FA-29019_48211_CA_SCH_20220531

Groundwater & Environmental Services, Inc.
104 Corporate Boulevard, Suite 411
West Columbia, SC 29169
T. 866.765.4851

GESonline.com
May 31, 2022
Sarah Brown
NCDEQ – DWM – UST Section – FRO
225 Green Street - #714 Systel Building
Fayetteville, North Carolina 28301

Re: Limited Site Check Report
Murphy Express 6760
909 US Highway 15-401 Bypass
Laurinburg, North Carolina 28352
UST Incident # 48211

Dear Ms. Brown:
As per your request in correspondence dated March 23, 2022, Groundwater & Environmental
Services, Inc., on behalf of the responsible party, is pleased to provide you with the enclosed
Limited Site Check Report for the referenced site for your review and approval. The report details
initial environmental assessment activities at the site. Following review should you have any
questions or require additional information, please do not hesitate to contact the undersigned by
phone at 866-765-4851 x4526 or by email at [e-mail].
Sincerely,
Groundwater & Environmental Services, Inc.

Aaron R. Williamson, PG Daniel Dabkowski
Staff Geologist Senior Project Manager

Enclosure
Cc: Jose Rios Cortes, Murphy USA, Project File

Murphy Oil USA, Inc.

Limited Site Check Report
Murphy USA #6760
909 US Highway 15
Laurinburg, North Carolina 28352
NCDEQ Incident #48211

May 31, 2022

Version 1

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Page i

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, North Carolina 28352
Prepared for:
Murphy Oil USA, Inc.
200 Peach Street, PO Box 7300
El Dorado, Arkansas 71731
Prepared by:
Groundwater & Environmental Services, Inc.
104 Corporate Boulevard – Suite 411
West Columbia, South Carolina 29169
TEL: [phone]
www.gesonline.com
GES Project:
2701928
Date:
May 31, 2022

Aaron Williamson, PG
Staff Geologist

Daniel Dabkowski
Senior Project Manager

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Page ii

Table of Contents
1 Introduction ......................................................................................................................... 1
2 Site History and Characterization ........................................................................................ 1
2.1 Owner/Operator Information ........................................................................................... 1
2.2 UST System Information ................................................................................................ 1
2.3 Past Releases ................................................................................................................ 1
2.4 Current Release ............................................................................................................. 2
2.5 Site Characteristics......................................................................................................... 2
2.5.1 Land Use ................................................................................................................. 2
2.5.2 Limited Receptor Survey ......................................................................................... 2
2.5.3 Site Geography/Geology/Hydrogeology ................................................................... 3
3 Limited Site Check .............................................................................................................. 3
3.1 Rationale & Scope of Work ............................................................................................. 3
3.2 Site Investigation ............................................................................................................ 4
3.2.1 Utility Designation .................................................................................................... 4
3.2.2 Soil Sample Collection ............................................................................................. 4
3.2.3 Groundwater Sample Collection .............................................................................. 5
3.2.4 Sample Handling and Analysis ................................................................................ 5
3.2.5 Analytical Results .................................................................................................... 5
4 Conclusions and Recommendations ................................................................................... 6

Figures
Figure 1 – Site Location Map
Figure 2 – Site Map
Figure 3 – Soil Analytical Data Map
Figure 4 – Groundwater Monitoring Map
Tables
Table 1 – Site History – UST Owner/Operator & Other Responsible Party Information
Table 2 – UST System & Other Release Information
Table 3 – Summary of Soil Analytical Results
Table 4 – Summary of Water Analytical Results
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Page iii

Appendices
Appendix A – Relevant Correspondence
Appendix B – Boring Logs
Appendix C – Laboratory Analytical Report

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Page iv

Acronyms
AMSL Above Mean Sea Level
AST Aboveground Storage Tank
BGS Below Ground Surface
DRO Diesel Range Organics
DWM Division of Waste Management
EDB Ethylene Dibromide
EPA Environmental Protection Agency
EPH Extractable Petroleum Hydrocarbons
GES Groundwater & Environmental Services, Inc.
GRO Gasoline Range Organics
LSA Limited Site Assessment
MADEP Massachusetts Department of Environmental Protection
MSCC Maximum Soil Contaminant Concentration
NCAC North Carolina Administrative Code
NCDEQ North Carolina Department of Environmental Quality
PID Photo-ionization Detector
ppm Parts per million
STW Soil-to-Water
SVOC Semi-volatile Organic Compound
TPH Total Petroleum Hydrocarbons
TWT Taylor Wiseman & Taylor
UDC Under Dispenser Containment
USCS Unified Soil Classification System
UST Underground Storage Tank
VERCO Versatile Environmental Resource Company
VOC Volatile Organic Compound
VPH Volatile Petroleum Hydrocarbons

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 1

SITE INFORMATION
Date of Report: May 31, 2022
SITE IDENTIFICATION
Facility ID: 00-0-0000036436
UST Incident No: 48211
Site Risk: Low (Previous Incident)
Agency Contact: Sarah Brown, NCDEQ, Fayetteville Regional Office
Site Name: Murphy USA #6760
Site Street Address: 909 Highway 15-401 Bypass
Laurinburg, North Carolina 28352
County: Scotland
Latitude / Longitude: 34.762245° / -79.482405° (UST Database)

SITE CONTACT INFORMATION
UST Owner/Operator: Murphy USA, Inc.
Address: 200 Peach Street / PO Box 7300
El Dorado, AR 71731
Telephone: [phone]
Contact: Jose Rios Cortes, Sr. Manager Environmental Strategy

Property Owner: Murphy Oil USA, Inc.
Address: PO Box 7300
El Dorado, AR 71731
Telephone [phone]
Contact Jose Rios Cortes

Consultant: Groundwater & Environmental Services, Inc.
Address: 104 Corporate Boulevard, Suite 411
West Columbia, SC 29169
Telephone: [phone]
NC License No: C-353

Analytical Laboratory: Pace Analytical Services, LLC
Address: 9800 Kincey Avenue
Huntersville, NC 28078
Telephone: [phone]
State Certification No: 12

INFORMATION ABOUT THE RELEASE
Date Discovered: December 12, 2021
Estimated Quantity of Release: 1,090-gallons premium gasoline
Cause of Release: Physical/Mechanical Damage (vehicle collision)
Source of Release: Dispenser 7/8 (Diesel and Gasoline)
UST(s) Size & Contents: See Table 2

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 2

CERTIFICATION
I, Aaron R. Williamson, a Licensed Geologist employed by Groundwater & Environmental
Services, Inc. do certify that the information contained in this report is correct and accurate to the
best of my knowledge.

Aaron R. Williamson, P.G.
P.G. License No. 2712

Groundwater & Environmental Services, Inc. is licensed to practice geology in North Carolina.
The certification number of the company or corporation to practice geology is C-353.

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 1

EXECUTIVE SUMMARY
As required, the following executive summary provides the most pertinent information discussed
in this report. For additional information please refer to subsequent sections of this report.
 GES performed a limited site check in response to regulatory requirements directing an
investigation to determine the presence of environmental contamination due to a release from
a damaged fuel dispenser.
 On May 4, 2022, six (6) soil borings were advanced around the subject dispenser for soil and
groundwater sample collection. Soils consisted primarily of sand, and groundwater was
encountered at approximately seven (7) feet below ground surface (BGS).
 One (1) soil sample was retained from unsaturated soils of each boring within the depth
interval exhibiting the greatest field screening results, and one (1) groundwater sample was
collected from the boring exhibiting the greatest overall field screening results.
 Results of laboratory analysis indicated that soil and groundwater at the site is impacted above
unrestricted use standards.
 Additional assessment is recommended.

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 1

1 Introduction
Groundwater & Environmental Services, Inc. (GES) was retained by Murphy Oil USA, Inc.
(Murphy) to perform a limited site check associated with a release of petroleum product at the
Murphy USA #6760 facility located at 909 US Highway 15-401 Bypass in Laurinburg, Scotland
County, North Carolina (site). The site location is illustrated on Figure 1. The purpose of this
“Limited Site Check Report” is to present results of a limited subsurface investigation at the site
and determine if environmental contamination is present at the site as a result of the recent
release. This report has been prepared in general accordance with Title 15A of the North Carolina
Administrative Code (NCAC), Subchapter 2L and the North Carolina Department of
Environmental Quality (NCDEQ), Division of Waste Management (DWM), Underground Storage
Tank (UST) Section Guidelines for Site Checks, Tank Closure, and Initial Response and
Abetment, Change 11 dated May 17, 2021.
2 Site History and Characterization
The site is located southwest of the intersection of McColl Road (US Highway 15/401/501) and
West Boulevard (NC Secondary Highway 1108). The site currently operates as a Murphy Express
gas station and convenience store with an active underground storage tank (UST) system. No
above ground storage tank (AST) systems are present at the site.
2.1 Owner/Operator Information
The UST system at the site is currently owned and operated by Murphy. Murphy has owned and
operated the UST system since it was installed in 2001. UST owner/operator information is
summarized in Table 1.
2.2 UST System Information
UST system information is summarized in Table 2 and illustrated on Figure 2. The system
consists of two (2) compartmentalized USTs oriented north-south within a common tank hold
located in the northeast quadrant of the site property. Four (4) dispenser islands are located
beneath a dispenser canopy trending east to west, with two (2) islands on either side of a centrally
located convenience store/kiosk building. Double-sided gasoline dispensers are present at each
dispenser island with the easternmost dispenser (#7/8) also serving diesel.
2.3 Past Releases
GES reviewed the North Carolina Department of Environmental Quality (NCDEQ) UST Incident
Management Database pertaining to past releases at the site. The site has one (1) closed release
incident registered with the NCDEQ identified as incident number 29897 which was associated
with a leak of gasoline from beneath dispenser 5/6 on January 10, 2014. Soil contamination was
discovered and approximately 4.24-tons of soil were excavated from the western side of the
oil/water separator (OWS) at the site, extending to a maximum depth of approximately one (1)
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 2

foot below ground surface (BGS); groundwater was not encountered in the excavation.
Confirmatory soil sampling revealed no exceedances of the regulatory limits. The incident
received regulatory closure on February 24, 2014. Please refer to historical reports for additional
information.
2.4 Current Release
The summary below is based on the Initial Abatement Action Report dated March 18, 2022.
On December 12, 2021, a release from the UST system occurred when a customer vehicle
collided with gasoline/diesel dispenser 7/8, the easternmost dispenser. The collision damaged
the dispenser and caused a release of petroleum product onto the ground surface around the
dispenser. The flow of fuel was eventually stopped, but free product was reportedly observed
flowing across the concrete parking lot and entering the site storm sewer system and OWS. An
emergency response contractor was retained to perform containment and cleanup activities.
Between December 12 and 13, 2021, approximately 4,948-gallons of liquid was recovered from
the site, consisting primarily of petroleum contact water rinsate from storm sewer and OWS
cleaning activities. Post-abatement field screening indicated no elevated photo-ionization detector
(PID) readings at the site. No soil staining or impact to the nearby surface water drainage feature
was identified. The release was reported to the NCDEQ on December 13, 2021. Statistical
inventory reconciliation records indicated a loss of approximately 1,090-gallons of premium
gasoline.
Tightness testing performed by MUSA on December 15, 2021 indicated that the regular gasoline
and diesel lines both passed. On January 3, 2022, the dispenser sump failed hydrostatic testing
and the premium gasoline line tested tight after repairs. The entire diesel piping system was also
tightness tested and passed on February 25, 2022.
2.5 Site Characteristics
2.5.1 Land Use
The site is located on a 0.49-acre parcel of land owned by MUSA and currently operates as
Murphy USA #6760, an active convenience store and fueling station with unbranded petroleum
retail. The site is utilized for commercial purposes with adjoining properties in all cardinal
directions also utilized for commercial purposes. The site is bound to the north by a commercial
strip mall with various tenants, to the east by US Highway 15/401/501 beyond which is a Lowes
Home Improvement store, to the south by Tidal Wave Auto Spa, and to the west by a Walmart
Supercenter. The nearest residential properties are located approximately 500-feet northwest of
the site.
2.5.2 Limited Receptor Survey
Municipal water appears to be supplied to the site and vicinity by the City of Laurinburg (PWS ID
NC0383010) sourced by groundwater from a series of wells. The NCDEQ SWAP Info 2.0
database indicates no water wells are present within approximately 1,500-feet of the site, and no
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 3

wellhead protection areas were identified on or near the site. On-site underground structures
include the UST system, OWS, storm sewer system, sanitary sewer, and municipal water;
additional utilities may be present. The closest natural surface water body to the site is Bridge
Creek located approximately 1,800-feet west of the site. A storm water drainage feature is
adjacent to the east of the site which drains toward Bridge Creek. Bridge Creek is classified as a
Class C: Swamp Water surface water body. A detailed receptor survey was not performed.
2.5.3 Site Geography/Geology/Hydrogeology
Site topography is relatively flat at an elevation of approximately 220-feet above mean sea level
(AMSL). Surface cover at the site consists primarily of concrete with landscaped areas along the
perimeter. Surface runoff at the site flows to the east towards a storm sewer system which
discharges to an open drainage ditch adjacent to the east of the site. Regional groundwater flow
is expected to follow surface topography towards the south or west.

The site is located within the Coastal Plain physiographic province of NC. According to the 1985
Geologic Map of North Carolina published by the North Carolina Geological Survey, the site is
underlain by the Middendorf Formation characterized by sand, sandstone, and mudstone with
clay balls and iron-cemented concretions; laterally discontinuous cross bedding is common.
Groundwater beneath the site is encountered approximately seven (7) feet BGS. Site-specific
groundwater flow direction, gradient, and seepage velocity are unknown. The surficial aquifer in
this area is estimated to be approximately 50-feet thick. Depth to bedrock beneath the site is
unknown.
3 Limited Site Check
3.1 Rationale & Scope of Work
In response to a Notice of Regulatory Requirements dated March 23, 2022, GES developed a
scope of work to complete a limited site check since the source of the release was known and
localized; the investigation focused around the source which was dispenser #7/8. To provide
sufficient spatial coverage, six (6) soil borings were proposed to be advanced in all cardinal
directions from the dispenser pending identification of the locations of existing underground
utilities and the UST system.
To provide sufficient vertical profiling, borings were planned to be advanced to 15-feet BGS or to
the top of the water table. Additionally, groundwater evaluation was proposed by collecting one
(1) groundwater sample from a temporary monitoring well installed in the worst-case soil boring.
The analytical suite included a broad spectrum of parameters for gasoline and diesel based on
the products served at the subject dispenser, the source of the release. The scope of work was
approved by the NCDEQ in email correspondence dated March 25, 2022. Relevant
correspondence is included in Appendix A.
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 4

3.2 Site Investigation
3.2.1 Utility Designation
GES contacted the NC 811 service to identify and mark public utilities at the site. GES also
contracted with Taylor Wiseman & Taylor (TWT), a private utility locator, to provide subsurface
utility clearance activities. GES and the utility locator mobilized to the site on May 2, 2022.
Between May 2 and 3, 2022, TWT performed utility locating and air knifing activities under GES
supervision. Utility locating was performed using ground penetrating radar (GPR) and
electromagnetic (EM) trace methods. To confirm the absence of underground utilities or structures
at the proposed boring locations, each location was saw cut and air knifed to approximately eight
(8) feet BGS. Material removed from air knifing was placed back into the hole, and the ground
surface was repaired with patch material.
3.2.2 Soil Sample Collection
Between May 2 and 3, 2022, soil samples were collected from six (6) boring locations (SB-1
through SB-6) as shown on Figure 3. Soil samples were collected via a decontaminated hand
auger at approximate two (2) foot intervals. In general, the soil borings were located within
concrete surfacing under the canopy, adjacent to the UST system, and advanced into native
material. Gravel fill material was encountered in boring locations SB-5 and SB-6 which were
adjacent to the west of the UST pit. Static groundwater was observed in the borings at
approximately seven (7) feet BGS.
A portion of the soils recovered from each depth interval were placed into sealable, air-tight
containers with headspace and allowed to volatilize at an ambient temperature of at least 68
degrees Fahrenheit (°F) for approximately 15-minutes prior to field screening with a Honeywell
MiniRAE 3000+ PID calibrated to 100 parts per million (ppm) isobutylene. The tip of the PID was
used to pierce the bag and the maximum response was recorded as the headspace was
withdrawn. Recovered soils were also classified per the Unified Soil Classification System
(USCS). The primary soil type was identified as clayey sand. Soils from the depth interval
exhibiting the highest PID result per boring were retained for laboratory analysis. Soils were not
collected below the water table Soil boring logs are included in Appendix B.
A summary of field data is provided below; elevated PID readings (>50 ppm) were not detected.
Boring/Sample
ID
Depth
(feet BGS)
PID
(ppm)
Soil Type Sample
Date/Time
SB-1 2.0-4.0 14.0 Clayey Sand 5/2/22 – 12:40
SB-2 4.0-6.0 2.0 Clayey Sand 5/2/22 – 13:00
SB-3 4.0-6.0 0.0 Clayey Sand 5/2/22 – 15:40
SB-4 4.0-6.0 0.0 Clayey Sand 5/3/22 – 12:15
SB-5 4.0-6.0 0.0 Clayey Sand 5/3/22 – 11:35
SB-6 4.0-6.0 0.0 Clayey Sand 5/3/22 – 10:00
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 5

3.2.3 Groundwater Sample Collection
Soil boring SB-1 exhibited the highest field screening result and was selected as the groundwater
sample location. On May 4, 2022, SB-1 was advanced to approximately 20 feet BGS using direct-
push technology by a licensed well driller employed by Versatile Environmental Resource
Company (VERCO). Groundwater samples (SB-1 Water) were collected through a 2 foot stainless
steel screen point sampler deployed at a depth of approximately 16 feet BGS using a peristaltic
pump and dedicated tubing. Following collection of samples, soil borings and the temporary
monitoring well were backfilled and abandoned with Portland cement grout and the ground
surface was patched with concrete.
3.2.4 Sample Handling and Analysis
To reduce the potential of cross contamination, dedicated nitrile gloves were worn during all
phases of sample handling. Non-disposable sampling equipment was decontaminated using a
non-phosphate detergent and potable water. Each laboratory sample was placed into pre-cleaned
laboratory provided containers pre-filled with appropriate preservatives, labeled with indelible ink,
entered into chain-of-custody, immediately placed on wet ice in a cooler maintained at
approximately four (4) degrees Celsius (°C), and transported to the contract laboratory under
standard chain-of-custody protocol for analysis. The samples were submitted to Pace Analytical
Services, LLC, a NCDEQ accredited laboratory (#12 and #40), for analyses as follows:
 Soil: Total Petroleum Hydrocarbons – Gasoline Range Organics (TPH-GRO) and Total
Petroleum Hydrocarbons – Diesel Range Organics (TPH-DRO) by US Environmental
Protection Agency (EPA) Method 8015 and volatile organic compounds (VOCs) by EPA
Method 8260; and
 Groundwater: VOCs via Standard Methods 6200B, semi-volatile organic compounds
(SVOCs) via EPA Method 625, ethylene dibromide (EDB) via EPA Method 504.1, total lead
by EPA Method 6010, and both Volatile Petroleum Hydrocarbons (VPH) and Extractable
Petroleum Hydrocarbons (EPH) via Massachusetts Department of Environmental Protection
(MADEP) Methods.
3.2.5 Analytical Results
The soil analytical results were compared to the NCDEQ Action Levels for TPH-GRO/DRO,
Industrial/Commercial Maximum Soil Contaminant Concentrations (MSCCs), and Soil-to-Water
(STW) MSCCs. The groundwater analytical results were compared to the groundwater quality
standards defined in Title 15A of the North Carolina Administrative Code (NCAC), Subchapter 2L,
Section .0202 (2L Standards) and the Gross Contamination Levels (GCLs) established by the
NCDEQ.
Soil analytical detections are summarized below:
 Benzene was reported in soil sample SB-1 (2-4’) at a concentration of 0.0614 milligrams
per kilogram (mg/kg) which exceeded the STW MSCC of 0.0072 mg/kg.
 No exceedances of the Industrial/Commercial MSCCs or Action Levels were reported.
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352
Privileged and confidential information Page 6

Groundwater analytical detections from sample SB-1 are summarized below:
 Benzene was reported at a concentration of 68.4 micrograms per liter (ug/L) which
exceeded the 2L Standard of 1 ug/L.
 VPH C5-C8 Aliphatics were reported at a concentration of 540 ug/L which exceeded the
2L Standard of 400 ug/L.
 VPH/EPH C9-C22 Aromatics were reported at a concentration of 1,000 ug/L which
exceeded the 2L Standard of 200 ug/L.
 No exceedances of the GCL were reported.
The laboratory analytical report is included in Appendix C with soil and groundwater analytical
results summarized on Figure 3 and Figure 4, respectively.
4 Conclusions and Recommendations
GES has performed a limited site check at the site in response to a release of petroleum product
resulting in suspected environmental contamination. Based on the results of subsurface
investigation, soil and groundwater at the site has been impacted by gasoline above unrestricted
use standards. GES recommends the following:
 Performance of a Limited Site Assessment (LSA) to confirm the site risk ranking as a route
to incident closure.

