FA-2935_29175_CA_MRP_20131209

EXECUTIVE SUMMARY

Han-Dee Hugo #5 is located at 1210 North Main Street, in Bladenboro, Bladen County, North Carolina.
The site is currently an active petroleum retail facility and convenience store. Three 8,000-gallon
gasoline USTs, one 8,000-gallon fuel oil, one 8,000-gallon diesel, and one 2,000-gallon kerosene USTs
are in use at the site.

A release at the site was discovered during Environmental Site Assessment activities. Four shallow
monitoring wells (MW-1 through MW-4) and one deep monitoring well (TW-1) were installed during
Limited Site Assessment activities. Contaminated soil was discovered during site renovations in May and
June 2012. A total of 2,162.49 tons of soil was removed from the site. GRI submitted an Initial Action
Abatement Report on August 27, 2012 and a Comprehensive Site Assessment in May 2013.

The site is ranked as high risk because one potable water supply well (WSW-7) was identified within
1,000-radius of the site. Another WSW was identified within a 1,500-foot radius of the subject site.
Three irrigation wells (WSW-1, WSW-2, and WSW-5) were confirmed within 1,000 feet of the site.
There are no water supply wells within 250 feet of the site. Municipal water is available to all properties
in the area. A well abandonment agreement was sent to the owner of WSW-7 who denied abandoning her
well and connecting to municipal water.

A total of 11,028 gallons of affected ground water was recovered during the MMPE event conducted on
monitoring wells MW-4R and MW-11 from September 23 to September 27, 2013. Based on mass-
removal calculations an additional 1,113.93 pounds or 181.07 gallons of vapor phase hydrocarbons were
removed.

On October 28, 2013, fourteen monitoring wells were gauged, purged, and sampled. Free product was
not measured in any monitoring well during the October 2013 sampling event. Concentrations of
individual BTEX constituents, MTBE, naphthalene, and/or 1,2,4 trimethylbenzene that exceeded the
maximum allowable concentrations specified in T15A NCAC 2L.0202 were reported in the ground water
samples. Detectable concentrations of benzene and MBTE exceeded the gross contaminant levels in the
ground water sample collected from MW-11. GRI recommends continued MMPE events to remove
contaminated ground water until the risk can be lowered.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION ....................................................................... 1
2.0 CURRENT SITE ASSESSMENT ................................................................................................ 1
3.0 FREE PRODUCT RECOVERY .................................................................................................. 2
4.0 GROUND WATER SAMPLING ACTIVITIES ......................................................................... 3
5.0 GROUND WATER QUALITY .................................................................................................... 3
6.0 CONCLUSIONS AND RECOMMENDATIONS ....................................................................... 4
7.0 LIMITATIONS .............................................................................................................................. 4

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map Figure 4: Water Table Surface Map
Figure 5: Water Quality Map
Figure 6: Benzene Isoconcentration Map
TABLES
Table 1: Well Construction and Gauging Information
Table 2: Free Product Recovery Results Table 3: Free Product Recovery Event Information Table 4: Free Product Recovery Cost Summary
Table 5: Summary of Ground Water Sample Analytical Results

APPENDIX
Appendix A: Well Abandonment Agreement
Appendix B: AES MMPE Report
Appendix C: Laboratory Report – Ground Water Samples

1

1.0 SITE HISTORY AND CHARACTERIZATION
Han-Dee Hugo #5 is located at 1210 North Main Street, in Bladenboro, Bladen County, North Carolina
(Figure 1). The site is currently an active petroleum retail facility and convenience store. Three 8,000-
gallon gasoline, one 8,000-gallon fuel oil, one 8,000-gallon diesel, and one 2,000-gallon kerosene USTs
are in use at the site.

According to the Phase II Limited Site Assessment (LSA) Report (April 25, 2005) submitted by CBM
Environmental Services, Inc., a release at the site was discovered during Environmental Site Assessment
activities. Four shallow monitoring wells (MW-1 through MW-4) and one deep monitoring well (TW-1)
were installed during LSA activities. Contaminated soil was discovered during site renovations in May
and June 2012. A total of 2,162.49 tons of soil was removed from the site. GRI submitted an Initial
Action Abatement Report on August 27, 2012. In December 2012 and January 2013, during the
Comprehensive Site Assessment (CSA), monitoring wells MW-1R, MW-2R, MW-4R, MW-5 through
MW-13, and TW-1R were installed. The CSA report was submitted by GRI in May 2013.

The site is ranked as high risk because one potable water supply well (WSW-7) was identified within
1,000-radius of the site. Another WSW was identified within a 1,500-foot radius of the subject site.
Three irrigation wells (WSW-1, WSW-2, and WSW-5) were confirmed within 1,000 feet of the site.
There are no water supply wells within 250 feet of the site. Municipal water is available to all properties
in the area. In October 2013, a well abandonment agreement was sent to the owner of WSW-7 who
denied abandoning her well and connecting to municipal water. A copy of the agreement is included in
Appendix A. A Site Vicinity Map showing the locations of water supply wells is included as Figure 2.
A Site Map showing the locations of the monitoring wells and the structures on-site and on surrounding
properties has been included as Figure 3.

