RA-3936_23651_CA_MRP_20211206_MRP2021

GROUNDWATER MONITORING REPORT
DUNCAN’S MINI MART
1909 BURLINGTON ROAD
ROXBORO, PERSON COUNTY,NORTH CAROLINA
PREPARED FOR:
MR.MICHAEL TOMPKINS
MCLEOD OIL COMPANY
PO BOX 100
MEBANE, NORTH CAROLINA 27302
PREPARED BY:
PILOT GEOLOGICAL, PLLC
PO BOX 128
KERNERSVILLE, NORTH CAROLINA 27285
DECEMBER 6, 2021
PILOT PROJECT NO.G-7289
SITE INFORMATION
Site Name and Location Duncan’s Mini Mart
1909 Burlington Road
Roxboro, North Carolina
Incident No.23651
Facility ID:00-0-0000018926
Latitude and Longitude:3621’56”N; 7901’17”W
Land Use Category:Commercial
Contacts
Owner of UST:McLeod Oil Company
PO Box 100
Mebane, North Carolina 27302
[phone]
Primary Contact:Mr.Michael Tompkins
McLeod Company
[phone]
Consultant:Pilot Geological, PLLC
PO Box 128
Kernersville, North Carolina 27285
[phone]
Laboratory:Pace Analytical
1377 South Park Drive
Kernersville, North Carolina 27284
[phone]
Laboratory I.D. #Various
Release Information:Information pertaining to the source or quantity of the release was not available,
other than the release being from a UST system.The release was reportedly identified on July 31, 2001.
Table of Contents
1.0 SITE HISTORY ...................................................................................................................1
1.1 UST Information .........................................................................................................................................2
2.0 SITE GEOLOGY AND HYDROGEOLOGY...............................................................................2
3.0 FIELD ACTIVITIES..............................................................................................................2
3.1 Monitoring Well Sampling ..........................................................................................................................3
3.2 Water Supply Wells ....................................................................................................................................3
3.3 Groundwater Modeling..............................................................................................................................3
3.4 Free Product Investigation and Recovery ...................................................................................................4
4.0 LABORATORY ANALYTICAL RESULTS.................................................................................4
4.1 Groundwater Sample Analysis....................................................................................................................4
5.0 CONCLUSIONS .................................................................................................................4
6.0 RECOMMENDATIONS.......................................................................................................5
7.0 QUALIFICATIONS OF REPORT ...........................................................................................5
8.0 STATEMENTS AND CERTIFICATIONS .................................................................................6
DRAWINGS
Drawing 1 USGS Topographic Map
Drawing 2 Site Map
Drawing 3 UST Location Map
Drawing 4 Sample Location Map
Drawing 5 Water Supply Well Location Map
Drawing 6 Potentiometric Surface Map
Drawing 7 Benzene Isoconcentration Map
Drawing 8 Ethylbenzene Isoconcentration Map
Drawing 9 n-Propylbenzene Isoconcentration Map
Drawing 10 1,2,4-Trimethylbenzene Isoconcentration Map
Drawing 11 1,3,5-Trimethylbenzene Isoconcentration Map
Drawing 12 Toluene Isoconcentration Map
Drawing 13 Xylenes Isoconcentration Map
TABLES
Table 1 UST Information
Table 2 Monitoring Well Construction Information
Table 3 Water Supply Well Information
Table 4 Summary of Groundwater Analytical Results
Table of Contents (Continued)
APPENDIX
Appendix Laboratory Data Sheets and Chain of Custody Record
Groundwater Monitoring Report
Duncan’s Mini Mart
Pilot Project G-7289
December 6, 2021
1
1.0 SITE HISTORY
The site is Duncan’s Mini Mart located at 1909 Burlington Road in Roxboro, North Carolina
(Drawings 1 and 2). The site is an active convenience store that contains five active underground
storage tanks (USTs) that store petroleum products for retail sale.
Based on the available information, the USTs include three 4,000-gallon gasoline USTs (installed
in 1985), one 1,000-gallon diesel UST (installed in 1964),and one 2,000-gallon kerosene UST
(installed in 1964).The USTs have been owned and operated by McLeod Oil Company, Inc.since
1985.NESCO, Inc. (NESCO) completed a Site Check as required by a Notice of Regulatory
Requirements (NORR) dated April 24, 2001 issued by the North Carolina Department of
Environmental Quality (NCDEQ). Based on laboratory analysis of soil samples collected during
the Site Check, the soil in the vicinity of the UST system was impacted above the North Carolina
Action Levels. NESCO completed a Limited Site Assessment (LSA) in January of 2002.Based on
the findings in the LSA, the NCDENR required a Comprehensive Site Assessment (CSA) be
completed which NESCO completed in March 2003.Fuss and O’Neill, Inc. also completed a Pre-
CAP Monitoring Report, dated October 2003. Based on the available information and historical
groundwater data, several constituents exceeded their respective North Carolina 2L
Groundwater Quality Standards (2L Standards) in groundwater samples collected from the on-
site monitoring wells.The detected concentrations of benzene and ethylene dibromide (EDB)
also exceeded their respective Gross Contamination Levels (GCLs).
Numerous groundwater monitoring events and several Mobile Multi-Phase Extraction (MMPE)
events have been completed at the site.Recently,Progress Environmental, Inc. (Progress)
collected groundwater samples from monitoring wells MW-1 through MW-4, MW-6 through
MW-8, MW-10, MW-11, MW-14, and DW-1 on September 24, 2020.Water samples were also
collected from water-supply wells WS-4 (1916), WS-5 or “WS” (1894), WS-6 (1864),and WS-12
(1975). The groundwater monitoring well and water supply well water samples were analyzed
by a North Carolina certified laboratory for the presence of volatile organic compounds using
Standard Method 6200B.Laboratory analysis of the groundwater samples collected from the
monitoring wells MW-7,MW8,MW-10, MW-11, and DW-1 did not detect targeted compounds
above the laboratory detection limit.Laboratory analysis of the groundwater samples collected
from monitoring wells MW-1, MW-2,MW-3, MW-4, and MW-14 detected several petroleum-
related compounds at concentrations above their respective 2L Standards.The concentrations
of benzene and MTBE detected in the groundwater sample collected from monitoring well MW-
2 exceeded their respective GCLs.The concentration of MTBE detected in the groundwater
sample collected from monitoring well MW-4 also exceeded its GCL.
The site is classified as “high risk” based on the presence of petroleum-related compounds in the
groundwater samples collected from the monitoring wells and the presence of numerous water-
supply wells within 1,500 feet of the site.
Groundwater Monitoring Report
Duncan’s Mini Mart
Pilot Project G-7289
December 6, 2021
2
Project information is based on information contained in the NCDEQ regulatory file and
conversations with Mr.Michael Tompkins of McLeod Oil Company.
1.1 UST Information
Four underground storage tanks (USTs)are located at the site. The USTs were installed in 1964
and 1985 and include three 8,000-gallon gasoline USTs and one 4,000-gallon kerosene UST.The
approximate locations of the USTs are shown on Drawing 3.UST information is summarized in
Table 1.
2.0 SITE GEOLOGY AND HYDROGEOLOGY
The United States Geological Survey (USGS) Topographic Map,Hurdle Mills, NC, Olive Hill, NC,
Roxboro, NC, and Timberlake, NC Quadrangles,depicts the site located along a broad northeast-
southwest trending ridge.The elevation at the site ranges from approximately 700 feet above
mean seal level (msl) on the northwestern portion of the site to 680 feet msl on the southeastern
portion of the site.
The subject site is located within the Piedmont Physiographic Province. The Piedmont
Physiographic Province generally consists of hills and ridges which are dissected by a system of
swales and stream. The Piedmont Physiographic Province is predominantly underlain by
metamorphic rock (formed by heat, pressure and/or chemical action) and igneous rock (formed
directly from molten material). The topography and relief of the Piedmont Province has
developed from differential weathering of the igneous and metamorphic rock. Ridges and hills
have been developed in areas of less weathered rock. Because of the continued chemical and
physical weathering, rock in the Piedmont Physiographic Province is generally covered with a
mantle of soil that has weathered in place from the parent bedrock. These soils vary in thickness
and are referred to as residuum or residual soils. The residuum is typically finer grained and has
higher clay content near the surface because of the advanced weathering. Similarly, the soils
typically become coarser grained with increasing depth because of decreased weathering. As the
weathering decreases, the residual soils generally retain the overall appearance, texture and
foliations of the parent rock.
In general, groundwater movement in the Piedmont Physiographic Province is from higher to
lower elevations.Based on topographic inference,groundwater beneath the site most likely
flows generally south-southwest toward an unnamed tributary to North Flat River.Based on the
presumed groundwater flow direction, areas immediately to the north-northeast are potentially
up-gradient of the site.
3.0 FIELD ACTIVITIES
The field activities were completed or observed by Pilot on October 27, 2021.The field activities
consisted of collecting groundwater samples from existing monitoring wells MW-1,MW-2, MW-
Groundwater Monitoring Report
Duncan’s Mini Mart
Pilot Project G-7289
December 6, 2021
3
3, MW-4, MW-6, MW-7, MW-8, MW-10, MW-11, MW-14 and DW-1 (Drawing 4)and from water
supply wells WS-4, WS-5, WS-6, and WS-12 (Drawing 5).
3.1 Monitoring Well Sampling
A groundwater sample was collected from the aforementioned monitoring wells using a
disposable bailer and new length of nylon string or peristaltic pump and new length of tubing.
Prior to sampling, approximately three well volumes were purged from the monitoring wells. The
monitoring wells were purged to remove silt and sediment from the groundwater and collect a
representative sample of groundwater.After the purging was completed, groundwater samples
were collected in the sample containers provided by the laboratory. Pilot personnel wore a new
pair of disposable nitrile gloves during purging and sampling. Each container was labeled and
placed in a cooler containing ice to maintain the samples at approximately 4Celsius. The
samples were then transported to Pace Analytical (Pace)in Kernersville, North Carolina for
chemical analysis. The groundwater samples collected were analyzed for volatile organic
compounds (VOCs) using Standard Method 6200B.A chain of custody was maintained and is
included in the Appendix.
The depth to the groundwater surface in monitoring wells MW-1, MW-2, MW-3, MW-4, MW-6,
MW-7, MW-8, MW-10, MW-11, MW-14, and DW-1 was measured using a decontaminated water
level indicator. The top of casing elevation for each well was previously surveyed by others.The
previously documented monitoring well elevations were utilized to prepare a potentiometric
surface map (Drawing 6). The relative groundwater elevations collected from each monitoring
well on October 27, 2021 are provided in Tables 2 and 4. Based on data collected during the
assessment activities, the groundwater flow direction appears to be generally toward the south-
southwest beneath the site.
3.2 Water Supply Wells
Based on the information in the previous report numerous water supply wells are located within
1,000 feet of the source area of the release. Pilot attempted to contact the City of Roxboro City
Public Works Department regarding the availability of municipal water in the vicinity of the site.
The City of Roxboro Public Works Department confirmed that municipal water is available in the
vicinity of the site.Pilot also provided a list of addresses inquiring about the water usage at the
properties documented to utilize a water supply well for potable purposes but have yet to receive
a response.Information pertaining to the water supply wells is provided in Table 3 and Drawing
5.
3.3 Groundwater Modeling
Groundwater modeling was not completed and there does not appear to be a surface water
feature within 500 feet of the site.
Groundwater Monitoring Report
Duncan’s Mini Mart
Pilot Project G-7289
December 6, 2021
4
3.4 Free Product Investigation and Recovery
Free product was not encountered in the groundwater monitoring wells sampled on October
27, 2021.
4.0 LABORATORY ANALYTICAL RESULTS
4.1 Groundwater Sample Analysis
Laboratory analysis of the groundwater samples collected from monitoring wells MW-6,MW-7,
MW-8,MW-10, MW-11 and DW-1 did not detect targeted compounds above the 2L Standards.
Laboratory analysis of the groundwater samples collected from groundwater monitoring wells
MW-1, MW-2, MW-3, MW-4 and MW-14 detected several targeted compounds at
concentrations above their respective 2L Standards,with benzene exceeding its GCL in the
sample collected from monitoring well MW-2.
Isoconcentration maps for benzene,ethylbenzene,n-propylbenzene,1,2,4-trimethylbenzene,
1,3,5-trimethylbenzene, toluene, and xylenes are included as Drawings 7 through 13,
respectively.A summary of the groundwater analytical results is presented in Table 4. The
laboratory data sheets are included in the Appendix.
5.0 CONCLUSIONS
Based on the results of the Groundwater Monitoring Report,Pilot concludes the following:
Laboratory analysis of the groundwater samples collected from monitoring wells MW-6, MW-
7, MW-8, MW-10, MW-11 and DW-1 did not detect targeted compounds above the 2L
Standards.
Laboratory analysis of the groundwater samples collected from groundwater monitoring wells
MW-1, MW-2, MW-3, MW-4 and MW-14 detected several targeted compounds at
concentrations above their respective 2L Standards, with benzene exceeding its GCL in the
sample collected from monitoring well MW-2.
Free product was not detected in during this monitoring event.
The groundwater flow was calculated to be to be generally to the south-southwest.
Groundwater Monitoring Report
Duncan’s Mini Mart
Pilot Project G-7289
December 6, 2021
5
Pilot contacted the City of Roxboro Public Works Department and confirmed that municipal
water is available in the vicinity of the site. The concentrations in the groundwater will need
to decrease to below the 2L Standards for incident closure to be obtained with a Notice of
Residual Petroleum (NORP)or each residence with a potable use well connected to the
municipal water supply.
The majority of the plume of impacted groundwater appears to be confined to the site.
Based on the findings,it appears that natural attenuation is occurring,and it is Pilot’s opinion
that monitoring activities should continue at the site.
6.0 RECOMMENDATIONS
Pilot recommends that the current property owner/responsible party submit a copy of this
Groundwater Monitoring Report to the NCDEQ, UST Section for their review.Prior to a property
transaction occurring a Notice of Residual Petroleum (NORP) is required to be recorded.
7.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those
normally employed in assessment projects of this type. Our evaluation of site conditions has
been based on our understanding of the site project information and the data obtained during
our field activities.
Groundwater Monitoring Report
Duncan’s Mini Mart
Pilot Project G-7289
December 6, 2021
6
8.0 STATEMENTS AND CERTIFICATIONS
1 Enter the date the monitoring report was due.Not Established Will this report be
submitted after the established due date?
YES NO
2 Was any required information from the above template missing from this report?YES NO
3 If applicable, will any of the proposed attenuation milestones under the scheduleapproved in the Corrective Action Plan not be met?(within a reasonable margin oferror)
YES NO
N/A
4 Does any known or suspected source zone soil contamination or free product remainoutside of the assessed area that could be inhibiting natural attenuation?YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest apotential new release from a separate onsite or offsite source?YES NO
Certification:
I,Jason T. Ricks, a Licensed Geologist for Pilot Geological, PLLC, do certify that the information
contained in this report is correct and accurate to the best of my knowledge.
Pilot Geological, PLLC is licensed to practice geology in North Carolina.The certification number of
the company is C-542.
DRAWINGS
SITE
USGS Topographic Map
Duncan’s Mini Mart
1909 Burlington Road
Roxboro, Person County, NC
Pilot Project G-7289
Drawing 1
USGS Topographic Map
Hurdle Mills, NC, Olive Hill, NC,
Roxboro, NC, and Timberlake, NC
Quadrangles
Scale: 1” = 2,000’
LEGEND
Site Boundary
Site Map
Duncan’s Mini Mart
1909 Burlington Road
Roxboro, Person County, NC
Pilot Project G-7289
Drawing 2
Google Earth
Interactive Mapping Software
Scale : 1”= 80’
LEGEND
Site BoundaryU. UST Location
U
UST Location Map
Duncan’s Mini Mart
1909 Burlington Road
Roxboro, Person County, NC
Pilot Project G-7289
Drawing 3
Google Earth
Interactive Mapping Software
Scale : 1”= 15’
LEGEND
Site Boundary
UST Location
UST-3
UST-2
UST-1
UST-4
UST-5
Drawing 4Scale1:60Sample Location MapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
V
a
n
c
e

W
r
e
n
n

R
o
a
d
Drawing 5ScaleShownWater Supply WellLocation MapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289Approximate Site Boundary
Approximate Water Supply Well Location
WS-7
WS-17WS-6
WS-5
WS-4
WS-18
WS-19
WS-20
WS-3
WS-2
WS-1
WS-12
WS-8
WS-15
WS-13
WS-14WS-16
WS-10
WS-9WS-11
1,000 ft. Radius
500 ft. Radius
Drawing 6Scale1:60Potentiometric SurfaceMapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Structure
Groundwater Elevation
Contour Elevation (CI = 5.00 ft.)
