FA-3431_29478_CA_SCP_20230328_Vertical Soil Profile Assessment

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
March 28, 2023

Mr. Ken Currie
NCDEQ-UST Section
Fayetteville Regional Office
Systel Building
225 Green Street, Suite 714
Fayetteville, NC 28301-5043

Re: Soil Assessment Report
March 2023
Former OM Mart
113 West Main Street
Biscoe, Montgomery County
North Carolina
Facility ID Number: 0-00-0000021206
Incident Number: 29478
GRI Project Number: 5685

Dear Mr. Currie,

Please find attached the referenced revised, report for the abovementioned site.
If you have any questions, please contact William Regenthal at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Mr. Jimmy McDonald; Quality Oil & Gas Company, file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127

Prepared for:

Mr. Jimmy McDonald
Quality Oil & Gas Company
203 West Broad Avenue
Rockingham, North Carolina 28379

March 28, 2023

William Regenthal, P.G.
Project Manager
Colton Coolbaugh
Report Writer

Soil Assessment Report
March 2023
Former OM Mart
113 West Main Street
Biscoe, Montgomery County
North Carolina
Facility ID Number: 0-00-0000021206
Incident Number: 29478
GRI Project Number: 5685

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
i
SITE INFORMATION
1. Site Identification
 Former OM Mart (Facility ID 0-00-0000021206)
 Incident Number 29478 – Intermediate Risk (I180A)
 Location of Source Area: 113 West Main Street
Biscoe, NC 27209
Montgomery County
35.359634°N, 79.781609°W (Topographical Map)
2. Information about Contacts Associated with the Leaking UST System

UST Owner
Quality Oil & Gas
203 W Broad Avenue
Rockingham, NC 28379
[e-mail]
910-997-3101

UST Operator
Quality Oil & Gas
203 W Broad Avenue
Rockingham, NC 28379
[e-mail]
910-997-3101

Property Owner
VISHALP, LLC
306 N Main Street
Biscoe, NC 27209
Email Unknown
919-271-7568

Property Occupant
Former OM Mart
113 W Main Street
Biscoe, NC 27209
Email Unknown
919-271-7568

Consultant/Contractor
Geological Resources, Inc.
3502 Hayes Road
Monroe, NC 28110
[e-mail]
704-845-4010

Analytical Laboratory
Waypoint Analytical
449 Springbrook Road
Charlotte, NC 28217
State Certification No. 37735/402
704-529-6364
3. Information about Release
 Release was discovered on September 26, 2007
 An unknown amount of product was released from the leaking UST System
 One 6,000-gallon gasoline, two 4,000-gallon gasoline, one 2,000-gallon gasoline USTs, one
kerosene AST and associated pumps and product piping are active at the site

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
ii
EXECUTIVE SUMMARY
Former OM Mart is located at 113 West Main Street in Biscoe, Montgomery County, North Carolina. The
site is currently owned by VISHALP, LLC and is operated by Quality Oil & Gas as a petroleum retail facility,
tire service and convenience store. A site check was conducted in November 2011 following a failed line
test that confirmed the presence of a release. Currently, one 6,000-gallon gasoline, two 4,000-gallon
gasoline, one 2,000-gallon gasoline USTs, one kerosene AST, associated dispensers and product piping are
active at the site.

The site contains one building and is primarily capped with concrete and asphalt. The overall topography
at the site is relatively flat. No surface water bodies were identified within a 500-foot radius of the site.

A Phase I LSA was conducted in January 2008 by a past consultant. There are four unused/irrigation wells
within 1,000 feet of the site. The Town of Biscoe well identified during January 2008 receptor survey
activities is reportedly out of service and has been capped off. Municipal water serves all properties within
1,000 feet of the site. Based on this information and the past presence of ground water contamination
exceeding the GCLs, the site risk ranking is intermediate.

On March 1 and 2, 2023, fourteen soil borings (SB-1 through SB-14) were each installed to depths between
30 to 36 feet BGS in and around the vicinity of the benzene contaminant concentration plume. Each soil
boring was screened using a PID and soil samples were collected from the unsaturated, smear and
saturated zones that displayed the highest PID readings. A total of 41 soil samples were collected and
submitted for analyses of TPH-GRO and TPH-DRO.

The concentration of TPH-DRO reported in SB-12-3’ exceeded the RAL.

The four soil samples with highest concentration of TPH-GRO and TPH-DRO (SB-3-12’, SB-5-12’, SB-6-18’
and SB-12-3’) were submitted for laboratory analyses of VOCs using EPA Method 8260, semi-VOCs using
EPA Method 8270, as well as VPH and EPH using the MADEP Methods.

Concentrations of MTBE, benzo(a)anthracene, benzo(b)fluoranthene and/or benzo(a)pyrene that
exceeded the soil-to-water MCCs were reported in the soil samples collected from SB-6-18’ and SB-12-3’.

Based on this information, the petroleum contaminant plume is localized to the ground water at the site
and soil appears to not be acting as a secondary source of contamination. A feasibility study should be
conducted to determine the effectiveness of either ground water extraction or the use of injections at
this site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
iii
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
HERR: HAZMAT Emergency Response and
Remediation, Inc.
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
PID: Photoionization Detector
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
TABLE OF CONTENTS
SITE INFORMATION ............................................................................................................................ i
EXECUTIVE SUMMARY ....................................................................................................................... ii
ACRONYMS ....................................................................................................................................... iii
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 SOIL QUALITY INFORMATION ..................................................................................................2
3.0 DISCUSSION ............................................................................................................................3
4.0 CONCLUSIONS .........................................................................................................................3
5.0 LIMITATIONS ...........................................................................................................................4
6.0 STATEMENTS AND CERTIFICATION ...........................................................................................4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Benzene Isoconcentration Map
Figure 4: Soil Quality Map
Figure 5: A-A’ Cross section
Figure 6: B-B’ Cross Section

TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Summary of Soil Sample Analytical Results

APPENDICES
Appendix A: State Correspondence
Appendix B: UVF Report
Appendix C: Laboratory Report – Soil Samples
Appendix D: Soil Boring Logs

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the March 2023 Soil Assessment event at the Former OM Mart site; located at
113 West Main Street in Biscoe, Montgomery County, North Carolina (Figure 1). These activities were
conducted in accordance with GRI Proposal No. 23-080, which was submitted to NCDEQ on January 25,
2023, and was approved as Task Authorization No. 29478-19 on February 2, 2023. State correspondence
is included as Appendix A.

The site is currently owned by VISHALP, LLC and is operated by Quality Oil & Gas as a petroleum retail
facility, convenience store and tire service. A Phase II ESA was conducted at the site on September 26,
2007. Soil and groundwater contamination were both detected exceeding applicable regulatory
standards. Currently, one 6,000-gallon gasoline, two 4,000-gallon gasoline, one 2,000-gallon gasoline
USTs and one kerosene AST are active at the site. UST owner/operator information and UST system
information are included as Tables 1 and 2, respectively. The Registered Tank Report is shown below:

The site and surrounding area are a mixture of multi-family residential, single family residential, and
commercial properties. The site contains one building and is primarily capped with concrete and asphalt.
The overall topography at the site is relatively flat. No surface water bodies were identified within a 500-
foot radius of the site. Thirteen Type II monitoring wells (MW-1 through MW-13) were installed at the
site during previous assessment activities. A Site Map showing the locations of the monitoring wells and
the structures on-site has been included as Figure 2.

A Phase I LSA was conducted by the previous consultant in January 2008. There are four unused/irrigation
wells within 1,000-feet of the site. The Town of Biscoe well identified during January 2008 receptor survey
activities is reportedly out of service and has been capped off. Municipal water serves all properties within

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
2
1,000 feet of the site. Based on the results of the receptor survey, as well as the past presence of ground
water contamination above the GCLs, the site risk ranking is intermediate.
2.0 SOIL QUALITY INFORMATION
On March 1 and 2, 2023, fourteen soil borings (SB-1 through SB-14) were installed in and around the
vicinity of the benzene contaminant concentration plume. SB-1 was installed to a depth of 30 feet BGS.
SB-2 through SB-14 were each installed to depths of 36 feet BGS. A Benzene Isoconcentration Map based
on the 2022 ground water sampling results has been included as Figure 3. Soil samples were collected at
three-foot intervals in the estimated unsaturated (0’ to 9’), smear (9’ to 12’) and saturated (12’ to 36’)
zones and screened with a PID. The soil sample exhibiting the highest PID reading from each of the zones
in each boring were submitted for on-site analyses of TPH-GRO and TPH-DRO using UVF technology. A
total of 41 samples were submitted for UVF analyses. A concentration of TPH-DRO that exceeded the RAL
was reported in soil sample SB-12-3’. A copy of the UVF analytical results has been included as Appendix
B. Soil samples SB-3-12’, SB-5-12’, SB-6-18’ and SB-12-3’ were reported to have the highest UVF results
were submitted for laboratory analyses of VOCs using EPA Method 8260, semi-VOCs using EPA Method
8270, as well as VPH and EPH using the MADEP Methods. Concentrations of MTBE, benzo(a)anthracene,
benzo(b)fluoranthene and/or benzo(a)pyrene that exceeded the soil-to-water MCCs were reported in the
soil samples collected from SB-6-18’ and SB-12-3’. A summary of the analytical results for the soil samples
collected in March 2023 is presented in Table 3. A Soil Quality Map based on the March 2023 data is
included as Figure 4. A complete report of laboratory analyses of the soil samples collected in March 2023
has been included as Appendix C. Boring logs are included as Appendix D. A summary of the current soil
analytical data is shown below:
Sample ID Date Collected (mm/dd/yy) Sample Depth (ft-BGS) PID Gasoline-Range TPH Diesel-Range TPH RAL (mg/kg) NE 50 100
SB-1-3’ 03/01/23 3 53.3 21 14.6
SB-1-12’ 03/01/23 12 52.3 <10 <2
SB-1-21’ 03/01/23 21 39.3 <10 <2
SB-2-3’ 03/01/23 3 0.8 <10 23.8
SB-2-12’ 03/01/23 12 0.9 <10 <2
SB-2-30’ 03/01/23 30 18.1 <10 2.2
SB-3-9’ 03/01/23 9 2.7 <10 <2
SB-3-12’ 03/01/23 12 1.3 11 42.8
SB-3-33’ 03/01/23 33 15.0 <20 2.5
SB-4-6’ 03/01/23 6 2.2 <10 2 Sample ID Date Collected (mm/dd/yy) Sample Depth (ft-BGS) PID Gasoline-Range TPH Diesel-Range TPH RAL (mg/kg) NE 50 100
SB-4-12’ 03/01/23 12 1.1 <10 <2
SB-4-36’ 03/01/23 36 27.8 <10 2.2
SB-5-9’ 03/01/23 9 10.8 <10 5.2
SB-5-12’ 03/01/23 12 8.5 24.8 4.8
SB-5-24’ 03/01/23 24 65.0 <20 2.2
SB-6-6’ 03/01/23 6 12.0 10.4 13
SB-6-12’ 03/01/23 12 7.4 <10 12.4
SB-6-18’ 03/01/23 18 264.0 38 13.2
SB-7-9’ 03/01/23 9 3.2 <10 2.2
SB-7-12’ 03/01/23 12 12.6 23.6 <2

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
3 Sample ID Date Collected (mm/dd/yy) Sample Depth (ft-BGS) PID Gasoline-Range TPH Diesel-Range TPH RAL (mg/kg) NE 50 100
SB-7-15’ 03/01/23 15 228.7 13.2 11
SB-8-9’ 03/02/23 9 0.9 <10 <2
SB-8-12’ 03/02/23 12 1.8 10.4 5.8
SB-8-24’ 03/02/23 24 292.1 <10 9.2
SB-9-9’ 03/02/23 9 3.5 <10 4.4
SB-9-12’ 03/02/23 12 3.9 <10 <2
SB-9-33’ 03/02/23 33 28.6 10.4 2
SB-10-9’ 03/02/23 9 2.4 <10 <2
SB-10-12’ 03/02/23 12 1.8 <10 4.2
SB-10-24’ 03/02/23 24 4.7 <10 4.2
SB-11-3’ 03/02/23 3 0.8 <10 4.6 Sample ID Date Collected (mm/dd/yy) Sample Depth (ft-BGS) PID Gasoline-Range TPH Diesel-Range TPH RAL (mg/kg) NE 50 100
SB-11-21’ 03/02/23 21 1.0 16.4 <2
SB-12-3’ 03/02/23 3 0.9 <10 166.4
SB-12-12’ 03/02/23 12 0.4 <10 7.8
SB-12-15’ 03/02/23 15 0.8 <10 8.4
SB-13-6’ 03/02/23 6 0.3 <10 2.6
SB-13-12’ 03/02/23 12 0.4 <10 <2
SB-13-30’ 03/02/23 30 74.8 13.8 7
SB-14-3’ 03/02/23 3 1.9 <10 4.8
SB-14-12’ 03/02/23 12 0.5 <10 <2
SB-14-30’ 03/02/23 30 0.5 <10 <2
3.0 DISCUSSION
Based on these results, the soil appears to not be acting as a secondary source of contamination. The
contamination plume has historically been down gradient from the active UST basin and is isolated within
the ground water. Cross sections A-A’ and B-B’ presented as Figures 5 and 6 respectively, show the
surrounding soil composition is predominantly silt and clay. The historical ground water flow at the site
appears to be toward the west. The location of the contaminant plume is consistent with the historical
ground water flow, to the west of the UST basin.

Soil characterization or excavation within the UST basin is not possible due to the active components.
Further remediation practices at this site should focus on ground water. The next course of action should
be to conduct a feasibility study utilizing either recovery wells within the contaminant plume for ground
water extraction or implementation of direct injections of petroleum reducing compounds into the
groundwater contaminant plume. Recovery wells could be installed within the center of the
contamination plume to maximize extraction potential, or injections focusing on groundwater could be
implemented within the core of the GCL plume.
4.0 CONCLUSIONS
 On March 1 and 2, 2023, 14 soil borings (SB-1 through SB-14) were installed to total depths
between 30 and 36 feet BGS.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Soil Assessment Report
Prepared on: March 28, 2023 Former OM Mart
Project Manager: William Regenthal GRI Project No. 5685
4
 Soil samples with the highest PID readings from the unsaturated, smear and saturated zones for
each soil boring were submitted analyses of TPH-GRO and TPH-DRO using UVF technology.
 A concentration of THP-DRO that exceeded the RAL was reported in the soil sample collected from
SB-12-3’.
 Concentrations of MTBE, benzo(a)anthracene, benzo(b)fluoranthene and/or benzo(a)pyrene that
exceeded the soil-to-water MCCs were reported in the soil samples collected from SB-6-18’ and
SB-12-3’.
 Based on this information, the next course of action should be to conduct a feasibility study for
ground water extraction or injections. Recovery wells could be installed within the center of the
contamination plume to maximize extraction potential, or injections focusing on groundwater
could be implemented within the core of the GCL plume.
5.0 LIMITATIONS
This report has been prepared for the exclusive use of Quality Oil & Gas for specific application to the
referenced site in Montgomery County, North Carolina. The assessment was conducted based on the
scope of work and level of effort desired by NCDEQ and with resources adequate only for that scope of
work. Our findings have been developed in accordance with generally accepted standards of
environmental practices in the State of North Carolina, available information, and our professional
judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.
6.0 STATEMENTS AND CERTIFICATION
1 Enter the date the monitoring report was due. n/a Will this report be submitted after the
established due date?
YES NO
2 Was any required information from the above template missing from this report? YES NO
IF the answer to question #1 or# 2 is “YES”, please provide additional information in this cell to explain
what was missing and why.
3 If applicable, will any of the proposed attenuation milestones under the schedule approved
in the Corrective Action Plan not be met? (within a reasonable margin of error)
YES NO
IF the answer to question #3 is “NO”, skip to the certification under #8 below.
IF the answer to question #3 is “YES”, please generally describe in this cell the possible reason(s) and
outline proposed remedies. (This should be described in more detail in the report text above.)

