RA-1939_11920_CA_RPTS_20210203_MRP

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

February 4, 2021

Mr. Jared Edwards
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Ground Water Monitoring Report
January 2021
Red Apple Market #9
100 West Jackson Street
Rich Square, Northampton County
North Carolina
Incident Number: 0-00-0000026624
Incident Number: 11920
GRI Project No. 4497

Dear Mr. Edwards,

Please find enclosed the referenced report, for the above mentioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Christa Benton
Administrative Assistant

Enclosure

Cc: Red Apple Markets, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Ground Water Monitoring Report
January 2021
Red Apple Market #9
100 West Jackson Street
Rich Square, Northampton County
North Carolina
Facility ID Number: 0-00-0000026624
Incident Number: 11920
GRI Project Number: 4497

Prepared for:

Red Apple Markets, Inc.
Post Office Box 1386
Ahoskie, North Carolina 27910

February 3, 2021

William Regenthal, P.G.
Project Manager
Matthew T. Smith
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
i
SITE INFORMATION
1. Site Identification
 Red Apple Market #9 (Facility ID 0-00-0000026624)
 Incident Number 11920 – Intermediate Risk (I140R)
 Location of Source Area: 100 West Jackson Street
Rich Square, NC 227869
Northampton County
36.2741410°N, 77.2842062°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
Jernigan Properties, Inc.
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

UST Operator
Jernigan Properties, Inc.
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

Property Owner
Jernigan Properties, Inc.
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

Property Occupant
Duck Thru Food Stores
P.O. Box 688
Ahoskie, NC 27910
[e-mail]
252-332-2131

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, Florida 32811
State Certification No. 573
[phone]
3. Information about Release
 Release was discovered on July 15, 1992
 An unknown amount of product was released from the leaking UST System
 One 8,000-gallon gasoline, one 5,000-gallon gasoline, two 3,000-gallon gasoline, two 3,000-gallon
#2 fuel oil and one 2,000-gallon kerosene USTs were removed and/or abandoned in place in July
1992. One 10,000-gallon and one 6,000-gallon gasoline and one 4,000-gallon kerosene USTs are
currently in use at the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
ii
EXECUTIVE SUMMARY
The former Red Apple Market #9 is located at 100 West Jackson Street in Rich Square, Northampton
County, North Carolina. The site is currently owned by Jernigan Properties, Inc. and is operated by Duck
Thru Food Stores as a petroleum retail facility. One 8,000-gallon gasoline, one 5,000-gallon gasoline, two
3,000-gallon gasoline, two 3,000-gallon #2 fuel oil and one 2,000-gallon kerosene USTs were removed
and/or abandoned in place in July 1992 confirming the presence of a release. Currently, one 10,000-gallon
and one 6,000-gallon gasoline and one 4,000-gallon kerosene USTs are in use at the site. The adjoining
properties are a mixture of commercial and residential properties. According to the information
determined during receptor survey activities, no water supply wells were identified within 1,500 feet of
the site. Public water is available to the site and surrounding properties within a 1,500-foot radius of the
site.

A Correct Action Plan (CAP) has not been submitted for the site. Free product recovery events have been
conducted at the site beginning in August 2017.

On January 6, 2021, four Type II monitoring wells, MW-11 through MW-14, were installed at the site.
MW-11 through MW-14 were each installed to a total depth of 17 feet below ground surface (ft bgs) with
a screened interval of 15 feet.

On January 6, 2021, thirteen Type II and one Type III monitoring wells were gauged, purged and/or
sampled in accordance with the NCDEQ Guidelines. Free product was observed in MW-1. Concentrations
of benzene, MTBE, naphthalene and/or n-propylbenzene that exceeded the Maximum Allowable
Concentrations (MACs) as specified in T15A NCAC 2L.0202 were reported in the ground water samples
collected from MW-2, MW-11, MW-13 and MW-14. All of the reported contaminant concentrations were
less than the Gross Contamination Levels (GCLs).

Upon completion of the January 2021 sampling event, an absorbent sock was installed in MW-1.

Based on this information, the risk classification for the site should remain intermediate risk. Free product
recovery events should continue to be conducted at the site until free product is no longer present and
contaminant concentrations are below the GCLs. Semi-annual ground water monitoring should continue
at the site. The next sampling event is tentatively scheduled for July 2021.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 MONITORING WELL INSTALLATION ..........................................................................................2
3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................3
4.0 FREE PRODUCT REMOVAL ........................................................................................................4
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................5
6.0 CONCLUSIONS .........................................................................................................................5
7.0 LIMITATIONS ...........................................................................................................................5
8.0 STATEMENTS AND CERTIFICATION ...........................................................................................6

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Site Vicinity Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Adjacent Property Owner Information
Table 4: Well Construction and Gauging Information
Table 5: Summary of Ground Water Sample Analytical Results
Table 6: Free Product Recovery Results
Table 7: Free Product Recovery Event Information
Table 8: Free Product Recovery Cost Summary

APPENDICES
Appendix A: State Correspondence
Appendix B: Well Construction Records and Subsurface Logs
Appendix C: Laboratory Report – Ground Water Samples

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
1
1.0 SITE HISTORY AND CHARACTERIZATION
Geological Resources, Inc. (GRI) presents the results of the January 2021 ground water sampling event at
the Red Apple Market #9 site located at 100 West Jackson Street in Rich Square, Northampton County,
North Carolina (Figure 1). These activities were conducted in accordance with GRI Proposal No. 20-470,
which was submitted to the North Carolina Department of Environmental Quality (NCDEQ) on October 1,
2020 and was approved as Task Authorization No. 11920-6 on October 16, 2020. State correspondence
has been included as Appendix A.

The site is currently owned by Jernigan Properties, Inc. and is operated by Duck Thru Food Stores as a
petroleum retail facility. One 8,000-gallon gasoline, one 5,000-gallon gasoline, two 3,000-gallon gasoline,
two 3,000-gallon #2 fuel oil and one 2,000-gallon kerosene USTs were removed and/or abandoned in
place in July 1992 confirming the presence of a release. Currently, one 10,000-gallon and one 6,000-gallon
gasoline and one 4,000-gallon kerosene USTs are in use at the site. UST owner/operator information and
UST system information are included as Tables 1 and 2, respectively. Please note that the information
presented in this report is based on information provided by the previous consultant and does not match
the NCDEQ Registered Tank Database. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of commercial and residential properties. The site contains
one building (the store) and is partially capped with concrete. The overall topography at the site is
relatively flat. No surface water bodies were identified within a 500-foot radius of the site. Nine Type II
monitoring wells (MW-1 through MW-5 and MW-7 through MW-10) and one Type III monitoring well

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
2
(MWD-6) were installed at the site during previous ground water assessment activities. A Site Map
showing the locations of the monitoring wells and the structures on-site has been included as Figure 2.

On May 2, 2017, GRI personnel conducted a receptor survey update at the site. The site lies within the
designated wellhead protection area for the Town of Rich Square. No water supply wells were identified
within a 1,500-foot radius of the site. Municipal water is available to the site and surrounding properties.
Adjacent property owner information is presented in Table 3. A Site Vicinity Map showing the adjacent
properties has been included as Figure 3.

A Corrective Action Plan (CAP) has not yet been developed for the site. To date, two MMPE events have
been conducted at the site along with hand bailing and an aggressive fluid-vapor recovery (AFVR) event.
Please note that no projected milestones have been established for this site.

2.0 MONITORING WELL INSTALLATION

On January 6, 2021, four Type II monitoring wells (MW-11 through MW-14) were installed at the site.
MW-11 through MW-14 were each installed to a total depth of 17 feet below ground surface (ft bgs) with
a screened interval of 15 feet. Copies of the subsurface logs and well construction records have been
included in Appendix B. Photos of the newly constructed wells are shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
3

3.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On January 6, 2021, thirteen Type II monitoring wells (MW-1 through MW-5 and MW-7 through MW-14)
and one Type III monitoring well (MWD-6) were gauged, purged, and sampled in accordance with NCDEQ
Guidelines. Free product was observed in MW-1. Depths to ground water in the Type II monitoring wells
ranged from 1.23 feet to 17.05 feet below the tops of well casings. Ground water elevations in the Type
II monitoring wells ranged from 82.54 feet to 99.84 feet. Ground water flow was generally to the south-
southeast from hydraulic highs at MW-5 and MW-1. The horizontal hydraulic gradient was approximately
0.16 feet per foot. The vertical gradient between paired wells MW-4 and MWD-6 was approximately 0.18
feet per foot in the downward direction. Well construction and gauging information is presented in Table
4. A Water Table Surface Map based on the Type II monitoring wells is included as Figure 4. A summary
of the current ground water gauging data is shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 8 – 18 18 100.00 3.31 0.26 96.91
MW-2 7 – 17 17 100.11 4.42 --- 95.69
MW-3 7 – 17 17 100.90 5.63 --- 95.27
MW-4 6 – 16 16 100.52 5.28 --- 95.24
MW-5 7 – 17 17 101.07 1.23 --- 99.84
MWD-6 30 – 35 35 100.91 9.47 --- 91.44
MW-7 6 – 16 16 99.61 3.47 --- 96.14
MW-8 6 – 16 16 100.21 6.24 --- 93.97
MW-9 6 – 16 16 100.63 5.34 --- 95.29
MW-10 6 - 16 16 101.06 8.32 --- 92.74
MW-11 2-17 17 100.47 6.70 --- 93.77
MW-12 2-17 17 99.82 12.21 --- 87.61
MW-13 2-17 17 99.53 15.72 --- 83.81
MW-14 2-17 17 99.59 17.05 --- 82.54

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
4

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. Concentrations of benzene, MTBE, naphthalene and/or n-propylbenzene that
exceeded the Maximum Allowable Concentrations (MACs) as specified in T15A NCAC 2L.0202 were
reported in the ground water samples collected from MW-2, MW-11, MW-13 and MW-14. All of the
reported contaminant concentrations were less than the Gross Contamination Levels (GCLs). A summary
of the analytical results for ground water samples collected on January 6, 2021, is presented in Table 5. A
Ground Water Quality Map based on the January 2021 data is included as Figure 5. A complete report of
laboratory analyses of the ground water samples collected from the monitoring wells during the January
2021 sampling event has been included as Appendix C. A summary of the current ground water analytical
data is shown below:

Contaminant
of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-1 FP FP FP FP FP FP
MW-2 652 29.1 25.4 82.4 22.6 453
MW-3 <0.13 <0.13 <0.13 <0.25 0.47 J <0.13
MW-4 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-5 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MWD-6 <0.13 <0.13 <0.13 <0.25 4.3 <0.13
MW-7 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-8 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13
MW-9 <0.13 <0.13 0.57 0.36 J <0.13 <0.13
MW-10 <0.13 <0.13 <0.13 <0.25 0.14 J <0.13
MW-11 <0.13 4.9 4.5 30.0 11.6 8.9
MW-12 <0.13 0.62 0.50 2.5 3.8 0.45 J
MW-13 58.6 41.5 160 407 37.6 101
MW-14 0.15 J 2.2 1.0 5.2 61.7 0.42 J

The baseline contaminant mass at the site cannot be determine due to the presence of free product in
MW-1. Contaminant mass calculations cannot be completed at this time.

