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Home My WebLink AboutRA-6738_33892_CA_RPTS_20191104_SCH609A Piner Road., Suite 115 Wilmington, North Carolina 28409 Telephone 919-871-0999 Fax 737-207-8261 www.atcgs.com November 4, 2019 Mr. Sean Patrick North Carolina Department of Environmental Quality Raleigh Regional Office Division of Waste Management - UST Section 1628 Mail Service Center Raleigh, North Carolina 27699-1628 Re: Site Check Report Circle K Store #2723471 4940 U.S. Highway 264 West Wilson, Wilson County, North Carolina NCDEQ Facility ID #00-0-0000035356 NCDEQ Incident No. 33892 Dear Mr. Patrick: ATC Associates of North Carolina, LLC (ATC), on behalf of Circle K Stores, Inc., is submitting this Site Check Report for the referenced facility. If you have any questions or require additional information, please contact our office at (919) 871-0999. Sincerely, ATC Associates of North Carolina, LLC Maureen Jackson, P.G. Senior Project Manager cc: Mr. Brent Puzak, Circle K Stores, Inc. SITE CHECK REPORT Circle K Store #2723471 4940 U.S. Highway 264 West Wilson, Wilson County, North Carolina NCDEQ Facility ID #00-0-0000035356 NCDEQ Incident No. 33892 Circle K Store #2723471 November 4, 2019 NCDEQ Facility ID #00-0-0000035356 Site Check Report B. Site History 1. Provide UST Owner and Operator Information See Table 1. 2. Provide UST Information See Table 2. 3. Provide Non-UST Information No ASTs or Surface Spills are known to exist at the site. 4. Describe relation of location of current UST system to historical UST releases. Various phases of assessment activities (UST incident #33892) have been conducted since 2009 in proximity to the gasoline UST basin and gasoline dispenser island area. Currently, biosocks have been placed in select monitoring wells to assist with natural attenuation and semi-annual groundwater sampling is being conducted. 5. Provide a Brief Description of Site Characteristics The subject property consists of one convenience store building and petroleum fueling equipment. The subject property and surrounding area are fairly level; however, the properties tend to slope to the north toward the retention ponds and swamp area. The subject property is located in a mainly commercial area of Wilson. Public water supplies in the area are provided by the City of Wilson. During assessment activities associated with UST incident #33892, two water supply wells were identified within 1,500 feet of the subject facility. One water supply well, PW-1, is located approximately 550 feet southwest of the site and is used for potable purposes. The second water supply well is located approximately 1,500 feet southwest of the site and is currently not in use. A topographic map and site map are attached as Figures 1 and 2, respectively. C. Site Check Procedures 1. UST System Testing On September 4, 2019, during semi-annual groundwater sampling activities, ATC personnel measured approximately three feet of free product in monitoring well MW-3. On September 5, 2019, Circle K contracted with Petroleum Service & Calibration (PS&C) to test the UST systems. On this date, the UST system passed its respective tests. A copy of the testing results is provided in Attachment I. 2. Site Check Procedure On September 30, 2019, ATC personnel contracted with Carolina Soil Investigations (CSI) to advance ten soil borings (labeled SB-1 through SB-10) around the active gasoline UST system. Circle K Store #2723471 November 4, 2019 NCDEQ Facility ID #00-0-0000035356 Site Check Report The soil borings were scheduled to be advanced to a depth of thirteen feet below ground surface (bgs). Refusal was noted to occur between 8 and 13 feet for each boring so the actual termination depth varies. Two soil samples were collected from each boring (with the exception of soil boring SB-5). The soil sample with the greatest PID reading from each boring was submitted to the laboratory for analyses. The location of the soil samples are provided on Figure 2. It should be noted the soil samples were collected as close as possible to the respective UST components. 3. Soil Excavation Activities Soil excavation was not performed as part of this site check. D. Site Investigation 1. Field Screening Soil samples SB-1 through SB-10 were screened with a photoionization detector (PID) following sample collection. The respective PID reading is provided on Table 3. 2. Soil Sampling Information On September 30, 2019, soil samples SB-1 through SB-10 were collected at varying depths due to refusal. The soil encountered at the sampling depths consisted of a predominantly grayish-brown silt. The boring logs for the respective soil borings are provided in Attachment II. The soil samples were shipped to a N.C. certified laboratory in a chilled cooler following proper chain-of-custody procedures. The soil samples were originally requested to be analyzed by TPH-Gasoline Range Organics (GRO) and Environmental Protection Agency (EPA) Method 8260. Upon receipt of the laboratory report and per conversations with NCDEQ personnel, ATC personnel requested the project laboratory analyze the soil samples by EPA Method 8270, Massachusetts Department of Environmental Protection (MADEP) Method for volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH), and Hexane Extractable Material (HEM) Petroleum Hydrocarbons by EPA Method 9071B. It should be noted the soil samples could not be analyzed by MADEP Method for VPH as sufficient methanol preserved soil was not available for the analysis to be run. Additionally, it should be noted EPA Methods 8270 and 9071B and MADEP Method for EPH were run on the soil samples outside of hold time. It should be noted a sample of the product detected in monitoring well MW-3 was also collected and submitted to the project laboratory for analyses by GC Fingerprint by method 8015C. 3. Groundwater and Surface Sampling Information Groundwater and surface water samples were not collected during site check activities. Circle K Store #2723471 November 4, 2019 NCDEQ Facility ID #00-0-0000035356 Site Check Report 4. Quality Control Measures The soil samples were placed in laboratory provided jars and vials. The samples were immediately placed on ice and contained in a cooler during transportation. The samples were transported by courier under a chain-of-custody to the laboratory for analysis. 5. Investigation Results Soil Laboratory analytical results of the soil samples collected during this site check did not detect TPH-GRO above the established State Action Level. Laboratory analytical results of the soil samples collected during this site check did not detect HEM petroleum hydrocarbons above laboratory method detection limits (MDLs). 1-Methylnaphthalene and C11-C22 Aromatics concentrations were detected in soil sample SB-2 above the established Soil-to-Groundwater (STGW) Maximum Contaminant Concentrations (MSCCs). This soil boring is located immediately adjacent to monitoring well MW-3. The results are provided in Table 3. A copy of the laboratory report and chain-of-custody documents are provided in Attachment III. Free Product Laboratory analyses of the product sample collected from monitoring well MW-3 determined that the hydrocarbon pattern of the sample was in the TPH-Diesel Range Organics (TPH-DRO) range C10-C28. The absence of the prominent n-alkane peaks suggested the sample was severely weathered diesel or refined mineral oil with components in the TPH-DRO range. A copy of the chromatograms are provided in Attachment III. E. Conclusion and Recommendations Laboratory analytical results of the soil samples do not indicate a release of petroleum has occurred from the gasoline UST system at the facility. Based on the available data, ATC is not clear as to where the free product detected in monitoring well MW-3 came from. ATC has requested Circle K test the onsite diesel UST system; however, the diesel UST system and its components are located hydraulically downgradient of monitoring well MW-3. F. Figures Figure 1 – USGS Topographic Map Figure 2 – Site Map G. Tables Table 1 – Site History - UST Owner and Operator Information Table 2 – Site History – UST/AST System Information Table 3 – Soil Analytical Results H. Attachments I – Notifications II – Boring Logs III – Laboratory Report and Chain-of-Custody Documents TABLES TABLE 1 SITE HISTORY - UST OWNER AND OPERATOR INFORMATION CIRCLE K STORE #2723471 4940 U.S. HIGHWAY 264 WEST WILSON, WILSON COUNTY, NORTH CAROLINA NCDEQ FACILITY ID #00-0-0000035356 NCDEQ INCIDENT NO. 33892 Revision Date:11/4/2019 Incident Number and Name:Circle K Store #2723471 UST ID Number All Facility ID Number 00-0-00000353656 City State Zip Telephone Number Raleigh NC 27606 919-774-6700 City State Zip Telephone Number Raleigh NC 27606 919-774-6700 Circle K Stores, Inc.2001 to Present 1100 Situs Court, Suite 100 Street Address Dates of Operation (MM/DD/YY to MM/DD/YY)Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)Name of Operator 1100 Situs Court, Suite 100 Circle K Stores, Inc.2001 to Present Street Address TABLE 2 SITE HISTORY - UST/AST SYSTEM INFORMATION CIRCLE K STORE #2723471 4940 U.S. HIGHWAY 264 WEST WILSON, WILSON COUNTY, NORTH CAROLINA NCDEQ FACILITY ID #00-0-0000035356 NCDEQ INCIDENT NO. 33892 Revision Date:11/4/2019 UST ID Number Current/Last Contents Previous Contents Capacity (gallons) Construction Details Tank Dimensions Description of Associated Piping and Pumps Date Tank Installed Status of UST Was Release Associates with the UST System? 63B Gasoline (Reg)None 15,000 Fiberglass Unknown DW Flex 12/18/19 Active 63C Gasoline (Prem)None 12,000 Fiberglass Unknown DW Flex 12/18/96 Active 63D Gasoline (Mid)None 10,000 Fiberglass Unknown DW Flex 12/18/96 Active 63E Diesel None 15,000 Fiberglass Unknown DW Flex 12/18/96 Active 63F Diesel None 15,000 Fiberglass Unknown DW Flex 12/18/96 Active 6 DEF None 8,000 Fiberglass Unknown DW Fiberglass 04/16/15 Active AST ID Number Current/Last Contents Previous Contents Capacity (gallons) Construction Details Tank Dimensions Description of Associated Piping and Pumps Date Tank Installed Status of AST Was Release Associates with the AST System? Incident Number and Name:Circle K Store #2723471 None associated with this site TABLE 3 SOIL ANALYTICAL RESULTS CIRCLE K STORE #2723471 4940 U.S. HIGHWAY 264 WEST WILSON, WILSON COUNTY, NORTH CAROLINA NCDEQ FACILITY ID #00-0-0000035356 NCDEQ INCIDENT NO. 33892 EPA Method 8015C Sample Depth (feet) PID Reading (ppm)Date Sampled TPH - GROBenzeneAcetoneNaphthalenen-Butylbenzene1-Methylnaphthalene2-MethylnaphthalenePhenanthrenePyreneC11-C22 AromaticsC9-C18 AliphaticsC19-C36 Aliphatics5 19.1 <9.7 <0.00071 0.126 <0.0071 <0.0071 <0.014 <0.014 <0.014 <0.014 <3.4 19.9 3.41 8 13.9 5 195.2 10.5 <0.00056 <0.056 0.0096 0.0056 0.0331 0.0312 0.022 0.0285 64.1 170 74 8 55.1 8 9.6 <6.5 <0.00051 0.099 <0.0051 <0.0051 <0.012 <0.012 <0.012 <0.012 <2.9 <2.9 <2.9 13 1.0 5 0.3 8 1.7 <6.8 <0.00053 <0.053 <0.0053 <0.0053 <0.012 <0.012 <0.012 <0.012 <3.0 <3.0 <3.0 SB-5 5 0.0 9/30/2019 <6.4 0.00056 <0.056 <0.0056 <0.0056 <0.011 <0.011 <0.011 <0.011 <2.7 <2.7 <2.7 5 0.1 10 0.8 <7.5 <0.00048 <0.048 <0.0048 <0.0048 <0.012 <0.012 <0.012 <0.012 <3.1 <3.1 <3.1 5 0.1 9 0.2 <6.8 <0.00055 0.0918 <0.0055 <0.0055 <0.012 <0.012 <0.012 <0.012 3.51 <3.0 <3.0 5 1.5 <7.1 <0.00055 <0.055 <0.0055 <0.0055 <0.012 <0.012 <0.012 <0.012 <3.0 <3.0 <3.0 10 1.0 5 0.7 <8.8 <0.00072 <0.072 <0.0072 <0.0072 <0.014 <0.014 <0.014 <0.014 <3.4 <3.4 <3.4 10 0.5 5 1.3 <8.6 <0.00064 <0.064 <0.0064 <0.0064 <0.014 <0.014 <0.014 <0.014 <3.4 <3.4 <3.4 10 0.9 50 ---------------------- --0.0056 24 0.16 4.3 0.004 3.6 56 270 31 540 # --18 14,000 313 626 20 63 469 469 469 1,500 31000 --164 360,000 8,176 16,350 100 1,635 12,264 12,264 12,264 40,000 810,000 Notes: 1. Concentrations reported in milligrams per kilogram (mg/kg). 2. PID denotes photoionization detector. 3. PPM denotes parts per million. 4. # denotes compound considered immobile. EPA Method 8270 MADEP Method for EPH Not Submitted for Analyses Not Submitted for Analyses Not Submitted for Analyses Not Submitted for Analyses Not Submitted for Analyses Not Submitted for Analyses Not Submitted for Analyses Not Submitted for Analyses Not Submitted for Analyses SB-7 9/30/2019 Soil-to-Groundwater MSCCs (mg/kg) SB-8 9/30/2019 SB-9 9/30/2019 SB-10 9/30/2019 Residential MSCCs (mg/kg) Commercial/Industrial MSCCs (mg/kg) EPA Method 8260 NCDEQ Action Level (mg/kg) Analytical Method SB-1 SB-2 SB-3 9/30/2019 9/30/2019 9/30/2019 SB-4 9/30/2019 SB-6 9/30/2019 FIGURES FIGURE 1 USGS TOPOGRAPHIC MAP Pantry # 3471 4940 US Highway 264 West Wilson, North Carolina 2725 E. Millbrook Road, Suite 121 Raleigh, NC 27604 (919) 871-0999 PROJECT NO: 45.24639.3471 SCALE: 1” = 600’ DATE: 7/7/2009 SITE ATTACHMENT I Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Comments and Problems Overview : 2019 Test Performed Tech Notes Anode Bag Installed Pictures Taken PS&C Will Make Repairs PS&C technician's disptached to site due to 3 feet of product was found in monitoring well (3) by MPD 11/12. q q q Per Brent Puzak (conference call with Zach/Jeff) testing was performed and completed on everything that was tied into the front of the store. q q q PS&C technician took a sample at the monitoring well closest to dispenser 11/12. Product in sample appears to be /smell/look like Diesel. q q q Technician Signature : 2019 Tester's Name Ryan S Blackmon Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# : 2019 Unleaded 15119 T1 63 Fiberglass Single Wall 1 NA SIR UST 63 0.026 1.638 0 0.036 0.000 1.638 90 0.036 3.240 -1.602 -1.102 0.500 63.5 119.000 182.5 63 0 67 90 07:50am 07:53am 08:14am 08:24am 08:24am 08:29am 0 0 .500 .658 .658 .658 I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Unleaded 15119 T1 63 Fiberglass Single Wall 1 NA SIR 210 205 200 205.000 205.000 0.054 1.085 1:05 Monitoring Well 8:40 am Tank Field 9:45 am Pass Pass Pass Not Applicable Technician Signature : 2019 Tester's Name Ryan S Blackmon Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# X : 2019 Premium 11528 T2 58 Fiberglass Single Wall 1 NA CSLD UST 58 0.026 1.508 0 0.036 0.000 1.508 43 0.036 1.548 -0.040 0.460 0.500 45.5 91.000 136.5 58 0 67 43 10:00am 10:04am 10:20am 10:30am 10:30am 10:33am 0 0 .500 .630 .630 .630 I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Premium 11528 T2 58 Fiberglass Single Wall 1 NA CSLD 205 200 195 200.000 200.000 0.053 1.058 1:03 Monitoring Well 10:45 am Tank Field 11:45 am Pass Pass Pass Not Applicable Technician Signature : 2019 Tester's Name Ryan S Blackmon Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Line Piping Identification : 2019 Product Type of Line Type of Piping Piping Configuration Unleaded Pressure Flex Double Wall Premium Pressure Flex Double Wall Auto/Truck Diesel Pressure Flex Double Wall (89) Non-Ethanol Pressure Flex Double Wall Line / Piping Testing : 2019 Reason For Test qAnnual qNew Installation qTroubleshooting q3Other qResponse To SIR Problem qLeak Detetection Piping Release Detection Method qELLD qAnnual Line Tightness Testing qSIR qInterstitial Monitoring q3Other Line Piping Test Procedure > In addition to these generalized requirements, testing must be conducted in accordance with the manufacturer’s requirements Rigid Pipelines > EZY-Chek Manual Line Leak Detector (for Rigid Pipelines) — Certification: Leak rate of 0.1 gph with PD = 98.0% and PFA = 1%. Leak Threshold: 0.05 pgh. A pipeline system should not be declared tight if the test result indicates a loss that equals or exceeds this threshold. > Maximum pipeline capacity of 426 gallons. Flexible Pipelines > EZY-Chek Manual Line Leak Detector (for Flexible Pipelines) — Certification: Leak rate of 0.1 gph with PD = 99.8% and PFA = 0.2%. Leak Threshold: 0.05 pgh. A pipeline system should not be declared tight if the test result indicates a loss that equals or exceeds this threshold. > Maximum pipeline capacity of 101 gallons (example: 275 feet of 3 inch line). Product Unique Tank ID #Line Type STP Type Piping Material # of Connected Dispensers # of Flex Connectors Unleaded T1 Pressure Red Jacket Flex 6 0 Premium T2 Pressure Red Jacket Flex 6 0 Auto/Truck Diesel T5 /T6 Pressure Red Jacket / FePtero Flex 12 0 (89) Non-Ethanol T3 Pressure Red Jacket Flex 1 0 Product Unique Tank ID #Pipe Diameter Approximate Elevation Difference ALLD And Dispenser Length of Pipe (IN) Line Size (GLNS) Isolation Device Test Pressure/Applied Pressure Unleaded T1 1.5 2 Feet 2160 16.524 Ball Valve 50 Premium T2 1.5 2 Feet 1800 13.770 Ball Valve 55 Auto/Truck Diesel T5 /T6 1.5/2 2 Feet 3600 0.000 Ball Valve 50 (89) Non-Ethanol T3 1.5 2 Feet 2340 17.901 Ball Valve 60 Technician Signature : 2019 Tester's Name Ryan S Blackmon Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Line / Piping Testing : 2019 Product Line Testing Data Collection Protocol : 2019 Unleaded Unique Tank ID: T1 Time Data +/-GPL RES GPH 8:15 am 26 0 0.0037 0.0000 0.0000 8:30 am 25 -1 0.0037 0.0037 0.0148 8:45 am 25 0 0.0037 0.0037 0.0148 Leak Rate 0.0148 Result (P/F)Pass Premium Unique Tank ID: T2 Time Data +/-GPL RES GPH 8:15 am 48 0 0.0037 0.0000 0.0000 8:30 am 47 -1 0.0037 0.0037 0.0148 8:45 am 47 0 0.0037 0.0037 0.0148 Leak Rate 0.0148 Result (P/F)Pass Auto/Truck Diesel Unique Tank ID: T5 /T6 Time Data +/-GPL RES GPH 11:00 am 49 0 0.0037 0.0000 0.0000 11:15 am 48 -1 0.0037 0.0037 0.0148 11:30 am 48 0 0.0037 0.0037 0.0148 Leak Rate 0.0148 Result (P/F)Pass (89) Non-Ethanol Unique Tank ID: T3 Time Data +/-GPL RES GPH 11:00 am 73 0 0.0037 0.0000 0.0000 11:15 am 72 -1 0.0037 0.0037 0.0148 11:30 am 72 0 0.0037 0.0037 0.0148 Leak Rate 0.0148 Result (P/F)Pass Technician Signature : 2019 Tester's Name Ryan S Blackmon Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Circle K Stores, Inc.2723471 0-035356 4934 Raleigh Road Parkway West Wilson Wilson Petroleum Service & Calibration, Inc.877-479-8152 jeff@testmytanks.com Ryan S Blackmon 09/05/2019 T1 15119 Unleaded Veeder Root FX1V T2 11528 Premium Veeder Root FX1V T3 9744 (89) Non-Ethanol Veeder Root FX1V T5 15192 Auto/Truck Diesel (T5) Veeder Root FX1DV T6 15192 Auto/Truck Diesel (T6) Veeder Root FX1DV 30 22 180 2 13 2 34 32 220 3 13 3 28 27 150 2 9 2 31 25 280 4 9 8 42 41 300 5 11 10 X X X X X X X X X X X X X X X X X X X X X X X X X Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Circle K Stores, Inc.2723471 0-035356 4934 Raleigh Road Parkway West Wilson Wilson Petroleum Service & Calibration, Inc.877-479-8152 jeff@testmytanks.com Ryan S Blackmon 09/05/2019 T1 15119 Unleaded OPW / 1C-3132P 12 < 5min 9:00 am 9:05 am 15" wc 15" wc T2 11528 Premium OPW / 1C-3132P 12 < 5 min 9:10 am 9:15 am 15" wc 15" wc X X X X X X X X X X X X X X X X Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Parts Replacement Inspection : 2019 No Parts Replaced Technician Signature : 2019 Tester's Name Ryan S Blackmon Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68135 PSCIN 100377-298 Facility ID#0-035356 Emission PO# TECHNICIAN LICENSING - Ryan S Blackmon : 2019 Type Certified State License Issue Expiration Class AB Operator Class A/B Operator Training South Carolina CK/Yam/Lowes/HT/Ingles 02/12/2016 NA Compliance with OSHA Standard 1910.146 Confined Space Entry Nationwide NA 03/15/2019 03/15/2020 Estabrooks Line Nationwide 75-6063 02/18/2018 02/18/2020 Estabrooks Tank Nationwide 75-6063 04/11/2019 04/11/2021 Estabrooks Leak Detector Nationwide 75-6063 02/18/2018 02/18/2020 Estabrooks-Equipment Tank Equipment ASP E0927008 08/06/2018 08/06/2019 Estabrooks-Equipment Tank Equipment DPS 405180713 08/06/2018 08/06/2019 Estabrooks-Equipment Tank Equipment DPS 1083750007 08/06/2018 08/06/2019 Estabrooks-Equipment Tank Equipment Headset 33-6003-45 04/25/2018 NA Estabrooks-Equipment Tank Equipment MIC M0935001 08/06/2018 08/06/2019 Estabrooks-Equipment Tank Equipment NPG NG0397641 08/06/2018 08/06/2019 Estabrooks-Equipment Tank Equipment NPG NG6842931 08/06/2018 08/06/2019 Estabrooks-Equipment Tank Equipment WSD D1706218 08/06/2018 08/06/2019 Estabrooks-Equipment Tank Equipment WSP P1104203 08/06/2018 08/06/2019 Fall Protection / Prevention OSHA-Fall Protection, Aerial Lifts, Ladders Nationwide NA 08/08/2019 08/08/2020 Fire Extinguisher Fire Extinguisher Nationwide NA 06/28/2019 06/28/2021 First Aid / CPR First Aid / CPR Training Nationwide NA 06/28/2019 06/28/2021 Meter Calibration Meter Calibration (5 Gallon & 100 Gallon)North Carolina 1964 12/21/2018 12/31/2019 Meter Calibration Meter Calibration (5 Gallon & 100 Gallon)Virginia 29499 07/27/2016 12/31/2019 OPW Installation Stage One Vapor Recovery Nationwide 0148106 06/18/2018 06/17/2020 ASSISTANT TECHNICIAN LICENSING - Garrett S Denny : 2019 Type Certified State License Issue Expiration Class AB Operator Class A/B Operator Training South Carolina CK/Yam/Lowes/HT/Ingles 08/05/2019 NA Compliance with OSHA Standard 1910.146 Confined Space Entry Nationwide NA 08/23/2019 03/15/2020 Fall Protection / Prevention OSHA-Fall Protection, Aerial Lifts, Ladders Nationwide NA 08/09/2019 Fire Extinguisher Fire Extinguisher Nationwide NA 06/28/2019 06/28/2021 First Aid / CPR First Aid / CPR Training Nationwide NA 06/28/2019 06/28/2021 Powered by TCPDF (www.tcpdf.org) Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68137 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Comments and Problems Overview : 2019 No Comments or Problems Technician Signature : 2019 Tester's Name Phillip A Bowman Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68137 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Circle K Stores, Inc.2723471 0-035356 4934 Raleigh Road Parkway West Wilson Wilson Petroleum Service & Calibration, Inc.877-479-8152 jeff@testmytanks.com Phillip A Bowman 09/05/2019 Unleaded (T1)Premium (T2)1/2 3/4 5/6 7/8 Opw OPW OPW OPW OPW OPW 35.5 36 32.5 32.5 32.5 32.5 12 15 15 15 15 15 15 min 15 min 15 min 15 min 15 min 15 min 1:40 pm 2:40 pm 1:45 pm 1:45 pm 3:50 pm 4:50 pm 3:45 pm 4:45 pm 3:55 pm 4:55 pm 4:00 pm 5:00 pm 16.5 16.5 19.75 19.75 19.25 19.25 19.5 19.5 20 20 19.5 19.5 09/06/2022 X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X Circle K Stores, Inc.2723471 0-035356 4934 Raleigh Road Parkway West Wilson Wilson Petroleum Service & Calibration, Inc.877-479-8152 jeff@testmytanks.com Phillip A Bowman 09/05/2019 9/10 11/12 13 OPW OPW OPW 32.5 32.5 32.5 15 17 13 15 min 15 min 15 min 4:05 pm 5:05 pm 1:55 pm 2:55 pm 1:50 pm 2:50 pm 20 20 21 21 18 18 09/06/2022 X X X X X X X X X X X X X X X X X X X X X Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68137 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Vacuum Truck : 2019 Vacuum Truck Services (Hours):2 Additional hours of labor for containments with special conditions (1 hr minimum - if applicable): Gallons and disposal of PCW pumped:695 Furnished Gallons Of Water:350 Vacuum Truck Mobilization Fee (1/2 hour minimum):1.5 Labor incurred due to filling containments with low water pressure:1 Total Mileage (if applicable):49.8 Technician Signature : 2019 Tester's Name Phillip A Bowman Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68137 PSCIN 100377-298 Facility ID#0-035356 Emission PO# PS&C 1 877-479-8152 68137 Circle K Stores, Inc. 1100 Situs Court Suite 100, Raleigh, NC 27606 704-583-5762 2723471 4934 Raleigh Road Parkway West, Wilson, North Carolina 27896 252-237-7200 Petroleum Service & Calibration, Inc. PCW 695 GAL None Phillip A Bowman 09 05 2019 Phillip A Bowman 09 05 2019 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68137 PSCIN 100377-298 Facility ID#0-035356 Emission PO# Parts Replacement Inspection : 2019 No Parts Replaced Technician Signature : 2019 Tester's Name Phillip A Bowman Test Date 09/05/2019 Tester's Signature I certify under penalty of law that the test was conducted according to the protocol of the test method used and was performed in accordance with all regulatory requirements of the state codes and that the submitted information is true, accurate and complete.q3 Petroleum Service & Calibration, Inc. www.testmytanks.com Customer/Facility Information Company Information Customer Name Circle K Stores, Inc.Company Name Petroleum Service & Calibration, Inc. Location Name 2723471 Company Phone Number 877-479-8152 Site Address 4934 Raleigh Road Parkway West Company Address P.O. Box 851 City/State/Zip Wilson, NC 27896 City Denver State NC County Wilson Site Phone Number 252-237-7200 Job Number 68137 PSCIN 100377-298 Facility ID#0-035356 Emission PO# TECHNICIAN LICENSING - Phillip A Bowman : 2019 Type Certified State License Issue Expiration Class AB Operator Class A/B Operator Training South Carolina CK/Yam/Lowes/HT/Ingles 07/29/2013 NA Compliance with OSHA Standard 1910.146 Confined Space Entry Nationwide NA 03/15/2019 03/15/2020 Estabrooks Leak Detector Nationwide 37-2728 08/23/2019 08/23/2021 Estabrooks Line Nationwide 37-2728 08/23/2019 08/23/2021 Fall Protection / Prevention OSHA-Fall Protection, Aerial Lifts, Ladders Nationwide NA 08/08/2019 08/08/2020 Fire Extinguisher Fire Extinguisher Nationwide NA 06/28/2019 06/28/2021 First Aid / CPR First Aid / CPR Training Nationwide NA 06/28/2019 06/28/2021 Meter Calibration Meter Calibration (5 Gallon & 100 Gallon)Virginia 29502 07/27/2016 12/31/2019 OPW Installation Stage One Vapor Recovery Nationwide 0148110 06/18/2018 06/17/2020 ASSISTANT TECHNICIAN LICENSING - Raymond G Sensing : 2019 Type Certified State License Issue Expiration Compliance with OSHA Standard 1910.146 Confined Space Entry Nationwide NA 09/03/2019 Fall Protection / Prevention OSHA-Fall Protection, Aerial Lifts, Ladders Nationwide NA 08/30/2019 08/08/2020 Fire Extinguisher Fire Extinguisher Nationwide NA 09/03/2019 First Aid / CPR First Aid / CPR Training Nationwide NA 09/03/2019 Powered by TCPDF (www.tcpdf.org) ATTACHMENT II 10-04-2019 S:\Enviro\DSCA Contract\Site #65-0004 Coastal Dry Cleaners, Wilmington, NC\Boring Logs\SB-6.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BGS - below ground surface. PID readings were screened at 5 and 8 feet bgs. Boring terminated at 8 feet bgs. SB-1 soil sample collected at 1020. BORING LOG: SB-1 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 USCSAR AR ML SM GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT End of boring PID (ppm) 19.1 13.9 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-1.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-2 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 USCSAR AR ML SM GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT End of boring PID (ppm) 195.2 55.1 BGS - below ground surface. PID readings were screened at 5 and 8 feet bgs. Boring terminated at 8 feet bgs. SB-2 soil sample collected at 1045. 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-2.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-3 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 USCSAR AR SP SM SM GRAPHICDESCRIPTION Asphalt Gravel Orange; SAND Brown; SIlty SAND Brown; Silty SAND; Saturated End of boring PID (ppm) 9.6 1.0 BGS - below ground surface. PID readings were screened at 8 and 13 feet bgs. Boring terminated at 15 feet bgs. SB-3 soil sample collected at 1100. 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-1.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-4 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 USCSAR AR ML SM GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT End of boring PID (ppm) 0.3 1.7 BGS - below ground surface. PID readings were screened at 5 and 8 feet bgs. Boring terminated at 8 feet bgs. SB-4 soil sample collected at 1120. 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-4.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-5 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 USCSAR AR ML ML GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Whiteish; SILT End of boring BGS - below ground surface. PID reading screened at 5 feet bgs. Boring hit refusal at 6 feet bgs. SB-5 soil sample collected at 1140. PID (ppm) 0.0 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-1.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-6 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 9 10 USCSAR AR ML SM GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT End of boring PID (ppm) 0.1 0.8 BGS - below ground surface. PID readings were screened at 5 and10 feet bgs. Boring hit refusal at 10 feet bgs. SB-6 soil sample collected at 1200. 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-7.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-7 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 9 10 USCSAR AR ML SM SM GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT Grayish brown; SILT; Saturated End of boring PID (ppm) 0.1 0.2 BGS - below ground surface. PID readings were screened at 5 and 9 feet bgs. Boring terminated at 10 feet bgs. SB-7 soil sample collected at 1230. 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-7.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-8 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 9 10 USCSAR AR ML SM SM GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT Grayish brown; SILT; Saturated End of boring PID (ppm) 1.5 1.0 BGS - below ground surface. PID readings were screened at 5 and 10 feet bgs. Boring hit refusal at 10 feet bgs. SB-8 soil sample collected at 1250. 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-8.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-9 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 9 10 USCSGRAPHICDESCRIPTION PID (ppm) 0.7 0.5 BGS - below ground surface. PID readings were screened at 5 and 10 feet bgs. Boring hit refusal at 10 feet bgs. SB-9 soil sample collected at 1310. AR AR ML SM Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT End of boring 10-04-2019 S:\Enviro\Pantry\Pantry 3471 - Wilson\Boring Logs\SB-9.borClient: The Pantry ATC Project No. CIRK3471SC Wilson, Wilson County, North Carolina 4940 US Highway 264 West Pantry #3471 BORING LOG: SB-10 (Page 1 of 1) Date(s) Drilled : 09/30/19 Drilling Contractor : CSI Drilling Method : Hand Auger / Direct Push Boring Diameter : 2 inches Sampling Method : Macrocore Sampling Interval : Continuous Logged By : Frank Beacher Depth In Feet (BGS)0 1 2 3 4 5 6 7 8 9 10 USCSAR AR ML SM GRAPHICDESCRIPTION Asphalt Gravel Grayish brown; CLayey SILT Grayish brown; SILT End of boring PID (ppm) 1.3 0.9 BGS - below ground surface. PID readings were screened at 5 and 10 feet bgs. Boring hit refusal at 10 feet bgs. SB-10 soil sample collected at 1330. ATTACHMENT III 11/01/19 Technical Report for ATC Group Services LLC Circle K #2723471-Wilson, NC Cirk3471SC SGS Job Number: LA58144 Sampling Date: 09/30/19 Report to: ATC Group Services LLC. 2725 East Millbrook Road Suite 121 Raleigh, NC 27604 maureen.jackson@atcgs.com ATTN: Maureen Jackson Total number of pages in report: Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), AZ(AZ0805), FL(E87657), IL(200082), KY(#31), NC(487), SC(73004001), NJ(LA007), TX(T104704186-18-16), WV(257) This report shall not be reproduced, except in its entirety, without the written approval of SGS. Test results relate only to samples analyzed. SGS North America Inc. • 500 Ambassador Caffery • Scott, LA 70583 • tel: 337-237-4775 Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Program and/or state specific certification programs as applicable. Client Service contact: Amy Jackson 337-237-4775 Ron Benjamin Lab Director Scott, LA 11/01/19 Reissue #1 e-Hardcopy 2.0 Automated Report 141 SGS is the sole authority for authorizing edits or modifications to this document. Unauthorized modification of this report is strictly prohibited. Review standard terms at: http://www.sgs.com/en/terms-and-conditions The results set forth herein are provided by SGS North America Inc. Please share your ideas about how we can serve you better at: EHS.US.CustomerCare@sgs.com 1 of 141 LA58144 SGS Scott, LA 500 Ambassador Caffery Parkway Scott, LA 70583, USA t +1 (0)337 237 4775 www.sgs.com Member of the SGS Group (SGS SA) SGS IS THE WORLD’S LEADING INSPECTION, VERIFICATION, TESTING AND CERTIFICATION COMPANY. November 1, 2019 ATC Group Services LLC ATTN: Maureen Jackson 2725 East Millbrook Road Suite 121 Raleigh, NC 27604 RE: SGS Job #LA58144 “Circle K #2726471-Wilson, NC“ Dear Ms. Jackson, The final report for SGS Job LA58144 has been amended from the original. This report replaces in its entirety any previously submitted copy. Semivolatile Organics Compounds (SVOCs) by EPA 8270E, Extractable Petroleum Hydrocarbons (EPH) by MADEP, and Hexane Extractable Material (HEM) Petroleum Hydrocarbons by EPA method 9071B analyses were added to all samples as requested. The results for the added analyses are included in this revised laboratory report. Sincerely, Amy Jackson Environment, Health and Safety Project Manager SGS-Scott 2 of 141 LA58144 Table of Contents -1- Sections: Section 1: Sample Summary ...................................................................................................5 Section 2: Case Narrative/Conformance Summary ..............................................................7 Section 3: Summary of Hits ....................................................................................................12 Section 4: Sample Results ........................................................................................................15 4.1: LA58144-1: SB-1 .........................................................................................................16 4.2: LA58144-1R: SB-1 .......................................................................................................20 4.3: LA58144-2: SB-2 .........................................................................................................25 4.4: LA58144-2R: SB-2 .......................................................................................................29 4.5: LA58144-3: SB-3 .........................................................................................................34 4.6: LA58144-3R: SB-3 .......................................................................................................38 4.7: LA58144-4: SB-4 .........................................................................................................43 4.8: LA58144-4R: SB-4 .......................................................................................................47 4.9: LA58144-5: SB-5 .........................................................................................................52 4.10: LA58144-5R: SB-5 .....................................................................................................56 4.11: LA58144-6: SB-6 ........................................................................................................61 4.12: LA58144-6R: SB-6 .....................................................................................................65 4.13: LA58144-7: SB-7 .......................................................................................................70 4.14: LA58144-7R: SB-7 .....................................................................................................74 4.15: LA58144-8: SB-8 .......................................................................................................79 4.16: LA58144-8R: SB-8 .....................................................................................................83 4.17: LA58144-9: SB-9 .......................................................................................................88 4.18: LA58144-9R: SB-9 .....................................................................................................92 4.19: LA58144-10: SB-10 ...................................................................................................97 4.20: LA58144-10R: SB-10 .................................................................................................101 4.21: LA58144-11: MW-3 ...................................................................................................106 Section 5: Misc. Forms ............................................................................................................107 5.1: Chain of Custody ...........................................................................................................108 Section 6: MS Volatiles - QC Data Summaries .....................................................................112 6.1: Method Blank Summary ................................................................................................113 6.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................116 Section 7: MS Semi-volatiles - QC Data Summaries ............................................................119 7.1: Method Blank Summary ................................................................................................120 7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................122 Section 8: GC Volatiles - QC Data Summaries .....................................................................125 8.1: Method Blank Summary ................................................................................................126 8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................128 8.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................130 Section 9: GC/LC Semi-volatiles - QC Data Summaries .....................................................132 9.1: Method Blank Summary ................................................................................................133 9.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................135 Section 10: General Chemistry - QC Data Summaries ........................................................137 10.1: Method Blank and Spike Results Summary ................................................................138 123456789103 of 141 LA58144 Table of Contents -2- Sections: 10.2: Duplicate Results Summary ........................................................................................139 10.3: Matrix Spike Results Summary ...................................................................................140 10.4: Matrix Spike Duplicate Results Summary ..................................................................141 123456789104 of 141 LA58144 SGS North America Inc. Sample Summary ATC Group Services LLC Job No:LA58144 Circle K #2723471-Wilson, NC Project No: Cirk3471SC Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID This report contains results reported as ND = Not detected. The following applies: Organics ND = Not detected above the RL LA58144-1 09/30/19 10:20 RB 10/02/19 SO Soil SB-1 LA58144-1R 09/30/19 10:20 RB 10/02/19 SO Soil SB-1 LA58144-2 09/30/19 10:45 RB 10/02/19 SO Soil SB-2 LA58144-2R 09/30/19 10:45 RB 10/02/19 SO Soil SB-2 LA58144-3 09/30/19 11:00 RB 10/02/19 SO Soil SB-3 LA58144-3R 09/30/19 11:00 RB 10/02/19 SO Soil SB-3 LA58144-4 09/30/19 11:20 RB 10/02/19 SO Soil SB-4 LA58144-4R 09/30/19 11:20 RB 10/02/19 SO Soil SB-4 LA58144-5 09/30/19 11:40 RB 10/02/19 SO Soil SB-5 LA58144-5R 09/30/19 11:40 RB 10/02/19 SO Soil SB-5 LA58144-6 09/30/19 12:00 RB 10/02/19 SO Soil SB-6 LA58144-6R 09/30/19 12:00 RB 10/02/19 SO Soil SB-6 Soil samples reported on a dry weight basis unless otherwise indicated on result page. 5 of 141 LA581441 SGS North America Inc. Sample Summary (continued) ATC Group Services LLC Job No:LA58144 Circle K #2723471-Wilson, NC Project No: Cirk3471SC Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID LA58144-7 09/30/19 12:30 RB 10/02/19 SO Soil SB-7 LA58144-7R 09/30/19 12:30 RB 10/02/19 SO Soil SB-7 LA58144-8 09/30/19 12:50 RB 10/02/19 SO Soil SB-8 LA58144-8R 09/30/19 12:50 RB 10/02/19 SO Soil SB-8 LA58144-9 09/30/19 13:10 RB 10/02/19 SO Soil SB-9 LA58144-9R 09/30/19 13:10 RB 10/02/19 SO Soil SB-9 LA58144-10 09/30/19 13:30 RB 10/02/19 SO Soil SB-10 LA58144-10R 09/30/19 13:30 RB 10/02/19 SO Soil SB-10 LA58144-11 09/30/19 13:45 RB 10/02/19 SO Oil MW-3 Soil samples reported on a dry weight basis unless otherwise indicated on result page. 6 of 141 LA581441 SGS Scott, LA 500 Ambassador Caffery Parkway Scott, LA 70583, USA t +1 (0)337 237 4775 www.sgs.com Member of the SGS Group (SGS SA) SGS IS THE WORLD’S LEADING INSPECTION, VERIFICATION, TESTING AND CERTIFICATION COMPANY. October 17, 2019 ATC Group Services ATTN: Maureen Jackson 2725 East Millbrook Road Suite 121 Raleigh, NC 27604 RE: SGS Job #LA58144 “Circle K #2723471-Wilson, NC“ Dear Ms. Jackson, The sample MW-3 collected on September 30, 2019 at 13:45 was analyzed for GC Fingerprint by method 8015C. The laboratory director reviewed the resulting chromatograms and determined that the hydrocarbon pattern was in the TPH-Diesel Range Organics (TPH-DRO) range of C10-C28. The absence of the prominent n-alkane peaks suggests severely weathered diesel of some type or refined mineral oil with components in the TPH-DRO range. The chromatograms are included in the laboratory report for your review. Sincerely, Amy Jackson Environment, Health and Safety Project Manager SGS-Scott 7 of 141 LA581442 Quantitation Report (QT Reviewed) Data File : Z:\GCSEMI\DATA\GCLG\191010\LG001326.D Vial: 84 Acq On : 11-Oct-2019, 14:09:00 Operator: PENNYC Sample : LA58144-11, Fing Inst : HP5890 Misc : OP15325,GLG886,1,,,10,1 Multiplr: 1.00 IntFile : AUTOINT1.E Quant Time: Oct 16 08:59:44 2019 Quant Results File: 190731ADRO_A.RES Quant Method : Z:\GCSEMI\D...