FA-8065_42273_CA_MRP_20230330

GROUNDWATER MONITORING REPORT

IN AND OUT CONVENIENCE
226 SOUTH NC HWY 705
ROBBINS, MOORE COUNTY, NORTH CAROLINA

PREPARED FOR:
MR. DAVID CHEEK
BIG CEDAR CREEK PROPERTIES, LLC
605 GEORGE P ROAD
ROBBINS, NORTH CAROLINA 27325

PREPARED BY:
PILOT GEOLOGICAL, PLLC
PO BOX 128
KERNERSVILLE, NORTH CAROLINA 27285

MARCH 30, 2023
PILOT PROJECT NO. G-5624.8

SITE INFORMATION

Site Name and Location In and Out
226 South NC Highway 705
Robbins, North Carolina

Incident No. 42273

Facility ID: 00-0-0000028988

Latitude and Longitude: 35 25’ 55.88”N; 79 35’ 07.33”W

Land Use Category: Commercial
Contacts
Owner of UST: Mr. David Cheek
Big Cedar Creek Properties, LLC
605 George P Road
Robbins, North Carolina 27325
[phone]

Primary Contact: Mr. David Cheek
Big Cedar Creek Properties, LLC
[phone]

Consultant: Pilot Geological, PLLC
PO Box 128
Kernersville, North Carolina 27285
[phone]

Laboratory: Pace Analytical
1377 South Park Drive
Kernersville, North Carolina 27284
[phone]
Laboratory I.D. # Various

Release Information: Laboratory analysis of soil samples collected on April 7, 2020 during closure activities
of three 8,000-gallon commercial gasoline USTs detected petroleum compounds above the North Carolina
Action Levels. The estimated quantity of the release is unknown. Free product was not observed during
the removal activities.

Table of Contents
1.0 SITE HISTORY ................................................................................................................... 1
1.1 UST Information ......................................................................................................................................... 2
2.0 SITE GEOLOGY AND HYDROGEOLOGY ............................................................................... 3
3.0 FIELD ACTIVITIES .............................................................................................................. 3
3.1 Monitoring Well Sampling .......................................................................................................................... 4
3.2 Water Supply Wells .................................................................................................................................... 4
3.3 Groundwater Modeling .............................................................................................................................. 4
3.4 Free Product Investigation and Recovery ................................................................................................... 4
4.0 LABORATORY ANALYTICAL RESULTS ................................................................................. 4
4.1 Groundwater Sample Analysis .................................................................................................................... 4
5.0 CONCLUSIONS ................................................................................................................. 5
6.0 RECOMMENDATIONS ....................................................................................................... 6
7.0 QUALIFICATIONS OF REPORT ........................................................................................... 6
8.0 STATEMENTS AND CERTIFICATIONS ................................................................................. 6

DRAWINGS

Drawing 1 USGS Topographic Map
Drawing 2 Site Map
Drawing 3 UST Location Map
Drawing 4 Monitoring Well Location Map
Drawing 5 Potentiometric Surface Map
Drawing 6 Receptor Survey Map
Drawing 7 Benzene Isoconcentration Map
Drawing 8 MTBE Isoconcentration Map
Drawing 9 Naphthalene Isoconcentration Map
Drawing 10 Toluene Isoconcentration Map
Drawing 11 1,2,4-Trimethylbenzene Isoconcentration Map
Drawing 12 Xylenes Isoconcentration Map

TABLE OF CONTENTS
(continued)
TABLES

Table 1 UST Information
Table 2 Monitoring Well Construction Information
Table 3 Water Supply Well Information
Table 4 Summary of Groundwater Analytical Results

APPENDICIES

Appendix A Groundwater Concentration Graphs and Monitoring Well Sampling
Sheets
Appendix B Laboratory Data Sheets and Chain of Custody Record
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Pilot Project G-5624.8
March 30, 2023
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1.0 SITE HISTORY

The site is located at 226 South NC Highway 705 in Robbins, Moore County, North Carolina
(Drawings 1 and 2). The site is occupied by the In and Out convenience store. Pilot completed an
Initial Abatement Action Report, dated May 22, 2020. A release was identified in the vicinity of the
former underground storage tank system (UST). Impacted soil above the North Carolina Soil-to-
Groundwater Maximum Soil Contaminant Concentrations (MSCCs) was identified in the vicinity of
the UST system. The North Carolina Department of Environmental Quality (NCDEQ) issued a Notice
of Regulatory Requirements (NORR) dated May 14, 2020 requesting that a Limited Site Assessment
(LSA) be completed. One inactive water supply well was identified approximately 330 feet to the
south of the site. The former USTs were located on an adjacent property to the north at 200 South
NC Highway 705. It is Pilot’s understanding that a legal easement is associated with the adjacent
property to the north where the USTs were located. The property located at 200 South NC Highway
705 formerly contained a NAPA auto parts store and an automotive service facility. An active gas
station is located northwest and adjacent to the 200 South NC Highway 705.

Pilot completed a LSA dated June 15, 2020. Based on the findings of the LSA, the NCDEQ issued
a NORR dated June 26, 2020 requiring that an Additional Risk Assessment Report (AAR) be
completed. A property transaction occurred subsequent to the completion of the LSA and a Notice
of Residual Petroleum (NORP) was filed.

Pilot completed an ARA dated August 26, 2020. Based on the findings of the ARA, the NCDEQ
issued a NORR dated October 8, 2020 requiring that a Comprehensive Site Assessment (CSA) be
completed. The ARA assessment indicated that the extent of the impacted soil has been
reasonably defined, but the extent of impacted groundwater had not. The detected
concentrations of benzene exceeded its Gross Contaminant Level (GCL) in monitoring wells MW-
1, MW-3 and MW-4.

Pilot completed a CSA dated March 22, 2021. Based on the findings of the CSA, laboratory
analysis of groundwater samples MW-5, MW-6 and MW-7 detected several targeted compounds
above their respective 2L Standards, but below their respective GCLs.

Pilot completed a Groundwater Monitoring Report for the site dated December 27, 2022. On
December 1, 2022, Pilot collected groundwater samples from existing monitoring wells MW-1,
MW-2, MW-4, MW-5, MW-6, MW-7 and DW-1. Monitoring well MW-3 was not sampled based
on approximately 0.31 feet of free-product being measured in the well. Laboratory analysis of
the groundwater samples collected from monitoring well MW-2 did not detect targeted
compounds above their respective 2L Standards. Laboratory analysis of the groundwater
samples collected from monitoring wells MW-1, MW-4, MW-5, MW-6, MW-7 and DW-1 detected
targeted compounds above their respective 2L Standards, with the concentration of benzene
exceeding its GCL in the samples collected from monitoring wells MW-1 and DW-1.

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Pilot conducted an Aggressive Fluid Vapor Recovery (AFVR) event in accordance with the NCDEQ
letter dated February 21, 2022. The field activities were completed by Pilot and EVO Corporation
on May 27, 2022. A total of 25 gallons of liquids were extracted from monitoring wells MW-1
and MW-3 during the AFVR event with approximately 1 gallon of which appeared to be free phase
petroleum product. Based on the data collected and calculations, approximately 47.56 pounds
of total VOC emissions were generated during the AFVR event. Approximately 8.67 gallons of
gasoline were calculated to be removed as liquid and emissions during the AFVR event.

Pilot completed a Groundwater Monitoring Report for the site dated August 22, 2022. On August
11, 2022, Pilot collected groundwater samples from existing monitoring wells MW-1, MW-2,
MW-4, MW-5, MW-6, MW-7 and DW-1. Monitoring well MW-3 was not sampled based on
approximately 0.46 feet of free-product being measured in the well. Laboratory analysis of the
groundwater samples collected from monitoring well MW-2 did not detect targeted compounds
above the 2L Standards. Laboratory analysis of the groundwater samples collected from
monitoring wells MW-1, MW-4, MW-5, MW-6, MW-7 and DW-1 detected several targeted
compounds above their respective 2L Standards, with the concentration of benzene exceeding
its GCL in the samples collected from monitoring wells MW-1 and DW-1.

Based on the presence of free product in monitoring well MW-3, the NCDEQ requested that a
free product recovery event be completed as documented in a letter dated October 21, 2022.

Pilot conducted a second AFVR event in accordance with the NCDEQ letter dated October 21,
2022. The field activities were completed by Pilot and EVO Corporation on November 10, 2022.
Monitoring wells MW-1, MW-3 and MW-4 (Drawing 4) were utilized as extraction points during
the AFVR event. A total of 45 gallons of liquids were extracted from monitoring wells MW-1, MW-
3 and MW-4 during the AFVR event with approximately 1 gallon of which appeared to be free
phase petroleum product. Based on the data collected and calculations, approximately 562.49
pounds of total VOC emissions were generated during the AFVR event. Approximately 90.85
gallons of gasoline were calculated to be removed as liquid and emissions during the AFVR event.

Project information is based on correspondence between NCDEQ personnel, Big Cedar Creek
Properties, LLC and Pilot, and the previously completed activities.

1.1 UST Information

A suspected release was identified during the removal of three 8,000-gallon gasoline USTs
(Drawing 3) on April 6 through 8, 2020. Laboratory analysis of soil samples confirmed the release
as well as on-site analysis by Red Lab, LLC (Red Lab) on April 9, 2020. Based on field observations
indicating a release beneath the USTs, approximately 169.86 tons of petroleum impacted soil was
excavated and transported to Earthtec of NC, Inc. (Earthtec) in Sanford, North Carolina for
disposal. UST information is summarized in Table 1.

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2.0 SITE GEOLOGY AND HYDROGEOLOGY

The United States Geological Survey (USGS) Topographic Map, Robbins, North Carolina
Quadrangles depicts a structure on the adjacent property north of the site. Elevations on the site
range from approximately 462 feet above mean sea level on the northwestern portion of the site
to approximately 460 feet above mean sea level on the southern portion of the site. Buck Branch
is depicted approximately 1,500 feet northeast of the site. Based on the review of the USGS
topographic map and observations of the general area and site topography, surface run-off
would be expected to flow generally to the northeast across the site.

The subject site is located within the Piedmont Physiographic Province. The Piedmont
Physiographic Province generally consists of hills and ridges which are dissected by a system of
swales and streams. The Piedmont Physiographic Province is predominantly underlain by
metamorphic rock (formed by heat, pressure and/or chemical action) and igneous rock (formed
directly from molten material). The topography and relief of the Piedmont Province has
developed from differential weathering of the igneous and metamorphic rock. Ridges and hills
have been developed in areas of less weathered rock. Because of the continued chemical and
physical weathering, rock in the Piedmont Physiographic Province is generally covered with a
mantle of soil that has weathered in place from the parent bedrock. These soils vary in thickness
and are referred to as residuum or residual soils. The residuum is typically finer grained and has
higher clay content near the surface because of the advanced weathering. Similarly, the soils
typically become coarser grained with increasing depth because of decreased weathering. As the
weathering decreases, the residual soils generally retain the overall appearance, texture and
foliations of the parent rock.

In general, groundwater movement in the Piedmont Physiographic Province is from higher to
lower elevations. As such, the presumed direction of groundwater flow is generally to the
northeast across the site. Based on the presumed groundwater flow direction, areas to the south
are potentially up-gradient of the site.

Soils at the site consist of sandy clay from the ground surface to approximately twelve feet bgs.
Saprolite was encountered at depths greater than 10 feet bgs. Partially weathered rock and
bedrock was encountered at approximately 18 feet bgs or greater.

3.0 FIELD ACTIVITIES

The field activities were completed by Pilot on March 14, 2023. The field activities consisted of
collecting groundwater samples from existing monitoring wells MW-1, MW-2, MW-3, MW-4,
MW-5, MW-6 and DW-1 (Drawing 4). Monitoring well MW-7 was not accessible due to a disabled
vehicle being parked over the well. Pilot personnel attempted to find the owner of the vehicle
but were unsuccessful.

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3.1 Monitoring Well Sampling

With the exception of monitoring well MW-7, a groundwater sample was collected from the
existing monitoring wells using a disposable bailer and new length of nylon string or pump and
decontaminated length of polyethylene tubing. Prior to sampling, approximately three well
volumes were purged from the monitoring wells. The monitoring wells were purged to remove
silt and sediment from the groundwater and collect a representative sample of groundwater.
After the purging was completed, groundwater samples were collected in the sample containers
provided by the laboratory. Pilot personnel wore a new pair of disposable nitrile gloves during
purging and sampling. Each container was labeled and placed in a cooler containing ice to
maintain the samples at approximately 4 Celsius. The samples were then transported to Pace
Analytical (Pace) for chemical analysis. The groundwater samples collected were analyzed for
volatile organic compounds (VOCs) using Standard Method 6200B plus oxygenates. A chain of
custody was maintained and is included in Appendix B. Isoconcentration maps for the
compounds that exceed their respective 2L Standard are included as Drawings 7 through 12,
respectively. A potentiometric surface map is included as Drawing 5. Copies of the Monitoring
Well Sampling Sheets are included in Appendix A.

3.2 Water Supply Wells

Based on the information in the previous reports one inactive water supply well is located
approximately 330 feet south of the source area of the release. Information pertaining to the
water supply wells is provided in Table 3 and Drawing 6.

3.3 Groundwater Modeling

Groundwater modeling was not completed based on a surface water featuring not being
identified within 500 feet of the source area of the release.

3.4 Free Product Investigation and Recovery

Two AFVRs were previously completed at the site as summarized in Section 1.0. Free product
was not observed in the monitoring wells during this sampling event.

4.0 LABORATORY ANALYTICAL RESULTS

4.1 Groundwater Sample Analysis

Laboratory analysis of the groundwater sample collected from monitoring well MW-2 did not
detect targeted compounds above the laboratory detection limits. Laboratory analysis of the
groundwater samples collected from monitoring wells MW-1, MW-3, MW-4, MW-5, MW-6 and
DW-1 detected targeted compounds above their respective 2L Standards, with the concentration
of benzene exceeding its GCL in the samples collected from monitoring wells MW-1 and DW-1.
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A summary of the groundwater analytical results is presented in Table 4. Groundwater
concentration graphs are included in Appendix A for monitoring wells MW-1, MW-3 and DW-1.
The laboratory data sheets are included in Appendix B.

5.0 CONCLUSIONS

Based on the activities, Pilot concludes the following:

 Monitoring well MW-7 was not accessible due to a disabled vehicle being parked over the well.
Pilot personnel attempted to find the owner of the vehicle but were unsuccessful.

 Laboratory analysis of the groundwater sample collected from monitoring well MW-2 did not
detect targeted compounds above the laboratory detection limits. Laboratory analysis of the
groundwater samples collected from monitoring wells MW-1, MW-3, MW-4, MW-5, MW-6
and DW-1 detected targeted compounds above their respective 2L Standards, with the
concentration of benzene exceeding its GCL in the samples collected from monitoring wells
MW-1 and DW-1.