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352

Figures

Murphy USAMUSA Store #6760909 US Highway 15Laurinburg, North Carolina
Site Location Map
Quadrangle Location
SITE
Source:
USGS 7.5 Minute Series
Topographic Quadrangle, Laurinburg, North CarolinaContour Interval =
1982
10'
North Carolina Designed
Approved
Scale In Feet
0 2000
W.G.S.Drawn
N Figure5/13/22Date
Groundwater & Environmental Services, Inc.M:\Graphics\2700-Columbia\MISC\Murphy Oil USA\6760 Laurinburg\6760 Laurinburg SLM.dwg, SLM, WShea1
3
0.614
4
540
1,00068.4
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352

Tables

Limited Site Check Report
Murphy Express #6760
909 US Highway 15-401 Bypass, Laurinburg, NC 28352
UST ID Number 1 through 2 Facility ID Number 00-0-0000036436
City State Zip Telephone Number
El Dorado AR 71730 [phone]
City State Zip Telephone Number
El Dorado AR 71730 [phone]
Incident Number 29897 Date Incident Occurred 1/10/2014
Date Incident Report 1/13/2014
Date Incident Closed 2/24/2014
City State Zip Telephone Number
El Dorado AR 71730 [phone]
200 Peach Street / PO Box 7300
Street Address
200 Peach Street / PO Box 7300
Other Incidents Onsite or Commingled/In Close Proximity
Name of Other Responsible Party
Murphy Oil USA, Inc.
Street Address
Street Address
200 Peach Street / PO Box 7300
Name of Operator Dates of Operation (MM/DD/YY to MM/DD/YY)
Murphy Oil USA, Inc.06/05/2008 to Present
TABLE 1
SITE HISTORY - UST OWNER / OPERATOR & OTHER RESPONSIBLE PARTY INFORMATION
Name of Owner Dates of Operation (MM/DD/YY to MM/DD/YY)
Murphy Oil USA, Inc.12/14/2001 to Present
Privileged and Confidential Page 1 of 1
Limited Site Check Report
Murphy Express #6760
909 US Highway 15-401 Bypass, Laurinburg, NC 28352
UST ID Number
Current/Last
Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
(feet)
Description of
Associated Piping
and Pumps
Date Tank
Installed
Status of
UST
Was Release
Associated with
the UST System?
1A Gasoline (Regular)N/A 14,000 DW FRP Unknown DW Poly/Pressure 12/14/01 Active No
1B Gasoline (Premium)N/A 7,000 DW FRP Unknown DW Poly/Pressure 12/14/01 Active Yes
2A Gasoline (Regular)N/A 14,000 DW FRP Unknown DW Poly/Pressure 12/14/01 Active No
2B Diesel N/A 7,000 DW FRP Unknown DW Poly/Pressure 12/14/01 Active No
AST ID Number
Current/Last
Contents Previous Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated Piping
and Pumps
Date Tank
Installed
Status of
AST
Was Release
Associated with
the AST System?
Incident
Number Material Released Date of Release
29897 Gasoline 1/10/2014
Notes:
SW = Single Wall
FRP = Fiberglass Reinforced Plastic
TABLE 2
UST SYSTEM AND OTHER RELEASE INFORMATION
None
Descrtiption of Release
Leak from under dispenser 5/6.
Privileged and Confidential Page 1 of 1
Limited Site Check Report
Murphy Express #6760
909 US Highway 15-401 Bypass, Laurinburg, NC 28352
Sample ID Sample
Date
50 100 --------------------------------------------
---- ----14,000 4,670 36 297 1,810 27 23,300 18,600 2,330 2,330 46,700
---- ---- 0.0072 0.4 0.0019 8 0.085 0.2 1.4 5.4 6.6 6.6 6
SB-1 (2-4') 5/2/2022 8.0 J <6.0 0.0614 <0.0108 <0.0108 0.0392 <0.0108 <0.0108 0.0112 0.165 0.0175 <0.0108 0.156
SB-2 (4-6') 5/2/2022 <12.8 <6.1 <0.0103 0.0057 J <0.0103 <0.0103 <0.0103 <0.0103 <0.0103 <0.0103 <0.0103 <0.0103 0.0106 J
SB-3 (4-6') 5/2/2022 <11.2 <5.7 <0.0103 0.006 J <0.0103 0.0064 J <0.0103 <0.0103 <0.0103 <0.0103 <0.0103 <0.0103 0.0099 J
SB-4 (4-6') 5/3/2022 <11.3 <5.9 <0.009 0.0052 J <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 <0.009 0.0089 J
SB-5 (4-6') 5/3/2022 <11.3 <5.6 <0.0095 0.0048 J <0.0095 <0.0095 <0.0095 <0.0095 <0.0095 <0.0095 <0.0095 <0.0095 <0.0095
SB-6 (4-6') 5/3/2022 <10.6 <5.3 <0.0084 0.0044 J <0.0084 0.0054 J <0.0084 <0.0084 <0.0084 0.0045 J <0.0084 <0.0084 0.0205
NOTES:
Units are milligrams per kilogram (mg/kg = ppm) unless otherwise noted
Bold typeface indicates concentration is greater than action level
Italic typface indicates the analyte was not detected, but the reporting limit exceeds the regulatory limit.
MSCCs = Maximum Soil Contaminant Concentration Levels
STW = Soil-to-water
Ind/Comm = Industrial/Commercial
BGS = Below Ground Surface
TPH = Total Petroleum Hydrocarbons
GRO = Gasoline Range Organics
DRO = Diesel Range Organics
Analytes not shown were below laboratory reporting limits in all samples; refer to the laboratory report for additional information
COC = Contaminant of Concern Naphthalenen-PropylbenzenTolueneTable 3
Summary of Soil Analytical Results
Action Level
Ind/Comm MSCCs
STW MSCCs
COC →TPH-GROTPH-DROChlorobenzeneBenzene1,2-Dichloroethane1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesEthylbenzeneMethyl-tert-butyl etherPrivileged and Confidential Page 1 of 1
Limited Site Check Report
Murphy Express #6760
909 US Highway 15-401, Laurinburg, NC 28352
504.1 6020
Sample ID Date
400 700 10,000 200 1 70 600 70 20 6 70 600 400 500 0.02 15
---- ---- ---- ---- 5,000 70,000 80,000 30,500 20,000 6,000 26,100 260,000 24,100 50,000 50 15,000
SB-1 5/4/2022 540 61.5 <98.0 1,000 68.4 2.8 11.6 0.39 J 5.5 <2.0 0.55 <0.50 0.69 2.58 <0.020 6.5
NOTES:
Units are micrograms per liter (ug/L) unless otherwise noted
Bold typeface indicates concentration is greater than the 2L Standards.
GCL = Gross Contaminant Level
Analytes not shown were below reporting limits; refer to the laboratory report for additional information.LeadAnalytical Method →MADEP SM 6200
GCL
Table 4
Summary of Water Analytical Results
Naphthalene1,3,5-TrimethylbenzeneEthylene DibromideVPH C5-C8 AliphaticsVPH/EPH C9-C18 AliphaticsEPH C19-C36 AliphaticsVPH/EPH C9-C22 Aromatics2L Standard
COC →BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl etherDiisopropyl etherIsopropylbenzene (Cumene)n-PropylbenzenePrivileged and Confidential Page 1 of 1
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352

Appendix A – Relevant Correspondence

March 23, 2022
Email Only
Murphy Oil USA, Inc.
Beth Titus
Re: Notice of Regulatory Requirements
15A NCAC 2N .0602 and .0603
Investigation and Confirmation of a Suspected
Release from an Underground Storage Tank
Murphy Oil USA, Inc. #6760
909 US Highway 15 - 401 Bypass Laurinburg
Scotland County
Incident Number: 48211
Risk Classification: Pending
Ranking: Pending
Dear Ms. Titus:
Information received by the Fayetteville Regional Office of the UST Section, Division of Waste
Management, on March 22, 2022 indicates the potential for a suspected subsurface release due to an
accident.
Records indicate that you are the owner or operator of a UST system suspected of being the source
for this release. Therefore, you must immediately investigate to confirm the suspected release pursuant
to Title 15A NCAC 2N .0603. To achieve compliance with this rule,
in accordance with 40 CFR
280.52(b) (as incorporated by Title 15A NCAC 2N .0603) as described in the most recent version of the
Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement Action
for UST Releases, as available at https://deq.nc.gov/about/divisions/waste-
management/ust/guidance-documents
The results of the site check must be received by this office within 30 days of receipt of this
notice. If a release or discharge is confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to
the Department of Environmental Quality in accordance with Title 15A NCAC 2L .0103(e) and
2L .0111(b).
Failure to comply in the manner and time specified may result in the assessment of
civil penalties and/or the use of other enforcement mechanisms.
If you have any questions regarding the actions that must be taken or the rules mentioned in this
letter, please contact Sarah Brown at the address or telephone number listed below.
cc: Scotland County Health Department Director: Eli Caldwell (email only)
GES Senior Project Manager: Daniel Dabkowski (email only)
Fayetteville Regional Office | 225 Green St | #714 Systel Building | Fayetteville, NC 28301 | [phone]
SITE CHECK 2N .0602 elig NOR 0718.dotx
Sarah Brown
Environmental Specialist II
Fayetteville Regional Office
UST Section, Division of Waste Management, NCDEQ
Sincerely,
1
Aaron Williamson
From:Brown, Sarah B <[e-mail]>
Sent:Tuesday, April 5, 2022 2:58 PM
To:Aaron Williamson
Subject:RE: [External] Murphy Oil USA, Inc. #6760 - Incident 48211
CAUTION: This email originated from outside your organization. Exercise caution when opening attachments
or clicking links, especially from unknown senders.
Hi Aaron,

Your request for an extension is granted. The new due date for the Site Check Report submittal is May 31, 2022.

Sincerely,

UST Web Page UST GIS Map PIB Records Laserfiche WebLink

For spills or other environmental emergencies after hours:
NC DEQ DWM Duty Phone [phone]
NC State Emergency Management 1-800-858-0368
National Response Center 1-800-424-8802

Based on the current guidance to minimize the spread of COVID-19, the Department of Environmental Quality has adjusted operations to protect the
health and safety of the staff and public. Many employees are working remotely or are on staggered shifts. To accommodate these staffing changes,
all DEQ office locations are limiting public access to appointments only. Please check with the appropriate staff before visiting our offices, as we
may be able to handle your requests by phone or email. We appreciate your patience as we continue to serve the public during this challenging time.

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Aaron Williamson <[e-mail]>
Sent: Tuesday, April 5, 2022 11:07 AM
To: Brown, Sarah B <[e-mail]>
Subject: RE: [External] Murphy Oil USA, Inc. #6760 - Incident 48211

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Hi Sarah,

Due to driller availability, we will not be able to complete this work within the 30 days from the date of your notice. The
earliest availability to begin drilling is May 1, 2022, therefore at this time we would like to request an extension of the
due date for the site check report to May 31, 2022. Please confirm.
2

Thank you,

Aaron R Williamson, PG
Staff Geologist

Office: 866.765.4851 ext. 4526
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
104 Corporate Blvd, Suite 411
West Columbia, SC 29169

Follow Us: Website | LinkedIn | Twitter

GES: Plan for Safety, Plan for Success

From: Brown, Sarah B <[e-mail]>
Sent: Friday, March 25, 2022 12:57 PM
To: Aaron Williamson <[e-mail]>
Subject: RE: [External] Murphy Oil USA, Inc. #6760 - Incident 48211

CAUTION: This email originated from outside your organization. Exercise caution when opening attachments
or clicking links, especially from unknown senders.
Good Afternoon Aaron,

If possible, place the borings closer to the dispenser. If piping, utilities, etc. prohibits that, then these distances should
be sufficient.

Thanks,

UST Web Page UST GIS Map PIB Records Laserfiche WebLink

For spills or other environmental emergencies after hours:
NC DEQ DWM Duty Phone [phone]
NC State Emergency Management 1-800-858-0368
National Response Center 1-800-424-8802

Based on the current guidance to minimize the spread of COVID-19, the Department of Environmental Quality has adjusted operations to protect the
3
health and safety of the staff and public. Many employees are working remotely or are on staggered shifts. To accommodate these staffing changes,
all DEQ office locations are limiting public access to appointments only. Please check with the appropriate staff before visiting our offices, as we
may be able to handle your requests by phone or email. We appreciate your patience as we continue to serve the public during this challenging time.

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

From: Aaron Williamson <[e-mail]>
Sent: Friday, March 25, 2022 8:05 AM
To: Brown, Sarah B <[e-mail]>
Subject: [External] Murphy Oil USA, Inc. #6760 - Incident 48211

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Good morning Sarah,

We are in receipt of your NORR dated March 23, 2022 for the subject site. I wanted let you know of our plan for the
limited site check. We are planning to do six soil borings around the affected dispenser which was the source of the
release as shown on the attached figure, and plan to bore to a maximum depth of 15-feet for soil sample collection. We
will be conducting field screening on the recovered soils and retaining one sample per boring which appears to be the
worst-case depth interval per the field screening. Since gravel backfill material around the UST system is assumed, we
also plan to convert the boring with the highest screening reading or, in the absence of elevated screening results, the
furthest down gradient boring into a temporary monitoring well to collect one groundwater sample.

Please confirm that this will meet the requirements.

Thanks,

Aaron R Williamson, PG
Staff Geologist

Office: 866.765.4851 ext. 4526
Mobile: [phone]
[e-mail]

Groundwater & Environmental Services, Inc.
104 Corporate Blvd, Suite 411
West Columbia, SC 29169

Follow Us: Website | LinkedIn | Twitter

GES: Plan for Safety, Plan for Success

Confidentiality Notice: This transmission (including any attachments) may contain confidential information belonging to
Groundwater & Environmental Services, Inc. and is intended only for the use of the party or entity to which it is
addressed. If you are not the intended recipient, you are hereby notified that any disclosure, copying, distribution,
retention or the taking of action in reliance on the contents of this transmission is strictly prohibited; provided, however,
the prohibition against disclosure shall not apply if the transmission is required by law to be disclosed by a governmental
4
intended party as a public record. If you have received this transmission in error, please immediately notify the sender
and erase all information and attachments. Thank You.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email
before responding back to, clicking on any links or opening any attachments. If it appears suspicious
delete it immediately.

TAKE NOTE: This E-Mail came from outside of GES. Please consider the sender and nature of email
before responding back to, clicking on any links or opening any attachments. If it appears suspicious
delete it immediately.
1/23/45/67/8Ri
p
-R
a
p
Tank
Pit
Source
DI1
OWS1
DI2
D2
D1
OWS3 OWS2
Culvert
Murphy USASite #6760909 US 15-401 Bypass (McColl Rd)Laurinburg, NC 28352
Site Map
Scale In Feet
0 20
N
Groundwater & Environmental Services, Inc.
Designed
ApprovedD.C.
X.X.Drawn
Figure03/21/22Date
2
L:\Projects\MurphyUSA\LaurinburgNC\CAD\Murphy_USA_site_6760_SM.dwg, B-, JWiggert
Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352

Appendix B – Soil Boring Logs

Limited Site Check Report
Murphy USA #6760
909 US Highway 15-401 Bypass
Laurinburg, NC 28352

