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HomeMy WebLinkAboutRA-641_4028_CA_MRP_20151125ATC Associates of North Carolina, P.C. 2512 Independence Boulevard Suite 200-34 Wilmington, NC 28412 Phone: +1 919 871 0999 Fax: +1 919 871 0335 www.atcgroupservices.com November 25, 2015 Ms. Brenda Hafshejani North Carolina Department of Environmental Quality Raleigh Regional Office Division of Waste Management - UST Section 1628 Mail Service Center Raleigh, North Carolina 27699 Re: Active Remediation Monitoring Report Pantry #3079 5102 Dortches Boulevard Rocky Mount, Nash County, North Carolina NCDEQ Facility ID No. 0-022631 NCDEQ Incident No. 4028 ATC Project No. PANT307923 Dear Ms. Hafshejani: ATC Associates of North Carolina, P.C. (ATC), on behalf of The Pantry, Inc., is submitting this Active Remediation Montioring Report to document the recent MMPE and groundwater sampling events. If you have any questions or require additional information, please contact our office at (919) 871-0999. Sincerely, ATC Associates of North Carolina, P.C. Maureen Jackson, P.G. Senior Project Manager cc: Mr. Brent Puzak, The Pantry, Inc. Active Remediation Monitoring Report Pantry #3079 5102 Dortches Boulevard Rocky Mount, Nash County, North Carolina Risk Classification: High NCDEQ Facility I.D. No. 0-022631 NCDEQ Incident No. 4028 ATC Project No. PANT307923 Prepared by: Submitted to: North Carolina Department of Environmental Quality Division of Waste Management UST Section Raleigh Regional Office 1628 Mail Service Center Raleigh, North Carolina 27699-1628 Elizabeth A. Allyn Project Scientist On Behalf Of: The Pantry, Inc. 305 Gregson Drive Cary, North Carolina 27511 Maureen Jackson, P.G. Phone: (919) 774-6700 Senior Project Manager NC Professional Geologist #2312 Submitted by: ATC Group Services, LLC 2512 Independence Blvd, Suite 200-34 Wilmington, North Carolina 28412 Phone: (919) 871-0999 Fax: (919) 871-0335 November 25, 2015 Active Remediation Monitoring Report Pantry #3079 5102 Dortches Boulevard Rocky Mount, Nash County, North Carolina Risk Classification: High NCDEQ Facility I.D. No. 0-022631 NCDEQ Incident No. 4028 ATC Project No. PANT307923 TABLE OF CONTENTS 1.0 INTRODUCTION .................................................................................................................... 1 2.0 SITE BACKGROUND ............................................................................................................ 1 3.0 MOBILE MULTI-PHASE EXTRACTION EVENT .......................................................... 2 4.0 GROUNDWATER CHARACTERIZATION ..................................................................... 3 4.1 Groundwater Levels ........................................................................................................ 3 4.2 Free Product .................................................................................................................... 3 4.3 Groundwater Quality....................................................................................................... 3 5.0 SUMMARY ............................................................................................................................... 4 TABLES Table 1 UST System Information Table 2 Water Supply Well Information Table 3 Table 4 Table 5 Monitoring Well Construction Information Groundwater Elevation Information Groundwater Analytical Data Table 6 Historical Groundwater Analytical Data FIGURES Figure 1 Topographic Map Figure 2 Site Map Figure 3 Site Vicinity Map Figure 4 Groundwater Elevation Contour Map Figure 5 Dissolved Benzene Isoconcentration Contour Map Figure 6 Figure 7 Dissolved MTBE Isoconcentration Contour Map Dissolved Naphthalene Isoconcentration Contour Map APPENDICES Appendix A Appendix B MMPE Summary Report and Disposal Manifests Laboratory Analytical Report Pantry #3079 – Active Remediation Monitoring Report November 25, 2015 NCDEQ Incident No. 4028 ATC Project No. PANT307923 1 1.0 INTRODUCTION ATC Group Services, LLC (ATC) was retained by The Pantry, Inc. (The Pantry) to perform assessment and corrective action activities at the Pantry #3079 site located at 5102 Dortches Boulevard in Rocky Mount, North Carolina. The site location is shown on Figure 1, and the site details are shown on Figure 2. This report presents a summary of a mobile multi-phase extraction (MMPE) event conducted in September 2015 and laboratory analytical results for the groundwater sampling event conducted in October 19, 2015. 2.0 SITE BACKGROUND The Pantry #3079 (DBA Zip Mart #6) is a convenience and gasoline retail store located at 5102 Dortches Boulevard (Highway 43 at I-95) in Rocky Mount, Nash County, North Carolina. The site is currently active and contains three 12,000-gallon gasoline underground storage tanks (USTs) and one 8,000-gallon diesel UST. Table 1 provides a summary of the current and former UST systems at the site. In February 1989, four 12,000-gallon USTs were removed from the Zip Mart #6 facility. Analytical results of the soil samples collected from the UST bed indicated elevated levels of total petroleum hydrocarbons (TPH) in both the gasoline and diesel range. Between April 1989 and May 1990, Applied Environmental Services, Inc. installed fifteen monitoring wells (MW-1 through MW-15). On July 2, 1990, Applied Environmental Services, Inc. submitted a Groundwater Assessment – Technical and Field Data Report and a Remedial Action Plan and Engineering Report. In July 1998, after discovery of the suspected release, The Pantry, Inc. assumed store operations from Stallings Oil Company, Inc. Subsequently, environmental services were transferred to SEI Environmental, Inc. and SEI Engineering and Geological Services, P.C. (formerly SPATCO Engineering and Geological Services, P.C.) (SEI). During September and November 1999 and again in April 2002, a 1,500-foot receptor survey was conducted which revealed the presence of two potable water supply wells. Public water is supplied to the area. An intermittent stream is located approximately 1,500 feet west of the subject property. Refer to Figure 3 for a site vicinity map. Information regarding properties Pantry #3079 – Active Remediation Monitoring Report November 25, 2015 NCDEQ Incident No. 4028 ATC Project No. PANT307923 2 with water supply wells is summarized in Table 2. On December 10, 1999, SEI submitted a Pre-Corrective Action Plan (CAP) Groundwater Monitoring Report. In February and March 2000, aggressive fluid vapor recovery (AFVR) was conducted on monitoring well MW-1 and recovery well RW-1, which have historically contained free product. The AFVR events were successful in removing approximately 5,605 gallons of contaminated groundwater, 62.03 pounds of petroleum vapors, and an immeasurable amount of free product. Free product has not been detected in any of the groundwater monitoring wells since March 23, 2000. On April 18, 2000, SEI submitted a Free Product Recovery Report. On November 21, 2000, three type II monitoring wells (MW-12A, MW-16, and MW-17) were installed. On August 15, 2001, two additional type II monitoring wells (MW-18 and MW-19) were installed. Monitoring well construction details are summarized in Table 3. On April 30, 2002, SEI submitted a Natural Attenuation CAP. On February 17, 2009, MDSA installed four additional type II monitoring wells (MW-19, MW-20, MW-21 and MW-22) in the apparent down gradient location of the release. The additional monitoring wells were installed in an effort to further delineate the extent of the release. Groundwater sampling events were conducted in July 2009, February 2010, July 2010, March 2011, and July 2011. This report presents the results of a MMPE event conducted in September 2015 and a groundwater sampling event conducted in October 2015. 3.0 MOBILE MULTI-PHASE EXTRACTION EVENT ATC subcontracted Eastern Environmental Management, LLC (EEM) to complete the MMPE event at the site. On September 14, 2015, EEM, mobilized to the site and connected the MMPE equipment to MW-8. The MMPE was conducted for five days and recovered a total of 1,547 gallons of impacted groundwater/free product. No measurable free product was observed in MW- 8 at the conclusion of the event. A copy of EEM’s summary of the MMPE event and disposal manifest is included in Appendix A. According to EEM’s event summary, a calculated 2.46 pounds or 0.39 gallons of VOCs (as gasoline) were removed as vapor. Pantry #3079 – Active Remediation Monitoring Report November 25, 2015 NCDEQ Incident No. 4028 ATC Project No. PANT307923 3 4.0 GROUNDWATER CHARACTERIZATION 4.1 Groundwater Levels Groundwater levels were measured during the recent groundwater sampling event performed on October 19, 2015. An oil/water interface probe was used to gauge depth-to-water and free product thickness, if encountered, from the top of each well casing. Free product was not encountered during the October 2015 event. Groundwater elevations ranged from 12.86 feet to 21.62 feet below ground surface (bgs) in monitoring wells MW-8 and MW-13, respectively. Monitoring well construction details are summarized in Table 3 and groundwater elevation data from the October 2015 sampling event is included in Table 4. A groundwater elevation map is included as Figure 4. 4.2 Free Product Free product was detected in MW-8 at a thickness of 0.83 feet prior to the September 2015 MMPE event. Free product was not detected at the conclusion of the MMPE event. Free product was initially detected in MW-8 in April 2015 groundwater sampling event. Historically at the site, free product has been detected in MW-1 and RW-1. No measureable free product was identified during the October 2015 groundwater sampling event. 4.3 Groundwater Quality Groundwater samples were collected from monitoring wells MW-1 through MW-3, MW-7 through MW-15, and MW-17 through MW-19 on October 19, 2015. Monitoring wells MW-4, MW-20, MW-21, and MW-22 were not located, and MW-16 has been paved over. ATC personnel were unable to access monitoring wells MW-5 and MW-6 as the wells appear to be damaged approximately three to four feet bgs. A disposable polyethylene bailer was used to purge a minimum of three well volumes from the monitoring wells and recovery wells prior to sample collection. Samples were placed in laboratory supplied sample containers and shipped on ice via overnight courier to Pace Analytical Services, Inc. (Pace) in Huntersville, North Carolina. Groundwater samples were analyzed for volatile organic compounds by EPA Method 6200B and lead by EPA Method 6010B. Pantry #3079 – Active Remediation Monitoring Report November 25, 2015 NCDEQ Incident No. 4028 ATC Project No. PANT307923 4 The results of the laboratory analyses indicated benzene, toluene, ethylbenzene, total xylenes, MTBE, naphthalene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1,2-dichloroethane, isopropylbenzene, n-butylbenzene, methylene chloride, n-propylbenzene, styrene, and lead at concentrations above 2L Standards in several wells. It should be noted dissolved benzene exceeded its established Gross Contamination Levels (GCL) in the groundwater sample collected from monitoring well MW-1. Analytical results for the monitoring well samples collected in October 2015 are summarized in Table 5. Historical groundwater analytical data are summarized in Table 6. Benzene, MTBE, and naphthalene isoconcentration contour maps are included as Figures 5 through 7, respectively. A copy of the laboratory analytical report is included in Appendix B. 5.0 SUMMARY During this reporting period, ATC conducted a MMPE event and a groundwater sampling event at the referenced facility. Based on the results of ATC’s assessment, the following conclusions are made: • Groundwater at the site flows towards a ditch located along western portion of the site and to the northwest. • Free product was detected in MW-8 at a thickness of 0.83 feet prior to the September 2015 MMPE event; however, free product was not detected in well MW-8 following the MMPE event or during the groundwater sampling event. • Groundwater samples collected from the monitoring wells in October 2015 contained volatile organic compounds at concentrations above 2L Standards. • Dissolved benzene exceeded its established GCL in the groundwater sample collected from monitoring well MW-1. Based on groundwater analytical results, ATC recommends the installation and maintenance of Biosocks in monitoring wells MW-1, MW-11, MW-13, MW-14, MW-17, and MW-18, on a quarterly basis, to assist with natural attenuation activities. Additionally, ATC recommends continued semi-annual groundwater sampling and reporting. TABLES TABLE 1 UST SYSTEM INFORMATION PANTRY #3079 5102 DORTCHES BOULEVARD ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA ATC PROJECT NO. PANT307923 NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 UST ID Number Product Capacity (gallons)Date Installed Date taken out of Use Date Permanently Closed Was Release Associated With UST System? 0-022631 Gasoline 12,000 2/8/1989 In Use In Use No 0-022631 Gasoline 12,000 2/8/1989 In Use In Use No 0-022631 Gasoline 12,000 2/8/1989 In Use In Use No 0-022631 Diesel 8,000 2/8/1989 In Use In Use No 0-022631 Gasoline 12,000 5/3/1979 Feb 1989 Feb 1989 Yes 0-022631 Gasoline 6,000 5/3/1979 Feb 1989 Feb 1989 Yes 0-022631 Gasoline 6,000 5/3/1979 Feb 1989 Feb 1989 Yes 0-022631 Gasoline 6,000 5/3/1979 Feb 1989 Feb 1989 Yes UST ID Number Owner or Operator?Name of Owner or Operator Dates of Ownership / Operation The Pantry, Inc.February 1989 to present Address Telephone Number 0-022631 Owner/Operator 315 West Ridge Street (919) 446-6184 0-022643 Stallings Oil Company 5/3/1979 to February 1989 Owner/Operator Address Telephone Number Rocky Mount, North Carolina 27801 Cary, North Carolina 27512 PO Box 8019 (919) 774-6700 TABLE 2 WATER SUPPLY WELL INFO PANTRY #3079 5102 DORTCHES BOULEVARD ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA ATC PROJECT NO. PANT307923 NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Well NumberWell OwnerAddressPhone NumberWell UseWell Depth (feet bls)Type of WellWell Casing (feet bls)Well Screen Interval (feet bls)Distance for source area release (feet)Cardinal Direction from releaseWW-1 Samuel Cecil Griffin 4976 Dortches Blvd, Rocky Mt, NC (919) 815-4342 Water Supply Unknown Unknown Unknown Unknown 560 E WW-2 Jennifer Masters 3662 N. Halifax Rd, Rocky Mt, NC (252) 822-3728 Water Supply 100 Unknown Unknown Unknown 930 E TABLE 3 MONITORING WELL CONSTRUCTION INFORMATION PANTRY #3079 5102 DORTCHES BOULEVARD ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA ATC PROJECT NO. PANT307923 NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 WELL I.D.Date Installed Well Diameter (inches) Screen Slot Size (inches) Screened Interval (feet) Total Depth (feet) Date Abandoned MW-1 4/4/1989 2 0.01 12-27 27 Active MW-2 4/4/1989 2 0.01 13-28 28 Active MW-3 4/5/1989 2 0.01 15-30 30 Active MW-4 12/4/1989 2 0.01 15.5-25.5 25.5 Active MW-5 12/4/1989 2 0.01 15.5-25.5 25.5 Active MW-6 12/5/1989 2 0.01 15-25 25 Active MW-7 12/5/1989 2 0.01 15-25 25 Active MW-8 12/5/1989 2 0.01 9-24 24 Active MW-9 3/14/1990 2 0.01 7.5-22.5 22.5 Active MW-10 3/14/1990 2 0.01 13-23 23 Active MW-11 3/14/1990 2 0.01 6-21 21 Active MW-12A 11/21/2000 2 0.01 13-28 28 Active MW-13 3/15/1990 2 0.01 9.5-24.5 24.5 Active MW-14 3/15/1990 2 0.01 15-30 30 Active MW-15 3/15/1990 2 0.01 5-25 25 Active MW-16 11/21/2000 2 0.01 57.5-60 60 ActiveMW-17 11/21/2000 2 0.01 9.5-24.5 24.5 Active MW-18 8/15/2001 2 0.01 9.5-24.5 24.5 Active MW-19 8/15/2001 2 0.01 10-25 25 Active MW-20 2/17/2009 2 0.01 5-20 20 Active MW-21 2/17/2009 2 0.01 5-20 20 ActiveMW-22 2/17/2009 2 0.01 5-20 20 Active TABLE 4 GROUNDWATER ELEVATION INFORMATION PANTRY #3079 5102 DORTCHES BOULEVARD ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA ATC PROJECT NO. PANT307923NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Well I.D. Date TOC Elevation (ft) Depth to Product (ft) Depth to Groundwater (ft) Product Thickness (ft) Groundwater Elevations (ft) MW-1 10/19/2015 503.67 --19.04 --484.63 MW-2 10/19/2015 503.96 --19.55 --484.41 MW-3 10/19/2015 504.40 --19.92 --484.48 MW-4 10/19/2015 NS MW-5 10/19/2015 500.84 MW-6 10/19/2015 500.32 MW-7 10/19/2015 499.58 --18.53 --481.05 MW-8 10/19/2015 498.49 --12.86 --485.63 MW-9 10/19/2015 498.97 --14.28 --484.69 MW-10 10/19/2015 502.28 --18.64 --483.64 MW-11 10/19/2015 503.81 --19.27 --484.54 MW-12A 10/19/2015 501.63 --16.93 --484.70 MW-13 10/19/2015 505.80 --21.62 --484.18 MW-14 10/19/2015 503.40 --18.83 --484.57 MW-15 10/19/2015 504.32 --21.42 --482.90 MW-16 10/19/2015 502.57 MW-17 10/19/2015 502.98 --18.36 --484.62 MW-18 10/19/2015 502.18 --17.76 --484.42 MW-19 10/19/2015 500.78 --13.63 --487.15 MW-20 10/19/2015 492.58 MW-21 10/19/2015 492.20 MW-22 10/19/2015 491.93 Notes: 1. TOC = Top of well casing. 2. NS = Not surveyed. 3. Corrected GW Elev.= (GW Elev. + (Product Thickness*0.76)) Could Not Locate Well Damaged Well Damaged Could Not Locate Could Not Locate Could Not Locate Could Not Locate TABLE 5 GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARD ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA ATC PROJECT NO. PANT307923 NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 6010B MW-1 10/19/2015 6,250 9,320 3,610 8,440 27,620 5,060 2,220 <6.2 2,800 2,040 134 <6.2 <6.2 <6.2 <6.2 212 <25.0 577 60.1 58.6 MW-2 10/19/2015 0.26J <0.25 <0.25 <0.75 0.26 3.8 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 7.3 MW-3 10/19/2015 <0.25 <0.25 <0.25 <0.75 <1.50 0.26J <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 19.6 MW-4 10/19/2015 MW-5 10/19/2015 MW-6 10/19/2015 MW-7 10/19/2015 <0.25 <0.25 <0.25 <0.75 <1.50 <0.25 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 2.5J MW-8 10/19/2015 <0.25 0.38J <0.25 90.4 90.78 <0.25 12.6 <0.25 74.4 <0.25 <0.25 1.6 <0.25 <0.25 7.7 1.9 <1.0 2.2 <0.25 <2.5 MW-9 10/19/2015 <0.25 <0.25 <0.25 <0.75 <1.50 <0.25 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 28.9 MW-10 10/19/2015 <0.25 <0.25 <0.25 <0.75 <1.50 <0.25 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 91.6 MW-11 10/19/2015 1,730 146 1,720 4,620 8,216 543 768 <2.5 1,870 478 9.1 <2.5 <2.5 <2.5 <2.5 77.0 10.4J 208 15.4 55.7 MW-12A 10/19/2015 <0.25 <0.25 <0.25 <0.75 <1.50 <0.25 <1.0 <0.25 1.5 <0.25 <0.25 <0.25 3.2 7.4 <0.25 4.3 <1.0 13.1 <0.25 35.1 MW-13 10/19/2015 77.1 13.8 52.7 48.5 192.1 28.5 40.7 <0.25 25.3 8.0 0.78 <0.25 <0.25 5.7 <0.25 7.6 <1.0 17.6 <0.25 654 MW-14 10/19/2015 1,910 739 1,770 4,060 8,479 116 808 <6.2 2,210 664 13.9 <6.2 <6.2 <6.2 <6.2 118 26.0J 378 <6.2 27.4 MW-15 10/19/2015 <0.25 <0.25 <0.25 <0.75 <1.50 <0.25 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <2.5 MW-16 10/19/2015 MW-17 10/19/2015 898 14,700 4,820 21,680 42,098 <25.0 3,160 31.1J 9,820 2,740 <25.0 <25.0 779 <25.0 <25.0 409 <100 1,400 93.4 60.3 MW-18 10/19/2015 77.3 157 127 401 762.3 2.1 29.7 9.3 69.2 18.0 0.31J <0.25 <0.25 <0.25 <0.25 5.4 <1.0 11.2 4.2 10.6 MW-19 10/19/2015 <0.25 <0.25 <0.25 <0.75 <1.50 <0.25 <1.0 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <0.25 <1.0 <0.25 <0.25 <2.5 MW-20 10/19/2015 MW-21 10/19/2015 MW-22 10/19/2015 RW-1 10/19/2015 1 600 600 500 NE 20 6 70 400 400 0.4 0.6 70 70 70 70 5 70 70 15 5,000 260,000 84,500 85,500 NE 20,000 6,000 70,000 28,500 25,000 400 NE 6,900 8,500 70,000 25,000 5,000 30,000 70,000 15,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDENR. 4. NE = Not established. 5. MTBE = Methyl tertiary butyl ether. 6. Values in BOLD indicate levels above 2L Groundwater Standards. 7. All concentrations in micrograms per liter (ug/L). 