Groundwater Flow Direction
Groundwater Elevation Not Available
Not Monitored
(92.12')
75.00'
(623.89')
(630.50')
( -- )
(624.19')
(623.89')
(624.04')
(623.58')
( -- )(631.95')
(624.08')
(624.11')
(NM)
(NM)
(619.41')
(NM)
(NM)
(Well Abandoned)
620'
620'
625'
625'
630'
630'
Drawing 7Scale1:60Benzene IsoconcentrationMapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
(931)
(ND)
(1,640)
(ND)
(54.1)
(7,740)
(ND)
(ND)
(ND)
(NS)
(NM)
(ND)
(NM)
(Well Abandoned)
1,000
5,000
3,000
ND
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
Concentration (ppb)
Not Sampled
Not Detected
Not Monitored
(931)
(NS)
(ND)
(NM)
Drawing 8Scale1:60EthylbenzeneIsoconcentration MapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
(2,560)
(ND)
(2,900)
(3,090)
(ND)
(2,520)
(ND)
(ND)
(ND)
(NS)
(NM)
(ND)
(NM)
(Well Abandoned)
3,
0
0
0
2,50
0
2,00
0
ND
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
Concentration (ppb)
Not Sampled
Not Detected
Not Monitored
(2,520)
(NS)
(ND)
(NM)
Drawing 9Scale1:60n-PropylbenzeneIsoconcentration MapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
(388)
(ND)
(515)
(501)
(ND)
(345)
(ND)
(ND)
(ND)
(NS)
(NM)
(ND)
(NM)
(Well Abandoned)
ND
300
400
500
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
Concentration (ppb)
Not Sampled
Not Detected
Not Monitored
(388)
(NS)
(ND)
(NM)
Drawing 10Scale1:601,2,4-TrimethylbenzeneIsoconcentration MapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
(2,760)
(ND)
(4,020)
(3,580)
(ND)
(2,530)
(ND)
(ND)
(ND)
(NS)
(NM)
(ND)
(NM)
(Well Abandoned)
ND
2,000
3,
0
0
0
4
,
0
0
0
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
Concentration (ppb)
Not Sampled
Not Detected
Not Monitored
(2,760)
(NS)
(ND)
(NM)
Drawing 11Scale1:601,3,5-TrimethylbenzeneIsoconcentration MapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
(720)
(ND)
(1,010)
(843)
(ND)
(649)
(ND)
(ND)
(ND)
(NS)
(NM)
(ND)
(NM)
(Well Abandoned)
ND
600
800
1,
0
0
0
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
Concentration (ppb)
Not Sampled
Not Detected
Not Monitored
(720)
(NS)
(ND)
(NM)
Drawing 12Scale1:60Toluene IsoconcentrationMapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
(15,400)
(ND)
(15,500)
(25,800)
(ND)
(77,600)
(ND)
(ND)
(ND)
(NS)
(NM)
(ND)
(NM)
(Well Abandoned)
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
Concentration (ppb)
Not Sampled
Not Detected
Not Monitored
(15,400)
(NS)
(ND)
(ND)
60,000
45,000
30,000
15,000
ND
(NM)
Drawing 13Scale1:60Xylenes IsoconcentrationMapDuncan's Mini Mart1909 Burlington RoadRoxboro, North CarolinaG-7289600 Burlington RoadMW-1
MW-14
MW-3
MW-2
MW-4
MW-6
MW-7
MW-10
MW-11
MW-13
MW-9
MW-12
MW-5
MW-8
DW-1
V
a
n
c
e

W
r
e
n
n

R
o
a
d
(12,480)
(ND)
(15,500)
(13,970)
(ND)
(12,240)
(ND)
(ND)
(ND)
(ND)
(NS)
(NM)
(ND)
(NM)
(Well Abandoned)
11,000
13,
0
0
0
ND
15
,
0
0
0
Approximate Site Boundary
Type II Monitoring Well Location
Type III Monitoring Well Location
Water Supply Well Location
Structure
Dispenser Island
Concentration (ppb)
Not Sampled
Not Detected
Not Monitored
(1,380)
(NS)
(ND)
(NM)
TABLES
UST ID
Number Owner Last
Contents
Previous
Contents
Capacity
(in Gallons)
Construction
Details
Tank
Dimensions
Installation
Date Status Release
Unknown 1/1/1964 Current Unknown4DieselDiesel1,000 Single Wall
Steel
1/1/1964 Current Unknown
McLeod Oil Company
PO Box 100
Mebane, North Carolina 27302
5 Kerosene Kerosene 2,000 Single Wall
Steel Unknown
4,000
2 Gasoline Gasoline 4,000
Single Wall
Steel
Table 1 - UST Information
Duncans Mini Mart
Roxboro, North Carolina
5/1/1985 Current Unknown1GasolineGasoline4,000 Single Wall
Steel Unknown
5/1/1985 Current Unknown
3 Gasoline Gasoline
Single Wall
Steel Unknown
Unknown 5/1/1985 Current Unknown
ID Number Date
Installed
Well
Depth
(feet TOC)
Screened
Interval
(feet TOC)
Well
Diameter
(inches)
Well
Elevation
(feet TOC)
Depth to
Groundwater
(feet TOC)
10/27/21
Product
Thickness
(feet)
10/27/21
Groundwater Elevation
(feet TOC)
10/27/21
MW-1 11/14/2001 35 15-35 2 649.22 25.33 N/A 623.89
MW-2 11/15/2001 35 15-35 2 649.49 25.45 N/A 624.04
MW-3 3/13/2002 40 20-40 2 649.39 25.20 N/A 624.19
MW-4 3/13/2002 40 20-40 2 649.32 25.43 N/A 623.89
MW-5 1/20/2003 35 10-35 2 643.41 NM N/A NM
MW-6 1/21/2003 40 6-40 2 648.94 24.83 N/A 624.11
MW-7 1/22/2003 40 15-40 2 649.75 23.28 N/A 624.08
MW-8 1/22/2003 40 15-40 2 640.88 21.47 N/A 619.41
MW-9 1/22/2003 35 7-35 2 636.18 NM N/A NM
MW-10 1/22/2003 40 10-40 2 650.05 18.12 N/A 631.93
MW-11 1/21/2003 40 10-40 2 648.62 18.12 N/A 630.50
MW-12 2/12/2003 35 10-35 2 634.10 NM N/A NM
MW-13 2/12/2003 35 10-35 2 636.20 NM N/A NM
MW-14 7/31/2003 45 5-45 6 --24.86 N/A --
*DW-1 3/18/2002 90 85-90 2 649.75 26.17 N/A 623.58
NF = Not Found
FP = Free Product
NM = Not Measured
-- = Not Available
N/A = Not Applicable
* = Type III Well - Not used in the groundwater flow calculation
Table 2 - Monitoring Well Construction Information
Duncan's Mini Mart
Roxboro, North Carolina
Historical information detailing monitoring well construction and Top of Casing (TOC) elevation obtained from Groundwater Monitoring Report,
Progress Environmental, October 20, 2020
WELL ID OWNER NAME PROPERTY ADDRESS MAILING ADDRESS (DURHAM, NC 27704)TELEPHONE NUMBERWELL DEPTH (FT.)APPROXIMATE DISTANCE OF WELL FROM SOURCE AREA (FT.)WELL USAGECONNECTED TO MUNICIPAL WATERWS-1 Viriginia Wrenn 1941 Burlington Road64 Vance Wrenn RoadBurlington, NC 27573Unknown--242 Not UsedUnknownWS-1 Viriginia Wrenn 46 Vance Wrenn Road46 Vance Wrenn Road Roxboro, NC 27573Unknown --242 UnknownUnknownWS-2 Blaine Fannie Talley Estate 201 Vance Wrenn Road2901 Scuoppernong LaneDurham, NC 27703Unknown--968DomesticWater SupplyUnknownWS-3 Viriginia Wrenn 46 Vance Wrenn Road46 Vance Wrenn Road Roxboro, NC 27573Unknown --310 Not UsedUnknownWS-4 Douglas Kibbey 1916 Burlington Road1916 Burlington RoadRoxboro, NC 27573Unknown--176DomesticWater SupplyUnknownWS-5 David Evans 1894 Burlington Road1894 Burlington RoadRoxboro, NC 27573Unknown--383DomesticWater SupplyUnknownWS-6 Dawn Oakley Whitt 1864 Burlington Road1864 Burlington RoadRoxboro, NC 27573Unknown--295DomesticWater SupplyUnknownWS-7 Robert Charles Carter 1786 Burlington Road1786 Burlington RoadRoxboro, NC 27573Unknown--603DomesticWater SupplyUnknownWS-8 Samuel Carroll 2002 Burlington Road2002 Burlington RoadRoxboro, NC 27573Unknown--693DomesticWater SupplyUnknownWS-9 Bradley Laws 2042 Burlington Road2042 Burlington RoadRoxboro, NC 27573Unknown--810 Not UsedUnknownWS-10 Lowell Oakley, Jr. 2082 Burlington Road2082 Burlington RoadRoxboro, NC 27573Unknown--693 Not UsedUnknownWS-11 Lowell Oakley, Jr. 2082 Burlington Road2082 Burlington RoadRoxboro, NC 27573Unknown--810 Not UsedUnknownWS-12 Ronnie L. Chandler 1975 Burlington Road1975 Burlington RoadRoxboro, NC 27573Unknown--440DomesticWater SupplyUnknownWS-13 Ronnie L. ChandlerSolomon CourtApartments2082 Burlington RoadRoxboro, NC 27573Unknown--640DomesticWater SupplyUnknownWS-14 Ronnie L. ChandlerSolomon CourtApartments2082 Burlington RoadRoxboro, NC 27573Unknown--640DomesticWater SupplyUnknownWS-15 Bruce Solomon 2029 Burlington Road2029 Burlington RoadRoxboro, NC 27573Unknown--652DomesticWater SupplyUnknownWS-16 Carroll Sumner 2071 Burlington Road2073 Burlington RoadRoxboro, NC 27573Unknown--860 Not UsedUnknownWS-16 Carroll Sumner 2073 Burlington Road2073 Burlington RoadRoxboro, NC 27573Unknown--860 Not UsedUnknownWS-17 Mitzi Warren Sherwood 1801 Burlington Road3608 Fernwood RoadRaleigh, NC 27612Unknown--578DomesticWater SupplyUnknownWS-18Ann Long Pergerson Life Estate1835 Burlington Road1801 Burlington RoadRoxboro, NC 27573Unknown--425DomesticWater SupplyUnknownWS-19Poindexter Property Management1865 Burlington RoadPO Box 677Roxboro, NC 27573Unknown--450DomesticWater SupplyUnknownWS-20Poindexter Property Management1883 Burlington RoadPO Box 677Roxboro, NC 27573Unknown --450DomesticWater SupplyUnknown-- = Not AvailableSee Drawing 5Information was obtained from Groundwater Monitorng Report, Progress Environmental, October 20, 2020Table 3 - Water Supply Well InformationDuncan's Mini MartRoxboro, North Carolina
Table 4 - Summary of Groundwater Analytical ResultsDuncan's Mini MartRoxboro, North Carolina504.1 3030/200.7Monitoring Well IDApproximate Water Level (ft BGS)Groundwater Elevation (ft. above msl)Sample Collection DateBenzene2-ButanoneChloroform1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene (1,1-Dichloroethylene)EthylbenzeneEDB2-HexanoneIsopropyl etherI-Propylbenzene (Isopropylbenzene)4-Methyl-2-Pentanone (Methyl isobutyl ketone - MIBK)Methyl tert-butyl ether (MTBE)Naphthalenen-Propylbenzenep-Isopropyltoluene (p-Cymene)n-Butylbenzenesec-Butylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenecis-1,2-DichloroetheneTetrachloroethene (Tetrachloroethylene)Trichloroethene (Trichloroethylene)Tert-amyl AlcoholTolueneXylenesEDBLead31.68617.5411/26/20016,430NA<1NA<1,000NA2,241NANA<1,000NANA1,485339NANANABQLNANANANANANA28,8249,7489<527.39621.831/27/200313,283NA<1NA<2,000NA2,740NANA<2,000NANA2,383269NANANABQLNANANANANANA47,31312,331--<519.17630.058/12/20037,708NA<1NA--NA2,060NANA171NANA4,766632NANANABQLNANANANANANA23,1389,62083--19.51629.719/4/20039,630NA<1NA--NA1,904NANA160NANA3,700532NANANABQLNANANANANANA29,0649,03179--28.11621.1110/14/200811,400NA<1NA<1NA3,170NANA<5NANA<5NANANANABQLNANANANANANA40,80010,300NANA29.60619.6210/27/201110,600BQLBQLBQLBQLBQL2,43033.31606.5J100BQLBQL550280BQLBQLBQL2,200508BQLBQLBQLNA37,70011,200NANA24.60624.625/23/20137,890BQLBQLBQLBQLBQL1,89037.5J148JBQL70JBQL1,940540238BQLBQLBQL2,180598BQLBQLBQL4,370J32,6009,970NANA25.10624.121/8/20148,030BQLBQLBQLBQLBQL2,390BQLBQLBQLBQLBQL2,370560250JBQLBQLBQL2,590680BQLBQLBQLBQL35,20012,700NANA21.40627.824/23/20155,410BQLBQLBQLBQLBQL2,070BQLBQLBQLBQLBQL1,7501,190BQLBQLBQLBQL2,810690BQLBQLBQLBQL33,00012,200NANA24.53624.6911/11/20155,100BQLBQLBQLBQLBQL2,280BQLBQLBQLBQLBQL500715300BQLBQLBQL2,430618BQLBQLBQLBQL23,80010,400NANA26.14623.0810/12/20173,040BQLBQLBQLBQLBQL2,350BQLBQLBQLBQLBQLBQL1,020335BQLBQLBQL2,490668BQLBQLBQLBQL34,70010,800NANA14.04635.185/7/20192,770BQLBQLBQLBQLBQL3,040BQLBQLBQL104BQL296924368BQLBQLBQL3,630834BQLBQLBQLBQL37,40015,800NANA22.68626.549/24/20201,400BQLBQLBQLBQLBQL2,030BQLBQLBQLBQLBQLBQL585268BQLBQLBQL2,220572BQLBQLBQLBQL22,20010,100NANA25.33623.8910/27/2021931NDNDNDNDND2,560NDNDND118NDND755388NDNDND2,760720NDNDNDND15,40012,480NANA31.76617.7311/26/200110,168NA<1NA<2,000NA2,568NANA<2,000NANA6,301280NANANABQLNANANANANANA69,25611,1781.61027.67621.821/27/200311,764NA<1NA<2,000NA2,605NANA<2,000NANA9,002236NANANABQLNANANANANANA75,99811,245--<519.45630.048/12/200310,300NA<1NA--NA2,184NANA491NANA8,600616NANANABQLNANANANANANA54,5009,938<50--19.75629.749/4/200311,300NA<1NA--NA2,170NANA<50NANA8,050465NANANABQLNANANANANANA54,4009,896<50--28.36621.1310/14/200810,900NA<1NA<1NA5,050NANA<5NANA<5NANANANABQLNANANANANANA72,10014,100NANA29.74619.7510/27/201111,0001,680BQLBQLBQLBQL2,350BQL29033.399.81278,04053528021.8BQLBQL2,150524BQLBQLBQLNA69,70011,000NANA24.95624.545/23/201311,600BQLBQLBQLBQLBQL2,470BQLBQL50J90JBQL12,800580310BQLBQLBQL2,340605BQLBQLBQL52,30088,10011,400NANA25.52623.971/8/20149,580BQLBQLBQLBQLBQL2,420BQLBQLBQLBQLBQL10,500480J260JBQLBQLBQL2,590680BQLBQLBQL41,800J84,90012,200NANA21.38628.114/23/20159,900BQLBQLBQLBQLBQL2,260BQLBQLBQLBQLBQL7,640415265BQLBQLBQL2,050550BQLBQLBQLBQL72,30010,600NANA24.92624.5711/11/20158,080BQLBQLBQLBQLBQL2,060BQLBQLBQLBQLBQL8,890520250BQLBQLBQL2,060480BQLBQLBQLBQL52,7009,850NANA26.23623.2610/12/20178,480BQLBQLBQLBQLBQL2,520BQLBQLBQLBQLBQL11,200860330BQLBQLBQL2,650685BQLBQLBQLBQL82,1006,520NANA14.24635.255/7/20199,370BQLBQLBQLBQLBQL2,020BQLBQLBQLBQLBQL15,200395BQLBQLBQLBQL2,340555BQLBQLBQLBQL74,70010,500NANA22.92626.579/24/20206,200BQLBQLBQLBQLBQL1,990BQLBQLBQLBQLBQL29,800470BQLBQLBQLBQL2,000535BQLBQLBQLBQL58,00010,000NANA25.45624.0410/27/20217,740NDNDNDNDND2,520NDNDNDNDND9,910ND345NDNDND2,530649NDNDNDND77,60012,240NANA30.28619.113/26/20021,554NA<1NA<1,000NA3,552NANA<1,000NANA<1,0001,269NANANABQLNANANANANANA57,42715,3410.34627.52621.871/27/2003<2,000NA<1NA<2,000NA3,600NANA<2,000NANA<2,000881NANANABQLNANANANANANA49,41715,790--<519.26630.138/12/2003560NA<1NA--NA1,496NANA78NANA134485NANANABQLNANANANANANA14,9085,699<10--19.55629.849/4/20031,399NA<1NA--NA2,017NANA160NANA<10521NANANABQLNANANANANANA32,9808,854<10--28.25621.1410/14/20082,660NA<1NA<1NA3,950NANA<5NANA<5NANANANABQLNANANANANANA32,50010,400NANA29.54619.8510/27/2011619BQLBQLBQLBQLBQL2,940BQL545BQL159BQLBQL78646939.8BQLBQL3,730797BQLBQLBQLNA31,80013,500NANA24.66624.735/23/201341JBQLBQLBQLBQLBQL62BQLBQLBQLBQLBQLBQL30J24JBQLBQL188274115BQLBQLBQLBQL522425NANA25.38624.011/8/20141.12BQLBQLBQLBQLBQL1.85BQLBQLBQLBQLBQLBQL0.610.25JBQLBQLBQL7.512.85BQLBQLBQLBQL20.423.5NANA21.25628.144/23/20156.6BQLBQLBQLBQLBQL25.6BQLBQLBQL2.8BQLBQL10.17.7BQLBQLBQL81.815.3BQLBQLBQLBQL58.2107NANA25.94623.4511/11/2015881BQLBQLBQLBQLBQL1,090BQL225BQL57BQL59641317619.5BQLBQL1,580504BQLBQLBQLBQL14,6005,600NANA25.94623.4510/12/20171,290BQLBQLBQLBQLBQL2,640BQLBQLBQL125BQL252742392BQL23.3BQL3,020839BQLBQLBQLBQL43,40011,900NANA13.82635.575/7/2019635BQLBQLBQLBQLBQL2,580BQLBQLBQL93BQLBQL679307BQLBQLBQL2,950762BQLBQLBQLBQL28,70011,000NANA22.63626.769/24/2020226BQLBQLBQLBQLBQL2,720BQLBQLBQL132BQLBQL740414BQLBQLBQL3,310904BQLBQLBQLBQL23,60012,800NANA25.20624.1910/27/2021NDNDNDNDNDND3,090NDNDND139NDND745501NDNDND3,580843NDNDNDND25,80013,970NANA30.40618.923/26/2002297NA<1NA35NA<20NANA21NANA53<10NANANABQLNANANANANANA5622110.31126.57622.751/27/20031,143NA<1NA<50NA<50NANA<50NANA5931NANANABQLNANANANANANA<50282--<519.46629.868/12/2003477NA<1NA--NA<1NANA9.9NANA1738NANANABQLNANANANANANA3.770.41.9--19.71629.619/4/2003454NA<1NA--NA<1NANA13NANA7928NANANABQLNANANANANANA3.778.94.4--28.30621.0210/14/20082,910NA<1NA<1NA186NANA<5NANA2,130NANANANABQLNANANANANANA142563NANA29.68619.6410/27/20112,790BQLBQL3.14223863.2BQLBQL12079.9BQL4,49017527.43.429BQL18.1BQLBQLBQLBQLNA9.29122NANA24.87624.455/23/2013540BQLBQL2.1J1483.2J671BQLBQL83.642BQL5,99052.517.32.20J6.88.230.76.4BQLBQL1.6J7,620BQL101NANA25.52623.801/8/20141,160BQLBQLBQL211BQL71BQLBQL10752BQL8,5308121.0JBQLBQLBQL33.0JBQLBQLBQLBQL8,210BQL86NANA21.37627.954/23/201543.2BQLBQLBQL101BQLBQLBQLBQL63.218.5BQL4,610BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA24.90624.4211/11/2015323BQLBQLBQL1422.7511.7BQLBQL10342.3BQL7,5404812.1BQL6.056.510.310.9BQLBQLBQLBQL2.919.1NANA26.16623.1610/12/2017370BQLBQLBQL176BQL7.1BQLBQL10545.7BQL8,33035.79.7BQL5.18.18.45BQLBQLBQLBQLBQL2.845.8NANA14.34634.985/7/201954.7BQLBQLBQL78.2BQLBQLBQLBQL46.6BQLBQL4,380BQLBQLBQLBQLBQL5.9BQLBQLBQLBQLBQL9.311.7NANA22.96626.369/24/202094.8BQLBQLBQL102BQL5.4BQLBQL7.117.8BQL26,30014.4BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA25.43623.8910/27/202154.1NDNDND120NDNDNDND76.0NDND10,800NDNDNDNDNDNDNDNDNDNDNDNDNDNANA21.64621.771/27/20031.2NA<1NA<1NA<1NANA<1NANA2<10NANANABQLNANANANANANA6<3<10<514.08629.339/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--22.38621.0310/14/2008<1NA<1NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA<1<1NANA24.04619.3710/27/2011BQLBQL0.59BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNABQLBQLNANA18.90624.5111/11/2015BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA26.49622.451/27/2003<1NA<1NA<1NA<1NANA<1NANA<1<10NANANABQLNANANANANANA<1<3<10<518.63630.319/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--27.72621.2210/14/2008<1NA<1NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA<1<1NANA29.10619.8410/27/2011BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNABQLBQLNANA24.16624.7811/11/2015BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA25.52623.4210/12/2017BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA14.12634.825/7/2019BQLBQL0.63BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA22.53626.419/24/2020BQLBQL0.62BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA24.83624.1110/27/2021NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANA27.40622.351/27/2003<1NA<1NA<1NA<1NANA<1NANA<1<10NANANABQLNANANANANANA<1<3<10<519.70630.059/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--28.51621.2410/14/2008<1NA2.8NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA<1<1NANA29.97619.7810/27/2011BQLBQL1.84BQLBQLBQLBQL0.23JBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNABQLBQLNANA25.00624.755/23/2013BQLBQL1.5BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA24.89624.8611/11/2015BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA26.45623.3010/12/2017BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA14.19635.565/7/2019BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA23.28626.479/24/2020BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL3.72BQLNANA25.67624.0810/27/2021NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANA21.11619.771/27/2003<1NA<1NA<1NA<1NANA<1NANA<1<10NANANABQLNANANANANANA<1<3<10<514.28626.609/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--21.54619.3410/14/2008<1NA<1NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA<1<1NANA25.57615.3110/27/2011BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNABQLBQLNANA17.26623.6211/11/2015BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA22.90617.9810/12/2017BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA9.72631.165/7/2019BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA18.00622.889/24/2020BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA21.47619.4110/27/2021NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANA16.35619.831/27/200349NA<1NA<10NA105NANA<10NANA<1022NANANABQLNANANANANANA4054080.061<59.59626.599/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--NFNM10/14/2008NFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNANFNFNFNF19.62630.431/27/2003<1NA<1NA<1NA<1NANA<1NANA<1<10NANANABQLNANANANANANA<1<3<0.02<512.21637.849/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--22.19627.8610/14/2008<1NA<1NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA<1<1NANA23.36626.6910/27/2011BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNABQLBQLNANA17.91632.1411/11/2015BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA19.27630.7810/12/2017BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA7.92642.135/7/2019BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA15.41634.649/24/2020BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA18.12631.9310/27/2021NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANATargeted Compound6200BMW-1MW-4MW-3MW-6MW-5MW-8MW-7MW-10MW-9MW-2
