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HomeMy WebLinkAboutFA-7738_42025_CA_MRP_20230313Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 i TABLE OF CONTENTS 1.0 BACKGROUND ............................................................................................................... 1 1.1 SITE INFORMATION .......................................................................................................... 1 1.2 HYDROGEOLOGICAL DESCRIPTION .................................................................................... 3 1.2.1 Regional Geologic Setting ...................................................................................... 3 1.2.2 Site Hydrogeology .................................................................................................. 3 1.2.3 Subsurface Lithology.............................................................................................. 4 2.0 SITE ACTIVITIES ............................................................................................................. 4 2.1 LIQUID LEVEL MONITORING AND SAMPLING ........................................................................ 4 2.2 GROUNDWATER SAMPLING AND ANALYSIS ......................................................................... 4 3.0 RESULTS ........................................................................................................................ 5 3.1 ELEVATION MEASUREMENTS, GROUNDWATER FLOW, AND GRADIENT ................................... 5 3.2 GROUNDWATER ANALYTICAL RESULTS .............................................................................. 5 4.0 CONCLUSIONS ............................................................................................................... 7 5.0 RECOMMENDATIONS .................................................................................................... 7 6.0 REFERENCES ................................................................................................................. 8 TABLES Table 1: Monitor Well Construction Table 2: Historical Groundwater Elevations Table 3: Groundwater Elevations – March 8, 2023 Table 4: Field Parameters Table 5: Historical Groundwater Sample Data Table 6: Groundwater Analytical Results – February 15, 2023 FIGURES Figure 1: Vicinity Map Figure 2: Site Map Figure 3: Groundwater Potentiometric Map (March 8, 2023) Figure 4: Groundwater Constituent Concentrations (February 15, 2023) Figure 5: Pre-Remedial Benzene Isoconcentration Map (November 1, 2017) Figure 6: Benzene Isoconcentration Map (February 15, 2023) APPENDICES Appendix I Standard Operating Procedures Appendix II Calculations Appendix III Laboratory Analytical Results and Chain of Custody Forms Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 1 1.0 BACKGROUND 1.1 Site Information The Seminole Mart No. 2 site is located at 691 Seminole Road in Broadway, North Carolina (Figure 1). According to reports prepared by East Coast Environmental (ECE), PA, underground storage tanks (USTs) were closed at the site in 2016. The UST closure assessment encountered diesel fuel constituents that were detected with concentrations above North Carolina Department of Environmental Quality (NCDEQ) action levels at the site. Based on findings by the previous consultant, the site was classified by the NCDEQ Division of Waste Management (DWM) UST Section as a “commercial high” risk site. The following are some of the activities that have taken place at the site since September 2016: Ø One 10,000-gallon gasoline and one 4,000-gallon diesel fuel petroleum USTs were permanently closed by removal in September 2016; Ø Petroleum contamination was evident in the excavation for the diesel fuel UST due to a hole in the tank and below the former product dispensers. Approximately 204 tons of contaminated soil from released diesel fuel were excavated and removed from the site. Ø A monitor well network (Table 1) was installed by ECE, PA, in January, March, May, October, and December of 2017. The borings and well network wells were used to assess the soil near the former UST system, delineate free product on the groundwater table and delineate dissolved petroleum constituents in the groundwater. Ø Baseline groundwater monitoring events were performed by ECE, PA, in 2017 prior to implementing the remedial program. The baseline data indicated that eleven of the existing monitor wells (MW-1, MW-2, MW-3, MW-4, MW-8, MW-11, MW-12, MW-13, MW-14, MW-17 and MW-19) had a measurable thickness of free product as diesel fuel. The initial maximum free product (diesel fuel) thickness recorded in network wells in 2017 included: MW-1 - 2.85 ft., MW-2 – 1.76 ft., MW-3 – 3.0 ft., MW-4 – 1.90 ft., MW-8 – 2.48 ft., MW-11 – 5.41 ft., MW- 12 – 1.71 ft., MW-13 – 2.07 ft., MW-14 – 1.67 ft., MW-17 – 2.0 ft. and MW-19 – 1.64 ft. Ø The NCDEQ issued Injection Permit WI0600195 for the remedial approach using injection of surfactant solutions. Ø Surfactant Injection (~19,165 gallons) was performed in April 30 – May 10, 2018. Ø Aggressive fluid-vapor recovery (AFVR) was performed May 21-24, 2018, from source wells impacted by petroleum, recovered 3,205 gallons of product, surfactant/product emulsion, surfactant and petroleum-contaminated water. Ø Total fluids recovery was performed between May 25, 2018 and October 26, 2021, using automated cycling of submersible pumps to recover free product, surfactant with emulsified petroleum product and contaminated groundwater. Ø Liquid level monitoring and well maintenance activities were performed by ECE, PA, in June 2018, and gasoline was observed as free product in addition to diesel fuel on the water table. Ø The baseline data was used to calculate the quantity and concentration of the surfactant solution that would be necessary to remediate the free product plume. However, the actual maximum free product thickness was subsequently found to Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 2 be approximately double the amount that was identified during the baseline assessment due to the presence of significant gasoline free product that was located on top of the diesel free product. The gasoline free product was not identified because it was initially located above the screened intervals of the monitor wells. As the thickness of the diesel free product was reduced to below the top of the screened interval, the gasoline free product was able to enter the monitor wells. Therefore, injecting additional surfactant solution was necessary to contact and remediate the additional gasoline free product plume that was located at shallower depths than the diesel free product. Ø Product thicknesses observed after the injection were a result of the surfactant stripping product from source area soils, which included both diesel fuel and gasoline products. Ø Liquid level data following the initial injection and extraction event indicated that now 13 of the existing monitor wells had a measurable thickness of free product as diesel fuel and/or gasoline. The maximum free product thickness recorded in network wells since the initial injection event included: MW-1 – 1.89 ft., MW-2 – 3.01 ft., MW-3 – 1.55 ft., MW-4 – 0.05 ft., MW-8 – 0.67 ft., MW-9 – 0.77 ft., MW- 10 – 4.54 ft., MW-11 – 4.43 ft. (gasoline), MW-12 – 0.23 ft., MW-14 – 0.33 ft., MW-15 – 1.82 ft., MW-16 – 1.34 ft., and MW-17 – 2.96 ft (red text used to identify locations where free product was not previously observed). Well locations MW- 13 and MW-19 had no measurable thickness of free product as gasoline or diesel fuel since the first injection/extraction event. Ø Approximately 2,750 gallons of surfactant solution were injected September 6-7, 2019, approximately 2,750 gallons of surfactant were injected between October 31, and November 6, 2019, and approximately 2,900 gallons of surfactant were injected into source area wells with evidence of product skim in the well screened intervals in June 2021. Ø Total fluids recovery has been performed on source area wells where free product is persistent on the water table. Since May 2018, over 45,000 gallons of liquids contaminated with petroleum have been recovered from the site. This Groundwater Monitoring Report details the site activities that were performed and observations made from July 2022 to March 2023. Ø CLES performed well maintenance, free product recovery and liquid level monitoring between July 2022 and March 2023. Product was removed either by bailers or with pumps based on the liquid column height in the well. Since October 2021, free product recovery has been performed manually to reduce the volume of recovered groundwater that is not necessary to remove from the site. Obsevations from the overall liquid level data indicate that the aerial extent of the free product plume continues to decrease as no measurable thickness of free product was observed in wells MW-2, MW-9, MW-4, MW-12, MW-8, MW-17, MW-15, or MW-16 this sampling event. Ø Measurements of product thicknesses were observed to rebound in wells MW-1, MW-3, MW-10 and MW-12 between June 2022 and October 2022. Product recovery slowed the rebound in MW-3, MW-10 and MW-12, however, the thickness in MW-1 remains persistent due to a likely perched source of diesel fuel that continues to seep to the water table intersected by MW-1. The product thickness in MW-2 has been decreasing durin this time and the thickness in MW-11 fluctuates at a thickness close to 0.6 feet. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 3 Ø The magnitude of total volatile organic compound concentrations measured in the monitor well network indicates a dcreasing trend likely due to the removal the secondary petroleum contaminant source. Some low level rebound in benzene concrentrations in wells MW-14 and MW-19 increase the aerial extent of the benzene plume shown in Figure 6.The total thickness of free phase petroleum (diesel fuel and gasoline) continue to be managed using total fluids removal from source area wells by bailing and/or pumping that was performed during site visits. Ø Prior to sampling on February 15, 2023, groundwater level measurements were attempted using an oil-water interface probe. The instrument probe malfunctioned and measurements could not be collected on February 15. CLES had repairs made to the interface probe and returned to the site March 8, 2023 to measure liquid levels from the well network to document groundwater elevations at the site and to estimate the groundwater flow direction and hydraulic gradient on-site. Ø Groundwater samples from 18 of the network monitor wells that intersect the water table at the site were collected on February 15, 2023. Groundwater samples were submitted for laboratory analysis for volatile organic compounds (VOCs) by Method 624.1. Figure 2, Site Map, presents the site features and monitor well locations. 1.2 Hydrogeological Description 1.2.1 Regional Geologic Setting According to the North Carolina Geologic Survey, Geologic Map of North Carolina, 1985, the site rests just east of the Fall Line, or boundary between the Piedmont Upland and the Coastal Plain. Unconsolidated sediments with varying thicknesses rest non- conformably over sedimentary deposits of the Middendorf formation. The Middendorf formation consists of Cretaceous Age sand, sandstone and mudstone deposits. Groundwater occurs in residual soils that were weathered from parent sedimentary rock. Based on the surface topography depicted in the United States Geologic Survey (USGS) National Map viewer of Topographic Maps, (Figure 1), the site rests at an elevation of approximately 475 feet above mean sea level (ft-MSL). Topography on site slopes down from Seminole Road to the north-northwest, and to the south-southwest. The surface water features in the vicinity of the site are shown on Figure 1. 1.2.2 Site Hydrogeology Monitor wells installed at the site, as well as published geologic information, were used to describe site-specific hydrology. A summary of the monitor well construction of on- site monitor wells is presented in Table 1. The monitor well locations are shown on Figure 2. Groundwater levels measured March 8, 2023 in the monitor wells on site indicate that groundwater is present at depths between 38.72 feet below the top of the well casing (ft-btoc) in MW-1 and 45.39 ft-btoc in MW-16. The monitor well relative top- of-casing elevations were previously reported by ECE, PA, as measured relative to an assigned elevation of a site reference point. Historical groundwater level and elevation data as reported by ECE, PA, and recent measurements by CLES are summarized in Table 2. The groundwater potentiometric map, based on maps prepared by ECE, PA, and measurements by CLES is presented on Figure 3. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 4 1.2.3 Subsurface Lithology According to ECE, PA, the subsurface residual soils were typically composed of fine- grained clayey silt or silty clay, silt and sand to approximately 12 feet below the ground surface (ft-bgs). The fine-grained soils rested over a zone of silty sand with rounded pebbles in some locations from approximately 12 to over 20 feet in depth. Silt with sand or silty sand from below the pebble zone rested over a white silty clay layer that was encountered between 35 and 49 ft-bgs. Zones of medium and coarse sand were also observed near and below the water table. The color of the soils varied from orange red brown, yellow, white, brown, tan, orange or white with black. Bedrock was not encountered to the termination depths of the borings. 2.0 SITE ACTIVITIES 2.1 Liquid Level Monitoring and Sampling Liquid levels in the 21 network wells were measured on March 8, 2023, using an oil- water interface probe. CLES’ personnel gauged liquid levels in general accordance with the CLES Standard Operating Procedures (SOP). A copy of the CLES SOP is presented in Appendix I. The measurement device was decontaminated between measurements. A measurable thickness of gasoline/diesel fuel (>0.02 feet) as free product was present in MW-1, MW-3, and MW-11. Well MW-10 had 0.01 feet of product. No measurable thickness of petroleum product was observed in the remaining network wells that were gauged. CLES initiated purging activities to prepare for sampling. Either submersible pump with a stainless-steel motor and impeller connected to polyethylene tubing that was decontaminated before inserting it into each well, or an unused disposable bailer with nylon cord, was used to purge the water column from the well before sampling. Purge parameters including pH, conductivity and temperature were measured and the values were recorded on field forms during well purging. Field parameters representative of the aquifer before samples were collected on February 15, 2023, are summarized in Table 4. A summary of the data recorded on the field forms is presented in Appendix II. Using the March 8, 2023, groundwater level data (summarized in Table 3), groundwater elevations were calculated for network monitor wells that intersect the water table. The potentiometric surface of the groundwater table was drawn using groundwater contours of equal elevation that were estimated to predict the groundwater flow direction across the site (Figure 3). Groundwater elevations on March 8, 2023, indicate that the site- specific groundwater flow direction is generally to the east-northeast and the hydraulic gradient, calculated using a three-point calculation from the water levels in MW-5, MW- 20, and MW-21, was estimated to be 5.8 x 10-3 feet/foot (ft/ft) to the east-northeast. 2.2 Groundwater Sampling and Analysis On February 15, 2023, CLES collected groundwater samples from 18 of the network monitor wells at the site. Samples were not collected from piezometers P-1 to P-6, or wells MW-1, MW-2, MW-3, or MW-4 that had insufficient water to sample during this event. Bailers with nylon cords and/or decontaminated sample pump with polyethylene tubing were used to collect groundwater samples from the monitor wells in general accordance with NCDEQ sampling guidance and CLES’ SOPs (Appendix I). Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 5 The groundwater samples were collected and analyzed to measure the dissolved VOC concentrations in the site monitor wells after implementing supplemental surfactant injection followed by total fluids extraction. Groundwater samples were submitted to Eurofins Environment Testing Southeast, LLC (formerly Environmental Conservation Laboratories, Inc.), for the following laboratory analyses: VOCs by USEPA Method 624.1. 3.0 RESULTS 3.1 Elevation Measurements, Groundwater Flow, and Gradient The depth to groundwater in the monitor wells measured from the top of casing ranged from 38.72 feet below the top of the well casing (ft-btoc) in MW-1 and 45.39 ft-btoc in MW-16 on March 8, 2023. Using the liquid levels measured this quarter and the relative top of casing (toc) elevation data provided by ECE, PA, groundwater surface elevations were calculated at each well location. Groundwater elevations across the site ranged from a high elevation of 55.00 ft-rel elevation in MW-1 1 (corrected for the presence of petroleum), to a low elevation of 48.50 ft-rel elevation in MW-21. Based on the potentiometric surface of the water table presented on Figure 3, in general, the groundwater flow appears to be to the east-northeast at a gradient of approximately 0.0058 ft/ft. The methods and calculations used to determine the hydraulic gradient and groundwater flow direction are presented in Appendix II. 3.2 Groundwater Analytical Results Groundwater samples from the network monitor wells at the site collected on February 15, 2023, were submitted for laboratory analysis. The table below provides a summary of the constituents and the well locations where the groundwater sample analysis identified concentrations that exceeded their respective Title 15A North Carolina Administrative Code 2L Groundwater Quality Standard (2L Standard). Constituent Wells with Concentrations above 2L Standard NCAC 2L Standard (µg/L) NCDEQ GCL (µg/L) Well with Maximum Concentration (µg/L) / Wells with Concentrations above GCL Benzene MW-8, MW-9, MW-10, MW-11, MW-12, MW-13, MW-14, MW-15, MW-17, MW-19, MW-20 1.0 5,000 MW-9: 15 MTBE MW-15, MW-17 20 20,000 MW-17: 33 Naphthalene MW-8, MW-9, MW-10, MW-11, MW-12, MW-13, MW-15, MW-16, MW-17, MW-19, MW-20 600 84,500 MW-11: 35 Total Xylenes MW-11 500 85,500 MW-11: 540 2L Standard = 15A North Carolina Administrative Code 2L Groundwater Quality Standard * Indicates IMAC value NCDEQ GCL = Gross Contamination Level in groundwater Groundwater samples collected from 11 monitor wells contained benzene, each of which had concentrations that exceed the benzene 2L Standard of 1 microgram per liter (μg/L). MW-1, MW-2, MW-3 and MW-4 were not sampled due to insufficient water in the well. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 6 Twelve of the groundwater samples analyzed contained ethylbenzene; however, none of the reported concentrations exceeded the 2L Standard of 600 μg/L. MTBE concentrations were reported in eight groundwater samples, two of the groundwater samples contained MTBE at concentrations that were above the 2L Standard of 20. Fourteen groundwater samples contained naphthalene and 11 of these samples were reported to contain naphthalene concentrations that were above the 2L Standard of 6 μg/L. Ten groundwater samples contained toluene; however, none of the samples were reported to be at concentrations that were above the 2L Standard of 600 μg/L. Total xylenes were detected in 12 groundwater samples analyzed for VOCs, of which, one sample was reported with total xylenes concentrations that were above the 2L Standard of 500 µg/L. Piezometers P-1 to P-6 do not intersect the groundwater table; thus, they were not sampled. Wells MW-1, MW-2, MW-3 and MW-4 were not sampled this event. Historical groundwater analytical data collected from 2017 to the current data set in July 2022 are compared to both the 2L Standards and the NCDEQ GCLs and are summarized in Table 5. A copy of the laboratory report for the groundwater analyses from samples collected February 15, 2023, is included in Appendix III. The locations of monitor wells and the petroleum constituents detected in the groundwater samples collected February 15, 2023, are presented in Figure 4. The pre-remedial benzene isoconcentration contours and the former area of free product that were plotted using the data reported November 1, 2017 (ECE, PA), are presented in Figure 5. Benzene concentrations in the groundwater sampled on February 15, 2023, are shown in the isoconcentration contour map presented in Figure 6. Comparing the pre-remediation data reported November 1, 2017 (Figure 5), and the post-remediation data from February 15, 2023 (Figure 6), shows the reduction of the petroleum plume area since the innovative remedial activities were implemented. The innovative remedial approach was initiated between April 30, 2018 and May 10, 2018 with supplemental injection events followed by extraction that were performed in September 6-7, 2018, October 31 to November 6, 2019, and June 17-19, 2021. Based on isoconcentration contours plotted from the 2017 pre-remedial data, the benzene plume was in an oval area approximately 75 feet by 101 feet, and the measurable free product was in a similarly oval area that was approximately 56 feet wide by 78 feet long. Note: The maximum thickness of product in 2017 as diesel fuel was 5.41 feet at MW- 11. Based on the February 15, 2023 laboratory data, the extent of the benzene plume where concentrations were reported above the 2L Standard was estimated to be in an area that ranges from 10 to 23 feet wide and a length that is approximately 39 feet. The area with measurable free product was in two intersecting oval areas, one that is approximately 10 feet by 18 feet and the second that is approximately 20 feet wide and up to 24 feet long. The new maximum product thickness measured March 8, 2023, was 3.62 (diesel fuel) feet in MW-1, central to the recovery area. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 7 4.0 CONCLUSIONS The activities conducted during the second half of 2022 and part od the first Quarter 2023 at the Seminole Mart No. 2 site included site maintenance, total fluids recovery, and sampling the groundwater from the well network to assess the current site conditions. Total fluids recovery was performed using, manual bailing, and/or manual pump operation during site visits. Groundwater monitoring was performed to evaluate the site for the presence of residual free product and to document the extent of dissolved concentrations remaining in the groundwater after the supplemental remedial actions were implemented. Liquid levels were measured in the monitor well network on March 8, 2023. Based on the potentiometric surface of the water table, the groundwater flow is generally to the east-northeast at a hydraulic gradient of approximately 0.0058 ft/ft. A measurable thickness of free product greater than 0.02 was present in three wells and one well had a thickness of 0.01 feet. No other liquid level measurements detected free product in the network monitor wells gauged or sampled in this event. Groundwater samples were collected from 18 of the network monitor wells at the site February 15, 2023. The benzene in eleven groundwater samples was measured at a concentration that was above the 2L Standard in this event. In addition to benzene, naphthalene,MTBE and total xylenes were reported at concentrations above their respective 2L Standard in one or more wells. Based on isoconcentration contours plotted using the February 15, 2023, laboratory data, the benzene concentrations were above the 2L Standard in an area that ranges from 10 to 23 feet wide and a length that is approximately 39 feet. The area with measurable free product was in two intersecting oval areas, one that is approximately 10 feet by 18 feet and the second that is approximately 20 feet wide and up to 24 feet long. The new maximum product thickness measured March 8, 2023, was 3.62 (diesel fuel) feet in MW-1, central to the recovery area. The product plume is significantly reduced from the free product area of 56 feet wide by 78 feet long that was observed in 2017. The product thickness in well MW-1 had a thickness of 2.85 in 2017. The surfactant injections has released fuel from the soil and the current thickness available for recovery is 3.62 feet. The product thickness in MW-11 was 0.61 feet on March 8, 2023, which is reduced from the greatest thickness of diesel fuel of 5.41 feet measured in MW-11 in 2017. 5.0 RECOMMENDATIONS CLES recommends that the following actions be taken for timely and cost-effective remediation to continue at the Seminole Mart No. 2 site: • Continue the groundwater quality monitoring program in general accordance with the approved revised semi-annual monitoring schedule. • Perform an aggressive product removal event using AFVR or MMPE from wells with residual free procuct. Following the aggressive product removal, continue free product recovery until the no measurable thickness of product in the well network on site is greater than 0.01 feet in the network wells. Groundwater Monitoring Report CLES Project No. 17-051A Seminole Mart No. 2, Broadway, NC March 13, 2023 8 • Use groundwater quality monitoring data to assess effectiveness of the corrective measures and make necessary modifications to the recovery operations to further attenuate the contaminant plume. After free product is not measurable in the wells at the site, sample the network quarterly to facilitate closure of the incident with NCDEQ. 6.0 REFERENCES Cape Lookout Environmental Sciences, PLLC, Groundwater Monitoring Report Seminole Mart No. 2, Broadway, NC August 8, 2022. Cape Lookout Environmental Sciences, PLLC, Groundwater Monitoring Report Seminole Mart No. 2, Broadway, NC February 18, 2022. North Carolina Department of Natural Resources and Community Development, Geologic Map of North Carolina, 1985. East Coast Environmental, PA, UST-3 Notice of Intent: UST Permanent Closure or Change-in-Service, August 24, 2016. East Coast Environmental, PA, UST-61 24-Hour Release and UST Leak Reporting Form, September 13, 2016. East Coast Environmental, PA, 20 Day Report, September 30, 2016. East Coast Environmental, PA, Initial Abatement Actions Report with UST Closure Report, October 3, 2016. East Coast Environmental, PA, Limited Site Assessment, Phase I, February 15, 2017. East Coast Environmental, PA, Free Product Assessment Report, June 8, 2017. East Coast Environmental, PA, MMPE Report, August 11, 2017. East Coast Environmental, PA, Free Product Removal/Corrective Action Plan, February 5, 2018. Cape Lookout Environmental Sciences, PLLC, Injection Well Permit Application, February 1, 2018. East Coast Environmental, PA, Free Product Removal Update and Groundwater Sampling Event, May 2, 2019. East Coast Environmental, PA, Free Product Removal Update and Groundwater Sampling Event, November 21, 2019. Cape Lookout Environmental Sciences, PLLC, Groundwater Monitoring Report, September 7, 2021. TABLES Table 1: Monitor Well Construction Table 2: Historical Groundwater Elevations Table 3: Groundwater Elevations – March 8, 2023 Table 4: Field Parameters Table 5: Historical Groundwater Sample Data Table 6: Groundwater Analytical Results – February 15, 2023 SEMINOLE MART 2 CLES PROJECT 17-051A GROUNDWATER MONIITORING REPORT MARCH 10, 2023 TABLE 1 MONITOR WELL CONSTRUCTION SEMNOLE MART NO. 2691 SEMINOLE ROADBROADWAY, HARNETT COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 42025 NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051A Well ID Contractor/C onsultant Date Installed (m/dd/yy) Date Water Level Measured (m/dd/yy) Well Casing Depth (ft-bgs) Bottom of Well (ft-bgs) ~Top of Ground Elevation (ft- rel) Top of Casing Elevation (ft-rel) Depth to Water from Top of Casing (ft-btoc) Free Product Thicknessa (ft.) Groundwater Elevation (ft-rel) Construction Details MW-1 Quantex/ECE 01/31/17 10/31/17 15 15 to 40.0 40 94.095 93.72 37.75 1.15 56.93 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-2 Quantex/ECE 03/13/17 10/31/17 30 30 to 45.0 45 94.610 94.36 44.45 0.45 50.28 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-3 Quantex/ECE 03/13/17 10/31/17 30 30 to 45.0 45 93.788 93.58 44.02 0.80 50.23 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-4 Quantex/ECE 03/13/17 10/31/17 30 30 to 45.0 45 93.787 93.52 43.50 0.20 50.19 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-5 Quantex/ECE 05/01/17 10/31/17 28 28 to 48.0 48 93.733 93.40 43.18 0.00 50.22 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-6 Quantex/ECE 05/01/17 10/31/17 29 29 to 49.0 49 93.115 92.84 42.77 0.00 50.07 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-7 Quantex/ECE 05/01/17 10/31/17 28 28 to 48.0 48 93.270 92.92 42.77 0.00 50.15 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-8 Quantex/ECE 10/24/17 10/31/17 30 30 to 50.0 50 93.880 93.38 45.03 1.95 49.97 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-9 Quantex/ECE 10/24/17 10/31/17 30 30 to 50.0 50 93.988 93.63 43.42 0.00 50.21 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-10 Quantex/ECE 10/25/17 10/31/17 30 30 to 50.0 50 94.747 94.48 44.22 0.00 50.26 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-11 Quantex/ECE 10/26/17 10/31/17 25 25 to 50.0 50 94.332 93.79 45.50 2.15 50.08 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-12 Quantex/ECE 10/26/17 10/31/17 35 35 to 50.0 50 93.462 92.92 43.64 1.02 50.13 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-13 Quantex/ECE 10/26/17 10/31/17 35 35 to 50.0 50 94.000 93.50 44.50 1.20 50.00 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-14 Quantex/ECE 10/26/17 10/31/17 35 35 to 50.0 50 93.113 92.78 43.80 1.30 50.06 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-15 Quantex/ECE 10/26/17 10/31/17 20 20 to 50.0 50 94.430 93.93 43.64 0.00 50.29 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-16 Quantex/ECE 10/26/17 10/31/17 30 30 to 50.0 50 94.890 94.64 44.40 0.00 50.24 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-17 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 94.182 93.74 45.85 2.00 49.55 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-18 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 92.743 92.31 42.90 0.00 49.41 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-19 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 93.192 92.65 44.42 1.44 49.43 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-20 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 94.258 93.65 44.23 0.00 49.42 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. MW-21 Quantex/ECE 11/29/17 12/05/17 30 30 to 50.0 50 93.378 92.92 43.98 0.00 48.94 Type II - 2" Sch. 40 PVC casing w/ 0.010 slot screen. Notes a If Diesel Fuel Free Product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.832]. ft-bgs Feet below ground surface.ft-btoc Feet below top of well casing.ft-rel Elevation relative to mean sea level as measured by east Coast Environmental, PA 10/31/17. Screen Interval (x to y ft-bgs) SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 TABLE 2HiSTORICAL PODUCT THICKNESS AND GROUNDWATER ELEVATIONSSEMINOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY, HARNETT COUNTY, NORTH CAROLINANCDEQ INCIDENT NO. 42025CLES PROJECT NO. 17-051 Well ID TOC (ft-rel)Date DTP (ft-btoc) Product Thickness (ft) DTW (ft-btoc) GW Elev (ft-rel)PRODUCT TYPE MW-1 93.72 3/27/17 36.00 1.90 37.90 57.40 5/1/17 36.65 2.30 38.95 56.685/25/17 36.25 2.85 39.10 56.995/26/17 36.75 1.00 37.75 56.806/1/17 36.53 0.62 37.15 57.09 7/10/17 36.24 2.00 38.24 57.14 8/1/17 36.38 1.04 37.42 57.1710/31/17 36.60 1.15 37.75 56.9311/29/17 36.60 2.15 38.75 56.7612/5/17 36.60 2.02 38.62 56.78 12/19/17 36.63 2.30 38.93 56.70 8/7/18 0.42 NCPUMP IN 8/20/18 0.41 NC8/24/18 35.78 0.06 35.84 57.939/6/18 0.01 NC 9/27/18 0.00 NC 10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 NM 0.00 34.93 58.7911/6/18 NM 0.00 34.98 58.74 12/2/18 NM 0.00 35.02 58.70 12/12/18 0.04 NC12/21/18 NM 0.00 34.73 58.991/15/19 35.09 0.02 35.11 58.63 gas2/5/19 35.02 0.16 35.18 58.67 2/25/19 35.18 0.25 35.43 58.50 3/1/19 35.19 0.22 35.41 58.494/25/19 34.98 0.67 35.65 58.635/16/19 35.03 1.07 36.10 58.515/31/19 35.10 1.30 36.40 58.40 6/19/19 35.14 1.72 36.86 58.29 7/5/19 35.50 1.73 37.23 57.93 diesel/gas7/15/19 35.58 1.42 37.00 57.907/29/19 35.66 1.10 36.76 57.888/3/19 35.78 0.76 36.54 57.81 8/21/19 35.86 0.93 36.79 57.70 9/18/19 36.00 1.08 37.08 57.5410/10/19 35.20 0.15 35.35 58.4911/20/19 NM 0.00 35.73 57.9912/23/19 36.07 0.20 36.27 57.62 12/31/19 36.14 0.21 36.35 57.54 1/16/20 34.83 0.26 35.09 58.852/19/20 34.82 1.89 36.71 57.012/27/20 34.93 0.47 35.40 58.323/5/20 34.94 0.96 35.90 57.82 3/10/20 34.62 0.66 35.28 58.44 3/16/20 NM 0.00 31.75 61.973/23/20 34.56 0.04 34.60 59.124/2/20 35.19 0.04 35.23 58.494/10/20 35.21 0.06 35.27 58.45 4/20/20 35.62 0.03 35.65 58.07 4/30/20 35 72 0.00 35.77 57.955/15/20 37.95 0.03 37.98 55.746/5/20 34.84 0.35 35.19 58.537/10/20 34.50 0.50 35.00 58.72 8/19/20 34.95 0.06 35.01 58.71 9/21/20 33.83 0.03 33.86 59.8610/5/20 32.73 0.00 32.73 60.9910/14/20 34.80 0.01 34.81 58.9110/28/20 NM 0.00 35.25 58.47 11/5/20 NM 0.00 35.41 58.31 11/10/20 35.43 0.02 35.45 58.2711/17/20 35.53 0.02 35.55 58.1712/3/20 35.60 0.05 35.65 58.0712/18/20 NM 0.00 30.43 63.29 1/15/21 35.15 0.03 35.18 58.54 2/1/21 35.31 0.02 35.33 58.392/25/21 35.47 0.01 35.48 58.243/5/21 35.33 0.03 35.36 58.363/11/21 34.49 0.03 34.52 59.20 3/15/21 34.51 0.02 34.53 59.19 4/7/21 35.02 0.06 35.08 58.644/12/21 35.21 0.03 35.24 58.484/19/21 35.38 0.01 35.39 58.335/6/21 35.44 0.03 35.47 58.25 6/3/21 36.06 0.02 36.08 57.64 6/9/21 35.65 0.08 35.73 57.997/7/21 NM 0.00 34.32 59.407/12/21 NM 0.00 35.50 58.227/22/21 NM 0.00 34.65 59.07 7/26/21 34.64 0.01 34.65 59.07 8/13/21 34.76 0.06 34.82 58.908/19/21 34.78 0.02 34.80 58.929/3/21 35.91 0.02 35.93 57.799/16/21 35.90 0.08 35.98 57.74 9/28/21 35.94 0.05 35.99 57.73 10/5/21 34.99 0.04 35.03 58.6910/7/21 35.00 0.04 35.04 58.6811/12/21 35.44 0.10 35.54 58.1811/15/21 35.54 0.04 35.58 58.14 11/18/21 35.97 0.04 36.01 57.71 11/24/21 36.19 0.12 36.31 57.4112/17/21 36.26 0.22 36.48 57.2412/28/21 36.32 0.32 36.64 57.081/5/22 1/11/22 36.47 0.28 36.75 56.97 1/28/22 36.43 0.39 36.82 56.902/3/22 36.48 0.34 36.82 56.902/17/22 36.45 0.33 36.78 56.943/15/22 36.52 0.65 37.17 56.55 3/18/22 0.00 93.72 4/12/22 35.67 1.65 37.32 56.404/25/22 35.24 1.99 37.23 56.495/12/22 35.88 1.48 37.36 56.365/27/22 36.09 1.32 37.41 56.31 6/10/22 36.18 0.94 37.12 56.60 7/21/22 35.18 2.48 37.66 56.068/26/22 35.21 2.70 37.91 55.819/9/22 35.99 2.48 38.47 55.25 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 9/23/22 36.38 2.54 38.92 54.8010/5/22 36.32 2.77 39.09 54.633/8/23 35.10 3.62 38.72 55.00 0.00 93.72 0.00 93.72 MW-2 94.36 3/27/17 NM 0.00 41.73 52.63 5/1/17 42.13 0.10 42.23 52.215/25/17 42.3 0.10 42.4 52.045/26/17 42.50 0.08 42.58 51.856/1/27 42.43 0.05 42.48 51.92 7/10/17 42.60 1.15 43.75 51.57 8/1/17 42.67 1.76 44.43 51.3910/31/17 44.00 0.45 44.45 50.2811/29/17 44.13 0.35 44.48 50.1712/5/17 44.23 0.27 44.50 50.08 12/19/17 44.42 0.06 44.48 49.93 8/7/18 0.20 NC8/20/18 0.25 NC8/24/18 43.43 0.30 43.73 50.639/6/18 0.55 NC 9/27/18 0.20 NC 10/10/18 0.16 NC10/29/18 40.60 1.22 41.82 53.56 gas11/6/18 44.23 0.27 44.50 50.0812/2/18 39.96 1.57 41.53 54.14 12/12/18 0.83 NC 12/21/18 38.67 2.00 40.67 55.351/15/19 37.99 3.01 41.00 55.86 gas2/5/19 37.91 1.47 39.38 56.202/25/19 37.48 1.91 39.39 56.56 3/1/19 37.45 1.86 39.31 56.60 4/10/19 37.02 1.11 38.13 57.154/25/19 37.00 0.61 37.61 57.265/16/19 37.82 0.63 38.45 56.435/31/19 37.27 2.14 39.41 56.73 6/4/19 37.28 0.92 38.20 56.93 6/19/19 37.96 1.06 39.02 56.227/5/19 38.64 0.30 38.94 55.67 gas/diesel7/15/19 38.86 1.02 39.88 55.337/29/19 39.01 1.85 40.86 55.04 8/3/19 39.42 0.36 39.78 54.88 8/21/19 39.77 1.45 41.22 54.359/18/19 40.43 1.89 42.32 53.6110/10/18 41.19 0.52 41.71 53.0811/20/19 42.21 0.12 42.33 52.13 12/23/19 42.89 0.21 43.10 51.43 12/31/19 42.54 0.24 42.78 51.781/16/20 43.36 0.56 43.92 50.443/16/20 27.87 0.02 27.89 66.47 MAKE UP FROM 173/23/20 42.72 0.01 42.73 51.63 4/2/20 NM 0.00 42.65 51.71 4/10/20 42.62 0.02 42.64 51.724/20/20 42.21 0.10 42.31 52.054/30/20 42.20 0.06 42.26 52.105/15/20 42.10 0.21 42.31 52.05 6/5/20 42.01 0.27 42.28 52.08 7/10/20 41.28 1.47 42.75 51.618/19/20 40.58 0.33 40.91 53.459/21/20 40.04 2.06 42.10 52.2610/5/20 39.73 0.02 39.75 54.61 10/14/20 NM 0.00 40.96 53.40 10/28/20 NM 0.00 40.16 54.2011/5/20 NM 0.00 40.68 53.6811/10/20 40.74 0.06 40.80 53.5611/17/20 NM 0.00 40.68 53.68 12/3/20 NM 0.00 40.53 53.83 12/18/20 NM 0.00 32.27 62.091/15/21 39.75 0.19 39.94 54.422/1/21 39.41 0.22 39.63 54.732/25/21 39.70 0.02 39.72 54.64 3/5/21 NM 0.00 39.61 54.75 3/11/21 NM 0.00 37.93 56.433/15/21 NM 0.00 37.94 56.424/7/21 37.14 0.15 37.29 57.074/12/21 NM 0.00 37.33 57.03 4/19/21 37.50 0.01 37.51 56.85 5/6/21 38.01 0.33 38.34 56.026/3/21 38.41 0.25 38.66 55.706/9/21 38.49 0.21 38.70 55.667/7/21 39.66 0.14 39.80 54.56 7/12/21 39.98 0.04 40.02 54.34 7/22/21 40.04 0.05 40.09 54.277/26/21 39.98 0.05 40.03 54.338/13/21 40.19 0.07 40.26 54.108/19/21 40.26 0.06 40.32 54.04 9/3/21 40.56 0.08 40.64 53.72 9/16/21 40.71 0.18 40.89 53.479/28/21 40.89 0.21 41.10 53.2610/5/21 40.05 0.63 40.68 53.6810/7/21 40.38 0.31 40.69 53.67 11/12/21 40.60 0.59 41.19 53.17 11/15/21 41.15 0.08 41.23 53.1311/18/21 41.62 0.04 41.66 52.7011/24/21 42.12 0.10 42.22 52.1412/17/21 42.52 0.08 42.60 51.76 12/28/21 42.74 0.14 42.88 51.48 1/11/22 43.04 0.12 43.16 51.201/28/22 43.14 0.51 43.65 50.712/3/22 43.26 0.42 43.68 50.682/17/22 43.34 0.55 43.89 50.47 3/15/22 43.69 0.52 44.21 50.15 3/18/22 43.74 0.56 44.30 50.064/12/22 43.28 0.58 43.86 50.504/25/22 43.82 0.38 44.20 50.16 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 5/12/22 43.88 0.44 44.32 50.045/27/22 43.91 0.45 44.36 50.006/10/22 43.99 0.33 44.32 50.04 7/21/22 44.15 0.11 44.26 50.10 8/26/22 44.16 0.06 44.22 50.149/9/22 44.14 0.06 44.20 50.169/23/22 NM 0.00 44.17 50.1910/5/22 NM 0.00 44.18 50.18 3/8/23 NM 0.00 44.54 49.82 MW-3 93.58 3/27/17 40.55 2.00 42.55 52.69 5/1/17 40.95 2.50 43.45 52.21 5/25/17 41.20 2.00 43.20 52.045/26/17 41.53 0.62 42.15 51.956/1/27 41.40 1.30 42.70 51.967/10/17 41.50 3.00 44.50 51.58 8/1/17 41.76 2.54 44.30 51.39 10/31/17 43.22 0.80 44.02 50.2311/29/17 43.42 1.24 44.66 49.9512/5/17 43.42 1.24 44.66 49.9512/19/17 43.41 1.25 44.66 49.96 8/7/18 0.01 NC 8/20/18 0.00 NC8/24/18 43.38 0.01 43.39 50.209/6/18 0.00 NC9/27/18 0.00 NC 10/10/18 0.02 NC 10/19/18 0.07 NC10/29/18 41.00 0.23 41.23 52.54 gas11/6/18 40.68 0.14 40.82 52.8812/2/18 39.70 0.38 40.08 53.82 12/12/18 0.00 NC 12/21/18 38.35 0.34 38.69 55.171/15/19 37.73 0.43 38.16 55.78 gas/diesel2/5/19 37.02 0.37 37.39 56.502/25/19 36.98 0.40 37.38 56.53 3/1/19 36.94 0.36 37.30 56.58 4/25/19 36.19 0.67 36.86 57.285/16/19 36.38 0.82 37.20 57.065/31/19 36.56 0.93 37.49 56.866/4/19 36.58 0.34 36.92 56.94 6/19/19 37.00 1.17 38.17 56.38 7/5/19 37.59 1.55 39.14 55.73 gas/diesel7/15/19 38.61 0.47 39.08 54.897/29/19 38.84 0.16 39.00 54.718/3/19 38.56 0.33 38.89 54.96 8/21/19 39.03 0.59 39.62 54.45 9/18/19 39.79 0.74 40.53 53.6710/10/19 40.33 0.50 40.83 53.1711/20/19 NM 0.00 41.35 52.2312/23/19 41.19 0.35 41.54 52.33 12/31/19 NM NC NM NC 1/16/20 NM 0.00 42.26 51.322/19/20 42.01 0.21 42.22 51.362/27/20 42.30 0.01 42.31 51.273/5/20 42.31 0.01 42.32 51.26 3/10/20 NM 0.00 41.59 51.99 3/16/20 NM 0.00 41.72 51.863/23/20 41.45 0.01 41.46 52.124/2/20 NM 0.00 41.39 52.194/10/20 41.39 0.01 41.38 52.20 4/20/20 NM 0.00 41.37 52.21 4/30/20 41.41 0.02 41.43 52.155/15/20 41.56 0.05 41.61 51.976/5/20 41.31 0.03 41.34 52.247/10/20 40.72 0.05 40.77 52.81 8/19/20 40.23 0.08 40.31 53.27 9/21/20 40.03 0.12 40.15 53.4310/5/20 40.00 0.10 40.10 53.4810/14/20 40.05 0.04 40.09 53.4910/28/20 40.09 0.04 40.13 53.45 11/5/20 40.12 0.04 40.16 53.42 11/10/20 40.14 0.06 40.20 53.3811/17/20 40.14 0.07 40.21 53.3712/18/20 40.3 0.08 40.38 54.781/15/21 39.45 