1M, MW-2M and MW-3M were surveyed on September 17, 2010 by GRI personnel.
• Monitoring wells MW-1, MW-1A, MW-2 through MW-5, MWD-6, MW-7, MW-9, MW-10A, MW-11 through MW-15, MW-15A, MW-17,
MW-19 through MW-22, MW-23A, MW-24, MW-25B, MW-26 through MW-29, MW-30A, MW-31, MW-33, MW-34, MW-36 through MW-48
were installed in order to assess UST Incident Nos. 11963 and 13592 (Todd's Service Center and Bowen's Grocery).
• NM: Not Measured.
RW-1 07/22/03 10 10-30 30 100.03
MW-3M 09/16/10 10 10-25 25 99.00
MW-2M 09/16/10 10 10-25 25 99.22
Page 6 of 6
Date: 07/24/15 Facility ID#: 0-022895
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-1M 2 ----
MW-2M 2 ----
MW-3M 2 ----
MW-22 2 ----
MW-1M 2 ----
MW-3M 2 ----
MW-22 2 ----
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
TABLE 2
FREE PRODUCT RECOVERY RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Interface probe at top-of-casing
Gasoline 06/01/15 -
06/05/15 MMPE 16,317 --
Gasoline 05/19/14 -
05/23/14 MMPE 13,479 --
Page 1 of 1
Date: 07/24/15
MW-1M
MW-2M
MW-3M
MW-22
MW-1M
MW-3M
MW-22
107.90 29,796 0 107.90
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
Facility ID #: 0-022895
Total To Date 29,903.90 107.90
SUMMARY OF FLUID REMOVAL
75.68
Summary Total Fluids Removed (in gallons)
Current Event 16,392.68
Total Product Removed (in gallons)
3,604.79 136.84 391.89
Totals
Average
Effluent
Concentration
(ppm)
05/19/14 -
05/23/14 MMPE
06/01/15 -
06/05/15 MMPE 1,758.92
Total Amount
of Product
Recovered
(gallons)
32.22 13,479
Amount of
Vaporized
Product
(gallons)
32.22---
TABLE 3
FREE PRODUCT RECOVERY EVENT INFORMATION
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
94.37 352.09 75.68 16,317 ---75.68
Page 1 of 1
Date: 07/24/15
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered (gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
(total liquids)
MW-1M, MW-2M,
MW-3M and MW-
22
MMPE 05/19/14 -
05/23/14 13,511.22 $11,786.11 $0.87
MW-1M, MW-3M
and MW-22 MMPE 06/01/15 -
06/05/15 16,392.68 $11,409.36 $0.70
29,903.90 $23,195.47 $0.78
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
TABLE 4
FREE PRODUCT RECOVERY COST SUMMARY
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Comments
TOTAL (to date)
Cost per gallon for the event is based on
volume of 13,511.22 gallons of total fluids
recovered.
Cost per gallon for the event is based on
volume of 16,392.68 gallons of total fluids
recovered.
Facility ID #: 0-022895
Page 1 of 1
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NE
10/31/07 10,100 23,700 1,570 9,290 648 286 33.1 16.0 <5.00 71.6 13.0 14.1 166 988 309 39.8 NR NR NR
09/17/09 2,110 8,190 552 2,660 814 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 <44.0 313 73.9 J 10.1 2,510 2,080 2,990
09/20/10 9,050 29,400 2,100 11,000 8,740 <250 <250 <250 <120 111 J <100 <100 221 J 1,530 398 J 31.8 NR NR NR
10/27/11 14,400 39,900 2,940 14,200 3,320 391 J <100 <100 <100 133 J <110 <100 262 J 1,840 439 J NR NR NR NR
01/07/13 4,940 25,700 1,980 10,400 2,710 327 <10 <10 <10 74.1 <10 <10 195 1,390 354 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 9,320 36,700 3,200 16,300 6,320 556 20.4 J 16.8 J <10 143 19.4 J <10 362 2,800 698 NR NR NR NR
07/06/15 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/31/07 10,600 39,000 2,420 11,300 1,870 439 37.8 <10.0 <10.0 86.0 11.2 <10.0 175 1,230 356 23.0 NR NR NR
09/17/09 5,830 28,800 2,110 10,600 660 376 <45.0 1,080 <60.0 91.6 J <50.0 <50.0 161 J 1,270 289 29.9 5,000 3,150 4,860
09/20/10 4,680 12,000 1,210 5,650 7,310 137 <50.0 <50.0 <24.0 41.3 J <20.0 <20.0 66.8 J 525 140 116 NR NR NR
10/27/11 3,940 15,000 1,170 6,410 897 149 <20 <20 <21 33.0 J <21 <20 74.8 J 634 144 NR NR NR NR
01/07/13 0.67 3.7 0.41 J 1.70 0.35 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.16 J <0.10 NR NR NR NR
07/30/13 3,130 22,300 1,620 8,970 952 265 <10 <10 <10 43.4 J <10 <10 93.2 825 179 NR NR NR NR
06/24/14 1,450 8,130 752 4,340 769 157 1.5 J 1.5 J <1.0 24.0 3.6 J <1.0 51.7 434 96.0 NR NR NR NR
07/06/15 2,290 11,100 1,420 7,930 4,540 248 <36 <35 <35 42.6 J <40 <31 98.2 J 900 208 NR NR NR NR
02/28/07 15.0 <0.500 3.36 1.43 <0.500 15.5 0.880 0.870 <0.500 2.24 <0.500 0.710 1.57 2.38 <0.500 15.9 NR NR NR
10/31/07 59.1 0.930 14.6 7.97 <0.500 16.4 4.10 4.09 <0.500 11.3 <0.500 4.09 9.58 3.22 4.16 29.9 NR NR NR
09/17/09 20.1 <0.190 2.31 <0.220 <0.250 1.58 <0.180 0.970 J <0.240 2.65 <0.200 <0.200 1.39 0.883 J <0.180 7.05 106 <100 <100
09/20/10 13.7 2.15 0.606 J 1.85 J <0.500 3.61 <1.00 <1.00 <0.480 2.69 <0.400 <0.400 0.776 J 0.488 J <0.360 14.3 NR NR NR
10/27/11 8.4 0.22 J 0.89 1.1 J <0.13 1.8 <0.10 0.42 J <0.10 1.6 <0.11 <0.10 0.93 0.19 J <0.10 NR NR NR NR
01/07/13 0.74 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 1.0 <0.10 <0.10 0.55 J <0.10 <0.10 <0.10 0.14 J <0.10 0.22 J 0.11 J <0.10 0.28 J 0.36 J 0.15 J NR NR NR NR
07/06/15 2.9 <0.17 <0.15 0.62 J <0.16 0.98 0.35 J 0.59 <0.14 0.79 <0.16 <0.12 0.63 1.7 0.16 J NR NR NR NR
09/20/10 1,500 45,000 9,170 53,400 309 J 2,870 1,830 <500 <240 852 J <200 <200 2,410 21,900 5,330 30.6 NR NR NR
10/27/11 1,700 33,200 6,290 33,500 2,880 1,180 201 J 120 J <100 457 J <110 <100 1,290 8,760 2,370 NR NR NR NR
01/07/13 509 19,500 4,620 24,300 737 960 58.1 43.7 J <10 249 <10 22.7 J 761 4,610 1,340 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 894 19,200 4,580 27,300 1,170 858 471 269 <2.5 725 7.6 J 144 920 6,200 1,730 NR NR NR NR
07/06/15 381 14,200 4,810 28,600 620 1,440 98.9 J 59.1 J <35 264 <40 34.7 J 763 7,110 1,890 NR NR NR NR
10/31/07 1,120 5,620 1,490 4,130 <5.00 283 36.3 17.0 <5.00 82.5 <5.00 20.2 141 682 287 16.0 NR NR NR
09/17/09 274 2,280 666 1,810 <10.0 168 <7.20 <5.60 <9.60 58.6 <8.00 <8.00 64.8 392 124 12.9 2,770 2,250 1,480
09/20/10 568 1,780 630 2,340 <5.00 95.9 40.7 <10.0 11.5 J 38.0 <4.00 <4.00 52.1 539 160 19.6 NR NR NR
10/27/11 130 456 267 617 <0.13 47.9 3.2 2.4 1.8 26.0 <0.11 3.3 34.0 108 32.8 NR NR NR NR
01/07/13 590 4,770 1,400 5,120 <1.0 391 9.0 8.8 4.9 J 80.0 <1.0 11.9 132 804 248 NR NR NR NR
07/30/13 69.0 705 485 1,670 <2.0 216 6.1 J 5.8 J <2.0 40.2 <2.0 8.0 J 70.3 314 121 NR NR NR NR
06/24/14 14.8 38.1 12.3 79.1 <0.10 8.7 0.29 J 0.26 J 0.30 J 1.8 <0.10 0.39 J 2.2 9.2 4.1 NR NR NR NR
07/06/15 5.3 40.7 9.2 38.4 <0.16 2.0 <0.14 <0.14 <0.14 0.55 <0.16 <0.12 0.86 3.4 1.3 NR NR NR NR
MW-3
MW-4
MW-5 C9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)
MW-1A
MW-2 p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
Page 1 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
10/31/07 2.72 3.43 <0.500 1.17 6.10 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <5.00 NR NR NR
09/17/09 0.627 J 0.602 J <0.150 <0.220 0.868 J <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.200 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.700 2.84 J 1.23 J 2.21 J <1.25 <2.50 <2.50 <2.50 <1.20 <0.750 <1.00 <1.00 <1.10 0.756 J <0.900 6.89 NR NR NR
10/27/11 <0.13 0.52 <0.15 0.56 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.38 J 0.46 J <0.10 0.21 J 0.59 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/31/07 36.9 <0.500 14.6 <1.00 <0.500 6.30 1.63 2.71 <0.500 7.20 1.53 3.14 6.78 <0.500 <0.500 <5.00 NR NR NR
09/17/09 10.3 0.366 J 179 3.61 <0.250 58.7 <0.180 7.46 <0.240 57.3 1.75 0.588 J 93.3 2.06 0.795 J <1.50 758 489 481
09/20/10 1.91 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 0.485 J <0.200 <0.200 <0.220 <0.150 <0.180 25.0 NR NR NR
10/27/11 3.7 0.30 J <0.15 <0.30 <0.13 0.53 <0.10 0.41 J <0.10 0.77 0.26 J <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 19.1 <0.10 13.1 <0.22 0.33 J 3.0 1.3 2.9 <0.10 12.5 0.90 1.5 19.2 <0.10 <0.10 NR NR NR NR
07/30/13 7.3 <0.10 7.0 <0.22 0.43 J 1.5 0.46 J 0.78 <0.10 4.7 0.78 0.34 J 7.2 <0.10 <0.10 NR NR NR NR
06/24/14 0.16 J <0.10 0.15 J <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.13 J <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 0.930 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.79 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 11.3 <100 <100 <100
09/20/10 0.284 J <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.1 NR NR NR
10/27/11 0.55 0.23 J <0.15 0.46 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 2.9 <0.10 <0.10 <0.22 0.11 J <0.15 <0.10 0.13 J <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.7 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 7.29 <100 <100 <100
09/20/10 0.475 J 2.95 0.384 J 1.90 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 0.503 J <0.180 27.9 NR NR NR
10/27/11 <0.13 0.14 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.11 J <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.19 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
10/31/07 617 191 366 652 52.0 132 9.58 4.13 <0.500 28.5 0.640 5.68 43.6 199 81.9 7.17 NR NR NR
09/17/09 1,560 3,120 687 1,920 43.6 J 208 <18.0 <14.0 <24.0 53.3 J <20.0 <20.0 52.5 J 316 88.1 J 12.5 3,150 1,430 1,870
09/20/10 29.2 1.68 0.400 J 13.3 11.1 3.56 <0.500 <0.500 <0.240 1.53 <0.200 <0.200 0.304 J 5.78 <0.180 25.6 NR NR NR
10/27/11 3.4 <0.13 <0.15 <0.30 1.2 0.37 J <0.10 <0.10 <0.10 0.11 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 324 E 97.6 114 188.9 121 44.3 1.2 1.5 0.38 J 12.3 0.83 1.6 18.7 55.5 11.3 NR NR NR NR
07/30/13 276 194 66.4 249 98.8 36.9 0.89 0.97 0.30 J 8.6 0.61 1.1 12.7 39.6 7.7 NR NR NR NR
06/24/14 152 20.5 11.5 89.9 29.3 21.9 0.40 J 0.37 J 0.29 J 3.2 <0.10 0.65 3.6 14.9 1.9 NR NR NR NR
07/06/15 33.8 0.38 J 6.5 12.8 7.6 16.0 0.28 J 0.25 J <0.14 1.7 <0.16 0.55 2.2 4.4 <0.14 NR NR NR NR
MW-10A
MW-11
MWD-6
MW-7
MW-9A
Page 2 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
11/01/07 8,470 20,300 2,100 8,390 9,250 449 27.3 8.19 <0.500 76.3 46.0 6.75 154 1,280 420 18.8 NR NR NR
09/17/09 2,560 8,380 778 2,500 330 <100 <36.0 <28.0 <48.0 <30.0 <40.0 <40.0 88.1 J 552 141 J 3.22 2,630 1,700 2,360
09/20/10 1,500 517 260 764 845 76.3 7.59 J <5.00 <2.40 17.7 <2.00 <2.00 32.3 174 65.7 74.5 NR NR NR
10/27/11 3,120 9,080 895 4,130 2,990 128 <20 <20 <21 35.1 J <21 <20 83.9 J 613 160 NR NR NR NR
01/07/13 4,010 15,500 1,400 6,790 1,790 235 <10 <10 <10 52.3 <10 <10 146 1,080 241 NR NR NR NR
07/30/13 1,640 6,850 785 3,230 1,140 152 <25 <25 <25 32.5 J <25 <25 89.0 J 503 126 J NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 12.9 <0.500 2.65 <1.00 <0.500 <5.00 <0.500 2.06 <0.500 2.57 <0.500 <0.500 2.69 <0.500 <0.500 45.0 NR NR NR
09/17/09 8.77 <0.190 43.7 <0.220 <0.250 3.50 <0.180 3.19 <0.240 20.3 <0.200 0.454 J 26.4 <0.150 0.624 J 12.1 246 179 183
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 42.1 NR NR NR
10/27/11 0.15 J 0.24 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 1.2 <0.10 0.11 J <0.22 <0.10 <0.15 <0.10 0.20 J <0.10 0.34 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.83 0.14 J <0.10 <0.22 <0.10 <0.15 <0.10 0.11 J <0.10 0.33 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 199 2.45 88.3 101 14.8 63.7 8.79 4.09 <0.500 26.8 <0.500 6.02 20.5 104 36.3 47.6 NR NR NR
10/31/07 212 11.4 280 185 8.98 144 17.4 6.66 <0.500 46.8 <0.500 10.2 54.8 87.4 90.8 12.4 NR NR NR
09/17/09 153 193 261 200 3.32 J 143 <1.80 <1.40 <2.40 22.5 <2.00 <2.00 20.7 62.4 21.5 13.6 1,100 504 506
09/20/10 64.5 6.39 68.7 41.7 <0.250 66.9 2.58 1.94 <0.240 16.6 <0.200 0.391 J 12.3 24.4 0.665 J 50.2 NR NR NR
10/27/11 183 5.0 148 12.2 12.3 78.6 2.7 3.8 <0.52 32.0 <0.54 3.5 23.3 5.0 0.66 J NR NR NR NR
01/07/13 144 170 228 237.8 9.5 135 3.2 3.4 <0.50 26.5 <0.50 2.8 25.6 50.2 10.5 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/06/15 0.89 0.34 J 2.3 2.1 0.20 J 1.5 <0.14 <0.14 <0.14 0.24 J <0.16 <0.12 0.29 J 0.51 0.16 J NR NR NR NR
MW-15 06/24/14 38.8 282 213 1,120 <0.10 120 4.9 4.3 <0.10 24.8 <0.10 7.2 31.5 224 74.6 NS NS NS NS
11/01/07 358 1,690 1,320 3,240 <0.500 358 36.4 12.0 <0.500 81.5 <0.500 17.1 116 721 333 56.4 NR NR NR
09/17/09 78.6 1,030 513 1,680 <5.00 170 <3.60 <2.80 <4.80 45.4 <4.00 <4.00 44.3 360 112 9.16 2,640 1,100 1,460
09/20/10 551 756 542 1,570 <50.0 343 J <36.0 <28.0 <48.0 576 <40.0 <40.0 413 482 313 64.5 NR NR NR
10/27/11 151 534 458 1,230 <2.6 150 7.1 J 5.5 J <2.1 44.5 <2.1 8.0 J 64.9 287 130 NR NR NR NR
01/07/13 59.0 477 353 885 <2.0 125 5.3 J 5.5 J <2.0 35.9 <2.0 5.1 J 50.7 172 101 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/24/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 55.2 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.79 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 1.83 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 15.5 NR NR NR
10/27/11 <0.13 0.22 J <0.15 0.36 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-17
MW-12
MW-13
MW-14
MW-15A
Page 3 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
11/01/07 6.58 1.13 10.5 3.33 4.88 25.9 6.63 4.30 <0.500 13.2 0.630 2.50 7.16 2.52 <0.500 45.3 NR NR NR
09/17/09 <0.140 <0.190 37.7 22.6 <0.250 66.2 <0.180 3.38 <0.240 34.8 <0.200 <0.200 41.2 116 47.4 14.6 243 394 505
09/20/10 0.917 J <0.190 <0.150 0.270 J 1.51 1.64 2.65 1.35 <0.240 1.15 <0.200 <0.200 <0.220 <0.150 <0.180 49.2 NR NR NR
10/27/11 <0.13 0.24 J <0.15 0.56 J <0.13 0.25 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.23 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 7.5 12.5 0.12 J 40.4 2.4 2.6 <0.10 16.7 <0.10 0.87 10.4 47.0 1.0 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 16.5 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 1.32 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 <1.50 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.3 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 30.6 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 2.69 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.4 NR NR NR
09/17/09 11.1 0.398 J 1.69 11.3 <0.250 <0.500 <0.180 <0.140 <0.240 0.773 J <0.200 <0.200 0.749 J 3.69 1.81 5.70 429 105 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 1.20 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 8.09 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 <0.10 0.11 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
02/28/07 291 387 345 1,020 34.5 35.3 19.1 6.00 <0.500 33.2 29.4 4.95 75.2 523 115 18.1 NR NR NR
10/31/07 95.7 1,020 795 2,820 <2.50 155 46.4 16.6 <2.50 79.4 <2.50 13.4 224 1,190 373 <5.00 NR NR NR
09/17/09 78.9 J 2,270 1,900 8,570 <50.0 324 <36.0 <28.0 <48.0 156 J <40.0 <40.0 305 2,430 558 3.75 4,900 5,980 393,000
09/20/10 158 58.2 188 156 16.9 20.8 24.0 15.9 <2.40 30.9 30.5 <2.00 60.6 288 53.9 37.2 NR NR NR
10/27/11 69.3 301 487 1,730 <2.6 78.9 16.6 12.7 <2.1 61.0 4.2 J 9.4 J 190 955 267 NR NR NR NR
01/07/13 90.4 261 1,180 4,820 29.5 240 27.3 24.5 <2.0 172 12.4 16.0 542 3,480 828 NR NR NR NR
07/30/13 91.0 199 648 2,480 9.7 J 115 27.0 22.5 J <5.0 99.2 12.5 J 15.6 J 382 1,680 486 NR NR NR NR
06/23/14 8.6 5.3 34.6 111 <0.10 6.4 4.2 3.3 <0.10 8.5 0.73 2.6 28.5 67.8 20.7 NR NR NR NR