2.0 CURRENT SITE ASSESSMENT
The purpose of this report is to present the results of Mobile Multi-Phase Extraction (MMPE) and
sampling activities conducted at the site. The activities were conducted in accordance with GRI Proposal
Number 13-328 which was submitted to NCDENR on July 11, 2013, and approved as Task Authorization
Number 29175-4 on July 30, 2013. The current scope of work includes: MMPE event and sampling
event.

2

3.0 FREE PRODUCT RECOVERY
An MMPE event was conducted at the site by Advanced Environmental Services, Inc. under the
supervision of GRI beginning on September 23 and ending on September 27, 2013. The MMPE
equipment included a liquid ring pump, 8,500-gallon capacity tankers, flexible vacuum hoses, 1-inch
diameter PVC stinger pipes and associated couplings and pipe fittings to manifold monitoring wells
simultaneously. The MMPE system was rated at 21 in./Hg at 130 cfm.

On September 23, 2013, monitoring wells MW-1R, MW-2R, MW-4R, and MW-11 were gauged. Free
product was not observed in any of the wells prior to the start of the event. The stinger pipes were set at
depths ranging from 5 to 10 feet in the extraction wells throughout the MMPE event.

Monitoring well MW-4R and MW-11 were vacuumed continuously during the 96 hours. Airflow was
reduced by 50% in monitoring well, MW-4R due to short-circuiting. Magnehelic gauges were connected
to monitoring wells MW-1R and MW-2R to monitor vacuum influence in the wells during extraction. No
measurable vacuum influence was observed at any monitoring point. The field parameters collected
during the initial ten hours have been tabulated and are included in Appendix B.

During the event, measurements of relative humidity, temperature, vacuum, exhaust velocity and off-gas
concentrations were recorded at the discharge stack either two or three times per 24-hour period. Vacuum
at the extraction wells ranged from 6.0 to 14.0 in./Hg. System vacuum ranged from 12.0 to 15.0 in./Hg.
Exhaust velocities ranged from 3,200 to 3,500 fpm. Temperatures ranged from 95.0 to 100.0 F and
humidity was 99 percent. Total VOC off-gas concentrations ranged from 52,000 to 100,000 ppm during
the event. No free product was reported in the extraction wells (MW-4R and MW-11) or in the
observation wells (MW-1R and MW-2R) at the end of the event. A summary of the gauging data
obtained prior to and at the conclusion of the MMPE event is presented in Table 1. A copy of the
Advanced MMPE Report has been included as Appendix B.

The results of the MMPE event indicate that a total of 11,028 gallons of fluids were removed during the
event. No measurable amount of free product was observed in the tanker at the end of the event. Based
on 96 hours of operation, the average fluid recovery rate was 114.87 gallons per hour. Based on mass-
removal calculations an additional 1,113.93 pounds or 181.07 gallons of vapor phase hydrocarbons were
removed. Based on 96 hours of operation, an average of 1.89 gallons of vapor phase free product was
removed per hour by the MMPE system. Summaries of free product recovery event data have been

3

included in Tables 2 through 4. At the conclusion of the MMPE event, all wastewater was transported to
a licensed facility for disposal.

4.0 GROUND WATER SAMPLING ACTIVITIES
4.1 Site Hydrogeology
On October 28, 2013, monitoring wells MW-1R, MW-2R, MW-3, MW-4R, MW-5 through MW-13 and
TW-1R were gauged. No free product was observed in any of the monitoring wells.

The depths to ground water in the Type II monitoring wells during the October 28, 2013, sampling event
ranged from 5.14 to 8.44 feet below the tops of well casings. Ground water elevations in the Type II
monitoring wells relative to a temporary benchmark with an assumed datum of 100.00 feet ranged from
93.75 to 95.11 feet. Based on these data, ground water flow across the site was generally toward the west
of the site. The average horizontal hydraulic gradient at the site during the October 28, 2013, sampling
event was less than 0.01 feet per foot. The locations of the monitoring wells are shown on Figure 3. A
Water Table Surface Map based on data obtained from the Type II wells in October 2013 is included as
Figure 4. A summary of well construction and gauging information is presented in Table 1.

4.2 Ground Water Sampling
On October 28, 2013, monitoring wells MW-1R, MW-2R, MW-3, MW-4R, MW-5 through MW-13 and
TW-1R were gauged, purged, and/or sampled. No free product was observed in any of the monitoring
wells. Laboratory analyses were performed on the ground water samples collected from the monitoring
wells for volatile organic compounds using EPA Method 6200B.

5.0 GROUND WATER QUALITY
Concentrations of individual BTEX constituents, MTBE, naphthalene, and/or 1,2,4 trimethylbenzene that
exceeded the maximum allowable concentrations (MACs) specified in T15A NCAC 2L.0202 were
reported in the ground water samples collected from MW-1R, MW-2R, MW-3, MW-4R, MW-7 and
MW-11. Detectable concentrations of benzene and MBTE exceeded the gross contamination levels
(GCLs) in the ground water sample collected from MW-11. A Ground Water Quality Map based on data
from the October 28, 2013, sampling event has been included as Figure 5. An inferred isoconcentration
map for benzene is included as Figure 6. A summary of ground water sampling analytical results is
presented in Table 5. A complete laboratory report has been included in Appendix C.