8. J values denotes estimated concentration by the laboratory. GCL 2L GW Standard Naphthalene1,3,5-TrimethylbenzeneIsopropylbenzene1,2-Dichloroethanen-ButylbenzeneNot SampledIsopropyl etherNot Sampled - Unable to Locate Not Sampled - Unable to LocateTotal BTEXNot Sampled - Unable to Access BromodichloromethaneBenzeneMTBEn-Propylbenzenesec-ButylbenzeneTotal XylenesEthylbenzeneNot Sampled - Paved Over EPA METHOD 6200B Methylene ChlorideTolueneNot Sampled - Unable to Locate Not Sampled - Unable to Access Analytical Methods: DATE SAMPLEDWELL I.D.LeadNot Sampled - Unable to Locate StyreneChloroform1,2,4-Trimethylbenzene TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 12/29/1989 pre-CAP 10/12/1999 pre-CAP 12/15/2000 pre-CAP 16,000 26,000 3,600 17,400 8,400 -- 9/4/2002 CAP 15,000 26,000 4,200 20,600 11,000 -- 11/26/2002 CAP 15,403.8 24,427.3 2,225.1 17,976.0 3,794.4 -- 2/28/2003 ARMR 8,200 15,000 2,900 15,800 290 -- 5/16/2003 ARMR 8,200 13,000 2,600 13,300 7,200 -- 11/10/2003 ARMR 9,100 13,000 3,000 14,300 12,000 -- 9/28/2004 ARMR 4,700 8,600 1,200 7,600 7,000 -- 12/15/2004 ARMR 9,050 18,800 3,920 18,200 4,050 -- 2/23/2009 ARMR 8,300 7,400 390 1,600 8,100 1,100 7/28/2009 ARMR 8,300 11,000 2,100 15,000 7,100 8202/17/2010 ARMR 4,800 6,300 1,300 16,000 2,800 820 7/9/2010 ARMR 10,000 16,000 2,500 15,000 6,700 8703/7/2011 ARMR 8,190 8,210 876 14,510 9,520 1,120 7/21/2011 ARMR 7,470 6,530 953 9,850 12,200 6913/21/2012 ARMR 3,700 4,500 2,000 11,500 1,800 960 11/17/2012 ARMR 8,700 8,600 2,500 15,600 6,300 970 4/8/2015 ARMR 2,280 3,530 1,610 6,510 1,310 788 10/19/2015 ARMR 6,250 9,320 3,610 8,440 5,060 2,220 12/29/1989 pre-CAP 32.5 BDL BDL 98.1 ---- 10/12/1999 pre-CAP 18 110 BDL BDL 48 -- 12/15/2000 pre-CAP 14 BDL BDL BDL 130 -- 9/4/2002 CAP 7.7 <1 <1 <3 100 -- 11/26/2002 ARMR 2.9 <0.5 <0.5 <1.5 33.8 -- 2/28/2003 ARMR 1.9 <5 <1 <3 52 -- 5/16/2003 ARMR 3.9 <5 <1 <3 51 -- 11/10/2003 ARMR 2 <5 <5 <3 33 -- 9/28/2004 ARMR <1 <5 <1 <3 31 -- 12/15/2004 ARMR 1.7 <1 <1 <3 44.6 -- 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 15 <0.39 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 14 <0.39 2/17/2010 ARMR 0.41 0.67 <0.1 0.58 13 <0.086 7/9/2010 ARMR 0.46 <0.053 <0.1 <0.22 10 <0.086 3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 16.4 <2 7/21/2011 ARMR 0.56 <0.5 <0.5 <1.5 11.2 0.17J 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 7 0.48 11/17/2012 ARMR 1.2 <0.2 <0.2 <0.6 8.9 0.62 4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 3.4 <0.5 10/19/2015 ARMR 0.26J <0.25 <0.25 <0.75 3.8 <1.0 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ. 4. Values in BOLD indicate levels above 2L Groundwater Standards. 5. MTBE = Methyl tertiary butyl ether. 6. All concentrations in micrograms per liter (ug/L). 7. BDL = Below Detection Limit. 8. J value denotes estimated concentration by the laboratory. Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident PhaseNot Sampled - Free Product MW-1 MTBENaphthaleneNot Sampled - Free ProductBenzeneTolueneEthylbenzeneTotal XylenesMW-2 2L GW Standard GCL TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/29/1989 pre-CAP BDL BDL BDL BDL ---- 4/6/1990 pre-CAP 6 BDL 3.5 BDL ---- 10/12/1999 pre-CAP BDL BDL BDL BDL 66 -- 12/15/2000 pre-CAP BDL BDL BDL BDL 53 -- 9/4/2002 CAP <1 <1 <1 <3 15 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 17.3 -- 2/28/2003 ARMR <1 <5 <1 <3 5.7 -- 5/16/2003 ARMR <1 <5 <1 <3 27 -- 11/10/2003 ARMR <1 <5 <1 <3 20 -- 9/28/2004 ARMR <1 <5 <1 <3 19 -- 12/15/2004 ARMR <1 <1 <1 <3 51.2 -- 2/23/2009 ARMR <2 <2.7 <2 <4 430 7.2 7/28/2009 ARMR <0.4 <0.54 <0.4 <0.8 220 <0.78 2/17/2010 ARMR <0.05 1.3 0.45 2 150 <0.086 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 89 <0.086 3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 23.6 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 196 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 16 <0.2 11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 33 <0.5 4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 0.56 <0.5 10/19/2015 ARMR <0.25 <0.25 <0.25 <0.75 0.26J <1.0 12/29/1989 pre-CAP BDL 4 BDL BDL ---- 4/6/1990 pre-CAP 85 170 22 160 ---- 10/12/1999 pre-CAP 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 7/28/2009 ARMR 2/17/2010 ARMR 4/8/2015 ARMR 10/19/2015 ARMR 12/29/1989 pre-CAP BDL BDL BDL BDL ---- 4/6/1990 pre-CAP 5.3 4 3.4 83 ---- 10/12/1999 pre-CAP BDL BDL BDL BDL BDL -- 9/4/2002 CAP <1 <1 <1 <3 <1 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR <1 <5 <1 <3 <5 -- 11/10/2003 ARMR <1 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.78 2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086 3/7/2011 ARMR <0.5 1.3 0.6 2.29 <0.5 <2 7/21/2011 ARMR <0.5 0.13J <0.5 <1.5 <0.5 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2 11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR 10/19/2015 ARMR 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ. 4. J value denotes estimated concentration by the laboratory. 5. Values in BOLD indicate levels above 2L Groundwater Standards. 6. MTBE = Methyl tertiary butyl ether. 7. All concentrations in micrograms per liter (ug/L). 8. BDL = Below Detection Limit. Not Sampled - Unable to Locate Not Sampled - Unable to Locate Not Sampled - Unable to Access Not Sampled - Unable to Locate Not Sampled - Unable to Access Not Sampled - Unable to Locate Not Sampled - Unable to Locate 2L GW Standard GCL MW-5 MW-4 MW-3 TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/29/1989 pre-CAP BDL BDL BDL BDL ---- 4/6/1990 pre-CAP 5.6 6 3.5 23 ---- 10/12/1999 pre-CAP BDL BDL BDL BDL ---- 12/15/2000 pre-CAP 1.5 BDL BDL BDL 15 -- 9/4/2002 CAP <1 <1 <1 <3 <1 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR <1 <5 <1 <3 <5 -- 11/10/2003 ARMR <1 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 1.2 <0.39 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 0.48 <0.78 2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086 7/15/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086 3/7/2011 ARMR <0.5 1 <0.5 1.2 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 3/21/2012 ARMR 11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR 10/19/2015 ARMR12/29/1989 pre-CAP 44.5 BDL BDL 46.6 ---- 4/6/1990 pre-CAP 18 BDL BDL 36 ---- 10/12/1999 pre-CAP BDL BDL BDL BDL 7 -- 12/15/2000 pre-CAP 49 BDL BDL 3.1 86 -- 9/4/2002 CAP <1 <1 <1 <3 6.3 -- 11/26/2002 CAP 11.4 5.8 <0.5 <1.5 34.9 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR 8.7 <5 <1 <3 15 -- 11/10/2003 ARMR 78 <5 <1 7 94 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 0.73 <0.086 3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2 11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 10/19/2015 ARMR <0.25 <0.25 <0.25 <0.75 <0.25 <1.0 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ. 4. J value denotes estimated concentration by the laboratory. 5. Values in BOLD indicate levels above 2L Groundwater Standards. 6. MTBE = Methyl tertiary butyl ether. 7. All concentrations in micrograms per liter (ug/L). 8. BDL = Below Detection Limit. Not Sampled Not Sampled - Unable to Access GCL MW-7 MW-6 2L GW Standard Not Sampled - Unable to Access TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/29/1989 pre-CAP 1.5 1.6 BDL 6.8 ---- 4/6/1990 pre-CAP 6.8 BDL BDL 14 ---- 10/12/1999 pre-CAP BDL BDL BDL BDL BDL -- 12/15/2000 pre-CAP BDL BDL BDL BDL BDL -- 9/4/2002 CAP <1 <1 <1 <3 <1 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR <1 <5 <1 <3 <5 -- 11/10/2003 ARMR <1 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086 3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2 11/18/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR 10/19/2015 ARMR <0.25 0.38J <0.25 90.4 <0.25 12.6 4/6/1990 pre-CAP BDL BDL BDL BDL ---- 10/12/1999 pre-CAP BDL 1.2 BDL BDL BDL -- 12/15/2000 pre-CAP BDL BDL BDL BDL BDL -- 9/4/2002 CAP <1 <1 <1 <3 <1 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR <1 <5 <1 <3 <5 -- 11/10/2003 ARMR <1 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086 3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2 11/18/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 10/19/2015 ARMR <0.25 <0.25 <0.25 <0.75 <0.25 <1.0 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ. 4. NA = Not analyzed. 5. Values in BOLD indicate levels above 2L Groundwater Standards. 6. MTBE = Methyl tertiary butyl ether. 7. All concentrations in micrograms per liter (ug/L). 8. BDL = Below Detection Limit. 9. NR = Not Reported in hisorical tables. Not Sampled - Free Product Not Sampled Not Sampled GCL MW-9 2L GW Standard MW-8 TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes4/6/1990 pre-CAP BDL BDL BDL BDL ---- 10/12/1999 pre-CAP BDL BDL BDL BDL BDL -- 12/15/2000 pre-CAP BDL BDL BDL BDL BDL -- 9/4/2002 CAP <1 <1 <1 <3 <1 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5.0 -- 5/16/2003 ARMR <1 <5 <1 <3 <5.0 -- 11/10/2003 ARMR <1 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 7/28/2009 ARMR 2/17/2010 ARMR 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 0.46 <0.086 3/7/2011 ARMR 1.5 3 0.6 6.4 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 0.55 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2 11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR <0.3 1.8 <0.2 <0.6 <0.2 <0.5 10/19/2015 ARMR <0.25 <0.25 <0.25 <0.75 <0.25 <1.0 4/6/1990 pre-CAP 10,000 13,000 14,000 9,300 ---- 10/12/1999 pre-CAP 9,300 19,000 2,500 13,300 4,500 -- 12/15/2000 pre-CAP 12,000 20,000 3,200 15,100 5,600 -- 9/4/2002 CAP 12,000 14,000 3,500 16,200 4,600 -- 11/26/2002 CAP 13,659.2 14,950.3 3,102.1 15,561.7 3,316.5 -- 2/28/2003 ARMR 7,300 13,000 3,200 16,000 940 -- 5/16/2003 ARMR 5,500 8,400 2,700 12,700 2,800 -- 11/10/2003 ARMR 5,500 9,400 2,600 11,400 2,400 -- 9/28/2004 ARMR 5,300 6,400 2,000 10,500 1,400 -- 12/15/2004 ARMR 5,760 9,090 3,360 14,400 2,910 -- 2/23/2009 ARMR 2,300 510 470 6,600 1,400 840 7/28/2009 ARMR 3,200 420 2,400 11,000 1,400 7802/17/2010 ARMR 3,200 1,000 2,700 12,000 860 710 7/9/2010 ARMR 3,000 330 3,500 12,000 950 1,0003/7/2011 ARMR 1,070 96 341 3,250 674 402 7/21/2011 ARMR 3/21/2012 ARMR 1,600 160 1,100 4,500 900 600 11/17/2012 ARMR 1,600 210 1,600 5,800 520 670 4/8/2015 ARMR 1,500 187 2,010 4,430 355 846 10/19/2015 ARMR 1,730 146 1,720 4,620 543 768 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ. 4. Values in BOLD indicate levels above 2L Groundwater Standards. 5. MTBE = Methyl tertiary butyl ether. 6. All concentrations in micrograms per liter (ug/L). 7. BDL = Below Detection Limit. Not Sampled Not Sampled MW-10 MW-11 2L GW Standard GCL Not sampled; insufficient water TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes4/6/1990 pre-CAP 8.7 BDL 4 17 ---- 10/12/1999 pre-CAP 7/28/2009 pre-CAP 12/15/2000 pre-CAP BDL BDL 1.1 53 9.1 -- 9/4/2002 CAP <5 <5 30 149 <5 -- 11/26/2002 CAP <0.5 <0.5 10.8 50.8 <1 -- 2/28/2003 ARMR 70 <250 180 720 <250 -- 5/16/2003 ARMR <1 <10 19 78 <10 -- 11/10/2003 ARMR 1.1 <5 13 41 <1 -- 9/28/2004 ARMR <1 <5 6.1 15.1 <1 -- 12/15/2004 ARMR 28.7 3.7 24.9 63.7 21.4 -- 2/23/2009 ARMR <0.2 <0.27 0.91 0.4 <0.38 6 7/28/2009 ARMR <0.2 <0.27 4.4 <0.4 <0.38 8 2/17/2010 ARMR 0.79 4.5 3.4 5.4 <0.12 9.5 7/9/2010 ARMR 2 <0.053 <0.1 0.8 <0.12 9.8 3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 0.32J <1.5 <0.5 4.9 3/21/2012 ARMR <0.2 <0.2 1.2 <0.3 <0.2 <0.2 11/18/2012 ARMR <0.3 <0.2 0.92 <0.6 <0.2 <0.5 4/8/2015 ARMR <0.3 <0.2 0.22 <0.6 <0.2 2.8 10/19/2015 ARMR <0.25 <0.25 <0.25 <0.75 <0.25 <1.0 4/6/1990 pre-CAP 36 1,200 580 3,500 ---- 10/12/1999 pre-CAP 290 70 140 BDL 84 -- 12/15/2000 pre-CAP 680 130 300 310 170 -- 9/4/2002 CAP 850 240 300 320 <10 -- 11/26/2002 CAP 103.4 13.7 123.7 35.4 22.1 -- 2/28/2003 ARMR 100 <50 99 39 <50 -- 5/16/2003 ARMR 79 33 58 52 <5 -- 11/10/2003 ARMR 52 17 66 17.9 <1 -- 9/28/2004 ARMR 27 <50 39 <30 <10 -- 12/15/2004 ARMR 41.7 3.3 55.9 5.6 17.7 -- 2/23/2009 ARMR 13 1 42 8.3 5.1 30 7/28/2009 ARMR 80 4 57 12 20 40 2/17/2010 ARMR 15 3.3 33 27 9.7 27 7/9/2010 ARMR 210 66 150 110 41 100 3/7/2011 ARMR 23.8 0.8 16 2.97 23.5 24.6 7/21/2011 ARMR 7 1.6 19.2 4.34 4.2 17.9 3/21/2012 ARMR 5.1 1.1 19 23.88 11 <0.2 11/18/2012 ARMR 4 0.54 18 8.3 4.1 <0.5 4/8/2015 ARMR 22.5 6.1 27.3 7.1 9.9 20.3 10/19/2015 ARMR 77.1 13.8 52.7 48.5 28.5 40.7 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ. 4. J value denotes estimated concentration by the laboratory. 5. Values in BOLD indicate levels above 2L Groundwater Standards. 6. MTBE = Methyl tertiary butyl ether. 7. All concentrations in micrograms per liter (ug/L). 8. BDL = Below Detection Limit. Not Sampled - Unable to Locate Not Sampled - Unable to Locate MW-12A MW-13 MW-12 2L GW StandardGCL TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes4/6/1990 pre-CAP 9,000 10,000 1,250 9,300 ---- 10/12/1999 pre-CAP 10,000 16,000 2,200 9,900 2,100 -- 12/15/2000 pre-CAP 10,000 23,000 5,300 21,600 BDL -- 9/4/2002 CAP 3,200 8,700 1,800 8,100 <75 -- 11/26/2002 CAP 3,169.4 6,320.2 946.9 4,690.8 <20 -- 2/28/2003 ARMR 4,500 8,700 1,300 6,200 <250 -- 5/16/2003 ARMR 73 100 21 97 12 -- 11/10/2003 ARMR 9,000 13,000 2,600 11,400 1,400 -- 9/28/2004 ARMR 8,000 12,000 2,000 8,700 700 -- 12/15/2004 ARMR 11,300 23,000 3,520 16,100 1,920 -- 2/23/2009 ARMR 950 1,700 650 2,600 56 260 7/28/2009 ARMR 8,300 14,000 2,900 13,000 640 810 2/17/2010 ARMR 5,500 7,500 1,900 7,700 360 470 7/9/2010 ARMR 4,300 5,800 2,200 8,300 350 920 3/7/2011 ARMR 2,450 1,830 1,530 6,340 121 652 7/21/2011 ARMR 2,670 3,180 1,190 4,920 164 507 3/21/2012 ARMR 4,000 5,300 1,700 7,800 280 720 11/18/2012 ARMR 4,100 5,900 2,400 9,100 180 820 4/8/2015 ARMR 3,400 1,740 2,200 4,510 399 888 10/19/2015 ARMR 1,910 739 1,770 4,060 116 808 5/4/1990 pre-CAP 3.3 6.2 1.4 0.56 ---- 10/12/1999 pre-CAP BDL BDL BDL BDL BDL -- 12/15/2000 pre-CAP BDL BDL BDL BDL BDL -- 9/4/2002 CAP <1 <1 <1 <3 <1 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR <1 <5 <1 <3 <5 -- 11/10/2003 ARMR <1 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 2/17/2010 ARMR <0.05 0.59 <0.1 1 <0.12 <0.086 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086 3/7/2011 ARMR <0.5 0.61 <0.5 <1.5 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2 11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 0.54 10/19/2015 ARMR <0.25 <0.25 <0.25 <0.75 <0.25 <1.0 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ.4. Values in BOLD indicate levels above 2L Groundwater Standards. 5. MTBE = Methyl tertiary butyl ether. 6. All concentrations in micrograms per liter (ug/L). 7. BDL = Below Detection Limit. MW-14 MW-15 2L GW Standard GCL TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/15/2000 pre-CAP 560 800 510 1,800 BDL -- 9/4/2002 CAP 20 74 480 1,140 <15 -- 11/26/2002 CAP <0.5 <0.5 17.1 56.3 <1 -- 2/28/2003 ARMR <5 <25 23 56.2 <25 -- 5/16/2003 ARMR 6 7.4 3.6 8.4 <5 -- 11/10/2003 ARMR 240 490 250 880 <10 -- 9/28/2004 ARMR 14 22 11 31 1.7 -- 12/15/2004 ARMR 12.9 15.3 4.9 10.2 4.4 -- 2/23/2009 ARMR 7/28/2009 ARMR 2/17/2010 ARMR 3/7/2011 ARMR 7/21/2011 ARMR 3/21/2012 ARMR 12/15/2000 pre-CAP 14,000 25,000 3,300 15,100 BDL -- 9/4/2002 CAP 9,400 27,000 3,200 14,800 <200 -- 11/26/2002 CAP 4,280 20,720 2,700 13,140 <5 -- 2/28/2003 ARMR 6,000 16,000 2,200 10,000 <250 -- 5/16/2003 ARMR 3,800 9,600 1,600 6,500 <50 -- 11/10/2003 ARMR 6,200 15,000 2,000 8,800 <25 -- 9/28/2004 ARMR 5,800 1,400 1,800 8,100 <200 -- 12/15/2004 ARMR 6,770 21,800 3,400 14,700 1,100 -- 2/23/2009 ARMR 5,000 19,000 3,100 14,000 <190 1,100 7/28/2009 ARMR 5,100 26,000 3,200 16,000 <190 1,200 2/17/2010 ARMR 4,800 15,000 2,400 12,000 <24 810 7/9/2010 ARMR 3,600 17,000 2,300 11,000 <24 780 3/7/2011 ARMR 3,900 17,900 3,140 14,380 84.2 1,110 7/21/2011 ARMR 3/21/2012 ARMR 1,600 6,600 2,100 8,200 39 2,700 11/18/2012 ARMR 2,400 13,000 2,400 10,600 25 1,100 4/8/2015 ARMR 794 6,520 1,740 5,980 16.4 1,070 10/19/2015 ARMR 898 14,700 4,820 21,680 <25.0 3,160 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ.4. Values in BOLD indicate levels above 2L Groundwater Standards. 5. MTBE = Methyl tertiary butyl ether. 6. All concentrations in micrograms per liter (ug/L). 7. BDL = Below Detection Limit. Not Sampled Not Sampled - Paved Over Not Sampled Not Sampled Not Sampled Not Sampled Not sampled; blockage at 21 ft MW-16 MW-17 2L GW Standard GCL TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes8/16/2001 pre-CAP 810 8,100 630 2,870 140 -- 9/4/2002 CAP 63 370 50 158 <5 -- 11/26/2002 CAP 56.9 157.3 117.8 237.4 <5 -- 2/28/2003 ARMR 2,100 19,000 1,300 5,900 270 -- 5/16/2003 ARMR 1,600 3,900 430 2,000 130 -- 11/10/2003 ARMR 72 40 8.8 21.8 17 -- 9/28/2004 ARMR 930 7,700 810 3,900 230 -- 12/15/2004 ARMR 7.3 15.6 <1 18 7.9 -- 2/23/2009 ARMR 550 5,100 900 3,700 230 180 7/28/2009 ARMR 3,700 20,000 1,700 8,000 600 110 2/17/2010 ARMR 1,600 30,000 2,700 13,000 3,800 1,400 7/9/2010 ARMR 3,000 17,000 1,800 8,800 670 510 3/7/2011 ARMR 88 550 165 730 18.7 36.5 7/21/2011 ARMR 2,720 11,800 1,240 5,440 294 269 3/21/2012 ARMR 26 84 99 300 1.9 20 11/18/2012 ARMR 640 2,900 1,400 4,900 20 330 4/8/2015 ARMR 2570 9840 1830 7980 34.5 696 10/19/2015 ARMR 77.3 157 127 401 2.1 29.7 8/16/2001 pre-CAP BDL 1.5 BDL BDL BDL -- 9/4/2002 CAP <1 <1 <1 <3 <1 -- 11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR <1 <5 <1 <3 <5 -- 11/10/2003 ARMR 1.5 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39 2/17/2010 ARMR 0.47 3.2 0.9 3.1 <0.12 <0.086 7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086 3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2 7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5 3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2 11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5 10/19/2015 ARMR <0.25 <0.25 <0.25 <0.75 <0.25 <1.0 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ.4. Values in BOLD indicate levels above 2L Groundwater Standards. 5. MTBE = Methyl tertiary butyl ether. 6. All concentrations in micrograms per liter (ug/L). 7. BDL = Below Detection Limit. 2L GW Standard GCL MW-18 MW-19 TABLE 6 HISTORICAL GROUNDWATER ANALYTICAL DATA PANTRY #3079 5102 DORTCHES BOULEVARDROCKY MOUNT, NASH COUNTY, NORTH CAROLINA NCDEQ FACILITY ID NO. 0-022631 NCDEQ INCIDENT NO. 4028 Analytical Methods:EPA METHOD 6010D or 6200B WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes2/23/2009 ARMR 50 38 23 200 <1.9 210 7/28/2009 ARMR 110 110 490 560 <3.8 3602/17/2010 ARMR 62 110 260 610 <0.6 120 7/9/2010 ARMR 110 140 330 860 <24 2503/7/2011 ARMR 28 11 12 172 <0.5 55 7/21/2011 ARMR 38.5 26.8 58.8 216.8 3.1 75.6 3/21/2012 ARMR 73 81 240 470 <1 230 11/18/2012 ARMR 4/8/2015 ARMR 10/19/2015 ARMR 2/23/2009 ARMR 3,200 6,900 1,500 2,500 1,600 5207/28/2009 ARMR 1,500 1,100 650 440 1,300 210 2/17/2010 ARMR 920 1,800 700 730 1,600 150 7/9/2010 ARMR 1,500 6,100 980 2,300 1,700 270 3/7/2011 ARMR 116 216 44.9 131.9 595 12.8 7/21/2011 ARMR 353 125 82.1 182.6 797 37.2 3/21/2012 ARMR 830 3,100 570 1,920 970 180 11/18/2012 ARMR 4/8/2015 ARMR 10/19/2015 ARMR 2/23/2009 ARMR 93 4.7 420 <4 480 300 3/13/2009 ARMR 68 3 290 <4 370 170 7/28/2009 ARMR 100 35 470 8.4 510 290 2/17/2010 ARMR 59 75 460 99 240 230 7/9/2010 ARMR 120 52 580 130 490 340 3/7/2011 ARMR 7.9 2 58.9 8 114 26.3 7/21/2011 ARMR 61.4 48.8 220 160.6 177 97.7 3/21/2012 ARMR 11/18/2012 ARMR 4/8/2015 ARMR 10/19/2015 ARMR 9/4/2002 CAP 29,000 34,000 2,800 16,200 160,000 -- 11/26/2002 CAP 2/28/2003 ARMR 2/23/2009 ARMR 2/17/2010 ARMR 3/21/2012 ARMR 11,000 22,000 3,800 66,000 130,000 6,900 4/8/2015 ARMR 10/19/2015 ARMR 8/16/2001 pre-CAP BDL BDL BDL BDL BDL -- 9/4/2002 pre-CAP <1 <1 <1 <3 <1 -- 11/26/2002 pre-CAP <0.5 <0.5 <0.5 <1.5 <1 -- 2/28/2003 ARMR <1 <5 <1 <3 <5 -- 5/16/2003 ARMR <1 <5 <1 <3 <5 -- 11/10/2003 ARMR <1 <5 <1 <3 <1 -- 7/21/2004 ARMR <1 <5 <1 <3 <1 -- 9/28/2004 ARMR <1 <5 <1 <3 <1 -- 12/15/2004 ARMR <1 <1 <1 <3 <1 -- 2/23/2009 ARMR 1 600 600 500 20 6 5,000 260,000 84,500 85,500 20,000 6,000 Notes: 1. "<" or ND = None detected above method detection limit. 2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard. 3. GCL = Gross Contaminant Level established by NCDEQ. 4. Values in BOLD indicate levels above 2L Groundwater Standards. 5. MTBE = Methyl tertiary butyl ether. 6. All concentrations in micrograms per liter (ug/L). 7. BDL = Below Detection Limit. Not Sampled Not Sampled - Unable to Locate Not Sampled - Unable to Locate Not Sampled - Unable to Locate Not Sampled - Unable to Locate 2L GW Standard GCL Not Sampled - Unable to Locate Not Sampled - Unable to Locate Not Sampled Not Sampled Not Sampled Not Sampled RW-1 MW-22 Not Sampled - Unable to Locate Not Sampled Not Sampled - Unable to Locate Not Sampled MW-21 MW-20 WW-1 Not Sampled - Unable to Locate Not Sampled - Unable to Locate FIGURES APPENDIX A MMPE SUMMARY REPORT AND DISPOSAL MANIFEST Event #1 Page 1 AGGRESSIVE FLUID VAPOR RECOVERY EVENTSite Name:Pantry #3079Incident Number:Average depth to groundwater (in feet):Soil Type in the Saturated Zone:Average Hydraulic Conductivity (if known):Wells (diameter in inches) used for AFVR:2"(1well)Blower specifications:410 CFMDate of Event:9/14/2015Total gallons of water recovered (Storage tank) ( gallons):1,547 NAPL recovered (measured storage tank) ( gallons):N/A Time of beginning of test:12:00 pm Average gallons per hr 16.11gph DRY STANDARD CUBIC FEET PER MINUTE (DSCFM) AIR FLOW CALCULATIONS (Qstd) Date Time Vacuum Velocity Pipe ID Temp Rel Humid lb. Water @ Qstd Bws (inches of Hg)(ft/min)(in)(°F)(%)lb. dry air *(flow) 9/14/2015 12:00 prior to starting 60 9/14/2015 13:00 22 680 2 138 100 0.015 13 0.025 9/15/2015 12:00 23 720 2 142 100 0.015 13 0.025 9/16/2015 12:00 23 702 2 140 100 0.015 13 0.025 9/17/2015 12:00 23 718 2 139 100 0.015 13 0.025 9/18/2015 12:00 22 690 2 142 100 0.015 13 0.025 NOTES * from psychrometric chart at http://birger.maskin.ntnu.no/kkt/grzifk/java/PsychProJava.html Bws = Water vapor percent by volume Bwsw = Pounds of water per pound of dry air, derived from the Psychrometric chart (temp Vs relative humidity) Qstd = Flow at DSCFM Vacuum = The level of vacuum being applied should be recorded from the vacuum truck tank (inches of Hg) Velocity = The rate at which air flows is measured at the blower discharge piping (anemometer or pitot tube) Pipe ID = The inside diameter of the blower discharge piping (from the vacuum truck) Temperature = The temperature of the air stream exiting the blower discharge piping (dry bulb temp., in deg.