07/06/15 12.6 17.4 97.2 379 <0.82 20.3 7.1 4.9 <0.71 13.1 <0.80 3.7 46.3 211 60.0 NR NR NR NR
MW-19
MW-20
MW-21
MW-22
Page 4 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
02/28/07 7.39 <0.500 4.73 7.21 <0.500 <5.00 <0.500 0.590 <0.500 1.88 <0.500 0.990 2.42 17.4 2.49 16.2 NR NR NR
10/31/07 3.32 <0.500 1.98 2.58 <0.500 <5.00 <0.500 <0.500 <0.500 1.53 <0.500 <0.500 0.810 6.75 1.27 16.4 NR NR NR
09/17/09 3.86 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 0.792 J <0.200 <0.200 0.387 J 3.64 <0.180 18.7 <100 <100 <100
09/20/10 14.2 0.242 J 2.39 9.05 <0.250 6.07 2.53 3.44 <0.240 6.40 <0.200 0.580 J 1.64 20.4 1.69 20.9 NR NR NR
10/27/11 7.0 0.22 J 3.7 3.1 <0.13 2.3 <0.10 0.61 <0.10 2.0 <0.11 0.95 1.8 6.8 <0.10 NR NR NR NR
01/07/13 1.7 <0.10 <0.10 0.28 J <0.10 0.41 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.96 <0.10 NR NR NR NR
07/30/13 12.3 0.15 J 4.1 5.5 <0.10 3.5 <0.10 1.4 <0.10 3.6 0.16 J 1.8 4.4 15.8 <0.10 NR NR NR NR
06/24/14 7.4 <0.10 3.1 3.0 <0.10 2.3 <0.10 0.83 <0.10 2.1 <0.10 1.1 2.4 8.6 0.14 J NR NR NR NR
07/06/15 22.0 0.47 J 11.7 19.8 <0.16 12.7 0.14 J 1.4 <0.14 4.7 <0.16 2.6 5.0 36.5 1.0 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 13.1 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 17.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 4.67 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
11/01/07 61.5 95.7 46.1 75.8 5.64 12.2 2.94 2.03 <0.500 3.77 5.95 <0.500 7.17 20.6 7.97 32.3 NR NR NR
09/17/09 11.5 <0.190 <0.150 <0.220 10.7 5.35 <0.180 <0.140 <0.240 0.515 J 12.7 <0.200 <0.220 <0.150 <0.180 8.33 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 26.8 NR NR NR
10/27/11 <0.13 0.15 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.49 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.57 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 4,210 2,780 1,120 2,200 2,350 1,690 12.8 4.70 3.71 53.9 11.0 3.30 96.9 594 143 6.94 NR NR NR
11/01/07 4,130 2,880 1,150 2,220 1,720 190 14.9 6.23 1.65 47.7 9.05 4.76 89.0 509 139 21.6 NR NR NR
09/17/09 3,910 6,350 952 2,950 1,730 172 <18.0 <14.0 <24.0 50.3 J <20.0 <20.0 75.4 J 424 117 4.19 1,950 1,670 83,000
09/20/10 25.1 <0.190 0.827 J <0.220 96.2 0.957 J <0.500 <0.500 <0.240 0.313 J <0.200 <0.200 <0.220 <0.150 <0.180 45.3 NR NR NR
10/27/11 4.1 0.22 J 0.54 <0.30 4.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 257 102 77.0 149.9 147 13.3 <1.0 <1.0 <1.0 4.7 J <1.0 <1.0 10.3 47.7 9.2 NR NR NR NR
07/30/13 180 173 40.7 120 188 7.3 <0.10 0.15 J <0.10 2.1 0.44 J <0.10 3.3 10.1 2.2 NR NR NR NR
06/23/14 14.6 1.6 1.5 4.7 86.5 0.46 J <0.10 <0.10 <0.10 0.15 J 0.13 J <0.10 0.13 J 0.73 <0.10 NR NR NR NR
07/06/15 2.4 <0.17 0.22 J <0.43 12.1 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 3.29 <5.00 <0.500 <0.500 <0.500 <0.500 2.81 <0.500 <0.500 <0.500 <0.500 9.40 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-24
MW-25B
MW-26
MW-27
MW-23A
Page 5 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.6 NR NR NR
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 692 90.3 93.4 81.7 120 15.4 3.91 2.96 <0.500 28.0 1.04 1.25 15.0 16.7 5.44 6.88 NR NR NR
11/01/07 3,810 2,110 788 1,580 1,370 148 13.7 6.32 <0.500 40.9 9.59 5.45 67.8 364 92.0 40.5 NR NR NR
09/17/09 2,860 5,780 696 2,320 869 127 <18.0 <14.0 <24.0 37.8 J <20.0 <20.0 61.2 J 370 91.5 J <1.50 1,690 1,280 1,800
09/20/10 1,140 939 266 636 402 <100 <18.0 <14.0 <24.0 28.8 J <20.0 <20.0 37.3 J 156 36.4 J 13.4 NR NR NR
10/28/11 2,130 1,340 487 762 1,060 80.2 6.4 J <5.1 <5.2 32.1 5.9 J <5.0 50.0 236 25.9 NR NR NR NR
01/07/13 2,110 6,130 731 3,300 1,110 150 <5.0 <5.0 <5.0 31.2 <5.0 <5.0 74.5 551 138 NR NR NR NR
07/30/13 1,420 3,280 438 1,590 858 78.8 <10 <10 <10 20.2 J <10 <10 43.0 J 289 69.7 NR NR NR NR
06/23/14 508 2,480 268 1,070 319 67.2 2.6 2.2 <0.10 19.9 1.4 1.4 38.7 206 42.7 NR NR NR NR
07/06/15 525 1,780 317 1,290 157 90.1 <7.2 <6.9 <7.1 21.4 J <8.0 <6.1 35.0 270 65.7 NR NR NR NR
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 69.0 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 218 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 28.4 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
02/28/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 12.2 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0500 <0.500 <0.500 90.3 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 13.9 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 27.6 NR NR NR
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 91.1 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 35.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-30A
MW-31
MW-33
MW-28
MW-29
Page 6 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
02/28/07 97.3 <0.500 <0.500 <1.00 50.9 <5.00 <0.500 <0.500 <0.500 1.13 <0.500 <0.500 <0.500 <0.500 <0.500 58.8 NR NR NR
11/01/07 146 <0.500 <0.500 <1.00 60.8 <5.00 <0.500 <0.500 <0.500 2.00 <0.500 <0.500 <0.500 <0.500 <0.500 165 NR NR NR
09/17/09 102 <0.190 <0.150 <0.220 32.2 <0.500 <0.180 <0.140 <0.240 1.10 <0.200 <0.200 <0.220 <0.150 0.525 J 12.5 <100 <100 <100
09/20/10 72.4 0.908 J 4.77 4.41 78.0 4.60 0.382 J 0.303 J <0.480 2.50 <0.400 <0.400 1.21 J <0.300 <0.360 40.4 NR NR NR
10/28/11 0.13 J 0.15 J <0.15 <0.30 1.9 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.12 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 3.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 11.7 J <10 <10 <22 451 <15 <10 <10 <10 <10 <10 <10 <10 <10 <10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 2.2 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 3.9 <0.17 0.17 J <0.43 5.1 0.45 J <0.14 <0.14 <0.14 0.17 J <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
03/01/07 <0.500 <0.500 <0.500 <1.00 2.36 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 28.4 NR NR NR
11/01/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 19.0 NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.75 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.410 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 24.6 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 20.3 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 <0.190 <0.150 <0.220 3.07 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 39.4 <100 <100 <100
09/20/10 <0.140 <0.190 <0.150 <0.220 0.794 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 77.4 NR NR NR
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 25.8 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
09/17/09 <0.140 1.82 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 14.0 <100 <100 <100
10/27/11 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-38
MW-39
MW-40
MW-34
MW-36
MW-37
Page 7 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 0.327 J <0.180 100 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
09/20/10 6.54 1.30 17.4 77.1 <0.250 1.43 J 3.24 0.680 J <0.240 1.85 <0.200 <0.200 4.04 25.8 9.18 80.2 1,450 431 665
10/27/11 10.7 1.3 1.5 11.0 0.15 J 0.12 J 0.14 J <0.10 <0.10 0.21 J <0.11 <0.10 0.29 J 1.6 2.1 NR NR NR NR
01/07/13 18.1 3.1 10.7 39.9 <0.10 <0.15 0.15 J 0.18 J <0.10 1.1 <0.10 0.12 J 2.0 7.7 5.1 NR NR NR NR
07/29/13 5.6 0.31 J 0.27 J 3.5 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 0.41 J 1.1 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 78.5 <100 <100 <100
10/27/11 <0.13 0.19 J <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.11 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 20.4 0.447 J 4.18 1.01 8.18 <1.00 <0.180 <0.140 <0.240 1.11 <0.200 <0.200 0.961 J <0.150 <0.180 104 <100 <100 <100
10/28/11 11.4 0.22 J <0.15 0.36 J 4.8 <0.10 <0.10 <0.10 <0.10 0.24 J <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 5.3 <0.10 0.11 J <0.22 4.6 <0.15 <0.10 <0.10 <0.10 0.11 J <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 46.7 0.25 J 2.7 <0.22 11.9 <0.15 0.13 J 0.13 J <0.10 1.1 <0.10 <0.10 0.60 <0.10 <0.10 NR NR NR NR
06/23/14 1.2 <0.10 <0.10 <0.20 2.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 229 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 1.17 <0.190 <0.150 0.276 J 1.99 <1.00 <0.180 <0.140 <0.240 0.415 J 2.32 <0.200 <0.220 <0.150 <0.180 106 <100 <100 <100
10/28/11 <0.13 0.14 J <0.15 0.48 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 0.17 J <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 0.17 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 0.25 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.40 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 26.6 <0.190 <0.150 <0.220 12.0 <1.00 0.201 J 0.177 J <0.240 1.43 <0.200 <0.200 <0.220 <0.150 <0.180 116 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 101 <0.50 <0.50 <1.08 11.0 <0.74 <0.50 <0.50 <0.50 1.8 J <0.50 <0.50 <0.50 <0.50 <0.50 NR NR NR NR
07/30/13 12.9 <0.10 <0.10 <0.22 1.9 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
MW-44
MW-45
MW-46
MW-47
MW-41
MW-42
MW-43
Page 8 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/20/10 <0.140 <0.190 <0.150 <0.220 0.502 J <1.00 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 49.9 <100 <100 <100
10/28/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 0.96 <0.10 <0.10 <0.22 1.6 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 0.18 J <0.10 <0.10 <0.22 0.38 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 <0.10 <0.10 <0.10 <0.20 0.69 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 9.6 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
09/20/10 4.95 4.15 4.89 18.1 <0.500 <2.00 2.10 <0.280 <0.480 5.78 <0.400 <0.400 4.07 2.60 2.52 3.41 <100 <100 <100
10/27/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/30/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <3.4 570 <3.0 <8.6 <3.3 <2.4 <2.9 <2.8 <2.8 <2.4 <3.2 <2.4 <3.1 <2.7 <2.7 NR NR NR NR
09/17/09 1,310 36,100 4,070 22,700 211 J 1,060 <90.0 4,200 <120 265 J <100 642 642 4,900 1,170 4.26 12,200 10,700 15,500
09/20/10 1,130 11,900 1,410 6,210 <100 1,640 608 <56.0 <96.0 1,150 792 <80.0 896 2,850 964 45.3 NR NR NR
10/27/11 1,460 24,100 3,970 22,300 244 J 1,000 <100 <100 <100 263 J 226 J <100 763 5,320 1,430 NR NR NR NR
01/07/13 528 16,300 3,830 21,920 45.6 1,000 50.6 27.8 <5.0 186 73.1 18.5 J 589 4,520 1,090 NR NR NR NR
07/30/13 982 23,500 3,030 15,600 208 J 523 <50 <50 <50 110 J 220 J <50 344 2,400 582 NR NR NR NR
06/24/14 1,210 10,600 2,990 21,600 273 1,930 240 128 J <25 296 491 90.4 J 1,140 11,100 3,000 NR NR NR NR
07/06/15 975 17,100 3,150 20,300 <82 1,100 <72 <69 <71 140 J <80 <61 427 4,270 1,040 NR NR NR NR
09/20/10 5.49 4.12 4.89 17.7 3.04 2.27 J 15.7 <0.280 <0.480 5.70 3.73 <0.400 4.07 5.24 6.11 33.2 496 <100 380
10/27/11 <0.13 0.37 J 0.26 J 1.4 J <0.13 0.24 J 6.9 2.6 <0.10 1.6 <0.11 0.59 0.13 J 0.95 3.2 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/30/13 <0.10 0.16 J 0.85 1.9 <0.10 0.99 5.8 2.7 <0.10 2.2 <0.10 0.81 0.27 J 5.9 9.6 NR NR NR NR
06/24/14 <0.10 <0.10 <0.10 <0.20 <0.10 0.34 J 0.91 0.40 J <0.10 <0.10 <0.10 0.25 J <0.10 0.32 J 0.34 J NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 2.5 0.92 <0.14 <0.12 <0.16 0.50 <0.16 <0.14 0.34 J NR NR NR NR
09/20/10 1,090 4,890 1,020 3,150 159 J 601 J 439 <56.0 <96.0 1,150 641 <80.0 829 1,030 606 28.8 25,900 5,280 16,900
10/27/11 1,430 12,300 1,610 6,600 158 352 <25 <26 <26 91.4 J 116 J <25 207 1,360 363 NR NR NR NR
01/07/13 1,120 13,500 1,670 7,150 54.8 312 <10 <10 <10 64.6 131 <10 192 1,390 319 NR NR NR NR
07/30/13 472 6,790 1,080 4,000 <25 171 <25 <25 <25 45.6 J 54.3 J <25 131 811 195 NR NR NR NR
06/24/14 161 2,150 288 1,290 12.6 J 37.2 <5.0 <5.0 <5.0 13.3 J 18.9 J <5.0 29.4 276 78.1 NR NR NR NR
07/06/15 220 4,690 564 2,660 <33 98.1 J <29 <28 <28 25.9 J <32 <24 65.3 J 503 134 NR NR NR NR
11/06/07 <0.500 <0.500 <0.500 <1.00 <0.500 <5.00 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <0.500 NR NR NR NR
09/17/09 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.180 <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 NR NR NR NR
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <0.500 <0.500 <0.500 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 3.45 NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-1M
MW-2M
MW-3M
WSW-5
MW-48
TW-1M
Page 9 of 10
Date : 07/27/15
EPA
Method
6010B
Well IDDate Sampled (mm/dd/yy)1 600 600 500 20 6 70 70 0.02 70 70 25 70 400 400 15 400 700 200
5,000 260,000 84,500 85,500 20,000 6,000 6,900 8,500 50 25,000 70,000 11,700 30,000 28,500 25,000 15,000 NE NE NEC9-C12 AliphaticsC9-C10 Aromatics2L Standard (mg/l)
GCL (mg/l)p-Isopropyltoluenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneLeadC5-C8 AliphaticsNaphthalenen-Butylbenzenesec-Butylbenzene1,2-DibromoethaneIsopropylbenzeneIPEContaminant of
Concern
BenzeneTolueneEthylbenzeneXylenesMTBE TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
MILLER'S COUNTRY STORE (INCIDENT NO. 31939)
Facility ID s: 0-022895
Analytical Method
EPA Method 6200B MADEP Method VPH
09/20/10 <0.140 <0.190 <0.150 <0.220 <0.250 <1.00 0.189 J <0.140 <0.240 <0.150 <0.200 <0.200 <0.220 <0.150 <0.180 2.44 J NR NR NR
10/28/11 <0.13 0.14 J <0.15 <0.30 <0.13 0.11 J <0.10 <0.10 <0.10 <0.10 <0.11 <0.10 <0.11 <0.10 <0.10 NR NR NR NR
01/07/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
07/29/13 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
06/23/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
07/06/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.14 <0.12 <0.16 <0.12 <0.16 <0.14 <0.14 NR NR NR NR
01/07/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR
06/23/14 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
Notes:
• Results reported in µg/l (micrograms per liter).
• NE: Standard not established.
• Concentrations in bold face type exceeded the 2L standards.
• J: Estimated value.
• E: Value exceeds calibration range.
• <: Less than the method detection limit specified in the laboratory report.
• NR: Analysis not requested.
• NS: Not sampled.
• Other compounds detected in the 07/06/15 sampling event that exceeded the 2L Standards: 1,2-DCA (0.42 J µg/l) in MW-11 and styrene (197 µg/l) in MW-1M.
• 2L Standard: as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• For other compounds detected that did not exceed the 2L Standard, please refer to the laboratory reports.
WSW-13
WSW-18
Page 10 of 10

APPENDICES

APPENDIX A
MMPE Data, Calculations and Disposal Manifests
Site Name :Miller's Country Store Incident Number :31939
Site Location:1706 US Highway 17 North, Merry Hill, NC
Client Name:Ms. Shirley Miller
Blower Specifications For Vacuum Truck (e.g: 2500 cfm @ 24 in. of Hg) :280 cfm @ 24 in. of Hg Stack Diameter (inches):2
Start Time :12:00 Start Date:06/01/15 End Time :12:00 End Date:06/05/15
Note: Take all the readings listed below about 3 to 4 times every day at approximately the same time.
MMPE Contractor:Greenwood Applied Services Consultant:Geological Resources, Inc.