 The groundwater flow was calculated to be to be generally to the north.

 The majority of the plume of impacted groundwater appears to be confined to the site.

 One inactive water supply well was previously identified within 1,000 feet of the source area
of the release. Municipal water is available in the surrounding area; therefore, the
concentrations in the groundwater will need to decrease to below the GCLs to qualify for
incident closure with the previously filed Notice of Residual Petroleum (NORP).

 It appears that the two AFVR events have been successful at removing the detected free
product in monitoring well MW-3 as well as aiding in the decrease of the dissolved phase
concentrations. The concentrations detected in the monitoring wells overall are exhibiting a
decreasing trend. The concentrations of benzene detected in monitoring wells MW-1 and DW-
1 are nearing its GCL. The concentrations detected in monitoring well MW-1 have fluctuated,
which may be the result of fluctuations in the water table as well as the movement of
groundwater being affected by the AFVR events.

 Based on the findings and removal of the UST system and a portion of the secondary source,
it is anticipated that natural attenuation will occur. It may be beneficial to complete a limited
number of additional impacted groundwater removal activities via AFVR or MMPE to aid in
decreasing the dissolved phase concentrations and expediting natural attenuation. It is Pilot’s
opinion that monitored natural attenuation activities should continue. Based on the removal
of free product, the overall decreasing trend in the dissolved phase concentrations, and the
intermediate ranking of the site, it does not appear that substantial corrective actions are
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warranted at this time.
6.0 RECOMMENDATIONS

Pilot recommends that the current property owner/responsible party submit a copy of this
Groundwater Monitoring Report to the NCDEQ, UST Section for their review.

7.0 QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in assessment projects of this type. Our evaluation of site conditions has
been based on our understanding of the site project information and the data obtained during
our field activities.

8.0 STATEMENTS AND CERTIFICATIONS

1 Enter the date the monitoring report was due. Not Established Will this report be
submitted after the established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
3 If applicable, will any of the proposed attenuation milestones under the schedule
approved in the Corrective Action Plan not be met? (within a reasonable margin of
error)
YES NO
N/A
4 Does any known or suspected source zone soil contamination or free product remain
outside of the assessed area that could be inhibiting natural attenuation?
YES NO
5 Has there been an unexpected increase in contaminant mass sufficient to suggest a
potential new release from a separate onsite or offsite source?
YES NO

Certification:
I, Jason T. Ricks, a Licensed Geologist for Pilot Geological, PLLC, do certify that the information
contained in this report is correct and accurate to the best of my knowledge.

Pilot Geological, PLLC is licensed to practice geology in North Carolina. The certification number of
the company is C-542.

DRAWINGS
SITE
USGS Topographic Map
226 South NC HWY 705
Robbins, Moore County, NC
Pilot Project G-5624.8
Drawing 1
USGS Topographic Map
Robbins, NC Quadrangle
Scale: 1” = 2,000’
LEGEND
Site Boundary
Site Map
226 South NC HWY 705
Robbins, Moore County, NC
Pilot Project G-5624.8
Drawing 2
Google Earth
Interactive Mapping Software
Scale : 1”= 60’
LEGEND
Site BoundaryU. UST SystemA. AST SystemG. Gas Station
U
A
G
UST Location Map
226 South NC HWY 705
Robbins, Moore County, NC
Pilot Project G-5624.8
Drawing 3
Google Earth
Interactive Mapping Software
Scale : 1”= 10’
LEGEND
Approximate Monitoring Well Location
Approximate Former UST Location
Approximate Extent
of the Impacted Soil
Excavation
MW-1
MW-4
MW-2
MW-3
DW-1
Receptor Survey Map
226 South NC HWY 705
Robbins, Moore County, NC
Pilot Project G-5624.8
Drawing 6
Google Earth
Interactive Mapping Software
Scale : 1”= 300’
LEGEND
Site Boundary
Approximate Inactive Water Supply Well Location
1
500’
1,000’

TABLES
UST ID
Number Owner Last Contents Previous
Contents
Capacity
(in Gallons)
Construction
Details Tank Dimensions Installation
Date Status Release
Table 1 - UST Information
In and Out
Robbins, North Carolina
1
Big Cedar Creek Properties, LLC
605 George P Road
Robbins, North Carolina 27325
Gasoline Gasoline 8,000 Single Wall Steel 96" x 255" 5/1/1982 Removed Yes
2 Gasoline Gasoline 8,000 Single Wall Steel 96" x 255" 5/1/1982
Yes
Removed Yes
96" x 255" 5/1/1982 Removed3 Gasoline Gasoline 8,000 Single Wall Steel
Monitoring Well
ID Date Installed TOC Elevation (feet)
Static Water Level
(feet below TOC)
3/14/23
Relative Groundwater
Elevation Total Depth Screened Interval
(feet)
Sand
Interval
Bentonite
Interval
*MW-1 5/26/2020 100.00 19.85 80.15 35 15-35 13-35 4-13
MW-2 8/6/2020 99.32 19.72 79.60 35 15-35 13-35 11-13
**MW-3 8/5/2020 97.63 18.09 79.54 35 15-35 13-35 11-13
MW-4 8/5/2020 96.40 18.78 77.62 35 15-35 13-35 11-13
MW-5 2/8/2021 97.71 7.87 89.84 30 10-30 8-30 6-8
MW-6 2/8/2021 97.14 22.00 75.14 30 15-30 13-30 11-13
MW-7 2/8/2021 95.76 NS NS 30 10-30 8-30 6-8
DW-1 8/5-6/2021 98.91 21.7 77.21 55 50-55 48-55 46-48
Table 2 - Monitoring Well Construction Information
In and Out
Robbins, North Carolina
*MW-1 was utilized as an arbitrary benchmark
**If free product is present the groundwater elevation is calculated by (TOC Elevation - Static) + (free product thickness x 0.8581)
Well ID
Number Owner Information Property Address Well Depth (feet) Well Use
Approximate Distance from
the Source Area
Is the Property Connected to
Municipal Water
See Drawing 6
240 South NC 705 HWY 340 Inactive 330
Table 3 - Water Supply Well Information
In and Out
Robbins, North Carolina
1 Yes
Coin Wash, Inc.
18674 NC Hwy 902
Bear Creek, NC 27207
504.1
Sample ID
Approximate
Water Level (ft.
BGS)
Groundwater
Elevation (ft.)
Sample
Collection
Date Benzenen-ButylbenzeneEthylbenzeneIsopropylether (IPE, Diisopropyl ether)I-Propylbenzene (Isopropylbenzene)Methylene ChlorideMTBENaphthaleneN-Propylbenzenep-IsopropyltolueneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesTert-amyl AlcoholTert-Butyl AlcoholEDBLeadC5-C8 AliphaticsC9-C12 AliphaticsC9-C10 Aromatics17.15 83.62 5/28/2020 6,140 BQL 2,050 124 92.8 BQL 444 220 234 22.0 21,300 1,720 401 11,680 3,150 ND BQL BQL 56,200 44,700 9,230
20.70 79.30 12/1/2021 9,970 ND 2,310 144 ND ND ND ND 311 ND 29,500 1,680 350 12,090 ND ND NA NA NA NA NA
20.53 79.47 8/11/2022 8,610 ND 2,560 ND 127 ND ND ND 311 ND 26,200 2,340 501 14,710 NA NA NA NA NA NA NA
19.85 80.15 3/14/2023 7,390 ND 3,280 ND 151 ND ND 647 490 ND 31,300 3,700 839 18,040 ND ND NA NA NA NA NA
24.91 74.41 8/7/2020 35.1 BQL 39.4 BQL BQL BQL BQL 12.9 9.34 1.06 111 61.4 20.1 295 NA ND BQL 9.02 509 595 1,620
20.06 79.26 12/1/2021 0.62 ND 0.57 ND ND ND ND ND ND ND 0.99 1.3 0.61 5.0 ND ND NA NA NA NA NA
20.80 78.52 8/11/2022 ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA
19.72 79.60 3/14/2023 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA
22.45 75.18 8/7/2020 10,200 BQL 2,840 208 3.97 BQL BQL 352 268 BQL 37,900 2,080 465 15,000 NA BQL 6.23 156,000 61,800 11,800
19.93 77.97 12/1/2021
20.11 77.91 8/11/2022
18.09 79.54 3/14/2023 4,500 ND 2,690 ND 125 ND ND 690 371 ND 25,600 3,180 769 16,220 ND ND NA NA NA NA NA
27.65 68.75 8/7/2020 7,380 BQL 2,020 180 BQL BQL BQL 252 192 BQL 27,500 1,670 342 11,900 NA ND BQL BQL 115,000 45,800 9,100
20.04 76.36 12/1/2021 3,460 ND 416 57.5 41.0 ND 176 122 61.3 ND 846 718 159 2,158 ND ND NA NA NA NA NA
19.22 77.18 8/11/2022 3,300 ND 748 44.6 49.3 ND 161 246 82.4 ND 2,210 884 197 4,740 NA NA NA NA NA NA NA
18.78 77.62 3/14/2023 265 ND 1,720 ND 118 ND ND 303 350 ND 8,570 2,610 618 10,050 ND ND NA NA NA NA NA
6.99 90.72 2/9/2021 0.53 ND ND ND ND ND 0.57 ND ND ND 1.4 0.54 ND ND ND ND ND 30.7 ND ND ND
12.93 84.78 12/1/2021 3.2 ND ND ND ND ND 4.1 ND ND ND 1.4 0.81 ND ND ND ND NA NA NA NA NA
11.31 86.40 8/11/2022 1.2 ND ND ND ND ND 2.8 2.5 ND ND 1.4 0.64 ND ND NA NA NA NA NA NA NA
7.87 89.84 3/14/2023 2.4 ND ND ND ND ND 4.5 ND ND ND 1.8 ND ND ND ND ND NA NA NA NA NA
15.02 82.12 2/9/2021 62.6 ND 22.7 ND ND ND 23.8 32.8 ND ND 221 18.5 ND 122.1 ND ND ND 488 982 557 152
21.53 75.61 12/1/2021 92.6 2.1 55.6 2.2 4.5 ND 48.3 39.1 9.5 ND 200 74.8 16.6 206 ND ND NA NA NA NA NA
17.75 79.39 8/11/2022 28.9 ND 29.4 ND 4.1 ND 23.1 16.3 9.7 ND 64.1 57.7 13.6 111.8 NA NA NA NA NA NA NA
22.00 75.14 3/14/2023 45.8 ND 38.6 ND 4.5 ND 24.5 11.0 ND ND 92.7 34.9 ND 173.5 ND ND NA NA NA NA NA
29.29 66.47 2/9/2021 1,080 ND 440 ND ND ND 42.1 133 ND ND 4,220 243 ND 2,639 ND ND ND ND 17,700 11,000 ND
20.46 75.30 12/1/2021 1,160 ND 380 16.5 29.9 ND 34.9 142 61.8 ND 1,540 788 164 4,610 ND ND NA NA NA NA NA
21.01 74.75 8/11/2022 1,360 ND 419 16.0 30.5 ND 32.0 145 57.3 ND 722 773 177 4,090 NA NA NA NA NA NA NA
16.08 82.83 8/7/2020 2,710 BQL 373 89.0 37.0 BQL 823 66.5 43.0 BQL 4,370 329 73.5 2,380 NA ND BQL BQL 24,300 8,340 2,090
18.85 80.06 12/1/2021 6,080 ND 931 110 50.9 ND 864 ND 95.2 ND 11,900 776 124 5,730 ND ND NA NA NA NA NA
19.56 79.35 8/11/2022 6,590 ND 1,100 92.0 63.3 209 519 333 ND ND 12,900 946 ND 6,410 NA NA NA NA NA NA NA
21.70 77.21 3/14/2023 5,620 ND 773 79.4 47.8 ND 603 204 94.9 ND 5,190 712 168 3,740 ND 2,590 NA NA NA NA NA
1 70 600 70 70 5 20 6 70 25 600 400 400 500 40 NS 0.02 15 400 700 200
5,000 5,900 80,000 70,000 30,500 5,000 20,000 6,000 26,100 11,700 260,000 28,500 24,100 50,000 40,000 NS 50 15,000 NS NS NS
= Concentration Exceeds the 2L Standard
= Concentration Exceeds the GCLs
ppb = Parts Per Billion
BGS = Below Ground Surface
N/A = Not Applicable
NS = No Standard
NA = Not Analyzed
BQL = Below Quantitation Limits
ND = Not Detected
MW-2
MW-1
FP - 0.31'
MW-6
MW-5
MW-4
MW-3 FP - 0.46'
Table 4 - Summary of Groundwater Analytical Results
In and Out
Robbins, North Carolina
Targeted Compounds VPH 6200B
NC 2L Standard (ppb)
GCLs (ppb)Standard
MW-7
DW-1

APPENDIX A
05,00010,00015,00020,00025,00030,00079.0079.5080.0080.5081.0081.5082.0082.5083.0083.5084.005/1/2020 11/1/2020 5/1/2021 11/1/2021 5/1/2022 11/1/2022Concentration (ug/L)Groundwater Elevation (Feet)DateMW-1Groundwater Elevation vs. Concentration vs. TimeGroundwater ElevationBenzeneEthylbenzeneTolueneTotal Xylenes
-2,0003,0008,00013,00018,00023,00028,00068.0069.0070.0071.0072.0073.0074.0075.0076.0077.0078.008/1/2020 2/1/2021 8/1/2021 2/1/2022 8/1/2022Concentration (ug/L)Groundwater Elevation (Feet)DateMW-4Groundwater Elevation vs. Concentration vs. TimeGroundwater ElevationBenzeneEthylbenzeneTolueneTotal Xylenes
02,0004,0006,0008,00010,00012,00077.0078.0079.0080.0081.0082.0083.008/1/2020 2/1/2021 8/1/2021 2/1/2022 8/1/2022 2/1/2023Concentration (ug/L)Groundwater Elevation (Feet)DateDW-1Groundwater Elevation vs. Concentation vs. TimeGroundwater ElevationBenzeneEthylbenzeneTolueneTotal Xylenes