The site is located in the Coastal Plain Physiographic Province of North Carolina. The water table has a
seasonal high depth to water of approximately 3 to 17 feet below ground surface (bgs).

Please note that while free product recovery events have been conducted, a Corrective Action Plan (CAP)
has not been developed for the site; therefore, a baseline contaminant mass prior to CAP implementation
has not been established at the site. Please note that milestones have not been established for this site.
4.0 FREE PRODUCT REMOVAL
Free product has historically been present in MW-1. Free product recovery should continue at the site
until free product is no longer present.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: February 3, 2021 Red Apple Market #9
Project Manager: William Regenthal, P.G. GRI Project No. 4497
5
Free product levels in MW-1 have been greatly reduced since the initiation of free product recovery at
the site; however, the free product thickness increased between the January 2020 and the January 2021
sampling events. Based on the increased free product thickness, as well as the relatively limited amount
of free product recovered as vapor during historical AFVR events, AFVR may not be the most effective or
cost-efficient method of free product removal. MMPE events have historically yielded greater recovery
with a lower cost per gallon recovered. Past free product recovery events are summarized in Tables 6, 7
and 8. Upon completion of the January 2021 sampling event, an absorbent sock was installed in MW-1.
5.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
Free product recovery events are being conducted at the site as the primary method of corrective action.
Due to the site being in the active remediation phase, no natural attenuation monitoring plan is currently
in place at the site.
6.0 CONCLUSIONS
 On January 6, 2021, thirteen Type II monitoring wells and one Type III monitoring well were
gauged, purged, and/or sampled. Monitoring well MW-1 contained free product and was not
sampled. Ground water flow was generally to the south-southeast from hydraulic highs at MW-
5 and MW-1 with a horizontal gradient of approximately 0.16 feet per foot. The vertical gradient
between paired wells MW-4 and MWD-6 was approximately 0.18 feet per foot in the downward
direction.
 Concentrations of benzene, MTBE, naphthalene, and/or n-propylbenzene that exceeded the
MACs were reported in the ground water samples collected from MW-2, MW-11, MW-13 and
MW-14. All of the reported contaminant concentrations were less than the GCLs.
 Upon completion of the January 2021 sampling event, an absorbent sock was installed in MW-1.
 Based on this information, the risk classification for the site should remain intermediate risk. Free
product recovery events should continue to be conducted at the site until free product is no
longer present and contaminant concentrations are below the GCLs. Semi-annual ground water
monitoring should be continued at the site. The next sampling event is tentatively scheduled for
July 2021.
7.0 LIMITATIONS
This report has been prepared for the exclusive use of Red Apple Markets, Inc. for specific application to
the referenced site in Northampton County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
Copyright (C) 2009 MyTopo, 2006-2017 TomTom
077.3000000° W
077.3000000° W
077.2833333° W
077.2833333° W
077.2666666° W
077.2666666° W36.300036.300036.2833333° N36.2833333° N36.2666666° N36.2666666° N6.2500000° N6.2500000° NName: Site Location Map Map Center Location: 036.2741410° N 077.2842062° W
Date: 05/16/17
Scale: 1 inch = 2,000 ft.
Generated by Geological Resources, Inc.
Declination
MN 10.12° WGN 1.35° W
MNGN
Figure 1
Red Apple Mart #9
100 W. Jackson Street
Rich Square, Northampton County
North Carolina
Incident No. 11920
GRI Project No. 4497
SCALE 1:24000
0 1000 2000 3000 4000 5000 6000
FEET
SITE
5902-53-7210
5902-52-5930 5902-53-60845902-53-8071
5902-52-7962
5902-52-7801
5902-52-89365902-52-8948
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P, NRCan, Esri Japan, METI, Esri China (Hong Kong), Esri Korea, Esri (Thailand), NGCC, ©OpenStreetMap contributors, and the GIS User Community
FIGURE 3: SITE VICINITY MAPRAM #9100 W. JACKSON STREETRICH SQUARE, NORTHAMPTON COUNTYNORTH CAROLINAINCIDENT NO. 11920GRI PROJECT NO. 4497
PREPARED BY:GEOLOGICAL RESOURCES,INC.APRIL 28, 2017
³
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
250-FOOT RADIUS
250-FOOT RADIUS
LEGEND
Adjacent Properties
ncrivers
nc_northampton_parcels_poly