EXTRACTION WELL INFORMATION:
MW-1M MW-3M MW-22
2 2 2
18.25 17.57 17.85
18.25 17.57 17.85
Date Time System Vacuum Exhaust Velocity Temperature Rel. Humidity OVA
(in. of Hg)(ft/min)(°F)(%)(ppm)
12:15 20.00 1,415 100.2 60.4 885.8 0
17:00 20.00 1,329 100.0 46.8 810.0 21
7:15 20.00 2,132 100.1 55.7 515.1 56
11:45 13.00 1,813 97.6 49.6 315.3 20
16:00 13.00 2,554 97.8 92.8 48.7 21
7:30 18.00 1,374 86.9 65.0 106.3 24
12:15 18.00 1,825 94.3 66.9 328.9 27
16:00 18.00 1,711 90.1 60.8 236.8 29
7:00 18.00 1,755 89.9 66.8 196.6 39
12:00 18.00 1,285 90.7 77.7 202.0 45
16:00 17.00 1,770 90.4 76.1 323.2 9
6:45 17.00 1,744 95.2 61.9 407.9 24
11:45 12.00 2,159 93.6 52.9 200.6 25
FLUID RECOVERY SUMMARY:
Day 1 (24 hours)Day 2 (48 hrs)Day 3 (72 hrs)Day 4 (96 hrs)
Total Fluid Recovered (gallons)8,876 1,211 3,275 2,955
Total Product Recovered (gallons)------------
Tank Stick
(inch)
Vol. Rec.
(gal)
06/01/15
06/02/15
06/03/15
06/04/15
06/05/15
0
Day
MOBILE MULTI-PHASE EXTRACTION EVENT DATA SHEET - FIELD LOG 1
Well Number
Diameter (inch)
Initial Stinger Depth (ft.)
TOTAL (event)
16,317
Final Stinger Depth (ft.)
Page 1 of 2
Site Name :Miller's Country Store Incident Number :31939
Site Location:1706 US Highway 17 North, Merry Hill, NC
Client Name:Ms. Shirley Miller
Start Time :12:00 06/05/15
Note: Take all the readings listed below about 3 to 4 times every day at approximately the same time.
MMPE Contractor:Greenwood Applied Services Consultant:Geological Resources, Inc.
MW-1M MW-3M MW-22
Initial DTW (ft.)17.75 17.07 17.35
Initial DTP (ft.)---------
Final DTW (ft.)18.09 17.47 17.65
Final DTP (ft.)---------
DTW = Depth to Water; DTP = Depth to Product
OBSERVATION WELLS (VACUUM /WATER LEVELS)
Well 1 Well 2 Well 3 Well 4 Well 5 Well 6
Vacuum Water Lvl Vacuum Water Lvl Vacuum Water Lvl
(in. H2O)(ft.)(in. H2O)(ft.)(in. H2O)(ft.)
12:15 19.00 20.00 20.00 0.20 1.50
17:00 19.00 20.00 20.00 0.20 1.50
7:15 19.00 19.00 20.00 0.30 17.78 1.40 17.53
11:45 6.00 10.00 12.00 0.30 1.40
16:00 6.00 10.00 14.00 0.30 1.40
7:30 10.00 18.00 14.00 0.30 1.40
12:15 12.00 17.00 12.00 0.30 17.99 1.40 17.67
16:00 12.00 17.00 11.00 0.30 2.00
7:00 11.00 18.00 11.00 0.30 2.00
12:00 11.00 10.00 10.00 0.30 18.06 2.00 17.98
16:00 11.00 10.00 10.00 0.30 2.00
6:45 12.00 17.00 10.00 0.30 2.00
11:45 12.00 16.00 11.00
17.64
OBSERVATION WELLS (WATER LEVELS)
EXTRACTION POINTS - VACUUM (inches of Hg)
MW-2M
MW-22
MW-23A
17.44
MOBILE MULTI-PHASE EXTRACTION EVENT DATA SHEET - FIELD LOG 2
Water/Product Levels
12:00
DATE TIME
------
MW-1M
Start Date:06/01/15
EXTRACTION POINTS - VACUUM (inches of Hg)
06/04/15
MW-2MMW-23A
06/02/15
MW-3M
06/01/15
06/05/15
End Date:End Time:
---
17.78 17.53
---
06/03/15
Page 2 of 2
MOBILE MULTI-PHASE EXTRACTION EVENT
SITE NAME:Miller's Country Store
INCIDENT NUMBER:31939
AVERAGE DEPTH TO GROUNDWATER:17.51 feet
DESCRIBE SOIL IN THE SATURATED ZONE:N/A
INDICATE AVERAGE HYDRAULIC CONDUCTIVITY (if known): Unknown
IDENTIFY THE WELL AND THE I.D. OF EACH WELL USED FOR AFVR:MW-1M, MW-3M and MW-22 - 2"
PROVIDE BLOWER SPECIFICATIONS OF THE VACUUM TRUCK (cfm @ in Hg):280 CFM @ 24" Hg
TOTAL NUMBER OF DATA POINTS :13 (No. of readings taken during MMPE event)
DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd)
Vacuum Velocity Pipe ID Temp Rel Humid Water Qstd
(inches of Hg)(ft/min)(in)(°F)(%)Vapor (%)(flow)
06/01/15 12:15 20.00 1,415 2 100.2 60.40 0.0255 28.35
06/01/15 17:00 20.00 1,329 2 100.0 46.80 0.0195 26.81
06/02/15 7:15 20.00 2,132 2 100.1 55.70 0.0234 42.82
06/02/15 11:45 13.00 1,813 2 97.6 49.60 0.0192 36.74
06/02/15 16:00 13.00 2,554 2 97.8 92.80 0.0371 50.79
06/03/15 7:30 18.00 1,374 2 86.9 65.00 0.0180 28.42
06/03/15 12:15 18.00 1,825 2 94.3 66.90 0.0235 37.03
06/03/15 16:00 18.00 1,711 2 90.1 60.80 0.0186 35.16
06/04/15 7:00 18.00 1,755 2 89.9 66.80 0.0204 36.01
06/04/15 12:00 18.00 1,285 2 90.7 77.70 0.0245 26.22
06/04/15 16:00 17.00 1,770 2 90.4 76.10 0.0237 36.17
06/05/15 6:45 17.00 1,744 2 95.2 61.90 0.0223 35.38
06/05/15 11:45 12.00 2,159 2 93.6 52.90 0.0181 44.11
0:00 0.00 0 0 0.0 0.00 0.0000 0.00
Averages --17.08 1,758.92 2.00 94.37 64.11 0.02259 35.69
NOTES
Qstd = Flow at DSCFM
Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg)
Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube)
Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck)
Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F)
Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping
Water Vapor in % = Pounds of water per pound of dry air, derived from the Psychrometric chart
(temp Vs relative humidity)
EQUATION
Qstd = (1-Water Vapor) * velocity * (PI * (diameter/24)^2) * (528°R/(Temp + 460))
Date Time
EMISSION CALCULATIONS
15 28.35 885.8 4 3,543.20 18,842.11 0.001176313 2.00 0.50
300 26.81 810.0 4 3,240.00 17,229.75 0.001075653 1.73 8.65
1,155 42.82 515.1 4 2,060.40 10,956.84 0.000684036 1.76 33.83
1,425 36.74 315.3 4 1,261.20 6,706.84 0.000418708 0.92 21.92
1,680 50.79 48.7 4 194.80 1,035.91 0.000064672 0.20 5.52
2,610 28.42 106.3 4 425.20 2,261.14 0.000141163 0.24 10.47
2,895 37.03 328.9 4 1,315.60 6,996.13 0.000436768 0.97 46.83
3,120 35.16 236.8 4 947.20 5,037.04 0.000314463 0.66 34.50
4,020 36.01 196.6 4 786.40 4,181.94 0.000261078 0.56 37.80
4,320 26.22 202.0 4 808.00 4,296.80 0.000268249 0.42 30.38
4,560 36.17 323.2 4 1,292.80 6,874.88 0.000429199 0.93 70.78
5,445 35.38 407.9 4 1,631.60 8,676.56 0.000541678 1.15 104.34
5,745 44.11 200.6 4 802.40 4,267.02 0.000266390 0.71 67.51
0.00 0.0 0 0.00 0.00 0.000000000 0.00 0.00
Averages 35.69 352.09 4.00 1408.37 7,489.46 0.000467567 0.94 36.39
Total emissions in pounds 473.03
NOTES
PPM measured = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping
K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6)
PPMg = PPMv, Volumetric concentration as gasoline emission, dry basis at STP
Cg:m = mg/dsm3, mass concentration of gasoline emission
Mg = 128 mg/mg-mole, molecular weight of gasoline (this value may vary depending on contaminant)
K3 = 24.07 dsm^3/1E6 mg-mole, mass to volume conversion factor at STP
Cg = lb/dcsf, mass concentration of gasoline emission, dry basis at STP
PMRg = lb/hr, pollutant mass removal rate of gasoline emission
PMR = pollutant mass removal of gasoline emission over time
NM = Not measured due to OVA malfunction.
EQUATIONS
PPMg = PPM measured * K
Cg:m = PPMg * (Mg / K3)
Cg = Cg:m * 62.43E-09 lb-m^3/mg-ft^3
PMRg = Cg * Qstd * 60 min/hr
PMR = PMRg * ((T2 - T1) / 60)
Elapsed
Time
(min)
Flow
(DSCFM)
Cg
(lb/dscf)
PMRg
(lb/hr)
PMR
(lb)
PPM
measured
(ppm)
K
(#C-gas)PPMg
Cg:m
(mg/dsm^3)

APPENDIX B
Laboratory Report – Ground Water Samples
07/14/15
Technical Report for
GRI (Geological Resources Inc.)
Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
31939/2721
Accutest Job Number: FA25800
Sampling Date: 07/06/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: Michael Senglaub
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
07/14/15
e-Hardcopy 2.0
Automated Report
35
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 35
FA25800
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA25800-1: MW-1M ....................................................................................................7
3.2: FA25800-2: MW-2M ....................................................................................................9
3.3: FA25800-3: MW-3M ....................................................................................................11
3.4: FA25800-4: MW-22 ......................................................................................................13
3.5: FA25800-5: TW-1M .....................................................................................................15
3.6: FA25800-6: TRIP BLANK ...........................................................................................17
Section 4: Misc. Forms ............................................................................................................19
4.1: Chain of Custody ...........................................................................................................20
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................23
5.1: Method Blank Summary ................................................................................................24
5.2: Blank Spike Summary ...................................................................................................28
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................32 123452 of 35
FA25800
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA25800
Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Project No: 31939/2721
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA25800-1 07/06/15 13:10 JHHM 07/07/15 AQ Ground Water MW-1M
FA25800-2 07/06/15 13:37 JHHM 07/07/15 AQ Ground Water MW-2M
FA25800-3 07/06/15 13:15 JHHM 07/07/15 AQ Ground Water MW-3M
FA25800-4 07/06/15 13:29 JHHM 07/07/15 AQ Ground Water MW-22
FA25800-5 07/06/15 13:25 JHHM 07/07/15 AQ Ground Water TW-1M
FA25800-6 07/06/15 00:00 JHHM 07/07/15 AQ Trip Blank Water TRIP BLANK
3 of 35
FA25800 1
Summary of Hits Page 1 of 2
Job Number:FA25800
Account:GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA25800-1 MW-1M
Benzene 975 250 86 ug/l SM 6200B
Ethylbenzene 3150 250 76 ug/l SM 6200B
Isopropylbenzene 140 J 250 59 ug/l SM 6200B
Naphthalene 1100 250 61 ug/l SM 6200B
n-Propylbenzene 427 250 78 ug/l SM 6200B
Styrene 197 J 250 60 ug/l SM 6200B
Toluene 17100 250 83 ug/l SM 6200B
1,2,4-Trimethylbenzene 4270 250 68 ug/l SM 6200B
1,3,5-Trimethylbenzene 1040 250 68 ug/l SM 6200B
m,p-Xylene 13600 500 150 ug/l SM 6200B
o-Xylene 6690 250 67 ug/l SM 6200B
Xylene (total)20300 750 220 ug/l SM 6200B
FA25800-2 MW-2M
n-Butylbenzene 2.5 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.92 0.50 0.14 ug/l SM 6200B
p-Isopropyltoluene 0.50 0.50 0.12 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.34 J 0.50 0.14 ug/l SM 6200B
FA25800-3 MW-3M
Benzene 220 100 34 ug/l SM 6200B
Ethylbenzene 564 100 30 ug/l SM 6200B
Isopropylbenzene 25.9 J 100 24 ug/l SM 6200B
Naphthalene 98.1 J 100 24 ug/l SM 6200B
n-Propylbenzene 65.3 J 100 31 ug/l SM 6200B
Styrene 37.1 J 100 24 ug/l SM 6200B
Toluene 4690 100 33 ug/l SM 6200B
1,2,4-Trimethylbenzene 503 100 27 ug/l SM 6200B
1,3,5-Trimethylbenzene 134 100 27 ug/l SM 6200B
m,p-Xylene 1760 200 59 ug/l SM 6200B
o-Xylene 896 100 27 ug/l SM 6200B
Xylene (total)2660 300 86 ug/l SM 6200B
FA25800-4 MW-22
Benzene 12.6 2.5 0.86 ug/l SM 6200B
n-Butylbenzene 7.1 2.5 0.72 ug/l SM 6200B
sec-Butylbenzene 4.9 2.5 0.69 ug/l SM 6200B
Ethylbenzene 97.2 2.5 0.76 ug/l SM 6200B
Isopropylbenzene 13.1 2.5 0.59 ug/l SM 6200B
p-Isopropyltoluene 3.7 2.5 0.61 ug/l SM 6200B
4 of 35
FA25800 2
Summary of Hits Page 2 of 2
Job Number:FA25800
Account:GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Naphthalene 20.3 2.5 0.61 ug/l SM 6200B
n-Propylbenzene 46.3 2.5 0.78 ug/l SM 6200B
Styrene 1.3 J 2.5 0.60 ug/l SM 6200B
Toluene 17.4 2.5 0.83 ug/l SM 6200B
1,2,4-Trimethylbenzene 211 2.5 0.68 ug/l SM 6200B
1,3,5-Trimethylbenzene 60.0 2.5 0.68 ug/l SM 6200B
m,p-Xylene 281 5.0 1.5 ug/l SM 6200B
o-Xylene 97.9 2.5 0.67 ug/l SM 6200B
Xylene (total)379 7.5 2.2 ug/l SM 6200B
FA25800-5 TW-1M
Toluene a 570 10 3.3 ug/l SM 6200B
FA25800-6 TRIP BLANK
Methyl Chloride 0.23 J 0.50 0.16 ug/l SM 6200B
(a) xNot used, dilution required
5 of 35
FA25800 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
6 of 35
FA25800 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1M
Lab Sample ID:FA25800-1 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039722.D 500 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 975 250 86 ug/l
108-86-1 Bromobenzene ND 250 80 ug/l
74-97-5 Bromochloromethane ND 250 80 ug/l
75-27-4 Bromodichloromethane ND 250 74 ug/l
75-25-2 Bromoform ND 250 55 ug/l
104-51-8 n-Butylbenzene ND 250 72 ug/l
135-98-8 sec-Butylbenzene ND 250 69 ug/l
98-06-6 tert-Butylbenzene ND 250 73 ug/l
56-23-5 Carbon Tetrachloride ND 250 77 ug/l
108-90-7 Chlorobenzene ND 250 79 ug/l
75-00-3 Chloroethane ND 250 100 ug/l
67-66-3 Chloroform ND 250 86 ug/l
95-49-8 o-Chlorotoluene ND 250 76 ug/l
106-43-4 p-Chlorotoluene ND 250 69 ug/l
124-48-1 Dibromochloromethane ND 250 62 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 99 ug/l
106-93-4 1,2-Dibromoethane ND 250 71 ug/l
75-71-8 Dichlorodifluoromethane ND 250 65 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 65 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 70 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 76 ug/l
75-34-3 1,1-Dichloroethane ND 250 91 ug/l
107-06-2 1,2-Dichloroethane ND 250 82 ug/l
75-35-4 1,1-Dichloroethylene ND 250 85 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 90 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 85 ug/l
78-87-5 1,2-Dichloropropane ND 250 87 ug/l
142-28-9 1,3-Dichloropropane ND 250 73 ug/l
594-20-7 2,2-Dichloropropane ND 250 61 ug/l
563-58-6 1,1-Dichloropropene ND 250 79 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 66 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 35
FA25800 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1M
Lab Sample ID:FA25800-1 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 250 80 ug/l
100-41-4 Ethylbenzene 3150 250 76 ug/l
87-68-3 Hexachlorobutadiene ND 250 61 ug/l
98-82-8 Isopropylbenzene 140 250 59 ug/l J
99-87-6 p-Isopropyltoluene ND 250 61 ug/l
74-83-9 Methyl Bromide ND 250 91 ug/l
74-87-3 Methyl Chloride ND 250 79 ug/l
74-95-3 Methylene Bromide ND 250 85 ug/l
75-09-2 Methylene Chloride ND 1000 500 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 250 82 ug/l
91-20-3 Naphthalene 1100 250 61 ug/l
103-65-1 n-Propylbenzene 427 250 78 ug/l
100-42-5 Styrene 197 250 60 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 71 ug/l
127-18-4 Tetrachloroethylene ND 250 74 ug/l
108-88-3 Toluene 17100 250 83 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 65 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 81 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 70 ug/l
79-01-6 Trichloroethylene ND 250 73 ug/l
75-69-4 Trichlorofluoromethane ND 250 81 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 64 ug/l
95-63-6 1,2,4-Trimethylbenzene 4270 250 68 ug/l
108-67-8 1,3,5-Trimethylbenzene 1040 250 68 ug/l
75-01-4 Vinyl Chloride ND 250 65 ug/l
m,p-Xylene 13600 500 150 ug/l
95-47-6 o-Xylene 6690 250 67 ug/l
1330-20-7 Xylene (total)20300 750 220 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 35
FA25800 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2M
Lab Sample ID:FA25800-2 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039749.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 2.5 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene 0.92 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 35
FA25800 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2M
Lab Sample ID:FA25800-2 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.50 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.34 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 35
FA25800 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3M
Lab Sample ID:FA25800-3 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039724.D 200 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 220 100 34 ug/l
108-86-1 Bromobenzene ND 100 32 ug/l
74-97-5 Bromochloromethane ND 100 32 ug/l
75-27-4 Bromodichloromethane ND 100 29 ug/l
75-25-2 Bromoform ND 100 22 ug/l
104-51-8 n-Butylbenzene ND 100 29 ug/l
135-98-8 sec-Butylbenzene ND 100 28 ug/l
98-06-6 tert-Butylbenzene ND 100 29 ug/l
56-23-5 Carbon Tetrachloride ND 100 31 ug/l
108-90-7 Chlorobenzene ND 100 32 ug/l
75-00-3 Chloroethane ND 100 41 ug/l
67-66-3 Chloroform ND 100 34 ug/l
95-49-8 o-Chlorotoluene ND 100 30 ug/l
106-43-4 p-Chlorotoluene ND 100 27 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 39 ug/l
106-93-4 1,2-Dibromoethane ND 100 28 ug/l
75-71-8 Dichlorodifluoromethane ND 100 26 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 26 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 28 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 30 ug/l
75-34-3 1,1-Dichloroethane ND 100 36 ug/l
107-06-2 1,2-Dichloroethane ND 100 33 ug/l
75-35-4 1,1-Dichloroethylene ND 100 34 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 36 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 34 ug/l
78-87-5 1,2-Dichloropropane ND 100 35 ug/l
142-28-9 1,3-Dichloropropane ND 100 29 ug/l
594-20-7 2,2-Dichloropropane ND 100 24 ug/l
563-58-6 1,1-Dichloropropene ND 100 32 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 26 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 35
FA25800 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3M
Lab Sample ID:FA25800-3 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 100 32 ug/l
100-41-4 Ethylbenzene 564 100 30 ug/l
87-68-3 Hexachlorobutadiene ND 100 24 ug/l
98-82-8 Isopropylbenzene 25.9 100 24 ug/l J
99-87-6 p-Isopropyltoluene ND 100 24 ug/l
74-83-9 Methyl Bromide ND 100 36 ug/l
74-87-3 Methyl Chloride ND 100 32 ug/l
74-95-3 Methylene Bromide ND 100 34 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 100 33 ug/l
91-20-3 Naphthalene 98.1 100 24 ug/l J
103-65-1 n-Propylbenzene 65.3 100 31 ug/l J
100-42-5 Styrene 37.1 100 24 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 28 ug/l
127-18-4 Tetrachloroethylene ND 100 30 ug/l
108-88-3 Toluene 4690 100 33 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 27 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 26 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 32 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 28 ug/l
79-01-6 Trichloroethylene ND 100 29 ug/l