APPENDIX B
#=CL#
March 28, 2023
LIMS USE: FR - JASON RICKS
LIMS OBJECT ID: 92656753
92656753
Project:
Pace Project No.:
RE:
Jason Ricks
Pilot Geological
P.O. Box 128
Kernersville, NC 27285
In & Out G-5624.8
Dear Jason Ricks:
Enclosed are the analytical results for sample(s) received by the laboratory on March 14, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Stephanie Knott
[e-mail]
Project Manager
704-977-0981
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 36
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Lab ID Sample ID Matrix Date Collected Date Received
92656753001 MW-1 Water 03/14/23 09:55 03/14/23 13:38
92656753002 MW-2 Water 03/14/23 09:50 03/14/23 13:38
92656753003 MW-3 Water 03/14/23 10:20 03/14/23 13:38
92656753004 MW-4 Water 03/14/23 11:00 03/14/23 13:38
92656753005 MW-5 Water 03/14/23 11:20 03/14/23 13:38
92656753006 MW-6 Water 03/14/23 10:40 03/14/23 13:38
92656753007 DW-1 Water 03/14/23 10:00 03/14/23 13:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 3 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92656753001 MW-1 SM 6200B 69 PASI-CLMB
92656753002 MW-2 SM 6200B 69 PASI-CLMB
92656753003 MW-3 SM 6200B 69 PASI-CLMB
92656753004 MW-4 SM 6200B 69 PASI-CLMB
92656753005 MW-5 SM 6200B 69 PASI-CLMB
92656753006 MW-6 SM 6200B 69 PASI-CSAS
92656753007 DW-1 SM 6200B 69 PASI-CLMB
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 4 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-1 Lab ID:92656753001 Collected:03/14/23 09:55 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 03/22/23 00:38 75-85-425000250
tert-Amylmethyl ether ND ug/L 03/22/23 00:38 994-05-82500250
Benzene 7390 ug/L 03/22/23 00:38 71-43-2125250
Bromobenzene ND ug/L 03/22/23 00:38 108-86-1125250
Bromochloromethane ND ug/L 03/22/23 00:38 74-97-5125250
Bromodichloromethane ND ug/L 03/22/23 00:38 75-27-4125250
Bromoform ND ug/L 03/22/23 00:38 75-25-2125250
Bromomethane ND ug/L 03/22/23 00:38 74-83-91250250
tert-Butyl Alcohol ND ug/L 03/22/23 00:38 75-65-012500250
n-Butylbenzene ND ug/L 03/22/23 00:38 104-51-8125250
sec-Butylbenzene ND ug/L 03/22/23 00:38 135-98-8125250
tert-Butylbenzene ND ug/L 03/22/23 00:38 98-06-6125250
tert-Butyl Formate ND ug/L 03/22/23 00:38 762-75-412500250
Carbon tetrachloride ND ug/L 03/22/23 00:38 56-23-5125250
Chlorobenzene ND ug/L 03/22/23 00:38 108-90-7125250
Chloroethane ND ug/L 03/22/23 00:38 75-00-3250250
Chloroform ND ug/L 03/22/23 00:38 67-66-3125250
Chloromethane ND ug/L 03/22/23 00:38 74-87-3250250
2-Chlorotoluene ND ug/L 03/22/23 00:38 95-49-8125250
4-Chlorotoluene ND ug/L 03/22/23 00:38 106-43-4125250
1,2-Dibromo-3-chloropropane ND ug/L 03/22/23 00:38 96-12-8250250
Dibromochloromethane ND ug/L 03/22/23 00:38 124-48-1125250
1,2-Dibromoethane (EDB)ND ug/L 03/22/23 00:38 106-93-4125250
Dibromomethane ND ug/L 03/22/23 00:38 74-95-3125250
1,2-Dichlorobenzene ND ug/L 03/22/23 00:38 95-50-1125250
1,3-Dichlorobenzene ND ug/L 03/22/23 00:38 541-73-1125250
1,4-Dichlorobenzene ND ug/L 03/22/23 00:38 106-46-7125250
Dichlorodifluoromethane ND ug/L 03/22/23 00:38 75-71-8125250
1,1-Dichloroethane ND ug/L 03/22/23 00:38 75-34-3125250
1,2-Dichloroethane ND ug/L 03/22/23 00:38 107-06-2125250
1,1-Dichloroethene ND ug/L 03/22/23 00:38 75-35-4125250
cis-1,2-Dichloroethene ND ug/L 03/22/23 00:38 156-59-2125250
trans-1,2-Dichloroethene ND ug/L 03/22/23 00:38 156-60-5125250
1,2-Dichloropropane ND ug/L 03/22/23 00:38 78-87-5125250
1,3-Dichloropropane ND ug/L 03/22/23 00:38 142-28-9125250
2,2-Dichloropropane ND ug/L 03/22/23 00:38 594-20-7125250
1,1-Dichloropropene ND ug/L 03/22/23 00:38 563-58-6125250
cis-1,3-Dichloropropene ND ug/L 03/22/23 00:38 10061-01-5125250
trans-1,3-Dichloropropene ND ug/L 03/22/23 00:38 10061-02-6125250
Diisopropyl ether ND ug/L 03/22/23 00:38 108-20-3125250
Ethanol ND ug/L 03/22/23 00:38 64-17-550000250
Ethylbenzene 3280 ug/L 03/22/23 00:38 100-41-4125250
Ethyl-tert-butyl ether ND ug/L 03/22/23 00:38 637-92-32500250
Hexachloro-1,3-butadiene ND ug/L 03/22/23 00:38 87-68-3500250
Isopropylbenzene (Cumene)151 ug/L 03/22/23 00:38 98-82-8125250
Methylene Chloride ND ug/L 03/22/23 00:38 75-09-2500250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-1 Lab ID:92656753001 Collected:03/14/23 09:55 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 03/22/23 00:38 1634-04-4125250
Naphthalene 647 ug/L 03/22/23 00:38 91-20-3500250
n-Propylbenzene 490 ug/L 03/22/23 00:38 103-65-1125250
Styrene ND ug/L 03/22/23 00:38 100-42-5125250
1,1,1,2-Tetrachloroethane ND ug/L 03/22/23 00:38 630-20-6125250
1,1,2,2-Tetrachloroethane ND ug/L 03/22/23 00:38 79-34-5125250
Tetrachloroethene ND ug/L 03/22/23 00:38 127-18-4125250
Toluene 31300 ug/L 03/22/23 00:38 108-88-3125250
1,2,3-Trichlorobenzene ND ug/L 03/22/23 00:38 87-61-6500250
1,2,4-Trichlorobenzene ND ug/L 03/22/23 00:38 120-82-1500250
1,1,1-Trichloroethane ND ug/L 03/22/23 00:38 71-55-6125250
1,1,2-Trichloroethane ND ug/L 03/22/23 00:38 79-00-5125250
Trichloroethene ND ug/L 03/22/23 00:38 79-01-6125250
Trichlorofluoromethane ND ug/L 03/22/23 00:38 75-69-4250250
1,2,3-Trichloropropane ND ug/L 03/22/23 00:38 96-18-4125250
1,2,4-Trimethylbenzene 3700 ug/L 03/22/23 00:38 95-63-6125250
1,3,5-Trimethylbenzene 839 ug/L 03/22/23 00:38 108-67-8125250
Vinyl chloride ND ug/L 03/22/23 00:38 75-01-4250250
m&p-Xylene 12400 ug/L 03/22/23 00:38 179601-23-1250250
o-Xylene 5640 ug/L 03/22/23 00:38 95-47-6125250
Surrogates
1,2-Dichloroethane-d4 (S)97 %03/22/23 00:38 17060-07-070-130 250
4-Bromofluorobenzene (S)97 %03/22/23 00:38 460-00-470-130 250
Toluene-d8 (S)102 %03/22/23 00:38 2037-26-570-130 250
Sample:MW-2 Lab ID:92656753002 Collected:03/14/23 09:50 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 03/21/23 19:35 75-85-41001
tert-Amylmethyl ether ND ug/L 03/21/23 19:35 994-05-810.0 1
Benzene ND ug/L 03/21/23 19:35 71-43-20.50 1
Bromobenzene ND ug/L 03/21/23 19:35 108-86-10.50 1
Bromochloromethane ND ug/L 03/21/23 19:35 74-97-50.50 1
Bromodichloromethane ND ug/L 03/21/23 19:35 75-27-40.50 1
Bromoform ND ug/L 03/21/23 19:35 75-25-20.50 1
Bromomethane ND ug/L 03/21/23 19:35 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 03/21/23 19:35 75-65-050.0 1
n-Butylbenzene ND ug/L 03/21/23 19:35 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/21/23 19:35 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/21/23 19:35 98-06-60.50 1
tert-Butyl Formate ND ug/L 03/21/23 19:35 762-75-450.0 1
Carbon tetrachloride ND ug/L 03/21/23 19:35 56-23-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-2 Lab ID:92656753002 Collected:03/14/23 09:50 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 03/21/23 19:35 108-90-70.50 1
Chloroethane ND ug/L 03/21/23 19:35 75-00-31.0 1
Chloroform ND ug/L 03/21/23 19:35 67-66-30.50 1
Chloromethane ND ug/L 03/21/23 19:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/21/23 19:35 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/21/23 19:35 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/21/23 19:35 96-12-81.0 1
Dibromochloromethane ND ug/L 03/21/23 19:35 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 03/21/23 19:35 106-93-40.50 1
Dibromomethane ND ug/L 03/21/23 19:35 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/21/23 19:35 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/21/23 19:35 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/21/23 19:35 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/21/23 19:35 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/21/23 19:35 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/21/23 19:35 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/21/23 19:35 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/21/23 19:35 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/21/23 19:35 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/21/23 19:35 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/21/23 19:35 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/21/23 19:35 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/21/23 19:35 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/21/23 19:35 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/21/23 19:35 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/21/23 19:35 108-20-30.50 1
Ethanol ND ug/L 03/21/23 19:35 64-17-52001
Ethylbenzene ND ug/L 03/21/23 19:35 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 03/21/23 19:35 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 03/21/23 19:35 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 03/21/23 19:35 98-82-80.50 1
Methylene Chloride ND ug/L 03/21/23 19:35 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 03/21/23 19:35 1634-04-40.50 1
Naphthalene ND ug/L 03/21/23 19:35 91-20-32.0 1
n-Propylbenzene ND ug/L 03/21/23 19:35 103-65-10.50 1
Styrene ND ug/L 03/21/23 19:35 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/21/23 19:35 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/21/23 19:35 79-34-50.50 1
Tetrachloroethene ND ug/L 03/21/23 19:35 127-18-40.50 1
Toluene ND ug/L 03/21/23 19:35 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/21/23 19:35 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/21/23 19:35 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/21/23 19:35 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/21/23 19:35 79-00-50.50 1
Trichloroethene ND ug/L 03/21/23 19:35 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/21/23 19:35 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-2 Lab ID:92656753002 Collected:03/14/23 09:50 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 03/21/23 19:35 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/21/23 19:35 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/21/23 19:35 108-67-80.50 1
Vinyl chloride ND ug/L 03/21/23 19:35 75-01-41.0 1
m&p-Xylene ND ug/L 03/21/23 19:35 179601-23-11.0 1
o-Xylene ND ug/L 03/21/23 19:35 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %03/21/23 19:35 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %03/21/23 19:35 460-00-470-130 1
Toluene-d8 (S)103 %03/21/23 19:35 2037-26-570-130 1
Sample:MW-3 Lab ID:92656753003 Collected:03/14/23 10:20 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 03/22/23 00:56 75-85-425000250
tert-Amylmethyl ether ND ug/L 03/22/23 00:56 994-05-82500250
Benzene 4500 ug/L 03/22/23 00:56 71-43-2125250
Bromobenzene ND ug/L 03/22/23 00:56 108-86-1125250
Bromochloromethane ND ug/L 03/22/23 00:56 74-97-5125250
Bromodichloromethane ND ug/L 03/22/23 00:56 75-27-4125250
Bromoform ND ug/L 03/22/23 00:56 75-25-2125250
Bromomethane ND ug/L 03/22/23 00:56 74-83-91250250
tert-Butyl Alcohol ND ug/L 03/22/23 00:56 75-65-012500250
n-Butylbenzene ND ug/L 03/22/23 00:56 104-51-8125250
sec-Butylbenzene ND ug/L 03/22/23 00:56 135-98-8125250
tert-Butylbenzene ND ug/L 03/22/23 00:56 98-06-6125250
tert-Butyl Formate ND ug/L 03/22/23 00:56 762-75-412500250
Carbon tetrachloride ND ug/L 03/22/23 00:56 56-23-5125250
Chlorobenzene ND ug/L 03/22/23 00:56 108-90-7125250
