RA-1098_7093_CA_RPTS_20211209_MRP

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

December 9, 2021

Mr. Jared Edwards
North Carolina Department of
Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Re: Ground Water Monitoring Report
November 2021
U-Filler Up #26
101 Smith Church Road
Roanoke Rapids, Halifax County
North Carolina
Facility ID Number: 0-010657
Incident Number: 7093
GRI Project Number: 2964

Dear Mr. Edwards,

Please find enclosed the referenced report, for the above mentioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Boyd Tolman; Stallings Oil Company, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Ground Water Monitoring Report
November 2021
U-Filler Up #26
101 Smith Church Road
Roanoke Rapids, Halifax County
North Carolina
Facility ID Number: 0-010657
Incident Number: 7093
GRI Project Number: 2964

Prepared for:

Mr. Boyd Tolman
Stallings Oil Company
300 South Wesleyan Boulevard
Rocky Mount, North Carolina 27804

December 9, 2021

William Regenthal, P. G.
Project Manager
Lisa Weathersby
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964
i
SITE INFORMATION
1. Site Identification
 U-Filler Up #26 (Facility ID 0-010657)
 Incident Number 7093 – Intermediate Risk (I170D)
 Location of Source Area: 101 Smith Church Road
Roanoke Rapids, NC 27870
Halifax County
36.4366577°N, 77.6458614°W (Topographical Map)

2. Information about Contacts Associated with the Leaking UST System
UST Owner
Stallings Oil Company
300 South Wesleyan Boulevard
Rocky Mount, NC 27804
[e-mail]
252-937-6184

UST Operator
Stallings Oil Company
300 South Wesleyan Boulevard
Rocky Mount, NC 27804
[e-mail]
252-937-6184

Property Owner
D.H. Roanoke, LLC c/o Walgreens
Post Office Box 1159
Deerfield, IL 60015
Email Unknown
Phone No. Unknown

Property Occupant
Walgreens
101 Smith Church Road
Roanoke Rapids, NC 27870
Email Unknown
252-535-4037
Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
SGS North America, Inc.
4405 Vineland Road, Suite C-15
Orlando, FL 32811
State Certification No. 573
615-758-5858
3. Information about Release
 Release was discovered on October 1991
 An unknown amount of product was released from the leaking UST System
 Three 12,000-gallon gasoline USTs were removed from the site in 1991

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964

ii
EXECUTIVE SUMMARY
The former U-Filler Up #26 site is located at 101 Smith Church Road in Roanoke Rapids, Halifax County,
North Carolina. The site is currently owned by D. H. Roanoke, LLC and is operated by Walgreens as a
drugstore. The site formerly operated as a petroleum retail facility. Three 12,000-gasoline USTs were
removed from the site in October 1991. The adjoining properties are a mixture of single family residential
and commercial properties.

A CSA was completed in 2003. A CAP proposing air sparge and soil-vapor extraction was developed for
this incident in 2003 but has not been fully implemented.

On November 16, 2021, six Type II monitoring wells were gauged, purged and sampled. No free product
was observed in the monitoring wells prior to sampling. Concentrations of individual BTEX constituents,
MTBE, naphthalene, methyl chloride, isopropylbenzene, methylene chloride, n-propylbenzene, 1,2,4-
trimethylbeneze and/or 1,3,5- trimethylbeneze that were above the MACs were reported in the ground
water samples collected from MW-1, MW-4, MW-5, MW-9, MW-12 and MW-13. Concentrations of
benzene reported in the ground water sample collected from MW-1 was above the GCL.

Contaminant mass as the site has decreased by 40.4% since May 2018.

Based on this information, the site incident can close once contaminant concentrations have been
reduced to less than the GCL for benzene. The CAP that was developed in 2003 could be implemented at
the site, however, a series of AFVR and/or MMPE events could be conducted at the site in order to reduce
contaminant mass in core monitoring wells MW-1, MW-4 and MW-5. Since the site is an active Walgreens,
soil excavation or the installation of additional wells is not practical and may not be allowed by the
property owner. A feasibility study discussing the implementation of the 2003 CAP and/or ground water
extraction events could be developed.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964

iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964

iv
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION ...................................................................................................2
3.0 FREE PRODUCT REMOVAL ........................................................................................................4
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS ..................................4
5.0 CONCLUSIONS .........................................................................................................................4
6.0 LIMITATIONS ...........................................................................................................................5
7.0 STATEMENTS AND CERTIFICATION ...........................................................................................5

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Ground Water Quality Map
Figure 6: Estimated Contaminant Mass Area Map

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Well Construction and Gauging Information
Table 4: Summary of Ground Water Sample Analytical Results
Table 5: Free Product Recovery Event Information

APPENDICES
Appendix A: State Correspondence
Appendix B: Laboratory Report – Ground Water Samples
Appendix C: Contaminant Mass Reduction Calculations

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the November 2021 ground water sampling event at the U-Filler Up #26 site;
located at 101 Smith Church Road in Roanoke Rapids, Halifax County, North Carolina (Figure 1). These
activities were conducted in accordance with GRI Proposal No. 21-663, which was submitted to NCDEQ
on October 28, 2021, and was approved as Task Authorization No. 7093-20 on October 29, 2021. NCDEQ
correspondence associated with the incident is included as Appendix A.

The site is currently owned by D. H. Roanoke, LLC and is operated by Walgreens as a drugstore. The site
formerly operated as U-Filler Up #26, a petroleum retail facility. According to available information, three
12,000-gallon gasoline USTs were removed from the site in October 1991 by Applied Environmental
Services, Inc. (AES). UST owner/operator information and UST system information are included as Tables
1 and 2, respectively. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of single family residential and commercial properties. The
site contains one building and is primarily capped with concrete and landscaping. The overall topography
at the site is relatively flat. Fifteen Type II and one Type III monitoring wells were installed at the site
during previous ground water assessment and corrective action activities. The Type III monitoring well
(MW-7) was abandoned in July 2019. A Site Vicinity Map showing the location of the site and surrounding
property boundaries is included as Figure 2. A Site Map showing the locations of the monitoring wells
and the structures on-site has been included as Figure 3.

According to the November 12, 1991, Tank Closure Assessment completed by AES, contaminated soil
encountered during UST closure activities was removed from the site and transported to a permitted
disposal facility. Excavation activities ceased when ground water was encountered in the excavation basin
at a depth of approximately 11.5 feet bgs.

A CSA was completed in 2003. A CAP proposing an air sparge and soil-vapor extraction remediation
system was developed in 2003, however it has not been fully implemented.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964
2

An AFVR event was conducted in February 2003 and a Free Product Evaluation/Recovery Event was
conducted in August 2009. These activities were conducted by AES and others. Between January 2015
and October 2017, GRI supervised three AFVR events to remove free product from the site.
2.0 PRESENTATION OF CURRENT SITE ASSESSMENT INFORMATION/ COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
On November 16, 2021, six Type II monitoring wells (MW-1, MW-4, MW-5, MW-9, MW-12 and MW-13)
were gauged, purged and sampled in accordance with the NCDEQ guidelines. Depths to ground water in
the Type II monitoring wells ranged from 9.58 feet to 11.98 feet below the tops of well casings. Ground
water elevations relative to a datum assumed by a previous consultant ranged from 131.09 to 132.64 feet.
Ground water flow was generally to the south-southeast with a horizontal hydraulic gradient of
approximately 0.03 feet per foot. Well construction and gauging information is presented in Table 3. A
water table surface map is included as Figure 4. A summary of the current ground water gauging data is
shown below:

Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 6-21 21 144.57 11.98 --- 132.59
MW-4 6-21 21 142.22 9.58 --- 132.64
MW-5 9-24 24 141.28 10.19 --- 131.09
MW-9 14-24 24 141.93 10.23 --- 131.70
MW-12 5-25 25 142.30 10.21 --- 132.09
MW-13 5-25 25 142.76 11.54 --- 131.22

Ground water samples collected from the monitoring wells were submitted for laboratory analyses using
EPA Method 6200B. Concentrations of individual BTEX constituents, MTBE, naphthalene, methyl chloride,
isopropylbenzene, methylene chloride, n-propylbenzene, 1,2,4-trimethylbeneze and/or 1,3,5-
trimethylbeneze that exceeded the MACs were reported in the ground water samples collected from MW-
1, MW-4, MW-5, MW-9, MW-12 and MW-13. Concentrations of benzene reported in the ground water
sample collected from MW-1 was above the GCL. A summary of the analytical results for ground water
samples collected on November 16, 2021, is presented in Table 4. A Ground Water Quality Map based on
the November 2021 data is included as Figure 5. A complete report of laboratory analyses of the ground
water samples collected from the monitoring wells during the November 2021 sampling event has been
included as Appendix B. A summary of the current ground water analytical data is shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964
3
Contaminant
of Concern  Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (mg/l) 1 600 600 500 20 6
GCL (mg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-1 7,350 3,540 4,050 12,700 753 563
MW-4 4,860 12,500 3,930 14,300 175 354
MW-5 4,770 15,900 1,650 8,230 216 J 158 J
MW-9 2.5 J 16.9 627 768 <2.5 160
MW-12 54.5 5.1 30.8 8.0 0.99 J 3.7
MW-13 2.3 2.6 0.85 8.6 <0.13 2.3

The baseline contaminant mass at the site was determined based on the total BTEX, MTBE and
naphthalene concentrations from the May 2018 ground water sampling event, as well as the maximum
historical water column height observed. The contaminant plume is based on a benzene isoconcentration
contour of 1 µg/L derived from the May 2018 ground water sampling event. The data indicates the
contaminant mass has been decreased by 40.4% since May 2018. Please note that the contaminant mass
cannot be calculated in wells containing free product; therefore, contaminant mass reduction calculations
began with the May 2018 sampling event. Contaminant mass calculations have been included as
Appendix C. A map of the contaminant mass area has been included as Figure 6. A chart depicting the
overall trend in contaminant mass is shown below:

The site is located along the eastern boundary of the Piedmont Physiographic Province of North Carolina.
The water table has a seasonal high depth to water of approximately 7 to 13 feet bgs. Since the CAP has
not been fully implemented for this site, cleanup milestones have not been established.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964
4
3.0 FREE PRODUCT REMOVAL
Free product has historically been observed at this site. GRI has supervised three AFVR events since
January 2015. These AFVR events have been conducted to remove free product. As of this report, a total
of 0.47 gallons of vapor phase product have been recovered. Free product has not been detected at the
site since the November 2017 sampling event. Past free product recovery events are summarized Table
5.
4.0 NATURAL ATTENUATION / NATURAL SOURCE ZONE DEPLETION STATUS
No natural attenuation monitoring plan is currently in place at the site. Contaminant mass at the site
continues to slowly decline since the last time free product was observed at the site (May 2018).
Additional AFVR and/or MMPE events could be conducted at the site to remove contaminant mass,
however, site restrictions may be prohibitive of conducting these activities. If contaminant concentrations
can be reduced to less than the GCLs, then the site risk classification can be re-evaluated.

Because the site is an active Walgreens, remediation activities will be restricted based on the site use. It
is not likely that the property owner will allow excavation in the vicinity of MW-1, nor would they be likely
to allow for the installation of additional monitoring wells in the parking lot of the drugstore. These factors
should be considered with assessing the feasibility of implementing the proposed 2003 CAP. Additional
ground water extraction events, via either AFVR or MMPE may be allowed.
5.0 CONCLUSIONS
 On November 16, 2021, six Type II monitoring wells (MW-1, MW-4, MW-5, MW-9, MW-12 and
MW-13) were gauged, purged and sampled. Ground water flow was generally to the south/
southeast with a horizontal hydraulic gradient of approximately 0.03 feet per foot.
 Concentrations of individual BTEX constituents, MTBE, naphthalene, methyl chloride,
isopropylbenzene, methylene chloride, n-propylbenzene, 1,2,4-trimethylbeneze and/or 1,3,5-
trimethylbeneze were above the MACs reported in the ground water samples collected from MW-
1, MW-4, MW-5, MW-12 and/or MW-13. Concentrations of benzene reported in the ground
water sample collected from MW-1 was above the GCL.
 Contaminant mass at the site has decreased by 40.4% since May 2018. Contaminant mass at the
site continues to slowly decline since the last time free product was observed at the site (May
2018).
 Based on this information, the site incident can close once contaminant concentrations have been
reduced to less than the GCL for benzene. The CAP that was developed in 2003 could be
implemented at the site, however, a series of AFVR and/or MMPE events could be conducted at
the site in order to reduce contaminant mass in core monitoring wells MW-1, MW-4 and MW-5.
Since the site is an active Walgreens, soil excavation or the installation of additional wells is not
practical and may not be allowed by the property owner. A feasibility study discussing the
implementation of the 2003 CAP and/or ground water extraction events could be developed.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Ground Water Monitoring Report
Prepared on: December 9, 2021 U-Filler Up #26
Project Manager: William Regenthal, P. G. GRI Project No. 2964
5
6.0 LIMITATIONS
This report has been prepared for the exclusive use of Stallings Oil Company and NCDEQ for specific
application to the referenced site in Halifax County, North Carolina. The assessment was conducted based
on the scope of work and level of effort desired by NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
7.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. N/A Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO
IF the answer to either question #4 or #5 is “YES”, generally describe in this cell any actions
recommended to further assess or clean up this known or suspected source. (This should be described
in more detail in the report text above.)