75-69-4 Trichlorofluoromethane ND 100 32 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 503 100 27 ug/l
108-67-8 1,3,5-Trimethylbenzene 134 100 27 ug/l
75-01-4 Vinyl Chloride ND 100 26 ug/l
m,p-Xylene 1760 200 59 ug/l
95-47-6 o-Xylene 896 100 27 ug/l
1330-20-7 Xylene (total)2660 300 86 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 35
FA25800 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-22
Lab Sample ID:FA25800-4 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039751.D 5 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 12.6 2.5 0.86 ug/l
108-86-1 Bromobenzene ND 2.5 0.80 ug/l
74-97-5 Bromochloromethane ND 2.5 0.80 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.74 ug/l
75-25-2 Bromoform ND 2.5 0.55 ug/l
104-51-8 n-Butylbenzene 7.1 2.5 0.72 ug/l
135-98-8 sec-Butylbenzene 4.9 2.5 0.69 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.73 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.77 ug/l
108-90-7 Chlorobenzene ND 2.5 0.79 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.86 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.76 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.69 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.62 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 0.99 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.71 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 0.65 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.65 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.70 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.76 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.91 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.82 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.85 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.90 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.85 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.87 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.73 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.61 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.79 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.66 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 35
FA25800 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-22
Lab Sample ID:FA25800-4 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 2.5 0.80 ug/l
100-41-4 Ethylbenzene 97.2 2.5 0.76 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.61 ug/l
98-82-8 Isopropylbenzene 13.1 2.5 0.59 ug/l
99-87-6 p-Isopropyltoluene 3.7 2.5 0.61 ug/l
74-83-9 Methyl Bromide ND 2.5 0.91 ug/l
74-87-3 Methyl Chloride ND 2.5 0.79 ug/l
74-95-3 Methylene Bromide ND 2.5 0.85 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 2.5 0.82 ug/l
91-20-3 Naphthalene 20.3 2.5 0.61 ug/l
103-65-1 n-Propylbenzene 46.3 2.5 0.78 ug/l
100-42-5 Styrene 1.3 2.5 0.60 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.71 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.74 ug/l
108-88-3 Toluene 17.4 2.5 0.83 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.65 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.81 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.70 ug/l
79-01-6 Trichloroethylene ND 2.5 0.73 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 0.81 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.64 ug/l
95-63-6 1,2,4-Trimethylbenzene 211 2.5 0.68 ug/l
108-67-8 1,3,5-Trimethylbenzene 60.0 2.5 0.68 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.65 ug/l
m,p-Xylene 281 5.0 1.5 ug/l
95-47-6 o-Xylene 97.9 2.5 0.67 ug/l
1330-20-7 Xylene (total)379 7.5 2.2 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 35
FA25800 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TW-1M
Lab Sample ID:FA25800-5 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a E039726.D 20 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 10 3.4 ug/l
108-86-1 Bromobenzene ND 10 3.2 ug/l
74-97-5 Bromochloromethane ND 10 3.2 ug/l
75-27-4 Bromodichloromethane ND 10 2.9 ug/l
75-25-2 Bromoform ND 10 2.2 ug/l
104-51-8 n-Butylbenzene ND 10 2.9 ug/l
135-98-8 sec-Butylbenzene ND 10 2.8 ug/l
98-06-6 tert-Butylbenzene ND 10 2.9 ug/l
56-23-5 Carbon Tetrachloride ND 10 3.1 ug/l
108-90-7 Chlorobenzene ND 10 3.2 ug/l
75-00-3 Chloroethane ND 10 4.1 ug/l
67-66-3 Chloroform ND 10 3.4 ug/l
95-49-8 o-Chlorotoluene ND 10 3.0 ug/l
106-43-4 p-Chlorotoluene ND 10 2.7 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 3.9 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.8 ug/l
75-71-8 Dichlorodifluoromethane ND 10 2.6 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.6 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.8 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 3.0 ug/l
75-34-3 1,1-Dichloroethane ND 10 3.6 ug/l
107-06-2 1,2-Dichloroethane ND 10 3.3 ug/l
75-35-4 1,1-Dichloroethylene ND 10 3.4 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 3.6 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 3.4 ug/l
78-87-5 1,2-Dichloropropane ND 10 3.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.9 ug/l
594-20-7 2,2-Dichloropropane ND 10 2.4 ug/l
563-58-6 1,1-Dichloropropene ND 10 3.2 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.6 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 35
FA25800 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TW-1M
Lab Sample ID:FA25800-5 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 10 3.2 ug/l
100-41-4 Ethylbenzene ND 10 3.0 ug/l
87-68-3 Hexachlorobutadiene ND 10 2.4 ug/l
98-82-8 Isopropylbenzene ND 10 2.4 ug/l
99-87-6 p-Isopropyltoluene ND 10 2.4 ug/l
74-83-9 Methyl Bromide ND 10 3.6 ug/l
74-87-3 Methyl Chloride ND 10 3.2 ug/l
74-95-3 Methylene Bromide ND 10 3.4 ug/l
75-09-2 Methylene Chloride ND 40 20 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 3.3 ug/l
91-20-3 Naphthalene ND 10 2.4 ug/l
103-65-1 n-Propylbenzene ND 10 3.1 ug/l
100-42-5 Styrene ND 10 2.4 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.8 ug/l
127-18-4 Tetrachloroethylene ND 10 3.0 ug/l
108-88-3 Toluene 570 10 3.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 2.7 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.6 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 3.2 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.8 ug/l
79-01-6 Trichloroethylene ND 10 2.9 ug/l
75-69-4 Trichlorofluoromethane ND 10 3.2 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 10 2.7 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 10 2.7 ug/l
75-01-4 Vinyl Chloride ND 10 2.6 ug/l
m,p-Xylene ND 20 5.9 ug/l
95-47-6 o-Xylene ND 10 2.7 ug/l
1330-20-7 Xylene (total)ND 30 8.6 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) xNot used, dilution required
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 35
FA25800 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA25800-6 Date Sampled:07/06/15
Matrix:AQ - Trip Blank Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039719.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 35
FA25800 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA25800-6 Date Sampled:07/06/15
Matrix:AQ - Trip Blank Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.23 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 35
FA25800 33.6
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
19 of 35
FA25800 4
FA25800: Chain of Custody
Page 1 of 3
20 of 35
FA25800 44.1
FA25800: Chain of Custody
Page 2 of 3
21 of 35
FA25800 44.1
FA25800: Chain of Custody
Page 3 of 3
22 of 35
FA25800 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
23 of 35
FA25800 5
Method Blank Summary Page 1 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-MB E039718.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-1, FA25800-3, FA25800-5, FA25800-6
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
24 of 35
FA25800 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-MB E039718.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-1, FA25800-3, FA25800-5, FA25800-6
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride 1.0 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
25 of 35
FA25800 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-MB E039748.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-2, FA25800-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
26 of 35
FA25800 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-MB E039748.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-2, FA25800-4
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
27 of 35
FA25800 55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-BS E039716.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-1, FA25800-3, FA25800-5, FA25800-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.3 93 70-130
108-86-1 Bromobenzene 10 9.2 92 70-130
74-97-5 Bromochloromethane 10 8.6 86 70-130
75-27-4 Bromodichloromethane 10 9.6 96 70-130
75-25-2 Bromoform 10 9.1 91 70-130
104-51-8 n-Butylbenzene 10 9.8 98 70-130
135-98-8 sec-Butylbenzene 10 9.9 99 70-130
98-06-6 tert-Butylbenzene 10 9.7 97 70-130
56-23-5 Carbon Tetrachloride 10 9.7 97 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 9.1 91 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 9.4 94 70-130
124-48-1 Dibromochloromethane 10 9.4 94 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.3 83 70-130
106-93-4 1,2-Dibromoethane 10 8.9 89 70-130
75-71-8 Dichlorodifluoromethane 10 8.8 88 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.6 96 70-130
106-46-7 1,4-Dichlorobenzene 10 9.2 92 70-130
75-34-3 1,1-Dichloroethane 10 9.5 95 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 9.7 97 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.8 88 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 8.8 88 70-130
594-20-7 2,2-Dichloropropane 10 9.8 98 70-130
563-58-6 1,1-Dichloropropene 10 9.7 97 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.4 104 70-130
108-20-3 Di-Isopropyl Ether 10 8.9 89 70-130
100-41-4 Ethylbenzene 10 9.5 95 70-130
87-68-3 Hexachlorobutadiene 10 9.5 95 70-130
98-82-8 Isopropylbenzene 10 9.9 99 70-130
* = Outside of Control Limits.
28 of 35
FA25800 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-BS E039716.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-1, FA25800-3, FA25800-5, FA25800-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.7 97 70-130
74-83-9 Methyl Bromide 10 10 100 60-140
74-87-3 Methyl Chloride 10 8.7 87 60-140
74-95-3 Methylene Bromide 10 9.3 93 70-130
75-09-2 Methylene Chloride 10 9.9 99 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.9 89 70-130
91-20-3 Naphthalene 10 9.5 95 70-130
103-65-1 n-Propylbenzene 10 9.9 99 70-130
100-42-5 Styrene 10 9.4 94 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.6 96 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.7 87 70-130
127-18-4 Tetrachloroethylene 10 9.6 96 70-130
108-88-3 Toluene 10 9.2 92 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.4 94 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.3 93 70-130
71-55-6 1,1,1-Trichloroethane 10 9.7 97 70-130
79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130
79-01-6 Trichloroethylene 10 9.3 93 70-130
75-69-4 Trichlorofluoromethane 10 10.5 105 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.5 95 70-130
75-01-4 Vinyl Chloride 10 10.2 102 60-140
m,p-Xylene 20 19.5 98 70-130
95-47-6 o-Xylene 10 9.5 95 70-130
1330-20-7 Xylene (total)30 29.0 97 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
29 of 35
FA25800 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-BS E039746.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-2, FA25800-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.1 111 70-130
108-86-1 Bromobenzene 10 11.1 111 70-130
74-97-5 Bromochloromethane 10 10.4 104 70-130
75-27-4 Bromodichloromethane 10 11.7 117 70-130
75-25-2 Bromoform 10 11.1 111 70-130
104-51-8 n-Butylbenzene 10 11.7 117 70-130
135-98-8 sec-Butylbenzene 10 11.8 118 70-130
98-06-6 tert-Butylbenzene 10 11.5 115 70-130
56-23-5 Carbon Tetrachloride 10 11.8 118 70-130
108-90-7 Chlorobenzene 10 11.3 113 70-130
75-00-3 Chloroethane 10 9.9 99 60-140
67-66-3 Chloroform 10 11.5 115 70-130
95-49-8 o-Chlorotoluene 10 11.5 115 70-130
106-43-4 p-Chlorotoluene 10 11.4 114 70-130
124-48-1 Dibromochloromethane 10 11.3 113 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.8 98 70-130
106-93-4 1,2-Dibromoethane 10 10.6 106 70-130
75-71-8 Dichlorodifluoromethane 10 10 100 60-140
95-50-1 1,2-Dichlorobenzene 10 11.3 113 70-130
541-73-1 1,3-Dichlorobenzene 10 11.6 116 70-130
106-46-7 1,4-Dichlorobenzene 10 11.2 112 70-130
75-34-3 1,1-Dichloroethane 10 11.6 116 70-130
107-06-2 1,2-Dichloroethane 10 11.0 110 70-130
75-35-4 1,1-Dichloroethylene 10 11.6 116 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.6 106 70-130
156-60-5 trans-1,2-Dichloroethylene 10 12.2 122 70-130
78-87-5 1,2-Dichloropropane 10 11.1 111 70-130
142-28-9 1,3-Dichloropropane 10 10.3 103 70-130
594-20-7 2,2-Dichloropropane 10 12.0 120 70-130
563-58-6 1,1-Dichloropropene 10 11.6 116 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.3 113 70-130
10061-02-6 trans-1,3-Dichloropropene 10 12.4 124 70-130
108-20-3 Di-Isopropyl Ether 10 10.5 105 70-130
100-41-4 Ethylbenzene 10 11.2 112 70-130
87-68-3 Hexachlorobutadiene 10 11.6 116 70-130
98-82-8 Isopropylbenzene 10 11.7 117 70-130
* = Outside of Control Limits.
30 of 35
FA25800 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-BS E039746.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-2, FA25800-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.6 116 70-130
74-83-9 Methyl Bromide 10 11.0 110 60-140
74-87-3 Methyl Chloride 10 9.9 99 60-140
74-95-3 Methylene Bromide 10 11.2 112 70-130
75-09-2 Methylene Chloride 10 10.8 108 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.5 105 70-130
91-20-3 Naphthalene 10 11.6 116 70-130
103-65-1 n-Propylbenzene 10 11.9 119 70-130
100-42-5 Styrene 10 11.4 114 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.3 113 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.3 103 70-130
127-18-4 Tetrachloroethylene 10 11.3 113 70-130
108-88-3 Toluene 10 10.9 109 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.3 113 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.2 112 70-130
71-55-6 1,1,1-Trichloroethane 10 11.7 117 70-130
79-00-5 1,1,2-Trichloroethane 10 10.8 108 70-130
79-01-6 Trichloroethylene 10 11.4 114 70-130
75-69-4 Trichlorofluoromethane 10 11.7 117 60-140
96-18-4 1,2,3-Trichloropropane 10 10.8 108 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.5 115 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.5 115 70-130
75-01-4 Vinyl Chloride 10 11.5 115 60-140
m,p-Xylene 20 22.9 115 70-130
95-47-6 o-Xylene 10 11.4 114 70-130
1330-20-7 Xylene (total)30 34.3 114 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
31 of 35
FA25800 55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25787-4MS E039729.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4MSD E039730.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4 E039721.D 5 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-1, FA25800-3, FA25800-5, FA25800-6
FA25787-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 182 50 231 98 50 231 98 0 70-130/20
108-86-1 Bromobenzene ND 50 57.3 115 50 57.6 115 1 70-130/20
74-97-5 Bromochloromethane ND 50 55.0 110 50 55.1 110 0 70-130/20
75-27-4 Bromodichloromethane ND 50 58.1 116 50 57.2 114 2 70-130/20
75-25-2 Bromoform ND 50 42.9 86 50 44.9 90 5 70-130/20
104-51-8 n-Butylbenzene ND 50 61.4 123 50 61.5 123 0 70-130/20
135-98-8 sec-Butylbenzene 0.83 J 50 62.5 123 50 63.0 124 1 70-130/20
98-06-6 tert-Butylbenzene ND 50 60.5 121 50 60.7 121 0 70-130/20
56-23-5 Carbon Tetrachloride ND 50 61.2 122 50 58.9 118 4 70-130/20
108-90-7 Chlorobenzene ND 50 58.9 118 50 59.2 118 1 70-130/20
75-00-3 Chloroethane ND 50 52.5 105 50 48.0 96 9 60-140/20
67-66-3 Chloroform ND 50 60.7 121 50 61.3 123 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 60.9 122 50 60.2 120 1 70-130/20
106-43-4 p-Chlorotoluene ND 50 60.1 120 50 59.4 119 1 70-130/20
124-48-1 Dibromochloromethane ND 50 49.3 99 50 51.4 103 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 53.1 106 50 54.6 109 3 70-130/20
106-93-4 1,2-Dibromoethane ND 50 56.6 113 50 58.0 116 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 55.3 111 50 53.6 107 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 58.7 117 50 58.6 117 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 60.5 121 50 59.6 119 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 58.2 116 50 58.3 117 0 70-130/20
75-34-3 1,1-Dichloroethane ND 50 61.0 122 50 61.5 123 1 70-130/20
107-06-2 1,2-Dichloroethane ND 50 58.3 117 50 60.4 121 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 62.0 124 50 62.1 124 0 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 55.1 110 50 55.9 112 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 64.7 129 50 64.6 129 0 70-130/20
78-87-5 1,2-Dichloropropane ND 50 59.7 119 50 59.6 119 0 70-130/20
142-28-9 1,3-Dichloropropane ND 50 55.3 111 50 56.2 112 2 70-130/20
594-20-7 2,2-Dichloropropane ND 50 61.7 123 50 59.4 119 4 70-130/20
563-58-6 1,1-Dichloropropene ND 50 61.3 123 50 61.1 122 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 59.2 118 50 57.5 115 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 63.2 126 50 62.8 126 1 70-130/20
108-20-3 Di-Isopropyl Ether 54.7 50 113 117 50 113 117 0 70-130/20
100-41-4 Ethylbenzene 39.0 50 95.8 114 50 95.9 114 0 70-130/20
87-68-3 Hexachlorobutadiene ND 50 56.4 113 50 59.8 120 6 70-130/20
98-82-8 Isopropylbenzene 5.3 50 67.1 124 50 67.2 124 0 70-130/20
* = Outside of Control Limits.