Appendix C – Laboratory Analytical Report

#=CL#
May 31, 2022
LIMS USE: FR - DANIEL DABKOWSKI
LIMS OBJECT ID: 92603521
92603521
Project:
Pace Project No.:
RE:
Daniel Dabkowski
GES
104 Corporate Blvd
Suite 411
West Columbia, SC 29169
MUSA 6760
Dear Daniel Dabkowski:
Enclosed are the analytical results for sample(s) received by the laboratory on May 06, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Peachtree Corners, GA
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 57
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92603521
MUSA 6760
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E87315
Georgia DW Inorganics Certification #: 812
North Carolina Certification #: 381
South Carolina Certification #: 98011001
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 57
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92603521
MUSA 6760
Lab ID Sample ID Matrix Date Collected Date Received
92603521001 SB-1 (2-4')Solid 05/02/22 12:40 05/06/22 12:30
92603521002 SB-2 (4-6')Solid 05/02/22 13:50 05/06/22 12:30
92603521003 SB-3 (4-6')Solid 05/02/22 15:40 05/06/22 12:30
92603521004 SB-4 (4-6')Solid 05/02/22 12:15 05/06/22 12:30
92603521005 SB-5 (4-6')Solid 05/02/22 11:35 05/06/22 12:30
92603521006 SB-6 (4-6')Solid 05/02/22 10:00 05/06/22 12:30
92603521007 SB-1 Water 05/02/22 10:00 05/06/22 12:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 57
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92603521
MUSA 6760
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92603521001 SB-1 (2-4')EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92603521002 SB-2 (4-6')EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92603521003 SB-3 (4-6')EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92603521004 SB-4 (4-6')EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92603521005 SB-5 (4-6')EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92603521006 SB-6 (4-6')EPA 8015C 2 PASI-CHH
EPA 8015C 2 PASI-CMAD
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
92603521007 SB-1 EPA 504.1 3 PASI-CAP2
MADEP EPH 7 PASI-CBAJ
MADEP VPH 5 PASI-CMAD
EPA 6020B 1 PASI-GACW1
EPA 625.1 66 PASI-CPKS
SM 6200B 63 PASI-CSAS
PASI-C = Pace Analytical Services - Charlotte
PASI-GA = Pace Analytical Services - Peachtree Corners, GA
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-1 (2-4')Lab ID: 92603521001 Collected: 05/02/22 12:40 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 05/13/22 20:3605/13/22 05:126.0 4.2 1
Surrogates
n-Pentacosane (S)88 %05/13/22 20:36 629-99-205/13/22 05:1210-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)8.0J mg/kg 05/13/22 05:0605/12/22 15:5912.9 3.6 1
Surrogates
4-Bromofluorobenzene (S)82 %05/13/22 05:06 460-00-405/12/22 15:5966-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/10/22 09:24 67-64-105/09/22 20:31217 69.7 1
Benzene 61.4 ug/kg 05/10/22 09:24 71-43-205/09/22 20:3110.8 4.3 1
Bromobenzene ND ug/kg 05/10/22 09:24 108-86-105/09/22 20:3110.8 3.5 1
Bromochloromethane ND ug/kg 05/10/22 09:24 74-97-505/09/22 20:3110.8 3.2 1
Bromodichloromethane ND ug/kg 05/10/22 09:24 75-27-405/09/22 20:3110.8 4.2 1
Bromoform ND ug/kg 05/10/22 09:24 75-25-205/09/22 20:3110.8 3.8 1
Bromomethane ND ug/kg 05/10/22 09:24 74-83-9 IK05/09/22 20:3121.7 17.1 1
2-Butanone (MEK)ND ug/kg 05/10/22 09:24 78-93-305/09/22 20:31217 52.1 1
n-Butylbenzene ND ug/kg 05/10/22 09:24 104-51-805/09/22 20:3110.8 5.1 1
sec-Butylbenzene ND ug/kg 05/10/22 09:24 135-98-805/09/22 20:3110.8 4.8 1
tert-Butylbenzene ND ug/kg 05/10/22 09:24 98-06-605/09/22 20:3110.8 3.9 1
Carbon tetrachloride ND ug/kg 05/10/22 09:24 56-23-505/09/22 20:3110.8 4.1 1
Chlorobenzene ND ug/kg 05/10/22 09:24 108-90-705/09/22 20:3110.8 2.1 1
Chloroethane ND ug/kg 05/10/22 09:24 75-00-305/09/22 20:3121.7 8.4 1
Chloroform ND ug/kg 05/10/22 09:24 67-66-305/09/22 20:3110.8 6.6 1
Chloromethane ND ug/kg 05/10/22 09:24 74-87-305/09/22 20:3121.7 9.1 1
2-Chlorotoluene ND ug/kg 05/10/22 09:24 95-49-805/09/22 20:3110.8 3.8 1
4-Chlorotoluene ND ug/kg 05/10/22 09:24 106-43-405/09/22 20:3110.8 1.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/10/22 09:24 96-12-805/09/22 20:3110.8 4.2 1
Dibromochloromethane ND ug/kg 05/10/22 09:24 124-48-105/09/22 20:3110.8 6.1 1
1,2-Dibromoethane (EDB)ND ug/kg 05/10/22 09:24 106-93-405/09/22 20:3110.8 4.8 1
Dibromomethane ND ug/kg 05/10/22 09:24 74-95-305/09/22 20:3110.8 2.3 1
1,2-Dichlorobenzene ND ug/kg 05/10/22 09:24 95-50-105/09/22 20:3110.8 3.9 1
1,3-Dichlorobenzene ND ug/kg 05/10/22 09:24 541-73-105/09/22 20:3110.8 3.4 1
1,4-Dichlorobenzene ND ug/kg 05/10/22 09:24 106-46-705/09/22 20:3110.8 2.8 1
Dichlorodifluoromethane ND ug/kg 05/10/22 09:24 75-71-805/09/22 20:3121.7 4.7 1
1,1-Dichloroethane ND ug/kg 05/10/22 09:24 75-34-305/09/22 20:3110.8 4.5 1
1,2-Dichloroethane ND ug/kg 05/10/22 09:24 107-06-205/09/22 20:3110.8 7.2 1
1,1-Dichloroethene ND ug/kg 05/10/22 09:24 75-35-405/09/22 20:3110.8 4.5 1
cis-1,2-Dichloroethene ND ug/kg 05/10/22 09:24 156-59-205/09/22 20:3110.8 3.7 1
trans-1,2-Dichloroethene ND ug/kg 05/10/22 09:24 156-60-505/09/22 20:3110.8 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-1 (2-4')Lab ID: 92603521001 Collected: 05/02/22 12:40 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 05/10/22 09:24 78-87-505/09/22 20:3110.8 3.3 1
1,3-Dichloropropane ND ug/kg 05/10/22 09:24 142-28-905/09/22 20:3110.8 3.4 1
2,2-Dichloropropane ND ug/kg 05/10/22 09:24 594-20-705/09/22 20:3110.8 3.5 1
1,1-Dichloropropene ND ug/kg 05/10/22 09:24 563-58-605/09/22 20:3110.8 5.2 1
cis-1,3-Dichloropropene ND ug/kg 05/10/22 09:24 10061-01-505/09/22 20:3110.8 3.0 1
trans-1,3-Dichloropropene ND ug/kg 05/10/22 09:24 10061-02-605/09/22 20:3110.8 3.7 1
Diisopropyl ether ND ug/kg 05/10/22 09:24 108-20-305/09/22 20:3110.8 2.9 1
Ethylbenzene 39.2 ug/kg 05/10/22 09:24 100-41-405/09/22 20:3110.8 5.1 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/22 09:24 87-68-305/09/22 20:3121.7 17.8 1
2-Hexanone ND ug/kg 05/10/22 09:24 591-78-605/09/22 20:31108 10.5 1
Isopropylbenzene (Cumene)ND ug/kg 05/10/22 09:24 98-82-805/09/22 20:3110.8 3.7 1
p-Isopropyltoluene ND ug/kg 05/10/22 09:24 99-87-605/09/22 20:3110.8 5.3 1
Methylene Chloride ND ug/kg 05/10/22 09:24 75-09-205/09/22 20:3143.4 29.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/10/22 09:24 108-10-105/09/22 20:31108 10.5 1
Methyl-tert-butyl ether ND ug/kg 05/10/22 09:24 1634-04-405/09/22 20:3110.8 4.1 1
Naphthalene ND ug/kg 05/10/22 09:24 91-20-305/09/22 20:3110.8 5.7 1
n-Propylbenzene 11.2 ug/kg 05/10/22 09:24 103-65-105/09/22 20:3110.8 3.9 1
Styrene ND ug/kg 05/10/22 09:24 100-42-505/09/22 20:3110.8 2.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/10/22 09:24 630-20-605/09/22 20:3110.8 4.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/10/22 09:24 79-34-505/09/22 20:3110.8 2.9 1
Tetrachloroethene ND ug/kg 05/10/22 09:24 127-18-405/09/22 20:3110.8 3.4 1
Toluene 165 ug/kg 05/10/22 09:24 108-88-305/09/22 20:3110.8 3.1 1
1,2,3-Trichlorobenzene ND ug/kg 05/10/22 09:24 87-61-605/09/22 20:3110.8 8.8 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/22 09:24 120-82-105/09/22 20:3110.8 9.1 1
1,1,1-Trichloroethane ND ug/kg 05/10/22 09:24 71-55-605/09/22 20:3110.8 5.6 1
1,1,2-Trichloroethane ND ug/kg 05/10/22 09:24 79-00-505/09/22 20:3110.8 3.6 1
Trichloroethene ND ug/kg 05/10/22 09:24 79-01-605/09/22 20:3110.8 2.8 1
Trichlorofluoromethane ND ug/kg 05/10/22 09:24 75-69-405/09/22 20:3110.8 6.0 1
1,2,3-Trichloropropane ND ug/kg 05/10/22 09:24 96-18-405/09/22 20:3110.8 5.5 1
1,2,4-Trimethylbenzene 17.5 ug/kg 05/10/22 09:24 95-63-605/09/22 20:3110.8 3.0 1
1,3,5-Trimethylbenzene ND ug/kg 05/10/22 09:24 108-67-805/09/22 20:3110.8 3.6 1
Vinyl acetate ND ug/kg 05/10/22 09:24 108-05-405/09/22 20:31108 7.9 1
Vinyl chloride ND ug/kg 05/10/22 09:24 75-01-405/09/22 20:3121.7 5.5 1
Xylene (Total)156 ug/kg 05/10/22 09:24 1330-20-705/09/22 20:3121.7 6.2 1
m&p-Xylene 114 ug/kg 05/10/22 09:24 179601-23-105/09/22 20:3121.7 7.4 1
o-Xylene 41.3 ug/kg 05/10/22 09:24 95-47-605/09/22 20:3110.8 4.8 1
Surrogates
Toluene-d8 (S)97 %05/10/22 09:24 2037-26-505/09/22 20:3170-130 1
4-Bromofluorobenzene (S)101 %05/10/22 09:24 460-00-405/09/22 20:3169-134 1
1,2-Dichloroethane-d4 (S)96 %05/10/22 09:24 17060-07-005/09/22 20:3170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 16.9 %05/10/22 14:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-2 (4-6')Lab ID: 92603521002 Collected: 05/02/22 13:50 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 05/13/22 20:5205/13/22 05:126.1 4.4 1
Surrogates
n-Pentacosane (S)87 %05/13/22 20:52 629-99-205/13/22 05:1210-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 05/13/22 05:3405/12/22 15:5912.8 3.6 1
Surrogates
4-Bromofluorobenzene (S)81 %05/13/22 05:34 460-00-405/12/22 15:5966-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/10/22 09:43 67-64-105/09/22 20:31206 66.2 1
Benzene ND ug/kg 05/10/22 09:43 71-43-205/09/22 20:3110.3 4.1 1
Bromobenzene ND ug/kg 05/10/22 09:43 108-86-105/09/22 20:3110.3 3.4 1
Bromochloromethane ND ug/kg 05/10/22 09:43 74-97-505/09/22 20:3110.3 3.1 1
Bromodichloromethane ND ug/kg 05/10/22 09:43 75-27-405/09/22 20:3110.3 4.0 1
Bromoform ND ug/kg 05/10/22 09:43 75-25-205/09/22 20:3110.3 3.6 1
Bromomethane ND ug/kg 05/10/22 09:43 74-83-9 IK05/09/22 20:3120.6 16.3 1
2-Butanone (MEK)ND ug/kg 05/10/22 09:43 78-93-305/09/22 20:31206 49.5 1
n-Butylbenzene ND ug/kg 05/10/22 09:43 104-51-805/09/22 20:3110.3 4.9 1
sec-Butylbenzene ND ug/kg 05/10/22 09:43 135-98-805/09/22 20:3110.3 4.5 1
tert-Butylbenzene ND ug/kg 05/10/22 09:43 98-06-605/09/22 20:3110.3 3.7 1
Carbon tetrachloride ND ug/kg 05/10/22 09:43 56-23-505/09/22 20:3110.3 3.9 1
Chlorobenzene 5.7J ug/kg 05/10/22 09:43 108-90-705/09/22 20:3110.3 2.0 1
Chloroethane ND ug/kg 05/10/22 09:43 75-00-305/09/22 20:3120.6 8.0 1
Chloroform ND ug/kg 05/10/22 09:43 67-66-305/09/22 20:3110.3 6.3 1
Chloromethane ND ug/kg 05/10/22 09:43 74-87-305/09/22 20:3120.6 8.7 1
2-Chlorotoluene ND ug/kg 05/10/22 09:43 95-49-805/09/22 20:3110.3 3.7 1
4-Chlorotoluene ND ug/kg 05/10/22 09:43 106-43-405/09/22 20:3110.3 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/10/22 09:43 96-12-805/09/22 20:3110.3 4.0 1
Dibromochloromethane ND ug/kg 05/10/22 09:43 124-48-105/09/22 20:3110.3 5.8 1
1,2-Dibromoethane (EDB)ND ug/kg 05/10/22 09:43 106-93-405/09/22 20:3110.3 4.5 1
Dibromomethane ND ug/kg 05/10/22 09:43 74-95-305/09/22 20:3110.3 2.2 1
1,2-Dichlorobenzene ND ug/kg 05/10/22 09:43 95-50-105/09/22 20:3110.3 3.7 1
1,3-Dichlorobenzene ND ug/kg 05/10/22 09:43 541-73-105/09/22 20:3110.3 3.2 1
1,4-Dichlorobenzene ND ug/kg 05/10/22 09:43 106-46-705/09/22 20:3110.3 2.7 1
Dichlorodifluoromethane ND ug/kg 05/10/22 09:43 75-71-805/09/22 20:3120.6 4.5 1
1,1-Dichloroethane ND ug/kg 05/10/22 09:43 75-34-305/09/22 20:3110.3 4.2 1
1,2-Dichloroethane ND ug/kg 05/10/22 09:43 107-06-205/09/22 20:3110.3 6.8 1
1,1-Dichloroethene ND ug/kg 05/10/22 09:43 75-35-405/09/22 20:3110.3 4.2 1
cis-1,2-Dichloroethene ND ug/kg 05/10/22 09:43 156-59-205/09/22 20:3110.3 3.5 1
trans-1,2-Dichloroethene ND ug/kg 05/10/22 09:43 156-60-505/09/22 20:3110.3 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-2 (4-6')Lab ID: 92603521002 Collected: 05/02/22 13:50 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 05/10/22 09:43 78-87-505/09/22 20:3110.3 3.1 1
1,3-Dichloropropane ND ug/kg 05/10/22 09:43 142-28-905/09/22 20:3110.3 3.2 1
2,2-Dichloropropane ND ug/kg 05/10/22 09:43 594-20-705/09/22 20:3110.3 3.4 1
1,1-Dichloropropene ND ug/kg 05/10/22 09:43 563-58-605/09/22 20:3110.3 4.9 1
cis-1,3-Dichloropropene ND ug/kg 05/10/22 09:43 10061-01-505/09/22 20:3110.3 2.8 1
trans-1,3-Dichloropropene ND ug/kg 05/10/22 09:43 10061-02-605/09/22 20:3110.3 3.5 1
Diisopropyl ether ND ug/kg 05/10/22 09:43 108-20-305/09/22 20:3110.3 2.8 1
Ethylbenzene ND ug/kg 05/10/22 09:43 100-41-405/09/22 20:3110.3 4.8 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/22 09:43 87-68-305/09/22 20:3120.6 16.9 1
2-Hexanone ND ug/kg 05/10/22 09:43 591-78-605/09/22 20:31103 9.9 1
Isopropylbenzene (Cumene)ND ug/kg 05/10/22 09:43 98-82-805/09/22 20:3110.3 3.5 1
p-Isopropyltoluene ND ug/kg 05/10/22 09:43 99-87-605/09/22 20:3110.3 5.1 1
Methylene Chloride ND ug/kg 05/10/22 09:43 75-09-205/09/22 20:3141.2 28.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/10/22 09:43 108-10-105/09/22 20:31103 9.9 1
Methyl-tert-butyl ether ND ug/kg 05/10/22 09:43 1634-04-405/09/22 20:3110.3 3.9 1
Naphthalene ND ug/kg 05/10/22 09:43 91-20-305/09/22 20:3110.3 5.4 1
n-Propylbenzene ND ug/kg 05/10/22 09:43 103-65-105/09/22 20:3110.3 3.7 1
Styrene ND ug/kg 05/10/22 09:43 100-42-505/09/22 20:3110.3 2.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/10/22 09:43 630-20-605/09/22 20:3110.3 4.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/10/22 09:43 79-34-505/09/22 20:3110.3 2.7 1
Tetrachloroethene ND ug/kg 05/10/22 09:43 127-18-405/09/22 20:3110.3 3.3 1
Toluene ND ug/kg 05/10/22 09:43 108-88-305/09/22 20:3110.3 2.9 1
1,2,3-Trichlorobenzene ND ug/kg 05/10/22 09:43 87-61-605/09/22 20:3110.3 8.3 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/22 09:43 120-82-105/09/22 20:3110.3 8.7 1
1,1,1-Trichloroethane ND ug/kg 05/10/22 09:43 71-55-605/09/22 20:3110.3 5.4 1
1,1,2-Trichloroethane ND ug/kg 05/10/22 09:43 79-00-505/09/22 20:3110.3 3.4 1
Trichloroethene ND ug/kg 05/10/22 09:43 79-01-605/09/22 20:3110.3 2.7 1
Trichlorofluoromethane ND ug/kg 05/10/22 09:43 75-69-405/09/22 20:3110.3 5.7 1
1,2,3-Trichloropropane ND ug/kg 05/10/22 09:43 96-18-405/09/22 20:3110.3 5.2 1
1,2,4-Trimethylbenzene ND ug/kg 05/10/22 09:43 95-63-605/09/22 20:3110.3 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 05/10/22 09:43 108-67-805/09/22 20:3110.3 3.5 1
Vinyl acetate ND ug/kg 05/10/22 09:43 108-05-405/09/22 20:31103 7.5 1
Vinyl chloride ND ug/kg 05/10/22 09:43 75-01-405/09/22 20:3120.6 5.2 1
Xylene (Total)10.6J ug/kg 05/10/22 09:43 1330-20-705/09/22 20:3120.6 5.9 1
m&p-Xylene ND ug/kg 05/10/22 09:43 179601-23-105/09/22 20:3120.6 7.1 1
o-Xylene 10.6 ug/kg 05/10/22 09:43 95-47-605/09/22 20:3110.3 4.6 1
Surrogates
Toluene-d8 (S)98 %05/10/22 09:43 2037-26-505/09/22 20:3170-130 1
4-Bromofluorobenzene (S)100 %05/10/22 09:43 460-00-405/09/22 20:3169-134 1
1,2-Dichloroethane-d4 (S)94 %05/10/22 09:43 17060-07-005/09/22 20:3170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.9 %05/10/22 14:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-3 (4-6')Lab ID: 92603521003 Collected: 05/02/22 15:40 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 05/13/22 21:0905/13/22 05:125.7 4.1 1
Surrogates
n-Pentacosane (S)85 %05/13/22 21:09 629-99-205/13/22 05:1210-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 05/13/22 06:0205/12/22 15:5911.2 3.1 1
Surrogates
4-Bromofluorobenzene (S)80 %05/13/22 06:02 460-00-405/12/22 15:5966-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/10/22 10:20 67-64-105/09/22 22:59206 66.0 1
Benzene ND ug/kg 05/10/22 10:20 71-43-205/09/22 22:5910.3 4.1 1
Bromobenzene ND ug/kg 05/10/22 10:20 108-86-105/09/22 22:5910.3 3.4 1
Bromochloromethane ND ug/kg 05/10/22 10:20 74-97-505/09/22 22:5910.3 3.0 1
Bromodichloromethane ND ug/kg 05/10/22 10:20 75-27-405/09/22 22:5910.3 4.0 1
Bromoform ND ug/kg 05/10/22 10:20 75-25-205/09/22 22:5910.3 3.6 1
Bromomethane ND ug/kg 05/10/22 10:20 74-83-9 IK05/09/22 22:5920.6 16.3 1
2-Butanone (MEK)ND ug/kg 05/10/22 10:20 78-93-305/09/22 22:59206 49.4 1
n-Butylbenzene ND ug/kg 05/10/22 10:20 104-51-805/09/22 22:5910.3 4.9 1
sec-Butylbenzene ND ug/kg 05/10/22 10:20 135-98-805/09/22 22:5910.3 4.5 1
tert-Butylbenzene ND ug/kg 05/10/22 10:20 98-06-605/09/22 22:5910.3 3.7 1
Carbon tetrachloride ND ug/kg 05/10/22 10:20 56-23-505/09/22 22:5910.3 3.8 1
Chlorobenzene 6.0J ug/kg 05/10/22 10:20 108-90-705/09/22 22:5910.3 2.0 1
Chloroethane ND ug/kg 05/10/22 10:20 75-00-305/09/22 22:5920.6 7.9 1
Chloroform ND ug/kg 05/10/22 10:20 67-66-305/09/22 22:5910.3 6.3 1
Chloromethane ND ug/kg 05/10/22 10:20 74-87-305/09/22 22:5920.6 8.6 1
2-Chlorotoluene ND ug/kg 05/10/22 10:20 95-49-805/09/22 22:5910.3 3.6 1
4-Chlorotoluene ND ug/kg 05/10/22 10:20 106-43-405/09/22 22:5910.3 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/10/22 10:20 96-12-805/09/22 22:5910.3 4.0 1
Dibromochloromethane ND ug/kg 05/10/22 10:20 124-48-105/09/22 22:5910.3 5.8 1
1,2-Dibromoethane (EDB)ND ug/kg 05/10/22 10:20 106-93-405/09/22 22:5910.3 4.5 1
Dibromomethane ND ug/kg 05/10/22 10:20 74-95-305/09/22 22:5910.3 2.2 1
1,2-Dichlorobenzene ND ug/kg 05/10/22 10:20 95-50-105/09/22 22:5910.3 3.7 1
1,3-Dichlorobenzene ND ug/kg 05/10/22 10:20 541-73-105/09/22 22:5910.3 3.2 1
1,4-Dichlorobenzene ND ug/kg 05/10/22 10:20 106-46-705/09/22 22:5910.3 2.7 1
Dichlorodifluoromethane ND ug/kg 05/10/22 10:20 75-71-805/09/22 22:5920.6 4.5 1
1,1-Dichloroethane ND ug/kg 05/10/22 10:20 75-34-305/09/22 22:5910.3 4.2 1