Chloroethane ND ug/L 03/22/23 00:56 75-00-3250250
Chloroform ND ug/L 03/22/23 00:56 67-66-3125250
Chloromethane ND ug/L 03/22/23 00:56 74-87-3250250
2-Chlorotoluene ND ug/L 03/22/23 00:56 95-49-8125250
4-Chlorotoluene ND ug/L 03/22/23 00:56 106-43-4125250
1,2-Dibromo-3-chloropropane ND ug/L 03/22/23 00:56 96-12-8250250
Dibromochloromethane ND ug/L 03/22/23 00:56 124-48-1125250
1,2-Dibromoethane (EDB)ND ug/L 03/22/23 00:56 106-93-4125250
Dibromomethane ND ug/L 03/22/23 00:56 74-95-3125250
1,2-Dichlorobenzene ND ug/L 03/22/23 00:56 95-50-1125250
1,3-Dichlorobenzene ND ug/L 03/22/23 00:56 541-73-1125250
1,4-Dichlorobenzene ND ug/L 03/22/23 00:56 106-46-7125250
Dichlorodifluoromethane ND ug/L 03/22/23 00:56 75-71-8125250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-3 Lab ID:92656753003 Collected:03/14/23 10:20 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloroethane ND ug/L 03/22/23 00:56 75-34-3125250
1,2-Dichloroethane ND ug/L 03/22/23 00:56 107-06-2125250
1,1-Dichloroethene ND ug/L 03/22/23 00:56 75-35-4125250
cis-1,2-Dichloroethene ND ug/L 03/22/23 00:56 156-59-2125250
trans-1,2-Dichloroethene ND ug/L 03/22/23 00:56 156-60-5125250
1,2-Dichloropropane ND ug/L 03/22/23 00:56 78-87-5125250
1,3-Dichloropropane ND ug/L 03/22/23 00:56 142-28-9125250
2,2-Dichloropropane ND ug/L 03/22/23 00:56 594-20-7125250
1,1-Dichloropropene ND ug/L 03/22/23 00:56 563-58-6125250
cis-1,3-Dichloropropene ND ug/L 03/22/23 00:56 10061-01-5125250
trans-1,3-Dichloropropene ND ug/L 03/22/23 00:56 10061-02-6125250
Diisopropyl ether ND ug/L 03/22/23 00:56 108-20-3125250
Ethanol ND ug/L 03/22/23 00:56 64-17-550000250
Ethylbenzene 2690 ug/L 03/22/23 00:56 100-41-4125250
Ethyl-tert-butyl ether ND ug/L 03/22/23 00:56 637-92-32500250
Hexachloro-1,3-butadiene ND ug/L 03/22/23 00:56 87-68-3500250
Isopropylbenzene (Cumene)125 ug/L 03/22/23 00:56 98-82-8125250
Methylene Chloride ND ug/L 03/22/23 00:56 75-09-2500250
Methyl-tert-butyl ether ND ug/L 03/22/23 00:56 1634-04-4125250
Naphthalene 690 ug/L 03/22/23 00:56 91-20-3500250
n-Propylbenzene 371 ug/L 03/22/23 00:56 103-65-1125250
Styrene ND ug/L 03/22/23 00:56 100-42-5125250
1,1,1,2-Tetrachloroethane ND ug/L 03/22/23 00:56 630-20-6125250
1,1,2,2-Tetrachloroethane ND ug/L 03/22/23 00:56 79-34-5125250
Tetrachloroethene ND ug/L 03/22/23 00:56 127-18-4125250
Toluene 25600 ug/L 03/22/23 00:56 108-88-3125250
1,2,3-Trichlorobenzene ND ug/L 03/22/23 00:56 87-61-6500250
1,2,4-Trichlorobenzene ND ug/L 03/22/23 00:56 120-82-1500250
1,1,1-Trichloroethane ND ug/L 03/22/23 00:56 71-55-6125250
1,1,2-Trichloroethane ND ug/L 03/22/23 00:56 79-00-5125250
Trichloroethene ND ug/L 03/22/23 00:56 79-01-6125250
Trichlorofluoromethane ND ug/L 03/22/23 00:56 75-69-4250250
1,2,3-Trichloropropane ND ug/L 03/22/23 00:56 96-18-4125250
1,2,4-Trimethylbenzene 3180 ug/L 03/22/23 00:56 95-63-6125250
1,3,5-Trimethylbenzene 769 ug/L 03/22/23 00:56 108-67-8125250
Vinyl chloride ND ug/L 03/22/23 00:56 75-01-4250250
m&p-Xylene 10800 ug/L 03/22/23 00:56 179601-23-1250250
o-Xylene 5420 ug/L 03/22/23 00:56 95-47-6125250
Surrogates
1,2-Dichloroethane-d4 (S)97 %03/22/23 00:56 17060-07-070-130 250
4-Bromofluorobenzene (S)97 %03/22/23 00:56 460-00-470-130 250
Toluene-d8 (S)102 %03/22/23 00:56 2037-26-570-130 250
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-4 Lab ID:92656753004 Collected:03/14/23 11:00 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 03/23/23 18:32 75-85-4500050
tert-Amylmethyl ether ND ug/L 03/23/23 18:32 994-05-850050
Benzene 265 ug/L 03/23/23 18:32 71-43-225.0 50
Bromobenzene ND ug/L 03/23/23 18:32 108-86-125.0 50
Bromochloromethane ND ug/L 03/23/23 18:32 74-97-525.0 50
Bromodichloromethane ND ug/L 03/23/23 18:32 75-27-425.0 50
Bromoform ND ug/L 03/23/23 18:32 75-25-225.0 50
Bromomethane ND ug/L 03/23/23 18:32 74-83-925050
tert-Butyl Alcohol ND ug/L 03/23/23 18:32 75-65-0250050
n-Butylbenzene ND ug/L 03/23/23 18:32 104-51-825.0 50
sec-Butylbenzene ND ug/L 03/23/23 18:32 135-98-825.0 50
tert-Butylbenzene ND ug/L 03/23/23 18:32 98-06-625.0 50
tert-Butyl Formate ND ug/L 03/23/23 18:32 762-75-4250050
Carbon tetrachloride ND ug/L 03/23/23 18:32 56-23-525.0 50
Chlorobenzene ND ug/L 03/23/23 18:32 108-90-725.0 50
Chloroethane ND ug/L 03/23/23 18:32 75-00-350.0 50
Chloroform ND ug/L 03/23/23 18:32 67-66-325.0 50
Chloromethane ND ug/L 03/23/23 18:32 74-87-350.0 50
2-Chlorotoluene ND ug/L 03/23/23 18:32 95-49-825.0 50
4-Chlorotoluene ND ug/L 03/23/23 18:32 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 03/23/23 18:32 96-12-850.0 50
Dibromochloromethane ND ug/L 03/23/23 18:32 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 03/23/23 18:32 106-93-425.0 50
Dibromomethane ND ug/L 03/23/23 18:32 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 03/23/23 18:32 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 03/23/23 18:32 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 03/23/23 18:32 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 03/23/23 18:32 75-71-825.0 50
1,1-Dichloroethane ND ug/L 03/23/23 18:32 75-34-325.0 50
1,2-Dichloroethane ND ug/L 03/23/23 18:32 107-06-225.0 50
1,1-Dichloroethene ND ug/L 03/23/23 18:32 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 03/23/23 18:32 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 03/23/23 18:32 156-60-525.0 50
1,2-Dichloropropane ND ug/L 03/23/23 18:32 78-87-525.0 50
1,3-Dichloropropane ND ug/L 03/23/23 18:32 142-28-925.0 50
2,2-Dichloropropane ND ug/L 03/23/23 18:32 594-20-725.0 50
1,1-Dichloropropene ND ug/L 03/23/23 18:32 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 03/23/23 18:32 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 03/23/23 18:32 10061-02-625.0 50
Diisopropyl ether ND ug/L 03/23/23 18:32 108-20-325.0 50
Ethanol ND ug/L 03/23/23 18:32 64-17-51000050
Ethylbenzene 1720 ug/L 03/23/23 18:32 100-41-425.0 50
Ethyl-tert-butyl ether ND ug/L 03/23/23 18:32 637-92-350050
Hexachloro-1,3-butadiene ND ug/L 03/23/23 18:32 87-68-310050
Isopropylbenzene (Cumene)118 ug/L 03/23/23 18:32 98-82-825.0 50
Methylene Chloride ND ug/L 03/23/23 18:32 75-09-210050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-4 Lab ID:92656753004 Collected:03/14/23 11:00 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether ND ug/L 03/23/23 18:32 1634-04-425.0 50
Naphthalene 303 ug/L 03/23/23 18:32 91-20-310050
n-Propylbenzene 350 ug/L 03/23/23 18:32 103-65-125.0 50
Styrene ND ug/L 03/23/23 18:32 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 03/23/23 18:32 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 03/23/23 18:32 79-34-525.0 50
Tetrachloroethene ND ug/L 03/23/23 18:32 127-18-425.0 50
Toluene 8570 ug/L 03/23/23 18:32 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 03/23/23 18:32 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 03/23/23 18:32 120-82-110050
1,1,1-Trichloroethane ND ug/L 03/23/23 18:32 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 03/23/23 18:32 79-00-525.0 50
Trichloroethene ND ug/L 03/23/23 18:32 79-01-625.0 50
Trichlorofluoromethane ND ug/L 03/23/23 18:32 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 03/23/23 18:32 96-18-425.0 50
1,2,4-Trimethylbenzene 2610 ug/L 03/23/23 18:32 95-63-625.0 50
1,3,5-Trimethylbenzene 618 ug/L 03/23/23 18:32 108-67-825.0 50
Vinyl chloride ND ug/L 03/23/23 18:32 75-01-450.0 50
m&p-Xylene 6860 ug/L 03/23/23 18:32 179601-23-150.0 50
o-Xylene 3190 ug/L 03/23/23 18:32 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)98 %03/23/23 18:32 17060-07-070-130 50
4-Bromofluorobenzene (S)96 %03/23/23 18:32 460-00-470-130 50
Toluene-d8 (S)100 %03/23/23 18:32 2037-26-570-130 50
Sample:MW-5 Lab ID:92656753005 Collected:03/14/23 11:20 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 03/21/23 19:53 75-85-41001
tert-Amylmethyl ether ND ug/L 03/21/23 19:53 994-05-810.0 1
Benzene 2.4 ug/L 03/21/23 19:53 71-43-20.50 1
Bromobenzene ND ug/L 03/21/23 19:53 108-86-10.50 1
Bromochloromethane ND ug/L 03/21/23 19:53 74-97-50.50 1
Bromodichloromethane ND ug/L 03/21/23 19:53 75-27-40.50 1
Bromoform ND ug/L 03/21/23 19:53 75-25-20.50 1
Bromomethane ND ug/L 03/21/23 19:53 74-83-95.0 1
tert-Butyl Alcohol ND ug/L 03/21/23 19:53 75-65-050.0 1
n-Butylbenzene ND ug/L 03/21/23 19:53 104-51-80.50 1
sec-Butylbenzene ND ug/L 03/21/23 19:53 135-98-80.50 1
tert-Butylbenzene ND ug/L 03/21/23 19:53 98-06-60.50 1
tert-Butyl Formate ND ug/L 03/21/23 19:53 762-75-450.0 1
Carbon tetrachloride ND ug/L 03/21/23 19:53 56-23-50.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-5 Lab ID:92656753005 Collected:03/14/23 11:20 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Chlorobenzene ND ug/L 03/21/23 19:53 108-90-70.50 1
Chloroethane ND ug/L 03/21/23 19:53 75-00-31.0 1
Chloroform ND ug/L 03/21/23 19:53 67-66-30.50 1
Chloromethane ND ug/L 03/21/23 19:53 74-87-31.0 1
2-Chlorotoluene ND ug/L 03/21/23 19:53 95-49-80.50 1
4-Chlorotoluene ND ug/L 03/21/23 19:53 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 03/21/23 19:53 96-12-81.0 1
Dibromochloromethane ND ug/L 03/21/23 19:53 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 03/21/23 19:53 106-93-40.50 1
Dibromomethane ND ug/L 03/21/23 19:53 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 03/21/23 19:53 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 03/21/23 19:53 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 03/21/23 19:53 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 03/21/23 19:53 75-71-80.50 1
1,1-Dichloroethane ND ug/L 03/21/23 19:53 75-34-30.50 1
1,2-Dichloroethane ND ug/L 03/21/23 19:53 107-06-20.50 1
1,1-Dichloroethene ND ug/L 03/21/23 19:53 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 03/21/23 19:53 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 03/21/23 19:53 156-60-50.50 1
1,2-Dichloropropane ND ug/L 03/21/23 19:53 78-87-50.50 1
1,3-Dichloropropane ND ug/L 03/21/23 19:53 142-28-90.50 1
2,2-Dichloropropane ND ug/L 03/21/23 19:53 594-20-70.50 1
1,1-Dichloropropene ND ug/L 03/21/23 19:53 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 03/21/23 19:53 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 03/21/23 19:53 10061-02-60.50 1
Diisopropyl ether ND ug/L 03/21/23 19:53 108-20-30.50 1
Ethanol ND ug/L 03/21/23 19:53 64-17-52001
Ethylbenzene ND ug/L 03/21/23 19:53 100-41-40.50 1
Ethyl-tert-butyl ether ND ug/L 03/21/23 19:53 637-92-310.0 1
Hexachloro-1,3-butadiene ND ug/L 03/21/23 19:53 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 03/21/23 19:53 98-82-80.50 1
Methylene Chloride ND ug/L 03/21/23 19:53 75-09-22.0 1
Methyl-tert-butyl ether 4.5 ug/L 03/21/23 19:53 1634-04-40.50 1
Naphthalene ND ug/L 03/21/23 19:53 91-20-32.0 1
n-Propylbenzene ND ug/L 03/21/23 19:53 103-65-10.50 1
Styrene ND ug/L 03/21/23 19:53 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 03/21/23 19:53 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 03/21/23 19:53 79-34-50.50 1
Tetrachloroethene ND ug/L 03/21/23 19:53 127-18-40.50 1