32 of 35
FA25800 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25787-4MS E039729.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4MSD E039730.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4 E039721.D 5 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-1, FA25800-3, FA25800-5, FA25800-6
FA25787-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 61.8 124 50 61.0 122 1 70-130/20
74-83-9 Methyl Bromide ND 50 58.9 118 50 57.0 114 3 60-140/20
74-87-3 Methyl Chloride ND 50 55.6 111 50 51.4 103 8 60-140/20
74-95-3 Methylene Bromide ND 50 59.9 120 50 61.0 122 2 70-130/20
75-09-2 Methylene Chloride ND 50 58.1 116 50 58.0 116 0 70-130/20
1634-04-4 Methyl Tert Butyl Ether 6.8 50 63.4 113 50 63.8 114 1 70-130/20
91-20-3 Naphthalene 14.6 50 76.9 125 50 83.8 138*9 70-130/20
103-65-1 n-Propylbenzene 8.5 50 70.7 124 50 69.8 123 1 70-130/20
100-42-5 Styrene ND 50 58.7 117 50 58.3 117 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 59.0 118 50 58.5 117 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 54.9 110 50 56.2 112 2 70-130/20
127-18-4 Tetrachloroethylene ND 50 59.2 118 50 59.2 118 0 70-130/20
108-88-3 Toluene 1.1 J 50 58.3 114 50 59.1 116 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 55.2 110 50 61.2 122 10 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 56.1 112 50 61.1 122 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 62.0 124 50 61.5 123 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 57.5 115 50 58.9 118 2 70-130/20
79-01-6 Trichloroethylene ND 50 59.1 118 50 58.9 118 0 70-130/20
75-69-4 Trichlorofluoromethane ND 50 62.8 126 50 60.4 121 4 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 56.3 113 50 58.1 116 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 25.2 50 88.1 126 50 87.2 124 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 3.5 50 64.2 121 50 63.5 120 1 70-130/20
75-01-4 Vinyl Chloride ND 50 60.1 120 50 58.9 118 2 60-140/20
m,p-Xylene 9.3 100 129 120 100 130 121 1 70-130/20
95-47-6 o-Xylene ND 50 60.1 120 50 60.7 121 1 70-130/20
1330-20-7 Xylene (total)9.3 150 189 120 150 190 120 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA25787-4 Limits
1868-53-7 Dibromofluoromethane 102%101%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%106%107%70-130%
2037-26-5 Toluene-D8 98%99%98%70-130%
460-00-4 4-Bromofluorobenzene 101%99%99%70-130%
* = Outside of Control Limits.
33 of 35
FA25800 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25800-4MS E039758.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4MSD E039759.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4 E039751.D 5 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-2, FA25800-4
FA25800-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 12.6 50 68.1 111 50 66.6 108 2 70-130/20
108-86-1 Bromobenzene ND 50 54.4 109 50 53.1 106 2 70-130/20
74-97-5 Bromochloromethane ND 50 52.7 105 50 52.4 105 1 70-130/20
75-27-4 Bromodichloromethane ND 50 54.9 110 50 53.9 108 2 70-130/20
75-25-2 Bromoform ND 50 42.0 84 50 45.1 90 7 70-130/20
104-51-8 n-Butylbenzene 7.1 50 65.4 117 50 64.7 115 1 70-130/20
135-98-8 sec-Butylbenzene 4.9 50 63.5 117 50 61.8 114 3 70-130/20
98-06-6 tert-Butylbenzene ND 50 58.5 117 50 56.1 112 4 70-130/20
56-23-5 Carbon Tetrachloride ND 50 58.7 117 50 55.8 112 5 70-130/20
108-90-7 Chlorobenzene ND 50 55.6 111 50 55.4 111 0 70-130/20
75-00-3 Chloroethane ND 50 46.6 93 50 43.5 87 7 60-140/20
67-66-3 Chloroform ND 50 58.5 117 50 57.9 116 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 63.8 128 50 62.1 124 3 70-130/20
106-43-4 p-Chlorotoluene ND 50 56.8 114 50 55.0 110 3 70-130/20
124-48-1 Dibromochloromethane ND 50 49.6 99 50 50.5 101 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 49.4 99 50 50.4 101 2 70-130/20
106-93-4 1,2-Dibromoethane ND 50 54.9 110 50 54.3 109 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 48.5 97 50 46.5 93 4 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 56.2 112 50 55.9 112 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 57.9 116 50 56.9 114 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 55.6 111 50 53.7 107 3 70-130/20
75-34-3 1,1-Dichloroethane ND 50 58.9 118 50 57.9 116 2 70-130/20
107-06-2 1,2-Dichloroethane ND 50 55.0 110 50 55.0 110 0 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 58.5 117 50 58.1 116 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 53.0 106 50 52.8 106 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 61.3 123 50 60.1 120 2 70-130/20
78-87-5 1,2-Dichloropropane ND 50 56.1 112 50 56.1 112 0 70-130/20
142-28-9 1,3-Dichloropropane ND 50 53.5 107 50 53.4 107 0 70-130/20
594-20-7 2,2-Dichloropropane ND 50 59.7 119 50 58.0 116 3 70-130/20
563-58-6 1,1-Dichloropropene ND 50 58.6 117 50 57.4 115 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 58.2 116 50 55.2 110 5 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 61.8 124 50 59.1 118 4 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 54.6 109 50 54.3 109 1 70-130/20
100-41-4 Ethylbenzene 97.2 50 147 100 50 145 96 1 70-130/20
87-68-3 Hexachlorobutadiene ND 50 54.2 108 50 58.7 117 8 70-130/20
98-82-8 Isopropylbenzene 13.1 50 72.4 119 50 71.6 117 1 70-130/20
* = Outside of Control Limits.
34 of 35
FA25800 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA25800
Account:GRINCC GRI (Geological Resources Inc.)
Project:Millers Country Store; 1706 US Hwy 17, Merry Hill, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25800-4MS E039758.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4MSD E039759.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4 E039751.D 5 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25800-2, FA25800-4
FA25800-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 3.7 50 62.6 118 50 61.2 115 2 70-130/20
74-83-9 Methyl Bromide ND 50 52.8 106 50 52.3 105 1 60-140/20
74-87-3 Methyl Chloride ND 50 47.2 94 50 47.6 95 1 60-140/20
74-95-3 Methylene Bromide ND 50 57.7 115 50 57.7 115 0 70-130/20
75-09-2 Methylene Chloride ND 50 63.2 126 50 62.8 126 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 53.7 107 50 55.2 110 3 70-130/20
91-20-3 Naphthalene 20.3 50 81.4 122 50 85.1 130 4 70-130/20
103-65-1 n-Propylbenzene 46.3 50 103 113 50 99.1 106 4 70-130/20
100-42-5 Styrene 1.3 J 50 59.1 116 50 57.9 113 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 57.8 116 50 55.9 112 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 52.3 105 50 51.6 103 1 70-130/20
127-18-4 Tetrachloroethylene ND 50 57.0 114 50 55.6 111 2 70-130/20
108-88-3 Toluene 17.4 50 71.3 108 50 70.2 106 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 55.9 112 50 59.4 119 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 57.1 114 50 58.0 116 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 58.8 118 50 58.0 116 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 56.3 113 50 55.8 112 1 70-130/20
79-01-6 Trichloroethylene ND 50 57.3 115 50 55.0 110 4 70-130/20
75-69-4 Trichlorofluoromethane ND 50 55.8 112 50 52.9 106 5 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 54.0 108 50 52.9 106 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 211 50 269 116 50 263 104 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 60.0 50 120 120 50 117 114 3 70-130/20
75-01-4 Vinyl Chloride ND 50 52.8 106 50 53.4 107 1 60-140/20
m,p-Xylene 281 100 384 103 100 377 96 2 70-130/20
95-47-6 o-Xylene 97.9 50 155 114 50 153 110 1 70-130/20
1330-20-7 Xylene (total)379 150 538 106 150 531 101 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA25800-4 Limits
1868-53-7 Dibromofluoromethane 102%102%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%106%105%70-130%
2037-26-5 Toluene-D8 99%99%97%70-130%
460-00-4 4-Bromofluorobenzene 101%99%99%70-130%
* = Outside of Control Limits.
35 of 35
FA25800 55.3.2
07/14/15
Technical Report for
GRI (Geological Resources Inc.)
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
2458/11963/13592
Accutest Job Number: FA25801
Sampling Date: 07/06/15
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: Nicole Long
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
07/14/15
e-Hardcopy 2.0
Automated Report
93
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 93
FA25801
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................6
Section 3: Sample Results ........................................................................................................12
3.1: FA25801-1: MW-2 ........................................................................................................13
3.2: FA25801-2: MW-3 ........................................................................................................15
3.3: FA25801-3: MW-4 ........................................................................................................17
3.4: FA25801-4: MW-5 ........................................................................................................19
3.5: FA25801-5: MW-7 ........................................................................................................21
3.6: FA25801-6: MW-9A .....................................................................................................23
3.7: FA25801-7: MW-10A ...................................................................................................25
3.8: FA25801-8: MW-11 ......................................................................................................27
3.9: FA25801-9: MW-14 ......................................................................................................29
3.10: FA25801-10: MW-17 ..................................................................................................31
3.11: FA25801-11: MW-20 ..................................................................................................33
3.12: FA25801-12: MW-23A ...............................................................................................35
3.13: FA25801-13: MW-25B ...............................................................................................37
3.14: FA25801-14: MW-26 ..................................................................................................39
3.15: FA25801-15: MW-29 ..................................................................................................41
3.16: FA25801-16: MW-31 ..................................................................................................43
3.17: FA25801-17: MW-34 ..................................................................................................45
3.18: FA25801-18: MW-36 ..................................................................................................47
3.19: FA25801-19: MW-38 ..................................................................................................49
3.20: FA25801-20: MW-42 ..................................................................................................51
3.21: FA25801-21: MW-43 ..................................................................................................53
3.22: FA25801-22: MW-44 ..................................................................................................55
3.23: FA25801-23: MW-45 ..................................................................................................57
3.24: FA25801-24: MW-46 ..................................................................................................59
3.25: FA25801-25: MW-47 ..................................................................................................61
3.26: FA25801-26: MW-48 ..................................................................................................63
3.27: FA25801-27: WSW-13 ...............................................................................................65
3.28: FA25801-28: TRIP BLANK .......................................................................................67
Section 4: Misc. Forms ............................................................................................................69
4.1: Chain of Custody ...........................................................................................................70
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................75
5.1: Method Blank Summary ................................................................................................76
5.2: Blank Spike Summary ...................................................................................................82
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................88 123452 of 93
FA25801
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA25801
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Project No: 2458/11963/13592
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA25801-1 07/06/15 12:22 HM 07/07/15 AQ Ground Water MW-2
FA25801-2 07/06/15 12:36 HM 07/07/15 AQ Ground Water MW-3
FA25801-3 07/06/15 12:40 HM 07/07/15 AQ Ground Water MW-4
FA25801-4 07/06/15 12:35 HM 07/07/15 AQ Ground Water MW-5
FA25801-5 07/06/15 12:29 HM 07/07/15 AQ Ground Water MW-7
FA25801-6 07/06/15 12:17 HM 07/07/15 AQ Ground Water MW-9A
FA25801-7 07/06/15 12:15 HM 07/07/15 AQ Ground Water MW-10A
FA25801-8 07/06/15 10:17 HM 07/07/15 AQ Ground Water MW-11
FA25801-9 07/06/15 12:24 HM 07/07/15 AQ Ground Water MW-14
FA25801-10 07/06/15 10:27 HM 07/07/15 AQ Ground Water MW-17
FA25801-11 07/06/15 10:25 HM 07/07/15 AQ Ground Water MW-20
FA25801-12 07/06/15 13:57 HM 07/07/15 AQ Ground Water MW-23A
FA25801-13 07/06/15 09:55 HM 07/07/15 AQ Ground Water MW-25B
3 of 93
FA25801 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA25801
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Project No: 2458/11963/13592
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA25801-14 07/06/15 09:46 HM 07/07/15 AQ Ground Water MW-26
FA25801-15 07/06/15 09:39 HM 07/07/15 AQ Ground Water MW-29
FA25801-16 07/06/15 09:44 HM 07/07/15 AQ Ground Water MW-31
FA25801-17 07/06/15 08:44 HM 07/07/15 AQ Ground Water MW-34
FA25801-18 07/06/15 09:10 HM 07/07/15 AQ Ground Water MW-36
FA25801-19 07/06/15 09:18 HM 07/07/15 AQ Ground Water MW-38
FA25801-20 07/06/15 10:42 HM 07/07/15 AQ Ground Water MW-42
FA25801-21 07/06/15 09:53 HM 07/07/15 AQ Ground Water MW-43
FA25801-22 07/06/15 09:34 HM 07/07/15 AQ Ground Water MW-44
FA25801-23 07/06/15 09:30 HM 07/07/15 AQ Ground Water MW-45
FA25801-24 07/06/15 08:39 HM 07/07/15 AQ Ground Water MW-46
FA25801-25 07/06/15 08:57 HM 07/07/15 AQ Ground Water MW-47
FA25801-26 07/06/15 09:25 HM 07/07/15 AQ Ground Water MW-48
4 of 93
FA25801 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA25801
Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Project No: 2458/11963/13592
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA25801-27 07/06/15 09:23 HM 07/07/15 AQ Water WSW-13
FA25801-28 07/06/15 00:00 HM 07/07/15 AQ Trip Blank Water TRIP BLANK
5 of 93
FA25801 1
Summary of Hits Page 1 of 6
Job Number:FA25801
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA25801-1 MW-2
Benzene 2290 130 43 ug/l SM 6200B
Ethylbenzene 1420 130 38 ug/l SM 6200B
Isopropylbenzene 42.6 J 130 30 ug/l SM 6200B
Methyl Tert Butyl Ether 4540 130 41 ug/l SM 6200B
Naphthalene 248 130 31 ug/l SM 6200B
n-Propylbenzene 98.2 J 130 39 ug/l SM 6200B
Toluene 11100 250 83 ug/l SM 6200B
1,2,4-Trimethylbenzene 900 130 34 ug/l SM 6200B
1,3,5-Trimethylbenzene 208 130 34 ug/l SM 6200B
m,p-Xylene 5070 250 74 ug/l SM 6200B
o-Xylene 2860 130 33 ug/l SM 6200B
Xylene (total)7930 380 110 ug/l SM 6200B
FA25801-2 MW-3
Benzene 2.9 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 0.35 J 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.59 0.50 0.14 ug/l SM 6200B
Isopropylbenzene 0.79 0.50 0.12 ug/l SM 6200B
Naphthalene 0.98 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 0.63 0.50 0.16 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.7 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.16 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 0.39 J 1.0 0.30 ug/l SM 6200B
o-Xylene 0.23 J 0.50 0.13 ug/l SM 6200B
Xylene (total)0.62 J 1.5 0.43 ug/l SM 6200B
FA25801-3 MW-4
Benzene 381 130 43 ug/l SM 6200B
n-Butylbenzene 98.9 J 130 36 ug/l SM 6200B
sec-Butylbenzene 59.1 J 130 35 ug/l SM 6200B
Ethylbenzene 4810 130 38 ug/l SM 6200B
Isopropylbenzene 264 130 30 ug/l SM 6200B
p-Isopropyltoluene 34.7 J 130 31 ug/l SM 6200B
Methyl Tert Butyl Ether 620 130 41 ug/l SM 6200B
Naphthalene 1440 130 31 ug/l SM 6200B
n-Propylbenzene 763 130 39 ug/l SM 6200B
Styrene 57.3 J 130 30 ug/l SM 6200B
Toluene 14200 250 83 ug/l SM 6200B
1,2,4-Trimethylbenzene 7110 130 34 ug/l SM 6200B
1,3,5-Trimethylbenzene 1890 130 34 ug/l SM 6200B
m,p-Xylene 18800 250 74 ug/l SM 6200B
6 of 93
FA25801 2
Summary of Hits Page 2 of 6
Job Number:FA25801
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
o-Xylene 9740 130 33 ug/l SM 6200B
Xylene (total)28600 380 110 ug/l SM 6200B
FA25801-4 MW-5
Benzene 5.3 0.50 0.17 ug/l SM 6200B
1,2-Dichloroethane 0.25 J 0.50 0.16 ug/l SM 6200B
Ethylbenzene 9.2 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.55 0.50 0.12 ug/l SM 6200B
Naphthalene 2.0 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 0.86 0.50 0.16 ug/l SM 6200B
Toluene 40.7 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 3.4 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 1.3 0.50 0.14 ug/l SM 6200B
m,p-Xylene 27.5 1.0 0.30 ug/l SM 6200B
o-Xylene 10.9 0.50 0.13 ug/l SM 6200B
Xylene (total)38.4 1.5 0.43 ug/l SM 6200B
FA25801-5 MW-7
No hits reported in this sample.
FA25801-6 MW-9A
Methyl Chloride 0.17 J 0.50 0.16 ug/l SM 6200B
FA25801-7 MW-10A
No hits reported in this sample.
FA25801-8 MW-11
Benzene 33.8 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 0.28 J 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 0.25 J 0.50 0.14 ug/l SM 6200B
Chloroethane 0.31 J 0.50 0.21 ug/l SM 6200B
1,2-Dichloroethane 0.42 J 0.50 0.16 ug/l SM 6200B
1,2-Dichloropropane 0.26 J 0.50 0.17 ug/l SM 6200B
Ethylbenzene 6.5 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 1.7 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 0.55 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.34 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 7.6 0.50 0.16 ug/l SM 6200B
Naphthalene 16.0 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 2.2 0.50 0.16 ug/l SM 6200B
7 of 93
FA25801 2
Summary of Hits Page 3 of 6
Job Number:FA25801
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Toluene 0.38 J 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 4.4 0.50 0.14 ug/l SM 6200B
m,p-Xylene 12.2 1.0 0.30 ug/l SM 6200B
o-Xylene 0.61 0.50 0.13 ug/l SM 6200B
Xylene (total)12.8 1.5 0.43 ug/l SM 6200B
FA25801-9 MW-14
Benzene 0.89 0.50 0.17 ug/l SM 6200B
Ethylbenzene 2.3 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.24 J 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.19 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 0.20 J 0.50 0.16 ug/l SM 6200B
Naphthalene 1.5 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 0.29 J 0.50 0.16 ug/l SM 6200B
Toluene 0.34 J 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.51 0.50 0.14 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.16 J 0.50 0.14 ug/l SM 6200B
m,p-Xylene 1.7 1.0 0.30 ug/l SM 6200B
o-Xylene 0.38 J 0.50 0.13 ug/l SM 6200B
Xylene (total)2.1 1.5 0.43 ug/l SM 6200B
FA25801-10 MW-17
No hits reported in this sample.
FA25801-11 MW-20
No hits reported in this sample.