FIGURES
SITEE Littleton Rd
Julian R Allsbrook Hwy
Vine St
Drake St
E 10th StSmith Church RdBuffaloe StSouth StPrice StMitchell StOld Farm RdCardinal DrPatsy Albritton StStancell StNorth StMurphrey StBoykins StYork StThanos Dr
Wood St
Old Farm Rd SSummitt AveDuke StDevonshire CirGeorgia AveBecker Dr
Leslie St
Horizon Ave Lowes Dr
Office Park DrGregory Dr CHOCKOYOTTE CREEK³
FIGURE 2: SITE VICINITY MAPU-FILLER UP #26101 SMITH CHURCH ROADROANOKE RAPIDS, HALIFAX COUNTYNORTH CAROLINAINCIDENT NO. 7093
PREPARED BY:GEOLOGICAL RESOURCES, INC.FEBRUARY 28, 2014
0 300150Feet1 inch = 300 feet
500-FOOT RADIUS
LEGEND
ncrivers
roads_01212013
parcels

TABLES
UST ID Number 1, 2, 3 Facility ID Number
Owner or Operator?
Owner
Name of Owner or Operator Dates of Ownership / Operation
TABLE 1
UST OWNER/OPERATOR INFORMATION
U-FILLER UP #26 (INCIDENT NO. 7093)
0-010657
Stallings Oil Company 06/03/1976 - 10/30/1991
Address Telephone Number
300 S Weslevan Boulevard Suite 200, Rocky Mount, NC 27803 252-937-6184
Page 1 of 1
Date: 11/27/17
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline Gasoline 12,000 6/3/1976 Single Wall Steel 8' x 32'Single Wall
Steel
Removed
(10/30/1991)Unknown
2 Gasoline Gasoline 12,000 6/3/1976 Single Wall Steel 8' x 32'Single Wall
Steel
Removed
(10/30/1991)Unknown
3 Gasoline Gasoline 12,000 6/3/1976 Single Wall Steel 8' x 32'Single Wall
Steel
Removed
(10/30/1991)Unknown
Tank
Dimensions
(diameter x length)
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
U-FILLER UP #26 (INCIDENT NO. 7093)
Facility ID #: 0-010657
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Date: 11/17/2021
01/23/2012 12.88 ---131.69
06/27/2012 12.23 ---132.34
01/02/2013 12.17 ---132.40
01/15/2015 10.91 ---133.66 Before AFVR
02/23/2015 10.52 ---134.05
03/16/2016 9.33 ---135.24 Before AFVR
03/16/2016 9.51 ---135.06 After AFVR
04/18/2016 9.53 ---135.04
10/12/2016 10.13 ---134.44
04/03/2017 11.95 ---132.62
11/14/2017 13.03 0.06 131.59
05/31/2018 11.52 ---133.05
12/27/2018 10.51 ---134.06
07/09/2019 10.82 ---133.75
01/16/2020 11.82 ---132.75
08/20/2020 11.30 ---133.27
05/18/2021 9.05 ---135.52
11/16/2021 11.98 ---132.59
01/23/2012 13.44 ---134.12
06/27/2012 12.74 ---134.82
01/02/2013 12.71 ---134.85
02/23/2015 10.99 ---136.57
05/31/2018 12.16 ---135.40
12/27/2018 NM ---NM
07/09/2019 NM ---NM
MW-3 08/19/02 01/23/2012 9 9-24 24 146.03 NM NM NM DESTROYED
01/23/2012 10.41 0.02 131.83
06/27/2012 9.89 ---132.33
01/02/2013 9.73 ---132.49
01/15/2015 8.44 ---133.78 Before AFVR
02/23/2015 8.13 ---134.09
03/16/2016 7.56 ---134.66 Before AFVR
03/16/2016 8.48 ---133.74 After AFVR
04/18/2016 7.31 ---134.91
10/12/2016 7.68 ---134.54
04/03/2017 9.48 ---132.74
10/10/2017 10.19 ---132.03 Before AFVR
10/10/2017 10.63 ---131.59 After AFVR
11/14/2017 10.55 ---131.67
05/31/2018 9.03 ---133.19
12/27/2018 7.98 ---134.24
07/09/2019 8.24 ---133.98
01/16/2020 9.29 ---132.93
08/20/2020 8.96 ---133.26
05/18/2021 6.76 ---135.46
11/16/2021 9.58 ---132.64
01/23/2012 11.07 ---130.21
06/27/2012 10.47 ---130.81
01/02/2013 10.40 ---130.88
01/15/2015 9.11 ---132.17 Before AFVR
02/23/2015 9.75 ---131.53
04/18/2016 7.80 ---133.48
10/12/2016 8.34 ---132.94
04/03/2017 10.03 ---131.25
10/10/2017 10.80 ---130.48 Before AFVR
10/10/2017 11.14 ---130.14 After AFVR
11/14/2017 11.20 ---130.08
05/31/2018 9.70 ---131.58
12/27/2018 8.32 ---132.96
07/09/2019 8.92 ---132.36
01/16/2020 9.95 ---131.33
08/20/2020 9.51 ---131.77
05/18/2021 7.27 ---134.01
11/16/2021 10.19 ---131.09
MW-6 08/20/02 01/23/2012 9 9-24 24 142.85 NM NM NM DESTROYED
08/15/02MW-1
142.22216-21608/20/02MW-4
144.57216-216
MW-2 08/19/02
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
U-FILLER UP #26 (INCIDENT NO. 7093)
Well ID Date Installed
(mm/dd/yy)
Date Water
Level Measured
(mm/dd/yyyy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval (x
to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of Casing
(feet)
Ground
Water
Elevation
(ft.)
CommentsFree Product
Thickness** (ft.)
Facility ID #: 0-010657
9-24908/20/02MW-5 141.2824
9 9-24 24 147.56
Page 1 of 3
Date: 11/17/2021
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
U-FILLER UP #26 (INCIDENT NO. 7093)
Well ID Date Installed
(mm/dd/yy)
Date Water
Level Measured
(mm/dd/yyyy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval (x
to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of Casing
(feet)
Ground
Water
Elevation
(ft.)
CommentsFree Product
Thickness** (ft.)
Facility ID #: 0-010657
01/23/2012 12.55 ---133.02
06/27/2012 11.95 ---132.14
01/02/2013 11.87 ---132.22
02/23/2015 10.22 ---133.87
04/18/2016 8.88 ---135.21
10/12/2016 9.79 ---134.30
04/03/2017 11.62 ---132.47
05/31/2018 1.21 ---142.88
12/27/2018 9.33 ---134.76
07/09/2019 10.14 ---133.95 Abandoned
01/23/2012 10.34 ---130.66
06/27/2012 9.91 ---131.09
01/02/2013 9.68 ---131.32
02/23/2015 9.28 ---131.72
04/18/2016 7.55 ---133.45
10/12/2016 7.67 ---133.33
04/03/2017 9.40 ---131.60
12/27/2018 8.12 ---132.88
07/09/2019 8.69 ---132.31
01/16/2020 9.30 ---131.70
01/23/2012 11.14 ---130.79
06/27/2012 10.98 ---130.95
01/02/2013 10.33 ---131.60
02/23/2015 8.95 ---132.98
04/18/2016 8.00 ---133.93
10/12/2016 8.89 ---133.04
04/03/2017 12.39 ---129.54
11/14/2017 11.27 ---130.66
05/31/2018 10.10 ---131.83
12/27/2018 8.84 ---133.09
07/09/2019 9.00 ---132.93
01/16/2020 10.25 ---131.68
08/20/2020 9.67 ---132.26
11/16/2021 10.23 ---131.70
01/23/2012 12.46 ---130.64
06/27/2012 11.95 ---131.15
01/02/2013 11.70 ---131.40
02/23/2015 10.31 ---132.79
05/31/2018 10.90 ---132.20
12/27/2018 10.12 ---132.98
07/09/2019 10.70 ---132.40
01/16/2020 11.20 ---131.90
MW-11 12/08/02 01/23/2012 10 10-25 25 140.84 NM NM NM NOT FOUND
02/23/2015 9.90 ---132.40
04/18/2016 9.19 ---133.11
10/12/2016 8.41 ---133.89
04/03/2017 11.12 ---131.18
11/14/2017 12.16 ---130.14
05/31/2018 10.79 ---131.51
12/27/2018 8.71 ---133.59
07/09/2019 10.09 ---132.21
01/16/2020 10.82 ---131.48
08/20/2020 10.76 ---131.54
05/18/2021 8.86 ---133.44
11/16/2021 10.21 ---132.09
02/23/2015 10.31 ---132.45
04/18/2016 9.45 ---133.31
10/12/2016 10.05 ---132.71
04/03/2017 11.59 ---131.17
11/14/2017 12.54 ---130.22
05/31/2018 11.37 ---131.39
12/27/2018 10.19 ---132.57
07/09/2019 10.41 ---132.35
01/16/2020 11.42 ---131.34
08/20/2020 11.06 ---131.70
05/18/2021 8.98 ---133.78
11/16/2021 11.54 ---131.22
02/23/2015 10.42 ---133.70
05/31/2018 11.62 ---132.50
12/27/2018 10.27 ---133.85
07/09/2019 10.33 ---133.79
01/16/2020 11.81 ---132.31
MW-7 08/19/02 35 35-40 40 144.09
MW-8
144.12
24 143.10
141.9324
142.3025
142.7625
2504/01/14MW-14 5 5-25
5-25504/01/14MW-12
5-25504/01/14MW-13
MW-10 14 14-2411/01/02
14-241411/01/02MW-9
11/14/02 14 14-24 24 141.00
Page 2 of 3
Date: 11/17/2021
TABLE 3
WELL CONSTRUCTION AND GAUGING INFORMATION
U-FILLER UP #26 (INCIDENT NO. 7093)
Well ID Date Installed
(mm/dd/yy)
Date Water
Level Measured
(mm/dd/yyyy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval (x
to y ft. BGS)
Bottom
of Well
(ft. BGS)
Top of Casing
Elevation*
(ft.)
Depth to
Water from
Top of Casing
(feet)
Ground
Water
Elevation
(ft.)
CommentsFree Product
Thickness** (ft.)
Facility ID #: 0-010657
02/23/2015 10.67 ---133.23
05/31/2018 11.86 ---132.04
12/27/2018 10.54 ---133.36
07/09/2019 10.67 ---133.23
01/16/2020 11.96 ---131.94
02/23/2015 10.48 ---133.86
04/18/2016 9.53 ---134.81
10/12/2016 10.31 ---134.03
04/03/2017 11.86 ---132.48
05/31/2018 11.65 ---132.69
12/27/2018 10.27 ---134.07
07/09/2019 10.14 ---134.20
01/16/2020 11.79 ---132.55
Notes:
• ** : If free product is present in a well, ground water elevation calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581].
• NM: Not measured.
dated September 10, 2009; prepared by Marshall Miller & Associates, Inc., and well constructions (where available).
• Top of casing elevations and well construction information for wells MW-1 through MW-11 obtained from report titled 'Free Product Recovery Report',
• * : Reference point for elevation measurements.
• ft BGS : feet below ground surface.
MW-16 5-25 25 144.3404/01/14 5
143.90MW-15 5 5-25 2504/01/14
Page 3 of 3
Well ID
Date
Collected
(mm/dd/yyyy)
1 600 600 500 20 6 70 70 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 70,000 26,100 28,500 24,100
01/23/2012 7,140 11,300 2,980 13,420 489 573 30.7 J <26 472 126 J <27 380 2,470 639
06/27/2012 7,180 11,600 3,610 14,290 287 548 26.5 J <20 <20 117 24.5 J 388 2,620 621
01/02/2013 6,360 11,000 2,800 12,300 546 473 <25 <25 <25 78.2 J 27.0 J 304 2,170 476
02/23/2015 429 3,180 1,680 8,460 <16 434 98.2 58.0 <15 157 <16 540 3,290 1,020
04/18/2016 144 51.4 36.7 136 49.4 27 43.0 21.5 <1.3 20.6 3.4 J 91.5 1,120 223
10/12/2016 4,190 4,750 1,090 4,920 1,040 227 57.2 J 34.6 J <25 68.6 J 37.4 J 249 1,520 516
04/03/2017 6,160 7,740 1,700 7,390 682 347 34.5 J 19.4 J <13 58.1 35.2 J 209 1,540 446
11/14/2017 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
05/31/2018 4,790 4,670 3,300 12,500 165 1,080 176 83 <6.3 209 26.7 667 3,320 1,170
12/27/2018 4,540 3,390 2,750 10,800 460 471 32.4 J 20.9 J <13 104 29.4 J 322 2,120 556
07/09/2019 7,440 4,990 3,270 11,700 1,150 523 38.9 J 26.0 J <25 109 51.1 J 341 2,380 649
01/16/2020 6,610 2,970 2,990 9,300 557 467 32.0 J <25 <25 102 38.7 J 308 1,810 497
08/20/2020 6,210 3,410 3,570 14,300 1,030 686 NR NR NR NR 49.7 J NR NR NR
05/18/2021 6,010 2,140 2,780 7,970 792 416 NR NR NR NR 45.0 J NR NR NR
11/16/2021 7,350 3,540 4,050 12,700 753 563 48.9 J 30.2 J <25 110 41.9 J 399 2,880 744
01/23/2012 <0.13 <0.13 <0.15 <0.30 0.64 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
06/27/2012 <0.13 <0.13 <0.15 <0.30 3.4 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
01/02/2013 <0.10 0.13 J <0.10 <0.22 3.4 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
02/23/2015 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.15 <0.12 <0.16 <0.16 <0.14 <0.14
05/31/2018 <0.13 <0.13 0.42 J 0.88 J <0.13 0.17 J <0.13 <0.13 <0.13 <0.13 <0.13 0.23 J 0.65 0.33 J
01/23/2012 FP FP FP FP FP FP FP FP FP FP FP FP FP FP
06/27/2012 7,920 29,500 3,770 16,130 876 511 <50 <51 <50 134 J <54 449 2,870 731
01/02/2013 6,800 28,400 3,220 15,800 452 454 21.2 J <20 <20 89.1 J <20 332 2,430 533
02/23/2015 7,560 29,800 4,360 21,400 295 J 686 <140 <140 <150 197 J <160 547 3,300 884
04/18/2016 6,160 25,900 8,970 41,100 249 2,270 893 431 <31 947 <31 3,800 18,000 5,700
10/12/2016 1,290 12,800 4,930 23,300 <63 1,390 588 312 <63 438 <63 2,110 10,400 3,520
04/03/2017 6,160 27,300 3,630 16,800 294 571 <63 <63 <63 95.9 J <63 332 2,200 540
11/14/2017 5,550 12,800 2,750 10,300 353 1,050 <63 <63 <63 102 J <63 284 1,470 401
05/31/2018 3,540 21,300 8,000 37,900 121 J 2,170 1,000 419 <63 897 <63 3,390 18,300 5,970
12/27/2018 4,710 19,500 3,620 16,900 <63 476 <63 <63 <63 130 J <63 401 2,570 666
07/09/2019 5,520 15,500 3,710 14,100 <63 396 <63 <63 <63 126 J <63 405 2,520 724
01/16/2020 4,430 19,700 3,990 17,400 69.4 J 499 <63 <63 <63 135 J <63 404 2,700 747
08/20/2020 4,190 16,500 3,660 17,100 93.5 J 484 NR NR NR NR <63 NR NR NR
05/18/2021 4,100 8,810 2,870 11,700 <25 384 NR NR NR NR <25 NR NR NR
11/16/2021 4,860 12,500 3,930 14,300 175 354 <25 <25 <25 91.8 J <25 326 2,180 534
01/23/2012 3,650 6,500 1,150 6,780 751 269 <20 <20 <20 52.4 J 24.4 J 155 1,580 475
06/27/2012 4,380 11,900 2,240 9,760 377 316 24.2 J <20 <20 89.4 J <21 299 2,130 517
01/02/2013 3,560 9,980 1,850 8,760 437 296 <20 <20 <20 66.1 J <20 258 1,890 430
02/23/2015 6,570 19,400 2,010 10,800 865 325 <72 <69 <73 87.1 J <80 240 J 1,670 476