\190731ADRO_A.M (Chemstation Integrator) Title : Diesel range organics by method 8015. Last Update : Mon Aug 19 10:32:40 2019 Response via : Initial Calibration DataAcq Meth : DRORCR.M Volume Inj. : Signal Phase : Signal Info : Compound R.T. Response Conc Units ------------------------------------------------------------------------- System Monitoring Compounds 7) S O-TERPHENYL 0.00 0 N.D. ppm Target Compounds 1) H TPH-ORO (C20-C34) 6.35 1843438083 BelowCal ppm 2) H ORO (C20-C28) 5.65 1887536097 30332.189 ppm 3) H DRO (C10-C20) 3.67 5841277728 81013.493 ppm 4) H DRO C10-C28 4.42 7761708181 107648.210 ppm 5) H ORO (C28-C35) 7.24 30596280 405.381 ppm 6) H TPH-ORO (>C28-C40) 8.25 36454454 497.517 ppm ----------------------------------------------------------------------------- (f)=RT Delta > 1/2 Window (m)=manual int. LG001326.D 190731ADRO_A.M Wed Oct 16 09:00:35 2019 Page 1 8 of 141 LA581442 Quantitation Report (QT Reviewed) Data File : Z:\GCSEMI\DATA\GCLG\191010\LG001326.D Vial: 84 Acq On : 11-Oct-2019, 14:09:00 Operator: PENNYC Sample : LA58144-11, Fing Inst : HP5890 Misc : OP15325,GLG886,1,,,10,1 Multiplr: 1.00 IntFile : AUTOINT1.E Quant Time: Oct 16 9:00 2019 Quant Results File: 190731ADRO_A.RES Quant Method : Z:\GCSEMI\D...\190731ADRO_A.M (Chemstation Integrator) Title : Diesel range organics by method 8015. Last Update : Mon Aug 19 10:32:40 2019 Response via : Multiple Level Calibration DataAcq Meth : DRORCR.M Volume Inj. : Signal Phase : Signal Info : 0.00 1.00 2.00 3.00 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 -1500000 -1000000 -500000 0 500000 1000000 1500000 2000000 2500000 3000000 3500000 4000000 4500000 5000000 5500000 6000000 6500000 7000000 7500000 8000000 8500000 9000000 9500000 Time Response_TIC: FID2B.CH 4.10 4.89 6.47TPH-ORO (>ORO (C28-CORO (C20-CDRO C10-C2DRO (C10-CLG001326.D 190731ADRO_A.M Wed Oct 16 09:00:35 2019 Page 2 9 of 141 LA581442 #1 TPH-ORO (C20-C34) R.T.: 6.350 min Delta R.T.: 0.000 min Response: 1843438083 Conc: N.D. 5.40 5.60 5.80 6.00 6.20 6.40 6.60 6.80 7.00 7.20 0 1000000 2000000 3000000 Time Response_TIC: FID2B.CH + #2 ORO (C20-C28) R.T.: 5.650 min Delta R.T.: 0.000 min Response: 1887536097 Conc: 30332.19 ppm m 4.50 5.00 5.50 6.00 6.50 0 2000000 4000000 6000000 Time Response_TIC: FID2B.CH 4.89 + #3 DRO (C10-C20) R.T.: 3.665 min Delta R.T.: 0.000 min Response: 5841277728 Conc: 81013.49 ppm m 2.00 2.50 3.00 3.50 4.00 4.50 5.00 0 2000000 4000000 6000000 Time Response_TIC: FID2B.CH 4.10 + #4 DRO C10-C28 R.T.: 4.425 min Delta R.T.: 0.000 min Response: 7761708181 Conc: 107648.21 ppm m 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 0 2000000 4000000 6000000 Time Response_TIC: FID2B.CH 4.10 + LG001326.D 190731ADRO_A.M Wed Oct 16 09:00:35 2019 Page 3 10 of 141 LA581442 #5 ORO (C28-C35) R.T.: 7.240 min Delta R.T.: 0.000 min Response: 30596280 Conc: 405.38 ppm m 6.00 6.50 7.00 7.50 8.00 0 200000 400000 600000 800000 1000000 Time Response_TIC: FID2B.CH 6.47 + #6 TPH-ORO (>C28-C40) R.T.: 8.250 min Delta R.T.: 0.000 min Response: 36454454 Conc: 497.52 ppm m 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 0 200000 400000 600000 800000 1000000 Time Response_TIC: FID2B.CH 6.47 + LG001326.D 190731ADRO_A.M Wed Oct 16 09:00:35 2019 Page 4 11 of 141 LA581442 Summary of Hits Page 1 of 3 Job Number:LA58144 Account:ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Collected:09/30/19 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method LA58144-1 SB-1 Acetone 126 71 ug/kg SW846 8260D LA58144-1R SB-1 C9-C18 Aliphatics a 19900 3400 ug/kg MADEP EPH REV 1.1 C19-C36 Aliphatics a 3410 3400 ug/kg MADEP EPH REV 1.1 LA58144-2 SB-2 n-Butylbenzene 5.6 5.6 ug/kg SW846 8260D Naphthalene 9.6 5.6 ug/kg SW846 8260D TPH-GRO (C6-C10)10.5 8.0 mg/kg SW846 8015C LA58144-2R SB-2 1-Methylnaphthalene a 33.1 12 ug/kg SW846 8270E 2-Methylnaphthalene a 31.2 12 ug/kg SW846 8270E Phenanthrene a 22.0 12 ug/kg SW846 8270E Pyrene a 28.5 12 ug/kg SW846 8270E C11-C22 Aromatics (Unadj.) a 64100 3000 ug/kg MADEP EPH REV 1.1 C9-C18 Aliphatics a 170000 3000 ug/kg MADEP EPH REV 1.1 C19-C36 Aliphatics a 74000 3000 ug/kg MADEP EPH REV 1.1 LA58144-3 SB-3 Acetone 99.0 51 ug/kg SW846 8260D LA58144-3R SB-3 No hits reported in this sample. LA58144-4 SB-4 No hits reported in this sample. LA58144-4R SB-4 No hits reported in this sample. LA58144-5 SB-5 Benzene 0.56 0.56 ug/kg SW846 8260D 12 of 141 LA581443 Summary of Hits Page 2 of 3 Job Number:LA58144 Account:ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Collected:09/30/19 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method LA58144-5R SB-5 No hits reported in this sample. LA58144-6 SB-6 No hits reported in this sample. LA58144-6R SB-6 No hits reported in this sample. LA58144-7 SB-7 Acetone 91.8 55 ug/kg SW846 8260D LA58144-7R SB-7 C11-C22 Aromatics (Unadj.) a 3510 3000 ug/kg MADEP EPH REV 1.1 LA58144-8 SB-8 No hits reported in this sample. LA58144-8R SB-8 No hits reported in this sample. LA58144-9 SB-9 No hits reported in this sample. LA58144-9R SB-9 No hits reported in this sample. LA58144-10 SB-10 No hits reported in this sample. LA58144-10R SB-10 No hits reported in this sample. 13 of 141 LA581443 Summary of Hits Page 3 of 3 Job Number:LA58144 Account:ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Collected:09/30/19 Lab Sample ID Client Sample ID Result/ Analyte Qual RL MDL Units Method LA58144-11 MW-3 TPH-GRO (C6-C10)166000 10000 mg/kg SW846 8015C (a) Sample extracted beyond hold time per client request. 14 of 141 LA581443 SGS North America Inc. Sample Results Report of Analysis Scott, LA Section 4 15 of 141 LA581444 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-1 Lab Sample ID:LA58144-1 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058557.D 1 10/05/19 13:46 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 4.9 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone 126 71 ug/kg 71-43-2 Benzene ND 0.71 ug/kg 108-86-1 Bromobenzene ND 1.4 ug/kg 74-97-5 Bromochloromethane ND 1.4 ug/kg 75-27-4 Bromodichloromethane ND 1.4 ug/kg 75-25-2 Bromoform ND 1.4 ug/kg 104-51-8 n-Butylbenzene ND 7.1 ug/kg 135-98-8 sec-Butylbenzene ND 7.1 ug/kg 98-06-6 tert-Butylbenzene ND 1.4 ug/kg 56-23-5 Carbon Tetrachloride ND 1.4 ug/kg 108-90-7 Chlorobenzene ND 1.4 ug/kg 75-00-3 Chloroethane ND 1.4 ug/kg 67-66-3 Chloroform ND 1.4 ug/kg 95-49-8 o-Chlorotoluene ND 7.1 ug/kg 106-43-4 p-Chlorotoluene ND 7.1 ug/kg 124-48-1 Dibromochloromethane ND 1.4 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 7.1 ug/kg 106-93-4 1,2-Dibromoethane ND 1.4 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.4 ug/kg 541-73-1 m-Dichlorobenzene ND 1.4 ug/kg 95-50-1 o-Dichlorobenzene ND 1.4 ug/kg 106-46-7 p-Dichlorobenzene ND 1.4 ug/kg 75-34-3 1,1-Dichloroethane ND 1.4 ug/kg 107-06-2 1,2-Dichloroethane ND 1.4 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.4 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.4 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.4 ug/kg 78-87-5 1,2-Dichloropropane ND 1.4 ug/kg 142-28-9 1,3-Dichloropropane ND 1.4 ug/kg 594-20-7 2,2-Dichloropropane ND 1.4 ug/kg 563-58-6 1,1-Dichloropropene ND 1.4 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.4 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 16 of 141 LA5814444.1 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-1 Lab Sample ID:LA58144-1 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.4 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.4 ug/kg 64-17-5 Ethyl Alcohol ND 570 ug/kg 100-41-4 Ethylbenzene ND 1.4 ug/kg 591-78-6 2-Hexanone ND 18 ug/kg 87-68-3 Hexachlorobutadiene ND 7.1 ug/kg 98-82-8 Isopropylbenzene ND 7.1 ug/kg 99-87-6 p-Isopropyltoluene ND 7.1 ug/kg 74-83-9 Methyl Bromide ND 14 ug/kg 74-87-3 Methyl Chloride ND 7.1 ug/kg 74-95-3 Methylene Bromide ND 1.4 ug/kg 75-09-2 Methylene Chloride ND 7.1 ug/kg 78-93-3 Methyl Ethyl Ketone ND 18 ug/kg 108-10-1 4-Methyl-2-pentanone ND 18 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.4 ug/kg 91-20-3 Naphthalene ND 7.1 ug/kg 103-65-1 n-Propylbenzene ND 7.1 ug/kg 100-42-5 Styrene ND 1.4 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.4 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.4 ug/kg 127-18-4 Tetrachloroethylene ND 1.4 ug/kg 108-88-3 Toluene ND 7.1 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 7.1 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 7.1 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.4 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.4 ug/kg 79-01-6 Trichloroethylene ND 1.4 ug/kg 75-69-4 Trichlorofluoromethane ND 1.4 ug/kg 96-18-4 1,2,3-Trichloropropane ND 7.1 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 7.1 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 7.1 ug/kg 108-05-4 Vinyl Acetate ND 7.1 ug/kg 75-01-4 Vinyl Chloride ND 1.4 ug/kg m,p-Xylene ND 2.9 ug/kg 95-47-6 o-Xylene ND 1.4 ug/kg 1330-20-7 Xylene (total)ND 2.9 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 124%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 17 of 141 LA5814444.1 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-1 Lab Sample ID:LA58144-1 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 104%52-159% 460-00-4 4-Bromofluorobenzene 103%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 18 of 141 LA5814444.1 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-1 Lab Sample ID:LA58144-1 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346243.D 1 10/05/19 14:21 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.50 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 9.7 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 91%63-139% 540-36-3 1,4-Difluorobenzene 88%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 19 of 141 LA5814444.1 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-1 Lab Sample ID:LA58144-1R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051843.D 1 10/24/19 23:17 PC 10/22/19 08:45 OP15444 EC2063 Run #2 Initial Weight Final Volume Run #1 20.3 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid b ND 1400 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 230 ug/kg 95-57-8 2-Chlorophenol ND 230 ug/kg 120-83-2 2,4-Dichlorophenol ND 230 ug/kg 105-67-9 2,4-Dimethylphenol ND 230 ug/kg 51-28-5 2,4-Dinitrophenol ND 910 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 230 ug/kg 95-48-7 2-Methylphenol ND 230 ug/kg 3&4-Methylphenol ND 230 ug/kg 88-75-5 2-Nitrophenol ND 230 ug/kg 100-02-7 4-Nitrophenol ND 910 ug/kg 87-86-5 Pentachlorophenol ND 230 ug/kg 108-95-2 Phenol ND 230 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 230 ug/kg 83-32-9 Acenaphthene ND 14 ug/kg 208-96-8 Acenaphthylene ND 14 ug/kg 120-12-7 Anthracene ND 14 ug/kg 56-55-3 Benzo(a)anthracene ND 14 ug/kg 50-32-8 Benzo(a)pyrene ND 14 ug/kg 205-99-2 Benzo(b)fluoranthene ND 14 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 14 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 230 ug/kg 100-51-6 Benzyl Alcohol ND 230 ug/kg 207-08-9 Benzo(k)fluoranthene ND 14 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 230 ug/kg 106-47-8 4-Chloroaniline ND 230 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 230 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 230 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 230 ug/kg 91-58-7 2-Chloronaphthalene ND 230 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 230 ug/kg 218-01-9 Chrysene ND 14 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 20 of 141 LA5814444.2 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-1 Lab Sample ID:LA58144-1R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 14 ug/kg 132-64-9 Dibenzofuran ND 230 ug/kg 95-50-1 1,2-Dichlorobenzene ND 230 ug/kg 541-73-1 1,3-Dichlorobenzene ND 230 ug/kg 106-46-7 1,4-Dichlorobenzene ND 230 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 230 ug/kg 84-66-2 Diethyl Phthalate ND 230 ug/kg 131-11-3 Dimethyl Phthalate ND 230 ug/kg 84-74-2 Di-n-butyl Phthalate ND 230 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 230 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 230 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 230 ug/kg 206-44-0 Fluoranthene ND 14 ug/kg 86-73-7 Fluorene ND 14 ug/kg 118-74-1 Hexachlorobenzene ND 230 ug/kg 87-68-3 Hexachlorobutadiene ND 230 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 910 ug/kg 67-72-1 Hexachloroethane ND 230 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 14 ug/kg 78-59-1 Isophorone ND 230 ug/kg 90-12-0 1-Methylnaphthalene ND 14 ug/kg 91-57-6 2-Methylnaphthalene ND 14 ug/kg 91-20-3 Naphthalene ND 14 ug/kg 98-95-3 Nitrobenzene ND 230 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 230 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 230 ug/kg 85-01-8 Phenanthrene ND 14 ug/kg 129-00-0 Pyrene ND 14 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 230 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 65%25-109% 4165-62-2 Phenol-d5 68%30-110% 118-79-6 2,4,6-Tribromophenol 80%27-127% 4165-60-0 Nitrobenzene-d5 60%24-123% 321-60-8 2-Fluorobiphenyl 56%32-112% 1718-51-0 Terphenyl-d14 69%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 21 of 141 LA5814444.2 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-1 Lab Sample ID:LA58144-1R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 22 of 141 LA5814444.2 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-1 Lab Sample ID:LA58144-1R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012462M.D 1 10/29/19 12:43 PC 10/22/19 08:45 OP15446 GLB2117 Run #2 a Y0012462M.D 1 10/29/19 12:44 PC 10/22/19 08:45 OP15446 GLB2118 Initial Weight Final Volume Run #1 20.5 g 10.0 ml Run #2 20.5 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 3400 ug/kg C9-C18 Aliphatics 19900 b 3400 ug/kg C19-C36 Aliphatics 3410 b 3400 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 86%40-140% 84-15-1 o-Terphenyl 85%40-140% 321-60-8 2-Fluorobiphenyl 75%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 23 of 141 LA5814444.2 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-1 Lab Sample ID:LA58144-1R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:71.6 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 24 of 141 LA5814444.2 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-2 Lab Sample ID:LA58144-2 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058558.D 1 10/05/19 14:10 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 5.4 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 56 ug/kg 71-43-2 Benzene ND 0.56 ug/kg 108-86-1 Bromobenzene ND 1.1 ug/kg 74-97-5 Bromochloromethane ND 1.1 ug/kg 75-27-4 Bromodichloromethane ND 1.1 ug/kg 75-25-2 Bromoform ND 1.1 ug/kg 104-51-8 n-Butylbenzene 5.6 5.6 ug/kg 135-98-8 sec-Butylbenzene ND 5.6 ug/kg 98-06-6 tert-Butylbenzene ND 1.1 ug/kg 56-23-5 Carbon Tetrachloride ND 1.1 ug/kg 108-90-7 Chlorobenzene ND 1.1 ug/kg 75-00-3 Chloroethane ND 1.1 ug/kg 67-66-3 Chloroform ND 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.6 ug/kg 106-43-4 p-Chlorotoluene ND 5.6 ug/kg 124-48-1 Dibromochloromethane ND 1.1 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.6 ug/kg 106-93-4 1,2-Dibromoethane ND 1.1 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.1 ug/kg 541-73-1 m-Dichlorobenzene ND 1.1 ug/kg 95-50-1 o-Dichlorobenzene ND 1.1 ug/kg 106-46-7 p-Dichlorobenzene ND 1.1 ug/kg 75-34-3 1,1-Dichloroethane ND 1.1 ug/kg 107-06-2 1,2-Dichloroethane ND 1.1 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.1 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.1 ug/kg 78-87-5 1,2-Dichloropropane ND 1.1 ug/kg 142-28-9 1,3-Dichloropropane ND 1.1 ug/kg 594-20-7 2,2-Dichloropropane ND 1.1 ug/kg 563-58-6 1,1-Dichloropropene ND 1.1 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.1 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 25 of 141 LA5814444.3 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-2 Lab Sample ID:LA58144-2 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.1 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.1 ug/kg 64-17-5 Ethyl Alcohol ND 450 ug/kg 100-41-4 Ethylbenzene ND 1.1 ug/kg 591-78-6 2-Hexanone ND 14 ug/kg 87-68-3 Hexachlorobutadiene ND 5.6 ug/kg 98-82-8 Isopropylbenzene ND 5.6 ug/kg 99-87-6 p-Isopropyltoluene ND 5.6 ug/kg 74-83-9 Methyl Bromide ND 11 ug/kg 74-87-3 Methyl Chloride ND 5.6 ug/kg 74-95-3 Methylene Bromide ND 1.1 ug/kg 75-09-2 Methylene Chloride ND 5.6 ug/kg 78-93-3 Methyl Ethyl Ketone ND 14 ug/kg 108-10-1 4-Methyl-2-pentanone ND 14 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.1 ug/kg 91-20-3 Naphthalene 9.6 5.6 ug/kg 103-65-1 n-Propylbenzene ND 5.6 ug/kg 100-42-5 Styrene ND 1.1 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.1 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.1 ug/kg 127-18-4 Tetrachloroethylene ND 1.1 ug/kg 108-88-3 Toluene ND 5.6 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.6 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.6 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.1 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.1 ug/kg 79-01-6 Trichloroethylene ND 1.1 ug/kg 75-69-4 Trichlorofluoromethane ND 1.1 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.6 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.6 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.6 ug/kg 108-05-4 Vinyl Acetate ND 5.6 ug/kg 75-01-4 Vinyl Chloride ND 1.1 ug/kg m,p-Xylene ND 2.2 ug/kg 95-47-6 o-Xylene ND 1.1 ug/kg 1330-20-7 Xylene (total)ND 2.2 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 116%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 26 of 141 LA5814444.3 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-2 Lab Sample ID:LA58144-2 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 111%52-159% 460-00-4 4-Bromofluorobenzene 110%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 27 of 141 LA5814444.3 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-2 Lab Sample ID:LA58144-2 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346253.D 1 10/05/19 16:14 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.40 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)10.5 8.0 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 90%63-139% 540-36-3 1,4-Difluorobenzene 88%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 28 of 141 LA5814444.3 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-2 Lab Sample ID:LA58144-2R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051844.D 1 10/24/19 23:39 PC 10/22/19 08:45 OP15444 EC2063 Run #2 Initial Weight Final Volume Run #1 20.5 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid b ND 1200 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 200 ug/kg 95-57-8 2-Chlorophenol ND 200 ug/kg 120-83-2 2,4-Dichlorophenol ND 200 ug/kg 105-67-9 2,4-Dimethylphenol ND 200 ug/kg 51-28-5 2,4-Dinitrophenol ND 780 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 200 ug/kg 95-48-7 2-Methylphenol ND 200 ug/kg 3&4-Methylphenol ND 200 ug/kg 88-75-5 2-Nitrophenol ND 200 ug/kg 100-02-7 4-Nitrophenol ND 780 ug/kg 87-86-5 Pentachlorophenol ND 200 ug/kg 108-95-2 Phenol ND 200 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 200 ug/kg 83-32-9 Acenaphthene ND 12 ug/kg 208-96-8 Acenaphthylene ND 12 ug/kg 120-12-7 Anthracene ND 12 ug/kg 56-55-3 Benzo(a)anthracene ND 12 ug/kg 50-32-8 Benzo(a)pyrene ND 12 ug/kg 205-99-2 Benzo(b)fluoranthene ND 12 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 12 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 200 ug/kg 100-51-6 Benzyl Alcohol ND 200 ug/kg 207-08-9 Benzo(k)fluoranthene ND 12 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 200 ug/kg 106-47-8 4-Chloroaniline ND 200 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 200 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 200 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 