TABLES
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1, A2 & A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 through 7 Facility ID Number
Owner or Operator?
Owner/Operator
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
Red Apple Markets, Inc./Eastern Fuels, Inc.08/26/1992 - 03/28/2002
Red Apple Markets, Inc./Eastern Fuels, Inc.12/30/1988 - 07/16/1992
Address Telephone Number
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
0-026624
804-590-3555
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Name of Owner or Operator Dates of Ownership / Operation
Eastern Fuels, Inc.08/26/1992 - 10/26/2006
Address Telephone Number
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Address Telephone Number
443-393-6270
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Classic Ventures, LLC 10/26/2006 - 10/27/2006
Address Telephone Number
710 North Hamilton Street, #200, Richmond, VA 23221
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Jernigan Oil Company, Inc.01/10/2012 - Current
Address
SDA Ventures, LLC 10/27/2006 - 01/10/2012
10211 Wincopin Circle, Suite 300, Columbia MD, 21044
P.O. Box 688, Ahoskie, NC 29710 252-332-2131
Telephone Number
TABLE 1
UST OWNER/OPERATOR INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Page 1 of 2
TABLE 1
UST OWNER/OPERATOR INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
UST ID Number 1 through 7 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 2 through 7 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
0-026624
Name of Owner or Operator Dates of Ownership / Operation
Unknown 10/09/1982 - 12/30/1988
Telephone Number
0-026624
P.O. Box 1386, Ahoskie, NC 27910 252-398-6022
Unknown 08/01/1975 - 10/09/1982
Name of Owner or Operator Dates of Ownership / Operation
Address
Page 2 of 2
Date: 01/16/20
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 8,000 10/9/1982 Single Wall Steel 8 x 21' 4"Single Wall Steel Removed
(07/16/92)Yes
2 Gasoline 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
3 Gasoline 5,000 8/1/1975 Single Wall Steel 8' x 13' 5"Single Wall FRP Removed
(07/16/92)Yes
4 Gasoline 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
5 #2 Fuel Oil 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
6 #2 Fuel Oil 3,000 8/1/1975 Single Wall Steel 64" x 18'Single Wall Steel Removed
(07/16/92)Yes
7 Kerosene 2,000 8/1/1975 Single Wall Steel 64" x 12'Single Wall Steel Removed
(07/16/92)Yes
A1 Gasoline 10,000 8/26/1992 Single Wall Steel 8' x 26' 7"Single Wall Flex Current No
A2 Gasoline 6,000 8/26/1992 Single Wall Steel 8' x 16'Single Wall Flex Current No
A3 Kerosene 4,000 8/26/1992 Single Wall Steel 64" x 24'Single Wall Flex Current No
Notes:
• FRP: Fiberglass reinforced plastic.
• This table is based off of historical information provided by a previous consultant and does not match the Resistered Tank Database.
TABLE 2
UST SYSTEM INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID # : 0-026624
Status
of
UST
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Page 1 of 1
Date: 01/16/20 Facility ID # : 0-025344
Parcel Number Owner Name Address
0604542 Jernigan Properties, Inc.Post Office Box 688
Ahoskie, NC 27910
0605367 Town of Rich Square
c/o Vernice B Long, Clerk
Post Office Box 336
Rich Square, NC 27869
1301125 Wayne Ray Parker &
Lisa Parker Evans
100 S. Main Street
Littleton, NC 27850
0600629 Themistoklis Zacharopoulous 209 S. Main Street
Rich Square, NC 27869
1300360 Darlene M. Zacharoloulos Post Office Box 1
Rich Square, NC 27869
0601555 Charles S. Simmons 110 Walnut Circle
Emporia, VA 23847
0601556 Charles S. Simmons 110 Walnut Circle
Emporia, VA 23847
0601561 Charles S. Simmons 110 Walnut Circle
Emporia, VA 23847
Note:
• Properties are keyed to Figure 3.
TABLE 3
ADJACENT PROPERTY OWNER INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920))
Page 1 of 1
Date: 01/17/2021
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
05/02/17 7.56 4.35 96.17
08/16/17 6.69 4.08 96.81
05/21/18 7.10 3.89 96.24 Before MMPE
05/25/18 13.56 ---86.44 After MMPE
07/18/18 4.60 0.08 95.47
02/25/19 1.82 0.06 98.23 Before MMPE
03/01/19 11.20 ---88.80 After MMPE
04/15/19 2.25 0.07 97.81
11/26/19 6.27 0.02 93.75 Before AFVR
11/26/19 13.28 ---86.72 After AFVR
01/07/20 2.28 0.05 97.76
01/06/21 3.31 0.26 96.91
05/02/17 5.23 ---94.88
05/21/18 4.54 ---95.57 Before MMPE
05/25/18 4.25 ---95.86 After MMPE
07/18/18 6.65 ---93.46
02/25/19 1.96 ---98.15
04/15/19 2.56 ---97.55
01/07/20 8.09 ---92.02
01/06/21 4.42 ---95.69
05/02/17 4.66 ---96.24
05/21/18 4.84 ---96.06 Before MMPE
05/25/18 4.35 ---96.55 After MMPE
07/18/18 7.07 ---93.83
04/15/19 2.17 ---98.73
01/07/20 7.75 ---93.15
01/06/21 5.63 ---95.27
05/02/17 4.21 ---96.31
07/18/18 7.00 ---93.52
04/15/19 3.63 ---96.89
01/07/20 7.72 ---92.80
01/06/21 5.28 ---95.24
05/02/17 2.32 ---98.75
07/18/18 5.17 ---95.90
02/25/19 0.70 ---100.37
04/15/19 0.95 ---100.12
01/07/20 1.14 ---99.93
01/06/21 1.23 ---99.84
05/02/17 9.54 ---91.37
07/18/18 10.49 ---90.42
04/15/19 6.89 ---94.02
01/07/20 12.14 ---88.77
01/06/21 9.47 ---91.44
05/02/17 5.07 ---94.54
07/18/18 5.21 ---94.40
04/15/19 3.93 ---95.68
01/07/20 6.03 ---93.58
01/06/21 3.47 ---96.14
05/02/17 6.14 ---94.07
05/21/18 6.01 ---94.20 Before MMPE
05/25/18 9.53 ---90.68 After MMPE
07/18/18 7.04 ---93.17
02/25/19 0.87 ---99.34
04/15/19 4.18 ---96.03
01/07/20 7.03 ---93.18
01/06/21 6.24 ---93.97
05/02/17 6.07 ---94.56
07/18/18 7.65 ---92.98
04/15/19 3.32 ---97.31
01/07/20 8.69 ---91.94
01/06/21 5.34 ---95.29
05/02/17 8.56 ---92.50
07/18/18 9.16 ---91.90
04/15/19 5.54 ---95.52
01/07/20 10.77 ---90.29
01/06/21 8.32 ---92.74
MW-11 01/06/21 01/06/21 2 2-17 17 100.47 6.70 ---93.77
MW-12 01/06/21 01/06/21 2 2-17 17 99.82 12.21 ---87.61
MW-13 01/06/21 01/06/21 2 2-17 17 99.53 15.72 ---83.81
MW-10 101.06166-16608/26/94
100.63166-16608/26/94
MW-3
100.52166-16606/24/93MW-4
7 100.90177-17
MW-1
706/23/93MW-2
100.00188-18
100.11177-17
101.07177-17
806/23/93
06/23/93
3008/25/94
706/24/93MW-5
99.61166-16
100.913530-35
MW-8
MW-9
TABLE 4
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID # : 0-026624
100.21166-16608/26/94
MWD-6
608/26/94MW-7
Page 1 of 2
Date: 01/17/2021
Well ID
Date
Installed
(m/dd/yy)
Date Water
Level
Measured
(m/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free Product
Thickness
(ft.)
Ground
Water
Elevation (ft.)
Comments
TABLE 4
WELL CONSTRUCTION AND GAUGING INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID # : 0-026624
MW-14 01/06/21 01/06/21 2 2-17 17 99.59 17.05 ---82.54
Notes:
• NM : Not measured.
• Elevation relative to mean sea level.
• ft BGS : feet below ground surface.
Page 2 of 2
Date : 02/01/2021 Facility ID #: 0-026624
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 1
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 1,000
05/02/17 FP FP FP FP FP FP FP FP FP FP FP FP FP
05/21/18 FP FP FP FP FP FP FP FP FP FP FP FP FP
07/18/18 FP FP FP FP FP FP FP FP FP FP FP FP FP
04/15/19 FP FP FP FP FP FP FP FP FP FP FP FP FP
01/07/20 FP FP FP FP FP FP FP FP FP FP FP FP FP
01/06/21 FP FP FP FP FP FP FP FP FP FP FP FP FP
05/02/17 452 8.3 12.2 13.0 18.4 67.2 <0.13 21.9 4.4 44.9 0.54 0.66 13.4
07/18/18 938 21.1 14.7 71.2 34.5 234 <1.3 29.5 39.8 56.1 <1.3 3.2 J NR
04/15/19 1,930 33.1 36.7 64.9 J 37.2 425 <6.3 34.7 9.6 J 104 <6.3 <6.3 NR
01/07/20 846 30.6 30.5 102 27.7 430 <3.1 51.8 16.6 100 <3.1 5.3 J NR
01/06/21 652 29.1 25.4 82.4 22.6 453 <2.5 44.0 16.0 87.7 <2.5 4.8 J NR
05/02/17 <0.13 <0.13 <0.13 <0.25 0.55 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 0.88 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 0.48 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 0.69 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 0.47 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 0.18 J <0.13 <0.13 <0.13 0.64 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 0.16 J <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 9.3 0.44 J 0.63 <0.13 63.0 <0.13 <0.13 <0.13 <0.38
07/18/18 <0.13 <0.13 <0.13 <0.25 8.0 <0.13 0.68 <0.13 69.3 <0.13 <0.13 <0.13 NR
04/15/19 <0.25 <0.25 <0.25 <0.50 6.1 <0.25 0.73 J <0.25 86.4 <0.25 <0.25 <0.25 NR
01/07/20 <0.31 <0.31 <0.31 <0.63 8.6 <0.31 0.70 J <0.31 101 <0.31 <0.31 <0.31 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 4.3 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.40
07/18/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
05/02/17 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.40
07/18/18 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 0.95 <0.13 1.3 1.6 0.43 J NR
05/02/17 0.17 J <0.13 0.27 J 0.78 J <0.13 0.58 <0.13 0.68 <0.13 1.7 23.0 7.5 2.3
07/18/18 15.0 47.0 40.6 46.1 <0.63 8.8 <0.63 25.2 <0.63 87.6 655 224 NR
04/15/19 <0.13 <0.13 0.70 <0.25 <0.13 0.18 J <0.13 0.23 J <0.13 0.56 3.4 0.74 NR
01/07/20 61.4 45.8 65.8 17.3 <0.31 4.5 <0.31 21.7 0.39 J 62.7 72.7 13.6 NR
01/06/21 <0.13 <0.13 0.57 0.36 J <0.13 <0.13 0.33 J <0.13 61.7 <0.13 <0.13 <0.13 NR
05/02/17 498 171 84.0 121 237 114 0.47 J 14.8 22.5 29.3 12.9 3.1 19.6
07/18/18 16.8 0.25 J 0.71 0.55 J 7.9 1.8 <0.13 0.20 J 0.71 0.20 J <0.13 <0.13 NR
04/15/19 <0.13 <0.13 <0.13 <0.25 1.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
01/07/20 16.6 0.27 J <0.13 <0.25 9.5 0.95 <0.13 <0.13 0.82 <0.13 0.15 J <0.13 NR
01/06/21 <0.13 <0.13 <0.13 <0.25 0.14 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 NR
MW-11 01/06/21 <0.13 4.9 4.5 30.0 11.6 8.9 <0.13 2.0 0.22 J 4.0 16.1 5.3 NR
MW-12 01/06/21 <0.13 0.62 0.50 2.5 3.8 0.45 J <0.13 0.22 J 0.59 0.78 1.6 0.45 J NR
MW-13 01/06/21 58.6 41.5 160 407 37.6 101 <0.63 20.4 4.8 60.6 207 72.6 NR
MW-8
MW-9
MW-10
MW-1
MW-2
MW-3
MW-4
MW-5
MWD-6
MW-7 1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1-MethylnaphthaleneMAC (µg/l)
GCL (µg/l)MTBENaphthalene1,2-DichloroethaneIsopropylbenzeneIPEn-PropylbenzeneTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Analytical Method
→ EPA Methods 6200B & 610
Contaminant of Concern
BenzeneTolueneEthylbenzeneXylenesPage 1 of 2
Date : 02/01/2021 Facility ID #: 0-026624
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 400 400 1
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 28,500 25,000 1,0001,2,4-Trimethylbenzene1,3,5-Trimethylbenzene1-MethylnaphthaleneMAC (µg/l)
GCL (µg/l)MTBENaphthalene1,2-DichloroethaneIsopropylbenzeneIPEn-PropylbenzeneTABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Analytical Method
→ EPA Methods 6200B & 610
Contaminant of Concern
BenzeneTolueneEthylbenzeneXylenesMW-14 01/06/21 0.15 J 2.2 1.0 5.2 61.7 0.42 J <0.13 0.16 J 0.36 J 0.41 J 2.8 0.95 NR
Notes:
• Results reported in µg/l (micrograms per liter).
• MAC: Maximum allowable concentrations also known as the 2L Standards specified in T15A NCAC 2L.0202.
• GCL : Gross contamination level.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L Standards; concentration in italics exceeded the GCLs.
• NS: Not Sampled, well not located and assumed to be destroyed.
• FP: Free Product.
• Please refer to the lab report for detectable concentrations which did not exceed the 2L Standards, or for which no standard has been established.
Page 2 of 2
Date: 01/16/20
Method of Measurement:
Well ID
Product Type
(gas, diesel,
etc.)
Date of Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness
before
Recovery
(feet)
Product
Thickness
after
Recovery
(feet)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
08/16/17 Hand Bailing 4.08 0.00 7 5.3
05/21/18 - 05/26/18 MMPE 3.89 0.00 1,811 0.00
02/25/19 - 03/01/19 MMPE 0.06 0.00 1,968 0.00
11/26/19 AFVR 0.02 0.00 160 0.00
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• **: No free product was observed during initial gauging event; however, free product entered the well during purging activities.
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
MW-1 Oil 2
TABLE 6
FREE PRODUCT RECOVERY RESULTS
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID#: 0-026624
Interface probe at top-of-casing
Page 1 of 1
Date: 01/16/20
08/16/17 Hand Bailing ------------7 5.25 5.25
05/21/18 - 05/26/18 MMPE 54.72 85.37 577.16 2.17 1,811 0 2.17
02/25/19 - 03/01/19 MMPE 521 58.6 24.3 2.27 1,968 0 2.27
11/26/19 AFVR 1,459 77.8 13.9 0.42 160 0 0.42
4.86 3,946 5.25 10.11
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.15
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
TABLE 7
FREE PRODUCT RECOVERY EVENT INFORMATION
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Facility ID #: 0-026624
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Totals
SUMMARY OF FLUID REMOVAL
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid (gallons)
Total Amount
of Product
Recovered
(gallons)
MW-1
Total To Date 3,951.11 10.11
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
Current Event 160.42 0.42
Page 1 of 1
Date: 01/16/20 Facility ID #: 0-026624
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered
(gallons)
Cost of Free
Product Recovery
Event
Cost Per Gallon
(total fluids)Comments
MMPE 05/21/18 -
05/26/18 1,813.17 $8,142.85 $4.49 Cost per gallon for the event is based on a total volume of
1,813.17 gallons of free product and water.
MMPE 02/25/19 -
03/01/19 1,970.27 $7,977.80 $4.05 Cost per gallon for the event is based on a total volume of
1,970.27 gallons of free product and water.
AFVR 11/26/2019 160.42 $2,070.00 $12.90 Cost per gallon for the event is based on a total volume of
160.42 gallons of free product and water.
3,943.86 $18,190.65 $4.61
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, MMPE sampling, MMPE sampling analytical and project
management.
MW-1
TOTAL (to date)
TABLE 8
FREE PRODUCT RECOVERY COST SUMMARY
RED APPLE MARKET #9 (INCIDENT NO. 11920)
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

APPENDIX B
Well Construction Records and Subsurface Logs
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Red Apple Market #9
Address 100 West Jackson Street, Rich Square, North Carolina
Boring Number MW-11 Date Drilled
Sample Method N/A Drilling Method Hand Auger/SSA
Completion Details
Driller Geological Resources, Inc. Log By Ethan Rogerson, GRI
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4

6
8
10

12
14
16
Terminal Depth = 17'
18
20

22

24
26

28

30
32
34

36

38

40

10' - 17' Brown silty CLAY
01/06/21
0' - 0.5' Concrete; 0.5' - 10' Gray silty CLAY

2" well completed to 17' w/15' screen interval; sand 1'-17'; bentonite 0.5'-1'; grout 0'-0.5'
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Red Apple Market #9
Address 100 West Jackson Street, Rich Square, North Carolina
Boring Number MW-12 Date Drilled
Sample Method N/A Drilling Method Hand Auger/SSA
Completion Details
Driller Geological Resources, Inc. Log By Ethan Rogerson, GRI
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4