1,2-Dichloroethane ND ug/kg 05/10/22 10:20 107-06-205/09/22 22:5910.3 6.8 1
1,1-Dichloroethene ND ug/kg 05/10/22 10:20 75-35-405/09/22 22:5910.3 4.2 1
cis-1,2-Dichloroethene ND ug/kg 05/10/22 10:20 156-59-205/09/22 22:5910.3 3.5 1
trans-1,2-Dichloroethene ND ug/kg 05/10/22 10:20 156-60-505/09/22 22:5910.3 3.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-3 (4-6')Lab ID: 92603521003 Collected: 05/02/22 15:40 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 05/10/22 10:20 78-87-505/09/22 22:5910.3 3.1 1
1,3-Dichloropropane ND ug/kg 05/10/22 10:20 142-28-905/09/22 22:5910.3 3.2 1
2,2-Dichloropropane ND ug/kg 05/10/22 10:20 594-20-705/09/22 22:5910.3 3.4 1
1,1-Dichloropropene ND ug/kg 05/10/22 10:20 563-58-605/09/22 22:5910.3 4.9 1
cis-1,3-Dichloropropene ND ug/kg 05/10/22 10:20 10061-01-505/09/22 22:5910.3 2.8 1
trans-1,3-Dichloropropene ND ug/kg 05/10/22 10:20 10061-02-605/09/22 22:5910.3 3.5 1
Diisopropyl ether ND ug/kg 05/10/22 10:20 108-20-305/09/22 22:5910.3 2.8 1
Ethylbenzene 6.4J ug/kg 05/10/22 10:20 100-41-405/09/22 22:5910.3 4.8 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/22 10:20 87-68-305/09/22 22:5920.6 16.8 1
2-Hexanone ND ug/kg 05/10/22 10:20 591-78-605/09/22 22:59103 9.9 1
Isopropylbenzene (Cumene)ND ug/kg 05/10/22 10:20 98-82-805/09/22 22:5910.3 3.5 1
p-Isopropyltoluene ND ug/kg 05/10/22 10:20 99-87-605/09/22 22:5910.3 5.1 1
Methylene Chloride ND ug/kg 05/10/22 10:20 75-09-205/09/22 22:5941.2 28.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/10/22 10:20 108-10-105/09/22 22:59103 9.9 1
Methyl-tert-butyl ether ND ug/kg 05/10/22 10:20 1634-04-405/09/22 22:5910.3 3.8 1
Naphthalene ND ug/kg 05/10/22 10:20 91-20-305/09/22 22:5910.3 5.4 1
n-Propylbenzene ND ug/kg 05/10/22 10:20 103-65-105/09/22 22:5910.3 3.7 1
Styrene ND ug/kg 05/10/22 10:20 100-42-505/09/22 22:5910.3 2.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/10/22 10:20 630-20-605/09/22 22:5910.3 4.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/10/22 10:20 79-34-505/09/22 22:5910.3 2.7 1
Tetrachloroethene ND ug/kg 05/10/22 10:20 127-18-405/09/22 22:5910.3 3.3 1
Toluene ND ug/kg 05/10/22 10:20 108-88-305/09/22 22:5910.3 2.9 1
1,2,3-Trichlorobenzene ND ug/kg 05/10/22 10:20 87-61-605/09/22 22:5910.3 8.3 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/22 10:20 120-82-105/09/22 22:5910.3 8.6 1
1,1,1-Trichloroethane ND ug/kg 05/10/22 10:20 71-55-605/09/22 22:5910.3 5.3 1
1,1,2-Trichloroethane ND ug/kg 05/10/22 10:20 79-00-505/09/22 22:5910.3 3.4 1
Trichloroethene ND ug/kg 05/10/22 10:20 79-01-605/09/22 22:5910.3 2.7 1
Trichlorofluoromethane ND ug/kg 05/10/22 10:20 75-69-405/09/22 22:5910.3 5.7 1
1,2,3-Trichloropropane ND ug/kg 05/10/22 10:20 96-18-405/09/22 22:5910.3 5.2 1
1,2,4-Trimethylbenzene ND ug/kg 05/10/22 10:20 95-63-605/09/22 22:5910.3 2.8 1
1,3,5-Trimethylbenzene ND ug/kg 05/10/22 10:20 108-67-805/09/22 22:5910.3 3.5 1
Vinyl acetate ND ug/kg 05/10/22 10:20 108-05-405/09/22 22:59103 7.5 1
Vinyl chloride ND ug/kg 05/10/22 10:20 75-01-405/09/22 22:5920.6 5.2 1
Xylene (Total)9.9J ug/kg 05/10/22 10:20 1330-20-705/09/22 22:5920.6 5.9 1
m&p-Xylene ND ug/kg 05/10/22 10:20 179601-23-105/09/22 22:5920.6 7.0 1
o-Xylene 9.9J ug/kg 05/10/22 10:20 95-47-605/09/22 22:5910.3 4.5 1
Surrogates
Toluene-d8 (S)98 %05/10/22 10:20 2037-26-505/09/22 22:5970-130 1
4-Bromofluorobenzene (S)100 %05/10/22 10:20 460-00-405/09/22 22:5969-134 1
1,2-Dichloroethane-d4 (S)95 %05/10/22 10:20 17060-07-005/09/22 22:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.1 %05/10/22 14:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-4 (4-6')Lab ID: 92603521004 Collected: 05/02/22 12:15 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 05/13/22 19:1305/13/22 11:385.9 4.2 1
Surrogates
n-Pentacosane (S)87 %05/13/22 19:13 629-99-205/13/22 11:3810-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 05/13/22 06:3105/12/22 15:5911.3 3.1 1
Surrogates
4-Bromofluorobenzene (S)79 %05/13/22 06:31 460-00-405/12/22 15:5966-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/10/22 10:58 67-64-105/09/22 22:59181 58.0 1
Benzene ND ug/kg 05/10/22 10:58 71-43-205/09/22 22:599.0 3.6 1
Bromobenzene ND ug/kg 05/10/22 10:58 108-86-105/09/22 22:599.0 2.9 1
Bromochloromethane ND ug/kg 05/10/22 10:58 74-97-505/09/22 22:599.0 2.7 1
Bromodichloromethane ND ug/kg 05/10/22 10:58 75-27-405/09/22 22:599.0 3.5 1
Bromoform ND ug/kg 05/10/22 10:58 75-25-205/09/22 22:599.0 3.2 1
Bromomethane ND ug/kg 05/10/22 10:58 74-83-9 IK05/09/22 22:5918.1 14.3 1
2-Butanone (MEK)ND ug/kg 05/10/22 10:58 78-93-305/09/22 22:59181 43.4 1
n-Butylbenzene ND ug/kg 05/10/22 10:58 104-51-805/09/22 22:599.0 4.3 1
sec-Butylbenzene ND ug/kg 05/10/22 10:58 135-98-805/09/22 22:599.0 4.0 1
tert-Butylbenzene ND ug/kg 05/10/22 10:58 98-06-605/09/22 22:599.0 3.2 1
Carbon tetrachloride ND ug/kg 05/10/22 10:58 56-23-505/09/22 22:599.0 3.4 1
Chlorobenzene 5.2J ug/kg 05/10/22 10:58 108-90-705/09/22 22:599.0 1.7 1
Chloroethane ND ug/kg 05/10/22 10:58 75-00-305/09/22 22:5918.1 7.0 1
Chloroform ND ug/kg 05/10/22 10:58 67-66-305/09/22 22:599.0 5.5 1
Chloromethane ND ug/kg 05/10/22 10:58 74-87-305/09/22 22:5918.1 7.6 1
2-Chlorotoluene ND ug/kg 05/10/22 10:58 95-49-805/09/22 22:599.0 3.2 1
4-Chlorotoluene ND ug/kg 05/10/22 10:58 106-43-405/09/22 22:599.0 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/10/22 10:58 96-12-805/09/22 22:599.0 3.5 1
Dibromochloromethane ND ug/kg 05/10/22 10:58 124-48-105/09/22 22:599.0 5.1 1
1,2-Dibromoethane (EDB)ND ug/kg 05/10/22 10:58 106-93-405/09/22 22:599.0 4.0 1
Dibromomethane ND ug/kg 05/10/22 10:58 74-95-305/09/22 22:599.0 1.9 1
1,2-Dichlorobenzene ND ug/kg 05/10/22 10:58 95-50-105/09/22 22:599.0 3.3 1
1,3-Dichlorobenzene ND ug/kg 05/10/22 10:58 541-73-105/09/22 22:599.0 2.8 1
1,4-Dichlorobenzene ND ug/kg 05/10/22 10:58 106-46-705/09/22 22:599.0 2.3 1
Dichlorodifluoromethane ND ug/kg 05/10/22 10:58 75-71-805/09/22 22:5918.1 3.9 1
1,1-Dichloroethane ND ug/kg 05/10/22 10:58 75-34-305/09/22 22:599.0 3.7 1
1,2-Dichloroethane ND ug/kg 05/10/22 10:58 107-06-205/09/22 22:599.0 6.0 1
1,1-Dichloroethene ND ug/kg 05/10/22 10:58 75-35-405/09/22 22:599.0 3.7 1
cis-1,2-Dichloroethene ND ug/kg 05/10/22 10:58 156-59-205/09/22 22:599.0 3.1 1
trans-1,2-Dichloroethene ND ug/kg 05/10/22 10:58 156-60-505/09/22 22:599.0 3.2 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-4 (4-6')Lab ID: 92603521004 Collected: 05/02/22 12:15 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 05/10/22 10:58 78-87-505/09/22 22:599.0 2.7 1
1,3-Dichloropropane ND ug/kg 05/10/22 10:58 142-28-905/09/22 22:599.0 2.8 1
2,2-Dichloropropane ND ug/kg 05/10/22 10:58 594-20-705/09/22 22:599.0 2.9 1
1,1-Dichloropropene ND ug/kg 05/10/22 10:58 563-58-605/09/22 22:599.0 4.3 1
cis-1,3-Dichloropropene ND ug/kg 05/10/22 10:58 10061-01-505/09/22 22:599.0 2.5 1
trans-1,3-Dichloropropene ND ug/kg 05/10/22 10:58 10061-02-605/09/22 22:599.0 3.1 1
Diisopropyl ether ND ug/kg 05/10/22 10:58 108-20-305/09/22 22:599.0 2.4 1
Ethylbenzene ND ug/kg 05/10/22 10:58 100-41-405/09/22 22:599.0 4.2 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/22 10:58 87-68-305/09/22 22:5918.1 14.8 1
2-Hexanone ND ug/kg 05/10/22 10:58 591-78-605/09/22 22:5990.4 8.7 1
Isopropylbenzene (Cumene)ND ug/kg 05/10/22 10:58 98-82-805/09/22 22:599.0 3.1 1
p-Isopropyltoluene ND ug/kg 05/10/22 10:58 99-87-605/09/22 22:599.0 4.4 1
Methylene Chloride ND ug/kg 05/10/22 10:58 75-09-205/09/22 22:5936.1 24.8 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/10/22 10:58 108-10-105/09/22 22:5990.4 8.7 1
Methyl-tert-butyl ether ND ug/kg 05/10/22 10:58 1634-04-405/09/22 22:599.0 3.4 1
Naphthalene ND ug/kg 05/10/22 10:58 91-20-305/09/22 22:599.0 4.8 1
n-Propylbenzene ND ug/kg 05/10/22 10:58 103-65-105/09/22 22:599.0 3.2 1
Styrene ND ug/kg 05/10/22 10:58 100-42-505/09/22 22:599.0 2.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/10/22 10:58 630-20-605/09/22 22:599.0 3.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/10/22 10:58 79-34-505/09/22 22:599.0 2.4 1
Tetrachloroethene ND ug/kg 05/10/22 10:58 127-18-405/09/22 22:599.0 2.9 1
Toluene ND ug/kg 05/10/22 10:58 108-88-305/09/22 22:599.0 2.6 1
1,2,3-Trichlorobenzene ND ug/kg 05/10/22 10:58 87-61-605/09/22 22:599.0 7.3 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/22 10:58 120-82-105/09/22 22:599.0 7.6 1
1,1,1-Trichloroethane ND ug/kg 05/10/22 10:58 71-55-605/09/22 22:599.0 4.7 1
1,1,2-Trichloroethane ND ug/kg 05/10/22 10:58 79-00-505/09/22 22:599.0 3.0 1
Trichloroethene ND ug/kg 05/10/22 10:58 79-01-605/09/22 22:599.0 2.3 1
Trichlorofluoromethane ND ug/kg 05/10/22 10:58 75-69-405/09/22 22:599.0 5.0 1
1,2,3-Trichloropropane ND ug/kg 05/10/22 10:58 96-18-405/09/22 22:599.0 4.6 1
1,2,4-Trimethylbenzene ND ug/kg 05/10/22 10:58 95-63-605/09/22 22:599.0 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 05/10/22 10:58 108-67-805/09/22 22:599.0 3.0 1
Vinyl acetate ND ug/kg 05/10/22 10:58 108-05-405/09/22 22:5990.4 6.6 1
Vinyl chloride ND ug/kg 05/10/22 10:58 75-01-405/09/22 22:5918.1 4.6 1
Xylene (Total)8.9J ug/kg 05/10/22 10:58 1330-20-705/09/22 22:5918.1 5.2 1
m&p-Xylene ND ug/kg 05/10/22 10:58 179601-23-105/09/22 22:5918.1 6.2 1
o-Xylene 8.9J ug/kg 05/10/22 10:58 95-47-605/09/22 22:599.0 4.0 1
Surrogates
Toluene-d8 (S)98 %05/10/22 10:58 2037-26-505/09/22 22:5970-130 1
4-Bromofluorobenzene (S)100 %05/10/22 10:58 460-00-405/09/22 22:5969-134 1
1,2-Dichloroethane-d4 (S)98 %05/10/22 10:58 17060-07-005/09/22 22:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.4 %05/10/22 14:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-5 (4-6')Lab ID: 92603521005 Collected: 05/02/22 11:35 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 05/13/22 19:3005/13/22 11:385.6 4.0 1
Surrogates
n-Pentacosane (S)84 %05/13/22 19:30 629-99-205/13/22 11:3810-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 05/13/22 06:5905/12/22 15:5911.3 3.1 1
Surrogates
4-Bromofluorobenzene (S)80 %05/13/22 06:59 460-00-405/12/22 15:5966-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/10/22 11:16 67-64-105/09/22 22:59189 60.8 1
Benzene ND ug/kg 05/10/22 11:16 71-43-205/09/22 22:599.5 3.8 1
Bromobenzene ND ug/kg 05/10/22 11:16 108-86-105/09/22 22:599.5 3.1 1
Bromochloromethane ND ug/kg 05/10/22 11:16 74-97-505/09/22 22:599.5 2.8 1
Bromodichloromethane ND ug/kg 05/10/22 11:16 75-27-405/09/22 22:599.5 3.7 1
Bromoform ND ug/kg 05/10/22 11:16 75-25-205/09/22 22:599.5 3.3 1
Bromomethane ND ug/kg 05/10/22 11:16 74-83-9 IK05/09/22 22:5918.9 15.0 1
2-Butanone (MEK)ND ug/kg 05/10/22 11:16 78-93-305/09/22 22:59189 45.4 1
n-Butylbenzene ND ug/kg 05/10/22 11:16 104-51-805/09/22 22:599.5 4.5 1
sec-Butylbenzene ND ug/kg 05/10/22 11:16 135-98-805/09/22 22:599.5 4.2 1
tert-Butylbenzene ND ug/kg 05/10/22 11:16 98-06-605/09/22 22:599.5 3.4 1
Carbon tetrachloride ND ug/kg 05/10/22 11:16 56-23-505/09/22 22:599.5 3.5 1
Chlorobenzene 4.8J ug/kg 05/10/22 11:16 108-90-705/09/22 22:599.5 1.8 1
Chloroethane ND ug/kg 05/10/22 11:16 75-00-305/09/22 22:5918.9 7.3 1
Chloroform ND ug/kg 05/10/22 11:16 67-66-305/09/22 22:599.5 5.8 1
Chloromethane ND ug/kg 05/10/22 11:16 74-87-305/09/22 22:5918.9 7.9 1
2-Chlorotoluene ND ug/kg 05/10/22 11:16 95-49-805/09/22 22:599.5 3.4 1
4-Chlorotoluene ND ug/kg 05/10/22 11:16 106-43-405/09/22 22:599.5 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/10/22 11:16 96-12-805/09/22 22:599.5 3.7 1
Dibromochloromethane ND ug/kg 05/10/22 11:16 124-48-105/09/22 22:599.5 5.3 1
1,2-Dibromoethane (EDB)ND ug/kg 05/10/22 11:16 106-93-405/09/22 22:599.5 4.2 1
Dibromomethane ND ug/kg 05/10/22 11:16 74-95-305/09/22 22:599.5 2.0 1
1,2-Dichlorobenzene ND ug/kg 05/10/22 11:16 95-50-105/09/22 22:599.5 3.4 1
1,3-Dichlorobenzene ND ug/kg 05/10/22 11:16 541-73-105/09/22 22:599.5 2.9 1
1,4-Dichlorobenzene ND ug/kg 05/10/22 11:16 106-46-705/09/22 22:599.5 2.5 1
Dichlorodifluoromethane ND ug/kg 05/10/22 11:16 75-71-805/09/22 22:5918.9 4.1 1
1,1-Dichloroethane ND ug/kg 05/10/22 11:16 75-34-305/09/22 22:599.5 3.9 1
1,2-Dichloroethane ND ug/kg 05/10/22 11:16 107-06-205/09/22 22:599.5 6.3 1
1,1-Dichloroethene ND ug/kg 05/10/22 11:16 75-35-405/09/22 22:599.5 3.9 1
cis-1,2-Dichloroethene ND ug/kg 05/10/22 11:16 156-59-205/09/22 22:599.5 3.2 1
trans-1,2-Dichloroethene ND ug/kg 05/10/22 11:16 156-60-505/09/22 22:599.5 3.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-5 (4-6')Lab ID: 92603521005 Collected: 05/02/22 11:35 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 05/10/22 11:16 78-87-505/09/22 22:599.5 2.8 1
1,3-Dichloropropane ND ug/kg 05/10/22 11:16 142-28-905/09/22 22:599.5 3.0 1
2,2-Dichloropropane ND ug/kg 05/10/22 11:16 594-20-705/09/22 22:599.5 3.1 1
1,1-Dichloropropene ND ug/kg 05/10/22 11:16 563-58-605/09/22 22:599.5 4.5 1
cis-1,3-Dichloropropene ND ug/kg 05/10/22 11:16 10061-01-505/09/22 22:599.5 2.6 1
trans-1,3-Dichloropropene ND ug/kg 05/10/22 11:16 10061-02-605/09/22 22:599.5 3.3 1
Diisopropyl ether ND ug/kg 05/10/22 11:16 108-20-305/09/22 22:599.5 2.6 1
Ethylbenzene ND ug/kg 05/10/22 11:16 100-41-405/09/22 22:599.5 4.4 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/22 11:16 87-68-305/09/22 22:5918.9 15.5 1
2-Hexanone ND ug/kg 05/10/22 11:16 591-78-605/09/22 22:5994.6 9.1 1
Isopropylbenzene (Cumene)ND ug/kg 05/10/22 11:16 98-82-805/09/22 22:599.5 3.2 1
p-Isopropyltoluene ND ug/kg 05/10/22 11:16 99-87-605/09/22 22:599.5 4.7 1
Methylene Chloride ND ug/kg 05/10/22 11:16 75-09-205/09/22 22:5937.9 25.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/10/22 11:16 108-10-105/09/22 22:5994.6 9.1 1
Methyl-tert-butyl ether ND ug/kg 05/10/22 11:16 1634-04-405/09/22 22:599.5 3.5 1
Naphthalene ND ug/kg 05/10/22 11:16 91-20-305/09/22 22:599.5 5.0 1
n-Propylbenzene ND ug/kg 05/10/22 11:16 103-65-105/09/22 22:599.5 3.4 1
Styrene ND ug/kg 05/10/22 11:16 100-42-505/09/22 22:599.5 2.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/10/22 11:16 630-20-605/09/22 22:599.5 3.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/10/22 11:16 79-34-505/09/22 22:599.5 2.5 1
Tetrachloroethene ND ug/kg 05/10/22 11:16 127-18-405/09/22 22:599.5 3.0 1
Toluene ND ug/kg 05/10/22 11:16 108-88-305/09/22 22:599.5 2.7 1
1,2,3-Trichlorobenzene ND ug/kg 05/10/22 11:16 87-61-605/09/22 22:599.5 7.6 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/22 11:16 120-82-105/09/22 22:599.5 7.9 1
1,1,1-Trichloroethane ND ug/kg 05/10/22 11:16 71-55-605/09/22 22:599.5 4.9 1
1,1,2-Trichloroethane ND ug/kg 05/10/22 11:16 79-00-505/09/22 22:599.5 3.1 1
Trichloroethene ND ug/kg 05/10/22 11:16 79-01-605/09/22 22:599.5 2.4 1
Trichlorofluoromethane ND ug/kg 05/10/22 11:16 75-69-405/09/22 22:599.5 5.2 1
1,2,3-Trichloropropane ND ug/kg 05/10/22 11:16 96-18-405/09/22 22:599.5 4.8 1
1,2,4-Trimethylbenzene ND ug/kg 05/10/22 11:16 95-63-605/09/22 22:599.5 2.6 1
1,3,5-Trimethylbenzene ND ug/kg 05/10/22 11:16 108-67-805/09/22 22:599.5 3.2 1
Vinyl acetate ND ug/kg 05/10/22 11:16 108-05-405/09/22 22:5994.6 6.9 1
Vinyl chloride ND ug/kg 05/10/22 11:16 75-01-405/09/22 22:5918.9 4.8 1
Xylene (Total)9.0J ug/kg 05/10/22 11:16 1330-20-705/09/22 22:5918.9 5.4 1
m&p-Xylene ND ug/kg 05/10/22 11:16 179601-23-105/09/22 22:5918.9 6.5 1
o-Xylene 9.0J ug/kg 05/10/22 11:16 95-47-605/09/22 22:599.5 4.2 1
Surrogates
Toluene-d8 (S)99 %05/10/22 11:16 2037-26-505/09/22 22:5970-130 1
4-Bromofluorobenzene (S)100 %05/10/22 11:16 460-00-405/09/22 22:5969-134 1
1,2-Dichloroethane-d4 (S)97 %05/10/22 11:16 17060-07-005/09/22 22:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.8 %05/10/22 14:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-6 (4-6')Lab ID: 92603521006 Collected: 05/02/22 10:00 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8015C Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)ND mg/kg 05/13/22 19:3005/13/22 11:385.3 3.7 1
Surrogates
n-Pentacosane (S)72 %05/13/22 19:30 629-99-205/13/22 11:3810-130 1
Analytical Method: EPA 8015C Preparation Method: EPA 5030B
Pace Analytical Services - Charlotte
Gasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 05/13/22 07:2705/12/22 15:5910.6 2.9 1
Surrogates
4-Bromofluorobenzene (S)76 %05/13/22 07:27 460-00-405/12/22 15:5966-130 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/10/22 11:35 67-64-105/09/22 22:59169 54.2 1
Benzene ND ug/kg 05/10/22 11:35 71-43-205/09/22 22:598.4 3.4 1
Bromobenzene ND ug/kg 05/10/22 11:35 108-86-105/09/22 22:598.4 2.8 1
Bromochloromethane ND ug/kg 05/10/22 11:35 74-97-505/09/22 22:598.4 2.5 1
Bromodichloromethane ND ug/kg 05/10/22 11:35 75-27-405/09/22 22:598.4 3.3 1
Bromoform ND ug/kg 05/10/22 11:35 75-25-205/09/22 22:598.4 3.0 1
Bromomethane ND ug/kg 05/10/22 11:35 74-83-9 IK05/09/22 22:5916.9 13.3 1
2-Butanone (MEK)ND ug/kg 05/10/22 11:35 78-93-305/09/22 22:59169 40.5 1
n-Butylbenzene ND ug/kg 05/10/22 11:35 104-51-805/09/22 22:598.4 4.0 1
sec-Butylbenzene ND ug/kg 05/10/22 11:35 135-98-805/09/22 22:598.4 3.7 1