0.09 39.54 55.46 2/1/21 39.02 0.04 39.06 55.70 2/25/21 38.44 0.08 38.52 55.173/5/21 NM MC NM NC3/11/21 37.75 0.04 37.79 56.933/15/21 37.79 0.01 37.8 56.03 4/7/21 37.09 0.05 37.14 56.61 4/12/21 37.27 0.03 37.3 56.454/19/21 37.44 0.05 37.49 56.235/6/21 37.62 0.11 37.73 55.876/3/21 38.21 0.10 38.31 55.27 6/9/21 38.28 0.07 38.35 55.23 7/7/21 38.95 0.02 38.97 54.617/12/21 39.09 0.01 39.1 54.487/22/21 39.18 0.01 39.19 54.397/26/21 39.11 0.01 39.12 54.46 8/13/21 39.31 0.02 39.33 54.25 8/19/21 39.38 0.01 39.39 54.199/3/21 39.66 0.01 39.67 53.939/16/21 39.84 0.01 39.85 53.739/28/21 40.01 0.02 40.03 53.55 10/5/21 40.21 0.01 40.22 53.36 10/7/21 NM 0.00 40.23 53.3511/12/21 NM 0.00 40.73 52.8511/15/21 NM 0.00 40.77 52.8111/18/21 NM 0.00 41.2 52.39 11/24/21 NM 0.00 41.32 52.26 12/17/21 NM 0.00 41.71 51.9112/28/21 NM 0.00 41.93 51.671/11/22 NM 0.00 42.31 51.281/28/22 NM 0.00 42.38 51.22 2/3/22 NM 0.00 42.53 51.07 2/17/22 NM 0.00 42.64 50.963/15/22 NM 0.00 43.05 50.55 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 3/18/22 NM NC NM NC4/12/22 43.23 0.01 43.24 50.354/25/22 NM 0.00 43.18 50.40 5/12/22 43.25 0.01 43.26 50.32 5/27/22 43.27 0.02 43.29 50.296/10/22 43.38 0.03 43.41 50.177/21/22 43.52 0.29 43.81 49.778/26/22 43.61 0.37 43.98 49.60 9/9/22 43.8 0.41 44.21 49.37 9/23/22 44.01 0.73 44.74 48.84 10/5/22 44.12 0.77 44.89 48.69 3/8/23 44.22 0.66 44.88 48.70 MW-4 93.52 3/27/17 40.55 1.90 42.45 52.65 5/1/17 41.04 1.71 42.75 52.195/25/17 41.30 1.42 42.72 51.985/26/17 41.62 0.13 41.75 51.886/1/27 41.44 1.18 42.62 51.88 7/10/17 41.73 1.37 43.10 51.56 8/1/17 42.10 0.30 42.40 51.3710/31/17 43.30 0.20 43.50 50.1911/29/17 43.73 0.20 43.93 49.7612/5/17 43.81 0.17 43.98 49.68 12/19/17 44.04 0.03 44.07 49.47 8/7/18 0.028/20/18 0.008/24/18 0.009/6/18 0.00 NC 9/27/18 0.00 NC 10/10/18 0.00 NC10/19/18 0.04 NC10/29/18 41.03 0.02 41.05 52.49 diesel11/6/18 NM 0.00 40.74 52.78 12/2/18 NM 0.00 39.77 53.75 12/12/18 0.01 NC diesel12/21/18 0.00 NC1/15/19 NM 0.00 37.78 55.742/5/19 NM 0.00 2/26/19 37.01 0.01 37.02 56.51 4/25/19 NM 0.00 36.25 57.276/19/19 37.14 0.05 37.19 56.377/5/19 37.78 0.03 37.81 55.73 diesel7/15/19 38.36 0.01 38.37 55.16 7/29/19 38.40 0.02 38.42 55.12 8/3/19 38.59 0.02 38.61 54.938/21/19 39.09 0.03 39.12 54.429/18/19 39.86 0.03 39.89 53.6511/20/19 41.40 0.02 41.42 52.12 12/23/19 42.08 0.01 42.09 51.44 12/31/19 0.001/16/20 42.24 0.01 42.25 51.273/10/20 NM 0.00 41.57 51.953/16/20 NM 0.00 41.71 51.81 3/23/20 41.41 0.01 41.42 52.10 4/2/20 NM 0.00 41.43 52.094/10/20 NM 0.00 41.41 52.114/20/20 NM 0.00 41.45 52.074/30/20 NM 0.00 41.44 52.08 5/15/20 NM 0.00 41.56 51.96 6/5/20 NM 0.00 41.29 52.237/10/20 NM 0.00 40.72 52.808/18/20 NM 0.00 40.23 53.299/21/20 NM 0.00 40.04 53.48 10/5/20 40.00 0.01 40.01 53.52 10/14/20 NM 0.00 40.04 53.4810/28/20 NM 0.00 40.08 53.4411/5/20 NM 0.00 40.10 53.4211/10/20 NM 0.00 40.12 53.40 11/17/20 NM 0.00 40.15 53.37 12/18/20 40.30 0.01 40.31 53.211/15/21 NM 0.00 39.44 54.082/1/21 NM 0.00 38.98 54.542/25/21 38.41 0.02 38.43 55.09 3/5/21 NM 0.00 38.02 55.50 3/11/21 NM 0.00 37.73 55.793/15/21 NM 0.00 38.40 55.124/7/21 NM 0.00 37.05 56.474/12/21 NM 0.00 37.79 55.73 4/19/21 NM 0.00 37.97 55.55 5/6/21 NM 0.00 37.60 55.926/3/21 38.16 0.03 38.19 55.336/9/21 38.31 0.02 38.33 55.197/7/21 NM 0.00 39.94 53.58 7/12/21 NM 0.00 39.06 54.46 7/22/21 39.12 0.01 39.13 54.397/26/21 39.08 0.01 39.09 54.438/13/21 39.29 0.01 39.30 54.228/19/21 39.34 0.01 39.35 54.17 9/3/21 39.64 0.01 39.65 53.87 9/16/21 NM 0.00 39.85 53.679/28/21 39.99 0.01 40.00 53.5210/5/21 NM 0.00 40.20 53.3210/7/21 0.00 93.52 11/12/21 0.00 93.52 11/15/21 0.00 93.5211/18/21 0.00 93.5211/24/21 0.00 41.32 52.20 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 12/17/21 0.00 41.70 51.8212/28/21 0.00 41.93 51.591/11/22 42.26 0.01 42.27 51.25 1/28/22 NM 0.00 42.42 51.10 2/17/22 42.82 0.01 42.83 50.693/15/22 NM 0.00 43.08 50.443/18/22 NM NC NM NC4/12/22 NM 0.00 43.25 50.27 4/25/22 NM 0.00 43.21 50.31 5/12/22 NM 0.00 43.26 50.265/27/22 NM 0.00 43.29 50.236/10/22 NM 0.00 43.38 50.147/21/22 NM 0.00 43.59 49.93 8/26/22 NM 0.00 44.20 49.32 9/9/22 NM 0.00 44.41 49.119/23/22 NM 0.00 44.20 49.3210/5/22 NM 0.00 44.24 49.283/8/23 NM 0.00 44.33 49.19 MW-5 93.4 5/25/17 NM 0.00 41.34 52.06 5/26/17 NM NC NM NC 6/1/27 NM 0.00 41.45 51.957/10/17 NM 0.00 41.80 51.608/1/17 NM 0.00 42.00 51.4010/31/17 NM 0.00 43.18 50.22 11/29/17 NM 0.00 43.60 49.80 12/5/17 NM 0.00 43.68 49.7212/19/17 NM 0.00 43.90 49.508/7/18 0.00 NC8/20/18 0.00 NC 8/24/18 NM 0.00 43.24 50.16 9/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 NM 0.00 NC 10/29/18 NM 0.00 43.68 49.72 11/6/18 0.00 NC12/2/18 NM 0.00 39.53 53.8712/12/18 0.00 NC12/21/18 0.00 NC 1/15/19 NM 0.00 37.57 55.83 2/5/19 NM2/25/19 NM 0.00 36.80 56.604/25/19 NM 0.00 36.04 57.366/19/19 NM 0.00 36.96 56.44 7/5/19 NM 0.00 37.61 55.79 11/20/19 NM 0.00 41.27 52.1312/23/19 NM 0.00 93.4012/31/19 NM 0.00 93.401/16/20 NM 0.00 42.09 51.31 3/10/20 NM 0.00 41.41 51.99 3/16/20 NM 0.00 41.52 51.886/5/20 NM 0.00 41.14 52.2610/5/20 NM 0.00 39.84 53.5610/14/20 NM 0.00 39.87 53.53 7/12/21 NM 0.00 38.89 54.51 1/28/22 NM 0.00 42.23 51.177/21/22 NM 0.00 43.42 49.983/8/23 NM 0.00 44.26 49.14 MW-6 92.84 5/25/17 NM 0.00 40.90 51.945/26/17 NM NC NM NC 6/1/27 NM 0.00 41.01 51.83 7/10/17 NM 0.00 41.35 51.498/1/17 NM 0.00 41.53 51.3110/31/17 NM 0.00 42.77 50.0711/29/17 NM 0.00 43.18 49.66 12/5/17 NM 0.00 43.25 49.59 12/19/17 NM 0.00 43.48 49.368/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 42.84 50.00 9/6/18 0.00 NC 9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 NM 0.00 NC10/29/18 NM 0.00 40.46 52.38 11/6/18 0.00 NC 12/2/118 NM 0.00 39.16 53.6812/12/18 0.00 NC12/21/18 0.00 NC1/15/19 NM 0.00 37.18 55.66 2/5/19 NM 2/26/19 NM 0.00 36.39 56.454/25/19 NM 0.00 35.63 57.216/19/19 NM 0.00 36.52 56.327/5/19 NM 0.00 37.14 55.70 11/20/19 NM 0.00 40.82 52.02 12/23/19 0.00 92.8412/31/19 0.00 92.841/16/20 NM 0.00 41.66 51.183/16/20 NM 0.00 41.10 51.74 6/5/20 NM 0.00 40.72 52.12 10/5/20 NM 0.00 39.39 53.4510/14/20 NM 0.00 39.41 53.437/12/21 NM 0.00 38.43 54.411/28/22 NM 0.00 41.76 51.08 7/21/22 NM 0.00 42.98 49.86 3/8/23 NM 0.00 43.73 49.11 MW-7 92.92 5/25/17 NM 0.00 40.9 52.02 5/26/17 NM NC NM NC6/1/27 NM 0.00 41.03 51.897/10/17 NM 0.00 41.37 51.558/1/17 NM 0.00 41.55 51.37 10/31/17 NM 0.00 42.77 50.15 11/29/17 NM 0.00 43.18 49.7412/5/17 NM 0.00 43.25 49.6712/19/17 NM 0.00 43.49 49.438/7/18 0.00 NC 8/20/18 0.00 NC 8/24/18 NM 0.00 42.84 50.089/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC 10/19/18 NM 0.00 NC 10/29/18 NM 0.00 40.45 52.4711/6/18 NM NC NM NC SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 12/2/18 NM 0.00 39.15 53.7712/12/18 0.00 NC12/21/18 0.00 NC 1/15/19 NM 0.00 37.15 55.77 2/5/19 NM2/26/19 NM 0.00 36.38 56.544/25/19 NM 0.00 35.63 57.296/19/19 NM 0.00 36.52 56.40 7/5/19 NM 0.00 37.14 55.70 11/20/19 NM 0.00 40.82 52.0212/23/19 0.00 92.8412/31/19 0.00 92.841/16/20 NM 0.00 41.66 51.18 3/16/20 NM 0.00 41.10 51.74 6/5/20 NM 0.00 40.71 52.1310/5/20 NM 0.00 34.00 58.8410/14/20 NM 0.00 39.43 53.417/12/21 NM 0.00 38.43 54.41 1/28/22 NM 0.00 41.79 51.05 7/21/22 NM 0.00 42.98 49.863/8/23 NM 0.00 43.73 49.11 MW-8 93.38 10/31/17 43.08 1.95 45.03 49.9711/29/17 43.45 2.48 45.93 49.5112/5/17 43.53 2.47 46.00 49.4412/19/17 44.02 0.48 44.50 49.28 8/7/18 0.00 NC 8/20/18 0.02 NC8/24/18 43.42 0.07 43.49 49.959/6/18 0.01 NC9/27/18 0.00 NC 10/10/18 0.00 NC 10/19/18 0.00 NC10/29/18 40.98 0.64 41.62 52.29 diesel11/6/18 40.59 0.63 41.22 52.6812/2/18 39.7 0.34 40.04 53.62 12/12/18 0.01 NC 12/21/18 NM 0.00 38.45 54.931/15/19 37.78 0.23 38.01 55.56 diesel2/5/19 37.06 0.21 37.27 56.282/25/19 37.01 0.43 37.44 56.30 3/1/19 36.98 0.43 37.41 56.33 4/10/19 36.34 0.47 36.81 56.964/25/19 36.23 0.48 36.71 57.075/16/19 36.42 0.58 37.00 56.865/31/19 36.59 0.62 37.21 56.69 6/4/19 36.6 0.16 36.76 56.75 6/19/19 37.13 0.39 37.52 56.187/5/19 37.72 0.67 38.39 55.55 diesel7/15/19 38.23 0.15 38.38 55.127/29/19 38.37 0.40 38.77 54.94 8/3/19 38.54 0.35 38.89 54.78 8/21/19 39.05 0.38 39.43 54.279/18/19 39.8 0.48 40.28 53.5011/20/19 41.42 0.02 41.44 51.9612/23/19 NM 0.00 42.08 51.30 12/31/19 0.00 93.38 1/16/20 42.24 0.03 42.27 51.112/19/20 42.17 0.11 42.28 51.102/27/20 42.29 0.04 42.33 51.053/5/20 42.30 0.02 42.32 51.06 3/10/20 41.56 0.03 41.59 51.79 3/16/20 41.79 0.14 41.93 51.453/23/20 41.40 0.10 41.50 51.884/2/20 41.43 0.11 41.54 51.844/10/20 41.41 0.06 41.47 51.91 4/20/20 41.45 0.01 41.46 51.92 4/30/20 41.44 0.16 41.60 51.785/15/20 41.41 0.17 41.58 51.806/5/20 41.26 0.32 41.58 51.807/10/20 40.71 0.09 40.79 52.59 8/19/20 40.2 0.20 40.40 52.98 9/21/20 40 0.30 40.30 53.0810/5/20 39.9 0.31 40.21 53.1710/14/20 40.01 0.19 40.20 53.1810/28/20 40.06 0.14 40.20 53.18 11/5/20 40.09 0.14 40.23 53.27 11/10/20 40.1 0.15 40.25 53.1311/17/20 40.13 0.10 40.23 53.1512/18/20 40.35 0.17 40.52 52.861/15/21 39.43 0.07 39.50 53.88 2/1/21 38.97 0.02 38.99 54.39 2/25/21 38.44 0.03 38.47 54.913/5/21 38.11 0.01 38.12 55.263/11/21 NM 0.00 37.78 55.603/15/21 NM 0.00 37.79 55.59 4/7/21 NM 0.00 37.08 56.30 4/12/21 NM 0.00 37.27 56.114/19/21 NM 0.00 37.45 55.935/6/21 37.63 0.01 37.64 55.746/3/21 38.19 0.01 38.20 55.18 6/9/21 38.31 0.02 38.33 55.05 7/7/21 39.04 0.08 39.12 54.267/12/21 NNM 0.00 39.09 54.297/22/21 39.17 0.01 39.18 54.207/26/21 39.11 0.01 39.12 54.26 8/13/21 39.3 0.01 39.31 54.07 8/19/21 39.38 0.01 39.39 53.999/3/21 39.66 0.01 39.67 53.719/16/21 NM 0.00 39.84 53.549/28/21 40 0.01 40.01 53.37 10/5/21 NM 0.00 40.16 53.22 10/7/21 NM 0.00 41.17 52.21 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 11/12/21 NM 0.00 41.59 51.7911/15/21 NM 0.00 41.63 51.7511/18/21 NM 0.00 42.21 51.18 11/24/21 NM 0.00 41.29 52.09 12/17/21 NM 0.00 41.70 51.6812/28/21 NM 0.00 41.92 51.461/11/22 NM 0.00 42.50 50.881/28/22 NM 0.00 42.40 50.98 2/3/22 NM 0.00 42.52 50.86 2/17/22 42.63 0.01 42.64 50.743/15/22 NM 0.00 43.07 50.313/18/22 NM NC NM NC4/12/22 43.25 0.01 43.26 50.12 4/25/22 NM 0.00 43.22 50.16 5/12/22 43.26 0.02 43.28 50.105/27/22 43.28 0.02 43.30 50.086/10/22 NM 0.00 43.38 50.007/21/22 NM 0.00 43.57 49.81 8/26/22 NM 0.00 44.18 49.20 9/9/22 NM 0.00 44.39 48.999/23/22 NM 0.00 44.18 49.2010/5/22 NM 0.00 44.22 49.163/8/23 NM 0.00 44.32 49.06 MW-9 93.63 10/31/17 NM 0.00 43.42 50.21 11/29/17 NM 0.00 43.82 49.81 12/5/17 NM 0.00 43.90 49.7312/19/17 NM 0.00 44.10 49.538/7/18 0.21 NCPUMP IN WELL 8/20/18 0.21 NC 8/24/18 0.21 NC 9/6/18 0.40 NC9/27/18 0.44 NC10/10/18 0.39 NCPUMP IN WELL 10/19/18 0.35 NC 10/29/18 41.09 0.34 41.43 52.48 diesel 11/6/18 40.72 0.07 40.79 52.9012/2/18 39.75 0.18 39.93 53.8512/12/18 0.42 NC12/21/18 38.48 0.06 38.54 55.14 1/15/19 37.79 0.39 38.18 55.77 diesel 2/5/19 37.10 0.23 37.33 56.492/25/19 37.08 0.20 37.28 56.523/1/19 37.05 0.19 37.24 56.554/10/19 36.38 0.41 36.79 57.18 4/25/19 36.28 0.50 36.78 57.27 5/16/19 36.49 0.61 37.10 57.045/31/19 36.64 0.68 37.32 56.886/4/19 36.66 0.12 36.78 56.956/19/19 37.16 0.68 37.84 56.36 7/5/19 37.80 0.77 38.57 55.70 diesel 7/15/19 38.21 0.22 38.43 55.387/29/19 38.50 0.15 38.65 55.108/3/19 38.69 0.09 38.78 54.928/21/19 39.20 0.15 39.35 54.40 9/18/19 39.97 0.18 40.15 53.63 11/20/19 41.54 0.04 41.58 52.0812/23/19 42.09 0.01 42.10 51.5412/31/19 0.00 93.631/16/20 42.34 0.02 42.36 51.27 2/19/20 42.18 0.10 42.28 51.35 2/27/20 42.31 0.03 42.34 51.293/5/20 42.30 0.02 42.32 51.313/10/20 41.63 0.04 41.67 51.963/16/20 41.76 0.02 41.78 51.85 3/23/20 41.48 0.32 41.80 51.83 4/2/20 41.51 0.18 41.69 51.944/10/20 41.48 0.05 41.53 52.104/20/20 41.53 0.17 41.70 51.934/30/20 41.47 0.11 41.58 52.05 5/15/20 41.52 0.16 41.68 51.95 6/5/20 41.36 0.12 41.48 52.157/10/20 40.80 0.10 40.90 52.738/19/20 40.23 0.48 40.71 52.929/21/20 40.09 0.40 40.49 53.14 10/5/20 40.07 0.53 40.60 53.03 10/14/20 40.11 0.28 40.39 53.4710/28/20 40.14 0.28 40.42 53.2111/5/20 40.17 0.26 40.43 53.2011/10/20 40.19 0.24 40.43 53.20 11/17/20 40.22 0.17 40.39 53.24 12/18/20 40.35 0.21 40.56 53.071/15/21 39.5 0.22 39.72 53.912/1/21 39.03 0.13 39.16 54.472/25/21 38.49 0.10 38.59 55.04 3/5/21 38.11 0.08 38.19 55.44 3/11/21 37.8 0.10 37.90 55.733/15/21 37.88 0.02 37.90 55.734/7/21 37.14 0.01 37.15 56.484/12/21 37.33 0.08 37.41 56.22 4/19/21 37.43 0.08 37.51 56.12 5/6/21 37.69 0.13 37.82 55.816/3/21 38.26 0.13 38.39 55.246/9/21 38.4 0.26 38.66 54.977/7/21 39.03 0.09 39.12 54.51 7/12/21 39.19 0.02 39.21 54.42 7/22/21 39.24 0.04 39.28 54.357/26/21 3919 0.01 39.20 54.438/13/21 39.39 0.04 39.43 54.208/19/21 39.46 0.03 39.49 54.14 9/3/21 39.77 0.02 39.79 53.84 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 9/16/21 39.94 0.01 39.95 53.689/28/21 40.13 0.01 40.14 53.4910/5/21 40.3 0.01 40.31 53.32 10/7/21 41.32 0.00 41.32 52.31 11/12/21 41.68 0.14 41.82 51.8111/15/21 41.8 0.06 41.86 51.7711/18/21 42.19 0.10 42.29 51.3411/24/21 41.35 0.06 41.41 52.22 12/17/21 41.71 0.11 41.82 51.81 12/28/21 41.97 0.07 42.04 51.591/11/22 42.42 0.16 42.58 51.051/28/22 NM 0.00 42.49 51.142/3/22 NM 0.00 42.54 51.09 2/17/22 43.73 0.01 43.74 49.89 3/15/22 NM 0.00 43.15 50.483/18/22 NM NC NM NC4/12/22 NM 0.00 43.33 50.304/25/22 NM 0.00 43.29 50.34 5/12/22 NM 0.00 43.30 50.33 5/27/22 43.36 0.01 43.37 50.266/10/22 NM 0.00 43.36 50.277/21/22 NM 0.00 43.65 49.988/26/22 NM 0.00 43.89 49.74 9/9/22 NM 0.00 44.10 49.53 9/23/22 NM 0.00 44.22 49.4110/5/22 NM 0.00 44.29 49.343/8/23 NM 0.00 44.42 49.21 MW-10 94.48 10/31/17 NM 0.00 44.22 50.2611/29/17 NM 0.00 44.61 49.87 12/5/17 NM 0.00 44.68 49.80 12/19/17 NM 0.00 44.88 49.608/7/18 0.42 NC dieselPUMP IN WELL 8/20/18 1.20 NC8/24/18 44.09 1.21 45.30 50.19 9/6/18 0.95 NC 9/27/18 1.31 NC10/10/18 0.43 NCPUMP IN WELL 10/19/18 0.50 NC10/29/18 42.03 0.07 42.10 52.44 diesel 11/6/18 41.55 0.48 42.03 52.85 12/2/18 40.35 2.10 42.45 53.7812/12/18 0.42 NC12/21/18 39.07 0.62 39.69 55.311/15/19 38.42 1.78 40.20 55.76 diesel 2/5/19 37.97 0.67 38.64 56.40 2/26/19 NM 0.00 38.08 56.40 PUMP ON3/1/19 38.04 0.24 38.28 56.404/10/19 37.32 0.70 38.02 57.044/25/19 37.15 1.09 38.24 57.15 gas 5/16/19 37.49 0.43 37.92 56.92 5/31/19 37.64 0.70 38.34 56.726/4/19 37.65 0.11 37.76 56.816/19/19 38.14 0.59 38.73 56.247/5/19 38.51 2.18 40.69 55.60 gas 7/15/19 38.6 3.11 41.71 55.36 7/29/19 38.73 4.54 43.27 54.99 gas light over black8/3/19 39.39 1.53 40.92 54.838/21/19 39.68 3.17 42.85 54.279/18/19 40.49 2.89 43.38 53.50 10/10/19 41.08 2.14 43.22 53.04 11/20/19 42.46 0.08 42.54 52.0112/23/19 42.98 0.43 43.41 51.4312/31/19 43.01 0.54 43.55 51.381/16/20 43.07 0.63 43.70 50.78 3/16/20 NM 0.00 41.11 53.37 3/23/20 42.17 0.46 42.63 51.854/2/20 41.4 0.50 41.90 52.584/10/20 42 0.48 42.48 52.004/20/20 41.93 0.44 42.37 52.11 4/30/20 42.18 0.33 42.51 51.97 5/15/20 42.21 0.84 43.05 51.436/5/20 42.08 1.06 43.14 51.347/10/20 41.47 1.33 42.80 51.688/19/20 40.89 1.91 42.80 51.68 9/21/20 40.93 1.25 42.18 52.30 10/5/20 40.98 0.93 41.91 52.5710/14/20 40.95 0.84 41.79 52.6910/28/20 40.94 0.96 41.90 53.3811/5/20 40.98 0.89 41.87 52.61 11/10/20 40.99 1.09 42.08 52.40 11/17/20 41 1.08 42.08 52.4012/3/20 40.96 1.04 42.00 52.4812/18/20 41.08 0.95 42.03 52.451/15/21 40.26 1.20 41.46 53.02 2/1/21 39.78 1.13 40.91 53.57 2/25/21 39.33 0.72 40.05 54.433/5/21 39.52 0.11 39.63 54.853/11/21 38.55 1.16 39.71 54.773/15/21 38.68 1.04 39.72 54.76 4/7/21 37.8 1.86 39.66 54.82 4/12/21 37.94 1.47 39.41 55.074/19/21 38.02 0.70 38.72 55.765/6/21 38.43 1.68 40.11 54.375/12/21 38.83 0.68 39.51 54.97 6/3/21 39.88 0.14 40.02 54.46 6/9/21 39.27 0.44 39.71 54.777/7/21 39.93 0.20 40.13 54.357/12/21 40.12 0.19 40.31 54.177/22/21 40.17 0.20 40.37 54.11 7/26/21 40.15 0.21 40.36 54.12 8/13/21 40.29 0.37 40.66 53.82 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 8/19/21 40.36 0.42 40.78 53.709/3/21 40.67 0.46 41.13 53.359/16/21 40.81 0.31 41.12 53.36 9/28/21 41.02 0.28 41.30 53.18 10/5/21 41.19 0.40 41.59 52.8910/7/21 41.42 0.18 41.60 52.8811/12/21 41.78 0.32 42.10 52.3811/15/21 42.1 0.04 42.14 52.34 11/18/21 42.54 0.03 42.57 51.91 11/24/21 42.29 0.05 42.34 52.1412/17/21 42.7 0.02 42.72 51.7612/28/21 42.91 0.02 42.93 51.551/11/22 43.28 0.05 43.33 51.15 1/28/22 43.28 0.01 43.29 51.19 2/3/22 43.45 0.03 43.48 51.002/17/22 43.54 0.01 43.55 50.933/15/22 43.95 0.03 43.98 50.503/18/22 43.98 0.01 43.99 50.49 4/12/22 44.13 0.07 44.20 50.28 4/25/22 44.1 0.05 44.15 50.335/12/22 44.14 0.06 44.20 50.285/27/22 44.15 0.10 44.25 50.236/10/22 44.24 0.12 44.36 50.12 7/21/22 44.44 0.15 44.59 49.89 8/26/22 44.54 0.16 44.70 49.789/9/22 44.64 0.15 44.79 49.699/23/22 44.85 0.13 44.98 49.5010/5/22 45 0.19 45.19 49.29 3/8/23 45.13 0.01 45.14 49.34 MW-11 93.79 10/31/17 43.55 1.95 45.50 49.91 diesel 11/29/17 43.35 5.41 48.76 49.5312/5/17 44.05 0.50 44.55 49.6612/19/17 44.28 0.35 44.63 49.458/7/18 0.42 NC 8/20/18 0.55 NC PUMP IN WELL 8/24/18 0.499/6/18 NC9/27/18 NC10/10/18 NC PUMP IN WELL 10/19/18 NC 10/29/18 41.31 0.49 41.81 52.39 gas orange11/6/18 40.97 0.10 41.07 52.8012/2/18 39.79 1.72 41.51 53.7112/12/18 1.20 NC 12/21/18 38.32 2.72 41.04 55.01 1/15/19 37.58 3.69 41.27 55.59 gas2/5/19 36.91 3.90 40.81 56.222/26/19 37.2 1.19 38.39 56.39 PUMP ON3/1/19 37.17 1.14 38.31 56.43 4/10/19 36.26 2.24 38.50 57.15 4/25/19 36.13 3.34 39.47 57.105/16/19 36.31 3.87 40.18 56.835/31/19 36.32 4.43 40.75 56.736/4/19 36.34 2.10 38.44 57.10 6/19/19 38.93 2.07 41.00 54.51 7/5/19 37.76 2.65 40.41 55.58 gas7/15/19 38.21 2.21 40.42 55.217/29/19 38.33 2.78 41.11 54.998/3/19 38.54 2.57 41.11 54.82 8/21/19 39.15 2.09 41.24 54.29 9/18/19 40.04 1.19 41.23 53.5510/10/19 40.51 1.11 41.62 53.0911/120/19 41.7 0.38 42.08 52.0312/23/19 42.25 0.82 43.07 51.40 12/31/19 42.31 0.78 43.09 51.35 1/16/20 42.43 0.68 43.11 50.683/16/20 41.96 0.74 42.70 51.093/23/20 41.72 0.38 42.10 51.694/2/20 41.72 0.40 42.12 51.67 4/10/20 41.7 0.37 42.07 51.72 4/20/20 41.69 0.32 42.01 51.784/30/20 41.7 0.32 42.02 51.775/15/20 41.64 0.33 41.97 51.826/5/20 41.5 0.29 41.79 52.00 7/10/20 40.92 0.56 41.48 52.31 8/19/20 40.38 1.40 41.78 52.019/21/20 40.22 0.97 41.19 52.6010/5/20 40.18 1.12 41.30 52.4910/14/20 40.22 1.01 41.23 52.56 10/28/20 40.3 0.80 41.10 53.36 11/5/20 40.35 0.73 41.08 52.7111/10/20 40.39 0.50 40.89 52.9011/17/20 NM 0.00 40.40 53.3912/3/20 NM 0.00 40.08 53.71 12/18/20 40.23 0.07 40.30 53.49 1/15/21 39.58 1.32 40.90 52.892/2/21 39.12 1.02 40.14 53.652/25/21 38.69 0.60 39.29 54.503/5/21 38.34 0.73 39.07 54.72 3/11/21 37.97 0.90 38.87 54.92 3/15/21 38.04 0.85 38.89 54.904/7/21 37.12 2.01 39.13 54.664/12/21 37.2 1.53 38.73 55.064/19/21 37.62 0.97 38.59 55.20 5/6/21 37.76 0.99 38.75 55.04 5/12/21 38.17 0.42 38.59 55.206/3/21 38.45 0.76 39.21 54.586/9/21 36.51 0.07 36.58 57.217/7/21 39.23 0.46 39.69 54.10 7/12/21 39.42 0.03 39.45 54.34 7/22/21 39.51 0.02 39.53 54.267/26/21 39.45 0.03 39.48 54.318/13/21 39.62 0.30 39.92 53.87 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 8/19/21 39.65 0.47 40.12 53.679/3/21 39.91 0.79 40.70 53.099/16/21 40.09 0.66 40.75 53.04 9/28/21 40.27 0.55 40.82 52.97 10/5/21 40.49 0.46 40.95 52.8410/7/21 40.5 0.46 40.96 52.8311/12/21 40.99 0.47 41.46 52.3311/15/21 41.01 0.49 41.50 52.29 11/18/21 41.37 0.56 41.93 51.86 11/24/21 41.52 0.46 41.98 51.8112/17/21 41.93 0.41 42.34 51.4512/28/21 42.13 0.56 42.69 51.101/11/22 42.31 0.60 42.91 50.88 1/28/22 42.61 0.47 43.08 50.71 2/3/22 42.74 0.43 43.17 50.622/17/22 42.88 0.33 43.21 50.583/15/22 43.39 0.39 43.78 50.013/18/22 43.35 0.15 43.50 50.29 4/12/22 43.44 0.49 43.93 49.86 4/25/22 43.41 0.47 43.88 49.915/12/22 43.44 0.50 43.94 49.855/27/22 43.47 0.51 43.98 49.816/10/22 43.55 0.56 44.11 49.68 7/21/22 43.71 0.73 44.44 49.35 8/26/22 43.82 0.78 44.60 49.199/9/22 43.91 0.74 44.65 49.149/23/22 43.92 0.71 44.63 49.1610/5/22 44.36 0.72 45.08 48.71 3/8/23 44.52 0.61 45.13 48.66 MW-12 92.92 10/31/17 42.62 1.02 43.64 50.13 diesel 11/29/17 42.95 1.71 44.66 49.6812/5/17 43.03 1.70 44.73 49.6012/19/17 43.45 1.34 44.79 49.248/7/18 0.01 NC 8/20/18 0.01 NC 8/24/18 42.9 0.01 42.91 50.029/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC 10/19/18 0.02 NC 10/29/18 40.51 0.01 40.52 52.41 diesel11/6/18 NM 0.00 40.13 52.7912/2/18 NM 0.00 39.19 53.7312/12/18 0.23 NC diesel 12/21/18 0.00 NC 1/15/19 NM 0.00 37.24 55.682/5/19 NM 0.002/26/19 NM 0.00 36.49 56.434/25/19 NM 0.00 35.72 57.20 6/19/19 NM 0.00 36.61 56.31 7/5/19 NM 0.00 37.22 55.707/15/19 0.00 92.927/29/19 0.00 