04/18/2016 2,870 11,700 1,770 9,370 326 447 72.5 J 41.5 J <31 108 J <31 379 2,630 781
10/12/2016 369 1,620 170 1,210 18.8 J 42.7 <6.3 <6.3 <6.3 <6.3 <6.3 17.2 J 189 66.6
04/03/2017 2,900 7,310 772 5,230 255 179 <13 <13 <13 24.4 J 15.4 J 79.5 936 274
11/14/2017 2,290 2,710 637 2,340 334 156 24.8 J 13.4 J <13 36.3 J <13 112 603 198
05/31/2018 4,910 16,400 1,840 13,900 388 565 23.5 J 18.2 J <13 82.2 23.0 J 208 2,590 864
12/27/2018 6,140 24,800 2,230 12,700 444 271 <63 <63 <63 70.1 J <63 173 J 1,490 416
07/09/2019 6,380 26,000 2,210 9,840 4.63 J 247 J <130 <130 <130 <130 <130 161 J 1,140 389 J
01/16/2020 4,200 15,100 1,320 7,520 286 142 J <63 <63 <63 <63 <63 82.6 J 753 284
08/20/2020 6,610 32,900 2,430 14,200 318 337 NR NR NR NR <63 NR NR NR
05/18/2021 9,120 38,000 3,270 18,400 471 J 407 J NR NR NR NR <130 NR NR NR
11/16/2021 4,770 15,900 1,650 8,230 216 J 158 J <63 <63 <63 <63 <63 147 J 737 247 J
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
U-FILLER UP #26 (INCIDENT NO. 7093)
Analytical Method →EPA Method 6200B
Date: 12/01/2021 Facility ID # : 0-010657
1,3,5-TrimethylbenzeneMAC (µg/l)
GCL (µg/l)IsopropylbenzeneIPENaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneContaminant of Concern →BenzeneTolueneEthylbenzeneXylenesMTBEMW-2 n-Propylbenzene1,2,4-TrimethylbenzeneMW-1
MW-5
MW-4
Page 1 of 4
Well ID
Date
Collected
(mm/dd/yyyy)
1 600 600 500 20 6 70 70 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 70,000 26,100 28,500 24,100
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
U-FILLER UP #26 (INCIDENT NO. 7093)
Analytical Method →EPA Method 6200B
Date: 12/01/2021 Facility ID # : 0-010657
1,3,5-TrimethylbenzeneMAC (µg/l)
GCL (µg/l)IsopropylbenzeneIPENaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneContaminant of Concern →BenzeneTolueneEthylbenzeneXylenesMTBEn-Propylbenzene1,2,4-Trimethylbenzene01/23/2012 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
06/27/2012 <0.13 1.4 <0.15 0.65 J <0.13 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
01/02/2013 0.31 J 1.9 0.43 J 2.3 <0.10 0.16 J <0.10 <0.10 <0.10 <0.10 <0.10 0.12 J 0.60 0.21 J
02/23/2015 <0.17 0.26 J <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.15 <0.12 <0.16 <0.16 <0.14 <0.14
04/18/2016 <0.13 3.5 <0.13 <0.31 <0.13 0.17 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
10/12/2016 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
04/03/2017 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/31/2018 <0.13 0.52 0.15 J 0.54 J <0.13 0.27 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 0.47 J 0.16 J
12/27/2018 <0.13 0.17 J <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/23/2012 <0.13 <0.13 <0.15 <0.30 0.94 <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
06/27/2012 <0.13 <0.13 <0.15 <0.30 0.25 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
01/02/2013 0.33 J <0.10 <0.10 1.2 J 0.13 J 0.81 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
02/23/2015 <0.17 <0.17 <0.15 <0.43 2.0 <0.12 <0.14 <0.14 <0.15 <0.12 <0.16 <0.16 <0.14 <0.14
04/18/2016 <0.13 0.16 J <0.13 <0.31 1.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
10/12/2016 <0.13 <0.13 <0.13 <0.31 1.2 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
04/03/2017 <0.13 <0.13 <0.13 <0.25 3.4 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
12/27/2018 <0.13 <0.13 <0.13 <0.25 0.71 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
07/09/2019 <0.13 <0.13 <0.13 <0.25 0.79 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/16/2020 <0.13 <0.13 <0.13 <0.25 1.6 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/23/2012 416 92.0 1,050 4,832.8 J <3.3 305 10.2 J 7.7 J <2.5 68.0 <2.7 136 1,130 297
06/27/2012 261 24.9 517 1,913 J <2.6 124 4.6 J 3.6 J <2.0 28.4 <2.1 60.6 549 132
01/02/2013 214 66.9 713 3470 4.7 J 232 7.2 J 6.9 J <2.0 52.2 <2.0 110 825 198
02/23/2015 138 43.9 725 2,100 <4.1 184 6.0 J 5.6 J <3.6 43.8 <4.0 104 721 149
04/18/2016 104 516 1,630 4,350 <6.3 398 13.6 J 10.6 J <6.3 83.6 <6.3 247 1,660 334
10/12/2016 13.5 94.1 589 1,070 <2.5 190 5.8 J 5.5 J <2.5 35.6 <2.5 99.6 639 54.8
04/03/2017 36.4 567 1,530 3,360 <6.3 358 10.1 J 9.9 J <6.3 63.3 <6.3 201 1,460 156
11/14/2017 4.5 J 15.9 596 634 <2.5 196 8.0 J 6.8 J <2.5 47.7 <2.5 115 356 10.7
05/31/2018 9.2 15.8 178 273 <0.63 64.5 2.4 J 2.0 J <0.63 14.1 <0.63 31.7 194 17.2
12/27/2018 24.1 116 976 1,900 <3.1 263 7.3 J 6.9 J <3.1 51 <3.1 136 995 86.7
07/09/2019 6.2 J 10.8 473 492 <2.5 121 6.9 J 6.6 J <2.5 33.2 <2.5 88.1 630 5.6 J
01/16/2020 8.3 J 31.6 511 937 <2.5 152 5.0 J 5.6 J <2.5 32.5 <2.5 83.3 635 46.2
08/20/2020 4.1 J 12.8 525 611 <1.3 188 NR NR NR NR <1.3 NR NR NR
11/16/2021 2.5 J 16.9 627 768 <2.5 160 8.6 J 8.4 J <2.5 38.2 <2.5 134 964 7.0 J
01/23/2012 <0.13 <0.13 <0.15 <0.30 0.16 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
06/27/2012 <0.13 <0.13 <0.15 <0.30 0.23 J <0.10 <0.10 <0.10 <0.10 <0.10 <0.11 <0.11 <0.10 <0.10
01/02/2013 <0.10 <0.10 <0.10 <0.22 0.23 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10
02/23/2015 <0.17 <0.17 <0.15 0.76 J 0.25 J <0.12 <0.14 <0.14 <0.15 <0.12 <0.16 <0.16 <0.14 <0.14
05/31/2018 <0.13 <0.13 <0.13 <0.25 0.19 J <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
12/27/2018 <0.13 0.16 J 0.18 J 0.68 J <0.13 0.53 0.20 J <0.13 <0.13 <0.13 <0.13 0.22 J 1.5 0.5
07/09/2019 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/16/2020 0.24 J <0.13 <0.13 2.1 0.20 J 3.1 <0.13 <0.13 <0.13 0.44 J <0.13 <0.13 0.14 J <0.13
MW-7
MW-8
MW-9
MW-10
Page 2 of 4
Well ID
Date
Collected
(mm/dd/yyyy)
1 600 600 500 20 6 70 70 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 70,000 26,100 28,500 24,100
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
U-FILLER UP #26 (INCIDENT NO. 7093)
Analytical Method →EPA Method 6200B
Date: 12/01/2021 Facility ID # : 0-010657
1,3,5-TrimethylbenzeneMAC (µg/l)
GCL (µg/l)IsopropylbenzeneIPENaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneContaminant of Concern →BenzeneTolueneEthylbenzeneXylenesMTBEn-Propylbenzene1,2,4-Trimethylbenzene02/23/2015 786 2,280 924 6,960 17.8 J 182 28.9 J 21.6 J <15 94.4 <16 301 2,480 741
04/18/2016 4,420 2,250 1,900 4,975 175 390 23.5 J 13.7 J <6.3 81.7 15.7 J 250 1,100 301
10/12/2016 359 1,540 1,080 3,660 <6.3 294 58.2 34.1 <6.3 92.4 <6.3 366 1,370 464
04/03/2017 5,340 2,370 2,460 5,140 155 554 30.3 J 17.0 J <13 80 15.5 J 297 1,270 336
11/14/2017 3,940 1,320 1,690 3,690 111 397 19.0 J 13.6 J <13 79.9 <13 221 681 173
05/31/2018 4,260 2,240 4,040 11,000 174 1,080 378 165 <13 407 14.8 J 1,400 2,580 1,890
12/27/2018 45.1 18 23.4 19 1.7 3 <0.13 <0.13 <0.13 0.73 0.18 J 2.2 1.90 0.5
07/09/2019 3,480 1,140 1,990 4,960 <13 306 21.1 J 16.5 J <13 66.1 <13 237 1,200 353
01/16/2020 3,460 1,250 1,800 4,330 57.6 372 38.2 J 25.6 J <13 88.5 <13 273 1,610 541
08/20/2020 3,800 1,350 1,970 3,640 61.7 379 NR NR NR NR <13 NR NR NR
05/18/2021 1,660 201 790 1,280 <6.3 156 NR NR NR NR <6.3 NR NR NR
11/16/2021 54.5 5.1 30.8 8.0 0.99 J 3.7 <0.25 <0.25 <0.25 0.67 J <0.25 2.8 0.38 J <0.25
02/23/2015 88.6 18.0 76.1 202 1.3 37.5 2.1 4.3 0.38 J 35.2 0.19 J 17.5 155 0.96
04/18/2016 26.8 6.1 2.8 57.3 0.60 J 3.6 0.52 J 3.3 0.29 J 22.7 <0.25 1.7 54.2 <0.25
10/12/2016 10.8 7 1.7 162 <0.25 6.2 0.70 J 4.6 0.39 J 28.1 <0.25 1.9 119 1.1
04/03/2017 5.1 1.8 0.67 34.6 <0.13 2 0.20 J 2.7 0.26 J 15.7 <0.13 0.53 32.9 <0.13
11/14/2017 9.5 5.8 1.2 180 0.42 J 9.7 0.64 4.4 0.45 J 28.4 <0.13 1.9 157 1.7
05/31/2018 40.4 135 38.1 101 0.62 16.6 1.2 2.3 0.23 J 16.3 <0.13 8.2 4.4 0.83
12/27/2018 10.4 1.5 5.3 4.1 <0.13 5.2 0.36 J 1.8 0.18 J 13.6 <0.13 1.5 0.21 J <0.13
07/09/2019 9.7 30.2 22.1 233 <0.13 28.3 1.8 4.3 0.40 J 32.2 <0.13 10.3 55.2 9.2
01/16/2020 4.3 2.6 8.6 36.6 <0.13 9.0 0.70 4.0 0.37 J 21.6 <0.13 3.1 8.8 0.17 J
08/20/2020 7.5 17.8 26.1 146 <0.25 20.3 NR NR NR NR <0.25 NR NR NR
05/18/2021 5.0 11.4 33.1 79.1 <0.13 25.0 NR NR NR NR <0.13 NR NR NR
11/16/2021 2.3 2.6 0.85 8.6 <0.13 2.3 0.74 5.0 0.43 J 25.5 <0.13 1.5 <0.13 0.18 J
02/23/2015 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.15 <0.12 <0.16 <0.16 <0.14 <0.14
05/31/2018 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
12/27/2018 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
07/09/2019 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/16/2020 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
02/23/2015 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.15 <0.12 <0.16 <0.16 <0.14 <0.14
05/31/2018 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
12/27/2018 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
07/09/2019 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/16/2020 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
02/23/2015 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.14 <0.14 <0.15 <0.12 <0.16 <0.16 <0.14 <0.14
04/18/2016 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
10/12/2016 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
05/31/2018 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
12/27/2018 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
07/09/2019 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
01/16/2020 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
MW-16
MW-15
MW-14
MW-13
MW-12
Page 3 of 4
Well ID
Date
Collected
(mm/dd/yyyy)
1 600 600 500 20 6 70 70 70 70 70 70 400 400
5,000 260,000 80,000 50,000 20,000 6,000 5,900 8,800 14,750 30,500 70,000 26,100 28,500 24,100
TABLE 4
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
U-FILLER UP #26 (INCIDENT NO. 7093)
Analytical Method →EPA Method 6200B
Date: 12/01/2021 Facility ID # : 0-010657
1,3,5-TrimethylbenzeneMAC (µg/l)
GCL (µg/l)IsopropylbenzeneIPENaphthalenen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneContaminant of Concern →BenzeneTolueneEthylbenzeneXylenesMTBEn-Propylbenzene1,2,4-Trimethylbenzene04/18/2016 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
10/12/2016 <0.13 <0.13 <0.13 <0.31 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
11/14/2017 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
11/16/2021 <0.13 <0.13 <0.13 <0.25 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13
Notes:
• Concentrations of methyl chloride (40.6 J µg/l in MW-1) and methylene chloride (518 J µg/l in MW-5) that exceeded the MACs were reported in the ground water sample collected on
November 16, 2021.
• J: Estimated value.
• For other compounds reported below the MACs, refer to the laboratory reports.
• GCL: Gross contamination level.
• Results reported in µg/l (micrograms per liter)
• MAC: Maximum Allowable Concenration as specified in T15A NCAC 2L.0202.
• NE: Standard not established.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type indicate the MACs were below the reported concentrations; concentrations in italics indicate the GCLs were below the reported concentrations.
TRIP BLANK
Page 4 of 4
MW-1 and
MW-4 01/15/15 AFVR 1,117.81 137.43 346.70 0.19 2,564 0 0.19
MW-4 03/16/16 AFVR 1,146.10 134.95 330.38 0.18 2,250 0 0.18
MW-4 and
MW-5 10/10/17 AFVR 1,150.42 175.26 284.69 0.10 3,220 0 0.10
0.47 8,034.00 0.00 0.47
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
TABLE 5
FREE PRODUCT RECOVERY EVENT INFORMATION
AFVR EVENT
U-FILLER UP #26 (INCIDENT NO. 7093)
Date: 11/27/17 Facility ID #: 0-010657
SUMMARY OF FLUID REMOVAL
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid (gallons)
Total Amount
of Product
Recovered
(gallons)
Totals
Total To Date 8,034.47 0.47
Summary Total Fluids Removed (in gallons)Total Amount of Product Removed (in gallons)
Current Event 3,220.10 0.10