Toluene 1.8 ug/L 03/21/23 19:53 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 03/21/23 19:53 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 03/21/23 19:53 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 03/21/23 19:53 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 03/21/23 19:53 79-00-50.50 1
Trichloroethene ND ug/L 03/21/23 19:53 79-01-60.50 1
Trichlorofluoromethane ND ug/L 03/21/23 19:53 75-69-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-5 Lab ID:92656753005 Collected:03/14/23 11:20 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,2,3-Trichloropropane ND ug/L 03/21/23 19:53 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 03/21/23 19:53 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 03/21/23 19:53 108-67-80.50 1
Vinyl chloride ND ug/L 03/21/23 19:53 75-01-41.0 1
m&p-Xylene ND ug/L 03/21/23 19:53 179601-23-11.0 1
o-Xylene ND ug/L 03/21/23 19:53 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)112 %03/21/23 19:53 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %03/21/23 19:53 460-00-470-130 1
Toluene-d8 (S)100 %03/21/23 19:53 2037-26-570-130 1
Sample:MW-6 Lab ID:92656753006 Collected:03/14/23 10:40 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 03/23/23 15:00 75-85-45005
tert-Amylmethyl ether ND ug/L 03/23/23 15:00 994-05-850.0 5
Benzene 45.8 ug/L 03/23/23 15:00 71-43-22.5 5
Bromobenzene ND ug/L 03/23/23 15:00 108-86-12.5 5
Bromochloromethane ND ug/L 03/23/23 15:00 74-97-52.5 5
Bromodichloromethane ND ug/L 03/23/23 15:00 75-27-42.5 5
Bromoform ND ug/L 03/23/23 15:00 75-25-22.5 5
Bromomethane ND ug/L 03/23/23 15:00 74-83-925.0 5
tert-Butyl Alcohol ND ug/L 03/23/23 15:00 75-65-02505
n-Butylbenzene ND ug/L 03/23/23 15:00 104-51-82.5 5
sec-Butylbenzene ND ug/L 03/23/23 15:00 135-98-82.5 5
tert-Butylbenzene ND ug/L 03/23/23 15:00 98-06-62.5 5
tert-Butyl Formate ND ug/L 03/23/23 15:00 762-75-42505
Carbon tetrachloride ND ug/L 03/23/23 15:00 56-23-52.5 5
Chlorobenzene ND ug/L 03/23/23 15:00 108-90-72.5 5
Chloroethane ND ug/L 03/23/23 15:00 75-00-35.0 5
Chloroform ND ug/L 03/23/23 15:00 67-66-32.5 5
Chloromethane ND ug/L 03/23/23 15:00 74-87-35.0 5
2-Chlorotoluene ND ug/L 03/23/23 15:00 95-49-82.5 5
4-Chlorotoluene ND ug/L 03/23/23 15:00 106-43-42.5 5
1,2-Dibromo-3-chloropropane ND ug/L 03/23/23 15:00 96-12-85.0 5
Dibromochloromethane ND ug/L 03/23/23 15:00 124-48-12.5 5
1,2-Dibromoethane (EDB)ND ug/L 03/23/23 15:00 106-93-42.5 5
Dibromomethane ND ug/L 03/23/23 15:00 74-95-32.5 5
1,2-Dichlorobenzene ND ug/L 03/23/23 15:00 95-50-12.5 5
1,3-Dichlorobenzene ND ug/L 03/23/23 15:00 541-73-12.5 5
1,4-Dichlorobenzene ND ug/L 03/23/23 15:00 106-46-72.5 5
Dichlorodifluoromethane ND ug/L 03/23/23 15:00 75-71-82.5 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 13 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:MW-6 Lab ID:92656753006 Collected:03/14/23 10:40 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1-Dichloroethane ND ug/L 03/23/23 15:00 75-34-32.5 5
1,2-Dichloroethane ND ug/L 03/23/23 15:00 107-06-22.5 5
1,1-Dichloroethene ND ug/L 03/23/23 15:00 75-35-42.5 5
cis-1,2-Dichloroethene ND ug/L 03/23/23 15:00 156-59-22.5 5
trans-1,2-Dichloroethene ND ug/L 03/23/23 15:00 156-60-52.5 5
1,2-Dichloropropane ND ug/L 03/23/23 15:00 78-87-52.5 5
1,3-Dichloropropane ND ug/L 03/23/23 15:00 142-28-92.5 5
2,2-Dichloropropane ND ug/L 03/23/23 15:00 594-20-72.5 5
1,1-Dichloropropene ND ug/L 03/23/23 15:00 563-58-62.5 5
cis-1,3-Dichloropropene ND ug/L 03/23/23 15:00 10061-01-52.5 5
trans-1,3-Dichloropropene ND ug/L 03/23/23 15:00 10061-02-62.5 5
Diisopropyl ether ND ug/L 03/23/23 15:00 108-20-32.5 5
Ethanol ND ug/L 03/23/23 15:00 64-17-510005
Ethylbenzene 38.6 ug/L 03/23/23 15:00 100-41-42.5 5
Ethyl-tert-butyl ether ND ug/L 03/23/23 15:00 637-92-350.0 5
Hexachloro-1,3-butadiene ND ug/L 03/23/23 15:00 87-68-310.0 5
Isopropylbenzene (Cumene)4.5 ug/L 03/23/23 15:00 98-82-82.5 5
Methylene Chloride ND ug/L 03/23/23 15:00 75-09-210.0 5
Methyl-tert-butyl ether 24.5 ug/L 03/23/23 15:00 1634-04-42.5 5
Naphthalene 11.0 ug/L 03/23/23 15:00 91-20-310.0 5
n-Propylbenzene ND ug/L 03/23/23 15:00 103-65-12.5 5
Styrene ND ug/L 03/23/23 15:00 100-42-52.5 5
1,1,1,2-Tetrachloroethane ND ug/L 03/23/23 15:00 630-20-62.5 5
1,1,2,2-Tetrachloroethane ND ug/L 03/23/23 15:00 79-34-52.5 5
Tetrachloroethene ND ug/L 03/23/23 15:00 127-18-42.5 5
Toluene 92.7 ug/L 03/23/23 15:00 108-88-32.5 5
1,2,3-Trichlorobenzene ND ug/L 03/23/23 15:00 87-61-610.0 5
1,2,4-Trichlorobenzene ND ug/L 03/23/23 15:00 120-82-110.0 5
1,1,1-Trichloroethane ND ug/L 03/23/23 15:00 71-55-62.5 5
1,1,2-Trichloroethane ND ug/L 03/23/23 15:00 79-00-52.5 5
Trichloroethene ND ug/L 03/23/23 15:00 79-01-62.5 5
Trichlorofluoromethane ND ug/L 03/23/23 15:00 75-69-45.0 5
1,2,3-Trichloropropane ND ug/L 03/23/23 15:00 96-18-42.5 5
1,2,4-Trimethylbenzene 34.9 ug/L 03/23/23 15:00 95-63-62.5 5
1,3,5-Trimethylbenzene ND ug/L 03/23/23 15:00 108-67-82.5 5
Vinyl chloride ND ug/L 03/23/23 15:00 75-01-45.0 5
m&p-Xylene 123 ug/L 03/23/23 15:00 179601-23-15.0 5
o-Xylene 50.5 ug/L 03/23/23 15:00 95-47-62.5 5
Surrogates
1,2-Dichloroethane-d4 (S)97 %03/23/23 15:00 17060-07-0 D370-130 5
4-Bromofluorobenzene (S)95 %03/23/23 15:00 460-00-470-130 5
Toluene-d8 (S)101 %03/23/23 15:00 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 14 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:DW-1 Lab ID:92656753007 Collected:03/14/23 10:00 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
tert-Amyl Alcohol ND ug/L 03/22/23 00:21 75-85-4500050
tert-Amylmethyl ether ND ug/L 03/22/23 00:21 994-05-850050
Benzene 5620 ug/L 03/22/23 00:21 71-43-225.0 50
Bromobenzene ND ug/L 03/22/23 00:21 108-86-125.0 50
Bromochloromethane ND ug/L 03/22/23 00:21 74-97-525.0 50
Bromodichloromethane ND ug/L 03/22/23 00:21 75-27-425.0 50
Bromoform ND ug/L 03/22/23 00:21 75-25-225.0 50
Bromomethane ND ug/L 03/22/23 00:21 74-83-925050
tert-Butyl Alcohol 2590 ug/L 03/22/23 00:21 75-65-0250050
n-Butylbenzene ND ug/L 03/22/23 00:21 104-51-825.0 50
sec-Butylbenzene ND ug/L 03/22/23 00:21 135-98-825.0 50
tert-Butylbenzene ND ug/L 03/22/23 00:21 98-06-625.0 50
tert-Butyl Formate ND ug/L 03/22/23 00:21 762-75-4250050
Carbon tetrachloride ND ug/L 03/22/23 00:21 56-23-525.0 50
Chlorobenzene ND ug/L 03/22/23 00:21 108-90-725.0 50
Chloroethane ND ug/L 03/22/23 00:21 75-00-350.0 50
Chloroform ND ug/L 03/22/23 00:21 67-66-325.0 50
Chloromethane ND ug/L 03/22/23 00:21 74-87-350.0 50
2-Chlorotoluene ND ug/L 03/22/23 00:21 95-49-825.0 50
4-Chlorotoluene ND ug/L 03/22/23 00:21 106-43-425.0 50
1,2-Dibromo-3-chloropropane ND ug/L 03/22/23 00:21 96-12-850.0 50
Dibromochloromethane ND ug/L 03/22/23 00:21 124-48-125.0 50
1,2-Dibromoethane (EDB)ND ug/L 03/22/23 00:21 106-93-425.0 50
Dibromomethane ND ug/L 03/22/23 00:21 74-95-325.0 50
1,2-Dichlorobenzene ND ug/L 03/22/23 00:21 95-50-125.0 50
1,3-Dichlorobenzene ND ug/L 03/22/23 00:21 541-73-125.0 50
1,4-Dichlorobenzene ND ug/L 03/22/23 00:21 106-46-725.0 50
Dichlorodifluoromethane ND ug/L 03/22/23 00:21 75-71-825.0 50
1,1-Dichloroethane ND ug/L 03/22/23 00:21 75-34-325.0 50
1,2-Dichloroethane ND ug/L 03/22/23 00:21 107-06-225.0 50
1,1-Dichloroethene ND ug/L 03/22/23 00:21 75-35-425.0 50
cis-1,2-Dichloroethene ND ug/L 03/22/23 00:21 156-59-225.0 50
trans-1,2-Dichloroethene ND ug/L 03/22/23 00:21 156-60-525.0 50
1,2-Dichloropropane ND ug/L 03/22/23 00:21 78-87-525.0 50
1,3-Dichloropropane ND ug/L 03/22/23 00:21 142-28-925.0 50
2,2-Dichloropropane ND ug/L 03/22/23 00:21 594-20-725.0 50
1,1-Dichloropropene ND ug/L 03/22/23 00:21 563-58-625.0 50
cis-1,3-Dichloropropene ND ug/L 03/22/23 00:21 10061-01-525.0 50
trans-1,3-Dichloropropene ND ug/L 03/22/23 00:21 10061-02-625.0 50
Diisopropyl ether 79.4 ug/L 03/22/23 00:21 108-20-325.0 50
Ethanol ND ug/L 03/22/23 00:21 64-17-51000050
Ethylbenzene 773 ug/L 03/22/23 00:21 100-41-425.0 50
Ethyl-tert-butyl ether ND ug/L 03/22/23 00:21 637-92-350050
Hexachloro-1,3-butadiene ND ug/L 03/22/23 00:21 87-68-310050
Isopropylbenzene (Cumene)47.8 ug/L 03/22/23 00:21 98-82-825.0 50
Methylene Chloride ND ug/L 03/22/23 00:21 75-09-210050
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 15 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Sample:DW-1 Lab ID:92656753007 Collected:03/14/23 10:00 Received:03/14/23 13:38 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Methyl-tert-butyl ether 603 ug/L 03/22/23 00:21 1634-04-425.0 50
Naphthalene 204 ug/L 03/22/23 00:21 91-20-310050
n-Propylbenzene 94.9 ug/L 03/22/23 00:21 103-65-125.0 50
Styrene ND ug/L 03/22/23 00:21 100-42-525.0 50
1,1,1,2-Tetrachloroethane ND ug/L 03/22/23 00:21 630-20-625.0 50
1,1,2,2-Tetrachloroethane ND ug/L 03/22/23 00:21 79-34-525.0 50
Tetrachloroethene ND ug/L 03/22/23 00:21 127-18-425.0 50
Toluene 5190 ug/L 03/22/23 00:21 108-88-325.0 50
1,2,3-Trichlorobenzene ND ug/L 03/22/23 00:21 87-61-610050
1,2,4-Trichlorobenzene ND ug/L 03/22/23 00:21 120-82-110050
1,1,1-Trichloroethane ND ug/L 03/22/23 00:21 71-55-625.0 50
1,1,2-Trichloroethane ND ug/L 03/22/23 00:21 79-00-525.0 50
Trichloroethene ND ug/L 03/22/23 00:21 79-01-625.0 50
Trichlorofluoromethane ND ug/L 03/22/23 00:21 75-69-450.0 50
1,2,3-Trichloropropane ND ug/L 03/22/23 00:21 96-18-425.0 50
1,2,4-Trimethylbenzene 712 ug/L 03/22/23 00:21 95-63-625.0 50
1,3,5-Trimethylbenzene 168 ug/L 03/22/23 00:21 108-67-825.0 50
Vinyl chloride ND ug/L 03/22/23 00:21 75-01-450.0 50
m&p-Xylene 2530 ug/L 03/22/23 00:21 179601-23-150.0 50
o-Xylene 1210 ug/L 03/22/23 00:21 95-47-625.0 50
Surrogates
1,2-Dichloroethane-d4 (S)101 %03/22/23 00:21 17060-07-070-130 50
4-Bromofluorobenzene (S)96 %03/22/23 00:21 460-00-470-130 50
Toluene-d8 (S)98 %03/22/23 00:21 2037-26-570-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 16 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
762628
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92656753001, 92656753002, 92656753003, 92656753005, 92656753007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3960535
Associated Lab Samples:92656753001, 92656753002, 92656753003, 92656753005, 92656753007
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/21/23 18:24
1,1,1-Trichloroethane ug/L ND 0.50 03/21/23 18:24
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/21/23 18:24
1,1,2-Trichloroethane ug/L ND 0.50 03/21/23 18:24
1,1-Dichloroethane ug/L ND 0.50 03/21/23 18:24
1,1-Dichloroethene ug/L ND 0.50 03/21/23 18:24
1,1-Dichloropropene ug/L ND 0.50 03/21/23 18:24
1,2,3-Trichlorobenzene ug/L ND 2.0 03/21/23 18:24
1,2,3-Trichloropropane ug/L ND 0.50 03/21/23 18:24
1,2,4-Trichlorobenzene ug/L ND 2.0 03/21/23 18:24
1,2,4-Trimethylbenzene ug/L ND 0.50 03/21/23 18:24
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/21/23 18:24
1,2-Dibromoethane (EDB)ug/L ND 0.50 03/21/23 18:24
1,2-Dichlorobenzene ug/L ND 0.50 03/21/23 18:24
1,2-Dichloroethane ug/L ND 0.50 03/21/23 18:24
1,2-Dichloropropane ug/L ND 0.50 03/21/23 18:24
1,3,5-Trimethylbenzene ug/L ND 0.50 03/21/23 18:24