92.9211/20/19 NM 0.00 40.90 52.02 12/23/19 0.00 92.92 12/31/19 0.00 92.921/16/20 NM 0.00 41.71 51.213/16/20 NM 0.00 41.16 51.766/5/20 NM 0.00 40.77 52.15 8/19/20 NM 0.00 39.69 53.23 10/5/20 39.46 0.11 39.57 53.3510/14/20 NM 0.00 92.927/12/21 NM 0.00 38.52 54.401/18/22 NM 0.00 41.84 51.08 3/15/22 NM 0.00 42.52 50.40 7/21/22 43.03 0.09 43.12 49.808/26/22 43.11 0.14 43.25 49.679/9/22 43.61 0.18 43.79 49.139/23/22 43.90 0.16 44.06 48.86 10/5/22 43.65 0.30 43.95 48.97 3/8/23 NM 0.00 43.81 49.11 MW-13 93.5 10/31/17 43.30 1.20 44.50 50.00 diesel11/29/17 43.59 2.07 45.66 49.5612/5/17 43.65 2.05 45.70 49.5112/19/17 44.10 0.58 44.68 49.30 8/7/18 0.00 NC 8/20/18 0.00 NC8/24/18 NM 0.00 43.59 49.919/6/18 0.00 NC9/27/18 0.00 NC 10/10/18 0.00 NC 10/19/18 0.00 NC10/29/18 NM 0.00 41.24 52.2611/6/18 NM NC NM NC12/2/18 NM 0.00 39.96 53.54 12/12/18 0.00 NC 12/21/18 0.00 NC1/15/19 NM 0.00 38.02 55.482/5/19 NM 0.002/26/19 NM 0.00 37.24 56.26 4/25/19 NM 0.00 36.48 57.02 6/19/19 NM 0.00 37.34 56.167/5/19 NM 0.00 37.95 55.5511/20/19 NM 0.00 41.56 51.9412/23/19 0.00 93.50 12/31/19 0.00 93.50 1/16/20 NM 0.00 42.39 51.113/16/20 NM 0.00 41.97 51.536/5/20 NM 0.00 41.46 52.048/19/20 NM 0.00 40.36 53.14 10/5/20 NM 0.00 40.16 53.34 10/14/20 NM 0.00 41.17 52.337/12/21 NM 0.00 39.23 54.271/28/22 NM 0.00 42.50 51.007/21/22 NM 0.00 43.73 49.77 3/8/23 NM 0.00 44.49 49.01 MW-14 92.78 10/31/17 42.50 1.30 43.80 50.06 diesel 11/29/17 42.88 1.67 44.55 49.6212/5/17 42.95 1.65 44.60 49.5512/19/17 43.35 0.55 43.90 49.348/7/18 0.00 NC 8/20/18 0.00 NC 8/24/18 NM 0.00 42.83 49.959/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 10/19/18 0.00 NC10/29/18 NM 0.00 40.45 52.3311/6/18 NM NC NM NC 12/2/18 NM 0.00 39.14 53.64 12/12/18 0.33 NC12/21/18 0.00 NC1/15/19 NM 0.00 37.20 55.582/5/19 NM 0.00 2/26/19 NM 0.00 36.42 56.36 4/25/19 NM 0.00 35.66 57.126/19/19 NM 0.00 36.54 56.247/5/19 NM 0.00 37.14 55.6411/20/19 NM 0.00 40.80 51.98 12/23/19 0.00 92.78 12/31/19 0.00 92.781/16/20 NM NC NM NC3/16/20 NM 0.00 41.13 51.656/5/20 NM NC NM NC Blocked 8/19/20 NM 0.00 39.60 53.18 10/5/20 NM 0.00 39.39 53.3910/14/20 NM 0.00 39.39 53.397/12/21 NM 0.00 38.42 54.361/28/22 NM 0.00 41.74 51.04 7/21/22 NM 0.00 42.97 49.81 3/8/23 NM 0.00 43.73 49.05 MW-15 93.93 10/31/17 NM 0.00 43.64 50.29 11/29/17 NM 0.00 44.03 49.9012/5/17 NM 0.00 44.11 49.8212/19/17 NM 0.00 44.29 49.648/7/18 0.01 NC 8/20/18 0.01 NC 8/24/18 44.71 0.38 45.09 49.16 gas9/6/18 0.31 NC9/27/18 0.17 NC10/10/18 0.20 NC PUMP IN WELL 10/19/18 0.20 NC 10/29/18 42.48 0.05 42.53 51.44 gas11/6/18 41.1 0.28 41.38 52.7812/2/18 40.16 0.15 40.31 53.7412/12/18 0.01 NC 12/21/18 38.79 0.24 39.03 55.10 1/15/19 38.19 0.58 38.77 55.64 gas2/5/19 37.52 0.38 37.90 56.352/25/19 37.49 0.31 37.80 56.393/1/19 37.18 0.36 37.54 56.69 4/25/19 ~1 Blocked 5/16/19 ~15/31/19 ~16/19/19 <17/5/19 38.27 0.41 38.68 55.59 gas black 7/15/19 38.68 0.21 38.89 55.21 7/29/19 38.92 0.19 39.11 54.98 gas black8/3/19 39.08 0.25 39.33 54.818/21/19 39.57 0.41 39.98 54.299/18/19 40.35 0.26 40.61 53.54 10/10/19 40.80 0.41 41.21 53.06 11/20/19 NM 0.00 41.88 52.0512/23/19 NM 0.00 42.49 51.4412/31/19 NM 0.00 42.55 51.381/16/20 NM 0.00 42.63 51.30 3/16/20 NM 0.00 46.21 47.72 3/23/20 NM 0.00 42.15 51.784/2/20 NM 0.00 42.08 51.854/10/20 NM 0.00 41.22 52.714/20/20 NM 0.00 41.78 52.15 4/30/20 NM 0.00 41.80 52.13 5/15/20 41.80 0.04 41.84 52.096/5/20 NM 0.00 41.70 52.237/10/20 NM 0.00 41.11 52.828/19/20 40.58 1.82 42.40 51.53 9/21/20 40.42 0.58 41.00 52.93 10/5/20 40.43 0.27 40.70 53.2310/14/20 40.49 0.04 40.53 53.4010/28/20 40.51 0.27 40.78 53.1511/5/20 40.50 0.25 40.75 53.18 11/10/20 40.52 0.33 40.85 53.08 11/17/20 40.57 0.11 40.68 53.2512/3/20 40.51 0.21 40.72 53.2112/18/20 40.55 0.88 41.43 52.501/15/21 39.78 0.88 40.66 53.27 2/1/21 39.24 0.93 40.17 53.76 2/25/21 38.78 0.80 39.58 54.353/5/21 38.47 0.83 39.30 54.633/11/21 38.09 0.78 38.87 55.063/15/21 38.28 0.60 38.88 55.05 4/7/21 37.43 0.90 38.33 55.60 4/12/21 37.52 0.73 38.25 55.684/19/21 37.93 0.48 38.41 55.525/6/21 38.02 0.85 38.87 55.065/12/21 38.32 0.39 38.71 55.22 6/3/21 38.75 0.11 38.86 55.07 6/9/21 38.74 0.01 38.75 55.187/7/21 39.44 0.06 39.50 54.437/12/21 NM 0.00 39.60 54.337/22/21 39.67 0.01 39.68 54.25 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 7/26/21 40.61 0.01 40.62 53.318/13/21 40.81 0.01 40.82 53.118/19/21 NM 0.00 40.86 53.07 9/3/21 NM 0.00 40.19 53.74 9/16/21 NM 0.00 40.33 53.609/28/21 40.50 0.01 40.51 53.4210/5/21 NM 0.00 40.68 53.2510/7/21 NM 0.00 40.69 53.24 11/12/21 NM 0.00 41.19 52.74 11/15/21 NM 0.00 41.23 52.7011/18/21 NM 0.00 41.66 52.2711/24/21 41.71 0.02 41.73 52.2012/17/21 42.11 0.01 42.12 51.81 12/28/21 NM 0.00 42.32 51.61 1/11/22 NM 0.00 42.64 51.291/28/22 NM 0.00 42.74 51.192/17/22 NM 0.00 43.36 50.573/15/22 NM 0.00 43.40 50.53 3/18/22 NM 0.00 43.39 50.54 4/12/22 43.57 0.02 43.58 50.354/25/22 43.53 0.02 43.55 50.385/12/22 NM 0.00 43.59 50.345/27/22 NM 0.00 43.60 50.33 6/10/22 NM 0.00 43.68 50.25 7/21/22 NM 0.00 43.87 50.068/26/22 NM 0.00 44.08 49.859/9/22 NM 0.00 44.29 49.649/23/22 NM 0.00 44.49 49.44 10/5/22 NM 0.00 44.51 49.42 3/8/23 NM 0.00 44.63 49.300.00 MW-16 94.64 10/31/17 NM 0.00 44.40 50.24 11/29/17 NM 0.00 44.77 49.8712/5/17 NM 0.00 44.83 49.8112/19/17 NM 0.00 45.12 49.528/7/18 0.00 NC 8/20/18 0.00 NC 8/24/18 NM 0.00 44.41 50.239/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC 10/19/18 0.00 NC 10/29/18 42.19 0.59 42.78 52.35 diesel11/6/18 41.86 0.14 42.00 52.7612/2/18 40.9 0.24 41.14 53.7012/12/18 0.00 NC 12/21/18 39.57 0.22 39.79 55.03 1/15/19 38.98 0.54 39.52 55.57 diesel2/5/19 38.32 0.36 38.68 56.262/25/19 38.24 0.58 38.82 56.303/1/19 38.14 0.33 38.47 56.44 4/10/19 37.55 1.05 38.60 56.91 4/25/19 37.42 1.07 38.49 57.045/16/19 37.64 1.34 38.98 56.775/31/19 37.97 0.23 38.20 56.636/4/19 37.99 0.02 38.01 56.65 6/19/19 38.49 0.13 38.62 56.13 7/5/19 39.12 0.20 39.32 55.49 diesel7/15/19 39.48 0.42 39.90 55.097/29/19 39.69 0.46 40.15 54.878/3/19 39.91 0.07 39.98 54.72 8/21/19 40.41 0.11 40.52 54.21 9/18/19 41.11 0.21 41.32 53.4910/10/19 41.61 0.37 41.98 52.9711/20/19 NM 0.00 42.67 51.9712/23/19 43.23 0.10 43.33 51.39 12/31/19 43.17 0.18 43.35 51.44 1/16/20 NM 0.00 43.37 51.273/16/20 NM 0.00 42.80 51.843/23/20 NM 0.00 41.78 52.864/2/20 NM 0.00 41.81 52.83 4/10/20 NM 0.00 42.41 52.23 4/20/20 NM 0.00 42.34 52.304/30/20 NM 0.00 42.59 52.055/15/20 NM 0.00 42.62 52.026/5/20 42.48 0.01 42.49 52.15 7/10/20 41.92 0.02 41.94 52.70 8/19/20 NM 0.00 41.47 53.179/21/20 NM 0.00 41.30 53.3410/5/20 41.27 0.06 41.33 53.3110/14/20 41.33 0.01 41.34 53.30 10/28/20 41.33 0.03 41.36 53.28 11/5/20 41.35 0.04 41.39 53.2511/10/20 41.39 0.02 41.41 53.2311/17/20 41.4 0.01 41.41 53.2312/3/20 NM 0.00 41.39 53.25 12/18/20 41.52 0.08 41.60 53.04 1/15/21 40.67 0.09 40.76 53.882/1/21 40.2 0.03 40.23 54.412/25/21 39.68 0.04 39.72 54.923/5/21 NM 0.00 39.39 55.25 3/11/21 NM 0.00 39.01 55.63 3/15/21 NM 0.00 39.02 55.624/7/21 38.35 0.04 38.39 56.254/12/21 38.96 0.02 38.98 55.664/19/21 NM 0.00 39.02 55.62 5/6/21 38.97 0.04 39.01 55.63 5/12/21 39.21 0.01 39.22 55.426/3/21 NM 0.00 39.57 55.076/9/21 NM 0.00 39.61 55.037/7/21 NM 0.00 40.28 54.36 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 7/12/21 NM 0.00 40.42 54.227/22/21 NM 0.00 40.49 54.157/26/21 NM 0.00 40.43 54.21 8/13/21 NM 0.00 40.61 54.03 8/19/21 NM 0.00 40.66 53.989/3/21 NM 0.00 41.01 53.639/16/21 NM 0.00 41.14 53.509/28/21 NM 0.00 40.33 54.31 10/5/21 NM 0.00 41.49 53.15 10/7/21 NM 0.00 41.50 53.1411/12/21 NM 0.00 42.00 52.6411/15/21 NM 0.00 42.04 52.6011/18/21 NM 0.00 42.47 52.17 11/24/21 NM 0.00 42.52 52.12 12/17/21 NM 0.00 42.91 51.7312/28/21 NM 0.00 43.12 51.521/11/22 43.45 0.04 43.49 51.151/28/22 NM 0.00 43.48 51.16 2/17/22 NM 0.00 43.72 50.92 3/15/22 NM 0.00 44.15 50.493/18/22 NM NC NM NC4/12/22 NM 0.00 44.34 50.304/25/22 44.3 0.01 44.31 50.33 5/12/22 NM 0.00 44.34 50.30 5/27/22 44.36 0.01 44.37 50.276/10/22 NM 0.00 44.44 50.207/21/22 NM 0.00 44.64 50.008/26/22 NM 0.00 44.84 49.80 9/9/22 NM 0.00 45.04 49.60 9/23/22 NM 0.00 45.24 49.4010/5/22 NM 0.00 45.24 49.403/8/23 NM 0.00 45.39 49.25 MW-17 93.74 12/5/17 43.85 2.00 45.85 49.55 diesel12/19/17 44.05 1.78 45.83 49.39 diesel 8/7/18 0.00 NC 8/20/18 0.00 NC8/24/18 NM 0.00 43.78 49.969/6/18 0.00 NC9/27/18 0.00 NC 10/10/18 0.00 NC 10/19/18 0.00 NC10/29/18 41.02 0.19 41.21 52.69 diesel/gas11/6/18 41.35 0.38 41.73 52.3312/2/18 40.08 0.26 40.34 53.62 12/12/18 2.00 NC 12/21/18 38.73 0.33 39.06 54.951/15/19 38.03 1.06 39.09 55.53 diesel2/5/19 37.22 1.57 38.79 56.262/26/19 37.48 0.00 37.48 56.26 PUMP ON 3/1/19 37.19 0.12 37.31 56.53 4/10/19 36.35 2.65 39.00 56.94 diesel4/25/19 36.14 2.96 39.10 57.105/16/19 36.76 0.92 37.68 56.835/31/19 36.96 0.52 37.48 56.69 6/4/19 36.97 0.08 37.05 56.76 6/19/19 37.47 0.53 38.00 56.187/5/19 38.03 0.83 38.86 55.57 diesel7/15/19 38.58 0.96 39.54 55.007/29/19 38.62 1.04 39.66 54.95 diesel 8/3/19 38.81 1.00 39.81 54.76 8/21/19 39.28 1.02 40.30 54.299/18/19 40.10 0.65 40.75 53.5310/10/19 40.66 0.28 40.94 53.0311/20/19 NM 0.00 40.78 52.96 12/23/19 NM 0.00 42.41 51.33 12/31/19 NM 0.00 42.50 51.241/16/20 NM 0.00 42.59 51.153/16/20 NM 0.00 41.72 52.023/23/20 41.73 0.18 41.91 51.83 4/2/20 41.72 0.19 41.91 51.83 4/10/20 41.75 0.21 41.96 51.784/20/20 41.73 0.17 41.90 51.844/30/20 41.72 0.18 41.90 51.845/15/20 41.73 0.19 41.92 51.82 6/5/20 41.61 0.19 41.80 51.94 7/10/20 41.03 0.10 41.13 52.618/19/20 40.50 0.42 40.92 52.829/21/20 40.36 0.11 40.47 53.2710/5/20 40.32 0.07 40.39 53.35 10/14/20 40.33 0.20 40.53 53.21 10/28/20 41.80 0.20 42.00 51.74 PUMP ON11/5/20 40.38 0.00 40.48 53.2611/10/20 40.43 0.07 40.50 53.2411/17/20 NM 0.00 42.01 51.73 12/3/20 NM 0.00 40.08 53.66 12/18/20 NM 0.00 43.57 50.171/15/21 39.78 0.08 39.86 53.882/1/21 NM 0.00 39.32 54.422/25/21 38.78 0.24 39.02 54.72 3/5/21 38.49 0.17 38.66 55.08 3/11/21 38.06 0.50 38.56 55.183/15/21 38.01 0.60 38.61 55.134/7/21 37.05 2.10 39.15 54.594/12/21 37.16 0.87 38.03 55.71 4/19/21 37.23 0.58 37.81 55.93 5/6/21 37.78 1.43 39.21 54.535/12/21 38.16 0.51 38.67 55.076/3/21 38.49 0.37 38.86 54.886/9/21 40.08 0.61 40.69 53.05 7/7/21 NM 0.00 39.29 54.45 7/12/21 NM 0.00 39.42 54.327/22/21 NM 0.00 39.52 54.227/26/21 NM 0.00 39.47 54.278/13/21 NM 0.00 39.65 54.09 8/19/21 NM 0.00 39.71 54.03 9/3/21 NM 0.00 40.03 53.719/16/21 NM 0.00 40.17 53.579/28/21 NM 0.00 40.34 53.4010/5/21 NM 0.00 40.52 53.22 10/7/21 NM 0.00 40.53 53.21 11/12/21 NM 0.00 41.03 52.7111/15/21 NM 0.00 41.07 52.6711/18/21 NM 0.00 41.50 52.2411/24/21 NM 0.00 41.62 52.12 12/17/21 NM 0.00 42.02 51.72 12/28/21 NM 0.00 42.23 51.511/11/22 42.59 0.01 42.60 51.141/28/22 NM 0.00 42.72 51.022/17/22 NM 0.00 42.97 50.77 3/15/22 NM 0.00 43.38 50.36 3/18/22 NM NC NM NC4/12/22 NM 0.00 43.56 50.184/25/22 NM 0.00 43.52 50.225/12/22 NM 0.00 43.57 50.17 5/27/22 NM 0.00 43.60 50.14 6/10/22 NM 0.00 43.69 50.057/21/22 NM 0.00 43.89 49.858/26/22 NM 0.00 44.12 49.629/9/22 NM 0.00 44.35 49.39 SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 9/23/22 NM 0.00 44.42 49.3210/5/22 NM 0.00 44.57 49.173/8/23 NM 0.00 44.69 49.05 MW-18 92.31 12/5/17 NM 0.00 42.90 49.41 12/19/17 NM 0.00 43.13 49.18 8/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 42.50 49.819/6/18 0.00 NC 9/27/18 0.00 NC 10/10/18 0.00 NC10/19/18 NM 0.00 NC10/29/18 NM 0.00 40.07 52.2411/6/18 NM NC NM NC 12/2/18 NM 0.00 38.73 53.58 12/12/18 0.00 NC12/21/18 0.00 NC1/15/19 NM 0.00 36.81 55.502/5/19 NM 2/26/19 NM 0.00 36.01 56.30 4/25/19 NM 0.00 35.25 57.066/19/19 NM 0.00 36.11 56.207/5/19 NM 0.00 36.73 55.5811/20/19 NM 0.00 40.43 51.88 12/23/19 0.00 12/31/19 0.001/16/20 NM 0.00 41.61 50.703/16/20 NM 0.00 40.71 51.606/5/20 NM 0.00 40.31 52.00 8/19/20 NM 0.00 39.21 53.10 10/5/20 NM 0.00 38.90 53.4110/14/20 NM 0.00 39.00 53.317/12/21 NM 0.00 38.03 54.281/28/22 NM 0.00 41.33 50.98 7/21/22 NM 0.00 42.63 49.68 3/8/23 NM 0.00 44.37 47.94 MW-19 92.65 12/5/17 42.98 1.44 44.42 49.43 diesel 12/19/17 43.18 1.64 44.82 49.198/7/18 0.00 NC8/20/18 0.00 NC8/24/18 NM 0.00 42.83 49.82 9/6/18 0.00 NC 9/27/18 0.00 NC10/10/18 0.00 NC10/19/18 0.00 NC10/29/18 NM 0.00 40.44 52.21 11/6/18 NM NC NM NC 12/2/18 NM 0.00 39.11 53.5412/12/18 NM 0.00 NC12/21/18 0.00 NC1/15/19 NM 0.00 37.20 55.45 2/5/19 NM 2/26/19 NM 0.00 36.41 56.244/25/19 NM 0.00 35.65 57.006/19/19 NM 0.00 36.51 56.147/5/19 NM 0.00 37.12 55.53 11/20/19 NM 0.00 40.76 51.89 12/23/19 0.0012/31/19 0.001/16/20 NM 0.00 42.65 50.003/16/20 NM 0.00 41.11 51.54 6/5/20 NM 0.00 40.68 51.97 8/19/20 NM 0.00 39.58 53.0710/5/20 NM 0.00 39.35 53.3010/14/20 NM 0.00 39.37 53.287/12/21 NM 0.00 38.40 54.25 1.28/22 NM 0.00 41.73 50.92 7/21/22 NM 0.00 42.94 49.713/8/23 NM 0.00 43.73 48.92 MW-20 93.65 12/5/17 NM 0.00 44.23 49.4212/19/17 NM 0.00 44.29 49.368/7/18 0.00 NC 8/20/18 0.00 NC 8/24/18 NM 0.00 43.86 49.799/6/18 0.00 NC9/27/18 0.00 NC10/10/18 0.00 NC 10/19/18 0.00 NC 10/29/18 NM 0.00 41.53 52.1211/6/18 NM NC NM NC12/2/18 NM 0.00 40.22 53.4312/12/18 NM 0.00 NC 12/21/18 0.00 NC 1/15/19 NM 0.00 38.32 55.332/5/19 NM 0.00 NC2/26/19 NM 0.00 37.53 56.124/25/19 NM 0.00 36.80 56.85 6/19/19 NM 0.00 37.64 56.01 7/5/19 NM 0.00 38.24 55.4111/20/19 NM 0.00 41.83 51.8212/23/19 0.00 93.6512/31/19 0.00 93.65 1/16/20 NM 0.00 42.65 51.00 3/16/20 NM 0.00 42.19 51.466/5/20 NM 0.00 41.70 51.9510/5/20 NM 0.00 40.45 53.2010/14/20 NM 0.00 40.25 53.40 7/12/21 NM 0.00 39.51 54.14 1/28/22 NM 0.00 42.75 50.907/21/22 NM 0.00 43.96 49.693/8/23 NM 0.00 44.74 48.91 MW-21 92.95 12/5/17 NM 0.00 43.98 48.9712/19/17 NM 0.00 44.22 48.73 8/7/18 NM NC NM NC 8/20/18 NM NC NM NC8/24/18 NM 0.00 43.59 49.369/6/18 NM NC NM NC SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 TABLE 3 GROUNDWATER ELEVATIONS - MARCH 8, 2023 SEMNOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY, HARNETT COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 42025 NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051A Page 1 of 1 Well ID TOC (ft-rel)Date DTP (ft- btoc) Product Thickness (ft) DTW (ft-btoc) GW Elev (ft-rel) MW-1 93.72 3/8/23 35.1 3.62 38.72 55.00 MW-2 94.36 3/8/23 NM 0 44.54 49.82 MW-3 93.58 3/8/23 44.22 0.66 44.88 48.70 MW-4 93.52 3/8/23 NM 0 44.33 49.19 MW-5 93.40 3/8/23 NM 0 44.26 49.14 MW-6 92.84 3/8/23 NM 0 43.73 49.11 MW-7 92.92 3/8/23 NM 0 43.73 49.19 MW-8 93.38 3/8/23 NM 0 44.32 49.06 MW-9 93.63 3/8/23 NM 0 44.42 49.21 MW-10 94.48 3/8/23 45.13 0.01 45.14 49.34 MW-11 93.79 3/8/23 44.52 0.61 45.13 48.66 MW-12 92.92 3/8/23 NM 0 43.81 49.11 MW-13 93.50 3/8/23 NM 0 44.49 49.01 MW-14 92.78 3/8/23 NM 0 43.73 49.05 MW-15 93.93 3/8/23 NM 0 44.63 49.30 MW-16 94.64 3/8/23 NM 0 45.39 49.25 MW-17 93.74 3/8/23 NM 0 44.69 49.05 MW-18 92.31 3/8/23 NM 0 43.37 48.94 MW-19 92.65 3/8/23 NM 0 43.73 48.92 MW-20 93.65 3/8/23 NM 0 44.74 48.91 MW-21 92.92 3/8/23 NM 0 44.42 48.50 Notes: NM = None measured. * If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.86] TOC = Top of well casing. DTP = Depth to product measured from the top of the well casing. ft-btoc = Feet below the top of the well casing. DTW = Depth to groundwater measured from the top of the well casing. ft-rel = Well casing elevations reported by East Coast Encironmental, PA CAP 11/1/17. SEMINOLE MART 2 CLES PROJECT 17-051A GROUNDWATER MONITORNIG REPORT MARCH 10, 2023 TABLE 4 FIELD PARAMETERS SEMNOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY, HARNETT COUNTY, NORTH CAROLINA NCDEQ INCIDENT NO. 42025 NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051A pH Conductivity (mS/Cm)1 Temperature (oC)2 MW-1 2/15/23 NM NM NM MW-2 2/15/23 NM NM NM MW-3 2/15/23 NM NM NM MW-4 2/15/23 NM NM NM MW-5 2/15/23 6.00 0.03 17.8 MW-6 2/15/23 6.00 0.07 17.6 MW-7 2/15/23 6.00 0.08 17.6 MW-8 2/15/23 6.0 0.13 17.7 MW-9 2/15/23 6.0 0.11 17.8 MW-10 2/15/23 6.0 0.04 17.6 MW-11 2/15/23 6.5 0.24 17.9 MW-12 2/15/23 6.0 0.09 17.9 MW-13 2/15/23 6.0 0.14 17.80 MW-14 2/15/23 6.0 0.07 18.00 MW-15 2/15/23 6.0 0.19 17.60 MW-16 2/15/23 6.5 0.19 17.40 MW-17 2/15/23 6.5 0.24 17.90 MW-18 2/15/23 6.50 0.01 17.3 MW-19 2/15/23 6.0 0.10 17.8 MW-20 2/15/23 6.0 0.28 17.6 MW-21 2/15/23 7.00 0.03 17.30 Notes: 2. oC = Degrees Celsius. 3. NM = Not measured.(pH sensor malfunctioned during event. Surfactant Injection June 17-18, 2021 Well ID Date Field Parameters 1. mS/cm = milli Siemens per centimeter. TABLE 5 GROUNDWATER ANALYTICAL RESULTS SEMNOLE MART NO. 2691 SEMINOLE ROAD BROADWAY. HARNETT COUNTY, NORTH CAROLINANCDENR INCIDENT NO. 42025NCDEQ UST SECTION FACILITY ID. 0-000014231CLES PROJECT NO. 17-051A Page 1 of 2EPAEPAEPAEPAEPAEPAEPAEPAEPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA 624 6200B 6200B 624 624 6200B 6200B 8260 624 625 6200B 624 6200B 6200B 6200B 6200B 624 624 624 Well ID Date Sampled (m/dd/yy) MW-1 NS MW-1 7/21/22 64 D NR NR 290 D <20 NR NR <20 210 D NR NR 370 D NR NR NR NR 830 D 1,100 D 1,900 DMW-1 7/12/21 <50 NR NR 170 D <50 NR NR <50 <50 <400 NR 140 D NR NR NR NR 480 D 610 D 1,100 DMW-1 10/14/20 <10 NR NR 76 <10 NR NR <10 34 <200 NR 92 NR NR NR NR 260 290 560MW-1 7/5/19 110 NR NR 940 <10 NR NR <10 <220,000 <220,000 NR 1300 NR NR NR NR 1800 3000 4900MW-1 12/3/18 43 NR NR 650 <10 NR NR <10 <50 <50 NR 530 NR NR NR NR 1200 1700 2900 MW-2 NSMW-2 7/21/22 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NRMW-2 7/12/21 80 D NR NR 74 D <20 NR NR <20 26 D <200 NR NR NR NR NR NR 230 D 230 D 460 DMW-2 10/14/20 37 NR NR 100 <10 NR NR <10 37 <200 NR NR NR NR NR NR 430 390 820MW-2 12/3/18 320 NR NR 770 <10 NR NR <10 <2,000 <2000 NR NR NR NR NR NR 1300 2100 3400 MW-3 NSMW-3 7/21/22 29 D NR NR 23 D <20 NR NR <20 54 D NR NR 47 NR NR NR NR 380 D 85 D 470 D MW-3 7/12/21 70 D NR NR 140 D <20 NR NR <20 33 D <50 NR 130 D NR NR NR NR 310 D 310 D 620 DMW-3 10/14/20 78 NR NR 170 <10 NR NR <10 45 <200 NR 120 NR NR NR NR 340 370 710MW-3 12/3/18 150 NR NR 170 <10 NR NR <10 14 JD 14 JD NR 180 NR NR NR NR 340 580 920 MW-4 NSMW-4 7/21/22 <5 NR NR 4.6 JD <5 NR NR <5 6 D NR NR <5 NR NR NR NR 13 D 8.8 D 22 D MW-4 7/12/21 3.4 JD NR NR 40 D <5 NR NR <5 12 D <50 NR <5 NR NR NR NR 220 D 47 D 270 DMW-4 10/14/20 5.6 NR NR 9.1 <1 NR NR <1 3.1 <50 NR 2.0 NR NR NR NR 110 17 130MW-4 12/3/18 21 NR NR 39 <1 NR NR 1.3 <2 <200 NR 21 NR NR NR NR 130 25 160 MW-5 2/15/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 <0.12 NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6MW-5 7/12/21 <1 NR NR <1 <1 NR NR <1 3.20 <10 NR <1 NR NR NR NR 40 7.0 47MW-5 10/14/20 8.1 NR NR 3.2 <1 NR NR <1 5 <10 NR <1 NR NR NR NR 61 53 110MW-5 7/5/19 <1 NR NR 2.3 <1 NR NR <1 5.3 J 5.3 J NR <1 NR NR NR NR 69 91 160MW-5 12/2/18 <1 NR NR <1 <1 NR NR <1 <2 <10 NR <1 NR NR NR NR 0.63 J <2 1.4 JMW-5 12/5/17 2.8 NR NR 1.2 <1 NR NR <1 0.91 J 3.4 J NR 9.2 NR NR NR NR 2.5 3.8 6.3 MW-6 2/15/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 <0.12 NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6MW-6 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3MW-6 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR 0.57 J <2 <3MW-6 7/5/19 <1 NR NR <1 <1 NR NR <1 <10 <10 NR <1 NR NR NR NR <1 <2 <3MW-6 12/2/18 <1 NR NR 0.72 J <1 NR NR <1 <2 <10 NR <1 NR NR NR NR 0.96 J 1.8 J 2.7 MW-6 12/5/17 54 NR NR 25 <1 NR NR 1.4 8.9 7.2 J NR 170 NR NR NR NR 39 94 130 MW-7 2/15/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 <0.12 NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6 MW-7 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3MW-7 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <2MW-7 3/16/20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <10 <1 <1 <1 <1 0.60 J <1 <1 <2 <2 MW-7 12/2/18 <1 NR NR <1 <1 NR NR <1 <2 <10 NR <1 NR NR NR NR 2.7 <2 3.7 MW-8 2/15/23 6.8 NR NR 22 <0.36 NR NR 5.0 13 NR NR 1.3 NR NR NR NR 63 48 110MW-8 7/21/22 12 D NR NR 70 D <5 NR NR <5 15 D NR NR 3.6 JD NR NR NR NR 160 D 130 D 290 DMW-8 7/12/21 19 D NR NR 60 D <5 NR NR <5 12 D <30 NR 26 D NR NR NR NR 150 D 110 D 260 DMW-8 10/14/20 5.6 NR NR 23 <1 NR NR <1 10 <200 NR 6.8 NR NR NR NR 66 31 96MW-8 12/3/18 11 NR NR 95 <10 NR NR <10 11 JD 11 JD NR 72 NR NR NR NR 180 230 410MW-8 12/5/17 45 D NR NR 520 D NR NR NR <1.6 92 D 770 JD NR 670 D NR NR NR NR 850 D 1400 D 2200 D MW-9 2/15/23 15 NR NR 25 <0.36 NR NR <0.26 10 NR NR 2.5 NR NR NR NR 59 47 110MW-9 7/21/22 <10 NR NR 48 D <10 NR NR <10 14 D NR NR 14 D NR NR NR NR 100 D 130 D 240 DMW-9 7/12/21 74 D NR NR 150 D <5 NR NR <5 26 D 12 JD NR 59 D NR NR NR NR 310 D 400 D 710 DMW-9 10/14/20 41 NR NR 130 <2 NR NR <2 21 20 NR 44 NR NR NR NR 250 370 620MW-9 3/16/20 18 JD 16 JD <20 50 D <20 12 JD <20 <20 <20 <20 23 D 12 JD <20 <20 87 D 33 D 110 D 86 D 200 DMW-9 12/3/18 7.4 NR NR 99 <5 NR NR <5 14 JD 14 JD NR 19 NR NR NR NR 210 220 430Note:Wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-9, MW-12 to MW-17, MW-19 and MW-21 not sampled 12/5/17. All sample analytical concentrations are reported in ug/l.Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard. GCL = gross contamination level.SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs.NL = Not Listed. NR = Not Requested or Not reported by laboratory.n-propylbenzenep-IsopropyltolueneIsopropylbenzeneIsopropyl Ethern-Butylbenzenesec-ButylbenzeneAnalytical Method Contaminant of Concern BenzeneEthylbenzeneMethyl tertiary butyl ether (MTBE)NaphthaleneNaphthaleneToluene0-xylenesM&P xylenesTotal XylenesTrichloroetheneTrichlorofluoro -methane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene Page 2 of 2EPAEPAEPAEPAEPAEPAEPAEPAEPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA 624 6200B 6200B 624 624 6200B 6200B 8260 624 625 6200B 624 6200B 6200B 6200B 6200B 624 624 624 Well ID Date Sampled (m/dd/yy) MW-10 2/15/23 10 NR NR 41 <0.36 NR NR <0.26 34 NR NR 9.2 NR NR NR NR 110 100 210 MW-10 7/21/22 38 D NR NR 70 D <20 NR NR <20 38 D NR NR 31 D NR NR NR NR 180 D 180 D 360 DMW-10 7/12/21 82 D NR NR 65 D <10 NR NR <10 21 D <50 NR 53 D NR NR NR NR 200 D 130 D 330 DMW-10 10/14/20 110 NR NR 89 <1 NR NR 1.70 25 <50 NR 55 NR NR NR NR 210 180 390 MW-10 7/5/19 21 NR NR 77 <5 NR NR <5 <100 <100 NR 75 NR NR NR NR 180 230 410MW-10 12/3/18 82 NR NR 120 <5 NR NR <5 39 JD 39 JD NR 190 NR NR NR NR 340 500 840MW-10 12/5/17 130 D NR NR 54 D <5 NR NR 3.8 JD 20 D 19 NR 430 D NR NR NR NR 110 D 230 D 340 D MW-11 2/15/23 9.1 NR NR 120 <0.36 NR NR 4 35 NR NR 97 NR NR NR NR 250 H 290 H 540 HMW-11 7/21/22 12 JD NR NR 340 D <20 NR NR <20 <20 NR NR 200 D NR NR NR NR 770 D 870 D 1,600 DMW-11 7/12/21 36 D NR NR 69 D <20 NR NR <20 16 JD <50 NR 100 D NR NR NR NR 180 180.0 360MW-11 10/14/20 65 NR NR 74 <10 NR NR <10 11 <100 NR 140 NR NR NR NR 210 200 420MW-11 3/16/20 40 D 35 D 15 D 99 D <20 20 27 D <20 21 D NR 37 D 180 D <20 <20 220 D 70 D 250 D 290 D 550 DMW-11 12/3/18 160 NR NR 220 <5 NR NR 3.5 35 JD 35 JD NR 440 NR NR NR NR 380 600 970MW-11 12/5/17 19 D NR NR 210 D NR NR NR <1.6 39 D 140 JD NR 200 D NR NR NR NR 350 D 630 D 990 D MW-12 2/15/23 3 NR NR 43 <0.36 NR NR <0.26 21 NR NR 2 NR NR NR NR 130 110 240MW-12 7/21/22 2.9 D NR NR 44 D <2 NR NR <2 16 D NR NR 19 D NR NR NR NR 140 D 130 D 270 DMW-12 7/12/21 <1 NR NR 15 <1 NR NR <1 5 <10 NR 2.9 NR NR NR NR 42 28 70MW-12 10/14/20 <1 NR NR 1.3 <1 NR NR <1 0.75 J <10 NR <1 NR NR NR NR 3.2 2.2 5.4MW-12 7/5/19 <1 NR NR 14 <1 NR NR <1 3.6 J 3.6 J NR 2.8 NR NR NR NR 45 12 56MW-12 12/3/18 <5 NR NR 12 <5 NR NR <5 <50 <50 NR 18 NR NR NR NR 35 18 53 MW-13 2/15/23 3 NR NR 44 <0.36 NR NR 3.1 20 NR NR 20 NR NR NR NR 86 130 220MW-13 7/21/22 3.5 JD NR NR 110 D <5 NR NR <5 19 D NR NR 59 D NR NR NR NR 230 D 330 D 560 DMW-13 7/12/21 0.84 J NR NR 63 <1 NR NR <1 8.5 5.2 J NR 34 NR NR NR NR 120 140 260 MW-13 10/14/20 2.4 NR NR 75 <1 NR NR <1 11 <50 NR 33 NR NR NR NR 150 230 380MW-13 12/2/18 <1 NR NR 9 <1 NR NR <1 6.1 JD 6.1 JD NR 6.6 NR NR NR NR 18 27 45 MW-14 2/15/23 1.3 NR NR 3 <0.36 NR NR <0.26 3.8 NR NR <0.57 NR NR NR NR 7 3 11MW-14 7/21/22 <1 NR NR 3 <1 NR NR <1 1.3 NR NR <1 NR NR NR NR 7.4 4.5 12MW-14 7/12/21 <1 NR NR 10 <1 NR NR <1 4.0 <10 NR <1 NR NR NR NR 47 5.9 52 MW-14 10/14/20 2.5 NR NR 43 <1 NR NR <1 11 6.8 NR 1.6 NR NR NR NR 110 30 140MW-14 3/16/20 <1 <1 2.7 51 <1 5.7 2.0 <1 13 10 7.9 <1 <1 23.0 25.0 160 32 190MW-14 12/2/18 <10 NR NR 50 <10 NR NR <10 <30 <30 NR 25 NR NR NR NR 140 39 180 MW-15 2/15/23 6 NR NR 9 <0.36 NR NR 30 10 NR NR 3.1 NR NR NR NR 60 27 87MW-15 7/21/22 26 D NR NR 14 D <2 NR NR 2.4 D 8 D NR NR 4.8 D NR NR NR NR 46 D 39 D 84 DMW-15 7/12/21 2.9 JD NR NR 11 D <5 NR NR 8.4 D 12 D <40 NR 12 D NR NR NR NR 48 D 29 D 78 DMW-15 10/14/20 23 NR NR 34 <1 NR NR 8.5 11 <200 NR 27 NR NR NR NR 180 110 290MW-15 7/5/19 9.8 NR NR 30 <1 NR NR 1.8 <100 <100 NR 15 NR NR NR NR 140 180 320MW-15 12/3/18 25 NR NR 150 <20 NR NR <20 28 JD 28 JD NR 66 NR NR NR NR 330 420 750 MW-16 2/15/23 <0.57 NR NR 7 H <0.36 NR NR 0.44 JH 6.5 H NR NR 2.5 H NR NR NR NR 27 H 15 H 42 HMW-16 7/21/22 10 D NR NR 6.7 D <2 NR NR <2 5.3 D NR NR <2 NR NR NR NR 32 D 18 D 49 DMW-16 7/12/21 <20 NR NR 23 D <20 NR NR <20 24 D <100 NR 17 JD NR NR NR NR 73 D 46 D 120 DMW-16 10/14/20 47 NR NR 42 <10 NR NR <10 9.4 D 7.9 J NR 11 NR NR NR NR 120 62 180MW-16 3/16/20 11 JD <20 <20 14 JD <20 <20 <20 <20 8.4 JD <20 <20 <20 <20 <20 38 D 18 D 62 D 30 JD 92MW-16 12/3/18 <10 NR NR 59 <10 NR NR <10 <100 <100 NR <10 NR NR NR NR 190 210 400 MW-17 2/15/23 5.9 H NR NR 64 H <0.36 NR NR 33 H 21 H NR NR 21 H NR NR NR NR 140 H 110 H 250 H MW-17 7/21/22 5.8 D NR NR 56 D <5 NR NR <5 14 D ND NR 22 D NR NR NR NR 160 D 150 D 310 DMW-17 7/12/21 <20 NR NR 70 D <20 NR NR <20 24 D <50 NR 70 D NR NR NR NR 180 D 180 D 370 DMW-17 10/14/20 <5 NR NR 40 <5 NR NR <5 17 <200 NR 51 NR NR NR NR 130 130 260 MW-17 7/5/19 14 NR NR 110 <5 NR NR <5 <100 <100 NR 68 NR NR NR NR 180 250 430MW-17 12/3/18 8.6 NR NR 240 <5 NR NR 4.8 <200 <200 NR 150 NR NR NR NR 460 670 1100NRNR MW-18 2/15/23 <0.57 H NR NR <0.46 H <0.36 NR NR <0.26 2.8 H NR NR <0.57 NR NR NR NR <0.44 <1.2 <1.6MW-18 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3MW-18 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <2MW-18 3/16/20 <1 0.83 J NR 0.92 J <1 0.56 J <1 <1 0.49 J <10 0.70 J <1 <1 <1 3.4 2.2 2.1 2.0 4.1MW-18 7/5/19 <1 NR NR NR <1 NR NR <1 <10 <10 NR <1 NR NR NR NR 1.6 <2 2.3MW-18 12/2/18 <1 NR NR 3.3 <1 NR NR <1 <10 <10 NR <1 NR NR NR NR 8.8 6.8 16MW-18 12/5/17 33 NR NR 9.4 <1 NR NR 0.75 J 2.5 3.6 J NR 110 NR NR NR NR 18 43 62 MW-19 2/15/23 5.6 H NR NR 7.6 H <0.36 NR NR 1.1 H 7.2 H NR NR <0.57 H NR NR NR NR 37 H 20 H 57 HMW-19 7/21/22 <2 NR NR 7.8 D <2 NR NR <2 5.4 D NR NR 22 D NR NR NR NR 160 D 150 D 310 DMW-19 7/12/21 <1 NR NR 9.50 <1 NR NR <1 4.8 <10 NR <1 NR NR NR NR 56 18.00 74MW-19 10/14/20 <1 NR NR 36 <1 NR NR <1 14 9.3 NR 2.5 NR NR NR NR 170 60 230MW-19 7/5/19 3.3 NR NR 24 <1 NR NR <1 7.8 J 7.8 J NR 21 NR NR NR NR 120 42 160MW-19 12/2/18 5.2 NR NR 46 <5 NR NR <5 11 JD 11 JD NR 24 NR NR NR NR 160 40 200 MW-20 2/15/23 5.1 H NR NR 130 H <0.36 H NR NR 1.20 24 H NR NR 28 H NR NR NR NR 160 H 150 H 310 HMW-20 7/21/22 7.6 JD NR NR 140 D <10 NR NR <10 28 D NR NR 170 D NR NR NR NR 270 D 380 D 660 DMW-20 7/12/21 <5 NR NR 130 D <5 NR NR <5 22 D <50 NR 53 D NR NR NR NR 230 D 310 D 540 DMW-20 10/14/20 8.0 NR NR 120 <1 NR NR 1.4 27 <50 NR 53 NR NR NR NR 160 210 370 MW-20 3/16/20 <20 16 JD <20 100 D <20 13 JD 16 JD <20 15 JD <20 26 D 9.8 JD <20 <20 160 D 49 D 160 D 200 D 360 DMW-20 12/2/18 17 NR NR 97 <2 NR NR <2 12 12 NR 14 NR NR NR NR 150 230 380MW-20 12/5/17 76 D NR NR 43 D <2 NR NR 4.3 D 12 D 12 NR 260 D NR NR NR NR 68 D 160 D 230 MW-21 2/15/23 <0.57 NR NR <0.46 <0.36 NR NR <0.26 2.8 H NR NR <0.57 H NR NR NR NR <0.44 H <1.2 <1.6 HMW-21 7/12/21 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <3 MW-21 10/14/20 <1 NR NR <1 <1 NR NR <1 <1 <10 NR <1 NR NR NR NR <1 <2 <2MW-21 3/16/20 <1 <1 NR <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.80 J <1 <1 0.40 J 0.40 JMW-21 12/2/18 <1 NR NR <1 <1 NR NR <1 <10 <10 NR <1 NR NR NR NR <1 <2 <2 NCAC 2L Standard (ug/L)1 70 70 600 70 70 25 20 6 6 70 600 3 2000 400 400 500 500 500NCDENR UST Section GCLs (ug/L)5,000 6,900 8,500 84,500 70,000 25,000 11,700 20,000 6,000 6,000 30,000 260,000 3,000 2,000,000 28,400 25,000 85,500 85,500 85,500Note:Wells MW-1, MW-2, MW-3, MW-4, MW-7, MW-9, MW-12 to MW-17, MW-19 and MW-21 not sampled 12/5/17.All sample analytical concentrations are reported in ug/l.Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard.GCL = gross contamination level.SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs.NL = Not Listed.NR = Not Requested or Not reported by laboratory. Analytical Method Contaminant of Concern Benzenen-Butylbenzenesec-ButylbenzeneEthylbenzeneIsopropyl EtherIsopropylbenzenep-IsopropyltolueneMethyl tertiary butyl ether (MTBE)NaphthaleneNaphthalenen-propylbenzeneTolueneTrichloroetheneTrichlorofluoro -methane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene0-xylenesM&P xylenesTotal Xylenes SEMINOLE MART 2 CLES PROJECT NO 17-051A GROUNDWATER MONITORING REPORT MARCH 10, 2023 TABLE 6 GROUNDWATER ANALYTICAL RESULTS SEMNOLE MART NO. 2 691 SEMINOLE ROAD BROADWAY. HARNETT COUNTY, NORTH CAROLINA NCDENR INCIDENT NO. 42025 NCDEQ UST SECTION FACILITY ID. 0-000014231 CLES PROJECT NO. 17-051A EPA EPA EPA EPA EPA EPA EPA EPA EPA 624 624 624 8260 624 624 624 624 624 Well ID Date Sampled (m/dd/yy) MW-1 NS MW-2 NS MW-3 NS MW-4 NS MW-5 2/15/23 <0.57 <0.46 <0.36 <0.26 <0.12 <0.57 <0.44 <1.2 <1.6 MW-6 2/15/23 <0.57 <0.46 <0.36 <0.26 <0.12 <0.57 <0.44 <1.2 <1.6 MW-7 2/15/23 <0.57 <0.46 <0.36 <0.26 <0.12 <0.57 <0.44 <1.2 <1.6 MW-8 2/15/23 6.8 22 <0.36 5 13 1.3 63 48 110 MW-9 2/15/23 15 25 <0.36 <0.26 10 2.5 59 47 110 MW-10 2/15/23 10 41 <0.36 <0.26 34 9.2 110 100 210 MW-11 2/15/23 9.1 120 <0.36 4.0 35 97 250 H 290 H 540 H MW-12 2/15/23 3 43 <0.36 <0.26 21 2 130 110 240 MW-13 2/15/23 3 44 <0.36 3.1 20 20 86 130 220 MW-14 2/15/23 1.3 3 <0.36 <0.26 3.8 <0.57 7 3 11 MW-15 2/15/23 6 9 <0.36 30 10 3.1 60 27 87 MW-16 2/15/23 <0.57 7 H <0.36 0.44 JH 6.5 H 2.5 H 27 H 15 H 42 H MW-17 2/15/23 5.9 H 64 H <0.36 33 H 21 H 21 H 140 H 110 H 250 H MW-18 2/15/23 <0.57 H <0.46 H <0.36 <0.26 2.8 H <0.57 <0.44 <1.2 <1.6 MW-19 2/15/23 5.6 H 7.6 H <0.36 1.1 H 7.2 H <0.57 H 37 H 20 H 57 H MW-20 2/15/23 5.1 H 130 H <0.36 H 1.20 24 H 28 H 160 H 150 H 310 H MW-21 2/15/23 <0.57 <0.46 <0.36 <0.26 2.8 H <0.57 <0.44 H <1.2 <1.6 H NCAC 2L Standard (ug/L)1 600 70 20 6 600 500 500 500 NCDENR UST Section GCLs (ug/L)5,000 84,500 70,000 20,000 6,000 260,000 85,500 85,500 85,500 Note: Wells MW-1, MW-2, MW-3 and MW-4 not sampled 2/15/23. All sample analytical concentrations are reported in ug/l. Bold depicts constiuents detected above the sample practical quantitation limit. SHADED AND BOLD numbers indicate concentrations above NCAC 2L Groundwater Quality Standard. GCL = gross contamination level. SHADED AND BOLD and RED numbers indicate concentrations above NCAC 2L Groundwater Quality Standard and NCDENR GCLs. NL = Not Listed. NR = Not Requested or Not reported by laboratory. SEE ANALYTICAL REPORT FOR FLAG DEFINITIONNS AND QUALITY ASSURANCE AND QUALITY CONTROL INFORMATION. Analytical Method Contaminant of Concern BenzeneTolueneEthylbenzeneIsopropyl EtherMethyl tertiary butyl ether (MTBE)Naphthalene0-xylenesM&P xylenesTotal Xylenes FIGURES Figure 1: Vicinity Map Figure 2: Site Map Figure 3: Groundwater Potentiometric Map (March 8, 2023) Figure 4: Groundwater Constituent Concentrations (February 15, 2023) Figure 5: Pre-Remedial Benzene Isoconcentration Map (November 1, 2017) Figure 6: Benzene Isoconcentration Map (February 15, 2023) ) 0.3 miles Source: https://apps.nationalmap.gov/downloader/#/startUp North Job No.: Scale: Date: Fig. No.: Broadway, North Carolina 8005 Clear Brook Drive Raleigh, NC 27615 17-051A March 10, 2023 VICINITY MAP Seminole Mart No. 2 As Shown 691 Seminole Road 1 SITE Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.: Broadway, North Carolina Raleigh, NC 27615 SITE MAP March 10, 2023 17-051A As Shown Seminole Mart No. 2 691 Seminole Road 8005 Clear Brook Drive 2Assumed North Base Map Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.: GROUNDWATER 17-051A POTENTIOMETRIC MAP (3-8-23)As Shown Seminole Mart No. 2 March 10, 2023 691 Seminole Road 8005 Clear Brook Drive 3Broadway, North Carolina Raleigh, NC 27615LEGENDApproximate Monitor Well LocationNote: Measurements fromMW-1not considered in groundwater contours.(50.10) Groundwater Elevation (Ft) 3-8-23 Top of casing elevations reported by by East Coast Environmental, PA. 51.00Groundwater Elevation Contour (Ft)Elevation units in feet relativeto an assigned elevation of an on-site benchmark.0.0084Groundwater Flow Direction andHydraulic Gradient(49.11)(49.19)(49.11)(48.50)(48.91)(48.92)(48.94)(49.05)(49.01)(49.05)(48.66)(49.06)(49.19)(49.14)(49.25)(49.30)(49.34(49.21)(48.70)(49.82)(55.0)*49.00 49.00 49 . 0 0 49.00 Assumed 0.0058 MW-12 Benzene 3 Ethylbenzene 43Toluene2o-xylenes 130m,p-xylenes 110 MW-13Benzene 3Ethylbenzene44MTBE 3.1 Toluene 20o-xylenes 86 MW-15 Benzene 6Ethylbenzene9MTBE30Toluene3.1o-xylenes 60m,p-xylenes 27 Naphthalene 10 MW-17 Benzene 5.9 Ethylenzene 64Toluene21o-xylenes 140m,p-xylenes 110 GROUNDWATER CONSTITUENTCONCENTRATION MAPFEBRUARY 15, 2023SEMINOLE MART NO. 2691 SEMINOLE ROADBROADWAY, NORTH CAROLINADATE: MARCH 10, 2023Note:Samples collected on February 15, 2023.Constiuent concentrations in micrograms per liter (ug/L).Source Map: East Coast Environmental, PA CAP 11/1/17 MW-10 Benzene 10 Ethylbenzene 41 Toluene 9.2o-xylenes 110m,p-xylenes 100Naphthalene34 MW-19 Benzene 5.6Ethylbenzene 7.6MTBE1.1o-xylenes 37m,p-xylenes 20 SCALE:AS SHOWNMW-6 No VOCs Detected MW-7 No VOCs Detected MW-8 Benzene 6.8Ethylbenzene22 MTBE 5Toluene1.3 o-xylenes 63 m,p-xylenes 48Naphthalene13 MW-3 Not Sampled MW-18 Naphthalene 2.8MW-9 Benzene 15 Ethylbenzene 25 Toluene 2.5o-xylenes 59m,p-xylenes 47Naphthalene10 MW-20 Benzene 5.1 Ethylbenzene 130 MTBE 1.1Toluene28o-xylenes 160m,p-xylenes 150 MW-21 Naphthalene 2.8MW-1Not Sampled MW-11 Benzene 9.1Ethylbenzene120MTBE4 Toluene 97o-xylenes 250m,p-xylenes 290 Naphthalene 35 MW-2 MW-4 Not Sampled MW-5 No VOCs Detected 8005 CLEAR BROOK DRIVERALEIGH, NC 27615PROJECT NO.: 17-MW-14 Benzene 1.3 Ethylbenzene 3o-xylenes 7 m,p-xylenes 3Naphthalene3.8 MW-16Benzene <0.57Ethylbenzene7Naphthalene6.5o xylenes 27 Map Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.: PREREMEDIAL BENZENE ISONCENTRATION MAP 17-051A (NOVEMBER 1, 2017)As Shown Seminole Mart No. 2 March 10, 2023 5691 Seminole Road 8005 Clear Brook Drive Broadway, North Carolina Raleigh, NC 27615 Assumed Base Map Source: East Coast Environmental, PA CAP 11/1/17 Job No.: Scale: Date: Fig. No.:691 Seminole Road 8005 Clear Brook Drive 6Broadway, North Carolina Raleigh, NC 27615 BENZENE CONCENTRATIONS 17-051A (February 15, 2023)As Shown Seminole Mart No. 2 July 25, 2022 (437.16) (438.79) (437.23) (435.17) (436.06) (435.07) (437.03) (437.23) (436.81) (437.16) (437.15)(436.89) (436.48) (437.23)* (437.08) LEGEND Approximate Monitor Well Location (15) Benzene concentration in groundwater in micrograms per liter (ug/L) from samples collected 2-15-23. 0.66 Free Product Thickness (Ft) on groundwater measured 3-8-23. Benzene concentrations above the 15A NCAC 2L Groundwater Quality Standard (1.0 ug/l). Approximate area with measurable thickness (0.01 FT.) or more of Free Product on the groundwater table. (<1.0) Benzene concentrations below the sample method reporting limit. (437.33)* Abandoed Abandoned Abandoned (NS)0.66(NS)<0.01(NS)<0.01(<0.57(15)<0.01(10)0.01(<0.57)(<0.57)(9.1)(6.8)<0.01(<0.57)(5.6)<0.01(6)<0.01(1.3)<0.01(3.0)<0.01(<0.57)<0.01(<0.57)<0.01(5.1)<0.01(3.0)<0.01(5.9)<0.01Assumed North1.0 UG/L 0.01(NS) 3.62 APPENDICES Appendix I Standard Operating Procedures Appendix II Calculations Appendix III Laboratory Analytical Results and Chain of Custody Forms APPENDIX I Standard Operating Procedures STANDARD OPERATING PROCEDURES Soil Sampling, Soil Boring and Monitor Well Installation, Well Development Soil borings are completed with a stainless steel hand auger, direct-push hydraulic drill or auger rotary drill using either a macro core sampler, 3-1/4, 4-1/4, or 6-1/4-inch inside diameter hollow stem augers. Soil borings are typically sampled at discrete intervals from the bucket of a clean stainless steel hand auger, direct push stainless steel sampler with acetate sleeve, or a split barrel sampler. Monitor wells are completed in selected soil borings using one, two, or four-inch inside diameter PVC casing and machine slotted screen intervals in accordance with North Carolina guidelines. Clean quartz sand is typically used to fill the boring annulus around the well screen to approximately one foot above the screened interval, approximately one foot of hydrated bentonite is placed over the sand pack and neat cement grout or bentonite is placed above the well seal. Concrete is placed to secure the wellhead in the top three feet of boring annulus. Wellheads may be completed with either flush mounted traffic-bearing protectors with bolt down covers or steel above-ground protectors set in a concrete pad. Temporary wells or piezometers may be completed with the PVC riser cut at or above grade. The wellheads are secured with locking caps. Wells may be developed using a bailer, electric submersible pump, pneumatic pump, or peristaltic pump. When wells are developed by the driller, they may be developed with air injection, water injection, pumping or bailing. Soil boring logs and well construction details are typically prepared for presentation in a report appendix. Borings completed in bedrock may be drilled using air rotary, coring, or sonic drilling methods. Liquid Levels Groundwater level measurements are typically obtained using an electronic sounding/interface detection device which registers a tone or illuminated light when a probe makes contact with the groundwater. Depth to groundwater measurements are obtained by lowering a probe attached to a cable marked in 0.01 feet intervals into the well until the probe of the meter intersects the product or water surface. The measurement from the top of the riser pipe or top of casing (T.O.C.) to the liquid level is recorded. The measurement is recorded to the nearest 0.01 foot. The electronic interface probe is decontaminated between measurement locations. LNAPL Measurements Light Non-Aqueous Phase Liquid (LNAPL) present on the water table is measured using an oil/water interface probe. The electronic meter has both an audible and illuminating light that indicate when a liquid level is encountered. The oil/water interface probe registers a solid tone/light when LNAPL petroleum product is encountered and a beeping tone/light when groundwater is encountered. Depth to LNAPL measurements are obtained by lowering a probe attached to a cable marked in 0.01 feet intervals into the well until the probe of the meter intersects the product or groundwater. The measurements from the top of the riser pipe or top of casing (T.O.C.) to the liquid level is recorded. The measurement is recorded to the nearest 0.01 foot. The thickness of LNAPL is calculated by subtracting the depth to LNAPL measurement from the depth to groundwater measurement. The electronic interface probe is decontaminated between measurement locations. Soil Sampling Soil sampling is performed in general accordance with ASTM: 1586-84 where applicable. Sampling procedures are followed to protect the chemical integrity of the soil samples and minimize the potential for cross contamination. This includes discarding of the exterior of the sample which contacts the auger bucket, acetate sleeve, or split barrel sampler, collecting the interior soil for screening with the PID or FID, and either pressure washing, steam cleaning, or washing with non-phosphate detergent and/or rinsing sampling equipment with clean water between sampling intervals. The samples are placed in glass jars, sealed, and placed in an ice filled cooler. An aliquot of the sample is typically placed in a clean sealable bag and allowed to reach ambient air temperature. The PID or FID is used to measure total organic vapors (TOV) in the head space in each sample bag. Excavation soil samples may also be collected from the bucket of excavation equipment. Care to collect soil samples from excavation equipment includes retrieving native soil from material that has not made contact with the excavating equipment. Samples are collected in sealable bags or by directly filling sample containers using new gloves, laboratory provided sampling utensils, or decontaminated stainless steel