200 ug/kg 91-58-7 2-Chloronaphthalene ND 200 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 200 ug/kg 218-01-9 Chrysene ND 12 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 29 of 141 LA5814444.4 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-2 Lab Sample ID:LA58144-2R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 12 ug/kg 132-64-9 Dibenzofuran ND 200 ug/kg 95-50-1 1,2-Dichlorobenzene ND 200 ug/kg 541-73-1 1,3-Dichlorobenzene ND 200 ug/kg 106-46-7 1,4-Dichlorobenzene ND 200 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 200 ug/kg 84-66-2 Diethyl Phthalate ND 200 ug/kg 131-11-3 Dimethyl Phthalate ND 200 ug/kg 84-74-2 Di-n-butyl Phthalate ND 200 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 200 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 200 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 200 ug/kg 206-44-0 Fluoranthene ND 12 ug/kg 86-73-7 Fluorene ND 12 ug/kg 118-74-1 Hexachlorobenzene ND 200 ug/kg 87-68-3 Hexachlorobutadiene ND 200 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 780 ug/kg 67-72-1 Hexachloroethane ND 200 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 12 ug/kg 78-59-1 Isophorone ND 200 ug/kg 90-12-0 1-Methylnaphthalene 33.1 12 ug/kg 91-57-6 2-Methylnaphthalene 31.2 12 ug/kg 91-20-3 Naphthalene ND 12 ug/kg 98-95-3 Nitrobenzene ND 200 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 200 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 200 ug/kg 85-01-8 Phenanthrene 22.0 12 ug/kg 129-00-0 Pyrene 28.5 12 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 200 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 53%25-109% 4165-62-2 Phenol-d5 55%30-110% 118-79-6 2,4,6-Tribromophenol 61%27-127% 4165-60-0 Nitrobenzene-d5 48%24-123% 321-60-8 2-Fluorobiphenyl 46%32-112% 1718-51-0 Terphenyl-d14 54%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 30 of 141 LA5814444.4 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-2 Lab Sample ID:LA58144-2R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 31 of 141 LA5814444.4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-2 Lab Sample ID:LA58144-2R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012430M.D 1 10/27/19 03:05 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012430M.D 1 10/27/19 03:06 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.3 g 10.0 ml Run #2 20.3 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)64100 3000 ug/kg C9-C18 Aliphatics 170000 b 3000 ug/kg C19-C36 Aliphatics 74000 b 3000 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 92%40-140% 84-15-1 o-Terphenyl 106%40-140% 321-60-8 2-Fluorobiphenyl 73%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 32 of 141 LA5814444.4 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-2 Lab Sample ID:LA58144-2R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 33 of 141 LA5814444.4 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-3 Lab Sample ID:LA58144-3 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058559.D 1 10/05/19 14:35 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 5.8 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone 99.0 51 ug/kg 71-43-2 Benzene ND 0.51 ug/kg 108-86-1 Bromobenzene ND 1.0 ug/kg 74-97-5 Bromochloromethane ND 1.0 ug/kg 75-27-4 Bromodichloromethane ND 1.0 ug/kg 75-25-2 Bromoform ND 1.0 ug/kg 104-51-8 n-Butylbenzene ND 5.1 ug/kg 135-98-8 sec-Butylbenzene ND 5.1 ug/kg 98-06-6 tert-Butylbenzene ND 1.0 ug/kg 56-23-5 Carbon Tetrachloride ND 1.0 ug/kg 108-90-7 Chlorobenzene ND 1.0 ug/kg 75-00-3 Chloroethane ND 1.0 ug/kg 67-66-3 Chloroform ND 1.0 ug/kg 95-49-8 o-Chlorotoluene ND 5.1 ug/kg 106-43-4 p-Chlorotoluene ND 5.1 ug/kg 124-48-1 Dibromochloromethane ND 1.0 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.1 ug/kg 106-93-4 1,2-Dibromoethane ND 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.0 ug/kg 541-73-1 m-Dichlorobenzene ND 1.0 ug/kg 95-50-1 o-Dichlorobenzene ND 1.0 ug/kg 106-46-7 p-Dichlorobenzene ND 1.0 ug/kg 75-34-3 1,1-Dichloroethane ND 1.0 ug/kg 107-06-2 1,2-Dichloroethane ND 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.0 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.0 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 1.0 ug/kg 142-28-9 1,3-Dichloropropane ND 1.0 ug/kg 594-20-7 2,2-Dichloropropane ND 1.0 ug/kg 563-58-6 1,1-Dichloropropene ND 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.0 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 34 of 141 LA5814444.5 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-3 Lab Sample ID:LA58144-3 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.0 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.0 ug/kg 64-17-5 Ethyl Alcohol ND 400 ug/kg 100-41-4 Ethylbenzene ND 1.0 ug/kg 591-78-6 2-Hexanone ND 13 ug/kg 87-68-3 Hexachlorobutadiene ND 5.1 ug/kg 98-82-8 Isopropylbenzene ND 5.1 ug/kg 99-87-6 p-Isopropyltoluene ND 5.1 ug/kg 74-83-9 Methyl Bromide ND 10 ug/kg 74-87-3 Methyl Chloride ND 5.1 ug/kg 74-95-3 Methylene Bromide ND 1.0 ug/kg 75-09-2 Methylene Chloride ND 5.1 ug/kg 78-93-3 Methyl Ethyl Ketone ND 13 ug/kg 108-10-1 4-Methyl-2-pentanone ND 13 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/kg 91-20-3 Naphthalene ND 5.1 ug/kg 103-65-1 n-Propylbenzene ND 5.1 ug/kg 100-42-5 Styrene ND 1.0 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 1.0 ug/kg 108-88-3 Toluene ND 5.1 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.1 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.1 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.0 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.0 ug/kg 79-01-6 Trichloroethylene ND 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 1.0 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.1 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.1 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.1 ug/kg 108-05-4 Vinyl Acetate ND 5.1 ug/kg 75-01-4 Vinyl Chloride ND 1.0 ug/kg m,p-Xylene ND 2.0 ug/kg 95-47-6 o-Xylene ND 1.0 ug/kg 1330-20-7 Xylene (total)ND 2.0 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 96%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 35 of 141 LA5814444.5 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-3 Lab Sample ID:LA58144-3 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 103%52-159% 460-00-4 4-Bromofluorobenzene 104%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 36 of 141 LA5814444.5 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-3 Lab Sample ID:LA58144-3 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346255.D 1 10/05/19 16:36 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.20 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 6.5 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 91%63-139% 540-36-3 1,4-Difluorobenzene 89%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 37 of 141 LA5814444.5 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-3 Lab Sample ID:LA58144-3R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051845.D 1 10/25/19 00:01 PC 10/22/19 08:45 OP15444 EC2063 Run #2 Initial Weight Final Volume Run #1 20.4 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid b ND 1200 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 200 ug/kg 95-57-8 2-Chlorophenol ND 200 ug/kg 120-83-2 2,4-Dichlorophenol ND 200 ug/kg 105-67-9 2,4-Dimethylphenol ND 200 ug/kg 51-28-5 2,4-Dinitrophenol ND 760 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 200 ug/kg 95-48-7 2-Methylphenol ND 200 ug/kg 3&4-Methylphenol ND 200 ug/kg 88-75-5 2-Nitrophenol ND 200 ug/kg 100-02-7 4-Nitrophenol ND 760 ug/kg 87-86-5 Pentachlorophenol ND 200 ug/kg 108-95-2 Phenol ND 200 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 200 ug/kg 83-32-9 Acenaphthene ND 12 ug/kg 208-96-8 Acenaphthylene ND 12 ug/kg 120-12-7 Anthracene ND 12 ug/kg 56-55-3 Benzo(a)anthracene ND 12 ug/kg 50-32-8 Benzo(a)pyrene ND 12 ug/kg 205-99-2 Benzo(b)fluoranthene ND 12 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 12 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 200 ug/kg 100-51-6 Benzyl Alcohol ND 200 ug/kg 207-08-9 Benzo(k)fluoranthene ND 12 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 200 ug/kg 106-47-8 4-Chloroaniline ND 200 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 200 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 200 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 200 ug/kg 91-58-7 2-Chloronaphthalene ND 200 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 200 ug/kg 218-01-9 Chrysene ND 12 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 38 of 141 LA5814444.6 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-3 Lab Sample ID:LA58144-3R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 12 ug/kg 132-64-9 Dibenzofuran ND 200 ug/kg 95-50-1 1,2-Dichlorobenzene ND 200 ug/kg 541-73-1 1,3-Dichlorobenzene ND 200 ug/kg 106-46-7 1,4-Dichlorobenzene ND 200 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 200 ug/kg 84-66-2 Diethyl Phthalate ND 200 ug/kg 131-11-3 Dimethyl Phthalate ND 200 ug/kg 84-74-2 Di-n-butyl Phthalate ND 200 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 200 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 200 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 200 ug/kg 206-44-0 Fluoranthene ND 12 ug/kg 86-73-7 Fluorene ND 12 ug/kg 118-74-1 Hexachlorobenzene ND 200 ug/kg 87-68-3 Hexachlorobutadiene ND 200 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 760 ug/kg 67-72-1 Hexachloroethane ND 200 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 12 ug/kg 78-59-1 Isophorone ND 200 ug/kg 90-12-0 1-Methylnaphthalene ND 12 ug/kg 91-57-6 2-Methylnaphthalene ND 12 ug/kg 91-20-3 Naphthalene ND 12 ug/kg 98-95-3 Nitrobenzene ND 200 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 200 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 200 ug/kg 85-01-8 Phenanthrene ND 12 ug/kg 129-00-0 Pyrene ND 12 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 200 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 65%25-109% 4165-62-2 Phenol-d5 67%30-110% 118-79-6 2,4,6-Tribromophenol 82%27-127% 4165-60-0 Nitrobenzene-d5 61%24-123% 321-60-8 2-Fluorobiphenyl 57%32-112% 1718-51-0 Terphenyl-d14 74%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 39 of 141 LA5814444.6 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-3 Lab Sample ID:LA58144-3R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 40 of 141 LA5814444.6 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-3 Lab Sample ID:LA58144-3R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012431M.D 1 10/27/19 03:28 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012431M.D 1 10/27/19 03:29 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.0 g 10.0 ml Run #2 20.0 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 2900 ug/kg C9-C18 Aliphatics ND b 2900 ug/kg C19-C36 Aliphatics ND b 2900 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 84%40-140% 84-15-1 o-Terphenyl 81%40-140% 321-60-8 2-Fluorobiphenyl 71%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 41 of 141 LA5814444.6 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-3 Lab Sample ID:LA58144-3R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:85.2 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 42 of 141 LA5814444.6 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-4 Lab Sample ID:LA58144-4 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058560.D 1 10/05/19 15:00 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 5.6 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 53 ug/kg 71-43-2 Benzene ND 0.53 ug/kg 108-86-1 Bromobenzene ND 1.1 ug/kg 74-97-5 Bromochloromethane ND 1.1 ug/kg 75-27-4 Bromodichloromethane ND 1.1 ug/kg 75-25-2 Bromoform ND 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.3 ug/kg 135-98-8 sec-Butylbenzene ND 5.3 ug/kg 98-06-6 tert-Butylbenzene ND 1.1 ug/kg 56-23-5 Carbon Tetrachloride ND 1.1 ug/kg 108-90-7 Chlorobenzene ND 1.1 ug/kg 75-00-3 Chloroethane ND 1.1 ug/kg 67-66-3 Chloroform ND 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.3 ug/kg 106-43-4 p-Chlorotoluene ND 5.3 ug/kg 124-48-1 Dibromochloromethane ND 1.1 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.3 ug/kg 106-93-4 1,2-Dibromoethane ND 1.1 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.1 ug/kg 541-73-1 m-Dichlorobenzene ND 1.1 ug/kg 95-50-1 o-Dichlorobenzene ND 1.1 ug/kg 106-46-7 p-Dichlorobenzene ND 1.1 ug/kg 75-34-3 1,1-Dichloroethane ND 1.1 ug/kg 107-06-2 1,2-Dichloroethane ND 1.1 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.1 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.1 ug/kg 78-87-5 1,2-Dichloropropane ND 1.1 ug/kg 142-28-9 1,3-Dichloropropane ND 1.1 ug/kg 594-20-7 2,2-Dichloropropane ND 1.1 ug/kg 563-58-6 1,1-Dichloropropene ND 1.1 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.1 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 43 of 141 LA5814444.7 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-4 Lab Sample ID:LA58144-4 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.1 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.1 ug/kg 64-17-5 Ethyl Alcohol ND 430 ug/kg 100-41-4 Ethylbenzene ND 1.1 ug/kg 591-78-6 2-Hexanone ND 13 ug/kg 87-68-3 Hexachlorobutadiene ND 5.3 ug/kg 98-82-8 Isopropylbenzene ND 5.3 ug/kg 99-87-6 p-Isopropyltoluene ND 5.3 ug/kg 74-83-9 Methyl Bromide ND 11 ug/kg 74-87-3 Methyl Chloride ND 5.3 ug/kg 74-95-3 Methylene Bromide ND 1.1 ug/kg 75-09-2 Methylene Chloride ND 5.3 ug/kg 78-93-3 Methyl Ethyl Ketone ND 13 ug/kg 108-10-1 4-Methyl-2-pentanone ND 13 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.1 ug/kg 91-20-3 Naphthalene ND 5.3 ug/kg 103-65-1 n-Propylbenzene ND 5.3 ug/kg 100-42-5 Styrene ND 1.1 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.1 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.1 ug/kg 127-18-4 Tetrachloroethylene ND 1.1 ug/kg 108-88-3 Toluene ND 5.3 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.3 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.3 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.1 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.1 ug/kg 79-01-6 Trichloroethylene ND 1.1 ug/kg 75-69-4 Trichlorofluoromethane ND 1.1 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.3 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.3 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.3 ug/kg 108-05-4 Vinyl Acetate ND 5.3 ug/kg 75-01-4 Vinyl Chloride ND 1.1 ug/kg m,p-Xylene ND 2.1 ug/kg 95-47-6 o-Xylene ND 1.1 ug/kg 1330-20-7 Xylene (total)ND 2.1 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 100%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 44 of 141 LA5814444.7 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-4 Lab Sample ID:LA58144-4 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 102%52-159% 460-00-4 4-Bromofluorobenzene 105%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 45 of 141 LA5814444.7 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-4 Lab Sample ID:LA58144-4 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346257.D 1 10/05/19 16:59 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.10 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 6.8 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 92%63-139% 540-36-3 1,4-Difluorobenzene 89%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 46 of 141 LA5814444.7 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-4 Lab Sample ID:LA58144-4R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051846.D 1 10/25/19 00:22 PC 10/22/19 08:45 OP15444 EC2063 Run #2 Initial Weight Final Volume Run #1 20.1 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid b ND 1200 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 200 ug/kg 95-57-8 2-Chlorophenol ND 200 ug/kg 120-83-2 2,4-Dichlorophenol ND 200 ug/kg 105-67-9 2,4-Dimethylphenol ND 200 ug/kg 51-28-5 2,4-Dinitrophenol ND 780 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 200 ug/kg 95-48-7 2-Methylphenol ND 200 ug/kg 3&4-Methylphenol ND 200 ug/kg 88-75-5 2-Nitrophenol ND 200 ug/kg 100-02-7 4-Nitrophenol ND 780 ug/kg 87-86-5 Pentachlorophenol ND 200 ug/kg 108-95-2 Phenol ND 200 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 200 ug/kg 83-32-9 Acenaphthene ND 12 ug/kg 208-96-8 Acenaphthylene ND 12 ug/kg 120-12-7 Anthracene ND 12 ug/kg 56-55-3 Benzo(a)anthracene ND 12 ug/kg 50-32-8 Benzo(a)pyrene ND 12 ug/kg 205-99-2 Benzo(b)fluoranthene ND 12 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 12 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 200 ug/kg 100-51-6 Benzyl Alcohol ND 200 ug/kg 207-08-9 Benzo(k)fluoranthene ND 12 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 200 ug/kg 106-47-8 4-Chloroaniline ND 200 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 200 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 200 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 200 ug/kg 91-58-7 2-Chloronaphthalene ND 200 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 200 ug/kg 218-01-9 Chrysene ND 12 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 47 of 141 LA5814444.8 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-4 Lab Sample ID:LA58144-4R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 12 ug/kg 132-64-9 Dibenzofuran ND 200 ug/kg 95-50-1 1,2-Dichlorobenzene ND 200 ug/kg 541-73-1 1,3-Dichlorobenzene ND 200 ug/kg 106-46-7 1,4-Dichlorobenzene ND 200 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 200 ug/kg 84-66-2 Diethyl Phthalate ND 200 ug/kg 131-11-3 Dimethyl Phthalate ND 200 ug/kg 84-74-2 Di-n-butyl Phthalate ND 200 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 200 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 200 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 200 ug/kg 206-44-0 Fluoranthene ND 12 ug/kg 86-73-7 Fluorene ND 12 ug/kg 118-74-1 Hexachlorobenzene ND 200 ug/kg 87-68-3 Hexachlorobutadiene ND 200 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 780 ug/kg 67-72-1 Hexachloroethane ND 200 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 12 ug/kg 78-59-1 Isophorone ND 200 ug/kg 90-12-0 1-Methylnaphthalene ND 12 ug/kg 91-57-6 2-Methylnaphthalene ND 12 ug/kg 91-20-3 Naphthalene ND 12 ug/kg 98-95-3 Nitrobenzene ND 200 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 200 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 200 ug/kg 85-01-8 Phenanthrene ND 12 ug/kg 129-00-0 Pyrene ND 12 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 200 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 73%25-109% 4165-62-2 Phenol-d5 76%30-110% 118-79-6 2,4,6-Tribromophenol 89%27-127% 4165-60-0 Nitrobenzene-d5 67%24-123% 321-60-8 2-Fluorobiphenyl 62%32-112% 1718-51-0 Terphenyl-d14 80%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 48 of 141 LA5814444.8 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-4 Lab Sample ID:LA58144-4R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 49 of 141 LA5814444.8 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-4 Lab Sample ID:LA58144-4R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012432M.D 1 10/27/19 03:52 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012432M.D 1 10/27/19 03:53 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.1 g 10.0 ml Run #2 20.1 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 3000 ug/kg C9-C18 Aliphatics ND b 3000 ug/kg C19-C36 Aliphatics ND b 3000 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 86%40-140% 84-15-1 o-Terphenyl 85%40-140% 321-60-8 2-Fluorobiphenyl 72%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 50 of 141 LA5814444.8 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-4 Lab Sample ID:LA58144-4R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:83.7 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 51 of 141 LA5814444.8 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-5 Lab Sample ID:LA58144-5 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058561.D 1 10/05/19 15:24 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 4.9 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 56 ug/kg 71-43-2 Benzene 0.56 0.56 ug/kg 108-86-1 Bromobenzene ND 1.1 ug/kg 74-97-5 Bromochloromethane ND 1.1 ug/kg 75-27-4 Bromodichloromethane ND 1.1 ug/kg 75-25-2 Bromoform ND 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.6 ug/kg 135-98-8 sec-Butylbenzene ND 5.6 ug/kg 98-06-6 tert-Butylbenzene ND 1.1 ug/kg 56-23-5 