RA-641_4028_CA_MRP_20150519

Active Remediation Monitoring Report

Pantry #3079
5102 Dortches Boulevard
Rocky Mount, Nash County, North Carolina
Risk Classification: High
NCDENR Facility I.D. No. 0-022631
NCDENR Incident No. 4028
ATC Project No. 45.42017.3079

TABLE OF CONTENTS
1.0 INTRODUCTION .................................................................................................................... 1
2.0 SITE BACKGROUND ............................................................................................................ 1
3.0 MOBILE MULTI-PHASE EXTRACTION EVENT .......................................................... 2
4.0 GROUNDWATER CHARACTERIZATION ..................................................................... 3 4.1 Groundwater Levels ........................................................................................................ 3
4.2 Free Product .................................................................................................................... 3
4.3 Groundwater Quality....................................................................................................... 4
5.0 SUMMARY ............................................................................................................................... 4

TABLES
Table 1 UST System Information Table 2 Water Supply Well Information Table 3 Table 4 Table 5
Monitoring Well Construction Information Groundwater Elevation Information Groundwater Analytical Data Table 6 Table 7
Historical Groundwater Analytical Data Natural Attenuation Data

FIGURES
Figure 1 Topographic Map Figure 2 Site Map Figure 3 Site Vicinity Map Figure 4 Groundwater Elevation Contour Map Figure 5 Dissolved Benzene Isoconcentration Contour Map Figure 6 Figure 7 Dissolved MTBE Isoconcentration Contour Map Dissolved Naphthalene Isoconcentration Contour Map

APPENDICES Appendix A Appendix B Appendix C
Methods MMPE Summary Report and Disposal Manifests Laboratory Analytical Report
Pantry #3079 – Active Remediation Monitoring Report May 19, 2015
NCDENR Incident No. 4028 ATC Project No. 45.42017.3079
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1.0 INTRODUCTION

ATC Associates of North Carolina, P.C. (ATC) was retained by The Pantry, Inc. (The Pantry) to
perform assessment and corrective action activities at the Pantry #3079 site located at 5102
Dortches Boulevard in Rocky Mount, North Carolina. The site location is shown on Figure 1, and
the site details are shown on Figure 2. This report presents a summary of a mobile multi-phase
extraction (MMPE) event conducted in March 2015 and laboratory analytical results for the
groundwater sampling event conducted in April 8, 2015.

2.0 SITE BACKGROUND

The Pantry #3079 (DBA Zip Mart #6) is a convenience and gasoline retail store located at 5102
Dortches Boulevard (Highway 43 at I-95) in Rocky Mount, Nash County, North Carolina. The site
is currently active and contains three 12,000-gallon gasoline underground storage tanks (USTs) and
one 8,000-gallon diesel UST. Table 1 provides a summary of the current and former UST
systems at the site.

In February 1989, four 12,000-gallon USTs were removed from the Zip Mart #6 facility. Analytical
results of the soil samples collected from the UST bed indicated elevated levels of total petroleum
hydrocarbons (TPH) in both the gasoline and diesel range. Between April 1989 and May 1990,
Applied Environmental Services, Inc. installed fifteen monitoring wells (MW-1 through MW-15).
On July 2, 1990, Applied Environmental Services, Inc. submitted a Groundwater Assessment –
Technical and Field Data Report and a Remedial Action Plan and Engineering Report.

In July 1998, after discovery of the suspected release, The Pantry, Inc. assumed store operations
from Stallings Oil Company, Inc. Subsequently, environmental services were transferred to SEI
Environmental, Inc. and SEI Engineering and Geological Services, P.C. (formerly SPATCO
Engineering and Geological Services, P.C.) (SEI).

During September and November 1999 and again in April 2002, a 1,500-foot receptor survey
was conducted which revealed the presence of two potable water supply wells. Public water is
Pantry #3079 – Active Remediation Monitoring Report May 19, 2015
NCDENR Incident No. 4028 ATC Project No. 45.42017.3079
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supplied to the area. An intermittent stream is located approximately 1,500 feet west of the
subject property. Refer to Figure 3 for a site vicinity map. Information regarding properties
with water supply wells is summarized in Table 2.

On December 10, 1999, SEI submitted a Pre-Corrective Action Plan (CAP) Groundwater
Monitoring Report. In February and March 2000, aggressive fluid vapor recovery (AFVR) was
conducted on monitoring well MW-1 and recovery well RW-1, which have historically contained
free product. The AFVR events were successful in removing approximately 5,605 gallons of
contaminated groundwater, 62.03 pounds of petroleum vapors, and an immeasurable amount of
free product. Free product has not been detected in any of the groundwater monitoring wells
since March 23, 2000. On April 18, 2000, SEI submitted a Free Product Recovery Report.

On November 21, 2000, three type II monitoring wells (MW-12A, MW-16, and MW-17) were
installed. On August 15, 2001, two additional type II monitoring wells (MW-18 and MW-19) were
installed. Monitoring well construction details are summarized in Table 3. On April 30, 2002, SEI
submitted a Natural Attenuation CAP.

On February 17, 2009, MDSA installed four additional type II monitoring wells (MW-19, MW-20,
MW-21 and MW-22) in the apparent down gradient location of the release. The additional
monitoring wells were installed in an effort to further delineate the extent of the release.
Groundwater sampling events were conducted in July 2009, February 2010, July 2010, March 2011,
and July 2011.
This report presents the results of a MMPE event conducted in March 2015 and a groundwater
sampling event conducted in April 2015.
3.0 MOBILE MULTI-PHASE EXTRACTION EVENT

ATC subcontracted Zebra Environmental to complete the MMPE event at the site. On March 2,
2015 Zebra’s subcontractor, Advanced Environmental (Advanced), mobilized to the site and
connected the MMPE equipment to MW-1 and RW-1. The MMPE was conducted for five days
and recovered a total of 10,007 gallons of impacted groundwater/free product. No measurable
Pantry #3079 – Active Remediation Monitoring Report May 19, 2015
NCDENR Incident No. 4028 ATC Project No. 45.42017.3079
3

free product was observed in MW-1 or RW-1 at the conclusion of the event. A copy of ATCs
standard operating procedures is included in Appendix A. A copy of Advanced’s summary of the
MMPE event and disposal manifest is included in Appendix B. According to Advanced’s event
summary, a calculated 252.85 pounds or 41.10 gallons of VOCs (as gasoline) were removed as
vapor.

4.0 GROUNDWATER CHARACTERIZATION

4.1 Groundwater Levels

Groundwater levels were measured during the recent groundwater sampling event performed on
April 8, 2015. An oil/water interface probe was used to gauge depth-to-water and free product
thickness, if encountered, from the top of each well casing. Free product was encountered in
MW-8 at a thickness of 0.92 feet during the April 2015 event. Groundwater elevations ranged
from 7.07 feet to 16.65 feet below ground surface (bgs) in monitoring wells MW-8 and MW-13,
respectively. A copy of ATCs standard operating procedures is included in Appendix A.

Monitoring well construction details are summarized in Table 3 and groundwater elevation data
from the April 2015 sampling event is included in Table 4. A groundwater elevation map is
included as Figure 4.

4.2 Free Product

Free product was detected in MW-8 at a thickness of 0.92 feet during the April 2015
groundwater sampling event. Free product has not historically been detected in MW-8.
Historically at the site, free product has been detected in MW-1 and RW-1. No measureable free
product was identified in MW-1 or RW-1 prior to the March 2015 MMPE event or at the
conclusion of the event.

Pantry #3079 – Active Remediation Monitoring Report May 19, 2015
NCDENR Incident No. 4028 ATC Project No. 45.42017.3079
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4.3 Groundwater Quality

Groundwater samples were collected from monitoring wells MW-1 through MW-3, MW-7,
MW-9 through MW-15, and MW-17 through MW-19 on April 8, 2015. Monitoring wells MW-
4, MW-20, MW-21, and MW-22 were not located, and MW-16 has been paved over and was
therefore not sampled. ATC personnel were unable to access monitoring wells MW-5 and MW-
6. A disposable polyethylene bailer was used to purge a minimum of three well volumes from
the monitoring wells and recovery wells prior to sample collection. Samples were placed in
laboratory supplied sample containers and shipped on ice via overnight courier to Accutest
Laboratories (Accutest) in Scott, Louisiana. Groundwater samples were analyzed for volatile
organic compounds by EPA Method 6200B and lead by EPA Method 6010B with EPA 3030C
preparation method. A copy of the laboratory analytical report is included in Appendix C.

The results of the laboratory analyses indicated benzene, toluene, ethylbenzene, total xylenes,
MTBE, isopropyl ether, naphthalene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, 1,2-
dibromoethane, 1,2-dichloroethane, isopropylbenzene, methylene chloride, n-propylbenzene,
styrene, and lead at concentrations above 2L Standards in several wells. No concentrations
exceeded the Gross Contamination Levels (GCLs) established by NCDENR. Analytical results
for the monitoring well samples collected in April 2015 are summarized in Table 5. Historical
groundwater analytical data are summarized in Table 6. Natural attenuation data are summarized
in Table 7. Benzene, MTBE, and naphthalene isoconcentration contour maps are included as
Figures 5 through 7, respectively.

5.0 SUMMARY

During this reporting period, ATC completed a groundwater sampling event. Based on the results
of ATC’s assessment, the following conclusions are made:

• Groundwater at the site flows towards a ditch located along western portion of the site and
to the northwest.
• Free product was detected in MW-8 at a thickness of 0.92 feet.
Pantry #3079 – Active Remediation Monitoring Report May 19, 2015
NCDENR Incident No. 4028 ATC Project No. 45.42017.3079
5

• Groundwater samples collected from the monitoring wells in April 2015 contained volatile
organic compounds at concentrations above 2L Standards.
• No concentrations exceeded the GCLs.

Based upon the information presented in this and historical reports, ATC recommends continued
quarterly MMPE events. ATC also recommends continued semi-annual groundwater sampling
events.