N/A

FIGURES
SITE LOCATIONFigure 1 Site Location Former OM Mart113 West Main StreetBiscoe, North CarolinaMontgomery CountyIncident No. 29478GRI Project No. 5685500 M2000 FTDate: 08/14/2021 Location: 35.359634° N -79.781609° W Dad

TABLES
UST ID Number 1-4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 2, 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner/Operator
TABLE 1
UST OWNER/OPERATOR INFORMATION
FORMER OM MART (INCIDENT NO. 29478)
00-0-0000021206
Name of Owner or Operator Dates of Ownership / Operation
VISHALP, LLC 08/01/2019 - Current
Address Telephone Number
306 N Main Street, Biscoe, NC 27209 919-271-7568
00-0-0000021206
Name of Owner or Operator Dates of Ownership / Operation
Quality Oil Company (Swink)01/01/1987 - 08/01/2019
Address Telephone Number
203 W Broad Avenue, Rockingham, NC 28379-3529 919-997-3101
00-0-0000021206
Name of Owner or Operator Dates of Ownership / Operation
Quality Oil Company (Swink)09/23/1984 - 08/01/2019
Address Telephone Number
203 W Broad Avenue, Rockingham, NC 28379-3529 919-997-3101
00-0-0000021206
Name of Owner or Operator Dates of Ownership / Operation
Quality Oil Company (Swink)05/21/1984 - 08/01/2019
Address Telephone Number
203 W Broad Avenue, Rockingham, NC 28379-3529 919-997-3101
Date: 08/12/21
Was Release
Associated
with UST
System?
(Yes / No)
1 Gasoline 6,000 01/01/1987 Single Wall Steel 8' x 16' Single Wall FRP Current Yes
2 Gasoline 4,000 09/23/1984 Single Wall Steel 64" x 24' Single Wall FRP Current Yes
3 Gasoline 4,000 09/23/1984 Single Wall Steel 64" x 24' Single Wall FRP Current Yes
4 Gasoline 2,000 05/21/1984 Single Wall Steel 64" x 12' Single Wall FRP Current Yes
Notes:
• FRP: Fiberglass reinforced plastic.
Date
Installed
Construction
Details
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
FORMER OM MART (INCIDENT NO. 29478)
Facility ID # : 00-0-0000021206
UST
ID
No.
Current
or Most
Recent
Contents
Capacity
(gallons)
Date: 03/14/23 Facility ID #: 00-0-0000021206
→
50 100 NA NA NA NA NA NA NA NA NA NA NA
NS NS 0.0072 5.4 8 6 0.085 0.2 0.023 68 540 NS 31
NS NS 12 1,250 60.3 3,120 156 5.5 93.8 625 1,560 31,200 469
SB-1-3'03/01/23 3 53.3 21 14.6 NR NR NR NR NR NR NR NR NR NR NR
SB-1-12'03/01/23 12 52.3 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-1-21'03/01/23 21 39.3 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-2-3'03/01/23 3 0.8 <10 23.8 NR NR NR NR NR NR NR NR NR NR NR
SB-2-12'03/01/23 12 0.9 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-2-30'03/01/23 30 18.1 <10 2.2 NR NR NR NR NR NR NR NR NR NR NR
SB-3-9'03/01/23 9 2.7 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-3-12'03/01/23 12 1.3 11 42.8 <0.006 0.002 J <0.0006 0.004 J 0.014 <0.001 <0.155 <1.94 <17.57 <13.6 <16.89
SB-3-33'03/01/23 33 15.0 <20 5.2 NR NR NR NR NR NR NR NR NR NR NR
SB-4-6'03/01/23 6 2.2 <10 2 NR NR NR NR NR NR NR NR NR NR NR
SB-4-12'03/01/23 12 1.1 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-4-36'03/01/23 36 27.8 <10 2.2 NR NR NR NR NR NR NR NR NR NR NR
SB-5-9'03/01/23 9 10.8 <10 5.2 NR NR NR NR NR NR NR NR NR NR NR
SB-5-12'03/01/23 12 8.5 24.8 4.8 <0.0008 0.001 J <0.0008 0.003 J 0.045 <0.001 <0.189 <1.69 <18.91 <16.6 <20.36
SB-5-24'03/01/23 24 65.0 <20 2.2 NR NR NR NR NR NR NR NR NR NR NR
SB-6-6'03/01/23 6 12.0 10.4 13 NR NR NR NR NR NR NR NR NR NR NR
SB-6-12'03/01/23 12 7.4 <10 12.4 NR NR NR NR NR NR NR NR NR NR NR
SB-6-18'03/01/23 18 264.0 38 13.2 0.001 J 0.006 J 0.001 J 0.003 J 0.195 0.004 J <0.194 2.43 J 27.5 J <17.1 <20.57
SB-7-9'03/01/23 9 3.2 <10 2.2 NR NR NR NR NR NR NR NR NR NR NR
SB-7-12'03/01/23 12 12.6 23.6 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-7-15'03/01/23 15 228.7 13.2 11 NR NR NR NR NR NR NR NR NR NR NR
SB-8-9'03/02/23 9 0.9 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-8-12'03/02/23 12 1.8 10.4 5.8 NR NR NR NR NR NR NR NR NR NR NR
SB-8-24'03/02/23 24 292.1 <10 9.2 NR NR NR NR NR NR NR NR NR NR NR
SB-9-9'03/02/23 9 3.5 <10 4.4 NR NR NR NR NR NR NR NR NR NR NR
SB-9-12'03/02/23 12 3.9 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-9-33'03/02/23 33 28.6 10.4 2 NR NR NR NR NR NR NR NR NR NR NR
SB-10-9'03/02/23 9 2.4 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-10-12'03/02/23 12 1.8 <10 4.2 NR NR NR NR NR NR NR NR NR NR NR
Soil-to-water MCCs
Residential Soil Cleanup Levels C5-C8 AliphaticsRAL Benzo(a)anthraceneBenzeneTolueneEthylbenzeneXylenesMTBENaphthaleneTABLE 3
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
FORMER OM MART (INCIDENT NO. 29478)
Analytical Method EPA Methods 8260 and 8270 MADEP Methods EPH and VPH
Sample IDDate Collected (mm/dd/yy)Sample Depth (ft-BGS)PID ResultsGasoline-Range TPHDiesel-Range TPHC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsUVF
Page 1 of 2
Date: 03/14/23 Facility ID #: 00-0-0000021206
→
50 100 NA NA NA NA NA NA NA NA NA NA NA
NS NS 0.0072 5.4 8 6 0.085 0.2 0.023 68 540 NS 31
NS NS 12 1,250 60.3 3,120 156 5.5 93.8 625 1,560 31,200 469
Soil-to-water MCCs
Residential Soil Cleanup Levels C5-C8 AliphaticsRAL Benzo(a)anthraceneBenzeneTolueneEthylbenzeneXylenesMTBENaphthaleneTABLE 3
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
FORMER OM MART (INCIDENT NO. 29478)
Analytical Method EPA Methods 8260 and 8270 MADEP Methods EPH and VPH
Sample IDDate Collected (mm/dd/yy)Sample Depth (ft-BGS)PID ResultsGasoline-Range TPHDiesel-Range TPHC9-C18 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsUVF
SB-10-24'03/02/23 24 4.7 <10 4.2 NR NR NR NR NR NR NR NR NR NR NR
SB-11-3'03/02/23 3 0.8 <10 4.6 NR NR NR NR NR NR NR NR NR NR NR
SB-11-21'03/02/23 21 1.0 16.4 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-12-3'03/02/23 3 0.9 <10 166.4 <0.0006 0.002 J <0.0006 0.003 J <0.0007 <0.001 0.611 J <23.0 102 <13.4 <27.3
SB-12-12'03/02/23 12 0.4 <10 7.8 NR NR NR NR NR NR NR NR NR NR NR
SB-12-15'03/02/23 15 0.8 <10 8.4 NR NR NR NR NR NR NR NR NR NR NR
SB-13-6'03/02/23 6 0.3 <10 2.6 NR NR NR NR NR NR NR NR NR NR NR
SB-13-12'03/02/23 12 0.4 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-13-30'03/02/23 30 74.8 13.8 7 NR NR NR NR NR NR NR NR NR NR NR
SB-14-3'03/02/23 3 1.9 <10 4.8 NR NR NR NR NR NR NR NR NR NR NR
SB-14-12'03/02/23 12 0.5 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
SB-14-30'03/02/23 30 0.5 <10 <2 NR NR NR NR NR NR NR NR NR NR NR
Notes:
• Results reported in mg/kg (milligrams per kilogram).
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations.
• <: Less than the reporting limit specified in the laboratory report.
• NA: Not Applicable.
• NR: Not Requested.
• J: Estimated value.
• Concentrations in bold face type exceed the RALs and/or soil-to-water MCCs.
• Concentrations of Benzo(b)fluoranthene (0.963 mg/kg) and Benzo(a)pyrene (0.680 J mg/kg) exceeded the soil-to-water MCCs in SB-12-3'.
• NS: No standard specified.
• Please see laboratory report for other compounds detected that did not exceed the soil-to-water MCCs.
Page 2 of 2

APPENDICES

APPENDIX A
State Correspondence
North Carolina Department of Environmental Quality | Division of Waste Management
Fayetteville Regional Office | 225 Green Street | Suite 714 | Systel Building | Fayetteville, NC 28301 | [phone]
January 24, 2023
DELIVERED BY EMAIL ATTACHMENT
Mr. Jimmy McDonald
Quality Oil Company, Inc.
203 W. Broad Avenue
Rockingham, NC 28379
Re: Notice of Regulatory Requirements
15A NCAC 2L .0407(d)
Risk-based Assessment and Corrective Action
for Petroleum Underground Storage Tanks
OM Mart (former)
113 West Main Street
Biscoe, Montgomery County
Incident Number: 29478
Risk Classification: Intermediate
Ranking: I-180-A
Dear Mr. McDonald:
The UST Section is in receipt of the Ground Water Monitoring Report, dated December 23, 2022. You are requested
to conduct a vertical soil profile event to obtain smear zone mass data within the ground water GCL (gross contaminant
level) plume. It is also requested that you obtain samples for Total Organic Carbon and grain size analysis during this
scope of work. The data should be submitted in the Soil Cleanup Plan format on or before May 31, 2023.
If you have any questions regarding trust fund eligibility or reimbursement from the Commercial Leaking Petroleum
Underground Storage Tank Cleanup Fund, please contact the UST Section Trust Fund Branch at [phone]. If
you have any questions regarding the actions that must be taken or the rules mentioned in this letter, please contact
me at the address or telephone number listed below.
Sincerely,
Kenneth E. Currie
Hydrogeologist
Fayetteville Regional Office
UST Section, Division of Waste Management, NCDEQ
c: Mr. William Regenthal, P.G., Geological Resources, Inc. (email copy)
FRO Digital Incident File #29478
5685 Received JAN 25 2023
5685 Received FEB 03 2023

APPENDIX B
UVF Report

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
UVF Trilogy Analytical Report

Samples Collected: March 1-2, 2023
Samples Analyzed: March 3, 2023
Site Name: Former OM Mart
Site Address: 113 W. Main St, Biscoe, NC
GRI Project Number: 5685

March 6, 2023

Xavier T. Farmer, G.I.T.
Operator

Technical Procedures
Calibration
The UFV Trilogy has standard calibrations stored for the following analysis:
 GRO
 DRO
 Total PAH
 Target PAH
 Heavy PAH
Prior to use, calibration standards are used to perform a 5-point verification on the factory stored
calibrations for GRO and DRO. The calibration standards used are as follows:
GRO
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
 10 ppm
DRO
 0.1 ppm
 0.5 ppm
 1 ppm
 3 ppm
 5 ppm
Operation
Sample Extraction
 5mg of soil are weighed into a clean extraction jar
 Methanol is added to the extraction jar to create a 2x or 4x dilution
o 2x Dilution: 10 mL of methanol
o 4x Dilution: 20 mL of methanol
 The extraction jar is shaken for several minutes to thoroughly mix the soil with solvent
(methanol)
 The mixture is allowed to settle for several minutes
 A clean syringe is used to draw liquid from the extraction jar
 A clean filter is attached to the end of the syringe and the liquid dispensed through the filter
into a clean test tube
 This liquid is referred to as the extraction
Dilution Preparation
 An adjustable micropipette is used to precisely measure out the amount of extract needed for
the dilution
 The measured out amount of the extract is added to a clean test tube and methanol is added
dilute the extract. Examples of dilutions are shown below:

Extract Amount
500 μL
200 μL
100 μL
50 μL
25 μL

Add Solvent to the
5 mL line
5 mL line
5 mL line
5 mL line
5 mL line
2x Extract
Dilution Factor
20x
50x
100x
200x
400x
4x Extract
Dilution Factor
40x
100x
200x
400x
800x

Technical Procedures
Sample Analyzation
 The dilution is shaken to thoroughly mix, then poured into a clean glass cuvette
 The desired module is inserted into the UVF Trilogy and the corresponding factory calibration is
selected
 “Measure Fluorescence” is pressed on the touchscreen and the reading is recorded
 The reading should be between the concentrations of the calibration standards (GRO: 0.5-10
ppm; DRO 0.1-5 ppm)
o Reading below the calibration standard range are recorded as below the detection limit
 Detection Limit = (lower range of calibration standards range) x dilution factor
(i.e. a GRO sample with a 100x dilution factor has a detection limit of 50 ppm)
o Readings above the calibration standard range should be further diluted and reanalyzed
o Negative readings are an indication of quenching (see below)
 The reading is multiplied by the dilution factor to calculate the final concentration
 Check suspected contaminated samples for quenching by running additional dilutions
o According to the siteLAB Quick Reference Guide:
“Quenching” can occur when the detector is swamped by too many hydrocarbons or
organic interferences, producing low or negative concentrations. Test the sample at
multiple dilutions to confirm results are linear and accurate.”
QA/QC
Method Blank
 A method blank of methanol will be analyzed following calibration and following the last sample
analyzed each day
Duplicates
 One duplicate will be analyzed for every 20 samples
 The duplicate will be prepared from the extract of the sample and diluted to the same factor as
the sample analyzed
Project Name:Date Collected:
Project Number:Date Analysed:
Project Manager:Operator:
Sample ID Matrix Dilution
Factor x
GRO
Output
(ppm)
=GRO Value
(mg/Kg)
Dilution
Factor x
DRO
Output
(ppm)
=DRO Value
(mg/Kg)
SB-1-3'Soil 20 1.05 21 20 0.73 14.6
SB-1-12'Soil 20 <0.5 <10 20 <0.1 <2
SB-1-21'Soil 20 <0.5 <10 20 <0.1 <2
SB-2-3'Soil 20 <0.5 <10 20 1.19 23.8
SB-2-12'Soil 20 <0.5 <10 20 <0.1 <2
SB-2-30'Soil 20 <0.5 <10 20 0.11 2.2
SB-3-9'Soil 20 <0.5 <10 20 <0.1 <2
SB-3-12'Soil 20 0.55 11 20 2.14 42.8
SB-3-33'Soil 40 <0.5 <20 40 0.13 5.2
SB-4-6'Soil 20 <0.5 <10 20 0.1 2
SB-4-12'Soil 20 <0.5 <10 20 <0.1 <2
SB-4-36'Soil 20 <0.5 <10 20 0.11 2.2
SB-5-9'Soil 20 <0.5 <10 20 0.26 5.2
SB-5-12'Soil 40 0.62 24.8 40 0.12 4.8
SB-5-24'40 <0.5 <20 20 0.11 2.2
SB-6-6'Soil 20 0.52 10.4 20 0.65 13
SB-6-12'Soil 20 <0.5 <10 20 0.62 12.4
SB-6-18'Soil 20 1.9 38 20 0.66 13.2
SB-7-9'Soil 20 <0.5 <10 20 0.11 2.2
SB-7-12'Soil 20 1.18 23.6 20 <0.1 <2
SB-7-15'Soil 20 0.66 13.2 20 0.55 11
SB-8-9 Soil 20 <0.5 <10 20 <0.1 <2
SB-8-12'Soil 20 0.52 10.4 20 0.29 5.8
SB-8-24'Soil 20 <0.5 <10 20 0.46 9.2
SB-9-9'Soil 20 <0.5 <10 20 0.22 4.4
SB-9-12'Soil 20 <0.5 <10 20 <0.1 <2
SB-9-33'Soil 20 0.52 10.4 20 0.1 2
SB-10-9'Soil 20 <0.5 <10 20 <0.1 <2
SB-10-12'Soil 20 <0.5 <10 20 0.21 4.2
SB-10-24'Soil 20 <0.5 <10 20 0.21 4.2
SB-11-3'Soil 20 <0.5 <10 20 0.23 4.6
SB-11-21'Soil 20 0.82 16.4 20 <0.1 <2
SB-12-3'Soil 20 <0.5 <10 40 4.16 166.4
UVF Analytical Report
siteLAB UVF Trilogy
3/3/2023
3/1/23 - 3/2/23
Xavier Farmer
Former OM Mart
5685
William Regenthal
Report Date:
3/6/2023
Page:
1 of 2
Page:
1 of 2
Project Name:Date Collected:
Project Number:Date Analysed:
Project Manager:Operator:
Sample ID Matrix Dilution
Factor x
GRO
Output
(ppm)
=GRO Value
(mg/Kg)
Dilution
Factor x
DRO
Output
(ppm)
=DRO Value
(mg/Kg)
UVF Analytical Report
siteLAB UVF Trilogy
3/3/2023
3/1/23 - 3/2/23
Xavier Farmer
Former OM Mart
5685
William Regenthal
SB-12-12'Soil 20 <0.5 <10 20 0.39 7.8
SB-12-15'Soil 20 <0.5 <10 20 0.42 8.4
SB-13-6'Soil 20 <0.5 <10 20 0.13 2.6
SB-13-12'Soil 20 <0.5 <10 20 <0.1 <2
SB-13-30'Soil 20 0.69 13.8 20 0.35 7
SB-14-3'Soil 20 <0.5 <10 20 0.24 4.8
SB-14-12'Soil 20 <0.5 <10 20 <0.1 <2
SB-14-30'Soil 20 <0.5 <10 20 <0.1 <2
Report Date:
3/6/2023
Page:
2 of 2
Page:
2 of 2