°F) Relative humidity = The % relative humidity of the air stream exiting the blower discharge piping EQUATION Qstd = (1-Bws) * velocity * (PI * (diameter/24)^2) * (528/°R[Temp + 460]) Eastern Environmental Management, LLC.(EEM) is pleased to provide this summary report documenting Mobile Multi- Phase Vacuum Extraction (MMPE) operation for the above referenced project. EEM utilized an Dekker Titan Series liquid ring Multi-phase Extractor with effluent pump, powered by a Baldor 60KW self-contained generator for the performance of this event. The event was conducted from 9-14-2015 to 9-18-2015. The total number of hours of unit operation was 96 hours. Liquids disposal manifests and emissions calculations are attached along with field data used in the emissions calculations. Tables with depth-to-water and depth-to-product information are included. Event #1 Page 2 EMISSION CALCULATIONS Elapsed Time Flow PPM measured PPMd PPMc Cc:m Cc PMRc PMRg (min)(DSCFM)(ppm)(mg/dsm3)(lb/dscf)(lb/elap. time)(lb/elap. time) 1440 13 441 452.2 441 220 0.0000137 0.25 0.29 2880 13 318 326.1 318 159 0.0000099 0.38 0.44 4320 13 318 326.1 318 159 0.0000099 0.56 0.65 5760 13 180 184.6 180 90 0.0000056 0.43 0.50 7200 13 171 175.4 171 85 0.0000053 0.49 0.57 Average:13.14 285.6 292.88 285.6 142.50 8.896E-06 0.425 0.49 Total emissions in pounds 2.46 Total gasoline emissions in gallons 0.39INPUTSK (calib gas)1 NOTES PPMw (measured) = Actual measurements (ppm) taken with a OVA or TVA at the blower discharge piping PPMd = dry concentration PPMc = volumetric concentration of VOCs as carbon, dry at STP K = Number of carbons in calibration gas: (Methane K = 1, or Propane K = 3, or Hexane K = 6) Cc:m = mg/dsm3, mass concentration of VOC emissions as carbon Mc = 12.01 mg/mg-mol, molecular weight of carbon K3 = 24.07 dsm^3/1E6 mg-mole, mass to volume conversion factor at STP Cc = lb/dcsf, mass concentration of gasoline emission, dry basis at STP PMRc = lb/hr, pollutant mass removal rate of carbon emission PMRg = lb/hr, pollutant mass removal rate of gasoline emission Mg = 103 mg/mg-mol, molecular wt. of gasoline (may vary depending on constituent) Mcg = 89 mg/mg-mol, wt. of carbon in gasoline molecule EQUATIONS PPMd = PPMw measured / 1-Bws PPMc = PPMd * K Cc:m = PPMc (Mc/K3) Cc = Cg:m * 62.43E-09 lb-m^3/mg-ft^3 PMRc = Cc (Qstd) (elapsed time between field measurements) PMRg = PMRc (Mg/Mcg) Event #1 Page 3 APPENDIX B LABORATORY ANALYTICAL REPORT AND CHAIN-OF-CUSTODY DOCUMENTS #=CL# October 29, 2015 LIMS USE: FR - MAUREEN JACKSON LIMS OBJECT ID: 92272667 92272667 Project: Pace Project No.: RE: Maureen Jackson Cardno AtC 2725 E. Millbrook Road Suite 121 Raleigh, NC 27604 PANTRY 3079 45.42017.3079 Dear Maureen Jackson: Enclosed are the analytical results for sample(s) received by the laboratory on October 20, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Godwin kevin.godwin@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 64 #=CP# CERTIFICATIONS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84 West Virginia Certification #: 357Virginia/VELAP Certification #: 460221 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 64 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Lab ID Sample ID Matrix Date Collected Date Received 92272667001 MW-1 Water 10/19/15 14:50 10/20/15 15:00 92272667002 MW-2 Water 10/19/15 12:40 10/20/15 15:00 92272667003 MW-3 Water 10/19/15 12:15 10/20/15 15:00 92272667004 MW-7 Water 10/19/15 11:35 10/20/15 15:00 92272667005 MW-8 Water 10/19/15 13:35 10/20/15 15:00 92272667006 MW-9 Water 10/19/15 16:55 10/20/15 15:00 92272667007 MW-10 Water 10/19/15 16:15 10/20/15 15:00 92272667008 MW-11 Water 10/19/15 15:40 10/20/15 15:00 92272667009 MW-12 Water 10/19/15 19:00 10/20/15 15:00 92272667010 MW-13 Water 10/19/15 17:45 10/20/15 15:00 92272667011 MW-14 Water 10/19/15 18:20 10/20/15 15:00 92272667012 MW-15 Water 10/19/15 14:10 10/20/15 15:00 92272667013 MW-17 Water 10/19/15 10:45 10/20/15 15:00 92272667014 MW-18 Water 10/19/15 10:05 10/20/15 15:00 92272667015 MW-19 Water 10/19/15 09:15 10/20/15 15:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 64 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92272667001 MW-1 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667002 MW-2 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667003 MW-3 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667004 MW-7 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667005 MW-8 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667006 MW-9 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667007 MW-10 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667008 MW-11 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667009 MW-12 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667010 MW-13 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667011 MW-14 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667012 MW-15 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667013 MW-17 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667014 MW-18 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH 92272667015 MW-19 EPA 6010 1 PASI-ACDF SM 6200B 63 PASI-CCAH REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 64 #=HO# SUMMARY OF DETECTION Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Parameters AnalyzedResult Lab Sample ID Report Limit QualifiersUnitsMethod Client Sample ID 92272667001 MW-1 Lead 58.6 ug/L 10/27/15 03:445.0EPA 6010 Benzene 6250 ug/L 10/28/15 13:34100SM 6200B 1,2-Dichloroethane 134 ug/L 10/24/15 20:1812.5SM 6200B Ethylbenzene 3610 ug/L 10/24/15 20:1812.5SM 6200B Isopropylbenzene (Cumene)212 ug/L 10/24/15 20:1812.5SM 6200B Methyl-tert-butyl ether 5060 ug/L 10/28/15 13:34100SM 6200B Naphthalene 2220 ug/L 10/24/15 20:1850.0SM 6200B n-Propylbenzene 577 ug/L 10/24/15 20:1812.5SM 6200B Styrene 60.1 ug/L 10/24/15 20:1812.5SM 6200B Toluene 9320 ug/L 10/28/15 13:34100SM 6200B 1,2,4-Trimethylbenzene 2800 ug/L 10/28/15 13:34100SM 6200B 1,3,5-Trimethylbenzene 2040 ug/L 10/24/15 20:1812.5SM 6200B m&p-Xylene 5640 ug/L 10/28/15 13:34200SM 6200B o-Xylene 2800 ug/L 10/28/15 13:34100SM 6200B 92272667002 MW-2 Lead 7.3 ug/L 10/27/15 03:475.0EPA 6010 Benzene 0.26J ug/L 10/25/15 20:160.50SM 6200B Methyl-tert-butyl ether 3.8 ug/L 10/25/15 20:160.50SM 6200B 92272667003 MW-3 Lead 19.6 ug/L 10/27/15 03:505.0EPA 6010 Methyl-tert-butyl ether 0.26J ug/L 10/25/15 20:330.50SM 6200B 92272667004 MW-7 Lead 2.5J ug/L 10/28/15 18:115.0EPA 6010 92272667005 MW-8 Bromodichloromethane 1.6 ug/L 10/26/15 03:300.50SM 6200B Chloroform 7.7 ug/L 10/26/15 03:300.50SM 6200B Isopropylbenzene (Cumene)1.9 ug/L 10/26/15 03:300.50SM 6200B Naphthalene 12.6 ug/L 10/26/15 03:302.0SM 6200B n-Propylbenzene 2.2 ug/L 10/26/15 03:300.50SM 6200B Toluene 0.38J ug/L 10/26/15 03:300.50SM 6200B 1,2,4-Trimethylbenzene 74.4 ug/L 10/26/15 03:300.50SM 6200B m&p-Xylene 60.3 ug/L 10/26/15 03:301.0SM 6200B o-Xylene 30.1 ug/L 10/26/15 03:300.50SM 6200B 92272667006 MW-9 Lead 28.9 ug/L 10/28/15 18:235.0EPA 6010 92272667007 MW-10 Lead 91.6 ug/L 10/28/15 18:265.0EPA 6010 92272667008 MW-11 Lead 55.7 ug/L 10/28/15 18:395.0EPA 6010 Benzene 1730 ug/L 10/25/15 00:285.0SM 6200B 1,2-Dichloroethane 9.1 ug/L 10/25/15 00:285.0SM 6200B Ethylbenzene 1720 ug/L 10/25/15 00:285.0SM 6200B Isopropylbenzene (Cumene)77.0 ug/L 10/25/15 00:285.0SM 6200B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 64 #=HO# SUMMARY OF DETECTION Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Parameters AnalyzedResult Lab Sample ID Report Limit QualifiersUnitsMethod Client Sample ID 92272667008 MW-11 Methylene Chloride 10.4J ug/L 10/25/15 00:2820.0SM 6200B Methyl-tert-butyl ether 543 ug/L 10/25/15 00:285.0SM 6200B Naphthalene 768 ug/L 10/25/15 00:2820.0SM 6200B n-Propylbenzene 208 ug/L 10/25/15 00:285.0SM 6200B Styrene 15.4 ug/L 10/25/15 00:285.0SM 6200B Toluene 146 ug/L 10/25/15 00:285.0SM 6200B 1,2,4-Trimethylbenzene 1870 ug/L 10/25/15 00:285.0SM 6200B 1,3,5-Trimethylbenzene 478 ug/L 10/25/15 00:285.0SM 6200B m&p-Xylene 3100 ug/L 10/25/15 00:2810.0SM 6200B o-Xylene 1520 ug/L 10/25/15 00:285.0SM 6200B 92272667009 MW-12 Lead 35.1 ug/L 10/28/15 18:425.0EPA 6010 n-Butylbenzene 3.2 ug/L 10/25/15 02:250.50SM 6200B sec-Butylbenzene 7.4 ug/L 10/25/15 02:250.50SM 6200B Isopropylbenzene (Cumene)4.3 ug/L 10/25/15 02:250.50SM 6200B n-Propylbenzene 13.1 ug/L 10/25/15 02:250.50SM 6200B 1,2,4-Trimethylbenzene 1.5 ug/L 10/25/15 02:250.50SM 6200B 92272667010 MW-13 Lead 654 ug/L 10/28/15 18:455.0EPA 6010 Benzene 77.1 ug/L 10/25/15 02:420.50SM 6200B sec-Butylbenzene 5.7 ug/L 10/25/15 02:420.50SM 6200B 1,2-Dichloroethane 0.78 ug/L 10/25/15 02:420.50SM 6200B Ethylbenzene 52.7 ug/L 10/25/15 02:420.50SM 6200B Isopropylbenzene (Cumene)7.6 ug/L 10/25/15 02:420.50SM 6200B Methyl-tert-butyl ether 28.5 ug/L 10/25/15 02:420.50SM 6200B Naphthalene 40.7 ug/L 10/25/15 02:422.0SM 6200B n-Propylbenzene 17.6 ug/L 10/25/15 02:420.50SM 6200B Toluene 13.8 ug/L 10/25/15 02:420.50SM 6200B 1,2,4-Trimethylbenzene 25.3 ug/L 10/25/15 02:420.50SM 6200B 1,3,5-Trimethylbenzene 8.0 ug/L 10/25/15 02:420.50SM 6200B m&p-Xylene 44.7 ug/L 10/25/15 02:421.0SM 6200B o-Xylene 3.8 ug/L 10/25/15 02:420.50SM 6200B 92272667011 MW-14 Lead 27.4 ug/L 10/28/15 18:485.0EPA 6010 Benzene 1910 ug/L 10/25/15 00:4512.5SM 6200B 1,2-Dichloroethane 13.9 ug/L 10/25/15 00:4512.5SM 6200B Ethylbenzene 1770 ug/L 10/25/15 00:4512.5SM 6200B Isopropylbenzene (Cumene)118 ug/L 10/25/15 00:4512.5SM 6200B Methylene Chloride 26.0J ug/L 10/25/15 00:4550.0SM 6200B Methyl-tert-butyl ether 116 ug/L 10/25/15 00:4512.5SM 6200B Naphthalene 808 ug/L 10/25/15 00:4550.0SM 6200B n-Propylbenzene 378 ug/L 10/25/15 00:4512.5SM 6200B Toluene 739 ug/L 10/25/15 00:4512.5SM 6200B 1,2,4-Trimethylbenzene 2210 ug/L 10/25/15 00:4512.5SM 6200B 1,3,5-Trimethylbenzene 664 ug/L 10/25/15 00:4512.5SM 6200B m&p-Xylene 2860 ug/L 10/25/15 00:4525.0SM 6200B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 64 #=HO# SUMMARY OF DETECTION Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Parameters AnalyzedResult Lab Sample ID Report Limit QualifiersUnitsMethod Client Sample ID 92272667011 MW-14 o-Xylene 1200 ug/L 10/25/15 00:4512.5SM 6200B 92272667013 MW-17 Lead 60.3 ug/L 10/28/15 18:545.0EPA 6010 Benzene 898 ug/L 10/25/15 01:0250.0SM 6200B n-Butylbenzene 779 ug/L 10/25/15 01:0250.0SM 6200B Diisopropyl ether 31.1J ug/L 10/25/15 01:0250.0SM 6200B Ethylbenzene 4820 ug/L 10/25/15 01:0250.0SM 6200B Isopropylbenzene (Cumene)409 ug/L 10/25/15 01:0250.0SM 6200B Naphthalene 3160 ug/L 10/25/15 01:02200SM 6200B n-Propylbenzene 1400 ug/L 10/25/15 01:0250.0SM 6200B Styrene 93.4 ug/L 10/25/15 01:0250.0SM 6200B Toluene 14700 ug/L 10/25/15 01:0250.0SM 6200B 1,2,4-Trimethylbenzene 9820 ug/L 10/25/15 01:0250.0SM 6200B 1,3,5-Trimethylbenzene 2740 ug/L 10/25/15 01:0250.0SM 6200B m&p-Xylene 14900 ug/L 10/25/15 01:02100SM 6200B o-Xylene 6780 ug/L 10/25/15 01:0250.0SM 6200B 92272667014 MW-18 Lead 10.6 ug/L 10/28/15 18:575.0EPA 6010 Benzene 77.3 ug/L 10/25/15 03:160.50SM 6200B 1,2-Dichloroethane 0.31J ug/L 10/25/15 03:160.50SM 6200B Diisopropyl ether 9.3 ug/L 10/25/15 03:160.50SM 6200B Ethylbenzene 127 ug/L 10/25/15 03:160.50SM 6200B Isopropylbenzene (Cumene)5.4 ug/L 10/25/15 03:160.50SM 6200B Methyl-tert-butyl ether 2.1 ug/L 10/25/15 03:160.50SM 6200B Naphthalene 29.7 ug/L 10/25/15 03:162.0SM 6200B n-Propylbenzene 11.2 ug/L 10/25/15 03:160.50SM 6200B Styrene 4.2 ug/L 10/25/15 03:160.50SM 6200B Toluene 157 ug/L 10/25/15 13:021.2SM 6200B 1,2,4-Trimethylbenzene 69.2 ug/L 10/25/15 03:160.50SM 6200B 1,3,5-Trimethylbenzene 18.0 ug/L 10/25/15 03:160.50SM 6200B m&p-Xylene 253 ug/L 10/25/15 03:161.0SM 6200B o-Xylene 148 ug/L 10/25/15 03:160.50SM 6200B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-1 Lab ID:92272667001 Collected:10/19/15 14:50 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 58.6 ug/L 10/27/15 03:44 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 6250 ug/L 10/28/15 13:34 71-43-210050.0 200 Bromobenzene <6.2 ug/L 10/24/15 20:18 108-86-112.5 6.2 25 Bromochloromethane <6.2 ug/L 10/24/15 20:18 74-97-512.5 6.2 25 Bromodichloromethane <6.2 ug/L 10/24/15 20:18 75-27-412.5 6.2 25 Bromoform <6.2 ug/L 10/24/15 20:18 75-25-212.5 6.2 25 Bromomethane <12.5 ug/L 10/24/15 20:18 74-83-912512.5 25 n-Butylbenzene <6.2 ug/L 10/24/15 20:18 104-51-812.5 6.2 25 sec-Butylbenzene <6.2 ug/L 10/24/15 20:18 135-98-812.5 6.2 25 tert-Butylbenzene <6.2 ug/L 10/24/15 20:18 98-06-612.5 6.2 25 Carbon tetrachloride <6.2 ug/L 10/24/15 20:18 56-23-512.5 6.2 25 Chlorobenzene <6.2 ug/L 10/24/15 20:18 108-90-712.5 6.2 25 Chloroethane <12.5 ug/L 10/24/15 20:18 75-00-325.0 12.5 25 Chloroform <6.2 ug/L 10/24/15 20:18 67-66-312.5 6.2 25 Chloromethane <12.5 ug/L 10/24/15 20:18 74-87-325.0 12.5 25 2-Chlorotoluene <6.2 ug/L 10/24/15 20:18 95-49-812.5 6.2 25 4-Chlorotoluene <6.2 ug/L 10/24/15 20:18 106-43-412.5 6.2 25 1,2-Dibromo-3-chloropropane <12.5 ug/L 10/24/15 20:18 96-12-825.0 12.5 25 Dibromochloromethane <6.2 ug/L 10/24/15 20:18 124-48-112.5 6.2 25 1,2-Dibromoethane (EDB)<6.2 ug/L 10/24/15 20:18 106-93-412.5 6.2 25 Dibromomethane <6.2 ug/L 10/24/15 20:18 74-95-312.5 6.2 25 1,2-Dichlorobenzene <6.2 ug/L 10/24/15 20:18 95-50-112.5 6.2 25 1,3-Dichlorobenzene <6.2 ug/L 10/24/15 20:18 541-73-112.5 6.2 25 1,4-Dichlorobenzene <6.2 ug/L 10/24/15 20:18 106-46-712.5 6.2 25 Dichlorodifluoromethane <6.2 ug/L 10/24/15 20:18 75-71-812.5 6.2 25 1,1-Dichloroethane <6.2 ug/L 10/24/15 20:18 75-34-312.5 6.2 25 1,2-Dichloroethane 134 ug/L 10/24/15 20:18 107-06-212.5 6.2 25 1,1-Dichloroethene <6.2 ug/L 10/24/15 20:18 75-35-412.5 6.2 25 cis-1,2-Dichloroethene <6.2 ug/L 10/24/15 20:18 156-59-212.5 6.2 25 trans-1,2-Dichloroethene <6.2 ug/L 10/24/15 20:18 156-60-512.5 6.2 25 1,2-Dichloropropane <6.2 ug/L 10/24/15 20:18 78-87-512.5 6.2 25 1,3-Dichloropropane <6.2 ug/L 10/24/15 20:18 142-28-912.5 6.2 25 2,2-Dichloropropane <6.2 ug/L 10/24/15 20:18 594-20-712.5 6.2 25 1,1-Dichloropropene <6.2 ug/L 10/24/15 20:18 563-58-612.5 6.2 25 cis-1,3-Dichloropropene <6.2 ug/L 10/24/15 20:18 10061-01-512.5 6.2 25 trans-1,3-Dichloropropene <6.2 ug/L 10/24/15 20:18 10061-02-612.5 6.2 25 Diisopropyl ether <6.2 ug/L 10/24/15 20:18 108-20-312.5 6.2 25 Ethylbenzene 3610 ug/L 10/24/15 20:18 100-41-412.5 6.2 25 Hexachloro-1,3-butadiene <25.0 ug/L 10/24/15 20:18 87-68-350.0 25.0 25 Isopropylbenzene (Cumene)212 ug/L 10/24/15 20:18 98-82-812.5 6.2 25 Methylene Chloride <25.0 ug/L 10/24/15 20:18 75-09-250.0 25.0 25 Methyl-tert-butyl ether 5060 ug/L 10/28/15 13:34 1634-04-410050.0 200 Naphthalene 2220 ug/L 10/24/15 20:18 91-20-350.0 25.0 25 n-Propylbenzene 577 ug/L 10/24/15 20:18 103-65-112.5 6.2 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-1 Lab ID:92272667001 Collected:10/19/15 14:50 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene 60.1 ug/L 10/24/15 20:18 100-42-512.5 6.2 25 1,1,1,2-Tetrachloroethane <6.2 ug/L 10/24/15 20:18 630-20-612.5 6.2 25 1,1,2,2-Tetrachloroethane <6.2 ug/L 10/24/15 20:18 79-34-512.5 6.2 25 Tetrachloroethene <6.2 ug/L 10/24/15 20:18 127-18-412.5 6.2 25 Toluene 9320 ug/L 10/28/15 13:34 108-88-310050.0 200 1,2,3-Trichlorobenzene <25.0 ug/L 10/24/15 20:18 87-61-650.0 25.0 25 1,2,4-Trichlorobenzene <25.0 ug/L 10/24/15 20:18 120-82-150.0 25.0 25 1,1,1-Trichloroethane <6.2 ug/L 10/24/15 20:18 71-55-612.5 6.2 25 1,1,2-Trichloroethane <6.2 ug/L 10/24/15 20:18 79-00-512.5 6.2 25 Trichloroethene <6.2 ug/L 10/24/15 20:18 79-01-612.5 6.2 25 Trichlorofluoromethane <12.5 ug/L 10/24/15 20:18 75-69-425.0 12.5 25 1,2,3-Trichloropropane <6.2 ug/L 10/24/15 20:18 96-18-412.5 6.2 25 1,2,4-Trimethylbenzene 2800 ug/L 10/28/15 13:34 95-63-610050.0 200 1,3,5-Trimethylbenzene 2040 ug/L 10/24/15 20:18 108-67-812.5 6.2 25 Vinyl chloride <6.2 ug/L 10/24/15 20:18 75-01-425.0 6.2 25 m&p-Xylene 5640 ug/L 10/28/15 13:34 179601-23-1200100200 o-Xylene 2800 ug/L 10/28/15 13:34 95-47-610050.0 200 Surrogates 1,2-Dichloroethane-d4 (S)103 %10/24/15 20:18 17060-07-070-130 25 4-Bromofluorobenzene (S)104 %10/24/15 20:18 460-00-470-130 25 Toluene-d8 (S)101 %10/24/15 20:18 2037-26-570-130 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-2 Lab ID:92272667002 Collected:10/19/15 12:40 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 7.3 ug/L 10/27/15 03:47 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 0.26J ug/L 10/25/15 20:16 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 20:16 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 20:16 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 20:16 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 20:16 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 20:16 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 20:16 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 20:16 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 20:16 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 20:16 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 20:16 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 20:16 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 20:16 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 20:16 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 20:16 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 20:16 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 20:16 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 20:16 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 20:16 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 20:16 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 20:16 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 20:16 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 20:16 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 20:16 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 20:16 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 20:16 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 20:16 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 20:16 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 20:16 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 20:16 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 20:16 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 20:16 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 20:16 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 20:16 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 20:16 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 20:16 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 20:16 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 20:16 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.25 ug/L 10/25/15 20:16 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 20:16 75-09-22.0 1.0 1 Methyl-tert-butyl ether 3.8 ug/L 10/25/15 20:16 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 20:16 91-20-32.0 1.0 1 n-Propylbenzene <0.25 ug/L 10/25/15 20:16 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-2 Lab ID:92272667002 Collected:10/19/15 12:40 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 20:16 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 20:16 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 20:16 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 20:16 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 20:16 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 20:16 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 20:16 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 20:16 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 20:16 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 20:16 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 20:16 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 20:16 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.25 ug/L 10/25/15 20:16 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 20:16 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 20:16 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 20:16 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 