6
8
10

12
14
16
Terminal Depth = 17'
18
20

22

24
26

28

30
32
34

36

38

40

01/06/21
2" well completed to 17' w/15' screen interval; sand 1'-17'; bentonite 0.5'-1'; grout 0'-0.5'
0' - 0.5' Concrete; 0.5' - 10' Gray silty CLAY

10' - 17' Brown silty CLAY
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Red Apple Market #9
Address 100 West Jackson Street, Rich Square, North Carolina
Boring Number MW-13 Date Drilled
Sample Method N/A Drilling Method Hand Auger/SSA
Completion Details
Driller Geological Resources, Inc. Log By Ethan Rogerson, GRI
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4

6
8
10

12
14
16
Terminal Depth = 17'
18
20

22

24
26

28

30
32
34

36

38

40

01/06/21
2" well completed to 17' w/15' screen interval; sand 1'-17'; bentonite 0.5'-1'; grout 0'-0.5'
0' - 0.5' Concrete; 0.5' - 10' Gray silty CLAY

10' - 17' Brown silty CLAY
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Red Apple Market #9
Address 100 West Jackson Street, Rich Square, North Carolina
Boring Number MW-14 Date Drilled
Sample Method N/A Drilling Method Hand Auger/SSA
Completion Details
Driller Geological Resources, Inc. Log By Ethan Rogerson, GRI
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY
0
2
4

6
8
10

12
14
16
Terminal Depth = 17'
18
20

22

24
26

28

30
32
34

36

38

40

01/06/21
2" well completed to 17' w/15' screen interval; sand 1'-17'; bentonite 0.5'-1'; grout 0'-0.5'
0' - 0.5' Concrete; 0.5' - 10' Gray silty CLAY