Table 4 - Summary of Groundwater Analytical ResultsDuncan's Mini MartRoxboro, North Carolina504.1 3030/200.7Monitoring Well IDApproximate Water Level (ft BGS)Groundwater Elevation (ft. above msl)Sample Collection DateBenzene2-ButanoneChloroform1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethene (1,1-Dichloroethylene)EthylbenzeneEDB2-HexanoneIsopropyl etherI-Propylbenzene (Isopropylbenzene)4-Methyl-2-Pentanone (Methyl isobutyl ketone - MIBK)Methyl tert-butyl ether (MTBE)Naphthalenen-Propylbenzenep-Isopropyltoluene (p-Cymene)n-Butylbenzenesec-Butylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzenecis-1,2-DichloroetheneTetrachloroethene (Tetrachloroethylene)Trichloroethene (Trichloroethylene)Tert-amyl AlcoholTolueneXylenesEDBLeadTargeted Compound6200B18.58630.041/27/2003<1NA<1NA<1NA<1NANA<1NANA<1<10NANANABQLNANANANANANA<1<3<10<511.49637.139/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--21.40627.2210/14/2008<1NA<1NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA<1<1NANA22.75625.8710/27/2011BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL0.43J1.880.18JNABQLBQLNANA17.88630.745/23/2013BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL0.29JBQLBQLBQLBQLNANA16.80631.8211/11/2015BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA18.55630.0710/12/2017BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA6.86641.765/7/2019BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA16.18632.449/24/2020BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA18.12630.5010/27/2021NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANA15.72618.382/13/2003<1NA<1NA<1NA<1NANA<1NANA<1<5.4NANANABQLNANANANANANA<1<1<0.0193111.24622.869/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--NFNM10/14/2008NFNA<1NANFNANFNANANFNANANFNFNANANABQLNANANANANANANFNFNFNFNFNM10/27/2011NFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFNFBQLNFNFNFNFNFNANFNFNFNF15.20621.002/13/2003<1NA<1NA<1NA<1NANA<1NANA<1<5.4NANANABQLNANANANANANA<1<1<0.01988.41627.799/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--17.57618.6310/14/2008<1NA<1NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA<1<1NANA19.41616.7910/27/2011BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNABQLBQLNANANS--10/14/2008NSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSNSBQLNSNSNSNSNSNANSNSNSNS----10/27/2011FPFPFPFPFPFPFPFPFPFPFPFPFPFPFPFPFPBQLFPFPFPFPFPNAFPFPFPFP24.35--5/23/20136,560BQLBQLBQLBQLBQL2,870BQLBQLBQL130JBQL2,650730490JBQLBQLBQL3,630900BQLBQLBQL9,110J70,10013,200NANA24.94--1/8/20145,580BQLBQLBQLBQLBQL2,740BQLBQLBQL100JBQL3,730760440JBQLBQLBQL3,980970BQLBQLBQLBQL78,10013,700NANA24.94--1/8/20143,430BQLBQLBQLBQLBQL1,970BQLBQLBQLBQLBQL930695390BQLBQLBQL3,280895BQLBQLBQLBQL45,10010,700NANA24.25--11/11/20153,690BQLBQLBQLBQLBQL1,510BQLBQLBQLBQLBQL650545250BQLBQLBQL2,110575BQLBQLBQLBQL39,2008,300NANANM--10/12/20173,980BQLBQLBQLBQLBQL2,680BQLBQLBQLBQLBQLBQL805400BQLBQLBQL3,280875BQLBQLBQLBQL70,70012,600NANANM--5/7/20191,760BQLBQLBQLBQLBQL2,020BQLBQLBQLBQLBQL325760375BQLBQLBQL4,0001,050BQLBQLBQLBQL54,50011,400NANA22.22--9/24/20201,620BQLBQLBQLBQLBQL2,110BQLBQLBQLBQLBQLBQL640340BQLBQLBQL3,220875BQLBQLBQLBQL46,40011,900NANA24.86--10/27/20211,620NDNDNDNDND2,900NDNDNDNDNDNDND515NDNDND4,0201,010NDNDNDND52,40015,500NANA30.75619.003/26/20028.6NA<1NA<1NA<1NANA<1NANA<1<10NANANABQLNANANANANANA210.40.04<527.90621.851/27/2003<1NA<1NA<1NA<1NANA<1NANA<1<10NANANABQLNANANANANANA<1<3--<520.24629.519/4/2003<1NA<1NA--NA<1NANA<1NANA<1<1NANANABQLNANANANANANA<1<3<1--28.72621.0310/14/20081NA<1NA<1NA<1NANA<5NANA<5NANANANABQLNANANANANANA1.4<1NANA30.31619.4410/27/2011BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL0.43JBQLBQLBQLBQL0.15JBQLBQLBQLBQLNA0.38J0.11JNANA21.65628.101/8/2014BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQL0.97BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNA1.14BQLNANA25.07624.6811/11/2015BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA26.92622.8310/12/2017BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA14.98634.775/7/2019BQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLBQLNANA23.59626.169/24/20200.6BQLBQLBQLBQLBQL0.68BQLBQLBQLBQLBQLBQL0.56BQLBQLBQLBQL1.07BQLBQLBQLBQLBQL7.113.62NANA26.17623.5810/27/2021NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNANAWS-4 -- -- 10/27/2021 ND ND2.6ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NAWS-5 -- -- 10/27/2021 ND ND1.2ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NAWS-6 -- -- 10/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NAWS-12 -- -- 10/27/2021 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NDND ND ND ND ND ND ND ND ND ND NA NA14,0007060.43506000.0240707010020670257070400400600.73406005000.02155,0004,000,00070,0006,000400350,00080,0005040,00070,00030,500100,00020,0006,00026,10011,7005,9008,80028,50024,10060,0007003,00040,000260,00050,0005015,000= Concentration Exceeds the 2L Standard= Concentration Exceeds the GCLsppb = Parts Per BillionBGS = Below Ground SurfaceN/A = Not ApplicableNS = Not SampledND = Not DetectedBQL = Below Quantitation LimitNA = Not Analyzed* = Type III Well-- = Not AvailableNE = Not EstablishedFP = Free ProductNF = Not FoundGCLs (ug/L)MW-12MW-11MW-14MW-132L Standard (ug/L)*DW-1
APPENDIX
#=CL#
November 04, 2021
LIMS USE: FR - JASON RICKS
LIMS OBJECT ID: 92569107
92569107
Project:
Pace Project No.:
RE:
Jason Ricks
Pilot Geological
P.O. Box 128
Kernersville, NC 27285
Pilot Geo G-7289
Dear Jason Ricks:
Enclosed are the analytical results for sample(s) received by the laboratory on October 27, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 48
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 48
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Lab ID Sample ID Matrix Date Collected Date Received
92569107001 MW-1 Water 10/27/21 11:45 10/27/21 15:45
92569107002 MW-2 Water 10/27/21 10:30 10/27/21 15:45
92569107003 MW-3 Water 10/27/21 10:15 10/27/21 15:45
92569107004 MW-4 Water 10/27/21 11:30 10/27/21 15:45
92569107005 MW-6 Water 10/27/21 12:05 10/27/21 15:45
92569107006 MW-7 Water 10/27/21 12:25 10/27/21 15:45
92569107007 MW-8 Water 10/27/21 11:15 10/27/21 15:45
92569107008 MW-10 Water 10/27/21 12:15 10/27/21 15:45
92569107009 MW-11 Water 10/27/21 12:45 10/27/21 15:45
92569107010 MW-14 Water 10/27/21 09:45 10/27/21 15:45
92569107011 DW-1 Water 10/27/21 10:40 10/27/21 15:45
92569107012 WS-4 Water 10/27/21 10:50 10/27/21 15:45
92569107013 WS-5 Water 10/27/21 11:10 10/27/21 15:45
92569107014 WS-6 Water 10/27/21 11:20 10/27/21 15:45
92569107015 WS-12 Water 10/27/21 13:00 10/27/21 15:45
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 48
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92569107001 MW-1 SM 6200B 63 PASI-CSAS
92569107002 MW-2 SM 6200B 63 PASI-CSAS
92569107003 MW-3 SM 6200B 63 PASI-CSAS
92569107004 MW-4 SM 6200B 63 PASI-CSAS
92569107005 MW-6 SM 6200B 63 PASI-CSAS
92569107006 MW-7 SM 6200B 63 PASI-CSAS
92569107007 MW-8 SM 6200B 63 PASI-CSAS
92569107008 MW-10 SM 6200B 63 PASI-CSAS
92569107009 MW-11 SM 6200B 63 PASI-CSAS
92569107010 MW-14 SM 6200B 63 PASI-CSAS
92569107011 DW-1 SM 6200B 63 PASI-CSAS
92569107012 WS-4 SM 6200B 63 PASI-CSAS
92569107013 WS-5 SM 6200B 63 PASI-CSAS
92569107014 WS-6 SM 6200B 63 PASI-CSAS
92569107015 WS-12 SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-1 Lab ID:92569107001 Collected:10/27/21 11:45 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 931 ug/L 10/30/21 16:24 71-43-262.5 125
Bromobenzene ND ug/L 10/30/21 16:24 108-86-162.5 125
Bromochloromethane ND ug/L 10/30/21 16:24 74-97-562.5 125
Bromodichloromethane ND ug/L 10/30/21 16:24 75-27-462.5 125
Bromoform ND ug/L 10/30/21 16:24 75-25-262.5 125
Bromomethane ND ug/L 10/30/21 16:24 74-83-9625125
n-Butylbenzene ND ug/L 10/30/21 16:24 104-51-862.5 125
sec-Butylbenzene ND ug/L 10/30/21 16:24 135-98-862.5 125
tert-Butylbenzene ND ug/L 10/30/21 16:24 98-06-662.5 125
Carbon tetrachloride ND ug/L 10/30/21 16:24 56-23-562.5 125
Chlorobenzene ND ug/L 10/30/21 16:24 108-90-762.5 125
Chloroethane ND ug/L 10/30/21 16:24 75-00-3125125
Chloroform ND ug/L 10/30/21 16:24 67-66-362.5 125
Chloromethane ND ug/L 10/30/21 16:24 74-87-3125125
2-Chlorotoluene ND ug/L 10/30/21 16:24 95-49-862.5 125
4-Chlorotoluene ND ug/L 10/30/21 16:24 106-43-462.5 125
1,2-Dibromo-3-chloropropane ND ug/L 10/30/21 16:24 96-12-8125125
Dibromochloromethane ND ug/L 10/30/21 16:24 124-48-162.5 125
1,2-Dibromoethane (EDB)ND ug/L 10/30/21 16:24 106-93-462.5 125
Dibromomethane ND ug/L 10/30/21 16:24 74-95-362.5 125
1,2-Dichlorobenzene ND ug/L 10/30/21 16:24 95-50-162.5 125
1,3-Dichlorobenzene ND ug/L 10/30/21 16:24 541-73-162.5 125
1,4-Dichlorobenzene ND ug/L 10/30/21 16:24 106-46-762.5 125
Dichlorodifluoromethane ND ug/L 10/30/21 16:24 75-71-862.5 125
1,1-Dichloroethane ND ug/L 10/30/21 16:24 75-34-362.5 125
1,2-Dichloroethane ND ug/L 10/30/21 16:24 107-06-262.5 125
1,1-Dichloroethene ND ug/L 10/30/21 16:24 75-35-462.5 125
cis-1,2-Dichloroethene ND ug/L 10/30/21 16:24 156-59-262.5 125
trans-1,2-Dichloroethene ND ug/L 10/30/21 16:24 156-60-562.5 125
1,2-Dichloropropane ND ug/L 10/30/21 16:24 78-87-562.5 125
1,3-Dichloropropane ND ug/L 10/30/21 16:24 142-28-962.5 125
2,2-Dichloropropane ND ug/L 10/30/21 16:24 594-20-762.5 125
1,1-Dichloropropene ND ug/L 10/30/21 16:24 563-58-662.5 125
cis-1,3-Dichloropropene ND ug/L 10/30/21 16:24 10061-01-562.5 125
trans-1,3-Dichloropropene ND ug/L 10/30/21 16:24 10061-02-662.5 125
Diisopropyl ether ND ug/L 10/30/21 16:24 108-20-362.5 125
Ethylbenzene 2560 ug/L 10/30/21 16:24 100-41-462.5 125
Hexachloro-1,3-butadiene ND ug/L 10/30/21 16:24 87-68-3250125
Isopropylbenzene (Cumene)118 ug/L 10/30/21 16:24 98-82-862.5 125
Methylene Chloride ND ug/L 10/30/21 16:24 75-09-2250125
Methyl-tert-butyl ether ND ug/L 10/30/21 16:24 1634-04-462.5 125
Naphthalene 755 ug/L 10/30/21 16:24 91-20-3250125
n-Propylbenzene 388 ug/L 10/30/21 16:24 103-65-162.5 125
Styrene ND ug/L 10/30/21 16:24 100-42-562.5 125
1,1,1,2-Tetrachloroethane ND ug/L 10/30/21 16:24 630-20-662.5 125
1,1,2,2-Tetrachloroethane ND ug/L 10/30/21 16:24 79-34-562.5 125
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-1 Lab ID:92569107001 Collected:10/27/21 11:45 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 10/30/21 16:24 127-18-462.5 125
Toluene 15400 ug/L 10/30/21 16:24 108-88-362.5 125
1,2,3-Trichlorobenzene ND ug/L 10/30/21 16:24 87-61-6250125
1,2,4-Trichlorobenzene ND ug/L 10/30/21 16:24 120-82-1250125
1,1,1-Trichloroethane ND ug/L 10/30/21 16:24 71-55-662.5 125
1,1,2-Trichloroethane ND ug/L 10/30/21 16:24 79-00-562.5 125
Trichloroethene ND ug/L 10/30/21 16:24 79-01-662.5 125
Trichlorofluoromethane ND ug/L 10/30/21 16:24 75-69-4125125
1,2,3-Trichloropropane ND ug/L 10/30/21 16:24 96-18-462.5 125
1,2,4-Trimethylbenzene 2760 ug/L 10/30/21 16:24 95-63-662.5 125
1,3,5-Trimethylbenzene 720 ug/L 10/30/21 16:24 108-67-862.5 125
Vinyl chloride ND ug/L 10/30/21 16:24 75-01-4125125
m&p-Xylene 8640 ug/L 10/30/21 16:24 179601-23-1125125
o-Xylene 3840 ug/L 10/30/21 16:24 95-47-662.5 125
Surrogates
1,2-Dichloroethane-d4 (S)96 %10/30/21 16:24 17060-07-070-130 125
4-Bromofluorobenzene (S)99 %10/30/21 16:24 460-00-470-130 125
Toluene-d8 (S)101 %10/30/21 16:24 2037-26-570-130 125
Sample:MW-2 Lab ID:92569107002 Collected:10/27/21 10:30 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 7740 ug/L 10/30/21 16:59 71-43-2250500
Bromobenzene ND ug/L 10/30/21 16:59 108-86-1250500
Bromochloromethane ND ug/L 10/30/21 16:59 74-97-5250500
Bromodichloromethane ND ug/L 10/30/21 16:59 75-27-4250500
Bromoform ND ug/L 10/30/21 16:59 75-25-2250500
Bromomethane ND ug/L 10/30/21 16:59 74-83-92500500
n-Butylbenzene ND ug/L 10/30/21 16:59 104-51-8250500
sec-Butylbenzene ND ug/L 10/30/21 16:59 135-98-8250500
tert-Butylbenzene ND ug/L 10/30/21 16:59 98-06-6250500
Carbon tetrachloride ND ug/L 10/30/21 16:59 56-23-5250500
Chlorobenzene ND ug/L 10/30/21 16:59 108-90-7250500
Chloroethane ND ug/L 10/30/21 16:59 75-00-3500500
Chloroform ND ug/L 10/30/21 16:59 67-66-3250500
Chloromethane ND ug/L 10/30/21 16:59 74-87-3500500
2-Chlorotoluene ND ug/L 10/30/21 16:59 95-49-8250500
4-Chlorotoluene ND ug/L 10/30/21 16:59 106-43-4250500
1,2-Dibromo-3-chloropropane ND ug/L 10/30/21 16:59 96-12-8500500
Dibromochloromethane ND ug/L 10/30/21 16:59 124-48-1250500
1,2-Dibromoethane (EDB)ND ug/L 10/30/21 16:59 106-93-4250500
Dibromomethane ND ug/L 10/30/21 16:59 74-95-3250500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-2 Lab ID:92569107002 Collected:10/27/21 10:30 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 10/30/21 16:59 95-50-1250500
1,3-Dichlorobenzene ND ug/L 10/30/21 16:59 541-73-1250500
1,4-Dichlorobenzene ND ug/L 10/30/21 16:59 106-46-7250500
Dichlorodifluoromethane ND ug/L 10/30/21 16:59 75-71-8250500
1,1-Dichloroethane ND ug/L 10/30/21 16:59 75-34-3250500
1,2-Dichloroethane ND ug/L 10/30/21 16:59 107-06-2250500
1,1-Dichloroethene ND ug/L 10/30/21 16:59 75-35-4250500
cis-1,2-Dichloroethene ND ug/L 10/30/21 16:59 156-59-2250500
trans-1,2-Dichloroethene ND ug/L 10/30/21 16:59 156-60-5250500
1,2-Dichloropropane ND ug/L 10/30/21 16:59 78-87-5250500
1,3-Dichloropropane ND ug/L 10/30/21 16:59 142-28-9250500
2,2-Dichloropropane ND ug/L 10/30/21 16:59 594-20-7250500
1,1-Dichloropropene ND ug/L 10/30/21 16:59 563-58-6250500
cis-1,3-Dichloropropene ND ug/L 10/30/21 16:59 10061-01-5250500
trans-1,3-Dichloropropene ND ug/L 10/30/21 16:59 10061-02-6250500
Diisopropyl ether ND ug/L 10/30/21 16:59 108-20-3250500
Ethylbenzene 2520 ug/L 10/30/21 16:59 100-41-4250500
Hexachloro-1,3-butadiene ND ug/L 10/30/21 16:59 87-68-31000500
Isopropylbenzene (Cumene)ND ug/L 10/30/21 16:59 98-82-8250500
Methylene Chloride ND ug/L 10/30/21 16:59 75-09-21000500
Methyl-tert-butyl ether 9910 ug/L 10/30/21 16:59 1634-04-4250500
Naphthalene ND ug/L 10/30/21 16:59 91-20-31000500
n-Propylbenzene 345 ug/L 10/30/21 16:59 103-65-1250500
Styrene ND ug/L 10/30/21 16:59 100-42-5250500
1,1,1,2-Tetrachloroethane ND ug/L 10/30/21 16:59 630-20-6250500
1,1,2,2-Tetrachloroethane ND ug/L 10/30/21 16:59 79-34-5250500
Tetrachloroethene ND ug/L 10/30/21 16:59 127-18-4250500
Toluene 77600 ug/L 10/30/21 16:59 108-88-3250500
1,2,3-Trichlorobenzene ND ug/L 10/30/21 16:59 87-61-61000500
1,2,4-Trichlorobenzene ND ug/L 10/30/21 16:59 120-82-11000500
1,1,1-Trichloroethane ND ug/L 10/30/21 16:59 71-55-6250500
1,1,2-Trichloroethane ND ug/L 10/30/21 16:59 79-00-5250500
Trichloroethene ND ug/L 10/30/21 16:59 79-01-6250500
Trichlorofluoromethane ND ug/L 10/30/21 16:59 75-69-4500500
1,2,3-Trichloropropane ND ug/L 10/30/21 16:59 96-18-4250500
1,2,4-Trimethylbenzene 2530 ug/L 10/30/21 16:59 95-63-6250500
1,3,5-Trimethylbenzene 649 ug/L 10/30/21 16:59 108-67-8250500
Vinyl chloride ND ug/L 10/30/21 16:59 75-01-4500500
m&p-Xylene 8220 ug/L 10/30/21 16:59 179601-23-1500500
o-Xylene 4020 ug/L 10/30/21 16:59 95-47-6250500
Surrogates
1,2-Dichloroethane-d4 (S)97 %10/30/21 16:59 17060-07-070-130 500
4-Bromofluorobenzene (S)98 %10/30/21 16:59 460-00-470-130 500
Toluene-d8 (S)97 %10/30/21 16:59 2037-26-570-130 500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-3 Lab ID:92569107003 Collected:10/27/21 10:15 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/03/21 01:47 71-43-2125250
Bromobenzene ND ug/L 11/03/21 01:47 108-86-1125250
Bromochloromethane ND ug/L 11/03/21 01:47 74-97-5125250
Bromodichloromethane ND ug/L 11/03/21 01:47 75-27-4125250