APPENDIX C
Laboratory Report – Soil Samples

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

3/15/2023
Geological Resources, Inc. William Regenthal
113 West Firetower Road, Suite G Winterville, NC, 28590
Ref: Analytical Testing
Lab Report Number: 23-065-0026 Client Project Description: Former OM Mart
GRI #5685
Dear William Regenthal:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 3/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Danyale Love Project Manager
Page 1 of 69
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
02/11/2023MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202368-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-065-0026
Page 2 of 69
Report Number:
Sample Summary Table
Client Project Description:
23-065-0026
Former OM Mart
GRI #5685
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
03/01/2023 11:45Solids 90259 SB-3-12'03/06/2023 16:12
03/01/2023 13:52Solids 90260 SB-5-12'03/06/2023 16:12
03/01/2023 14:35Solids 90261 SB-6-18'03/06/2023 16:12
03/02/2023 12:45Solids 90262 SB-12-3'03/06/2023 16:12
03/02/2023 11:53Solids 90263 SB-11-30'03/06/2023 16:12 SIEVE TEST WP MTN -
03/02/2023 11:53Solids 90263 SB-11-30'03/06/2023 16:12 Texture WP MTN -
03/02/2023 11:53Solids 90263 SB-11-30'03/06/2023 16:12 SIEVE WP MTN -
03/02/2023 11:53Solids 90263 SB-11-30'03/06/2023 16:12 WALK-BLACK WP MTN -
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 69
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-065-0026
Report Limit
Project:Former OM Mart
V 90259SB-3-12'
0.023 03/07/2023 18:348260DAcetonemg/Kg - dry 0.002
J0.020 03/07/2023 18:348260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0007
0.014 03/07/2023 18:348260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0007
J0.002 03/07/2023 18:348260DToluenemg/Kg - dry 0.0007
J0.002 03/07/2023 18:348260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0005
J0.001 03/07/2023 18:348260Do-Xylene mg/Kg - dry 0.0006
J0.003 03/07/2023 18:348260Dm,p-Xylene mg/Kg - dry 0.001
J0.004 03/07/2023 18:348260DXylene (Total)mg/Kg - dry 0.0006
10.6 06/07/2023 16:20SW-DRYWT Moisture %
V 90260SB-5-12'
J0.018 03/07/2023 19:018260DAcetonemg/Kg - dry 0.003
J0.007 03/07/2023 19:018260DMethyl Ethyl Ketone (MEK)mg/Kg - dry 0.0009
0.045 03/07/2023 19:018260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0008
J0.001 03/07/2023 19:018260DToluenemg/Kg - dry 0.0009
J0.001 03/07/2023 19:018260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
J0.0008 03/07/2023 19:018260Do-Xylene mg/Kg - dry 0.0007
J0.003 03/07/2023 19:018260Dm,p-Xylene mg/Kg - dry 0.001
J0.003 03/07/2023 19:018260DXylene (Total)mg/Kg - dry 0.0007
26.6 06/07/2023 16:20SW-DRYWT Moisture %
V 90261SB-6-18'
0.059 03/07/2023 19:558260DAcetonemg/Kg - dry 0.003
J0.001 03/07/2023 19:558260DBenzenemg/Kg - dry 0.0008
0.012 03/07/2023 19:558260Dn-Butylbenzene mg/Kg - dry 0.0007
J0.004 03/07/2023 19:558260Dsec-Butyl benzene mg/Kg - dry 0.0008
J0.001 03/07/2023 19:558260DEthylbenzenemg/Kg - dry 0.0008
0.062 03/07/2023 19:558260Dn-Hexane mg/Kg - dry 0.0009
J0.001 03/07/2023 19:558260DIsopropylbenzenemg/Kg - dry 0.0006
J0.002 03/07/2023 19:558260D4-Isopropyl toluene mg/Kg - dry 0.001
0.195 03/07/2023 19:558260DMethyl tert-butyl ether (MTBE)mg/Kg - dry 0.0009
J0.004 03/07/2023 19:558260DNaphthalenemg/Kg - dry 0.001
0.012 03/07/2023 19:558260Dn-Propylbenzene mg/Kg - dry 0.0008
J0.006 03/07/2023 19:558260DToluenemg/Kg - dry 0.0009
0.042 03/07/2023 19:558260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0007
0.021 03/07/2023 19:558260D1,3,5-Trimethylbenzene mg/Kg - dry 0.0008
J0.001 03/07/2023 19:558260Do-Xylene mg/Kg - dry 0.0007
J0.002 03/07/2023 19:558260Dm,p-Xylene mg/Kg - dry 0.001
Page 4 of 69
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-065-0026
Report Limit
Project:Former OM Mart
V 90261SB-6-18'
J0.003 03/07/2023 19:558260DXylene (Total)mg/Kg - dry 0.0007
J0.241 03/14/2023 00:168270E2-Methylnaphthalene mg/Kg - dry 0.139
J2.43 03/07/2023 11:40CALCULATIONAliphatic C5-C8 (Adjusted)mg/Kg - dry 1.71
J12.8 03/07/2023 11:40CALCULATIONAliphatics C9-C12 (Adjusted)mg/Kg - dry 6.38
J14.7 03/13/2023 14:20MADEP-EPH Aliphatic C9-C18 mg/Kg - dry 12.8
J2.45 03/07/2023 11:40MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 1.71
12.8 03/07/2023 11:40MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 6.38
28.5 06/07/2023 16:20SW-DRYWT Moisture %
V 90262SB-12-3'
J0.021 03/07/2023 19:288260DAcetonemg/Kg - dry 0.002
J0.002 03/07/2023 19:288260DToluenemg/Kg - dry 0.0007
J0.001 03/07/2023 19:288260D1,2,4-Trimethylbenzene mg/Kg - dry 0.0005
J0.0009 03/07/2023 19:288260Do-Xylene mg/Kg - dry 0.0005
J0.002 03/07/2023 19:288260Dm,p-Xylene mg/Kg - dry 0.001
J0.003 03/07/2023 19:288260DXylene (Total)mg/Kg - dry 0.0005
J0.611 03/14/2023 00:388270EBenzo(a)anthracene mg/Kg - dry 0.152
J0.680 03/14/2023 00:388270EBenzo(a)pyrene mg/Kg - dry 0.160
0.963 03/14/2023 00:388270EBenzo(b)fluoranthene mg/Kg - dry 0.159
J0.444 03/14/2023 00:388270EBenzo(g,h,i)perylene mg/Kg - dry 0.148
J0.333 03/14/2023 00:388270EBenzo(k)fluoranthene mg/Kg - dry 0.149
0.825 03/14/2023 00:388270EChrysenemg/Kg - dry 0.155
2.04 03/14/2023 00:388270EFluoranthenemg/Kg - dry 0.134
J0.493 03/14/2023 00:388270EIndeno(1,2,3-cd)pyrene mg/Kg - dry 0.195
1.58 03/14/2023 00:388270EPhenanthrenemg/Kg - dry 0.227
1.65 03/14/2023 00:388270EPyrenemg/Kg - dry 0.146
J10203/07/2023 11:16CALCULATIONAliphatics C9-C12 (Adjusted)mg/Kg - dry 86.2
J10203/07/2023 11:16MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 86.2
8.66 06/07/2023 16:20SW-DRYWT Moisture %
V 90263SB-11-30'
100.0 03/13/2023 12:45SIEVE% Passing 10 Mesh %0.1
99.3 03/13/2023 12:45SIEVE% Passing 40 Mesh %0.1
98.6 03/13/2023 12:45SIEVE% Passing 60 Mesh %0.1
95.4 03/13/2023 12:45SIEVE TEST % Passing 100 Mesh %0.1
99.7 03/13/2023 12:45SIEVE TEST % Passing 20 Mesh %0.1
85.6 03/13/2023 12:45SIEVE TEST % Passing 200 Mesh %0.1
100.0 03/13/2023 12:45SIEVE TEST % Passing 4 Mesh %0.1
Page 5 of 69
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-065-0026
Report Limit
Project:Former OM Mart
V 90263SB-11-30'
37.0 03/09/2023 09:49Texture%Clay %0.1
21.0 03/09/2023 09:49Texture%Sand %0.1
42.0 03/09/2023 09:49Texture%Silt %0.1
Clay Loam 03/09/2023 09:49TextureSoil Classification
0.17 03/14/2023 15:45WALK-BLACK Total Organic Carbon %0.05
Page 6 of 69