20:16 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)107 %10/25/15 20:16 17060-07-070-130 1 4-Bromofluorobenzene (S)98 %10/25/15 20:16 460-00-470-130 1 Toluene-d8 (S)100 %10/25/15 20:16 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-3 Lab ID:92272667003 Collected:10/19/15 12:15 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 19.6 ug/L 10/27/15 03:50 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/25/15 20:33 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 20:33 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 20:33 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 20:33 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 20:33 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 20:33 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 20:33 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 20:33 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 20:33 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 20:33 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 20:33 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 20:33 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 20:33 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 20:33 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 20:33 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 20:33 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 20:33 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 20:33 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 20:33 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 20:33 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 20:33 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 20:33 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 20:33 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 20:33 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 20:33 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 20:33 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 20:33 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 20:33 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 20:33 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 20:33 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 20:33 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 20:33 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 20:33 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 20:33 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 20:33 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 20:33 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 20:33 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 20:33 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.25 ug/L 10/25/15 20:33 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 20:33 75-09-22.0 1.0 1 Methyl-tert-butyl ether 0.26J ug/L 10/25/15 20:33 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 20:33 91-20-32.0 1.0 1 n-Propylbenzene <0.25 ug/L 10/25/15 20:33 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-3 Lab ID:92272667003 Collected:10/19/15 12:15 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 20:33 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 20:33 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 20:33 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 20:33 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 20:33 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 20:33 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 20:33 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 20:33 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 20:33 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 20:33 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 20:33 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 20:33 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.25 ug/L 10/25/15 20:33 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 20:33 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 20:33 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 20:33 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 20:33 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)106 %10/25/15 20:33 17060-07-070-130 1 4-Bromofluorobenzene (S)98 %10/25/15 20:33 460-00-470-130 1 Toluene-d8 (S)102 %10/25/15 20:33 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-7 Lab ID:92272667004 Collected:10/19/15 11:35 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 2.5J ug/L 10/28/15 18:11 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/25/15 20:49 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 20:49 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 20:49 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 20:49 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 20:49 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 20:49 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 20:49 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 20:49 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 20:49 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 20:49 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 20:49 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 20:49 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 20:49 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 20:49 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 20:49 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 20:49 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 20:49 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 20:49 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 20:49 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 20:49 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 20:49 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 20:49 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 20:49 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 20:49 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 20:49 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 20:49 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 20:49 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 20:49 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 20:49 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 20:49 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 20:49 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 20:49 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 20:49 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 20:49 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 20:49 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 20:49 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 20:49 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 20:49 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.25 ug/L 10/25/15 20:49 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 20:49 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.25 ug/L 10/25/15 20:49 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 20:49 91-20-32.0 1.0 1 n-Propylbenzene <0.25 ug/L 10/25/15 20:49 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-7 Lab ID:92272667004 Collected:10/19/15 11:35 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 20:49 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 20:49 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 20:49 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 20:49 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 20:49 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 20:49 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 20:49 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 20:49 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 20:49 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 20:49 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 20:49 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 20:49 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.25 ug/L 10/25/15 20:49 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 20:49 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 20:49 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 20:49 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 20:49 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)105 %10/25/15 20:49 17060-07-070-130 1 4-Bromofluorobenzene (S)97 %10/25/15 20:49 460-00-470-130 1 Toluene-d8 (S)101 %10/25/15 20:49 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-8 Lab ID:92272667005 Collected:10/19/15 13:35 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead <2.5 ug/L 10/28/15 18:20 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/26/15 03:30 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/26/15 03:30 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/26/15 03:30 74-97-50.50 0.25 1 Bromodichloromethane 1.6 ug/L 10/26/15 03:30 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/26/15 03:30 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/26/15 03:30 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/26/15 03:30 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/26/15 03:30 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/26/15 03:30 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/26/15 03:30 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/26/15 03:30 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/26/15 03:30 75-00-31.0 0.50 1 Chloroform 7.7 ug/L 10/26/15 03:30 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/26/15 03:30 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/26/15 03:30 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/26/15 03:30 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/26/15 03:30 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/26/15 03:30 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/26/15 03:30 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/26/15 03:30 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/26/15 03:30 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/26/15 03:30 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/26/15 03:30 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/26/15 03:30 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/26/15 03:30 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/26/15 03:30 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/26/15 03:30 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/26/15 03:30 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/26/15 03:30 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/26/15 03:30 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/26/15 03:30 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/26/15 03:30 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/26/15 03:30 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/26/15 03:30 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/26/15 03:30 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/26/15 03:30 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/26/15 03:30 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/26/15 03:30 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)1.9 ug/L 10/26/15 03:30 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/26/15 03:30 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.25 ug/L 10/26/15 03:30 1634-04-40.50 0.25 1 Naphthalene 12.6 ug/L 10/26/15 03:30 91-20-32.0 1.0 1 n-Propylbenzene 2.2 ug/L 10/26/15 03:30 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-8 Lab ID:92272667005 Collected:10/19/15 13:35 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/26/15 03:30 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/26/15 03:30 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/26/15 03:30 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/26/15 03:30 127-18-40.50 0.25 1 Toluene 0.38J ug/L 10/26/15 03:30 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/26/15 03:30 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/26/15 03:30 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/26/15 03:30 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/26/15 03:30 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/26/15 03:30 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/26/15 03:30 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/26/15 03:30 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 74.4 ug/L 10/26/15 03:30 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/26/15 03:30 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/26/15 03:30 75-01-41.0 0.25 1 m&p-Xylene 60.3 ug/L 10/26/15 03:30 179601-23-11.0 0.50 1 o-Xylene 30.1 ug/L 10/26/15 03:30 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)107 %10/26/15 03:30 17060-07-070-130 1 4-Bromofluorobenzene (S)98 %10/26/15 03:30 460-00-470-130 1 Toluene-d8 (S)99 %10/26/15 03:30 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-9 Lab ID:92272667006 Collected:10/19/15 16:55 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 28.9 ug/L 10/28/15 18:23 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/25/15 01:52 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 01:52 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 01:52 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 01:52 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 01:52 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 01:52 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 01:52 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 01:52 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 01:52 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 01:52 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 01:52 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 01:52 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 01:52 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 01:52 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 01:52 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 01:52 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 01:52 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 01:52 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 01:52 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 01:52 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 01:52 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 01:52 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 01:52 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 01:52 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 01:52 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 01:52 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 01:52 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 01:52 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 01:52 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 01:52 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 01:52 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 01:52 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 01:52 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 01:52 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 01:52 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 01:52 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 01:52 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 01:52 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.25 ug/L 10/25/15 01:52 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 01:52 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.25 ug/L 10/25/15 01:52 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 01:52 91-20-32.0 1.0 1 n-Propylbenzene <0.25 ug/L 10/25/15 01:52 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-9 Lab ID:92272667006 Collected:10/19/15 16:55 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 01:52 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 01:52 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 01:52 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 01:52 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 01:52 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 01:52 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 01:52 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 01:52 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 01:52 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 01:52 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 01:52 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 01:52 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.25 ug/L 10/25/15 01:52 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 01:52 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 01:52 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 01:52 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 01:52 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %10/25/15 01:52 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %10/25/15 01:52 460-00-470-130 1 Toluene-d8 (S)101 %10/25/15 01:52 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-10 Lab ID:92272667007 Collected:10/19/15 16:15 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 91.6 ug/L 10/28/15 18:26 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/25/15 02:09 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 02:09 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 02:09 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 02:09 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 02:09 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 02:09 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 02:09 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 02:09 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 02:09 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 02:09 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 02:09 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 02:09 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 02:09 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 02:09 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 02:09 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 02:09 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 02:09 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 02:09 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 02:09 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 02:09 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 02:09 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 02:09 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 02:09 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 02:09 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 02:09 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 02:09 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 02:09 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:09 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:09 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 02:09 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 02:09 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 02:09 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 02:09 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:09 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:09 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 02:09 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 02:09 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 02:09 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.25 ug/L 10/25/15 02:09 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 02:09 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.25 ug/L 10/25/15 02:09 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 02:09 91-20-32.0 1.0 1 n-Propylbenzene <0.25 ug/L 10/25/15 02:09 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-10 Lab ID:92272667007 Collected:10/19/15 16:15 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 02:09 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:09 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:09 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 02:09 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 02:09 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 02:09 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 02:09 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 02:09 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 02:09 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 02:09 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 02:09 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 02:09 