10' - 17' Brown silty CLAY

APPENDIX C
Laboratory Report – Ground Water Samples
01/15/21
Technical Report for
GRI (Geological Resources Inc.)
RAM 9; 100 Jackson St, Rich Square, NC
4497
SGS Job Number: FA82247
Sampling Date: 01/06/21
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]; [e-mail]
ATTN: William Regenthall
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 01/15/21
e-Hardcopy 2.0
Automated Report
58
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 58
FA82247
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: FA82247-1: MW-3 ........................................................................................................10
3.2: FA82247-2: MW-2 ........................................................................................................12
3.3: FA82247-3: MW-5 ........................................................................................................14
3.4: FA82247-4: MW-4 ........................................................................................................16
3.5: FA82247-5: MW-9 ........................................................................................................18
3.6: FA82247-6: MWD-6 .....................................................................................................20
3.7: FA82247-7: MW-10 ......................................................................................................22
3.8: FA82247-8: MW-8 ........................................................................................................24
3.9: FA82247-9: MW-11 ......................................................................................................26
3.10: FA82247-10: MW-14 ..................................................................................................28
3.11: FA82247-11: MW-12 ..................................................................................................30
3.12: FA82247-12: MW-13 ..................................................................................................32
3.13: FA82247-13: MW-7 ....................................................................................................34
Section 4: Misc. Forms ............................................................................................................36
4.1: Chain of Custody ...........................................................................................................37
Section 5: MS Volatiles - QC Data Summaries .....................................................................40
5.1: Method Blank Summary ................................................................................................41
5.2: Blank Spike Summary ...................................................................................................47
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................53 123452 of 58
FA82247
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA82247
RAM 9; 100 Jackson St, Rich Square, NC
Project No: 4497
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA82247-1 01/06/21 14:08 MEER 01/08/21 AQ Ground Water MW-3
FA82247-2 01/06/21 14:15 MEER 01/08/21 AQ Ground Water MW-2
FA82247-3 01/06/21 14:21 MEER 01/08/21 AQ Ground Water MW-5
FA82247-4 01/06/21 14:24 MEER 01/08/21 AQ Ground Water MW-4
FA82247-5 01/06/21 14:31 MEER 01/08/21 AQ Ground Water MW-9
FA82247-6 01/06/21 14:39 MEER 01/08/21 AQ Ground Water MWD-6
FA82247-7 01/06/21 14:42 MEER 01/08/21 AQ Ground Water MW-10
FA82247-8 01/06/21 14:49 MEER 01/08/21 AQ Ground Water MW-8
FA82247-9 01/06/21 14:56 MEER 01/08/21 AQ Ground Water MW-11
FA82247-10 01/06/21 15:00 MEER 01/08/21 AQ Ground Water MW-14
FA82247-11 01/06/21 15:07 MEER 01/08/21 AQ Ground Water MW-12
FA82247-12 01/06/21 15:10 MEER 01/08/21 AQ Ground Water MW-13
3 of 58
FA822471
SGS North America Inc.
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA82247
RAM 9; 100 Jackson St, Rich Square, NC
Project No: 4497
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA82247-13 01/06/21 14:53 MEER 01/08/21 AQ Ground Water MW-7
4 of 58
FA822471
Summary of Hits Page 1 of 4
Job Number:FA82247
Account:GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Collected:01/06/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA82247-1 MW-3
Methyl Tert Butyl Ether 0.47 J 0.50 0.13 ug/l SM 6200B
FA82247-2 MW-2
Benzene 652 10 2.5 ug/l SM 6200B
n-Butylbenzene 10.3 10 2.5 ug/l SM 6200B
sec-Butylbenzene 12.9 10 2.5 ug/l SM 6200B
Chloroform 3.1 J 10 2.5 ug/l SM 6200B
Di-Isopropyl Ether 16.0 10 2.5 ug/l SM 6200B
Ethylbenzene 25.4 10 2.5 ug/l SM 6200B
Isopropylbenzene 44.0 10 2.5 ug/l SM 6200B
Methyl Tert Butyl Ether 22.6 10 2.5 ug/l SM 6200B
Naphthalene 453 10 2.5 ug/l SM 6200B
n-Propylbenzene 87.7 10 2.5 ug/l SM 6200B
Toluene 29.1 10 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 4.8 J 10 2.5 ug/l SM 6200B
m,p-Xylene 75.6 20 2.5 ug/l SM 6200B
o-Xylene 6.8 J 10 2.5 ug/l SM 6200B
Xylene (total)82.4 30 5.0 ug/l SM 6200B
FA82247-3 MW-5
No hits reported in this sample.
FA82247-4 MW-4
No hits reported in this sample.
FA82247-5 MW-9
n-Butylbenzene 0.58 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.55 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.57 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.95 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.60 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 1.3 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.6 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.43 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 0.21 J 1.0 0.13 ug/l SM 6200B
o-Xylene 0.15 J 0.50 0.13 ug/l SM 6200B
Xylene (total)0.36 J 1.5 0.25 ug/l SM 6200B
5 of 58
FA822472
Summary of Hits Page 2 of 4
Job Number:FA82247
Account:GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Collected:01/06/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA82247-6 MWD-6
1,2-Dichloroethane 0.33 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 61.7 1.0 0.25 ug/l SM 6200B
Methyl Tert Butyl Ether 4.3 0.50 0.13 ug/l SM 6200B
Tetrachloroethylene 0.13 J 0.50 0.13 ug/l SM 6200B
Trichloroethylene 0.31 J 0.50 0.13 ug/l SM 6200B
FA82247-7 MW-10
sec-Butylbenzene 0.20 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 0.14 J 0.50 0.13 ug/l SM 6200B
FA82247-8 MW-8
No hits reported in this sample.
FA82247-9 MW-11
n-Butylbenzene 1.0 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 1.6 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.64 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.22 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 4.5 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 2.0 0.50 0.13 ug/l SM 6200B
p-Isopropyltoluene 0.23 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 11.6 0.50 0.13 ug/l SM 6200B
Naphthalene 8.9 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 4.0 0.50 0.13 ug/l SM 6200B
Toluene 4.9 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 16.1 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 5.3 0.50 0.13 ug/l SM 6200B
m,p-Xylene 20.3 1.0 0.13 ug/l SM 6200B
o-Xylene 9.7 0.50 0.13 ug/l SM 6200B
Xylene (total)30.0 1.5 0.25 ug/l SM 6200B
FA82247-10 MW-14
Benzene 0.15 J 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 0.30 J 0.50 0.13 ug/l SM 6200B
Di-Isopropyl Ether 0.36 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 1.0 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.16 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 61.7 1.0 0.25 ug/l SM 6200B
Naphthalene 0.42 J 0.50 0.13 ug/l SM 6200B
6 of 58
FA822472
Summary of Hits Page 3 of 4
Job Number:FA82247
Account:GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Collected:01/06/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
n-Propylbenzene 0.41 J 0.50 0.13 ug/l SM 6200B
Toluene 2.2 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 2.8 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.95 0.50 0.13 ug/l SM 6200B
m,p-Xylene 3.6 1.0 0.13 ug/l SM 6200B
o-Xylene 1.5 0.50 0.13 ug/l SM 6200B
Xylene (total)5.2 1.5 0.25 ug/l SM 6200B
FA82247-11 MW-12
Di-Isopropyl Ether 0.59 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.50 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 0.22 J 0.50 0.13 ug/l SM 6200B
Methyl Tert Butyl Ether 3.8 0.50 0.13 ug/l SM 6200B
Naphthalene 0.45 J 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 0.78 0.50 0.13 ug/l SM 6200B
Toluene 0.62 0.50 0.13 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.6 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.45 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 1.9 1.0 0.13 ug/l SM 6200B
o-Xylene 0.62 0.50 0.13 ug/l SM 6200B
Xylene (total)2.5 1.5 0.25 ug/l SM 6200B
FA82247-12 MW-13
Benzene a 58.6 2.5 0.63 ug/l SM 6200B
n-Butylbenzene a 6.6 2.5 0.63 ug/l SM 6200B
sec-Butylbenzene a 4.7 2.5 0.63 ug/l SM 6200B
Di-Isopropyl Ether a 4.8 2.5 0.63 ug/l SM 6200B
Ethylbenzene a 160 2.5 0.63 ug/l SM 6200B
Isopropylbenzene a 20.4 2.5 0.63 ug/l SM 6200B
p-Isopropyltoluene a 4.0 2.5 0.63 ug/l SM 6200B
Methyl Tert Butyl Ether a 37.6 2.5 0.63 ug/l SM 6200B
Naphthalene a 101 2.5 0.63 ug/l SM 6200B
n-Propylbenzene a 60.6 2.5 0.63 ug/l SM 6200B
Toluene a 41.5 2.5 0.63 ug/l SM 6200B
1,2,4-Trimethylbenzene a 207 2.5 0.63 ug/l SM 6200B
1,3,5-Trimethylbenzene a 72.6 2.5 0.63 ug/l SM 6200B
m,p-Xylene a 301 5.0 0.63 ug/l SM 6200B
o-Xylene a 106 2.5 0.63 ug/l SM 6200B
Xylene (total) a 407 7.5 1.3 ug/l SM 6200B
FA82247-13 MW-7
No hits reported in this sample.
7 of 58
FA822472
Summary of Hits Page 4 of 4
Job Number:FA82247
Account:GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Collected:01/06/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
8 of 58
FA822472
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
9 of 58
FA822473
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA82247-1 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105675.D 1 01/12/21 12:41 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 58
FA8224733.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA82247-1 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.47 0.50 0.13 ug/l J
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 93%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 58
FA8224733.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA82247-2 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105676.D 20 01/12/21 13:04 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 652 10 2.5 ug/l
108-86-1 Bromobenzene ND 10 2.5 ug/l
74-97-5 Bromochloromethane ND 10 2.5 ug/l
75-27-4 Bromodichloromethane ND 10 2.5 ug/l
75-25-2 Bromoform ND 10 2.5 ug/l
104-51-8 n-Butylbenzene 10.3 10 2.5 ug/l
135-98-8 sec-Butylbenzene 12.9 10 2.5 ug/l
98-06-6 tert-Butylbenzene ND 10 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
75-00-3 Chloroethane ND 10 4.0 ug/l
67-66-3 Chloroform 3.1 10 2.5 ug/l J
95-49-8 o-Chlorotoluene ND 10 2.5 ug/l
106-43-4 p-Chlorotoluene ND 10 2.5 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 10 4.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l
594-20-7 2,2-Dichloropropane ND 10 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 58
FA8224733.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA82247-2 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 16.0 10 2.5 ug/l
100-41-4 Ethylbenzene 25.4 10 2.5 ug/l
87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l
98-82-8 Isopropylbenzene 44.0 10 2.5 ug/l
99-87-6 p-Isopropyltoluene ND 10 2.5 ug/l
74-83-9 Methyl Bromide ND 10 4.0 ug/l
74-87-3 Methyl Chloride ND 10 4.0 ug/l
74-95-3 Methylene Bromide ND 10 2.5 ug/l
75-09-2 Methylene Chloride ND 40 20 ug/l
1634-04-4 Methyl Tert Butyl Ether 22.6 10 2.5 ug/l
91-20-3 Naphthalene 453 10 2.5 ug/l
103-65-1 n-Propylbenzene 87.7 10 2.5 ug/l
100-42-5 Styrene ND 10 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l
127-18-4 Tetrachloroethylene ND 10 2.5 ug/l
108-88-3 Toluene 29.1 10 2.5 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l
79-01-6 Trichloroethylene ND 10 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 10 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene 4.8 10 2.5 ug/l J
75-01-4 Vinyl Chloride ND 10 2.5 ug/l
m,p-Xylene 75.6 20 2.5 ug/l
95-47-6 o-Xylene 6.8 10 2.5 ug/l J
1330-20-7 Xylene (total)82.4 30 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 58
FA8224733.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA82247-3 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105677.D 1 01/12/21 13:27 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 58
FA8224733.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA82247-3 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 58
FA8224733.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-4
Lab Sample ID:FA82247-4 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105684.D 1 01/12/21 16:09 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 58
FA8224733.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-4