Bromoform ND ug/L 11/03/21 01:47 75-25-2125250
Bromomethane ND ug/L 11/03/21 01:47 74-83-91250250
n-Butylbenzene ND ug/L 11/03/21 01:47 104-51-8125250
sec-Butylbenzene ND ug/L 11/03/21 01:47 135-98-8125250
tert-Butylbenzene ND ug/L 11/03/21 01:47 98-06-6125250
Carbon tetrachloride ND ug/L 11/03/21 01:47 56-23-5125250
Chlorobenzene ND ug/L 11/03/21 01:47 108-90-7125250
Chloroethane ND ug/L 11/03/21 01:47 75-00-3250250
Chloroform ND ug/L 11/03/21 01:47 67-66-3125250
Chloromethane ND ug/L 11/03/21 01:47 74-87-3250250
2-Chlorotoluene ND ug/L 11/03/21 01:47 95-49-8125250
4-Chlorotoluene ND ug/L 11/03/21 01:47 106-43-4125250
1,2-Dibromo-3-chloropropane ND ug/L 11/03/21 01:47 96-12-8250250
Dibromochloromethane ND ug/L 11/03/21 01:47 124-48-1125250
1,2-Dibromoethane (EDB)ND ug/L 11/03/21 01:47 106-93-4125250
Dibromomethane ND ug/L 11/03/21 01:47 74-95-3125250
1,2-Dichlorobenzene ND ug/L 11/03/21 01:47 95-50-1125250
1,3-Dichlorobenzene ND ug/L 11/03/21 01:47 541-73-1125250
1,4-Dichlorobenzene ND ug/L 11/03/21 01:47 106-46-7125250
Dichlorodifluoromethane ND ug/L 11/03/21 01:47 75-71-8125250
1,1-Dichloroethane ND ug/L 11/03/21 01:47 75-34-3125250
1,2-Dichloroethane ND ug/L 11/03/21 01:47 107-06-2125250
1,1-Dichloroethene ND ug/L 11/03/21 01:47 75-35-4125250
cis-1,2-Dichloroethene ND ug/L 11/03/21 01:47 156-59-2125250
trans-1,2-Dichloroethene ND ug/L 11/03/21 01:47 156-60-5125250
1,2-Dichloropropane ND ug/L 11/03/21 01:47 78-87-5125250
1,3-Dichloropropane ND ug/L 11/03/21 01:47 142-28-9125250
2,2-Dichloropropane ND ug/L 11/03/21 01:47 594-20-7125250
1,1-Dichloropropene ND ug/L 11/03/21 01:47 563-58-6125250
cis-1,3-Dichloropropene ND ug/L 11/03/21 01:47 10061-01-5125250
trans-1,3-Dichloropropene ND ug/L 11/03/21 01:47 10061-02-6125250
Diisopropyl ether ND ug/L 11/03/21 01:47 108-20-3125250
Ethylbenzene 3090 ug/L 11/03/21 01:47 100-41-4125250
Hexachloro-1,3-butadiene ND ug/L 11/03/21 01:47 87-68-3500250
Isopropylbenzene (Cumene)139 ug/L 11/03/21 01:47 98-82-8125250
Methylene Chloride ND ug/L 11/03/21 01:47 75-09-2500250
Methyl-tert-butyl ether ND ug/L 11/03/21 01:47 1634-04-4125250
Naphthalene 745 ug/L 11/03/21 01:47 91-20-3500250
n-Propylbenzene 501 ug/L 11/03/21 01:47 103-65-1125250
Styrene ND ug/L 11/03/21 01:47 100-42-5125250
1,1,1,2-Tetrachloroethane ND ug/L 11/03/21 01:47 630-20-6125250
1,1,2,2-Tetrachloroethane ND ug/L 11/03/21 01:47 79-34-5125250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-3 Lab ID:92569107003 Collected:10/27/21 10:15 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/03/21 01:47 127-18-4125250
Toluene 25800 ug/L 11/03/21 01:47 108-88-3125250
1,2,3-Trichlorobenzene ND ug/L 11/03/21 01:47 87-61-6500250
1,2,4-Trichlorobenzene ND ug/L 11/03/21 01:47 120-82-1500250
1,1,1-Trichloroethane ND ug/L 11/03/21 01:47 71-55-6125250
1,1,2-Trichloroethane ND ug/L 11/03/21 01:47 79-00-5125250
Trichloroethene ND ug/L 11/03/21 01:47 79-01-6125250
Trichlorofluoromethane ND ug/L 11/03/21 01:47 75-69-4250250
1,2,3-Trichloropropane ND ug/L 11/03/21 01:47 96-18-4125250
1,2,4-Trimethylbenzene 3580 ug/L 11/03/21 01:47 95-63-6125250
1,3,5-Trimethylbenzene 843 ug/L 11/03/21 01:47 108-67-8125250
Vinyl chloride ND ug/L 11/03/21 01:47 75-01-4250250
m&p-Xylene 9570 ug/L 11/03/21 01:47 179601-23-1250250
o-Xylene 4400 ug/L 11/03/21 01:47 95-47-6125250
Surrogates
1,2-Dichloroethane-d4 (S)89 %11/03/21 01:47 17060-07-070-130 250
4-Bromofluorobenzene (S)93 %11/03/21 01:47 460-00-470-130 250
Toluene-d8 (S)98 %11/03/21 01:47 2037-26-570-130 250
Sample:MW-4 Lab ID:92569107004 Collected:10/27/21 11:30 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 54.1 ug/L 11/03/21 00:54 71-43-250.0 100
Bromobenzene ND ug/L 11/03/21 00:54 108-86-150.0 100
Bromochloromethane ND ug/L 11/03/21 00:54 74-97-550.0 100
Bromodichloromethane ND ug/L 11/03/21 00:54 75-27-450.0 100
Bromoform ND ug/L 11/03/21 00:54 75-25-250.0 100
Bromomethane ND ug/L 11/03/21 00:54 74-83-9500100
n-Butylbenzene ND ug/L 11/03/21 00:54 104-51-850.0 100
sec-Butylbenzene ND ug/L 11/03/21 00:54 135-98-850.0 100
tert-Butylbenzene ND ug/L 11/03/21 00:54 98-06-650.0 100
Carbon tetrachloride ND ug/L 11/03/21 00:54 56-23-550.0 100
Chlorobenzene ND ug/L 11/03/21 00:54 108-90-750.0 100
Chloroethane ND ug/L 11/03/21 00:54 75-00-3100100
Chloroform ND ug/L 11/03/21 00:54 67-66-350.0 100
Chloromethane ND ug/L 11/03/21 00:54 74-87-3100100
2-Chlorotoluene ND ug/L 11/03/21 00:54 95-49-850.0 100
4-Chlorotoluene ND ug/L 11/03/21 00:54 106-43-450.0 100
1,2-Dibromo-3-chloropropane ND ug/L 11/03/21 00:54 96-12-8100100
Dibromochloromethane ND ug/L 11/03/21 00:54 124-48-150.0 100
1,2-Dibromoethane (EDB)ND ug/L 11/03/21 00:54 106-93-450.0 100
Dibromomethane ND ug/L 11/03/21 00:54 74-95-350.0 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-4 Lab ID:92569107004 Collected:10/27/21 11:30 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 11/03/21 00:54 95-50-150.0 100
1,3-Dichlorobenzene ND ug/L 11/03/21 00:54 541-73-150.0 100
1,4-Dichlorobenzene ND ug/L 11/03/21 00:54 106-46-750.0 100
Dichlorodifluoromethane ND ug/L 11/03/21 00:54 75-71-850.0 100
1,1-Dichloroethane ND ug/L 11/03/21 00:54 75-34-350.0 100
1,2-Dichloroethane 120 ug/L 11/03/21 00:54 107-06-250.0 100
1,1-Dichloroethene ND ug/L 11/03/21 00:54 75-35-450.0 100
cis-1,2-Dichloroethene ND ug/L 11/03/21 00:54 156-59-250.0 100
trans-1,2-Dichloroethene ND ug/L 11/03/21 00:54 156-60-550.0 100
1,2-Dichloropropane ND ug/L 11/03/21 00:54 78-87-550.0 100
1,3-Dichloropropane ND ug/L 11/03/21 00:54 142-28-950.0 100
2,2-Dichloropropane ND ug/L 11/03/21 00:54 594-20-750.0 100
1,1-Dichloropropene ND ug/L 11/03/21 00:54 563-58-650.0 100
cis-1,3-Dichloropropene ND ug/L 11/03/21 00:54 10061-01-550.0 100
trans-1,3-Dichloropropene ND ug/L 11/03/21 00:54 10061-02-650.0 100
Diisopropyl ether 76.0 ug/L 11/03/21 00:54 108-20-350.0 100
Ethylbenzene ND ug/L 11/03/21 00:54 100-41-450.0 100
Hexachloro-1,3-butadiene ND ug/L 11/03/21 00:54 87-68-3200100
Isopropylbenzene (Cumene)ND ug/L 11/03/21 00:54 98-82-850.0 100
Methylene Chloride ND ug/L 11/03/21 00:54 75-09-2200100
Methyl-tert-butyl ether 10800 ug/L 11/03/21 00:54 1634-04-450.0 100
Naphthalene ND ug/L 11/03/21 00:54 91-20-3200100
n-Propylbenzene ND ug/L 11/03/21 00:54 103-65-150.0 100
Styrene ND ug/L 11/03/21 00:54 100-42-550.0 100
1,1,1,2-Tetrachloroethane ND ug/L 11/03/21 00:54 630-20-650.0 100
1,1,2,2-Tetrachloroethane ND ug/L 11/03/21 00:54 79-34-550.0 100
Tetrachloroethene ND ug/L 11/03/21 00:54 127-18-450.0 100
Toluene ND ug/L 11/03/21 00:54 108-88-350.0 100
1,2,3-Trichlorobenzene ND ug/L 11/03/21 00:54 87-61-6200100
1,2,4-Trichlorobenzene ND ug/L 11/03/21 00:54 120-82-1200100
1,1,1-Trichloroethane ND ug/L 11/03/21 00:54 71-55-650.0 100
1,1,2-Trichloroethane ND ug/L 11/03/21 00:54 79-00-550.0 100
Trichloroethene ND ug/L 11/03/21 00:54 79-01-650.0 100
Trichlorofluoromethane ND ug/L 11/03/21 00:54 75-69-4100100
1,2,3-Trichloropropane ND ug/L 11/03/21 00:54 96-18-450.0 100
1,2,4-Trimethylbenzene ND ug/L 11/03/21 00:54 95-63-650.0 100
1,3,5-Trimethylbenzene ND ug/L 11/03/21 00:54 108-67-850.0 100
Vinyl chloride ND ug/L 11/03/21 00:54 75-01-4100100
m&p-Xylene ND ug/L 11/03/21 00:54 179601-23-1100100
o-Xylene ND ug/L 11/03/21 00:54 95-47-650.0 100
Surrogates
1,2-Dichloroethane-d4 (S)92 %11/03/21 00:54 17060-07-070-130 100
4-Bromofluorobenzene (S)95 %11/03/21 00:54 460-00-470-130 100
Toluene-d8 (S)96 %11/03/21 00:54 2037-26-570-130 100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-6 Lab ID:92569107005 Collected:10/27/21 12:05 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 15:18 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 15:18 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 15:18 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 15:18 75-27-40.50 1
Bromoform ND ug/L 11/01/21 15:18 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 15:18 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 15:18 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 15:18 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 15:18 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 15:18 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 15:18 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 15:18 75-00-31.0 1
Chloroform ND ug/L 11/01/21 15:18 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 15:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 15:18 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 15:18 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 15:18 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 15:18 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 15:18 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 15:18 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/01/21 15:18 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 15:18 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 15:18 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 15:18 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 15:18 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 15:18 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 15:18 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 15:18 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 15:18 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 15:18 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 15:18 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 15:18 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 15:18 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 15:18 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 15:18 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 15:18 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 15:18 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 15:18 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 15:18 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 15:18 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 15:18 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 15:18 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 15:18 103-65-10.50 1
Styrene ND ug/L 11/01/21 15:18 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 15:18 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 15:18 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-6 Lab ID:92569107005 Collected:10/27/21 12:05 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/01/21 15:18 127-18-40.50 1
Toluene ND ug/L 11/01/21 15:18 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 15:18 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 15:18 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 15:18 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 15:18 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 15:18 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 15:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 15:18 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 15:18 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 15:18 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 15:18 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 15:18 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 15:18 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/01/21 15:18 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %11/01/21 15:18 460-00-470-130 1
Toluene-d8 (S)99 %11/01/21 15:18 2037-26-570-130 1
Sample:MW-7 Lab ID:92569107006 Collected:10/27/21 12:25 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 15:36 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 15:36 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 15:36 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 15:36 75-27-40.50 1
Bromoform ND ug/L 11/01/21 15:36 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 15:36 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 15:36 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 15:36 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 15:36 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 15:36 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 15:36 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 15:36 75-00-31.0 1
Chloroform ND ug/L 11/01/21 15:36 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 15:36 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 15:36 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 15:36 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 15:36 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 15:36 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 15:36 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 15:36 74-95-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-7 Lab ID:92569107006 Collected:10/27/21 12:25 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 11/01/21 15:36 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 15:36 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 15:36 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 15:36 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 15:36 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 15:36 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 15:36 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 15:36 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 15:36 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 15:36 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 15:36 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 15:36 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 15:36 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 15:36 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 15:36 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 15:36 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 15:36 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 15:36 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 15:36 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 15:36 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 15:36 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 15:36 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 15:36 103-65-10.50 1
Styrene ND ug/L 11/01/21 15:36 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 15:36 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 15:36 79-34-50.50 1
Tetrachloroethene ND ug/L 11/01/21 15:36 127-18-40.50 1
Toluene ND ug/L 11/01/21 15:36 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 15:36 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 15:36 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 15:36 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 15:36 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 15:36 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 15:36 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 15:36 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 15:36 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 15:36 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 15:36 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 15:36 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 15:36 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %11/01/21 15:36 17060-07-070-130 1
4-Bromofluorobenzene (S)92 %11/01/21 15:36 460-00-470-130 1
Toluene-d8 (S)95 %11/01/21 15:36 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 13 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-8 Lab ID:92569107007 Collected:10/27/21 11:15 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 15:54 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 15:54 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 15:54 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 15:54 75-27-40.50 1
Bromoform ND ug/L 11/01/21 15:54 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 15:54 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 15:54 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 15:54 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 15:54 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 15:54 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 15:54 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 15:54 75-00-31.0 1