Client: Geological Resources, Inc. CASE NARRATIVE
Project: Former OM Mart Lab Report Number: 23-065-0026
Date: 3/15/2023
Volatile Organic Compounds - GC/MS Method 8260D Analyte: Methylene chloride QC Batch No: V30563/V30561
CCV result is below control limits but within method parameters. A standard at or below the RL was analyzed and found acceptable. Results are reported but considered estimated.
Semivolatile Organic Compounds - GC/MS Method 8270E
Analyte: Aniline QC Batch No: V30753/V30730
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be
acceptable.
Sample 89932 (P1S4) Analyte: Bis(2-chloroethyl)ether
QC Batch No: V30753/V30730 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 7 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
10.6 %Moisture 1 06/07/23 16:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.023 mg/Kg - dry 0.002 0.022Acetone 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 03/07/23 18:34 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.022Acrylonitrile 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 03/07/23 18:34 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 03/07/23 18:34 V30563TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 03/07/23 18:34 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 03/07/23 18:34 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 03/07/23 18:34 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 03/07/23 18:34 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 03/07/23 18:34 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.011Chloroethane 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 03/07/23 18:34 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 03/07/23 18:34 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 03/07/23 18:34 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 03/07/23 18:34 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 03/07/23 18:34 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 03/07/23 18:34 V30563TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 03/07/23 18:34 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 03/07/23 18:34 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 03/07/23 18:34 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 03/07/23 18:34 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 03/07/23 18:34 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 03/07/23 18:34 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 03/07/23 18:34 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 03/07/23 18:34 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 03/07/23 18:34 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.055Ethyl Tertiary Butyl Ether (ETBE)1 03/07/23 18:34 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 03/07/23 18:34 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.011n-Hexane 1 03/07/23 18:34 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 03/07/23 18:34 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 03/07/23 18:34 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 03/07/23 18:34 V30563TBL
0.020 J mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 03/07/23 18:34 V30563TBL
0.014 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 03/07/23 18:34 V30563TBL
<0.016 mg/Kg - dry 0.016 0.0224-Methyl-2-Pentanone 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 03/07/23 18:34 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 03/07/23 18:34 V30563TBL
0.002 J mg/Kg - dry 0.0007 0.005Toluene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 03/07/23 18:34 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 03/07/23 18:34 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 03/07/23 18:34 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 03/07/23 18:34 V30563TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 03/07/23 18:34 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 03/07/23 18:34 V30563TBL
0.002 J mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 03/07/23 18:34 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 03/07/23 18:34 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 03/07/23 18:34 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 03/07/23 18:34 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.001 J mg/Kg - dry 0.0006 0.005o-Xylene 1 03/07/23 18:34 V30563TBL
0.003 J mg/Kg - dry 0.001 0.011m,p-Xylene 1 03/07/23 18:34 V30563TBL
0.004 J mg/Kg - dry 0.0006 0.005Xylene (Total)1 03/07/23 18:34 V30563KCC
Surrogate: 4-Bromofluorobenzene 90.6 Limits: 70-130%03/07/23 18:341 TBL V30563
Surrogate: Dibromofluoromethane 104 Limits: 84-123%03/07/23 18:341 TBL V30563
Surrogate: Toluene-d8 100 Limits: 76-129%03/07/23 18:341 TBL V30563
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.129 mg/Kg - dry 0.129 0.738Acenaphthene 1 03/13/23 23:31 V30753JMV
<0.117 mg/Kg - dry 0.117 0.738Acenaphthylene 1 03/13/23 23:31 V30753JMV
<0.170 mg/Kg - dry 0.170 0.738Aniline 1 03/13/23 23:31 V30753JMV
<0.159 mg/Kg - dry 0.159 0.738Anthracene 1 03/13/23 23:31 V30753JMV
<0.155 mg/Kg - dry 0.155 0.738Benzo(a)anthracene 1 03/13/23 23:31 V30753JMV
<0.164 mg/Kg - dry 0.164 0.738Benzo(a)pyrene 1 03/13/23 23:31 V30753JMV
<0.163 mg/Kg - dry 0.163 0.738Benzo(b)fluoranthene 1 03/13/23 23:31 V30753JMV
<0.152 mg/Kg - dry 0.152 0.738Benzo(g,h,i)perylene 1 03/13/23 23:31 V30753JMV
<0.153 mg/Kg - dry 0.153 0.738Benzo(k)fluoranthene 1 03/13/23 23:31 V30753JMV
<0.648 mg/Kg - dry 0.648 2.24Benzoic Acid 1 03/13/23 23:31 V30753JMV
<0.117 mg/Kg - dry 0.117 0.738Benzyl alcohol 1 03/13/23 23:31 V30753JMV
<0.131 mg/Kg - dry 0.131 0.738Bis(2-Chloroethoxy)methane 1 03/13/23 23:31 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.119 mg/Kg - dry 0.119 0.738Bis(2-Chloroethyl)ether 1 03/13/23 23:31 V30753JMV
<0.152 mg/Kg - dry 0.152 0.369Bis(2-Chloroisopropyl)ether 1 03/13/23 23:31 V30753JMV
<0.134 mg/Kg - dry 0.134 0.738Bis(2-ethylhexyl)phthalate 1 03/13/23 23:31 V30753JMV
<0.121 mg/Kg - dry 0.121 0.7384-Bromophenyl phenyl ether 1 03/13/23 23:31 V30753JMV
<0.126 mg/Kg - dry 0.126 0.369Butyl benzyl phthalate 1 03/13/23 23:31 V30753JMV
<0.103 mg/Kg - dry 0.103 0.7384-Chloro-3-methylphenol 1 03/13/23 23:31 V30753JMV
<0.125 mg/Kg - dry 0.125 0.3694-Chloroaniline 1 03/13/23 23:31 V30753JMV
<0.129 mg/Kg - dry 0.129 0.7382-Chloronaphthalene 1 03/13/23 23:31 V30753JMV
<0.109 mg/Kg - dry 0.109 0.7382-Chlorophenol 1 03/13/23 23:31 V30753JMV
<0.140 mg/Kg - dry 0.140 1.124-Chlorophenyl phenyl ether 1 03/13/23 23:31 V30753JMV
<0.158 mg/Kg - dry 0.158 0.738Chrysene 1 03/13/23 23:31 V30753JMV
<0.257 mg/Kg - dry 0.257 0.738Dibenz(a,h)anthracene 1 03/13/23 23:31 V30753JMV
<0.133 mg/Kg - dry 0.133 0.738Dibenzofuran 1 03/13/23 23:31 V30753JMV
<0.105 mg/Kg - dry 0.105 0.7381,2-Dichlorobenzene 1 03/13/23 23:31 V30753JMV
<0.108 mg/Kg - dry 0.108 0.7381,3-Dichlorobenzene 1 03/13/23 23:31 V30753JMV
<0.109 mg/Kg - dry 0.109 0.3691,4-Dichlorobenzene 1 03/13/23 23:31 V30753JMV
<0.164 mg/Kg - dry 0.164 0.7383,3'-Dichlorobenzidine 1 03/13/23 23:31 V30753JMV
<0.107 mg/Kg - dry 0.107 0.7382,4-Dichlorophenol 1 03/13/23 23:31 V30753JMV
<0.201 mg/Kg - dry 0.201 0.738Diethyl phthalate 1 03/13/23 23:31 V30753JMV
<0.194 mg/Kg - dry 0.194 0.738Dimethyl phthalate 1 03/13/23 23:31 V30753JMV
<0.120 mg/Kg - dry 0.120 0.3692,4-Dimethylphenol 1 03/13/23 23:31 V30753JMV
<0.119 mg/Kg - dry 0.119 0.738Di-n-butyl phthalate 1 03/13/23 23:31 V30753JMV
<0.268 mg/Kg - dry 0.268 1.684,6-Dinitro-2-methylphenol 1 03/13/23 23:31 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.581 mg/Kg - dry 0.581 1.682,4-Dinitrophenol 1 03/13/23 23:31 V30753JMV
<0.108 mg/Kg - dry 0.108 0.7382,4-Dinitrotoluene 1 03/13/23 23:31 V30753JMV
<0.120 mg/Kg - dry 0.120 0.7382,6-Dinitrotoluene 1 03/13/23 23:31 V30753JMV
<0.159 mg/Kg - dry 0.159 0.369Di-n-Octyl Phthalate 1 03/13/23 23:31 V30753JMV
<0.137 mg/Kg - dry 0.137 0.738Fluoranthene 1 03/13/23 23:31 V30753JMV
<0.143 mg/Kg - dry 0.143 0.738Fluorene 1 03/13/23 23:31 V30753JMV
<0.118 mg/Kg - dry 0.118 0.738Hexachlorobenzene 1 03/13/23 23:31 V30753JMV
<0.109 mg/Kg - dry 0.109 0.738Hexachlorobutadiene 1 03/13/23 23:31 V30753JMV
<0.175 mg/Kg - dry 0.175 0.738Hexachlorocyclopentadiene 1 03/13/23 23:31 V30753JMV
<0.088 mg/Kg - dry 0.088 0.738Hexachloroethane 1 03/13/23 23:31 V30753JMV
<0.200 mg/Kg - dry 0.200 0.738Indeno(1,2,3-cd)pyrene 1 03/13/23 23:31 V30753JMV
<0.213 mg/Kg - dry 0.213 0.738Isophorone 1 03/13/23 23:31 V30753JMV
<0.118 mg/Kg - dry 0.118 0.7381-Methylnaphthalene 1 03/13/23 23:31 V30753JMV
<0.111 mg/Kg - dry 0.111 0.7382-Methylnaphthalene 1 03/13/23 23:31 V30753JMV
<0.108 mg/Kg - dry 0.108 0.7382-Methylphenol 1 03/13/23 23:31 V30753JMV
<0.094 mg/Kg - dry 0.094 0.7383&4 Methylphenol 1 03/13/23 23:31 V30753JMV
<0.161 mg/Kg - dry 0.161 0.738Naphthalene 1 03/13/23 23:31 V30753JMV
<0.108 mg/Kg - dry 0.108 0.7382-Nitroaniline 1 03/13/23 23:31 V30753JMV
<0.134 mg/Kg - dry 0.134 0.7383-Nitroaniline 1 03/13/23 23:31 V30753JMV
<0.104 mg/Kg - dry 0.104 0.3694-Nitroaniline 1 03/13/23 23:31 V30753JMV
<0.129 mg/Kg - dry 0.129 0.369Nitrobenzene 1 03/13/23 23:31 V30753JMV
<0.099 mg/Kg - dry 0.099 0.7382-Nitrophenol 1 03/13/23 23:31 V30753JMV
<0.130 mg/Kg - dry 0.130 0.7384-Nitrophenol 1 03/13/23 23:31 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.294 mg/Kg - dry 0.294 0.738N-Nitrosodimethylamine 1 03/13/23 23:31 V30753JMV
<0.202 mg/Kg - dry 0.202 0.738N-Nitrosodiphenylamine 1 03/13/23 23:31 V30753JMV
<0.131 mg/Kg - dry 0.131 0.738N-Nitroso-di-n-propylamine 1 03/13/23 23:31 V30753JMV
<0.388 mg/Kg - dry 0.388 1.12Pentachlorophenol 1 03/13/23 23:31 V30753JMV
<0.232 mg/Kg - dry 0.232 0.738Phenanthrene 1 03/13/23 23:31 V30753JMV
<0.125 mg/Kg - dry 0.125 0.738Phenol 1 03/13/23 23:31 V30753JMV
<0.149 mg/Kg - dry 0.149 0.738Pyrene 1 03/13/23 23:31 V30753JMV
<0.088 mg/Kg - dry 0.088 0.369Pyridine 1 03/13/23 23:31 V30753JMV
<0.119 mg/Kg - dry 0.119 0.7381,2,4-Trichlorobenzene 1 03/13/23 23:31 V30753JMV
<0.107 mg/Kg - dry 0.107 0.7382,4,5-Trichlorophenol 1 03/13/23 23:31 V30753JMV
<0.108 mg/Kg - dry 0.108 0.7382,4,6-Trichlorophenol 1 03/13/23 23:31 V30753JMV
8270ESurrogate: Phenol-d5 82.0 Limits: 34-121%03/13/23 23:311 JMV
Surrogate: 2-Fluorobiphenyl 85.6 Limits: 44-115%03/13/23 23:311 JMV V30753
Surrogate: 2-Fluorophenol 85.3 Limits: 35-115%03/13/23 23:311 JMV V30753
Surrogate: Nitrobenzene-d5 79.0 Limits: 37-122%03/13/23 23:311 JMV V30753
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%03/13/23 23:311 JMV V30753
Surrogate: 2,4,6-Tribromophenol 87.7 Limits: 39-132%03/13/23 23:311 JMV V30753
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.94 mg/Kg - dry 1.94 12.8Aliphatic C5-C8 (Adjusted)100 03/07/28 10:28
<7.27 mg/Kg - dry 7.27 12.8Aliphatics C9-C12 (Adjusted)100 03/07/23 10:28
<0.994 mg/Kg - dry 0.994 12.8Aromatic C9-C10 (Adjusted)100 03/07/23 10:28
<15.9 mg/Kg - dry 15.9 56.0Aromatic C11-C22 (Adjusted)1 03/13/23 13:07
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V30678 03/10/23 10:30
<10.3 mg/Kg - dry 10.3 56.0Aliphatic C9-C18 1 03/13/23 13:07 V30725AMP
<13.6 mg/Kg - dry 13.6 56.0Aliphatic C19-C36 1 03/13/23 13:07 V30725AMP
<15.9 mg/Kg - dry 15.9 56.0Aromatic C11-C22 1 03/13/23 13:07 V30725AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 80.5 Limits: 40-140%03/13/23 13:071 AMP
MADEP-EPHSurrogate: Chlorooctadecane 88.7 Limits: 40-140%03/13/23 13:071 AMP
MADEP-EPHSurrogate: OTP Surrogate 78.9 Limits: 40-140%03/13/23 13:071 AMP
Surrogate: 2-Fluorobiphenyl 90.0 Limits: 40-140%03/13/23 13:071 AMP V30725
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
<1.94 mg/Kg - dry 1.94 12.8Aliphatic C5-C8 100 03/07/23 10:28 V30530TBL
<7.27 mg/Kg - dry 7.27 12.8Aliphatic C9-C12 100 03/07/23 10:28 V30530TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-3-12'
90259 Matrix:
3/1/2023 11:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
<0.994 mg/Kg - dry 0.994 12.8Aromatic C9-C10 100 03/07/23 10:28 V30530TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)92.8 Limits: 70-130%03/07/23 10:28100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)94.5 Limits: 70-130%03/07/23 10:28100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
26.6 %Moisture 1 06/07/23 16:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.018 J mg/Kg - dry 0.003 0.027Acetone 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 03/07/23 19:01 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.006Benzene 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/07/23 19:01 V30563TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 03/07/23 19:01 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/07/23 19:01 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 03/07/23 19:01 V30563TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 03/07/23 19:01 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/07/23 19:01 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 03/07/23 19:01 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/07/23 19:01 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.006Di-Isopropyl Ether (DIPE)1 03/07/23 19:01 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 03/07/23 19:01 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 03/07/23 19:01 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 03/07/23 19:01 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/07/23 19:01 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/07/23 19:01 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 03/07/23 19:01 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloroethene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/07/23 19:01 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 03/07/23 19:01 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.006Ethylbenzene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.068Ethyl Tertiary Butyl Ether (ETBE)1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 03/07/23 19:01 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.013n-Hexane 1 03/07/23 19:01 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0272-Hexanone 1 03/07/23 19:01 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/07/23 19:01 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/07/23 19:01 V30563TBL
0.007 J mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 03/07/23 19:01 V30563TBL
0.045 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 03/07/23 19:01 V30563TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 03/07/23 19:01 V30563TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.013Naphthalene 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/07/23 19:01 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/07/23 19:01 V30563TBL
0.001 J mg/Kg - dry 0.0009 0.006Toluene 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0131,2,3-Trichlorobenzene 1 03/07/23 19:01 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 03/07/23 19:01 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 03/07/23 19:01 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/07/23 19:01 V30563TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 03/07/23 19:01 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,2,3-Trichloropropane 1 03/07/23 19:01 V30563TBL
0.001 J mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 03/07/23 19:01 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 03/07/23 19:01 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 03/07/23 19:01 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.0008 J mg/Kg - dry 0.0007 0.006o-Xylene 1 03/07/23 19:01 V30563TBL
0.003 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 03/07/23 19:01 V30563TBL
0.003 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/07/23 19:01 V30563KCC
Surrogate: 4-Bromofluorobenzene 91.9 Limits: 70-130%03/07/23 19:011 TBL V30563
Surrogate: Dibromofluoromethane 102 Limits: 84-123%03/07/23 19:011 TBL V30563
Surrogate: Toluene-d8 101 Limits: 76-129%03/07/23 19:011 TBL V30563
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.158 mg/Kg - dry 0.158 0.899Acenaphthene 1 03/13/23 23:53 V30753JMV
<0.143 mg/Kg - dry 0.143 0.899Acenaphthylene 1 03/13/23 23:53 V30753JMV
<0.207 mg/Kg - dry 0.207 0.899Aniline 1 03/13/23 23:53 V30753JMV
<0.194 mg/Kg - dry 0.194 0.899Anthracene 1 03/13/23 23:53 V30753JMV
<0.189 mg/Kg - dry 0.189 0.899Benzo(a)anthracene 1 03/13/23 23:53 V30753JMV
<0.200 mg/Kg - dry 0.200 0.899Benzo(a)pyrene 1 03/13/23 23:53 V30753JMV
<0.198 mg/Kg - dry 0.198 0.899Benzo(b)fluoranthene 1 03/13/23 23:53 V30753JMV
<0.185 mg/Kg - dry 0.185 0.899Benzo(g,h,i)perylene 1 03/13/23 23:53 V30753JMV
<0.186 mg/Kg - dry 0.186 0.899Benzo(k)fluoranthene 1 03/13/23 23:53 V30753JMV
<0.790 mg/Kg - dry 0.790 2.72Benzoic Acid 1 03/13/23 23:53 V30753JMV
<0.143 mg/Kg - dry 0.143 0.899Benzyl alcohol 1 03/13/23 23:53 V30753JMV
<0.160 mg/Kg - dry 0.160 0.899Bis(2-Chloroethoxy)methane 1 03/13/23 23:53 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.145 mg/Kg - dry 0.145 0.899Bis(2-Chloroethyl)ether 1 03/13/23 23:53 V30753JMV
<0.185 mg/Kg - dry 0.185 0.449Bis(2-Chloroisopropyl)ether 1 03/13/23 23:53 V30753JMV
<0.163 mg/Kg - dry 0.163 0.899Bis(2-ethylhexyl)phthalate 1 03/13/23 23:53 V30753JMV
<0.148 mg/Kg - dry 0.148 0.8994-Bromophenyl phenyl ether 1 03/13/23 23:53 V30753JMV
<0.153 mg/Kg - dry 0.153 0.449Butyl benzyl phthalate 1 03/13/23 23:53 V30753JMV
<0.125 mg/Kg - dry 0.125 0.8994-Chloro-3-methylphenol 1 03/13/23 23:53 V30753JMV
<0.152 mg/Kg - dry 0.152 0.4494-Chloroaniline 1 03/13/23 23:53 V30753JMV
<0.158 mg/Kg - dry 0.158 0.8992-Chloronaphthalene 1 03/13/23 23:53 V30753JMV
<0.133 mg/Kg - dry 0.133 0.8992-Chlorophenol 1 03/13/23 23:53 V30753JMV
<0.171 mg/Kg - dry 0.171 1.364-Chlorophenyl phenyl ether 1 03/13/23 23:53 V30753JMV
<0.193 mg/Kg - dry 0.193 0.899Chrysene 1 03/13/23 23:53 V30753JMV
<0.313 mg/Kg - dry 0.313 0.899Dibenz(a,h)anthracene 1 03/13/23 23:53 V30753JMV
<0.162 mg/Kg - dry 0.162 0.899Dibenzofuran 1 03/13/23 23:53 V30753JMV
<0.128 mg/Kg - dry 0.128 0.8991,2-Dichlorobenzene 1 03/13/23 23:53 V30753JMV
<0.132 mg/Kg - dry 0.132 0.8991,3-Dichlorobenzene 1 03/13/23 23:53 V30753JMV
<0.132 mg/Kg - dry 0.132 0.4491,4-Dichlorobenzene 1 03/13/23 23:53 V30753JMV
<0.200 mg/Kg - dry 0.200 0.8993,3'-Dichlorobenzidine 1 03/13/23 23:53 V30753JMV
<0.130 mg/Kg - dry 0.130 0.8992,4-Dichlorophenol 1 03/13/23 23:53 V30753JMV
<0.245 mg/Kg - dry 0.245 0.899Diethyl phthalate 1 03/13/23 23:53 V30753JMV
<0.237 mg/Kg - dry 0.237 0.899Dimethyl phthalate 1 03/13/23 23:53 V30753JMV
<0.147 mg/Kg - dry 0.147 0.4492,4-Dimethylphenol 1 03/13/23 23:53 V30753JMV
<0.145 mg/Kg - dry 0.145 0.899Di-n-butyl phthalate 1 03/13/23 23:53 V30753JMV
<0.326 mg/Kg - dry 0.326 2.044,6-Dinitro-2-methylphenol 1 03/13/23 23:53 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.708 mg/Kg - dry 0.708 2.042,4-Dinitrophenol 1 03/13/23 23:53 V30753JMV
<0.131 mg/Kg - dry 0.131 0.8992,4-Dinitrotoluene 1 03/13/23 23:53 V30753JMV