APPENDICES

APPENDIX A
State Correspondence
52223(5

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2964 Received JUN 16 2021
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2964 Received OCT 29 2021

APPENDIX B
Laboratory Report – Ground Water Samples

11/30/21
Technical Report for
GRI (Geological Resources Inc.)
U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
7093/2964
SGS Job Number: FA90889
Sampling Date: 11/16/21
Report to:
GRI
3502 Hayes Rd
Monroe, NC 28110
[e-mail]; [e-mail];
[e-mail]
ATTN: William Regenthal
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AL, AK, AR, CT, IA, KY, MA, MI. MS, ND, NH, NV, OK, OR, UT, VT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Orlando, FL 11/30/21
e-Hardcopy 2.0
Automated Report
39
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 39
FA90889
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................7
3.1: FA90889-1: MW-1 ........................................................................................................8
3.2: FA90889-2: MW-4 ........................................................................................................10
3.3: FA90889-3: MW-5 ........................................................................................................13
3.4: FA90889-4: MW-9 ........................................................................................................15
3.5: FA90889-5: MW-12 ......................................................................................................17
3.6: FA90889-6: MW-13 ......................................................................................................19
3.7: FA90889-7: TRIP BLANK ...........................................................................................21
Section 4: Misc. Forms ............................................................................................................24
4.1: Chain of Custody ...........................................................................................................25
Section 5: MS Volatiles - QC Data Summaries .....................................................................27
5.1: Method Blank Summary ................................................................................................28
5.2: Blank Spike Summary ...................................................................................................32
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................36 123452 of 39
FA90889
SGS North America Inc.
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA90889
U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Project No: 7093/2964
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA90889-1 11/16/21 10:20 ER 11/17/21 AQ Ground Water MW-1
FA90889-2 11/16/21 10:32 ER 11/17/21 AQ Ground Water MW-4
FA90889-3 11/16/21 10:06 ER 11/17/21 AQ Ground Water MW-5
FA90889-4 11/16/21 10:48 ER 11/17/21 AQ Ground Water MW-9
FA90889-5 11/16/21 11:01 ER 11/17/21 AQ Ground Water MW-12
FA90889-6 11/16/21 11:15 ER 11/17/21 AQ Ground Water MW-13
FA90889-7 11/16/21 09:30 ER 11/17/21 AQ Ground Water TRIP BLANK
3 of 39
FA908891
Summary of Hits Page 1 of 3
Job Number:FA90889
Account:GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Collected:11/16/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA90889-1 MW-1
Benzene 7350 100 25 ug/l SM 6200B
n-Butylbenzene 48.9 J 100 25 ug/l SM 6200B
sec-Butylbenzene 30.2 J 100 25 ug/l SM 6200B
Di-Isopropyl Ether 41.9 J 100 25 ug/l SM 6200B
Ethylbenzene 4050 100 25 ug/l SM 6200B
Isopropylbenzene 110 100 25 ug/l SM 6200B
Methyl Chloride 40.6 J 100 40 ug/l SM 6200B
Methyl Tert Butyl Ether 753 100 25 ug/l SM 6200B
Naphthalene 563 100 25 ug/l SM 6200B
n-Propylbenzene 399 100 25 ug/l SM 6200B
Toluene 3540 100 25 ug/l SM 6200B
1,2,4-Trimethylbenzene 2880 100 25 ug/l SM 6200B
1,3,5-Trimethylbenzene 744 100 25 ug/l SM 6200B
m,p-Xylene 10400 200 25 ug/l SM 6200B
o-Xylene 2260 100 25 ug/l SM 6200B
Xylene (total)12700 300 50 ug/l SM 6200B
FA90889-2 MW-4
Benzene 4860 100 25 ug/l SM 6200B
Ethylbenzene 3930 100 25 ug/l SM 6200B
Isopropylbenzene 91.8 J 100 25 ug/l SM 6200B
Methyl Tert Butyl Ether 175 100 25 ug/l SM 6200B
Naphthalene 354 100 25 ug/l SM 6200B
n-Propylbenzene 326 100 25 ug/l SM 6200B
Toluene 12500 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 2180 100 25 ug/l SM 6200B
1,3,5-Trimethylbenzene 534 100 25 ug/l SM 6200B
m,p-Xylene 10900 200 25 ug/l SM 6200B
o-Xylene 3370 100 25 ug/l SM 6200B
Xylene (total)14300 300 50 ug/l SM 6200B
FA90889-3 MW-5
Benzene 4770 250 63 ug/l SM 6200B
Ethylbenzene 1650 250 63 ug/l SM 6200B
Methylene Chloride a 518 J 1000 500 ug/l SM 6200B
Methyl Tert Butyl Ether 216 J 250 63 ug/l SM 6200B
Naphthalene 158 J 250 63 ug/l SM 6200B
n-Propylbenzene 147 J 250 63 ug/l SM 6200B
Toluene 15900 250 63 ug/l SM 6200B
1,2,4-Trimethylbenzene 737 250 63 ug/l SM 6200B
1,3,5-Trimethylbenzene 247 J 250 63 ug/l SM 6200B
4 of 39
FA908892
Summary of Hits Page 2 of 3
Job Number:FA90889
Account:GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Collected:11/16/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
m,p-Xylene 5960 500 63 ug/l SM 6200B
o-Xylene 2270 250 63 ug/l SM 6200B
Xylene (total)8230 750 130 ug/l SM 6200B
FA90889-4 MW-9
Benzene 2.5 J 10 2.5 ug/l SM 6200B
n-Butylbenzene 8.6 J 10 2.5 ug/l SM 6200B
sec-Butylbenzene 8.4 J 10 2.5 ug/l SM 6200B
Ethylbenzene 627 10 2.5 ug/l SM 6200B
Isopropylbenzene 38.2 10 2.5 ug/l SM 6200B
Naphthalene 160 10 2.5 ug/l SM 6200B
n-Propylbenzene 134 10 2.5 ug/l SM 6200B
Toluene 16.9 10 2.5 ug/l SM 6200B
1,2,4-Trimethylbenzene 964 10 2.5 ug/l SM 6200B
1,3,5-Trimethylbenzene 7.0 J 10 2.5 ug/l SM 6200B
m,p-Xylene 768 20 2.5 ug/l SM 6200B
Xylene (total)768 30 5.0 ug/l SM 6200B
FA90889-5 MW-12
Benzene 54.5 1.0 0.25 ug/l SM 6200B
Chloroform 0.27 J 1.0 0.25 ug/l SM 6200B
Ethylbenzene 30.8 1.0 0.25 ug/l SM 6200B
Isopropylbenzene 0.67 J 1.0 0.25 ug/l SM 6200B
Methylene Chloride a 3.3 J 4.0 2.0 ug/l SM 6200B
Methyl Tert Butyl Ether 0.99 J 1.0 0.25 ug/l SM 6200B
Naphthalene 3.7 1.0 0.25 ug/l SM 6200B
n-Propylbenzene 2.8 1.0 0.25 ug/l SM 6200B
Toluene 5.1 1.0 0.25 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.38 J 1.0 0.25 ug/l SM 6200B
m,p-Xylene 7.3 2.0 0.25 ug/l SM 6200B
o-Xylene 0.67 J 1.0 0.25 ug/l SM 6200B
Xylene (total)8.0 3.0 0.50 ug/l SM 6200B
FA90889-6 MW-13
Benzene 2.3 0.50 0.13 ug/l SM 6200B
n-Butylbenzene 0.74 0.50 0.13 ug/l SM 6200B
sec-Butylbenzene 5.0 0.50 0.13 ug/l SM 6200B
tert-Butylbenzene 0.43 J 0.50 0.13 ug/l SM 6200B
Ethylbenzene 0.85 0.50 0.13 ug/l SM 6200B
Isopropylbenzene 25.5 0.50 0.13 ug/l SM 6200B
Naphthalene 2.3 0.50 0.13 ug/l SM 6200B
n-Propylbenzene 1.5 0.50 0.13 ug/l SM 6200B
5 of 39
FA908892
Summary of Hits Page 3 of 3
Job Number:FA90889
Account:GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Collected:11/16/21
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Toluene 2.6 0.50 0.13 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.18 J 0.50 0.13 ug/l SM 6200B
m,p-Xylene 8.3 1.0 0.13 ug/l SM 6200B
o-Xylene 0.27 J 0.50 0.13 ug/l SM 6200B
Xylene (total)8.6 1.5 0.25 ug/l SM 6200B
FA90889-7 TRIP BLANK
Methylene Chloride a 1.8 J 2.0 1.0 ug/l SM 6200B
(a) Suspected laboratory contaminant.
6 of 39
FA908892
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
7 of 39
FA908893
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA90889-1 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0228749.D 200 11/20/21 13:05 JL n/a n/a VA2997
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 7350 100 25 ug/l
108-86-1 Bromobenzene ND 100 25 ug/l
74-97-5 Bromochloromethane ND 100 25 ug/l
75-27-4 Bromodichloromethane ND 100 25 ug/l
75-25-2 Bromoform ND 100 25 ug/l
104-51-8 n-Butylbenzene 48.9 100 25 ug/l J
135-98-8 sec-Butylbenzene 30.2 100 25 ug/l J
98-06-6 tert-Butylbenzene ND 100 25 ug/l
56-23-5 Carbon Tetrachloride ND 100 25 ug/l
108-90-7 Chlorobenzene ND 100 25 ug/l
75-00-3 Chloroethane a ND 100 40 ug/l
67-66-3 Chloroform ND 100 25 ug/l
95-49-8 o-Chlorotoluene ND 100 25 ug/l
106-43-4 p-Chlorotoluene ND 100 25 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l
106-93-4 1,2-Dibromoethane ND 100 25 ug/l
75-71-8 Dichlorodifluoromethane ND 100 40 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 25 ug/l
107-06-2 1,2-Dichloroethane ND 100 25 ug/l
75-35-4 1,1-Dichloroethylene ND 100 25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l
78-87-5 1,2-Dichloropropane ND 100 25 ug/l
142-28-9 1,3-Dichloropropane ND 100 25 ug/l
594-20-7 2,2-Dichloropropane b ND 100 25 ug/l
563-58-6 1,1-Dichloropropene ND 100 25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 39
FA9088933.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA90889-1 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether 41.9 100 25 ug/l J
100-41-4 Ethylbenzene 4050 100 25 ug/l
87-68-3 Hexachlorobutadiene ND 100 25 ug/l
98-82-8 Isopropylbenzene 110 100 25 ug/l
99-87-6 p-Isopropyltoluene ND 100 25 ug/l
74-83-9 Methyl Bromide ND 100 40 ug/l
74-87-3 Methyl Chloride 40.6 100 40 ug/l J
74-95-3 Methylene Bromide ND 100 25 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether 753 100 25 ug/l
91-20-3 Naphthalene 563 100 25 ug/l
103-65-1 n-Propylbenzene 399 100 25 ug/l
100-42-5 Styrene ND 100 25 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l
127-18-4 Tetrachloroethylene ND 100 25 ug/l
108-88-3 Toluene 3540 100 25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l
79-01-6 Trichloroethylene ND 100 25 ug/l
75-69-4 Trichlorofluoromethane ND 100 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 2880 100 25 ug/l
108-67-8 1,3,5-Trimethylbenzene 744 100 25 ug/l
75-01-4 Vinyl Chloride ND 100 25 ug/l
m,p-Xylene 10400 200 25 ug/l
95-47-6 o-Xylene 2260 100 25 ug/l
1330-20-7 Xylene (total)12700 300 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
(a) Associated CCV and ECC recovery outside control limits high, sample was ND.
(b) Associated CCV and BS recovery outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 39
FA9088933.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-4
Lab Sample ID:FA90889-2 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0228750.D 200 11/20/21 13:28 JL n/a n/a VA2997
Run #2 A0228797.D 500 11/23/21 13:42 JL n/a n/a VA3000
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4860 100 25 ug/l
108-86-1 Bromobenzene ND 100 25 ug/l
74-97-5 Bromochloromethane ND 100 25 ug/l
75-27-4 Bromodichloromethane ND 100 25 ug/l
75-25-2 Bromoform ND 100 25 ug/l
104-51-8 n-Butylbenzene ND 100 25 ug/l
135-98-8 sec-Butylbenzene ND 100 25 ug/l
98-06-6 tert-Butylbenzene ND 100 25 ug/l
56-23-5 Carbon Tetrachloride ND 100 25 ug/l
108-90-7 Chlorobenzene ND 100 25 ug/l
75-00-3 Chloroethane a ND 100 40 ug/l
67-66-3 Chloroform ND 100 25 ug/l
95-49-8 o-Chlorotoluene ND 100 25 ug/l
106-43-4 p-Chlorotoluene ND 100 25 ug/l
124-48-1 Dibromochloromethane ND 100 25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 49 ug/l
106-93-4 1,2-Dibromoethane ND 100 25 ug/l
75-71-8 Dichlorodifluoromethane ND 100 40 ug/l
95-50-1 1,2-Dichlorobenzene ND 100 25 ug/l
541-73-1 1,3-Dichlorobenzene ND 100 25 ug/l
106-46-7 1,4-Dichlorobenzene ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 25 ug/l
107-06-2 1,2-Dichloroethane ND 100 25 ug/l
75-35-4 1,1-Dichloroethylene ND 100 25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 25 ug/l
78-87-5 1,2-Dichloropropane ND 100 25 ug/l
142-28-9 1,3-Dichloropropane ND 100 25 ug/l
594-20-7 2,2-Dichloropropane b ND 100 25 ug/l
563-58-6 1,1-Dichloropropene ND 100 25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 100 25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 39
FA9088933.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-4
Lab Sample ID:FA90889-2 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 100 25 ug/l
100-41-4 Ethylbenzene 3930 100 25 ug/l
87-68-3 Hexachlorobutadiene ND 100 25 ug/l
98-82-8 Isopropylbenzene 91.8 100 25 ug/l J
99-87-6 p-Isopropyltoluene ND 100 25 ug/l