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.25 ug/L 10/25/15 02:09 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 02:09 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 02:09 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 02:09 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 02:09 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %10/25/15 02:09 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %10/25/15 02:09 460-00-470-130 1 Toluene-d8 (S)100 %10/25/15 02:09 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-11 Lab ID:92272667008 Collected:10/19/15 15:40 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 55.7 ug/L 10/28/15 18:39 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 1730 ug/L 10/25/15 00:28 71-43-25.0 2.5 10 Bromobenzene <2.5 ug/L 10/25/15 00:28 108-86-15.0 2.5 10 Bromochloromethane <2.5 ug/L 10/25/15 00:28 74-97-55.0 2.5 10 Bromodichloromethane <2.5 ug/L 10/25/15 00:28 75-27-45.0 2.5 10 Bromoform <2.5 ug/L 10/25/15 00:28 75-25-25.0 2.5 10 Bromomethane <5.0 ug/L 10/25/15 00:28 74-83-950.0 5.0 10 n-Butylbenzene <2.5 ug/L 10/25/15 00:28 104-51-85.0 2.5 10 sec-Butylbenzene <2.5 ug/L 10/25/15 00:28 135-98-85.0 2.5 10 tert-Butylbenzene <2.5 ug/L 10/25/15 00:28 98-06-65.0 2.5 10 Carbon tetrachloride <2.5 ug/L 10/25/15 00:28 56-23-55.0 2.5 10 Chlorobenzene <2.5 ug/L 10/25/15 00:28 108-90-75.0 2.5 10 Chloroethane <5.0 ug/L 10/25/15 00:28 75-00-310.0 5.0 10 Chloroform <2.5 ug/L 10/25/15 00:28 67-66-35.0 2.5 10 Chloromethane <5.0 ug/L 10/25/15 00:28 74-87-310.0 5.0 10 2-Chlorotoluene <2.5 ug/L 10/25/15 00:28 95-49-85.0 2.5 10 4-Chlorotoluene <2.5 ug/L 10/25/15 00:28 106-43-45.0 2.5 10 1,2-Dibromo-3-chloropropane <5.0 ug/L 10/25/15 00:28 96-12-810.0 5.0 10 Dibromochloromethane <2.5 ug/L 10/25/15 00:28 124-48-15.0 2.5 10 1,2-Dibromoethane (EDB)<2.5 ug/L 10/25/15 00:28 106-93-45.0 2.5 10 Dibromomethane <2.5 ug/L 10/25/15 00:28 74-95-35.0 2.5 10 1,2-Dichlorobenzene <2.5 ug/L 10/25/15 00:28 95-50-15.0 2.5 10 1,3-Dichlorobenzene <2.5 ug/L 10/25/15 00:28 541-73-15.0 2.5 10 1,4-Dichlorobenzene <2.5 ug/L 10/25/15 00:28 106-46-75.0 2.5 10 Dichlorodifluoromethane <2.5 ug/L 10/25/15 00:28 75-71-85.0 2.5 10 1,1-Dichloroethane <2.5 ug/L 10/25/15 00:28 75-34-35.0 2.5 10 1,2-Dichloroethane 9.1 ug/L 10/25/15 00:28 107-06-25.0 2.5 10 1,1-Dichloroethene <2.5 ug/L 10/25/15 00:28 75-35-45.0 2.5 10 cis-1,2-Dichloroethene <2.5 ug/L 10/25/15 00:28 156-59-25.0 2.5 10 trans-1,2-Dichloroethene <2.5 ug/L 10/25/15 00:28 156-60-55.0 2.5 10 1,2-Dichloropropane <2.5 ug/L 10/25/15 00:28 78-87-55.0 2.5 10 1,3-Dichloropropane <2.5 ug/L 10/25/15 00:28 142-28-95.0 2.5 10 2,2-Dichloropropane <2.5 ug/L 10/25/15 00:28 594-20-75.0 2.5 10 1,1-Dichloropropene <2.5 ug/L 10/25/15 00:28 563-58-65.0 2.5 10 cis-1,3-Dichloropropene <2.5 ug/L 10/25/15 00:28 10061-01-55.0 2.5 10 trans-1,3-Dichloropropene <2.5 ug/L 10/25/15 00:28 10061-02-65.0 2.5 10 Diisopropyl ether <2.5 ug/L 10/25/15 00:28 108-20-35.0 2.5 10 Ethylbenzene 1720 ug/L 10/25/15 00:28 100-41-45.0 2.5 10 Hexachloro-1,3-butadiene <10.0 ug/L 10/25/15 00:28 87-68-320.0 10.0 10 Isopropylbenzene (Cumene)77.0 ug/L 10/25/15 00:28 98-82-85.0 2.5 10 Methylene Chloride 10.4J ug/L 10/25/15 00:28 75-09-220.0 10.0 10 Methyl-tert-butyl ether 543 ug/L 10/25/15 00:28 1634-04-45.0 2.5 10 Naphthalene 768 ug/L 10/25/15 00:28 91-20-320.0 10.0 10 n-Propylbenzene 208 ug/L 10/25/15 00:28 103-65-15.0 2.5 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-11 Lab ID:92272667008 Collected:10/19/15 15:40 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene 15.4 ug/L 10/25/15 00:28 100-42-55.0 2.5 10 1,1,1,2-Tetrachloroethane <2.5 ug/L 10/25/15 00:28 630-20-65.0 2.5 10 1,1,2,2-Tetrachloroethane <2.5 ug/L 10/25/15 00:28 79-34-55.0 2.5 10 Tetrachloroethene <2.5 ug/L 10/25/15 00:28 127-18-45.0 2.5 10 Toluene 146 ug/L 10/25/15 00:28 108-88-35.0 2.5 10 1,2,3-Trichlorobenzene <10.0 ug/L 10/25/15 00:28 87-61-620.0 10.0 10 1,2,4-Trichlorobenzene <10.0 ug/L 10/25/15 00:28 120-82-120.0 10.0 10 1,1,1-Trichloroethane <2.5 ug/L 10/25/15 00:28 71-55-65.0 2.5 10 1,1,2-Trichloroethane <2.5 ug/L 10/25/15 00:28 79-00-55.0 2.5 10 Trichloroethene <2.5 ug/L 10/25/15 00:28 79-01-65.0 2.5 10 Trichlorofluoromethane <5.0 ug/L 10/25/15 00:28 75-69-410.0 5.0 10 1,2,3-Trichloropropane <2.5 ug/L 10/25/15 00:28 96-18-45.0 2.5 10 1,2,4-Trimethylbenzene 1870 ug/L 10/25/15 00:28 95-63-65.0 2.5 10 1,3,5-Trimethylbenzene 478 ug/L 10/25/15 00:28 108-67-85.0 2.5 10 Vinyl chloride <2.5 ug/L 10/25/15 00:28 75-01-410.0 2.5 10 m&p-Xylene 3100 ug/L 10/25/15 00:28 179601-23-110.0 5.0 10 o-Xylene 1520 ug/L 10/25/15 00:28 95-47-65.0 2.5 10 Surrogates 1,2-Dichloroethane-d4 (S)102 %10/25/15 00:28 17060-07-070-130 10 4-Bromofluorobenzene (S)102 %10/25/15 00:28 460-00-470-130 10 Toluene-d8 (S)99 %10/25/15 00:28 2037-26-570-130 10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-12 Lab ID:92272667009 Collected:10/19/15 19:00 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 35.1 ug/L 10/28/15 18:42 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/25/15 02:25 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 02:25 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 02:25 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 02:25 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 02:25 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 02:25 74-83-95.0 0.50 1 n-Butylbenzene 3.2 ug/L 10/25/15 02:25 104-51-80.50 0.25 1 sec-Butylbenzene 7.4 ug/L 10/25/15 02:25 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 02:25 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 02:25 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 02:25 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 02:25 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 02:25 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 02:25 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 02:25 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 02:25 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 02:25 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 02:25 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 02:25 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 02:25 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 02:25 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 02:25 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 02:25 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 02:25 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 02:25 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 02:25 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 02:25 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:25 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:25 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 02:25 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 02:25 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 02:25 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 02:25 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:25 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:25 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 02:25 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 02:25 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 02:25 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)4.3 ug/L 10/25/15 02:25 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 02:25 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.25 ug/L 10/25/15 02:25 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 02:25 91-20-32.0 1.0 1 n-Propylbenzene 13.1 ug/L 10/25/15 02:25 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-12 Lab ID:92272667009 Collected:10/19/15 19:00 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 02:25 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:25 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:25 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 02:25 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 02:25 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 02:25 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 02:25 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 02:25 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 02:25 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 02:25 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 02:25 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 02:25 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 1.5 ug/L 10/25/15 02:25 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 02:25 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 02:25 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 02:25 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 02:25 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %10/25/15 02:25 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %10/25/15 02:25 460-00-470-130 1 Toluene-d8 (S)101 %10/25/15 02:25 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-13 Lab ID:92272667010 Collected:10/19/15 17:45 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 654 ug/L 10/28/15 18:45 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 77.1 ug/L 10/25/15 02:42 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 02:42 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 02:42 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 02:42 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 02:42 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 02:42 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 02:42 104-51-80.50 0.25 1 sec-Butylbenzene 5.7 ug/L 10/25/15 02:42 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 02:42 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 02:42 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 02:42 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 02:42 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 02:42 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 02:42 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 02:42 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 02:42 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 02:42 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 02:42 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 02:42 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 02:42 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 02:42 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 02:42 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 02:42 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 02:42 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 02:42 75-34-30.50 0.25 1 1,2-Dichloroethane 0.78 ug/L 10/25/15 02:42 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 02:42 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:42 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:42 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 02:42 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 02:42 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 02:42 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 02:42 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:42 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:42 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 02:42 108-20-30.50 0.25 1 Ethylbenzene 52.7 ug/L 10/25/15 02:42 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 02:42 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)7.6 ug/L 10/25/15 02:42 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 02:42 75-09-22.0 1.0 1 Methyl-tert-butyl ether 28.5 ug/L 10/25/15 02:42 1634-04-40.50 0.25 1 Naphthalene 40.7 ug/L 10/25/15 02:42 91-20-32.0 1.0 1 n-Propylbenzene 17.6 ug/L 10/25/15 02:42 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-13 Lab ID:92272667010 Collected:10/19/15 17:45 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 02:42 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:42 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:42 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 02:42 127-18-40.50 0.25 1 Toluene 13.8 ug/L 10/25/15 02:42 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 02:42 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 02:42 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 02:42 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 02:42 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 02:42 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 02:42 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 02:42 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 25.3 ug/L 10/25/15 02:42 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene 8.0 ug/L 10/25/15 02:42 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 02:42 75-01-41.0 0.25 1 m&p-Xylene 44.7 ug/L 10/25/15 02:42 179601-23-11.0 0.50 1 o-Xylene 3.8 ug/L 10/25/15 02:42 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %10/25/15 02:42 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %10/25/15 02:42 460-00-470-130 1 Toluene-d8 (S)100 %10/25/15 02:42 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-14 Lab ID:92272667011 Collected:10/19/15 18:20 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 27.4 ug/L 10/28/15 18:48 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 1910 ug/L 10/25/15 00:45 71-43-212.5 6.2 25 Bromobenzene <6.2 ug/L 10/25/15 00:45 108-86-112.5 6.2 25 Bromochloromethane <6.2 ug/L 10/25/15 00:45 74-97-512.5 6.2 25 Bromodichloromethane <6.2 ug/L 10/25/15 00:45 75-27-412.5 6.2 25 Bromoform <6.2 ug/L 10/25/15 00:45 75-25-212.5 6.2 25 Bromomethane <12.5 ug/L 10/25/15 00:45 74-83-912512.5 25 n-Butylbenzene <6.2 ug/L 10/25/15 00:45 104-51-812.5 6.2 25 sec-Butylbenzene <6.2 ug/L 10/25/15 00:45 135-98-812.5 6.2 25 tert-Butylbenzene <6.2 ug/L 10/25/15 00:45 98-06-612.5 6.2 25 Carbon tetrachloride <6.2 ug/L 10/25/15 00:45 56-23-512.5 6.2 25 Chlorobenzene <6.2 ug/L 10/25/15 00:45 108-90-712.5 6.2 25 Chloroethane <12.5 ug/L 10/25/15 00:45 75-00-325.0 12.5 25 Chloroform <6.2 ug/L 10/25/15 00:45 67-66-312.5 6.2 25 Chloromethane <12.5 ug/L 10/25/15 00:45 74-87-325.0 12.5 25 2-Chlorotoluene <6.2 ug/L 10/25/15 00:45 95-49-812.5 6.2 25 4-Chlorotoluene <6.2 ug/L 10/25/15 00:45 106-43-412.5 6.2 25 1,2-Dibromo-3-chloropropane <12.5 ug/L 10/25/15 00:45 96-12-825.0 12.5 25 Dibromochloromethane <6.2 ug/L 10/25/15 00:45 124-48-112.5 6.2 25 1,2-Dibromoethane (EDB)<6.2 ug/L 10/25/15 00:45 106-93-412.5 6.2 25 Dibromomethane <6.2 ug/L 10/25/15 00:45 74-95-312.5 6.2 25 1,2-Dichlorobenzene <6.2 ug/L 10/25/15 00:45 95-50-112.5 6.2 25 1,3-Dichlorobenzene <6.2 ug/L 10/25/15 00:45 541-73-112.5 6.2 25 1,4-Dichlorobenzene <6.2 ug/L 10/25/15 00:45 106-46-712.5 6.2 25 Dichlorodifluoromethane <6.2 ug/L 10/25/15 00:45 75-71-812.5 6.2 25 1,1-Dichloroethane <6.2 ug/L 10/25/15 00:45 75-34-312.5 6.2 25 1,2-Dichloroethane 13.9 ug/L 10/25/15 00:45 107-06-212.5 6.2 25 1,1-Dichloroethene <6.2 ug/L 10/25/15 00:45 75-35-412.5 6.2 25 cis-1,2-Dichloroethene <6.2 ug/L 10/25/15 00:45 156-59-212.5 6.2 25 trans-1,2-Dichloroethene <6.2 ug/L 10/25/15 00:45 156-60-512.5 6.2 25 1,2-Dichloropropane <6.2 ug/L 10/25/15 00:45 78-87-512.5 6.2 25 1,3-Dichloropropane <6.2 ug/L 10/25/15 00:45 142-28-912.5 6.2 25 2,2-Dichloropropane <6.2 ug/L 10/25/15 00:45 594-20-712.5 6.2 25 1,1-Dichloropropene <6.2 ug/L 10/25/15 00:45 563-58-612.5 6.2 25 cis-1,3-Dichloropropene <6.2 ug/L 10/25/15 00:45 10061-01-512.5 6.2 25 trans-1,3-Dichloropropene <6.2 ug/L 10/25/15 00:45 10061-02-612.5 6.2 25 Diisopropyl ether <6.2 ug/L 10/25/15 00:45 108-20-312.5 6.2 25 Ethylbenzene 1770 ug/L 10/25/15 00:45 100-41-412.5 6.2 25 Hexachloro-1,3-butadiene <25.0 ug/L 10/25/15 00:45 87-68-350.0 25.0 25 Isopropylbenzene (Cumene)118 ug/L 10/25/15 00:45 98-82-812.5 6.2 25 Methylene Chloride 26.0J ug/L 10/25/15 00:45 75-09-250.0 25.0 25 Methyl-tert-butyl ether 116 ug/L 10/25/15 00:45 1634-04-412.5 6.2 25 Naphthalene 808 ug/L 10/25/15 00:45 91-20-350.0 25.0 25 n-Propylbenzene 378 ug/L 10/25/15 00:45 103-65-112.5 6.2 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-14 Lab ID:92272667011 Collected:10/19/15 18:20 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <6.2 ug/L 10/25/15 00:45 100-42-512.5 6.2 25 1,1,1,2-Tetrachloroethane <6.2 ug/L 10/25/15 00:45 630-20-612.5 6.2 25 1,1,2,2-Tetrachloroethane <6.2 ug/L 10/25/15 00:45 79-34-512.5 6.2 25 Tetrachloroethene <6.2 ug/L 10/25/15 00:45 127-18-412.5 6.2 25 Toluene 739 ug/L 10/25/15 00:45 108-88-312.5 6.2 25 1,2,3-Trichlorobenzene <25.0 ug/L 10/25/15 00:45 87-61-650.0 25.0 25 1,2,4-Trichlorobenzene <25.0 ug/L 10/25/15 00:45 120-82-150.0 25.0 25 1,1,1-Trichloroethane <6.2 ug/L 10/25/15 00:45 71-55-612.5 6.2 25 1,1,2-Trichloroethane <6.2 ug/L 10/25/15 00:45 79-00-512.5 6.2 25 Trichloroethene <6.2 ug/L 10/25/15 00:45 79-01-612.5 6.2 25 Trichlorofluoromethane <12.5 ug/L 10/25/15 00:45 75-69-425.0 12.5 25 1,2,3-Trichloropropane <6.2 ug/L 10/25/15 00:45 96-18-412.5 6.2 25 1,2,4-Trimethylbenzene 2210 ug/L 10/25/15 00:45 95-63-612.5 6.2 25 1,3,5-Trimethylbenzene 664 ug/L 10/25/15 00:45 108-67-812.5 6.2 25 Vinyl chloride <6.2 ug/L 10/25/15 00:45 75-01-425.0 6.2 25 m&p-Xylene 2860 ug/L 10/25/15 00:45 179601-23-125.0 12.5 25 o-Xylene 1200 ug/L 10/25/15 00:45 95-47-612.5 6.2 25 Surrogates 1,2-Dichloroethane-d4 (S)103 %10/25/15 00:45 17060-07-070-130 25 4-Bromofluorobenzene (S)101 %10/25/15 00:45 460-00-470-130 25 Toluene-d8 (S)102 %10/25/15 00:45 2037-26-570-130 25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 29 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-15 Lab ID:92272667012 Collected:10/19/15 14:10 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead <2.5 ug/L 10/28/15 18:51 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/25/15 02:59 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 02:59 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 02:59 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 02:59 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 02:59 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 02:59 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 02:59 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 02:59 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 02:59 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 02:59 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 02:59 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 02:59 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 02:59 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 02:59 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 02:59 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 02:59 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 02:59 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 02:59 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 02:59 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 02:59 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 02:59 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 02:59 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 02:59 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 02:59 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 02:59 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 02:59 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 02:59 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:59 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 02:59 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 02:59 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 02:59 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 02:59 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 02:59 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:59 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 02:59 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 02:59 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 02:59 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 02:59 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.25 ug/L 10/25/15 02:59 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 02:59 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.25 ug/L 10/25/15 02:59 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 02:59 91-20-32.0 1.0 1 n-Propylbenzene <0.25 ug/L 10/25/15 02:59 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 30 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-15 Lab ID:92272667012 Collected:10/19/15 14:10 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 02:59 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:59 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 02:59 