4

6.0 CONCLUSIONS AND RECOMMENDATIONS
• A total of 11,028 gallons of affected ground water was recovered during the MMPE event
conducted on monitoring wells MW-4R and MW-11 from September 23 to September 27, 2013.
No free product was reported in the extraction wells (MW-4R and MW-11) or in the observation
wells (MW-1R and MW-2R) at the end of the event. The average fluid recovery rate was 114.87
gallons per hour. Based on mass-removal calculations an additional 1,113.93 pounds or 181.07
gallons of vapor phase hydrocarbons were removed at an average rate of 1.89 gallons per hour.
• Concentrations of individual BTEX constituents, MTBE, naphthalene, and/or 1,2,4
trimethylbenzene that exceeded the MACs were reported in the ground water samples collected
from MW-1R, MW-2R, MW-3, MW-4R, MW-7 and MW-11. Detectable concentrations of
benzene and MBTE exceeded the GCLs in the ground water sample collected from MW-11.
• MMPE events and semi-annual ground water sampling events should be conducted to remove
contaminated ground water until the risk can be lowered.

7.0 LIMITATIONS
This report has been prepared for the exclusive use of Sampson-Bladen Oil Company, Inc. for specific
application to the referenced site in Bladen County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by the NCDENR and with resources adequate
only for that scope of work. Our findings have been developed in accordance with generally accepted
standards of geology and hydrogeology practices in the State of North Carolina, available information,
and our professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES

TABLES
Date: 11/7/13
04/04/05 3.35 ---96.65
05/30/12 3.10 ---96.90
01/04/13 2.30 ---97.70
09/23/13 4.49 ---95.51
09/27/13 4.90 ---95.10
10/28/13 5.90 ---94.10
04/04/05 6.35 ---97.03
05/30/12 NM ---NM
01/04/13 5.68 ---96.53
09/23/13 6.46 ---95.75
09/27/13 6.80 ---95.41
10/28/13 8.03 ---94.18
04/04/05 5.70 ---97.45
05/30/12 5.46 ---97.69
01/04/13 5.08 ---96.78
10/28/13 6.75 ---95.11
04/04/05 5.68 ---96.71
05/30/12 4.60 ---97.79
01/04/13 4.74 ---96.86
09/23/13 5.38 ----5.38 Before MMPE
09/27/13 ---0.00 After MMPE
10/28/13 6.96 ---94.64
01/04/13 4.28 ---97.27
10/28/13 7.73 ---93.82
01/04/13 5.28 ---96.55
10/28/13 7.89 ---93.94
01/04/13 2.92 ---97.08
10/28/13 5.88 ---94.12
01/04/13 3.24 ---97.02
10/28/13 6.21 ---94.05
Destroyed
Destroyed102.39
15
Destroyed
103.15
155 - 155
03/31/05 14
4 - 14403/31/05
4 - 14
12/20/12
100.00
100.00
Ground
Water
Elevation
(ft.)
MW-1
MW-2
2 2 - 1202/25/05
03/10/05
12
2 2 - 12 12
5 - 155
MW-4R
101.86
14MW-3
Well
Installation
Date
(mm/dd/yy)
01/02/13MW-1R
101.6015
Comments
5 - 155
103.38
12/20/12
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
Facility ID # : 0-023752
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Depth to
Water from
Top of Casing
(feet)
Top of Casing
Elevation
(ft.)
Free
Product
Thickness
(ft.)
MW-2R 102.21
4MW-4
100.00155 - 15512/20/12MW-7
101.83122 - 12212/20/12MW-6
101.55155 - 15512/20/12MW-5
100.26155 - 15512/20/12MW-8
Date: 11/7/13
Ground
Water
Elevation
(ft.)
Well
Installation
Date
(mm/dd/yy)
Comments
TABLE 1
WELL CONSTRUCTION AND GAUGING INFORMATION
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
Facility ID # : 0-023752
Well ID
Date
Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Depth to
Water from
Top of Casing
(feet)
Top of Casing
Elevation
(ft.)
Free
Product
Thickness
(ft.)
01/04/13 1.85 ---97.52
10/28/13 5.19 ---94.18
01/04/13 2.00 ---97.32
10/28/13 5.24 ---94.08
01/04/13 5.30 ---96.89
09/23/13 7.03 ---95.16 Before MMPE
09/27/13 10.90 ---91.29 After MMPE
10/28/13 8.44 ---93.75
01/04/13 0.88 ---98.07
10/28/13 5.14 ---93.81
01/04/13 1.68 ---98.31
10/28/13 5.39 ---94.60
04/04/05 7.77 ---95.64
05/30/12 NM ---NM
10/28/13 9.81 ---93.60
TW-1R 01/03/13 01/04/13 43 43 - 48 48 101.86 6.68 ---95.18
Notes:
• NA: Data not available.
• Top of Casing information obtained from report titled 'Phase II LSA', dated 2005by CBM Environmental Services, Inc.
• Well construction details obtained from historical well logs.
Destroyed
99.32
• ft BGS : feet below ground surface.
155 - 15512/20/12MW-10
99.37155 - 15512/20/12MW-9
99.9972 - 7212/20/12MW-13
98.9572 - 7212/20/12MW-12
102.19155 - 15512/20/12MW-11
103.414843 - 484303/31/05TW-1
Page 1 of 1
Date:11/25/13 Facility ID#:0-023752
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product
Thickness
before Recovery
(feet)
Product
Thickness after
Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-4R 0.00 0.00
MW-11 0.00 0.00
Notes :
• *: Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
TABLE 2
FREE PRODUCT RECOVERY RESULTS
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
Interface probe at top-of-casing
Gasoline 09/23/13 - 09/27/13 MMPE 2 11,028 Sheen
Date:11/25/13 Facility ID #:0-023752
MW-4R
MW-11
181.07 11,028.0 0 181.07
Notes:
• *: Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = lbs emitted/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
Current Event 11,028.00 181.07
Total To Date 11,028.00 181.07
0 181.07
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
Total Amount
of Product
Recovered
(gallons)
09/23/13 - 09/27/13 MMPE 3,320 106.4 74,000 181.07 11,028
TABLE 3
FREE PRODUCT RECOVERY EVENT INFORMATION
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
Well ID Date (mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Date:11/25/13 Facility ID #:0-023752
Wells Included in
Event
Product
Recovery
Method*
Date of Event
(mm/dd/yy)
Total Amount of
Free Product plus
Ground Water
Recovered
(gallons)
Cost of Free
Product
Recovery Event
Cost Per Gallon
(total liquids)
MW-4R and
MW-11 MMPE 09/23/13-
09/27/13 11,209.07 $11,128.10 $0.99
11,209.07 $11,128.10 $0.99
Notes:
• *: Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
TABLE 4
FREE PRODUCT RECOVERY COST SUMMARY
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
Comments
Cost per gallon for the event is based on a
total volume of 11,209.07 gallons of fluids
recovered.
TOTAL (to date)
Page 1 of 3
Date : 11/12/13
SM 3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 400 400 15 400 4,200 700 200
5,000 260,000 84,500 85,500 20,000 6,000 28,500 25,000 15,000 NE NE NE NE
02/28/05 1.2 0.44 J 3.7 0.43 J 60 6.6 NR NR NR <100 <200 <100 44 J
05/30/12 <0.13 0.21 J 0.88 0.47 J 12.2 29.7 NR NR NR NR NR NR NR
01/04/13 84.5 323 32.5 215 2.1 16.8 10.5 2.3 85.0 563 75.7 J <97 113