74-83-9 Methyl Bromide ND 100 40 ug/l
74-87-3 Methyl Chloride ND 100 40 ug/l
74-95-3 Methylene Bromide ND 100 25 ug/l
75-09-2 Methylene Chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether 175 100 25 ug/l
91-20-3 Naphthalene 354 100 25 ug/l
103-65-1 n-Propylbenzene 326 100 25 ug/l
100-42-5 Styrene ND 100 25 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 100 25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 25 ug/l
127-18-4 Tetrachloroethylene ND 100 25 ug/l
108-88-3 Toluene 12500 c 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 25 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 25 ug/l
79-01-6 Trichloroethylene ND 100 25 ug/l
75-69-4 Trichlorofluoromethane ND 100 40 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 25 ug/l
95-63-6 1,2,4-Trimethylbenzene 2180 100 25 ug/l
108-67-8 1,3,5-Trimethylbenzene 534 100 25 ug/l
75-01-4 Vinyl Chloride ND 100 25 ug/l
m,p-Xylene 10900 200 25 ug/l
95-47-6 o-Xylene 3370 100 25 ug/l
1330-20-7 Xylene (total)14300 300 50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%102%70-130%
2037-26-5 Toluene-D8 101%103%70-130%
460-00-4 4-Bromofluorobenzene 99%100%70-130%
(a) Associated CCV and ECC recovery outside control limits high, sample was ND.
(b) Associated CCV and BS recovery outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 39
FA9088933.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-4
Lab Sample ID:FA90889-2 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 39
FA9088933.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA90889-3 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0228798.D 500 11/23/21 14:05 JL n/a n/a VA3000
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 4770 250 63 ug/l
108-86-1 Bromobenzene ND 250 63 ug/l
74-97-5 Bromochloromethane ND 250 63 ug/l
75-27-4 Bromodichloromethane ND 250 63 ug/l
75-25-2 Bromoform ND 250 63 ug/l
104-51-8 n-Butylbenzene ND 250 63 ug/l
135-98-8 sec-Butylbenzene ND 250 63 ug/l
98-06-6 tert-Butylbenzene ND 250 63 ug/l
56-23-5 Carbon Tetrachloride ND 250 63 ug/l
108-90-7 Chlorobenzene ND 250 63 ug/l
75-00-3 Chloroethane ND 250 100 ug/l
67-66-3 Chloroform ND 250 63 ug/l
95-49-8 o-Chlorotoluene ND 250 63 ug/l
106-43-4 p-Chlorotoluene ND 250 63 ug/l
124-48-1 Dibromochloromethane ND 250 63 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 250 120 ug/l
106-93-4 1,2-Dibromoethane ND 250 63 ug/l
75-71-8 Dichlorodifluoromethane a ND 250 100 ug/l
95-50-1 1,2-Dichlorobenzene ND 250 63 ug/l
541-73-1 1,3-Dichlorobenzene ND 250 63 ug/l
106-46-7 1,4-Dichlorobenzene ND 250 63 ug/l
75-34-3 1,1-Dichloroethane ND 250 63 ug/l
107-06-2 1,2-Dichloroethane ND 250 63 ug/l
75-35-4 1,1-Dichloroethylene ND 250 63 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 250 63 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 250 63 ug/l
78-87-5 1,2-Dichloropropane ND 250 63 ug/l
142-28-9 1,3-Dichloropropane ND 250 63 ug/l
594-20-7 2,2-Dichloropropane ND 250 63 ug/l
563-58-6 1,1-Dichloropropene ND 250 63 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 250 63 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 250 63 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 39
FA9088933.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA90889-3 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 250 63 ug/l
100-41-4 Ethylbenzene 1650 250 63 ug/l
87-68-3 Hexachlorobutadiene ND 250 63 ug/l
98-82-8 Isopropylbenzene ND 250 63 ug/l
99-87-6 p-Isopropyltoluene ND 250 63 ug/l
74-83-9 Methyl Bromide ND 250 100 ug/l
74-87-3 Methyl Chloride ND 250 100 ug/l
74-95-3 Methylene Bromide ND 250 63 ug/l
75-09-2 Methylene Chloride b 518 1000 500 ug/l J
1634-04-4 Methyl Tert Butyl Ether 216 250 63 ug/l J
91-20-3 Naphthalene 158 250 63 ug/l J
103-65-1 n-Propylbenzene 147 250 63 ug/l J
100-42-5 Styrene ND 250 63 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 250 63 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 250 63 ug/l
127-18-4 Tetrachloroethylene ND 250 63 ug/l
108-88-3 Toluene 15900 250 63 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 250 63 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 250 63 ug/l
71-55-6 1,1,1-Trichloroethane ND 250 63 ug/l
79-00-5 1,1,2-Trichloroethane ND 250 63 ug/l
79-01-6 Trichloroethylene ND 250 63 ug/l
75-69-4 Trichlorofluoromethane ND 250 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 250 63 ug/l
95-63-6 1,2,4-Trimethylbenzene 737 250 63 ug/l
108-67-8 1,3,5-Trimethylbenzene 247 250 63 ug/l J
75-01-4 Vinyl Chloride ND 250 63 ug/l
m,p-Xylene 5960 500 63 ug/l
95-47-6 o-Xylene 2270 250 63 ug/l
1330-20-7 Xylene (total)8230 750 130 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
(b) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 39
FA9088933.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA90889-4 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0228752.D 20 11/20/21 14:14 JL n/a n/a VA2997
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.5 10 2.5 ug/l J
108-86-1 Bromobenzene ND 10 2.5 ug/l
74-97-5 Bromochloromethane ND 10 2.5 ug/l
75-27-4 Bromodichloromethane ND 10 2.5 ug/l
75-25-2 Bromoform ND 10 2.5 ug/l
104-51-8 n-Butylbenzene 8.6 10 2.5 ug/l J
135-98-8 sec-Butylbenzene 8.4 10 2.5 ug/l J
98-06-6 tert-Butylbenzene ND 10 2.5 ug/l
56-23-5 Carbon Tetrachloride ND 10 2.5 ug/l
108-90-7 Chlorobenzene ND 10 2.5 ug/l
75-00-3 Chloroethane a ND 10 4.0 ug/l
67-66-3 Chloroform ND 10 2.5 ug/l
95-49-8 o-Chlorotoluene ND 10 2.5 ug/l
106-43-4 p-Chlorotoluene ND 10 2.5 ug/l
124-48-1 Dibromochloromethane ND 10 2.5 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 10 4.9 ug/l
106-93-4 1,2-Dibromoethane ND 10 2.5 ug/l
75-71-8 Dichlorodifluoromethane ND 10 4.0 ug/l
95-50-1 1,2-Dichlorobenzene ND 10 2.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 10 2.5 ug/l
106-46-7 1,4-Dichlorobenzene ND 10 2.5 ug/l
75-34-3 1,1-Dichloroethane ND 10 2.5 ug/l
107-06-2 1,2-Dichloroethane ND 10 2.5 ug/l
75-35-4 1,1-Dichloroethylene ND 10 2.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 10 2.5 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 10 2.5 ug/l
78-87-5 1,2-Dichloropropane ND 10 2.5 ug/l
142-28-9 1,3-Dichloropropane ND 10 2.5 ug/l
594-20-7 2,2-Dichloropropane b ND 10 2.5 ug/l
563-58-6 1,1-Dichloropropene ND 10 2.5 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 2.5 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 10 2.5 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 39
FA9088933.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA90889-4 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 10 2.5 ug/l
100-41-4 Ethylbenzene 627 10 2.5 ug/l
87-68-3 Hexachlorobutadiene ND 10 2.5 ug/l
98-82-8 Isopropylbenzene 38.2 10 2.5 ug/l
99-87-6 p-Isopropyltoluene ND 10 2.5 ug/l
74-83-9 Methyl Bromide ND 10 4.0 ug/l
74-87-3 Methyl Chloride ND 10 4.0 ug/l
74-95-3 Methylene Bromide ND 10 2.5 ug/l
75-09-2 Methylene Chloride ND 40 20 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 10 2.5 ug/l
91-20-3 Naphthalene 160 10 2.5 ug/l
103-65-1 n-Propylbenzene 134 10 2.5 ug/l
100-42-5 Styrene ND 10 2.5 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 10 2.5 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.5 ug/l
127-18-4 Tetrachloroethylene ND 10 2.5 ug/l
108-88-3 Toluene 16.9 10 2.5 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 2.5 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 2.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 10 2.5 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 2.5 ug/l
79-01-6 Trichloroethylene ND 10 2.5 ug/l
75-69-4 Trichlorofluoromethane ND 10 4.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 10 2.5 ug/l
95-63-6 1,2,4-Trimethylbenzene 964 10 2.5 ug/l
108-67-8 1,3,5-Trimethylbenzene 7.0 10 2.5 ug/l J
75-01-4 Vinyl Chloride ND 10 2.5 ug/l
m,p-Xylene 768 20 2.5 ug/l
95-47-6 o-Xylene ND 10 2.5 ug/l
1330-20-7 Xylene (total)768 30 5.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
(a) Associated CCV and ECC recovery outside control limits high, sample was ND.
(b) Associated CCV and BS recovery outside control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 39
FA9088933.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA90889-5 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0228799.D 2 11/23/21 14:28 JL n/a n/a VA3000
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 54.5 1.0 0.25 ug/l
108-86-1 Bromobenzene ND 1.0 0.25 ug/l
74-97-5 Bromochloromethane ND 1.0 0.25 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.25 ug/l
75-25-2 Bromoform ND 1.0 0.25 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.25 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.25 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.25 ug/l
108-90-7 Chlorobenzene ND 1.0 0.25 ug/l
75-00-3 Chloroethane ND 1.0 0.40 ug/l
67-66-3 Chloroform 0.27 1.0 0.25 ug/l J
95-49-8 o-Chlorotoluene ND 1.0 0.25 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 0.49 ug/l
106-93-4 1,2-Dibromoethane ND 1.0 0.25 ug/l
75-71-8 Dichlorodifluoromethane a ND 1.0 0.40 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.25 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.25 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.25 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.25 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.25 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.25 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.25 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.25 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.25 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.25 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.25 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.25 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 39
FA9088933.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA90889-5 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 1.0 0.25 ug/l
100-41-4 Ethylbenzene 30.8 1.0 0.25 ug/l
87-68-3 Hexachlorobutadiene ND 1.0 0.25 ug/l
98-82-8 Isopropylbenzene 0.67 1.0 0.25 ug/l J
99-87-6 p-Isopropyltoluene ND 1.0 0.25 ug/l
74-83-9 Methyl Bromide ND 1.0 0.40 ug/l
74-87-3 Methyl Chloride ND 1.0 0.40 ug/l
74-95-3 Methylene Bromide ND 1.0 0.25 ug/l
75-09-2 Methylene Chloride b 3.3 4.0 2.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether 0.99 1.0 0.25 ug/l J
91-20-3 Naphthalene 3.7 1.0 0.25 ug/l
103-65-1 n-Propylbenzene 2.8 1.0 0.25 ug/l
100-42-5 Styrene ND 1.0 0.25 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.25 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.25 ug/l
108-88-3 Toluene 5.1 1.0 0.25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.0 0.25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.0 0.25 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.25 ug/l
79-01-6 Trichloroethylene ND 1.0 0.25 ug/l
75-69-4 Trichlorofluoromethane ND 1.0 0.40 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.0 0.25 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.38 1.0 0.25 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.25 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.25 ug/l
m,p-Xylene 7.3 2.0 0.25 ug/l
95-47-6 o-Xylene 0.67 1.0 0.25 ug/l J
1330-20-7 Xylene (total)8.0 3.0 0.50 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
(b) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 39
FA9088933.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-13
Lab Sample ID:FA90889-6 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0228796.D 1 11/23/21 13:19 JL n/a n/a VA3000
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2.3 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene 0.74 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene 5.0 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene 0.43 0.50 0.13 ug/l J
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 39
FA9088933.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-13