Chloroform ND ug/L 11/01/21 15:54 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 15:54 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 15:54 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 15:54 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 15:54 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 15:54 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 15:54 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 15:54 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/01/21 15:54 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 15:54 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 15:54 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 15:54 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 15:54 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 15:54 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 15:54 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 15:54 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 15:54 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 15:54 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 15:54 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 15:54 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 15:54 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 15:54 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 15:54 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 15:54 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 15:54 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 15:54 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 15:54 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 15:54 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 15:54 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 15:54 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 15:54 103-65-10.50 1
Styrene ND ug/L 11/01/21 15:54 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 15:54 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 15:54 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 14 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-8 Lab ID:92569107007 Collected:10/27/21 11:15 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/01/21 15:54 127-18-40.50 1
Toluene ND ug/L 11/01/21 15:54 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 15:54 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 15:54 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 15:54 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 15:54 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 15:54 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 15:54 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 15:54 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 15:54 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 15:54 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 15:54 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 15:54 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 15:54 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %11/01/21 15:54 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %11/01/21 15:54 460-00-470-130 1
Toluene-d8 (S)99 %11/01/21 15:54 2037-26-570-130 1
Sample:MW-10 Lab ID:92569107008 Collected:10/27/21 12:15 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 16:12 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 16:12 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 16:12 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 16:12 75-27-40.50 1
Bromoform ND ug/L 11/01/21 16:12 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 16:12 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 16:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 16:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 16:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 16:12 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 16:12 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 16:12 75-00-31.0 1
Chloroform ND ug/L 11/01/21 16:12 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 16:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 16:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 16:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 16:12 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 16:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 16:12 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 16:12 74-95-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 15 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-10 Lab ID:92569107008 Collected:10/27/21 12:15 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 11/01/21 16:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 16:12 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 16:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 16:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 16:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 16:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 16:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 16:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 16:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 16:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 16:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 16:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 16:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 16:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 16:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 16:12 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 16:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 16:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 16:12 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 16:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 16:12 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 16:12 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 16:12 103-65-10.50 1
Styrene ND ug/L 11/01/21 16:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 16:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 16:12 79-34-50.50 1
Tetrachloroethene ND ug/L 11/01/21 16:12 127-18-40.50 1
Toluene ND ug/L 11/01/21 16:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 16:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 16:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 16:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 16:12 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 16:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 16:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 16:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 16:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 16:12 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 16:12 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 16:12 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 16:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %11/01/21 16:12 17060-07-070-130 1
4-Bromofluorobenzene (S)92 %11/01/21 16:12 460-00-470-130 1
Toluene-d8 (S)96 %11/01/21 16:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 16 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-11 Lab ID:92569107009 Collected:10/27/21 12:45 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 16:30 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 16:30 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 16:30 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 16:30 75-27-40.50 1
Bromoform ND ug/L 11/01/21 16:30 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 16:30 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 16:30 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 16:30 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 16:30 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 16:30 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 16:30 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 16:30 75-00-31.0 1
Chloroform ND ug/L 11/01/21 16:30 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 16:30 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 16:30 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 16:30 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 16:30 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 16:30 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 16:30 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 16:30 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/01/21 16:30 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 16:30 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 16:30 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 16:30 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 16:30 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 16:30 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 16:30 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 16:30 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 16:30 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 16:30 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 16:30 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 16:30 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 16:30 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 16:30 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 16:30 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 16:30 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 16:30 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 16:30 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 16:30 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 16:30 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 16:30 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 16:30 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 16:30 103-65-10.50 1
Styrene ND ug/L 11/01/21 16:30 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 16:30 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 16:30 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 17 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-11 Lab ID:92569107009 Collected:10/27/21 12:45 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/01/21 16:30 127-18-40.50 1
Toluene ND ug/L 11/01/21 16:30 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 16:30 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 16:30 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 16:30 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 16:30 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 16:30 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 16:30 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 16:30 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 16:30 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 16:30 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 16:30 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 16:30 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 16:30 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %11/01/21 16:30 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %11/01/21 16:30 460-00-470-130 1
Toluene-d8 (S)96 %11/01/21 16:30 2037-26-570-130 1
Sample:MW-14 Lab ID:92569107010 Collected:10/27/21 09:45 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 1620 ug/L 11/03/21 02:05 71-43-2250500
Bromobenzene ND ug/L 11/03/21 02:05 108-86-1250500
Bromochloromethane ND ug/L 11/03/21 02:05 74-97-5250500
Bromodichloromethane ND ug/L 11/03/21 02:05 75-27-4250500
Bromoform ND ug/L 11/03/21 02:05 75-25-2250500
Bromomethane ND ug/L 11/03/21 02:05 74-83-92500500
n-Butylbenzene ND ug/L 11/03/21 02:05 104-51-8250500
sec-Butylbenzene ND ug/L 11/03/21 02:05 135-98-8250500
tert-Butylbenzene ND ug/L 11/03/21 02:05 98-06-6250500
Carbon tetrachloride ND ug/L 11/03/21 02:05 56-23-5250500
Chlorobenzene ND ug/L 11/03/21 02:05 108-90-7250500
Chloroethane ND ug/L 11/03/21 02:05 75-00-3500500
Chloroform ND ug/L 11/03/21 02:05 67-66-3250500
Chloromethane ND ug/L 11/03/21 02:05 74-87-3500500
2-Chlorotoluene ND ug/L 11/03/21 02:05 95-49-8250500
4-Chlorotoluene ND ug/L 11/03/21 02:05 106-43-4250500
1,2-Dibromo-3-chloropropane ND ug/L 11/03/21 02:05 96-12-8500500
Dibromochloromethane ND ug/L 11/03/21 02:05 124-48-1250500
1,2-Dibromoethane (EDB)ND ug/L 11/03/21 02:05 106-93-4250500
Dibromomethane ND ug/L 11/03/21 02:05 74-95-3250500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 18 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:MW-14 Lab ID:92569107010 Collected:10/27/21 09:45 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 11/03/21 02:05 95-50-1250500
1,3-Dichlorobenzene ND ug/L 11/03/21 02:05 541-73-1250500
1,4-Dichlorobenzene ND ug/L 11/03/21 02:05 106-46-7250500
Dichlorodifluoromethane ND ug/L 11/03/21 02:05 75-71-8250500
1,1-Dichloroethane ND ug/L 11/03/21 02:05 75-34-3250500
1,2-Dichloroethane ND ug/L 11/03/21 02:05 107-06-2250500
1,1-Dichloroethene ND ug/L 11/03/21 02:05 75-35-4250500
cis-1,2-Dichloroethene ND ug/L 11/03/21 02:05 156-59-2250500
trans-1,2-Dichloroethene ND ug/L 11/03/21 02:05 156-60-5250500
1,2-Dichloropropane ND ug/L 11/03/21 02:05 78-87-5250500
1,3-Dichloropropane ND ug/L 11/03/21 02:05 142-28-9250500
2,2-Dichloropropane ND ug/L 11/03/21 02:05 594-20-7250500
1,1-Dichloropropene ND ug/L 11/03/21 02:05 563-58-6250500
cis-1,3-Dichloropropene ND ug/L 11/03/21 02:05 10061-01-5250500
trans-1,3-Dichloropropene ND ug/L 11/03/21 02:05 10061-02-6250500
Diisopropyl ether ND ug/L 11/03/21 02:05 108-20-3250500
Ethylbenzene 2900 ug/L 11/03/21 02:05 100-41-4250500
Hexachloro-1,3-butadiene ND ug/L 11/03/21 02:05 87-68-31000500
Isopropylbenzene (Cumene)ND ug/L 11/03/21 02:05 98-82-8250500
Methylene Chloride ND ug/L 11/03/21 02:05 75-09-21000500
Methyl-tert-butyl ether ND ug/L 11/03/21 02:05 1634-04-4250500
Naphthalene ND ug/L 11/03/21 02:05 91-20-31000500
n-Propylbenzene 515 ug/L 11/03/21 02:05 103-65-1250500
Styrene ND ug/L 11/03/21 02:05 100-42-5250500
1,1,1,2-Tetrachloroethane ND ug/L 11/03/21 02:05 630-20-6250500
1,1,2,2-Tetrachloroethane ND ug/L 11/03/21 02:05 79-34-5250500
Tetrachloroethene ND ug/L 11/03/21 02:05 127-18-4250500
Toluene 52400 ug/L 11/03/21 02:05 108-88-3250500
1,2,3-Trichlorobenzene ND ug/L 11/03/21 02:05 87-61-61000500
1,2,4-Trichlorobenzene ND ug/L 11/03/21 02:05 120-82-11000500
1,1,1-Trichloroethane ND ug/L 11/03/21 02:05 71-55-6250500
1,1,2-Trichloroethane ND ug/L 11/03/21 02:05 79-00-5250500
Trichloroethene ND ug/L 11/03/21 02:05 79-01-6250500
Trichlorofluoromethane ND ug/L 11/03/21 02:05 75-69-4500500
1,2,3-Trichloropropane ND ug/L 11/03/21 02:05 96-18-4250500
1,2,4-Trimethylbenzene 4020 ug/L 11/03/21 02:05 95-63-6250500
1,3,5-Trimethylbenzene 1010 ug/L 11/03/21 02:05 108-67-8250500
Vinyl chloride ND ug/L 11/03/21 02:05 75-01-4500500
m&p-Xylene 10200 ug/L 11/03/21 02:05 179601-23-1500500
o-Xylene 5300 ug/L 11/03/21 02:05 95-47-6250500
Surrogates
1,2-Dichloroethane-d4 (S)92 %11/03/21 02:05 17060-07-070-130 500
4-Bromofluorobenzene (S)94 %11/03/21 02:05 460-00-470-130 500
Toluene-d8 (S)98 %11/03/21 02:05 2037-26-570-130 500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 19 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:DW-1 Lab ID:92569107011 Collected:10/27/21 10:40 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 16:48 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 16:48 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 16:48 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 16:48 75-27-40.50 1
Bromoform ND ug/L 11/01/21 16:48 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 16:48 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 16:48 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 16:48 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 16:48 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 16:48 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 16:48 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 16:48 75-00-31.0 1
Chloroform ND ug/L 11/01/21 16:48 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 16:48 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 16:48 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 16:48 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 16:48 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 16:48 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 16:48 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 16:48 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/01/21 16:48 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 16:48 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 16:48 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 16:48 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 16:48 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 16:48 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 16:48 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 16:48 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 16:48 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 16:48 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 16:48 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 16:48 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 16:48 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 16:48 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 16:48 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 16:48 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 16:48 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 16:48 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 16:48 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 16:48 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 16:48 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 16:48 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 16:48 103-65-10.50 1