FA25801-12 MW-23A
Benzene 22.0 0.50 0.17 ug/l SM 6200B
n-Butylbenzene 0.14 J 0.50 0.14 ug/l SM 6200B
sec-Butylbenzene 1.4 0.50 0.14 ug/l SM 6200B
tert-Butylbenzene 0.45 J 0.50 0.15 ug/l SM 6200B
1,2-Dichloroethane 0.19 J 0.50 0.16 ug/l SM 6200B
Ethylbenzene 11.7 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 4.7 0.50 0.12 ug/l SM 6200B
p-Isopropyltoluene 2.6 0.50 0.12 ug/l SM 6200B
Methyl Chloride 0.22 J 0.50 0.16 ug/l SM 6200B
Naphthalene 12.7 0.50 0.12 ug/l SM 6200B
n-Propylbenzene 5.0 0.50 0.16 ug/l SM 6200B
Toluene 0.47 J 0.50 0.17 ug/l SM 6200B
1,2,4-Trimethylbenzene 36.5 0.50 0.14 ug/l SM 6200B
8 of 93
FA25801 2
Summary of Hits Page 4 of 6
Job Number:FA25801
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1,3,5-Trimethylbenzene 1.0 0.50 0.14 ug/l SM 6200B
m,p-Xylene 19.3 1.0 0.30 ug/l SM 6200B
o-Xylene 0.46 J 0.50 0.13 ug/l SM 6200B
Xylene (total)19.8 1.5 0.43 ug/l SM 6200B
FA25801-13 MW-25B
No hits reported in this sample.
FA25801-14 MW-26
Benzene 2.4 0.50 0.17 ug/l SM 6200B
Chloroethane 0.34 J 0.50 0.21 ug/l SM 6200B
Ethylbenzene 0.22 J 0.50 0.15 ug/l SM 6200B
Methyl Chloride 0.27 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 12.1 0.50 0.16 ug/l SM 6200B
FA25801-15 MW-29
Benzene 525 25 8.6 ug/l SM 6200B
Chlorobenzene 10.4 J 25 7.9 ug/l SM 6200B
Ethylbenzene 317 25 7.6 ug/l SM 6200B
Isopropylbenzene 21.4 J 25 5.9 ug/l SM 6200B
Methyl Tert Butyl Ether 157 25 8.2 ug/l SM 6200B
Naphthalene 90.1 25 6.1 ug/l SM 6200B
n-Propylbenzene 35.0 25 7.8 ug/l SM 6200B
Toluene 1780 25 8.3 ug/l SM 6200B
1,2,4-Trimethylbenzene 270 25 6.8 ug/l SM 6200B
1,3,5-Trimethylbenzene 65.7 25 6.8 ug/l SM 6200B
m,p-Xylene 821 50 15 ug/l SM 6200B
o-Xylene 471 25 6.7 ug/l SM 6200B
Xylene (total)1290 75 22 ug/l SM 6200B
FA25801-16 MW-31
Chloroform 0.18 J 0.50 0.17 ug/l SM 6200B
FA25801-17 MW-34
Benzene 3.9 0.50 0.17 ug/l SM 6200B
Ethylbenzene 0.17 J 0.50 0.15 ug/l SM 6200B
Isopropylbenzene 0.17 J 0.50 0.12 ug/l SM 6200B
Methyl Tert Butyl Ether 5.1 0.50 0.16 ug/l SM 6200B
Naphthalene 0.45 J 0.50 0.12 ug/l SM 6200B
9 of 93
FA25801 2
Summary of Hits Page 5 of 6
Job Number:FA25801
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA25801-18 MW-36
Methyl Chloride 0.25 J 0.50 0.16 ug/l SM 6200B
FA25801-19 MW-38
Methyl Chloride 0.24 J 0.50 0.16 ug/l SM 6200B
FA25801-20 MW-42
Methyl Chloride 0.17 J 0.50 0.16 ug/l SM 6200B
FA25801-21 MW-43
No hits reported in this sample.
FA25801-22 MW-44
Methyl Chloride 0.20 J 0.50 0.16 ug/l SM 6200B
FA25801-23 MW-45
Methyl Chloride 0.20 J 0.50 0.16 ug/l SM 6200B
FA25801-24 MW-46
Methyl Chloride 0.20 J 0.50 0.16 ug/l SM 6200B
FA25801-25 MW-47
Chloroform 4.7 0.50 0.17 ug/l SM 6200B
Methyl Chloride 0.25 J 0.50 0.16 ug/l SM 6200B
FA25801-26 MW-48
Chloroform 0.44 J 0.50 0.17 ug/l SM 6200B
Methyl Chloride 0.21 J 0.50 0.16 ug/l SM 6200B
Methyl Tert Butyl Ether 9.6 0.50 0.16 ug/l SM 6200B
FA25801-27 WSW-13
Methyl Chloride 0.22 J 0.50 0.16 ug/l SM 6200B
10 of 93
FA25801 2
Summary of Hits Page 6 of 6
Job Number:FA25801
Account:GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Collected:07/06/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA25801-28 TRIP BLANK
No hits reported in this sample.
11 of 93
FA25801 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
12 of 93
FA25801 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA25801-1 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039727.D 250 07/09/15 DP n/a n/a VE1320
Run #2 E039761.D 500 07/10/15 EG n/a n/a VE1321
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2290 130 43 ug/l
108-86-1 Bromobenzene ND 130 40 ug/l
74-97-5 Bromochloromethane ND 130 40 ug/l
75-27-4 Bromodichloromethane ND 130 37 ug/l
75-25-2 Bromoform ND 130 27 ug/l
104-51-8 n-Butylbenzene ND 130 36 ug/l
135-98-8 sec-Butylbenzene ND 130 35 ug/l
98-06-6 tert-Butylbenzene ND 130 36 ug/l
56-23-5 Carbon Tetrachloride ND 130 38 ug/l
108-90-7 Chlorobenzene ND 130 40 ug/l
75-00-3 Chloroethane ND 130 52 ug/l
67-66-3 Chloroform ND 130 43 ug/l
95-49-8 o-Chlorotoluene ND 130 38 ug/l
106-43-4 p-Chlorotoluene ND 130 34 ug/l
124-48-1 Dibromochloromethane ND 130 31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 130 49 ug/l
106-93-4 1,2-Dibromoethane ND 130 35 ug/l
75-71-8 Dichlorodifluoromethane ND 130 32 ug/l
95-50-1 1,2-Dichlorobenzene ND 130 32 ug/l
541-73-1 1,3-Dichlorobenzene ND 130 35 ug/l
106-46-7 1,4-Dichlorobenzene ND 130 38 ug/l
75-34-3 1,1-Dichloroethane ND 130 45 ug/l
107-06-2 1,2-Dichloroethane ND 130 41 ug/l
75-35-4 1,1-Dichloroethylene ND 130 43 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 130 45 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 130 42 ug/l
78-87-5 1,2-Dichloropropane ND 130 43 ug/l
142-28-9 1,3-Dichloropropane ND 130 37 ug/l
594-20-7 2,2-Dichloropropane ND 130 30 ug/l
563-58-6 1,1-Dichloropropene ND 130 40 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 130 33 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 130 32 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 93
FA25801 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA25801-1 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 130 40 ug/l
100-41-4 Ethylbenzene 1420 130 38 ug/l
87-68-3 Hexachlorobutadiene ND 130 31 ug/l
98-82-8 Isopropylbenzene 42.6 130 30 ug/l J
99-87-6 p-Isopropyltoluene ND 130 31 ug/l
74-83-9 Methyl Bromide ND 130 46 ug/l
74-87-3 Methyl Chloride ND 130 40 ug/l
74-95-3 Methylene Bromide ND 130 43 ug/l
75-09-2 Methylene Chloride ND 500 250 ug/l
1634-04-4 Methyl Tert Butyl Ether 4540 130 41 ug/l
91-20-3 Naphthalene 248 130 31 ug/l
103-65-1 n-Propylbenzene 98.2 130 39 ug/l J
100-42-5 Styrene ND 130 30 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 130 36 ug/l
127-18-4 Tetrachloroethylene ND 130 37 ug/l
108-88-3 Toluene 11100 a 250 83 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 130 34 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 130 33 ug/l
71-55-6 1,1,1-Trichloroethane ND 130 40 ug/l
79-00-5 1,1,2-Trichloroethane ND 130 35 ug/l
79-01-6 Trichloroethylene ND 130 37 ug/l
75-69-4 Trichlorofluoromethane ND 130 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 130 32 ug/l
95-63-6 1,2,4-Trimethylbenzene 900 130 34 ug/l
108-67-8 1,3,5-Trimethylbenzene 208 130 34 ug/l
75-01-4 Vinyl Chloride ND 130 33 ug/l
m,p-Xylene 5070 250 74 ug/l
95-47-6 o-Xylene 2860 130 33 ug/l
1330-20-7 Xylene (total)7930 380 110 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%102%70-130%
2037-26-5 Toluene-D8 99%99%70-130%
460-00-4 4-Bromofluorobenzene 100%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 93
FA25801 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA25801-2 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039728.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.9 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.35 0.50 0.14 ug/l J
135-98-8 sec-Butylbenzene 0.59 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 93
FA25801 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA25801-2 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.79 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 0.98 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 0.63 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.7 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.16 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.39 1.0 0.30 ug/l J
95-47-6 o-Xylene 0.23 0.50 0.13 ug/l J
1330-20-7 Xylene (total)0.62 1.5 0.43 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 93
FA25801 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA25801-3 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039733.D 250 07/09/15 DP n/a n/a VE1320
Run #2 E039762.D 500 07/10/15 EG n/a n/a VE1321
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 381 130 43 ug/l
108-86-1 Bromobenzene ND 130 40 ug/l
74-97-5 Bromochloromethane ND 130 40 ug/l
75-27-4 Bromodichloromethane ND 130 37 ug/l
75-25-2 Bromoform ND 130 27 ug/l
104-51-8 n-Butylbenzene 98.9 130 36 ug/l J
135-98-8 sec-Butylbenzene 59.1 130 35 ug/l J
98-06-6 tert-Butylbenzene ND 130 36 ug/l
56-23-5 Carbon Tetrachloride ND 130 38 ug/l
108-90-7 Chlorobenzene ND 130 40 ug/l
75-00-3 Chloroethane ND 130 52 ug/l
67-66-3 Chloroform ND 130 43 ug/l
95-49-8 o-Chlorotoluene ND 130 38 ug/l
106-43-4 p-Chlorotoluene ND 130 34 ug/l
124-48-1 Dibromochloromethane ND 130 31 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 130 49 ug/l
106-93-4 1,2-Dibromoethane ND 130 35 ug/l
75-71-8 Dichlorodifluoromethane ND 130 32 ug/l
95-50-1 1,2-Dichlorobenzene ND 130 32 ug/l
541-73-1 1,3-Dichlorobenzene ND 130 35 ug/l
106-46-7 1,4-Dichlorobenzene ND 130 38 ug/l
75-34-3 1,1-Dichloroethane ND 130 45 ug/l
107-06-2 1,2-Dichloroethane ND 130 41 ug/l
75-35-4 1,1-Dichloroethylene ND 130 43 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 130 45 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 130 42 ug/l
78-87-5 1,2-Dichloropropane ND 130 43 ug/l
142-28-9 1,3-Dichloropropane ND 130 37 ug/l
594-20-7 2,2-Dichloropropane ND 130 30 ug/l
563-58-6 1,1-Dichloropropene ND 130 40 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 130 33 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 130 32 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 93
FA25801 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA25801-3 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 130 40 ug/l
100-41-4 Ethylbenzene 4810 130 38 ug/l
87-68-3 Hexachlorobutadiene ND 130 31 ug/l
98-82-8 Isopropylbenzene 264 130 30 ug/l
99-87-6 p-Isopropyltoluene 34.7 130 31 ug/l J
74-83-9 Methyl Bromide ND 130 46 ug/l
74-87-3 Methyl Chloride ND 130 40 ug/l
74-95-3 Methylene Bromide ND 130 43 ug/l
75-09-2 Methylene Chloride ND 500 250 ug/l
1634-04-4 Methyl Tert Butyl Ether 620 130 41 ug/l
91-20-3 Naphthalene 1440 130 31 ug/l
103-65-1 n-Propylbenzene 763 130 39 ug/l
100-42-5 Styrene 57.3 130 30 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 130 31 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 130 36 ug/l
127-18-4 Tetrachloroethylene ND 130 37 ug/l
108-88-3 Toluene 14200 a 250 83 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 130 34 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 130 33 ug/l
71-55-6 1,1,1-Trichloroethane ND 130 40 ug/l
79-00-5 1,1,2-Trichloroethane ND 130 35 ug/l
79-01-6 Trichloroethylene ND 130 37 ug/l
75-69-4 Trichlorofluoromethane ND 130 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 130 32 ug/l
95-63-6 1,2,4-Trimethylbenzene 7110 130 34 ug/l
108-67-8 1,3,5-Trimethylbenzene 1890 130 34 ug/l
75-01-4 Vinyl Chloride ND 130 33 ug/l
m,p-Xylene 18800 250 74 ug/l
95-47-6 o-Xylene 9740 130 33 ug/l
1330-20-7 Xylene (total)28600 380 110 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%103%70-130%
2037-26-5 Toluene-D8 99%99%70-130%
460-00-4 4-Bromofluorobenzene 100%98%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 93
FA25801 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA25801-4 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039750.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 5.3 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 0.25 0.50 0.16 ug/l J
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 93
FA25801 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA25801-4 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 9.2 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.55 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 2.0 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 0.86 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 40.7 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 3.4 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.3 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 27.5 1.0 0.30 ug/l
95-47-6 o-Xylene 10.9 0.50 0.13 ug/l
1330-20-7 Xylene (total)38.4 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 93
FA25801 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA25801-5 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039735.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 93
FA25801 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA25801-5 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 93
FA25801 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9A
Lab Sample ID:FA25801-6 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039736.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 93
FA25801 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9A
Lab Sample ID:FA25801-6 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.17 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 93
FA25801 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10A
Lab Sample ID:FA25801-7 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039737.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 93
FA25801 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10A
Lab Sample ID:FA25801-7 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 93
FA25801 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA25801-8 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039738.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 33.8 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.28 0.50 0.14 ug/l J
135-98-8 sec-Butylbenzene 0.25 0.50 0.14 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane 0.31 0.50 0.21 ug/l J
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 0.42 0.50 0.16 ug/l J
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane 0.26 0.50 0.17 ug/l J
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 93
FA25801 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA25801-8 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 6.5 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 1.7 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 0.55 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.34 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 7.6 0.50 0.16 ug/l
91-20-3 Naphthalene 16.0 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 2.2 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.38 0.50 0.17 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 4.4 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 12.2 1.0 0.30 ug/l
95-47-6 o-Xylene 0.61 0.50 0.13 ug/l
1330-20-7 Xylene (total)12.8 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 93
FA25801 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA25801-9 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039739.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.89 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 93
FA25801 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA25801-9 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 2.3 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.24 0.50 0.12 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.19 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.20 0.50 0.16 ug/l J
91-20-3 Naphthalene 1.5 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 0.29 0.50 0.16 ug/l J
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.34 0.50 0.17 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.51 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.16 0.50 0.14 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.7 1.0 0.30 ug/l
95-47-6 o-Xylene 0.38 0.50 0.13 ug/l J
1330-20-7 Xylene (total)2.1 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 93
FA25801 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-17
Lab Sample ID:FA25801-10 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039740.D 1 07/09/15 DP n/a n/a VE1320
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 93
FA25801 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-17
Lab Sample ID:FA25801-10 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 93
FA25801 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-20
Lab Sample ID:FA25801-11 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039752.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 93
FA25801 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-20
Lab Sample ID:FA25801-11 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 93
FA25801 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-23A
Lab Sample ID:FA25801-12 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039753.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 22.0 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene 0.14 0.50 0.14 ug/l J
135-98-8 sec-Butylbenzene 1.4 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene 0.45 0.50 0.15 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane 0.19 0.50 0.16 ug/l J
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 93
FA25801 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-23A
Lab Sample ID:FA25801-12 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 11.7 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 4.7 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene 2.6 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.22 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene 12.7 0.50 0.12 ug/l
103-65-1 n-Propylbenzene 5.0 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene 0.47 0.50 0.17 ug/l J
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 36.5 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.0 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 19.3 1.0 0.30 ug/l
95-47-6 o-Xylene 0.46 0.50 0.13 ug/l J
1330-20-7 Xylene (total)19.8 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 93
FA25801 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-25B
Lab Sample ID:FA25801-13 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039754.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 93
FA25801 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-25B
Lab Sample ID:FA25801-13 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 93
FA25801 33.13
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-26
Lab Sample ID:FA25801-14 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039755.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.4 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane 0.34 0.50 0.21 ug/l J
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 93
FA25801 33.14
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-26
Lab Sample ID:FA25801-14 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 0.22 0.50 0.15 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.27 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 12.1 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 89%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 93
FA25801 33.14
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-29
Lab Sample ID:FA25801-15 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039756.D 50 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 525 25 8.6 ug/l
108-86-1 Bromobenzene ND 25 8.0 ug/l
74-97-5 Bromochloromethane ND 25 8.0 ug/l
75-27-4 Bromodichloromethane ND 25 7.4 ug/l
75-25-2 Bromoform ND 25 5.5 ug/l
104-51-8 n-Butylbenzene ND 25 7.2 ug/l
135-98-8 sec-Butylbenzene ND 25 6.9 ug/l
98-06-6 tert-Butylbenzene ND 25 7.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 7.7 ug/l
108-90-7 Chlorobenzene 10.4 25 7.9 ug/l J
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 8.6 ug/l
95-49-8 o-Chlorotoluene ND 25 7.6 ug/l
106-43-4 p-Chlorotoluene ND 25 6.9 ug/l
124-48-1 Dibromochloromethane ND 25 6.2 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 9.9 ug/l
106-93-4 1,2-Dibromoethane ND 25 7.1 ug/l
75-71-8 Dichlorodifluoromethane ND 25 6.5 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 7.0 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 7.6 ug/l
75-34-3 1,1-Dichloroethane ND 25 9.1 ug/l