TABLES
TABLE 1
UST SYSTEM INFORMATION
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
UST ID
Number Product Capacity (gallons)Date
Installed
Date taken
out of Use
Date
Permanently
Closed
Was Release
Associated With UST
System?
0-022631 Gasoline 12,000 2/8/1989 In Use In Use No
0-022631 Gasoline 12,000 2/8/1989 In Use In Use No
0-022631 Gasoline 12,000 2/8/1989 In Use In Use No
0-022631 Diesel 8,000 2/8/1989 In Use In Use No
0-022631 Gasoline 12,000 5/3/1979 Feb 1989 Feb 1989 Yes
0-022631 Gasoline 6,000 5/3/1979 Feb 1989 Feb 1989 Yes
0-022631 Gasoline 6,000 5/3/1979 Feb 1989 Feb 1989 Yes
0-022631 Gasoline 6,000 5/3/1979 Feb 1989 Feb 1989 Yes
UST ID
Number Owner or Operator?Name of Owner or Operator Dates of Ownership / Operation
The Pantry, Inc.February 1989 to present
Address Telephone Number
0-022631 Owner/Operator
315 West Ridge Street [phone]
0-022643 Stallings Oil Company 5/3/1979 to February 1989 Owner/Operator
Address Telephone Number
Rocky Mount, North Carolina 27801
Cary, North Carolina 27512
PO Box 8019 [phone]
TABLE 2
WATER SUPPLY WELL INFO
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Well NumberWell OwnerAddressPhone NumberWell UseWell Depth (feet bls)Type of WellWell Casing (feet bls)Well Screen Interval (feet bls)Distance for source area release (feet)Cardinal Direction from releaseWW-1 Samuel Cecil Griffin 4976 Dortches Blvd, Rocky Mt, NC [phone] Water Supply Unknown Unknown Unknown Unknown 560 E
WW-2 Jennifer Masters 3662 N. Halifax Rd, Rocky Mt, NC [phone] Water Supply 100 Unknown Unknown Unknown 930 E
TABLE 3
MONITORING WELL CONSTRUCTION INFORMATION
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
WELL I.D.Date Installed
Well
Diameter
(inches)
Screen Slot
Size (inches)
Screened
Interval
(feet)
Total
Depth
(feet)
Date
Abandoned
MW-1 4/4/1989 2 0.01 12-27 27 Active
MW-2 4/4/1989 2 0.01 13-28 28 Active
MW-3 4/5/1989 2 0.01 15-30 30 Active
MW-4 12/4/1989 2 0.01 15.5-25.5 25.5 Active
MW-5 12/4/1989 2 0.01 15.5-25.5 25.5 Active
MW-6 12/5/1989 2 0.01 15-25 25 Active
MW-7 12/5/1989 2 0.01 15-25 25 Active
MW-8 12/5/1989 2 0.01 9-24 24 Active
MW-9 3/14/1990 2 0.01 7.5-22.5 22.5 Active
MW-10 3/14/1990 2 0.01 13-23 23 Active
MW-11 3/14/1990 2 0.01 6-21 21 Active
MW-12A 11/21/2000 2 0.01 13-28 28 Active
MW-13 3/15/1990 2 0.01 9.5-24.5 24.5 Active
MW-14 3/15/1990 2 0.01 15-30 30 Active
MW-15 3/15/1990 2 0.01 5-25 25 Active
MW-16 11/21/2000 2 0.01 57.5-60 60 ActiveMW-17 11/21/2000 2 0.01 9.5-24.5 24.5 Active
MW-18 8/15/2001 2 0.01 9.5-24.5 24.5 Active
MW-19 8/15/2001 2 0.01 10-25 25 Active
MW-20 2/17/2009 2 0.01 5-20 20 Active
MW-21 2/17/2009 2 0.01 5-20 20 ActiveMW-22 2/17/2009 2 0.01 5-20 20 Active
TABLE 4
GROUNDWATER ELEVATION INFORMATION
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
WELL I.D. Date TOC Elevation
(ft)
Depth to
Product (ft)
Depth to
Groundwater (ft)
Product Thickness
(ft)
Groundwater
Elevations (ft)
MW-1 4/8/2015 503.67 --13.48 --490.19
MW-2 4/8/2015 503.96 --14.48 --489.48
MW-3 4/8/2015 504.40 --14.03 --490.37
MW-4 4/8/2015 NS --NM --NM
MW-5 4/8/2015 500.84 --NM --NM
MW-6 4/8/2015 500.32 --NM --NM
MW-7 4/8/2015 499.58 --13.28 --486.30
MW-8 4/8/2015 498.49 6.15 7.07 0.92 492.12
MW-9 4/8/2015 498.97 --8.37 --490.60
MW-10 4/8/2015 502.28 --13.61 --488.67
MW-11 4/8/2015 503.81 --13.60 --490.21
MW-12A 4/8/2015 501.63 --11.96 --489.67
MW-13 4/8/2015 505.80 --16.65 --489.15
MW-14 4/8/2015 503.40 --13.74 --489.66
MW-15 4/8/2015 504.32 --14.81 --489.51
MW-16 4/8/2015 502.57 --NM --NM
MW-17 4/8/2015 502.98 --13.54 --489.44
MW-18 4/8/2015 502.18 --13.25 --488.93
MW-19 4/8/2015 500.78 --11.70 --489.08
MW-20 4/8/2015 492.58 --NM --NM
MW-21 4/8/2015 492.20 --NM --NM
MW-22 4/8/2015 491.93 --NM --NM
Notes:
1. TOC = Top of well casing.
2. NS = Not surveyed.
3. NM = Not monitored during this sampling event.
4. Corrected GW Elev.= (GW Elev. + (Product Thickness*0.76))
TABLE 5
GROUNDWATER ANALYTICAL DATA
PANTRY #30795102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
6010B
MW-1 4/8/2015 2,280 3,530 1,610 6,510 13,930 1,310 788 2.5 2,180 654 15.4 14.7 17.7 <10 <200 <2 79 7.4 <10 <2 11.1 <2 203 15.8 <4 16.5
MW-2 4/8/2015 <0.3 <0.2 <0.2 <0.6 ND 3.4 <0.5 0.1 <0.3 <0.3 <0.1 <0.2 <0.5 <0.5 <10 <0.1 <0.2 <0.1 <0.5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 29.4
MW-3 4/8/2015 <0.3 <0.2 <0.2 <0.6 ND 0.56 <0.5 <0.1 <0.3 <0.3 <0.1 <0.2 <0.5 <0.5 <10 <0.1 <0.2 <0.1 <0.5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 16.7
MW-4 4/8/2015
MW-5 4/8/2015
MW-6 4/8/2015
MW-7 4/8/2015 <0.3 <0.2 <0.2 <0.6 ND <0.2 <0.5 <0.1 <0.3 <0.3 <0.1 <0.2 <0.5 <0.5 <10 <0.1 <0.2 <0.1 <0.5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <10
MW-8 4/8/2015
MW-9 4/8/2015 <0.3 <0.2 <0.2 <0.6 ND <0.2 <0.5 <0.1 <0.3 <0.3 <0.1 <0.2 <0.5 <0.5 <10 0.26 <0.2 <0.1 <0.5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 37.1
MW-10 4/8/2015 <0.3 1.8 <0.2 <0.6 ND <0.2 <0.5 <0.1 <0.3 <0.3 <0.1 <0.2 <0.5 <0.5 <10 <0.1 <0.2 23.5 <0.5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 32.5
MW-11 4/8/2015 1,500 187 2,010 4,430 8,127 355 846 2.1 1,830 611 <2 5.1 <10 <10 <200 <2 106 5.7 <10 <2 12.5 <2 253 14 <4 39.9
MW-12A 4/8/2015 <0.3 <0.2 0.22 <0.6 ND <0.2 2.8 <0.1 0.99 0.57 <0.1 <0.2 <0.5 <0.5 <10 <0.1 4.4 2.3 <0.5 <0.1 6.8 0.17 13.1 <0.1 <0.2 31.4
MW-13 4/8/2015 22.5 6.1 27.3 7.1 63.0 9.9 20.3 <0.1 8.2 2.3 <0.1 0.26 <0.5 <0.5 <10 <0.1 4.7 2.2 <0.5 5.4 4.7 0.13 13.1 0.15 0.55 70
MW-14 4/8/2015 3,400 1,740 2,200 4,510 11,850 399 888 3.9 2,110 685 <2 26 <10 <10 <200 <2 127 8.7 <10 <2 18.5 <2 346 11.2 <4 15.3
MW-15 4/8/2015 <0.3 <0.2 <0.2 <0.6 ND <0.2 0.54 <0.1 <0.3 <0.3 <0.1 <0.2 <0.5 <0.5 <10 <0.1 <0.2 <0.1 <0.5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <10
MW-16 4/8/2015
MW-17 4/8/2015 794 6,520 1,740 5,980 15,034 16.4 1,070 35.7 1,830 465 <5 <10 <25 <25 <500 <5 90.2 10.5 35.6 <5 <5 <5 235 32.4 <10 36.8
MW-18 4/8/2015 2,570 9,840 1,830 7,980 22,220 34.5 696 305 1,280 291 14.5 13.1 <25 <25 <500 <5 66.1 <5 <25 <5 <5 <5 150 72.6 <10 73
MW-19 4/8/2015 <0.3 <0.2 <0.2 <0.6 ND <0.2 <0.5 <0.1 <0.3 <0.3 <0.1 <0.2 <0.5 <0.5 <10 <0.1 <0.2 <0.1 <0.5 <0.1 <0.1 <0.1 <0.1 <0.1 <0.2 <10
MW-20 4/8/2015
MW-21 4/8/2015
MW-22 4/8/2015
RW-1 4/8/2015
1 600 600 500 NE 20 6 70 400 400 0.02 0.4 NE NE 6,000 70 70 25 5 70 70 70 70 70 88 15
5,000 260,000 84,500 85,500 NE 20,000 6,000 70,000 28,500 25,000 50 400 NE NE 6,000,000 70,000 25,000 11,700 5,000 6,900 8,500 15,000 30,000 70,000 88,000 15,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NE = Not established.
5. MTBE = Methyl tertiary butyl ether.
6. Values in BOLD indicate levels above 2L Groundwater Standards.
7. All concentrations in micrograms per liter (ug/L).
Not Sampled - Unable to Access n-PropylbenzeneGCL
2L GW Standard Naphthalene1,3,5-TrimethylbenzeneIsopropylbenzene1,2-Dichloroethane4-Methyl-2-pentanoneActeoneTotal XylenesNot SampledIsopropyl ether1,2-Dibromoethanetert-Butylbenzenep-IsopropyltolueneEPA METHOD 6200B
Methylene Chloride2-HexanoneTolueneNot Sampled - Unable to Locate
Not Sampled - Free Product
Analytical Methods:
DATE
SAMPLEDWELL I.D.LeadNot Sampled - Unable to Locate StyreneBenzeneMTBEn-Butylbenzenesec-ButylbenzeneChloroformVinyl AcetateNot Sampled - Unable to Locate1,2,4-TrimethylbenzeneTotal BTEXEthylbenzeneNot Sampled - Paved Over
Not Sampled - Unable to Locate
Not Sampled - Unable to Access
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
12/29/1989 pre-CAP
10/12/1999 pre-CAP
12/15/2000 pre-CAP 16,000 26,000 3,600 17,400 8,400 NR
9/4/2002 CAP 15,000 26,000 4,200 20,600 11,000 NR
11/26/2002 CAP 15,403.8 24,427.3 2,225.1 17,976.0 3,794.4 NR
2/28/2003 ARMR 8,200 15,000 2,900 15,800 290 NR
5/16/2003 ARMR 8,200 13,000 2,600 13,300 7,200 NR
11/10/2003 ARMR 9,100 13,000 3,000 14,300 12,000 NR
9/28/2004 ARMR 4,700 8,600 1,200 7,600 7,000 NR
12/15/2004 ARMR 9,050 18,800 3,920 18,200 4,050 NR
2/23/2009 ARMR 8,300 7,400 390 1,600 8,100 1,100
7/28/2009 ARMR 8,300 11,000 2,100 15,000 7,100 820
2/17/2010 ARMR 4,800 6,300 1,300 16,000 2,800 820
7/9/2010 ARMR 10,000 16,000 2,500 15,000 6,700 870
3/7/2011 ARMR 8,190 8,210 876 14,510 9,520 1,120
7/21/2011 ARMR 7,470 6,530 953 9,850 12,200 691
3/21/2012 ARMR 3,700 4,500 2,000 11,500 1,800 960
11/17/2012 ARMR 8,700 8,600 2,500 15,600 6,300 970
4/8/2015 ARMR 2,280 3,530 1,610 6,510 1,310 788
12/29/1989 pre-CAP 32.5 BDL BDL 98.1 NA NR
10/12/1999 pre-CAP 18 110 BDL BDL 48 NR
12/15/2000 pre-CAP 14 BDL BDL BDL 130 NR
9/4/2002 CAP 7.7 <1 <1 <3 100 NR
11/26/2002 ARMR 2.9 <0.5 <0.5 <1.5 33.8 NR
2/28/2003 ARMR 1.9 <5 <1 <3 52 NR
5/16/2003 ARMR 3.9 <5 <1 <3 51 NR
11/10/2003 ARMR 2 <5 <5 <3 33 NR
9/28/2004 ARMR <1 <5 <1 <3 31 NR
12/15/2004 ARMR 1.7 <1 <1 <3 44.6 NR
2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 15 <0.39
7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 14 <0.39
2/17/2010 ARMR 0.41 0.67 <0.1 0.58 13 <0.086
7/9/2010 ARMR 0.46 <0.053 <0.1 <0.22 10 <0.086
3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 16.4 <2
7/21/2011 ARMR 0.56 <0.5 <0.5 <1.5 11.2 0.17J
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 7 0.48
11/17/2012 ARMR 1.2 <0.2 <0.2 <0.6 8.9 0.62
4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 3.4 <0.5
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident PhaseNot Sampled - Free Product
MW-1 MTBENaphthaleneNot Sampled - Free ProductBenzeneTolueneEthylbenzeneTotal XylenesMW-2
2L GW Standard
GCL
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/29/1989 pre-CAP BDL BDL BDL BDL NA NR
4/6/1990 pre-CAP 6 BDL 3.5 BDL NA NR
10/12/1999 pre-CAP BDL BDL BDL BDL 66 NR
12/15/2000 pre-CAP BDL BDL BDL BDL 53 NR
9/4/2002 CAP <1 <1 <1 <3 15 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 17.3 NR
2/28/2003 ARMR <1 <5 <1 <3 5.7 NR
5/16/2003 ARMR <1 <5 <1 <3 27 NR
11/10/2003 ARMR <1 <5 <1 <3 20 NR
9/28/2004 ARMR <1 <5 <1 <3 19 NR
12/15/2004 ARMR <1 <1 <1 <3 51.2 NR
2/23/2009 ARMR <2 <2.7 <2 <4 430 7.2
7/28/2009 ARMR <0.4 <0.54 <0.4 <0.8 220 <0.78
2/17/2010 ARMR <0.05 1.3 0.45 2 150 <0.086
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 89 <0.086
3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 23.6 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 196 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 16 <0.2
11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 33 <0.5
4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 0.56 <0.5
12/29/1989 pre-CAP BDL 4 BDL BDL NA NR
4/6/1990 pre-CAP 85 170 22 160 NA NR
10/12/1999 pre-CAP2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
7/28/2009 ARMR
2/17/2010 ARMR
4/8/2015 ARMR
12/29/1989 pre-CAP BDL BDL BDL BDL NA NR
4/6/1990 pre-CAP 5.3 4 3.4 83 NA NR
10/12/1999 pre-CAP BDL BDL BDL BDL BDL NR
9/4/2002 CAP <1 <1 <1 <3 <1 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR <1 <5 <1 <3 <5 NR
11/10/2003 ARMR <1 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.78
2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086
3/7/2011 ARMR <0.5 1.3 0.6 2.29 <0.5 <2
7/21/2011 ARMR <0.5 0.13 J <0.5 <1.5 <0.5 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2
11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
Not Sampled - Unable to Locate
Not Sampled - Unable to Locate
Not Sampled - Unable to Locate
MW-3
2L GW Standard
GCL
MW-5
MW-4
Not Sampled - Unable to Locate
Not Sampled - Unable to Access
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/29/1989 pre-CAP BDL BDL BDL BDL NA NR
4/6/1990 pre-CAP 5.6 6 3.5 23 NA NR
10/12/1999 pre-CAP BDL BDL BDL BDL NA NR
12/15/2000 pre-CAP 1.5 BDL BDL BDL 15 NR
9/4/2002 CAP <1 <1 <1 <3 <1 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR <1 <5 <1 <3 <5 NR
11/10/2003 ARMR <1 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 1.2 <0.39
7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 0.48 <0.78
2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086
7/15/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086
3/7/2011 ARMR <0.5 1 <0.5 1.2 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
3/21/2012 ARMR11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR
12/29/1989 pre-CAP 44.5 BDL BDL 46.6 NA NR
4/6/1990 pre-CAP 18 BDL BDL 36 NA NR
10/12/1999 pre-CAP BDL BDL BDL BDL 7 NR
12/15/2000 pre-CAP 49 BDL BDL 3.1 86 NR
9/4/2002 CAP <1 <1 <1 <3 6.3 NR
11/26/2002 CAP 11.4 5.8 <0.5 <1.5 34.9 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR 8.7 <5 <1 <3 15 NR
11/10/2003 ARMR 78 <5 <1 7 94 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 0.73 <0.086
3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2
11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.
5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
2L GW Standard
GCL
MW-7
MW-6
Not Sampled
Not Sampled - Unable to Access
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/29/1989 pre-CAP 1.5 1.6 BDL 6.8 NA NR
4/6/1990 pre-CAP 6.8 BDL BDL 14 NA NR
10/12/1999 pre-CAP BDL BDL BDL BDL BDL NR
12/15/2000 pre-CAP BDL BDL BDL BDL BDL NR
9/4/2002 CAP <1 <1 <1 <3 <1 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR <1 <5 <1 <3 <5 NR
11/10/2003 ARMR <1 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR
7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086
3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2
11/18/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR
4/6/1990 pre-CAP BDL BDL BDL BDL NA NR
10/12/1999 pre-CAP BDL 1.2 BDL BDL BDL NR
12/15/2000 pre-CAP BDL BDL BDL BDL BDL NR
9/4/2002 CAP <1 <1 <1 <3 <1 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR <1 <5 <1 <3 <5 NR