Carbon Tetrachloride ND 1.1 ug/kg 108-90-7 Chlorobenzene ND 1.1 ug/kg 75-00-3 Chloroethane ND 1.1 ug/kg 67-66-3 Chloroform ND 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.6 ug/kg 106-43-4 p-Chlorotoluene ND 5.6 ug/kg 124-48-1 Dibromochloromethane ND 1.1 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.6 ug/kg 106-93-4 1,2-Dibromoethane ND 1.1 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.1 ug/kg 541-73-1 m-Dichlorobenzene ND 1.1 ug/kg 95-50-1 o-Dichlorobenzene ND 1.1 ug/kg 106-46-7 p-Dichlorobenzene ND 1.1 ug/kg 75-34-3 1,1-Dichloroethane ND 1.1 ug/kg 107-06-2 1,2-Dichloroethane ND 1.1 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.1 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.1 ug/kg 78-87-5 1,2-Dichloropropane ND 1.1 ug/kg 142-28-9 1,3-Dichloropropane ND 1.1 ug/kg 594-20-7 2,2-Dichloropropane ND 1.1 ug/kg 563-58-6 1,1-Dichloropropene ND 1.1 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.1 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 52 of 141 LA5814444.9 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-5 Lab Sample ID:LA58144-5 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.1 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.1 ug/kg 64-17-5 Ethyl Alcohol ND 450 ug/kg 100-41-4 Ethylbenzene ND 1.1 ug/kg 591-78-6 2-Hexanone ND 14 ug/kg 87-68-3 Hexachlorobutadiene ND 5.6 ug/kg 98-82-8 Isopropylbenzene ND 5.6 ug/kg 99-87-6 p-Isopropyltoluene ND 5.6 ug/kg 74-83-9 Methyl Bromide ND 11 ug/kg 74-87-3 Methyl Chloride ND 5.6 ug/kg 74-95-3 Methylene Bromide ND 1.1 ug/kg 75-09-2 Methylene Chloride ND 5.6 ug/kg 78-93-3 Methyl Ethyl Ketone ND 14 ug/kg 108-10-1 4-Methyl-2-pentanone ND 14 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.1 ug/kg 91-20-3 Naphthalene ND 5.6 ug/kg 103-65-1 n-Propylbenzene ND 5.6 ug/kg 100-42-5 Styrene ND 1.1 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.1 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.1 ug/kg 127-18-4 Tetrachloroethylene ND 1.1 ug/kg 108-88-3 Toluene ND 5.6 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.6 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.6 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.1 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.1 ug/kg 79-01-6 Trichloroethylene ND 1.1 ug/kg 75-69-4 Trichlorofluoromethane ND 1.1 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.6 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.6 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.6 ug/kg 108-05-4 Vinyl Acetate ND 5.6 ug/kg 75-01-4 Vinyl Chloride ND 1.1 ug/kg m,p-Xylene ND 2.2 ug/kg 95-47-6 o-Xylene ND 1.1 ug/kg 1330-20-7 Xylene (total)ND 2.2 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 90%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 53 of 141 LA5814444.9 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-5 Lab Sample ID:LA58144-5 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 100%52-159% 460-00-4 4-Bromofluorobenzene 99%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 54 of 141 LA5814444.9 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-5 Lab Sample ID:LA58144-5 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346259.D 1 10/05/19 17:22 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.60 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 6.4 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 91%63-139% 540-36-3 1,4-Difluorobenzene 88%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 55 of 141 LA5814444.9 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-5 Lab Sample ID:LA58144-5R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051847.D 1 10/25/19 00:44 PC 10/22/19 08:45 OP15444 EC2063 Run #2 Initial Weight Final Volume Run #1 20.4 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid b ND 1100 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 180 ug/kg 95-57-8 2-Chlorophenol ND 180 ug/kg 120-83-2 2,4-Dichlorophenol ND 180 ug/kg 105-67-9 2,4-Dimethylphenol ND 180 ug/kg 51-28-5 2,4-Dinitrophenol ND 710 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 180 ug/kg 95-48-7 2-Methylphenol ND 180 ug/kg 3&4-Methylphenol ND 180 ug/kg 88-75-5 2-Nitrophenol ND 180 ug/kg 100-02-7 4-Nitrophenol ND 710 ug/kg 87-86-5 Pentachlorophenol ND 180 ug/kg 108-95-2 Phenol ND 180 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 180 ug/kg 83-32-9 Acenaphthene ND 11 ug/kg 208-96-8 Acenaphthylene ND 11 ug/kg 120-12-7 Anthracene ND 11 ug/kg 56-55-3 Benzo(a)anthracene ND 11 ug/kg 50-32-8 Benzo(a)pyrene ND 11 ug/kg 205-99-2 Benzo(b)fluoranthene ND 11 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 11 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 180 ug/kg 100-51-6 Benzyl Alcohol ND 180 ug/kg 207-08-9 Benzo(k)fluoranthene ND 11 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 180 ug/kg 106-47-8 4-Chloroaniline ND 180 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 180 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 180 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 180 ug/kg 91-58-7 2-Chloronaphthalene ND 180 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 180 ug/kg 218-01-9 Chrysene ND 11 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 56 of 141 LA5814444.10 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-5 Lab Sample ID:LA58144-5R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 11 ug/kg 132-64-9 Dibenzofuran ND 180 ug/kg 95-50-1 1,2-Dichlorobenzene ND 180 ug/kg 541-73-1 1,3-Dichlorobenzene ND 180 ug/kg 106-46-7 1,4-Dichlorobenzene ND 180 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 180 ug/kg 84-66-2 Diethyl Phthalate ND 180 ug/kg 131-11-3 Dimethyl Phthalate ND 180 ug/kg 84-74-2 Di-n-butyl Phthalate ND 180 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 180 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 180 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 180 ug/kg 206-44-0 Fluoranthene ND 11 ug/kg 86-73-7 Fluorene ND 11 ug/kg 118-74-1 Hexachlorobenzene ND 180 ug/kg 87-68-3 Hexachlorobutadiene ND 180 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 710 ug/kg 67-72-1 Hexachloroethane ND 180 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 11 ug/kg 78-59-1 Isophorone ND 180 ug/kg 90-12-0 1-Methylnaphthalene ND 11 ug/kg 91-57-6 2-Methylnaphthalene ND 11 ug/kg 91-20-3 Naphthalene ND 11 ug/kg 98-95-3 Nitrobenzene ND 180 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 180 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 180 ug/kg 85-01-8 Phenanthrene ND 11 ug/kg 129-00-0 Pyrene ND 11 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 180 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 62%25-109% 4165-62-2 Phenol-d5 65%30-110% 118-79-6 2,4,6-Tribromophenol 74%27-127% 4165-60-0 Nitrobenzene-d5 57%24-123% 321-60-8 2-Fluorobiphenyl 55%32-112% 1718-51-0 Terphenyl-d14 67%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 57 of 141 LA5814444.10 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-5 Lab Sample ID:LA58144-5R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 58 of 141 LA5814444.10 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-5 Lab Sample ID:LA58144-5R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012433M.D 1 10/27/19 04:15 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012433M.D 1 10/27/19 04:16 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.3 g 10.0 ml Run #2 20.3 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 2700 ug/kg C9-C18 Aliphatics ND b 2700 ug/kg C19-C36 Aliphatics ND b 2700 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 86%40-140% 84-15-1 o-Terphenyl 83%40-140% 321-60-8 2-Fluorobiphenyl 71%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 59 of 141 LA5814444.10 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-5 Lab Sample ID:LA58144-5R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:91.4 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 60 of 141 LA5814444.10 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-6 Lab Sample ID:LA58144-6 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058562.D 1 10/05/19 15:49 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 6.4 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 48 ug/kg 71-43-2 Benzene ND 0.48 ug/kg 108-86-1 Bromobenzene ND 0.96 ug/kg 74-97-5 Bromochloromethane ND 0.96 ug/kg 75-27-4 Bromodichloromethane ND 0.96 ug/kg 75-25-2 Bromoform ND 0.96 ug/kg 104-51-8 n-Butylbenzene ND 4.8 ug/kg 135-98-8 sec-Butylbenzene ND 4.8 ug/kg 98-06-6 tert-Butylbenzene ND 0.96 ug/kg 56-23-5 Carbon Tetrachloride ND 0.96 ug/kg 108-90-7 Chlorobenzene ND 0.96 ug/kg 75-00-3 Chloroethane ND 0.96 ug/kg 67-66-3 Chloroform ND 0.96 ug/kg 95-49-8 o-Chlorotoluene ND 4.8 ug/kg 106-43-4 p-Chlorotoluene ND 4.8 ug/kg 124-48-1 Dibromochloromethane ND 0.96 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 4.8 ug/kg 106-93-4 1,2-Dibromoethane ND 0.96 ug/kg 75-71-8 Dichlorodifluoromethane ND 0.96 ug/kg 541-73-1 m-Dichlorobenzene ND 0.96 ug/kg 95-50-1 o-Dichlorobenzene ND 0.96 ug/kg 106-46-7 p-Dichlorobenzene ND 0.96 ug/kg 75-34-3 1,1-Dichloroethane ND 0.96 ug/kg 107-06-2 1,2-Dichloroethane ND 0.96 ug/kg 75-35-4 1,1-Dichloroethylene ND 0.96 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 0.96 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 0.96 ug/kg 78-87-5 1,2-Dichloropropane ND 0.96 ug/kg 142-28-9 1,3-Dichloropropane ND 0.96 ug/kg 594-20-7 2,2-Dichloropropane ND 0.96 ug/kg 563-58-6 1,1-Dichloropropene ND 0.96 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 0.96 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 61 of 141 LA5814444.11 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-6 Lab Sample ID:LA58144-6 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 0.96 ug/kg 108-20-3 Di-Isopropyl Ether ND 0.96 ug/kg 64-17-5 Ethyl Alcohol ND 390 ug/kg 100-41-4 Ethylbenzene ND 0.96 ug/kg 591-78-6 2-Hexanone ND 12 ug/kg 87-68-3 Hexachlorobutadiene ND 4.8 ug/kg 98-82-8 Isopropylbenzene ND 4.8 ug/kg 99-87-6 p-Isopropyltoluene ND 4.8 ug/kg 74-83-9 Methyl Bromide ND 9.6 ug/kg 74-87-3 Methyl Chloride ND 4.8 ug/kg 74-95-3 Methylene Bromide ND 0.96 ug/kg 75-09-2 Methylene Chloride ND 4.8 ug/kg 78-93-3 Methyl Ethyl Ketone ND 12 ug/kg 108-10-1 4-Methyl-2-pentanone ND 12 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 0.96 ug/kg 91-20-3 Naphthalene ND 4.8 ug/kg 103-65-1 n-Propylbenzene ND 4.8 ug/kg 100-42-5 Styrene ND 0.96 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 0.96 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 0.96 ug/kg 127-18-4 Tetrachloroethylene ND 0.96 ug/kg 108-88-3 Toluene ND 4.8 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 4.8 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 4.8 ug/kg 71-55-6 1,1,1-Trichloroethane ND 0.96 ug/kg 79-00-5 1,1,2-Trichloroethane ND 0.96 ug/kg 79-01-6 Trichloroethylene ND 0.96 ug/kg 75-69-4 Trichlorofluoromethane ND 0.96 ug/kg 96-18-4 1,2,3-Trichloropropane ND 4.8 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 4.8 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 4.8 ug/kg 108-05-4 Vinyl Acetate ND 4.8 ug/kg 75-01-4 Vinyl Chloride ND 0.96 ug/kg m,p-Xylene ND 1.9 ug/kg 95-47-6 o-Xylene ND 0.96 ug/kg 1330-20-7 Xylene (total)ND 1.9 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 95%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 62 of 141 LA5814444.11 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-6 Lab Sample ID:LA58144-6 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 101%52-159% 460-00-4 4-Bromofluorobenzene 100%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 63 of 141 LA5814444.11 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-6 Lab Sample ID:LA58144-6 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346261.D 1 10/05/19 17:45 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 4.90 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 7.5 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 92%63-139% 540-36-3 1,4-Difluorobenzene 89%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 64 of 141 LA5814444.11 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-6 Lab Sample ID:LA58144-6R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051898.D 1 10/25/19 21:28 PC 10/22/19 08:45 OP15444 EC2065 Run #2 Initial Weight Final Volume Run #1 20.0 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid ND 1200 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 210 ug/kg 95-57-8 2-Chlorophenol ND 210 ug/kg 120-83-2 2,4-Dichlorophenol ND 210 ug/kg 105-67-9 2,4-Dimethylphenol ND 210 ug/kg 51-28-5 2,4-Dinitrophenol ND 810 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 210 ug/kg 95-48-7 2-Methylphenol ND 210 ug/kg 3&4-Methylphenol ND 210 ug/kg 88-75-5 2-Nitrophenol ND 210 ug/kg 100-02-7 4-Nitrophenol ND 810 ug/kg 87-86-5 Pentachlorophenol ND 210 ug/kg 108-95-2 Phenol ND 210 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 210 ug/kg 83-32-9 Acenaphthene ND 12 ug/kg 208-96-8 Acenaphthylene ND 12 ug/kg 120-12-7 Anthracene ND 12 ug/kg 56-55-3 Benzo(a)anthracene ND 12 ug/kg 50-32-8 Benzo(a)pyrene ND 12 ug/kg 205-99-2 Benzo(b)fluoranthene ND 12 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 12 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 210 ug/kg 100-51-6 Benzyl Alcohol ND 210 ug/kg 207-08-9 Benzo(k)fluoranthene ND 12 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 210 ug/kg 106-47-8 4-Chloroaniline ND 210 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 210 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 210 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 210 ug/kg 91-58-7 2-Chloronaphthalene ND 210 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 210 ug/kg 218-01-9 Chrysene ND 12 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 65 of 141 LA5814444.12 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-6 Lab Sample ID:LA58144-6R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 12 ug/kg 132-64-9 Dibenzofuran ND 210 ug/kg 95-50-1 1,2-Dichlorobenzene ND 210 ug/kg 541-73-1 1,3-Dichlorobenzene ND 210 ug/kg 106-46-7 1,4-Dichlorobenzene ND 210 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 210 ug/kg 84-66-2 Diethyl Phthalate ND 210 ug/kg 131-11-3 Dimethyl Phthalate ND 210 ug/kg 84-74-2 Di-n-butyl Phthalate ND 210 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 210 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 210 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 210 ug/kg 206-44-0 Fluoranthene ND 12 ug/kg 86-73-7 Fluorene ND 12 ug/kg 118-74-1 Hexachlorobenzene ND 210 ug/kg 87-68-3 Hexachlorobutadiene ND 210 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 810 ug/kg 67-72-1 Hexachloroethane ND 210 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 12 ug/kg 78-59-1 Isophorone ND 210 ug/kg 90-12-0 1-Methylnaphthalene ND 12 ug/kg 91-57-6 2-Methylnaphthalene ND 12 ug/kg 91-20-3 Naphthalene ND 12 ug/kg 98-95-3 Nitrobenzene ND 210 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 210 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 210 ug/kg 85-01-8 Phenanthrene ND 12 ug/kg 129-00-0 Pyrene ND 12 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 210 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 43%25-109% 4165-62-2 Phenol-d5 45%30-110% 118-79-6 2,4,6-Tribromophenol 44%27-127% 4165-60-0 Nitrobenzene-d5 40%24-123% 321-60-8 2-Fluorobiphenyl 38%32-112% 1718-51-0 Terphenyl-d14 46%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 66 of 141 LA5814444.12 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-6 Lab Sample ID:LA58144-6R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 67 of 141 LA5814444.12 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-6 Lab Sample ID:LA58144-6R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012434M.D 1 10/27/19 04:38 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012434M.D 1 10/27/19 04:39 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.0 g 10.0 ml Run #2 20.0 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 3100 ug/kg C9-C18 Aliphatics ND b 3100 ug/kg C19-C36 Aliphatics ND b 3100 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 85%40-140% 84-15-1 o-Terphenyl 90%40-140% 321-60-8 2-Fluorobiphenyl 74%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 68 of 141 LA5814444.12 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-6 Lab Sample ID:LA58144-6R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:81.0 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 69 of 141 LA5814444.12 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-7 Lab Sample ID:LA58144-7 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058563.D 1 10/05/19 16:14 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 5.5 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone 91.8 55 ug/kg 71-43-2 Benzene ND 0.55 ug/kg 108-86-1 Bromobenzene ND 1.1 ug/kg 74-97-5 Bromochloromethane ND 1.1 ug/kg 75-27-4 Bromodichloromethane ND 1.1 ug/kg 75-25-2 Bromoform ND 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.5 ug/kg 135-98-8 sec-Butylbenzene ND 5.5 ug/kg 98-06-6 tert-Butylbenzene ND 1.1 ug/kg 56-23-5 Carbon Tetrachloride ND 1.1 ug/kg 108-90-7 Chlorobenzene ND 1.1 ug/kg 75-00-3 Chloroethane ND 1.1 ug/kg 67-66-3 Chloroform ND 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.5 ug/kg 106-43-4 p-Chlorotoluene ND 5.5 ug/kg 124-48-1 Dibromochloromethane ND 1.1 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.5 ug/kg 106-93-4 1,2-Dibromoethane ND 1.1 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.1 ug/kg 541-73-1 m-Dichlorobenzene ND 1.1 ug/kg 95-50-1 o-Dichlorobenzene ND 1.1 ug/kg 106-46-7 p-Dichlorobenzene ND 1.1 ug/kg 75-34-3 1,1-Dichloroethane ND 1.1 ug/kg 107-06-2 1,2-Dichloroethane ND 1.1 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.1 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.1 ug/kg 78-87-5 1,2-Dichloropropane ND 1.1 ug/kg 142-28-9 1,3-Dichloropropane ND 1.1 ug/kg 594-20-7 2,2-Dichloropropane ND 1.1 ug/kg 563-58-6 1,1-Dichloropropene ND 1.1 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.1 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 70 of 141 LA5814444.13 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-7 Lab Sample ID:LA58144-7 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.1 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.1 ug/kg 64-17-5 Ethyl Alcohol ND 440 ug/kg 100-41-4 Ethylbenzene ND 1.1 ug/kg 591-78-6 2-Hexanone ND 14 ug/kg 87-68-3 Hexachlorobutadiene ND 5.5 ug/kg 98-82-8 Isopropylbenzene ND 5.5 ug/kg 99-87-6 p-Isopropyltoluene ND 5.5 ug/kg 74-83-9 Methyl Bromide ND 11 ug/kg 74-87-3 Methyl Chloride ND 5.5 ug/kg 74-95-3 Methylene Bromide ND 1.1 ug/kg 75-09-2 Methylene Chloride ND 5.5 ug/kg 78-93-3 Methyl Ethyl Ketone ND 14 ug/kg 108-10-1 4-Methyl-2-pentanone ND 14 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.1 ug/kg 91-20-3 Naphthalene ND 5.5 ug/kg 103-65-1 n-Propylbenzene ND 5.5 ug/kg 100-42-5 Styrene ND 1.1 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.1 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.1 ug/kg 127-18-4 Tetrachloroethylene ND 1.1 ug/kg 108-88-3 Toluene ND 5.5 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.5 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.5 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.1 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.1 ug/kg 79-01-6 Trichloroethylene ND 1.1 ug/kg 75-69-4 Trichlorofluoromethane ND 1.1 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.5 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.5 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.5 ug/kg 108-05-4 Vinyl Acetate ND 5.5 ug/kg 75-01-4 Vinyl Chloride ND 1.1 ug/kg m,p-Xylene ND 2.2 ug/kg 95-47-6 o-Xylene ND 1.1 ug/kg 1330-20-7 Xylene (total)ND 2.2 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 99%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 71 of 141 LA5814444.13 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-7 Lab Sample ID:LA58144-7 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 102%52-159% 460-00-4 4-Bromofluorobenzene 100%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 72 of 141 LA5814444.13 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-7 Lab Sample ID:LA58144-7 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346263.D 1 10/05/19 18:08 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.30 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 6.8 