tert-Butylbenzene ND ug/kg 05/10/22 11:35 98-06-605/09/22 22:598.4 3.0 1
Carbon tetrachloride ND ug/kg 05/10/22 11:35 56-23-505/09/22 22:598.4 3.2 1
Chlorobenzene 4.4J ug/kg 05/10/22 11:35 108-90-705/09/22 22:598.4 1.6 1
Chloroethane ND ug/kg 05/10/22 11:35 75-00-305/09/22 22:5916.9 6.5 1
Chloroform ND ug/kg 05/10/22 11:35 67-66-305/09/22 22:598.4 5.1 1
Chloromethane ND ug/kg 05/10/22 11:35 74-87-305/09/22 22:5916.9 7.1 1
2-Chlorotoluene ND ug/kg 05/10/22 11:35 95-49-805/09/22 22:598.4 3.0 1
4-Chlorotoluene ND ug/kg 05/10/22 11:35 106-43-405/09/22 22:598.4 1.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/10/22 11:35 96-12-805/09/22 22:598.4 3.3 1
Dibromochloromethane ND ug/kg 05/10/22 11:35 124-48-105/09/22 22:598.4 4.7 1
1,2-Dibromoethane (EDB)ND ug/kg 05/10/22 11:35 106-93-405/09/22 22:598.4 3.7 1
Dibromomethane ND ug/kg 05/10/22 11:35 74-95-305/09/22 22:598.4 1.8 1
1,2-Dichlorobenzene ND ug/kg 05/10/22 11:35 95-50-105/09/22 22:598.4 3.0 1
1,3-Dichlorobenzene ND ug/kg 05/10/22 11:35 541-73-105/09/22 22:598.4 2.6 1
1,4-Dichlorobenzene ND ug/kg 05/10/22 11:35 106-46-705/09/22 22:598.4 2.2 1
Dichlorodifluoromethane ND ug/kg 05/10/22 11:35 75-71-805/09/22 22:5916.9 3.7 1
1,1-Dichloroethane ND ug/kg 05/10/22 11:35 75-34-305/09/22 22:598.4 3.5 1
1,2-Dichloroethane ND ug/kg 05/10/22 11:35 107-06-205/09/22 22:598.4 5.6 1
1,1-Dichloroethene ND ug/kg 05/10/22 11:35 75-35-405/09/22 22:598.4 3.5 1
cis-1,2-Dichloroethene ND ug/kg 05/10/22 11:35 156-59-205/09/22 22:598.4 2.9 1
trans-1,2-Dichloroethene ND ug/kg 05/10/22 11:35 156-60-505/09/22 22:598.4 3.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-6 (4-6')Lab ID: 92603521006 Collected: 05/02/22 10:00 Received: 05/06/22 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
1,2-Dichloropropane ND ug/kg 05/10/22 11:35 78-87-505/09/22 22:598.4 2.5 1
1,3-Dichloropropane ND ug/kg 05/10/22 11:35 142-28-905/09/22 22:598.4 2.6 1
2,2-Dichloropropane ND ug/kg 05/10/22 11:35 594-20-705/09/22 22:598.4 2.8 1
1,1-Dichloropropene ND ug/kg 05/10/22 11:35 563-58-605/09/22 22:598.4 4.0 1
cis-1,3-Dichloropropene ND ug/kg 05/10/22 11:35 10061-01-505/09/22 22:598.4 2.3 1
trans-1,3-Dichloropropene ND ug/kg 05/10/22 11:35 10061-02-605/09/22 22:598.4 2.9 1
Diisopropyl ether ND ug/kg 05/10/22 11:35 108-20-305/09/22 22:598.4 2.3 1
Ethylbenzene 5.4J ug/kg 05/10/22 11:35 100-41-405/09/22 22:598.4 3.9 1
Hexachloro-1,3-butadiene ND ug/kg 05/10/22 11:35 87-68-305/09/22 22:5916.9 13.8 1
2-Hexanone ND ug/kg 05/10/22 11:35 591-78-605/09/22 22:5984.4 8.1 1
Isopropylbenzene (Cumene)ND ug/kg 05/10/22 11:35 98-82-805/09/22 22:598.4 2.9 1
p-Isopropyltoluene ND ug/kg 05/10/22 11:35 99-87-605/09/22 22:598.4 4.2 1
Methylene Chloride ND ug/kg 05/10/22 11:35 75-09-205/09/22 22:5933.7 23.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/10/22 11:35 108-10-105/09/22 22:5984.4 8.1 1
Methyl-tert-butyl ether ND ug/kg 05/10/22 11:35 1634-04-405/09/22 22:598.4 3.2 1
Naphthalene ND ug/kg 05/10/22 11:35 91-20-305/09/22 22:598.4 4.4 1
n-Propylbenzene ND ug/kg 05/10/22 11:35 103-65-105/09/22 22:598.4 3.0 1
Styrene ND ug/kg 05/10/22 11:35 100-42-505/09/22 22:598.4 2.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/10/22 11:35 630-20-605/09/22 22:598.4 3.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/10/22 11:35 79-34-505/09/22 22:598.4 2.2 1
Tetrachloroethene ND ug/kg 05/10/22 11:35 127-18-405/09/22 22:598.4 2.7 1
Toluene 4.5J ug/kg 05/10/22 11:35 108-88-305/09/22 22:598.4 2.4 1
1,2,3-Trichlorobenzene ND ug/kg 05/10/22 11:35 87-61-605/09/22 22:598.4 6.8 1
1,2,4-Trichlorobenzene ND ug/kg 05/10/22 11:35 120-82-105/09/22 22:598.4 7.1 1
1,1,1-Trichloroethane ND ug/kg 05/10/22 11:35 71-55-605/09/22 22:598.4 4.4 1
1,1,2-Trichloroethane ND ug/kg 05/10/22 11:35 79-00-505/09/22 22:598.4 2.8 1
Trichloroethene ND ug/kg 05/10/22 11:35 79-01-605/09/22 22:598.4 2.2 1
Trichlorofluoromethane ND ug/kg 05/10/22 11:35 75-69-405/09/22 22:598.4 4.6 1
1,2,3-Trichloropropane ND ug/kg 05/10/22 11:35 96-18-405/09/22 22:598.4 4.3 1
1,2,4-Trimethylbenzene ND ug/kg 05/10/22 11:35 95-63-605/09/22 22:598.4 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 05/10/22 11:35 108-67-805/09/22 22:598.4 2.8 1
Vinyl acetate ND ug/kg 05/10/22 11:35 108-05-405/09/22 22:5984.4 6.1 1
Vinyl chloride ND ug/kg 05/10/22 11:35 75-01-405/09/22 22:5916.9 4.3 1
Xylene (Total)20.5 ug/kg 05/10/22 11:35 1330-20-705/09/22 22:5916.9 4.8 1
m&p-Xylene 10.5J ug/kg 05/10/22 11:35 179601-23-105/09/22 22:5916.9 5.8 1
o-Xylene 10 ug/kg 05/10/22 11:35 95-47-605/09/22 22:598.4 3.7 1
Surrogates
Toluene-d8 (S)98 %05/10/22 11:35 2037-26-505/09/22 22:5970-130 1
4-Bromofluorobenzene (S)100 %05/10/22 11:35 460-00-405/09/22 22:5969-134 1
1,2-Dichloroethane-d4 (S)97 %05/10/22 11:35 17060-07-005/09/22 22:5970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 6.8 %05/10/22 14:59 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-1 Lab ID: 92603521007 Collected: 05/02/22 10:00 Received: 05/06/22 12:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 504.1 Preparation Method: EPA 504.1
Pace Analytical Services - Charlotte
504 GCS EDB and DBCP
1,2-Dibromo-3-chloropropane ND ug/L 05/13/22 15:41 96-12-805/13/22 11:080.050 0.0027 1
1,2-Dibromoethane (EDB)ND ug/L 05/13/22 15:41 106-93-405/13/22 11:080.020 0.0036 1
Surrogates
1-Chloro-2-bromopropane (S)88 %05/13/22 15:41 301-79-5605/13/22 11:0870-130 1
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 05/17/22 21:28 N205/16/22 17:3598.0 98.0 1
Aliphatic (C19-C36)ND ug/L 05/17/22 21:28 N205/16/22 17:3598.0 98.0 1
Aromatic (C11-C22)1000 ug/L 05/17/22 21:28 1g,N205/16/22 17:3598.0 98.0 1
Surrogates
1-Chlorooctadecane (S)51 %05/17/22 21:28 3386-33-2 P205/16/22 17:3540-140 1
o-Terphenyl (S)82 %05/17/22 21:28 84-15-105/16/22 17:3540-140 1
2-Fluorobiphenyl (S)58 %05/17/22 21:28 321-60-805/16/22 17:3540-140 1
2-Bromonaphthalene (S)75 %05/17/22 21:28 580-13-205/16/22 17:3540-140 1
Analytical Method: MADEP VPH
Pace Analytical Services - Charlotte
VPH NC Water
Aliphatic (C05-C08)540 ug/L 05/14/22 01:14 N250.0 50.0 1
Aliphatic(C09-C12) Adjusted 61.5 ug/L 05/14/22 01:14 N250.0 50.0 1
Aromatic (C09-C10)ND ug/L 05/14/22 01:14 N250.0 50.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)104 %05/14/22 01:14 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)98 %05/14/22 01:14 460-00-470-130 1
Analytical Method: EPA 6020B Preparation Method: EPA 3005A
Pace Analytical Services - Peachtree Corners, GA
6020 MET ICPMS
Lead 6.5 ug/L 05/27/22 22:52 7439-92-105/26/22 11:521.0 0.89 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 05/10/22 13:34 83-32-905/09/22 17:514.5 1.8 1
Acenaphthylene ND ug/L 05/10/22 13:34 208-96-805/09/22 17:514.5 1.8 1
Anthracene ND ug/L 05/10/22 13:34 120-12-705/09/22 17:514.5 2.1 1
Benzo(a)anthracene ND ug/L 05/10/22 13:34 56-55-305/09/22 17:514.5 2.4 1
Benzo(a)pyrene ND ug/L 05/10/22 13:34 50-32-805/09/22 17:514.5 2.5 1
Benzo(b)fluoranthene ND ug/L 05/10/22 13:34 205-99-205/09/22 17:514.5 2.4 1
Benzo(g,h,i)perylene ND ug/L 05/10/22 13:34 191-24-205/09/22 17:514.5 2.6 1
Benzo(k)fluoranthene ND ug/L 05/10/22 13:34 207-08-905/09/22 17:514.5 2.5 1
4-Bromophenylphenyl ether ND ug/L 05/10/22 13:34 101-55-305/09/22 17:514.5 1.6 1
Butylbenzylphthalate ND ug/L 05/10/22 13:34 85-68-705/09/22 17:514.5 2.9 1
4-Chloro-3-methylphenol ND ug/L 05/10/22 13:34 59-50-705/09/22 17:514.5 3.0 1
bis(2-Chloroethoxy)methane ND ug/L 05/10/22 13:34 111-91-105/09/22 17:519.1 1.7 1
bis(2-Chloroethyl) ether ND ug/L 05/10/22 13:34 111-44-405/09/22 17:514.5 1.7 1
2-Chloronaphthalene ND ug/L 05/10/22 13:34 91-58-705/09/22 17:514.5 1.6 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-1 Lab ID: 92603521007 Collected: 05/02/22 10:00 Received: 05/06/22 12:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
2-Chlorophenol ND ug/L 05/10/22 13:34 95-57-805/09/22 17:514.5 1.1 1
4-Chlorophenylphenyl ether ND ug/L 05/10/22 13:34 7005-72-305/09/22 17:514.5 1.8 1
Chrysene ND ug/L 05/10/22 13:34 218-01-905/09/22 17:514.5 2.5 1
Dibenz(a,h)anthracene ND ug/L 05/10/22 13:34 53-70-305/09/22 17:514.5 2.7 1
3,3'-Dichlorobenzidine ND ug/L 05/10/22 13:34 91-94-105/09/22 17:519.1 7.4 1
2,4-Dichlorophenol ND ug/L 05/10/22 13:34 120-83-205/09/22 17:514.5 1.3 1
Diethylphthalate ND ug/L 05/10/22 13:34 84-66-205/09/22 17:514.5 1.9 1
2,4-Dimethylphenol ND ug/L 05/10/22 13:34 105-67-905/09/22 17:519.1 1.5 1
Dimethylphthalate ND ug/L 05/10/22 13:34 131-11-305/09/22 17:514.5 1.9 1
Di-n-butylphthalate ND ug/L 05/10/22 13:34 84-74-205/09/22 17:514.5 2.0 1
4,6-Dinitro-2-methylphenol ND ug/L 05/10/22 13:34 534-52-105/09/22 17:519.1 7.1 1
2,4-Dinitrophenol ND ug/L 05/10/22 13:34 51-28-505/09/22 17:5145.5 23.6 1
2,4-Dinitrotoluene ND ug/L 05/10/22 13:34 121-14-205/09/22 17:514.5 1.5 1
2,6-Dinitrotoluene ND ug/L 05/10/22 13:34 606-20-205/09/22 17:514.5 1.6 1
Di-n-octylphthalate ND ug/L 05/10/22 13:34 117-84-005/09/22 17:514.5 3.6 1
bis(2-Ethylhexyl)phthalate ND ug/L 05/10/22 13:34 117-81-705/09/22 17:514.5 3.4 1
Fluoranthene ND ug/L 05/10/22 13:34 206-44-005/09/22 17:514.5 2.0 1
Fluorene ND ug/L 05/10/22 13:34 86-73-705/09/22 17:514.5 1.9 1
Hexachloro-1,3-butadiene ND ug/L 05/10/22 13:34 87-68-305/09/22 17:514.5 1.6 1
Hexachlorobenzene ND ug/L 05/10/22 13:34 118-74-105/09/22 17:514.5 2.0 1
Hexachlorocyclopentadiene ND ug/L 05/10/22 13:34 77-47-405/09/22 17:519.1 1.4 1
Hexachloroethane ND ug/L 05/10/22 13:34 67-72-105/09/22 17:514.5 1.3 1
Indeno(1,2,3-cd)pyrene ND ug/L 05/10/22 13:34 193-39-505/09/22 17:514.5 2.6 1
Isophorone ND ug/L 05/10/22 13:34 78-59-105/09/22 17:519.1 1.5 1
Naphthalene ND ug/L 05/10/22 13:34 91-20-305/09/22 17:514.5 1.9 1
Nitrobenzene ND ug/L 05/10/22 13:34 98-95-305/09/22 17:514.5 1.7 1
2-Nitrophenol ND ug/L 05/10/22 13:34 88-75-505/09/22 17:514.5 1.3 1
4-Nitrophenol ND ug/L 05/10/22 13:34 100-02-705/09/22 17:519.1 6.0 1
N-Nitrosodimethylamine ND ug/L 05/10/22 13:34 62-75-905/09/22 17:514.5 1.7 1
N-Nitroso-di-n-propylamine ND ug/L 05/10/22 13:34 621-64-705/09/22 17:514.5 1.2 1
N-Nitrosodiphenylamine ND ug/L 05/10/22 13:34 86-30-605/09/22 17:519.1 2.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 05/10/22 13:34 108-60-105/09/22 17:514.5 1.0 1
Pentachlorophenol ND ug/L 05/10/22 13:34 87-86-505/09/22 17:519.1 3.4 1
Phenanthrene ND ug/L 05/10/22 13:34 85-01-805/09/22 17:514.5 1.8 1
Phenol ND ug/L 05/10/22 13:34 108-95-205/09/22 17:514.5 1.2 1
Pyrene ND ug/L 05/10/22 13:34 129-00-005/09/22 17:514.5 2.0 1
1,2,4-Trichlorobenzene ND ug/L 05/10/22 13:34 120-82-105/09/22 17:514.5 1.6 1
2,4,6-Trichlorophenol ND ug/L 05/10/22 13:34 88-06-205/09/22 17:519.1 1.4 1
Surrogates
Nitrobenzene-d5 (S)97 %05/10/22 13:34 4165-60-005/09/22 17:5110-120 1
2-Fluorobiphenyl (S)88 %05/10/22 13:34 321-60-805/09/22 17:5115-120 1
Terphenyl-d14 (S)102 %05/10/22 13:34 1718-51-005/09/22 17:5111-131 1
Phenol-d6 (S)43 %05/10/22 13:34 13127-88-305/09/22 17:5110-120 1
2-Fluorophenol (S)56 %05/10/22 13:34 367-12-405/09/22 17:5110-120 1
2,4,6-Tribromophenol (S)104 %05/10/22 13:34 118-79-605/09/22 17:5110-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-1 Lab ID: 92603521007 Collected: 05/02/22 10:00 Received: 05/06/22 12:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Tentatively Identified Compounds
Unknown 6.7J ug/L 05/10/22 13:3405/09/22 17:511
Ethylbenzene 13.2J ug/L 05/10/22 13:34 100-41-4 N05/09/22 17:511
Unknown 5.6J ug/L 05/10/22 13:3405/09/22 17:511
Unknown 5.9J ug/L 05/10/22 13:3405/09/22 17:511
Unknown 11.1J ug/L 05/10/22 13:3405/09/22 17:511
Unknown 14.0J ug/L 05/10/22 13:3405/09/22 17:511
Unknown 6.8J ug/L 05/10/22 13:3405/09/22 17:511
Unknown 110J ug/L 05/10/22 13:3405/09/22 17:511
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene 68.4 ug/L 05/10/22 18:39 71-43-20.50 0.34 1
Bromobenzene ND ug/L 05/10/22 18:39 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 05/10/22 18:39 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 05/10/22 18:39 75-27-40.50 0.31 1
Bromoform ND ug/L 05/10/22 18:39 75-25-20.50 0.34 1
Bromomethane ND ug/L 05/10/22 18:39 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 05/10/22 18:39 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 05/10/22 18:39 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 05/10/22 18:39 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 05/10/22 18:39 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 05/10/22 18:39 108-90-70.50 0.28 1
Chloroethane ND ug/L 05/10/22 18:39 75-00-31.0 0.65 1
Chloroform ND ug/L 05/10/22 18:39 67-66-30.50 0.43 1
Chloromethane ND ug/L 05/10/22 18:39 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 05/10/22 18:39 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 05/10/22 18:39 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 05/10/22 18:39 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 05/10/22 18:39 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 05/10/22 18:39 106-93-40.50 0.27 1
Dibromomethane ND ug/L 05/10/22 18:39 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 05/10/22 18:39 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 05/10/22 18:39 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 05/10/22 18:39 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 05/10/22 18:39 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 05/10/22 18:39 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 05/10/22 18:39 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 05/10/22 18:39 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 05/10/22 18:39 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 05/10/22 18:39 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 05/10/22 18:39 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 05/10/22 18:39 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 05/10/22 18:39 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 05/10/22 18:39 563-58-60.50 0.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 57
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92603521
MUSA 6760
Sample: SB-1 Lab ID: 92603521007 Collected: 05/02/22 10:00 Received: 05/06/22 12:30 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
cis-1,3-Dichloropropene ND ug/L 05/10/22 18:39 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 05/10/22 18:39 10061-02-60.50 0.36 1
Diisopropyl ether 2.8 ug/L 05/10/22 18:39 108-20-30.50 0.31 1
Ethylbenzene 11.6 ug/L 05/10/22 18:39 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 05/10/22 18:39 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)0.39J ug/L 05/10/22 18:39 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 05/10/22 18:39 75-09-22.0 2.0 1
Methyl-tert-butyl ether 5.5 ug/L 05/10/22 18:39 1634-04-40.50 0.42 1
Naphthalene ND ug/L 05/10/22 18:39 91-20-32.0 0.64 1
n-Propylbenzene 0.55 ug/L 05/10/22 18:39 103-65-10.50 0.34 1
Styrene ND ug/L 05/10/22 18:39 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 05/10/22 18:39 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 05/10/22 18:39 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 05/10/22 18:39 127-18-40.50 0.29 1
Toluene ND ug/L 05/10/22 18:39 108-88-30.50 0.48 1
1,2,3-Trichlorobenzene ND ug/L 05/10/22 18:39 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 05/10/22 18:39 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 05/10/22 18:39 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 05/10/22 18:39 79-00-50.50 0.32 1
Trichloroethene ND ug/L 05/10/22 18:39 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 05/10/22 18:39 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 05/10/22 18:39 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 05/10/22 18:39 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene 0.69 ug/L 05/10/22 18:39 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 05/10/22 18:39 75-01-41.0 0.39 1
m&p-Xylene 2.0 ug/L 05/10/22 18:39 179601-23-11.0 0.71 1
o-Xylene 0.58 ug/L 05/10/22 18:39 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %05/10/22 18:39 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %05/10/22 18:39 460-00-470-130 1
Toluene-d8 (S)99 %05/10/22 18:39 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
697858
EPA 5030B
EPA 8015C
Gasoline Range Organics
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521001, 92603521002, 92603521003, 92603521004, 92603521005, 92603521006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3643978
Associated Lab Samples:92603521001, 92603521002, 92603521003, 92603521004, 92603521005, 92603521006
Matrix: Solid
AnalyzedMDL
Gas Range Organics (C6-C10)mg/kg ND 6.0 05/13/22 00:471.7
4-Bromofluorobenzene (S)%83 66-130 05/13/22 00:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3643979LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 45.650.3 91 70-130
4-Bromofluorobenzene (S)%87 66-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3643981MATRIX SPIKE SAMPLE:
MSSpike
Result
92603995014