11/10/2003 ARMR <1 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
2/17/2010 ARMR <0.05 <0.11 <0.1 <0.22 <0.12 <0.086
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086
3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2
11/18/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.
5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
Not Sampled
Not Sampled
MW-9
2L GW Standard
GCL
MW-8
Not Sampled - Free Product
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes4/6/1990 pre-CAP BDL BDL BDL BDL NA NR
10/12/1999 pre-CAP BDL BDL BDL BDL BDL NR
12/15/2000 pre-CAP BDL BDL BDL BDL BDL NR
9/4/2002 CAP <1 <1 <1 <3 <1 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5.0 NR
5/16/2003 ARMR <1 <5 <1 <3 <5.0 NR
11/10/2003 ARMR <1 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
7/28/2009 ARMR
2/17/2010 ARMR
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 0.46 <0.086
3/7/2011 ARMR 1.5 3 0.6 6.4 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 0.55 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2
11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR <0.3 1.8 <0.2 <0.6 <0.2 <0.5
4/6/1990 pre-CAP 10,000 13,000 14,000 9,300 NA NR
10/12/1999 pre-CAP 9,300 19,000 2,500 13,300 4,500 NR
12/15/2000 pre-CAP 12,000 20,000 3,200 15,100 5,600 NR
9/4/2002 CAP 12,000 14,000 3,500 16,200 4,600 NR
11/26/2002 CAP 13,659.2 14,950.3 3,102.1 15,561.7 3,316.5 NR
2/28/2003 ARMR 7,300 13,000 3,200 16,000 940 NR
5/16/2003 ARMR 5,500 8,400 2,700 12,700 2,800 NR
11/10/2003 ARMR 5,500 9,400 2,600 11,400 2,400 NR
9/28/2004 ARMR 5,300 6,400 2,000 10,500 1,400 NR
12/15/2004 ARMR 5,760 9,090 3,360 14,400 2,910 NR
2/23/2009 ARMR 2,300 510 470 6,600 1,400 840
7/28/2009 ARMR 3,200 420 2,400 11,000 1,400 780
2/17/2010 ARMR 3,200 1,000 2,700 12,000 860 710
7/9/2010 ARMR 3,000 330 3,500 12,000 950 1,000
3/7/2011 ARMR 1,070 96 341 3,250 674 402
7/21/2011 ARMR
3/21/2012 ARMR 1,600 160 1,100 4,500 900 600
11/17/2012 ARMR 1,600 210 1,600 5,800 520 670
4/8/2015 ARMR 1,500 187 2,010 4,430 355 846
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.
5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
Not Sampled
Not Sampled
MW-11
2L GW Standard
GCL
MW-10
Not sampled; insufficient water
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes4/6/1990 pre-CAP 8.7 BDL 4 17 NA NR
10/12/1999 pre-CAP
7/28/2009 pre-CAP
12/15/2000 pre-CAP BDL BDL 1.1 53 9.1 NR
9/4/2002 CAP <5 <5 30 149 <5 NR
11/26/2002 CAP <0.5 <0.5 10.8 50.8 <1 NR
2/28/2003 ARMR 70 <250 180 720 <250 NR
5/16/2003 ARMR <1 <10 19 78 <10 NR
11/10/2003 ARMR 1.1 <5 13 41 <1 NR
9/28/2004 ARMR <1 <5 6.1 15.1 <1 NR
12/15/2004 ARMR 28.7 3.7 24.9 63.7 21.4 NR
2/23/2009 ARMR <0.2 <0.27 0.91 0.4 <0.38 6
7/28/2009 ARMR <0.2 <0.27 4.4 <0.4 <0.38 8
2/17/2010 ARMR 0.79 4.5 3.4 5.4 <0.12 9.5
7/9/2010 ARMR 2 <0.053 <0.1 0.8 <0.12 9.8
3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 0.32 J <1.5 <0.5 4.9
3/21/2012 ARMR <0.2 <0.2 1.2 <0.3 <0.2 <0.2
11/18/2012 ARMR <0.3 <0.2 0.92 <0.6 <0.2 <0.5
4/8/2015 ARMR <0.3 <0.2 0.22 <0.6 <0.2 2.8
4/6/1990 pre-CAP 36 1,200 580 3,500 NA NR
10/12/1999 pre-CAP 290 70 140 BDL 84 NR
12/15/2000 pre-CAP 680 130 300 310 170 NR
9/4/2002 CAP 850 240 300 320 <10 NR
11/26/2002 CAP 103.4 13.7 123.7 35.4 22.1 NR
2/28/2003 ARMR 100 <50 99 39 <50 NR
5/16/2003 ARMR 79 33 58 52 <5 NR
11/10/2003 ARMR 52 17 66 17.9 <1 NR
9/28/2004 ARMR 27 <50 39 <30 <10 NR
12/15/2004 ARMR 41.7 3.3 55.9 5.6 17.7 NR
2/23/2009 ARMR 13 1 42 8.3 5.1 30
7/28/2009 ARMR 80 4 57 12 20 40
2/17/2010 ARMR 15 3.3 33 27 9.7 27
7/9/2010 ARMR 210 66 150 110 41 100
3/7/2011 ARMR 23.8 0.8 16 2.97 23.5 24.6
7/21/2011 ARMR 7 1.6 19.2 4.34 4.2 17.9
3/21/2012 ARMR 5.1 1.1 19 23.88 11 <0.2
11/18/2012 ARMR 4 0.54 18 8.3 4.1 <0.5
4/8/2015 ARMR 22.5 6.1 27.3 7.1 9.9 20.3
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.
5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
Not Sampled - Unable to Locate
Not Sampled - Unable to Locate
MW-12A
MW-13
MW-12
2L GW Standard
GCL
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes4/6/1990 pre-CAP 9,000 10,000 1,250 9,300 NA NR
10/12/1999 pre-CAP 10,000 16,000 2,200 9,900 2,100 NR
12/15/2000 pre-CAP 10,000 23,000 5,300 21,600 BDL NR
9/4/2002 CAP 3,200 8,700 1,800 8,100 <75 NR
11/26/2002 CAP 3,169.4 6,320.2 946.9 4,690.8 <20 NR
2/28/2003 ARMR 4,500 8,700 1,300 6,200 <250 NR
5/16/2003 ARMR 73 100 21 97 12 NR
11/10/2003 ARMR 9,000 13,000 2,600 11,400 1,400 NR
9/28/2004 ARMR 8,000 12,000 2,000 8,700 700 NR
12/15/2004 ARMR 11,300 23,000 3,520 16,100 1,920 NR
2/23/2009 ARMR 950 1,700 650 2,600 56 260
7/28/2009 ARMR 8,300 14,000 2,900 13,000 640 810
2/17/2010 ARMR 5,500 7,500 1,900 7,700 360 470
7/9/2010 ARMR 4,300 5,800 2,200 8,300 350 920
3/7/2011 ARMR 2,450 1,830 1,530 6,340 121 652
7/21/2011 ARMR 2,670 3,180 1,190 4,920 164 507
3/21/2012 ARMR 4,000 5,300 1,700 7,800 280 720
11/18/2012 ARMR 4,100 5,900 2,400 9,100 180 820
4/8/2015 ARMR 3,400 1,740 2,200 4,510 399 888
5/4/1990 pre-CAP 3.3 6.2 1.4 0.56 NA NR
10/12/1999 pre-CAP BDL BDL BDL BDL BDL NR
12/15/2000 pre-CAP BDL BDL BDL BDL BDL NR
9/4/2002 CAP <1 <1 <1 <3 <1 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR <1 <5 <1 <3 <5 NR
11/10/2003 ARMR <1 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
2/17/2010 ARMR <0.05 0.59 <0.1 1 <0.12 <0.086
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086
3/7/2011 ARMR <0.5 0.61 <0.5 <1.5 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2
11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 0.54
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
MW-14
MW-15
2L GW Standard
GCL
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes12/15/2000 pre-CAP 560 800 510 1,800 BDL NR
9/4/2002 CAP 20 74 480 1,140 <15 NR
11/26/2002 CAP <0.5 <0.5 17.1 56.3 <1 NR
2/28/2003 ARMR <5 <25 23 56.2 <25 NR
5/16/2003 ARMR 6 7.4 3.6 8.4 <5 NR
11/10/2003 ARMR 240 490 250 880 <10 NR
9/28/2004 ARMR 14 22 11 31 1.7 NR
12/15/2004 ARMR 12.9 15.3 4.9 10.2 4.4 NR
2/23/2009 ARMR
7/28/2009 ARMR2/17/2010 ARMR
3/7/2011 ARMR
7/21/2011 ARMR
3/21/2012 ARMR
12/15/2000 pre-CAP 14,000 25,000 3,300 15,100 BDL NR
9/4/2002 CAP 9,400 27,000 3,200 14,800 <200 NR
11/26/2002 CAP 4,280 20,720 2,700 13,140 <5 NR
2/28/2003 ARMR 6,000 16,000 2,200 10,000 <250 NR
5/16/2003 ARMR 3,800 9,600 1,600 6,500 <50 NR
11/10/2003 ARMR 6,200 15,000 2,000 8,800 <25 NR
9/28/2004 ARMR 5,800 1,400 1,800 8,100 <200 NR
12/15/2004 ARMR 6,770 21,800 3,400 14,700 1,100 NR
2/23/2009 ARMR 5,000 19,000 3,100 14,000 <190 1,100
7/28/2009 ARMR 5,100 26,000 3,200 16,000 <190 1,200
2/17/2010 ARMR 4,800 15,000 2,400 12,000 <24 810
7/9/2010 ARMR 3,600 17,000 2,300 11,000 <24 780
3/7/2011 ARMR 3,900 17,900 3,140 14,380 84.2 1,110
7/21/2011 ARMR
3/21/2012 ARMR 1,600 6,600 2,100 8,200 39 2,700
11/18/2012 ARMR 2,400 13,000 2,400 10,600 25 1,100
4/8/2015 ARMR 794 6,520 1,740 5,980 16.4 1,070
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.
5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
Not Sampled
Not Sampled - Paved Over
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not sampled; blockage at 21 ft
MW-16
MW-17
2L GW Standard
GCL
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes8/16/2001 pre-CAP 810 8,100 630 2,870 140 NR
9/4/2002 CAP 63 370 50 158 <5 NR
11/26/2002 CAP 56.9 157.3 117.8 237.4 <5 NR
2/28/2003 ARMR 2,100 19,000 1,300 5,900 270 NR
5/16/2003 ARMR 1,600 3,900 430 2,000 130 NR
11/10/2003 ARMR 72 40 8.8 21.8 17 NR
9/28/2004 ARMR 930 7,700 810 3,900 230 NR
12/15/2004 ARMR 7.3 15.6 <1 18 7.9 NR
2/23/2009 ARMR 550 5,100 900 3,700 230 180
7/28/2009 ARMR 3,700 20,000 1,700 8,000 600 110
2/17/2010 ARMR 1,600 30,000 2,700 13,000 3,800 1,400
7/9/2010 ARMR 3,000 17,000 1,800 8,800 670 510
3/7/2011 ARMR 88 550 165 730 18.7 36.5
7/21/2011 ARMR 2,720 11,800 1,240 5,440 294 269
3/21/2012 ARMR 26 84 99 300 1.9 20
11/18/2012 ARMR 640 2,900 1,400 4,900 20 330
4/8/2015 ARMR 2570 9840 1830 7980 34.5 696
8/16/2001 pre-CAP BDL 1.5 BDL BDL BDL NR
9/4/2002 CAP <1 <1 <1 <3 <1 NR
11/26/2002 CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR <1 <5 <1 <3 <5 NR
11/10/2003 ARMR 1.5 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
7/28/2009 ARMR <0.2 <0.27 <0.2 <0.4 <0.38 <0.39
2/17/2010 ARMR 0.47 3.2 0.9 3.1 <0.12 <0.086
7/9/2010 ARMR <0.05 <0.053 <0.1 <0.22 <0.12 <0.086
3/7/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <2
7/21/2011 ARMR <0.5 <0.5 <0.5 <1.5 <0.5 <0.5
3/21/2012 ARMR <0.2 <0.2 <0.1 <0.3 <0.2 <0.2
11/17/2012 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
4/8/2015 ARMR <0.3 <0.2 <0.2 <0.6 <0.2 <0.5
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.
5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
2L GW Standard
GCL
MW-18
MW-19
TABLE 6 (ctd)
HISTORICAL GROUNDWATER ANALYTICAL DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
Analytical Methods:EPA METHOD 6010D or 6200B
WellDate SampledIncident Phase MTBENaphthaleneBenzeneTolueneEthylbenzeneTotal Xylenes2/23/2009 ARMR 50 38 23 200 <1.9 210
7/28/2009 ARMR 110 110 490 560 <3.8 360
2/17/2010 ARMR 62 110 260 610 <0.6 120
7/9/2010 ARMR 110 140 330 860 <24 250
3/7/2011 ARMR 28 11 12 172 <0.5 55
7/21/2011 ARMR 38.5 26.8 58.8 216.8 3.1 75.6
3/21/2012 ARMR 73 81 240 470 <1 230
11/18/2012 ARMR
4/8/2015 ARMR
2/23/2009 ARMR 3,200 6,900 1,500 2,500 1,600 520
7/28/2009 ARMR 1,500 1,100 650 440 1,300 210
2/17/2010 ARMR 920 1,800 700 730 1,600 150
7/9/2010 ARMR 1,500 6,100 980 2,300 1,700 270
3/7/2011 ARMR 116 216 44.9 131.9 595 12.8
7/21/2011 ARMR 353 125 82.1 182.6 797 37.2
3/21/2012 ARMR 830 3,100 570 1,920 970 180
11/18/2012 ARMR
4/8/2015 ARMR
2/23/2009 ARMR 93 4.7 420 <4 480 3003/13/2009 ARMR 68 3 290 <4 370 170
7/28/2009 ARMR 100 35 470 8.4 510 290
2/17/2010 ARMR 59 75 460 99 240 230
7/9/2010 ARMR 120 52 580 130 490 340
3/7/2011 ARMR 7.9 2 58.9 8 114 26.3
7/21/2011 ARMR 61.4 48.8 220 160.6 177 97.7
3/21/2012 ARMR
11/18/2012 ARMR
4/8/2015 ARMR
9/4/2002 CAP 29,000 34,000 2,800 16,200 160,000
11/26/2002 CAP
2/28/2003 ARMR2/23/2009 ARMR
2/17/2010 ARMR
3/21/2012 ARMR 11,000 22,000 3,800 66,000 130,000 6,900
4/8/2015 ARMR
8/16/2001 pre-CAP BDL BDL BDL BDL BDL NR
9/4/2002 pre-CAP <1 <1 <1 <3 <1 NR
11/26/2002 pre-CAP <0.5 <0.5 <0.5 <1.5 <1 NR
2/28/2003 ARMR <1 <5 <1 <3 <5 NR
5/16/2003 ARMR <1 <5 <1 <3 <5 NR
11/10/2003 ARMR <1 <5 <1 <3 <1 NR
7/21/2004 ARMR <1 <5 <1 <3 <1 NR
9/28/2004 ARMR <1 <5 <1 <3 <1 NR
12/15/2004 ARMR <1 <1 <1 <3 <1 NR
2/23/2009 ARMR
1 600 600 500 20 6
5,000 260,000 84,500 85,500 20,000 6,000
Notes:
1. "<" or ND = None detected above method detection limit.
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard.
3. GCL = Gross Contaminant Level established by NCDENR.
4. NA = Not analyzed.
5. Values in BOLD indicate levels above 2L Groundwater Standards.
6. MTBE = Methyl tertiary butyl ether.
7. All concentrations in micrograms per liter (ug/L).
8. BDL = Below Detection Limit.
9. NR = Not Reported in hisorical tables.
2L GW Standard
GCL
Not Sampled - Unable to Locate
Not Sampled
Not Sampled
Not Sampled
Not Sampled
Not Sampled
RW-1
MW-22
Not Sampled - Unable to Locate
Not Sampled
Not Sampled - Unable to Locate
MW-21
MW-20
WW-1
Not Sampled - Unable to Locate
Not Sampled - Unable to Locate
Not Sampled - Unable to Locate
Not Sampled - Unable to Locate
TABLE 7
NATURAL ATTENUATION DATA
PANTRY #3079
5102 DORTCHES BOULEVARD
ROCKY MOUNT, NASH COUNTY, NORTH CAROLINA
ATC PROJECT NO. 45.42017.3079
NCDENR FACILITY ID NO. 0-022631
NCDENR INCIDENT NO. 4028
3/21/2012 5.86 19.44 0.102 2.69 103.0 NA NA NA NA
4/8/2015 6.05 22.94 0.195 2.46 -61.6 NA NA NA NA
3/21/2012 4.54 20.91 0.080 2.05 3.7 NA NA NA NA
4/8/2015 5.31 21.31 0.101 2.21 8.5 NA NA NA NA
3/21/2012 4.11 18.30 0.340 3.67 42.1 NA NA NA NA
4/8/2015 4.87 19.19 0.260 4.72 38.1 NA NA NA NA
MW-4 3/21/2012 NA NA NA NA NA NA NA NA NA
MW-5 3/21/2012 4.65 19.00 0.139 6 23.9 NA NA NA NA
MW-6 3/21/2012 NA NA NA NA NA NA NA NA NA
3/21/2012 4.33 19.88 0.061 3.78 19.7 NA NA NA NA
4/8/2015 5.39 19.88 0.062 5 7.9 NA NA NA NA
3/21/2012 4.86 18.20 0.082 3.99 -28.1 NA NA NA NA
4/8/2015 NA NA NA NA NA NA NA NA NA
3/21/2012 4.67 17.91 0.099 4.45 -17.3 NA NA NA NA
4/8/2015 5.88 19.51 0.101 5.77 -4.5 NA NA NA NA
3/21/2012 4.60 18.13 0.232 1.61 -12.9 NA NA NA NA
4/8/2015 6.16 20.08 0.237 2.85 -74.2 NA NA NA NA
3/21/2012 5.32 19.60 0.106 2.6 -68.7 NA NA NA NA
4/8/2015 6.57 23.48 0.192 3.86 -23.9 NA NA NA NA
3/21/2012 4.83 20.96 0.094 2.52 -63.3 NA NA NA NA
4/8/2015 6.91 21.17 0.149 3.33 -9.3 NA NA NA NA
3/21/2012 4.98 20.45 0.159 1.24 -96 NA NA NA NA
4/8/2015 6.11 21.50 0.138 1.73 3 NA NA NA NA
3/21/2012 4.92 21.68 0.155 2.31 -90.8 NA NA NA NA
4/8/2015 6.33 23.35 0.270 2.39 -41 NA NA NA NA
3/21/2012 7.07 18.50 0.135 6.47 -21.3 NA NA NA NA
4/8/2015 6.35 24.14 0.047 6.42 22.9 NA NA NA NA
MW-16 3/21/2012 NA NA NA NA NA NA NA NA NA
3/21/2012 NA NA NA NA NA NA NA NA NA
4/8/2015 6.41 20.81 0.160 2.05 -23 NA NA NA NA
3/21/2012 4.99 17.32 0.072 3.25 -83.7 NA NA NA NA
4/8/2015 6.26 21.04 0.150 2.62 -5 NA NA NA NA
3/21/2012 4.70 17.86 0.079 1.96 -71.6 NA NA NA NA
4/8/2015 6.95 22.63 0.401 5.11 56.8 NA NA NA NA
MW-20 3/21/2012 4.56 17.89 0.057 3.96 -36.7 NA NA NA NA
MW-21 3/21/2012 4.75 17.68 0.056 3.41 -75.5 NA NA NA NA
MW-22 3/21/2012 NA NA NA NA NA NA NA NA NA
Notes:
1. NA = Not Analyzed
2. ND = None Detected
MW-15
MW-17
MW-18
MW-19
MW-9
MW-10
MW-11
MW-12A
MW-13
MW-14
Dissolved
Oxygen (%)
MW-1
MW-2
MW-3
MW-7
MW-8
Redox
Potential (mV)
Ferrous Iron
(mg/L)
Nitrate
(mg/L)Nitrite (mg/L)Sulfate
(mg/L)Well ID Date
Measured pH
Temperature
Degrees
Celsius
Conductivity
(ms/cm)