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 91%63-139% 540-36-3 1,4-Difluorobenzene 88%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 73 of 141 LA5814444.13 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-7 Lab Sample ID:LA58144-7R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051899.D 1 10/25/19 21:50 PC 10/22/19 08:45 OP15444 EC2065 Run #2 Initial Weight Final Volume Run #1 20.4 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid ND 1200 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 200 ug/kg 95-57-8 2-Chlorophenol ND 200 ug/kg 120-83-2 2,4-Dichlorophenol ND 200 ug/kg 105-67-9 2,4-Dimethylphenol ND 200 ug/kg 51-28-5 2,4-Dinitrophenol ND 780 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 200 ug/kg 95-48-7 2-Methylphenol ND 200 ug/kg 3&4-Methylphenol ND 200 ug/kg 88-75-5 2-Nitrophenol ND 200 ug/kg 100-02-7 4-Nitrophenol ND 780 ug/kg 87-86-5 Pentachlorophenol ND 200 ug/kg 108-95-2 Phenol ND 200 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 200 ug/kg 83-32-9 Acenaphthene ND 12 ug/kg 208-96-8 Acenaphthylene ND 12 ug/kg 120-12-7 Anthracene ND 12 ug/kg 56-55-3 Benzo(a)anthracene ND 12 ug/kg 50-32-8 Benzo(a)pyrene ND 12 ug/kg 205-99-2 Benzo(b)fluoranthene ND 12 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 12 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 200 ug/kg 100-51-6 Benzyl Alcohol ND 200 ug/kg 207-08-9 Benzo(k)fluoranthene ND 12 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 200 ug/kg 106-47-8 4-Chloroaniline ND 200 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 200 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 200 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 200 ug/kg 91-58-7 2-Chloronaphthalene ND 200 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 200 ug/kg 218-01-9 Chrysene ND 12 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 74 of 141 LA5814444.14 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-7 Lab Sample ID:LA58144-7R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 12 ug/kg 132-64-9 Dibenzofuran ND 200 ug/kg 95-50-1 1,2-Dichlorobenzene ND 200 ug/kg 541-73-1 1,3-Dichlorobenzene ND 200 ug/kg 106-46-7 1,4-Dichlorobenzene ND 200 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 200 ug/kg 84-66-2 Diethyl Phthalate ND 200 ug/kg 131-11-3 Dimethyl Phthalate ND 200 ug/kg 84-74-2 Di-n-butyl Phthalate ND 200 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 200 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 200 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 200 ug/kg 206-44-0 Fluoranthene ND 12 ug/kg 86-73-7 Fluorene ND 12 ug/kg 118-74-1 Hexachlorobenzene ND 200 ug/kg 87-68-3 Hexachlorobutadiene ND 200 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 780 ug/kg 67-72-1 Hexachloroethane ND 200 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 12 ug/kg 78-59-1 Isophorone ND 200 ug/kg 90-12-0 1-Methylnaphthalene ND 12 ug/kg 91-57-6 2-Methylnaphthalene ND 12 ug/kg 91-20-3 Naphthalene ND 12 ug/kg 98-95-3 Nitrobenzene ND 200 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 200 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 200 ug/kg 85-01-8 Phenanthrene ND 12 ug/kg 129-00-0 Pyrene ND 12 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 200 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 64%25-109% 4165-62-2 Phenol-d5 66%30-110% 118-79-6 2,4,6-Tribromophenol 70%27-127% 4165-60-0 Nitrobenzene-d5 59%24-123% 321-60-8 2-Fluorobiphenyl 56%32-112% 1718-51-0 Terphenyl-d14 68%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 75 of 141 LA5814444.14 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-7 Lab Sample ID:LA58144-7R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 76 of 141 LA5814444.14 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-7 Lab Sample ID:LA58144-7R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012435M.D 1 10/27/19 05:02 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012435M.D 1 10/27/19 05:03 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.2 g 10.0 ml Run #2 20.2 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)3510 3000 ug/kg C9-C18 Aliphatics ND b 3000 ug/kg C19-C36 Aliphatics ND b 3000 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 97%40-140% 84-15-1 o-Terphenyl 93%40-140% 321-60-8 2-Fluorobiphenyl 72%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 77 of 141 LA5814444.14 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-7 Lab Sample ID:LA58144-7R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:82.6 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 78 of 141 LA5814444.14 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-8 Lab Sample ID:LA58144-8 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058564.D 1 10/05/19 16:38 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 5.5 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 55 ug/kg 71-43-2 Benzene ND 0.55 ug/kg 108-86-1 Bromobenzene ND 1.1 ug/kg 74-97-5 Bromochloromethane ND 1.1 ug/kg 75-27-4 Bromodichloromethane ND 1.1 ug/kg 75-25-2 Bromoform ND 1.1 ug/kg 104-51-8 n-Butylbenzene ND 5.5 ug/kg 135-98-8 sec-Butylbenzene ND 5.5 ug/kg 98-06-6 tert-Butylbenzene ND 1.1 ug/kg 56-23-5 Carbon Tetrachloride ND 1.1 ug/kg 108-90-7 Chlorobenzene ND 1.1 ug/kg 75-00-3 Chloroethane ND 1.1 ug/kg 67-66-3 Chloroform ND 1.1 ug/kg 95-49-8 o-Chlorotoluene ND 5.5 ug/kg 106-43-4 p-Chlorotoluene ND 5.5 ug/kg 124-48-1 Dibromochloromethane ND 1.1 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.5 ug/kg 106-93-4 1,2-Dibromoethane ND 1.1 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.1 ug/kg 541-73-1 m-Dichlorobenzene ND 1.1 ug/kg 95-50-1 o-Dichlorobenzene ND 1.1 ug/kg 106-46-7 p-Dichlorobenzene ND 1.1 ug/kg 75-34-3 1,1-Dichloroethane ND 1.1 ug/kg 107-06-2 1,2-Dichloroethane ND 1.1 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.1 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.1 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.1 ug/kg 78-87-5 1,2-Dichloropropane ND 1.1 ug/kg 142-28-9 1,3-Dichloropropane ND 1.1 ug/kg 594-20-7 2,2-Dichloropropane ND 1.1 ug/kg 563-58-6 1,1-Dichloropropene ND 1.1 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.1 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 79 of 141 LA5814444.15 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-8 Lab Sample ID:LA58144-8 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.1 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.1 ug/kg 64-17-5 Ethyl Alcohol ND 440 ug/kg 100-41-4 Ethylbenzene ND 1.1 ug/kg 591-78-6 2-Hexanone ND 14 ug/kg 87-68-3 Hexachlorobutadiene ND 5.5 ug/kg 98-82-8 Isopropylbenzene ND 5.5 ug/kg 99-87-6 p-Isopropyltoluene ND 5.5 ug/kg 74-83-9 Methyl Bromide ND 11 ug/kg 74-87-3 Methyl Chloride ND 5.5 ug/kg 74-95-3 Methylene Bromide ND 1.1 ug/kg 75-09-2 Methylene Chloride ND 5.5 ug/kg 78-93-3 Methyl Ethyl Ketone ND 14 ug/kg 108-10-1 4-Methyl-2-pentanone ND 14 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.1 ug/kg 91-20-3 Naphthalene ND 5.5 ug/kg 103-65-1 n-Propylbenzene ND 5.5 ug/kg 100-42-5 Styrene ND 1.1 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.1 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.1 ug/kg 127-18-4 Tetrachloroethylene ND 1.1 ug/kg 108-88-3 Toluene ND 5.5 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.5 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.5 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.1 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.1 ug/kg 79-01-6 Trichloroethylene ND 1.1 ug/kg 75-69-4 Trichlorofluoromethane ND 1.1 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.5 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.5 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.5 ug/kg 108-05-4 Vinyl Acetate ND 5.5 ug/kg 75-01-4 Vinyl Chloride ND 1.1 ug/kg m,p-Xylene ND 2.2 ug/kg 95-47-6 o-Xylene ND 1.1 ug/kg 1330-20-7 Xylene (total)ND 2.2 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 98%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 80 of 141 LA5814444.15 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-8 Lab Sample ID:LA58144-8 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 104%52-159% 460-00-4 4-Bromofluorobenzene 102%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 81 of 141 LA5814444.15 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-8 Lab Sample ID:LA58144-8 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346265.D 1 10/05/19 18:30 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.00 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 7.1 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 93%63-139% 540-36-3 1,4-Difluorobenzene 88%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 82 of 141 LA5814444.15 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-8 Lab Sample ID:LA58144-8R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051900.D 1 10/25/19 22:12 PC 10/22/19 08:45 OP15444 EC2065 Run #2 Initial Weight Final Volume Run #1 20.0 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid ND 1200 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 210 ug/kg 95-57-8 2-Chlorophenol ND 210 ug/kg 120-83-2 2,4-Dichlorophenol ND 210 ug/kg 105-67-9 2,4-Dimethylphenol ND 210 ug/kg 51-28-5 2,4-Dinitrophenol ND 800 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 210 ug/kg 95-48-7 2-Methylphenol ND 210 ug/kg 3&4-Methylphenol ND 210 ug/kg 88-75-5 2-Nitrophenol ND 210 ug/kg 100-02-7 4-Nitrophenol ND 800 ug/kg 87-86-5 Pentachlorophenol ND 210 ug/kg 108-95-2 Phenol ND 210 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 210 ug/kg 83-32-9 Acenaphthene ND 12 ug/kg 208-96-8 Acenaphthylene ND 12 ug/kg 120-12-7 Anthracene ND 12 ug/kg 56-55-3 Benzo(a)anthracene ND 12 ug/kg 50-32-8 Benzo(a)pyrene ND 12 ug/kg 205-99-2 Benzo(b)fluoranthene ND 12 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 12 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 210 ug/kg 100-51-6 Benzyl Alcohol ND 210 ug/kg 207-08-9 Benzo(k)fluoranthene ND 12 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 210 ug/kg 106-47-8 4-Chloroaniline ND 210 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 210 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 210 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 210 ug/kg 91-58-7 2-Chloronaphthalene ND 210 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 210 ug/kg 218-01-9 Chrysene ND 12 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 83 of 141 LA5814444.16 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-8 Lab Sample ID:LA58144-8R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 12 ug/kg 132-64-9 Dibenzofuran ND 210 ug/kg 95-50-1 1,2-Dichlorobenzene ND 210 ug/kg 541-73-1 1,3-Dichlorobenzene ND 210 ug/kg 106-46-7 1,4-Dichlorobenzene ND 210 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 210 ug/kg 84-66-2 Diethyl Phthalate ND 210 ug/kg 131-11-3 Dimethyl Phthalate ND 210 ug/kg 84-74-2 Di-n-butyl Phthalate ND 210 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 210 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 210 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 210 ug/kg 206-44-0 Fluoranthene ND 12 ug/kg 86-73-7 Fluorene ND 12 ug/kg 118-74-1 Hexachlorobenzene ND 210 ug/kg 87-68-3 Hexachlorobutadiene ND 210 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 800 ug/kg 67-72-1 Hexachloroethane ND 210 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 12 ug/kg 78-59-1 Isophorone ND 210 ug/kg 90-12-0 1-Methylnaphthalene ND 12 ug/kg 91-57-6 2-Methylnaphthalene ND 12 ug/kg 91-20-3 Naphthalene ND 12 ug/kg 98-95-3 Nitrobenzene ND 210 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 210 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 210 ug/kg 85-01-8 Phenanthrene ND 12 ug/kg 129-00-0 Pyrene ND 12 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 210 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 52%25-109% 4165-62-2 Phenol-d5 53%30-110% 118-79-6 2,4,6-Tribromophenol 57%27-127% 4165-60-0 Nitrobenzene-d5 49%24-123% 321-60-8 2-Fluorobiphenyl 46%32-112% 1718-51-0 Terphenyl-d14 55%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 84 of 141 LA5814444.16 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-8 Lab Sample ID:LA58144-8R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 85 of 141 LA5814444.16 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-8 Lab Sample ID:LA58144-8R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012436M.D 1 10/27/19 05:26 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012436M.D 1 10/27/19 05:27 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.3 g 10.0 ml Run #2 20.3 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 3000 ug/kg C9-C18 Aliphatics ND b 3000 ug/kg C19-C36 Aliphatics ND b 3000 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 91%40-140% 84-15-1 o-Terphenyl 96%40-140% 321-60-8 2-Fluorobiphenyl 71%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 86 of 141 LA5814444.16 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-8 Lab Sample ID:LA58144-8R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:82.4 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 87 of 141 LA5814444.16 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-9 Lab Sample ID:LA58144-9 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058565.D 1 10/05/19 17:03 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 4.9 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 72 ug/kg 71-43-2 Benzene ND 0.72 ug/kg 108-86-1 Bromobenzene ND 1.4 ug/kg 74-97-5 Bromochloromethane ND 1.4 ug/kg 75-27-4 Bromodichloromethane ND 1.4 ug/kg 75-25-2 Bromoform ND 1.4 ug/kg 104-51-8 n-Butylbenzene ND 7.2 ug/kg 135-98-8 sec-Butylbenzene ND 7.2 ug/kg 98-06-6 tert-Butylbenzene ND 1.4 ug/kg 56-23-5 Carbon Tetrachloride ND 1.4 ug/kg 108-90-7 Chlorobenzene ND 1.4 ug/kg 75-00-3 Chloroethane ND 1.4 ug/kg 67-66-3 Chloroform ND 1.4 ug/kg 95-49-8 o-Chlorotoluene ND 7.2 ug/kg 106-43-4 p-Chlorotoluene ND 7.2 ug/kg 124-48-1 Dibromochloromethane ND 1.4 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 7.2 ug/kg 106-93-4 1,2-Dibromoethane ND 1.4 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.4 ug/kg 541-73-1 m-Dichlorobenzene ND 1.4 ug/kg 95-50-1 o-Dichlorobenzene ND 1.4 ug/kg 106-46-7 p-Dichlorobenzene ND 1.4 ug/kg 75-34-3 1,1-Dichloroethane ND 1.4 ug/kg 107-06-2 1,2-Dichloroethane ND 1.4 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.4 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.4 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.4 ug/kg 78-87-5 1,2-Dichloropropane ND 1.4 ug/kg 142-28-9 1,3-Dichloropropane ND 1.4 ug/kg 594-20-7 2,2-Dichloropropane ND 1.4 ug/kg 563-58-6 1,1-Dichloropropene ND 1.4 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.4 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 88 of 141 LA5814444.17 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-9 Lab Sample ID:LA58144-9 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.4 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.4 ug/kg 64-17-5 Ethyl Alcohol ND 570 ug/kg 100-41-4 Ethylbenzene ND 1.4 ug/kg 591-78-6 2-Hexanone ND 18 ug/kg 87-68-3 Hexachlorobutadiene ND 7.2 ug/kg 98-82-8 Isopropylbenzene ND 7.2 ug/kg 99-87-6 p-Isopropyltoluene ND 7.2 ug/kg 74-83-9 Methyl Bromide ND 14 ug/kg 74-87-3 Methyl Chloride ND 7.2 ug/kg 74-95-3 Methylene Bromide ND 1.4 ug/kg 75-09-2 Methylene Chloride ND 7.2 ug/kg 78-93-3 Methyl Ethyl Ketone ND 18 ug/kg 108-10-1 4-Methyl-2-pentanone ND 18 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.4 ug/kg 91-20-3 Naphthalene ND 7.2 ug/kg 103-65-1 n-Propylbenzene ND 7.2 ug/kg 100-42-5 Styrene ND 1.4 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.4 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.4 ug/kg 127-18-4 Tetrachloroethylene ND 1.4 ug/kg 108-88-3 Toluene ND 7.2 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 7.2 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 7.2 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.4 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.4 ug/kg 79-01-6 Trichloroethylene ND 1.4 ug/kg 75-69-4 Trichlorofluoromethane ND 1.4 ug/kg 96-18-4 1,2,3-Trichloropropane ND 7.2 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 7.2 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 7.2 ug/kg 108-05-4 Vinyl Acetate ND 7.2 ug/kg 75-01-4 Vinyl Chloride ND 1.4 ug/kg m,p-Xylene ND 2.9 ug/kg 95-47-6 o-Xylene ND 1.4 ug/kg 1330-20-7 Xylene (total)ND 2.9 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 99%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 89 of 141 LA5814444.17 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-9 Lab Sample ID:LA58144-9 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 102%52-159% 460-00-4 4-Bromofluorobenzene 101%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 90 of 141 LA5814444.17 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-9 Lab Sample ID:LA58144-9 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346267.D 1 10/05/19 18:53 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.20 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 8.8 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 92%63-139% 540-36-3 1,4-Difluorobenzene 88%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 91 of 141 LA5814444.17 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-9 Lab Sample ID:LA58144-9R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051901.D 1 10/25/19 22:33 PC 10/22/19 08:45 OP15444 EC2065 Run #2 Initial Weight Final Volume Run #1 20.3 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid ND 1400 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 240 ug/kg 95-57-8 2-Chlorophenol ND 240 ug/kg 120-83-2 2,4-Dichlorophenol ND 240 ug/kg 105-67-9 2,4-Dimethylphenol ND 240 ug/kg 51-28-5 2,4-Dinitrophenol ND 910 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 240 ug/kg 95-48-7 2-Methylphenol ND 240 ug/kg 3&4-Methylphenol ND 240 ug/kg 88-75-5 2-Nitrophenol ND 240 ug/kg 100-02-7 4-Nitrophenol ND 910 ug/kg 87-86-5 Pentachlorophenol ND 240 ug/kg 108-95-2 Phenol ND 240 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 240 ug/kg 83-32-9 Acenaphthene ND 14 ug/kg 208-96-8 Acenaphthylene ND 14 ug/kg 120-12-7 Anthracene ND 14 ug/kg 56-55-3 Benzo(a)anthracene ND 14 ug/kg 50-32-8 Benzo(a)pyrene ND 14 ug/kg 205-99-2 Benzo(b)fluoranthene ND 14 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 14 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 240 ug/kg 100-51-6 Benzyl Alcohol ND 240 ug/kg 207-08-9 Benzo(k)fluoranthene ND 14 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 240 ug/kg 106-47-8 4-Chloroaniline ND 240 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 240 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 240 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 240 ug/kg 91-58-7 2-Chloronaphthalene ND 240 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 240 ug/kg 218-01-9 Chrysene ND 14 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 92 of 141 LA5814444.18 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-9 Lab Sample ID:LA58144-9R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 14 ug/kg 132-64-9 Dibenzofuran ND 240 ug/kg 95-50-1 1,2-Dichlorobenzene ND 240 ug/kg 541-73-1 1,3-Dichlorobenzene ND 240 ug/kg 106-46-7 1,4-Dichlorobenzene ND 240 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 240 ug/kg 84-66-2 Diethyl Phthalate ND 240 ug/kg 131-11-3 Dimethyl Phthalate ND 240 ug/kg 84-74-2 Di-n-butyl Phthalate ND 240 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 240 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 240 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 240 ug/kg 206-44-0 Fluoranthene ND 14 ug/kg 86-73-7 Fluorene ND 14 ug/kg 118-74-1 Hexachlorobenzene ND 240 ug/kg 87-68-3 Hexachlorobutadiene ND 240 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 910 ug/kg 67-72-1 Hexachloroethane ND 240 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 14 ug/kg 78-59-1 Isophorone ND 240 ug/kg 90-12-0 1-Methylnaphthalene ND 14 ug/kg 91-57-6 2-Methylnaphthalene ND 14 ug/kg 91-20-3 Naphthalene ND 14 ug/kg 98-95-3 Nitrobenzene ND 240 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 240 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 240 ug/kg 85-01-8 Phenanthrene ND 14 ug/kg 129-00-0 Pyrene ND 14 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 240 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 54%25-109% 