Styrene ND ug/L 11/01/21 16:48 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 16:48 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 16:48 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 20 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:DW-1 Lab ID:92569107011 Collected:10/27/21 10:40 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/01/21 16:48 127-18-40.50 1
Toluene ND ug/L 11/01/21 16:48 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 16:48 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 16:48 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 16:48 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 16:48 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 16:48 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 16:48 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 16:48 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 16:48 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 16:48 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 16:48 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 16:48 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 16:48 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %11/01/21 16:48 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %11/01/21 16:48 460-00-470-130 1
Toluene-d8 (S)97 %11/01/21 16:48 2037-26-570-130 1
Sample:WS-4 Lab ID:92569107012 Collected:10/27/21 10:50 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 17:06 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 17:06 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 17:06 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 17:06 75-27-40.50 1
Bromoform ND ug/L 11/01/21 17:06 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 17:06 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 17:06 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 17:06 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 17:06 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 17:06 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 17:06 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 17:06 75-00-31.0 1
Chloroform 2.6 ug/L 11/01/21 17:06 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 17:06 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 17:06 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 17:06 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 17:06 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 17:06 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 17:06 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 17:06 74-95-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 21 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:WS-4 Lab ID:92569107012 Collected:10/27/21 10:50 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 11/01/21 17:06 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 17:06 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 17:06 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 17:06 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 17:06 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 17:06 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 17:06 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 17:06 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 17:06 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 17:06 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 17:06 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 17:06 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 17:06 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 17:06 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 17:06 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 17:06 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 17:06 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 17:06 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 17:06 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 17:06 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 17:06 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 17:06 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 17:06 103-65-10.50 1
Styrene ND ug/L 11/01/21 17:06 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 17:06 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 17:06 79-34-50.50 1
Tetrachloroethene ND ug/L 11/01/21 17:06 127-18-40.50 1
Toluene ND ug/L 11/01/21 17:06 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 17:06 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 17:06 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 17:06 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 17:06 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 17:06 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 17:06 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 17:06 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 17:06 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 17:06 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 17:06 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 17:06 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 17:06 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/01/21 17:06 17060-07-070-130 1
4-Bromofluorobenzene (S)92 %11/01/21 17:06 460-00-470-130 1
Toluene-d8 (S)96 %11/01/21 17:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 22 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:WS-5 Lab ID:92569107013 Collected:10/27/21 11:10 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 17:24 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 17:24 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 17:24 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 17:24 75-27-40.50 1
Bromoform ND ug/L 11/01/21 17:24 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 17:24 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 17:24 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 17:24 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 17:24 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 17:24 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 17:24 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 17:24 75-00-31.0 1
Chloroform 1.2 ug/L 11/01/21 17:24 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 17:24 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 17:24 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 17:24 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 17:24 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 17:24 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 17:24 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 17:24 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/01/21 17:24 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 17:24 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 17:24 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 17:24 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 17:24 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 17:24 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 17:24 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 17:24 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 17:24 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 17:24 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 17:24 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 17:24 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 17:24 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 17:24 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 17:24 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 17:24 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 17:24 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 17:24 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 17:24 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 17:24 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 17:24 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 17:24 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 17:24 103-65-10.50 1
Styrene ND ug/L 11/01/21 17:24 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 17:24 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 17:24 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 23 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:WS-5 Lab ID:92569107013 Collected:10/27/21 11:10 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/01/21 17:24 127-18-40.50 1
Toluene ND ug/L 11/01/21 17:24 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 17:24 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 17:24 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 17:24 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 17:24 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 17:24 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 17:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 17:24 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 17:24 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 17:24 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 17:24 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 17:24 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 17:24 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %11/01/21 17:24 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %11/01/21 17:24 460-00-470-130 1
Toluene-d8 (S)96 %11/01/21 17:24 2037-26-570-130 1
Sample:WS-6 Lab ID:92569107014 Collected:10/27/21 11:20 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/01/21 17:42 71-43-20.50 1
Bromobenzene ND ug/L 11/01/21 17:42 108-86-10.50 1
Bromochloromethane ND ug/L 11/01/21 17:42 74-97-50.50 1
Bromodichloromethane ND ug/L 11/01/21 17:42 75-27-40.50 1
Bromoform ND ug/L 11/01/21 17:42 75-25-20.50 1
Bromomethane ND ug/L 11/01/21 17:42 74-83-95.0 1
n-Butylbenzene ND ug/L 11/01/21 17:42 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/01/21 17:42 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/01/21 17:42 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/01/21 17:42 56-23-50.50 1
Chlorobenzene ND ug/L 11/01/21 17:42 108-90-70.50 1
Chloroethane ND ug/L 11/01/21 17:42 75-00-31.0 1
Chloroform ND ug/L 11/01/21 17:42 67-66-30.50 1
Chloromethane ND ug/L 11/01/21 17:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/01/21 17:42 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/01/21 17:42 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/01/21 17:42 96-12-81.0 1
Dibromochloromethane ND ug/L 11/01/21 17:42 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/01/21 17:42 106-93-40.50 1
Dibromomethane ND ug/L 11/01/21 17:42 74-95-30.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 24 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:WS-6 Lab ID:92569107014 Collected:10/27/21 11:20 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2-Dichlorobenzene ND ug/L 11/01/21 17:42 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/01/21 17:42 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/01/21 17:42 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/01/21 17:42 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/01/21 17:42 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/01/21 17:42 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/01/21 17:42 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/01/21 17:42 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/01/21 17:42 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/01/21 17:42 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/01/21 17:42 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/01/21 17:42 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/01/21 17:42 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/01/21 17:42 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/01/21 17:42 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/01/21 17:42 108-20-30.50 1
Ethylbenzene ND ug/L 11/01/21 17:42 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/01/21 17:42 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/01/21 17:42 98-82-80.50 1
Methylene Chloride ND ug/L 11/01/21 17:42 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/01/21 17:42 1634-04-40.50 1
Naphthalene ND ug/L 11/01/21 17:42 91-20-32.0 1
n-Propylbenzene ND ug/L 11/01/21 17:42 103-65-10.50 1
Styrene ND ug/L 11/01/21 17:42 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/01/21 17:42 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/01/21 17:42 79-34-50.50 1
Tetrachloroethene ND ug/L 11/01/21 17:42 127-18-40.50 1
Toluene ND ug/L 11/01/21 17:42 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/01/21 17:42 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/01/21 17:42 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/01/21 17:42 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/01/21 17:42 79-00-50.50 1
Trichloroethene ND ug/L 11/01/21 17:42 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/01/21 17:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/01/21 17:42 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/01/21 17:42 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/01/21 17:42 108-67-80.50 1
Vinyl chloride ND ug/L 11/01/21 17:42 75-01-41.0 1
m&p-Xylene ND ug/L 11/01/21 17:42 179601-23-11.0 1
o-Xylene ND ug/L 11/01/21 17:42 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)91 %11/01/21 17:42 17060-07-070-130 1
4-Bromofluorobenzene (S)91 %11/01/21 17:42 460-00-470-130 1
Toluene-d8 (S)95 %11/01/21 17:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 25 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:WS-12 Lab ID:92569107015 Collected:10/27/21 13:00 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 11/03/21 02:41 71-43-20.50 1
Bromobenzene ND ug/L 11/03/21 02:41 108-86-10.50 1
Bromochloromethane ND ug/L 11/03/21 02:41 74-97-50.50 1
Bromodichloromethane ND ug/L 11/03/21 02:41 75-27-40.50 1
Bromoform ND ug/L 11/03/21 02:41 75-25-20.50 1
Bromomethane ND ug/L 11/03/21 02:41 74-83-95.0 1
n-Butylbenzene ND ug/L 11/03/21 02:41 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/03/21 02:41 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/03/21 02:41 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/03/21 02:41 56-23-50.50 1
Chlorobenzene ND ug/L 11/03/21 02:41 108-90-70.50 1
Chloroethane ND ug/L 11/03/21 02:41 75-00-31.0 1
Chloroform ND ug/L 11/03/21 02:41 67-66-30.50 1
Chloromethane ND ug/L 11/03/21 02:41 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/03/21 02:41 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/03/21 02:41 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/03/21 02:41 96-12-81.0 1
Dibromochloromethane ND ug/L 11/03/21 02:41 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/03/21 02:41 106-93-40.50 1
Dibromomethane ND ug/L 11/03/21 02:41 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/03/21 02:41 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/03/21 02:41 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/03/21 02:41 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/03/21 02:41 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/03/21 02:41 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/03/21 02:41 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/03/21 02:41 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/03/21 02:41 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/03/21 02:41 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/03/21 02:41 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/03/21 02:41 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/03/21 02:41 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/03/21 02:41 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/03/21 02:41 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/03/21 02:41 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/03/21 02:41 108-20-30.50 1
Ethylbenzene ND ug/L 11/03/21 02:41 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/03/21 02:41 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/03/21 02:41 98-82-80.50 1
Methylene Chloride ND ug/L 11/03/21 02:41 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/03/21 02:41 1634-04-40.50 1
Naphthalene ND ug/L 11/03/21 02:41 91-20-32.0 1
n-Propylbenzene ND ug/L 11/03/21 02:41 103-65-10.50 1
Styrene ND ug/L 11/03/21 02:41 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/03/21 02:41 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/03/21 02:41 79-34-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 26 of 48
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Sample:WS-12 Lab ID:92569107015 Collected:10/27/21 13:00 Received:10/27/21 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 11/03/21 02:41 127-18-40.50 1