FIGURES

APPENDIX A

METHODS

METHODS

Groundwater Levels

Groundwater level measurements were obtained by using an electronic sounding/interface
detection device which registers when a probe makes contact with petroleum product and/or
water. Depth to groundwater measurements were obtained by lowering the device into the well
until it indicated that the water surface had been encountered, at which point the level was
recorded to the nearest 0.01 foot.

Groundwater Sampling

Groundwater samples were collected using new, dedicated plastic bailers at each monitoring
well. Before obtaining a sample, a minimum of three well volumes of groundwater was
evacuated to ensure collection of a sample representative of the in-situ groundwater conditions.
Samples were collected using dedicated bailers, transferred to containers supplied by the
laboratory, and placed in an ice filled cooler.

Chemical Analysis

Samples were shipped by overnight courier under chain-of-custody to Accutest Laboratories in
Scott, Louisiana. Groundwater samples were analyzed for purgeable volatile hydrocarbons and
aromatics by EPA Method 6200B and for lead by EPA Method 6010B with 3030C prep.

APPENDIX B

MMPE SUMMARY REPORT AND DISPOSAL MANIFEST

APPENDIX C

LABORATORY ANALYTICAL REPORT

04/20/15
Technical Report for
Cardno ATC
Pantry #3079, Rocky Mount, NC
Accutest Job Number: LA5660
Sampling Date: 04/08/15
Report to:
Cardno ATC
2725 East Millbrook Road Suite 121
Raleigh, NC 27604
[e-mail]
ATTN: Kurt Ness
Total number of pages in report:
Certifications: LDEQ(2048), LDHH(LA150012), AR(14-045-04), FL(E87657), KY(#31), NC(487), SC(73004001),
TX(T104704186-15-7), WV(257)
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Lafayette • 500 Ambassafor Caffery • Scott, LA 70583 • tel: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Christina Hebert 337-237-4775
Ron Benjamin
Lab Director
Lafayette
04/20/15
e-Hardcopy 2.0
Automated Report
104
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 104
LA5660
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: LA5660-1: MW-1 .........................................................................................................10
3.2: LA5660-2: MW-2 .........................................................................................................14
3.3: LA5660-3: MW-3 .........................................................................................................18
3.4: LA5660-4: MW-7 .........................................................................................................22
3.5: LA5660-5: MW-9 .........................................................................................................26
3.6: LA5660-6: MW-10 .......................................................................................................30
3.7: LA5660-7: MW-11 .......................................................................................................34
3.8: LA5660-8: MW-12A ....................................................................................................38
3.9: LA5660-9: MW-13 .......................................................................................................42
3.10: LA5660-10: MW-14 ...................................................................................................46
3.11: LA5660-11: MW-15 ...................................................................................................50
3.12: LA5660-12: MW-17 ...................................................................................................54
3.13: LA5660-13: MW-18 ...................................................................................................58
3.14: LA5660-14: MW-19 ...................................................................................................62
Section 4: Misc. Forms ............................................................................................................66
4.1: Chain of Custody ...........................................................................................................67
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................71
5.1: Method Blank Summary ................................................................................................72
5.2: Blank Spike Summary ...................................................................................................81
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................90
Section 6: Metals Analysis - QC Data Summaries ................................................................99
6.1: Prep QC MP815: Pb ......................................................................................................100 1234562 of 104
LA5660
Accutest Laboratories
Sample Summary
Cardno ATC
Job No:LA5660
Pantry #3079, Rocky Mount, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
LA5660-1 04/08/15 16:25 04/10/15 AQ Ground Water MW-1
LA5660-2 04/08/15 15:05 04/10/15 AQ Ground Water MW-2
LA5660-3 04/08/15 15:50 04/10/15 AQ Ground Water MW-3
LA5660-4 04/08/15 14:20 04/10/15 AQ Ground Water MW-7
LA5660-5 04/08/15 17:05 04/10/15 AQ Ground Water MW-9
LA5660-6 04/08/15 13:45 04/10/15 AQ Ground Water MW-10
LA5660-7 04/08/15 12:10 04/10/15 AQ Ground Water MW-11
LA5660-8 04/08/15 09:10 04/10/15 AQ Ground Water MW-12A
LA5660-9 04/08/15 11:00 04/10/15 AQ Ground Water MW-13
LA5660-10 04/08/15 09:55 04/10/15 AQ Ground Water MW-14
LA5660-11 04/08/15 12:55 04/10/15 AQ Ground Water MW-15
LA5660-12 04/08/15 11:40 04/10/15 AQ Ground Water MW-17
LA5660-13 04/08/15 10:20 04/10/15 AQ Ground Water MW-18
3 of 104
LA5660 1
Accutest Laboratories
Sample Summary
(continued)
Cardno ATC
Job No:LA5660
Pantry #3079, Rocky Mount, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
LA5660-14 04/08/15 08:30 04/10/15 AQ Ground Water MW-19
4 of 104
LA5660 1
Summary of Hits Page 1 of 4
Job Number:LA5660
Account:Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Collected:04/08/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA5660-1 MW-1
Benzene 2280 6.0 ug/l SM 6200B
sec-Butylbenzene 11.1 2.0 ug/l SM 6200B
1,2-Dibromoethane 15.4 2.0 ug/l SM 6200B
1,2-Dichloroethane 14.7 4.0 ug/l SM 6200B
Di-Isopropyl Ether 2.5 2.0 ug/l SM 6200B
Ethylbenzene 1610 4.0 ug/l SM 6200B
2-Hexanone 17.7 10 ug/l SM 6200B
Isopropylbenzene 79.0 4.0 ug/l SM 6200B
p-Isopropyltoluene 7.4 2.0 ug/l SM 6200B
Methyl Tert Butyl Ether 1310 4.0 ug/l SM 6200B
Naphthalene 788 10 ug/l SM 6200B
n-Propylbenzene 203 2.0 ug/l SM 6200B
Styrene 15.8 2.0 ug/l SM 6200B
Toluene 3530 4.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 2180 30 ug/l SM 6200B
1,3,5-Trimethylbenzene 654 6.0 ug/l SM 6200B
m,p-Xylene 3320 8.0 ug/l SM 6200B
o-Xylene 1990 20 ug/l SM 6200B
Xylene (total)6510 60 ug/l SM 6200B
Lead 16.5 10 ug/l SW846 6010B
LA5660-2 MW-2
Di-Isopropyl Ether 0.10 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 3.4 0.20 ug/l SM 6200B
Lead 29.4 10 ug/l SW846 6010B
LA5660-3 MW-3
Methyl Tert Butyl Ether 0.56 0.20 ug/l SM 6200B
Lead 16.7 10 ug/l SW846 6010B
LA5660-4 MW-7
No hits reported in this sample.
LA5660-5 MW-9
Chloroform 0.26 0.10 ug/l SM 6200B
Lead 37.1 10 ug/l SW846 6010B
5 of 104
LA5660 2
Summary of Hits Page 2 of 4
Job Number:LA5660
Account:Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Collected:04/08/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA5660-6 MW-10
p-Isopropyltoluene 23.5 0.10 ug/l SM 6200B
Toluene 1.8 0.20 ug/l SM 6200B
Lead 32.5 10 ug/l SW846 6010B
LA5660-7 MW-11
Benzene 1500 6.0 ug/l SM 6200B
sec-Butylbenzene 12.5 2.0 ug/l SM 6200B
1,2-Dichloroethane 5.1 4.0 ug/l SM 6200B
Di-Isopropyl Ether 2.1 2.0 ug/l SM 6200B
Ethylbenzene 2010 4.0 ug/l SM 6200B
Isopropylbenzene 106 4.0 ug/l SM 6200B
p-Isopropyltoluene 5.7 2.0 ug/l SM 6200B
Methyl Tert Butyl Ether 355 4.0 ug/l SM 6200B
Naphthalene 846 10 ug/l SM 6200B
n-Propylbenzene 253 2.0 ug/l SM 6200B
Styrene 14.0 2.0 ug/l SM 6200B
Toluene 187 4.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 1830 15 ug/l SM 6200B
1,3,5-Trimethylbenzene 611 6.0 ug/l SM 6200B
m,p-Xylene 2840 8.0 ug/l SM 6200B
o-Xylene 1590 4.0 ug/l SM 6200B
Xylene (total)4430 12 ug/l SM 6200B
Lead 39.9 10 ug/l SW846 6010B
LA5660-8 MW-12A
sec-Butylbenzene 6.8 0.10 ug/l SM 6200B
tert-Butylbenzene 0.17 0.10 ug/l SM 6200B
Ethylbenzene 0.22 0.20 ug/l SM 6200B
Isopropylbenzene 4.4 0.20 ug/l SM 6200B
p-Isopropyltoluene 2.3 0.10 ug/l SM 6200B
Naphthalene 2.8 0.50 ug/l SM 6200B
n-Propylbenzene 13.1 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.99 0.30 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.57 0.30 ug/l SM 6200B
Lead 31.4 10 ug/l SW846 6010B
LA5660-9 MW-13
Benzene 22.5 0.30 ug/l SM 6200B
n-Butylbenzene 5.4 0.10 ug/l SM 6200B
sec-Butylbenzene 4.7 0.10 ug/l SM 6200B
6 of 104
LA5660 2
Summary of Hits Page 3 of 4
Job Number:LA5660
Account:Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Collected:04/08/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
tert-Butylbenzene 0.13 0.10 ug/l SM 6200B
1,2-Dichloroethane 0.26 0.20 ug/l SM 6200B
Ethylbenzene 27.3 0.20 ug/l SM 6200B
Isopropylbenzene 4.7 0.20 ug/l SM 6200B
p-Isopropyltoluene 2.2 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 9.9 0.20 ug/l SM 6200B
Naphthalene 20.3 0.50 ug/l SM 6200B
n-Propylbenzene 13.1 0.10 ug/l SM 6200B
Styrene 0.15 0.10 ug/l SM 6200B
Toluene 6.1 0.20 ug/l SM 6200B
1,2,4-Trimethylbenzene 8.2 0.30 ug/l SM 6200B
1,3,5-Trimethylbenzene 2.3 0.30 ug/l SM 6200B
Vinyl Acetate 0.55 0.20 ug/l SM 6200B
m,p-Xylene 4.5 0.40 ug/l SM 6200B
o-Xylene 2.7 0.20 ug/l SM 6200B
Xylene (total)7.1 0.60 ug/l SM 6200B
Lead 70.0 10 ug/l SW846 6010B
LA5660-10 MW-14
Benzene 3400 6.0 ug/l SM 6200B
sec-Butylbenzene 18.5 2.0 ug/l SM 6200B
1,2-Dichloroethane 26.0 4.0 ug/l SM 6200B
Di-Isopropyl Ether 3.9 2.0 ug/l SM 6200B
Ethylbenzene 2200 4.0 ug/l SM 6200B
Isopropylbenzene 127 4.0 ug/l SM 6200B
p-Isopropyltoluene 8.7 2.0 ug/l SM 6200B
Methyl Tert Butyl Ether 399 4.0 ug/l SM 6200B
Naphthalene 888 10 ug/l SM 6200B
n-Propylbenzene 346 2.0 ug/l SM 6200B
Styrene 11.2 2.0 ug/l SM 6200B
Toluene 1740 4.0 ug/l SM 6200B
1,2,4-Trimethylbenzene 2110 15 ug/l SM 6200B
1,3,5-Trimethylbenzene 685 6.0 ug/l SM 6200B
m,p-Xylene 2990 8.0 ug/l SM 6200B
o-Xylene 1530 4.0 ug/l SM 6200B
Xylene (total)4510 12 ug/l SM 6200B
Lead 15.3 10 ug/l SW846 6010B
LA5660-11 MW-15
Naphthalene 0.54 0.50 ug/l SM 6200B
7 of 104
LA5660 2
Summary of Hits Page 4 of 4
Job Number:LA5660
Account:Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Collected:04/08/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
LA5660-12 MW-17
Benzene 794 15 ug/l SM 6200B
Di-Isopropyl Ether 35.7 5.0 ug/l SM 6200B
Ethylbenzene 1740 10 ug/l SM 6200B
Isopropylbenzene 90.2 10 ug/l SM 6200B
p-Isopropyltoluene 10.5 5.0 ug/l SM 6200B
Methylene Chloride 35.6 25 ug/l SM 6200B
Methyl Tert Butyl Ether 16.4 10 ug/l SM 6200B
Naphthalene 1070 25 ug/l SM 6200B
n-Propylbenzene 235 5.0 ug/l SM 6200B
Styrene 32.4 5.0 ug/l SM 6200B
Toluene 6520 10 ug/l SM 6200B
1,2,4-Trimethylbenzene 1830 15 ug/l SM 6200B
1,3,5-Trimethylbenzene 465 15 ug/l SM 6200B
m,p-Xylene 4030 20 ug/l SM 6200B
o-Xylene 1950 10 ug/l SM 6200B
Xylene (total)5980 30 ug/l SM 6200B
Lead 36.8 10 ug/l SW846 6010B
LA5660-13 MW-18
Benzene 2570 15 ug/l SM 6200B
1,2-Dibromoethane 14.5 5.0 ug/l SM 6200B
1,2-Dichloroethane 13.1 10 ug/l SM 6200B
Di-Isopropyl Ether 305 5.0 ug/l SM 6200B
Ethylbenzene 1830 10 ug/l SM 6200B
Isopropylbenzene 66.1 10 ug/l SM 6200B
Methyl Tert Butyl Ether 34.5 10 ug/l SM 6200B
Naphthalene 696 25 ug/l SM 6200B
n-Propylbenzene 150 5.0 ug/l SM 6200B
Styrene 72.6 5.0 ug/l SM 6200B
Toluene 9840 10 ug/l SM 6200B
1,2,4-Trimethylbenzene 1280 15 ug/l SM 6200B
1,3,5-Trimethylbenzene 291 15 ug/l SM 6200B
m,p-Xylene 5330 20 ug/l SM 6200B
o-Xylene 2650 10 ug/l SM 6200B
Xylene (total)7980 30 ug/l SM 6200B
Lead 73.0 10 ug/l SW846 6010B
LA5660-14 MW-19
No hits reported in this sample.
8 of 104
LA5660 2
Accutest Laboratories
Sample Results
Report of Analysis
Lafayette
Section 3
9 of 104
LA5660 3
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:LA5660-1 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001887.D 20 04/13/15 CR n/a n/a V2I60
Run #2 2I001886.D 100 04/13/15 CR n/a n/a V2I60
Purge Volume
Run #1 25.0 ml
Run #2 25.0 ml
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 200 ug/l
71-43-2 Benzene 2280 6.0 ug/l
108-86-1 Bromobenzene ND 2.0 ug/l
74-97-5 Bromochloromethane ND 2.0 ug/l
75-27-4 Bromodichloromethane ND 2.0 ug/l
75-25-2 Bromoform ND 4.0 ug/l
104-51-8 n-Butylbenzene ND 2.0 ug/l
135-98-8 sec-Butylbenzene 11.1 2.0 ug/l
98-06-6 tert-Butylbenzene ND 2.0 ug/l
56-23-5 Carbon Tetrachloride ND 2.0 ug/l
108-90-7 Chlorobenzene ND 2.0 ug/l
75-00-3 Chloroethane ND 4.0 ug/l
67-66-3 Chloroform ND 2.0 ug/l
95-49-8 o-Chlorotoluene ND 4.0 ug/l
106-43-4 p-Chlorotoluene ND 2.0 ug/l
124-48-1 Dibromochloromethane ND 2.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 20 ug/l
106-93-4 1,2-Dibromoethane 15.4 2.0 ug/l
75-71-8 Dichlorodifluoromethane ND 4.0 ug/l
541-73-1 m-Dichlorobenzene ND 4.0 ug/l
95-50-1 o-Dichlorobenzene ND 4.0 ug/l
106-46-7 p-Dichlorobenzene ND 10 ug/l
75-34-3 1,1-Dichloroethane ND 2.0 ug/l
107-06-2 1,2-Dichloroethane 14.7 4.0 ug/l
75-35-4 1,1-Dichloroethylene ND 2.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.0 ug/l
78-87-5 1,2-Dichloropropane ND 2.0 ug/l
142-28-9 1,3-Dichloropropane ND 2.0 ug/l
594-20-7 2,2-Dichloropropane ND 2.0 ug/l
563-58-6 1,1-Dichloropropene ND 2.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 4.0 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 104
LA5660 33.1
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:LA5660-1 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.0 ug/l
108-20-3 Di-Isopropyl Ether 2.5 2.0 ug/l
64-17-5 Ethyl Alcohol ND 1000 ug/l
100-41-4 Ethylbenzene 1610 4.0 ug/l
591-78-6 2-Hexanone 17.7 10 ug/l
87-68-3 Hexachlorobutadiene ND 10 ug/l
98-82-8 Isopropylbenzene 79.0 4.0 ug/l
99-87-6 p-Isopropyltoluene 7.4 2.0 ug/l
74-83-9 Methyl Bromide ND 10 ug/l
74-87-3 Methyl Chloride ND 4.0 ug/l
74-95-3 Methylene Bromide ND 2.0 ug/l
75-09-2 Methylene Chloride ND 10 ug/l
78-93-3 Methyl Ethyl Ketone ND 250 ug/l
108-10-1 4-Methyl-2-pentanone ND 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 1310 4.0 ug/l
91-20-3 Naphthalene 788 10 ug/l
103-65-1 n-Propylbenzene 203 2.0 ug/l
100-42-5 Styrene 15.8 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.0 ug/l
127-18-4 Tetrachloroethylene ND 4.0 ug/l
108-88-3 Toluene 3530 4.0 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 4.0 ug/l
79-01-6 Trichloroethylene ND 2.0 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 2180 a 30 ug/l
108-67-8 1,3,5-Trimethylbenzene 654 6.0 ug/l
108-05-4 Vinyl Acetate ND 4.0 ug/l
75-01-4 Vinyl Chloride ND 2.0 ug/l
m,p-Xylene 3320 8.0 ug/l
95-47-6 o-Xylene 1990 a 20 ug/l
1330-20-7 Xylene (total)6510 a 60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 103%98%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 104
LA5660 33.1
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:LA5660-1 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%101%70-130%
460-00-4 4-Bromofluorobenzene 101%99%70-130%
(a) Result is from Run# 2
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 104
LA5660 33.1
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-1
Lab Sample ID:LA5660-1 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 16.5 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
13 of 104
LA5660 33.1
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:LA5660-2 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001884.D 1 04/13/15 CR n/a n/a V2I60
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 104
LA5660 33.2