4165-62-2 Phenol-d5 55%30-110% 118-79-6 2,4,6-Tribromophenol 58%27-127% 4165-60-0 Nitrobenzene-d5 51%24-123% 321-60-8 2-Fluorobiphenyl 48%32-112% 1718-51-0 Terphenyl-d14 59%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 93 of 141 LA5814444.18 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-9 Lab Sample ID:LA58144-9R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 94 of 141 LA5814444.18 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-9 Lab Sample ID:LA58144-9R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012437M.D 1 10/27/19 05:49 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012437M.D 1 10/27/19 05:50 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.4 g 10.0 ml Run #2 20.4 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 3400 ug/kg C9-C18 Aliphatics ND b 3400 ug/kg C19-C36 Aliphatics ND b 3400 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 88%40-140% 84-15-1 o-Terphenyl 91%40-140% 321-60-8 2-Fluorobiphenyl 69%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 95 of 141 LA5814444.18 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-9 Lab Sample ID:LA58144-9R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:71.1 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 96 of 141 LA5814444.18 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-10 Lab Sample ID:LA58144-10 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 2H0058566.D 1 10/05/19 17:28 PJ 10/02/19 17:00 n/a V2H2338 Run #2 Initial Weight Run #1 5.4 g Run #2 VOA List for NC CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 64 ug/kg 71-43-2 Benzene ND 0.64 ug/kg 108-86-1 Bromobenzene ND 1.3 ug/kg 74-97-5 Bromochloromethane ND 1.3 ug/kg 75-27-4 Bromodichloromethane ND 1.3 ug/kg 75-25-2 Bromoform ND 1.3 ug/kg 104-51-8 n-Butylbenzene ND 6.4 ug/kg 135-98-8 sec-Butylbenzene ND 6.4 ug/kg 98-06-6 tert-Butylbenzene ND 1.3 ug/kg 56-23-5 Carbon Tetrachloride ND 1.3 ug/kg 108-90-7 Chlorobenzene ND 1.3 ug/kg 75-00-3 Chloroethane ND 1.3 ug/kg 67-66-3 Chloroform ND 1.3 ug/kg 95-49-8 o-Chlorotoluene ND 6.4 ug/kg 106-43-4 p-Chlorotoluene ND 6.4 ug/kg 124-48-1 Dibromochloromethane ND 1.3 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 6.4 ug/kg 106-93-4 1,2-Dibromoethane ND 1.3 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.3 ug/kg 541-73-1 m-Dichlorobenzene ND 1.3 ug/kg 95-50-1 o-Dichlorobenzene ND 1.3 ug/kg 106-46-7 p-Dichlorobenzene ND 1.3 ug/kg 75-34-3 1,1-Dichloroethane ND 1.3 ug/kg 107-06-2 1,2-Dichloroethane ND 1.3 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.3 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.3 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.3 ug/kg 78-87-5 1,2-Dichloropropane ND 1.3 ug/kg 142-28-9 1,3-Dichloropropane ND 1.3 ug/kg 594-20-7 2,2-Dichloropropane ND 1.3 ug/kg 563-58-6 1,1-Dichloropropene ND 1.3 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.3 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 97 of 141 LA5814444.19 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-10 Lab Sample ID:LA58144-10 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Compound Result RL Units Q 10061-02-6 trans-1,3-Dichloropropene ND 1.3 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.3 ug/kg 64-17-5 Ethyl Alcohol ND 510 ug/kg 100-41-4 Ethylbenzene ND 1.3 ug/kg 591-78-6 2-Hexanone ND 16 ug/kg 87-68-3 Hexachlorobutadiene ND 6.4 ug/kg 98-82-8 Isopropylbenzene ND 6.4 ug/kg 99-87-6 p-Isopropyltoluene ND 6.4 ug/kg 74-83-9 Methyl Bromide ND 13 ug/kg 74-87-3 Methyl Chloride ND 6.4 ug/kg 74-95-3 Methylene Bromide ND 1.3 ug/kg 75-09-2 Methylene Chloride ND 6.4 ug/kg 78-93-3 Methyl Ethyl Ketone ND 16 ug/kg 108-10-1 4-Methyl-2-pentanone ND 16 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.3 ug/kg 91-20-3 Naphthalene ND 6.4 ug/kg 103-65-1 n-Propylbenzene ND 6.4 ug/kg 100-42-5 Styrene ND 1.3 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 ug/kg 127-18-4 Tetrachloroethylene ND 1.3 ug/kg 108-88-3 Toluene ND 6.4 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 6.4 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 6.4 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.3 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.3 ug/kg 79-01-6 Trichloroethylene ND 1.3 ug/kg 75-69-4 Trichlorofluoromethane ND 1.3 ug/kg 96-18-4 1,2,3-Trichloropropane ND 6.4 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 6.4 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 6.4 ug/kg 108-05-4 Vinyl Acetate ND 6.4 ug/kg 75-01-4 Vinyl Chloride ND 1.3 ug/kg m,p-Xylene ND 2.5 ug/kg 95-47-6 o-Xylene ND 1.3 ug/kg 1330-20-7 Xylene (total)ND 2.5 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 17060-07-0 1,2-Dichloroethane-D4 103%59-143% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 98 of 141 LA5814444.19 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-10 Lab Sample ID:LA58144-10 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8260D SW846 5035 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC VOA List for NC CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 2037-26-5 Toluene-D8 105%52-159% 460-00-4 4-Bromofluorobenzene 106%38-183% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 99 of 141 LA5814444.19 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-10 Lab Sample ID:LA58144-10 Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8015C SW846 5035 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346273.D 1 10/05/19 20:02 NN 10/02/19 17:00 n/a GLA2710 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 5.10 g 5.0 ml 100 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 8.6 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 93%63-139% 540-36-3 1,4-Difluorobenzene 89%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 100 of 141 LA5814444.19 SGS North America Inc. Report of Analysis Page 1 of 3 Client Sample ID:SB-10 Lab Sample ID:LA58144-10R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a C0051902.D 1 10/25/19 22:55 PC 10/22/19 08:45 OP15444 EC2065 Run #2 Initial Weight Final Volume Run #1 20.2 g 1.0 ml Run #2 ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid ND 1400 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 230 ug/kg 95-57-8 2-Chlorophenol ND 230 ug/kg 120-83-2 2,4-Dichlorophenol ND 230 ug/kg 105-67-9 2,4-Dimethylphenol ND 230 ug/kg 51-28-5 2,4-Dinitrophenol ND 900 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 230 ug/kg 95-48-7 2-Methylphenol ND 230 ug/kg 3&4-Methylphenol ND 230 ug/kg 88-75-5 2-Nitrophenol ND 230 ug/kg 100-02-7 4-Nitrophenol ND 900 ug/kg 87-86-5 Pentachlorophenol ND 230 ug/kg 108-95-2 Phenol ND 230 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 230 ug/kg 83-32-9 Acenaphthene ND 14 ug/kg 208-96-8 Acenaphthylene ND 14 ug/kg 120-12-7 Anthracene ND 14 ug/kg 56-55-3 Benzo(a)anthracene ND 14 ug/kg 50-32-8 Benzo(a)pyrene ND 14 ug/kg 205-99-2 Benzo(b)fluoranthene ND 14 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 14 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 230 ug/kg 100-51-6 Benzyl Alcohol ND 230 ug/kg 207-08-9 Benzo(k)fluoranthene ND 14 ug/kg 85-68-7 Butyl Benzyl Phthalate b ND 230 ug/kg 106-47-8 4-Chloroaniline ND 230 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 230 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 230 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 230 ug/kg 91-58-7 2-Chloronaphthalene ND 230 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 230 ug/kg 218-01-9 Chrysene ND 14 ug/kg ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 101 of 141 LA5814444.20 SGS North America Inc. Report of Analysis Page 2 of 3 Client Sample ID:SB-10 Lab Sample ID:LA58144-10R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q 53-70-3 Dibenzo(a,h)anthracene ND 14 ug/kg 132-64-9 Dibenzofuran ND 230 ug/kg 95-50-1 1,2-Dichlorobenzene ND 230 ug/kg 541-73-1 1,3-Dichlorobenzene ND 230 ug/kg 106-46-7 1,4-Dichlorobenzene ND 230 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 230 ug/kg 84-66-2 Diethyl Phthalate ND 230 ug/kg 131-11-3 Dimethyl Phthalate ND 230 ug/kg 84-74-2 Di-n-butyl Phthalate ND 230 ug/kg 117-84-0 Di-n-octyl Phthalate b ND 230 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 230 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate b ND 230 ug/kg 206-44-0 Fluoranthene ND 14 ug/kg 86-73-7 Fluorene ND 14 ug/kg 118-74-1 Hexachlorobenzene ND 230 ug/kg 87-68-3 Hexachlorobutadiene ND 230 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 900 ug/kg 67-72-1 Hexachloroethane ND 230 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 14 ug/kg 78-59-1 Isophorone ND 230 ug/kg 90-12-0 1-Methylnaphthalene ND 14 ug/kg 91-57-6 2-Methylnaphthalene ND 14 ug/kg 91-20-3 Naphthalene ND 14 ug/kg 98-95-3 Nitrobenzene ND 230 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 230 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 230 ug/kg 85-01-8 Phenanthrene ND 14 ug/kg 129-00-0 Pyrene ND 14 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 230 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 367-12-4 2-Fluorophenol 58%25-109% 4165-62-2 Phenol-d5 59%30-110% 118-79-6 2,4,6-Tribromophenol 60%27-127% 4165-60-0 Nitrobenzene-d5 54%24-123% 321-60-8 2-Fluorobiphenyl 52%32-112% 1718-51-0 Terphenyl-d14 62%41-115% (a) Sample extracted beyond hold time per client request. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 102 of 141 LA5814444.20 SGS North America Inc. Report of Analysis Page 3 of 3 Client Sample ID:SB-10 Lab Sample ID:LA58144-10R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:SW846 8270E SW846 3546 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC ABN List for NC, May 2012 CAS No.Compound Result RL Units Q (b) Associated CCV outside of control limits high, sample was ND. ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 103 of 141 LA5814444.20 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-10 Lab Sample ID:LA58144-10R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Method:MADEP EPH REV 1.1 SW846 3546 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 a X0012438M.D 1 10/27/19 06:13 LS 10/22/19 08:45 OP15446 GLB2111 Run #2 a Y0012438M.D 1 10/27/19 06:14 LS 10/22/19 08:45 OP15446 GLB2112 Initial Weight Final Volume Run #1 20.5 g 10.0 ml Run #2 20.5 g 10.0 ml MAEPH List CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)ND 3400 ug/kg C9-C18 Aliphatics ND b 3400 ug/kg C19-C36 Aliphatics ND b 3400 ug/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 3386-33-2 1-Chlorooctadecane 83%40-140% 84-15-1 o-Terphenyl 87%40-140% 321-60-8 2-Fluorobiphenyl 72%40-140% (a) Sample extracted beyond hold time per client request. (b) Result is from Run# 2 ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 104 of 141 LA5814444.20 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:SB-10 Lab Sample ID:LA58144-10R Date Sampled:09/30/19 Matrix:SO - Soil Date Received:10/02/19 Percent Solids:72.8 Project:Circle K #2723471-Wilson, NC General Chemistry Analyte Result RL Units DF Analyzed By Method HEM Petroleum Hydrocarbons <50 50 mg/kg 1 10/23/19 10:40 HD SW846 9071B M RL = Reporting Limit 105 of 141 LA5814444.20 SGS North America Inc. Report of Analysis Page 1 of 1 Client Sample ID:MW-3 Lab Sample ID:LA58144-11 Date Sampled:09/30/19 Matrix:SO - Oil Date Received:10/02/19 Method:SW846 8015C Percent Solids:n/a Project:Circle K #2723471-Wilson, NC File ID DF Analyzed By Prep Date Prep Batch Analytical Batch Run #1 LA346966.D 1 10/12/19 13:31 NN n/a n/a GLA2722 Run #2 Initial Weight Final Volume Methanol Aliquot Run #1 1.00 g 10.0 ml 0.50 ul Run #2 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)166000 10000 mg/kg CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits 460-00-4 4-Bromofluorobenzene 63%63-139% 540-36-3 1,4-Difluorobenzene 88%52-140% ND = Not detected J = Indicates an estimated value RL = Reporting Limit B = Indicates analyte found in associated method blank E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound 106 of 141 LA5814444.21 SGS North America Inc. Misc. Forms Custody Documents and Other Forms Includes the following where applicable: • Chain of Custody Scott, LA Section 5 107 of 141 LA581445 LA58144: Chain of Custody Page 1 of 4 108 of 141 LA5814455.1 LA58144: Chain of Custody Page 2 of 4 109 of 141 LA5814455.1 SGS Sample Receipt Summary Job Number:LA58144 Client:ATC Date / Time Received:10/2/2019 9:40:00 AM Delivery Method:FedEx Project:CIRCLE K-2723471 4. No. Coolers:1 Airbill #'s:491386905944 Cooler Security 1. Custody Seals Present: Y or N 2. Custody Seals Intact: 3. COC Present: 4. Smpl Dates/Time OK 2. Thermometer ID: Cooler Temperature Y or N 1. Temp criteria achieved: 3. Cooler media: DV440; Ice (direct contact) Quality Control Preservation Y or N N/A 1. Trip Blank present / cooler: 2. Trip Blank listed on COC: 3. Samples preserved properly: 4. VOCs headspace free: Sample Integrity - Documentation Y or N 1. Sample labels present on bottles: 2. Container labeling complete: 3. Sample container label / COC agree: Sample Integrity - Condition Y or N 1. Sample recvd within HT: 3. Condition of sample: 2. All containers accounted for: Sample Integrity - Instructions 1. Analysis requested is clear: 2. Bottles received for unspecified tests 3. Sufficient volume recvd for analysis: 4. Compositing instructions clear: 5. Filtering instructions clear: Intact Y or N Comments Y or N N/A Cooler Temps (Initial/Adjusted):#1: (3.4/3.4); LA58144: Chain of Custody Page 3 of 4 110 of 141 LA5814455.1 TAT (Days):7Received Date:10/2/2019Due Date:10/9/2019Project Description:Circle K #2723471-Wilson, NCAccount Name:ATC Group Services LLCDeliverable:COMMBCSR:AJRequested Date:10/21/2019Job Change Order:LA58144Sample #:LA58144-1R, 2R, 3R, 4R, 5R, 6R, 7R, 8R, 9R, 10RChange:Relog PHC1664, VMAVPHR, BMAEPHR, AB8270NC.Dept:========================================================================================================================================================================================================================================TAT:7Above Changes Per:To Client: This Change Order is confirmation of the revisions, previously discussed with the a Client Service Representative.Date/Time:10/21/2019 10:01:59 AMPage 1 of 1Maureen JacksonLA58144: Chain of Custody Page 4 of 4 111 of 141 LA5814455.1 SGS North America Inc. MS Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Scott, LA Section 6 112 of 141 LA581446 Method Blank Summary Page 1 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2H2338-MB1 2H0058556.D 1 10/05/19 PJ n/a n/a V2H2338 The QC reported here applies to the following samples:Method: SW846 8260D LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 CAS No.Compound Result RL Units Q 67-64-1 Acetone ND 50 ug/kg 71-43-2 Benzene ND 0.50 ug/kg 108-86-1 Bromobenzene ND 1.0 ug/kg 74-97-5 Bromochloromethane ND 1.0 ug/kg 75-27-4 Bromodichloromethane ND 1.0 ug/kg 75-25-2 Bromoform ND 1.0 ug/kg 104-51-8 n-Butylbenzene ND 5.0 ug/kg 135-98-8 sec-Butylbenzene ND 5.0 ug/kg 98-06-6 tert-Butylbenzene ND 1.0 ug/kg 56-23-5 Carbon Tetrachloride ND 1.0 ug/kg 108-90-7 Chlorobenzene ND 1.0 ug/kg 75-00-3 Chloroethane ND 1.0 ug/kg 67-66-3 Chloroform ND 1.0 ug/kg 95-49-8 o-Chlorotoluene ND 5.0 ug/kg 106-43-4 p-Chlorotoluene ND 5.0 ug/kg 124-48-1 Dibromochloromethane ND 1.0 ug/kg 96-12-8 1,2-Dibromo-3-chloropropane ND 5.0 ug/kg 106-93-4 1,2-Dibromoethane ND 1.0 ug/kg 75-71-8 Dichlorodifluoromethane ND 1.0 ug/kg 541-73-1 m-Dichlorobenzene ND 1.0 ug/kg 95-50-1 o-Dichlorobenzene ND 1.0 ug/kg 106-46-7 p-Dichlorobenzene ND 1.0 ug/kg 75-34-3 1,1-Dichloroethane ND 1.0 ug/kg 107-06-2 1,2-Dichloroethane ND 1.0 ug/kg 75-35-4 1,1-Dichloroethylene ND 1.0 ug/kg 156-59-2 cis-1,2-Dichloroethylene ND 1.0 ug/kg 156-60-5 trans-1,2-Dichloroethylene ND 1.0 ug/kg 78-87-5 1,2-Dichloropropane ND 1.0 ug/kg 142-28-9 1,3-Dichloropropane ND 1.0 ug/kg 594-20-7 2,2-Dichloropropane ND 1.0 ug/kg 563-58-6 1,1-Dichloropropene ND 1.0 ug/kg 10061-01-5 cis-1,3-Dichloropropene ND 1.0 ug/kg 10061-02-6 trans-1,3-Dichloropropene ND 1.0 ug/kg 108-20-3 Di-Isopropyl Ether ND 1.0 ug/kg 64-17-5 Ethyl Alcohol ND 400 ug/kg 100-41-4 Ethylbenzene ND 1.0 ug/kg 113 of 141 LA5814466.1.1 Method Blank Summary Page 2 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2H2338-MB1 2H0058556.D 1 10/05/19 PJ n/a n/a V2H2338 The QC reported here applies to the following samples:Method: SW846 8260D LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 CAS No.Compound Result RL Units Q 591-78-6 2-Hexanone ND 13 ug/kg 87-68-3 Hexachlorobutadiene ND 5.0 ug/kg 98-82-8 Isopropylbenzene ND 5.0 ug/kg 99-87-6 p-Isopropyltoluene ND 5.0 ug/kg 74-83-9 Methyl Bromide ND 10 ug/kg 74-87-3 Methyl Chloride ND 5.0 ug/kg 74-95-3 Methylene Bromide ND 1.0 ug/kg 75-09-2 Methylene Chloride ND 5.0 ug/kg 78-93-3 Methyl Ethyl Ketone ND 13 ug/kg 108-10-1 4-Methyl-2-pentanone ND 13 ug/kg 1634-04-4 Methyl Tert Butyl Ether ND 1.0 ug/kg 91-20-3 Naphthalene ND 5.0 ug/kg 103-65-1 n-Propylbenzene ND 5.0 ug/kg 100-42-5 Styrene ND 1.0 ug/kg 630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 ug/kg 79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 ug/kg 127-18-4 Tetrachloroethylene ND 1.0 ug/kg 108-88-3 Toluene ND 5.0 ug/kg 87-61-6 1,2,3-Trichlorobenzene ND 5.0 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 5.0 ug/kg 71-55-6 1,1,1-Trichloroethane ND 1.0 ug/kg 79-00-5 1,1,2-Trichloroethane ND 1.0 ug/kg 79-01-6 Trichloroethylene ND 1.0 ug/kg 75-69-4 Trichlorofluoromethane ND 1.0 ug/kg 96-18-4 1,2,3-Trichloropropane ND 5.0 ug/kg 95-63-6 1,2,4-Trimethylbenzene ND 5.0 ug/kg 108-67-8 1,3,5-Trimethylbenzene ND 5.0 ug/kg 108-05-4 Vinyl Acetate ND 5.0 ug/kg 75-01-4 Vinyl Chloride ND 1.0 ug/kg m,p-Xylene ND 2.0 ug/kg 95-47-6 o-Xylene ND 1.0 ug/kg 1330-20-7 Xylene (total)ND 2.0 ug/kg 114 of 141 LA5814466.1.1 Method Blank Summary Page 3 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2H2338-MB1 2H0058556.D 1 10/05/19 PJ n/a n/a V2H2338 The QC reported here applies to the following samples:Method: SW846 8260D LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 CAS No.Surrogate Recoveries Limits 17060-07-0 1,2-Dichloroethane-D4 120%59-143% 2037-26-5 Toluene-D8 105%52-159% 460-00-4 4-Bromofluorobenzene 95%38-183% 115 of 141 LA5814466.1.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2H2338-BS1 2H0058553.D 1 10/05/19 PJ n/a n/a V2H2338 V2H2338-BSD1 2H0058554.D 1 10/05/19 PJ n/a n/a V2H2338 The QC reported here applies to the following samples:Method: SW846 8260D LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD 67-64-1 Acetone 50 45.6 91 39.5 79 14 40-153/30 71-43-2 Benzene 20 16.9 85 16.6 83 2 67-135/30 108-86-1 Bromobenzene 20 17.2 86 17.4 87 1 54-144/30 74-97-5 Bromochloromethane 20 20.7 104 19.0 95 9 50-147/30 75-27-4 Bromodichloromethane 20 17.4 87 17.4 87 0 54-146/30 75-25-2 Bromoform 20 15.7 79 14.9 75 5 49-145/30 104-51-8 n-Butylbenzene 20 19.7 99 18.8 94 5 47-160/30 135-98-8 sec-Butylbenzene 20 19.2 96 18.7 94 3 51-155/30 98-06-6 tert-Butylbenzene 20 18.8 94 18.9 95 1 53-152/30 56-23-5 Carbon Tetrachloride 20 21.8 109 21.3 107 2 50-152/30 108-90-7 Chlorobenzene 20 18.4 92 18.9 95 3 57-144/30 75-00-3 Chloroethane 20 25.1 126 21.6 108 15 38-176/30 67-66-3 Chloroform 20 20.3 102 19.6 98 4 53-147/30 95-49-8 o-Chlorotoluene 20 17.9 90 16.3 82 9 52-151/30 106-43-4 p-Chlorotoluene 20 16.8 84 17.5 88 4 52-150/30 124-48-1 Dibromochloromethane 20 16.3 82 17.2 86 5 54-146/30 96-12-8 1,2-Dibromo-3-chloropropane 20 18.3 92 16.8 84 9 51-145/30 106-93-4 1,2-Dibromoethane 20 18.2 91 17.3 87 5 55-145/30 75-71-8 Dichlorodifluoromethane 20 20.7 104 20.5 103 1 24-179/30 541-73-1 m-Dichlorobenzene 20 18.0 90 17.2 86 5 54-147/30 95-50-1 o-Dichlorobenzene 20 16.8 84 16.9 85 1 55-144/30 106-46-7 p-Dichlorobenzene 20 19.4 97 20.7 104 6 54-147/30 75-34-3 1,1-Dichloroethane 20 20.6 103 19.8 99 4 53-148/30 107-06-2 1,2-Dichloroethane 20 16.9 85 17.3 87 2 55-144/30 75-35-4 1,1-Dichloroethylene 20 21.8 109 21.2 106 3 49-153/30 156-59-2 cis-1,2-Dichloroethylene 20 16.5 83 17.9 90 8 52-147/30 156-60-5 trans-1,2-Dichloroethylene 20 21.0 105 20.2 101 4 51-152/30 78-87-5 1,2-Dichloropropane 20 17.6 88 17.6 88 0 56-145/30 142-28-9 1,3-Dichloropropane 20 16.4 82 16.5 83 1 53-145/30 594-20-7 2,2-Dichloropropane 20 19.6 98 18.5 93 6 35-176/30 563-58-6 1,1-Dichloropropene 20 17.6 88 17.7 89 1 49-157/30 10061-01-5 cis-1,3-Dichloropropene 20 16.7 84 16.7 84 0 54-148/30 10061-02-6 trans-1,3-Dichloropropene 20 17.4 87 16.9 85 3 53-151/30 108-20-3 Di-Isopropyl Ether 20 17.7 89 17.8 89 1 85-120/30 64-17-5 Ethyl Alcohol 400 393 98 386 97 2 31-164/30 100-41-4 Ethylbenzene 20 19.0 95 19.5 98 3 69-136/30 * = Outside of Control Limits. 