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 02:59 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 02:59 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 02:59 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 02:59 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 02:59 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 02:59 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 02:59 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 02:59 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 02:59 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.25 ug/L 10/25/15 02:59 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 02:59 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 02:59 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 02:59 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 02:59 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %10/25/15 02:59 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %10/25/15 02:59 460-00-470-130 1 Toluene-d8 (S)100 %10/25/15 02:59 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 31 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-17 Lab ID:92272667013 Collected:10/19/15 10:45 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 60.3 ug/L 10/28/15 18:54 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 898 ug/L 10/25/15 01:02 71-43-250.0 25.0 100 Bromobenzene <25.0 ug/L 10/25/15 01:02 108-86-150.0 25.0 100 Bromochloromethane <25.0 ug/L 10/25/15 01:02 74-97-550.0 25.0 100 Bromodichloromethane <25.0 ug/L 10/25/15 01:02 75-27-450.0 25.0 100 Bromoform <25.0 ug/L 10/25/15 01:02 75-25-250.0 25.0 100 Bromomethane <50.0 ug/L 10/25/15 01:02 74-83-950050.0 100 n-Butylbenzene 779 ug/L 10/25/15 01:02 104-51-850.0 25.0 100 sec-Butylbenzene <25.0 ug/L 10/25/15 01:02 135-98-850.0 25.0 100 tert-Butylbenzene <25.0 ug/L 10/25/15 01:02 98-06-650.0 25.0 100 Carbon tetrachloride <25.0 ug/L 10/25/15 01:02 56-23-550.0 25.0 100 Chlorobenzene <25.0 ug/L 10/25/15 01:02 108-90-750.0 25.0 100 Chloroethane <50.0 ug/L 10/25/15 01:02 75-00-310050.0 100 Chloroform <25.0 ug/L 10/25/15 01:02 67-66-350.0 25.0 100 Chloromethane <50.0 ug/L 10/25/15 01:02 74-87-310050.0 100 2-Chlorotoluene <25.0 ug/L 10/25/15 01:02 95-49-850.0 25.0 100 4-Chlorotoluene <25.0 ug/L 10/25/15 01:02 106-43-450.0 25.0 100 1,2-Dibromo-3-chloropropane <50.0 ug/L 10/25/15 01:02 96-12-810050.0 100 Dibromochloromethane <25.0 ug/L 10/25/15 01:02 124-48-150.0 25.0 100 1,2-Dibromoethane (EDB)<25.0 ug/L 10/25/15 01:02 106-93-450.0 25.0 100 Dibromomethane <25.0 ug/L 10/25/15 01:02 74-95-350.0 25.0 100 1,2-Dichlorobenzene <25.0 ug/L 10/25/15 01:02 95-50-150.0 25.0 100 1,3-Dichlorobenzene <25.0 ug/L 10/25/15 01:02 541-73-150.0 25.0 100 1,4-Dichlorobenzene <25.0 ug/L 10/25/15 01:02 106-46-750.0 25.0 100 Dichlorodifluoromethane <25.0 ug/L 10/25/15 01:02 75-71-850.0 25.0 100 1,1-Dichloroethane <25.0 ug/L 10/25/15 01:02 75-34-350.0 25.0 100 1,2-Dichloroethane <25.0 ug/L 10/25/15 01:02 107-06-250.0 25.0 100 1,1-Dichloroethene <25.0 ug/L 10/25/15 01:02 75-35-450.0 25.0 100 cis-1,2-Dichloroethene <25.0 ug/L 10/25/15 01:02 156-59-250.0 25.0 100 trans-1,2-Dichloroethene <25.0 ug/L 10/25/15 01:02 156-60-550.0 25.0 100 1,2-Dichloropropane <25.0 ug/L 10/25/15 01:02 78-87-550.0 25.0 100 1,3-Dichloropropane <25.0 ug/L 10/25/15 01:02 142-28-950.0 25.0 100 2,2-Dichloropropane <25.0 ug/L 10/25/15 01:02 594-20-750.0 25.0 100 1,1-Dichloropropene <25.0 ug/L 10/25/15 01:02 563-58-650.0 25.0 100 cis-1,3-Dichloropropene <25.0 ug/L 10/25/15 01:02 10061-01-550.0 25.0 100 trans-1,3-Dichloropropene <25.0 ug/L 10/25/15 01:02 10061-02-650.0 25.0 100 Diisopropyl ether 31.1J ug/L 10/25/15 01:02 108-20-350.0 25.0 100 Ethylbenzene 4820 ug/L 10/25/15 01:02 100-41-450.0 25.0 100 Hexachloro-1,3-butadiene <100 ug/L 10/25/15 01:02 87-68-3200100100 Isopropylbenzene (Cumene)409 ug/L 10/25/15 01:02 98-82-850.0 25.0 100 Methylene Chloride <100 ug/L 10/25/15 01:02 75-09-2200100100 Methyl-tert-butyl ether <25.0 ug/L 10/25/15 01:02 1634-04-450.0 25.0 100 Naphthalene 3160 ug/L 10/25/15 01:02 91-20-3200100100 n-Propylbenzene 1400 ug/L 10/25/15 01:02 103-65-150.0 25.0 100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 32 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-17 Lab ID:92272667013 Collected:10/19/15 10:45 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene 93.4 ug/L 10/25/15 01:02 100-42-550.0 25.0 100 1,1,1,2-Tetrachloroethane <25.0 ug/L 10/25/15 01:02 630-20-650.0 25.0 100 1,1,2,2-Tetrachloroethane <25.0 ug/L 10/25/15 01:02 79-34-550.0 25.0 100 Tetrachloroethene <25.0 ug/L 10/25/15 01:02 127-18-450.0 25.0 100 Toluene 14700 ug/L 10/25/15 01:02 108-88-350.0 25.0 100 1,2,3-Trichlorobenzene <100 ug/L 10/25/15 01:02 87-61-6200100100 1,2,4-Trichlorobenzene <100 ug/L 10/25/15 01:02 120-82-1200100100 1,1,1-Trichloroethane <25.0 ug/L 10/25/15 01:02 71-55-650.0 25.0 100 1,1,2-Trichloroethane <25.0 ug/L 10/25/15 01:02 79-00-550.0 25.0 100 Trichloroethene <25.0 ug/L 10/25/15 01:02 79-01-650.0 25.0 100 Trichlorofluoromethane <50.0 ug/L 10/25/15 01:02 75-69-410050.0 100 1,2,3-Trichloropropane <25.0 ug/L 10/25/15 01:02 96-18-450.0 25.0 100 1,2,4-Trimethylbenzene 9820 ug/L 10/25/15 01:02 95-63-650.0 25.0 100 1,3,5-Trimethylbenzene 2740 ug/L 10/25/15 01:02 108-67-850.0 25.0 100 Vinyl chloride <25.0 ug/L 10/25/15 01:02 75-01-410025.0 100 m&p-Xylene 14900 ug/L 10/25/15 01:02 179601-23-110050.0 100 o-Xylene 6780 ug/L 10/25/15 01:02 95-47-650.0 25.0 100 Surrogates 1,2-Dichloroethane-d4 (S)103 %10/25/15 01:02 17060-07-070-130 100 4-Bromofluorobenzene (S)102 %10/25/15 01:02 460-00-470-130 100 Toluene-d8 (S)100 %10/25/15 01:02 2037-26-570-130 100 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 33 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-18 Lab ID:92272667014 Collected:10/19/15 10:05 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead 10.6 ug/L 10/28/15 18:57 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene 77.3 ug/L 10/25/15 03:16 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 03:16 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 03:16 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 03:16 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 03:16 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 03:16 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 03:16 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 03:16 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 03:16 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 03:16 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 03:16 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 03:16 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 03:16 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 03:16 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 03:16 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 03:16 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 03:16 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 03:16 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 03:16 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 03:16 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 03:16 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 03:16 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 03:16 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 03:16 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 03:16 75-34-30.50 0.25 1 1,2-Dichloroethane 0.31J ug/L 10/25/15 03:16 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 03:16 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 03:16 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 03:16 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 03:16 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 03:16 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 03:16 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 03:16 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 03:16 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 03:16 10061-02-60.50 0.25 1 Diisopropyl ether 9.3 ug/L 10/25/15 03:16 108-20-30.50 0.25 1 Ethylbenzene 127 ug/L 10/25/15 03:16 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 03:16 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)5.4 ug/L 10/25/15 03:16 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 03:16 75-09-22.0 1.0 1 Methyl-tert-butyl ether 2.1 ug/L 10/25/15 03:16 1634-04-40.50 0.25 1 Naphthalene 29.7 ug/L 10/25/15 03:16 91-20-32.0 1.0 1 n-Propylbenzene 11.2 ug/L 10/25/15 03:16 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 34 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-18 Lab ID:92272667014 Collected:10/19/15 10:05 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene 4.2 ug/L 10/25/15 03:16 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 03:16 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 03:16 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 03:16 127-18-40.50 0.25 1 Toluene 157 ug/L 10/25/15 13:02 108-88-31.2 0.62 2.5 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 03:16 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 03:16 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 03:16 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 03:16 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 03:16 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 03:16 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 03:16 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene 69.2 ug/L 10/25/15 03:16 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene 18.0 ug/L 10/25/15 03:16 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 03:16 75-01-41.0 0.25 1 m&p-Xylene 253 ug/L 10/25/15 03:16 179601-23-11.0 0.50 1 o-Xylene 148 ug/L 10/25/15 03:16 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %10/25/15 03:16 17060-07-070-130 1 4-Bromofluorobenzene (S)102 %10/25/15 03:16 460-00-470-130 1 Toluene-d8 (S)100 %10/25/15 03:16 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 35 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-19 Lab ID:92272667015 Collected:10/19/15 09:15 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: EPA 6010 Preparation Method: EPA 30106010 MET ICP Lead <2.5 ug/L 10/28/15 19:00 7439-92-110/23/15 18:305.0 2.5 1 Analytical Method: SM 6200B6200B MSV Benzene <0.25 ug/L 10/25/15 03:32 71-43-20.50 0.25 1 Bromobenzene <0.25 ug/L 10/25/15 03:32 108-86-10.50 0.25 1 Bromochloromethane <0.25 ug/L 10/25/15 03:32 74-97-50.50 0.25 1 Bromodichloromethane <0.25 ug/L 10/25/15 03:32 75-27-40.50 0.25 1 Bromoform <0.25 ug/L 10/25/15 03:32 75-25-20.50 0.25 1 Bromomethane <0.50 ug/L 10/25/15 03:32 74-83-95.0 0.50 1 n-Butylbenzene <0.25 ug/L 10/25/15 03:32 104-51-80.50 0.25 1 sec-Butylbenzene <0.25 ug/L 10/25/15 03:32 135-98-80.50 0.25 1 tert-Butylbenzene <0.25 ug/L 10/25/15 03:32 98-06-60.50 0.25 1 Carbon tetrachloride <0.25 ug/L 10/25/15 03:32 56-23-50.50 0.25 1 Chlorobenzene <0.25 ug/L 10/25/15 03:32 108-90-70.50 0.25 1 Chloroethane <0.50 ug/L 10/25/15 03:32 75-00-31.0 0.50 1 Chloroform <0.25 ug/L 10/25/15 03:32 67-66-30.50 0.25 1 Chloromethane <0.50 ug/L 10/25/15 03:32 74-87-31.0 0.50 1 2-Chlorotoluene <0.25 ug/L 10/25/15 03:32 95-49-80.50 0.25 1 4-Chlorotoluene <0.25 ug/L 10/25/15 03:32 106-43-40.50 0.25 1 1,2-Dibromo-3-chloropropane <0.50 ug/L 10/25/15 03:32 96-12-81.0 0.50 1 Dibromochloromethane <0.25 ug/L 10/25/15 03:32 124-48-10.50 0.25 1 1,2-Dibromoethane (EDB)<0.25 ug/L 10/25/15 03:32 106-93-40.50 0.25 1 Dibromomethane <0.25 ug/L 10/25/15 03:32 74-95-30.50 0.25 1 1,2-Dichlorobenzene <0.25 ug/L 10/25/15 03:32 95-50-10.50 0.25 1 1,3-Dichlorobenzene <0.25 ug/L 10/25/15 03:32 541-73-10.50 0.25 1 1,4-Dichlorobenzene <0.25 ug/L 10/25/15 03:32 106-46-70.50 0.25 1 Dichlorodifluoromethane <0.25 ug/L 10/25/15 03:32 75-71-80.50 0.25 1 1,1-Dichloroethane <0.25 ug/L 10/25/15 03:32 75-34-30.50 0.25 1 1,2-Dichloroethane <0.25 ug/L 10/25/15 03:32 107-06-20.50 0.25 1 1,1-Dichloroethene <0.25 ug/L 10/25/15 03:32 75-35-40.50 0.25 1 cis-1,2-Dichloroethene <0.25 ug/L 10/25/15 03:32 156-59-20.50 0.25 1 trans-1,2-Dichloroethene <0.25 ug/L 10/25/15 03:32 156-60-50.50 0.25 1 1,2-Dichloropropane <0.25 ug/L 10/25/15 03:32 78-87-50.50 0.25 1 1,3-Dichloropropane <0.25 ug/L 10/25/15 03:32 142-28-90.50 0.25 1 2,2-Dichloropropane <0.25 ug/L 10/25/15 03:32 594-20-70.50 0.25 1 1,1-Dichloropropene <0.25 ug/L 10/25/15 03:32 563-58-60.50 0.25 1 cis-1,3-Dichloropropene <0.25 ug/L 10/25/15 03:32 10061-01-50.50 0.25 1 trans-1,3-Dichloropropene <0.25 ug/L 10/25/15 03:32 10061-02-60.50 0.25 1 Diisopropyl ether <0.25 ug/L 10/25/15 03:32 108-20-30.50 0.25 1 Ethylbenzene <0.25 ug/L 10/25/15 03:32 100-41-40.50 0.25 1 Hexachloro-1,3-butadiene <1.0 ug/L 10/25/15 03:32 87-68-32.0 1.0 1 Isopropylbenzene (Cumene)<0.25 ug/L 10/25/15 03:32 98-82-80.50 0.25 1 Methylene Chloride <1.0 ug/L 10/25/15 03:32 75-09-22.0 1.0 1 Methyl-tert-butyl ether <0.25 ug/L 10/25/15 03:32 1634-04-40.50 0.25 1 Naphthalene <1.0 ug/L 10/25/15 03:32 91-20-32.0 1.0 1 n-Propylbenzene <0.25 ug/L 10/25/15 03:32 103-65-10.50 0.25 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 36 of 64 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Sample:MW-19 Lab ID:92272667015 Collected:10/19/15 09:15 Received:10/20/15 15:00 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL Analytical Method: SM 6200B6200B MSV Styrene <0.25 ug/L 10/25/15 03:32 100-42-50.50 0.25 1 1,1,1,2-Tetrachloroethane <0.25 ug/L 10/25/15 03:32 630-20-60.50 0.25 1 1,1,2,2-Tetrachloroethane <0.25 ug/L 10/25/15 03:32 79-34-50.50 0.25 1 Tetrachloroethene <0.25 ug/L 10/25/15 03:32 127-18-40.50 0.25 1 Toluene <0.25 ug/L 10/25/15 03:32 108-88-30.50 0.25 1 1,2,3-Trichlorobenzene <1.0 ug/L 10/25/15 03:32 87-61-62.0 1.0 1 1,2,4-Trichlorobenzene <1.0 ug/L 10/25/15 03:32 120-82-12.0 1.0 1 1,1,1-Trichloroethane <0.25 ug/L 10/25/15 03:32 71-55-60.50 0.25 1 1,1,2-Trichloroethane <0.25 ug/L 10/25/15 03:32 79-00-50.50 0.25 1 Trichloroethene <0.25 ug/L 10/25/15 03:32 79-01-60.50 0.25 1 Trichlorofluoromethane <0.50 ug/L 10/25/15 03:32 75-69-41.0 0.50 1 1,2,3-Trichloropropane <0.25 ug/L 10/25/15 03:32 96-18-40.50 0.25 1 1,2,4-Trimethylbenzene <0.25 ug/L 10/25/15 03:32 95-63-60.50 0.25 1 1,3,5-Trimethylbenzene <0.25 ug/L 10/25/15 03:32 108-67-80.50 0.25 1 Vinyl chloride <0.25 ug/L 10/25/15 03:32 75-01-41.0 0.25 1 m&p-Xylene <0.50 ug/L 10/25/15 03:32 179601-23-11.0 0.50 1 o-Xylene <0.25 ug/L 10/25/15 03:32 95-47-60.50 0.25 1 Surrogates 1,2-Dichloroethane-d4 (S)105 %10/25/15 03:32 17060-07-070-130 1 4-Bromofluorobenzene (S)99 %10/25/15 03:32 460-00-470-130 1 Toluene-d8 (S)101 %10/25/15 03:32 2037-26-570-130 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 37 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/19875 EPA 3010 EPA 6010 6010 MET Associated Lab Samples:92272667001, 92272667002, 92272667003 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1589166 Associated Lab Samples:92272667001, 92272667002, 92272667003 Matrix:Water AnalyzedMDL Lead ug/L <2.5 5.0 10/27/15 02:212.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1589167LABORATORY CONTROL SAMPLE: LCSSpike Lead ug/L 485500 97 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1589168MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92272764003 1589169 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Lead ug/L 500 87 75-12588 2 20500ND434443 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 38 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/19876 EPA 3010 EPA 6010 6010 MET Associated Lab Samples:92272667004, 92272667005, 92272667006, 92272667007, 92272667008, 92272667009, 92272667010, 92272667011, 92272667012, 92272667013, 92272667014, 92272667015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1589225 Associated Lab Samples:92272667004, 92272667005, 92272667006, 92272667007, 92272667008, 92272667009, 92272667010, 92272667011, 92272667012, 92272667013, 92272667014, 92272667015 Matrix:Water AnalyzedMDL Lead ug/L <2.5 5.0 10/28/15 18:052.5 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1589226LABORATORY CONTROL SAMPLE: LCSSpike Lead ug/L 490500 98 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1589227MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92272667004 1589228 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Lead ug/L 500 96 75-12597 1 205002.5J 481 488 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 39 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/33965 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92272667001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591077 Associated Lab Samples:92272667001 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.25 0.50 10/24/15 16:240.25 1,1,1-Trichloroethane ug/L <0.25 0.50 10/24/15 16:240.25 1,1,2,2-Tetrachloroethane ug/L <0.25 0.50 10/24/15 16:240.25 1,1,2-Trichloroethane ug/L <0.25 0.50 10/24/15 16:240.25 1,1-Dichloroethane ug/L <0.25 0.50 10/24/15 16:240.25 1,1-Dichloroethene ug/L <0.25 0.50 10/24/15 16:240.25 1,1-Dichloropropene ug/L <0.25 0.50 10/24/15 16:240.25 1,2,3-Trichlorobenzene ug/L <1.0 2.0 10/24/15 16:241.0 1,2,3-Trichloropropane ug/L <0.25 0.50 10/24/15 16:240.25 1,2,4-Trichlorobenzene ug/L <1.0 2.0 10/24/15 16:241.0 1,2,4-Trimethylbenzene ug/L <0.25 0.50 10/24/15 16:240.25 1,2-Dibromo-3-chloropropane ug/L <0.50 1.0 10/24/15 16:240.50 1,2-Dibromoethane (EDB)ug/L <0.25 0.50 10/24/15 16:240.25 1,2-Dichlorobenzene ug/L <0.25 0.50 10/24/15 16:240.25 1,2-Dichloroethane ug/L <0.25 0.50 10/24/15 16:240.25 1,2-Dichloropropane ug/L <0.25 0.50 10/24/15 16:240.25 1,3,5-Trimethylbenzene ug/L <0.25 0.50 10/24/15 16:240.25 1,3-Dichlorobenzene ug/L <0.25 0.50 10/24/15 16:240.25 1,3-Dichloropropane ug/L <0.25 0.50 10/24/15 16:240.25 1,4-Dichlorobenzene ug/L <0.25 0.50 10/24/15 16:240.25 2,2-Dichloropropane ug/L <0.25 0.50 10/24/15 16:240.25 2-Chlorotoluene ug/L <0.25 0.50 10/24/15 16:240.25 4-Chlorotoluene ug/L <0.25 0.50 10/24/15 16:240.25 Benzene ug/L <0.25 0.50 10/24/15 16:240.25 Bromobenzene ug/L <0.25 0.50 10/24/15 16:240.25 Bromochloromethane ug/L <0.25 0.50 10/24/15 16:240.25 Bromodichloromethane ug/L <0.25 0.50 10/24/15 16:240.25 Bromoform ug/L <0.25 0.50 10/24/15 16:240.25 Bromomethane ug/L <0.50 5.0 10/24/15 16:240.50 Carbon tetrachloride ug/L <0.25 0.50 10/24/15 16:240.25 Chlorobenzene ug/L <0.25 0.50 10/24/15 16:240.25 Chloroethane ug/L <0.50 1.0 10/24/15 16:240.50 Chloroform ug/L <0.25 0.50 10/24/15 16:240.25 Chloromethane ug/L <0.50 1.0 10/24/15 16:240.50 cis-1,2-Dichloroethene ug/L <0.25 0.50 10/24/15 16:240.25 cis-1,3-Dichloropropene ug/L <0.25 0.50 10/24/15 16:240.25 Dibromochloromethane ug/L <0.25 0.50 10/24/15 16:240.25 Dibromomethane ug/L <0.25 0.50 10/24/15 16:240.25 Dichlorodifluoromethane ug/L <0.25 0.50 10/24/15 16:240.25 Diisopropyl ether ug/L <0.25 0.50 10/24/15 16:240.25 Ethylbenzene ug/L <0.25 0.50 10/24/15 16:240.