1,3-Dichlorobenzene ug/L ND 0.50 03/21/23 18:24
1,3-Dichloropropane ug/L ND 0.50 03/21/23 18:24
1,4-Dichlorobenzene ug/L ND 0.50 03/21/23 18:24
2,2-Dichloropropane ug/L ND 0.50 03/21/23 18:24
2-Chlorotoluene ug/L ND 0.50 03/21/23 18:24
4-Chlorotoluene ug/L ND 0.50 03/21/23 18:24
Benzene ug/L ND 0.50 03/21/23 18:24
Bromobenzene ug/L ND 0.50 03/21/23 18:24
Bromochloromethane ug/L ND 0.50 03/21/23 18:24
Bromodichloromethane ug/L ND 0.50 03/21/23 18:24
Bromoform ug/L ND 0.50 03/21/23 18:24
Bromomethane ug/L ND 5.0 03/21/23 18:24
Carbon tetrachloride ug/L ND 0.50 03/21/23 18:24
Chlorobenzene ug/L ND 0.50 03/21/23 18:24
Chloroethane ug/L ND 1.0 03/21/23 18:24
Chloroform ug/L ND 0.50 03/21/23 18:24
Chloromethane ug/L ND 1.0 03/21/23 18:24
cis-1,2-Dichloroethene ug/L ND 0.50 03/21/23 18:24
cis-1,3-Dichloropropene ug/L ND 0.50 03/21/23 18:24
Dibromochloromethane ug/L ND 0.50 03/21/23 18:24
Dibromomethane ug/L ND 0.50 03/21/23 18:24
Dichlorodifluoromethane ug/L ND 0.50 03/21/23 18:24
Diisopropyl ether ug/L ND 0.50 03/21/23 18:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 17 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3960535
Associated Lab Samples:92656753001, 92656753002, 92656753003, 92656753005, 92656753007
Matrix:Water
Analyzed
Ethanol ug/L ND 200 03/21/23 18:24
Ethyl-tert-butyl ether ug/L ND 10.0 03/21/23 18:24
Ethylbenzene ug/L ND 0.50 03/21/23 18:24
Hexachloro-1,3-butadiene ug/L ND 2.0 03/21/23 18:24
Isopropylbenzene (Cumene)ug/L ND 0.50 03/21/23 18:24
m&p-Xylene ug/L ND 1.0 03/21/23 18:24
Methyl-tert-butyl ether ug/L ND 0.50 03/21/23 18:24
Methylene Chloride ug/L ND 2.0 03/21/23 18:24
n-Butylbenzene ug/L ND 0.50 03/21/23 18:24
n-Propylbenzene ug/L ND 0.50 03/21/23 18:24
Naphthalene ug/L ND 2.0 03/21/23 18:24
o-Xylene ug/L ND 0.50 03/21/23 18:24
sec-Butylbenzene ug/L ND 0.50 03/21/23 18:24
Styrene ug/L ND 0.50 03/21/23 18:24
tert-Amyl Alcohol ug/L ND 100 03/21/23 18:24
tert-Amylmethyl ether ug/L ND 10.0 03/21/23 18:24
tert-Butyl Alcohol ug/L ND 50.0 03/21/23 18:24
tert-Butyl Formate ug/L ND 50.0 03/21/23 18:24
tert-Butylbenzene ug/L ND 0.50 03/21/23 18:24
Tetrachloroethene ug/L ND 0.50 03/21/23 18:24
Toluene ug/L ND 0.50 03/21/23 18:24
trans-1,2-Dichloroethene ug/L ND 0.50 03/21/23 18:24
trans-1,3-Dichloropropene ug/L ND 0.50 03/21/23 18:24
Trichloroethene ug/L ND 0.50 03/21/23 18:24
Trichlorofluoromethane ug/L ND 1.0 03/21/23 18:24
Vinyl chloride ug/L ND 1.0 03/21/23 18:24
1,2-Dichloroethane-d4 (S)%98 70-130 03/21/23 18:24
4-Bromofluorobenzene (S)%98 70-130 03/21/23 18:24
Toluene-d8 (S)%104 70-130 03/21/23 18:24
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3960536LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.220 96 60-140
1,1,1-Trichloroethane ug/L 18.920 94 60-140
1,1,2,2-Tetrachloroethane ug/L 19.520 98 60-140
1,1,2-Trichloroethane ug/L 17.720 88 60-140
1,1-Dichloroethane ug/L 19.020 95 60-140
1,1-Dichloroethene ug/L 19.620 98 60-140
1,1-Dichloropropene ug/L 21.320 107 60-140
1,2,3-Trichlorobenzene ug/L 19.420 97 60-140
1,2,3-Trichloropropane ug/L 19.320 96 60-140
1,2,4-Trichlorobenzene ug/L 19.120 95 60-140
1,2,4-Trimethylbenzene ug/L 19.820 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 18 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3960536LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 18.120 91 60-140
1,2-Dibromoethane (EDB)ug/L 19.220 96 60-140
1,2-Dichlorobenzene ug/L 19.920 99 60-140
1,2-Dichloroethane ug/L 18.920 94 60-140
1,2-Dichloropropane ug/L 18.820 94 60-140
1,3,5-Trimethylbenzene ug/L 19.920 100 60-140
1,3-Dichlorobenzene ug/L 20.120 101 60-140
1,3-Dichloropropane ug/L 19.320 97 60-140
1,4-Dichlorobenzene ug/L 19.620 98 60-140
2,2-Dichloropropane ug/L 18.920 95 60-140
2-Chlorotoluene ug/L 20.220 101 60-140
4-Chlorotoluene ug/L 20.420 102 60-140
Benzene ug/L 19.620 98 60-140
Bromobenzene ug/L 19.420 97 60-140
Bromochloromethane ug/L 18.820 94 60-140
Bromodichloromethane ug/L 17.820 89 60-140
Bromoform ug/L 17.720 89 60-140
Bromomethane ug/L 21.220 106 60-140
Carbon tetrachloride ug/L 19.720 99 60-140
Chlorobenzene ug/L 19.320 96 60-140
Chloroethane ug/L 23.420 117 60-140
Chloroform ug/L 19.620 98 60-140
Chloromethane ug/L 20.520 102 60-140
cis-1,2-Dichloroethene ug/L 18.820 94 60-140
cis-1,3-Dichloropropene ug/L 18.820 94 60-140
Dibromochloromethane ug/L 18.020 90 60-140
Dibromomethane ug/L 18.220 91 60-140
Dichlorodifluoromethane ug/L 22.120 110 60-140
Diisopropyl ether ug/L 17.320 86 60-140
Ethanol ug/L 908800 113 60-140
Ethyl-tert-butyl ether ug/L 34.740 87 60-140
Ethylbenzene ug/L 19.820 99 60-140
Hexachloro-1,3-butadiene ug/L 19.720 99 60-140
Isopropylbenzene (Cumene)ug/L 19.620 98 60-140
m&p-Xylene ug/L 39.540 99 60-140
Methyl-tert-butyl ether ug/L 17.920 89 60-140
Methylene Chloride ug/L 20.420 102 60-140
n-Butylbenzene ug/L 20.920 105 60-140
n-Propylbenzene ug/L 19.920 99 60-140
Naphthalene ug/L 20.020 100 60-140
o-Xylene ug/L 18.920 95 60-140
sec-Butylbenzene ug/L 19.920 100 60-140
Styrene ug/L 19.120 95 60-140
tert-Amyl Alcohol ug/L 364400 91 60-140
tert-Amylmethyl ether ug/L 38.140 95 60-140
tert-Butyl Alcohol ug/L 173200 86 60-140
tert-Butyl Formate ug/L 142160 89 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 19 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3960536LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 16.520 83 60-140
Tetrachloroethene ug/L 18.620 93 60-140
Toluene ug/L 18.920 94 60-140
trans-1,2-Dichloroethene ug/L 18.820 94 60-140
trans-1,3-Dichloropropene ug/L 18.320 92 60-140
Trichloroethene ug/L 19.520 98 60-140
Trichlorofluoromethane ug/L 22.420 112 60-140
Vinyl chloride ug/L 17.020 85 60-140
1,2-Dichloroethane-d4 (S)%106 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3960537MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92657441005
3960538
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 114 60-140107 6 3020ND22.8 21.4
1,1,1-Trichloroethane ug/L 20 87 60-14080 8 3020ND17.4 16.1
1,1,2,2-Tetrachloroethane ug/L 20 120 60-140108 10 3020ND23.9 21.7
1,1,2-Trichloroethane ug/L 20 100 60-14091 9 3020ND19.9 18.2
1,1-Dichloroethane ug/L 20 84 60-14074 12 3020ND16.8 14.9
1,1-Dichloroethene ug/L 20 73 60-14066 10 3020ND14.6 13.2
1,1-Dichloropropene ug/L 20 93 60-14087 7 3020ND18.7 17.3
1,2,3-Trichlorobenzene ug/L 20 120 60-140116 3 3020ND23.9 23.2
1,2,3-Trichloropropane ug/L 20 118 60-140109 8 3020ND23.7 21.7
1,2,4-Trichlorobenzene ug/L 20 117 60-140111 5 3020ND23.4 22.3
1,2,4-Trimethylbenzene ug/L 20 119 60-140110 8 3020ND23.8 21.9
1,2-Dibromo-3-
chloropropane ug/L 20 103 60-140100 2 3020ND20.5 20.0
1,2-Dibromoethane (EDB)ug/L 20 111 60-140101 9 3020ND22.2 20.2
1,2-Dichlorobenzene ug/L 20 119 60-140111 7 3020ND23.9 22.3
1,2-Dichloroethane ug/L 20 95 60-14086 10 3020ND19.1 17.2
1,2-Dichloropropane ug/L 20 98 60-14090 9 3020ND19.6 18.0
1,3,5-Trimethylbenzene ug/L 20 119 60-140110 8 3020ND23.9 22.1
1,3-Dichlorobenzene ug/L 20 118 60-140113 4 3020ND23.7 22.7
1,3-Dichloropropane ug/L 20 112 60-140104 8 3020ND22.4 20.7
1,4-Dichlorobenzene ug/L 20 118 60-140111 7 3020ND23.7 22.1
2,2-Dichloropropane ug/L 20 85 60-14076 11 3020ND17.0 15.3
2-Chlorotoluene ug/L 20 118 60-140108 9 3020ND23.5 21.5
4-Chlorotoluene ug/L 20 119 60-140111 6 3020ND23.7 22.2
Benzene ug/L 20 90 60-14081 10 3020ND18.0 16.3
Bromobenzene ug/L 20 114 60-140108 5 3020ND22.7 21.5
Bromochloromethane ug/L 20 88 60-14077 13 3020ND17.6 15.4
Bromodichloromethane ug/L 20 98 60-14089 9 3020ND19.6 17.9
Bromoform ug/L 20 106 60-140100 6 3020ND21.2 19.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 20 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3960537MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92657441005
3960538
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L M1206160-14053 14 3020ND12.2 10.6
Carbon tetrachloride ug/L 20 91 60-14085 6 3020ND18.1 17.1
Chlorobenzene ug/L 20 112 60-140103 8 3020ND22.4 20.6
Chloroethane ug/L 20 76 60-14068 12 3020ND15.2 13.5
Chloroform ug/L 20 95 60-14086 9 3020ND19.0 17.3
Chloromethane ug/L M1203460-14030 11 3020ND6.8 6.1
cis-1,2-Dichloroethene ug/L 20 86 60-14078 10 3020ND17.2 15.6
cis-1,3-Dichloropropene ug/L 20 99 60-14091 8 3020ND19.9 18.3
Dibromochloromethane ug/L 20 105 60-14098 7 3020ND21.0 19.5
Dibromomethane ug/L 20 96 60-14087 9 3020ND19.1 17.4
Dichlorodifluoromethane ug/L M1201660-14014 13 3020ND3.1 2.7
Diisopropyl ether ug/L 20 82 60-14074 10 3020ND16.3 14.7
Ethanol ug/L 800 121 60-140119 1 30800ND967955
Ethyl-tert-butyl ether ug/L 40 82 60-14075 8 3040ND32.8 30.1
Ethylbenzene ug/L 20 114 60-140106 7 3020ND22.7 21.2
Hexachloro-1,3-butadiene ug/L 20 128 60-140118 8 3020ND25.5 23.6
Isopropylbenzene
(Cumene)ug/L 20 117 60-140107 9 3020ND23.5 21.4
m&p-Xylene ug/L 40 113 60-140104 8 3040ND45.3 41.7
Methyl-tert-butyl ether ug/L 20 75 60-14069 8 3020ND15.1 13.9
Methylene Chloride ug/L 20 91 60-14080 14 3020ND18.2 15.9
n-Butylbenzene ug/L 20 131 60-140121 7 3020ND26.1 24.3
n-Propylbenzene ug/L 20 120 60-140111 8 3020ND23.9 22.2
Naphthalene ug/L 20 116 60-140113 2 3020ND23.1 22.7
o-Xylene ug/L 20 109 60-140101 8 3020ND21.9 20.3
sec-Butylbenzene ug/L 20 125 60-140115 8 3020ND24.9 22.9
Styrene ug/L 20 112 60-140102 9 3020ND22.4 20.5
tert-Amyl Alcohol ug/L 400 106 60-140107 1 30400ND422427
tert-Amylmethyl ether ug/L 40 98 60-14090 8 3040ND39.1 36.1
tert-Butyl Alcohol ug/L 200 112 60-140118 6 30200ND224237
tert-Butyl Formate ug/L M11602760-14022 30160ND43.8J 35.6J
tert-Butylbenzene ug/L 20 99 60-14093 7 3020ND19.9 18.6
Tetrachloroethene ug/L 20 99 60-14096 4 3020ND19.9 19.2
Toluene ug/L 20 99 60-14091 8 3020ND19.7 18.2
trans-1,2-Dichloroethene ug/L 20 76 60-14070 8 3020ND15.2 14.0
trans-1,3-Dichloropropene ug/L 20 102 60-14094 8 3020ND20.3 18.7
Trichloroethene ug/L 20 96 60-14089 8 3020ND19.3 17.8
Trichlorofluoromethane ug/L 20 80 60-14071 11 3020ND15.9 14.2
Vinyl chloride ug/L M1203960-14034 15 3020ND7.8 6.8
1,2-Dichloroethane-d4 (S)%108 70-130104
4-Bromofluorobenzene (S)%98 70-13097
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 21 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
763134
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92656753006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3963479
Associated Lab Samples:92656753006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/23/23 11:23
1,1,1-Trichloroethane ug/L ND 0.50 03/23/23 11:23
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/23/23 11:23
1,1,2-Trichloroethane ug/L ND 0.50 03/23/23 11:23
1,1-Dichloroethane ug/L ND 0.50 03/23/23 11:23
1,1-Dichloroethene ug/L ND 0.50 03/23/23 11:23
1,1-Dichloropropene ug/L ND 0.50 03/23/23 11:23
1,2,3-Trichlorobenzene ug/L ND 2.0 03/23/23 11:23
1,2,3-Trichloropropane ug/L ND 0.50 03/23/23 11:23
1,2,4-Trichlorobenzene ug/L ND 2.0 03/23/23 11:23
1,2,4-Trimethylbenzene ug/L ND 0.50 03/23/23 11:23
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/23/23 11:23
1,2-Dibromoethane (EDB)ug/L ND 0.50 03/23/23 11:23
1,2-Dichlorobenzene ug/L ND 0.50 03/23/23 11:23