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:LA5660-2 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether 0.10 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.4 0.20 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 94%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 104
LA5660 33.2
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:LA5660-2 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 98%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 104
LA5660 33.2
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-2
Lab Sample ID:LA5660-2 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 29.4 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
17 of 104
LA5660 33.2
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:LA5660-3 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001883.D 1 04/13/15 CR n/a n/a V2I60
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 104
LA5660 33.3
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:LA5660-3 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.56 0.20 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 104
LA5660 33.3
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:LA5660-3 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 104
LA5660 33.3
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-3
Lab Sample ID:LA5660-3 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 16.7 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
21 of 104
LA5660 33.3
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-7
Lab Sample ID:LA5660-4 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001882.D 1 04/13/15 CR n/a n/a V2I60
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 104
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-7
Lab Sample ID:LA5660-4 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 104
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Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-7
Lab Sample ID:LA5660-4 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 104
LA5660 33.4
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-7
Lab Sample ID:LA5660-4 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead <10 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
25 of 104
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Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-9
Lab Sample ID:LA5660-5 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001885.D 1 04/13/15 CR n/a n/a V2I60
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform 0.26 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 104
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-9
Lab Sample ID:LA5660-5 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 104
LA5660 33.5
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-9
Lab Sample ID:LA5660-5 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 104
LA5660 33.5
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-9
Lab Sample ID:LA5660-5 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 37.1 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
29 of 104
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Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-10
Lab Sample ID:LA5660-6 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001881.D 1 04/13/15 CR n/a n/a V2I60
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 104
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-10
Lab Sample ID:LA5660-6 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene 23.5 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene 1.8 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 104
LA5660 33.6
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-10
Lab Sample ID:LA5660-6 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 104
LA5660 33.6
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-10
Lab Sample ID:LA5660-6 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 32.5 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
33 of 104
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Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-11
Lab Sample ID:LA5660-7 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001941.D 20 04/15/15 SV n/a n/a V2I65
Run #2 2I001920.D 50 04/14/15 SV n/a n/a V2I63
Purge Volume
Run #1 25.0 ml
Run #2 25.0 ml
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 200 ug/l
71-43-2 Benzene 1500 6.0 ug/l
108-86-1 Bromobenzene ND 2.0 ug/l
74-97-5 Bromochloromethane ND 2.0 ug/l
75-27-4 Bromodichloromethane ND 2.0 ug/l
75-25-2 Bromoform ND 4.0 ug/l
104-51-8 n-Butylbenzene ND 2.0 ug/l
135-98-8 sec-Butylbenzene 12.5 2.0 ug/l
98-06-6 tert-Butylbenzene ND 2.0 ug/l
56-23-5 Carbon Tetrachloride ND 2.0 ug/l
108-90-7 Chlorobenzene ND 2.0 ug/l
75-00-3 Chloroethane ND 4.0 ug/l
67-66-3 Chloroform ND 2.0 ug/l
95-49-8 o-Chlorotoluene ND 4.0 ug/l
106-43-4 p-Chlorotoluene ND 2.0 ug/l
124-48-1 Dibromochloromethane ND 2.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 20 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 ug/l
75-71-8 Dichlorodifluoromethane ND 4.0 ug/l
541-73-1 m-Dichlorobenzene ND 4.0 ug/l
95-50-1 o-Dichlorobenzene ND 4.0 ug/l
106-46-7 p-Dichlorobenzene ND 10 ug/l
75-34-3 1,1-Dichloroethane ND 2.0 ug/l
107-06-2 1,2-Dichloroethane 5.1 4.0 ug/l
75-35-4 1,1-Dichloroethylene ND 2.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.0 ug/l
78-87-5 1,2-Dichloropropane ND 2.0 ug/l
142-28-9 1,3-Dichloropropane ND 2.0 ug/l
594-20-7 2,2-Dichloropropane ND 2.0 ug/l
563-58-6 1,1-Dichloropropene ND 2.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 4.0 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 104
LA5660 33.7
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-11
Lab Sample ID:LA5660-7 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.0 ug/l
108-20-3 Di-Isopropyl Ether 2.1 2.0 ug/l
64-17-5 Ethyl Alcohol ND 1000 ug/l
100-41-4 Ethylbenzene 2010 4.0 ug/l
591-78-6 2-Hexanone ND 10 ug/l
87-68-3 Hexachlorobutadiene ND 10 ug/l
98-82-8 Isopropylbenzene 106 4.0 ug/l
99-87-6 p-Isopropyltoluene 5.7 2.0 ug/l
74-83-9 Methyl Bromide ND 10 ug/l
74-87-3 Methyl Chloride ND 4.0 ug/l
74-95-3 Methylene Bromide ND 2.0 ug/l
75-09-2 Methylene Chloride ND 10 ug/l
78-93-3 Methyl Ethyl Ketone ND 250 ug/l
108-10-1 4-Methyl-2-pentanone ND 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 355 4.0 ug/l
91-20-3 Naphthalene 846 10 ug/l
103-65-1 n-Propylbenzene 253 2.0 ug/l
100-42-5 Styrene 14.0 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.0 ug/l
127-18-4 Tetrachloroethylene ND 4.0 ug/l
108-88-3 Toluene 187 4.0 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 4.0 ug/l
79-01-6 Trichloroethylene ND 2.0 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 1830 a 15 ug/l
108-67-8 1,3,5-Trimethylbenzene 611 6.0 ug/l
108-05-4 Vinyl Acetate ND 4.0 ug/l
75-01-4 Vinyl Chloride ND 2.0 ug/l
m,p-Xylene 2840 8.0 ug/l
95-47-6 o-Xylene 1590 4.0 ug/l
1330-20-7 Xylene (total)4430 12 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 104%104%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 104
LA5660 33.7
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-11
Lab Sample ID:LA5660-7 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%100%70-130%
460-00-4 4-Bromofluorobenzene 101%103%70-130%
(a) Result is from Run# 2
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 104
LA5660 33.7
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-11
Lab Sample ID:LA5660-7 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 39.9 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
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Report of Analysis Page 1 of 3
Client Sample ID:MW-12A
Lab Sample ID:LA5660-8 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001937.D 1 04/15/15 SV n/a n/a V2I65
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene 6.8 0.10 ug/l
98-06-6 tert-Butylbenzene 0.17 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 104
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Report of Analysis Page 2 of 3
Client Sample ID:MW-12A
Lab Sample ID:LA5660-8 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene 0.22 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene 4.4 0.20 ug/l
99-87-6 p-Isopropyltoluene 2.3 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene 2.8 0.50 ug/l
103-65-1 n-Propylbenzene 13.1 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.99 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.57 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 104
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Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-12A
Lab Sample ID:LA5660-8 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 104
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Report of Analysis Page 1 of 1
Client Sample ID:MW-12A
Lab Sample ID:LA5660-8 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 31.4 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
41 of 104
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Report of Analysis Page 1 of 3
Client Sample ID:MW-13
Lab Sample ID:LA5660-9 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001938.D 1 04/15/15 SV n/a n/a V2I65
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene 22.5 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene 5.4 0.10 ug/l
135-98-8 sec-Butylbenzene 4.7 0.10 ug/l
98-06-6 tert-Butylbenzene 0.13 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane 0.26 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 104
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-13
Lab Sample ID:LA5660-9 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene 27.3 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene 4.7 0.20 ug/l
99-87-6 p-Isopropyltoluene 2.2 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether 9.9 0.20 ug/l
91-20-3 Naphthalene 20.3 0.50 ug/l
103-65-1 n-Propylbenzene 13.1 0.10 ug/l
100-42-5 Styrene 0.15 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene 6.1 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 8.2 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene 2.3 0.30 ug/l
108-05-4 Vinyl Acetate 0.55 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene 4.5 0.40 ug/l
95-47-6 o-Xylene 2.7 0.20 ug/l
1330-20-7 Xylene (total)7.1 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 104
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Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-13
Lab Sample ID:LA5660-9 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 106%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 104
LA5660 33.9
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Report of Analysis Page 1 of 1
Client Sample ID:MW-13
Lab Sample ID:LA5660-9 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 70.0 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
45 of 104
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Report of Analysis Page 1 of 3
Client Sample ID:MW-14
Lab Sample ID:LA5660-10 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001943.D 20 04/15/15 SV n/a n/a V2I65
Run #2 2I001921.D 50 04/14/15 SV n/a n/a V2I63
Purge Volume
Run #1 25.0 ml
Run #2 25.0 ml
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 200 ug/l
71-43-2 Benzene 3400 6.0 ug/l
108-86-1 Bromobenzene ND 2.0 ug/l
74-97-5 Bromochloromethane ND 2.0 ug/l
75-27-4 Bromodichloromethane ND 2.0 ug/l
75-25-2 Bromoform ND 4.0 ug/l
104-51-8 n-Butylbenzene ND 2.0 ug/l
135-98-8 sec-Butylbenzene 18.5 2.0 ug/l
98-06-6 tert-Butylbenzene ND 2.0 ug/l
56-23-5 Carbon Tetrachloride ND 2.0 ug/l
108-90-7 Chlorobenzene ND 2.0 ug/l
75-00-3 Chloroethane ND 4.0 ug/l
67-66-3 Chloroform ND 2.0 ug/l
95-49-8 o-Chlorotoluene ND 4.0 ug/l
106-43-4 p-Chlorotoluene ND 2.0 ug/l
124-48-1 Dibromochloromethane ND 2.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 20 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 ug/l
75-71-8 Dichlorodifluoromethane ND 4.0 ug/l
541-73-1 m-Dichlorobenzene ND 4.0 ug/l
95-50-1 o-Dichlorobenzene ND 4.0 ug/l
106-46-7 p-Dichlorobenzene ND 10 ug/l
75-34-3 1,1-Dichloroethane ND 2.0 ug/l
107-06-2 1,2-Dichloroethane 26.0 4.0 ug/l
75-35-4 1,1-Dichloroethylene ND 2.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 2.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 2.0 ug/l
78-87-5 1,2-Dichloropropane ND 2.0 ug/l
142-28-9 1,3-Dichloropropane ND 2.0 ug/l
594-20-7 2,2-Dichloropropane ND 2.0 ug/l
563-58-6 1,1-Dichloropropene ND 2.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 4.0 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 104
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-14
Lab Sample ID:LA5660-10 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 4.0 ug/l
108-20-3 Di-Isopropyl Ether 3.9 2.0 ug/l
64-17-5 Ethyl Alcohol ND 1000 ug/l
100-41-4 Ethylbenzene 2200 4.0 ug/l
591-78-6 2-Hexanone ND 10 ug/l
87-68-3 Hexachlorobutadiene ND 10 ug/l
98-82-8 Isopropylbenzene 127 4.0 ug/l
99-87-6 p-Isopropyltoluene 8.7 2.0 ug/l
74-83-9 Methyl Bromide ND 10 ug/l
74-87-3 Methyl Chloride ND 4.0 ug/l
74-95-3 Methylene Bromide ND 2.0 ug/l
75-09-2 Methylene Chloride ND 10 ug/l
78-93-3 Methyl Ethyl Ketone ND 250 ug/l
108-10-1 4-Methyl-2-pentanone ND 10 ug/l
1634-04-4 Methyl Tert Butyl Ether 399 4.0 ug/l
91-20-3 Naphthalene 888 10 ug/l
103-65-1 n-Propylbenzene 346 2.0 ug/l
100-42-5 Styrene 11.2 2.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 2.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 2.0 ug/l
127-18-4 Tetrachloroethylene ND 4.0 ug/l
108-88-3 Toluene 1740 4.0 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 10 ug/l
71-55-6 1,1,1-Trichloroethane ND 2.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 4.0 ug/l
79-01-6 Trichloroethylene ND 2.0 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 2110 a 15 ug/l
108-67-8 1,3,5-Trimethylbenzene 685 6.0 ug/l
108-05-4 Vinyl Acetate ND 4.0 ug/l
75-01-4 Vinyl Chloride ND 2.0 ug/l
m,p-Xylene 2990 8.0 ug/l
95-47-6 o-Xylene 1530 4.0 ug/l
1330-20-7 Xylene (total)4510 12 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 104%99%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 104
LA5660 33.10
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-14
Lab Sample ID:LA5660-10 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 100%100%70-130%
460-00-4 4-Bromofluorobenzene 102%103%70-130%
(a) Result is from Run# 2
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
48 of 104
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Report of Analysis Page 1 of 1
Client Sample ID:MW-14
Lab Sample ID:LA5660-10 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 15.3 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
49 of 104
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Report of Analysis Page 1 of 3
Client Sample ID:MW-15
Lab Sample ID:LA5660-11 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001939.D 1 04/15/15 SV n/a n/a V2I65
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
50 of 104
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-15
Lab Sample ID:LA5660-11 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene 0.54 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
51 of 104
LA5660 33.11
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-15
Lab Sample ID:LA5660-11 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
52 of 104
LA5660 33.11
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-15
Lab Sample ID:LA5660-11 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead <10 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
53 of 104
LA5660 33.11
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-17
Lab Sample ID:LA5660-12 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001922.D 50 04/14/15 SV n/a n/a V2I63
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 500 ug/l