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 40 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591077 Associated Lab Samples:92272667001 Matrix:Water AnalyzedMDL Hexachloro-1,3-butadiene ug/L <1.0 2.0 10/24/15 16:241.0 Isopropylbenzene (Cumene)ug/L <0.25 0.50 10/24/15 16:240.25 m&p-Xylene ug/L <0.50 1.0 10/24/15 16:240.50 Methyl-tert-butyl ether ug/L <0.25 0.50 10/24/15 16:240.25 Methylene Chloride ug/L <1.0 2.0 10/24/15 16:241.0 n-Butylbenzene ug/L <0.25 0.50 10/24/15 16:240.25 n-Propylbenzene ug/L <0.25 0.50 10/24/15 16:240.25 Naphthalene ug/L <1.0 2.0 10/24/15 16:241.0 o-Xylene ug/L <0.25 0.50 10/24/15 16:240.25 sec-Butylbenzene ug/L <0.25 0.50 10/24/15 16:240.25 Styrene ug/L <0.25 0.50 10/24/15 16:240.25 tert-Butylbenzene ug/L <0.25 0.50 10/24/15 16:240.25 Tetrachloroethene ug/L <0.25 0.50 10/24/15 16:240.25 Toluene ug/L <0.25 0.50 10/24/15 16:240.25 trans-1,2-Dichloroethene ug/L <0.25 0.50 10/24/15 16:240.25 trans-1,3-Dichloropropene ug/L <0.25 0.50 10/24/15 16:240.25 Trichloroethene ug/L <0.25 0.50 10/24/15 16:240.25 Trichlorofluoromethane ug/L <0.50 1.0 10/24/15 16:240.50 Vinyl chloride ug/L <0.25 1.0 10/24/15 16:240.25 1,2-Dichloroethane-d4 (S)%98 70-130 10/24/15 16:24 4-Bromofluorobenzene (S)%100 70-130 10/24/15 16:24 Toluene-d8 (S)%101 70-130 10/24/15 16:24 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591078LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 51.250 102 60-140 1,1,1-Trichloroethane ug/L 52.950 106 60-140 1,1,2,2-Tetrachloroethane ug/L 51.350 103 60-140 1,1,2-Trichloroethane ug/L 49.150 98 60-140 1,1-Dichloroethane ug/L 50.750 101 60-140 1,1-Dichloroethene ug/L 52.650 105 60-140 1,1-Dichloropropene ug/L 50.250 100 60-140 1,2,3-Trichlorobenzene ug/L 51.550 103 60-140 1,2,3-Trichloropropane ug/L 50.650 101 60-140 1,2,4-Trichlorobenzene ug/L 50.750 101 60-140 1,2,4-Trimethylbenzene ug/L 50.050 100 60-140 1,2-Dibromo-3-chloropropane ug/L 53.250 106 60-140 1,2-Dibromoethane (EDB)ug/L 51.050 102 60-140 1,2-Dichlorobenzene ug/L 49.950 100 60-140 1,2-Dichloroethane ug/L 45.350 91 60-140 1,2-Dichloropropane ug/L 49.050 98 60-140 1,3,5-Trimethylbenzene ug/L 50.750 101 60-140 1,3-Dichlorobenzene ug/L 50.350 101 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 41 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591078LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 50.550 101 60-140 1,4-Dichlorobenzene ug/L 49.750 99 60-140 2,2-Dichloropropane ug/L 52.850 106 60-140 2-Chlorotoluene ug/L 49.650 99 60-140 4-Chlorotoluene ug/L 50.250 100 60-140 Benzene ug/L 50.450 101 60-140 Bromobenzene ug/L 50.250 100 60-140 Bromochloromethane ug/L 52.950 106 60-140 Bromodichloromethane ug/L 53.150 106 60-140 Bromoform ug/L 53.650 107 60-140 Bromomethane ug/L 52.950 106 60-140 Carbon tetrachloride ug/L 54.550 109 60-140 Chlorobenzene ug/L 49.150 98 60-140 Chloroethane ug/L 44.150 88 60-140 Chloroform ug/L 50.550 101 60-140 Chloromethane ug/L 52.950 106 60-140 cis-1,2-Dichloroethene ug/L 48.650 97 60-140 cis-1,3-Dichloropropene ug/L 52.350 105 60-140 Dibromochloromethane ug/L 54.350 109 60-140 Dibromomethane ug/L 51.650 103 60-140 Dichlorodifluoromethane ug/L 44.650 89 60-140 Diisopropyl ether ug/L 51.650 103 60-140 Ethylbenzene ug/L 49.950 100 60-140 Hexachloro-1,3-butadiene ug/L 52.850 106 60-140 Isopropylbenzene (Cumene)ug/L 54.750 109 60-140 m&p-Xylene ug/L 100100 100 60-140 Methyl-tert-butyl ether ug/L 51.950 104 60-140 Methylene Chloride ug/L 52.950 106 60-140 n-Butylbenzene ug/L 51.250 102 60-140 n-Propylbenzene ug/L 50.650 101 60-140 Naphthalene ug/L 53.550 107 60-140 o-Xylene ug/L 50.650 101 60-140 sec-Butylbenzene ug/L 53.050 106 60-140 Styrene ug/L 51.450 103 60-140 tert-Butylbenzene ug/L 50.450 101 60-140 Tetrachloroethene ug/L 51.050 102 60-140 Toluene ug/L 50.150 100 60-140 trans-1,2-Dichloroethene ug/L 49.950 100 60-140 trans-1,3-Dichloropropene ug/L 52.750 105 60-140 Trichloroethene ug/L 48.650 97 60-140 Trichlorofluoromethane ug/L 48.350 97 60-140 Vinyl chloride ug/L 49.250 98 60-140 1,2-Dichloroethane-d4 (S)%102 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%101 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 42 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591565MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92272322009 1591566 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 88 60-140104 17 3020<0.25 17.6 20.9 1,1,1-Trichloroethane ug/L 20 107 60-140123 14 3020<0.25 21.4 24.6 1,1,2,2-Tetrachloroethane ug/L 20 88 60-140100 14 3020<0.25 17.5 20.1 1,1,2-Trichloroethane ug/L 20 85 60-14099 15 3020<0.25 17.0 19.7 1,1-Dichloroethane ug/L 20 100 60-140114 13 3020<0.25 20.0 22.8 1,1-Dichloroethene ug/L 20 111 60-140127 13 3020<0.25 22.3 25.3 1,1-Dichloropropene ug/L 20 97 60-140112 14 3020<0.25 19.5 22.4 1,2,3-Trichlorobenzene ug/L 20 81 60-14089 10 3020<1.0 16.2 17.9 1,2,3-Trichloropropane ug/L 20 87 60-140101 14 3020<0.25 17.5 20.2 1,2,4-Trichlorobenzene ug/L 20 81 60-14089 9 3020<1.0 16.3 17.9 1,2,4-Trimethylbenzene ug/L 20 94 60-140107 13 3020<0.25 18.8 21.4 1,2-Dibromo-3- chloropropane ug/L 20 87 60-140103 17 3020<0.50 17.4 20.6 1,2-Dibromoethane (EDB)ug/L 20 88 60-140101 14 3020<0.25 17.7 20.3 1,2-Dichlorobenzene ug/L 20 90 60-140102 13 3020<0.25 17.9 20.4 1,2-Dichloroethane ug/L 20 87 60-140100 14 3020<0.25 17.5 20.1 1,2-Dichloropropane ug/L 20 90 60-140104 14 3020<0.25 18.1 20.9 1,3,5-Trimethylbenzene ug/L 20 96 60-140110 14 3020<0.25 19.2 22.0 1,3-Dichlorobenzene ug/L 20 91 60-140103 12 3020<0.25 18.3 20.6 1,3-Dichloropropane ug/L 20 89 60-140103 14 3020<0.25 17.8 20.5 1,4-Dichlorobenzene ug/L 20 88 60-140102 14 3020<0.25 17.6 20.3 2,2-Dichloropropane ug/L 20 110 60-140123 11 3020<0.25 22.0 24.6 2-Chlorotoluene ug/L 20 96 60-140108 12 3020<0.25 19.3 21.7 4-Chlorotoluene ug/L 20 94 60-140109 14 3020<0.25 18.9 21.7 Benzene ug/L 20 91 60-140104 13 3020<0.25 18.3 20.8 Bromobenzene ug/L 20 94 60-140107 13 3020<0.25 18.9 21.4 Bromochloromethane ug/L 20 93 60-140109 15 3020<0.25 18.7 21.7 Bromodichloromethane ug/L 20 92 60-140106 15 3020<0.25 18.4 21.3 Bromoform ug/L 20 70 60-14083 17 3020<0.25 14.1 16.7 Bromomethane ug/L 20 81 60-14092 12 3020<0.50 16.3 18.3 Carbon tetrachloride ug/L 20 105 60-140121 14 3020<0.25 21.0 24.2 Chlorobenzene ug/L 20 88 60-140102 14 3020<0.25 17.7 20.4 Chloroethane ug/L 20 83 60-14096 15 3020<0.50 16.6 19.3 Chloroform ug/L 20 97 60-140113 15 3020<0.25 19.5 22.6 Chloromethane ug/L 20 86 60-14099 14 3020<0.50 17.3 19.8 cis-1,2-Dichloroethene ug/L 20 97 60-140111 13 3020<0.25 19.4 22.2 cis-1,3-Dichloropropene ug/L 20 90 60-140104 14 3020<0.25 18.1 20.9 Dibromochloromethane ug/L 20 87 60-14099 14 3020<0.25 17.3 19.9 Dibromomethane ug/L 20 83 60-14095 14 3020<0.25 16.5 18.9 Dichlorodifluoromethane ug/L 20 76 60-14088 14 3020<0.25 15.2 17.5 Diisopropyl ether ug/L 20 102 60-140119 15 3020<0.25 20.4 23.7 Ethylbenzene ug/L 20 92 60-140106 14 3020<0.25 18.5 21.3 Hexachloro-1,3-butadiene ug/L 20 103 60-140115 11 3020<1.0 20.6 23.0 Isopropylbenzene (Cumene)ug/L 20 102 60-140116 13 3020<0.25 20.4 23.2 m&p-Xylene ug/L 40 93 60-140107 14 3040<0.50 37.2 42.7 Methyl-tert-butyl ether ug/L 20 94 60-140108 13 30200.63 19.5 22.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 43 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591565MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92272322009 1591566 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 101 60-140113 11 3020<1.0 20.3 22.7 n-Butylbenzene ug/L 20 95 60-140107 12 3020<0.25 19.0 21.4 n-Propylbenzene ug/L 20 98 60-140111 13 3020<0.25 19.6 22.3 Naphthalene ug/L 20 85 60-14097 13 3020<1.0 17.1 19.4 o-Xylene ug/L 20 92 60-140106 14 3020<0.25 18.3 21.1 sec-Butylbenzene ug/L 20 102 60-140116 13 3020<0.25 20.4 23.3 Styrene ug/L 20 87 60-140102 16 3020<0.25 17.5 20.5 tert-Butylbenzene ug/L 20 97 60-140110 13 3020<0.25 19.3 21.9 Tetrachloroethene ug/L 20 94 60-140109 15 3020<0.25 18.7 21.8 Toluene ug/L 20 92 60-140105 14 3020<0.25 18.3 21.0 trans-1,2-Dichloroethene ug/L 20 103 60-140116 12 3020<0.25 20.6 23.2 trans-1,3-Dichloropropene ug/L 20 91 60-140104 13 3020<0.25 18.2 20.8 Trichloroethene ug/L 20 91 60-140103 13 3020<0.25 18.1 20.6 Trichlorofluoromethane ug/L 20 94 60-140108 14 3020<0.50 18.8 21.7 Vinyl chloride ug/L 20 92 60-140107 15 3020<0.25 18.5 21.5 1,2-Dichloroethane-d4 (S)%109 70-130109 4-Bromofluorobenzene (S)%96 70-13095 Toluene-d8 (S)%101 70-130101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 44 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/33966 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92272667006, 92272667007, 92272667008, 92272667009, 92272667010, 92272667011, 92272667012, 92272667013, 92272667014, 92272667015 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591079 Associated Lab Samples:92272667006, 92272667007, 92272667008, 92272667009, 92272667010, 92272667011, 92272667012, 92272667013, 92272667014, 92272667015 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.25 0.50 10/24/15 23:210.25 1,1,1-Trichloroethane ug/L <0.25 0.50 10/24/15 23:210.25 1,1,2,2-Tetrachloroethane ug/L <0.25 0.50 10/24/15 23:210.25 1,1,2-Trichloroethane ug/L <0.25 0.50 10/24/15 23:210.25 1,1-Dichloroethane ug/L <0.25 0.50 10/24/15 23:210.25 1,1-Dichloroethene ug/L <0.25 0.50 10/24/15 23:210.25 1,1-Dichloropropene ug/L <0.25 0.50 10/24/15 23:210.25 1,2,3-Trichlorobenzene ug/L <1.0 2.0 10/24/15 23:211.0 1,2,3-Trichloropropane ug/L <0.25 0.50 10/24/15 23:210.25 1,2,4-Trichlorobenzene ug/L <1.0 2.0 10/24/15 23:211.0 1,2,4-Trimethylbenzene ug/L <0.25 0.50 10/24/15 23:210.25 1,2-Dibromo-3-chloropropane ug/L <0.50 1.0 10/24/15 23:210.50 1,2-Dibromoethane (EDB)ug/L <0.25 0.50 10/24/15 23:210.25 1,2-Dichlorobenzene ug/L <0.25 0.50 10/24/15 23:210.25 1,2-Dichloroethane ug/L <0.25 0.50 10/24/15 23:210.25 1,2-Dichloropropane ug/L <0.25 0.50 10/24/15 23:210.25 1,3,5-Trimethylbenzene ug/L <0.25 0.50 10/24/15 23:210.25 1,3-Dichlorobenzene ug/L <0.25 0.50 10/24/15 23:210.25 1,3-Dichloropropane ug/L <0.25 0.50 10/24/15 23:210.25 1,4-Dichlorobenzene ug/L <0.25 0.50 10/24/15 23:210.25 2,2-Dichloropropane ug/L <0.25 0.50 10/24/15 23:210.25 2-Chlorotoluene ug/L <0.25 0.50 10/24/15 23:210.25 4-Chlorotoluene ug/L <0.25 0.50 10/24/15 23:210.25 Benzene ug/L <0.25 0.50 10/24/15 23:210.25 Bromobenzene ug/L <0.25 0.50 10/24/15 23:210.25 Bromochloromethane ug/L <0.25 0.50 10/24/15 23:210.25 Bromodichloromethane ug/L <0.25 0.50 10/24/15 23:210.25 Bromoform ug/L <0.25 0.50 10/24/15 23:210.25 Bromomethane ug/L <0.50 5.0 10/24/15 23:210.50 Carbon tetrachloride ug/L <0.25 0.50 10/24/15 23:210.25 Chlorobenzene ug/L <0.25 0.50 10/24/15 23:210.25 Chloroethane ug/L <0.50 1.0 10/24/15 23:210.50 Chloroform ug/L <0.25 0.50 10/24/15 23:210.25 Chloromethane ug/L <0.50 1.0 10/24/15 23:210.50 cis-1,2-Dichloroethene ug/L <0.25 0.50 10/24/15 23:210.25 cis-1,3-Dichloropropene ug/L <0.25 0.50 10/24/15 23:210.25 Dibromochloromethane ug/L <0.25 0.50 10/24/15 23:210.25 Dibromomethane ug/L <0.25 0.50 10/24/15 23:210.25 Dichlorodifluoromethane ug/L <0.25 0.50 10/24/15 23:210.25 Diisopropyl ether ug/L <0.25 0.50 10/24/15 23:210.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 45 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591079 Associated Lab Samples:92272667006, 92272667007, 92272667008, 92272667009, 92272667010, 92272667011, 92272667012, 92272667013, 92272667014, 92272667015 Matrix:Water AnalyzedMDL Ethylbenzene ug/L <0.25 0.50 10/24/15 23:210.25 Hexachloro-1,3-butadiene ug/L <1.0 2.0 10/24/15 23:211.0 Isopropylbenzene (Cumene)ug/L <0.25 0.50 10/24/15 23:210.25 m&p-Xylene ug/L <0.50 1.0 10/24/15 23:210.50 Methyl-tert-butyl ether ug/L <0.25 0.50 10/24/15 23:210.25 Methylene Chloride ug/L <1.0 2.0 10/24/15 23:211.0 n-Butylbenzene ug/L <0.25 0.50 10/24/15 23:210.25 n-Propylbenzene ug/L <0.25 0.50 10/24/15 23:210.25 Naphthalene ug/L <1.0 2.0 10/24/15 23:211.0 o-Xylene ug/L <0.25 0.50 10/24/15 23:210.25 sec-Butylbenzene ug/L <0.25 0.50 10/24/15 23:210.25 Styrene ug/L <0.25 0.50 10/24/15 23:210.25 tert-Butylbenzene ug/L <0.25 0.50 10/24/15 23:210.25 Tetrachloroethene ug/L <0.25 0.50 10/24/15 23:210.25 Toluene ug/L <0.25 0.50 10/24/15 23:210.25 trans-1,2-Dichloroethene ug/L <0.25 0.50 10/24/15 23:210.25 trans-1,3-Dichloropropene ug/L <0.25 0.50 10/24/15 23:210.25 Trichloroethene ug/L <0.25 0.50 10/24/15 23:210.25 Trichlorofluoromethane ug/L <0.50 1.0 10/24/15 23:210.50 Vinyl chloride ug/L <0.25 1.0 10/24/15 23:210.25 1,2-Dichloroethane-d4 (S)%100 70-130 10/24/15 23:21 4-Bromofluorobenzene (S)%99 70-130 10/24/15 23:21 Toluene-d8 (S)%102 70-130 10/24/15 23:21 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591080LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 51.950 104 60-140 1,1,1-Trichloroethane ug/L 52.950 106 60-140 1,1,2,2-Tetrachloroethane ug/L 51.950 104 60-140 1,1,2-Trichloroethane ug/L 48.250 96 60-140 1,1-Dichloroethane ug/L 50.950 102 60-140 1,1-Dichloroethene ug/L 53.550 107 60-140 1,1-Dichloropropene ug/L 50.850 102 60-140 1,2,3-Trichlorobenzene ug/L 51.350 103 60-140 1,2,3-Trichloropropane ug/L 51.450 103 60-140 1,2,4-Trichlorobenzene ug/L 51.150 102 60-140 1,2,4-Trimethylbenzene ug/L 51.950 104 60-140 1,2-Dibromo-3-chloropropane ug/L 53.550 107 60-140 1,2-Dibromoethane (EDB)ug/L 51.850 104 60-140 1,2-Dichlorobenzene ug/L 51.650 103 60-140 1,2-Dichloroethane ug/L 45.050 90 60-140 1,2-Dichloropropane ug/L 48.950 98 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 46 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591080LABORATORY CONTROL SAMPLE: LCSSpike 1,3,5-Trimethylbenzene ug/L 52.350 105 60-140 1,3-Dichlorobenzene ug/L 51.650 103 60-140 1,3-Dichloropropane ug/L 51.350 103 60-140 1,4-Dichlorobenzene ug/L 50.450 101 60-140 2,2-Dichloropropane ug/L 51.250 102 60-140 2-Chlorotoluene ug/L 50.450 101 60-140 4-Chlorotoluene ug/L 51.450 103 60-140 Benzene ug/L 50.350 101 60-140 Bromobenzene ug/L 48.150 96 60-140 Bromochloromethane ug/L 50.350 101 60-140 Bromodichloromethane ug/L 51.950 104 60-140 Bromoform ug/L 49.750 99 60-140 Bromomethane ug/L 41.250 82 60-140 Carbon tetrachloride ug/L 54.450 109 60-140 Chlorobenzene ug/L 49.650 99 60-140 Chloroethane ug/L 45.350 91 60-140 Chloroform ug/L 49.650 99 60-140 Chloromethane ug/L 48.250 96 60-140 cis-1,2-Dichloroethene ug/L 48.950 98 60-140 cis-1,3-Dichloropropene ug/L 51.750 103 60-140 Dibromochloromethane ug/L 52.950 106 60-140 Dibromomethane ug/L 48.350 97 60-140 Dichlorodifluoromethane ug/L 43.550 87 60-140 Diisopropyl ether ug/L 51.850 104 60-140 Ethylbenzene ug/L 51.350 103 60-140 Hexachloro-1,3-butadiene ug/L 52.750 105 60-140 Isopropylbenzene (Cumene)ug/L 56.250 112 60-140 m&p-Xylene ug/L 103100 103 60-140 Methyl-tert-butyl ether ug/L 50.250 100 60-140 Methylene Chloride ug/L 53.450 107 60-140 n-Butylbenzene ug/L 53.650 107 60-140 n-Propylbenzene ug/L 52.250 104 60-140 Naphthalene ug/L 53.250 106 60-140 o-Xylene ug/L 51.450 103 60-140 sec-Butylbenzene ug/L 55.750 111 60-140 Styrene ug/L 52.050 104 60-140 tert-Butylbenzene ug/L 52.050 104 60-140 Tetrachloroethene ug/L 53.050 106 60-140 Toluene ug/L 50.450 101 60-140 trans-1,2-Dichloroethene ug/L 50.050 100 60-140 trans-1,3-Dichloropropene ug/L 52.250 104 60-140 Trichloroethene ug/L 49.250 98 60-140 Trichlorofluoromethane ug/L 48.750 97 60-140 Vinyl chloride ug/L 49.150 98 60-140 1,2-Dichloroethane-d4 (S)%101 70-130 4-Bromofluorobenzene (S)%100 70-130 Toluene-d8 (S)%100 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 47 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591572MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92273062004 1591573 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 114 60-140116 2 3020ND22.8 23.2 1,1,1-Trichloroethane ug/L 20 134 60-140136 1 3020ND26.9 27.2 1,1,2,2-Tetrachloroethane ug/L 20 113 60-140112 0 3020ND22.5 22.5 1,1,2-Trichloroethane ug/L 20 107 60-140107 0 3020ND21.4 21.4 1,1-Dichloroethane ug/L 20 127 60-140127 0 3020ND25.3 25.4 1,1-Dichloroethene ug/L M12013960-140142 2 3020ND27.9 28.4 1,1-Dichloropropene ug/L 20 124 60-140127 2 3020ND24.9 25.5 1,2,3-Trichlorobenzene ug/L 20 96 60-14098 1 3020ND19.3 19.5 1,2,3-Trichloropropane ug/L 20 112 60-140110 1 3020ND22.3 22.1 1,2,4-Trichlorobenzene ug/L 20 99 60-14099 0 3020ND19.8 19.7 1,2,4-Trimethylbenzene ug/L 20 115 60-140117 2 3020ND23.0 23.4 1,2-Dibromo-3- chloropropane ug/L 20 116 60-140113 3 3020ND23.3 22.6 1,2-Dibromoethane (EDB)ug/L 20 113 60-140113 0 3020ND22.6 22.6 1,2-Dichlorobenzene ug/L 20 110 60-140113 2 3020ND22.0 22.6 1,2-Dichloroethane ug/L 20 110 60-140108 1 3020ND22.1 21.8 1,2-Dichloropropane ug/L 20 115 60-140116 0 3020ND23.1 23.1 1,3,5-Trimethylbenzene ug/L 20 116 60-140118 2 3020ND23.1 23.6 1,3-Dichlorobenzene ug/L 20 113 60-140115 1 3020ND22.6 22.9 1,3-Dichloropropane ug/L 20 113 60-140114 0 3020ND22.7 22.8 1,4-Dichlorobenzene ug/L 20 110 60-140113 2 3020ND22.1 22.6 2,2-Dichloropropane ug/L 20 140 60-140137 2 3020ND27.9 27.4 2-Chlorotoluene ug/L 20 122 60-140120 1 3020ND24.4 24.0 4-Chlorotoluene ug/L 20 120 60-140120 0 3020ND24.0 24.1 Benzene ug/L 20 115 60-140115 0 3020ND23.0 23.0 Bromobenzene ug/L 20 118 60-140118 1 3020ND23.5 23.6 Bromochloromethane ug/L 20 118 60-140117 1 3020ND23.6 23.3 Bromodichloromethane ug/L 20 118 60-140116 2 3020ND23.6 23.2 Bromoform ug/L 20 93 60-14093 0 3020ND18.5 18.5 Bromomethane ug/L 20 101 60-140100 1 3020ND20.1 20.0 Carbon tetrachloride ug/L 20 132 60-140134 2 3020ND26.4 26.9 Chlorobenzene ug/L 20 112 60-140113 1 3020ND22.4 22.6 Chloroethane ug/L 20 111 60-140109 2 3020ND22.2 21.9 Chloroform ug/L 20 124 60-140123 1 3020ND24.9 24.6 Chloromethane ug/L 20 125 60-140123 1 3020ND24.9 24.6 cis-1,2-Dichloroethene ug/L 20 124 60-140123 0 3020ND24.8 24.6 cis-1,3-Dichloropropene ug/L 20 114 60-140113 2 3020ND22.9 22.5 Dibromochloromethane ug/L 20 112 60-140111 1 3020ND22.4 22.2 Dibromomethane ug/L 20 102 60-140103 1 3020ND20.3 20.6 Dichlorodifluoromethane ug/L 20 119 60-140119 0 3020ND23.8 23.8 Diisopropyl ether ug/L 20 130 60-140129 1 3020ND26.1 25.9 Ethylbenzene ug/L 20 118 60-140118 0 3020ND23.6 23.6 Hexachloro-1,3-butadiene ug/L 20 96 60-140101 6 3020ND19.2 20.3 Isopropylbenzene (Cumene)ug/L 20 127 60-140127 0 3020ND25.3 25.4 m&p-Xylene ug/L 40 117 60-140117 1 3040ND47.0 46.7 Methyl-tert-butyl ether ug/L 20 119 60-140118 0 3020ND23.8 23.7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 48 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591572MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92273062004 1591573 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 128 60-140128 0 3020ND25.5 25.6 n-Butylbenzene ug/L 20 110 60-140114 4 3020ND21.9 22.8 n-Propylbenzene ug/L 20 120 60-140122 1 3020ND24.1 24.4 Naphthalene ug/L 20 106 60-140105 1 3020ND21.2 21.1 o-Xylene ug/L 20 117 60-140117 0 3020ND23.3 23.4 sec-Butylbenzene ug/L 20 120 60-140125 4 3020ND24.0 25.1 Styrene ug/L 20 112 60-140112 0 3020ND22.4 22.4 tert-Butylbenzene ug/L 20 117 60-140119 2 3020ND23.3 23.9 Tetrachloroethene ug/L 20 118 60-140121 2 3020ND23.7 24.1 Toluene ug/L 20 94 60-140114 14 30207.9 26.6 30.6 trans-1,2-Dichloroethene ug/L 20 130 60-140129 1 3020ND26.0 25.8 trans-1,3-Dichloropropene ug/L 20 116 60-140116 0 3020ND23.1 23.1 Trichloroethene ug/L 20 112 60-140112 1 3020ND22.3 22.5 Trichlorofluoromethane ug/L 20 123 60-140123 0 3020ND24.5 24.5 Vinyl chloride ug/L 20 126 60-140126 0 3020ND25.2 25.2 1,2-Dichloroethane-d4 (S)%108 70-130108 4-Bromofluorobenzene (S)%96 70-13095 Toluene-d8 (S)%100 70-13099 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 49 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/33973 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92272667002, 92272667003, 92272667004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591165 Associated Lab Samples:92272667002, 92272667003, 92272667004 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.25 0.50 10/25/15 16:560.25 1,1,1-Trichloroethane ug/L <0.25 0.50 10/25/15 16:560.25 1,1,2,2-Tetrachloroethane ug/L <0.25 0.50 10/25/15 16:560.25 1,1,2-Trichloroethane ug/L <0.25 0.50 10/25/15 16:560.25 1,1-Dichloroethane ug/L <0.25 0.50 10/25/15 16:560.25 1,1-Dichloroethene ug/L <0.25 0.50 10/25/15 16:560.25 1,1-Dichloropropene ug/L <0.25 0.50 10/25/15 16:560.25 1,2,3-Trichlorobenzene ug/L <1.0 2.0 10/25/15 16:561.0 1,2,3-Trichloropropane ug/L <0.25 0.50 10/25/15 16:560.25 1,2,4-Trichlorobenzene ug/L <1.0 2.0 10/25/15 16:561.0 1,2,4-Trimethylbenzene ug/L <0.25 0.50 10/25/15 16:560.25 1,2-Dibromo-3-chloropropane ug/L <0.50 1.0 10/25/15 16:560.50 1,2-Dibromoethane (EDB)ug/L <0.25 0.50 10/25/15 16:560.25 1,2-Dichlorobenzene ug/L <0.25 0.50 10/25/15 16:560.25 1,2-Dichloroethane ug/L <0.25 0.50 10/25/15 16:560.25 1,2-Dichloropropane ug/L <0.25 0.50 10/25/15 16:560.25 1,3,5-Trimethylbenzene ug/L <0.25 0.50 10/25/15 16:560.25 1,3-Dichlorobenzene ug/L <0.25 0.50 10/25/15 16:560.25 1,3-Dichloropropane ug/L <0.25 0.50 10/25/15 16:560.25 1,4-Dichlorobenzene ug/L <0.25 0.50 10/25/15 16:560.25 2,2-Dichloropropane ug/L <0.25 0.50 10/25/15 16:560.25 2-Chlorotoluene ug/L <0.25 0.50 10/25/15 16:560.25 4-Chlorotoluene ug/L <0.25 0.50 10/25/15 16:560.25 Benzene ug/L <0.25 0.50 10/25/15 16:560.25 Bromobenzene ug/L <0.25 0.50 10/25/15 16:560.25 Bromochloromethane ug/L <0.25 0.50 10/25/15 16:560.25 Bromodichloromethane ug/L <0.25 0.50 10/25/15 16:560.25 Bromoform ug/L <0.25 0.50 10/25/15 16:560.25 Bromomethane ug/L <0.50 5.0 10/25/15 16:560.50 Carbon tetrachloride ug/L <0.25 0.50 10/25/15 16:560.25 Chlorobenzene ug/L <0.25 0.50 10/25/15 16:560.25 Chloroethane ug/L <0.50 1.0 10/25/15 16:560.50 Chloroform ug/L <0.25 0.50 10/25/15 16:560.25 Chloromethane ug/L <0.50 1.0 10/25/15 16:560.50 cis-1,2-Dichloroethene ug/L <0.25 0.50 10/25/15 16:560.25 cis-1,3-Dichloropropene ug/L <0.25 0.50 10/25/15 16:560.25 Dibromochloromethane ug/L <0.25 0.50 10/25/15 16:560.25 Dibromomethane ug/L <0.25 0.50 10/25/15 16:560.25 Dichlorodifluoromethane ug/L <0.25 0.50 10/25/15 16:560.25 Diisopropyl ether ug/L <0.25 0.50 10/25/15 16:560.25 Ethylbenzene ug/L <0.25 0.50 10/25/15 16:560.