10/28/13 0.65 0.49 J 7.8 1.5 7.8 38.8 0.81 <0.10 NR NR NR NR NR
03/15/05 330 370 130 390 4,500 8.1 J NR NR NR 3,900 360 <150 320
05/30/12
01/04/13 38.4 0.93 1.3 6.5 292 57.0 27.1 1.9 14.7 124 <132 <97 241 J
10/28/13 25.6 1.8 1.1 J 4.1 104 57.1 17.2 1.4 NR NR NR NR NR
04/05/05 3.2 9 2.0 8.5 450 13 NR NR NR 98 J <200 <100 43 J
05/30/12 0.56 0.20 J <0.15 0.33 J 120 8.8 NR NR NR NR NR NR NR
01/04/13 1.8 0.25 J 0.13 J 0.35 J 95.9 5.4 0.54 0.12 J 9.8 <35 <132 <97 <132
10/28/13 0.72 <0.10 <0.10 <0.22 54.1 3.7 0.35 J <0.10 NR NR NR NR NR
04/05/05 6,500 2,100 2,000 10,400 140,000 520 NR NR NR 41,000 5,490 <100 3,370
05/30/12 12,000 33,300 1,410 16,500 409,000 776 NR NR NR NR NR NR NR
01/04/13 1,430 1,480 166 1,100 27,500 67.2 J 208 49.5 J 6.5 <700 <132 <97 1,262 J
10/28/13 2,200 2,300 512 2,009 7,130 119 558 133 NR NR NR NR NR
01/04/13 <0.10 <0.10 <0.10 <0.22 0.19 J <0.15 <0.10 <0.10 6.8 <35 <132 <97 <132
10/28/13 <0.10 <0.10 <0.10 <0.22 0.29 J <0.15 <0.10 <0.10 NR NR NR NR NR
01/04/13 <0.10 <0.10 <0.10 <0.22 0.12 J <0.15 <0.10 <0.10 8.3 <35 <132 <97 <132
10/28/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 NR NR NR NR NR
MW-4R
MW-3
MW-2R
MW-1R XylenesMW-6
MW-5 BenzeneMW-1 NaphthaleneGCL
TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
2L Standard
Analytical Method MTBEFacility ID # : 0-023752
C5-C8 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsDestroyed
Contaminant of
Concern
1,2,4 Trimethylbenzene1,3,5 TrimethylbenzeneTolueneMW-4
MADEP Methods EPH and VPH
MW-2 EthylbenzeneC9-C18 AliphaticsEPA Method 6200B and 625
Lead
Page 2 of 3
Date : 11/12/13
SM 3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 400 400 15 400 4,200 700 200
5,000 260,000 84,500 85,500 20,000 6,000 28,500 25,000 15,000 NE NE NE NEXylenesBenzeneNaphthaleneGCL
TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
2L Standard
Analytical Method MTBEFacility ID # : 0-023752
C5-C8 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsContaminant of
Concern
1,2,4 Trimethylbenzene1,3,5 TrimethylbenzeneTolueneMADEP Methods EPH and VPH
EthylbenzeneC9-C18 AliphaticsEPA Method 6200B and 625
Lead01/04/13 <0.10 <0.10 <0.10 <0.21 J 1.5 1.3 1.6 0.22 J 9.0 64.9 J <132 <97 <132
10/28/13 239 2.7 22.4 11.4 10.4 0.27 J 0.97 0.28 J NR NR NR NR NR
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 8.3 <35 <132 <97 <132
10/28/13 0.29 J <0.10 <0.10 <0.22 3.3 0.70 1.1 <0.10 NR NR NR NR NR
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 16.7 <35 <132 <97 <132
10/28/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 NR NR NR NR NR
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 36.9 <35 <132 <97 <132
10/28/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 NR NR NR NR NR
01/04/13 8,470 34,900 2,830 15,200 75,400 392 2,650 695 23.8 25,000 J 5,170 J <97 7,943
10/28/13 12,300 42,300 1,870 11,100 52,700 230 J 1,030 362 J NR NR NR NR NR
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 19.6 <35 <132 <97 131 J
10/28/13 <0.10 0.13 J <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 NR NR NR NR NR
01/04/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 625 <35 <132 <97 <132
10/28/13 <0.10 0.13 J <0.10 <0.22 0.15 J <0.15 <0.10 <0.10 NR NR NR NR NR
04/05/05 2.5 13 1.9 9.7 28 <1.0 NR NR NR <100 <200 <100 <200
05/30/12
01/04/13 2.5 5.3 0.44 J 1.5 J 17.1 <0.15 0.13 J <0.10 44.7 <35 <132 <97 <132
10/28/13 <0.10 <0.10 <0.10 <0.22 0.44 J <0.15 <0.10 <0.10 NR NR NR NR NR
TW-1
MW-13
MW-12
MW-11
MW-10
MW-9
MW-8
MW-7
TW-1R
Destroyed
Page 3 of 3
Date : 11/12/13
SM 3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 400 400 15 400 4,200 700 200
5,000 260,000 84,500 85,500 20,000 6,000 28,500 25,000 15,000 NE NE NE NEXylenesBenzeneNaphthaleneGCL
TABLE 5
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
HAN-DEE HUGO #5 (INCIDENT NO. 29175)
2L Standard
Analytical Method MTBEFacility ID # : 0-023752
C5-C8 AliphaticsC19-C36 AliphaticsC9-C22 AromaticsContaminant of
Concern
1,2,4 Trimethylbenzene1,3,5 TrimethylbenzeneTolueneMADEP Methods EPH and VPH
EthylbenzeneC9-C18 AliphaticsEPA Method 6200B and 625
LeadNotes:
• Results reported in µg/l (micrograms per liter).
• NE: Not established
• < : Less than the reporting limit specified in the laboratory report.
• Concentrations in bold face type exceeded the 2L standard.
• J: Estimated value.
• NR: Not Requested
• Detectable concentrations of the following contaminant constituents that exceeded the MACs were reported in the ground water samples collected in January 2013: IPE (696 µg/L) in
MW-4R; and IPE (4,470 µg/L), Isopropylbenzene (122 µg/L), n-Propylbenzene (392 µg/L), Styrene (93.5 J µg/L), and 2-Methylnaphthalene (77.3 µg/L) in MW-11.
• GCL: Gross contamination level.
• 2L Standard: as specified in T15A NCAC 2L.0202.