Lab Sample ID:FA90889-6 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene 0.85 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene 25.5 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene 2.3 0.50 0.13 ug/l
103-65-1 n-Propylbenzene 1.5 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene 2.6 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.18 0.50 0.13 ug/l J
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene 8.3 1.0 0.13 ug/l
95-47-6 o-Xylene 0.27 0.50 0.13 ug/l J
1330-20-7 Xylene (total)8.6 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 102%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 39
FA9088933.6
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA90889-7 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0228795.D 1 11/23/21 12:56 JL n/a n/a VA3000
Run #2 a A0228748.D 1 11/20/21 12:41 JL n/a n/a VA2997
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane b ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 39
FA9088933.7
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA90889-7 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride c 1.8 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%109%70-130%
17060-07-0 1,2-Dichloroethane-D4 109%113%70-130%
2037-26-5 Toluene-D8 102%101%70-130%
460-00-4 4-Bromofluorobenzene 98%100%70-130%
(a) Associated internal standard response outside control limits. Confirmation run.
(b) Associated ECC outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 39
FA9088933.7
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA90889-7 Date Sampled:11/16/21
Matrix:AQ - Ground Water Date Received:11/17/21
Method:SM 6200B Percent Solids:n/a
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
(c) Suspected laboratory contaminant.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 39
FA9088933.7
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
24 of 39
FA908894
FA90889: Chain of Custody
Page 1 of 2
25 of 39
FA9088944.1
Job Number:FA90889 Client:GEOLOGICAL RESOURCES INC.
Date / Time Received:11/17/2021 2:30:00 PM Delivery Method:FED EX
Project:U-FILLER UP #26
Airbill #'s:1009 6379 2881
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (4.6);
Cooler 1: (4.8);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:CARLOSD Date:Date:11/17/2021 2:30:00 P
FA90889: Chain of Custody
Page 2 of 2
26 of 39
FA9088944.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
27 of 39
FA908895
Method Blank Summary Page 1 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2997-MB A0228747.D 1 11/20/21 JL n/a n/a VA2997
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-1, FA90889-2, FA90889-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
28 of 39
FA9088955.1.1
Method Blank Summary Page 2 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2997-MB A0228747.D 1 11/20/21 JL n/a n/a VA2997
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-1, FA90889-2, FA90889-4
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 110%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
29 of 39
FA9088955.1.1
Method Blank Summary Page 1 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3000-MB A0228794.D 1 11/23/21 JL n/a n/a VA3000
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-2, FA90889-3, FA90889-5, FA90889-6, FA90889-7
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.13 ug/l
108-86-1 Bromobenzene ND 0.50 0.13 ug/l
74-97-5 Bromochloromethane ND 0.50 0.13 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.13 ug/l
75-25-2 Bromoform ND 0.50 0.13 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.13 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.13 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.13 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.13 ug/l
108-90-7 Chlorobenzene ND 0.50 0.13 ug/l
75-00-3 Chloroethane ND 0.50 0.20 ug/l
67-66-3 Chloroform ND 0.50 0.13 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.13 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.13 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.13 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.25 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.13 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.20 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.13 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.13 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.13 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.13 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.13 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.13 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.13 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.13 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.13 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.13 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.13 ug/l
100-41-4 Ethylbenzene ND 0.50 0.13 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.13 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.13 ug/l
30 of 39
FA9088955.1.2
Method Blank Summary Page 2 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3000-MB A0228794.D 1 11/23/21 JL n/a n/a VA3000
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-2, FA90889-3, FA90889-5, FA90889-6, FA90889-7
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.13 ug/l
74-83-9 Methyl Bromide ND 0.50 0.20 ug/l
74-87-3 Methyl Chloride ND 0.50 0.20 ug/l
74-95-3 Methylene Bromide ND 0.50 0.13 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.13 ug/l
91-20-3 Naphthalene ND 0.50 0.13 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.13 ug/l
100-42-5 Styrene ND 0.50 0.13 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.13 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.13 ug/l
108-88-3 Toluene ND 0.50 0.13 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.13 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.13 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.13 ug/l
79-01-6 Trichloroethylene ND 0.50 0.13 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.20 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.13 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.13 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.13 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.25 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 107%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
31 of 39
FA9088955.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2997-BS A0228745.D 1 11/20/21 JL n/a n/a VA2997
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-1, FA90889-2, FA90889-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.1 111 70-130
108-86-1 Bromobenzene 10 9.9 99 70-130
74-97-5 Bromochloromethane 10 8.9 89 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 9.2 92 70-130
104-51-8 n-Butylbenzene 10 9.8 98 70-130
135-98-8 sec-Butylbenzene 10 11.0 110 70-130
98-06-6 tert-Butylbenzene 10 10.6 106 70-130
56-23-5 Carbon Tetrachloride 10 11.9 119 70-130
108-90-7 Chlorobenzene 10 10.5 105 70-130
75-00-3 Chloroethane 10 10.6 106 60-140
67-66-3 Chloroform 10 10.8 108 70-130
95-49-8 o-Chlorotoluene 10 10.4 104 70-130
106-43-4 p-Chlorotoluene 10 10.2 102 70-130
124-48-1 Dibromochloromethane 10 8.9 89 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.0 90 70-130
106-93-4 1,2-Dibromoethane 10 9.3 93 70-130
75-71-8 Dichlorodifluoromethane 10 11.1 111 60-140
95-50-1 1,2-Dichlorobenzene 10 10.1 101 70-130
541-73-1 1,3-Dichlorobenzene 10 10.8 108 70-130
106-46-7 1,4-Dichlorobenzene 10 10.3 103 70-130
75-34-3 1,1-Dichloroethane 10 11.5 115 70-130
107-06-2 1,2-Dichloroethane 10 10.4 104 70-130
75-35-4 1,1-Dichloroethylene 10 12.5 125 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.9 109 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.5 115 70-130
78-87-5 1,2-Dichloropropane 10 10.4 104 70-130
142-28-9 1,3-Dichloropropane 10 9.3 93 70-130
594-20-7 2,2-Dichloropropane 10 14.5 145*70-130
563-58-6 1,1-Dichloropropene 10 11.0 110 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.3 93 70-130
10061-02-6 trans-1,3-Dichloropropene 10 9.9 99 70-130
108-20-3 Di-Isopropyl Ether 10 9.4 94 70-130
100-41-4 Ethylbenzene 10 10.9 109 70-130
87-68-3 Hexachlorobutadiene 10 10.7 107 70-130
98-82-8 Isopropylbenzene 10 10.4 104 70-130
* = Outside of Control Limits.
32 of 39
FA9088955.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA2997-BS A0228745.D 1 11/20/21 JL n/a n/a VA2997
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-1, FA90889-2, FA90889-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.5 105 70-130
74-83-9 Methyl Bromide 10 10.6 106 60-140
74-87-3 Methyl Chloride 10 10.4 104 60-140
74-95-3 Methylene Bromide 10 9.5 95 70-130
75-09-2 Methylene Chloride 10 8.6 86 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
91-20-3 Naphthalene 10 7.9 79 70-130
103-65-1 n-Propylbenzene 10 10.4 104 70-130
100-42-5 Styrene 10 9.6 96 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.1 101 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.9 89 70-130
127-18-4 Tetrachloroethylene 10 11.1 111 70-130
108-88-3 Toluene 10 10.2 102 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.0 90 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.7 87 70-130
71-55-6 1,1,1-Trichloroethane 10 11.4 114 70-130
79-00-5 1,1,2-Trichloroethane 10 9.6 96 70-130
79-01-6 Trichloroethylene 10 11.1 111 70-130
75-69-4 Trichlorofluoromethane 10 10.8 108 60-140
96-18-4 1,2,3-Trichloropropane 10 9.0 90 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.9 99 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10 100 70-130
75-01-4 Vinyl Chloride 10 10.2 102 60-140
m,p-Xylene 20 20.8 104 70-130
95-47-6 o-Xylene 10 9.9 99 70-130
1330-20-7 Xylene (total)30 30.7 102 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
* = Outside of Control Limits.
33 of 39
FA9088955.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3000-BS A0228792.D 1 11/23/21 JL n/a n/a VA3000
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-2, FA90889-3, FA90889-5, FA90889-6, FA90889-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 9.8 98 70-130
108-86-1 Bromobenzene 10 9.1 91 70-130
74-97-5 Bromochloromethane 10 8.3 83 70-130
75-27-4 Bromodichloromethane 10 9.3 93 70-130
75-25-2 Bromoform 10 9.3 93 70-130
104-51-8 n-Butylbenzene 10 8.8 88 70-130
135-98-8 sec-Butylbenzene 10 10.1 101 70-130
98-06-6 tert-Butylbenzene 10 9.4 94 70-130
56-23-5 Carbon Tetrachloride 10 10.2 102 70-130
108-90-7 Chlorobenzene 10 9.4 94 70-130
75-00-3 Chloroethane 10 8.9 89 60-140
67-66-3 Chloroform 10 9.5 95 70-130
95-49-8 o-Chlorotoluene 10 10.2 102 70-130
106-43-4 p-Chlorotoluene 10 9.1 91 70-130
124-48-1 Dibromochloromethane 10 8.7 87 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.5 95 70-130
106-93-4 1,2-Dibromoethane 10 9.1 91 70-130
75-71-8 Dichlorodifluoromethane 10 12.4 124 60-140
95-50-1 1,2-Dichlorobenzene 10 9.5 95 70-130
541-73-1 1,3-Dichlorobenzene 10 9.9 99 70-130
106-46-7 1,4-Dichlorobenzene 10 9.2 92 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
107-06-2 1,2-Dichloroethane 10 9.2 92 70-130
75-35-4 1,1-Dichloroethylene 10 10.5 105 70-130
156-59-2 cis-1,2-Dichloroethylene 10 9.8 98 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10 100 70-130
78-87-5 1,2-Dichloropropane 10 9.4 94 70-130
142-28-9 1,3-Dichloropropane 10 8.9 89 70-130
594-20-7 2,2-Dichloropropane 10 11.5 115 70-130
563-58-6 1,1-Dichloropropene 10 10.5 105 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.4 94 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.1 101 70-130
108-20-3 Di-Isopropyl Ether 10 9.6 96 70-130
100-41-4 Ethylbenzene 10 9.9 99 70-130
87-68-3 Hexachlorobutadiene 10 10.3 103 70-130
98-82-8 Isopropylbenzene 10 9.6 96 70-130
* = Outside of Control Limits.
34 of 39
FA9088955.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA3000-BS A0228792.D 1 11/23/21 JL n/a n/a VA3000
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-2, FA90889-3, FA90889-5, FA90889-6, FA90889-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 9.6 96 70-130