71-43-2 Benzene 794 15 ug/l
108-86-1 Bromobenzene ND 5.0 ug/l
74-97-5 Bromochloromethane ND 5.0 ug/l
75-27-4 Bromodichloromethane ND 5.0 ug/l
75-25-2 Bromoform ND 10 ug/l
104-51-8 n-Butylbenzene ND 5.0 ug/l
135-98-8 sec-Butylbenzene ND 5.0 ug/l
98-06-6 tert-Butylbenzene ND 5.0 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 ug/l
108-90-7 Chlorobenzene ND 5.0 ug/l
75-00-3 Chloroethane ND 10 ug/l
67-66-3 Chloroform ND 5.0 ug/l
95-49-8 o-Chlorotoluene ND 10 ug/l
106-43-4 p-Chlorotoluene ND 5.0 ug/l
124-48-1 Dibromochloromethane ND 5.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 ug/l
106-93-4 1,2-Dibromoethane ND 5.0 ug/l
75-71-8 Dichlorodifluoromethane ND 10 ug/l
541-73-1 m-Dichlorobenzene ND 10 ug/l
95-50-1 o-Dichlorobenzene ND 10 ug/l
106-46-7 p-Dichlorobenzene ND 25 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 ug/l
107-06-2 1,2-Dichloroethane ND 10 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
54 of 104
LA5660 33.12
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-17
Lab Sample ID:LA5660-12 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 10 ug/l
108-20-3 Di-Isopropyl Ether 35.7 5.0 ug/l
64-17-5 Ethyl Alcohol ND 2500 ug/l
100-41-4 Ethylbenzene 1740 10 ug/l
591-78-6 2-Hexanone ND 25 ug/l
87-68-3 Hexachlorobutadiene ND 25 ug/l
98-82-8 Isopropylbenzene 90.2 10 ug/l
99-87-6 p-Isopropyltoluene 10.5 5.0 ug/l
74-83-9 Methyl Bromide ND 25 ug/l
74-87-3 Methyl Chloride ND 10 ug/l
74-95-3 Methylene Bromide ND 5.0 ug/l
75-09-2 Methylene Chloride 35.6 25 ug/l
78-93-3 Methyl Ethyl Ketone ND 630 ug/l
108-10-1 4-Methyl-2-pentanone ND 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 16.4 10 ug/l
91-20-3 Naphthalene 1070 25 ug/l
103-65-1 n-Propylbenzene 235 5.0 ug/l
100-42-5 Styrene 32.4 5.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 ug/l
127-18-4 Tetrachloroethylene ND 10 ug/l
108-88-3 Toluene 6520 10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 ug/l
79-01-6 Trichloroethylene ND 5.0 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 1830 15 ug/l
108-67-8 1,3,5-Trimethylbenzene 465 15 ug/l
108-05-4 Vinyl Acetate ND 10 ug/l
75-01-4 Vinyl Chloride ND 5.0 ug/l
m,p-Xylene 4030 20 ug/l
95-47-6 o-Xylene 1950 10 ug/l
1330-20-7 Xylene (total)5980 30 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
55 of 104
LA5660 33.12
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-17
Lab Sample ID:LA5660-12 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
56 of 104
LA5660 33.12
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-17
Lab Sample ID:LA5660-12 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 36.8 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
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LA5660 33.12
Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-18
Lab Sample ID:LA5660-13 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001923.D 50 04/14/15 SV n/a n/a V2I63
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 500 ug/l
71-43-2 Benzene 2570 15 ug/l
108-86-1 Bromobenzene ND 5.0 ug/l
74-97-5 Bromochloromethane ND 5.0 ug/l
75-27-4 Bromodichloromethane ND 5.0 ug/l
75-25-2 Bromoform ND 10 ug/l
104-51-8 n-Butylbenzene ND 5.0 ug/l
135-98-8 sec-Butylbenzene ND 5.0 ug/l
98-06-6 tert-Butylbenzene ND 5.0 ug/l
56-23-5 Carbon Tetrachloride ND 5.0 ug/l
108-90-7 Chlorobenzene ND 5.0 ug/l
75-00-3 Chloroethane ND 10 ug/l
67-66-3 Chloroform ND 5.0 ug/l
95-49-8 o-Chlorotoluene ND 10 ug/l
106-43-4 p-Chlorotoluene ND 5.0 ug/l
124-48-1 Dibromochloromethane ND 5.0 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 50 ug/l
106-93-4 1,2-Dibromoethane 14.5 5.0 ug/l
75-71-8 Dichlorodifluoromethane ND 10 ug/l
541-73-1 m-Dichlorobenzene ND 10 ug/l
95-50-1 o-Dichlorobenzene ND 10 ug/l
106-46-7 p-Dichlorobenzene ND 25 ug/l
75-34-3 1,1-Dichloroethane ND 5.0 ug/l
107-06-2 1,2-Dichloroethane 13.1 10 ug/l
75-35-4 1,1-Dichloroethylene ND 5.0 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 5.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 5.0 ug/l
78-87-5 1,2-Dichloropropane ND 5.0 ug/l
142-28-9 1,3-Dichloropropane ND 5.0 ug/l
594-20-7 2,2-Dichloropropane ND 5.0 ug/l
563-58-6 1,1-Dichloropropene ND 5.0 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 10 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
58 of 104
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Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-18
Lab Sample ID:LA5660-13 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 10 ug/l
108-20-3 Di-Isopropyl Ether 305 5.0 ug/l
64-17-5 Ethyl Alcohol ND 2500 ug/l
100-41-4 Ethylbenzene 1830 10 ug/l
591-78-6 2-Hexanone ND 25 ug/l
87-68-3 Hexachlorobutadiene ND 25 ug/l
98-82-8 Isopropylbenzene 66.1 10 ug/l
99-87-6 p-Isopropyltoluene ND 5.0 ug/l
74-83-9 Methyl Bromide ND 25 ug/l
74-87-3 Methyl Chloride ND 10 ug/l
74-95-3 Methylene Bromide ND 5.0 ug/l
75-09-2 Methylene Chloride ND 25 ug/l
78-93-3 Methyl Ethyl Ketone ND 630 ug/l
108-10-1 4-Methyl-2-pentanone ND 25 ug/l
1634-04-4 Methyl Tert Butyl Ether 34.5 10 ug/l
91-20-3 Naphthalene 696 25 ug/l
103-65-1 n-Propylbenzene 150 5.0 ug/l
100-42-5 Styrene 72.6 5.0 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 ug/l
127-18-4 Tetrachloroethylene ND 10 ug/l
108-88-3 Toluene 9840 10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 ug/l
71-55-6 1,1,1-Trichloroethane ND 5.0 ug/l
79-00-5 1,1,2-Trichloroethane ND 10 ug/l
79-01-6 Trichloroethylene ND 5.0 ug/l
75-69-4 Trichlorofluoromethane ND 5.0 ug/l
96-18-4 1,2,3-Trichloropropane ND 5.0 ug/l
95-63-6 1,2,4-Trimethylbenzene 1280 15 ug/l
108-67-8 1,3,5-Trimethylbenzene 291 15 ug/l
108-05-4 Vinyl Acetate ND 10 ug/l
75-01-4 Vinyl Chloride ND 5.0 ug/l
m,p-Xylene 5330 20 ug/l
95-47-6 o-Xylene 2650 10 ug/l
1330-20-7 Xylene (total)7980 30 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
59 of 104
LA5660 33.13
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-18
Lab Sample ID:LA5660-13 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
60 of 104
LA5660 33.13
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-18
Lab Sample ID:LA5660-13 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 73.0 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
61 of 104
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Accutest Laboratories
Report of Analysis Page 1 of 3
Client Sample ID:MW-19
Lab Sample ID:LA5660-14 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2I001940.D 1 04/15/15 SV n/a n/a V2I65
Run #2
Purge Volume
Run #1 25.0 ml
Run #2
VOA Special List
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.30 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.20 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.0 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.20 ug/l
541-73-1 m-Dichlorobenzene ND 0.20 ug/l
95-50-1 o-Dichlorobenzene ND 0.20 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
62 of 104
LA5660 33.14
Accutest Laboratories
Report of Analysis Page 2 of 3
Client Sample ID:MW-19
Lab Sample ID:LA5660-14 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Compound Result RL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.20 ug/l
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.50 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.20 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.30 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.30 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.40 ug/l
95-47-6 o-Xylene ND 0.20 ug/l
1330-20-7 Xylene (total)ND 0.60 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17060-07-0 1,2-Dichloroethane-D4 105%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
63 of 104
LA5660 33.14
Accutest Laboratories
Report of Analysis Page 3 of 3
Client Sample ID:MW-19
Lab Sample ID:LA5660-14 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Method:SM 6200B Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
VOA Special List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
64 of 104
LA5660 33.14
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID:MW-19
Lab Sample ID:LA5660-14 Date Sampled:04/08/15
Matrix:AQ - Ground Water Date Received:04/10/15
Percent Solids:n/a
Project:Pantry #3079, Rocky Mount, NC
Total Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead <10 10 ug/l 1 04/10/15 04/13/15 RT SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA531
(2) Prep QC Batch: MP815
RL = Reporting Limit
65 of 104
LA5660 33.14
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Lafayette
Section 4
66 of 104
LA5660 4
LA5660: Chain of Custody
Page 1 of 4
67 of 104
LA5660 44.1
LA5660: Chain of Custody
Page 2 of 4
68 of 104
LA5660 44.1
LA5660: Chain of Custody
Page 3 of 4
69 of 104
LA5660 44.1
Accutest Laboratories Sample Receipt Summary
Accutest LaboratoriesV:[phone] 500 Ambassador Caffery Parkway Scott, Louisiana 70583www.accutest.com
Accutest Job Number:LA5660 Client:CARDNO
Date / Time Received:4/10/2015 10:00:00 AM Delivery Method:FedEx
Project:PANTRY #3079
4. No. Coolers:1
Airbill #'s:804612306644
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Thermometer ID:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
DV260;
Ice (direct contact)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Initial/Adjusted):#1: (1.6/1.5);
LA5660: Chain of Custody
Page 4 of 4
70 of 104
LA5660 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Lafayette
Section 5
71 of 104
LA5660 5
Method Blank Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I60-MB1 2I001865.D 1 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.10 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.10 ug/l
72 of 104
LA5660 55.1.1
Method Blank Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I60-MB1 2I001865.D 1 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
CAS No.Compound Result RL Units Q
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.20 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene ND 0.50 ug/l
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.20 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.10 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.10 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.20 ug/l
95-47-6 o-Xylene ND 0.10 ug/l
1330-20-7 Xylene (total)ND 0.10 ug/l
73 of 104
LA5660 55.1.1
Method Blank Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I60-MB1 2I001865.D 1 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 91%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
74 of 104
LA5660 55.1.1
Method Blank Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I63-MB3 2I001919.D 1 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.10 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.10 ug/l
75 of 104
LA5660 55.1.2
Method Blank Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I63-MB3 2I001919.D 1 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
CAS No.Compound Result RL Units Q
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.20 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene 0.33 0.50 ug/l J
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene a 0.26 0.20 ug/l
120-82-1 1,2,4-Trichlorobenzene a 0.21 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.10 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.10 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.20 ug/l
95-47-6 o-Xylene ND 0.10 ug/l
1330-20-7 Xylene (total)ND 0.10 ug/l
76 of 104
LA5660 55.1.2
Method Blank Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I63-MB3 2I001919.D 1 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
(a) Analyte was not detected in any of the samples associated with this Method Blank.
77 of 104
LA5660 55.1.2
Method Blank Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I65-MB1 2I001935.D 1 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
CAS No.Compound Result RL Units Q
67-64-1 Acetone ND 10 ug/l
71-43-2 Benzene ND 0.10 ug/l
108-86-1 Bromobenzene ND 0.10 ug/l
74-97-5 Bromochloromethane ND 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.10 ug/l
75-25-2 Bromoform ND 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.10 ug/l
56-23-5 Carbon Tetrachloride ND 0.10 ug/l
108-90-7 Chlorobenzene ND 0.10 ug/l
75-00-3 Chloroethane ND 0.20 ug/l
67-66-3 Chloroform ND 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.20 ug/l
106-43-4 p-Chlorotoluene ND 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 ug/l
106-93-4 1,2-Dibromoethane ND 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.10 ug/l
75-34-3 1,1-Dichloroethane ND 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.20 ug/l
75-35-4 1,1-Dichloroethylene ND 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.10 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.20 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.20 ug/l
108-20-3 Di-Isopropyl Ether ND 0.10 ug/l
64-17-5 Ethyl Alcohol ND 50 ug/l
100-41-4 Ethylbenzene ND 0.10 ug/l
78 of 104
LA5660 55.1.3
Method Blank Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I65-MB1 2I001935.D 1 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
CAS No.Compound Result RL Units Q
591-78-6 2-Hexanone ND 0.50 ug/l
87-68-3 Hexachlorobutadiene ND 0.20 ug/l
98-82-8 Isopropylbenzene ND 0.20 ug/l
99-87-6 p-Isopropyltoluene ND 0.10 ug/l
74-83-9 Methyl Bromide ND 0.50 ug/l
74-87-3 Methyl Chloride ND 0.20 ug/l
74-95-3 Methylene Bromide ND 0.10 ug/l
75-09-2 Methylene Chloride ND 0.20 ug/l
78-93-3 Methyl Ethyl Ketone ND 13 ug/l
108-10-1 4-Methyl-2-pentanone ND 0.50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.20 ug/l
91-20-3 Naphthalene 0.21 0.50 ug/l J
103-65-1 n-Propylbenzene ND 0.10 ug/l
100-42-5 Styrene ND 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.20 ug/l
108-88-3 Toluene ND 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene 0.16 0.20 ug/l J
120-82-1 1,2,4-Trichlorobenzene a 0.12 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.10 ug/l
79-01-6 Trichloroethylene ND 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.10 ug/l
108-05-4 Vinyl Acetate ND 0.20 ug/l
75-01-4 Vinyl Chloride ND 0.10 ug/l
m,p-Xylene ND 0.20 ug/l
95-47-6 o-Xylene ND 0.10 ug/l
1330-20-7 Xylene (total)ND 0.10 ug/l
79 of 104
LA5660 55.1.3
Method Blank Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I65-MB1 2I001935.D 1 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
CAS No.Surrogate Recoveries Limits
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 96%70-130%
(a) Analyte was not detected in any of the samples associated with this Method Blank.
80 of 104
LA5660 55.1.3
Blank Spike Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I60-BS1 2I001863.D 1 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 45.6 91 70-130
71-43-2 Benzene 20 21.1 106 70-130
108-86-1 Bromobenzene 20 20.0 100 70-130
74-97-5 Bromochloromethane 20 18.8 94 70-130
75-27-4 Bromodichloromethane 20 20.3 102 70-130
75-25-2 Bromoform 20 20.3 102 70-130
104-51-8 n-Butylbenzene 20 20.2 101 70-130
135-98-8 sec-Butylbenzene 20 21.7 109 70-130
98-06-6 tert-Butylbenzene 20 21.1 106 70-130
56-23-5 Carbon Tetrachloride 20 22.5 113 70-130
108-90-7 Chlorobenzene 20 20.2 101 70-130
75-00-3 Chloroethane 20 19.4 97 70-130
67-66-3 Chloroform 20 20.3 102 70-130
95-49-8 o-Chlorotoluene 20 20.2 101 70-130
106-43-4 p-Chlorotoluene 20 19.6 98 70-130
124-48-1 Dibromochloromethane 20 19.7 99 70-130
96-12-8 1,2-Dibromo-3-chloropropane 20 16.7 84 70-130
106-93-4 1,2-Dibromoethane 20 19.3 97 70-130
75-71-8 Dichlorodifluoromethane 20 24.2 121 70-130
541-73-1 m-Dichlorobenzene 20 19.4 97 70-130
95-50-1 o-Dichlorobenzene 20 19.0 95 70-130
106-46-7 p-Dichlorobenzene 20 19.0 95 70-130
75-34-3 1,1-Dichloroethane 20 20.5 103 70-130
107-06-2 1,2-Dichloroethane 20 19.9 100 70-130
75-35-4 1,1-Dichloroethylene 20 21.3 107 70-130
156-59-2 cis-1,2-Dichloroethylene 20 19.2 96 70-130
156-60-5 trans-1,2-Dichloroethylene 20 20.1 101 70-130