APPENDICES

APPENDIX A
Well Abandonment Agreement
GRI Phone Log
Name/Company Dorothy Russ
Date/Time 11/21/13 1415
Phone Number 910-863-3528
Project HH 5
Status Outgoing call; Rae Brown
Reason for Call Request information regarding Well Survey Response
Comments
Call Summary
Spoke Mrs. Russ. She is elderly and didn’t seem to hear well. I asked if she got water from the town.
She said she had her own well but she doesn’t drink the water. She said she would see me later and
ended the call.

APPENDIX B
AES MMPE Report

APPENDIX C
Laboratory Report –Ground Water Samples
11/08/13
Technical Report for
GRI (Geological Resources Inc.)
Handee Hugo 5; 1210 N Main St, Bladenboro, NC
29175
Accutest Job Number: FA9570
Sampling Date: 10/28/13
Report to:
GRI
2301 F Crown Point EX Dr
Charlotte, NC 28207
[e-mail]; [e-mail];
[e-mail]; [e-mail];
ATTN: Rae Brown
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (04226CA), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Harry Behzadi, Ph.D.
Laboratory Director
Southeast
11/08/13
e-Hardcopy 2.0
Automated Report
54
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 54
FA9570
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................9
3.1: FA9570-1: MW-1R .......................................................................................................10
3.2: FA9570-2: MW-2R .......................................................................................................12
3.3: FA9570-3: MW-3 ..........................................................................................................14
3.4: FA9570-4: MW-4R .......................................................................................................16
3.5: FA9570-5: MW-5 ..........................................................................................................18
3.6: FA9570-6: MW-6 ..........................................................................................................20
3.7: FA9570-7: MW-7 ..........................................................................................................22
3.8: FA9570-8: MW-8 ..........................................................................................................24
3.9: FA9570-9: MW-9 ..........................................................................................................26
3.10: FA9570-10: MW-10 ....................................................................................................28
3.11: FA9570-11: MW-11 ....................................................................................................30
3.12: FA9570-12: MW-12 ....................................................................................................32
3.13: FA9570-13: MW-13 ....................................................................................................34
3.14: FA9570-14: TW-1 .......................................................................................................36
Section 4: Misc. Forms ............................................................................................................38
4.1: Chain of Custody ...........................................................................................................39
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................42
5.1: Method Blank Summary ................................................................................................43
5.2: Blank Spike Summary ...................................................................................................47
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................51 123452 of 54
FA9570
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA9570
Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Project No: 29175
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA9570-1 10/28/13 15:01 HZ 10/31/13 AQ Ground Water MW-1R
FA9570-2 10/28/13 16:02 HZ 10/31/13 AQ Ground Water MW-2R
FA9570-3 10/28/13 15:29 HZ 10/31/13 AQ Ground Water MW-3
FA9570-4 10/28/13 15:15 HZ 10/31/13 AQ Ground Water MW-4R
FA9570-5 10/28/13 16:11 HZ 10/31/13 AQ Ground Water MW-5
FA9570-6 10/28/13 16:18 HZ 10/31/13 AQ Ground Water MW-6
FA9570-7 10/28/13 14:26 HZ 10/31/13 AQ Ground Water MW-7
FA9570-8 10/28/13 14:33 HZ 10/31/13 AQ Ground Water MW-8
FA9570-9 10/28/13 14:41 HZ 10/31/13 AQ Ground Water MW-9
FA9570-10 10/28/13 14:50 HZ 10/31/13 AQ Ground Water MW-10
FA9570-11 10/28/13 15:22 HZ 10/31/13 AQ Ground Water MW-11
FA9570-12 10/28/13 16:23 HZ 10/31/13 AQ Ground Water MW-12