Lab Sample ID:FA82247-4 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 91%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 58
FA8224733.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA82247-5 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105685.D 1 01/12/21 16:32 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.58 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.55 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 58
FA8224733.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA82247-5 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.57 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.95 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.60 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 1.3 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.6 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.43 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 0.21 1.0 0.13 ug/l J
95-47-6 o-Xylene 0.15 0.50 0.13 ug/l J
1330-20-7 Xylene (total)0.36 1.5 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 58
FA8224733.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MWD-6
Lab Sample ID:FA82247-6 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105686.D 1 01/12/21 16:55 CV n/a n/a VE2413
Run #2 E105702.D 2 01/13/21 13:00 CV n/a n/a VE2414
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane 0.33 0.50 0.13 ug/l J
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 58
FA8224733.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MWD-6
Lab Sample ID:FA82247-6 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 61.7 a 1.0 0.25 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 4.3 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene 0.13 0.50 0.13 ug/l J
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene 0.31 0.50 0.13 ug/l J
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 95%100%70-130%
2037-26-5 Toluene-D8 96%95%70-130%
460-00-4 4-Bromofluorobenzene 103%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 58
FA8224733.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA82247-7 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105687.D 1 01/12/21 17:19 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.20 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 58
FA8224733.7
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA82247-7 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.14 0.50 0.13 ug/l J
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 58
FA8224733.7
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA82247-8 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105688.D 1 01/12/21 17:42 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 58
FA8224733.8
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA82247-8 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 58
FA8224733.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA82247-9 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105689.D 1 01/12/21 18:04 CV n/a n/a VE2413
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 1.0 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 1.6 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.64 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 58
FA8224733.9
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA82247-9 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.22 0.50 0.13 ug/l J
100-41-4 Ethylbenzene 4.5 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 2.0 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene 0.23 0.50 0.13 ug/l J
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 11.6 0.50 0.13 ug/l
91-20-3 Naphthalene 8.9 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 4.0 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 4.9 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 16.1 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 5.3 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 20.3 1.0 0.13 ug/l
95-47-6 o-Xylene 9.7 0.50 0.13 ug/l
1330-20-7 Xylene (total)30.0 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 58
FA8224733.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA82247-10 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105690.D 1 01/12/21 18:28 CV n/a n/a VE2413
Run #2 E105703.D 2 01/13/21 13:23 CV n/a n/a VE2414
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.15 0.50 0.13 ug/l J
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 0.30 0.50 0.13 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 58
FA8224733.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA82247-10 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.36 0.50 0.13 ug/l J
100-41-4 Ethylbenzene 1.0 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.16 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 61.7 a 1.0 0.25 ug/l
91-20-3 Naphthalene 0.42 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene 0.41 0.50 0.13 ug/l J
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 2.2 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 2.8 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.95 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 3.6 1.0 0.13 ug/l
95-47-6 o-Xylene 1.5 0.50 0.13 ug/l
1330-20-7 Xylene (total)5.2 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 96%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 94%101%70-130%
2037-26-5 Toluene-D8 96%96%70-130%
460-00-4 4-Bromofluorobenzene 103%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 58
FA8224733.10
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA82247-11 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105704.D 1 01/13/21 13:46 CV n/a n/a VE2414
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA82247-11 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 0.59 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.50 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 0.22 0.50 0.13 ug/l J
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.8 0.50 0.13 ug/l
91-20-3 Naphthalene 0.45 0.50 0.13 ug/l J
103-65-1 n-Propylbenzene 0.78 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 0.62 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.6 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.45 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 1.9 1.0 0.13 ug/l
95-47-6 o-Xylene 0.62 0.50 0.13 ug/l
1330-20-7 Xylene (total)2.5 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 2
Client Sample ID:MW-13
Lab Sample ID:FA82247-12 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0225137.D 5 01/14/21 14:57 LR n/a n/a VA2848
Run #2 b E105705.D 50 01/13/21 14:09 CV n/a n/a VE2414
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 58.6 2.5 0.63 ug/l
108-86-1 Bromobenzene ND 2.5 0.63 ug/l
74-97-5 Bromochloromethane ND 2.5 0.63 ug/l
75-27-4 Bromodichloromethane ND 2.5 0.63 ug/l
75-25-2 Bromoform ND 2.5 0.63 ug/l
104-51-8 n-Butylbenzene 6.6 2.5 0.63 ug/l
135-98-8 sec-Butylbenzene 4.7 2.5 0.63 ug/l
98-06-6 tert-Butylbenzene ND 2.5 0.63 ug/l
56-23-5 Carbon Tetrachloride ND 2.5 0.63 ug/l
108-90-7 Chlorobenzene ND 2.5 0.63 ug/l
75-00-3 Chloroethane ND 2.5 1.0 ug/l
67-66-3 Chloroform ND 2.5 0.63 ug/l
95-49-8 o-Chlorotoluene ND 2.5 0.63 ug/l
106-43-4 p-Chlorotoluene ND 2.5 0.63 ug/l
124-48-1 Dibromochloromethane ND 2.5 0.63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 2.5 1.2 ug/l
106-93-4 1,2-Dibromoethane ND 2.5 0.63 ug/l
75-71-8 Dichlorodifluoromethane ND 2.5 1.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 2.5 0.63 ug/l
541-73-1 1,3-Dichlorobenzene ND 2.5 0.63 ug/l
106-46-7 1,4-Dichlorobenzene ND 2.5 0.63 ug/l
75-34-3 1,1-Dichloroethane ND 2.5 0.63 ug/l
107-06-2 1,2-Dichloroethane ND 2.5 0.63 ug/l
75-35-4 1,1-Dichloroethylene ND 2.5 0.63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.5 0.63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.5 0.63 ug/l
78-87-5 1,2-Dichloropropane ND 2.5 0.63 ug/l
142-28-9 1,3-Dichloropropane ND 2.5 0.63 ug/l
594-20-7 2,2-Dichloropropane ND 2.5 0.63 ug/l
563-58-6 1,1-Dichloropropene ND 2.5 0.63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 2.5 0.63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 2.5 0.63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 2
Client Sample ID:MW-13
Lab Sample ID:FA82247-12 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 4.8 2.5 0.63 ug/l
100-41-4 Ethylbenzene 160 2.5 0.63 ug/l
87-68-3 Hexachlorobutadiene ND 2.5 0.63 ug/l
98-82-8 Isopropylbenzene 20.4 2.5 0.63 ug/l
99-87-6 p-Isopropyltoluene 4.0 2.5 0.63 ug/l
74-83-9 Methyl Bromide ND 2.5 1.0 ug/l
74-87-3 Methyl Chloride ND 2.5 1.0 ug/l
74-95-3 Methylene Bromide ND 2.5 0.63 ug/l
75-09-2 Methylene Chloride ND 10 5.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 37.6 2.5 0.63 ug/l
91-20-3 Naphthalene 101 2.5 0.63 ug/l
103-65-1 n-Propylbenzene 60.6 2.5 0.63 ug/l
100-42-5 Styrene ND 2.5 0.63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.5 0.63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.5 0.63 ug/l
127-18-4 Tetrachloroethylene ND 2.5 0.63 ug/l
108-88-3 Toluene 41.5 2.5 0.63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.5 0.63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.5 0.63 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.5 0.63 ug/l
79-00-5 1,1,2-Trichloroethane ND 2.5 0.63 ug/l
79-01-6 Trichloroethylene ND 2.5 0.63 ug/l
75-69-4 Trichlorofluoromethane ND 2.5 1.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.5 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 207 2.5 0.63 ug/l
108-67-8 1,3,5-Trimethylbenzene 72.6 2.5 0.63 ug/l
75-01-4 Vinyl Chloride ND 2.5 0.63 ug/l
m,p-Xylene 301 5.0 0.63 ug/l
95-47-6 o-Xylene 106 2.5 0.63 ug/l
1330-20-7 Xylene (total)407 7.5 1.3 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%100%70-130%
2037-26-5 Toluene-D8 98%96%70-130%
460-00-4 4-Bromofluorobenzene 98%99%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
(b) Confirmation run.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA82247-13 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 E105706.D 1 01/13/21 14:32 CV n/a n/a VE2414
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 58
FA8224733.13
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA82247-13 Date Sampled:01/06/21
Matrix:AQ - Ground Water Date Received:01/08/21
Method:SM 6200B Percent Solids:n/a
Project:RAM 9; 100 Jackson St, Rich Square, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA8224733.13
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
36 of 58
FA822474
FA82247: Chain of Custody
Page 1 of 3
37 of 58
FA8224744.1
SGS Sample Receipt Summary
Job Number:FA82247 Client:GEOLOGICAL RESOURCES
Date / Time Received:1/8/2021 10:00:00 AM Delivery Method:FX
Project:RAM #9
Airbill #'s:1009 6378 6040
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments RECEIVED EXTRA SAMPLE.
SAMPLE ID "MW-7" TIME "1453"
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.5);
Cooler 1: (1.7);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH Date:Date: 1/8/2021 10:00:00 AM
SM001Rev. Date 05/24/17
FA82247: Chain of Custody
Page 2 of 3
38 of 58
FA8224744.1
Per client analyze sample MW-7.Response:
Response Date:1/8/21CSR:Muna Mohammed
SM001Rev. Date 05/24/17
FA82247: Chain of Custody
Page 3 of 3
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FA8224744.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
40 of 58
FA822475
Method Blank Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2413-MB E105669.D 1 01/12/21 CV n/a n/a VE2413
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-1, FA82247-2, FA82247-3, FA82247-4, FA82247-5, FA82247-6, FA82247-7, FA82247-8, FA82247-9,
FA82247-10
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
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FA8224755.1.1
Method Blank Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2413-MB E105669.D 1 01/12/21 CV n/a n/a VE2413
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-1, FA82247-2, FA82247-3, FA82247-4, FA82247-5, FA82247-6, FA82247-7, FA82247-8, FA82247-9,
FA82247-10
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 98%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
42 of 58
FA8224755.1.1
Method Blank Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2414-MB E105697.D 1 01/13/21 CV n/a n/a VE2414
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-6, FA82247-10, FA82247-11, FA82247-13
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
43 of 58
FA8224755.1.2
Method Blank Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2414-MB E105697.D 1 01/13/21 CV n/a n/a VE2414
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-6, FA82247-10, FA82247-11, FA82247-13
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
44 of 58
FA8224755.1.2
Method Blank Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2848-MB A0225129.D 1 01/14/21 LR n/a n/a VA2848
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-12
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
45 of 58
FA8224755.1.3
Method Blank Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2848-MB A0225129.D 1 01/14/21 LR n/a n/a VA2848