<0.147 mg/Kg - dry 0.147 0.8992,6-Dinitrotoluene 1 03/13/23 23:53 V30753JMV
<0.194 mg/Kg - dry 0.194 0.449Di-n-Octyl Phthalate 1 03/13/23 23:53 V30753JMV
<0.167 mg/Kg - dry 0.167 0.899Fluoranthene 1 03/13/23 23:53 V30753JMV
<0.174 mg/Kg - dry 0.174 0.899Fluorene 1 03/13/23 23:53 V30753JMV
<0.144 mg/Kg - dry 0.144 0.899Hexachlorobenzene 1 03/13/23 23:53 V30753JMV
<0.132 mg/Kg - dry 0.132 0.899Hexachlorobutadiene 1 03/13/23 23:53 V30753JMV
<0.213 mg/Kg - dry 0.213 0.899Hexachlorocyclopentadiene 1 03/13/23 23:53 V30753JMV
<0.107 mg/Kg - dry 0.107 0.899Hexachloroethane 1 03/13/23 23:53 V30753JMV
<0.243 mg/Kg - dry 0.243 0.899Indeno(1,2,3-cd)pyrene 1 03/13/23 23:53 V30753JMV
<0.260 mg/Kg - dry 0.260 0.899Isophorone 1 03/13/23 23:53 V30753JMV
<0.144 mg/Kg - dry 0.144 0.8991-Methylnaphthalene 1 03/13/23 23:53 V30753JMV
<0.136 mg/Kg - dry 0.136 0.8992-Methylnaphthalene 1 03/13/23 23:53 V30753JMV
<0.132 mg/Kg - dry 0.132 0.8992-Methylphenol 1 03/13/23 23:53 V30753JMV
<0.115 mg/Kg - dry 0.115 0.8993&4 Methylphenol 1 03/13/23 23:53 V30753JMV
<0.196 mg/Kg - dry 0.196 0.899Naphthalene 1 03/13/23 23:53 V30753JMV
<0.131 mg/Kg - dry 0.131 0.8992-Nitroaniline 1 03/13/23 23:53 V30753JMV
<0.163 mg/Kg - dry 0.163 0.8993-Nitroaniline 1 03/13/23 23:53 V30753JMV
<0.127 mg/Kg - dry 0.127 0.4494-Nitroaniline 1 03/13/23 23:53 V30753JMV
<0.158 mg/Kg - dry 0.158 0.449Nitrobenzene 1 03/13/23 23:53 V30753JMV
<0.120 mg/Kg - dry 0.120 0.8992-Nitrophenol 1 03/13/23 23:53 V30753JMV
<0.159 mg/Kg - dry 0.159 0.8994-Nitrophenol 1 03/13/23 23:53 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.358 mg/Kg - dry 0.358 0.899N-Nitrosodimethylamine 1 03/13/23 23:53 V30753JMV
<0.246 mg/Kg - dry 0.246 0.899N-Nitrosodiphenylamine 1 03/13/23 23:53 V30753JMV
<0.160 mg/Kg - dry 0.160 0.899N-Nitroso-di-n-propylamine 1 03/13/23 23:53 V30753JMV
<0.472 mg/Kg - dry 0.472 1.36Pentachlorophenol 1 03/13/23 23:53 V30753JMV
<0.283 mg/Kg - dry 0.283 0.899Phenanthrene 1 03/13/23 23:53 V30753JMV
<0.152 mg/Kg - dry 0.152 0.899Phenol 1 03/13/23 23:53 V30753JMV
<0.182 mg/Kg - dry 0.182 0.899Pyrene 1 03/13/23 23:53 V30753JMV
<0.107 mg/Kg - dry 0.107 0.449Pyridine 1 03/13/23 23:53 V30753JMV
<0.145 mg/Kg - dry 0.145 0.8991,2,4-Trichlorobenzene 1 03/13/23 23:53 V30753JMV
<0.131 mg/Kg - dry 0.131 0.8992,4,5-Trichlorophenol 1 03/13/23 23:53 V30753JMV
<0.131 mg/Kg - dry 0.131 0.8992,4,6-Trichlorophenol 1 03/13/23 23:53 V30753JMV
8270ESurrogate: Phenol-d5 79.0 Limits: 34-121%03/13/23 23:531 JMV
Surrogate: 2-Fluorobiphenyl 85.0 Limits: 44-115%03/13/23 23:531 JMV V30753
Surrogate: 2-Fluorophenol 81.7 Limits: 35-115%03/13/23 23:531 JMV V30753
Surrogate: Nitrobenzene-d5 77.8 Limits: 37-122%03/13/23 23:531 JMV V30753
Surrogate: 4-Terphenyl-d14 106 Limits: 54-127%03/13/23 23:531 JMV V30753
Surrogate: 2,4,6-Tribromophenol 88.0 Limits: 39-132%03/13/23 23:531 JMV V30753
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<1.69 mg/Kg - dry 1.69 11.1Aliphatic C5-C8 (Adjusted)100 03/07/23 10:52
<6.31 mg/Kg - dry 6.31 11.1Aliphatics C9-C12 (Adjusted)100 03/07/23 10:52
<0.863 mg/Kg - dry 0.863 11.1Aromatic C9-C10 (Adjusted)100 03/07/23 10:52
<19.5 mg/Kg - dry 19.5 68.4Aromatic C11-C22 (Adjusted)1 03/13/23 13:44
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V30678 03/10/23 10:30
<12.6 mg/Kg - dry 12.6 68.4Aliphatic C9-C18 1 03/13/23 13:44 V30725AMP
<16.6 mg/Kg - dry 16.6 68.4Aliphatic C19-C36 1 03/13/23 13:44 V30725AMP
<19.5 mg/Kg - dry 19.5 68.4Aromatic C11-C22 1 03/13/23 13:44 V30725AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 78.8 Limits: 40-140%03/13/23 13:441 AMP
MADEP-EPHSurrogate: Chlorooctadecane 85.2 Limits: 40-140%03/13/23 13:441 AMP
MADEP-EPHSurrogate: OTP Surrogate 72.3 Limits: 40-140%03/13/23 13:441 AMP
Surrogate: 2-Fluorobiphenyl 85.5 Limits: 40-140%03/13/23 13:441 AMP V30725
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
<1.69 mg/Kg - dry 1.69 11.1Aliphatic C5-C8 100 03/07/23 10:52 V30530TBL
<6.31 mg/Kg - dry 6.31 11.1Aliphatic C9-C12 100 03/07/23 10:52 V30530TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-5-12'
90260 Matrix:
3/1/2023 13:52
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
<0.863 mg/Kg - dry 0.863 11.1Aromatic C9-C10 100 03/07/23 10:52 V30530TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)119 Limits: 70-130%03/07/23 10:52100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)119 Limits: 70-130%03/07/23 10:52100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
28.5 %Moisture 1 06/07/23 16:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.059 mg/Kg - dry 0.003 0.027Acetone 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.027Acrolein 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.027Acrylonitrile 1 03/07/23 19:55 V30563TBL
0.001 J mg/Kg - dry 0.0008 0.006Benzene 1 03/07/23 19:55 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.006Bromobenzene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 03/07/23 19:55 V30563TBL
<0.002 mg/Kg - dry 0.002 0.013Bromomethane 1 03/07/23 19:55 V30563TBL
0.012 mg/Kg - dry 0.0007 0.006n-Butylbenzene 1 03/07/23 19:55 V30563TBL
0.004 J mg/Kg - dry 0.0008 0.006sec-Butyl benzene 1 03/07/23 19:55 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.006tert-Butyl benzene 1 03/07/23 19:55 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.006Carbon Disulfide 1 03/07/23 19:55 V30563TBL
<0.002 mg/Kg - dry 0.002 0.006Carbon Tetrachloride 1 03/07/23 19:55 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.006Chlorobenzene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.013Chloroethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 03/07/23 19:55 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.013Chloromethane 1 03/07/23 19:55 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0062-Chlorotoluene 1 03/07/23 19:55 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Di-Isopropyl Ether (DIPE)1 03/07/23 19:55 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0131,2-Dibromo-3-Chloropropane 1 03/07/23 19:55 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
<0.0008 mg/Kg - dry 0.0008 0.0061,2-Dibromoethane 1 03/07/23 19:55 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.006Dibromomethane 1 03/07/23 19:55 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 03/07/23 19:55 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 03/07/23 19:55 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.013Dichlorodifluoromethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006cis-1,2-Dichloroethene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 03/07/23 19:55 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 03/07/23 19:55 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,3-Dichloropropane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloropropene 1 03/07/23 19:55 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.006cis-1,3-Dichloropropene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 03/07/23 19:55 V30563TBL
0.001 J mg/Kg - dry 0.0008 0.006Ethylbenzene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.069Ethyl Tertiary Butyl Ether (ETBE)1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.013Hexachlorobutadiene 1 03/07/23 19:55 V30563TBL
0.062 mg/Kg - dry 0.0009 0.013n-Hexane 1 03/07/23 19:55 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.0272-Hexanone 1 03/07/23 19:55 V30563TBL
0.001 J mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 03/07/23 19:55 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.002 J mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 03/07/23 19:55 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.027Methyl Ethyl Ketone (MEK)1 03/07/23 19:55 V30563TBL
0.195 mg/Kg - dry 0.0009 0.006Methyl tert-butyl ether (MTBE)1 03/07/23 19:55 V30563TBL
<0.020 mg/Kg - dry 0.020 0.0274-Methyl-2-Pentanone 1 03/07/23 19:55 V30563TBL
<0.002 mg/Kg - dry 0.002 0.013Methylene Chloride 1 03/07/23 19:55 V30563TBL
0.004 J mg/Kg - dry 0.001 0.013Naphthalene 1 03/07/23 19:55 V30563TBL
0.012 mg/Kg - dry 0.0008 0.006n-Propylbenzene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 03/07/23 19:55 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 03/07/23 19:55 V30563TBL
0.006 J mg/Kg - dry 0.0009 0.006Toluene 1 03/07/23 19:55 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0131,2,3-Trichlorobenzene 1 03/07/23 19:55 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.0131,2,4-Trichlorobenzene 1 03/07/23 19:55 V30563TBL
<0.002 mg/Kg - dry 0.002 0.0061,1,1-Trichloroethane 1 03/07/23 19:55 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,1,2-Trichloroethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 03/07/23 19:55 V30563TBL
<0.002 mg/Kg - dry 0.002 0.013Trichlorofluoromethane 1 03/07/23 19:55 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0061,2,3-Trichloropropane 1 03/07/23 19:55 V30563TBL
0.042 mg/Kg - dry 0.0007 0.0061,2,4-Trimethylbenzene 1 03/07/23 19:55 V30563TBL
0.021 mg/Kg - dry 0.0008 0.0061,3,5-Trimethylbenzene 1 03/07/23 19:55 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.013Vinyl Acetate 1 03/07/23 19:55 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.013Vinyl Chloride 1 03/07/23 19:55 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.001 J mg/Kg - dry 0.0007 0.006o-Xylene 1 03/07/23 19:55 V30563TBL
0.002 J mg/Kg - dry 0.001 0.013m,p-Xylene 1 03/07/23 19:55 V30563TBL
0.003 J mg/Kg - dry 0.0007 0.006Xylene (Total)1 03/07/23 19:55 V30563KCC
Surrogate: 4-Bromofluorobenzene 90.6 Limits: 70-130%03/07/23 19:551 TBL V30563
Surrogate: Dibromofluoromethane 103 Limits: 84-123%03/07/23 19:551 TBL V30563
Surrogate: Toluene-d8 102 Limits: 76-129%03/07/23 19:551 TBL V30563
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.162 mg/Kg - dry 0.162 0.924Acenaphthene 1 03/14/23 00:16 V30753JMV
<0.146 mg/Kg - dry 0.146 0.924Acenaphthylene 1 03/14/23 00:16 V30753JMV
<0.212 mg/Kg - dry 0.212 0.924Aniline 1 03/14/23 00:16 V30753JMV
<0.200 mg/Kg - dry 0.200 0.924Anthracene 1 03/14/23 00:16 V30753JMV
<0.194 mg/Kg - dry 0.194 0.924Benzo(a)anthracene 1 03/14/23 00:16 V30753JMV
<0.205 mg/Kg - dry 0.205 0.924Benzo(a)pyrene 1 03/14/23 00:16 V30753JMV
<0.204 mg/Kg - dry 0.204 0.924Benzo(b)fluoranthene 1 03/14/23 00:16 V30753JMV
<0.190 mg/Kg - dry 0.190 0.924Benzo(g,h,i)perylene 1 03/14/23 00:16 V30753JMV
<0.191 mg/Kg - dry 0.191 0.924Benzo(k)fluoranthene 1 03/14/23 00:16 V30753JMV
<0.811 mg/Kg - dry 0.811 2.80Benzoic Acid 1 03/14/23 00:16 V30753JMV
<0.146 mg/Kg - dry 0.146 0.924Benzyl alcohol 1 03/14/23 00:16 V30753JMV
<0.165 mg/Kg - dry 0.165 0.924Bis(2-Chloroethoxy)methane 1 03/14/23 00:16 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.149 mg/Kg - dry 0.149 0.924Bis(2-Chloroethyl)ether 1 03/14/23 00:16 V30753JMV
<0.190 mg/Kg - dry 0.190 0.462Bis(2-Chloroisopropyl)ether 1 03/14/23 00:16 V30753JMV
<0.167 mg/Kg - dry 0.167 0.924Bis(2-ethylhexyl)phthalate 1 03/14/23 00:16 V30753JMV
<0.152 mg/Kg - dry 0.152 0.9244-Bromophenyl phenyl ether 1 03/14/23 00:16 V30753JMV
<0.158 mg/Kg - dry 0.158 0.462Butyl benzyl phthalate 1 03/14/23 00:16 V30753JMV
<0.129 mg/Kg - dry 0.129 0.9244-Chloro-3-methylphenol 1 03/14/23 00:16 V30753JMV
<0.156 mg/Kg - dry 0.156 0.4624-Chloroaniline 1 03/14/23 00:16 V30753JMV
<0.162 mg/Kg - dry 0.162 0.9242-Chloronaphthalene 1 03/14/23 00:16 V30753JMV
<0.137 mg/Kg - dry 0.137 0.9242-Chlorophenol 1 03/14/23 00:16 V30753JMV
<0.176 mg/Kg - dry 0.176 1.404-Chlorophenyl phenyl ether 1 03/14/23 00:16 V30753JMV
<0.198 mg/Kg - dry 0.198 0.924Chrysene 1 03/14/23 00:16 V30753JMV
<0.321 mg/Kg - dry 0.321 0.924Dibenz(a,h)anthracene 1 03/14/23 00:16 V30753JMV
<0.166 mg/Kg - dry 0.166 0.924Dibenzofuran 1 03/14/23 00:16 V30753JMV
<0.132 mg/Kg - dry 0.132 0.9241,2-Dichlorobenzene 1 03/14/23 00:16 V30753JMV
<0.136 mg/Kg - dry 0.136 0.9241,3-Dichlorobenzene 1 03/14/23 00:16 V30753JMV
<0.136 mg/Kg - dry 0.136 0.4621,4-Dichlorobenzene 1 03/14/23 00:16 V30753JMV
<0.205 mg/Kg - dry 0.205 0.9243,3'-Dichlorobenzidine 1 03/14/23 00:16 V30753JMV
<0.134 mg/Kg - dry 0.134 0.9242,4-Dichlorophenol 1 03/14/23 00:16 V30753JMV
<0.251 mg/Kg - dry 0.251 0.924Diethyl phthalate 1 03/14/23 00:16 V30753JMV
<0.243 mg/Kg - dry 0.243 0.924Dimethyl phthalate 1 03/14/23 00:16 V30753JMV
<0.151 mg/Kg - dry 0.151 0.4622,4-Dimethylphenol 1 03/14/23 00:16 V30753JMV
<0.149 mg/Kg - dry 0.149 0.924Di-n-butyl phthalate 1 03/14/23 00:16 V30753JMV
<0.335 mg/Kg - dry 0.335 2.104,6-Dinitro-2-methylphenol 1 03/14/23 00:16 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.727 mg/Kg - dry 0.727 2.102,4-Dinitrophenol 1 03/14/23 00:16 V30753JMV
<0.135 mg/Kg - dry 0.135 0.9242,4-Dinitrotoluene 1 03/14/23 00:16 V30753JMV
<0.151 mg/Kg - dry 0.151 0.9242,6-Dinitrotoluene 1 03/14/23 00:16 V30753JMV
<0.200 mg/Kg - dry 0.200 0.462Di-n-Octyl Phthalate 1 03/14/23 00:16 V30753JMV
<0.172 mg/Kg - dry 0.172 0.924Fluoranthene 1 03/14/23 00:16 V30753JMV
<0.179 mg/Kg - dry 0.179 0.924Fluorene 1 03/14/23 00:16 V30753JMV
<0.148 mg/Kg - dry 0.148 0.924Hexachlorobenzene 1 03/14/23 00:16 V30753JMV
<0.136 mg/Kg - dry 0.136 0.924Hexachlorobutadiene 1 03/14/23 00:16 V30753JMV
<0.219 mg/Kg - dry 0.219 0.924Hexachlorocyclopentadiene 1 03/14/23 00:16 V30753JMV
<0.110 mg/Kg - dry 0.110 0.924Hexachloroethane 1 03/14/23 00:16 V30753JMV
<0.250 mg/Kg - dry 0.250 0.924Indeno(1,2,3-cd)pyrene 1 03/14/23 00:16 V30753JMV
<0.267 mg/Kg - dry 0.267 0.924Isophorone 1 03/14/23 00:16 V30753JMV
<0.148 mg/Kg - dry 0.148 0.9241-Methylnaphthalene 1 03/14/23 00:16 V30753JMV
0.241 J mg/Kg - dry 0.139 0.9242-Methylnaphthalene 1 03/14/23 00:16 V30753JMV
<0.135 mg/Kg - dry 0.135 0.9242-Methylphenol 1 03/14/23 00:16 V30753JMV
<0.118 mg/Kg - dry 0.118 0.9243&4 Methylphenol 1 03/14/23 00:16 V30753JMV
<0.201 mg/Kg - dry 0.201 0.924Naphthalene 1 03/14/23 00:16 V30753JMV
<0.135 mg/Kg - dry 0.135 0.9242-Nitroaniline 1 03/14/23 00:16 V30753JMV
<0.167 mg/Kg - dry 0.167 0.9243-Nitroaniline 1 03/14/23 00:16 V30753JMV
<0.130 mg/Kg - dry 0.130 0.4624-Nitroaniline 1 03/14/23 00:16 V30753JMV
<0.162 mg/Kg - dry 0.162 0.462Nitrobenzene 1 03/14/23 00:16 V30753JMV
<0.124 mg/Kg - dry 0.124 0.9242-Nitrophenol 1 03/14/23 00:16 V30753JMV
<0.163 mg/Kg - dry 0.163 0.9244-Nitrophenol 1 03/14/23 00:16 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.367 mg/Kg - dry 0.367 0.924N-Nitrosodimethylamine 1 03/14/23 00:16 V30753JMV
<0.253 mg/Kg - dry 0.253 0.924N-Nitrosodiphenylamine 1 03/14/23 00:16 V30753JMV
<0.165 mg/Kg - dry 0.165 0.924N-Nitroso-di-n-propylamine 1 03/14/23 00:16 V30753JMV
<0.485 mg/Kg - dry 0.485 1.40Pentachlorophenol 1 03/14/23 00:16 V30753JMV
<0.290 mg/Kg - dry 0.290 0.924Phenanthrene 1 03/14/23 00:16 V30753JMV
<0.156 mg/Kg - dry 0.156 0.924Phenol 1 03/14/23 00:16 V30753JMV
<0.187 mg/Kg - dry 0.187 0.924Pyrene 1 03/14/23 00:16 V30753JMV
<0.111 mg/Kg - dry 0.111 0.462Pyridine 1 03/14/23 00:16 V30753JMV
<0.149 mg/Kg - dry 0.149 0.9241,2,4-Trichlorobenzene 1 03/14/23 00:16 V30753JMV
<0.134 mg/Kg - dry 0.134 0.9242,4,5-Trichlorophenol 1 03/14/23 00:16 V30753JMV
<0.135 mg/Kg - dry 0.135 0.9242,4,6-Trichlorophenol 1 03/14/23 00:16 V30753JMV
8270ESurrogate: Phenol-d5 76.3 Limits: 34-121%03/14/23 00:161 JMV
Surrogate: 2-Fluorobiphenyl 83.2 Limits: 44-115%03/14/23 00:161 JMV V30753
Surrogate: 2-Fluorophenol 81.7 Limits: 35-115%03/14/23 00:161 JMV V30753
Surrogate: Nitrobenzene-d5 75.4 Limits: 37-122%03/14/23 00:161 JMV V30753
Surrogate: 4-Terphenyl-d14 105 Limits: 54-127%03/14/23 00:161 JMV V30753
Surrogate: 2,4,6-Tribromophenol 93.4 Limits: 39-132%03/14/23 00:161 JMV V30753
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
2.43 J mg/Kg - dry 1.71 11.2Aliphatic C5-C8 (Adjusted)1 03/07/23 11:40
12.8 J mg/Kg - dry 6.38 11.2Aliphatics C9-C12 (Adjusted)1 03/07/23 11:40
<0.872 mg/Kg - dry 0.872 11.2Aromatic C9-C10 (Adjusted)100 03/07/23 11:40
<19.7 mg/Kg - dry 19.7 69.7Aromatic C11-C22 (Adjusted)1 03/13/23 14:20
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V30678 03/10/23 10:30
14.7 J mg/Kg - dry 12.8 69.7Aliphatic C9-C18 1 03/13/23 14:20 V30725AMP
<17.1 mg/Kg - dry 17.1 69.7Aliphatic C19-C36 1 03/13/23 14:20 V30725AMP
<19.7 mg/Kg - dry 19.7 69.7Aromatic C11-C22 1 03/13/23 14:20 V30725AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 79.6 Limits: 40-140%03/13/23 14:201 AMP
MADEP-EPHSurrogate: Chlorooctadecane 85.1 Limits: 40-140%03/13/23 14:201 AMP
MADEP-EPHSurrogate: OTP Surrogate 67.6 Limits: 40-140%03/13/23 14:201 AMP
Surrogate: 2-Fluorobiphenyl 86.9 Limits: 40-140%03/13/23 14:201 AMP V30725
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
2.45 J mg/Kg - dry 1.71 11.2Aliphatic C5-C8 100 03/07/23 11:40 V30530TBL
12.8 mg/Kg - dry 6.38 11.2Aliphatic C9-C12 100 03/07/23 11:40 V30530TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-6-18'
90261 Matrix:
3/1/2023 14:35
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
<0.872 mg/Kg - dry 0.872 11.2Aromatic C9-C10 100 03/07/23 11:40 V30530TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)104 Limits: 70-130%03/07/23 11:40100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)101 Limits: 70-130%03/07/23 11:40100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
8.66 %Moisture 1 06/07/23 16:20 SW-DRYWTAMB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.021 J mg/Kg - dry 0.002 0.021Acetone 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.021Acrolein 1 03/07/23 19:28 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.021Acrylonitrile 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005Benzene 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.005Bromobenzene 1 03/07/23 19:28 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.010Bromomethane 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.005n-Butylbenzene 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.005tert-Butyl benzene 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.005Chlorobenzene 1 03/07/23 19:28 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.005Chlorodibromomethane 1 03/07/23 19:28 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.010Chloroethane 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.010Chloromethane 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 03/07/23 19:28 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 03/07/23 19:28 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0101,2-Dibromo-3-Chloropropane 1 03/07/23 19:28 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.0051,2-Dibromoethane 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 03/07/23 19:28 V30563TBL
<0.0003 mg/Kg - dry 0.0003 0.0051,2-Dichlorobenzene 1 03/07/23 19:28 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.010Dichlorodifluoromethane 1 03/07/23 19:28 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 03/07/23 19:28 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 03/07/23 19:28 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 03/07/23 19:28 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloropropene 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 03/07/23 19:28 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005Ethylbenzene 1 03/07/23 19:28 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.054Ethyl Tertiary Butyl Ether (ETBE)1 03/07/23 19:28 V30563TBL