FA9570-13 10/28/13 16:28 HZ 10/31/13 AQ Ground Water MW-13
3 of 54
FA9570 1
Accutest Laboratories
Sample Summary
(continued)
GRI (Geological Resources Inc.)
Job No:FA9570
Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Project No: 29175
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA9570-14 10/28/13 15:57 HZ 10/31/13 AQ Ground Water TW-1
4 of 54
FA9570 1
Summary of Hits Page 1 of 4
Job Number:FA9570
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Collected:10/28/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA9570-1 MW-1R
Benzene 0.65 0.50 0.10 ug/l SM 6200B
n-Butylbenzene 3.0 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 4.5 0.50 0.10 ug/l SM 6200B
tert-Butylbenzene 0.28 J 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 1.4 0.50 0.10 ug/l SM 6200B
Ethylbenzene 7.8 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 18.5 0.50 0.10 ug/l SM 6200B
Methyl chloride 0.24 J 0.50 0.11 ug/l SM 6200B
Methyl Tert Butyl Ether 7.8 0.50 0.10 ug/l SM 6200B
Naphthalene 38.8 0.50 0.15 ug/l SM 6200B
n-Propylbenzene 43.7 2.5 0.50 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.81 0.50 0.10 ug/l SM 6200B
Toluene 0.49 J 0.50 0.10 ug/l SM 6200B
Xylene (total)1.5 1.5 0.22 ug/l SM 6200B
m,p-Xylene 0.68 J 1.0 0.12 ug/l SM 6200B
o-Xylene 0.78 0.50 0.10 ug/l SM 6200B
FA9570-2 MW-2R
Benzene 25.6 1.3 0.25 ug/l SM 6200B
Di-Isopropyl ether 0.54 J 1.3 0.25 ug/l SM 6200B
Ethylbenzene 1.1 J 1.3 0.25 ug/l SM 6200B
Isopropylbenzene 0.75 J 1.3 0.25 ug/l SM 6200B
p-Isopropyltoluene 0.38 J 1.3 0.25 ug/l SM 6200B
Methyl Tert Butyl Ether 104 1.3 0.25 ug/l SM 6200B
Naphthalene 57.1 1.3 0.37 ug/l SM 6200B
n-Propylbenzene 0.36 J 1.3 0.25 ug/l SM 6200B
1,2,4-Trimethylbenzene 17.2 1.3 0.25 ug/l SM 6200B
1,3,5-Trimethylbenzene 1.4 1.3 0.25 ug/l SM 6200B
Toluene 1.8 1.3 0.25 ug/l SM 6200B
Xylene (total)4.1 3.8 0.54 ug/l SM 6200B
m,p-Xylene 3.5 2.5 0.29 ug/l SM 6200B
o-Xylene 0.51 J 1.3 0.25 ug/l SM 6200B
FA9570-3 MW-3
Benzene 0.72 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.70 0.50 0.10 ug/l SM 6200B
cis-1,2-Dichloroethylene 0.31 J 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 54.1 1.0 0.20 ug/l SM 6200B
Naphthalene 3.7 0.50 0.15 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.35 J 0.50 0.10 ug/l SM 6200B
5 of 54
FA9570 2
Summary of Hits Page 2 of 4
Job Number:FA9570
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Collected:10/28/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA9570-4 MW-4R
Benzene 2200 100 20 ug/l SM 6200B
Di-Isopropyl ether 1240 100 20 ug/l SM 6200B
Ethylbenzene 512 100 20 ug/l SM 6200B
Isopropylbenzene 30.0 J 100 20 ug/l SM 6200B
Methyl Tert Butyl Ether 7130 100 20 ug/l SM 6200B
Naphthalene 119 100 30 ug/l SM 6200B
n-Propylbenzene 82.5 J 100 20 ug/l SM 6200B
1,2,4-Trimethylbenzene 558 100 20 ug/l SM 6200B
1,3,5-Trimethylbenzene 133 100 20 ug/l SM 6200B
Toluene 2300 100 20 ug/l SM 6200B
m,p-Xylene 1180 200 23 ug/l SM 6200B
o-Xylene 829 100 20 ug/l SM 6200B
FA9570-5 MW-5
Methyl chloride 0.40 J 0.50 0.11 ug/l SM 6200B
Methyl Tert Butyl Ether 0.29 J 0.50 0.10 ug/l SM 6200B
FA9570-6 MW-6
Methyl chloride 0.23 J 0.50 0.11 ug/l SM 6200B
FA9570-7 MW-7
Benzene 239 5.0 1.0 ug/l SM 6200B
Di-Isopropyl ether 2.0 0.50 0.10 ug/l SM 6200B
Ethylbenzene 22.4 0.50 0.10 ug/l SM 6200B
Isopropylbenzene 0.75 0.50 0.10 ug/l SM 6200B
Methyl Tert Butyl Ether 10.4 0.50 0.10 ug/l SM 6200B
Naphthalene 0.27 J 0.50 0.15 ug/l SM 6200B
n-Propylbenzene 0.76 0.50 0.10 ug/l SM 6200B
1,2,4-Trimethylbenzene 0.97 0.50 0.10 ug/l SM 6200B
1,3,5-Trimethylbenzene 0.28 J 0.50 0.10 ug/l SM 6200B
Toluene 2.7 0.50 0.10 ug/l SM 6200B
Xylene (total)11.4 1.5 0.22 ug/l SM 6200B
m,p-Xylene 7.1 1.0 0.12 ug/l SM 6200B
o-Xylene 4.3 0.50 0.10 ug/l SM 6200B
FA9570-8 MW-8
Benzene 0.29 J 0.50 0.10 ug/l SM 6200B
sec-Butylbenzene 0.17 J 0.50 0.10 ug/l SM 6200B
Di-Isopropyl ether 0.16 J 0.50 0.10 ug/l SM 6200B
6 of 54
FA9570 2
Summary of Hits Page 3 of 4
Job Number:FA9570
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Collected:10/28/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Methyl chloride 0.18 J 0.50 0.11 ug/l SM 6200B
Methyl Tert Butyl Ether 3.3 0.50 0.10 ug/l SM 6200B
Naphthalene 0.70 0.50 0.15 ug/l SM 6200B
1,2,4-Trimethylbenzene 1.1 0.50 0.10 ug/l SM 6200B
m,p-Xylene 0.12 J 1.0 0.12 ug/l SM 6200B
FA9570-9 MW-9
Methyl chloride 0.14 J 0.50 0.11 ug/l SM 6200B
FA9570-10 MW-10
No hits reported in this sample.
FA9570-11 MW-11
Benzene 12300 500 100 ug/l SM 6200B
Di-Isopropyl ether 4820 500 100 ug/l SM 6200B
Ethylbenzene 1870 500 100 ug/l SM 6200B
Methylene chloride 1410 J 2000 1000 ug/l SM 6200B