78-87-5 1,2-Dichloropropane 20 19.7 99 70-130
142-28-9 1,3-Dichloropropane 20 18.2 91 70-130
594-20-7 2,2-Dichloropropane 20 21.2 106 70-130
563-58-6 1,1-Dichloropropene 20 20.8 104 70-130
10061-01-5 cis-1,3-Dichloropropene 20 19.1 96 70-130
10061-02-6 trans-1,3-Dichloropropene 20 18.0 90 70-130
108-20-3 Di-Isopropyl Ether 20 19.0 95 70-130
64-17-5 Ethyl Alcohol 400 338 85 70-130
100-41-4 Ethylbenzene 20 21.0 105 70-130
* = Outside of Control Limits.
81 of 104
LA5660 55.2.1
Blank Spike Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I60-BS1 2I001863.D 1 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 50 39.4 79 70-130
87-68-3 Hexachlorobutadiene 20 21.4 107 70-130
98-82-8 Isopropylbenzene 20 21.7 109 70-130
99-87-6 p-Isopropyltoluene 20 22.1 111 70-130
74-83-9 Methyl Bromide 20 14.9 75 70-130
74-87-3 Methyl Chloride 20 17.8 89 70-130
74-95-3 Methylene Bromide 20 19.0 95 70-130
75-09-2 Methylene Chloride 20 19.9 100 70-130
78-93-3 Methyl Ethyl Ketone 50 46.0 92 70-130
108-10-1 4-Methyl-2-pentanone 50 42.8 86 70-130
1634-04-4 Methyl Tert Butyl Ether 20 18.5 93 70-130
91-20-3 Naphthalene 20 19.1 96 70-130
103-65-1 n-Propylbenzene 20 20.5 103 70-130
100-42-5 Styrene 20 20.2 101 70-130
630-20-6 1,1,1,2-Tetrachloroethane 20 20.5 103 70-130
79-34-5 1,1,2,2-Tetrachloroethane 20 16.5 83 70-130
127-18-4 Tetrachloroethylene 20 22.1 111 70-130
108-88-3 Toluene 20 20.3 102 70-130
87-61-6 1,2,3-Trichlorobenzene 20 21.0 105 70-130
120-82-1 1,2,4-Trichlorobenzene 20 21.0 105 70-130
71-55-6 1,1,1-Trichloroethane 20 22.2 111 70-130
79-00-5 1,1,2-Trichloroethane 20 18.8 94 70-130
79-01-6 Trichloroethylene 20 21.7 109 70-130
75-69-4 Trichlorofluoromethane 20 23.8 119 70-130
96-18-4 1,2,3-Trichloropropane 20 15.7 79 70-130
95-63-6 1,2,4-Trimethylbenzene 20 20.0 100 70-130
108-67-8 1,3,5-Trimethylbenzene 20 21.1 106 70-130
108-05-4 Vinyl Acetate 20 17.6 88 70-130
75-01-4 Vinyl Chloride 20 20.0 100 70-130
m,p-Xylene 40 45.0 113 70-130
95-47-6 o-Xylene 20 20.0 100 70-130
1330-20-7 Xylene (total)60 65.0 108 70-130
* = Outside of Control Limits.
82 of 104
LA5660 55.2.1
Blank Spike Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I60-BS1 2I001863.D 1 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 90%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 95%70-130%
* = Outside of Control Limits.
83 of 104
LA5660 55.2.1
Blank Spike Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I63-BS3 2I001917.D 1 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 47.5 95 70-130
71-43-2 Benzene 20 18.3 92 70-130
108-86-1 Bromobenzene 20 19.2 96 70-130
74-97-5 Bromochloromethane 20 18.2 91 70-130
75-27-4 Bromodichloromethane 20 19.2 96 70-130
75-25-2 Bromoform 20 19.6 98 70-130
104-51-8 n-Butylbenzene 20 20.4 102 70-130
135-98-8 sec-Butylbenzene 20 20.5 103 70-130
98-06-6 tert-Butylbenzene 20 19.4 97 70-130
56-23-5 Carbon Tetrachloride 20 18.4 92 70-130
108-90-7 Chlorobenzene 20 18.8 94 70-130
75-00-3 Chloroethane 20 18.6 93 70-130
67-66-3 Chloroform 20 18.3 92 70-130
95-49-8 o-Chlorotoluene 20 18.8 94 70-130
106-43-4 p-Chlorotoluene 20 18.7 94 70-130
124-48-1 Dibromochloromethane 20 19.3 97 70-130
96-12-8 1,2-Dibromo-3-chloropropane 20 20.2 101 70-130
106-93-4 1,2-Dibromoethane 20 19.3 97 70-130
75-71-8 Dichlorodifluoromethane 20 19.9 100 70-130
541-73-1 m-Dichlorobenzene 20 18.9 95 70-130
95-50-1 o-Dichlorobenzene 20 19.3 97 70-130
106-46-7 p-Dichlorobenzene 20 18.6 93 70-130
75-34-3 1,1-Dichloroethane 20 17.3 87 70-130
107-06-2 1,2-Dichloroethane 20 18.8 94 70-130
75-35-4 1,1-Dichloroethylene 20 17.8 89 70-130
156-59-2 cis-1,2-Dichloroethylene 20 18.6 93 70-130
156-60-5 trans-1,2-Dichloroethylene 20 17.7 89 70-130
78-87-5 1,2-Dichloropropane 20 18.7 94 70-130
142-28-9 1,3-Dichloropropane 20 18.8 94 70-130
594-20-7 2,2-Dichloropropane 20 17.2 86 70-130
563-58-6 1,1-Dichloropropene 20 19.2 96 70-130
10061-01-5 cis-1,3-Dichloropropene 20 18.9 95 70-130
10061-02-6 trans-1,3-Dichloropropene 20 19.5 98 70-130
108-20-3 Di-Isopropyl Ether 20 19.1 96 70-130
64-17-5 Ethyl Alcohol 400 413 103 70-130
100-41-4 Ethylbenzene 20 19.0 95 70-130
* = Outside of Control Limits.
84 of 104
LA5660 55.2.2
Blank Spike Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I63-BS3 2I001917.D 1 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 50 48.1 96 70-130
87-68-3 Hexachlorobutadiene 20 19.9 100 70-130
98-82-8 Isopropylbenzene 20 20.6 103 70-130
99-87-6 p-Isopropyltoluene 20 20.5 103 70-130
74-83-9 Methyl Bromide 20 17.0 85 70-130
74-87-3 Methyl Chloride 20 19.9 100 70-130
74-95-3 Methylene Bromide 20 18.9 95 70-130
75-09-2 Methylene Chloride 20 18.5 93 70-130
78-93-3 Methyl Ethyl Ketone 50 46.9 94 70-130
108-10-1 4-Methyl-2-pentanone 50 46.4 93 70-130
1634-04-4 Methyl Tert Butyl Ether 20 18.2 91 70-130
91-20-3 Naphthalene 20 20.5 103 70-130
103-65-1 n-Propylbenzene 20 18.9 95 70-130
100-42-5 Styrene 20 19.8 99 70-130
630-20-6 1,1,1,2-Tetrachloroethane 20 18.8 94 70-130
79-34-5 1,1,2,2-Tetrachloroethane 20 20.4 102 70-130
127-18-4 Tetrachloroethylene 20 17.5 88 70-130
108-88-3 Toluene 20 18.3 92 70-130
87-61-6 1,2,3-Trichlorobenzene 20 20.2 101 70-130
120-82-1 1,2,4-Trichlorobenzene 20 19.4 97 70-130
71-55-6 1,1,1-Trichloroethane 20 18.0 90 70-130
79-00-5 1,1,2-Trichloroethane 20 18.8 94 70-130
79-01-6 Trichloroethylene 20 18.4 92 70-130
75-69-4 Trichlorofluoromethane 20 18.5 93 70-130
96-18-4 1,2,3-Trichloropropane 20 16.6 83 70-130
95-63-6 1,2,4-Trimethylbenzene 20 19.8 99 70-130
108-67-8 1,3,5-Trimethylbenzene 20 19.8 99 70-130
108-05-4 Vinyl Acetate 20 18.1 91 70-130
75-01-4 Vinyl Chloride 20 19.5 98 70-130
m,p-Xylene 40 37.8 95 70-130
95-47-6 o-Xylene 20 18.7 94 70-130
1330-20-7 Xylene (total)60 56.5 94 70-130
* = Outside of Control Limits.
85 of 104
LA5660 55.2.2
Blank Spike Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I63-BS3 2I001917.D 1 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
86 of 104
LA5660 55.2.2
Blank Spike Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I65-BS1 2I001933.D 1 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 50 48.0 96 70-130
71-43-2 Benzene 20 19.1 96 70-130
108-86-1 Bromobenzene 20 20.1 101 70-130
74-97-5 Bromochloromethane 20 19.2 96 70-130
75-27-4 Bromodichloromethane 20 20.4 102 70-130
75-25-2 Bromoform 20 20.8 104 70-130
104-51-8 n-Butylbenzene 20 21.3 107 70-130
135-98-8 sec-Butylbenzene 20 21.4 107 70-130
98-06-6 tert-Butylbenzene 20 20.0 100 70-130
56-23-5 Carbon Tetrachloride 20 18.8 94 70-130
108-90-7 Chlorobenzene 20 19.4 97 70-130
75-00-3 Chloroethane 20 19.6 98 70-130
67-66-3 Chloroform 20 18.9 95 70-130
95-49-8 o-Chlorotoluene 20 19.4 97 70-130
106-43-4 p-Chlorotoluene 20 19.8 99 70-130
124-48-1 Dibromochloromethane 20 20.7 104 70-130
96-12-8 1,2-Dibromo-3-chloropropane 20 21.2 106 70-130
106-93-4 1,2-Dibromoethane 20 19.9 100 70-130
75-71-8 Dichlorodifluoromethane 20 19.9 100 70-130
541-73-1 m-Dichlorobenzene 20 19.7 99 70-130
95-50-1 o-Dichlorobenzene 20 19.9 100 70-130
106-46-7 p-Dichlorobenzene 20 19.4 97 70-130
75-34-3 1,1-Dichloroethane 20 18.3 92 70-130
107-06-2 1,2-Dichloroethane 20 19.9 100 70-130
75-35-4 1,1-Dichloroethylene 20 18.8 94 70-130
156-59-2 cis-1,2-Dichloroethylene 20 19.0 95 70-130
156-60-5 trans-1,2-Dichloroethylene 20 18.5 93 70-130
78-87-5 1,2-Dichloropropane 20 19.2 96 70-130
142-28-9 1,3-Dichloropropane 20 20.2 101 70-130
594-20-7 2,2-Dichloropropane 20 19.0 95 70-130
563-58-6 1,1-Dichloropropene 20 20.0 100 70-130
10061-01-5 cis-1,3-Dichloropropene 20 19.5 98 70-130
10061-02-6 trans-1,3-Dichloropropene 20 20.4 102 70-130
108-20-3 Di-Isopropyl Ether 20 20.1 101 70-130
64-17-5 Ethyl Alcohol 400 402 101 70-130
100-41-4 Ethylbenzene 20 19.6 98 70-130
* = Outside of Control Limits.
87 of 104
LA5660 55.2.3
Blank Spike Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I65-BS1 2I001933.D 1 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 50 50.4 101 70-130
87-68-3 Hexachlorobutadiene 20 20.4 102 70-130
98-82-8 Isopropylbenzene 20 21.4 107 70-130
99-87-6 p-Isopropyltoluene 20 21.3 107 70-130
74-83-9 Methyl Bromide 20 17.9 90 70-130
74-87-3 Methyl Chloride 20 21.1 106 70-130
74-95-3 Methylene Bromide 20 19.7 99 70-130
75-09-2 Methylene Chloride 20 18.8 94 70-130
78-93-3 Methyl Ethyl Ketone 50 47.6 95 70-130
108-10-1 4-Methyl-2-pentanone 50 50.2 100 70-130
1634-04-4 Methyl Tert Butyl Ether 20 19.3 97 70-130
91-20-3 Naphthalene 20 21.4 107 70-130
103-65-1 n-Propylbenzene 20 19.4 97 70-130
100-42-5 Styrene 20 20.8 104 70-130
630-20-6 1,1,1,2-Tetrachloroethane 20 19.8 99 70-130
79-34-5 1,1,2,2-Tetrachloroethane 20 20.9 105 70-130
127-18-4 Tetrachloroethylene 20 18.3 92 70-130
108-88-3 Toluene 20 19.3 97 70-130
87-61-6 1,2,3-Trichlorobenzene 20 21.0 105 70-130
120-82-1 1,2,4-Trichlorobenzene 20 20.3 102 70-130
71-55-6 1,1,1-Trichloroethane 20 18.5 93 70-130
79-00-5 1,1,2-Trichloroethane 20 19.8 99 70-130
79-01-6 Trichloroethylene 20 19.1 96 70-130
75-69-4 Trichlorofluoromethane 20 19.2 96 70-130
96-18-4 1,2,3-Trichloropropane 20 16.7 84 70-130
95-63-6 1,2,4-Trimethylbenzene 20 20.5 103 70-130
108-67-8 1,3,5-Trimethylbenzene 20 20.2 101 70-130
108-05-4 Vinyl Acetate 20 19.1 96 70-130
75-01-4 Vinyl Chloride 20 20.1 101 70-130
m,p-Xylene 40 39.4 99 70-130
95-47-6 o-Xylene 20 19.6 98 70-130
1330-20-7 Xylene (total)60 59.0 98 70-130
* = Outside of Control Limits.
88 of 104
LA5660 55.2.3
Blank Spike Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2I65-BS1 2I001933.D 1 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
CAS No.Surrogate Recoveries BSP Limits
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
* = Outside of Control Limits.
89 of 104
LA5660 55.2.3
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-12MS 2I001875.D 10 04/13/15 CR n/a n/a V2I60
LA5660-12MSD 2I001876.D 10 04/13/15 CR n/a n/a V2I60
LA5660-12 a 2I001872.D 10 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
LA5660-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 500 450 90 500 482 96 7 70-130/20
71-43-2 Benzene 957 200 1080 62* b 200 1070 57* b 1 70-130/20
108-86-1 Bromobenzene ND 200 202 101 200 198 99 2 70-130/20
74-97-5 Bromochloromethane ND 200 194 97 200 207 104 6 70-130/20
75-27-4 Bromodichloromethane ND 200 211 106 200 206 103 2 70-130/20
75-25-2 Bromoform ND 200 215 108 200 209 105 3 70-130/20
104-51-8 n-Butylbenzene ND 200 276 138* c 200 270 135* c 2 70-130/20
135-98-8 sec-Butylbenzene 25.3 200 235 105 200 226 100 4 70-130/20
98-06-6 tert-Butylbenzene ND 200 211 106 200 201 101 5 70-130/20
56-23-5 Carbon Tetrachloride ND 200 256 128 200 246 123 4 70-130/20
108-90-7 Chlorobenzene ND 200 206 103 200 198 99 4 70-130/20
75-00-3 Chloroethane ND 200 200 100 200 202 101 1 70-130/20
67-66-3 Chloroform ND 200 219 110 200 216 108 1 70-130/20
95-49-8 o-Chlorotoluene ND 200 197 99 200 193 97 2 70-130/20
106-43-4 p-Chlorotoluene ND 200 194 97 200 193 97 1 70-130/20
124-48-1 Dibromochloromethane ND 200 213 107 200 206 103 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 200 182 91 200 191 96 5 70-130/20
106-93-4 1,2-Dibromoethane ND 200 204 102 200 199 100 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 200 178 89 200 176 88 1 70-130/20
541-73-1 m-Dichlorobenzene ND 200 193 97 200 188 94 3 70-130/20
95-50-1 o-Dichlorobenzene ND 200 188 94 200 183 92 3 70-130/20
106-46-7 p-Dichlorobenzene ND 200 184 92 200 182 91 1 70-130/20
75-34-3 1,1-Dichloroethane ND 200 218 109 200 207 104 5 70-130/20
107-06-2 1,2-Dichloroethane ND 200 209 105 200 211 106 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 200 211 106 200 208 104 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 200 198 99 200 198 99 0 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 200 193 97 200 193 97 0 70-130/20
78-87-5 1,2-Dichloropropane ND 200 206 103 200 200 100 3 70-130/20
142-28-9 1,3-Dichloropropane ND 200 198 99 200 194 97 2 70-130/20
594-20-7 2,2-Dichloropropane ND 200 187 94 200 182 91 3 70-130/20
563-58-6 1,1-Dichloropropene ND 200 208 104 200 208 104 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 200 189 95 200 187 94 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 200 191 96 200 186 93 3 70-130/20
108-20-3 Di-Isopropyl Ether 35.1 200 242 103 200 243 104 0 70-130/20
64-17-5 Ethyl Alcohol ND 4000 4210 105 4000 3680 92 13 70-130/20
100-41-4 Ethylbenzene 1200 E 200 1220 10* b 200 1230 15* b 1 70-130/20
* = Outside of Control Limits.
90 of 104
LA5660 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-12MS 2I001875.D 10 04/13/15 CR n/a n/a V2I60
LA5660-12MSD 2I001876.D 10 04/13/15 CR n/a n/a V2I60
LA5660-12 a 2I001872.D 10 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
LA5660-12 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 500 453 91 500 459 92 1 70-130/20
87-68-3 Hexachlorobutadiene ND 200 162 81 200 158 79 3 70-130/20
98-82-8 Isopropylbenzene 119 200 327 104 200 314 98 4 70-130/20
99-87-6 p-Isopropyltoluene 16.9 200 252 118 200 243 113 4 70-130/20
74-83-9 Methyl Bromide ND 200 86.8 43* c 200 119 60* c 31* c 70-130/20
74-87-3 Methyl Chloride ND 200 142 71 200 136 68* c 4 70-130/20
74-95-3 Methylene Bromide ND 200 196 98 200 197 99 1 70-130/20
75-09-2 Methylene Chloride ND 200 207 104 200 206 103 0 70-130/20
78-93-3 Methyl Ethyl Ketone ND 500 485 97 500 500 100 3 70-130/20
108-10-1 4-Methyl-2-pentanone ND 500 477 95 500 473 95 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether 16.1 200 221 102 200 224 104 1 70-130/20
91-20-3 Naphthalene 1250 200 1420 85 200 1450 100 2 70-130/20
103-65-1 n-Propylbenzene 348 200 491 72 200 481 67* c 2 70-130/20
100-42-5 Styrene 33.2 200 243 105 200 236 101 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 200 217 109 200 208 104 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 200 181 91 200 179 90 1 70-130/20
127-18-4 Tetrachloroethylene ND 200 212 106 200 203 102 4 70-130/20
108-88-3 Toluene 2820 E 200 2820 0* b 200 2820 0* b 0 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 200 193 97 200 195 98 1 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 200 197 99 200 199 100 1 70-130/20
71-55-6 1,1,1-Trichloroethane ND 200 229 115 200 223 112 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 200 249 125 200 248 124 0 70-130/20
79-01-6 Trichloroethylene ND 200 209 105 200 202 101 3 70-130/20
75-69-4 Trichlorofluoromethane ND 200 233 117 200 230 115 1 70-130/20
96-18-4 1,2,3-Trichloropropane ND 200 210 105 200 202 101 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1420 E 200 1370 -25* b 200 1390 -15* b 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene 653 200 786 67* b 200 779 63* b 1 70-130/20
108-05-4 Vinyl Acetate ND 200 205 103 200 207 104 1 70-130/20
75-01-4 Vinyl Chloride ND 200 194 97 200 195 98 1 70-130/20
m,p-Xylene 2010 E 400 2040 8* b 400 2050 10* b 0 70-130/20
95-47-6 o-Xylene 1480 E 200 1480 0* b 200 1480 0* b 0 70-130/20
1330-20-7 Xylene (total)3490 E 600 3520 5* b 600 3530 7* b 0 70-130/20
* = Outside of Control Limits.
91 of 104
LA5660 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-12MS 2I001875.D 10 04/13/15 CR n/a n/a V2I60
LA5660-12MSD 2I001876.D 10 04/13/15 CR n/a n/a V2I60
LA5660-12 a 2I001872.D 10 04/13/15 CR n/a n/a V2I60
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6
CAS No.Surrogate Recoveries MS MSD LA5660-12 Limits
17060-07-0 1,2-Dichloroethane-D4 101%106%70-130%
2037-26-5 Toluene-D8 99%99%70-130%
460-00-4 4-Bromofluorobenzene 102%101%70-130%
(a) Sample used for QC purposes only.
(b) Outside control limits due to high level in sample relative to spike amount.
(c) Outside control limits due to matrix interference. Blank Spike meets acceptance criteria.
* = Outside of Control Limits.
92 of 104
LA5660 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-13MS 2I001924.D 50 04/14/15 SV n/a n/a V2I63