<0.0009 mg/Kg - dry 0.0009 0.010Hexachlorobutadiene 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.010n-Hexane 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0212-Hexanone 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 03/07/23 19:28 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.021Methyl Ethyl Ketone (MEK)1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 03/07/23 19:28 V30563TBL
<0.016 mg/Kg - dry 0.016 0.0214-Methyl-2-Pentanone 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.010Methylene Chloride 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.010Naphthalene 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 03/07/23 19:28 V30563TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 03/07/23 19:28 V30563TBL
<0.0010 mg/Kg - dry 0.0010 0.005Tetrachloroethene 1 03/07/23 19:28 V30563TBL
0.002 J mg/Kg - dry 0.0007 0.005Toluene 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0101,2,3-Trichlorobenzene 1 03/07/23 19:28 V30563TBL
<0.0007 mg/Kg - dry 0.0007 0.0101,2,4-Trichlorobenzene 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 03/07/23 19:28 V30563TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 03/07/23 19:28 V30563TBL
<0.002 mg/Kg - dry 0.002 0.010Trichlorofluoromethane 1 03/07/23 19:28 V30563TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 03/07/23 19:28 V30563TBL
0.001 J mg/Kg - dry 0.0005 0.0051,2,4-Trimethylbenzene 1 03/07/23 19:28 V30563TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Acetate 1 03/07/23 19:28 V30563TBL
<0.0005 mg/Kg - dry 0.0005 0.010Vinyl Chloride 1 03/07/23 19:28 V30563TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V30561 03/07/23 08:00
0.0009 J mg/Kg - dry 0.0005 0.005o-Xylene 1 03/07/23 19:28 V30563TBL
0.002 J mg/Kg - dry 0.001 0.010m,p-Xylene 1 03/07/23 19:28 V30563TBL
0.003 J mg/Kg - dry 0.0005 0.005Xylene (Total)1 03/07/23 19:28 V30563KCC
Surrogate: 4-Bromofluorobenzene 89.5 Limits: 70-130%03/07/23 19:281 TBL V30563
Surrogate: Dibromofluoromethane 102 Limits: 84-123%03/07/23 19:281 TBL V30563
Surrogate: Toluene-d8 100 Limits: 76-129%03/07/23 19:281 TBL V30563
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.126 mg/Kg - dry 0.126 0.722Acenaphthene 1 03/14/23 00:38 V30753JMV
<0.114 mg/Kg - dry 0.114 0.722Acenaphthylene 1 03/14/23 00:38 V30753JMV
<0.166 mg/Kg - dry 0.166 0.722Aniline 1 03/14/23 00:38 V30753JMV
<0.156 mg/Kg - dry 0.156 0.722Anthracene 1 03/14/23 00:38 V30753JMV
0.611 J mg/Kg - dry 0.152 0.722Benzo(a)anthracene 1 03/14/23 00:38 V30753JMV
0.680 J mg/Kg - dry 0.160 0.722Benzo(a)pyrene 1 03/14/23 00:38 V30753JMV
0.963 mg/Kg - dry 0.159 0.722Benzo(b)fluoranthene 1 03/14/23 00:38 V30753JMV
0.444 J mg/Kg - dry 0.148 0.722Benzo(g,h,i)perylene 1 03/14/23 00:38 V30753JMV
0.333 J mg/Kg - dry 0.149 0.722Benzo(k)fluoranthene 1 03/14/23 00:38 V30753JMV
<0.634 mg/Kg - dry 0.634 2.19Benzoic Acid 1 03/14/23 00:38 V30753JMV
<0.114 mg/Kg - dry 0.114 0.722Benzyl alcohol 1 03/14/23 00:38 V30753JMV
<0.129 mg/Kg - dry 0.129 0.722Bis(2-Chloroethoxy)methane 1 03/14/23 00:38 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.117 mg/Kg - dry 0.117 0.722Bis(2-Chloroethyl)ether 1 03/14/23 00:38 V30753JMV
<0.148 mg/Kg - dry 0.148 0.361Bis(2-Chloroisopropyl)ether 1 03/14/23 00:38 V30753JMV
<0.131 mg/Kg - dry 0.131 0.722Bis(2-ethylhexyl)phthalate 1 03/14/23 00:38 V30753JMV
<0.119 mg/Kg - dry 0.119 0.7224-Bromophenyl phenyl ether 1 03/14/23 00:38 V30753JMV
<0.123 mg/Kg - dry 0.123 0.361Butyl benzyl phthalate 1 03/14/23 00:38 V30753JMV
<0.101 mg/Kg - dry 0.101 0.7224-Chloro-3-methylphenol 1 03/14/23 00:38 V30753JMV
<0.122 mg/Kg - dry 0.122 0.3614-Chloroaniline 1 03/14/23 00:38 V30753JMV
<0.126 mg/Kg - dry 0.126 0.7222-Chloronaphthalene 1 03/14/23 00:38 V30753JMV
<0.107 mg/Kg - dry 0.107 0.7222-Chlorophenol 1 03/14/23 00:38 V30753JMV
<0.137 mg/Kg - dry 0.137 1.094-Chlorophenyl phenyl ether 1 03/14/23 00:38 V30753JMV
0.825 mg/Kg - dry 0.155 0.722Chrysene 1 03/14/23 00:38 V30753JMV
<0.251 mg/Kg - dry 0.251 0.722Dibenz(a,h)anthracene 1 03/14/23 00:38 V30753JMV
<0.130 mg/Kg - dry 0.130 0.722Dibenzofuran 1 03/14/23 00:38 V30753JMV
<0.103 mg/Kg - dry 0.103 0.7221,2-Dichlorobenzene 1 03/14/23 00:38 V30753JMV
<0.106 mg/Kg - dry 0.106 0.7221,3-Dichlorobenzene 1 03/14/23 00:38 V30753JMV
<0.106 mg/Kg - dry 0.106 0.3611,4-Dichlorobenzene 1 03/14/23 00:38 V30753JMV
<0.160 mg/Kg - dry 0.160 0.7223,3'-Dichlorobenzidine 1 03/14/23 00:38 V30753JMV
<0.104 mg/Kg - dry 0.104 0.7222,4-Dichlorophenol 1 03/14/23 00:38 V30753JMV
<0.197 mg/Kg - dry 0.197 0.722Diethyl phthalate 1 03/14/23 00:38 V30753JMV
<0.190 mg/Kg - dry 0.190 0.722Dimethyl phthalate 1 03/14/23 00:38 V30753JMV
<0.118 mg/Kg - dry 0.118 0.3612,4-Dimethylphenol 1 03/14/23 00:38 V30753JMV
<0.117 mg/Kg - dry 0.117 0.722Di-n-butyl phthalate 1 03/14/23 00:38 V30753JMV
<0.262 mg/Kg - dry 0.262 1.644,6-Dinitro-2-methylphenol 1 03/14/23 00:38 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.569 mg/Kg - dry 0.569 1.642,4-Dinitrophenol 1 03/14/23 00:38 V30753JMV
<0.105 mg/Kg - dry 0.105 0.7222,4-Dinitrotoluene 1 03/14/23 00:38 V30753JMV
<0.118 mg/Kg - dry 0.118 0.7222,6-Dinitrotoluene 1 03/14/23 00:38 V30753JMV
<0.156 mg/Kg - dry 0.156 0.361Di-n-Octyl Phthalate 1 03/14/23 00:38 V30753JMV
2.04 mg/Kg - dry 0.134 0.722Fluoranthene 1 03/14/23 00:38 V30753JMV
<0.140 mg/Kg - dry 0.140 0.722Fluorene 1 03/14/23 00:38 V30753JMV
<0.116 mg/Kg - dry 0.116 0.722Hexachlorobenzene 1 03/14/23 00:38 V30753JMV
<0.106 mg/Kg - dry 0.106 0.722Hexachlorobutadiene 1 03/14/23 00:38 V30753JMV
<0.171 mg/Kg - dry 0.171 0.722Hexachlorocyclopentadiene 1 03/14/23 00:38 V30753JMV
<0.086 mg/Kg - dry 0.086 0.722Hexachloroethane 1 03/14/23 00:38 V30753JMV
0.493 J mg/Kg - dry 0.195 0.722Indeno(1,2,3-cd)pyrene 1 03/14/23 00:38 V30753JMV
<0.209 mg/Kg - dry 0.209 0.722Isophorone 1 03/14/23 00:38 V30753JMV
<0.116 mg/Kg - dry 0.116 0.7221-Methylnaphthalene 1 03/14/23 00:38 V30753JMV
<0.109 mg/Kg - dry 0.109 0.7222-Methylnaphthalene 1 03/14/23 00:38 V30753JMV
<0.106 mg/Kg - dry 0.106 0.7222-Methylphenol 1 03/14/23 00:38 V30753JMV
<0.092 mg/Kg - dry 0.092 0.7223&4 Methylphenol 1 03/14/23 00:38 V30753JMV
<0.157 mg/Kg - dry 0.157 0.722Naphthalene 1 03/14/23 00:38 V30753JMV
<0.105 mg/Kg - dry 0.105 0.7222-Nitroaniline 1 03/14/23 00:38 V30753JMV
<0.131 mg/Kg - dry 0.131 0.7223-Nitroaniline 1 03/14/23 00:38 V30753JMV
<0.102 mg/Kg - dry 0.102 0.3614-Nitroaniline 1 03/14/23 00:38 V30753JMV
<0.126 mg/Kg - dry 0.126 0.361Nitrobenzene 1 03/14/23 00:38 V30753JMV
<0.097 mg/Kg - dry 0.097 0.7222-Nitrophenol 1 03/14/23 00:38 V30753JMV
<0.128 mg/Kg - dry 0.128 0.7224-Nitrophenol 1 03/14/23 00:38 V30753JMV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V30730 03/13/23 10:00
<0.287 mg/Kg - dry 0.287 0.722N-Nitrosodimethylamine 1 03/14/23 00:38 V30753JMV
<0.198 mg/Kg - dry 0.198 0.722N-Nitrosodiphenylamine 1 03/14/23 00:38 V30753JMV
<0.129 mg/Kg - dry 0.129 0.722N-Nitroso-di-n-propylamine 1 03/14/23 00:38 V30753JMV
<0.379 mg/Kg - dry 0.379 1.09Pentachlorophenol 1 03/14/23 00:38 V30753JMV
1.58 mg/Kg - dry 0.227 0.722Phenanthrene 1 03/14/23 00:38 V30753JMV
<0.122 mg/Kg - dry 0.122 0.722Phenol 1 03/14/23 00:38 V30753JMV
1.65 mg/Kg - dry 0.146 0.722Pyrene 1 03/14/23 00:38 V30753JMV
<0.086 mg/Kg - dry 0.086 0.361Pyridine 1 03/14/23 00:38 V30753JMV
<0.117 mg/Kg - dry 0.117 0.7221,2,4-Trichlorobenzene 1 03/14/23 00:38 V30753JMV
<0.105 mg/Kg - dry 0.105 0.7222,4,5-Trichlorophenol 1 03/14/23 00:38 V30753JMV
<0.105 mg/Kg - dry 0.105 0.7222,4,6-Trichlorophenol 1 03/14/23 00:38 V30753JMV
8270ESurrogate: Phenol-d5 76.3 Limits: 34-121%03/14/23 00:381 JMV
Surrogate: 2-Fluorobiphenyl 86.2 Limits: 44-115%03/14/23 00:381 JMV V30753
Surrogate: 2-Fluorophenol 78.4 Limits: 35-115%03/14/23 00:381 JMV V30753
Surrogate: Nitrobenzene-d5 75.4 Limits: 37-122%03/14/23 00:381 JMV V30753
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%03/14/23 00:381 JMV V30753
Surrogate: 2,4,6-Tribromophenol 85.6 Limits: 39-132%03/14/23 00:381 JMV V30753
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
<23.0 mg/Kg - dry 23.0 151Aliphatic C5-C8 (Adjusted)100 03/07/23 11:16
102 J mg/Kg - dry 86.2 151Aliphatics C9-C12 (Adjusted)1 03/07/23 11:16
<11.8 mg/Kg - dry 11.8 151Aromatic C9-C10 (Adjusted)100 03/07/23 11:16
<15.5 mg/Kg - dry 15.5 54.7Aromatic C11-C22 (Adjusted)1 03/13/23 14:56
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V30678 03/10/23 10:30
<10.1 mg/Kg - dry 10.1 54.7Aliphatic C9-C18 1 03/13/23 14:56 V30725AMP
<13.4 mg/Kg - dry 13.4 54.7Aliphatic C19-C36 1 03/13/23 14:56 V30725AMP
<15.5 mg/Kg - dry 15.5 54.7Aromatic C11-C22 1 03/13/23 14:56 V30725AMP
MADEP-EPHSurrogate: 2-Bromonaphthalene 82.0 Limits: 40-140%03/13/23 14:561 AMP
MADEP-EPHSurrogate: Chlorooctadecane 93.4 Limits: 40-140%03/13/23 14:561 AMP
MADEP-EPHSurrogate: OTP Surrogate 73.8 Limits: 40-140%03/13/23 14:561 AMP
Surrogate: 2-Fluorobiphenyl 88.3 Limits: 40-140%03/13/23 14:561 AMP V30725
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
<23.0 mg/Kg - dry 23.0 151Aliphatic C5-C8 100 03/07/23 11:16 V30530TBL
102 J mg/Kg - dry 86.2 151Aliphatic C9-C12 100 03/07/23 11:16 V30530TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-12-3'
90262 Matrix:
3/2/2023 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V30529 03/07/23 08:00
<11.8 mg/Kg - dry 11.8 151Aromatic C9-C10 100 03/07/23 11:16 V30530TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)90.6 Limits: 70-130%03/07/23 11:16100 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)83.3 Limits: 70-130%03/07/23 11:16100 TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 69
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28590
23-065-0026
00087
Geological Resources, Inc.
113 West Firetower Road, Suite G
William Regenthal
Winterville
Danyale Love
Project Manager
GRI #5685 Received : 03/06/2023
Former OM Mart
Report Date : 03/15/2023
Sample ID :
Lab No :
Sampled:SB-11-30'
90263 Matrix:
3/2/2023 11:53
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
37.0 %0.1%Clay 1 03/09/23 09:49 TextureEB
21.0 %0.1%Sand 1 03/09/23 09:49 TextureEB
42.0 %0.1%Silt 1 03/09/23 09:49 TextureEB
Clay LoamSoil Classification 1 03/09/23 09:49 TextureEB
0.17 %0.05Total Organic Carbon 1 03/14/23 15:45 WALK-BLACKAAB
100.0 %0.1% Passing 4 Mesh 1 03/13/23 12:45 SIEVE TESTVVP
100.0 %0.1% Passing 10 Mesh 1 03/13/23 12:45 SIEVEVVP
99.7 %0.1% Passing 20 Mesh 1 03/13/23 12:45 SIEVE TESTVVP
99.3 %0.1% Passing 40 Mesh 1 03/13/23 12:45 SIEVEVVP
98.6 %0.1% Passing 60 Mesh 1 03/13/23 12:45 SIEVEVVP
95.4 %0.1% Passing 100 Mesh 1 03/13/23 12:45 SIEVE TESTVVP
85.6 %0.1% Passing 200 Mesh 1 03/13/23 12:45 SIEVE TESTVVP
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30561
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30561 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/07/23 11:460.0200.002<0.002mg/KgAcetone
03/07/23 11:460.0200.001<0.001mg/KgAcrolein
03/07/23 11:460.0200.0008<0.0008mg/KgAcrylonitrile
03/07/23 11:460.0050.0006<0.0006mg/KgBenzene
03/07/23 11:460.0050.0005<0.0005mg/KgBromobenzene
03/07/23 11:460.0050.0008<0.0008mg/KgBromochloromethane
03/07/23 11:460.0050.001<0.001mg/KgBromodichloromethane
03/07/23 11:460.0050.001<0.001mg/KgBromoform
03/07/23 11:460.0100.001<0.001mg/KgBromomethane
03/07/23 11:460.0050.0005<0.0005mg/Kgn-Butylbenzene
03/07/23 11:460.0050.0006<0.0006mg/Kgsec-Butyl benzene
03/07/23 11:460.0050.0005<0.0005mg/Kgtert-Butyl benzene
03/07/23 11:460.0050.0006<0.0006mg/KgCarbon Disulfide
03/07/23 11:460.0050.001<0.001mg/KgCarbon Tetrachloride
03/07/23 11:460.0050.0007<0.0007mg/KgChlorobenzene
03/07/23 11:460.0050.0009<0.0009mg/KgChlorodibromomethane
03/07/23 11:460.0100.0009<0.0009mg/KgChloroethane
03/07/23 11:460.0050.001<0.001mg/KgChloroform
03/07/23 11:460.0100.0006<0.0006mg/KgChloromethane
03/07/23 11:460.0050.0005<0.0005mg/Kg2-Chlorotoluene
03/07/23 11:460.0050.0004<0.0004mg/Kg4-Chlorotoluene
03/07/23 11:460.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
03/07/23 11:460.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
03/07/23 11:460.0050.0006<0.0006mg/Kg1,2-Dibromoethane
03/07/23 11:460.0050.0006<0.0006mg/KgDibromomethane
03/07/23 11:460.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
03/07/23 11:460.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 1 of 19Date:03/15/2023 06:31 PM
Page 49 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30561
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30561 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/07/23 11:460.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
03/07/23 11:460.0100.001<0.001mg/KgDichlorodifluoromethane
03/07/23 11:460.0050.0008<0.0008mg/Kg1,1-Dichloroethane
03/07/23 11:460.0050.001<0.001mg/Kg1,2-Dichloroethane
03/07/23 11:460.0050.0007<0.0007mg/Kg1,1-Dichloroethene
03/07/23 11:460.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
03/07/23 11:460.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
03/07/23 11:460.0050.0004<0.0004mg/Kg1,2-Dichloropropane
03/07/23 11:460.0050.0006<0.0006mg/Kg1,3-Dichloropropane
03/07/23 11:460.0050.001<0.001mg/Kg2,2-Dichloropropane
03/07/23 11:460.0050.0008<0.0008mg/Kg1,1-Dichloropropene
03/07/23 11:460.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
03/07/23 11:460.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
03/07/23 11:460.0050.0006<0.0006mg/KgEthylbenzene
03/07/23 11:460.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
03/07/23 11:460.0100.0008<0.0008mg/KgHexachlorobutadiene
03/07/23 11:460.0100.0007<0.0007mg/Kgn-Hexane
03/07/23 11:460.0200.0006<0.0006mg/Kg2-Hexanone
03/07/23 11:460.0050.0005<0.0005mg/KgIsopropylbenzene
03/07/23 11:460.0050.001<0.001mg/Kg4-Isopropyl toluene
03/07/23 11:460.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
03/07/23 11:460.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
03/07/23 11:460.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
03/07/23 11:460.0100.001<0.001mg/KgMethylene Chloride
03/07/23 11:460.0100.0010<0.0010mg/KgNaphthalene
03/07/23 11:460.0050.0005<0.0005mg/Kgn-Propylbenzene
03/07/23 11:460.0050.001<0.001mg/KgStyrene
Page 2 of 19Date:03/15/2023 06:31 PM
Page 50 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30561
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30561 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/07/23 11:460.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
03/07/23 11:460.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
03/07/23 11:460.0050.0009<0.0009mg/KgTetrachloroethene
03/07/23 11:460.0050.0007<0.0007mg/KgToluene
03/07/23 11:460.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
03/07/23 11:460.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
03/07/23 11:460.0050.001<0.001mg/Kg1,1,1-Trichloroethane
03/07/23 11:460.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
03/07/23 11:460.0050.0009<0.0009mg/KgTrichloroethene
03/07/23 11:460.0100.002<0.002mg/KgTrichlorofluoromethane
03/07/23 11:460.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
03/07/23 11:460.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
03/07/23 11:460.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
03/07/23 11:460.0100.0005<0.0005mg/KgVinyl Acetate
03/07/23 11:460.0100.0005<0.0005mg/KgVinyl Chloride
03/07/23 11:460.0050.0005<0.0005mg/Kgo-Xylene
03/07/23 11:460.0100.001<0.001mg/Kgm,p-Xylene
03/07/23 11:464-Bromofluorobenzene (S)92.0 70-130
03/07/23 11:46Dibromofluoromethane (S)100 84-123
03/07/23 11:46Toluene-d8 (S)102 76-129
LCS-V30561 LCSD-V30561Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.085 85.088.10.0880.100mg/KgAcetone 29-198 3.5 20
0.092 92.296.50.0960.100mg/KgAcrolein 70-130 4.5 20
Page 3 of 19Date:03/15/2023 06:31 PM
Page 51 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30561
LCS-V30561 LCSD-V30561Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.598.70.0980.100mg/KgAcrylonitrile 65-134 1.2 20
0.049 99.81050.0520.050mg/KgBenzene 74-127 4.8 20
0.056 1131160.0580.050mg/KgBromobenzene 73-125 2.4 20
0.050 10099.40.0490.050mg/KgBromochloromethane 72-134 0.8 20
0.057 1161160.0570.050mg/KgBromodichloromethane 75-122 0.1 20
0.045 90.091.00.0450.050mg/KgBromoform 66-135 1.1 20
0.053 1071250.0620.050mg/KgBromomethane 20-180 15.5 20
0.046 93.41000.0500.050mg/Kgn-Butylbenzene 65-135 7.2 20
0.044 89.895.60.0470.050mg/Kgsec-Butyl benzene 66-131 6.2 20
0.046 92.81010.0500.050mg/Kgtert-Butyl benzene 67-132 8.2 20
0.048 97.01040.0520.050mg/KgCarbon Disulfide 61-129 7.1 20
0.047 94.81040.0520.050mg/KgCarbon Tetrachloride 64-143 9.6 20
0.050 1021080.0530.050mg/KgChlorobenzene 74-118 5.5 20
0.053 1081150.0570.050mg/KgChlorodibromomethane 73-122 6.2 20
0.044 88.091.80.0450.050mg/KgChloroethane 33-149 4.2 20
0.056 1121180.0580.050mg/KgChloroform 73-127 4.6 20
0.038 77.286.60.0430.050mg/KgChloromethane 45-143 11.4 20
0.049 98.01000.0500.050mg/Kg2-Chlorotoluene 67-124 2.4 20
0.049 98.01010.0500.050mg/Kg4-Chlorotoluene 71-126 2.6 20
0.039 79.083.20.0410.050mg/KgDi-Isopropyl Ether (DIPE)59-159 5.1 20
0.044 88.494.80.0470.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 6.9 20
0.052 1041090.0540.050mg/Kg1,2-Dibromoethane 70-132 4.5 20
0.052 1061080.0540.050mg/KgDibromomethane 74-133 2.2 20
0.044 88.691.00.0450.050mg/Kg1,2-Dichlorobenzene 72-123 2.6 20
0.043 87.690.40.0450.050mg/Kg1,3-Dichlorobenzene 71-120 3.1 20
0.041 83.886.00.0430.050mg/Kg1,4-Dichlorobenzene 71-123 2.5 20
Page 4 of 19Date:03/15/2023 06:31 PM
Page 52 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30561
LCS-V30561 LCSD-V30561Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.048 96.41050.0520.050mg/KgDichlorodifluoromethane 26-146 8.9 20
0.049 99.21060.0520.050mg/Kg1,1-Dichloroethane 74-127 6.2 20
0.050 1011020.0510.050mg/Kg1,2-Dichloroethane 68-128 1.1 20
0.042 85.491.40.0450.050mg/Kg1,1-Dichloroethene 67-149 6.7 20
0.047 94.896.80.0480.050mg/Kgcis-1,2-Dichloroethene 76-134 2.0 20
0.046 92.299.60.0490.050mg/Kgtrans-1,2-Dichloroethene 73-132 7.7 20
0.049 98.21030.0510.050mg/Kg1,2-Dichloropropane 73-130 5.1 20
0.055 1111140.0570.050mg/Kg1,3-Dichloropropane 75-124 3.3 20
0.053 1081160.0580.050mg/Kg2,2-Dichloropropane 50-142 7.6 20
0.050 1001090.0540.050mg/Kg1,1-Dichloropropene 71-130 8.7 20
0.056 1121190.0590.050mg/Kgcis-1,3-Dichloropropene 71-125 5.5 20
0.060 1201220.0610.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.6 20
0.047 95.41020.0510.050mg/KgEthylbenzene 74-128 6.6 20
0.097 97.498.70.0980.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.3 20
0.032 65.673.20.0360.050mg/KgHexachlorobutadiene 64-125 10.9 20
0.046 93.21060.0530.050mg/Kgn-Hexane 70-130 13.0 20
0.042 84.890.80.0450.050mg/Kg2-Hexanone 61-157 6.8 20
0.045 91.495.80.0470.050mg/KgIsopropylbenzene 68-126 4.7 20