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 50 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591165 Associated Lab Samples:92272667002, 92272667003, 92272667004 Matrix:Water AnalyzedMDL Hexachloro-1,3-butadiene ug/L <1.0 2.0 10/25/15 16:561.0 Isopropylbenzene (Cumene)ug/L <0.25 0.50 10/25/15 16:560.25 m&p-Xylene ug/L <0.50 1.0 10/25/15 16:560.50 Methyl-tert-butyl ether ug/L <0.25 0.50 10/25/15 16:560.25 Methylene Chloride ug/L <1.0 2.0 10/25/15 16:561.0 n-Butylbenzene ug/L <0.25 0.50 10/25/15 16:560.25 n-Propylbenzene ug/L <0.25 0.50 10/25/15 16:560.25 Naphthalene ug/L <1.0 2.0 10/25/15 16:561.0 o-Xylene ug/L <0.25 0.50 10/25/15 16:560.25 sec-Butylbenzene ug/L <0.25 0.50 10/25/15 16:560.25 Styrene ug/L <0.25 0.50 10/25/15 16:560.25 tert-Butylbenzene ug/L <0.25 0.50 10/25/15 16:560.25 Tetrachloroethene ug/L <0.25 0.50 10/25/15 16:560.25 Toluene ug/L <0.25 0.50 10/25/15 16:560.25 trans-1,2-Dichloroethene ug/L <0.25 0.50 10/25/15 16:560.25 trans-1,3-Dichloropropene ug/L <0.25 0.50 10/25/15 16:560.25 Trichloroethene ug/L <0.25 0.50 10/25/15 16:560.25 Trichlorofluoromethane ug/L <0.50 1.0 10/25/15 16:560.50 Vinyl chloride ug/L <0.25 1.0 10/25/15 16:560.25 1,2-Dichloroethane-d4 (S)%109 70-130 10/25/15 16:56 4-Bromofluorobenzene (S)%99 70-130 10/25/15 16:56 Toluene-d8 (S)%101 70-130 10/25/15 16:56 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591166LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 51.450 103 60-140 1,1,1-Trichloroethane ug/L 55.750 111 60-140 1,1,2,2-Tetrachloroethane ug/L 50.850 102 60-140 1,1,2-Trichloroethane ug/L 46.850 94 60-140 1,1-Dichloroethane ug/L 53.550 107 60-140 1,1-Dichloroethene ug/L 57.150 114 60-140 1,1-Dichloropropene ug/L 52.550 105 60-140 1,2,3-Trichlorobenzene ug/L 45.650 91 60-140 1,2,3-Trichloropropane ug/L 50.150 100 60-140 1,2,4-Trichlorobenzene ug/L 46.950 94 60-140 1,2,4-Trimethylbenzene ug/L 51.250 102 60-140 1,2-Dibromo-3-chloropropane ug/L 51.050 102 60-140 1,2-Dibromoethane (EDB)ug/L 50.450 101 60-140 1,2-Dichlorobenzene ug/L 49.450 99 60-140 1,2-Dichloroethane ug/L 47.050 94 60-140 1,2-Dichloropropane ug/L 49.150 98 60-140 1,3,5-Trimethylbenzene ug/L 52.250 104 60-140 1,3-Dichlorobenzene ug/L 50.250 100 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 51 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591166LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 50.450 101 60-140 1,4-Dichlorobenzene ug/L 49.650 99 60-140 2,2-Dichloropropane ug/L 58.050 116 60-140 2-Chlorotoluene ug/L 50.950 102 60-140 4-Chlorotoluene ug/L 51.250 102 60-140 Benzene ug/L 49.650 99 60-140 Bromobenzene ug/L 50.550 101 60-140 Bromochloromethane ug/L 51.350 103 60-140 Bromodichloromethane ug/L 52.350 105 60-140 Bromoform ug/L 47.250 94 60-140 Bromomethane ug/L 34.250 68 60-140 Carbon tetrachloride ug/L 55.550 111 60-140 Chlorobenzene ug/L 49.150 98 60-140 Chloroethane ug/L 44.850 90 60-140 Chloroform ug/L 53.250 106 60-140 Chloromethane ug/L 46.950 94 60-140 cis-1,2-Dichloroethene ug/L 51.650 103 60-140 cis-1,3-Dichloropropene ug/L 51.950 104 60-140 Dibromochloromethane ug/L 51.950 104 60-140 Dibromomethane ug/L 46.950 94 60-140 Dichlorodifluoromethane ug/L 44.750 89 60-140 Diisopropyl ether ug/L 54.850 110 60-140 Ethylbenzene ug/L 51.450 103 60-140 Hexachloro-1,3-butadiene ug/L 56.150 112 60-140 Isopropylbenzene (Cumene)ug/L 56.250 112 60-140 m&p-Xylene ug/L 104100 104 60-140 Methyl-tert-butyl ether ug/L 51.650 103 60-140 Methylene Chloride ug/L 55.450 111 60-140 n-Butylbenzene ug/L 53.550 107 60-140 n-Propylbenzene ug/L 51.950 104 60-140 Naphthalene ug/L 48.150 96 60-140 o-Xylene ug/L 51.650 103 60-140 sec-Butylbenzene ug/L 55.450 111 60-140 Styrene ug/L 51.450 103 60-140 tert-Butylbenzene ug/L 51.550 103 60-140 Tetrachloroethene ug/L 52.350 105 60-140 Toluene ug/L 49.550 99 60-140 trans-1,2-Dichloroethene ug/L 53.650 107 60-140 trans-1,3-Dichloropropene ug/L 51.350 103 60-140 Trichloroethene ug/L 49.050 98 60-140 Trichlorofluoromethane ug/L 50.350 101 60-140 Vinyl chloride ug/L 49.150 98 60-140 1,2-Dichloroethane-d4 (S)%108 70-130 4-Bromofluorobenzene (S)%99 70-130 Toluene-d8 (S)%99 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 52 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591722MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92272667004 1591723 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 110 60-140112 2 3020<0.25 22.0 22.3 1,1,1-Trichloroethane ug/L 20 128 60-140133 4 3020<0.25 25.7 26.6 1,1,2,2-Tetrachloroethane ug/L 20 105 60-140109 4 3020<0.25 21.1 21.9 1,1,2-Trichloroethane ug/L 20 102 60-140106 4 3020<0.25 20.4 21.1 1,1-Dichloroethane ug/L 20 121 60-140124 3 3020<0.25 24.1 24.9 1,1-Dichloroethene ug/L 20 135 60-140140 3 3020<0.25 27.0 28.0 1,1-Dichloropropene ug/L 20 119 60-140124 4 3020<0.25 23.8 24.8 1,2,3-Trichlorobenzene ug/L 20 100 60-140103 3 3020<1.0 19.9 20.6 1,2,3-Trichloropropane ug/L 20 105 60-140108 3 3020<0.25 21.0 21.7 1,2,4-Trichlorobenzene ug/L 20 100 60-140101 2 3020<1.0 19.9 20.2 1,2,4-Trimethylbenzene ug/L 20 111 60-140113 1 3020<0.25 22.3 22.6 1,2-Dibromo-3- chloropropane ug/L 20 107 60-140112 4 3020<0.50 21.4 22.4 1,2-Dibromoethane (EDB)ug/L 20 108 60-140111 3 3020<0.25 21.6 22.2 1,2-Dichlorobenzene ug/L 20 109 60-140110 1 3020<0.25 21.9 22.1 1,2-Dichloroethane ug/L 20 104 60-140108 4 3020<0.25 20.9 21.7 1,2-Dichloropropane ug/L 20 111 60-140114 3 3020<0.25 22.2 22.8 1,3,5-Trimethylbenzene ug/L 20 111 60-140113 1 3020<0.25 22.3 22.6 1,3-Dichlorobenzene ug/L 20 110 60-140113 3 3020<0.25 21.9 22.5 1,3-Dichloropropane ug/L 20 107 60-140110 3 3020<0.25 21.5 22.1 1,4-Dichlorobenzene ug/L 20 109 60-140111 2 3020<0.25 21.8 22.2 2,2-Dichloropropane ug/L 20 132 60-140136 3 3020<0.25 26.4 27.3 2-Chlorotoluene ug/L 20 114 60-140118 3 3020<0.25 22.9 23.6 4-Chlorotoluene ug/L 20 115 60-140117 2 3020<0.25 23.0 23.5 Benzene ug/L 20 110 60-140114 4 3020<0.25 22.0 22.8 Bromobenzene ug/L 20 114 60-140116 1 3020<0.25 22.9 23.1 Bromochloromethane ug/L 20 113 60-140116 2 3020<0.25 22.7 23.1 Bromodichloromethane ug/L 20 111 60-140117 5 3020<0.25 22.2 23.4 Bromoform ug/L 20 87 60-14092 5 3020<0.25 17.5 18.3 Bromomethane ug/L 20 102 60-140104 2 3020<0.50 20.4 20.7 Carbon tetrachloride ug/L 20 129 60-140133 3 3020<0.25 25.8 26.6 Chlorobenzene ug/L 20 107 60-140111 3 3020<0.25 21.4 22.1 Chloroethane ug/L 20 102 60-140108 5 3020<0.50 20.5 21.6 Chloroform ug/L 20 116 60-140121 4 3020<0.25 23.3 24.3 Chloromethane ug/L 20 121 60-140125 4 3020<0.50 24.1 25.1 cis-1,2-Dichloroethene ug/L 20 116 60-140122 5 3020<0.25 23.3 24.4 cis-1,3-Dichloropropene ug/L 20 109 60-140112 3 3020<0.25 21.7 22.5 Dibromochloromethane ug/L 20 104 60-140109 5 3020<0.25 20.9 21.9 Dibromomethane ug/L 20 99 60-140104 5 3020<0.25 19.8 20.8 Dichlorodifluoromethane ug/L 20 114 60-140120 5 3020<0.25 22.9 24.1 Diisopropyl ether ug/L 20 124 60-140128 4 3020<0.25 24.7 25.7 Ethylbenzene ug/L 20 112 60-140115 3 3020<0.25 22.3 23.0 Hexachloro-1,3-butadiene ug/L 20 111 60-140110 1 3020<1.0 22.1 21.9 Isopropylbenzene (Cumene)ug/L 20 119 60-140122 2 3020<0.25 23.9 24.4 m&p-Xylene ug/L 40 111 60-140115 4 3040<0.50 44.2 45.9 Methyl-tert-butyl ether ug/L 20 113 60-140118 4 3020<0.25 22.6 23.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 53 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591722MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92272667004 1591723 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 117 60-140125 6 3020<1.0 23.5 24.9 n-Butylbenzene ug/L 20 109 60-140108 0 3020<0.25 21.7 21.6 n-Propylbenzene ug/L 20 116 60-140117 1 3020<0.25 23.1 23.4 Naphthalene ug/L 20 105 60-140106 1 3020<1.0 21.0 21.1 o-Xylene ug/L 20 111 60-140114 3 3020<0.25 22.2 22.9 sec-Butylbenzene ug/L 20 117 60-140119 1 3020<0.25 23.4 23.7 Styrene ug/L 20 107 60-140109 2 3020<0.25 21.5 21.9 tert-Butylbenzene ug/L 20 110 60-140113 3 3020<0.25 22.1 22.6 Tetrachloroethene ug/L 20 114 60-140116 2 3020<0.25 22.8 23.2 Toluene ug/L 20 109 60-140114 5 3020<0.25 21.7 22.7 trans-1,2-Dichloroethene ug/L 20 124 60-140128 4 3020<0.25 24.7 25.6 trans-1,3-Dichloropropene ug/L 20 110 60-140115 4 3020<0.25 22.1 22.9 Trichloroethene ug/L 20 110 60-140112 2 3020<0.25 22.0 22.4 Trichlorofluoromethane ug/L 20 118 60-140121 2 3020<0.50 23.6 24.1 Vinyl chloride ug/L 20 122 60-140124 2 3020<0.25 24.3 24.8 1,2-Dichloroethane-d4 (S)%109 70-130109 4-Bromofluorobenzene (S)%95 70-13097 Toluene-d8 (S)%100 70-130101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 54 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MSV/33974 SM 6200B SM 6200B 6200B MSV Associated Lab Samples:92272667005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591167 Associated Lab Samples:92272667005 Matrix:Water AnalyzedMDL 1,1,1,2-Tetrachloroethane ug/L <0.25 0.50 10/25/15 23:530.25 1,1,1-Trichloroethane ug/L <0.25 0.50 10/25/15 23:530.25 1,1,2,2-Tetrachloroethane ug/L <0.25 0.50 10/25/15 23:530.25 1,1,2-Trichloroethane ug/L <0.25 0.50 10/25/15 23:530.25 1,1-Dichloroethane ug/L <0.25 0.50 10/25/15 23:530.25 1,1-Dichloroethene ug/L <0.25 0.50 10/25/15 23:530.25 1,1-Dichloropropene ug/L <0.25 0.50 10/25/15 23:530.25 1,2,3-Trichlorobenzene ug/L <1.0 2.0 10/25/15 23:531.0 1,2,3-Trichloropropane ug/L <0.25 0.50 10/25/15 23:530.25 1,2,4-Trichlorobenzene ug/L <1.0 2.0 10/25/15 23:531.0 1,2,4-Trimethylbenzene ug/L <0.25 0.50 10/25/15 23:530.25 1,2-Dibromo-3-chloropropane ug/L <0.50 1.0 10/25/15 23:530.50 1,2-Dibromoethane (EDB)ug/L <0.25 0.50 10/25/15 23:530.25 1,2-Dichlorobenzene ug/L <0.25 0.50 10/25/15 23:530.25 1,2-Dichloroethane ug/L <0.25 0.50 10/25/15 23:530.25 1,2-Dichloropropane ug/L <0.25 0.50 10/25/15 23:530.25 1,3,5-Trimethylbenzene ug/L <0.25 0.50 10/25/15 23:530.25 1,3-Dichlorobenzene ug/L <0.25 0.50 10/25/15 23:530.25 1,3-Dichloropropane ug/L <0.25 0.50 10/25/15 23:530.25 1,4-Dichlorobenzene ug/L <0.25 0.50 10/25/15 23:530.25 2,2-Dichloropropane ug/L <0.25 0.50 10/25/15 23:530.25 2-Chlorotoluene ug/L <0.25 0.50 10/25/15 23:530.25 4-Chlorotoluene ug/L <0.25 0.50 10/25/15 23:530.25 Benzene ug/L <0.25 0.50 10/25/15 23:530.25 Bromobenzene ug/L <0.25 0.50 10/25/15 23:530.25 Bromochloromethane ug/L <0.25 0.50 10/25/15 23:530.25 Bromodichloromethane ug/L <0.25 0.50 10/25/15 23:530.25 Bromoform ug/L <0.25 0.50 10/25/15 23:530.25 Bromomethane ug/L <0.50 5.0 10/25/15 23:530.50 Carbon tetrachloride ug/L <0.25 0.50 10/25/15 23:530.25 Chlorobenzene ug/L <0.25 0.50 10/25/15 23:530.25 Chloroethane ug/L <0.50 1.0 10/25/15 23:530.50 Chloroform ug/L <0.25 0.50 10/25/15 23:530.25 Chloromethane ug/L <0.50 1.0 10/25/15 23:530.50 cis-1,2-Dichloroethene ug/L <0.25 0.50 10/25/15 23:530.25 cis-1,3-Dichloropropene ug/L <0.25 0.50 10/25/15 23:530.25 Dibromochloromethane ug/L <0.25 0.50 10/25/15 23:530.25 Dibromomethane ug/L <0.25 0.50 10/25/15 23:530.25 Dichlorodifluoromethane ug/L <0.25 0.50 10/25/15 23:530.25 Diisopropyl ether ug/L <0.25 0.50 10/25/15 23:530.25 Ethylbenzene ug/L <0.25 0.50 10/25/15 23:530.25 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 55 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1591167 Associated Lab Samples:92272667005 Matrix:Water AnalyzedMDL Hexachloro-1,3-butadiene ug/L <1.0 2.0 10/25/15 23:531.0 Isopropylbenzene (Cumene)ug/L <0.25 0.50 10/25/15 23:530.25 m&p-Xylene ug/L <0.50 1.0 10/25/15 23:530.50 Methyl-tert-butyl ether ug/L <0.25 0.50 10/25/15 23:530.25 Methylene Chloride ug/L <1.0 2.0 10/25/15 23:531.0 n-Butylbenzene ug/L <0.25 0.50 10/25/15 23:530.25 n-Propylbenzene ug/L <0.25 0.50 10/25/15 23:530.25 Naphthalene ug/L <1.0 2.0 10/25/15 23:531.0 o-Xylene ug/L <0.25 0.50 10/25/15 23:530.25 sec-Butylbenzene ug/L <0.25 0.50 10/25/15 23:530.25 Styrene ug/L <0.25 0.50 10/25/15 23:530.25 tert-Butylbenzene ug/L <0.25 0.50 10/25/15 23:530.25 Tetrachloroethene ug/L <0.25 0.50 10/25/15 23:530.25 Toluene ug/L <0.25 0.50 10/25/15 23:530.25 trans-1,2-Dichloroethene ug/L <0.25 0.50 10/25/15 23:530.25 trans-1,3-Dichloropropene ug/L <0.25 0.50 10/25/15 23:530.25 Trichloroethene ug/L <0.25 0.50 10/25/15 23:530.25 Trichlorofluoromethane ug/L <0.50 1.0 10/25/15 23:530.50 Vinyl chloride ug/L <0.25 1.0 10/25/15 23:530.25 1,2-Dichloroethane-d4 (S)%107 70-130 10/25/15 23:53 4-Bromofluorobenzene (S)%97 70-130 10/25/15 23:53 Toluene-d8 (S)%100 70-130 10/25/15 23:53 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591168LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 50.250 100 60-140 1,1,1-Trichloroethane ug/L 55.650 111 60-140 1,1,2,2-Tetrachloroethane ug/L 50.650 101 60-140 1,1,2-Trichloroethane ug/L 47.450 95 60-140 1,1-Dichloroethane ug/L 52.550 105 60-140 1,1-Dichloroethene ug/L 56.050 112 60-140 1,1-Dichloropropene ug/L 51.550 103 60-140 1,2,3-Trichlorobenzene ug/L 45.550 91 60-140 1,2,3-Trichloropropane ug/L 50.850 102 60-140 1,2,4-Trichlorobenzene ug/L 46.750 93 60-140 1,2,4-Trimethylbenzene ug/L 51.250 102 60-140 1,2-Dibromo-3-chloropropane ug/L 53.850 108 60-140 1,2-Dibromoethane (EDB)ug/L 50.050 100 60-140 1,2-Dichlorobenzene ug/L 50.350 101 60-140 1,2-Dichloroethane ug/L 47.250 94 60-140 1,2-Dichloropropane ug/L 48.650 97 60-140 1,3,5-Trimethylbenzene ug/L 52.150 104 60-140 1,3-Dichlorobenzene ug/L 50.250 100 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 56 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1591168LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichloropropane ug/L 49.750 99 60-140 1,4-Dichlorobenzene ug/L 49.350 99 60-140 2,2-Dichloropropane ug/L 50.950 102 60-140 2-Chlorotoluene ug/L 51.150 102 60-140 4-Chlorotoluene ug/L 51.550 103 60-140 Benzene ug/L 49.050 98 60-140 Bromobenzene ug/L 51.050 102 60-140 Bromochloromethane ug/L 52.350 105 60-140 Bromodichloromethane ug/L 52.050 104 60-140 Bromoform ug/L 45.950 92 60-140 Bromomethane ug/L 31.950 64 60-140 Carbon tetrachloride ug/L 55.450 111 60-140 Chlorobenzene ug/L 48.250 96 60-140 Chloroethane ug/L 43.550 87 60-140 Chloroform ug/L 51.950 104 60-140 Chloromethane ug/L 41.150 82 60-140 cis-1,2-Dichloroethene ug/L 51.550 103 60-140 cis-1,3-Dichloropropene ug/L 50.150 100 60-140 Dibromochloromethane ug/L 51.150 102 60-140 Dibromomethane ug/L 46.950 94 60-140 Dichlorodifluoromethane ug/L 43.450 87 60-140 Diisopropyl ether ug/L 55.150 110 60-140 Ethylbenzene ug/L 49.950 100 60-140 Hexachloro-1,3-butadiene ug/L 53.550 107 60-140 Isopropylbenzene (Cumene)ug/L 54.550 109 60-140 m&p-Xylene ug/L 100100 100 60-140 Methyl-tert-butyl ether ug/L 51.950 104 60-140 Methylene Chloride ug/L 55.150 110 60-140 n-Butylbenzene ug/L 51.750 103 60-140 n-Propylbenzene ug/L 51.650 103 60-140 Naphthalene ug/L 49.150 98 60-140 o-Xylene ug/L 50.450 101 60-140 sec-Butylbenzene ug/L 54.050 108 60-140 Styrene ug/L 50.450 101 60-140 tert-Butylbenzene ug/L 51.250 102 60-140 Tetrachloroethene ug/L 49.650 99 60-140 Toluene ug/L 49.150 98 60-140 trans-1,2-Dichloroethene ug/L 53.350 107 60-140 trans-1,3-Dichloropropene ug/L 51.750 103 60-140 Trichloroethene ug/L 47.650 95 60-140 Trichlorofluoromethane ug/L 48.650 97 60-140 Vinyl chloride ug/L 48.350 97 60-140 1,2-Dichloroethane-d4 (S)%108 70-130 4-Bromofluorobenzene (S)%97 70-130 Toluene-d8 (S)%98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 57 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591724MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92273005002 1591725 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 111 60-140112 1 3020ND22.2 22.3 1,1,1-Trichloroethane ug/L 20 131 60-140133 2 3020ND26.2 26.7 1,1,2,2-Tetrachloroethane ug/L 20 107 60-140111 4 3020ND21.3 22.2 1,1,2-Trichloroethane ug/L 20 104 60-140105 1 3020ND20.7 21.0 1,1-Dichloroethane ug/L 20 122 60-140126 3 3020ND24.5 25.1 1,1-Dichloroethene ug/L M12013860-140141 3 3020ND27.5 28.2 1,1-Dichloropropene ug/L 20 121 60-140123 2 3020ND24.2 24.7 1,2,3-Trichlorobenzene ug/L 20 103 60-140104 1 3020ND20.7 20.9 1,2,3-Trichloropropane ug/L 20 108 60-140110 2 3020ND21.6 21.9 1,2,4-Trichlorobenzene ug/L 20 103 60-140102 1 3020ND20.6 20.3 1,2,4-Trimethylbenzene ug/L 20 116 60-140117 1 3020ND23.1 23.4 1,2-Dibromo-3- chloropropane ug/L 20 112 60-140120 7 3020ND22.4 24.0 1,2-Dibromoethane (EDB)ug/L 20 109 60-140111 2 3020ND21.8 22.3 1,2-Dichlorobenzene ug/L 20 112 60-140111 0 3020ND22.4 22.3 1,2-Dichloroethane ug/L 20 108 60-140108 1 30200.53 22.1 22.2 1,2-Dichloropropane ug/L 20 112 60-140113 1 3020ND22.3 22.6 1,3,5-Trimethylbenzene ug/L 20 118 60-140118 0 3020ND23.5 23.6 1,3-Dichlorobenzene ug/L 20 113 60-140114 1 3020ND22.6 22.7 1,3-Dichloropropane ug/L 20 110 60-140112 2 3020ND22.0 22.4 1,4-Dichlorobenzene ug/L 20 110 60-140111 1 3020ND21.9 22.2 2,2-Dichloropropane ug/L 20 134 60-140136 2 3020ND26.7 27.3 2-Chlorotoluene ug/L 20 116 60-140119 3 3020ND23.2 23.9 4-Chlorotoluene ug/L 20 117 60-140119 1 3020ND23.4 23.7 Benzene ug/L 20 112 60-140113 1 3020ND22.4 22.6 Bromobenzene ug/L 20 110 60-140116 6 3020ND22.0 23.3 Bromochloromethane ug/L 20 114 60-140118 4 3020ND22.7 23.6 Bromodichloromethane ug/L 20 113 60-140116 2 3020ND22.6 23.1 Bromoform ug/L 20 89 60-14094 6 3020ND17.8 18.9 Bromomethane ug/L 20 102 60-140103 0 3020ND20.5 20.6 Carbon tetrachloride ug/L 20 130 60-140131 1 3020ND25.9 26.1 Chlorobenzene ug/L 20 109 60-140111 2 3020ND21.9 22.2 Chloroethane ug/L 20 104 60-140108 4 3020ND20.9 21.7 Chloroform ug/L 20 120 60-140123 2 3020ND24.1 24.6 Chloromethane ug/L 20 122 60-140127 4 3020ND24.5 25.5 cis-1,2-Dichloroethene ug/L 20 120 60-140122 1 3020ND24.0 24.3 cis-1,3-Dichloropropene ug/L 20 111 60-140113 1 3020ND22.2 22.5 Dibromochloromethane ug/L 20 106 60-140110 4 3020ND21.2 22.0 Dibromomethane ug/L 20 101 60-140101 0 3020ND20.2 20.2 Dichlorodifluoromethane ug/L 20 119 60-140118 1 3020ND23.9 23.6 Diisopropyl ether ug/L 20 127 60-140129 1 3020ND25.6 25.9 Ethylbenzene ug/L 20 113 60-140116 3 3020ND22.7 23.3 Hexachloro-1,3-butadiene ug/L 20 112 60-140115 3 3020ND22.4 23.1 Isopropylbenzene (Cumene)ug/L 20 121 60-140124 3 3020ND24.2 24.9 m&p-Xylene ug/L 40 114 60-140116 2 3040ND45.5 46.4 Methyl-tert-butyl ether ug/L 20 116 60-140119 3 30201.1 24.2 24.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 58 of 64 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1591724MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92273005002 1591725 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Methylene Chloride ug/L 20 123 60-140126 2 3020ND24.6 25.2 n-Butylbenzene ug/L 20 111 60-140113 2 3020ND22.1 22.5 n-Propylbenzene ug/L 20 118 60-140120 2 3020ND23.6 24.0 Naphthalene ug/L 20 110 60-140114 3 3020ND22.0 22.8 o-Xylene ug/L 20 113 60-140116 3 3020ND22.6 23.3 sec-Butylbenzene ug/L 20 118 60-140122 3 3020ND23.7 24.4 Styrene ug/L 20 109 60-140111 2 3020ND21.8 22.2 tert-Butylbenzene ug/L 20 114 60-140116 2 3020ND22.8 23.3 Tetrachloroethene ug/L 20 114 60-140119 4 3020ND22.8 23.8 Toluene ug/L 20 111 60-140112 1 3020ND22.2 22.4 trans-1,2-Dichloroethene ug/L 20 128 60-140130 2 3020ND25.5 25.9 trans-1,3-Dichloropropene ug/L 20 113 60-140114 1 3020ND22.6 22.9 Trichloroethene ug/L 20 111 60-140112 1 3020ND22.2 22.3 Trichlorofluoromethane ug/L 20 120 60-140121 1 3020ND24.0 24.2 Vinyl chloride ug/L 20 121 60-140125 3 3020ND24.2 24.9 1,2-Dichloroethane-d4 (S)%110 70-130110 4-Bromofluorobenzene (S)%95 70-13097 Toluene-d8 (S)%99 70-13099 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 59 of 64 #=QL# QUALIFIERS Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - CharlottePASI-C ANALYTE QUALIFIERS Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 60 of 64 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92272667 PANTRY 3079 45.42017.3079 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92272667001 MPRP/19875 ICP/17929MW-1 EPA 3010 EPA 6010 92272667002 MPRP/19875 ICP/17929MW-2 EPA 3010 EPA 6010 92272667003 MPRP/19875 ICP/17929MW-3 EPA 3010 EPA 6010 92272667004 MPRP/19876 ICP/17931MW-7 EPA 3010 EPA 6010 92272667005 MPRP/19876 ICP/17931MW-8 EPA 3010 EPA 6010 92272667006 MPRP/19876 ICP/17931MW-9 EPA 3010 EPA 6010 92272667007 MPRP/19876 ICP/17931MW-10 EPA 3010 EPA 6010 92272667008 MPRP/19876 ICP/17931MW-11 EPA 3010 EPA 6010 92272667009 MPRP/19876 ICP/17931MW-12 EPA 3010 EPA 6010 92272667010 MPRP/19876 ICP/17931MW-13 EPA 3010 EPA 6010 92272667011 MPRP/19876 ICP/17931MW-14 EPA 3010 EPA 6010 92272667012 MPRP/19876 ICP/17931MW-15 EPA 3010 EPA 6010 92272667013 MPRP/19876 ICP/17931MW-17 EPA 3010 EPA 6010 92272667014 MPRP/19876 ICP/17931MW-18 EPA 3010 EPA 6010 92272667015 MPRP/19876 ICP/17931MW-19 EPA 3010 EPA 6010 92272667001 MSV/33965MW-1 SM 6200B 92272667002 MSV/33973MW-2 SM 6200B 92272667003 MSV/33973MW-3 SM 6200B 92272667004 MSV/33973MW-7 SM 6200B 92272667005 MSV/33974MW-8 SM 6200B 92272667006 MSV/33966MW-9 SM 6200B 92272667007 MSV/33966MW-10 SM 6200B 92272667008 MSV/33966MW-11 SM 6200B 92272667009 MSV/33966MW-12 SM 6200B 92272667010 MSV/33966MW-13 SM 6200B 92272667011 MSV/33966MW-14 SM 6200B 92272667012 MSV/33966MW-15 SM 6200B 92272667013 MSV/33966MW-17 SM 6200B 92272667014 MSV/33966MW-18 SM 6200B 92272667015 MSV/33966MW-19 SM 6200B REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 10/29/2015 03:06 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 61 of 64 Page 62 of 64 Page 63 of 64 Page 64 of 64