107-06-2 1,2-Dichloroethane ND 25 8.2 ug/l
75-35-4 1,1-Dichloroethylene ND 25 8.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 9.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 8.5 ug/l
78-87-5 1,2-Dichloropropane ND 25 8.7 ug/l
142-28-9 1,3-Dichloropropane ND 25 7.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.1 ug/l
563-58-6 1,1-Dichloropropene ND 25 7.9 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.6 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 93
FA25801 33.15
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-29
Lab Sample ID:FA25801-15 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 25 8.0 ug/l
100-41-4 Ethylbenzene 317 25 7.6 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.1 ug/l
98-82-8 Isopropylbenzene 21.4 25 5.9 ug/l J
99-87-6 p-Isopropyltoluene ND 25 6.1 ug/l
74-83-9 Methyl Bromide ND 25 9.1 ug/l
74-87-3 Methyl Chloride ND 25 7.9 ug/l
74-95-3 Methylene Bromide ND 25 8.5 ug/l
75-09-2 Methylene Chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether 157 25 8.2 ug/l
91-20-3 Naphthalene 90.1 25 6.1 ug/l
103-65-1 n-Propylbenzene 35.0 25 7.8 ug/l
100-42-5 Styrene ND 25 6.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 7.1 ug/l
127-18-4 Tetrachloroethylene ND 25 7.4 ug/l
108-88-3 Toluene 1780 25 8.3 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 6.8 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 8.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 7.0 ug/l
79-01-6 Trichloroethylene ND 25 7.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 8.1 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 6.4 ug/l
95-63-6 1,2,4-Trimethylbenzene 270 25 6.8 ug/l
108-67-8 1,3,5-Trimethylbenzene 65.7 25 6.8 ug/l
75-01-4 Vinyl Chloride ND 25 6.5 ug/l
m,p-Xylene 821 50 15 ug/l
95-47-6 o-Xylene 471 25 6.7 ug/l
1330-20-7 Xylene (total)1290 75 22 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 93
FA25801 33.15
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-31
Lab Sample ID:FA25801-16 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039757.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform 0.18 0.50 0.17 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 93
FA25801 33.16
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-31
Lab Sample ID:FA25801-16 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 93
FA25801 33.16
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-34
Lab Sample ID:FA25801-17 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039763.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 3.9 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 93
FA25801 33.17
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-34
Lab Sample ID:FA25801-17 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene 0.17 0.50 0.15 ug/l J
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene 0.17 0.50 0.12 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 5.1 0.50 0.16 ug/l
91-20-3 Naphthalene 0.45 0.50 0.12 ug/l J
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 93
FA25801 33.17
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-36
Lab Sample ID:FA25801-18 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039764.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 93
FA25801 33.18
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-36
Lab Sample ID:FA25801-18 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.25 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 90%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 93
FA25801 33.18
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-38
Lab Sample ID:FA25801-19 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039765.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
49 of 93
FA25801 33.19
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-38
Lab Sample ID:FA25801-19 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.24 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 93
FA25801 33.19
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-42
Lab Sample ID:FA25801-20 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039766.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 93
FA25801 33.20
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-42
Lab Sample ID:FA25801-20 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.17 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 93
FA25801 33.20
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-43
Lab Sample ID:FA25801-21 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039767.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
53 of 93
FA25801 33.21
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-43
Lab Sample ID:FA25801-21 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 93
FA25801 33.21
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-44
Lab Sample ID:FA25801-22 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039768.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
55 of 93
FA25801 33.22
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-44
Lab Sample ID:FA25801-22 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.20 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
56 of 93
FA25801 33.22
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-45
Lab Sample ID:FA25801-23 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039769.D 1 07/10/15 EG n/a n/a VE1321
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
57 of 93
FA25801 33.23
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-45
Lab Sample ID:FA25801-23 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.20 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
58 of 93
FA25801 33.23
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-46
Lab Sample ID:FA25801-24 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039777.D 1 07/13/15 TD n/a n/a VE1322
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
59 of 93
FA25801 33.24
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-46
Lab Sample ID:FA25801-24 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.20 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
60 of 93
FA25801 33.24
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-47
Lab Sample ID:FA25801-25 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039778.D 1 07/13/15 TD n/a n/a VE1322
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform 4.7 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
61 of 93
FA25801 33.25
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-47
Lab Sample ID:FA25801-25 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.25 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
62 of 93
FA25801 33.25
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-48
Lab Sample ID:FA25801-26 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039779.D 1 07/13/15 TD n/a n/a VE1322
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform 0.44 0.50 0.17 ug/l J
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
63 of 93
FA25801 33.26
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-48
Lab Sample ID:FA25801-26 Date Sampled:07/06/15
Matrix:AQ - Ground Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.21 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 9.6 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
64 of 93
FA25801 33.26
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:WSW-13
Lab Sample ID:FA25801-27 Date Sampled:07/06/15
Matrix:AQ - Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039781.D 1 07/13/15 TD n/a n/a VE1322
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
65 of 93
FA25801 33.27
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:WSW-13
Lab Sample ID:FA25801-27 Date Sampled:07/06/15
Matrix:AQ - Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride 0.22 0.50 0.16 ug/l J
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
66 of 93
FA25801 33.27
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA25801-28 Date Sampled:07/06/15
Matrix:AQ - Trip Blank Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E039782.D 1 07/13/15 TD n/a n/a VE1322
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
67 of 93
FA25801 33.28
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TRIP BLANK
Lab Sample ID:FA25801-28 Date Sampled:07/06/15
Matrix:AQ - Trip Blank Water Date Received:07/07/15
Method:SM 6200B Percent Solids:n/a
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
68 of 93
FA25801 33.28
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
69 of 93
FA25801 4
FA25801: Chain of Custody
Page 1 of 5
70 of 93
FA25801 44.1
FA25801: Chain of Custody
Page 2 of 5
71 of 93
FA25801 44.1
FA25801: Chain of Custody
Page 3 of 5
72 of 93
FA25801 44.1
FA25801: Chain of Custody
Page 4 of 5
73 of 93
FA25801 44.1
FA25801: Chain of Custody
Page 5 of 5
74 of 93
FA25801 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
75 of 93
FA25801 5
Method Blank Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-MB E039718.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-2, FA25801-3, FA25801-5, FA25801-6, FA25801-7, FA25801-8, FA25801-9, FA25801-10
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
76 of 93
FA25801 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-MB E039718.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-2, FA25801-3, FA25801-5, FA25801-6, FA25801-7, FA25801-8, FA25801-9, FA25801-10
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride 1.0 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
77 of 93
FA25801 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-MB E039748.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-3, FA25801-4, FA25801-11, FA25801-12, FA25801-13, FA25801-14, FA25801-15, FA25801-16,
FA25801-17, FA25801-18, FA25801-19, FA25801-20, FA25801-21, FA25801-22, FA25801-23
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
78 of 93
FA25801 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-MB E039748.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-3, FA25801-4, FA25801-11, FA25801-12, FA25801-13, FA25801-14, FA25801-15, FA25801-16,
FA25801-17, FA25801-18, FA25801-19, FA25801-20, FA25801-21, FA25801-22, FA25801-23
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
79 of 93
FA25801 55.1.2
Method Blank Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1322-MB E039776.D 1 07/13/15 TD n/a n/a VE1322
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-24, FA25801-25, FA25801-26, FA25801-27, FA25801-28
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
80 of 93
FA25801 55.1.3
Method Blank Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1322-MB E039776.D 1 07/13/15 TD n/a n/a VE1322
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-24, FA25801-25, FA25801-26, FA25801-27, FA25801-28
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
81 of 93
FA25801 55.1.3
Blank Spike Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-BS E039716.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-2, FA25801-3, FA25801-5, FA25801-6, FA25801-7, FA25801-8, FA25801-9, FA25801-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.3 93 70-130
108-86-1 Bromobenzene 10 9.2 92 70-130
74-97-5 Bromochloromethane 10 8.6 86 70-130
75-27-4 Bromodichloromethane 10 9.6 96 70-130
75-25-2 Bromoform 10 9.1 91 70-130
104-51-8 n-Butylbenzene 10 9.8 98 70-130
135-98-8 sec-Butylbenzene 10 9.9 99 70-130
98-06-6 tert-Butylbenzene 10 9.7 97 70-130
56-23-5 Carbon Tetrachloride 10 9.7 97 70-130
108-90-7 Chlorobenzene 10 9.3 93 70-130
75-00-3 Chloroethane 10 9.1 91 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 9.7 97 70-130
106-43-4 p-Chlorotoluene 10 9.4 94 70-130
124-48-1 Dibromochloromethane 10 9.4 94 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.3 83 70-130
106-93-4 1,2-Dibromoethane 10 8.9 89 70-130
75-71-8 Dichlorodifluoromethane 10 8.8 88 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.6 96 70-130
106-46-7 1,4-Dichlorobenzene 10 9.2 92 70-130
75-34-3 1,1-Dichloroethane 10 9.5 95 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 9.7 97 70-130
156-59-2 cis-1,2-Dichloroethylene 10 8.8 88 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 9.3 93 70-130
142-28-9 1,3-Dichloropropane 10 8.8 88 70-130
594-20-7 2,2-Dichloropropane 10 9.8 98 70-130
563-58-6 1,1-Dichloropropene 10 9.7 97 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.4 104 70-130
108-20-3 Di-Isopropyl Ether 10 8.9 89 70-130
100-41-4 Ethylbenzene 10 9.5 95 70-130
87-68-3 Hexachlorobutadiene 10 9.5 95 70-130
98-82-8 Isopropylbenzene 10 9.9 99 70-130
* = Outside of Control Limits.
82 of 93
FA25801 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1320-BS E039716.D 1 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-2, FA25801-3, FA25801-5, FA25801-6, FA25801-7, FA25801-8, FA25801-9, FA25801-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.7 97 70-130
74-83-9 Methyl Bromide 10 10 100 60-140
74-87-3 Methyl Chloride 10 8.7 87 60-140
74-95-3 Methylene Bromide 10 9.3 93 70-130
75-09-2 Methylene Chloride 10 9.9 99 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.9 89 70-130
91-20-3 Naphthalene 10 9.5 95 70-130
103-65-1 n-Propylbenzene 10 9.9 99 70-130
100-42-5 Styrene 10 9.4 94 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.6 96 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.7 87 70-130
127-18-4 Tetrachloroethylene 10 9.6 96 70-130
108-88-3 Toluene 10 9.2 92 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.4 94 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.3 93 70-130
71-55-6 1,1,1-Trichloroethane 10 9.7 97 70-130
79-00-5 1,1,2-Trichloroethane 10 9.2 92 70-130
79-01-6 Trichloroethylene 10 9.3 93 70-130
75-69-4 Trichlorofluoromethane 10 10.5 105 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.6 96 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.5 95 70-130
75-01-4 Vinyl Chloride 10 10.2 102 60-140
m,p-Xylene 20 19.5 98 70-130
95-47-6 o-Xylene 10 9.5 95 70-130
1330-20-7 Xylene (total)30 29.0 97 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
83 of 93
FA25801 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-BS E039746.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-3, FA25801-4, FA25801-11, FA25801-12, FA25801-13, FA25801-14, FA25801-15, FA25801-16,
FA25801-17, FA25801-18, FA25801-19, FA25801-20, FA25801-21, FA25801-22, FA25801-23
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.1 111 70-130
108-86-1 Bromobenzene 10 11.1 111 70-130
74-97-5 Bromochloromethane 10 10.4 104 70-130
75-27-4 Bromodichloromethane 10 11.7 117 70-130
75-25-2 Bromoform 10 11.1 111 70-130
104-51-8 n-Butylbenzene 10 11.7 117 70-130
135-98-8 sec-Butylbenzene 10 11.8 118 70-130
98-06-6 tert-Butylbenzene 10 11.5 115 70-130
56-23-5 Carbon Tetrachloride 10 11.8 118 70-130
108-90-7 Chlorobenzene 10 11.3 113 70-130
75-00-3 Chloroethane 10 9.9 99 60-140
67-66-3 Chloroform 10 11.5 115 70-130
95-49-8 o-Chlorotoluene 10 11.5 115 70-130
106-43-4 p-Chlorotoluene 10 11.4 114 70-130
124-48-1 Dibromochloromethane 10 11.3 113 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.8 98 70-130
106-93-4 1,2-Dibromoethane 10 10.6 106 70-130
75-71-8 Dichlorodifluoromethane 10 10 100 60-140
95-50-1 1,2-Dichlorobenzene 10 11.3 113 70-130
541-73-1 1,3-Dichlorobenzene 10 11.6 116 70-130
106-46-7 1,4-Dichlorobenzene 10 11.2 112 70-130
75-34-3 1,1-Dichloroethane 10 11.6 116 70-130
107-06-2 1,2-Dichloroethane 10 11.0 110 70-130
75-35-4 1,1-Dichloroethylene 10 11.6 116 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.6 106 70-130
156-60-5 trans-1,2-Dichloroethylene 10 12.2 122 70-130
78-87-5 1,2-Dichloropropane 10 11.1 111 70-130
142-28-9 1,3-Dichloropropane 10 10.3 103 70-130
594-20-7 2,2-Dichloropropane 10 12.0 120 70-130
563-58-6 1,1-Dichloropropene 10 11.6 116 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.3 113 70-130
10061-02-6 trans-1,3-Dichloropropene 10 12.4 124 70-130
108-20-3 Di-Isopropyl Ether 10 10.5 105 70-130
100-41-4 Ethylbenzene 10 11.2 112 70-130
87-68-3 Hexachlorobutadiene 10 11.6 116 70-130
98-82-8 Isopropylbenzene 10 11.7 117 70-130
* = Outside of Control Limits.
84 of 93
FA25801 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1321-BS E039746.D 1 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-3, FA25801-4, FA25801-11, FA25801-12, FA25801-13, FA25801-14, FA25801-15, FA25801-16,
FA25801-17, FA25801-18, FA25801-19, FA25801-20, FA25801-21, FA25801-22, FA25801-23
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.6 116 70-130
74-83-9 Methyl Bromide 10 11.0 110 60-140
74-87-3 Methyl Chloride 10 9.9 99 60-140
74-95-3 Methylene Bromide 10 11.2 112 70-130
75-09-2 Methylene Chloride 10 10.8 108 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.5 105 70-130
91-20-3 Naphthalene 10 11.6 116 70-130
103-65-1 n-Propylbenzene 10 11.9 119 70-130
100-42-5 Styrene 10 11.4 114 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.3 113 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.3 103 70-130
127-18-4 Tetrachloroethylene 10 11.3 113 70-130
108-88-3 Toluene 10 10.9 109 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.3 113 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.2 112 70-130
71-55-6 1,1,1-Trichloroethane 10 11.7 117 70-130
79-00-5 1,1,2-Trichloroethane 10 10.8 108 70-130
79-01-6 Trichloroethylene 10 11.4 114 70-130
75-69-4 Trichlorofluoromethane 10 11.7 117 60-140
96-18-4 1,2,3-Trichloropropane 10 10.8 108 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.5 115 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.5 115 70-130
75-01-4 Vinyl Chloride 10 11.5 115 60-140
m,p-Xylene 20 22.9 115 70-130
95-47-6 o-Xylene 10 11.4 114 70-130
1330-20-7 Xylene (total)30 34.3 114 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
85 of 93
FA25801 55.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1322-BS E039774.D 1 07/13/15 TD n/a n/a VE1322
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-24, FA25801-25, FA25801-26, FA25801-27, FA25801-28
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.9 109 70-130
108-86-1 Bromobenzene 10 10.9 109 70-130
74-97-5 Bromochloromethane 10 10.5 105 70-130
75-27-4 Bromodichloromethane 10 11.8 118 70-130
75-25-2 Bromoform 10 11.5 115 70-130
104-51-8 n-Butylbenzene 10 11.5 115 70-130
135-98-8 sec-Butylbenzene 10 11.6 116 70-130
98-06-6 tert-Butylbenzene 10 11.3 113 70-130
56-23-5 Carbon Tetrachloride 10 11.9 119 70-130
108-90-7 Chlorobenzene 10 11.2 112 70-130
75-00-3 Chloroethane 10 11.3 113 60-140
67-66-3 Chloroform 10 11.4 114 70-130
95-49-8 o-Chlorotoluene 10 11.2 112 70-130
106-43-4 p-Chlorotoluene 10 11.2 112 70-130
124-48-1 Dibromochloromethane 10 11.7 117 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.9 99 70-130
106-93-4 1,2-Dibromoethane 10 10.9 109 70-130
75-71-8 Dichlorodifluoromethane 10 12.0 120 60-140
95-50-1 1,2-Dichlorobenzene 10 11.0 110 70-130
541-73-1 1,3-Dichlorobenzene 10 11.4 114 70-130
106-46-7 1,4-Dichlorobenzene 10 10.9 109 70-130
75-34-3 1,1-Dichloroethane 10 11.3 113 70-130
107-06-2 1,2-Dichloroethane 10 11.0 110 70-130
75-35-4 1,1-Dichloroethylene 10 11.3 113 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130
156-60-5 trans-1,2-Dichloroethylene 10 12.0 120 70-130
78-87-5 1,2-Dichloropropane 10 11.2 112 70-130
142-28-9 1,3-Dichloropropane 10 10.4 104 70-130
594-20-7 2,2-Dichloropropane 10 11.8 118 70-130
563-58-6 1,1-Dichloropropene 10 11.5 115 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.8 118 70-130
10061-02-6 trans-1,3-Dichloropropene 10 12.4 124 70-130
108-20-3 Di-Isopropyl Ether 10 10.4 104 70-130
100-41-4 Ethylbenzene 10 11.2 112 70-130
87-68-3 Hexachlorobutadiene 10 11.6 116 70-130
98-82-8 Isopropylbenzene 10 11.6 116 70-130
* = Outside of Control Limits.