Gas Range Organics (C6-C10)mg/kg 50.154.8 92 65-146<1.8
4-Bromofluorobenzene (S)%82 66-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603995013
3643980SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg ND 30<2.9
4-Bromofluorobenzene (S)%8687
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
698185
MADEP VPH
MADEP VPH
VPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3645776
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
Aliphatic (C05-C08)ug/L ND 50.0 N205/13/22 21:2250.0
Aromatic (C09-C10)ug/L ND 50.0 N205/13/22 21:2250.0
4-Bromofluorobenzene (FID) (S)%107 70-130 05/13/22 21:22
4-Bromofluorobenzene (PID) (S)%105 70-130 05/13/22 21:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3645777LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3645778
Aliphatic (C05-C08)ug/L 293 N23009870-130101304 4 25
Aromatic (C09-C10)ug/L 103 N210010370-130107107 4 25
4-Bromofluorobenzene (FID) (S)%99 70-130101
4-Bromofluorobenzene (PID) (S)%100 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
700699
EPA 3005A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Peachtree Corners, GA
Associated Lab Samples: 92603521007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3657411
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
Lead ug/L ND 1.0 05/27/22 22:400.89
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3657412LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 104100 104 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3658157MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92606207001
3658158
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Lead ug/L 100 101 75-12598 3 20100ND101 98.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
697129
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3640342
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/10/22 12:530.31
1,1,1-Trichloroethane ug/L ND 0.50 05/10/22 12:530.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/10/22 12:530.22
1,1,2-Trichloroethane ug/L ND 0.50 05/10/22 12:530.32
1,1-Dichloroethane ug/L ND 0.50 05/10/22 12:530.37
1,1-Dichloroethene ug/L ND 0.50 05/10/22 12:530.35
1,1-Dichloropropene ug/L ND 0.50 05/10/22 12:530.43
1,2,3-Trichlorobenzene ug/L ND 2.0 05/10/22 12:530.81
1,2,3-Trichloropropane ug/L ND 0.50 05/10/22 12:530.26
1,2,4-Trichlorobenzene ug/L ND 2.0 05/10/22 12:530.64
1,2,4-Trimethylbenzene ug/L ND 0.50 05/10/22 12:530.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/10/22 12:530.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/10/22 12:530.27
1,2-Dichlorobenzene ug/L ND 0.50 05/10/22 12:530.34
1,2-Dichloroethane ug/L ND 0.50 05/10/22 12:530.32
1,2-Dichloropropane ug/L ND 0.50 05/10/22 12:530.36
1,3,5-Trimethylbenzene ug/L ND 0.50 05/10/22 12:530.33
1,3-Dichlorobenzene ug/L ND 0.50 05/10/22 12:530.34
1,3-Dichloropropane ug/L ND 0.50 05/10/22 12:530.28
1,4-Dichlorobenzene ug/L ND 0.50 05/10/22 12:530.33
2,2-Dichloropropane ug/L ND 0.50 05/10/22 12:530.39
2-Chlorotoluene ug/L ND 0.50 05/10/22 12:530.32
4-Chlorotoluene ug/L ND 0.50 05/10/22 12:530.32
Benzene ug/L ND 0.50 05/10/22 12:530.34
Bromobenzene ug/L ND 0.50 05/10/22 12:530.29
Bromochloromethane ug/L ND 0.50 05/10/22 12:530.47
Bromodichloromethane ug/L ND 0.50 05/10/22 12:530.31
Bromoform ug/L ND 0.50 05/10/22 12:530.34
Bromomethane ug/L ND 5.0 05/10/22 12:531.7
Carbon tetrachloride ug/L ND 0.50 05/10/22 12:530.33
Chlorobenzene ug/L ND 0.50 05/10/22 12:530.28
Chloroethane ug/L ND 1.0 05/10/22 12:530.65
Chloroform ug/L ND 0.50 05/10/22 12:530.43
Chloromethane ug/L ND 1.0 05/10/22 12:530.54
cis-1,2-Dichloroethene ug/L ND 0.50 05/10/22 12:530.38
cis-1,3-Dichloropropene ug/L ND 0.50 05/10/22 12:530.36
Dibromochloromethane ug/L ND 0.50 05/10/22 12:530.36
Dibromomethane ug/L ND 0.50 05/10/22 12:530.39
Dichlorodifluoromethane ug/L ND 0.50 05/10/22 12:530.35
Diisopropyl ether ug/L ND 0.50 05/10/22 12:530.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3640342
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 05/10/22 12:530.30
Hexachloro-1,3-butadiene ug/L ND 2.0 05/10/22 12:531.5
Isopropylbenzene (Cumene)ug/L ND 0.50 05/10/22 12:530.33
m&p-Xylene ug/L ND 1.0 05/10/22 12:530.71
Methyl-tert-butyl ether ug/L ND 0.50 05/10/22 12:530.42
Methylene Chloride ug/L ND 2.0 05/10/22 12:532.0
n-Butylbenzene ug/L ND 0.50 05/10/22 12:530.49
n-Propylbenzene ug/L ND 0.50 05/10/22 12:530.34
Naphthalene ug/L ND 2.0 05/10/22 12:530.64
o-Xylene ug/L ND 0.50 05/10/22 12:530.34
sec-Butylbenzene ug/L ND 0.50 05/10/22 12:530.40
Styrene ug/L ND 0.50 05/10/22 12:530.29
tert-Butylbenzene ug/L ND 0.50 05/10/22 12:530.32
Tetrachloroethene ug/L ND 0.50 05/10/22 12:530.29
Toluene ug/L ND 0.50 05/10/22 12:530.48
trans-1,2-Dichloroethene ug/L ND 0.50 05/10/22 12:530.40
trans-1,3-Dichloropropene ug/L ND 0.50 05/10/22 12:530.36
Trichloroethene ug/L ND 0.50 05/10/22 12:530.38
Trichlorofluoromethane ug/L ND 1.0 05/10/22 12:530.30
Vinyl chloride ug/L ND 1.0 05/10/22 12:530.39
1,2-Dichloroethane-d4 (S)%93 70-130 05/10/22 12:53
4-Bromofluorobenzene (S)%100 70-130 05/10/22 12:53
Toluene-d8 (S)%99 70-130 05/10/22 12:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3640343LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 47.550 95 60-140
1,1,1-Trichloroethane ug/L 42.450 85 60-140
1,1,2,2-Tetrachloroethane ug/L 43.950 88 60-140
1,1,2-Trichloroethane ug/L 48.650 97 60-140
1,1-Dichloroethane ug/L 41.850 84 60-140
1,1-Dichloroethene ug/L 43.750 87 60-140
1,1-Dichloropropene ug/L 43.850 88 60-140
1,2,3-Trichlorobenzene ug/L 57.950 116 60-140
1,2,3-Trichloropropane ug/L 44.150 88 60-140
1,2,4-Trichlorobenzene ug/L 52.750 105 60-140
1,2,4-Trimethylbenzene ug/L 46.550 93 60-140
1,2-Dibromo-3-chloropropane ug/L 43.450 87 60-140
1,2-Dibromoethane (EDB)ug/L 46.650 93 60-140
1,2-Dichlorobenzene ug/L 49.650 99 60-140
1,2-Dichloroethane ug/L 42.150 84 60-140
1,2-Dichloropropane ug/L 45.550 91 60-140
1,3,5-Trimethylbenzene ug/L 47.150 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3640343LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 49.650 99 60-140
1,3-Dichloropropane ug/L 47.150 94 60-140
1,4-Dichlorobenzene ug/L 47.950 96 60-140
2,2-Dichloropropane ug/L 49.850 100 60-140
2-Chlorotoluene ug/L 46.350 93 60-140
4-Chlorotoluene ug/L 44.150 88 60-140
Benzene ug/L 43.250 86 60-140
Bromobenzene ug/L 47.250 94 60-140
Bromochloromethane ug/L 43.850 88 60-140
Bromodichloromethane ug/L 44.650 89 60-140
Bromoform ug/L 50.550 101 60-140
Bromomethane ug/L 42.150 84 60-140
Carbon tetrachloride ug/L 44.250 88 60-140
Chlorobenzene ug/L 48.550 97 60-140
Chloroethane ug/L 54.850 110 60-140
Chloroform ug/L 41.250 82 60-140
Chloromethane ug/L 47.550 95 60-140
cis-1,2-Dichloroethene ug/L 42.050 84 60-140
cis-1,3-Dichloropropene ug/L 46.650 93 60-140
Dibromochloromethane ug/L 47.450 95 60-140
Dibromomethane ug/L 48.750 97 60-140
Dichlorodifluoromethane ug/L 48.650 97 60-140
Diisopropyl ether ug/L 42.850 86 60-140
Ethylbenzene ug/L 48.950 98 60-140
Hexachloro-1,3-butadiene ug/L 55.850 112 60-140
Isopropylbenzene (Cumene)ug/L 49.150 98 60-140
m&p-Xylene ug/L 97.7100 98 60-140
Methyl-tert-butyl ether ug/L 43.350 87 60-140
Methylene Chloride ug/L 48.350 97 60-140
n-Butylbenzene ug/L 47.250 94 60-140
n-Propylbenzene ug/L 47.350 95 60-140
Naphthalene ug/L 50.450 101 60-140
o-Xylene ug/L 49.250 98 60-140
sec-Butylbenzene ug/L 48.250 96 60-140
Styrene ug/L 51.450 103 60-140
tert-Butylbenzene ug/L 41.250 82 60-140
Tetrachloroethene ug/L 50.350 101 60-140
Toluene ug/L 51.750 103 60-140
trans-1,2-Dichloroethene ug/L 43.850 88 60-140
trans-1,3-Dichloropropene ug/L 46.350 93 60-140
Trichloroethene ug/L 49.050 98 60-140
Trichlorofluoromethane ug/L 51.150 102 60-140
Vinyl chloride ug/L 50.350 101 60-140
1,2-Dichloroethane-d4 (S)%84 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3640344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92603347001
3640345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 94 60-14098 5 3020ND18.7 19.6
1,1,1-Trichloroethane ug/L 20 82 60-14088 8 3020ND16.4 17.7
1,1,2,2-Tetrachloroethane ug/L 20 83 60-14088 7 3020ND16.6 17.7
1,1,2-Trichloroethane ug/L 20 90 60-14096 7 3020ND18.0 19.2
1,1-Dichloroethane ug/L 20 80 60-14087 9 3020ND16.0 17.5
1,1-Dichloroethene ug/L 20 86 60-14094 9 3020ND17.1 18.7
1,1-Dichloropropene ug/L 20 85 60-14093 9 3020ND17.0 18.6
1,2,3-Trichlorobenzene ug/L 20 117 60-140119 2 3020ND23.4 23.8
1,2,3-Trichloropropane ug/L 20 88 60-14091 4 3020ND17.5 18.2
1,2,4-Trichlorobenzene ug/L 20 100 60-140108 7 3020ND20.0 21.5
1,2,4-Trimethylbenzene ug/L 20 88 60-14094 7 3020ND17.5 18.7
1,2-Dibromo-3-
chloropropane ug/L 20 77 60-14086 12 3020ND15.3 17.2
1,2-Dibromoethane (EDB) ug/L 20 91 60-14095 4 3020ND18.1 18.9
1,2-Dichlorobenzene ug/L 20 90 60-14099 10 3020ND17.9 19.8
1,2-Dichloroethane ug/L 20 76 60-14085 11 3020ND15.2 17.0
1,2-Dichloropropane ug/L 20 90 60-14095 6 3020ND17.9 19.0
1,3,5-Trimethylbenzene ug/L 20 90 60-14096 7 3020ND17.9 19.3
1,3-Dichlorobenzene ug/L 20 91 60-14097 7 3020ND18.2 19.4
1,3-Dichloropropane ug/L 20 91 60-14097 7 3020ND18.2 19.5
1,4-Dichlorobenzene ug/L 20 88 60-14090 2 3020ND17.5 17.9
2,2-Dichloropropane ug/L 20 97 60-140101 4 3020ND19.3 20.2
2-Chlorotoluene ug/L 20 81 60-14094 14 3020ND16.2 18.7
4-Chlorotoluene ug/L 20 85 60-14091 7 3020ND17.0 18.2
Benzene ug/L 20 84 60-14092 9 3020ND16.8 18.3
Bromobenzene ug/L 20 88 60-14095 8 3020ND17.5 19.0
Bromochloromethane ug/L 20 85 60-14093 9 3020ND17.1 18.6
Bromodichloromethane ug/L 20 85 60-14092 8 3020ND17.0 18.4
Bromoform ug/L 20 93 60-14099 5 3020ND18.7 19.7
Bromomethane ug/L 20 96 60-140101 5 3020ND19.2 20.2
Carbon tetrachloride ug/L 20 88 60-14095 8 3020ND17.6 19.1
Chlorobenzene ug/L 20 94 60-140100 6 3020ND18.8 19.9
Chloroethane ug/L 20 109 60-140116 7 3020ND21.8 23.3
Chloroform ug/L 20 81 60-14086 5 3020ND16.3 17.2
Chloromethane ug/L 20 94 60-140100 6 3020ND18.8 20.1
cis-1,2-Dichloroethene ug/L 20 82 60-14089 8 3020ND16.4 17.7
cis-1,3-Dichloropropene ug/L 20 89 60-14097 8 3020ND17.9 19.4
Dibromochloromethane ug/L 20 89 60-14093 4 3020ND17.9 18.6
Dibromomethane ug/L 20 95 60-140103 8 3020ND19.0 20.7
Dichlorodifluoromethane ug/L 20 87 60-14094 8 3020ND17.4 18.8
Diisopropyl ether ug/L 20 81 60-14087 7 3020ND16.2 17.3
Ethylbenzene ug/L 20 96 60-140101 5 3020ND19.2 20.2
Hexachloro-1,3-butadiene ug/L 20 114 60-140118 4 3020ND22.7 23.6
Isopropylbenzene(Cumene)ug/L 20 96 60-140101 5 3020ND19.3 20.3
m&p-Xylene ug/L 40 96 60-140100 4 3040ND38.4 40.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3640344MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92603347001
3640345
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 81 60-14090 10 3020ND16.3 18.0
Methylene Chloride ug/L 20 89 60-14097 8 3020ND17.9 19.4
n-Butylbenzene ug/L 20 91 60-14095 5 3020ND18.2 19.1
n-Propylbenzene ug/L 20 90 60-14099 9 3020ND18.0 19.7
Naphthalene ug/L 20 96 60-14099 4 3020ND19.1 19.9
o-Xylene ug/L 20 96 60-140102 6 3020ND19.2 20.3
sec-Butylbenzene ug/L 20 92 60-14099 7 3020ND18.5 19.8
Styrene ug/L 20 96 60-140101 5 3020ND19.2 20.2
tert-Butylbenzene ug/L 20 78 60-14086 10 3020ND15.7 17.2
Tetrachloroethene ug/L 20 100 60-140104 4 3020ND20.1 20.9
Toluene ug/L 20 99 60-140107 8 3020ND19.8 21.4
trans-1,2-Dichloroethene ug/L 20 85 60-14091 7 3020ND17.1 18.2
trans-1,3-Dichloropropene ug/L 20 90 60-14096 7 3020ND17.9 19.3
Trichloroethene ug/L 20 96 60-140106 9 3020ND19.3 21.2
Trichlorofluoromethane ug/L 20 94 60-140103 9 3020ND18.8 20.6
Vinyl chloride ug/L 20 97 60-140102 5 3020ND19.4 20.4
1,2-Dichloroethane-d4 (S) %84 70-13084
4-Bromofluorobenzene (S) %105 70-130102
Toluene-d8 (S)%97 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
696975
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521001, 92603521002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3639832
Associated Lab Samples:92603521001, 92603521002
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/10/22 03:101.9
1,1,1-Trichloroethane ug/kg ND 5.0 05/10/22 03:102.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/10/22 03:101.3
1,1,2-Trichloroethane ug/kg ND 5.0 05/10/22 03:101.7
1,1-Dichloroethane ug/kg ND 5.0 05/10/22 03:102.1
1,1-Dichloroethene ug/kg ND 5.0 05/10/22 03:102.1
1,1-Dichloropropene ug/kg ND 5.0 05/10/22 03:102.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/10/22 03:104.0
1,2,3-Trichloropropane ug/kg ND 5.0 05/10/22 03:102.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/10/22 03:104.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/10/22 03:101.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/10/22 03:101.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 05/10/22 03:102.2
1,2-Dichlorobenzene ug/kg ND 5.0 05/10/22 03:101.8
1,2-Dichloroethane ug/kg ND 5.0 05/10/22 03:103.3
1,2-Dichloropropane ug/kg ND 5.0 05/10/22 03:101.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/10/22 03:101.7
1,3-Dichlorobenzene ug/kg ND 5.0 05/10/22 03:101.6
1,3-Dichloropropane ug/kg ND 5.0 05/10/22 03:101.6
1,4-Dichlorobenzene ug/kg ND 5.0 05/10/22 03:101.3
2,2-Dichloropropane ug/kg ND 5.0 05/10/22 03:101.6
2-Butanone (MEK)ug/kg ND 100 05/10/22 03:1024.0
2-Chlorotoluene ug/kg ND 5.0 05/10/22 03:101.8
2-Hexanone ug/kg ND 50.0 05/10/22 03:104.8
4-Chlorotoluene ug/kg ND 5.0 05/10/22 03:100.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 05/10/22 03:104.8
Acetone ug/kg ND 100 05/10/22 03:1032.1
Benzene ug/kg ND 5.0 05/10/22 03:102.0
Bromobenzene ug/kg ND 5.0 05/10/22 03:101.6
Bromochloromethane ug/kg ND 5.0 05/10/22 03:101.5
Bromodichloromethane ug/kg ND 5.0 05/10/22 03:101.9
Bromoform ug/kg ND 5.0 05/10/22 03:101.8
Bromomethane ug/kg ND 10.0 IK05/10/22 03:107.9
Carbon tetrachloride ug/kg ND 5.0 05/10/22 03:101.9
Chlorobenzene ug/kg ND 5.0 05/10/22 03:100.96
Chloroethane ug/kg ND 10.0 05/10/22 03:103.9
Chloroform ug/kg ND 5.0 05/10/22 03:103.0
Chloromethane ug/kg ND 10.0 05/10/22 03:104.2
cis-1,2-Dichloroethene ug/kg ND 5.0 05/10/22 03:101.7
cis-1,3-Dichloropropene ug/kg ND 5.0 05/10/22 03:101.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3639832
Associated Lab Samples:92603521001, 92603521002
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 05/10/22 03:102.8
Dibromomethane ug/kg ND 5.0 05/10/22 03:101.1
Dichlorodifluoromethane ug/kg ND 10.0 05/10/22 03:102.2
Diisopropyl ether ug/kg ND 5.0 05/10/22 03:101.4
Ethylbenzene ug/kg ND 5.0 05/10/22 03:102.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/10/22 03:108.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 05/10/22 03:101.7
m&p-Xylene ug/kg ND 10.0 05/10/22 03:103.4
Methyl-tert-butyl ether ug/kg ND 5.0 05/10/22 03:101.9
Methylene Chloride ug/kg ND 20.0 05/10/22 03:1013.7
n-Butylbenzene ug/kg ND 5.0 05/10/22 03:102.4
n-Propylbenzene ug/kg ND 5.0 05/10/22 03:101.8
Naphthalene ug/kg ND 5.0 05/10/22 03:102.6
o-Xylene ug/kg ND 5.0 05/10/22 03:102.2
p-Isopropyltoluene ug/kg ND 5.0 05/10/22 03:102.5
sec-Butylbenzene ug/kg ND 5.0 05/10/22 03:102.2
Styrene ug/kg ND 5.0 05/10/22 03:101.3
tert-Butylbenzene ug/kg ND 5.0 05/10/22 03:101.8
Tetrachloroethene ug/kg ND 5.0 05/10/22 03:101.6
Toluene ug/kg ND 5.0 05/10/22 03:101.4
trans-1,2-Dichloroethene ug/kg ND 5.0 05/10/22 03:101.8
trans-1,3-Dichloropropene ug/kg ND 5.0 05/10/22 03:101.7
Trichloroethene ug/kg ND 5.0 05/10/22 03:101.3
Trichlorofluoromethane ug/kg ND 5.0 05/10/22 03:102.8
Vinyl acetate ug/kg ND 50.0 05/10/22 03:103.6
Vinyl chloride ug/kg ND 10.0 05/10/22 03:102.5
Xylene (Total)ug/kg ND 10.0 05/10/22 03:102.8
1,2-Dichloroethane-d4 (S)%101 70-130 05/10/22 03:10
4-Bromofluorobenzene (S)%99 69-134 05/10/22 03:10
Toluene-d8 (S)%97 70-130 05/10/22 03:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3639833LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12801250 103 70-130
1,1,1-Trichloroethane ug/kg 12901250 103 70-130
1,1,2,2-Tetrachloroethane ug/kg 12201250 98 70-130
1,1,2-Trichloroethane ug/kg 12801250 102 70-130
1,1-Dichloroethane ug/kg 12601250 100 70-130
1,1-Dichloroethene ug/kg 14001250 112 70-130
1,1-Dichloropropene ug/kg 13401250 107 70-130
1,2,3-Trichlorobenzene ug/kg 12301250 98 65-130
1,2,3-Trichloropropane ug/kg 12201250 97 70-130
1,2,4-Trichlorobenzene ug/kg 12401250 99 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3639833LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12301250 98 70-130
1,2-Dibromo-3-chloropropane ug/kg 11901250 95 70-130
1,2-Dibromoethane (EDB)ug/kg 13201250 106 70-130
1,2-Dichlorobenzene ug/kg 12501250 100 70-130
1,2-Dichloroethane ug/kg 12301250 98 63-130
1,2-Dichloropropane ug/kg 12501250 100 70-130
1,3,5-Trimethylbenzene ug/kg 12701250 101 70-130
1,3-Dichlorobenzene ug/kg 12801250 102 70-130
1,3-Dichloropropane ug/kg 12701250 101 70-130
1,4-Dichlorobenzene ug/kg 12101250 97 70-130
2,2-Dichloropropane ug/kg 11701250 93 66-130
2-Butanone (MEK)ug/kg 23802500 95 70-130
2-Chlorotoluene ug/kg 12801250 102 70-130
2-Hexanone ug/kg 24602500 98 70-130