Toluene ND ug/L 11/03/21 02:41 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/03/21 02:41 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/03/21 02:41 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/03/21 02:41 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/03/21 02:41 79-00-50.50 1
Trichloroethene ND ug/L 11/03/21 02:41 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/03/21 02:41 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/03/21 02:41 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/03/21 02:41 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/03/21 02:41 108-67-80.50 1
Vinyl chloride ND ug/L 11/03/21 02:41 75-01-41.0 1
m&p-Xylene ND ug/L 11/03/21 02:41 179601-23-11.0 1
o-Xylene ND ug/L 11/03/21 02:41 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %11/03/21 02:41 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %11/03/21 02:41 460-00-470-130 1
Toluene-d8 (S)95 %11/03/21 02:41 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 27 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
656318
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92569107001, 92569107002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3440722
Associated Lab Samples:92569107001, 92569107002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/30/21 12:00
1,1,1-Trichloroethane ug/L ND 0.50 10/30/21 12:00
1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/30/21 12:00
1,1,2-Trichloroethane ug/L ND 0.50 10/30/21 12:00
1,1-Dichloroethane ug/L ND 0.50 10/30/21 12:00
1,1-Dichloroethene ug/L ND 0.50 10/30/21 12:00
1,1-Dichloropropene ug/L ND 0.50 10/30/21 12:00
1,2,3-Trichlorobenzene ug/L ND 2.0 10/30/21 12:00
1,2,3-Trichloropropane ug/L ND 0.50 10/30/21 12:00
1,2,4-Trichlorobenzene ug/L ND 2.0 10/30/21 12:00
1,2,4-Trimethylbenzene ug/L ND 0.50 10/30/21 12:00
1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/30/21 12:00
1,2-Dibromoethane (EDB)ug/L ND 0.50 10/30/21 12:00
1,2-Dichlorobenzene ug/L ND 0.50 10/30/21 12:00
1,2-Dichloroethane ug/L ND 0.50 10/30/21 12:00
1,2-Dichloropropane ug/L ND 0.50 10/30/21 12:00
1,3,5-Trimethylbenzene ug/L ND 0.50 10/30/21 12:00
1,3-Dichlorobenzene ug/L ND 0.50 10/30/21 12:00
1,3-Dichloropropane ug/L ND 0.50 10/30/21 12:00
1,4-Dichlorobenzene ug/L ND 0.50 10/30/21 12:00
2,2-Dichloropropane ug/L ND 0.50 10/30/21 12:00
2-Chlorotoluene ug/L ND 0.50 10/30/21 12:00
4-Chlorotoluene ug/L ND 0.50 10/30/21 12:00
Benzene ug/L ND 0.50 10/30/21 12:00
Bromobenzene ug/L ND 0.50 10/30/21 12:00
Bromochloromethane ug/L ND 0.50 10/30/21 12:00
Bromodichloromethane ug/L ND 0.50 10/30/21 12:00
Bromoform ug/L ND 0.50 10/30/21 12:00
Bromomethane ug/L ND 5.0 10/30/21 12:00
Carbon tetrachloride ug/L ND 0.50 10/30/21 12:00
Chlorobenzene ug/L ND 0.50 10/30/21 12:00
Chloroethane ug/L ND 1.0 10/30/21 12:00
Chloroform ug/L ND 0.50 10/30/21 12:00
Chloromethane ug/L ND 1.0 10/30/21 12:00
cis-1,2-Dichloroethene ug/L ND 0.50 10/30/21 12:00
cis-1,3-Dichloropropene ug/L ND 0.50 10/30/21 12:00
Dibromochloromethane ug/L ND 0.50 10/30/21 12:00
Dibromomethane ug/L ND 0.50 10/30/21 12:00
Dichlorodifluoromethane ug/L ND 0.50 10/30/21 12:00
Diisopropyl ether ug/L ND 0.50 10/30/21 12:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 28 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3440722
Associated Lab Samples:92569107001, 92569107002
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 10/30/21 12:00
Hexachloro-1,3-butadiene ug/L ND 2.0 10/30/21 12:00
Isopropylbenzene (Cumene)ug/L ND 0.50 10/30/21 12:00
m&p-Xylene ug/L ND 1.0 10/30/21 12:00
Methyl-tert-butyl ether ug/L ND 0.50 10/30/21 12:00
Methylene Chloride ug/L ND 2.0 10/30/21 12:00
n-Butylbenzene ug/L ND 0.50 10/30/21 12:00
n-Propylbenzene ug/L ND 0.50 10/30/21 12:00
Naphthalene ug/L ND 2.0 10/30/21 12:00
o-Xylene ug/L ND 0.50 10/30/21 12:00
sec-Butylbenzene ug/L ND 0.50 10/30/21 12:00
Styrene ug/L ND 0.50 10/30/21 12:00
tert-Butylbenzene ug/L ND 0.50 10/30/21 12:00
Tetrachloroethene ug/L ND 0.50 10/30/21 12:00
Toluene ug/L ND 0.50 10/30/21 12:00
trans-1,2-Dichloroethene ug/L ND 0.50 10/30/21 12:00
trans-1,3-Dichloropropene ug/L ND 0.50 10/30/21 12:00
Trichloroethene ug/L ND 0.50 10/30/21 12:00
Trichlorofluoromethane ug/L ND 1.0 10/30/21 12:00
Vinyl chloride ug/L ND 1.0 10/30/21 12:00
1,2-Dichloroethane-d4 (S)%97 70-130 10/30/21 12:00
4-Bromofluorobenzene (S)%100 70-130 10/30/21 12:00
Toluene-d8 (S)%102 70-130 10/30/21 12:00
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3440723LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.550 107 60-140
1,1,1-Trichloroethane ug/L 53.750 107 60-140
1,1,2,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,2-Trichloroethane ug/L 53.950 108 60-140
1,1-Dichloroethane ug/L 50.750 101 60-140
1,1-Dichloroethene ug/L 52.850 106 60-140
1,1-Dichloropropene ug/L 54.750 109 60-140
1,2,3-Trichlorobenzene ug/L 57.150 114 60-140
1,2,3-Trichloropropane ug/L 49.550 99 60-140
1,2,4-Trichlorobenzene ug/L 57.550 115 60-140
1,2,4-Trimethylbenzene ug/L 52.350 105 60-140
1,2-Dibromo-3-chloropropane ug/L 57.650 115 60-140
1,2-Dibromoethane (EDB)ug/L 54.050 108 60-140
1,2-Dichlorobenzene ug/L 51.250 102 60-140
1,2-Dichloroethane ug/L 50.350 101 60-140
1,2-Dichloropropane ug/L 52.850 106 60-140
1,3,5-Trimethylbenzene ug/L 53.450 107 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 29 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3440723LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 51.450 103 60-140
1,3-Dichloropropane ug/L 53.450 107 60-140
1,4-Dichlorobenzene ug/L 52.050 104 60-140
2,2-Dichloropropane ug/L 56.050 112 60-140
2-Chlorotoluene ug/L 52.850 106 60-140
4-Chlorotoluene ug/L 50.050 100 60-140
Benzene ug/L 50.850 102 60-140
Bromobenzene ug/L 52.550 105 60-140
Bromochloromethane ug/L 53.350 107 60-140
Bromodichloromethane ug/L 50.050 100 60-140
Bromoform ug/L 54.250 108 60-140
Bromomethane ug/L 51.950 104 60-140
Carbon tetrachloride ug/L 54.350 109 60-140
Chlorobenzene ug/L 49.250 98 60-140
Chloroethane ug/L 46.050 92 60-140
Chloroform ug/L 49.550 99 60-140
Chloromethane ug/L 52.550 105 60-140
cis-1,2-Dichloroethene ug/L 49.650 99 60-140
cis-1,3-Dichloropropene ug/L 54.450 109 60-140
Dibromochloromethane ug/L 55.850 112 60-140
Dibromomethane ug/L 50.050 100 60-140
Dichlorodifluoromethane ug/L 60.350 121 60-140
Diisopropyl ether ug/L 53.150 106 60-140
Ethylbenzene ug/L 50.550 101 60-140
Hexachloro-1,3-butadiene ug/L 62.350 125 60-140
Isopropylbenzene (Cumene)ug/L 52.450 105 60-140
m&p-Xylene ug/L 100100 100 60-140
Methyl-tert-butyl ether ug/L 53.650 107 60-140
Methylene Chloride ug/L 49.550 99 60-140
n-Butylbenzene ug/L 55.350 111 60-140
n-Propylbenzene ug/L 53.850 108 60-140
Naphthalene ug/L 56.650 113 60-140
o-Xylene ug/L 49.950 100 60-140
sec-Butylbenzene ug/L 53.450 107 60-140
Styrene ug/L 52.050 104 60-140
tert-Butylbenzene ug/L 44.850 90 60-140
Tetrachloroethene ug/L 52.450 105 60-140
Toluene ug/L 48.950 98 60-140
trans-1,2-Dichloroethene ug/L 52.350 105 60-140
trans-1,3-Dichloropropene ug/L 53.550 107 60-140
Trichloroethene ug/L 52.650 105 60-140
Trichlorofluoromethane ug/L 46.250 92 60-140
Vinyl chloride ug/L 51.950 104 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 30 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3440724MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92568923003
3440725
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 500 114 60-140107 6 30500ND571537
1,1,1-Trichloroethane ug/L 500 115 60-140113 1 30500ND575567
1,1,2,2-Tetrachloroethane ug/L 500 107 60-140100 7 30500ND533498
1,1,2-Trichloroethane ug/L 500 104 60-140103 1 30500ND521515
1,1-Dichloroethane ug/L 500 106 60-140104 2 30500ND530520
1,1-Dichloroethene ug/L 500 96 60-14096 0 30500ND480480
1,1-Dichloropropene ug/L 500 107 60-140105 2 30500ND536527
1,2,3-Trichlorobenzene ug/L 500 128 60-140114 12 30500ND642569
1,2,3-Trichloropropane ug/L 500 103 60-14090 14 30500ND517451
1,2,4-Trichlorobenzene ug/L 500 123 60-140112 9 30500ND617562
1,2,4-Trimethylbenzene ug/L 500 101 60-14092 3 30500144019501900
1,2-Dibromo-3-
chloropropane ug/L 500 117 60-14099 17 30500ND584493
1,2-Dibromoethane (EDB)ug/L 500 119 60-140107 10 30500ND593534
1,2-Dichlorobenzene ug/L 500 113 60-140105 8 30500ND566523
1,2-Dichloroethane ug/L 500 99 60-14099 1 3050044.7 539 542
1,2-Dichloropropane ug/L 500 103 60-140103 0 30500ND514514
1,3,5-Trimethylbenzene ug/L 500 107 60-14098 5 30500401938892
1,3-Dichlorobenzene ug/L 500 111 60-140107 3 30500ND556537
1,3-Dichloropropane ug/L 500 108 60-140100 7 30500ND538501
1,4-Dichlorobenzene ug/L 500 114 60-140109 5 30500ND572544
2,2-Dichloropropane ug/L M15006160-14055 9 30500ND311283
2-Chlorotoluene ug/L 500 118 60-140115 2 30500ND588575
4-Chlorotoluene ug/L 500 104 60-14097 7 30500ND521487
Benzene ug/L M15004660-14031 2 30500343036603580
Bromobenzene ug/L 500 119 60-140113 5 30500ND597566
Bromochloromethane ug/L 500 114 60-140109 4 30500ND571547
Bromodichloromethane ug/L 500 111 60-140106 4 30500ND553531
Bromoform ug/L 500 113 60-140102 11 30500ND566508
Bromomethane ug/L 500 107 60-140116 7 30500ND536578
Carbon tetrachloride ug/L 500 116 60-140109 6 30500ND578546
Chlorobenzene ug/L 500 113 60-140109 4 30500ND566545
Chloroethane ug/L 500 134 60-140125 7 30500ND672626
Chloroform ug/L 500 108 60-140103 4 30500ND545523
Chloromethane ug/L 500 103 60-140103 1 30500ND516513
cis-1,2-Dichloroethene ug/L 500 102 60-140102 0 30500ND514516
cis-1,3-Dichloropropene ug/L 500 89 60-14088 1 30500ND447442
Dibromochloromethane ug/L 500 113 60-140105 8 30500ND567526
Dibromomethane ug/L 500 111 60-140109 2 30500ND554544
Dichlorodifluoromethane ug/L M150015360-140153 0 30500ND764766
Diisopropyl ether ug/L 500 90 60-14089 1 3050063.1 513 508
Ethylbenzene ug/L 500 119 60-140109 3 3050096115501510
Hexachloro-1,3-butadiene ug/L M150014260-140125 12 30500ND710627
Isopropylbenzene(Cumene)ug/L 500 117 60-140110 6 3050038.0 623 587
m&p-Xylene ug/L M1100014860-140117 5 301000446059405630
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 31 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3440724MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92568923003
3440725
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 500 97 60-14092 4 3050070.4 553 531
Methylene Chloride ug/L 500 110 60-140107 3 30500ND551535
n-Butylbenzene ug/L 500 116 60-140110 6 30500ND581549
n-Propylbenzene ug/L 500 104 60-14097 6 30500107625590
Naphthalene ug/L 500 117 60-140103 6 3050059411801110
o-Xylene ug/L M150014360-140125 4 30500177024902400
sec-Butylbenzene ug/L 500 114 60-140108 6 30500ND572540
Styrene ug/L 500 102 60-14096 6 3050053.2 564 531
tert-Butylbenzene ug/L 500 94 60-14090 4 30500ND468448
Tetrachloroethene ug/L 500 119 60-140112 6 30500ND605571
Toluene ug/L 500 87 60-14069 4 30500194023802280
trans-1,2-Dichloroethene ug/L 500 113 60-140107 6 30500ND566534
trans-1,3-Dichloropropene ug/L 500 93 60-14087 7 30500ND464435
Trichloroethene ug/L 500 118 60-140113 4 30500ND589566
Trichlorofluoromethane ug/L 500 112 60-140109 3 30500ND559543
Vinyl chloride ug/L 500 123 60-140122 1 30500ND615608
1,2-Dichloroethane-d4 (S)%95 70-13097
4-Bromofluorobenzene (S)%97 70-13096
Toluene-d8 (S)%99 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 32 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
656545
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92569107005, 92569107006, 92569107007, 92569107008, 92569107009, 92569107011, 92569107012,
92569107013, 92569107014
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3441747
Associated Lab Samples:92569107005, 92569107006, 92569107007, 92569107008, 92569107009, 92569107011, 92569107012,
92569107013, 92569107014
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/01/21 11:24
1,1,1-Trichloroethane ug/L ND 0.50 11/01/21 11:24
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/01/21 11:24
1,1,2-Trichloroethane ug/L ND 0.50 11/01/21 11:24
1,1-Dichloroethane ug/L ND 0.50 11/01/21 11:24
1,1-Dichloroethene ug/L ND 0.50 11/01/21 11:24
1,1-Dichloropropene ug/L ND 0.50 11/01/21 11:24
1,2,3-Trichlorobenzene ug/L ND 2.0 11/01/21 11:24
1,2,3-Trichloropropane ug/L ND 0.50 11/01/21 11:24
1,2,4-Trichlorobenzene ug/L ND 2.0 11/01/21 11:24
1,2,4-Trimethylbenzene ug/L ND 0.50 11/01/21 11:24
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/01/21 11:24
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/01/21 11:24
1,2-Dichlorobenzene ug/L ND 0.50 11/01/21 11:24
1,2-Dichloroethane ug/L ND 0.50 11/01/21 11:24
1,2-Dichloropropane ug/L ND 0.50 11/01/21 11:24
1,3,5-Trimethylbenzene ug/L ND 0.50 11/01/21 11:24
1,3-Dichlorobenzene ug/L ND 0.50 11/01/21 11:24
1,3-Dichloropropane ug/L ND 0.50 11/01/21 11:24
1,4-Dichlorobenzene ug/L ND 0.50 11/01/21 11:24
2,2-Dichloropropane ug/L ND 0.50 11/01/21 11:24
2-Chlorotoluene ug/L ND 0.50 11/01/21 11:24
4-Chlorotoluene ug/L ND 0.50 11/01/21 11:24
Benzene ug/L ND 0.50 11/01/21 11:24
Bromobenzene ug/L ND 0.50 11/01/21 11:24
Bromochloromethane ug/L ND 0.50 11/01/21 11:24
Bromodichloromethane ug/L ND 0.50 11/01/21 11:24
Bromoform ug/L ND 0.50 11/01/21 11:24
Bromomethane ug/L ND 5.0 11/01/21 11:24
Carbon tetrachloride ug/L ND 0.50 11/01/21 11:24
Chlorobenzene ug/L ND 0.50 11/01/21 11:24
Chloroethane ug/L ND 1.0 11/01/21 11:24
Chloroform ug/L ND 0.50 11/01/21 11:24
Chloromethane ug/L ND 1.0 11/01/21 11:24
cis-1,2-Dichloroethene ug/L ND 0.50 11/01/21 11:24
cis-1,3-Dichloropropene ug/L ND 0.50 11/01/21 11:24
Dibromochloromethane ug/L ND 0.50 11/01/21 11:24
Dibromomethane ug/L ND 0.50 11/01/21 11:24
Dichlorodifluoromethane ug/L ND 0.50 11/01/21 11:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 33 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3441747
Associated Lab Samples:92569107005, 92569107006, 92569107007, 92569107008, 92569107009, 92569107011, 92569107012,
92569107013, 92569107014
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 0.50 11/01/21 11:24
Ethylbenzene ug/L ND 0.50 11/01/21 11:24
Hexachloro-1,3-butadiene ug/L ND 2.0 11/01/21 11:24
Isopropylbenzene (Cumene)ug/L ND 0.50 11/01/21 11:24
m&p-Xylene ug/L ND 1.0 11/01/21 11:24
Methyl-tert-butyl ether ug/L ND 0.50 11/01/21 11:24
Methylene Chloride ug/L ND 2.0 11/01/21 11:24
n-Butylbenzene ug/L ND 0.50 11/01/21 11:24
n-Propylbenzene ug/L ND 0.50 11/01/21 11:24
Naphthalene ug/L ND 2.0 11/01/21 11:24
o-Xylene ug/L ND 0.50 11/01/21 11:24
sec-Butylbenzene ug/L ND 0.50 11/01/21 11:24
Styrene ug/L ND 0.50 11/01/21 11:24
tert-Butylbenzene ug/L ND 0.50 11/01/21 11:24
Tetrachloroethene ug/L ND 0.50 11/01/21 11:24
Toluene ug/L ND 0.50 11/01/21 11:24
trans-1,2-Dichloroethene ug/L ND 0.50 11/01/21 11:24
trans-1,3-Dichloropropene ug/L ND 0.50 11/01/21 11:24
Trichloroethene ug/L ND 0.50 11/01/21 11:24
Trichlorofluoromethane ug/L ND 1.0 11/01/21 11:24
Vinyl chloride ug/L ND 1.0 11/01/21 11:24
1,2-Dichloroethane-d4 (S)%95 70-130 11/01/21 11:24
4-Bromofluorobenzene (S)%94 70-130 11/01/21 11:24
Toluene-d8 (S)%98 70-130 11/01/21 11:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3441748LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.050 106 60-140
1,1,1-Trichloroethane ug/L 49.250 98 60-140
1,1,2,2-Tetrachloroethane ug/L 50.950 102 60-140
1,1,2-Trichloroethane ug/L 50.650 101 60-140
1,1-Dichloroethane ug/L 45.850 92 60-140
1,1-Dichloroethene ug/L 42.750 85 60-140
1,1-Dichloropropene ug/L 46.250 92 60-140
1,2,3-Trichlorobenzene ug/L 57.650 115 60-140
1,2,3-Trichloropropane ug/L 47.550 95 60-140
1,2,4-Trichlorobenzene ug/L 58.550 117 60-140
1,2,4-Trimethylbenzene ug/L 52.550 105 60-140
1,2-Dibromo-3-chloropropane ug/L 54.750 109 60-140
1,2-Dibromoethane (EDB)ug/L 53.550 107 60-140
1,2-Dichlorobenzene ug/L 55.350 111 60-140
1,2-Dichloroethane ug/L 44.650 89 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 34 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3441748LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 47.950 96 60-140
1,3,5-Trimethylbenzene ug/L 52.550 105 60-140
1,3-Dichlorobenzene ug/L 55.750 111 60-140
1,3-Dichloropropane ug/L 50.750 101 60-140
1,4-Dichlorobenzene ug/L 54.550 109 60-140
2,2-Dichloropropane ug/L 47.050 94 60-140
2-Chlorotoluene ug/L 54.450 109 60-140
4-Chlorotoluene ug/L 50.750 101 60-140
Benzene ug/L 47.350 95 60-140
Bromobenzene ug/L 56.950 114 60-140
Bromochloromethane ug/L 50.050 100 60-140
Bromodichloromethane ug/L 51.750 103 60-140
Bromoform ug/L 56.050 112 60-140
Bromomethane ug/L 50.050 100 60-140
Carbon tetrachloride ug/L 52.150 104 60-140
Chlorobenzene ug/L 52.850 106 60-140
Chloroethane ug/L 54.150 108 60-140
Chloroform ug/L 45.350 91 60-140
Chloromethane ug/L 43.050 86 60-140
cis-1,2-Dichloroethene ug/L 44.550 89 60-140
cis-1,3-Dichloropropene ug/L 48.750 97 60-140
Dibromochloromethane ug/L 53.750 107 60-140
Dibromomethane ug/L 55.550 111 60-140
Dichlorodifluoromethane ug/L 69.950 140 60-140
Diisopropyl ether ug/L 40.950 82 60-140
Ethylbenzene ug/L 53.250 106 60-140
Hexachloro-1,3-butadiene ug/L 64.750 129 60-140