86 of 93
FA25801 55.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE1322-BS E039774.D 1 07/13/15 TD n/a n/a VE1322
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-24, FA25801-25, FA25801-26, FA25801-27, FA25801-28
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.6 116 70-130
74-83-9 Methyl Bromide 10 12.2 122 60-140
74-87-3 Methyl Chloride 10 11.9 119 60-140
74-95-3 Methylene Bromide 10 11.3 113 70-130
75-09-2 Methylene Chloride 10 10.2 102 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.8 108 70-130
91-20-3 Naphthalene 10 11.6 116 70-130
103-65-1 n-Propylbenzene 10 11.6 116 70-130
100-42-5 Styrene 10 11.4 114 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.4 114 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 11.2 112 70-130
108-88-3 Toluene 10 10.8 108 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.3 113 70-130
120-82-1 1,2,4-Trichlorobenzene 10 11.2 112 70-130
71-55-6 1,1,1-Trichloroethane 10 11.7 117 70-130
79-00-5 1,1,2-Trichloroethane 10 10.7 107 70-130
79-01-6 Trichloroethylene 10 11.3 113 70-130
75-69-4 Trichlorofluoromethane 10 12.3 123 60-140
96-18-4 1,2,3-Trichloropropane 10 10.9 109 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.4 114 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.2 112 70-130
75-01-4 Vinyl Chloride 10 12.5 125 60-140
m,p-Xylene 20 22.7 114 70-130
95-47-6 o-Xylene 10 11.2 112 70-130
1330-20-7 Xylene (total)30 33.9 113 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
87 of 93
FA25801 55.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25787-4MS E039729.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4MSD E039730.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4 E039721.D 5 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-2, FA25801-3, FA25801-5, FA25801-6, FA25801-7, FA25801-8, FA25801-9, FA25801-10
FA25787-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 182 50 231 98 50 231 98 0 70-130/20
108-86-1 Bromobenzene ND 50 57.3 115 50 57.6 115 1 70-130/20
74-97-5 Bromochloromethane ND 50 55.0 110 50 55.1 110 0 70-130/20
75-27-4 Bromodichloromethane ND 50 58.1 116 50 57.2 114 2 70-130/20
75-25-2 Bromoform ND 50 42.9 86 50 44.9 90 5 70-130/20
104-51-8 n-Butylbenzene ND 50 61.4 123 50 61.5 123 0 70-130/20
135-98-8 sec-Butylbenzene 0.83 J 50 62.5 123 50 63.0 124 1 70-130/20
98-06-6 tert-Butylbenzene ND 50 60.5 121 50 60.7 121 0 70-130/20
56-23-5 Carbon Tetrachloride ND 50 61.2 122 50 58.9 118 4 70-130/20
108-90-7 Chlorobenzene ND 50 58.9 118 50 59.2 118 1 70-130/20
75-00-3 Chloroethane ND 50 52.5 105 50 48.0 96 9 60-140/20
67-66-3 Chloroform ND 50 60.7 121 50 61.3 123 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 60.9 122 50 60.2 120 1 70-130/20
106-43-4 p-Chlorotoluene ND 50 60.1 120 50 59.4 119 1 70-130/20
124-48-1 Dibromochloromethane ND 50 49.3 99 50 51.4 103 4 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 53.1 106 50 54.6 109 3 70-130/20
106-93-4 1,2-Dibromoethane ND 50 56.6 113 50 58.0 116 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 55.3 111 50 53.6 107 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 58.7 117 50 58.6 117 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 60.5 121 50 59.6 119 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 58.2 116 50 58.3 117 0 70-130/20
75-34-3 1,1-Dichloroethane ND 50 61.0 122 50 61.5 123 1 70-130/20
107-06-2 1,2-Dichloroethane ND 50 58.3 117 50 60.4 121 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 62.0 124 50 62.1 124 0 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 55.1 110 50 55.9 112 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 64.7 129 50 64.6 129 0 70-130/20
78-87-5 1,2-Dichloropropane ND 50 59.7 119 50 59.6 119 0 70-130/20
142-28-9 1,3-Dichloropropane ND 50 55.3 111 50 56.2 112 2 70-130/20
594-20-7 2,2-Dichloropropane ND 50 61.7 123 50 59.4 119 4 70-130/20
563-58-6 1,1-Dichloropropene ND 50 61.3 123 50 61.1 122 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 59.2 118 50 57.5 115 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 63.2 126 50 62.8 126 1 70-130/20
108-20-3 Di-Isopropyl Ether 54.7 50 113 117 50 113 117 0 70-130/20
100-41-4 Ethylbenzene 39.0 50 95.8 114 50 95.9 114 0 70-130/20
87-68-3 Hexachlorobutadiene ND 50 56.4 113 50 59.8 120 6 70-130/20
98-82-8 Isopropylbenzene 5.3 50 67.1 124 50 67.2 124 0 70-130/20
* = Outside of Control Limits.
88 of 93
FA25801 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25787-4MS E039729.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4MSD E039730.D 5 07/09/15 DP n/a n/a VE1320
FA25787-4 E039721.D 5 07/09/15 DP n/a n/a VE1320
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-2, FA25801-3, FA25801-5, FA25801-6, FA25801-7, FA25801-8, FA25801-9, FA25801-10
FA25787-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 61.8 124 50 61.0 122 1 70-130/20
74-83-9 Methyl Bromide ND 50 58.9 118 50 57.0 114 3 60-140/20
74-87-3 Methyl Chloride ND 50 55.6 111 50 51.4 103 8 60-140/20
74-95-3 Methylene Bromide ND 50 59.9 120 50 61.0 122 2 70-130/20
75-09-2 Methylene Chloride ND 50 58.1 116 50 58.0 116 0 70-130/20
1634-04-4 Methyl Tert Butyl Ether 6.8 50 63.4 113 50 63.8 114 1 70-130/20
91-20-3 Naphthalene 14.6 50 76.9 125 50 83.8 138*9 70-130/20
103-65-1 n-Propylbenzene 8.5 50 70.7 124 50 69.8 123 1 70-130/20
100-42-5 Styrene ND 50 58.7 117 50 58.3 117 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 59.0 118 50 58.5 117 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 54.9 110 50 56.2 112 2 70-130/20
127-18-4 Tetrachloroethylene ND 50 59.2 118 50 59.2 118 0 70-130/20
108-88-3 Toluene 1.1 J 50 58.3 114 50 59.1 116 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 55.2 110 50 61.2 122 10 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 56.1 112 50 61.1 122 9 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 62.0 124 50 61.5 123 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 57.5 115 50 58.9 118 2 70-130/20
79-01-6 Trichloroethylene ND 50 59.1 118 50 58.9 118 0 70-130/20
75-69-4 Trichlorofluoromethane ND 50 62.8 126 50 60.4 121 4 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 56.3 113 50 58.1 116 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene 25.2 50 88.1 126 50 87.2 124 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 3.5 50 64.2 121 50 63.5 120 1 70-130/20
75-01-4 Vinyl Chloride ND 50 60.1 120 50 58.9 118 2 60-140/20
m,p-Xylene 9.3 100 129 120 100 130 121 1 70-130/20
95-47-6 o-Xylene ND 50 60.1 120 50 60.7 121 1 70-130/20
1330-20-7 Xylene (total)9.3 150 189 120 150 190 120 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA25787-4 Limits
1868-53-7 Dibromofluoromethane 102%101%104%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%106%107%70-130%
2037-26-5 Toluene-D8 98%99%98%70-130%
460-00-4 4-Bromofluorobenzene 101%99%99%70-130%
* = Outside of Control Limits.
89 of 93
FA25801 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25800-4MS E039758.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4MSD E039759.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4 E039751.D 5 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-3, FA25801-4, FA25801-11, FA25801-12, FA25801-13, FA25801-14, FA25801-15, FA25801-16,
FA25801-17, FA25801-18, FA25801-19, FA25801-20, FA25801-21, FA25801-22, FA25801-23
FA25800-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 12.6 50 68.1 111 50 66.6 108 2 70-130/20
108-86-1 Bromobenzene ND 50 54.4 109 50 53.1 106 2 70-130/20
74-97-5 Bromochloromethane ND 50 52.7 105 50 52.4 105 1 70-130/20
75-27-4 Bromodichloromethane ND 50 54.9 110 50 53.9 108 2 70-130/20
75-25-2 Bromoform ND 50 42.0 84 50 45.1 90 7 70-130/20
104-51-8 n-Butylbenzene 7.1 50 65.4 117 50 64.7 115 1 70-130/20
135-98-8 sec-Butylbenzene 4.9 50 63.5 117 50 61.8 114 3 70-130/20
98-06-6 tert-Butylbenzene ND 50 58.5 117 50 56.1 112 4 70-130/20
56-23-5 Carbon Tetrachloride ND 50 58.7 117 50 55.8 112 5 70-130/20
108-90-7 Chlorobenzene ND 50 55.6 111 50 55.4 111 0 70-130/20
75-00-3 Chloroethane ND 50 46.6 93 50 43.5 87 7 60-140/20
67-66-3 Chloroform ND 50 58.5 117 50 57.9 116 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 63.8 128 50 62.1 124 3 70-130/20
106-43-4 p-Chlorotoluene ND 50 56.8 114 50 55.0 110 3 70-130/20
124-48-1 Dibromochloromethane ND 50 49.6 99 50 50.5 101 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 49.4 99 50 50.4 101 2 70-130/20
106-93-4 1,2-Dibromoethane ND 50 54.9 110 50 54.3 109 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 48.5 97 50 46.5 93 4 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 56.2 112 50 55.9 112 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 57.9 116 50 56.9 114 2 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 55.6 111 50 53.7 107 3 70-130/20
75-34-3 1,1-Dichloroethane ND 50 58.9 118 50 57.9 116 2 70-130/20
107-06-2 1,2-Dichloroethane ND 50 55.0 110 50 55.0 110 0 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 58.5 117 50 58.1 116 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 53.0 106 50 52.8 106 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 61.3 123 50 60.1 120 2 70-130/20
78-87-5 1,2-Dichloropropane ND 50 56.1 112 50 56.1 112 0 70-130/20
142-28-9 1,3-Dichloropropane ND 50 53.5 107 50 53.4 107 0 70-130/20
594-20-7 2,2-Dichloropropane ND 50 59.7 119 50 58.0 116 3 70-130/20
563-58-6 1,1-Dichloropropene ND 50 58.6 117 50 57.4 115 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 58.2 116 50 55.2 110 5 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 61.8 124 50 59.1 118 4 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 54.6 109 50 54.3 109 1 70-130/20
100-41-4 Ethylbenzene 97.2 50 147 100 50 145 96 1 70-130/20
87-68-3 Hexachlorobutadiene ND 50 54.2 108 50 58.7 117 8 70-130/20
98-82-8 Isopropylbenzene 13.1 50 72.4 119 50 71.6 117 1 70-130/20
* = Outside of Control Limits.
90 of 93
FA25801 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25800-4MS E039758.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4MSD E039759.D 5 07/10/15 EG n/a n/a VE1321
FA25800-4 E039751.D 5 07/10/15 EG n/a n/a VE1321
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-1, FA25801-3, FA25801-4, FA25801-11, FA25801-12, FA25801-13, FA25801-14, FA25801-15, FA25801-16,
FA25801-17, FA25801-18, FA25801-19, FA25801-20, FA25801-21, FA25801-22, FA25801-23
FA25800-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 3.7 50 62.6 118 50 61.2 115 2 70-130/20
74-83-9 Methyl Bromide ND 50 52.8 106 50 52.3 105 1 60-140/20
74-87-3 Methyl Chloride ND 50 47.2 94 50 47.6 95 1 60-140/20
74-95-3 Methylene Bromide ND 50 57.7 115 50 57.7 115 0 70-130/20
75-09-2 Methylene Chloride ND 50 63.2 126 50 62.8 126 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 53.7 107 50 55.2 110 3 70-130/20
91-20-3 Naphthalene 20.3 50 81.4 122 50 85.1 130 4 70-130/20
103-65-1 n-Propylbenzene 46.3 50 103 113 50 99.1 106 4 70-130/20
100-42-5 Styrene 1.3 J 50 59.1 116 50 57.9 113 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 57.8 116 50 55.9 112 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 52.3 105 50 51.6 103 1 70-130/20
127-18-4 Tetrachloroethylene ND 50 57.0 114 50 55.6 111 2 70-130/20
108-88-3 Toluene 17.4 50 71.3 108 50 70.2 106 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 55.9 112 50 59.4 119 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 57.1 114 50 58.0 116 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 58.8 118 50 58.0 116 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 56.3 113 50 55.8 112 1 70-130/20
79-01-6 Trichloroethylene ND 50 57.3 115 50 55.0 110 4 70-130/20
75-69-4 Trichlorofluoromethane ND 50 55.8 112 50 52.9 106 5 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 54.0 108 50 52.9 106 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 211 50 269 116 50 263 104 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 60.0 50 120 120 50 117 114 3 70-130/20
75-01-4 Vinyl Chloride ND 50 52.8 106 50 53.4 107 1 60-140/20
m,p-Xylene 281 100 384 103 100 377 96 2 70-130/20
95-47-6 o-Xylene 97.9 50 155 114 50 153 110 1 70-130/20
1330-20-7 Xylene (total)379 150 538 106 150 531 101 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA25800-4 Limits
1868-53-7 Dibromofluoromethane 102%102%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%106%105%70-130%
2037-26-5 Toluene-D8 99%99%97%70-130%
460-00-4 4-Bromofluorobenzene 101%99%99%70-130%
* = Outside of Control Limits.
91 of 93
FA25801 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25849-2MS E039787.D 500 07/13/15 TD n/a n/a VE1322
FA25849-2MSD E039788.D 500 07/13/15 TD n/a n/a VE1322
FA25849-2 E039794.D 100 07/13/15 TD n/a n/a VE1322
FA25849-2 E039790.D 500 07/13/15 TD n/a n/a VE1322
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-24, FA25801-25, FA25801-26, FA25801-27, FA25801-28
FA25849-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 6070 a 5000 11600 111 5000 11300 105 3 70-130/20
108-86-1 Bromobenzene ND 5000 4870 97 5000 4850 97 0 70-130/20
74-97-5 Bromochloromethane ND 5000 5040 101 5000 5010 100 1 70-130/20
75-27-4 Bromodichloromethane ND 5000 5440 109 5000 5340 107 2 70-130/20
75-25-2 Bromoform ND 5000 4870 97 5000 4860 97 0 70-130/20
104-51-8 n-Butylbenzene 35.7 J 5000 5310 105 5000 5200 103 2 70-130/20
135-98-8 sec-Butylbenzene 17.9 J 5000 5260 105 5000 5200 104 1 70-130/20
98-06-6 tert-Butylbenzene ND 5000 5150 103 5000 4990 100 3 70-130/20
56-23-5 Carbon Tetrachloride ND 5000 5580 112 5000 5410 108 3 70-130/20
108-90-7 Chlorobenzene ND 5000 5170 103 5000 5040 101 3 70-130/20
75-00-3 Chloroethane ND 5000 5550 111 5000 5400 108 3 60-140/20
67-66-3 Chloroform ND 5000 5390 108 5000 5250 105 3 70-130/20
95-49-8 o-Chlorotoluene ND 5000 5190 104 5000 5160 103 1 70-130/20
106-43-4 p-Chlorotoluene ND 5000 5000 100 5000 4990 100 0 70-130/20
124-48-1 Dibromochloromethane ND 5000 5130 103 5000 5050 101 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 5000 4620 92 5000 4610 92 0 70-130/20
106-93-4 1,2-Dibromoethane ND 5000 4770 95 5000 4820 96 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 5000 7380 148*5000 7270 145*2 60-140/20
95-50-1 1,2-Dichlorobenzene ND 5000 4920 98 5000 4910 98 0 70-130/20
541-73-1 1,3-Dichlorobenzene ND 5000 5120 102 5000 5080 102 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 5000 5000 100 5000 4920 98 2 70-130/20
75-34-3 1,1-Dichloroethane ND 5000 5370 107 5000 5300 106 1 70-130/20
107-06-2 1,2-Dichloroethane ND 5000 5290 106 5000 5120 102 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 5000 5450 109 5000 5320 106 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 5000 4810 96 5000 4780 96 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 5000 5740 115 5000 5580 112 3 70-130/20
78-87-5 1,2-Dichloropropane ND 5000 5180 104 5000 4960 99 4 70-130/20
142-28-9 1,3-Dichloropropane ND 5000 4660 93 5000 4630 93 1 70-130/20
594-20-7 2,2-Dichloropropane ND 5000 5490 110 5000 5390 108 2 70-130/20
563-58-6 1,1-Dichloropropene ND 5000 5400 108 5000 5250 105 3 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 5000 5180 104 5000 5080 102 2 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 5000 5610 112 5000 5580 112 1 70-130/20
108-20-3 Di-Isopropyl Ether 25.6 J 5000 5160 103 5000 5120 102 1 70-130/20
100-41-4 Ethylbenzene 3170 5000 8480 106 5000 8310 103 2 70-130/20
87-68-3 Hexachlorobutadiene ND 5000 5030 101 5000 5110 102 2 70-130/20
98-82-8 Isopropylbenzene 99.8 5000 5360 105 5000 5270 103 2 70-130/20
* = Outside of Control Limits.
92 of 93
FA25801 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA25801
Account:GRINCC GRI (Geological Resources Inc.)
Project:Todd & Bowen's; NC Hwy 17 & 45, Midway, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA25849-2MS E039787.D 500 07/13/15 TD n/a n/a VE1322
FA25849-2MSD E039788.D 500 07/13/15 TD n/a n/a VE1322
FA25849-2 E039794.D 100 07/13/15 TD n/a n/a VE1322
FA25849-2 E039790.D 500 07/13/15 TD n/a n/a VE1322
The QC reported here applies to the following samples:Method: SM 6200B
FA25801-24, FA25801-25, FA25801-26, FA25801-27, FA25801-28
FA25849-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 5000 5120 102 5000 5180 104 1 70-130/20
74-83-9 Methyl Bromide ND 5000 6070 121 5000 6020 120 1 60-140/20
74-87-3 Methyl Chloride ND 5000 6740 135 5000 6390 128 5 60-140/20
74-95-3 Methylene Bromide ND 5000 5320 106 5000 5300 106 0 70-130/20
75-09-2 Methylene Chloride ND 5000 5270 105 5000 5200 104 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether 279 5000 5380 102 5000 5430 103 1 70-130/20
91-20-3 Naphthalene 1130 5000 6230 102 5000 6490 107 4 70-130/20
103-65-1 n-Propylbenzene 346 5000 5640 106 5000 5590 105 1 70-130/20
100-42-5 Styrene 32.4 J 5000 5180 103 5000 5130 102 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 5000 5210 104 5000 5140 103 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 5000 4560 91 5000 4620 92 1 70-130/20
127-18-4 Tetrachloroethylene ND 5000 5150 103 5000 4940 99 4 70-130/20
108-88-3 Toluene 15800 a 5000 21000 104 5000 20400 92 3 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 5000 4980 100 5000 5110 102 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 5000 4970 99 5000 5030 101 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 5000 5490 110 5000 5310 106 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 5000 4880 98 5000 4860 97 0 70-130/20
79-01-6 Trichloroethylene ND 5000 5260 105 5000 5050 101 4 70-130/20
75-69-4 Trichlorofluoromethane ND 5000 6410 128 5000 6140 123 4 60-140/20
96-18-4 1,2,3-Trichloropropane ND 5000 4660 93 5000 4840 97 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2910 5000 8430 110 5000 8390 110 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene 774 5000 5980 104 5000 5940 103 1 70-130/20
75-01-4 Vinyl Chloride ND 5000 6520 130 5000 6210 124 5 60-140/20
m,p-Xylene 8870 10000 20400 115 10000 19900 110 2 70-130/20
95-47-6 o-Xylene 3820 5000 9220 108 5000 9060 105 2 70-130/20
1330-20-7 Xylene (total)12700 15000 29600 113 15000 29000 109 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA25849-2 FA25849-2 Limits
1868-53-7 Dibromofluoromethane 105%105%102%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%108%104%102%70-130%
2037-26-5 Toluene-D8 97%97%99%99%70-130%
460-00-4 4-Bromofluorobenzene 98%100%98%99%70-130%
(a) Result is from Run #2.
* = Outside of Control Limits.
93 of 93
FA25801 55.3.3