116 of 141 LA5814466.2.1 Blank Spike/Blank Spike Duplicate Summary Page 2 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2H2338-BS1 2H0058553.D 1 10/05/19 PJ n/a n/a V2H2338 V2H2338-BSD1 2H0058554.D 1 10/05/19 PJ n/a n/a V2H2338 The QC reported here applies to the following samples:Method: SW846 8260D LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD 591-78-6 2-Hexanone 50 41.2 82 38.6 77 7 45-148/30 87-68-3 Hexachlorobutadiene 20 23.3 117 23.8 119 2 48-168/30 98-82-8 Isopropylbenzene 20 17.7 89 18.0 90 2 52-151/30 99-87-6 p-Isopropyltoluene 20 18.2 91 18.5 93 2 50-155/30 74-83-9 Methyl Bromide 20 22.8 114 22.8 114 0 40-170/30 74-87-3 Methyl Chloride 20 21.7 109 20.9 105 4 39-152/30 74-95-3 Methylene Bromide 20 18.1 91 18.2 91 1 53-147/30 75-09-2 Methylene Chloride 20 18.9 95 18.4 92 3 51-142/30 78-93-3 Methyl Ethyl Ketone 50 47.9 96 46.7 93 3 48-150/30 108-10-1 4-Methyl-2-pentanone 50 41.0 82 39.3 79 4 50-151/30 1634-04-4 Methyl Tert Butyl Ether 20 17.3 87 17.1 86 1 61-142/30 91-20-3 Naphthalene 20 18.6 93 17.8 89 4 58-147/30 103-65-1 n-Propylbenzene 20 18.1 91 17.3 87 5 50-154/30 100-42-5 Styrene 20 16.8 84 18.0 90 7 56-145/30 630-20-6 1,1,1,2-Tetrachloroethane 20 18.1 91 18.8 94 4 56-147/30 79-34-5 1,1,2,2-Tetrachloroethane 20 20.6 103 18.2 91 12 55-141/30 127-18-4 Tetrachloroethylene 20 17.3 87 17.0 85 2 54-156/30 108-88-3 Toluene 20 16.9 85 17.5 88 3 71-135/30 87-61-6 1,2,3-Trichlorobenzene 20 17.1 86 16.6 83 3 51-157/30 120-82-1 1,2,4-Trichlorobenzene 20 15.9 80 16.1 81 1 48-163/30 71-55-6 1,1,1-Trichloroethane 20 17.8 89 17.7 89 1 52-153/30 79-00-5 1,1,2-Trichloroethane 20 17.2 86 16.7 84 3 55-144/30 79-01-6 Trichloroethylene 20 17.0 85 15.5 78 9 56-151/30 75-69-4 Trichlorofluoromethane 20 23.5 118 22.5 113 4 36-171/30 96-18-4 1,2,3-Trichloropropane 20 17.3 87 16.9 85 2 45-139/30 95-63-6 1,2,4-Trimethylbenzene 20 19.0 95 18.5 93 3 50-153/30 108-67-8 1,3,5-Trimethylbenzene 20 19.2 96 18.3 92 5 51-153/30 108-05-4 Vinyl Acetate 20 23.0 115 20.5 103 11 23-188/30 75-01-4 Vinyl Chloride 20 20.5 103 20.4 102 0 42-155/30 m,p-Xylene 40 36.8 92 37.6 94 2 70-140/30 95-47-6 o-Xylene 20 16.7 84 16.9 85 1 70-132/30 1330-20-7 Xylene (total)60 53.5 89 54.5 91 2 69-138/30 * = Outside of Control Limits. 117 of 141 LA5814466.2.1 Blank Spike/Blank Spike Duplicate Summary Page 3 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch V2H2338-BS1 2H0058553.D 1 10/05/19 PJ n/a n/a V2H2338 V2H2338-BSD1 2H0058554.D 1 10/05/19 PJ n/a n/a V2H2338 The QC reported here applies to the following samples:Method: SW846 8260D LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 CAS No.Surrogate Recoveries BSP BSD Limits 17060-07-0 1,2-Dichloroethane-D4 112%105%59-143% 2037-26-5 Toluene-D8 97%98%52-159% 460-00-4 4-Bromofluorobenzene 100%102%38-183% * = Outside of Control Limits. 118 of 141 LA5814466.2.1 SGS North America Inc. MS Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Scott, LA Section 7 119 of 141 LA581447 Method Blank Summary Page 1 of 2 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15444-MB C0051835.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 The QC reported here applies to the following samples:Method: SW846 8270E LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R CAS No.Compound Result RL Units Q 65-85-0 Benzoic acid ND 1000 ug/kg 59-50-7 4-Chloro-3-methyl Phenol ND 170 ug/kg 95-57-8 2-Chlorophenol ND 170 ug/kg 120-83-2 2,4-Dichlorophenol ND 170 ug/kg 105-67-9 2,4-Dimethylphenol ND 170 ug/kg 51-28-5 2,4-Dinitrophenol ND 660 ug/kg 534-52-1 4,6-Dinitro-o-cresol ND 170 ug/kg 95-48-7 2-Methylphenol ND 170 ug/kg 3&4-Methylphenol ND 170 ug/kg 88-75-5 2-Nitrophenol ND 170 ug/kg 100-02-7 4-Nitrophenol ND 660 ug/kg 87-86-5 Pentachlorophenol ND 170 ug/kg 108-95-2 Phenol ND 170 ug/kg 88-06-2 2,4,6-Trichlorophenol ND 170 ug/kg 83-32-9 Acenaphthene ND 10 ug/kg 208-96-8 Acenaphthylene ND 10 ug/kg 120-12-7 Anthracene ND 10 ug/kg 56-55-3 Benzo(a)anthracene ND 10 ug/kg 50-32-8 Benzo(a)pyrene ND 10 ug/kg 205-99-2 Benzo(b)fluoranthene ND 10 ug/kg 191-24-2 Benzo(g,h,i)perylene ND 10 ug/kg 101-55-3 4-Bromophenyl Phenyl Ether ND 170 ug/kg 100-51-6 Benzyl Alcohol ND 170 ug/kg 207-08-9 Benzo(k)fluoranthene ND 10 ug/kg 85-68-7 Butyl Benzyl Phthalate ND 170 ug/kg 106-47-8 4-Chloroaniline ND 170 ug/kg 111-91-1 bis(2-Chloroethoxy)methane ND 170 ug/kg 111-44-4 bis(2-Chloroethyl)ether ND 170 ug/kg 108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 ug/kg 91-58-7 2-Chloronaphthalene ND 170 ug/kg 7005-72-3 4-Chlorophenyl Phenyl Ether ND 170 ug/kg 218-01-9 Chrysene ND 10 ug/kg 53-70-3 Dibenzo(a,h)anthracene ND 10 ug/kg 132-64-9 Dibenzofuran ND 170 ug/kg 95-50-1 1,2-Dichlorobenzene ND 170 ug/kg 541-73-1 1,3-Dichlorobenzene ND 170 ug/kg 120 of 141 LA5814477.1.1 Method Blank Summary Page 2 of 2 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15444-MB C0051835.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 The QC reported here applies to the following samples:Method: SW846 8270E LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R CAS No.Compound Result RL Units Q 106-46-7 1,4-Dichlorobenzene ND 170 ug/kg 91-94-1 3,3'-Dichlorobenzidine ND 170 ug/kg 84-66-2 Diethyl Phthalate ND 170 ug/kg 131-11-3 Dimethyl Phthalate ND 170 ug/kg 84-74-2 Di-n-butyl Phthalate ND 170 ug/kg 117-84-0 Di-n-octyl Phthalate ND 170 ug/kg 122-66-7 1,2-Diphenylhydrazine ND 170 ug/kg 117-81-7 bis(2-Ethylhexyl)phthalate ND 170 ug/kg 206-44-0 Fluoranthene ND 10 ug/kg 86-73-7 Fluorene ND 10 ug/kg 118-74-1 Hexachlorobenzene ND 170 ug/kg 87-68-3 Hexachlorobutadiene ND 170 ug/kg 77-47-4 Hexachlorocyclopentadiene ND 660 ug/kg 67-72-1 Hexachloroethane ND 170 ug/kg 193-39-5 Indeno(1,2,3-cd)pyrene ND 10 ug/kg 78-59-1 Isophorone ND 170 ug/kg 90-12-0 1-Methylnaphthalene ND 10 ug/kg 91-57-6 2-Methylnaphthalene ND 10 ug/kg 91-20-3 Naphthalene ND 10 ug/kg 98-95-3 Nitrobenzene ND 170 ug/kg 621-64-7 N-Nitroso-di-n-propylamine ND 170 ug/kg 86-30-6 N-Nitrosodiphenylamine ND 170 ug/kg 85-01-8 Phenanthrene ND 10 ug/kg 129-00-0 Pyrene ND 10 ug/kg 120-82-1 1,2,4-Trichlorobenzene ND 170 ug/kg CAS No.Surrogate Recoveries Limits 367-12-4 2-Fluorophenol 93%25-109% 4165-62-2 Phenol-d5 95%30-110% 118-79-6 2,4,6-Tribromophenol 99%27-127% 4165-60-0 Nitrobenzene-d5 82%24-123% 321-60-8 2-Fluorobiphenyl 79%32-112% 1718-51-0 Terphenyl-d14 95%41-115% 121 of 141 LA5814477.1.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15444-BS C0051836.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 OP15444-BSD C0051837.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 The QC reported here applies to the following samples:Method: SW846 8270E LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD 65-85-0 Benzoic acid 4930 4330 88 4690 95 8 33-107/25 59-50-7 4-Chloro-3-methyl Phenol 2460 2440 99 2610 106 7 69-110/16 95-57-8 2-Chlorophenol 2460 2120 86 2210 90 4 67-104/14 120-83-2 2,4-Dichlorophenol 2460 2410 98 2580 105 7 70-106/15 105-67-9 2,4-Dimethylphenol 2460 1730 70 1860 76 7 67-108/15 51-28-5 2,4-Dinitrophenol 2460 2660 108 2830 115 6 49-119/23 534-52-1 4,6-Dinitro-o-cresol 2460 2620 106 2770 112 6 57-115/21 95-48-7 2-Methylphenol 2460 2010 82 2160 88 7 66-103/14 3&4-Methylphenol 2460 2180 89 2360 96 8 68-104/14 88-75-5 2-Nitrophenol 2460 2270 92 2420 98 6 69-112/16 100-02-7 4-Nitrophenol 2460 2160 88 2360 96 9 55-123/18 87-86-5 Pentachlorophenol 2460 2420 98 2530 103 4 61-106/20 108-95-2 Phenol 2460 2330 95 2530 103 8 63-110/14 88-06-2 2,4,6-Trichlorophenol 2460 2290 93 2480 101 8 66-112/17 83-32-9 Acenaphthene 2460 1970 80 2110 86 7 68-102/15 208-96-8 Acenaphthylene 2460 2260 92 2390 97 6 69-106/15 120-12-7 Anthracene 2460 2150 87 2230 91 4 70-105/16 56-55-3 Benzo(a)anthracene 2460 2180 89 2300 93 5 66-102/16 50-32-8 Benzo(a)pyrene 2460 2340 95 2430 99 4 69-110/16 205-99-2 Benzo(b)fluoranthene 2460 2410 98 2530 103 5 66-109/18 191-24-2 Benzo(g,h,i)perylene 2460 2260 92 2350 95 4 67-107/17 101-55-3 4-Bromophenyl Phenyl Ether 2460 2530 103 2670 108 5 67-108/17 100-51-6 Benzyl Alcohol 2460 2280 93 2460 100 8 67-108/15 207-08-9 Benzo(k)fluoranthene 2460 2410 98 2450 99 2 68-110/17 85-68-7 Butyl Benzyl Phthalate 2460 3280 133* a 3380 137* a 3 64-117/18 106-47-8 4-Chloroaniline 2460 1780 72 1930 78 8 66-113/15 111-91-1 bis(2-Chloroethoxy)methane 2460 2240 91 2390 97 6 66-104/15 111-44-4 bis(2-Chloroethyl)ether 2460 2140 87 2280 93 6 58-109/17 108-60-1 2,2'-Oxybis(1-chloropropane)2460 2250 91 2390 97 6 48-115/16 91-58-7 2-Chloronaphthalene 2460 2130 86 2290 93 7 69-103/15 7005-72-3 4-Chlorophenyl Phenyl Ether 2460 2270 92 2440 99 7 67-106/17 218-01-9 Chrysene 2460 2170 88 2290 93 5 66-104/16 53-70-3 Dibenzo(a,h)anthracene 2460 2300 93 2410 98 5 68-108/16 132-64-9 Dibenzofuran 2460 2110 86 2250 91 6 68-103/16 95-50-1 1,2-Dichlorobenzene 2460 2050 83 2190 89 7 66-100/14 541-73-1 1,3-Dichlorobenzene 2460 2010 82 2110 86 5 66-100/14 * = Outside of Control Limits. 122 of 141 LA5814477.2.1 Blank Spike/Blank Spike Duplicate Summary Page 2 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15444-BS C0051836.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 OP15444-BSD C0051837.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 The QC reported here applies to the following samples:Method: SW846 8270E LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD 106-46-7 1,4-Dichlorobenzene 2460 1890 77 2000 81 6 66-98/14 91-94-1 3,3'-Dichlorobenzidine 2460 2480 101 2570 104 4 64-116/18 84-66-2 Diethyl Phthalate 2460 2320 94 2460 100 6 68-108/17 131-11-3 Dimethyl Phthalate 2460 2330 95 2500 101 7 69-106/16 84-74-2 Di-n-butyl Phthalate 2460 2590 105 2700 110 4 67-115/18 117-84-0 Di-n-octyl Phthalate 2460 3480 141* a 3580 145* a 3 62-115/18 122-66-7 1,2-Diphenylhydrazine 2460 2300 93 2410 98 5 64-115/17 117-81-7 bis(2-Ethylhexyl)phthalate 2460 3230 131* a 3360 136* a 4 63-116/19 206-44-0 Fluoranthene 2460 2250 91 2370 96 5 70-108/17 86-73-7 Fluorene 2460 2200 89 2350 95 7 69-104/16 118-74-1 Hexachlorobenzene 2460 2490 101 2630 107 5 68-107/17 87-68-3 Hexachlorobutadiene 2460 2380 97 2550 104 7 64-107/14 77-47-4 Hexachlorocyclopentadiene 2460 2180 89 2310 94 6 51-120/16 67-72-1 Hexachloroethane 2460 2010 82 2140 87 6 65-103/15 193-39-5 Indeno(1,2,3-cd)pyrene 2460 2330 95 2420 98 4 68-108/16 78-59-1 Isophorone 2460 2340 95 2530 103 8 65-111/16 90-12-0 1-Methylnaphthalene 2460 2070 84 2210 90 7 70-102/15 91-57-6 2-Methylnaphthalene 2460 2080 84 2180 89 5 70-102/14 91-20-3 Naphthalene 2460 2000 81 2130 86 6 68-100/14 98-95-3 Nitrobenzene 2460 2440 99 2640 107* b 8 68-106/14 621-64-7 N-Nitroso-di-n-propylamine 2460 2410 98 2510 102 4 61-111/16 86-30-6 N-Nitrosodiphenylamine 2460 1890 77 1970 80 4 69-106/17 85-01-8 Phenanthrene 2460 2080 84 2230 91 7 68-101/16 129-00-0 Pyrene 2460 2250 91 2330 95 3 67-107/16 120-82-1 1,2,4-Trichlorobenzene 2460 2190 89 2320 94 6 67-104/14 CAS No.Surrogate Recoveries BSP BSD Limits 367-12-4 2-Fluorophenol 81%88%25-109% 4165-62-2 Phenol-d5 86%92%30-110% 118-79-6 2,4,6-Tribromophenol 108%116%27-127% 4165-60-0 Nitrobenzene-d5 77%84%24-123% 321-60-8 2-Fluorobiphenyl 73%79%32-112% 1718-51-0 Terphenyl-d14 86%91%41-115% * = Outside of Control Limits. 123 of 141 LA5814477.2.1 Blank Spike/Blank Spike Duplicate Summary Page 3 of 3 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15444-BS C0051836.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 OP15444-BSD C0051837.D 1 10/24/19 PC 10/22/19 OP15444 EC2063 The QC reported here applies to the following samples:Method: SW846 8270E LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R (a) Outside control limits biased high. Analyte not detected in associated samples. (b) Outside laboratory control limits but within reasonable method acceptance limits. * = Outside of Control Limits. 124 of 141 LA5814477.2.1 SGS North America Inc. GC Volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Scott, LA Section 8 125 of 141 LA581448 Method Blank Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GLA2710-MB1 LA346239.D 1 10/05/19 NN n/a n/a GLA2710 The QC reported here applies to the following samples:Method: SW846 8015C LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 5.0 mg/kg CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 91%63-139% 540-36-3 1,4-Difluorobenzene 90%52-140% 126 of 141 LA5814488.1.1 Method Blank Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GLA2722-MB1 LA346938.D 1 10/12/19 NN n/a n/a GLA2722 The QC reported here applies to the following samples:Method: SW846 8015C LA58144-11 CAS No.Compound Result RL Units Q TPH-GRO (C6-C10)ND 5.0 mg/kg CAS No.Surrogate Recoveries Limits 460-00-4 4-Bromofluorobenzene 94%63-139% 540-36-3 1,4-Difluorobenzene 90%52-140% 127 of 141 LA5814488.1.2 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GLA2710-BS2 LA346235.D 1 10/05/19 NN n/a n/a GLA2710 GLA2710-BSD2 LA346237.D 1 10/05/19 NN n/a n/a GLA2710 The QC reported here applies to the following samples:Method: SW846 8015C LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 Spike BSP BSP BSD BSD Limits CAS No.Compound mg/kg mg/kg %mg/kg %RPD Rec/RPD TPH-GRO (C6-C10)50 46.7 93 46.7 93 0 79-121/6 CAS No.Surrogate Recoveries BSP BSD Limits 460-00-4 4-Bromofluorobenzene 90%89%63-139% 540-36-3 1,4-Difluorobenzene 91%89%52-140% * = Outside of Control Limits. 128 of 141 LA5814488.2.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch GLA2722-BS1 LA346934.D 1 10/12/19 NN n/a n/a GLA2722 GLA2722-BSD1 LA346936.D 1 10/12/19 NN n/a n/a GLA2722 The QC reported here applies to the following samples:Method: SW846 8015C LA58144-11 Spike BSP BSP BSD BSD Limits CAS No.Compound mg/kg mg/kg %mg/kg %RPD Rec/RPD TPH-GRO (C6-C10)50 47.9 96 48.6 97 1 79-121/6 CAS No.Surrogate Recoveries BSP BSD Limits 460-00-4 4-Bromofluorobenzene 93%93%63-139% 540-36-3 1,4-Difluorobenzene 91%90%52-140% * = Outside of Control Limits. 129 of 141 LA5814488.2.2 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch LA58144-1MS LA346245.D 1 10/05/19 NN n/a n/a GLA2710 LA58144-1MSD LA346247.D 1 10/05/19 NN n/a n/a GLA2710 LA58144-1 LA346243.D 1 10/05/19 NN n/a n/a GLA2710 The QC reported here applies to the following samples:Method: SW846 8015C LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144-10 LA58144-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD TPH-GRO (C6-C10)ND 974 938 96 974 926 95 1 79-121/6 CAS No.Surrogate Recoveries MS MSD LA58144-1 Limits 460-00-4 4-Bromofluorobenzene 91%92%91%63-139% 540-36-3 1,4-Difluorobenzene 90%92%88%52-140% * = Outside of Control Limits. 130 of 141 LA5814488.3.1 Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch LA58208-1MS LA346988.D 1 10/12/19 NN n/a n/a GLA2722 LA58208-1MSD LA346990.D 1 10/12/19 NN n/a n/a GLA2722 LA58208-1 LA346958.D 1 10/12/19 NN n/a n/a GLA2722 The QC reported here applies to the following samples:Method: SW846 8015C LA58144-11 LA58208-1 Spike MS MS Spike MSD MSD Limits CAS No.Compound mg/kg Q mg/kg mg/kg %mg/kg mg/kg %RPD Rec/RPD TPH-GRO (C6-C10)ND 424 360 85 424 317 75* a 13* a 79-121/6 CAS No.Surrogate Recoveries MS MSD LA58208-1 Limits 460-00-4 4-Bromofluorobenzene 92%94%93%63-139% 540-36-3 1,4-Difluorobenzene 90%90%87%52-140% (a) Outside control limits due to matrix interference. Blank Spike meets acceptance criteria. * = Outside of Control Limits. 131 of 141 LA5814488.3.2 SGS North America Inc. GC/LC Semi-volatiles QC Data Summaries Includes the following where applicable: • Method Blank Summaries • Blank Spike Summaries • Matrix Spike and Duplicate Summaries Scott, LA Section 9 132 of 141 LA581449 Method Blank Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15446-MB X0012418M.D 1 10/26/19 LS 10/22/19 OP15446 GLB2111 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R CAS No.Compound Result RL Units Q C11-C22 Aromatics (Unadj.)18.2 2500 ug/kg J CAS No.Surrogate Recoveries Limits 84-15-1 o-Terphenyl 100%40-140% 321-60-8 2-Fluorobiphenyl 73%40-140% 133 of 141 LA5814499.1.1 Method Blank Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15446-MB Y0012418M.D 1 10/26/19 LS 10/22/19 OP15446 GLB2112 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R CAS No.Compound Result RL Units Q C9-C18 Aliphatics 322 2500 ug/kg J C19-C36 Aliphatics ND 2500 ug/kg CAS No.Surrogate Recoveries Limits 3386-33-2 1-Chlorooctadecane 99%40-140% 134 of 141 LA5814499.1.2 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15446-BS X0012419M.D 1 10/26/19 LS 10/22/19 OP15446 GLB2111 OP15446-BSD X0012420M.D 1 10/26/19 LS 10/22/19 OP15446 GLB2111 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD C11-C22 Aromatics (Unadj.)85000 75000 88 78700 93 5 40-140/30 CAS No.Surrogate Recoveries BSP BSD Limits 84-15-1 o-Terphenyl 86%92%40-140% 321-60-8 2-Fluorobiphenyl 71%68%40-140% * = Outside of Control Limits. 135 of 141 LA5814499.2.1 Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number:LA58144 Account:ATCNCR ATC Group Services LLC Project:Circle K #2723471-Wilson, NC Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch OP15446-BS Y0012419M.D 1 10/26/19 LS 10/22/19 OP15446 GLB2112 OP15446-BSD Y0012420M.D 1 10/26/19 LS 10/22/19 OP15446 GLB2112 The QC reported here applies to the following samples:Method: MADEP EPH REV 1.1 LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R Spike BSP BSP BSD BSD Limits CAS No.Compound ug/kg ug/kg %ug/kg %RPD Rec/RPD C9-C18 Aliphatics 30000 24200 81 29700 99 20 40-140/30 C19-C36 Aliphatics 40000 36100 90 41600 105 14 40-140/30 CAS No.Surrogate Recoveries BSP BSD Limits 3386-33-2 1-Chlorooctadecane 82%96%40-140% * = Outside of Control Limits. 136 of 141 LA5814499.2.2 SGS North America Inc. General Chemistry QC Data Summaries Includes the following where applicable: • Method Blank and Blank Spike Summaries • Duplicate Summaries • Matrix Spike Summaries Scott, LA Section 10 137 of 141 LA5814410 METHOD BLANK AND SPIKE RESULTS SUMMARY GENERAL CHEMISTRY Login Number: LA58144 Account: ATCNCR - ATC Group Services LLC Project: Circle K #2723471-Wilson, NC MB Spike BSP BSP QC Analyte Batch ID RL Result Units Amount Result %Recov Limits HEM Petroleum Hydrocarbons GP7325/GN15858 50 0.0 mg/kg 500 530 106.0 80-120% Associated Samples: Batch GP7325: LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R (*) Outside of QC limits __________________________________________________________________________________________________________________________ Page 1 138 of 141 LA581441010.1 DUPLICATE RESULTS SUMMARY GENERAL CHEMISTRY Login Number: LA58144 Account: ATCNCR - ATC Group Services LLC Project: Circle K #2723471-Wilson, NC QC Original DUP QC Analyte Batch ID Sample Units Result Result RPD Limits Solids, Percent GN15741 LA58144-10 % 72.8 72.9 0.1 0-20% Associated Samples: Batch GN15741: LA58144-1, LA58144-2, LA58144-3, LA58144-4, LA58144-5, LA58144-6, LA58144-7, LA58144-8, LA58144-9, LA58144- 10 (*) Outside of QC limits __________________________________________________________________________________________________________________________ Page 1 139 of 141 LA581441010.2 MATRIX SPIKE RESULTS SUMMARY GENERAL CHEMISTRY Login Number: LA58144 Account: ATCNCR - ATC Group Services LLC Project: Circle K #2723471-Wilson, NC QC Original Spike MS QC Analyte Batch ID Sample Units Result Amount Result %Rec Limits HEM Petroleum Hydrocarbons GP7325/GN15858 LA58454-6 mg/kg 0.0 500 421 84.0 75-125% Associated Samples: Batch GP7325: LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits __________________________________________________________________________________________________________________________ Page 1 140 of 141 LA581441010.3 MATRIX SPIKE DUPLICATE RESULTS SUMMARY GENERAL CHEMISTRY Login Number: LA58144 Account: ATCNCR - ATC Group Services LLC Project: Circle K #2723471-Wilson, NC QC Original Spike MSD QC Analyte Batch ID Sample Units Result Amount Result RPD Limit HEM Petroleum Hydrocarbons GP7325/GN15858 LA58454-6 mg/kg 0.0 500 429 1.9 Associated Samples: Batch GP7325: LA58144-1R, LA58144-2R, LA58144-3R, LA58144-4R, LA58144-5R, LA58144-6R, LA58144-7R, LA58144-8R, LA58144-9R, LA58144-10R (*) Outside of QC limits (N) Matrix Spike Rec. outside of QC limits __________________________________________________________________________________________________________________________ Page 1 141 of 141 LA581441010.4