0.046 93.099.40.0490.050mg/Kg4-Isopropyl toluene 68-129 6.6 20
0.048 96.292.60.0460.050mg/KgMethyl Ethyl Ketone (MEK)63-149 3.8 20
0.053 1071080.0530.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.7 20
0.045 91.892.00.0460.050mg/Kg4-Methyl-2-Pentanone 57-162 0.2 20
0.037 75.077.40.0380.050mg/KgMethylene Chloride 74-129 3.1 20
0.053 1071060.0530.050mg/KgNaphthalene 57-157 1.3 20
0.046 92.097.80.0480.050mg/Kgn-Propylbenzene 67-130 6.1 20
0.050 1011060.0530.050mg/KgStyrene 77-121 4.8 20
Page 5 of 19Date:03/15/2023 06:31 PM
Page 53 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V30563QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V30561
LCS-V30561 LCSD-V30561Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.047 95.81040.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 8.0 20
0.053 1081090.0540.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.4 20
0.042 85.892.00.0460.050mg/KgTetrachloroethene 68-130 6.9 20
0.049 98.61020.0510.050mg/KgToluene 71-129 3.5 20
0.043 87.687.20.0430.050mg/Kg1,2,3-Trichlorobenzene 68-130 0.4 20
0.047 94.294.80.0470.050mg/Kg1,2,4-Trichlorobenzene 66-125 0.6 20
0.051 1031090.0540.050mg/Kg1,1,1-Trichloroethane 67-131 5.4 20
0.052 1061080.0530.050mg/Kg1,1,2-Trichloroethane 70-133 1.6 20
0.049 99.01090.0540.050mg/KgTrichloroethene 75-133 9.6 20
0.042 85.298.00.0490.050mg/KgTrichlorofluoromethane 44-146 13.9 20
0.048 97.01060.0530.050mg/Kg1,2,3-Trichloropropane 60-137 9.0 20
0.047 94.699.00.0490.050mg/Kg1,2,4-Trimethylbenzene 69-129 4.5 20
0.046 93.098.00.0490.050mg/Kg1,3,5-Trimethylbenzene 69-128 5.2 20
0.061 1231270.0630.050mg/KgVinyl Acetate 60-140 3.6 20
0.041 83.692.00.0460.050mg/KgVinyl Chloride 48-147 9.5 20
0.050 1011070.0530.050mg/Kgo-Xylene 74-126 5.3 20
0.099 99.41070.1070.100mg/Kgm,p-Xylene 75-124 7.3 20
89.289.04-Bromofluorobenzene (S)70-130
99.8101Dibromofluoromethane (S)84-123
104103Toluene-d8 (S)76-129
Page 6 of 19Date:03/15/2023 06:31 PM
Page 54 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30730 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 22:000.6600.116<0.116mg/KgAcenaphthene
03/13/23 22:000.6600.105<0.105mg/KgAcenaphthylene
03/13/23 22:000.6600.152<0.152mg/KgAniline
03/13/23 22:000.6600.143<0.143mg/KgAnthracene
03/13/23 22:000.6600.139<0.139mg/KgBenzo(a)anthracene
03/13/23 22:000.6600.147<0.147mg/KgBenzo(a)pyrene
03/13/23 22:000.6600.146<0.146mg/KgBenzo(b)fluoranthene
03/13/23 22:000.6600.136<0.136mg/KgBenzo(g,h,i)perylene
03/13/23 22:000.6600.137<0.137mg/KgBenzo(k)fluoranthene
03/13/23 22:002.000.580<0.580mg/KgBenzoic Acid
03/13/23 22:000.6600.105<0.105mg/KgBenzyl alcohol
03/13/23 22:000.6600.118<0.118mg/KgBis(2-Chloroethoxy)methane
03/13/23 22:000.6600.107<0.107mg/KgBis(2-Chloroethyl)ether
03/13/23 22:000.3300.136<0.136mg/KgBis(2-Chloroisopropyl)ether
03/13/23 22:000.6600.120<0.120mg/KgBis(2-ethylhexyl)phthalate
03/13/23 22:000.6600.109<0.109mg/Kg4-Bromophenyl phenyl ether
03/13/23 22:000.3300.113<0.113mg/KgButyl benzyl phthalate
03/13/23 22:000.6600.092<0.092mg/Kg4-Chloro-3-methylphenol
03/13/23 22:000.3300.112<0.112mg/Kg4-Chloroaniline
03/13/23 22:000.6600.116<0.116mg/Kg2-Chloronaphthalene
03/13/23 22:000.6600.098<0.098mg/Kg2-Chlorophenol
03/13/23 22:001.000.126<0.126mg/Kg4-Chlorophenyl phenyl ether
03/13/23 22:000.6600.142<0.142mg/KgChrysene
03/13/23 22:000.6600.230<0.230mg/KgDibenz(a,h)anthracene
03/13/23 22:000.6600.119<0.119mg/KgDibenzofuran
03/13/23 22:000.6600.094<0.094mg/Kg1,2-Dichlorobenzene
03/13/23 22:000.6600.097<0.097mg/Kg1,3-Dichlorobenzene
Page 7 of 19Date:03/15/2023 06:31 PM
Page 55 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30730 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 22:000.3300.097<0.097mg/Kg1,4-Dichlorobenzene
03/13/23 22:000.6600.147<0.147mg/Kg3,3'-Dichlorobenzidine
03/13/23 22:000.6600.095<0.095mg/Kg2,4-Dichlorophenol
03/13/23 22:000.6600.180<0.180mg/KgDiethyl phthalate
03/13/23 22:000.6600.174<0.174mg/KgDimethyl phthalate
03/13/23 22:000.3300.108<0.108mg/Kg2,4-Dimethylphenol
03/13/23 22:000.6600.107<0.107mg/KgDi-n-butyl phthalate
03/13/23 22:001.500.240<0.240mg/Kg4,6-Dinitro-2-methylphenol
03/13/23 22:001.500.520<0.520mg/Kg2,4-Dinitrophenol
03/13/23 22:000.6600.096<0.096mg/Kg2,4-Dinitrotoluene
03/13/23 22:000.6600.108<0.108mg/Kg2,6-Dinitrotoluene
03/13/23 22:000.3300.143<0.143mg/KgDi-n-Octyl Phthalate
03/13/23 22:000.6600.123<0.123mg/KgFluoranthene
03/13/23 22:000.6600.128<0.128mg/KgFluorene
03/13/23 22:000.6600.106<0.106mg/KgHexachlorobenzene
03/13/23 22:000.6600.097<0.097mg/KgHexachlorobutadiene
03/13/23 22:000.6600.157<0.157mg/KgHexachlorocyclopentadiene
03/13/23 22:000.6600.079<0.079mg/KgHexachloroethane
03/13/23 22:000.6600.179<0.179mg/KgIndeno(1,2,3-cd)pyrene
03/13/23 22:000.6600.191<0.191mg/KgIsophorone
03/13/23 22:000.6600.106<0.106mg/Kg1-Methylnaphthalene
03/13/23 22:000.6600.100<0.100mg/Kg2-Methylnaphthalene
03/13/23 22:000.6600.097<0.097mg/Kg2-Methylphenol
03/13/23 22:000.6600.084<0.084mg/Kg3&4 Methylphenol
03/13/23 22:000.6600.144<0.144mg/KgNaphthalene
03/13/23 22:000.6600.096<0.096mg/Kg2-Nitroaniline
03/13/23 22:000.6600.120<0.120mg/Kg3-Nitroaniline
Page 8 of 19Date:03/15/2023 06:31 PM
Page 56 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30730 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 22:000.3300.093<0.093mg/Kg4-Nitroaniline
03/13/23 22:000.3300.116<0.116mg/KgNitrobenzene
03/13/23 22:000.6600.088<0.088mg/Kg2-Nitrophenol
03/13/23 22:000.6600.117<0.117mg/Kg4-Nitrophenol
03/13/23 22:000.6600.263<0.263mg/KgN-Nitrosodimethylamine
03/13/23 22:000.6600.181<0.181mg/KgN-Nitrosodiphenylamine
03/13/23 22:000.6600.118<0.118mg/KgN-Nitroso-di-n-propylamine
03/13/23 22:001.000.347<0.347mg/KgPentachlorophenol
03/13/23 22:000.6600.208<0.208mg/KgPhenanthrene
03/13/23 22:000.6600.112<0.112mg/KgPhenol
03/13/23 22:000.6600.134<0.134mg/KgPyrene
03/13/23 22:000.3300.079<0.079mg/KgPyridine
03/13/23 22:000.6600.107<0.107mg/Kg1,2,4-Trichlorobenzene
03/13/23 22:000.6600.096<0.096mg/Kg2,4,5-Trichlorophenol
03/13/23 22:000.6600.096<0.096mg/Kg2,4,6-Trichlorophenol
03/13/23 22:002-Fluorobiphenyl (S)93.4 44-115
03/13/23 22:002-Fluorophenol (S)91.5 35-115
03/13/23 22:00Nitrobenzene-d5 (S)85.0 37-122
03/13/23 22:004-Terphenyl-d14 (S)105 54-127
03/13/23 22:002,4,6-Tribromophenol (S)83.7 39-132
03/13/23 22:00Phenol-d5 (S)88.5 34-121
LCS-V30730Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
88.01.471.67mg/KgAcenaphthene 40-123
86.21.441.67mg/KgAcenaphthylene 32-132
Page 9 of 19Date:03/15/2023 06:31 PM
Page 57 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
LCS-V30730Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
222*3.711.67mg/KgAniline 12-197
97.61.631.67mg/KgAnthracene 47-123
99.41.661.67mg/KgBenzo(a)anthracene 49-126
1101.831.67mg/KgBenzo(a)pyrene 45-129
1011.681.67mg/KgBenzo(b)fluoranthene 45-132
95.81.601.67mg/KgBenzo(g,h,i)perylene 43-134
98.81.651.67mg/KgBenzo(k)fluoranthene 47-132
47.60.7961.67mg/KgBenzoic Acid 10-83
90.41.511.67mg/KgBenzyl alcohol 29-122
81.41.361.67mg/KgBis(2-Chloroethoxy)methane 36-121
74.21.241.67mg/KgBis(2-Chloroethyl)ether 31-120
85.61.431.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1111.861.67mg/KgBis(2-ethylhexyl)phthalate 51-133
94.61.581.67mg/Kg4-Bromophenyl phenyl ether 46-124
1141.911.67mg/KgButyl benzyl phthalate 48-132
79.01.321.67mg/Kg4-Chloro-3-methylphenol 45-122
74.81.251.67mg/Kg4-Chloroaniline 17-106
88.61.481.67mg/Kg2-Chloronaphthalene 41-114
82.61.381.67mg/Kg2-Chlorophenol 34-121
86.81.451.67mg/Kg4-Chlorophenyl phenyl ether 45-121
1021.711.67mg/KgChrysene 50-124
85.61.431.67mg/KgDibenz(a,h)anthracene 45-134
88.61.481.67mg/KgDibenzofuran 44-120
75.41.261.67mg/Kg1,2-Dichlorobenzene 33-117
74.21.241.67mg/Kg1,3-Dichlorobenzene 30-115
74.21.241.67mg/Kg1,4-Dichlorobenzene 31-115
71.21.191.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 10 of 19* QC Fail Date:03/15/2023 06:31 PM
Page 58 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
LCS-V30730Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
80.81.351.67mg/Kg2,4-Dichlorophenol 40-122
95.21.591.67mg/KgDiethyl phthalate 50-124
90.41.511.67mg/KgDimethyl phthalate 48-124
81.41.361.67mg/Kg2,4-Dimethylphenol 30-127
1101.831.67mg/KgDi-n-butyl phthalate 51-128
88.01.471.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
76.01.271.67mg/Kg2,4-Dinitrophenol 27-129
96.41.611.67mg/Kg2,4-Dinitrotoluene 48-126
94.01.571.67mg/Kg2,6-Dinitrotoluene 46-124
1081.801.67mg/KgDi-n-Octyl Phthalate 45-140
98.81.651.67mg/KgFluoranthene 50-127
91.01.521.67mg/KgFluorene 43-125
94.61.581.67mg/KgHexachlorobenzene 45-122
72.41.211.67mg/KgHexachlorobutadiene 32-123
71.21.191.67mg/KgHexachlorocyclopentadiene 32-117
73.01.221.67mg/KgHexachloroethane 28-117
94.61.581.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
80.21.341.67mg/KgIsophorone 30-122
77.81.301.67mg/Kg1-Methylnaphthalene 40-119
73.61.231.67mg/Kg2-Methylnaphthalene 38-122
86.21.441.67mg/Kg2-Methylphenol 32-122
76.61.281.67mg/Kg3&4 Methylphenol 34-119
75.41.261.67mg/KgNaphthalene 35-123
89.21.491.67mg/Kg2-Nitroaniline 44-127
86.81.451.67mg/Kg3-Nitroaniline 33-119
89.81.501.67mg/Kg4-Nitroaniline 63-147
75.41.261.67mg/KgNitrobenzene 34-122
Page 11 of 19Date:03/15/2023 06:31 PM
Page 59 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
LCS-V30730Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
76.01.271.67mg/Kg2-Nitrophenol 36-123
1262.101.67mg/Kg4-Nitrophenol 30-132
57.30.9571.67mg/KgN-Nitrosodimethylamine 10-146
1191.981.67mg/KgN-Nitrosodiphenylamine 38-127
81.41.361.67mg/KgN-Nitroso-di-n-propylamine 36-120
97.01.621.67mg/KgPentachlorophenol 25-133
98.21.641.67mg/KgPhenanthrene 50-121
90.41.511.67mg/KgPhenol 34-121
1051.751.67mg/KgPyrene 47-127
40.20.6731.67mg/KgPyridine 10-80
73.01.221.67mg/Kg1,2,4-Trichlorobenzene 34-118
87.41.461.67mg/Kg2,4,5-Trichlorophenol 41-124
86.21.441.67mg/Kg2,4,6-Trichlorophenol 39-126
90.42-Fluorobiphenyl (S)44-115
90.32-Fluorophenol (S)35-115
74.8Nitrobenzene-d5 (S)37-122
1104-Terphenyl-d14 (S)54-127
91.82,4,6-Tribromophenol (S)39-132
88.2Phenol-d5 (S)34-121
V 89932-MS-V30730 V 89932-MSD-V30730Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.43 85.61.281.671.67<0.116mg/KgAcenaphthene 76.6 40-123 11.0 20
1.42 85.01.271.671.67<0.105mg/KgAcenaphthylene 76.0 32-132 11.1 20
3.04 1822.921.671.67<0.152mg/KgAniline 175 12-197 4.0 20
Page 12 of 19Date:03/15/2023 06:31 PM
Page 60 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
V 89932-MS-V30730 V 89932-MSD-V30730Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.54 92.21.411.671.67<0.143mg/KgAnthracene 84.4 47-123 8.8 20
1.47 88.01.391.671.67<0.139mg/KgBenzo(a)anthracene 83.2 49-126 5.5 20
1.62 97.01.501.671.67<0.147mg/KgBenzo(a)pyrene 89.8 45-129 7.6 20
1.52 91.01.381.671.67<0.146mg/KgBenzo(b)fluoranthene 82.6 45-132 9.6 20
1.41 84.41.331.671.67<0.136mg/KgBenzo(g,h,i)perylene 79.6 43-134 5.8 20
1.41 84.41.371.671.67<0.137mg/KgBenzo(k)fluoranthene 82.0 47-132 2.8 20
1.31 78.41.201.671.67<0.580mg/KgBenzoic Acid 71.8 10-83 8.7 20
1.43 85.61.271.671.67<0.105mg/KgBenzyl alcohol 76.0 29-122 11.8 20
1.29 77.21.151.671.67<0.118mg/KgBis(2-Chloroethoxy)methane 68.8 36-121 11.4 20
1.33 79.61.061.671.67<0.107mg/KgBis(2-Chloroethyl)ether 63.4 31-120 22.5*20
1.36 81.41.211.671.67<0.136mg/KgBis(2-Chloroisopropyl)ether 72.4 33-131 11.6 20
1.63 97.61.541.671.67<0.120mg/KgBis(2-ethylhexyl)phthalate 92.2 51-133 5.6 20
1.46 87.41.291.671.67<0.109mg/Kg4-Bromophenyl phenyl ether 77.2 46-124 12.3 20
1.65 98.81.571.671.67<0.113mg/KgButyl benzyl phthalate 94.0 48-132 4.9 20
1.23 73.61.131.671.67<0.092mg/Kg4-Chloro-3-methylphenol 67.6 45-122 8.4 20
1.15 68.81.031.671.67<0.112mg/Kg4-Chloroaniline 61.6 17-106 11.0 20
1.43 85.61.271.671.67<0.116mg/Kg2-Chloronaphthalene 76.0 41-114 11.8 20
1.35 80.81.191.671.67<0.098mg/Kg2-Chlorophenol 71.2 34-121 12.5 20
1.40 83.81.291.671.67<0.126mg/Kg4-Chlorophenyl phenyl ether 77.2 45-121 8.1 20
1.52 91.01.441.671.67<0.142mg/KgChrysene 86.2 50-124 5.4 20
1.27 76.01.191.671.67<0.230mg/KgDibenz(a,h)anthracene 71.2 45-134 6.5 20
1.43 85.61.351.671.67<0.119mg/KgDibenzofuran 80.8 44-120 5.7 20
1.24 74.21.081.671.67<0.094mg/Kg1,2-Dichlorobenzene 64.6 33-117 13.7 20
1.20 71.81.081.671.67<0.097mg/Kg1,3-Dichlorobenzene 64.6 30-115 10.5 20
1.19 71.21.071.671.67<0.097mg/Kg1,4-Dichlorobenzene 64.0 31-115 10.6 20
0.930 55.60.9041.671.67<0.147mg/Kg3,3'-Dichlorobenzidine 54.1 22-121 2.8 20
Page 13 of 19* QC Fail Date:03/15/2023 06:31 PM
Page 61 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
V 89932-MS-V30730 V 89932-MSD-V30730Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.28 76.61.151.671.67<0.095mg/Kg2,4-Dichlorophenol 68.8 40-122 10.6 20
1.45 86.81.361.671.67<0.180mg/KgDiethyl phthalate 81.4 50-124 6.4 20
1.42 85.01.301.671.67<0.174mg/KgDimethyl phthalate 77.8 48-124 8.8 30
1.37 82.01.221.671.67<0.108mg/Kg2,4-Dimethylphenol 73.0 30-127 11.5 20
1.62 97.01.501.671.67<0.107mg/KgDi-n-butyl phthalate 89.8 51-128 7.6 20
1.46 87.41.371.671.67<0.240mg/Kg4,6-Dinitro-2-methylphenol 82.0 29-132 6.3 20
1.53 91.61.381.671.67<0.520mg/Kg2,4-Dinitrophenol 82.6 27-129 10.3 20
1.49 89.21.371.671.67<0.096mg/Kg2,4-Dinitrotoluene 82.0 48-126 8.3 20
1.47 88.01.341.671.67<0.108mg/Kg2,6-Dinitrotoluene 80.2 46-124 9.2 20
1.55 92.81.451.671.67<0.143mg/KgDi-n-Octyl Phthalate 86.8 45-140 6.6 20
1.50 89.81.371.671.67<0.123mg/KgFluoranthene 82.0 50-127 9.0 20
1.48 88.61.341.671.67<0.128mg/KgFluorene 80.2 43-125 9.9 20
1.47 88.01.321.671.67<0.106mg/KgHexachlorobenzene 79.0 45-122 10.7 20
1.20 71.81.071.671.67<0.097mg/KgHexachlorobutadiene 64.0 32-123 11.4 20
1.21 72.41.041.671.67<0.157mg/KgHexachlorocyclopentadiene 62.2 32-117 15.1 20
1.25 74.81.091.671.67<0.079mg/KgHexachloroethane 65.2 28-117 13.6 20
1.38 82.61.281.671.67<0.179mg/KgIndeno(1,2,3-cd)pyrene 76.6 45-133 7.5 20
1.26 75.41.121.671.67<0.191mg/KgIsophorone 67.0 30-122 11.7 20
1.28 76.61.151.671.67<0.106mg/Kg1-Methylnaphthalene 68.8 40-119 10.6 20
1.22 73.01.111.671.67<0.100mg/Kg2-Methylnaphthalene 66.4 38-122 9.4 20
1.37 82.01.201.671.67<0.097mg/Kg2-Methylphenol 71.8 32-122 13.2 20
1.23 73.61.081.671.67<0.084mg/Kg3&4 Methylphenol 64.6 34-119 12.9 20
1.23 73.61.091.671.67<0.144mg/KgNaphthalene 65.2 35-123 12.0 20
1.44 86.21.301.671.67<0.096mg/Kg2-Nitroaniline 77.8 44-127 10.2 20
1.28 76.61.181.671.67<0.120mg/Kg3-Nitroaniline 70.6 33-119 8.1 20
1.43 85.61.321.671.67<0.093mg/Kg4-Nitroaniline 79.0 63-147 8.0 20
Page 14 of 19Date:03/15/2023 06:31 PM
Page 62 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V30753QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V30730
V 89932-MS-V30730 V 89932-MSD-V30730Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.21 72.41.111.671.67<0.116mg/KgNitrobenzene 66.4 34-122 8.6 20
1.17 70.01.091.671.67<0.088mg/Kg2-Nitrophenol 65.2 32-123 7.0 20
1.63 97.61.741.671.67<0.117mg/Kg4-Nitrophenol 104 30-132 6.5 20
0.799 47.80.7351.671.67<0.263mg/KgN-Nitrosodimethylamine 44.0 10-146 8.3 30
1.96 1171.761.671.67<0.181mg/KgN-Nitrosodiphenylamine 105 38-127 10.7 20
1.32 79.01.121.671.67<0.118mg/KgN-Nitroso-di-n-propylamine 67.0 36-120 16.3 20
1.57 94.01.451.671.67<0.347mg/KgPentachlorophenol 86.8 25-133 7.9 20
1.54 92.21.401.671.67<0.208mg/KgPhenanthrene 83.8 50-121 9.5 20
1.43 85.61.251.671.67<0.112mg/KgPhenol 74.8 34-121 13.4 20
1.55 92.81.451.671.67<0.134mg/KgPyrene 86.8 47-127 6.6 20
0.576 34.40.5241.671.67<0.079mg/KgPyridine 31.3 10-80 9.4 20
1.17 70.01.071.671.67<0.107mg/Kg1,2,4-Trichlorobenzene 64.0 34-118 8.9 20
1.38 82.61.281.671.67<0.096mg/Kg2,4,5-Trichlorophenol 76.6 41-124 7.5 20
1.41 84.41.251.671.67<0.096mg/Kg2,4,6-Trichlorophenol 74.8 39-126 12.0 20
87.42-Fluorobiphenyl (S)76.6 44-115
84.92-Fluorophenol (S)74.2 35-115
71.2Nitrobenzene-d5 (S)62.2 37-122
93.44-Terphenyl-d14 (S)87.4 54-127
86.12,4,6-Tribromophenol (S)78.4 39-132
81.0Phenol-d5 (S)70.9 34-121
Page 15 of 19Date:03/15/2023 06:31 PM
Page 63 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V30725QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V30678
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30678 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/13/23 11:1850.09.20<9.20mg/KgAliphatic C9-C18
03/13/23 11:1850.012.2<12.2mg/KgAliphatic C19-C36
03/13/23 11:1850.014.2<14.2mg/KgAromatic C11-C22
03/13/23 11:182-Fluorobiphenyl (S)91.2 40-140
03/13/23 11:182-Bromonaphthalene (S)81.5 40-140
03/13/23 11:18Chlorooctadecane (S)91.1 40-140
03/13/23 11:18OTP Surrogate (S)79.6 40-140
LCS-V30678 LCSD-V30678Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
45.7 76.166.539.960.0mg/KgAliphatic C9-C18 40-140 13.5 50
79.2 99.097.177.780.0mg/KgAliphatic C19-C36 40-140 1.9 50
158 92.9122208170mg/KgAromatic C11-C22 40-140 27.3 50
87.01132-Fluorobiphenyl (S)40-140
75.01032-Bromonaphthalene (S)40-140
96.192.0Chlorooctadecane (S)40-140
76.894.1OTP Surrogate (S)40-140
Page 16 of 19Date:03/15/2023 06:31 PM
Page 64 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V30530QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V30529
Associated Lab Samples: 90259, 90260, 90261, 90262
LRB-V30529 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
03/07/23 10:048.001.22<1.22mg/KgAliphatic C5-C8
03/07/23 10:048.004.56<4.56mg/KgAliphatic C9-C12
03/07/23 10:048.000.624<0.624mg/KgAromatic C9-C10
03/07/23 10:042,5-Dibromotoluene (FID) (S)93.3 70-130
03/07/23 10:042,5-Dibromotoluene (PID) (S)94.3 70-130
LCS-V30529 LCSD-V30529Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
31.0 96.899.031.732.0mg/KgAliphatic C5-C8 70-130 2.2 50
38.4 12012339.232.0mg/KgAliphatic C9-C12 70-130 2.0 50
11.7 10911312.110.7mg/KgAromatic C9-C10 70-130 3.3 50
91.491.32,5-Dibromotoluene (FID) (S)70-130
82.291.02,5-Dibromotoluene (PID) (S)70-130
Page 17 of 19Date:03/15/2023 06:31 PM
Page 65 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
Dry Weight Determination
SW-DRYWT
V30557QC Analytical Batch:
Analysis Method:
Analysis Description:
V 90196-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 06/07/23 16:200.026.926.9%Moisture
V 90259-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 06/07/23 16:202.810.310.6%Moisture
Page 18 of 19Date:03/15/2023 06:31 PM
Page 66 of 69
Quality Control Data
23-065-0026Report No:
Project Description:
Client ID:Geological Resources, Inc.
Former OM Mart
Total Organic Carbon - Walkley Black
WALK-BLACK
L669487QC Analytical Batch:
Analysis Method:
Analysis Description:
Associated Lab Samples: 90263
LRB Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
03/14/23 15:450.05< 0.05%Total Organic Carbon
V 90263-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 03/14/23 15:450.00.170.17%Total Organic Carbon
Page 19 of 19Date:03/15/2023 06:31 PM
Page 67 of 69
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-065-0026
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT15 0.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angelo Norvell Date & Time:03/06/2023 18:17:37
Special precautions or instructions included?
Comments:
Page 68 of 69
Page 69 of 69