4-Chlorotoluene ug/kg 12501250 100 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24502500 98 70-130
Acetone ug/kg 24702500 99 69-130
Benzene ug/kg 11901250 96 70-130
Bromobenzene ug/kg 12801250 103 70-130
Bromochloromethane ug/kg 14401250 115 70-130
Bromodichloromethane ug/kg 12801250 103 69-130
Bromoform ug/kg 13301250 106 70-130
Bromomethane ug/kg 1070 IK125086 52-130
Carbon tetrachloride ug/kg 12901250 103 70-130
Chlorobenzene ug/kg 12601250 101 70-130
Chloroethane ug/kg 14001250 112 65-130
Chloroform ug/kg 12901250 103 70-130
Chloromethane ug/kg 13901250 111 55-130
cis-1,2-Dichloroethene ug/kg 12901250 103 70-130
cis-1,3-Dichloropropene ug/kg 13201250 105 70-130
Dibromochloromethane ug/kg 12901250 104 70-130
Dibromomethane ug/kg 13401250 107 70-130
Dichlorodifluoromethane ug/kg 14201250 114 45-156
Diisopropyl ether ug/kg 12301250 98 70-130
Ethylbenzene ug/kg 11801250 95 70-130
Hexachloro-1,3-butadiene ug/kg 12001250 96 66-130
Isopropylbenzene (Cumene)ug/kg 12801250 102 70-130
m&p-Xylene ug/kg 25402500 102 70-130
Methyl-tert-butyl ether ug/kg 12801250 102 70-130
Methylene Chloride ug/kg 12401250 100 65-130
n-Butylbenzene ug/kg 12501250 100 67-130
n-Propylbenzene ug/kg 12601250 101 70-130
Naphthalene ug/kg 13001250 104 70-130
o-Xylene ug/kg 12701250 102 70-130
p-Isopropyltoluene ug/kg 12901250 103 67-130
sec-Butylbenzene ug/kg 12701250 102 69-130
Styrene ug/kg 13601250 109 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3639833LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12901250 103 67-130
Tetrachloroethene ug/kg 13101250 105 70-130
Toluene ug/kg 12101250 97 70-130
trans-1,2-Dichloroethene ug/kg 13201250 106 70-130
trans-1,3-Dichloropropene ug/kg 13001250 104 68-130
Trichloroethene ug/kg 12701250 102 70-130
Trichlorofluoromethane ug/kg 13101250 105 70-130
Vinyl acetate ug/kg 27002500 108 70-130
Vinyl chloride ug/kg 13501250 108 61-130
Xylene (Total)ug/kg 38103750 102 70-130
1,2-Dichloroethane-d4 (S)%89 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3639834MATRIX SPIKE SAMPLE:
MSSpike
Result
92603219006
1,1,1,2-Tetrachloroethane ug/kg 306 M168545 70-131ND
1,1,1-Trichloroethane ug/kg 293 M168543 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 308 M168545 66-130ND
1,1,2-Trichloroethane ug/kg 301 M168544 66-133ND
1,1-Dichloroethane ug/kg 284 M168541 65-130ND
1,1-Dichloroethene ug/kg 283685 41 10-158ND
1,1-Dichloropropene ug/kg 270 M168539 68-133ND
1,2,3-Trichlorobenzene ug/kg 258685 38 27-138ND
1,2,3-Trichloropropane ug/kg 295 M168543 67-130ND
1,2,4-Trichlorobenzene ug/kg 236 M168534 51-134ND
1,2,4-Trimethylbenzene ug/kg 247 M168536 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 264685 39 32-130ND
1,2-Dibromoethane (EDB)ug/kg 321 M168547 70-130ND
1,2-Dichlorobenzene ug/kg 280 M168541 69-130ND
1,2-Dichloroethane ug/kg 300 M168544 59-130ND
1,2-Dichloropropane ug/kg 300 M168544 70-130ND
1,3,5-Trimethylbenzene ug/kg 246 M168536 65-137ND
1,3-Dichlorobenzene ug/kg 253 M168537 70-130ND
1,3-Dichloropropane ug/kg 313 M168546 70-130ND
1,4-Dichlorobenzene ug/kg 257 M168537 68-130ND
2,2-Dichloropropane ug/kg 236685 34 32-130ND
2-Butanone (MEK)ug/kg 5191370 36 10-136ND
2-Chlorotoluene ug/kg 258 M168538 69-141ND
2-Hexanone ug/kg 5451370 40 10-144ND
4-Chlorotoluene ug/kg 244 M168536 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 5341370 39 25-143ND
Acetone ug/kg 4151370 30 10-130ND
Benzene ug/kg 297 M168543 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3639834MATRIX SPIKE SAMPLE:
MSSpike
Result
92603219006
Bromobenzene ug/kg 285 M168542 70-130ND
Bromochloromethane ug/kg 338 M168549 69-134ND
Bromodichloromethane ug/kg 285 M168541 64-130ND
Bromoform ug/kg 283 M168541 62-130ND
Bromomethane ug/kg 154 IK68522 20-176ND
Carbon tetrachloride ug/kg 276 M168540 65-140ND
Chlorobenzene ug/kg 290 M168542 70-130ND
Chloroethane ug/kg 60.4 M16859 10-130ND
Chloroform ug/kg 292 M168543 63-130ND
Chloromethane ug/kg 350 M168551 58-130ND
cis-1,2-Dichloroethene ug/kg 297 M168543 66-130ND
cis-1,3-Dichloropropene ug/kg 295 M168543 67-130ND
Dibromochloromethane ug/kg 281 M168541 67-130ND
Dibromomethane ug/kg 322 M168547 63-131ND
Dichlorodifluoromethane ug/kg 286 M168542 44-180ND
Diisopropyl ether ug/kg 282 M168541 63-130ND
Ethylbenzene ug/kg 263 M168538 66-130ND
Hexachloro-1,3-butadiene ug/kg 200 M168529 64-150ND
Isopropylbenzene (Cumene)ug/kg 274 M168540 69-135ND
m&p-Xylene ug/kg 536 M1137039 60-133ND
Methyl-tert-butyl ether ug/kg 287 M168542 65-130ND
Methylene Chloride ug/kg 267 M168539 61-130ND
n-Butylbenzene ug/kg 194 M168528 65-140ND
n-Propylbenzene ug/kg 236 M168534 67-140ND
Naphthalene ug/kg 285685 41 15-145ND
o-Xylene ug/kg 290 M168542 66-133ND
p-Isopropyltoluene ug/kg 227 M168533 56-147ND
sec-Butylbenzene ug/kg 250 M168536 65-139ND
Styrene ug/kg 285 M168542 70-132ND
tert-Butylbenzene ug/kg 272 M168540 62-135ND
Tetrachloroethene ug/kg 248 M168536 70-135ND
Toluene ug/kg 281 M168541 67-130ND
trans-1,2-Dichloroethene ug/kg 277 M168540 69-130ND
trans-1,3-Dichloropropene ug/kg 280 M168541 62-130ND
Trichloroethene ug/kg 285 M168542 70-135ND
Trichlorofluoromethane ug/kg 46.9 M16857 10-130ND
Vinyl acetate ug/kg 553 M1137040 53-130ND
Vinyl chloride ug/kg 297 M168543 61-148ND
Xylene (Total)ug/kg 827 MS206040 63-132ND
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603219007
3639835SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603219007
3639835SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg ND 30ND
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9797
4-Bromofluorobenzene (S)%101100
Toluene-d8 (S)%9898
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
697025
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521003, 92603521004, 92603521005, 92603521006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3640005
Associated Lab Samples:92603521003, 92603521004, 92603521005, 92603521006
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/10/22 03:281.9
1,1,1-Trichloroethane ug/kg ND 5.0 05/10/22 03:282.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/10/22 03:281.3
1,1,2-Trichloroethane ug/kg ND 5.0 05/10/22 03:281.7
1,1-Dichloroethane ug/kg ND 5.0 05/10/22 03:282.1
1,1-Dichloroethene ug/kg ND 5.0 05/10/22 03:282.1
1,1-Dichloropropene ug/kg ND 5.0 05/10/22 03:282.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/10/22 03:284.0
1,2,3-Trichloropropane ug/kg ND 5.0 05/10/22 03:282.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/10/22 03:284.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/10/22 03:281.4
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/10/22 03:281.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 05/10/22 03:282.2
1,2-Dichlorobenzene ug/kg ND 5.0 05/10/22 03:281.8
1,2-Dichloroethane ug/kg ND 5.0 05/10/22 03:283.3
1,2-Dichloropropane ug/kg ND 5.0 05/10/22 03:281.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/10/22 03:281.7
1,3-Dichlorobenzene ug/kg ND 5.0 05/10/22 03:281.6
1,3-Dichloropropane ug/kg ND 5.0 05/10/22 03:281.6
1,4-Dichlorobenzene ug/kg ND 5.0 05/10/22 03:281.3
2,2-Dichloropropane ug/kg ND 5.0 05/10/22 03:281.6
2-Butanone (MEK)ug/kg ND 100 05/10/22 03:2824.0
2-Chlorotoluene ug/kg ND 5.0 05/10/22 03:281.8
2-Hexanone ug/kg ND 50.0 05/10/22 03:284.8
4-Chlorotoluene ug/kg ND 5.0 05/10/22 03:280.88
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 05/10/22 03:284.8
Acetone ug/kg ND 100 05/10/22 03:2832.1
Benzene ug/kg ND 5.0 05/10/22 03:282.0
Bromobenzene ug/kg ND 5.0 05/10/22 03:281.6
Bromochloromethane ug/kg ND 5.0 05/10/22 03:281.5
Bromodichloromethane ug/kg ND 5.0 05/10/22 03:281.9
Bromoform ug/kg ND 5.0 05/10/22 03:281.8
Bromomethane ug/kg ND 10.0 IK05/10/22 03:287.9
Carbon tetrachloride ug/kg ND 5.0 05/10/22 03:281.9
Chlorobenzene ug/kg ND 5.0 05/10/22 03:280.96
Chloroethane ug/kg ND 10.0 05/10/22 03:283.9
Chloroform ug/kg ND 5.0 05/10/22 03:283.0
Chloromethane ug/kg ND 10.0 05/10/22 03:284.2
cis-1,2-Dichloroethene ug/kg ND 5.0 05/10/22 03:281.7
cis-1,3-Dichloropropene ug/kg ND 5.0 05/10/22 03:281.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3640005
Associated Lab Samples:92603521003, 92603521004, 92603521005, 92603521006
Matrix: Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 05/10/22 03:282.8
Dibromomethane ug/kg ND 5.0 05/10/22 03:281.1
Dichlorodifluoromethane ug/kg ND 10.0 05/10/22 03:282.2
Diisopropyl ether ug/kg ND 5.0 05/10/22 03:281.4
Ethylbenzene ug/kg ND 5.0 05/10/22 03:282.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/10/22 03:288.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 05/10/22 03:281.7
m&p-Xylene ug/kg ND 10.0 05/10/22 03:283.4
Methyl-tert-butyl ether ug/kg ND 5.0 05/10/22 03:281.9
Methylene Chloride ug/kg ND 20.0 05/10/22 03:2813.7
n-Butylbenzene ug/kg ND 5.0 05/10/22 03:282.4
n-Propylbenzene ug/kg ND 5.0 05/10/22 03:281.8
Naphthalene ug/kg ND 5.0 05/10/22 03:282.6
o-Xylene ug/kg ND 5.0 05/10/22 03:282.2
p-Isopropyltoluene ug/kg ND 5.0 05/10/22 03:282.5
sec-Butylbenzene ug/kg ND 5.0 05/10/22 03:282.2
Styrene ug/kg ND 5.0 05/10/22 03:281.3
tert-Butylbenzene ug/kg ND 5.0 05/10/22 03:281.8
Tetrachloroethene ug/kg ND 5.0 05/10/22 03:281.6
Toluene ug/kg ND 5.0 05/10/22 03:281.4
trans-1,2-Dichloroethene ug/kg ND 5.0 05/10/22 03:281.8
trans-1,3-Dichloropropene ug/kg ND 5.0 05/10/22 03:281.7
Trichloroethene ug/kg ND 5.0 05/10/22 03:281.3
Trichlorofluoromethane ug/kg ND 5.0 05/10/22 03:282.8
Vinyl acetate ug/kg ND 50.0 05/10/22 03:283.6
Vinyl chloride ug/kg ND 10.0 05/10/22 03:282.5
Xylene (Total)ug/kg ND 10.0 05/10/22 03:282.8
1,2-Dichloroethane-d4 (S)%100 70-130 05/10/22 03:28
4-Bromofluorobenzene (S)%100 69-134 05/10/22 03:28
Toluene-d8 (S)%98 70-130 05/10/22 03:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3640006LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12201250 97 70-130
1,1,1-Trichloroethane ug/kg 12101250 97 70-130
1,1,2,2-Tetrachloroethane ug/kg 11901250 95 70-130
1,1,2-Trichloroethane ug/kg 12201250 98 70-130
1,1-Dichloroethane ug/kg 11901250 95 70-130
1,1-Dichloroethene ug/kg 13001250 104 70-130
1,1-Dichloropropene ug/kg 12401250 99 70-130
1,2,3-Trichlorobenzene ug/kg 11601250 93 65-130
1,2,3-Trichloropropane ug/kg 11901250 95 70-130
1,2,4-Trichlorobenzene ug/kg 11701250 94 68-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3640006LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11701250 94 70-130
1,2-Dibromo-3-chloropropane ug/kg 12201250 98 70-130
1,2-Dibromoethane (EDB)ug/kg 12801250 102 70-130
1,2-Dichlorobenzene ug/kg 11801250 95 70-130
1,2-Dichloroethane ug/kg 11701250 93 63-130
1,2-Dichloropropane ug/kg 11801250 94 70-130
1,3,5-Trimethylbenzene ug/kg 11801250 95 70-130
1,3-Dichlorobenzene ug/kg 11901250 95 70-130
1,3-Dichloropropane ug/kg 12201250 98 70-130
1,4-Dichlorobenzene ug/kg 11301250 90 70-130
2,2-Dichloropropane ug/kg 10901250 87 66-130
2-Butanone (MEK)ug/kg 24302500 97 70-130
2-Chlorotoluene ug/kg 11901250 95 70-130
2-Hexanone ug/kg 25002500 100 70-130
4-Chlorotoluene ug/kg 11601250 93 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 24502500 98 70-130
Acetone ug/kg 25102500 101 69-130
Benzene ug/kg 11101250 89 70-130
Bromobenzene ug/kg 12101250 97 70-130
Bromochloromethane ug/kg 13801250 110 70-130
Bromodichloromethane ug/kg 12101250 97 69-130
Bromoform ug/kg 12801250 103 70-130
Bromomethane ug/kg 1010 IK125081 52-130
Carbon tetrachloride ug/kg 11901250 95 70-130
Chlorobenzene ug/kg 11801250 95 70-130
Chloroethane ug/kg 12801250 102 65-130
Chloroform ug/kg 12201250 97 70-130
Chloromethane ug/kg 12801250 102 55-130
cis-1,2-Dichloroethene ug/kg 12201250 97 70-130
cis-1,3-Dichloropropene ug/kg 12501250 100 70-130
Dibromochloromethane ug/kg 12401250 99 70-130
Dibromomethane ug/kg 12801250 102 70-130
Dichlorodifluoromethane ug/kg 13201250 106 45-156
Diisopropyl ether ug/kg 11801250 94 70-130
Ethylbenzene ug/kg 11101250 88 70-130
Hexachloro-1,3-butadiene ug/kg 11301250 90 66-130
Isopropylbenzene (Cumene)ug/kg 11901250 95 70-130
m&p-Xylene ug/kg 23802500 95 70-130
Methyl-tert-butyl ether ug/kg 12401250 99 70-130
Methylene Chloride ug/kg 11801250 95 65-130
n-Butylbenzene ug/kg 11401250 91 67-130
n-Propylbenzene ug/kg 11701250 93 70-130
Naphthalene ug/kg 12701250 102 70-130
o-Xylene ug/kg 12001250 96 70-130
p-Isopropyltoluene ug/kg 11901250 95 67-130
sec-Butylbenzene ug/kg 11801250 94 69-130
Styrene ug/kg 12801250 102 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3640006LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12101250 97 67-130
Tetrachloroethene ug/kg 12201250 98 70-130
Toluene ug/kg 11301250 91 70-130
trans-1,2-Dichloroethene ug/kg 12501250 100 70-130
trans-1,3-Dichloropropene ug/kg 12301250 99 68-130
Trichloroethene ug/kg 11901250 95 70-130
Trichlorofluoromethane ug/kg 12201250 98 70-130
Vinyl acetate ug/kg 26302500 105 70-130
Vinyl chloride ug/kg 12301250 99 61-130
Xylene (Total)ug/kg 35803750 95 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%101 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3640007MATRIX SPIKE SAMPLE:
MSSpike
Result
92603482005
1,1,1,2-Tetrachloroethane ug/kg 534625 85 70-131ND
1,1,1-Trichloroethane ug/kg 519625 83 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 518625 83 66-130ND
1,1,2-Trichloroethane ug/kg 523625 84 66-133ND
1,1-Dichloroethane ug/kg 484625 77 65-130ND
1,1-Dichloroethene ug/kg 506625 81 10-158ND
1,1-Dichloropropene ug/kg 507625 81 68-133ND
1,2,3-Trichlorobenzene ug/kg 485625 78 27-138ND
1,2,3-Trichloropropane ug/kg 498625 80 67-130ND
1,2,4-Trichlorobenzene ug/kg 473625 76 51-134ND
1,2,4-Trimethylbenzene ug/kg 472625 75 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 444625 71 32-130ND
1,2-Dibromoethane (EDB)ug/kg 546625 87 70-130ND
1,2-Dichlorobenzene ug/kg 510625 82 69-130ND
1,2-Dichloroethane ug/kg 499625 80 59-130ND
1,2-Dichloropropane ug/kg 528625 84 70-130ND
1,3,5-Trimethylbenzene ug/kg 463625 74 65-137ND
1,3-Dichlorobenzene ug/kg 473625 76 70-130ND
1,3-Dichloropropane ug/kg 536625 86 70-130ND
1,4-Dichlorobenzene ug/kg 478625 76 68-130ND
2,2-Dichloropropane ug/kg 439625 70 32-130ND
2-Butanone (MEK)ug/kg 7641250 61 10-136ND
2-Chlorotoluene ug/kg 476625 76 69-141ND
2-Hexanone ug/kg 9131250 73 10-144ND
4-Chlorotoluene ug/kg 464625 74 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 9171250 73 25-143ND
Acetone ug/kg 6881250 55 10-130ND
Benzene ug/kg 521625 83 67-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3640007MATRIX SPIKE SAMPLE:
MSSpike
Result
92603482005
Bromobenzene ug/kg 507625 81 70-130ND
Bromochloromethane ug/kg 562625 90 69-134ND
Bromodichloromethane ug/kg 499625 80 64-130ND
Bromoform ug/kg 515625 82 62-130ND
Bromomethane ug/kg 246 IK62539 20-176ND
Carbon tetrachloride ug/kg 522625 83 65-140ND
Chlorobenzene ug/kg 518625 83 70-130ND
Chloroethane ug/kg 53.9 M16259 10-130ND
Chloroform ug/kg 496625 79 63-130ND
Chloromethane ug/kg 587625 94 58-130ND
cis-1,2-Dichloroethene ug/kg 504625 81 66-130ND
cis-1,3-Dichloropropene ug/kg 523625 84 67-130ND
Dibromochloromethane ug/kg 508625 81 67-130ND
Dibromomethane ug/kg 548625 88 63-131ND
Dichlorodifluoromethane ug/kg 558625 89 44-180ND
Diisopropyl ether ug/kg 485625 77 63-130ND
Ethylbenzene ug/kg 479625 77 66-130ND
Hexachloro-1,3-butadiene ug/kg 449625 72 64-150ND
Isopropylbenzene (Cumene)ug/kg 505625 81 69-135ND
m&p-Xylene ug/kg 9941250 79 60-133ND
Methyl-tert-butyl ether ug/kg 493625 79 65-130ND
Methylene Chloride ug/kg 431625 69 61-130ND
n-Butylbenzene ug/kg 409625 65 65-140ND
n-Propylbenzene ug/kg 449625 72 67-140ND
Naphthalene ug/kg 505625 81 15-145ND
o-Xylene ug/kg 513625 82 66-133ND
p-Isopropyltoluene ug/kg 465625 74 56-147ND
sec-Butylbenzene ug/kg 484625 77 65-139ND
Styrene ug/kg 523625 84 70-132ND
tert-Butylbenzene ug/kg 506625 81 62-135ND
Tetrachloroethene ug/kg 485625 78 70-135ND
Toluene ug/kg 503625 80 67-130ND
trans-1,2-Dichloroethene ug/kg 485625 78 69-130ND
trans-1,3-Dichloropropene ug/kg 507625 81 62-130ND
Trichloroethene ug/kg 531625 85 70-135ND
Trichlorofluoromethane ug/kg 98.2625 16 10-130ND
Vinyl acetate ug/kg 9511250 76 53-130ND
Vinyl chloride ug/kg 525625 84 61-148ND
Xylene (Total)ug/kg 15101880 80 63-132ND
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603521003
3640008SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND IK30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg 5.5J 306.0J
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg ND 306.4J
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603521003
3640008SAMPLE DUPLICATE:
m&p-Xylene ug/kg ND 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg 11.3 309.9J
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg ND 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg 11.3J 309.9J
1,2-Dichloroethane-d4 (S)%9795
4-Bromofluorobenzene (S)%101100
Toluene-d8 (S)%9898
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
698062
EPA 504.1
EPA 504.1
GCS 504 EDB DBCP
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3644972