74-83-9 Methyl Bromide 10 10.6 106 60-140
74-87-3 Methyl Chloride 10 10.4 104 60-140
74-95-3 Methylene Bromide 10 8.7 87 70-130
75-09-2 Methylene Chloride 10 9.9 99 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.5 95 70-130
91-20-3 Naphthalene 10 8.3 83 70-130
103-65-1 n-Propylbenzene 10 10.3 103 70-130
100-42-5 Styrene 10 8.8 88 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.3 93 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.9 89 70-130
127-18-4 Tetrachloroethylene 10 10.1 101 70-130
108-88-3 Toluene 10 9.4 94 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.6 96 70-130
120-82-1 1,2,4-Trichlorobenzene 10 8.6 86 70-130
71-55-6 1,1,1-Trichloroethane 10 10 100 70-130
79-00-5 1,1,2-Trichloroethane 10 9.1 91 70-130
79-01-6 Trichloroethylene 10 9.7 97 70-130
75-69-4 Trichlorofluoromethane 10 11.0 110 60-140
96-18-4 1,2,3-Trichloropropane 10 8.9 89 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.9 89 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.1 91 70-130
75-01-4 Vinyl Chloride 10 10.8 108 60-140
m,p-Xylene 20 20.7 104 70-130
95-47-6 o-Xylene 10 9.2 92 70-130
1330-20-7 Xylene (total)30 29.8 99 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
35 of 39
FA9088955.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA90926-4MS A0228770.D 5 11/20/21 JL n/a n/a VA2997
FA90926-4MSD A0228771.D 5 11/20/21 JL n/a n/a VA2997
FA90926-4 A0228757.D 5 11/20/21 JL n/a n/a VA2997
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-1, FA90889-2, FA90889-4
FA90926-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 4.0 50 62.6 117 50 62.6 117 0 70-130/20
108-86-1 Bromobenzene ND 50 52.9 106 50 53.6 107 1 70-130/20
74-97-5 Bromochloromethane ND 50 46.9 94 50 47.0 94 0 70-130/20
75-27-4 Bromodichloromethane ND 50 50.4 101 50 50.6 101 0 70-130/20
75-25-2 Bromoform ND 50 37.6 75 50 37.8 76 1 70-130/20
104-51-8 n-Butylbenzene ND 50 51.9 104 50 52.6 105 1 70-130/20
135-98-8 sec-Butylbenzene 0.73 J 50 58.8 116 50 59.1 117 1 70-130/20
98-06-6 tert-Butylbenzene ND 50 56.6 113 50 57.5 115 2 70-130/20
56-23-5 Carbon Tetrachloride ND 50 59.7 119 50 59.0 118 1 70-130/20
108-90-7 Chlorobenzene ND 50 55.5 111 50 55.4 111 0 70-130/20
75-00-3 Chloroethane ND 50 53.5 107 50 62.6 125 16 60-140/20
67-66-3 Chloroform ND 50 58.2 116 50 57.6 115 1 70-130/20
95-49-8 o-Chlorotoluene ND 50 55.7 111 50 56.1 112 1 70-130/20
106-43-4 p-Chlorotoluene ND 50 53.8 108 50 54.2 108 1 70-130/20
124-48-1 Dibromochloromethane ND 50 40.5 81 50 40.3 81 0 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 50 47.9 96 50 48.3 97 1 70-130/20
106-93-4 1,2-Dibromoethane ND 50 48.6 97 50 50.0 100 3 70-130/20
75-71-8 Dichlorodifluoromethane ND 50 54.0 108 50 62.1 124 14 60-140/20
95-50-1 1,2-Dichlorobenzene ND 50 54.2 108 50 54.9 110 1 70-130/20
541-73-1 1,3-Dichlorobenzene ND 50 57.0 114 50 57.2 114 0 70-130/20
106-46-7 1,4-Dichlorobenzene ND 50 53.8 108 50 53.8 108 0 70-130/20
75-34-3 1,1-Dichloroethane ND 50 60.8 122 50 61.0 122 0 70-130/20
107-06-2 1,2-Dichloroethane ND 50 54.9 110 50 55.4 111 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 50 64.2 128 50 64.4 129 0 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 50 57.2 114 50 57.5 115 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 50 60.1 120 50 60.1 120 0 70-130/20
78-87-5 1,2-Dichloropropane ND 50 57.0 114 50 57.0 114 0 70-130/20
142-28-9 1,3-Dichloropropane ND 50 49.4 99 50 49.9 100 1 70-130/20
594-20-7 2,2-Dichloropropane ND 50 68.2 136*50 68.0 136*0 70-130/20
563-58-6 1,1-Dichloropropene ND 50 57.6 115 50 57.7 115 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 50 39.9 80 50 39.6 79 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 50 46.7 93 50 45.9 92 2 70-130/20
108-20-3 Di-Isopropyl Ether 194 50 219 50* a 50 217 46* a 1 70-130/20
100-41-4 Ethylbenzene 5.4 50 63.3 116 50 63.2 116 0 70-130/20
87-68-3 Hexachlorobutadiene ND 50 57.3 115 50 57.6 115 1 70-130/20
98-82-8 Isopropylbenzene 1.1 J 50 57.9 114 50 58.2 114 1 70-130/20
* = Outside of Control Limits.
36 of 39
FA9088955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA90926-4MS A0228770.D 5 11/20/21 JL n/a n/a VA2997
FA90926-4MSD A0228771.D 5 11/20/21 JL n/a n/a VA2997
FA90926-4 A0228757.D 5 11/20/21 JL n/a n/a VA2997
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-1, FA90889-2, FA90889-4
FA90926-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 50 55.8 112 50 56.2 112 1 70-130/20
74-83-9 Methyl Bromide ND 50 52.0 104 50 60.2 120 15 60-140/20
74-87-3 Methyl Chloride ND 50 49.4 99 50 56.1 112 13 60-140/20
74-95-3 Methylene Bromide ND 50 49.6 99 50 50.3 101 1 70-130/20
75-09-2 Methylene Chloride ND 50 44.6 89 50 44.6 89 0 70-130/20
1634-04-4 Methyl Tert Butyl Ether 59.0 50 106 94 50 107 96 1 70-130/20
91-20-3 Naphthalene 3.5 50 48.5 90 50 49.9 93 3 70-130/20
103-65-1 n-Propylbenzene 1.1 J 50 57.0 112 50 56.9 112 0 70-130/20
100-42-5 Styrene ND 50 49.4 99 50 49.9 100 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 50 52.9 106 50 53.5 107 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 50 48.0 96 50 48.5 97 1 70-130/20
127-18-4 Tetrachloroethylene ND 50 58.4 117 50 58.9 118 1 70-130/20
108-88-3 Toluene 12.6 50 65.9 107 50 65.7 106 0 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 50 48.0 96 50 49.1 98 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 50 51.3 103 50 52.0 104 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 50 60.1 120 50 59.5 119 1 70-130/20
79-00-5 1,1,2-Trichloroethane ND 50 50.3 101 50 50.7 101 1 70-130/20
79-01-6 Trichloroethylene ND 50 58.6 117 50 59.1 118 1 70-130/20
75-69-4 Trichlorofluoromethane ND 50 53.7 107 50 60.5 121 12 60-140/20
96-18-4 1,2,3-Trichloropropane ND 50 45.4 91 50 45.4 91 0 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2.7 50 57.1 109 50 57.2 109 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene 0.95 J 50 55.0 108 50 55.2 109 0 70-130/20
75-01-4 Vinyl Chloride ND 50 49.2 98 50 56.9 114 15 60-140/20
m,p-Xylene 4.9 J 100 117 112 100 116 111 1 70-130/20
95-47-6 o-Xylene 2.3 J 50 57.4 110 50 58.0 111 1 70-130/20
1330-20-7 Xylene (total)7.3 J 150 174 111 150 174 111 0 70-130/20
CAS No.Surrogate Recoveries MS MSD FA90926-4 Limits
1868-53-7 Dibromofluoromethane 100%99%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%100%103%70-130%
2037-26-5 Toluene-D8 100%100%102%70-130%
460-00-4 4-Bromofluorobenzene 100%101%103%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
37 of 39
FA9088955.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA90926-4MS A0228817.D 10 11/23/21 JL n/a n/a VA3000
FA90926-4MSD A0228818.D 10 11/23/21 JL n/a n/a VA3000
FA90926-4 a A0228803.D 10 11/23/21 JL n/a n/a VA3000
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-2, FA90889-3, FA90889-5, FA90889-6, FA90889-7
FA90926-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 3.4 J 100 130 127 100 118 115 10 70-130/20
108-86-1 Bromobenzene ND 100 117 117 100 106 106 10 70-130/20
74-97-5 Bromochloromethane ND 100 107 107 100 94.8 95 12 70-130/20
75-27-4 Bromodichloromethane ND 100 121 121 100 107 107 12 70-130/20
75-25-2 Bromoform ND 100 113 113 100 100 100 12 70-130/20
104-51-8 n-Butylbenzene ND 100 118 118 100 107 107 10 70-130/20
135-98-8 sec-Butylbenzene ND 100 133 133*100 119 119 11 70-130/20
98-06-6 tert-Butylbenzene ND 100 125 125 100 112 112 11 70-130/20
56-23-5 Carbon Tetrachloride ND 100 135 135*100 119 119 13 70-130/20
108-90-7 Chlorobenzene ND 100 123 123 100 110 110 11 70-130/20
75-00-3 Chloroethane ND 100 84.8 85 100 106 106 22*60-140/20
67-66-3 Chloroform ND 100 126 126 100 112 112 12 70-130/20
95-49-8 o-Chlorotoluene ND 100 135 135*100 121 121 11 70-130/20
106-43-4 p-Chlorotoluene ND 100 118 118 100 107 107 10 70-130/20
124-48-1 Dibromochloromethane ND 100 110 110 100 97.8 98 12 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 100 118 118 100 109 109 8 70-130/20
106-93-4 1,2-Dibromoethane ND 100 113 113 100 104 104 8 70-130/20
75-71-8 Dichlorodifluoromethane ND 100 110 110 100 134 134 20 60-140/20
95-50-1 1,2-Dichlorobenzene ND 100 122 122 100 111 111 9 70-130/20
541-73-1 1,3-Dichlorobenzene ND 100 128 128 100 116 116 10 70-130/20
106-46-7 1,4-Dichlorobenzene ND 100 117 117 100 107 107 9 70-130/20
75-34-3 1,1-Dichloroethane ND 100 132 132*100 119 119 10 70-130/20
107-06-2 1,2-Dichloroethane ND 100 119 119 100 107 107 11 70-130/20
75-35-4 1,1-Dichloroethylene ND 100 135 135*100 123 123 9 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 100 123 123 100 113 113 8 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 100 129 129 100 116 116 11 70-130/20
78-87-5 1,2-Dichloropropane ND 100 123 123 100 109 109 12 70-130/20
142-28-9 1,3-Dichloropropane ND 100 112 112 100 103 103 8 70-130/20
594-20-7 2,2-Dichloropropane ND 100 131 131*100 119 119 10 70-130/20
563-58-6 1,1-Dichloropropene ND 100 134 134*100 122 122 9 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 100 115 115 100 105 105 9 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 100 124 124 100 112 112 10 70-130/20
108-20-3 Di-Isopropyl Ether 196 100 344 148*100 327 131*5 70-130/20
100-41-4 Ethylbenzene 4.8 J 100 134 129 100 120 115 11 70-130/20
87-68-3 Hexachlorobutadiene ND 100 133 133*100 120 120 10 70-130/20
98-82-8 Isopropylbenzene ND 100 128 128 100 115 115 11 70-130/20
* = Outside of Control Limits.
38 of 39
FA9088955.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA90889
Account:GRINCC GRI (Geological Resources Inc.)
Project:U Filler Up 26; 101 Smith Church Rd, Roanoke Rapids, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA90926-4MS A0228817.D 10 11/23/21 JL n/a n/a VA3000
FA90926-4MSD A0228818.D 10 11/23/21 JL n/a n/a VA3000
FA90926-4 a A0228803.D 10 11/23/21 JL n/a n/a VA3000
The QC reported here applies to the following samples:Method: SM 6200B
FA90889-2, FA90889-3, FA90889-5, FA90889-6, FA90889-7
FA90926-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 100 122 122 100 111 111 9 70-130/20
74-83-9 Methyl Bromide ND 100 101 101 100 125 125 21*60-140/20
74-87-3 Methyl Chloride ND 100 102 102 100 123 123 19 60-140/20
74-95-3 Methylene Bromide ND 100 112 112 100 100 100 11 70-130/20
75-09-2 Methylene Chloride 12.0 J 100 132 120 100 120 108 10 70-130/20
1634-04-4 Methyl Tert Butyl Ether 49.4 100 180 131*100 169 120 6 70-130/20
91-20-3 Naphthalene 2.3 J 100 116 114 100 108 106 7 70-130/20
103-65-1 n-Propylbenzene ND 100 137 137*100 123 123 11 70-130/20
100-42-5 Styrene ND 100 114 114 100 102 102 11 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 100 124 124 100 108 108 14 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 100 116 116 100 106 106 9 70-130/20
127-18-4 Tetrachloroethylene ND 100 128 128 100 115 115 11 70-130/20
108-88-3 Toluene 11.6 100 133 121 100 120 108 10 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 100 124 124 100 115 115 8 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 100 118 118 100 109 109 8 70-130/20
71-55-6 1,1,1-Trichloroethane ND 100 130 130 100 117 117 11 70-130/20
79-00-5 1,1,2-Trichloroethane ND 100 115 115 100 105 105 9 70-130/20
79-01-6 Trichloroethylene ND 100 127 127 100 114 114 11 70-130/20
75-69-4 Trichlorofluoromethane ND 100 109 109 100 133 133 20 60-140/20
96-18-4 1,2,3-Trichloropropane ND 100 113 113 100 102 102 10 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2.0 J 100 122 120 100 110 108 10 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 100 121 121 100 109 109 10 70-130/20
75-01-4 Vinyl Chloride ND 100 99.7 100 100 128 128 25*60-140/20
m,p-Xylene 4.2 J 200 277 136*200 249 122 11 70-130/20
95-47-6 o-Xylene 1.8 J 100 124 122 100 111 109 11 70-130/20
1330-20-7 Xylene (total)6.0 J 300 400 131*300 360 118 11 70-130/20
CAS No.Surrogate Recoveries MS MSD FA90926-4 Limits
1868-53-7 Dibromofluoromethane 101%100%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%100%100%70-130%
2037-26-5 Toluene-D8 102%101%105%70-130%
460-00-4 4-Bromofluorobenzene 97%99%104%70-130%
(a) Confirmation run.
* = Outside of Control Limits.
39 of 39
FA9088955.3.2