sampling equipment. Field personnel don new, unused, disposable nitrile gloves at soil boring and sampling locations. Gloves are changed between each sample interval. Sampling equipment such as hand auger extensions and buckets, direct push samplers, split spoons and/or drilling augers, are decontaminated before collecting samples. Groundwater Sampling Bailer or Dedicated Pump Groundwater samples are collected using new dedicated polyethylene bailers or dedicated pump with polyethylene tubing (or equal) at each monitor well. Before obtaining a sample, a minimum of three well volumes of groundwater is typically evacuated from the well to ensure collection of a sample representative of the in-situ groundwater conditions. Field parameters (not limited to pH, specific conductance and temperature) are measured on purged groundwater after each volume approximately equal to one water column in the well is evacuated to monitor the changes of the field parameters in the groundwater as the monitor wells are purged. Once the fluctuation of field parameters stabilizes to within ten percent over three consecutive purge parameter measurements, or after the well is purged dry and allowed to recover, the record sample is collected. The groundwater samples are collected by directly filling laboratory-supplied containers with groundwater poured directly from the dedicated disposable bailer or polyethylene tubing attached to the dedicated well pump. Samples will be then transferred to insulated containers with ice for transport to the laboratory. Field personnel don clean chemical resistant/non-reactive gloves at each well during purging and don a new pair of gloves before filing sample containers. Peristaltic Pump (Low Flow Method) Groundwater is purged from the monitor wells using a peristaltic pump with either dedicated Teflon-lined or PVC tubing inserted into the well, or using a clean section of disposable silicon and a clean section of PVC tubing inserted into the well by the following low flow sampling methods. The silicon tubing is inserted into the peristaltic pump. The silicon is attached to the PVC or Teflon-lined tubing that is inserted into the monitor well to the bottom of the well screen. The tubing is pulled back off of the bottom of the well with the end located within the screened interval of the well and the peristaltic pump is started. The initial flow from the well that passes through the peristaltic pump tubing is discharged into a bucket or container. Once the initial turbid liquid effluent becomes relatively clear (lower turbidity) the effluent may be passed through a flow cell for parameter measurements or captured in a container so that a multi meter can be used to monitor field parameters. This minimizes potential fowling of the flow cell and meters used to monitor field parameters. Field parameters will be measured on groundwater purged from each well to monitor the changes of the field parameters in the groundwater as the monitor wells will be purged. Field parameters will be recorded after approximately each consecutive two minutes of pumping from the peristaltic pump. Once the fluctuation of field parameters stabilizes at each well to within ten percent over three consecutive measurements, the record sample is collected. If the well is purged dry, it is allowed to recharge sufficiently for a sample to have be collected. Samples will then be transferred directly from the section of silicon tubing into containers supplied by the laboratory. Field personnel don clean chemical resitant/non-reactive gloves at each well during purging and before sampling activities. Decontamination Procedures The potential for cross-contamination between sample locations is minimized by thoroughly cleaning the sampling equipment, both prior to the initiation of sampling and between uses. Glass and Teflon® sampling equipment, in-situ hydraulic conductivity measurement equipment, bucket augers and split-spoon samplers used for soil sampling, and other tools and equipment will be decontaminated between each use according to the following procedures: • Remove excess soil/sludge as necessary. • Wash and scrub the equipment with a phosphate-free detergent in a hot tap water (prior to field use) or ambient tap water solution. Use a brush to remove particulate matter and surface films. Repeat as necessary. • Rinse thoroughly with tap water. • Rinse thoroughly with analyte-free water (deionized water). • Allow the equipment to air dry. • Prevent inadvertent contamination during storage and transport. All personnel engaged in equipment decontamination wear clean, disposable chemical resistant non-reactive gloves. Aquifer Testing Procedures Aquifer hydraulic conductivity testing is performed at selected wells to evaluate the relative hydraulic conductivity at targeted locations. Rising head slug tests will be performed at target monitor well/piezometer locations. Prior to performing the tests, the monitor wells/piezometers will be opened and allowed to equilibrate. The water level in each well/piezometer is measured to the nearest 0.01 feet using a decontaminated water level probe. This reading is used as the initial reading for the tests. Slug tests will be performed in the monitor wells/piezometers by installing into the monitor well a pressure transducer equipped with a data recorder or that is attached to a data recorder. After obtaining an initial water level reading, a clean polyethylene bailer of known volume is submerged in the water in the well/piezometer. The filled bailer is removed and the water level in the well/piezometer is monitored with the pressure transducer as the water level in the well/piezometer returned to static conditions. The volume of water removed by the bailer is noted. Tests may be repeated on or more times in each test well/piezometer. The transducer data is graphically evaluated in the field using Win-Situ (or equal) computer software. The Win-Situ data is imported into an MS Excel® Workbook for analysis by Bouwer-Rice techniques for partially or fully penetrating well screens using Aqtesolv® computer software. The Bouwer-Rice techniques make a variety of simplifying assumptions in the evaluation of slug test data. These include the assumptions that the aquifer in question is homogenous, isotropic, and extends infinitely in the horizontal direction (Bouwer-Rice, 1976). APPENDIX II Calculations Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SW Site Name:Temperature oF Low: 40 High: 60 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order LL 21 LL 18 LL 19 LL 11 LL 5 Total Well Depth (ft) Depth to liquid Depth to Water (ft) Water Column (ft) Well Volume (X3) Product thickness Purge Time Interval Temp. oC v1 v4 v1 v4 v1 v4 v1 v4 v1 17.8 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity mS/cm v1 v4 v1 v4 v1 v4 v1 v4 v1 0.03 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 v4 v1 v4 v1 v4 v1 v4 v1 6 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 2/15/23 NS 2/15/23 NS 2/15/23 NS 2/15/23 NS 2/25/23 1255 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments:diesel fuel dry after product removed Dry MW-4 MW-5 40 45 45 45 48 Scott Yow 17-051A Seminole Mart 691 Seminole Road MW-1 MW-2 MW-3 35.10 44.54 44.22 44.33 44.26 38.72 44.54 44.88 44.33 44.26 1.28 0.46 0.12 0.67 3.74 0.6 0.2 0.1 0.3 1.8 Dry 3.62 0.00 0.66 0.00 0.00 dry after product removed Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order LL 3 LL 4 LL 13 LL 20 LL 15 Total Well Depth (ft) Depth to Product Depth to Water (ft) Water Column (ft) Well Volume (X3) Product Thickness Purge Time Interval Temp. oC v1 17.6 v4 v1 17.6 v4 v1 17.7 v4 v1 17.8 v4 v1 17.6 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.07 v4 v1 0.08 v4 v1 0.13 v4 v1 0.11 v4 v1 0.04 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.00 v4 v1 6.00 v4 v1 6.00 v4 v1 6.00 v4 v1 6.00 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 2/15/23 1330 2/15/23 1315 2/15/23 1500 2/15/23 1445 2/25/23 1415 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments:clear cloudy cloudy Scott Yow 17-051A Seminole Mart 691 Seminole Road MW-6 MW-7 MW-8 MW-9 MW-10 48 48 50 50 50 43.73 43.73 44.32 44.42 45.13 43.73 43.73 44.32 44.42 45.14 4.27 4.27 5.68 5.58 4.86 2.1 2.1 2.8 2.7 2.4 clear cloudy 0.00 0.00 0.00 0.00 0.01 Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order LL 16 LL 8 LL 12 LL 6 LL 9 Total Well Depth (ft) Depth to Product Depth to Water (ft) Water Column (ft) Well Volume (X3) Product Thickness Purge Time Interval Temp. oC v1 17.9 v4 v1 17.9 v4 v1 17.8 v4 v1 18 v4 v1 17.6 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.24 v4 v1 0.09 v4 v1 0.14 v4 v1 0.07 v4 v1 0.19 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.5 v4 v1 6 v4 v1 6 v4 v1 6 v4 v1 6 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 2/15/23 1600 2/15/23 1405 2/15/23 1505 2/15/23 1425 2/25/23 1430 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments:cloudy to clear cloudy clear Scott Yow 17-051A Seminole Mart 691 Seminole Road MW-11 MW-12 MW-13 MW-14 MW-15 50 50 50 50 50 44.52 43.81 44.49 43.73 44.63 45.13 43.81 44.49 43.73 44.63 4.87 6.19 5.51 6.27 5.37 2.4 3.0 2.7 3.1 2.6 tan to clear gray to cloudy 0.61 0.00 0.00 0.00 0.00 Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order LL 10 LL 14 LL 2 LL 7 LL 17 Total Well Depth (ft)Depth to Product/1st liquid Depth to Water (ft) Water Column (ft) Well Volume (X3) Product Thickness Purge Time Interval Temp. oC v1 17.4 v4 v1 17.9 v4 v1 17.3 v4 v1 17.8 v4 v1 17.6 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.19 v4 v1 0.24 v4 v1 0.03 v4 v1 0.1 v4 v1 0.28 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 6.50 v4 v1 6.50 v4 v1 6.50 v4 v1 6.00 v4 v1 6.00 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 2/15/23 1345 2/15/23 1550 2/15/23 1345 2/15/23 1445 2/25/23 1615 Preservative HCL Nitric HCL Nitric HCL Nitric HCL Nitric HCL Nitric Sampler's Name: Comments:cloudy to clear yellow brown to clear cloudy Scott Yow 17-051A Seminole Mart 691 Seminole Road MW-16 MW-17 MW-18 MW-19 MW-20 50 50 45 45 4845.39 44.69 43.37 43.73 44.74 45.39 44.69 43.37 43.73 44.74 4.61 5.31 1.63 1.27 3.26 2.3 2.6 0.8 0.6 1.6 cloudy cloudy to clear 0.00 0.00 0.00 0.00 0.00 Groundwater Sampling Form - Cape Lookout Environmental Sciences, PLLC Client:CLES Project No.: Wind Speed: 0-10 mph Direction From: SSW Site Name:Temperature oF Low: 70 High: 90 Site Address:Cloud Cover: 10 % Rain: 0 inches Well ID / Diameter Collection Order LL 1 Total Well Depth (ft)Depth to Product Depth to Water (ft) Water Column (ft) Well Volume (X3) Product ThicknessPurge Time Interval Temp. oC v1 17.3 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Barometric pressure mmHgv1 v4 v1 v4 v1 v4 v1 v4 v1 v4v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO %v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 DO mg/L v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Conductivity uS/cm v1 0.03 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH v1 7.00 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 pH mV v1 v4 v1 v4 v1 v4 v1 v4 v1 v4v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 ORP v1 v4 v1 v4 v1 v4 v1 v4 v1 v4 v2 v5 v2 v5 v2 v5 v2 v5 v2 v5 v3 v6 v3 v6 v3 v6 v3 v6 v3 v6 Purge Rate In. Fin.In. Fin.In. Fin.In. Fin.In. Fin. Final Dissolved O2 mg/L oC mg/L oC mg/L oC mg/L oC mg/L oC Final Turbidity (ntu) Well Condition Date/Time Collected 2/15/23 1315 Field Calibration Date/Time:Date/Time:Date/Time:Date/Time:Date/Time:pH 4 7 10 pH pH pH pH C 1413 C C C C DO DO DO DO DO Tur.Tur.Tur.Tur.Tur. Preservative HCL Nitric HCL Nitric Sampler's Name: Comments:p Scott Yow 17-051A Seminole Mart 691 Seminole Road MW-21 5044.42 44.42 5.58 0 0 0 0 2.7 0.00 0.00 0.00 0.00 0.00 HYDRAULIC GRADIENT CALCULATIONS - MARCH 8, 2023 SEMINOLE MART NO. 2 691 SEMINOLE ROAD, BROADWAY, NC Purpose: To determine the hydraulic gradient Given: Gradient (a) CALCULATED FROM THREE POINT SOLUTION GRADIENT (a): i = h1 – h2 distance WHERE DISTANCE BETWEEN h1 AND h2 IS PARALLEL TO FLOW DETERMINED FROM 3 POINT PROBLEM BY PROJECTION i2 = MW-5-MW-21=49.14 -48.50 =0.0051 distance Calculate Distance for point with Elevation = MW-20 between MW-5 and MW-21 MW-5 - MW-20 = 49.14 -48.91 =45.28 0.0051 Place point on line 45.28 feet from MW-5 toward MW-21, Draw line from point to MW-20 45.28 feet from MW-5. Project MW-5 and MW-21 locations onto perpendicular line and measure new distance between projected well locations. Gradient (a): divide change in head between MW-5 to MW-21 and divide by new distance to predict gradient. MW-5- MW-21 = 49.14 -48.50 =0.0058 east-northeast flow New Distance 110.8 CLES Project No. 17-051A USING MONITOR WELLS MW-5, MW-20 and MW-21 126 0.0051 Draw line perpendicular to line drawn between MW-20 and Point APPENDIX III Laboratory Analytical Results and Chain of Custody Forms ANALYTICAL REPORT PREPARED FOR Attn: David Wells Cape Lookout Environmental Services 8005 Clear Brook Drive Raleigh, North Carolina 27615 Generated 3/8/2023 4:54:07 PM JOB DESCRIPTION Seminole Mart #2/ Cape Lookout Env. JOB NUMBER 752-3131-1 See page two for job notes and contact information. Cary NC 27511 102-A Woodwinds Industrial Court Eurofins Raleigh Page 1 of 32 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Eurofins Raleigh Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Job Notes The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Authorization Generated 3/8/2023 4:54:07 PM Authorized for release by Bill Scott, Project Manager Bill.Scott@et.eurofinsus.com (919)677-1669 Page 2 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Table of Contents Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Laboratory Job ID: 752-3131-1 Page 3 of 32 Eurofins Raleigh3/8/2023 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5 Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9 Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .18 QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .23 Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .24 Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27 Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30 Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .32 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Definitions/Glossary Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Qualifiers GC/MS VOA Qualifier Description *3 ISTD response or retention time outside acceptable limits. Qualifier H Sample was prepped or analyzed beyond the specified holding time J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. S1+Surrogate recovery exceeds control limits, high biased. Glossary These commonly used abbreviations may or may not be present in this report. ¤Listed under the "D" column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Raleigh Page 4 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Case Narrative Client: Cape Lookout Environmental Services Job ID: 752-3131-1 Project/Site: Seminole Mart #2/ Cape Lookout Env. Job ID: 752-3131-1 Laboratory: Eurofins Raleigh Narrative Job Narrative 752-3131-1 Receipt The samples were received on 2/15/2023 5:20 PM. Unless otherwise noted below, the samples arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 1.6°C GC/MS VOA Method 624.1_PREC: The surrogate recovery for the blank associated with analytical batch 752-1361 was outside the upper control limits. Method 624.1_PREC: The LCSD was biased high in recovery for: Toluene-d8 (Surr). The LCS and LCSD recovered in a similar manner; however, the LCSD was just outside of the acceptable range. All client samples had acceptable surrogate recoveries. (LCSD 752-1361/8) Method 624.1_PREC: The surrogate recovery for the blank associated with analytical batch 752-1540 was outside the upper control limits. Method 624.1_PREC: The following samples were prepped and loaded on the instrument within holding time, but due to the instrumentation sequence the data were acquired after midnight. The data were reported.MW-16 (752-3131-12), MW-17 (752-3131-13), MW-18 (752-3131-14), MW-19 (752-3131-15), MW-20 (752-3131-16) and MW-21 (752-3131-17) Method 624.1_PREC: The following samples were diluted to bring the concentration of target analytes within the calibration range: MW-11 (752-3131-7), MW-17 (752-3131-13) and MW-20 (752-3131-16). Elevated reporting limits (RLs) are provided. Method 624.1_PREC: Reanalysis of the following samples were performed outside of the analytical holding time due to over range target compounds : MW-11 (752-3131-7), MW-17 (752-3131-13) and MW-20 (752-3131-16). Method 624.1_PREC: Internal standard (ISTD) response for the following samples were outside of acceptance limits: MW-16 (752-3131-12), MW-17 (752-3131-13), MW-18 (752-3131-14), MW-20 (752-3131-16) and MW-21 (752-3131-17). The sample(s) was not re-analyzed due to insufficient volume and/or the holding time had expired. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins RaleighPage 5 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Client Sample ID: MW-5 Lab Sample ID: 752-3131-1 No Detections. Client Sample ID: MW-6 Lab Sample ID: 752-3131-2 No Detections. Client Sample ID: MW-7 Lab Sample ID: 752-3131-3 No Detections. Client Sample ID: MW-8 Lab Sample ID: 752-3131-4 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA16.8 624.1 Toluene 1.0 ug/L0.57 Total/NA11.3 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA122624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA148624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA15.0 624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA1110624.1 o-Xylene 1.0 ug/L0.44 Total/NA163624.1 Naphthalene 1.0 ug/L0.12 Total/NA113624.1 Client Sample ID: MW-9 Lab Sample ID: 752-3131-5 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA115624.1 Toluene 1.0 ug/L0.57 Total/NA12.5 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA125624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA147624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA1110624.1 o-Xylene 1.0 ug/L0.44 Total/NA159624.1 Naphthalene 1.0 ug/L0.12 Total/NA110624.1 Client Sample ID: MW-10 Lab Sample ID: 752-3131-6 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA110624.1 Toluene 1.0 ug/L0.57 Total/NA19.2 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA141624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA1100624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA1210624.1 o-Xylene 1.0 ug/L0.44 Total/NA1110624.1 Naphthalene 1.0 ug/L0.12 Total/NA134624.1 Client Sample ID: MW-11 Lab Sample ID: 752-3131-7 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA19.1 624.1 Toluene 1.0 ug/L0.57 Total/NA197624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA1120624.1 m-Xylene & p-Xylene 10 ug/L6.0 Total/NA5290H624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA14.0 624.1 Xylenes, Total 15 ug/L8.0 Total/NA5540H624.1 o-Xylene 5.0 ug/L2.2 Total/NA5250H624.1 Naphthalene 1.0 ug/L0.12 Total/NA135624.1 Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 6 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Client Sample ID: MW-12 Lab Sample ID: 752-3131-8 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA13.0 624.1 Toluene 1.0 ug/L0.57 Total/NA12.4 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA143624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA1110624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA1240624.1 o-Xylene 1.0 ug/L0.44 Total/NA1130624.1 Naphthalene 1.0 ug/L0.12 Total/NA121624.1 Client Sample ID: MW-13 Lab Sample ID: 752-3131-9 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA13.0 624.1 Toluene 1.0 ug/L0.57 Total/NA120624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA144624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA1130624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA13.1 624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA1220624.1 o-Xylene 1.0 ug/L0.44 Total/NA186624.1 Naphthalene 1.0 ug/L0.12 Total/NA120624.1 Client Sample ID: MW-14 Lab Sample ID: 752-3131-10 