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-12
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
46 of 58
FA8224755.1.3
Blank Spike Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2413-BS E105667.D 1 01/12/21 CV n/a n/a VE2413
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-1, FA82247-2, FA82247-3, FA82247-4, FA82247-5, FA82247-6, FA82247-7, FA82247-8, FA82247-9,
FA82247-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.3 93 70-130
108-86-1 Bromobenzene 10 8.4 84 70-130
74-97-5 Bromochloromethane 10 8.5 85 70-130
75-27-4 Bromodichloromethane 10 9.2 92 70-130
75-25-2 Bromoform 10 8.5 85 70-130
104-51-8 n-Butylbenzene 10 8.6 86 70-130
135-98-8 sec-Butylbenzene 10 9.0 90 70-130
98-06-6 tert-Butylbenzene 10 8.5 85 70-130
56-23-5 Carbon Tetrachloride 10 9.6 96 70-130
108-90-7 Chlorobenzene 10 8.2 82 70-130
75-00-3 Chloroethane 10 10.3 103 60-140
67-66-3 Chloroform 10 9.0 90 70-130
95-49-8 o-Chlorotoluene 10 8.3 83 70-130
106-43-4 p-Chlorotoluene 10 8.4 84 70-130
124-48-1 Dibromochloromethane 10 8.5 85 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.7 77 70-130
106-93-4 1,2-Dibromoethane 10 8.3 83 70-130
75-71-8 Dichlorodifluoromethane 10 9.6 96 60-140
95-50-1 1,2-Dichlorobenzene 10 8.0 80 70-130
541-73-1 1,3-Dichlorobenzene 10 8.3 83 70-130
106-46-7 1,4-Dichlorobenzene 10 8.4 84 70-130
75-34-3 1,1-Dichloroethane 10 9.7 97 70-130
107-06-2 1,2-Dichloroethane 10 8.6 86 70-130
75-35-4 1,1-Dichloroethylene 10 10.2 102 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.6 96 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.5 95 70-130
78-87-5 1,2-Dichloropropane 10 8.8 88 70-130
142-28-9 1,3-Dichloropropane 10 8.1 81 70-130
594-20-7 2,2-Dichloropropane 10 9.7 97 70-130
563-58-6 1,1-Dichloropropene 10 9.1 91 70-130
10061-01-5 cis-1,3-Dichloropropene 10 8.9 89 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.9 89 70-130
108-20-3 Di-Isopropyl Ether 10 8.5 85 70-130
100-41-4 Ethylbenzene 10 8.6 86 70-130
87-68-3 Hexachlorobutadiene 10 8.2 82 70-130
98-82-8 Isopropylbenzene 10 8.8 88 70-130
* = Outside of Control Limits.
47 of 58
FA8224755.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2413-BS E105667.D 1 01/12/21 CV n/a n/a VE2413
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-1, FA82247-2, FA82247-3, FA82247-4, FA82247-5, FA82247-6, FA82247-7, FA82247-8, FA82247-9,
FA82247-10
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.0 90 70-130
74-83-9 Methyl Bromide 10 9.5 95 60-140
74-87-3 Methyl Chloride 10 10 100 60-140
74-95-3 Methylene Bromide 10 8.8 88 70-130
75-09-2 Methylene Chloride 10 8.8 88 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.4 84 70-130
91-20-3 Naphthalene 10 7.9 79 70-130
103-65-1 n-Propylbenzene 10 8.5 85 70-130
100-42-5 Styrene 10 8.7 87 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.2 82 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.3 83 70-130
127-18-4 Tetrachloroethylene 10 9.0 90 70-130
108-88-3 Toluene 10 8.5 85 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.6 76 70-130
120-82-1 1,2,4-Trichlorobenzene 10 7.8 78 70-130
71-55-6 1,1,1-Trichloroethane 10 9.3 93 70-130
79-00-5 1,1,2-Trichloroethane 10 8.4 84 70-130
79-01-6 Trichloroethylene 10 9.1 91 70-130
75-69-4 Trichlorofluoromethane 10 10.7 107 60-140
96-18-4 1,2,3-Trichloropropane 10 8.4 84 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.3 83 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.6 86 70-130
75-01-4 Vinyl Chloride 10 10.5 105 60-140
m,p-Xylene 20 17.4 87 70-130
95-47-6 o-Xylene 10 8.5 85 70-130
1330-20-7 Xylene (total)30 25.9 86 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
48 of 58
FA8224755.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2414-BS E105695.D 1 01/13/21 CV n/a n/a VE2414
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-6, FA82247-10, FA82247-11, FA82247-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.7 97 70-130
108-86-1 Bromobenzene 10 8.6 86 70-130
74-97-5 Bromochloromethane 10 8.7 87 70-130
75-27-4 Bromodichloromethane 10 9.4 94 70-130
75-25-2 Bromoform 10 8.5 85 70-130
104-51-8 n-Butylbenzene 10 8.8 88 70-130
135-98-8 sec-Butylbenzene 10 9.4 94 70-130
98-06-6 tert-Butylbenzene 10 8.8 88 70-130
56-23-5 Carbon Tetrachloride 10 10.1 101 70-130
108-90-7 Chlorobenzene 10 8.6 86 70-130
75-00-3 Chloroethane 10 10.4 104 60-140
67-66-3 Chloroform 10 9.4 94 70-130
95-49-8 o-Chlorotoluene 10 8.7 87 70-130
106-43-4 p-Chlorotoluene 10 8.8 88 70-130
124-48-1 Dibromochloromethane 10 8.6 86 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 7.8 78 70-130
106-93-4 1,2-Dibromoethane 10 8.5 85 70-130
75-71-8 Dichlorodifluoromethane 10 8.9 89 60-140
95-50-1 1,2-Dichlorobenzene 10 8.2 82 70-130
541-73-1 1,3-Dichlorobenzene 10 8.6 86 70-130
106-46-7 1,4-Dichlorobenzene 10 8.7 87 70-130
75-34-3 1,1-Dichloroethane 10 10.0 100 70-130
107-06-2 1,2-Dichloroethane 10 8.5 85 70-130
75-35-4 1,1-Dichloroethylene 10 10.4 104 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.9 99 70-130
156-60-5 trans-1,2-Dichloroethylene 10 9.8 98 70-130
78-87-5 1,2-Dichloropropane 10 9.2 92 70-130
142-28-9 1,3-Dichloropropane 10 8.1 81 70-130
594-20-7 2,2-Dichloropropane 10 10.1 101 70-130
563-58-6 1,1-Dichloropropene 10 9.6 96 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.1 91 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.9 89 70-130
108-20-3 Di-Isopropyl Ether 10 8.7 87 70-130
100-41-4 Ethylbenzene 10 8.8 88 70-130
87-68-3 Hexachlorobutadiene 10 8.5 85 70-130
98-82-8 Isopropylbenzene 10 9.1 91 70-130
* = Outside of Control Limits.
49 of 58
FA8224755.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VE2414-BS E105695.D 1 01/13/21 CV n/a n/a VE2414
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-6, FA82247-10, FA82247-11, FA82247-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.4 94 70-130
74-83-9 Methyl Bromide 10 9.1 91 60-140
74-87-3 Methyl Chloride 10 9.3 93 60-140
74-95-3 Methylene Bromide 10 8.8 88 70-130
75-09-2 Methylene Chloride 10 9.0 90 70-130
1634-04-4 Methyl Tert Butyl Ether 10 8.6 86 70-130
91-20-3 Naphthalene 10 8.0 80 70-130
103-65-1 n-Propylbenzene 10 8.9 89 70-130
100-42-5 Styrene 10 9.0 90 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 8.4 84 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.3 83 70-130
127-18-4 Tetrachloroethylene 10 9.4 94 70-130
108-88-3 Toluene 10 8.9 89 70-130
87-61-6 1,2,3-Trichlorobenzene 10 7.7 77 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.1 81 70-130
71-55-6 1,1,1-Trichloroethane 10 9.7 97 70-130
79-00-5 1,1,2-Trichloroethane 10 8.5 85 70-130
79-01-6 Trichloroethylene 10 9.7 97 70-130
75-69-4 Trichlorofluoromethane 10 9.9 99 60-140
96-18-4 1,2,3-Trichloropropane 10 8.5 85 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.6 86 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.0 90 70-130
75-01-4 Vinyl Chloride 10 9.9 99 60-140
m,p-Xylene 20 18.0 90 70-130
95-47-6 o-Xylene 10 8.8 88 70-130
1330-20-7 Xylene (total)30 26.8 89 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
50 of 58
FA8224755.2.2
Blank Spike Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2848-BS A0225127.D 1 01/14/21 LR n/a n/a VA2848
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.3 103 70-130
108-86-1 Bromobenzene 10 9.7 97 70-130
74-97-5 Bromochloromethane 10 9.4 94 70-130
75-27-4 Bromodichloromethane 10 10.3 103 70-130
75-25-2 Bromoform 10 9.5 95 70-130
104-51-8 n-Butylbenzene 10 9.8 98 70-130
135-98-8 sec-Butylbenzene 10 10.6 106 70-130
98-06-6 tert-Butylbenzene 10 10 100 70-130
56-23-5 Carbon Tetrachloride 10 12.0 120 70-130
108-90-7 Chlorobenzene 10 9.8 98 70-130
75-00-3 Chloroethane 10 8.8 88 60-140
67-66-3 Chloroform 10 10.4 104 70-130
95-49-8 o-Chlorotoluene 10 9.6 96 70-130
106-43-4 p-Chlorotoluene 10 9.6 96 70-130
124-48-1 Dibromochloromethane 10 9.6 96 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.3 83 70-130
106-93-4 1,2-Dibromoethane 10 9.3 93 70-130
75-71-8 Dichlorodifluoromethane 10 9.3 93 60-140
95-50-1 1,2-Dichlorobenzene 10 9.4 94 70-130
541-73-1 1,3-Dichlorobenzene 10 9.7 97 70-130
106-46-7 1,4-Dichlorobenzene 10 9.5 95 70-130
75-34-3 1,1-Dichloroethane 10 10.9 109 70-130
107-06-2 1,2-Dichloroethane 10 9.6 96 70-130
75-35-4 1,1-Dichloroethylene 10 11.6 116 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.7 107 70-130
78-87-5 1,2-Dichloropropane 10 9.8 98 70-130
142-28-9 1,3-Dichloropropane 10 9.1 91 70-130
594-20-7 2,2-Dichloropropane 10 10.7 107 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.5 95 70-130
108-20-3 Di-Isopropyl Ether 10 9.2 92 70-130
100-41-4 Ethylbenzene 10 10.1 101 70-130
87-68-3 Hexachlorobutadiene 10 11.5 115 70-130
98-82-8 Isopropylbenzene 10 10.2 102 70-130
* = Outside of Control Limits.
51 of 58
FA8224755.2.3
Blank Spike Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2848-BS A0225127.D 1 01/14/21 LR n/a n/a VA2848
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-12
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.5 105 70-130
74-83-9 Methyl Bromide 10 8.3 83 60-140
74-87-3 Methyl Chloride 10 9.5 95 60-140
74-95-3 Methylene Bromide 10 9.5 95 70-130
75-09-2 Methylene Chloride 10 10.2 102 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.0 90 70-130
91-20-3 Naphthalene 10 9.2 92 70-130
103-65-1 n-Propylbenzene 10 10.0 100 70-130
100-42-5 Styrene 10 9.6 96 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.8 98 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.8 88 70-130
127-18-4 Tetrachloroethylene 10 11.1 111 70-130
108-88-3 Toluene 10 10 100 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.7 97 70-130
71-55-6 1,1,1-Trichloroethane 10 11.3 113 70-130
79-00-5 1,1,2-Trichloroethane 10 9.4 94 70-130
79-01-6 Trichloroethylene 10 10.4 104 70-130
75-69-4 Trichlorofluoromethane 10 11.4 114 60-140
96-18-4 1,2,3-Trichloropropane 10 9.0 90 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.4 94 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.8 98 70-130
75-01-4 Vinyl Chloride 10 9.7 97 60-140
m,p-Xylene 20 20.0 100 70-130
95-47-6 o-Xylene 10 9.7 97 70-130
1330-20-7 Xylene (total)30 29.7 99 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 97%70-130%
* = Outside of Control Limits.
52 of 58
FA8224755.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA82165-3MS E105678.D 5 01/12/21 CV n/a n/a VE2413
FA82165-3MSD E105679.D 5 01/12/21 CV n/a n/a VE2413
FA82165-3 E105672.D 1 01/12/21 CV n/a n/a VE2413
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-1, FA82247-2, FA82247-3, FA82247-4, FA82247-5, FA82247-6, FA82247-7, FA82247-8, FA82247-9,
FA82247-10
FA82165-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 51.1 102 50 50.9 102 0 70-130/20
108-86-1 Bromobenzene ND 50 45.3 91 50 44.1 88 3 70-130/20
74-97-5 Bromochloromethane ND 50 45.8 92 50 46.2 92 1 70-130/20
75-27-4 Bromodichloromethane ND 50 47.6 95 50 46.4 93 3 70-130/20
75-25-2 Bromoform ND 50 35.2 70 50 34.7 69*1 70-130/20
104-51-8 n-Butylbenzene ND 50 45.7 91 50 46.5 93 2 70-130/20
135-98-8 sec-Butylbenzene ND 50 49.4 99 50 50.0 100 1 70-130/20
98-06-6 tert-Butylbenzene ND 50 47.1 94 50 47.2 94 0 70-130/20
56-23-5 Carbon Tetrachloride ND 50 52.3 105 50 53.6 107 2 70-130/20
108-90-7 Chlorobenzene ND 50 45.2 90 50 44.8 90 1 70-130/20
75-00-3 Chloroethane ND 50 45.4 91 50 53.8 108 17 60-140/20
67-66-3 Chloroform ND 50 49.4 99 50 51.1 102 3 70-130/20
95-49-8 o-Chlorotoluene ND 50 45.7 91 50 46.1 92 1 70-130/20
106-43-4 p-Chlorotoluene ND 50 46.0 92 50 45.2 90 2 70-130/20
124-48-1 Dibromochloromethane ND 50 39.4 79 50 38.8 78 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 42.0 84 50 43.5 87 4 70-130/20
106-93-4 1,2-Dibromoethane ND 50 45.6 91 50 43.6 87 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 42.6 85 50 50.2 100 16 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 43.2 86 50 43.8 88 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 45.3 91 50 45.2 90 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 45.7 91 50 45.5 91 0 70-130/20
75-34-3 1,1-Dichloroethane ND 50 53.4 107 50 55.2 110 3 70-130/20
107-06-2 1,2-Dichloroethane ND 50 47.9 96 50 46.2 92 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 56.0 112 50 58.5 117 4 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 51.2 102 50 53.2 106 4 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 52.1 104 50 54.2 108 4 70-130/20
78-87-5 1,2-Dichloropropane ND 50 49.8 100 50 47.2 94 5 70-130/20
142-28-9 1,3-Dichloropropane ND 50 43.8 88 50 41.9 84 4 70-130/20
594-20-7 2,2-Dichloropropane ND 50 52.0 104 50 54.5 109 5 70-130/20
563-58-6 1,1-Dichloropropene ND 50 50.3 101 50 51.1 102 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 47.1 94 50 43.6 87 8 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 48.2 96 50 46.0 92 5 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 45.9 92 50 47.3 95 3 70-130/20
100-41-4 Ethylbenzene ND 50 46.8 94 50 47.3 95 1 70-130/20
87-68-3 Hexachlorobutadiene ND 50 43.6 87 50 46.1 92 6 70-130/20
98-82-8 Isopropylbenzene ND 50 47.5 95 50 49.6 99 4 70-130/20
* = Outside of Control Limits.