APPENDIX C
Contaminant Mass Calculations

Area ID Well IDs Area (ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³)Volume (L)Effective
Porosity
Effective
Volume (L)
MW-1
MW-4
MW-5
MW-9
MW-12
MW-13
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red.To Date Red.
MW-1 4,790 4,670 3,300 12,500 165 1,080 26505.00 11.52
MW-4 3,540 21,300 8,000 37,900 121 2,170 73031.00 9.03
MW-5 4,910 16,400 1,840 13,900 388 565 38003.00 9.70
MW-9 9.2 15.8 178 273 0.00 64.5 540.50 10.10
MW-12 4,260 2,240 4,040 11,000 174 1,080 22794.00 10.79
MW-13 40.4 135 38.1 101 0.62 16.6 331.72 11.37
Avg.2,924.93 7,460.13 2,899.35 12,612.33 141.44 829.35 26,867.54 10.42
MW-1 4,540 3,390 2,750 10,800 460 471 22411.00 10.51
MW-4 4,710 19,500 3,620 16,900 0.00 476 45206.00 7.98
MW-5 6,140 24,800 2,230 12,700 444 271 46585.00 8.32
MW-9 24.1 116 976 1,900 0.00 263 3279.10 8.84
MW-12 45.1 18 23.4 19 1.7 3 110.20 8.71
MW-13 10.4 1.5 5.3 4.1 0.00 5.2 26.50 10.19
Avg.2,578.27 7,970.92 1,600.78 7,053.85 150.95 248.20 19,602.97 9.09
MW-1 7,440 4,990 3,270 11,700 1,150 523 29073.00 10.82
MW-4 5,520 15,500 3,710 14,100 0 396 39226.00 8.24
MW-5 6,380 26,000 2,210 9,840 4.63 247 44681.63 8.92
MW-9 6.2 10.8 473 492 0.00 121 1103.00 9.00
MW-12 3,480 1,140 1,990 4,960 0.00 306 11876.00 10.09
MW-13 9.7 30.2 22.1 233 0.00 28.3 323.30 10.41
Avg.3,805.98 7,945.17 1,945.85 6,887.50 192.44 270.22 21,047.16 9.58
MW-1 6,610.00 2,970.00 2,990.00 9,300.00 557.00 467.00 22,894.00 11.82
MW-4 4,430.00 19,700.00 3,990.00 17,400.00 69.40 499.00 46,088.40 9.29
MW-5 4,200.00 15,100.00 1,320.00 7,520.00 286.00 142.00 28,568.00 9.95
MW-9 8.30 31.60 511.00 937.00 0.00 152.00 1,639.90 9.30
MW-12 3,460.00 1,250.00 1,800.00 4,330.00 57.60 372.00 11,269.60 10.82
MW-13 4.30 2.60 8.60 36.60 0.00 9.00 61.10 11.42
Avg.3,118.77 6,509.03 1,769.93 6,587.27 161.67 273.50 18,420.17 10.43
MW-1 6,210.00 3,410.00 3,570.00 14,300.00 1,030.00 686.00 29,206.00 11.30
MW-4 4,190.00 16,500.00 3,660.00 17,100.00 93.50 484.00 42,027.50 8.96
MW-5 6,610.00 32,900.00 2,430.00 14,200.00 318.00 337.00 56,795.00 9.51
MW-9 4.10 12.80 525.00 611.00 0.00 188.00 1,340.90 9.67
MW-12 3,800.00 1,350.00 1,970.00 3,640.00 61.70 379.00 11,200.70 10.76
MW-13 7.50 17.80 26.10 146.00 0.00 20.30 217.70 11.06
Avg.3,470.27 9,031.77 2,030.18 8,332.83 250.53 349.05 23,464.63 10.21
1 01/16/20
1 08/20/20
APPENDIX C
PERCENTAGE REDUCTIONS
U-FILLER UP #26 (INCIDENT NO. 7093)
110,000.0 12.911 1,420,100
Baseline Event
23.33 10.42 0.20 8,042,53840,212,688
1 12/27/18
05/31/18
07/09/19
1
1
191,784.92 -29.6%11.3%
---216,111.07
180,286.39 -3.7%
---
173,879.27 19.5%19.5%
16.6%
147,991.88 17.9%31.5%
12.91
14.24
13.75
12.90
13.12
Area ID Well IDs Area (ft²)
Average Well
Depth
(ft.)
Average
Depth to
Water
(ft.)
Water Column
Height (ft)Volume (ft³)Volume (L)Effective
Porosity
Effective
Volume (L)
MW-1
MW-4
MW-5
MW-9
MW-12
MW-13
Area Date Well Benzene
(μ/L)
Toluene
(μ/L)
Ethylbenzene
(μ/L)
Xylenes
(μ/L)
MTBE
(μ/L)
Naphthalene
(μ/L)
Total
(μ/L)
DTW
(ft.)
Average Water
Column Height
(ft.)
Total Average Mass
(g)Percent Red.To Date Red.
APPENDIX C
PERCENTAGE REDUCTIONS
U-FILLER UP #26 (INCIDENT NO. 7093)
110,000.0 12.911 1,420,100
Baseline Event
23.33 10.42 0.20 8,042,53840,212,688
MW-1 6,010.00 2,140.00 2,780.00 7,970.00 792.00 416.00 20,108.00 9.05
MW-4 4,100.00 8,810.00 2,870.00 11,700.00 0.00 384.00 27,864.00 6.76
MW-5 9,120.00 38,000.00 3,270.00 18,400.00 471.00 407.00 69,668.00 7.27
MW-9 4.10 12.80 525.00 611.00 0.00 188.00 1,340.90 9.67
MW-12 1,660.00 201.00 790.00 1,280.00 0.00 156.00 4,087.00 8.86
MW-13 5.00 11.40 33.10 79.10 0.00 25.00 153.60 8.98
Avg.3,483.18 8,195.87 1,711.35 6,673.35 210.50 262.67 20,536.92 8.43
MW-1 7,350.00 3,540.00 4,050.00 12,700.00 753.00 563.00 28,956.00 11.98
MW-4 4,860.00 12,500.00 3,930.00 14,300.00 175.00 354.00 36,119.00 9.58
MW-5 4,770.00 15,900.00 1,650.00 8,230.00 216.00 158.00 30,924.00 10.19
MW-9 2.50 16.90 627.00 768.00 0.00 160.00 1,574.40 10.23
MW-12 54.50 5.10 30.80 8.00 0.99 3.70 103.09 10.21
MW-13 2.30 2.60 0.85 8.60 0.00 2.30 16.65 11.54
Avg.2,839.88 5,327.43 1,714.78 6,002.43 190.83 206.83 16,282.19 10.62
Date
Average Water
Column Height
(ft.)
05/31/2018 12.91
12/27/2018 14.24
07/08/2019 13.75
01/16/2020 12.90
08/20/2020 13.12
05/18/2021 14.90
11/16/2021 12.71
Notes:
• Baseline contaminant mass was calculated using the maximum water column observed as well as the results from the May 2018 ground water sampling event.
190,607.41 1%12%
Total Contaminant Mass (g)
216,111.07
1 05/18/21
1 11/16/21
40%
128,904.56
Percent Reduction To DatePercent Reduction Compared
to Previous Event
20%
17%
32%
40%
---
20%
-4%
18%
32%
---
147,991.88
11%-30%191,784.92
11.8%0.6%190,607.4114.90
173,879.27
180,286.39
40.4%32.4%128,904.5612.71