1,2-Dichloroethane ug/L ND 0.50 03/23/23 11:23
1,2-Dichloropropane ug/L ND 0.50 03/23/23 11:23
1,3,5-Trimethylbenzene ug/L ND 0.50 03/23/23 11:23
1,3-Dichlorobenzene ug/L ND 0.50 03/23/23 11:23
1,3-Dichloropropane ug/L ND 0.50 03/23/23 11:23
1,4-Dichlorobenzene ug/L ND 0.50 03/23/23 11:23
2,2-Dichloropropane ug/L ND 0.50 03/23/23 11:23
2-Chlorotoluene ug/L ND 0.50 03/23/23 11:23
4-Chlorotoluene ug/L ND 0.50 03/23/23 11:23
Benzene ug/L ND 0.50 03/23/23 11:23
Bromobenzene ug/L ND 0.50 03/23/23 11:23
Bromochloromethane ug/L ND 0.50 03/23/23 11:23
Bromodichloromethane ug/L ND 0.50 03/23/23 11:23
Bromoform ug/L ND 0.50 03/23/23 11:23
Bromomethane ug/L ND 5.0 03/23/23 11:23
Carbon tetrachloride ug/L ND 0.50 03/23/23 11:23
Chlorobenzene ug/L ND 0.50 03/23/23 11:23
Chloroethane ug/L ND 1.0 03/23/23 11:23
Chloroform ug/L ND 0.50 03/23/23 11:23
Chloromethane ug/L ND 1.0 03/23/23 11:23
cis-1,2-Dichloroethene ug/L ND 0.50 03/23/23 11:23
cis-1,3-Dichloropropene ug/L ND 0.50 03/23/23 11:23
Dibromochloromethane ug/L ND 0.50 03/23/23 11:23
Dibromomethane ug/L ND 0.50 03/23/23 11:23
Dichlorodifluoromethane ug/L ND 0.50 03/23/23 11:23
Diisopropyl ether ug/L ND 0.50 03/23/23 11:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 22 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3963479
Associated Lab Samples:92656753006
Matrix:Water
Analyzed
Ethanol ug/L ND 200 03/23/23 11:23
Ethyl-tert-butyl ether ug/L ND 10.0 03/23/23 11:23
Ethylbenzene ug/L ND 0.50 03/23/23 11:23
Hexachloro-1,3-butadiene ug/L ND 2.0 03/23/23 11:23
Isopropylbenzene (Cumene)ug/L ND 0.50 03/23/23 11:23
m&p-Xylene ug/L ND 1.0 03/23/23 11:23
Methyl-tert-butyl ether ug/L ND 0.50 03/23/23 11:23
Methylene Chloride ug/L ND 2.0 03/23/23 11:23
n-Butylbenzene ug/L ND 0.50 03/23/23 11:23
n-Propylbenzene ug/L ND 0.50 03/23/23 11:23
Naphthalene ug/L ND 2.0 03/23/23 11:23
o-Xylene ug/L ND 0.50 03/23/23 11:23
sec-Butylbenzene ug/L ND 0.50 03/23/23 11:23
Styrene ug/L ND 0.50 03/23/23 11:23
tert-Amyl Alcohol ug/L ND 100 03/23/23 11:23
tert-Amylmethyl ether ug/L ND 10.0 03/23/23 11:23
tert-Butyl Alcohol ug/L ND 50.0 03/23/23 11:23
tert-Butyl Formate ug/L ND 50.0 03/23/23 11:23
tert-Butylbenzene ug/L ND 0.50 03/23/23 11:23
Tetrachloroethene ug/L ND 0.50 03/23/23 11:23
Toluene ug/L ND 0.50 03/23/23 11:23
trans-1,2-Dichloroethene ug/L ND 0.50 03/23/23 11:23
trans-1,3-Dichloropropene ug/L ND 0.50 03/23/23 11:23
Trichloroethene ug/L ND 0.50 03/23/23 11:23
Trichlorofluoromethane ug/L ND 1.0 03/23/23 11:23
Vinyl chloride ug/L ND 1.0 03/23/23 11:23
1,2-Dichloroethane-d4 (S)%94 70-130 03/23/23 11:23
4-Bromofluorobenzene (S)%92 70-130 03/23/23 11:23
Toluene-d8 (S)%107 70-130 03/23/23 11:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3963480LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 22.220 111 60-140
1,1,1-Trichloroethane ug/L 21.520 108 60-140
1,1,2,2-Tetrachloroethane ug/L 21.720 109 60-140
1,1,2-Trichloroethane ug/L 22.620 113 60-140
1,1-Dichloroethane ug/L 20.520 102 60-140
1,1-Dichloroethene ug/L 20.920 104 60-140
1,1-Dichloropropene ug/L 23.420 117 60-140
1,2,3-Trichlorobenzene ug/L 20.120 101 60-140
1,2,3-Trichloropropane ug/L 22.620 113 60-140
1,2,4-Trichlorobenzene ug/L 20.520 103 60-140
1,2,4-Trimethylbenzene ug/L 20.220 101 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 23 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3963480LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 21.120 106 60-140
1,2-Dibromoethane (EDB)ug/L 21.820 109 60-140
1,2-Dichlorobenzene ug/L 21.820 109 60-140
1,2-Dichloroethane ug/L 20.120 100 60-140
1,2-Dichloropropane ug/L 21.420 107 60-140
1,3,5-Trimethylbenzene ug/L 21.920 110 60-140
1,3-Dichlorobenzene ug/L 22.220 111 60-140
1,3-Dichloropropane ug/L 20.420 102 60-140
1,4-Dichlorobenzene ug/L 22.620 113 60-140
2,2-Dichloropropane ug/L 20.120 101 60-140
2-Chlorotoluene ug/L 20.420 102 60-140
4-Chlorotoluene ug/L 21.420 107 60-140
Benzene ug/L 21.120 106 60-140
Bromobenzene ug/L 21.320 107 60-140
Bromochloromethane ug/L 19.520 98 60-140
Bromodichloromethane ug/L 21.820 109 60-140
Bromoform ug/L 21.020 105 60-140
Bromomethane ug/L 18.020 90 60-140
Carbon tetrachloride ug/L 21.020 105 60-140
Chlorobenzene ug/L 23.220 116 60-140
Chloroethane ug/L 21.820 109 60-140
Chloroform ug/L 21.320 106 60-140
Chloromethane ug/L 21.320 106 60-140
cis-1,2-Dichloroethene ug/L 20.820 104 60-140
cis-1,3-Dichloropropene ug/L 20.920 104 60-140
Dibromochloromethane ug/L 21.520 108 60-140
Dibromomethane ug/L 20.920 105 60-140
Dichlorodifluoromethane ug/L 18.620 93 60-140
Diisopropyl ether ug/L 18.820 94 60-140
Ethanol ug/L 725800 91 60-140
Ethyl-tert-butyl ether ug/L 36.840 92 60-140
Ethylbenzene ug/L 21.120 106 60-140
Hexachloro-1,3-butadiene ug/L 18.720 94 60-140
Isopropylbenzene (Cumene)ug/L 22.720 113 60-140
m&p-Xylene ug/L 42.040 105 60-140
Methyl-tert-butyl ether ug/L 18.920 95 60-140
Methylene Chloride ug/L 21.720 109 60-140
n-Butylbenzene ug/L 21.720 109 60-140
n-Propylbenzene ug/L 21.320 106 60-140
Naphthalene ug/L 19.320 96 60-140
o-Xylene ug/L 22.420 112 60-140
sec-Butylbenzene ug/L 21.120 105 60-140
Styrene ug/L 21.720 108 60-140
tert-Amyl Alcohol ug/L 379400 95 60-140
tert-Amylmethyl ether ug/L 38.840 97 60-140
tert-Butyl Alcohol ug/L 174200 87 60-140
tert-Butyl Formate ug/L 150160 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 24 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3963480LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 18.020 90 60-140
Tetrachloroethene ug/L 20.720 103 60-140
Toluene ug/L 21.020 105 60-140
trans-1,2-Dichloroethene ug/L 21.920 109 60-140
trans-1,3-Dichloropropene ug/L 20.920 104 60-140
Trichloroethene ug/L 22.720 114 60-140
Trichlorofluoromethane ug/L 19.020 95 60-140
Vinyl chloride ug/L 17.320 86 60-140
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3963481MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92657997001
3963482
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 111 60-140123 11 3020ND22.1 24.6
1,1,1-Trichloroethane ug/L 20 107 60-140119 10 3020ND21.5 23.8
1,1,2,2-Tetrachloroethane ug/L 20 106 60-140115 8 3020ND21.2 23.0
1,1,2-Trichloroethane ug/L 20 113 60-140117 3 3020ND22.7 23.3
1,1-Dichloroethane ug/L 20 101 60-140108 6 3020ND20.2 21.5
1,1-Dichloroethene ug/L 20 108 60-140121 12 3020ND21.5 24.2
1,1-Dichloropropene ug/L 20 123 60-140132 7 3020ND24.6 26.5
1,2,3-Trichlorobenzene ug/L 20 90 60-140103 13 3020ND18.1 20.6
1,2,3-Trichloropropane ug/L 20 104 60-140121 15 3020ND20.8 24.3
1,2,4-Trichlorobenzene ug/L 20 88 60-140101 14 3020ND17.7 20.2
1,2,4-Trimethylbenzene ug/L 20 93 60-140109 16 3020ND18.6 21.8
1,2-Dibromo-3-
chloropropane ug/L 20 96 60-140104 8 3020ND19.2 20.8
1,2-Dibromoethane (EDB)ug/L 20 108 60-140122 12 3020ND21.6 24.5
1,2-Dichlorobenzene ug/L 20 98 60-140111 13 3020ND19.5 22.2
1,2-Dichloroethane ug/L 20 102 60-140109 6 3020ND20.5 21.8
1,2-Dichloropropane ug/L 20 113 60-140117 4 3020ND22.6 23.5
1,3,5-Trimethylbenzene ug/L 20 100 60-140112 12 3020ND19.9 22.5
1,3-Dichlorobenzene ug/L 20 100 60-140114 13 3020ND19.9 22.8
1,3-Dichloropropane ug/L 20 98 60-140114 15 3020ND19.5 22.7
1,4-Dichlorobenzene ug/L 20 95 60-140107 11 3020ND19.0 21.3
2,2-Dichloropropane ug/L 20 101 60-140109 8 3020ND20.2 21.9
2-Chlorotoluene ug/L 20 95 60-140104 9 3020ND18.9 20.7
4-Chlorotoluene ug/L 20 93 60-140109 15 3020ND18.7 21.8
Benzene ug/L 20 108 60-140112 3 3020ND21.6 22.4
Bromobenzene ug/L 20 95 60-140106 11 3020ND19.0 21.2
Bromochloromethane ug/L 20 106 60-140114 8 3020ND21.2 22.9
Bromodichloromethane ug/L 20 110 60-140113 3 3020ND21.9 22.7
Bromoform ug/L 20 103 60-140109 6 3020ND20.5 21.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 25 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3963481MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92657997001
3963482
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 86 60-14096 10 3020ND17.3 19.2
Carbon tetrachloride ug/L 20 115 60-140124 7 3020ND23.1 24.7
Chlorobenzene ug/L 20 110 60-140118 8 3020ND21.9 23.6
Chloroethane ug/L 20 124 60-140123 1 3020ND24.7 24.5
Chloroform ug/L 20 104 60-140120 14 3020ND20.8 23.9
Chloromethane ug/L 20 102 60-140113 10 3020ND20.4 22.5
cis-1,2-Dichloroethene ug/L 20 100 60-140110 9 3020ND20.1 22.0
cis-1,3-Dichloropropene ug/L 20 105 60-140113 7 3020ND21.0 22.5
Dibromochloromethane ug/L 20 96 60-140112 16 3020ND19.1 22.4
Dibromomethane ug/L 20 104 60-140113 8 3020ND20.8 22.6
Dichlorodifluoromethane ug/L 20 100 60-140118 16 3020ND20.1 23.6
Diisopropyl ether ug/L 20 96 60-140104 8 3020ND19.1 20.8
Ethanol ug/L 800 94 60-14098 3 30800ND755780
Ethyl-tert-butyl ether ug/L 40 91 60-140100 9 3040ND36.5 39.9
Ethylbenzene ug/L 20 101 60-140112 10 3020ND20.2 22.4
Hexachloro-1,3-butadiene ug/L 20 81 60-140104 25 3020ND16.1 20.7
Isopropylbenzene
(Cumene)ug/L 20 106 60-140117 10 3020ND21.1 23.3
m&p-Xylene ug/L 40 105 60-140111 6 3040ND42.0 44.4
Methyl-tert-butyl ether ug/L 20 93 60-14098 5 3020ND18.6 19.6
Methylene Chloride ug/L 20 96 60-140109 13 3020ND19.1 21.9
n-Butylbenzene ug/L 20 94 60-140108 13 3020ND18.9 21.5
n-Propylbenzene ug/L 20 96 60-140108 12 3020ND19.1 21.6
Naphthalene ug/L 20 90 60-140106 17 3020ND17.9 21.2
o-Xylene ug/L 20 104 60-140116 10 3020ND20.9 23.1
sec-Butylbenzene ug/L 20 95 60-140111 15 3020ND19.1 22.3
Styrene ug/L 20 100 60-140109 9 3020ND20.0 21.8
tert-Amyl Alcohol ug/L 400 99 60-140102 3 30400ND397408
tert-Amylmethyl ether ug/L 40 99 60-140107 8 3040ND39.7 42.9
tert-Butyl Alcohol ug/L 200 129 60-140140 8 30200ND258281
tert-Butyl Formate ug/L P5160560-1406 30160NDNDND
tert-Butylbenzene ug/L 20 82 60-14095 14 3020ND16.4 18.9
Tetrachloroethene ug/L 20 103 60-140111 7 3020ND20.6 22.2
Toluene ug/L 20 106 60-140114 7 3020ND21.2 22.8
trans-1,2-Dichloroethene ug/L 20 110 60-140119 7 3020ND22.1 23.7
trans-1,3-Dichloropropene ug/L 20 102 60-140106 4 3020ND20.5 21.3
Trichloroethene ug/L 20 118 60-140122 3 3020ND23.6 24.3
Trichlorofluoromethane ug/L 20 110 60-140116 5 3020ND22.1 23.3
Vinyl chloride ug/L 20 87 60-140103 17 3020ND17.5 20.6
1,2-Dichloroethane-d4 (S)%101 70-130103
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%98 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
763139
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92656753004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3963499
Associated Lab Samples:92656753004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 03/23/23 15:17
1,1,1-Trichloroethane ug/L ND 0.50 03/23/23 15:17
1,1,2,2-Tetrachloroethane ug/L ND 0.50 03/23/23 15:17
1,1,2-Trichloroethane ug/L ND 0.50 03/23/23 15:17
1,1-Dichloroethane ug/L ND 0.50 03/23/23 15:17
1,1-Dichloroethene ug/L ND 0.50 03/23/23 15:17
1,1-Dichloropropene ug/L ND 0.50 03/23/23 15:17
1,2,3-Trichlorobenzene ug/L ND 2.0 03/23/23 15:17
1,2,3-Trichloropropane ug/L ND 0.50 03/23/23 15:17
1,2,4-Trichlorobenzene ug/L ND 2.0 03/23/23 15:17
1,2,4-Trimethylbenzene ug/L ND 0.50 03/23/23 15:17
1,2-Dibromo-3-chloropropane ug/L ND 1.0 03/23/23 15:17