53 of 58
FA8224755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA82165-3MS E105678.D 5 01/12/21 CV n/a n/a VE2413
FA82165-3MSD E105679.D 5 01/12/21 CV n/a n/a VE2413
FA82165-3 E105672.D 1 01/12/21 CV n/a n/a VE2413
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-1, FA82247-2, FA82247-3, FA82247-4, FA82247-5, FA82247-6, FA82247-7, FA82247-8, FA82247-9,
FA82247-10
FA82165-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 0.41 J 50 49.0 97 50 49.5 98 1 70-130/20
74-83-9 Methyl Bromide ND 50 41.7 83 50 50.7 101 19 60-140/20
74-87-3 Methyl Chloride ND 50 45.5 91 50 54.4 109 18 60-140/20
74-95-3 Methylene Bromide ND 50 48.4 97 50 47.0 94 3 70-130/20
75-09-2 Methylene Chloride ND 50 49.2 98 50 51.5 103 5 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 44.7 89 50 46.4 93 4 70-130/20
91-20-3 Naphthalene 0.25 J 50 41.7 83 50 45.0 90 8 70-130/20
103-65-1 n-Propylbenzene ND 50 47.1 94 50 46.9 94 0 70-130/20
100-42-5 Styrene ND 50 46.1 92 50 45.5 91 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 44.1 88 50 46.2 92 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 45.1 90 50 44.9 90 0 70-130/20
127-18-4 Tetrachloroethylene ND 50 48.7 97 50 49.4 99 1 70-130/20
108-88-3 Toluene ND 50 46.4 93 50 46.9 94 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 39.7 79 50 42.0 84 6 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 41.5 83 50 43.8 88 5 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 51.9 104 50 53.2 106 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 45.6 91 50 45.0 90 1 70-130/20
79-01-6 Trichloroethylene ND 50 50.4 101 50 49.9 100 1 70-130/20
75-69-4 Trichlorofluoromethane ND 50 48.0 96 50 55.3 111 14 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 45.3 91 50 45.2 90 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 45.4 91 50 45.6 91 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 47.0 94 50 47.7 95 1 70-130/20
75-01-4 Vinyl Chloride ND 50 45.1 90 50 54.8 110 19 60-140/20
m,p-Xylene ND 100 94.6 95 100 96.0 96 1 70-130/20
95-47-6 o-Xylene ND 50 45.9 92 50 47.4 95 3 70-130/20
1330-20-7 Xylene (total)ND 150 141 94 150 143 95 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA82165-3 Limits
1868-53-7 Dibromofluoromethane 99%101%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%102%101%70-130%
2037-26-5 Toluene-D8 96%97%92%70-130%
460-00-4 4-Bromofluorobenzene 100%98%100%70-130%
* = Outside of Control Limits.
54 of 58
FA8224755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA82247-12MS E105707.D 50 01/13/21 CV n/a n/a VE2414
FA82247-12MSD E105708.D 50 01/13/21 CV n/a n/a VE2414
FA82247-12 a E105705.D 50 01/13/21 CV n/a n/a VE2414
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-6, FA82247-10, FA82247-11, FA82247-13
FA82247-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 67.6 500 583 103 500 577 102 1 70-130/20
108-86-1 Bromobenzene ND 500 455 91 500 454 91 0 70-130/20
74-97-5 Bromochloromethane ND 500 463 93 500 455 91 2 70-130/20
75-27-4 Bromodichloromethane ND 500 524 105 500 517 103 1 70-130/20
75-25-2 Bromoform ND 500 457 91 500 448 90 2 70-130/20
104-51-8 n-Butylbenzene ND 500 491 98 500 484 97 1 70-130/20
135-98-8 sec-Butylbenzene ND 500 511 102 500 507 101 1 70-130/20
98-06-6 tert-Butylbenzene ND 500 485 97 500 479 96 1 70-130/20
56-23-5 Carbon Tetrachloride ND 500 553 111 500 557 111 1 70-130/20
108-90-7 Chlorobenzene ND 500 454 91 500 450 90 1 70-130/20
75-00-3 Chloroethane ND 500 552 110 500 561 112 2 60-140/20
67-66-3 Chloroform ND 500 514 103 500 505 101 2 70-130/20
95-49-8 o-Chlorotoluene ND 500 479 96 500 475 95 1 70-130/20
106-43-4 p-Chlorotoluene ND 500 463 93 500 461 92 0 70-130/20
124-48-1 Dibromochloromethane ND 500 452 90 500 445 89 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 467 93 500 440 88 6 70-130/20
106-93-4 1,2-Dibromoethane ND 500 450 90 500 444 89 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 452 90 500 486 97 7 60-140/20
95-50-1 1,2-Dichlorobenzene ND 500 444 89 500 438 88 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 500 461 92 500 458 92 1 70-130/20
106-46-7 1,4-Dichlorobenzene ND 500 466 93 500 461 92 1 70-130/20
75-34-3 1,1-Dichloroethane ND 500 555 111 500 548 110 1 70-130/20
107-06-2 1,2-Dichloroethane ND 500 480 96 500 468 94 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 500 586 117 500 575 115 2 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 500 534 107 500 526 105 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 544 109 500 539 108 1 70-130/20
78-87-5 1,2-Dichloropropane ND 500 496 99 500 497 99 0 70-130/20
142-28-9 1,3-Dichloropropane ND 500 431 86 500 424 85 2 70-130/20
594-20-7 2,2-Dichloropropane ND 500 553 111 500 548 110 1 70-130/20
563-58-6 1,1-Dichloropropene ND 500 517 103 500 509 102 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 488 98 500 481 96 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 478 96 500 470 94 2 70-130/20
108-20-3 Di-Isopropyl Ether ND 500 481 96 500 477 95 1 70-130/20
100-41-4 Ethylbenzene 165 500 633 94 500 628 93 1 70-130/20
87-68-3 Hexachlorobutadiene ND 500 474 95 500 464 93 2 70-130/20
98-82-8 Isopropylbenzene 16.6 J 500 507 98 500 507 98 0 70-130/20
* = Outside of Control Limits.
55 of 58
FA8224755.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA82247-12MS E105707.D 50 01/13/21 CV n/a n/a VE2414
FA82247-12MSD E105708.D 50 01/13/21 CV n/a n/a VE2414
FA82247-12 a E105705.D 50 01/13/21 CV n/a n/a VE2414
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-6, FA82247-10, FA82247-11, FA82247-13
FA82247-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 500 504 101 500 503 101 0 70-130/20
74-83-9 Methyl Bromide ND 500 462 92 500 497 99 7 60-140/20
74-87-3 Methyl Chloride ND 500 482 96 500 515 103 7 60-140/20
74-95-3 Methylene Bromide ND 500 483 97 500 467 93 3 70-130/20
75-09-2 Methylene Chloride ND 500 530 106 500 519 104 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether 39.7 500 501 92 500 490 90 2 70-130/20
91-20-3 Naphthalene 85.1 500 536 90 500 543 92 1 70-130/20
103-65-1 n-Propylbenzene 52.6 500 533 96 500 532 96 0 70-130/20
100-42-5 Styrene ND 500 478 96 500 477 95 0 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 453 91 500 450 90 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 457 91 500 450 90 2 70-130/20
127-18-4 Tetrachloroethylene ND 500 498 100 500 495 99 1 70-130/20
108-88-3 Toluene 53.7 500 512 92 500 507 91 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 424 85 500 416 83 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 448 90 500 441 88 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 500 536 107 500 527 105 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 464 93 500 458 92 1 70-130/20
79-01-6 Trichloroethylene ND 500 519 104 500 519 104 0 70-130/20
75-69-4 Trichlorofluoromethane ND 500 521 104 500 547 109 5 60-140/20
96-18-4 1,2,3-Trichloropropane ND 500 450 90 500 452 90 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene 203 500 684 96 500 679 95 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 71.1 500 566 99 500 557 97 2 70-130/20
75-01-4 Vinyl Chloride ND 500 482 96 500 529 106 9 60-140/20
m,p-Xylene 310 1000 1280 97 1000 1260 95 2 70-130/20
95-47-6 o-Xylene 102 500 581 96 500 579 95 0 70-130/20
1330-20-7 Xylene (total)413 1500 1860 96 1500 1840 95 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA82247-12 Limits
1868-53-7 Dibromofluoromethane 101%100%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%102%100%70-130%
2037-26-5 Toluene-D8 96%97%96%70-130%
460-00-4 4-Bromofluorobenzene 101%101%99%70-130%
(a) Confirmation run.
* = Outside of Control Limits.
56 of 58
FA8224755.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA82331-8MS A0225140.D 5 01/14/21 LR n/a n/a VA2848
FA82331-8MSD A0225141.D 5 01/14/21 LR n/a n/a VA2848
FA82331-8 A0225130.D 1 01/14/21 LR n/a n/a VA2848
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-12
FA82331-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene ND 50 50.8 102 50 53.3 107 5 70-130/20
108-86-1 Bromobenzene ND 50 49.4 99 50 50.4 101 2 70-130/20
74-97-5 Bromochloromethane ND 50 46.4 93 50 49.3 99 6 70-130/20
75-27-4 Bromodichloromethane ND 50 48.3 97 50 51.6 103 7 70-130/20
75-25-2 Bromoform ND 50 36.9 74 50 39.5 79 7 70-130/20
104-51-8 n-Butylbenzene ND 50 46.3 93 50 49.7 99 7 70-130/20
135-98-8 sec-Butylbenzene ND 50 51.8 104 50 54.6 109 5 70-130/20
98-06-6 tert-Butylbenzene ND 50 48.7 97 50 51.8 104 6 70-130/20
56-23-5 Carbon Tetrachloride ND 50 57.8 116 50 66.4 133*14 70-130/20
108-90-7 Chlorobenzene ND 50 48.7 97 50 50.8 102 4 70-130/20
75-00-3 Chloroethane ND 50 49.6 99 50 53.0 106 7 60-140/20
67-66-3 Chloroform ND 50 50.5 101 50 53.1 106 5 70-130/20
95-49-8 o-Chlorotoluene ND 50 47.8 96 50 50.0 100 4 70-130/20
106-43-4 p-Chlorotoluene ND 50 48.0 96 50 49.3 99 3 70-130/20
124-48-1 Dibromochloromethane ND 50 42.2 84 50 45.2 90 7 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 36.9 74 50 40.3 81 9 70-130/20
106-93-4 1,2-Dibromoethane ND 50 46.0 92 50 47.0 94 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 45.4 91 50 53.1 106 16 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 45.6 91 50 48.9 98 7 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 47.9 96 50 50.2 100 5 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 46.7 93 50 48.6 97 4 70-130/20
75-34-3 1,1-Dichloroethane ND 50 52.9 106 50 56.4 113 6 70-130/20
107-06-2 1,2-Dichloroethane ND 50 48.7 97 50 50.0 100 3 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 55.8 112 50 59.2 118 6 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 51.1 102 50 54.7 109 7 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 52.1 104 50 56.1 112 7 70-130/20
78-87-5 1,2-Dichloropropane ND 50 49.2 98 50 50.7 101 3 70-130/20
142-28-9 1,3-Dichloropropane ND 50 46.0 92 50 47.0 94 2 70-130/20
594-20-7 2,2-Dichloropropane ND 50 48.7 97 50 54.9 110 12 70-130/20
563-58-6 1,1-Dichloropropene ND 50 52.0 104 50 55.2 110 6 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 45.0 90 50 45.5 91 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 45.5 91 50 46.9 94 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 50 44.8 90 50 47.4 95 6 70-130/20
100-41-4 Ethylbenzene ND 50 49.5 99 50 52.5 105 6 70-130/20
87-68-3 Hexachlorobutadiene ND 50 49.9 100 50 58.5 117 16 70-130/20
98-82-8 Isopropylbenzene ND 50 49.2 98 50 53.2 106 8 70-130/20
* = Outside of Control Limits.
57 of 58
FA8224755.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA82247
Account:GRINCC GRI (Geological Resources Inc.)
Project:RAM 9; 100 Jackson St, Rich Square, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA82331-8MS A0225140.D 5 01/14/21 LR n/a n/a VA2848
FA82331-8MSD A0225141.D 5 01/14/21 LR n/a n/a VA2848
FA82331-8 A0225130.D 1 01/14/21 LR n/a n/a VA2848
The QC reported here applies to the following samples:Method: SM 6200B
FA82247-12
FA82331-8 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 50.9 102 50 54.2 108 6 70-130/20
74-83-9 Methyl Bromide ND 50 53.0 106 50 54.0 108 2 60-140/20
74-87-3 Methyl Chloride ND 50 46.9 94 50 51.4 103 9 60-140/20
74-95-3 Methylene Bromide ND 50 47.9 96 50 49.2 98 3 70-130/20
75-09-2 Methylene Chloride ND 50 49.7 99 50 54.9 110 10 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 50 43.1 86 50 46.3 93 7 70-130/20
91-20-3 Naphthalene ND 50 39.8 80 50 46.2 92 15 70-130/20
103-65-1 n-Propylbenzene ND 50 49.8 100 50 51.8 104 4 70-130/20
100-42-5 Styrene ND 50 44.6 89 50 46.3 93 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 45.8 92 50 51.5 103 12 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 43.3 87 50 44.6 89 3 70-130/20
127-18-4 Tetrachloroethylene ND 50 54.7 109 50 58.6 117 7 70-130/20
108-88-3 Toluene ND 50 49.2 98 50 52.2 104 6 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 42.0 84 50 48.7 97 15 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 42.7 85 50 49.5 99 15 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 54.9 110 50 59.9 120 9 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 47.3 95 50 47.8 96 1 70-130/20
79-01-6 Trichloroethylene ND 50 51.0 102 50 53.6 107 5 70-130/20
75-69-4 Trichlorofluoromethane ND 50 57.4 115 50 67.2 134 16 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 44.7 89 50 46.1 92 3 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 50 46.0 92 50 48.7 97 6 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 50 48.5 97 50 51.0 102 5 70-130/20
75-01-4 Vinyl Chloride ND 50 46.8 94 50 54.8 110 16 60-140/20
m,p-Xylene ND 100 97.3 97 100 103 103 6 70-130/20
95-47-6 o-Xylene ND 50 46.9 94 50 50.6 101 8 70-130/20
1330-20-7 Xylene (total)ND 150 144 96 150 153 102 6 70-130/20
CAS No.Surrogate Recoveries MS MSD FA82331-8 Limits
1868-53-7 Dibromofluoromethane 102%103%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%101%102%70-130%
2037-26-5 Toluene-D8 99%101%100%70-130%
460-00-4 4-Bromofluorobenzene 99%95%100%70-130%
* = Outside of Control Limits.
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FA8224755.3.3