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
1,2-Dibromo-3-chloropropane ug/L ND 0.050 05/13/22 15:090.0027
1,2-Dibromoethane (EDB)ug/L ND 0.020 05/13/22 15:090.0036
1-Chloro-2-bromopropane (S)%81 70-130 05/13/22 15:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3644973LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3644974
1,2-Dibromo-3-chloropropane ug/L 0.260.25 103 70-1301000.25 3 20
1,2-Dibromoethane (EDB)ug/L 0.230.25 91 70-130890.22 2 20
1-Chloro-2-bromopropane (S)%101 70-13092
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3644976MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92604185027
3644977
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dibromo-3-
chloropropane ug/L 0.26 100 65-135103 3 200.26ND 0.25 0.26
1,2-Dibromoethane (EDB) ug/L 0.26 89 65-13591 2 200.26ND 0.23 0.23
1-Chloro-2-bromopropane
(S)
%93 70-13095
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92604185026
3644975SAMPLE DUPLICATE:
1,2-Dibromo-3-chloropropane ug/L ND 20ND
1,2-Dibromoethane (EDB)ug/L ND 20ND
1-Chloro-2-bromopropane (S)%9794
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
696952
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3639633
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 5.0 05/10/22 09:321.7
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 05/10/22 09:321.2
2,4,6-Trichlorophenol ug/L ND 10.0 05/10/22 09:321.6
2,4-Dichlorophenol ug/L ND 5.0 05/10/22 09:321.4
2,4-Dimethylphenol ug/L ND 10.0 05/10/22 09:321.7
2,4-Dinitrophenol ug/L ND 50.0 05/10/22 09:3226.0
2,4-Dinitrotoluene ug/L ND 5.0 05/10/22 09:321.6
2,6-Dinitrotoluene ug/L ND 5.0 05/10/22 09:321.7
2-Chloronaphthalene ug/L ND 5.0 05/10/22 09:321.7
2-Chlorophenol ug/L ND 5.0 05/10/22 09:321.2
2-Nitrophenol ug/L ND 5.0 05/10/22 09:321.4
3,3'-Dichlorobenzidine ug/L ND 10.0 05/10/22 09:328.1
4,6-Dinitro-2-methylphenol ug/L ND 10.0 05/10/22 09:327.8
4-Bromophenylphenyl ether ug/L ND 5.0 05/10/22 09:321.8
4-Chloro-3-methylphenol ug/L ND 5.0 05/10/22 09:323.3
4-Chlorophenylphenyl ether ug/L ND 5.0 05/10/22 09:322.0
4-Nitrophenol ug/L ND 10.0 05/10/22 09:326.6
Acenaphthene ug/L ND 5.0 05/10/22 09:322.0
Acenaphthylene ug/L ND 5.0 05/10/22 09:322.0
Anthracene ug/L ND 5.0 05/10/22 09:322.3
Benzo(a)anthracene ug/L ND 5.0 05/10/22 09:322.7
Benzo(a)pyrene ug/L ND 5.0 05/10/22 09:322.8
Benzo(b)fluoranthene ug/L ND 5.0 05/10/22 09:322.6
Benzo(g,h,i)perylene ug/L ND 5.0 05/10/22 09:322.8
Benzo(k)fluoranthene ug/L ND 5.0 05/10/22 09:322.7
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/10/22 09:321.8
bis(2-Chloroethyl) ether ug/L ND 5.0 05/10/22 09:321.9
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 05/10/22 09:323.7
Butylbenzylphthalate ug/L ND 5.0 05/10/22 09:323.1
Chrysene ug/L ND 5.0 05/10/22 09:322.8
Di-n-butylphthalate ug/L ND 5.0 05/10/22 09:322.2
Di-n-octylphthalate ug/L ND 5.0 05/10/22 09:323.9
Dibenz(a,h)anthracene ug/L ND 5.0 05/10/22 09:323.0
Diethylphthalate ug/L ND 5.0 05/10/22 09:322.0
Dimethylphthalate ug/L ND 5.0 05/10/22 09:322.1
Fluoranthene ug/L ND 5.0 05/10/22 09:322.2
Fluorene ug/L ND 5.0 05/10/22 09:322.1
Hexachloro-1,3-butadiene ug/L ND 5.0 05/10/22 09:321.8
Hexachlorobenzene ug/L ND 5.0 05/10/22 09:322.2
Hexachlorocyclopentadiene ug/L ND 10.0 05/10/22 09:321.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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9800 Kincey Ave. Suite 100
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Page 44 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3639633
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
Hexachloroethane ug/L ND 5.0 05/10/22 09:321.4
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 05/10/22 09:322.9
Isophorone ug/L ND 10.0 05/10/22 09:321.7
N-Nitroso-di-n-propylamine ug/L ND 5.0 05/10/22 09:321.3
N-Nitrosodimethylamine ug/L ND 5.0 05/10/22 09:321.9
N-Nitrosodiphenylamine ug/L ND 10.0 05/10/22 09:323.0
Naphthalene ug/L ND 5.0 05/10/22 09:322.1
Nitrobenzene ug/L ND 5.0 05/10/22 09:321.9
Pentachlorophenol ug/L ND 10.0 05/10/22 09:323.8
Phenanthrene ug/L ND 5.0 05/10/22 09:322.0
Phenol ug/L ND 5.0 05/10/22 09:321.4
Pyrene ug/L ND 5.0 05/10/22 09:322.2
2,4,6-Tribromophenol (S)%64 10-137 05/10/22 09:32
2-Fluorobiphenyl (S)%57 15-120 05/10/22 09:32
2-Fluorophenol (S)%47 10-120 05/10/22 09:32
Nitrobenzene-d5 (S)%71 10-120 05/10/22 09:32
Phenol-d6 (S)%35 10-120 05/10/22 09:32
Terphenyl-d14 (S)%70 11-131 05/10/22 09:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3639634LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 38.650 77 44-142
2,2'-Oxybis(1-chloropropane)ug/L 40.250 80 36-166
2,4,6-Trichlorophenol ug/L 51.450 103 37-144
2,4-Dichlorophenol ug/L 49.950 100 1-191
2,4-Dimethylphenol ug/L 46.450 93 32-119
2,4-Dinitrophenol ug/L 323250 129 1-181
2,4-Dinitrotoluene ug/L 54.850 110 39-139
2,6-Dinitrotoluene ug/L 53.750 107 50-158
2-Chloronaphthalene ug/L 43.050 86 60-118
2-Chlorophenol ug/L 45.050 90 23-134
2-Nitrophenol ug/L 53.650 107 29-182
3,3'-Dichlorobenzidine ug/L 103100 103 1-262
4,6-Dinitro-2-methylphenol ug/L 124100 124 1-181
4-Bromophenylphenyl ether ug/L 47.950 96 53-127
4-Chloro-3-methylphenol ug/L 97.5100 97 22-147
4-Chlorophenylphenyl ether ug/L 47.850 96 25-158
4-Nitrophenol ug/L 160250 64 1-132
Acenaphthene ug/L 45.850 92 47-145
Acenaphthylene ug/L 46.650 93 33-145
Anthracene ug/L 43.850 88 1-166
Benzo(a)anthracene ug/L 49.150 98 33-143
Benzo(a)pyrene ug/L 51.450 103 17-163
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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Huntersville, NC 28078
[phone]
Page 45 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3639634LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 47.650 95 24-159
Benzo(g,h,i)perylene ug/L 47.550 95 1-219
Benzo(k)fluoranthene ug/L 49.550 99 11-162
bis(2-Chloroethoxy)methane ug/L 50.050 100 33-184
bis(2-Chloroethyl) ether ug/L 47.450 95 12-158
bis(2-Ethylhexyl)phthalate ug/L 50.350 101 8-158
Butylbenzylphthalate ug/L 49.450 99 1-152
Chrysene ug/L 46.650 93 17-168
Di-n-butylphthalate ug/L 51.150 102 1-118
Di-n-octylphthalate ug/L 53.850 108 4-146
Dibenz(a,h)anthracene ug/L 50.150 100 1-227
Diethylphthalate ug/L 50.450 101 1-114
Dimethylphthalate ug/L 49.250 98 1-112
Fluoranthene ug/L 50.850 102 26-137
Fluorene ug/L 48.850 98 59-121
Hexachloro-1,3-butadiene ug/L 34.450 69 24-116
Hexachlorobenzene ug/L 43.750 87 1-152
Hexachlorocyclopentadiene ug/L 38.550 77 25-150
Hexachloroethane ug/L 33.550 67 40-113
Indeno(1,2,3-cd)pyrene ug/L 49.250 98 1-171
Isophorone ug/L 47.550 95 21-196
N-Nitroso-di-n-propylamine ug/L 49.950 100 1-230
N-Nitrosodimethylamine ug/L 40.450 81 25-150
N-Nitrosodiphenylamine ug/L 46.950 94 25-150
Naphthalene ug/L 41.450 83 21-133
Nitrobenzene ug/L 49.350 99 35-180
Pentachlorophenol ug/L 97.5100 97 14-176
Phenanthrene ug/L 47.750 95 54-120
Phenol ug/L 31.350 63 5-112
Pyrene ug/L 46.050 92 52-115
2,4,6-Tribromophenol (S)%100 10-137
2-Fluorobiphenyl (S)%82 15-120
2-Fluorophenol (S)%68 10-120
Nitrobenzene-d5 (S)%98 10-120
Phenol-d6 (S)%56 10-120
Terphenyl-d14 (S)%90 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3639635MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92603059002
3639636
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 83.3 54 44-14255 2 3083.3ND 44.7 45.6
2,2'-Oxybis(1-
chloropropane)ug/L 83.3 92 36-16690 2 3083.3ND 76.7 74.9
2,4,6-Trichlorophenol ug/L 83.3 80 37-14482 2 3083.3ND 67.0 68.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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[phone]
Page 46 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3639635MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92603059002
3639636
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dichlorophenol ug/L 83.3 69 1-19172 4 3083.3ND 57.2 59.7
2,4-Dimethylphenol ug/L 83.3 78 32-11978 0 3083.3ND 65.1 64.8
2,4-Dinitrophenol ug/L 417 122 1-181119 2 30417ND507 495
2,4-Dinitrotoluene ug/L 83.3 121 39-139111 9 3083.3ND 101 92.1
2,6-Dinitrotoluene ug/L 83.3 83 50-15888 6 3083.3ND 69.3 73.5
2-Chloronaphthalene ug/L 83.3 62 60-11863 1 3083.3ND 52.0 52.6
2-Chlorophenol ug/L 83.3 60 23-13462 4 3083.3ND 49.6 51.8
2-Nitrophenol ug/L 83.3 79 29-18282 4 3083.3ND 66.1 68.5
3,3'-Dichlorobenzidine ug/L 167 79 1-26289 11 30167ND132 148
4,6-Dinitro-2-methylphenol ug/L 167 130 1-181141 8 30167ND217 236
4-Bromophenylphenyl ether ug/L 83.3 87 53-12795 9 3083.3ND 72.1 79.0
4-Chloro-3-methylphenol ug/L 167 65 22-14773 10 30167ND109 121
4-Chlorophenylphenyl ether ug/L 83.3 111 25-15891 20 3083.3ND 92.6 75.5
4-Nitrophenol ug/L 417 80 1-13271 12 30417ND333 295
Acenaphthene ug/L 83.3 74 47-14569 6 3083.3ND 61.3 57.9
Acenaphthylene ug/L 83.3 68 33-14567 0 3083.3ND 56.3 56.1
Anthracene ug/L 83.3 78 1-16685 8 3083.3ND 65.0 70.5
Benzo(a)anthracene ug/L 83.3 103 33-143103 0 3083.3ND 85.8 85.6
Benzo(a)pyrene ug/L 83.3 98 17-163102 4 3083.3ND 81.7 84.7
Benzo(b)fluoranthene ug/L 83.3 99 24-15997 2 3083.3ND 82.6 81.1
Benzo(g,h,i)perylene ug/L 83.3 97 1-21996 1 3083.3ND 81.2 80.3
Benzo(k)fluoranthene ug/L 83.3 95 11-16292 3 3083.3ND 79.1 76.5
bis(2-
Chloroethoxy)methane ug/L 83.3 71 33-18471 1 3083.3ND 59.2 58.8
bis(2-Chloroethyl) ether ug/L 83.3 67 12-15868 3 3083.3ND 55.4 56.9
bis(2-Ethylhexyl)phthalate ug/L 83.3 105 8-158109 4 3083.3ND 88.3 91.9
Butylbenzylphthalate ug/L 83.3 119 1-152120 1 3083.3ND 99.2 100
Chrysene ug/L 83.3 89 17-16891 2 3083.3ND 74.1 75.8
Di-n-butylphthalate ug/L 83.3 93 1-118101 8 3083.3ND 77.3 84.0
Di-n-octylphthalate ug/L 83.3 107 4-146111 3 3083.3ND 89.2 92.2
Dibenz(a,h)anthracene ug/L 83.3 96 1-22795 2 3083.3ND 80.4 78.8
Diethylphthalate ug/L M183.3 118 1-114105 12 3083.3ND 98.2 87.2
Dimethylphthalate ug/L 83.3 74 1-11278 6 3083.3ND 61.7 65.3
Fluoranthene ug/L 83.3 89 26-13795 6 3083.3ND 74.4 78.8
Fluorene ug/L 83.3 106 59-12194 13 3083.3ND 88.4 78.0
Hexachloro-1,3-butadiene ug/L 83.3 50 24-11648 3 3083.3ND 41.5 40.4
Hexachlorobenzene ug/L 83.3 81 1-15289 8 3083.3ND 67.9 73.9
Hexachlorocyclopentadiene ug/L 83.3 60 25-15053 13 3083.3ND 50.2 43.9
Hexachloroethane ug/L 83.3 45 40-11345 0 3083.3ND 37.4 37.5
Indeno(1,2,3-cd)pyrene ug/L 83.3 101 1-17198 3 3083.3ND 84.5 81.7
Isophorone ug/L 83.3 74 21-19673 1 3083.3ND 61.7 61.1
N-Nitroso-di-n-propylamine ug/L 83.3 79 1-23079 0 3083.3ND 65.9 65.8
N-Nitrosodimethylamine ug/L 83.3 58 25-15062 7 3083.3ND 48.7 52.1
N-Nitrosodiphenylamine ug/L 83.3 81 25-15087 7 3083.3ND 67.3 72.1
Naphthalene ug/L 83.3 57 21-13358 3 3083.3ND 47.1 48.6
Nitrobenzene ug/L 83.3 74 35-18076 2 3083.3ND 62.0 63.2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3639635MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92603059002
3639636
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/L 167 108 14-176116 7 30167ND179 193
Phenanthrene ug/L 83.3 86 54-12095 10 3083.3ND 71.7 79.1
Phenol ug/L 83.3 39 5-11241 3 3083.3ND 32.6 33.8
Pyrene ug/L M183.3 116 52-115112 4 3083.3ND 96.9 93.0
2,4,6-Tribromophenol (S) %99 10-137104
2-Fluorobiphenyl (S)%61 15-12057
2-Fluorophenol (S)%42 10-12044
Nitrobenzene-d5 (S)%73 10-12071
Phenol-d6 (S)%37 10-12036
Terphenyl-d14 (S)%106 11-131103
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
697972
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521001, 92603521002, 92603521003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3644633
Associated Lab Samples:92603521001, 92603521002, 92603521003
Matrix: Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 5.0 05/13/22 20:193.6
n-Pentacosane (S)%89 10-130 05/13/22 20:19
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3644634LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 47.466.4 71 44-130
n-Pentacosane (S)%82 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3644636MATRIX SPIKE SAMPLE:
MSSpike
Result
92603521002
Diesel Range Organics(C10-C28)mg/kg 63.881.9 74 10-130ND
n-Pentacosane (S)%93 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603521001
3644635SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg ND 30ND
n-Pentacosane (S)%9588
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
698034
EPA 3546
EPA 8015C
8015 Solid GCSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521004, 92603521005, 92603521006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3644787
Associated Lab Samples:92603521004, 92603521005, 92603521006
Matrix: Solid
AnalyzedMDL
Diesel Range Organics(C10-C28)mg/kg ND 4.9 05/13/22 18:573.5
n-Pentacosane (S)%89 10-130 05/13/22 18:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3644788LABORATORY CONTROL SAMPLE:
LCSSpike
Diesel Range Organics(C10-C28)mg/kg 50.267.3 75 44-130
n-Pentacosane (S)%80 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3644789MATRIX SPIKE SAMPLE:
MSSpike
Result
92603521004
Diesel Range Organics(C10-C28)mg/kg 57.478.6 71 10-130ND
n-Pentacosane (S)%76 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92604320001
3644790SAMPLE DUPLICATE:
Diesel Range Organics(C10-C28)mg/kg 32600 8 3035400
n-Pentacosane (S)%0 S40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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[phone]
Page 50 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
698494
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3646880
Associated Lab Samples:92603521007
Matrix: Water
AnalyzedMDL
Aliphatic (C09-C18)ug/L 133 100 N205/17/22 17:15100
Aliphatic (C19-C36)ug/L 376 100 N205/17/22 17:15100
Aromatic (C11-C22)ug/L 683 100 N205/17/22 17:15100
1-Chlorooctadecane (S)%104 40-140 05/17/22 17:15
2-Bromonaphthalene (S)%85 40-140 05/17/22 17:15
2-Fluorobiphenyl (S)%72 40-140 05/17/22 17:15
o-Terphenyl (S)%91 40-140 05/17/22 17:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3646881LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3646882
Aliphatic (C09-C18)ug/L 148 N23004940-14047140 5 50
Aliphatic (C19-C36)ug/L 368 N24009240-14083332 11 50
Aromatic (C11-C22)ug/L 664 N28507840-14059501 28 50
1-Chlorooctadecane (S)%95 40-14098
2-Bromonaphthalene (S)%85 40-14051
2-Fluorobiphenyl (S)%75 40-14042
o-Terphenyl (S)%99 40-14072
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 57
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92603521
MUSA 6760
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
696988
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92603521001, 92603521002, 92603521003, 92603521004, 92603521005, 92603521006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603537001
3639918SAMPLE DUPLICATE:
Percent Moisture %25.9 N212525.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92603540003
3639919SAMPLE DUPLICATE:
Percent Moisture %71.5 N202571.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
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Huntersville, NC 28078
[phone]
Page 52 of 57
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92603521
MUSA 6760
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte detected in associated method blank due to extraction error.1g
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.MS
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 57
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92603521
MUSA 6760
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92603521007 698062 698144SB-1 EPA 504.1 EPA 504.1
92603521001 697972 698201SB-1 (2-4')EPA 3546 EPA 8015C
92603521002 697972 698201SB-2 (4-6')EPA 3546 EPA 8015C
92603521003 697972 698201SB-3 (4-6')EPA 3546 EPA 8015C
92603521004 698034 698200SB-4 (4-6')EPA 3546 EPA 8015C
92603521005 698034 698200SB-5 (4-6')EPA 3546 EPA 8015C
92603521006 698034 698200SB-6 (4-6')EPA 3546 EPA 8015C
92603521007 698494 698789SB-1 MADEP EPH MADEP EPH
92603521001 697858 697885SB-1 (2-4')EPA 5030B EPA 8015C
92603521002 697858 697885SB-2 (4-6')EPA 5030B EPA 8015C
92603521003 697858 697885SB-3 (4-6')EPA 5030B EPA 8015C
92603521004 697858 697885SB-4 (4-6')EPA 5030B EPA 8015C
92603521005 697858 697885SB-5 (4-6')EPA 5030B EPA 8015C
92603521006 697858 697885SB-6 (4-6')EPA 5030B EPA 8015C
92603521007 698185SB-1 MADEP VPH
92603521007 700699 700811SB-1 EPA 3005A EPA 6020B
92603521007 696952 697086SB-1 EPA 625.1 EPA 625.1
92603521007 697129SB-1 SM 6200B
92603521001 696975 697121SB-1 (2-4')EPA 5035A/5030B EPA 8260D
92603521002 696975 697121SB-2 (4-6')EPA 5035A/5030B EPA 8260D
92603521003 697025 697120SB-3 (4-6')EPA 5035A/5030B EPA 8260D
92603521004 697025 697120SB-4 (4-6')EPA 5035A/5030B EPA 8260D
92603521005 697025 697120SB-5 (4-6')EPA 5035A/5030B EPA 8260D
92603521006 697025 697120SB-6 (4-6')EPA 5035A/5030B EPA 8260D
92603521001 696988SB-1 (2-4')SW-846
92603521002 696988SB-2 (4-6')SW-846
92603521003 696988SB-3 (4-6')SW-846
92603521004 696988SB-4 (4-6')SW-846
92603521005 696988SB-5 (4-6')SW-846
92603521006 696988SB-6 (4-6')SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/31/2022 12:10 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 57
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