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA11.3 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA12.8 624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA13.1 624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA111624.1 o-Xylene 1.0 ug/L0.44 Total/NA17.4 624.1 Naphthalene 1.0 ug/L0.12 Total/NA13.8 624.1 Client Sample ID: MW-15 Lab Sample ID: 752-3131-11 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA16.2 624.1 Toluene 1.0 ug/L0.57 Total/NA13.1 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA19.2 624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA127624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA130624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA187624.1 o-Xylene 1.0 ug/L0.44 Total/NA160624.1 Naphthalene 1.0 ug/L0.12 Total/NA19.7 624.1 Client Sample ID: MW-16 Lab Sample ID: 752-3131-12 Toluene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1H2.5 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA17.0 H 624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA115H624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA10.44 J H 624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA142H624.1 o-Xylene 1.0 ug/L0.44 Total/NA127H624.1 Naphthalene 1.0 ug/L0.12 Total/NA16.5 H 624.1 Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 7 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Detection Summary Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Client Sample ID: MW-17 Lab Sample ID: 752-3131-13 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1H5.9 624.1 Toluene 1.0 ug/L0.57 Total/NA121H624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA164H624.1 m-Xylene & p-Xylene 10 ug/L6.0 Total/NA5110H624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA133H624.1 Xylenes, Total 15 ug/L8.0 Total/NA5250H624.1 o-Xylene 5.0 ug/L2.2 Total/NA5140H624.1 Naphthalene 1.0 ug/L0.12 Total/NA121H624.1 Client Sample ID: MW-18 Lab Sample ID: 752-3131-14 Naphthalene RL 1.0 ug/L MDL 0.12 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1H2.8 624.1 Client Sample ID: MW-19 Lab Sample ID: 752-3131-15 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1H5.6 624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA17.6 H 624.1 m-Xylene & p-Xylene 2.0 ug/L1.2 Total/NA120H624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA11.1 H 624.1 Xylenes, Total 3.0 ug/L1.6 Total/NA157H624.1 o-Xylene 1.0 ug/L0.44 Total/NA137H624.1 Naphthalene 1.0 ug/L0.12 Total/NA17.2 H 624.1 Client Sample ID: MW-20 Lab Sample ID: 752-3131-16 Benzene RL 1.0 ug/L MDL 0.57 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1H5.1 624.1 Toluene 1.0 ug/L0.57 Total/NA128H624.1 Ethylbenzene 1.0 ug/L0.46 Total/NA1130H624.1 m-Xylene & p-Xylene 10 ug/L6.0 Total/NA5150H624.1 Methyl tert-butyl ether 1.0 ug/L0.26 Total/NA11.2 H 624.1 Xylenes, Total 15 ug/L8.0 Total/NA5310H624.1 o-Xylene 5.0 ug/L2.2 Total/NA5160H624.1 Naphthalene 1.0 ug/L0.12 Total/NA124H624.1 Client Sample ID: MW-21 Lab Sample ID: 752-3131-17 Naphthalene RL 1.0 ug/L MDL 0.12 Analyte Result Qualifier Unit Dil Fac D Method Prep Type Total/NA1H2.8 624.1 Eurofins Raleigh This Detection Summary does not include radiochemical test results. Page 8 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-1Client Sample ID: MW-5 Matrix: WaterDate Collected: 02/15/23 12:55 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 1.0 0.57 ug/L 02/23/23 02:12 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 02:12 1<0.57Toluene 1.0 0.46 ug/L 02/23/23 02:12 1<0.46Ethylbenzene 1.0 0.36 ug/L 02/23/23 02:12 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 02:12 1<1.2m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 02:12 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 02/23/23 02:12 1<1.6Xylenes, Total 1.0 0.44 ug/L 02/23/23 02:12 1<0.44o-Xylene 1.0 0.12 ug/L 02/23/23 02:12 1<0.12Naphthalene Dibromofluoromethane (Surr)124 67-129 02/23/23 02:12 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)101 02/23/23 02:12 153-136 Toluene-d8 (Surr)119 02/23/23 02:12 159-134 Lab Sample ID: 752-3131-2Client Sample ID: MW-6 Matrix: WaterDate Collected: 02/15/23 13:30 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 1.0 0.57 ug/L 02/23/23 02:43 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 02:43 1<0.57Toluene 1.0 0.46 ug/L 02/23/23 02:43 1<0.46Ethylbenzene 1.0 0.36 ug/L 02/23/23 02:43 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 02:43 1<1.2m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 02:43 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 02/23/23 02:43 1<1.6Xylenes, Total 1.0 0.44 ug/L 02/23/23 02:43 1<0.44o-Xylene 1.0 0.12 ug/L 02/23/23 02:43 1<0.12Naphthalene Dibromofluoromethane (Surr)127 67-129 02/23/23 02:43 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)102 02/23/23 02:43 153-136 Toluene-d8 (Surr)123 02/23/23 02:43 159-134 Lab Sample ID: 752-3131-3Client Sample ID: MW-7 Matrix: WaterDate Collected: 02/15/23 13:15 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 1.0 0.57 ug/L 02/23/23 03:14 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 03:14 1<0.57Toluene 1.0 0.46 ug/L 02/23/23 03:14 1<0.46Ethylbenzene 1.0 0.36 ug/L 02/23/23 03:14 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 03:14 1<1.2m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 03:14 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 02/23/23 03:14 1<1.6Xylenes, Total 1.0 0.44 ug/L 02/23/23 03:14 1<0.44o-Xylene 1.0 0.12 ug/L 02/23/23 03:14 1<0.12Naphthalene Eurofins Raleigh Page 9 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-3Client Sample ID: MW-7 Matrix: WaterDate Collected: 02/15/23 13:15 Date Received: 02/15/23 17:20 Dibromofluoromethane (Surr)129 67-129 02/23/23 03:14 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)103 02/23/23 03:14 153-136 Toluene-d8 (Surr)119 02/23/23 03:14 159-134 Lab Sample ID: 752-3131-4Client Sample ID: MW-8 Matrix: WaterDate Collected: 02/15/23 15:00 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 6.8 1.0 0.57 ug/L 02/23/23 03:45 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 03:45 11.3Toluene 1.0 0.46 ug/L 02/23/23 03:45 122Ethylbenzene 1.0 0.36 ug/L 02/23/23 03:45 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 03:45 148m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 03:45 15.0Methyl tert-butyl ether 3.0 1.6 ug/L 02/23/23 03:45 1110Xylenes, Total 1.0 0.44 ug/L 02/23/23 03:45 163o-Xylene 1.0 0.12 ug/L 02/23/23 03:45 113Naphthalene Dibromofluoromethane (Surr)120 67-129 02/23/23 03:45 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)108 02/23/23 03:45 153-136 Toluene-d8 (Surr)116 02/23/23 03:45 159-134 Lab Sample ID: 752-3131-5Client Sample ID: MW-9 Matrix: WaterDate Collected: 02/15/23 14:45 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 15 1.0 0.57 ug/L 02/23/23 04:16 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 04:16 12.5Toluene 1.0 0.46 ug/L 02/23/23 04:16 125Ethylbenzene 1.0 0.36 ug/L 02/23/23 04:16 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 04:16 147m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 04:16 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 02/23/23 04:16 1110Xylenes, Total 1.0 0.44 ug/L 02/23/23 04:16 159o-Xylene 1.0 0.12 ug/L 02/23/23 04:16 110Naphthalene Dibromofluoromethane (Surr)112 67-129 02/23/23 04:16 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)115 02/23/23 04:16 153-136 Toluene-d8 (Surr)117 02/23/23 04:16 159-134 Eurofins Raleigh Page 10 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-6Client Sample ID: MW-10 Matrix: WaterDate Collected: 02/15/23 14:15 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 10 1.0 0.57 ug/L 02/23/23 04:47 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 04:47 19.2Toluene 1.0 0.46 ug/L 02/23/23 04:47 141Ethylbenzene 1.0 0.36 ug/L 02/23/23 04:47 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 04:47 1100m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 04:47 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 02/23/23 04:47 1210Xylenes, Total 1.0 0.44 ug/L 02/23/23 04:47 1110o-Xylene 1.0 0.12 ug/L 02/23/23 04:47 134Naphthalene Dibromofluoromethane (Surr)94 67-129 02/23/23 04:47 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)108 02/23/23 04:47 153-136 Toluene-d8 (Surr)73 02/23/23 04:47 159-134 Lab Sample ID: 752-3131-7Client Sample ID: MW-11 Matrix: WaterDate Collected: 02/15/23 16:00 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 9.1 1.0 0.57 ug/L 02/23/23 05:18 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 05:18 197Toluene 1.0 0.46 ug/L 02/23/23 05:18 1120Ethylbenzene 1.0 0.36 ug/L 02/23/23 05:18 1<0.36Isopropyl ether 10 6.0 ug/L 03/08/23 06:46 5290Hm-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 05:18 14.0Methyl tert-butyl ether 15 8.0 ug/L 03/08/23 06:46 5540HXylenes, Total 5.0 2.2 ug/L 03/08/23 06:46 5250Ho-Xylene 1.0 0.12 ug/L 02/23/23 05:18 135Naphthalene Dibromofluoromethane (Surr)94 67-129 02/23/23 05:18 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)107 03/08/23 06:46 567-129 4-Bromofluorobenzene (Surr)110 02/23/23 05:18 153-136 4-Bromofluorobenzene (Surr)106 03/08/23 06:46 553-136 Toluene-d8 (Surr)106 02/23/23 05:18 159-134 Toluene-d8 (Surr)110 03/08/23 06:46 559-134 Lab Sample ID: 752-3131-8Client Sample ID: MW-12 Matrix: WaterDate Collected: 02/15/23 14:05 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 3.0 1.0 0.57 ug/L 02/23/23 05:49 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 05:49 12.4Toluene 1.0 0.46 ug/L 02/23/23 05:49 143Ethylbenzene 1.0 0.36 ug/L 02/23/23 05:49 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 05:49 1110m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 05:49 1<0.26Methyl tert-butyl ether Eurofins Raleigh Page 11 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-8Client Sample ID: MW-12 Matrix: WaterDate Collected: 02/15/23 14:05 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) RL MDL 240 3.0 1.6 ug/L 02/23/23 05:49 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Xylenes, Total 1.0 0.44 ug/L 02/23/23 05:49 1130o-Xylene 1.0 0.12 ug/L 02/23/23 05:49 121Naphthalene Dibromofluoromethane (Surr)96 67-129 02/23/23 05:49 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)126 02/23/23 05:49 153-136 Toluene-d8 (Surr)120 02/23/23 05:49 159-134 Lab Sample ID: 752-3131-9Client Sample ID: MW-13 Matrix: WaterDate Collected: 02/15/23 15:05 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 3.0 1.0 0.57 ug/L 02/23/23 06:21 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 02/23/23 06:21 120Toluene 1.0 0.46 ug/L 02/23/23 06:21 144Ethylbenzene 1.0 0.36 ug/L 02/23/23 06:21 1<0.36Isopropyl ether 2.0 1.2 ug/L 02/23/23 06:21 1130m-Xylene & p-Xylene 1.0 0.26 ug/L 02/23/23 06:21 13.1Methyl tert-butyl ether 3.0 1.6 ug/L 02/23/23 06:21 1220Xylenes, Total 1.0 0.44 ug/L 02/23/23 06:21 186o-Xylene 1.0 0.12 ug/L 02/23/23 06:21 120Naphthalene Dibromofluoromethane (Surr)89 67-129 02/23/23 06:21 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery 4-Bromofluorobenzene (Surr)113 02/23/23 06:21 153-136 Toluene-d8 (Surr)111 02/23/23 06:21 159-134 Lab Sample ID: 752-3131-10Client Sample ID: MW-14 Matrix: WaterDate Collected: 02/15/23 14:25 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 1.3 1.0 0.57 ug/L 03/01/23 23:19 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/01/23 23:19 1<0.57Toluene 1.0 0.46 ug/L 03/01/23 23:19 12.8Ethylbenzene 1.0 0.36 ug/L 03/01/23 23:19 1<0.36Isopropyl ether 2.0 1.2 ug/L 03/01/23 23:19 13.1m-Xylene & p-Xylene 1.0 0.26 ug/L 03/01/23 23:19 1<0.26Methyl tert-butyl ether 3.0 1.6 ug/L 03/01/23 23:19 111Xylenes, Total 1.0 0.44 ug/L 03/01/23 23:19 17.4o-Xylene 1.0 0.12 ug/L 03/01/23 23:19 13.8Naphthalene Dibromofluoromethane (Surr)116 67-129 03/01/23 23:19 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)122 03/08/23 03:41 167-129 4-Bromofluorobenzene (Surr)122 03/01/23 23:19 153-136 4-Bromofluorobenzene (Surr)107 03/08/23 03:41 153-136 Eurofins Raleigh Page 12 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-10Client Sample ID: MW-14 Matrix: WaterDate Collected: 02/15/23 14:25 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Toluene-d8 (Surr)119 59-134 03/01/23 23:19 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Toluene-d8 (Surr)119 03/08/23 03:41 159-134 Lab Sample ID: 752-3131-11Client Sample ID: MW-15 Matrix: WaterDate Collected: 02/15/23 14:30 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 6.2 1.0 0.57 ug/L 03/01/23 23:51 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/01/23 23:51 13.1Toluene 1.0 0.46 ug/L 03/01/23 23:51 19.2Ethylbenzene 1.0 0.36 ug/L 03/01/23 23:51 1<0.36Isopropyl ether 2.0 1.2 ug/L 03/01/23 23:51 127m-Xylene & p-Xylene 1.0 0.26 ug/L 03/01/23 23:51 130Methyl tert-butyl ether 3.0 1.6 ug/L 03/01/23 23:51 187Xylenes, Total 1.0 0.44 ug/L 03/01/23 23:51 160o-Xylene 1.0 0.12 ug/L 03/01/23 23:51 19.7Naphthalene Dibromofluoromethane (Surr)121 67-129 03/01/23 23:51 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)122 03/08/23 04:12 167-129 4-Bromofluorobenzene (Surr)135 03/01/23 23:51 153-136 4-Bromofluorobenzene (Surr)113 03/08/23 04:12 153-136 Toluene-d8 (Surr)118 03/01/23 23:51 159-134 Toluene-d8 (Surr)114 03/08/23 04:12 159-134 Lab Sample ID: 752-3131-12Client Sample ID: MW-16 Matrix: WaterDate Collected: 02/15/23 13:45 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 H 1.0 0.57 ug/L 03/02/23 00:22 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/02/23 00:22 12.5 HToluene 1.0 0.46 ug/L 03/02/23 00:22 17.0 HEthylbenzene 1.0 0.36 ug/L 03/02/23 00:22 1<0.36 HIsopropyl ether 2.0 1.2 ug/L 03/02/23 00:22 115Hm-Xylene & p-Xylene 1.0 0.26 ug/L 03/02/23 00:22 10.44 J HMethyl tert-butyl ether 3.0 1.6 ug/L 03/02/23 00:22 142HXylenes, Total 1.0 0.44 ug/L 03/02/23 00:22 127Ho-Xylene 1.0 0.12 ug/L 03/02/23 00:22 16.5 HNaphthalene Dibromofluoromethane (Surr)108 67-129 03/02/23 00:22 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)100 *3 03/08/23 04:43 167-129 4-Bromofluorobenzene (Surr)126 03/02/23 00:22 153-136 4-Bromofluorobenzene (Surr)100 03/08/23 04:43 153-136 Toluene-d8 (Surr)120 03/02/23 00:22 159-134 Toluene-d8 (Surr)108 03/08/23 04:43 159-134 Eurofins Raleigh Page 13 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-13Client Sample ID: MW-17 Matrix: WaterDate Collected: 02/15/23 15:50 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 5.9 H 1.0 0.57 ug/L 03/02/23 00:54 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/02/23 00:54 121HToluene 1.0 0.46 ug/L 03/02/23 00:54 164HEthylbenzene 1.0 0.36 ug/L 03/02/23 00:54 1<0.36 HIsopropyl ether 10 6.0 ug/L 03/08/23 07:17 5110Hm-Xylene & p-Xylene 1.0 0.26 ug/L 03/02/23 00:54 133HMethyl tert-butyl ether 15 8.0 ug/L 03/08/23 07:17 5250HXylenes, Total 5.0 2.2 ug/L 03/08/23 07:17 5140Ho-Xylene 1.0 0.12 ug/L 03/02/23 00:54 121HNaphthalene Dibromofluoromethane (Surr)99 67-129 03/02/23 00:54 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)100 *3 03/08/23 07:17 567-129 4-Bromofluorobenzene (Surr)125 03/02/23 00:54 153-136 4-Bromofluorobenzene (Surr)108 03/08/23 07:17 553-136 Toluene-d8 (Surr)116 03/02/23 00:54 159-134 Toluene-d8 (Surr)111 *3 03/08/23 07:17 559-134 Lab Sample ID: 752-3131-14Client Sample ID: MW-18 Matrix: WaterDate Collected: 02/15/23 13:45 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 H 1.0 0.57 ug/L 03/02/23 01:26 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/02/23 01:26 1<0.57 HToluene 1.0 0.46 ug/L 03/02/23 01:26 1<0.46 HEthylbenzene 1.0 0.36 ug/L 03/02/23 01:26 1<0.36 HIsopropyl ether 2.0 1.2 ug/L 03/02/23 01:26 1<1.2 Hm-Xylene & p-Xylene 1.0 0.26 ug/L 03/02/23 01:26 1<0.26 HMethyl tert-butyl ether 3.0 1.6 ug/L 03/02/23 01:26 1<1.6 HXylenes, Total 1.0 0.44 ug/L 03/02/23 01:26 1<0.44 Ho-Xylene 1.0 0.12 ug/L 03/02/23 01:26 12.8 HNaphthalene Dibromofluoromethane (Surr)106 67-129 03/02/23 01:26 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)102 *3 03/08/23 05:14 167-129 4-Bromofluorobenzene (Surr)129 03/02/23 01:26 153-136 4-Bromofluorobenzene (Surr)104 03/08/23 05:14 153-136 Toluene-d8 (Surr)126 03/02/23 01:26 159-134 Toluene-d8 (Surr)111 *3 03/08/23 05:14 159-134 Lab Sample ID: 752-3131-15Client Sample ID: MW-19 Matrix: WaterDate Collected: 02/15/23 14:45 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 5.6 H 1.0 0.57 ug/L 03/02/23 01:57 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/02/23 01:57 1<0.57 HToluene 1.0 0.46 ug/L 03/02/23 01:57 17.6 HEthylbenzene Eurofins Raleigh Page 14 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-15Client Sample ID: MW-19 Matrix: WaterDate Collected: 02/15/23 14:45 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) RL MDL <0.36 H 1.0 0.36 ug/L 03/02/23 01:57 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Isopropyl ether 2.0 1.2 ug/L 03/02/23 01:57 120Hm-Xylene & p-Xylene 1.0 0.26 ug/L 03/02/23 01:57 11.1 HMethyl tert-butyl ether 3.0 1.6 ug/L 03/02/23 01:57 157HXylenes, Total 1.0 0.44 ug/L 03/02/23 01:57 137Ho-Xylene 1.0 0.12 ug/L 03/02/23 01:57 17.2 HNaphthalene Dibromofluoromethane (Surr)96 67-129 03/02/23 01:57 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)101 *3 03/08/23 05:45 167-129 4-Bromofluorobenzene (Surr)120 03/02/23 01:57 153-136 4-Bromofluorobenzene (Surr)107 03/08/23 05:45 153-136 Toluene-d8 (Surr)110 03/02/23 01:57 159-134 Toluene-d8 (Surr)110 03/08/23 05:45 159-134 Lab Sample ID: 752-3131-16Client Sample ID: MW-20 Matrix: WaterDate Collected: 02/15/23 16:15 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL 5.1 H 1.0 0.57 ug/L 03/02/23 02:29 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/02/23 02:29 128HToluene 1.0 0.46 ug/L 03/02/23 02:29 1130HEthylbenzene 1.0 0.36 ug/L 03/02/23 02:29 1<0.36 HIsopropyl ether 10 6.0 ug/L 03/08/23 07:48 5150Hm-Xylene & p-Xylene 1.0 0.26 ug/L 03/02/23 02:29 11.2 HMethyl tert-butyl ether 15 8.0 ug/L 03/08/23 07:48 5310HXylenes, Total 5.0 2.2 ug/L 03/08/23 07:48 5160Ho-Xylene 1.0 0.12 ug/L 03/02/23 02:29 124HNaphthalene Dibromofluoromethane (Surr)90 67-129 03/02/23 02:29 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)100 *3 03/08/23 07:48 567-129 4-Bromofluorobenzene (Surr)116 03/02/23 02:29 153-136 4-Bromofluorobenzene (Surr)100 03/08/23 07:48 553-136 Toluene-d8 (Surr)106 03/02/23 02:29 159-134 Toluene-d8 (Surr)109 *3 03/08/23 07:48 559-134 Lab Sample ID: 752-3131-17Client Sample ID: MW-21 Matrix: WaterDate Collected: 02/15/23 13:15 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) RL MDL <0.57 H 1.0 0.57 ug/L 03/02/23 03:01 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Benzene 1.0 0.57 ug/L 03/02/23 03:01 1<0.57 HToluene 1.0 0.46 ug/L 03/02/23 03:01 1<0.46 HEthylbenzene 1.0 0.36 ug/L 03/02/23 03:01 1<0.36 HIsopropyl ether 2.0 1.2 ug/L 03/02/23 03:01 1<1.2 Hm-Xylene & p-Xylene 1.0 0.26 ug/L 03/02/23 03:01 1<0.26 HMethyl tert-butyl ether Eurofins Raleigh Page 15 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Client Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID: 752-3131-17Client Sample ID: MW-21 Matrix: WaterDate Collected: 02/15/23 13:15 Date Received: 02/15/23 17:20 Method: EPA 624.1 - Volatile Organic Compounds (GC/MS) (Continued) RL MDL <1.6 H 3.0 1.6 ug/L 03/02/23 03:01 1 Analyte Dil FacAnalyzedPreparedUnitDResultQualifier Xylenes, Total 1.0 0.44 ug/L 03/02/23 03:01 1<0.44 Ho-Xylene 1.0 0.12 ug/L 03/02/23 03:01 12.8 HNaphthalene Dibromofluoromethane (Surr)94 67-129 03/02/23 03:01 1 Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery Dibromofluoromethane (Surr)103 *3 03/08/23 06:15 167-129 4-Bromofluorobenzene (Surr)112 03/02/23 03:01 153-136 4-Bromofluorobenzene (Surr)105 03/08/23 06:15 153-136 Toluene-d8 (Surr)107 03/02/23 03:01 159-134 Toluene-d8 (Surr)109 03/08/23 06:15 159-134 Eurofins Raleigh Page 16 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Surrogate Summary Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Method: 624.1 - Volatile Organic Compounds (GC/MS) Prep Type: Total/NAMatrix: Water Lab Sample ID Client Sample ID (67-129)(53-136)(59-134) DBFM BFB TOL 124 101 119752-3131-1 Percent Surrogate Recovery (Acceptance Limits) MW-5 127 102 123752-3131-2 MW-6 129 103 119752-3131-3 MW-7 120 108 116752-3131-4 MW-8 