1,2-Dibromoethane (EDB)ug/L ND 0.50 03/23/23 15:17
1,2-Dichlorobenzene ug/L ND 0.50 03/23/23 15:17
1,2-Dichloroethane ug/L ND 0.50 03/23/23 15:17
1,2-Dichloropropane ug/L ND 0.50 03/23/23 15:17
1,3,5-Trimethylbenzene ug/L ND 0.50 03/23/23 15:17
1,3-Dichlorobenzene ug/L ND 0.50 03/23/23 15:17
1,3-Dichloropropane ug/L ND 0.50 03/23/23 15:17
1,4-Dichlorobenzene ug/L ND 0.50 03/23/23 15:17
2,2-Dichloropropane ug/L ND 0.50 03/23/23 15:17
2-Chlorotoluene ug/L ND 0.50 03/23/23 15:17
4-Chlorotoluene ug/L ND 0.50 03/23/23 15:17
Benzene ug/L ND 0.50 03/23/23 15:17
Bromobenzene ug/L ND 0.50 03/23/23 15:17
Bromochloromethane ug/L ND 0.50 03/23/23 15:17
Bromodichloromethane ug/L ND 0.50 03/23/23 15:17
Bromoform ug/L ND 0.50 03/23/23 15:17
Bromomethane ug/L ND 5.0 03/23/23 15:17
Carbon tetrachloride ug/L ND 0.50 03/23/23 15:17
Chlorobenzene ug/L ND 0.50 03/23/23 15:17
Chloroethane ug/L ND 1.0 03/23/23 15:17
Chloroform ug/L ND 0.50 03/23/23 15:17
Chloromethane ug/L ND 1.0 03/23/23 15:17
cis-1,2-Dichloroethene ug/L ND 0.50 03/23/23 15:17
cis-1,3-Dichloropropene ug/L ND 0.50 03/23/23 15:17
Dibromochloromethane ug/L ND 0.50 03/23/23 15:17
Dibromomethane ug/L ND 0.50 03/23/23 15:17
Dichlorodifluoromethane ug/L ND 0.50 03/23/23 15:17
Diisopropyl ether ug/L ND 0.50 03/23/23 15:17
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3963499
Associated Lab Samples:92656753004
Matrix:Water
Analyzed
Ethanol ug/L ND 200 03/23/23 15:17
Ethyl-tert-butyl ether ug/L ND 10.0 03/23/23 15:17
Ethylbenzene ug/L ND 0.50 03/23/23 15:17
Hexachloro-1,3-butadiene ug/L ND 2.0 03/23/23 15:17
Isopropylbenzene (Cumene)ug/L ND 0.50 03/23/23 15:17
m&p-Xylene ug/L ND 1.0 03/23/23 15:17
Methyl-tert-butyl ether ug/L ND 0.50 03/23/23 15:17
Methylene Chloride ug/L ND 2.0 03/23/23 15:17
n-Butylbenzene ug/L ND 0.50 03/23/23 15:17
n-Propylbenzene ug/L ND 0.50 03/23/23 15:17
Naphthalene ug/L ND 2.0 03/23/23 15:17
o-Xylene ug/L ND 0.50 03/23/23 15:17
sec-Butylbenzene ug/L ND 0.50 03/23/23 15:17
Styrene ug/L ND 0.50 03/23/23 15:17
tert-Amyl Alcohol ug/L ND 100 03/23/23 15:17
tert-Amylmethyl ether ug/L ND 10.0 03/23/23 15:17
tert-Butyl Alcohol ug/L ND 50.0 03/23/23 15:17
tert-Butyl Formate ug/L ND 50.0 03/23/23 15:17
tert-Butylbenzene ug/L ND 0.50 03/23/23 15:17
Tetrachloroethene ug/L ND 0.50 03/23/23 15:17
Toluene ug/L ND 0.50 03/23/23 15:17
trans-1,2-Dichloroethene ug/L ND 0.50 03/23/23 15:17
trans-1,3-Dichloropropene ug/L ND 0.50 03/23/23 15:17
Trichloroethene ug/L ND 0.50 03/23/23 15:17
Trichlorofluoromethane ug/L ND 1.0 03/23/23 15:17
Vinyl chloride ug/L ND 1.0 03/23/23 15:17
1,2-Dichloroethane-d4 (S)%100 70-130 03/23/23 15:17
4-Bromofluorobenzene (S)%97 70-130 03/23/23 15:17
Toluene-d8 (S)%102 70-130 03/23/23 15:17
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3963500LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.120 90 60-140
1,1,1-Trichloroethane ug/L 16.920 85 60-140
1,1,2,2-Tetrachloroethane ug/L 18.320 91 60-140
1,1,2-Trichloroethane ug/L 16.720 83 60-140
1,1-Dichloroethane ug/L 16.920 84 60-140
1,1-Dichloroethene ug/L 17.020 85 60-140
1,1-Dichloropropene ug/L 19.120 96 60-140
1,2,3-Trichlorobenzene ug/L 18.820 94 60-140
1,2,3-Trichloropropane ug/L 18.620 93 60-140
1,2,4-Trichlorobenzene ug/L 18.820 94 60-140
1,2,4-Trimethylbenzene ug/L 19.020 95 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3963500LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/L 16.820 84 60-140
1,2-Dibromoethane (EDB)ug/L 17.920 89 60-140
1,2-Dichlorobenzene ug/L 19.520 98 60-140
1,2-Dichloroethane ug/L 17.820 89 60-140
1,2-Dichloropropane ug/L 18.220 91 60-140
1,3,5-Trimethylbenzene ug/L 19.120 96 60-140
1,3-Dichlorobenzene ug/L 19.020 95 60-140
1,3-Dichloropropane ug/L 18.220 91 60-140
1,4-Dichlorobenzene ug/L 18.720 93 60-140
2,2-Dichloropropane ug/L 16.520 83 60-140
2-Chlorotoluene ug/L 18.920 94 60-140
4-Chlorotoluene ug/L 19.420 97 60-140
Benzene ug/L 18.220 91 60-140
Bromobenzene ug/L 18.520 92 60-140
Bromochloromethane ug/L 16.520 83 60-140
Bromodichloromethane ug/L 16.520 82 60-140
Bromoform ug/L 15.720 78 60-140
Bromomethane ug/L 20.620 103 60-140
Carbon tetrachloride ug/L 18.020 90 60-140
Chlorobenzene ug/L 18.220 91 60-140
Chloroethane ug/L 21.620 108 60-140
Chloroform ug/L 17.420 87 60-140
Chloromethane ug/L 17.620 88 60-140
cis-1,2-Dichloroethene ug/L 16.920 85 60-140
cis-1,3-Dichloropropene ug/L 17.320 87 60-140
Dibromochloromethane ug/L 16.520 82 60-140
Dibromomethane ug/L 17.220 86 60-140
Dichlorodifluoromethane ug/L 16.320 81 60-140
Diisopropyl ether ug/L 16.420 82 60-140
Ethanol ug/L 882800 110 60-140
Ethyl-tert-butyl ether ug/L 32.440 81 60-140
Ethylbenzene ug/L 18.320 92 60-140
Hexachloro-1,3-butadiene ug/L 19.220 96 60-140
Isopropylbenzene (Cumene)ug/L 18.220 91 60-140
m&p-Xylene ug/L 36.640 91 60-140
Methyl-tert-butyl ether ug/L 16.520 82 60-140
Methylene Chloride ug/L 18.220 91 60-140
n-Butylbenzene ug/L 20.020 100 60-140
n-Propylbenzene ug/L 19.020 95 60-140
Naphthalene ug/L 18.920 95 60-140
o-Xylene ug/L 17.620 88 60-140
sec-Butylbenzene ug/L 19.220 96 60-140
Styrene ug/L 17.920 90 60-140
tert-Amyl Alcohol ug/L 390400 98 60-140
tert-Amylmethyl ether ug/L 37.040 92 60-140
tert-Butyl Alcohol ug/L 179200 89 60-140
tert-Butyl Formate ug/L 128160 80 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 29 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3963500LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/L 15.420 77 60-140
Tetrachloroethene ug/L 17.620 88 60-140
Toluene ug/L 17.720 89 60-140
trans-1,2-Dichloroethene ug/L 16.720 84 60-140
trans-1,3-Dichloropropene ug/L 17.020 85 60-140
Trichloroethene ug/L 18.120 91 60-140
Trichlorofluoromethane ug/L 20.220 101 60-140
Vinyl chloride ug/L 14.020 70 60-140
1,2-Dichloroethane-d4 (S)%104 70-130
4-Bromofluorobenzene (S)%95 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3963501MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92657944008
3963502
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 126 60-14098 26 3020ND25.2 19.5
1,1,1-Trichloroethane ug/L 20 135 60-140106 24 3020ND27.0 21.3
1,1,2,2-Tetrachloroethane ug/L 20 122 60-14097 22 3020ND24.3 19.4
1,1,2-Trichloroethane ug/L 20 125 60-14093 29 3020ND25.0 18.7
1,1-Dichloroethane ug/L 20 132 60-140103 24 3020ND26.3 20.6
1,1-Dichloroethene ug/L M12014360-140116 21 3020ND28.7 23.2
1,1-Dichloropropene ug/L M12014160-140111 24 3020ND28.3 22.2
1,2,3-Trichlorobenzene ug/L 20 103 60-14083 21 3020ND20.6 16.7
1,2,3-Trichloropropane ug/L 20 115 60-14091 23 3020ND23.1 18.3
1,2,4-Trichlorobenzene ug/L 20 100 60-14085 17 3020ND20.1 16.9
1,2,4-Trimethylbenzene ug/L 20 121 60-14095 23 3020ND24.1 19.1
1,2-Dibromo-3-
chloropropane ug/L 20 104 60-14081 24 3020ND20.7 16.2
1,2-Dibromoethane (EDB)ug/L 20 123 60-14096 25 3020ND24.6 19.1
1,2-Dichlorobenzene ug/L 20 113 60-14091 21 3020ND22.7 18.3
1,2-Dichloroethane ug/L 20 125 60-14094 28 3020ND25.0 18.8
1,2-Dichloropropane ug/L 20 125 60-14097 26 3020ND25.1 19.4
1,3,5-Trimethylbenzene ug/L 20 120 60-14096 23 3020ND24.1 19.1
1,3-Dichlorobenzene ug/L 20 115 60-14091 24 3020ND23.1 18.2
1,3-Dichloropropane ug/L 20 120 60-14094 24 3020ND24.0 18.8
1,4-Dichlorobenzene ug/L 20 112 60-14091 21 3020ND22.5 18.3
2,2-Dichloropropane ug/L 20 128 60-140100 24 3020ND25.6 20.1
2-Chlorotoluene ug/L 20 118 60-14093 24 3020ND23.7 18.5
4-Chlorotoluene ug/L 20 116 60-14094 22 3020ND23.3 18.7
Benzene ug/L 20 129 60-140102 24 3020ND25.8 20.3
Bromobenzene ug/L 20 110 60-14087 24 3020ND22.0 17.3
Bromochloromethane ug/L 20 127 60-14097 26 3020ND25.4 19.5
Bromodichloromethane ug/L 20 120 60-14093 25 3020ND23.9 18.6
Bromoform ug/L 20 116 60-14088 28 3020ND23.3 17.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 30 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3963501MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92657944008
3963502
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Bromomethane ug/L 20 100 60-14094 6 3020ND19.9 18.8
Carbon tetrachloride ug/L 20 129 60-140105 20 3020ND25.8 21.1
Chlorobenzene ug/L 20 120 60-14097 22 3020ND24.1 19.4
Chloroethane ug/L M12014460-140111 26 3020ND28.8 22.3
Chloroform ug/L 20 127 60-140103 21 3020ND25.5 20.6
Chloromethane ug/L M12014460-140117 20 3020ND28.7 23.4
cis-1,2-Dichloroethene ug/L 20 129 60-140102 23 3020ND25.9 20.5
cis-1,3-Dichloropropene ug/L 20 118 60-14091 26 3020ND23.7 18.2
Dibromochloromethane ug/L 20 123 60-14094 26 3020ND24.5 18.9
Dibromomethane ug/L 20 121 60-14092 27 3020ND24.2 18.4
Dichlorodifluoromethane ug/L M12018460-140147 22 3020ND36.7 29.4
Diisopropyl ether ug/L 20 124 60-14094 27 3020ND24.7 18.9
Ethanol ug/L 800 119 60-14099 19 30800ND956793
Ethyl-tert-butyl ether ug/L 40 116 60-14088 27 3040ND46.4 35.3
Ethylbenzene ug/L 20 120 60-14098 21 3020ND24.0 19.5
Hexachloro-1,3-butadiene ug/L 20 112 60-14094 17 3020ND22.4 18.9
Isopropylbenzene
(Cumene)ug/L 20 125 60-140100 22 3020ND25.0 20.1
m&p-Xylene ug/L 40 120 60-14097 21 3040ND47.9 38.9
Methyl-tert-butyl ether ug/L 20 112 60-14085 28 3020ND22.5 16.9
Methylene Chloride ug/L 20 121 60-14092 27 3020ND24.1 18.3
n-Butylbenzene ug/L 20 121 60-140100 19 3020ND24.3 20.1
n-Propylbenzene ug/L 20 119 60-14094 24 3020ND23.8 18.7
Naphthalene ug/L 20 107 60-14089 19 3020ND21.5 17.8
o-Xylene ug/L 20 120 60-14098 20 3020ND24.0 19.6
sec-Butylbenzene ug/L 20 123 60-14099 22 3020ND24.6 19.7
Styrene ug/L 20 120 60-14098 21 3020ND24.1 19.5
tert-Amyl Alcohol ug/L 400 107 60-14083 26 30400ND427331
tert-Amylmethyl ether ug/L 40 118 60-14090 27 3040ND47.4 36.0
tert-Butyl Alcohol ug/L 200 137 60-140114 19 30200ND275227
tert-Butyl Formate ug/L M1160160-1400 30160NDNDND
tert-Butylbenzene ug/L 20 101 60-14081 22 3020ND20.1 16.2
Tetrachloroethene ug/L 20 115 60-14095 18 3020ND22.9 19.1
Toluene ug/L 20 119 60-14095 23 3020ND23.8 19.0
trans-1,2-Dichloroethene ug/L 20 136 60-140107 23 3020ND27.1 21.5
trans-1,3-Dichloropropene ug/L 20 117 60-14089 27 3020ND23.4 17.8
Trichloroethene ug/L 20 127 60-140100 24 3020ND25.5 20.1
Trichlorofluoromethane ug/L M12014460-140115 23 3020ND28.9 23.0
Vinyl chloride ug/L 20 118 60-14095 22 3020ND23.7 19.0
1,2-Dichloroethane-d4 (S)%100 70-130101
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%97 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 31 of 36
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92656753
In & Out G-5624.8
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.P5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 32 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92656753
In & Out G-5624.8
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92656753001 762628MW-1 SM 6200B
92656753002 762628MW-2 SM 6200B
92656753003 762628MW-3 SM 6200B
92656753004 763139MW-4 SM 6200B
92656753005 762628MW-5 SM 6200B
92656753006 763134MW-6 SM 6200B
92656753007 762628DW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/28/2023 10:53 AM
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 33 of 36
Page 34 of 36
Page 35 of 36
Page 36 of 36