Isopropylbenzene (Cumene)ug/L 55.050 110 60-140
m&p-Xylene ug/L 105100 105 60-140
Methyl-tert-butyl ether ug/L 42.750 85 60-140
Methylene Chloride ug/L 47.950 96 60-140
n-Butylbenzene ug/L 53.250 106 60-140
n-Propylbenzene ug/L 50.550 101 60-140
Naphthalene ug/L 56.750 113 60-140
o-Xylene ug/L 52.450 105 60-140
sec-Butylbenzene ug/L 51.450 103 60-140
Styrene ug/L 53.950 108 60-140
tert-Butylbenzene ug/L 43.650 87 60-140
Tetrachloroethene ug/L 55.450 111 60-140
Toluene ug/L 48.550 97 60-140
trans-1,2-Dichloroethene ug/L 46.450 93 60-140
trans-1,3-Dichloropropene ug/L 48.750 97 60-140
Trichloroethene ug/L 54.350 109 60-140
Trichlorofluoromethane ug/L 53.950 108 60-140
Vinyl chloride ug/L 51.050 102 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 35 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3441748LABORATORY CONTROL SAMPLE:
LCSSpike
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3441749MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92569505001
3441750
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 5000 107 60-140102 5 305000<77.8 5330 5090
1,1,1-Trichloroethane ug/L 5000 103 60-140102 1 305000<83.0 5150 5090
1,1,2,2-Tetrachloroethane ug/L 5000 99 60-14094 5 305000<56.2 4930 4690
1,1,2-Trichloroethane ug/L 5000 95 60-14095 0 305000<81.2 4750 4740
1,1-Dichloroethane ug/L 5000 98 60-14092 6 305000<91.8 4890 4600
1,1-Dichloroethene ug/L 5000 92 60-14084 9 305000<87.0 4580 4180
1,1-Dichloropropene ug/L 5000 100 60-14096 4 305000<107 5010 4820
1,2,3-Trichlorobenzene ug/L 5000 118 60-140115 3 305000<202 5910 5730
1,2,3-Trichloropropane ug/L 5000 88 60-14085 4 305000<65.2 4420 4250
1,2,4-Trichlorobenzene ug/L 5000 119 60-140114 4 305000<160 5940 5710
1,2,4-Trimethylbenzene ug/L 5000 106 60-140104 1 305000276080707980
1,2-Dibromo-3-
chloropropane ug/L 5000 98 60-14092 7 305000<85.0 4920 4590
1,2-Dibromoethane (EDB)ug/L 5000 107 60-140103 4 305000<68.0 5350 5130
1,2-Dichlorobenzene ug/L 5000 109 60-140108 1 305000<84.8 5440 5390
1,2-Dichloroethane ug/L 5000 89 60-14086 3 305000<80.5 4440 4300
1,2-Dichloropropane ug/L 5000 92 60-14099 7 305000<88.8 4620 4940
1,3,5-Trimethylbenzene ug/L 5000 109 60-140104 4 30500066061205870
1,3-Dichlorobenzene ug/L 5000 110 60-140107 3 305000<85.0 5510 5360
1,3-Dichloropropane ug/L 5000 102 60-14098 4 305000<71.0 5100 4900
1,4-Dichlorobenzene ug/L 5000 111 60-140106 4 305000<83.2 5560 5320
2,2-Dichloropropane ug/L 5000 93 60-14086 8 305000<97.0 4640 4280
2-Chlorotoluene ug/L 5000 112 60-140109 2 305000<80.2 5600 5470
4-Chlorotoluene ug/L 5000 102 60-140100 2 305000<81.0 5100 4980
Benzene ug/L 5000 89 60-14099 4 30500090801350014000
Bromobenzene ug/L 5000 115 60-140113 2 305000<72.5 5770 5640
Bromochloromethane ug/L 5000 108 60-140102 5 305000<117 5390 5110
Bromodichloromethane ug/L 5000 96 60-14098 2 305000<76.8 4790 4880
Bromoform ug/L 5000 101 60-14090 11 305000<85.2 5060 4520
Bromomethane ug/L 5000 101 60-14096 5 305000<415 5060 4820
Carbon tetrachloride ug/L 5000 103 60-140103 1 305000<83.2 5140 5160
Chlorobenzene ug/L 5000 110 60-140105 4 305000<71.0 5490 5260
Chloroethane ug/L 5000 109 60-140101 7 305000<162 5460 5070
Chloroform ug/L 5000 101 60-14097 4 305000<88.2 5050 4840
Chloromethane ug/L 5000 82 60-14083 1 305000<135 4110 4140
cis-1,2-Dichloroethene ug/L 5000 97 60-14092 6 305000<96.0 4850 4590
cis-1,3-Dichloropropene ug/L 5000 92 60-14091 1 305000<91.2 4600 4550
Dibromochloromethane ug/L 5000 107 60-14099 7 305000<89.8 5360 4970
Dibromomethane ug/L 5000 103 60-140104 0 305000<98.5 5150 5180
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 36 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3441749MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92569505001
3441750
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Dichlorodifluoromethane ug/L 5000 104 60-14098 6 305000<86.5 5190 4880
Diisopropyl ether ug/L 5000 87 60-14084 4 305000<77.0 4350 4180
Ethylbenzene ug/L 5000 109 60-140108 1 305000320086508590
Hexachloro-1,3-butadiene ug/L 5000 127 60-140125 2 305000<382 6360 6250
Isopropylbenzene
(Cumene)
ug/L 5000 113 60-140109 4 305000118J57805570
m&p-Xylene ug/L 10000 104 60-140106 1 3010000116002200022200
Methyl-tert-butyl ether ug/L 5000 91 60-14088 3 305000<106 4540 4390
Methylene Chloride ug/L 5000 99 60-14095 3 305000<488 5270 5100
n-Butylbenzene ug/L 5000 108 60-140105 3 305000<122 5380 5240
n-Propylbenzene ug/L 5000 104 60-140101 3 30500030755105350
Naphthalene ug/L 5000 109 60-140105 3 30500077162006030
o-Xylene ug/L 5000 109 60-140108 0 30500065201200011900
sec-Butylbenzene ug/L 5000 108 60-140106 2 305000<100 5410 5310
Styrene ug/L 5000 108 60-140103 5 305000<73.0 5390 5140
tert-Butylbenzene ug/L 5000 90 60-14088 3 305000<80.8 4520 4400
Tetrachloroethene ug/L 5000 111 60-140108 3 305000<73.0 5540 5400
Toluene ug/L 5000 70 60-140134 7 305000385004200045200
trans-1,2-Dichloroethene ug/L 5000 102 60-14095 7 305000<99.0 5080 4730
trans-1,3-Dichloropropene ug/L 5000 89 60-14091 3 305000<90.8 4430 4540
Trichloroethene ug/L 5000 109 60-140111 2 305000<95.8 5450 5530
Trichlorofluoromethane ug/L 5000 94 60-14090 4 305000<74.5 4680 4510
Vinyl chloride ug/L 5000 105 60-14099 7 305000<96.5 5270 4930
1,2-Dichloroethane-d4 (S)%90 70-13090
4-Bromofluorobenzene (S)%97 70-13095
Toluene-d8 (S)%95 70-130100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 37 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
656890
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92569107003, 92569107004, 92569107010, 92569107015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3443309
Associated Lab Samples:92569107003, 92569107004, 92569107010, 92569107015
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/02/21 20:42
1,1,1-Trichloroethane ug/L ND 0.50 11/02/21 20:42
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/02/21 20:42
1,1,2-Trichloroethane ug/L ND 0.50 11/02/21 20:42
1,1-Dichloroethane ug/L ND 0.50 11/02/21 20:42
1,1-Dichloroethene ug/L ND 0.50 11/02/21 20:42
1,1-Dichloropropene ug/L ND 0.50 11/02/21 20:42
1,2,3-Trichlorobenzene ug/L ND 2.0 11/02/21 20:42
1,2,3-Trichloropropane ug/L ND 0.50 11/02/21 20:42
1,2,4-Trichlorobenzene ug/L ND 2.0 11/02/21 20:42
1,2,4-Trimethylbenzene ug/L ND 0.50 11/02/21 20:42
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/02/21 20:42
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/02/21 20:42
1,2-Dichlorobenzene ug/L ND 0.50 11/02/21 20:42
1,2-Dichloroethane ug/L ND 0.50 11/02/21 20:42
1,2-Dichloropropane ug/L ND 0.50 11/02/21 20:42
1,3,5-Trimethylbenzene ug/L ND 0.50 11/02/21 20:42
1,3-Dichlorobenzene ug/L ND 0.50 11/02/21 20:42
1,3-Dichloropropane ug/L ND 0.50 11/02/21 20:42
1,4-Dichlorobenzene ug/L ND 0.50 11/02/21 20:42
2,2-Dichloropropane ug/L ND 0.50 11/02/21 20:42
2-Chlorotoluene ug/L ND 0.50 11/02/21 20:42
4-Chlorotoluene ug/L ND 0.50 11/02/21 20:42
Benzene ug/L ND 0.50 11/02/21 20:42
Bromobenzene ug/L ND 0.50 11/02/21 20:42
Bromochloromethane ug/L ND 0.50 11/02/21 20:42
Bromodichloromethane ug/L ND 0.50 11/02/21 20:42
Bromoform ug/L ND 0.50 11/02/21 20:42
Bromomethane ug/L ND 5.0 11/02/21 20:42
Carbon tetrachloride ug/L ND 0.50 11/02/21 20:42
Chlorobenzene ug/L ND 0.50 11/02/21 20:42
Chloroethane ug/L ND 1.0 11/02/21 20:42
Chloroform ug/L ND 0.50 11/02/21 20:42
Chloromethane ug/L ND 1.0 11/02/21 20:42
cis-1,2-Dichloroethene ug/L ND 0.50 11/02/21 20:42
cis-1,3-Dichloropropene ug/L ND 0.50 11/02/21 20:42
Dibromochloromethane ug/L ND 0.50 11/02/21 20:42
Dibromomethane ug/L ND 0.50 11/02/21 20:42
Dichlorodifluoromethane ug/L ND 0.50 11/02/21 20:42
Diisopropyl ether ug/L ND 0.50 11/02/21 20:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 38 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3443309
Associated Lab Samples:92569107003, 92569107004, 92569107010, 92569107015
Matrix:Water
Analyzed
Ethylbenzene ug/L ND 0.50 11/02/21 20:42
Hexachloro-1,3-butadiene ug/L ND 2.0 11/02/21 20:42
Isopropylbenzene (Cumene)ug/L ND 0.50 11/02/21 20:42
m&p-Xylene ug/L ND 1.0 11/02/21 20:42
Methyl-tert-butyl ether ug/L ND 0.50 11/02/21 20:42
Methylene Chloride ug/L ND 2.0 11/02/21 20:42
n-Butylbenzene ug/L ND 0.50 11/02/21 20:42
n-Propylbenzene ug/L ND 0.50 11/02/21 20:42
Naphthalene ug/L ND 2.0 11/02/21 20:42
o-Xylene ug/L ND 0.50 11/02/21 20:42
sec-Butylbenzene ug/L ND 0.50 11/02/21 20:42
Styrene ug/L ND 0.50 11/02/21 20:42
tert-Butylbenzene ug/L ND 0.50 11/02/21 20:42
Tetrachloroethene ug/L ND 0.50 11/02/21 20:42
Toluene ug/L ND 0.50 11/02/21 20:42
trans-1,2-Dichloroethene ug/L ND 0.50 11/02/21 20:42
trans-1,3-Dichloropropene ug/L ND 0.50 11/02/21 20:42
Trichloroethene ug/L ND 0.50 11/02/21 20:42
Trichlorofluoromethane ug/L ND 1.0 11/02/21 20:42
Vinyl chloride ug/L ND 1.0 11/02/21 20:42
1,2-Dichloroethane-d4 (S)%90 70-130 11/02/21 20:42
4-Bromofluorobenzene (S)%92 70-130 11/02/21 20:42
Toluene-d8 (S)%95 70-130 11/02/21 20:42
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3443310LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.650 103 60-140
1,1,1-Trichloroethane ug/L 46.850 94 60-140
1,1,2,2-Tetrachloroethane ug/L 44.750 89 60-140
1,1,2-Trichloroethane ug/L 47.150 94 60-140
1,1-Dichloroethane ug/L 42.950 86 60-140
1,1-Dichloroethene ug/L 38.150 76 60-140
1,1-Dichloropropene ug/L 44.150 88 60-140
1,2,3-Trichlorobenzene ug/L 53.550 107 60-140
1,2,3-Trichloropropane ug/L 41.350 83 60-140
1,2,4-Trichlorobenzene ug/L 55.550 111 60-140
1,2,4-Trimethylbenzene ug/L 49.550 99 60-140
1,2-Dibromo-3-chloropropane ug/L 45.050 90 60-140
1,2-Dibromoethane (EDB)ug/L 51.750 103 60-140
1,2-Dichlorobenzene ug/L 53.250 106 60-140
1,2-Dichloroethane ug/L 41.450 83 60-140
1,2-Dichloropropane ug/L 43.850 88 60-140
1,3,5-Trimethylbenzene ug/L 50.750 101 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 39 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3443310LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 53.050 106 60-140
1,3-Dichloropropane ug/L 47.450 95 60-140
1,4-Dichlorobenzene ug/L 52.150 104 60-140
2,2-Dichloropropane ug/L 43.950 88 60-140
2-Chlorotoluene ug/L 50.950 102 60-140
4-Chlorotoluene ug/L 47.250 94 60-140
Benzene ug/L 43.750 87 60-140
Bromobenzene ug/L 53.850 108 60-140
Bromochloromethane ug/L 49.550 99 60-140
Bromodichloromethane ug/L 48.150 96 60-140
Bromoform ug/L 50.050 100 60-140
Bromomethane ug/L 48.750 97 60-140
Carbon tetrachloride ug/L 49.650 99 60-140
Chlorobenzene ug/L 51.650 103 60-140
Chloroethane ug/L 53.350 107 60-140
Chloroform ug/L 44.250 88 60-140
Chloromethane ug/L 40.150 80 60-140
cis-1,2-Dichloroethene ug/L 42.450 85 60-140
cis-1,3-Dichloropropene ug/L 44.450 89 60-140
Dibromochloromethane ug/L 50.150 100 60-140
Dibromomethane ug/L 49.950 100 60-140
Dichlorodifluoromethane ug/L 60.350 121 60-140
Diisopropyl ether ug/L 38.750 77 60-140
Ethylbenzene ug/L 50.050 100 60-140
Hexachloro-1,3-butadiene ug/L 61.850 124 60-140
Isopropylbenzene (Cumene)ug/L 53.650 107 60-140
m&p-Xylene ug/L 99.4100 99 60-140
Methyl-tert-butyl ether ug/L 40.750 81 60-140
Methylene Chloride ug/L 45.550 91 60-140
n-Butylbenzene ug/L 50.550 101 60-140
n-Propylbenzene ug/L 47.450 95 60-140
Naphthalene ug/L 49.750 99 60-140
o-Xylene ug/L 50.750 101 60-140
sec-Butylbenzene ug/L 50.850 102 60-140
Styrene ug/L 50.950 102 60-140
tert-Butylbenzene ug/L 42.250 84 60-140
Tetrachloroethene ug/L 52.550 105 60-140
Toluene ug/L 46.350 93 60-140
trans-1,2-Dichloroethene ug/L 43.850 88 60-140
trans-1,3-Dichloropropene ug/L 44.550 89 60-140
Trichloroethene ug/L 50.950 102 60-140
Trichlorofluoromethane ug/L 44.950 90 60-140
Vinyl chloride ug/L 46.650 93 60-140
1,2-Dichloroethane-d4 (S)%84 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 40 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3443311MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92569107010
3443312
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 10000 108 60-140108 0 3010000ND1080010800
1,1,1-Trichloroethane ug/L 10000 110 60-140108 2 3010000ND1100010800
1,1,2,2-Tetrachloroethane ug/L 10000 96 60-140100 3 3010000ND96309960
1,1,2-Trichloroethane ug/L 10000 96 60-14098 2 3010000ND95809780
1,1-Dichloroethane ug/L 10000 94 60-14093 1 3010000ND94009270
1,1-Dichloroethene ug/L 10000 87 60-14086 1 3010000ND86608610
1,1-Dichloropropene ug/L 10000 100 60-14097 2 3010000ND99809740
1,2,3-Trichlorobenzene ug/L 10000 111 60-140117 5 3010000ND1110011700
1,2,3-Trichloropropane ug/L 10000 89 60-14091 3 3010000ND88709140
1,2,4-Trichlorobenzene ug/L 10000 111 60-140118 5 3010000ND1110011800
1,2,4-Trimethylbenzene ug/L 10000 107 60-140108 1 301000040201470014800
1,2-Dibromo-3-
chloropropane ug/L 10000 90 60-14097 7 3010000ND90409680
1,2-Dibromoethane (EDB)ug/L 10000 107 60-140105 2 3010000ND1070010500
1,2-Dichlorobenzene ug/L 10000 110 60-140111 1 3010000ND1100011100
1,2-Dichloroethane ug/L 10000 90 60-14087 4 3010000ND90308700
1,2-Dichloropropane ug/L 10000 94 60-14094 1 3010000ND93609430
1,3,5-Trimethylbenzene ug/L 10000 105 60-140110 4 301000010101150012000
1,3-Dichlorobenzene ug/L 10000 112 60-140112 0 3010000ND1120011200
1,3-Dichloropropane ug/L 10000 96 60-140101 5 3010000ND955010100
1,4-Dichlorobenzene ug/L 10000 107 60-140111 4 3010000ND1070011100
2,2-Dichloropropane ug/L 10000 87 60-14086 2 3010000ND86808550
2-Chlorotoluene ug/L 10000 112 60-140108 3 3010000ND1120010800
4-Chlorotoluene ug/L 10000 101 60-140103 2 3010000ND1010010300
Benzene ug/L 10000 96 60-14094 2 301000016201120011000
Bromobenzene ug/L 10000 116 60-140119 3 3010000ND1160011900
Bromochloromethane ug/L 10000 107 60-140103 4 3010000ND1070010300
Bromodichloromethane ug/L 10000 94 60-14092 2 3010000ND94309200
Bromoform ug/L 10000 96 60-14097 1 3010000ND96009710
Bromomethane ug/L 10000 91 60-140108 17 3010000ND911010800
Carbon tetrachloride ug/L 10000 102 60-140102 0 3010000ND1020010200
Chlorobenzene ug/L 10000 110 60-140109 1 3010000ND1100010900
Chloroethane ug/L 10000 111 60-140104 6 3010000ND1110010400
Chloroform ug/L 10000 100 60-14094 7 3010000ND100009360
Chloromethane ug/L 10000 92 60-14092 0 3010000ND92009190
cis-1,2-Dichloroethene ug/L 10000 97 60-14095 2 3010000ND96609480
cis-1,3-Dichloropropene ug/L 10000 89 60-14090 1 3010000ND88708960
Dibromochloromethane ug/L 10000 103 60-140102 2 3010000ND1030010200
Dibromomethane ug/L 10000 105 60-140104 1 3010000ND1050010400
Dichlorodifluoromethane ug/L 10000 127 60-140131 3 3010000ND1270013100
Diisopropyl ether ug/L 10000 86 60-14082 5 3010000ND85708170
Ethylbenzene ug/L 10000 114 60-140111 2 301000029001430014000
Hexachloro-1,3-butadiene ug/L 10000 122 60-140126 3 3010000ND1220012600
Isopropylbenzene(Cumene)ug/L 10000 119 60-140116 3 3010000ND1190011600
m&p-Xylene ug/L 20000 110 60-140111 0 3020000102003220032300
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 41 of 48
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3443311MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92569107010
3443312
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 10000 90 60-14087 3 3010000ND89708730
Methylene Chloride ug/L 10000 102 60-14098 5 3010000ND102009780
n-Butylbenzene ug/L 10000 104 60-140106 2 3010000ND1040010600
n-Propylbenzene ug/L 10000 104 60-140102 2 30100005151090010700
Naphthalene ug/L 10000 99 60-140105 5 3010000ND1070011300
o-Xylene ug/L 10000 113 60-140113 0 301000053001660016600
sec-Butylbenzene ug/L 10000 110 60-140110 0 3010000ND1100011000
Styrene ug/L 10000 87 60-140109 23 3010000ND865010900
tert-Butylbenzene ug/L 10000 91 60-14091 0 3010000ND91009100
Tetrachloroethene ug/L 10000 117 60-140112 4 3010000ND1170011200
Toluene ug/L 10000 88 60-14094 1 3010000524006120061800
trans-1,2-Dichloroethene ug/L 10000 100 60-14099 1 3010000ND100009900
trans-1,3-Dichloropropene ug/L 10000 89 60-14089 0 3010000ND88908900
Trichloroethene ug/L 10000 110 60-140107 2 3010000ND1100010700
Trichlorofluoromethane ug/L 10000 93 60-14089 5 3010000ND93408910
Vinyl chloride ug/L 10000 109 60-140108 1 3010000ND1090010800
1,2-Dichloroethane-d4 (S)%88 70-13086
4-Bromofluorobenzene (S)%98 70-13097
Toluene-d8 (S)%92 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 42 of 48
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 43 of 48
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92569107
Pilot Geo G-7289
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92569107001 656318MW-1 SM 6200B
92569107002 656318MW-2 SM 6200B
92569107003 656890MW-3 SM 6200B
92569107004 656890MW-4 SM 6200B
92569107005 656545MW-6 SM 6200B
92569107006 656545MW-7 SM 6200B
92569107007 656545MW-8 SM 6200B
92569107008 656545MW-10 SM 6200B
92569107009 656545MW-11 SM 6200B
92569107010 656890MW-14 SM 6200B
92569107011 656545DW-1 SM 6200B
92569107012 656545WS-4 SM 6200B
92569107013 656545WS-5 SM 6200B
92569107014 656545WS-6 SM 6200B
92569107015 656890WS-12 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/04/2021 02:24 PM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 44 of 48
Page 45 of 48
Page 46 of 48
Page 47 of 48
Page 48 of 48