LA5660-13MSD 2I001925.D 50 04/14/15 SV n/a n/a V2I63
LA5660-13 2I001923.D 50 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
LA5660-13 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 2500 2750 110 2500 2850 114 4 70-130/20
71-43-2 Benzene 2570 1000 2340 -23* a 1000 2440 -13* a 4 70-130/20
108-86-1 Bromobenzene ND 1000 1040 104 1000 1050 105 1 70-130/20
74-97-5 Bromochloromethane ND 1000 965 97 1000 989 99 2 70-130/20
75-27-4 Bromodichloromethane ND 1000 1020 102 1000 1050 105 3 70-130/20
75-25-2 Bromoform ND 1000 1020 102 1000 1090 109 7 70-130/20
104-51-8 n-Butylbenzene ND 1000 1050 105 1000 1010 101 4 70-130/20
135-98-8 sec-Butylbenzene ND 1000 1070 107 1000 1030 103 4 70-130/20
98-06-6 tert-Butylbenzene ND 1000 1000 100 1000 963 96 4 70-130/20
56-23-5 Carbon Tetrachloride ND 1000 958 96 1000 936 94 2 70-130/20
108-90-7 Chlorobenzene ND 1000 995 100 1000 1000 100 1 70-130/20
75-00-3 Chloroethane ND 1000 944 94 1000 906 91 4 70-130/20
67-66-3 Chloroform ND 1000 973 97 1000 971 97 0 70-130/20
95-49-8 o-Chlorotoluene ND 1000 980 98 1000 940 94 4 70-130/20
106-43-4 p-Chlorotoluene ND 1000 998 100 1000 958 96 4 70-130/20
124-48-1 Dibromochloromethane ND 1000 1030 103 1000 1060 106 3 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 1000 1010 101 1000 1050 105 4 70-130/20
106-93-4 1,2-Dibromoethane 14.5 1000 1010 100 1000 1030 102 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 1000 916 92 1000 890 89 3 70-130/20
541-73-1 m-Dichlorobenzene ND 1000 964 96 1000 943 94 2 70-130/20
95-50-1 o-Dichlorobenzene ND 1000 972 97 1000 963 96 1 70-130/20
106-46-7 p-Dichlorobenzene ND 1000 950 95 1000 948 95 0 70-130/20
75-34-3 1,1-Dichloroethane ND 1000 943 94 1000 919 92 3 70-130/20
107-06-2 1,2-Dichloroethane 13.1 1000 997 98 1000 1050 104 5 70-130/20
75-35-4 1,1-Dichloroethylene ND 1000 947 95 1000 940 94 1 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 1000 993 99 1000 974 97 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 1000 939 94 1000 932 93 1 70-130/20
78-87-5 1,2-Dichloropropane ND 1000 963 96 1000 1010 101 5 70-130/20
142-28-9 1,3-Dichloropropane ND 1000 996 100 1000 1040 104 4 70-130/20
594-20-7 2,2-Dichloropropane ND 1000 823 82 1000 804 80 2 70-130/20
563-58-6 1,1-Dichloropropene ND 1000 1020 102 1000 1020 102 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 1000 962 96 1000 1010 101 5 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 1000 1010 101 1000 1030 103 2 70-130/20
108-20-3 Di-Isopropyl Ether 305 1000 1170 87 1000 1190 89 2 70-130/20
64-17-5 Ethyl Alcohol ND 20000 19900 100 20000 21100 106 6 70-130/20
100-41-4 Ethylbenzene 1830 1000 2060 23* b 1000 2010 18* b 2 70-130/20
* = Outside of Control Limits.
93 of 104
LA5660 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-13MS 2I001924.D 50 04/14/15 SV n/a n/a V2I63
LA5660-13MSD 2I001925.D 50 04/14/15 SV n/a n/a V2I63
LA5660-13 2I001923.D 50 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
LA5660-13 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 2500 2440 98 2500 2630 105 7 70-130/20
87-68-3 Hexachlorobutadiene ND 1000 911 91 1000 915 92 0 70-130/20
98-82-8 Isopropylbenzene 66.1 1000 1130 106 1000 1110 104 2 70-130/20
99-87-6 p-Isopropyltoluene ND 1000 1050 105 1000 1030 103 2 70-130/20
74-83-9 Methyl Bromide ND 1000 597 60* b 1000 717 72 18 70-130/20
74-87-3 Methyl Chloride ND 1000 1080 108 1000 1050 105 3 70-130/20
74-95-3 Methylene Bromide ND 1000 983 98 1000 1050 105 7 70-130/20
75-09-2 Methylene Chloride ND 1000 1010 101 1000 1010 101 0 70-130/20
78-93-3 Methyl Ethyl Ketone ND 2500 2440 98 2500 2350 94 4 70-130/20
108-10-1 4-Methyl-2-pentanone ND 2500 2350 94 2500 2710 108 14 70-130/20
1634-04-4 Methyl Tert Butyl Ether 34.5 1000 961 93 1000 1010 98 5 70-130/20
91-20-3 Naphthalene 696 1000 1310 61* b 1000 1390 69* b 6 70-130/20
103-65-1 n-Propylbenzene 150 1000 1070 92 1000 1020 87 5 70-130/20
100-42-5 Styrene 72.6 1000 1080 101 1000 1100 103 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 1000 1000 100 1000 1020 102 2 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 1000 1050 105 1000 1040 104 1 70-130/20
127-18-4 Tetrachloroethylene ND 1000 914 91 1000 892 89 2 70-130/20
108-88-3 Toluene 9840 1000 6820 -302* a 1000 6710 -313* a 2 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 1000 961 96 1000 999 100 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 1000 944 94 1000 970 97 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 1000 943 94 1000 920 92 2 70-130/20
79-00-5 1,1,2-Trichloroethane ND 1000 984 98 1000 1030 103 5 70-130/20
79-01-6 Trichloroethylene ND 1000 958 96 1000 990 99 3 70-130/20
75-69-4 Trichlorofluoromethane ND 1000 940 94 1000 910 91 3 70-130/20
96-18-4 1,2,3-Trichloropropane ND 1000 1030 103 1000 1070 107 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1280 1000 1710 43* b 1000 1670 39* b 2 70-130/20
108-67-8 1,3,5-Trimethylbenzene 291 1000 1190 90 1000 1140 85 4 70-130/20
108-05-4 Vinyl Acetate ND 1000 974 97 1000 1020 102 5 70-130/20
75-01-4 Vinyl Chloride ND 1000 972 97 1000 958 96 1 70-130/20
m,p-Xylene 5330 2000 5040 -15* a 2000 5020 -16* a 0 70-130/20
95-47-6 o-Xylene 2650 1000 2440 -21* a 1000 2420 -23* a 1 70-130/20
1330-20-7 Xylene (total)7980 3000 7470 -17* a 3000 7440 -18* a 0 70-130/20
* = Outside of Control Limits.
94 of 104
LA5660 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-13MS 2I001924.D 50 04/14/15 SV n/a n/a V2I63
LA5660-13MSD 2I001925.D 50 04/14/15 SV n/a n/a V2I63
LA5660-13 2I001923.D 50 04/14/15 SV n/a n/a V2I63
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-10, LA5660-12, LA5660-13
CAS No.Surrogate Recoveries MS MSD LA5660-13 Limits
17060-07-0 1,2-Dichloroethane-D4 99%102%105%70-130%
2037-26-5 Toluene-D8 99%104%98%70-130%
460-00-4 4-Bromofluorobenzene 103%105%105%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
(b) Outside control limits due to matrix interference. Blank Spike meets acceptance criteria.
* = Outside of Control Limits.
95 of 104
LA5660 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-10MS 2I001944.D 20 04/15/15 SV n/a n/a V2I65
LA5660-10MSD 2I001945.D 20 04/15/15 SV n/a n/a V2I65
LA5660-10 2I001943.D 20 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
LA5660-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone ND 1000 1490 149* a 1000 889 89 51* a 70-130/20
71-43-2 Benzene 3400 400 3530 33* b 400 3390 -3* b 4 70-130/20
108-86-1 Bromobenzene ND 400 425 106 400 421 105 1 70-130/20
74-97-5 Bromochloromethane ND 400 364 91 400 370 93 2 70-130/20
75-27-4 Bromodichloromethane ND 400 431 108 400 425 106 1 70-130/20
75-25-2 Bromoform ND 400 427 107 400 434 109 2 70-130/20
104-51-8 n-Butylbenzene ND 400 520 130 400 517 129 1 70-130/20
135-98-8 sec-Butylbenzene 18.5 400 474 114 400 458 110 3 70-130/20
98-06-6 tert-Butylbenzene ND 400 425 106 400 418 105 2 70-130/20
56-23-5 Carbon Tetrachloride ND 400 430 108 400 374 94 14 70-130/20
108-90-7 Chlorobenzene ND 400 411 103 400 394 99 4 70-130/20
75-00-3 Chloroethane ND 400 394 99 400 383 96 3 70-130/20
67-66-3 Chloroform ND 400 399 100 400 390 98 2 70-130/20
95-49-8 o-Chlorotoluene ND 400 410 103 400 400 100 2 70-130/20
106-43-4 p-Chlorotoluene ND 400 423 106 400 415 104 2 70-130/20
124-48-1 Dibromochloromethane ND 400 433 108 400 431 108 0 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 400 409 102 400 446 112 9 70-130/20
106-93-4 1,2-Dibromoethane ND 400 416 104 400 418 105 0 70-130/20
75-71-8 Dichlorodifluoromethane ND 400 356 89 400 342 86 4 70-130/20
541-73-1 m-Dichlorobenzene ND 400 402 101 400 391 98 3 70-130/20
95-50-1 o-Dichlorobenzene ND 400 393 98 400 403 101 3 70-130/20
106-46-7 p-Dichlorobenzene ND 400 398 100 400 393 98 1 70-130/20
75-34-3 1,1-Dichloroethane ND 400 373 93 400 359 90 4 70-130/20
107-06-2 1,2-Dichloroethane 26.0 400 424 100 400 428 101 1 70-130/20
75-35-4 1,1-Dichloroethylene ND 400 354 89 400 335 84 6 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 400 390 98 400 380 95 3 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 400 359 90 400 348 87 3 70-130/20
78-87-5 1,2-Dichloropropane ND 400 395 99 400 384 96 3 70-130/20
142-28-9 1,3-Dichloropropane ND 400 415 104 400 413 103 0 70-130/20
594-20-7 2,2-Dichloropropane ND 400 386 97 400 365 91 6 70-130/20
563-58-6 1,1-Dichloropropene ND 400 409 102 400 392 98 4 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 400 407 102 400 401 100 1 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 400 429 107 400 425 106 1 70-130/20
108-20-3 Di-Isopropyl Ether 3.9 400 402 100 400 396 98 2 70-130/20
64-17-5 Ethyl Alcohol ND 8000 9130 114 8000 9270 116 2 70-130/20
100-41-4 Ethylbenzene 2200 400 2330 33* b 400 2230 8* b 4 70-130/20
* = Outside of Control Limits.
96 of 104
LA5660 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-10MS 2I001944.D 20 04/15/15 SV n/a n/a V2I65
LA5660-10MSD 2I001945.D 20 04/15/15 SV n/a n/a V2I65
LA5660-10 2I001943.D 20 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
LA5660-10 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 1000 1000 100 1000 1060 106 6 70-130/20
87-68-3 Hexachlorobutadiene ND 400 383 96 400 373 93 3 70-130/20
98-82-8 Isopropylbenzene 127 400 596 117 400 572 111 4 70-130/20
99-87-6 p-Isopropyltoluene 8.7 400 480 118 400 474 116 1 70-130/20
74-83-9 Methyl Bromide ND 400 203 51* a 400 273 68* a 29* a 70-130/20
74-87-3 Methyl Chloride ND 400 396 99 400 383 96 3 70-130/20
74-95-3 Methylene Bromide ND 400 400 100 400 407 102 2 70-130/20
75-09-2 Methylene Chloride ND 400 372 93 400 368 92 1 70-130/20
78-93-3 Methyl Ethyl Ketone ND 1000 977 98 1000 960 96 2 70-130/20
108-10-1 4-Methyl-2-pentanone ND 1000 1010 101 1000 1070 107 6 70-130/20
1634-04-4 Methyl Tert Butyl Ether 399 400 774 94 400 798 100 3 70-130/20
91-20-3 Naphthalene 888 400 1310 106 400 1330 111 2 70-130/20
103-65-1 n-Propylbenzene 346 400 764 105 400 747 100 2 70-130/20
100-42-5 Styrene 11.2 400 451 110 400 437 106 3 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 400 424 106 400 413 103 3 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 400 431 108 400 442 111 3 70-130/20
127-18-4 Tetrachloroethylene ND 400 383 96 400 366 92 5 70-130/20
108-88-3 Toluene 1740 400 2260 130 400 2150 103 5 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 400 396 99 400 403 101 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 400 386 97 400 386 97 0 70-130/20
71-55-6 1,1,1-Trichloroethane ND 400 383 96 400 369 92 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 400 446 112 400 431 108 3 70-130/20
79-01-6 Trichloroethylene ND 400 393 98 400 379 95 4 70-130/20
75-69-4 Trichlorofluoromethane ND 400 403 101 400 391 98 3 70-130/20
96-18-4 1,2,3-Trichloropropane ND 400 439 110 400 434 109 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2210 E 400 2390 45* b 400 2380 43* b 0 70-130/20
108-67-8 1,3,5-Trimethylbenzene 685 400 1150 116 400 1130 111 2 70-130/20
108-05-4 Vinyl Acetate ND 400 401 100 400 405 101 1 70-130/20
75-01-4 Vinyl Chloride ND 400 395 99 400 377 94 5 70-130/20
m,p-Xylene 2990 800 3210 28* b 800 3150 20* b 2 70-130/20
95-47-6 o-Xylene 1530 400 2020 123 400 1930 100 5 70-130/20
1330-20-7 Xylene (total)4510 1200 5220 59* b 1200 5070 47* b 3 70-130/20
* = Outside of Control Limits.
97 of 104
LA5660 55.3.3
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:LA5660
Account:ATCNCR Cardno ATC
Project:Pantry #3079, Rocky Mount, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
LA5660-10MS 2I001944.D 20 04/15/15 SV n/a n/a V2I65
LA5660-10MSD 2I001945.D 20 04/15/15 SV n/a n/a V2I65
LA5660-10 2I001943.D 20 04/15/15 SV n/a n/a V2I65
The QC reported here applies to the following samples:Method: SM 6200B
LA5660-7, LA5660-8, LA5660-9, LA5660-10, LA5660-11, LA5660-14
CAS No.Surrogate Recoveries MS MSD LA5660-10 Limits
17060-07-0 1,2-Dichloroethane-D4 105%106%104%70-130%
2037-26-5 Toluene-D8 98%98%100%70-130%
460-00-4 4-Bromofluorobenzene 105%103%102%70-130%
(a) Outside control limits due to matrix interference. Blank Spike meets acceptance criteria.
(b) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
98 of 104
LA5660 55.3.3
Accutest Laboratories
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Lafayette
Section 6
99 of 104
LA5660 6
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: LA5660
Account: ATCNCR - Cardno ATC
Project: Pantry #3079, Rocky Mount, NC
QC Batch ID: MP815 Methods: SW846 6010B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 04/10/15
MB
Metal RL IDL MDL raw final
Aluminum 100 36 87
Antimony 10 2.3 3.6
Arsenic 20 2.1 5
Barium 10 .2 .47
Beryllium 10 .1 .13
Boron 100 .5 .91
Cadmium 10 .3 .44
Calcium 100 4.5 47
Chromium 10 .4 .47
Cobalt 10 .3 .73
Copper 10 1 2.2
Iron 100 7.1 32
Lead 10 1.1 3.6 -0.10 <10
Lithium 10 1.9 2.4
Magnesium 100 8.3 54
Manganese 10 .1 .11
Molybdenum 10 .4 .8
Nickel 10 .5 1.8
Potassium 100 77 20
Selenium 20 2.4 9.2
Silver 10 .7 1.3
Sodium 100 26 14
Strontium 10 .1 .38
Thallium 10 1.6 4.4
Tin 10 1.1 4.3
Titanium 10 .1 .41
Vanadium 10 1 2.8
Zinc 20 4.8 2.1
Associated samples MP815: LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6, LA5660-7, LA5660-8,
LA5660-9, LA5660-10, LA5660-11, LA5660-12, LA5660-13, LA5660-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
100 of 104
LA5660 66.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LA5660
Account: ATCNCR - Cardno ATC
Project: Pantry #3079, Rocky Mount, NC
QC Batch ID: MP815 Methods: SW846 6010B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 04/10/15
LA5660-1 Spikelot QC
Metal Original MS ICPSPIKE % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 16.5 975 1000 95.9 75-125
Lithium
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP815: LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6, LA5660-7, LA5660-8,
LA5660-9, LA5660-10, LA5660-11, LA5660-12, LA5660-13, LA5660-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
101 of 104
LA5660 66.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: LA5660
Account: ATCNCR - Cardno ATC
Project: Pantry #3079, Rocky Mount, NC
QC Batch ID: MP815 Methods: SW846 6010B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 04/10/15
LA5660-1 Spikelot MSD QC
Metal Original MSD ICPSPIKE % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 16.5 989 1000 97.3 1.4 20
Lithium
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP815: LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6, LA5660-7, LA5660-8,
LA5660-9, LA5660-10, LA5660-11, LA5660-12, LA5660-13, LA5660-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
102 of 104
LA5660 66.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: LA5660
Account: ATCNCR - Cardno ATC
Project: Pantry #3079, Rocky Mount, NC
QC Batch ID: MP815 Methods: SW846 6010B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 04/10/15
BSP Spikelot QC
Metal Result ICPSPIKE % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 973 1000 97.3 80-120
Lithium
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP815: LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6, LA5660-7, LA5660-8,
LA5660-9, LA5660-10, LA5660-11, LA5660-12, LA5660-13, LA5660-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
103 of 104
LA5660 66.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: LA5660
Account: ATCNCR - Cardno ATC
Project: Pantry #3079, Rocky Mount, NC
QC Batch ID: MP815 Methods: SW846 6010B
Matrix Type: AQUEOUS Units: ug/l
Prep Date: 04/10/15
LA5660-1 QC
Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 16.5 24.5 48.5 (a) 0-10
Lithium
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP815: LA5660-1, LA5660-2, LA5660-3, LA5660-4, LA5660-5, LA5660-6, LA5660-7, LA5660-8,
LA5660-9, LA5660-10, LA5660-11, LA5660-12, LA5660-13, LA5660-14
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
104 of 104
LA5660 66.1.4