APPENDIX D
Boring Logs
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-1 Date Drilled 3/01/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 3.0 red/brown dry none
2
53.3 21 14.6 3.0 30.0 golden brown dry present
4
6 0.0
8
0.2
10

12 52.3 <10 <2
14
30.8
16

18 17.8
20
39.3 <10 <2
22

24 11.3
26
10.5
28

30 2.6
32
34

36
38
40
Boring terminated at 30'
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Asphalt
Hard-packed silt
Silt
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-2 Date Drilled 3/01/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 36.0 golden brown dry present
2
0.8 <10 23.8
4
6 0.1
8
0.4
10

12 0.9 <10 <2
14
0.6
16

18 1.9
20
7.8
22

24 13.9
26
10.9
28

30 18.1 <10 2.2
32
4.4
34

36 10.4
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Gravel
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-3 Date Drilled 3/01/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 36.0 golden brown dry/moist none
2
0.2
4
6 0.6
8
2.7 <10 <2
10

12 1.3 11 42.8
14
1.4
16

18 1.9
20
3.4
22

24 2.5
26
5.1
28

30 3.1
32
15.0 <20 5.2
34

36 4.2
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Asphalt
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-4 Date Drilled 3/01/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 36.0 golden brown dry/moist none
2
0.0
4
6 2.2 <10 2.0
8
1.6
10

12 1.1 <10 <2
14
8.9
16

18 10.4
20
14.9
22

24 3.0
26
7.2
28

30 9.9
32
5.0
34

36 27.8 <10 2.2
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Asphalt
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-5 Date Drilled 3/01/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 9.0 red/brown moist present
2
0.8
4
6 2.4
8
10.8 <10 5.2 9.0 36.0 golden brown moist present
10

12 8.5 24.8 4.8
14
51.7
16

18 69.4
20
13.4
22

24 65.0 <20 2.2
26
11.7
28

30 26.8
32
50.4
34

36 6.1
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Asphalt
Clayey silt
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-6 Date Drilled 3/01/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 7.0 orange/brown dry present
2
2.2
4
6 12.0 10.4 13.0
7.0 36.0 golden brown moist present
8
9.0
10

12 7.4 <10 12.4
14
42.1
16

18 264.0 38 13.2
20
103.3
22

24 25.4
26
35.5
28

30 62.8
32
27.2
34

36 2.6
38
40
Clayey silt
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Asphalt
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-7 Date Drilled 3/01/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 5.0 orange/brown dry none
2
0.8
4
5.0 17.0 golden brown dry none
6 1.5
8
3.2 <10 2.2
10

12 12.6 23.6 <2
14
228.7 13.2 11.0
16
17.0 36.0 red/brown moist none
18 77.4
20
48.6
22

24 97.7
26
61.3
28

30 21.4
32
17.9
34

36 10.5
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Asphalt
Silt
Silt
Silty clay
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-8 Date Drilled 3/02/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 5.0 golden brown moist none
2
0.1
4
5.0 7.0 orange moist none
6 0.1
7.0 11.0 light tan moist none
8
0.9 <10 <2
10
11.0 36.0 golden brown moist present
12 1.8 10.4 5.8
14
1.3
16

18 2.1
20
14.5
22

24 292.1 <10 9.2
26
60.1
28

30 25.1
32
25.7
34

36 11.1
38
40
Sand
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Topsoil/gravel
Sand
Silt
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-9 Date Drilled 3/02/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 4.0 black/brown dry none
2
3.0
4 4.0 36.0 golden brown moist none
6 3.1
8
3.5 <10 4.4
10

12 3.9 <10 <2
14
6.7
16

18 4.8
20
5.8
22

24 10.9
26
19.4
28

30 12.8
32
28.6 10.4 2
34

36 4.3
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Gravel/asphalt
Sand
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-10 Date Drilled 3/02/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 2.0 black dry none
2 2.0 8.0 orange/brown dry none
0.3
4
6 1.2
8 8.0 36.0 golden brown dry present
2.4 <10 <2
10

12 1.8 <10 4.2
14
2.0
16

18 2.5
20
3.4
22

24 4.7 <10 4.2
26
3.3
28

30 2.6
32
3.2
34

36 0.6
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Gravel/asphalt
Sand
Silt
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-11 Date Drilled 3/02/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 8.0 brown moist none
2
0.8 <10 4.6
4
6 0.3
8 8.0 36.0 red/brown moist none
0.0
10

12 0.0
14
0.0
16

18 0.0
20
1.0 16.4 <2
22

24 0.0
26
0.4
28

30 0.0
32
0.0
34

36 0.0
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Gravel/asphalt
Silty clay
Clayey silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-12 Date Drilled 3/02/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 36.0 golden brown dry none
2
0.9 <10 166.4
4
6 0.8
8
0.2
10

12 0.4 <10 7.8
14
0.8 <10 8.4
16

18 0.1
20
0.5
22

24 0.5
26
0.0
28

30 0.1
32
0.2
34

36 0.0
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Topsoil
Silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-13 Date Drilled 3/02/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 27.0 light brown dry none
2
0.2
4
6 0.3 <10 2.6
8
0.2
10

12 0.4 <10 <2
14
0.2
16

18 2.0
20
34.9
22

24 16.7
26
16.3 27.0 36.0 golden brown wet present
28

30 74.8 13.8 7
32
10.4
34

36 1.9
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Topsoil
Silt
Clayey silt
Boring terminated at 36'.
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
Project Former OM Mart Project #5685
Address 113 West Main Street, Biscoe, NC
Boring Number SB-14 Date Drilled 3/02/2023
Sample Method Grab Drilling Method 6.25" Hollow Stem Augers
Completion DetailsDirect push, borehole abandoned with Bentonite, Capped with concrete
Driller Matt Steele License #4548-A Log By Xavier Farmer
Boring PID GRO DRO GW USCS
Depth ppm ppm ppm depth class From To Color Moisture Odor
0 0.0 0.5 dry none
0.5 17.0 orange/brown dry none
2
1.9 <10 4.8
4
6 0.6
8
0.4
10

12 0.5 <10 <2
14
0.5
16
17.0 36.0 golden brown moist present
18 0.5
20
0.4
22

24 0.4
26
0.3
28

30 0.5 <10 <2
32
0.4
34

36 0.2
38
40
SUBSURFACE LOG
Depth (feet)LITHOLOGY
Soil Type
Topsoil
Silt
Silty clay
Boring terminated at 36'.