112 115 117752-3131-5 MW-9 94 108 73752-3131-6 MW-10 94 110 106752-3131-7 MW-11 107 106 110752-3131-7 MW-11 96 126 120752-3131-8 MW-12 89 113 111752-3131-9 MW-13 116 122 119752-3131-10 MW-14 122 107 119752-3131-10 MW-14 121 135 118752-3131-11 MW-15 122 113 114752-3131-11 MW-15 108 126 120752-3131-12 MW-16 100 *3 100 108752-3131-12 MW-16 99 125 116752-3131-13 MW-17 100 *3 108 111 *3752-3131-13 MW-17 106 129 126752-3131-14 MW-18 102 *3 104 111 *3752-3131-14 MW-18 96 120 110752-3131-15 MW-19 101 *3 107 110752-3131-15 MW-19 90 116 106752-3131-16 MW-20 100 *3 100 109 *3752-3131-16 MW-20 94 112 107752-3131-17 MW-21 103 *3 105 109752-3131-17 MW-21 118 120 129LCS 752-1361/7 Lab Control Sample 112 104 109LCS 752-1540/4 Lab Control Sample 127 111 124LCS 752-1689/4 Lab Control Sample 123 128 135 S1+LCSD 752-1361/8 Lab Control Sample Dup 116 116 118LCSD 752-1540/5 Lab Control Sample Dup 125 113 124LCSD 752-1689/5 Lab Control Sample Dup 133 S1+112 125MB 752-1361/10 Method Blank 146 S1+103 107MB 752-1540/7 Method Blank 124 105 121MB 752-1689/7 Method Blank 129 125 131MRL 752-1361/28 Lab Control Sample 139 127 134MRL 752-1540/3 Lab Control Sample 123 109 122MRL 752-1689/3 Lab Control Sample Surrogate Legend DBFM = Dibromofluoromethane (Surr) BFB = 4-Bromofluorobenzene (Surr) TOL = Toluene-d8 (Surr) Eurofins Raleigh Page 17 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Method: 624.1 - Volatile Organic Compounds (GC/MS) Client Sample ID: Method BlankLab Sample ID: MB 752-1361/10 Matrix: Water Prep Type: Total/NA Analysis Batch: 1361 RL MDL Benzene <0.57 1.0 0.57 ug/L 02/22/23 22:35 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.57 0.571.0 ug/L 02/22/23 22:35 1Toluene <0.46 0.461.0 ug/L 02/22/23 22:35 1Ethylbenzene <0.36 0.361.0 ug/L 02/22/23 22:35 1Isopropyl ether <1.2 1.22.0 ug/L 02/22/23 22:35 1m-Xylene & p-Xylene <0.26 0.261.0 ug/L 02/22/23 22:35 1Methyl tert-butyl ether <1.6 1.63.0 ug/L 02/22/23 22:35 1Xylenes, Total <0.44 0.441.0 ug/L 02/22/23 22:35 1o-Xylene <0.12 0.121.0 ug/L 02/22/23 22:35 1Naphthalene Dibromofluoromethane (Surr)133 S1+67-129 02/22/23 22:35 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 112 02/22/23 22:35 14-Bromofluorobenzene (Surr)53-136 125 02/22/23 22:35 1Toluene-d8 (Surr)59-134 Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-1361/7 Matrix: Water Prep Type: Total/NA Analysis Batch: 1361 Benzene 20.0 17.3 ug/L 86 65-135 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 20.0 19.2 ug/L 96 70-130 Ethylbenzene 20.0 16.5 ug/L 83 60-140 Isopropyl ether 20.0 17.4 ug/L 87 37-134 m-Xylene & p-Xylene 40.0 35.1 ug/L 88 79-121 Methyl tert-butyl ether 20.0 17.6 ug/L 88 57-133 Xylenes, Total 60.0 49.8 ug/L 83 73-120 o-Xylene 20.0 14.7 ug/L 73 65-120 Naphthalene 20.0 18.0 ug/L 90 56-133 Dibromofluoromethane (Surr)67 -129 Surrogate 118 LCS LCS Qualifier Limits%Recovery 1204-Bromofluorobenzene (Surr)53 -136 129Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-1361/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 1361 Benzene 20.0 18.2 ug/L 91 65-135 5 61 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Toluene 20.0 20.7 ug/L 104 70-130 8 41 Ethylbenzene 20.0 18.1 ug/L 91 60-140 9 63 Isopropyl ether 20.0 19.0 ug/L 95 37-134 9 20 m-Xylene & p-Xylene 40.0 38.4 ug/L 96 79-121 9 16 Methyl tert-butyl ether 20.0 19.3 ug/L 96 57-133 9 21 Xylenes, Total 60.0 54.9 ug/L 92 73-120 10 16 o-Xylene 20.0 16.5 ug/L 82 65-120 11 15 Eurofins Raleigh Page 18 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-1361/8 Matrix: Water Prep Type: Total/NA Analysis Batch: 1361 Naphthalene 20.0 19.7 ug/L 99 56-133 9 19 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Dibromofluoromethane (Surr)67 -129 Surrogate 123 LCSD LCSD Qualifier Limits%Recovery 1284-Bromofluorobenzene (Surr)53 -136 135 S1+Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-1361/28 Matrix: Water Prep Type: Total/NA Analysis Batch: 1361 Benzene 1.00 1.19 ug/L 119 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 1.00 1.56 ug/L 156 Ethylbenzene 1.00 1.18 ug/L 118 Isopropyl ether 1.00 0.898 J ug/L 90 m-Xylene & p-Xylene 2.00 2.20 ug/L 110 Methyl tert-butyl ether 1.00 0.992 J ug/L 99 Xylenes, Total 3.00 3.10 ug/L 103 o-Xylene 1.00 0.901 J ug/L 90 Naphthalene 1.00 2.77 ug/L 277 Dibromofluoromethane (Surr)67 -129 Surrogate 129 MRL MRL Qualifier Limits%Recovery 1254-Bromofluorobenzene (Surr)53 -136 131Toluene-d8 (Surr)59 -134 Client Sample ID: Method BlankLab Sample ID: MB 752-1540/7 Matrix: Water Prep Type: Total/NA Analysis Batch: 1540 RL MDL Benzene <0.57 1.0 0.57 ug/L 03/01/23 18:35 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.57 0.571.0 ug/L 03/01/23 18:35 1Toluene <0.46 0.461.0 ug/L 03/01/23 18:35 1Ethylbenzene <0.36 0.361.0 ug/L 03/01/23 18:35 1Isopropyl ether <1.2 1.22.0 ug/L 03/01/23 18:35 1m-Xylene & p-Xylene <0.26 0.261.0 ug/L 03/01/23 18:35 1Methyl tert-butyl ether <1.6 1.63.0 ug/L 03/01/23 18:35 1Xylenes, Total <0.44 0.441.0 ug/L 03/01/23 18:35 1o-Xylene <0.12 0.121.0 ug/L 03/01/23 18:35 1Naphthalene Dibromofluoromethane (Surr)146 S1+67-129 03/01/23 18:35 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 103 03/01/23 18:35 14-Bromofluorobenzene (Surr)53-136 107 03/01/23 18:35 1Toluene-d8 (Surr)59-134 Eurofins Raleigh Page 19 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-1540/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 1540 Benzene 20.0 18.8 ug/L 94 65-135 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 20.0 21.4 ug/L 107 70-130 Ethylbenzene 20.0 19.3 ug/L 97 60-140 Isopropyl ether 20.0 22.4 ug/L 112 37-134 m-Xylene & p-Xylene 40.0 40.8 ug/L 102 79-121 Methyl tert-butyl ether 20.0 21.3 ug/L 107 57-133 Xylenes, Total 60.0 61.2 ug/L 102 73-120 o-Xylene 20.0 20.4 ug/L 102 65-120 Naphthalene 20.0 16.4 ug/L 82 56-133 Dibromofluoromethane (Surr)67 -129 Surrogate 112 LCS LCS Qualifier Limits%Recovery 1044-Bromofluorobenzene (Surr)53 -136 109Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-1540/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 1540 Benzene 20.0 19.6 ug/L 98 65-135 4 61 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Toluene 20.0 23.0 ug/L 115 70-130 7 41 Ethylbenzene 20.0 20.8 ug/L 104 60-140 8 63 Isopropyl ether 20.0 23.3 ug/L 117 37-134 4 20 m-Xylene & p-Xylene 40.0 43.9 ug/L 110 79-121 7 16 Methyl tert-butyl ether 20.0 22.4 ug/L 112 57-133 5 21 Xylenes, Total 60.0 66.1 ug/L 110 73-120 8 16 o-Xylene 20.0 22.2 ug/L 111 65-120 8 15 Naphthalene 20.0 18.5 ug/L 92 56-133 12 19 Dibromofluoromethane (Surr)67 -129 Surrogate 116 LCSD LCSD Qualifier Limits%Recovery 1164-Bromofluorobenzene (Surr)53 -136 118Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-1540/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 1540 Benzene 1.00 1.22 ug/L 122 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 1.00 1.49 ug/L 149 Ethylbenzene 1.00 1.07 ug/L 107 Isopropyl ether 1.00 0.908 J ug/L 91 m-Xylene & p-Xylene 2.00 2.14 ug/L 107 Methyl tert-butyl ether 1.00 0.955 J ug/L 96 Xylenes, Total 3.00 3.16 ug/L 105 o-Xylene 1.00 1.02 ug/L 102 Eurofins Raleigh Page 20 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-1540/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 1540 Naphthalene 1.00 4.10 ug/L 410 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Dibromofluoromethane (Surr)67 -129 Surrogate 139 MRL MRL Qualifier Limits%Recovery 1274-Bromofluorobenzene (Surr)53 -136 134Toluene-d8 (Surr)59 -134 Client Sample ID: Method BlankLab Sample ID: MB 752-1689/7 Matrix: Water Prep Type: Total/NA Analysis Batch: 1689 RL MDL Benzene <0.57 1.0 0.57 ug/L 03/07/23 22:02 1 MB MB Analyte Dil FacAnalyzedPreparedDUnitResultQualifier <0.57 0.571.0 ug/L 03/07/23 22:02 1Toluene <0.46 0.461.0 ug/L 03/07/23 22:02 1Ethylbenzene <0.36 0.361.0 ug/L 03/07/23 22:02 1Isopropyl ether <1.2 1.22.0 ug/L 03/07/23 22:02 1m-Xylene & p-Xylene <0.26 0.261.0 ug/L 03/07/23 22:02 1Methyl tert-butyl ether <1.6 1.63.0 ug/L 03/07/23 22:02 1Xylenes, Total <0.44 0.441.0 ug/L 03/07/23 22:02 1o-Xylene <0.12 0.121.0 ug/L 03/07/23 22:02 1Naphthalene Dibromofluoromethane (Surr)124 67-129 03/07/23 22:02 1 MB MB Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery 105 03/07/23 22:02 14-Bromofluorobenzene (Surr)53-136 121 03/07/23 22:02 1Toluene-d8 (Surr)59-134 Client Sample ID: Lab Control SampleLab Sample ID: LCS 752-1689/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 1689 Benzene 20.0 18.0 ug/L 90 65-135 Analyte LCS LCS DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 20.0 18.1 ug/L 90 70-130 Ethylbenzene 20.0 17.9 ug/L 89 60-140 Isopropyl ether 20.0 19.1 ug/L 96 37-134 m-Xylene & p-Xylene 40.0 36.1 ug/L 90 79-121 Methyl tert-butyl ether 20.0 18.7 ug/L 94 57-133 Xylenes, Total 60.0 54.1 ug/L 90 73-120 o-Xylene 20.0 18.0 ug/L 90 65-120 Naphthalene 20.0 19.0 ug/L 95 56-133 Dibromofluoromethane (Surr)67 -129 Surrogate 127 LCS LCS Qualifier Limits%Recovery 1114-Bromofluorobenzene (Surr)53 -136 124Toluene-d8 (Surr)59 -134 Eurofins Raleigh Page 21 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Sample Results Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Method: 624.1 - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 752-1689/5 Matrix: Water Prep Type: Total/NA Analysis Batch: 1689 Benzene 20.0 19.1 ug/L 96 65-135 6 61 Analyte LCSD LCSD DUnitResultQualifier %Rec Spike Added %Rec Limits LimitRPD RPD Toluene 20.0 18.8 ug/L 94 70-130 4 41 Ethylbenzene 20.0 19.0 ug/L 95 60-140 6 63 Isopropyl ether 20.0 19.8 ug/L 99 37-134 4 20 m-Xylene & p-Xylene 40.0 38.0 ug/L 95 79-121 5 16 Methyl tert-butyl ether 20.0 19.6 ug/L 98 57-133 5 21 Xylenes, Total 60.0 56.8 ug/L 95 73-120 5 16 o-Xylene 20.0 18.8 ug/L 94 65-120 5 15 Naphthalene 20.0 20.3 ug/L 101 56-133 6 19 Dibromofluoromethane (Surr)67 -129 Surrogate 125 LCSD LCSD Qualifier Limits%Recovery 1134-Bromofluorobenzene (Surr)53 -136 124Toluene-d8 (Surr)59 -134 Client Sample ID: Lab Control SampleLab Sample ID: MRL 752-1689/3 Matrix: Water Prep Type: Total/NA Analysis Batch: 1689 Benzene 1.00 1.03 ug/L 103 Analyte MRL MRL DUnitResultQualifier %Rec Spike Added %Rec Limits Toluene 1.00 1.19 ug/L 119 Ethylbenzene 1.00 1.08 ug/L 108 Isopropyl ether 1.00 0.953 J ug/L 95 m-Xylene & p-Xylene 2.00 2.18 ug/L 109 Methyl tert-butyl ether 1.00 1.03 ug/L 103 Xylenes, Total 3.00 3.11 ug/L 104 o-Xylene 1.00 0.934 J ug/L 93 Naphthalene 1.00 1.67 ug/L 167 Dibromofluoromethane (Surr)67 -129 Surrogate 123 MRL MRL Qualifier Limits%Recovery 1094-Bromofluorobenzene (Surr)53 -136 122Toluene-d8 (Surr)59 -134 Eurofins Raleigh Page 22 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 QC Association Summary Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. GC/MS VOA Analysis Batch: 1361 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 624.1752-3131-1 MW-5 Total/NA Water 624.1752-3131-2 MW-6 Total/NA Water 624.1752-3131-3 MW-7 Total/NA Water 624.1752-3131-4 MW-8 Total/NA Water 624.1752-3131-5 MW-9 Total/NA Water 624.1752-3131-6 MW-10 Total/NA Water 624.1752-3131-7 MW-11 Total/NA Water 624.1752-3131-8 MW-12 Total/NA Water 624.1752-3131-9 MW-13 Total/NA Water 624.1MB 752-1361/10 Method Blank Total/NA Water 624.1LCS 752-1361/7 Lab Control Sample Total/NA Water 624.1LCSD 752-1361/8 Lab Control Sample Dup Total/NA Water 624.1MRL 752-1361/28 Lab Control Sample Total/NA Analysis Batch: 1540 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 624.1752-3131-10 MW-14 Total/NA Water 624.1752-3131-11 MW-15 Total/NA Water 624.1752-3131-12 MW-16 Total/NA Water 624.1752-3131-13 MW-17 Total/NA Water 624.1752-3131-14 MW-18 Total/NA Water 624.1752-3131-15 MW-19 Total/NA Water 624.1752-3131-16 MW-20 Total/NA Water 624.1752-3131-17 MW-21 Total/NA Water 624.1MB 752-1540/7 Method Blank Total/NA Water 624.1LCS 752-1540/4 Lab Control Sample Total/NA Water 624.1LCSD 752-1540/5 Lab Control Sample Dup Total/NA Water 624.1MRL 752-1540/3 Lab Control Sample Total/NA Analysis Batch: 1689 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch Water 624.1752-3131-7 MW-11 Total/NA Water 624.1752-3131-10 MW-14 Total/NA Water 624.1752-3131-11 MW-15 Total/NA Water 624.1752-3131-12 MW-16 Total/NA Water 624.1752-3131-13 MW-17 Total/NA Water 624.1752-3131-14 MW-18 Total/NA Water 624.1752-3131-15 MW-19 Total/NA Water 624.1752-3131-16 MW-20 Total/NA Water 624.1752-3131-17 MW-21 Total/NA Water 624.1MB 752-1689/7 Method Blank Total/NA Water 624.1LCS 752-1689/4 Lab Control Sample Total/NA Water 624.1LCSD 752-1689/5 Lab Control Sample Dup Total/NA Water 624.1MRL 752-1689/3 Lab Control Sample Total/NA Eurofins Raleigh Page 23 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Cape Lookout Environmental Services Job ID: 752-3131-1 Project/Site: Seminole Mart #2/ Cape Lookout Env. Client Sample ID: MW-5 Lab Sample ID: 752-3131-1 Matrix: WaterDate Collected: 02/15/23 12:55 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 02:12 Client Sample ID: MW-6 Lab Sample ID: 752-3131-2 Matrix: WaterDate Collected: 02/15/23 13:30 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 02:43 Client Sample ID: MW-7 Lab Sample ID: 752-3131-3 Matrix: WaterDate Collected: 02/15/23 13:15 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 03:14 Client Sample ID: MW-8 Lab Sample ID: 752-3131-4 Matrix: WaterDate Collected: 02/15/23 15:00 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 03:45 Client Sample ID: MW-9 Lab Sample ID: 752-3131-5 Matrix: WaterDate Collected: 02/15/23 14:45 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 04:16 Client Sample ID: MW-10 Lab Sample ID: 752-3131-6 Matrix: WaterDate Collected: 02/15/23 14:15 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 04:47 Client Sample ID: MW-11 Lab Sample ID: 752-3131-7 Matrix: WaterDate Collected: 02/15/23 16:00 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 05:18 Analysis 624.1 5 1689 RY EET ESCTotal/NA 03/08/23 06:46 Eurofins Raleigh Page 24 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Cape Lookout Environmental Services Job ID: 752-3131-1 Project/Site: Seminole Mart #2/ Cape Lookout Env. Client Sample ID: MW-12 Lab Sample ID: 752-3131-8 Matrix: WaterDate Collected: 02/15/23 14:05 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 05:49 Client Sample ID: MW-13 Lab Sample ID: 752-3131-9 Matrix: WaterDate Collected: 02/15/23 15:05 Date Received: 02/15/23 17:20 Analysis 624.1 RY11361 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 02/23/23 06:21 Client Sample ID: MW-14 Lab Sample ID: 752-3131-10 Matrix: WaterDate Collected: 02/15/23 14:25 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/01/23 23:19 Analysis 624.1 1 1689 RY EET ESCTotal/NA 03/08/23 03:41 Client Sample ID: MW-15 Lab Sample ID: 752-3131-11 Matrix: WaterDate Collected: 02/15/23 14:30 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/01/23 23:51 Analysis 624.1 1 1689 RY EET ESCTotal/NA 03/08/23 04:12 Client Sample ID: MW-16 Lab Sample ID: 752-3131-12 Matrix: WaterDate Collected: 02/15/23 13:45 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/02/23 00:22 Analysis 624.1 1 1689 RY EET ESCTotal/NA 03/08/23 04:43 Client Sample ID: MW-17 Lab Sample ID: 752-3131-13 Matrix: WaterDate Collected: 02/15/23 15:50 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/02/23 00:54 Analysis 624.1 5 1689 RY EET ESCTotal/NA 03/08/23 07:17 Eurofins Raleigh Page 25 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Lab Chronicle Client: Cape Lookout Environmental Services Job ID: 752-3131-1 Project/Site: Seminole Mart #2/ Cape Lookout Env. Client Sample ID: MW-18 Lab Sample ID: 752-3131-14 Matrix: WaterDate Collected: 02/15/23 13:45 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/02/23 01:26 Analysis 624.1 1 1689 RY EET ESCTotal/NA 03/08/23 05:14 Client Sample ID: MW-19 Lab Sample ID: 752-3131-15 Matrix: WaterDate Collected: 02/15/23 14:45 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/02/23 01:57 Analysis 624.1 1 1689 RY EET ESCTotal/NA 03/08/23 05:45 Client Sample ID: MW-20 Lab Sample ID: 752-3131-16 Matrix: WaterDate Collected: 02/15/23 16:15 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/02/23 02:29 Analysis 624.1 5 1689 RY EET ESCTotal/NA 03/08/23 07:48 Client Sample ID: MW-21 Lab Sample ID: 752-3131-17 Matrix: WaterDate Collected: 02/15/23 13:15 Date Received: 02/15/23 17:20 Analysis 624.1 RY11540 EET ESC Type Batch Batch MethodPrep Type LabAnalystRun Prepared or Analyzed Batch Number Dilution Factor Total/NA 03/02/23 03:01 Analysis 624.1 1 1689 RY EET ESCTotal/NA 03/08/23 06:15 Laboratory References: EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL (919)677-1669 Eurofins Raleigh Page 26 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Accreditation/Certification Summary Client: Cape Lookout Environmental Services Job ID: 752-3131-1 Project/Site: Seminole Mart #2/ Cape Lookout Env. Laboratory: Eurofins Raleigh The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW)State 591 12-31-23 Eurofins Raleigh Page 27 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Method Summary Job ID: 752-3131-1Client: Cape Lookout Environmental Services Project/Site: Seminole Mart #2/ Cape Lookout Env. Method Method Description LaboratoryProtocol EPA624.1 Volatile Organic Compounds (GC/MS)EET ESC Protocol References: EPA = US Environmental Protection Agency Laboratory References: EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL (919)677-1669 Eurofins Raleigh Page 28 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Sample Summary Client: Cape Lookout Environmental Services Job ID: 752-3131-1 Project/Site: Seminole Mart #2/ Cape Lookout Env. Lab Sample ID Client Sample ID Matrix Collected Received 752-3131-1 MW-5 Water 02/15/23 12:55 02/15/23 17:20 752-3131-2 MW-6 Water 02/15/23 13:30 02/15/23 17:20 752-3131-3 MW-7 Water 02/15/23 13:15 02/15/23 17:20 752-3131-4 MW-8 Water 02/15/23 15:00 02/15/23 17:20 752-3131-5 MW-9 Water 02/15/23 14:45 02/15/23 17:20 752-3131-6 MW-10 Water 02/15/23 14:15 02/15/23 17:20 752-3131-7 MW-11 Water 02/15/23 16:00 02/15/23 17:20 752-3131-8 MW-12 Water 02/15/23 14:05 02/15/23 17:20 752-3131-9 MW-13 Water 02/15/23 15:05 02/15/23 17:20 752-3131-10 MW-14 Water 02/15/23 14:25 02/15/23 17:20 752-3131-11 MW-15 Water 02/15/23 14:30 02/15/23 17:20 752-3131-12 MW-16 Water 02/15/23 13:45 02/15/23 17:20 752-3131-13 MW-17 Water 02/15/23 15:50 02/15/23 17:20 752-3131-14 MW-18 Water 02/15/23 13:45 02/15/23 17:20 752-3131-15 MW-19 Water 02/15/23 14:45 02/15/23 17:20 752-3131-16 MW-20 Water 02/15/23 16:15 02/15/23 17:20 752-3131-17 MW-21 Water 02/15/23 13:15 02/15/23 17:20 Eurofins RaleighPage 29 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 30 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Page 31 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Login Sample Receipt Checklist Client: Cape Lookout Environmental Services Job Number: 752-3131-1 Login Number: 3131 Question Answer Comment Creator: Hyatt, Samantha List Source: Eurofins Raleigh List Number: 1 TrueRadioactivity wasn't checked or is </= background as measured by a survey meter. TrueThe cooler's custody seal, if present, is intact. TrueSample custody seals, if present, are intact. TrueThe cooler or samples do not appear to have been compromised or tampered with. TrueSamples were received on ice. TrueCooler Temperature is acceptable. TrueCooler Temperature is recorded. TrueCOC is present. TrueCOC is filled out in ink and legible. TrueCOC is filled out with all pertinent information. TrueIs the Field Sampler's name present on COC? TrueThere are no discrepancies between the containers received and the COC. TrueSamples are received within Holding Time (excluding tests with immediate HTs) TrueSample containers have legible labels. TrueContainers are not broken or leaking. TrueSample collection date/times are provided. TrueAppropriate sample containers are used. TrueSample bottles are completely filled. TrueSample Preservation Verified. TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4"). TrueMultiphasic samples are not present. TrueSamples do not require splitting or compositing. TrueResidual Chlorine Checked. Eurofins Raleigh Page 32 of 32 3/8/2023 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15