Methyl Tert Butyl Ether 52700 1000 200 ug/l SM 6200B
Naphthalene 230 J 500 150 ug/l SM 6200B
n-Propylbenzene 161 J 500 100 ug/l SM 6200B
1,2,4-Trimethylbenzene 1030 500 100 ug/l SM 6200B
1,3,5-Trimethylbenzene 362 J 500 100 ug/l SM 6200B
Toluene 42300 500 100 ug/l SM 6200B
Xylene (total)11100 1500 220 ug/l SM 6200B
m,p-Xylene 6750 1000 120 ug/l SM 6200B
o-Xylene 4350 500 100 ug/l SM 6200B
FA9570-12 MW-12
Toluene 0.13 J 0.50 0.10 ug/l SM 6200B
FA9570-13 MW-13
Methylene chloride a 1.4 J 2.0 1.0 ug/l SM 6200B
Methyl Tert Butyl Ether a 0.15 J 0.50 0.10 ug/l SM 6200B
Toluene a 0.13 J 0.50 0.10 ug/l SM 6200B
FA9570-14 TW-1
Methyl chloride 0.15 J 0.50 0.11 ug/l SM 6200B
Methyl Tert Butyl Ether 0.44 J 0.50 0.10 ug/l SM 6200B
7 of 54
FA9570 2
Summary of Hits Page 4 of 4
Job Number:FA9570
Account:GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Collected:10/28/13
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
8 of 54
FA9570 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
9 of 54
FA9570 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA9570-1 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183674.D 1 11/05/13 TD n/a n/a VA1368
Run #2 A0183632.D 5 11/04/13 TD n/a n/a VA1367
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.65 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene 3.0 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 4.5 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene 0.28 0.50 0.10 ug/l J
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 1.4 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 54
FA9570 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-1R
Lab Sample ID:FA9570-1 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 7.8 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 18.5 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride 0.24 0.50 0.11 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 7.8 0.50 0.10 ug/l
91-20-3 Naphthalene 38.8 0.50 0.15 ug/l
103-65-1 n-Propylbenzene 43.7 a 2.5 0.50 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.81 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 0.49 0.50 0.10 ug/l J
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)1.5 1.5 0.22 ug/l
m,p-Xylene 0.68 1.0 0.12 ug/l J
95-47-6 o-Xylene 0.78 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%102%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%100%70-130%
2037-26-5 Toluene-D8 99%99%70-130%
460-00-4 4-Bromofluorobenzene 105%102%70-130%
(a) Result is from Run# 2
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 54
FA9570 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA9570-2 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183675.D 2.5 11/05/13 TD n/a n/a VA1368
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 25.6 1.3 0.25 ug/l
108-86-1 Bromobenzene ND 1.3 0.25 ug/l
74-97-5 Bromochloromethane ND 1.3 0.25 ug/l
75-27-4 Bromodichloromethane ND 1.3 0.25 ug/l
75-25-2 Bromoform ND 1.3 0.25 ug/l
104-51-8 n-Butylbenzene ND 1.3 0.25 ug/l
135-98-8 sec-Butylbenzene ND 1.3 0.25 ug/l
98-06-6 tert-Butylbenzene ND 1.3 0.25 ug/l
108-90-7 Chlorobenzene ND 1.3 0.25 ug/l
75-00-3 Chloroethane ND 1.3 0.33 ug/l
67-66-3 Chloroform ND 1.3 0.25 ug/l
95-49-8 o-Chlorotoluene ND 1.3 0.25 ug/l
106-43-4 p-Chlorotoluene ND 1.3 0.25 ug/l
56-23-5 Carbon tetrachloride ND 1.3 0.32 ug/l
75-34-3 1,1-Dichloroethane ND 1.3 0.25 ug/l
75-35-4 1,1-Dichloroethylene ND 1.3 0.25 ug/l
563-58-6 1,1-Dichloropropene ND 1.3 0.25 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 1.3 0.41 ug/l
106-93-4 1,2-Dibromoethane ND 1.3 0.25 ug/l
107-06-2 1,2-Dichloroethane ND 1.3 0.25 ug/l
78-87-5 1,2-Dichloropropane ND 1.3 0.25 ug/l
142-28-9 1,3-Dichloropropane ND 1.3 0.25 ug/l
108-20-3 Di-Isopropyl ether 0.54 1.3 0.25 ug/l J
594-20-7 2,2-Dichloropropane ND 1.3 0.25 ug/l
124-48-1 Dibromochloromethane ND 1.3 0.25 ug/l
75-71-8 Dichlorodifluoromethane ND 1.3 0.25 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.3 0.25 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.3 0.25 ug/l
541-73-1 m-Dichlorobenzene ND 1.3 0.25 ug/l
95-50-1 o-Dichlorobenzene ND 1.3 0.25 ug/l
106-46-7 p-Dichlorobenzene ND 1.3 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.3 0.25 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 54
FA9570 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-2R
Lab Sample ID:FA9570-2 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.3 0.25 ug/l
100-41-4 Ethylbenzene 1.1 1.3 0.25 ug/l J
87-68-3 Hexachlorobutadiene ND 1.3 0.25 ug/l
98-82-8 Isopropylbenzene 0.75 1.3 0.25 ug/l J
99-87-6 p-Isopropyltoluene 0.38 1.3 0.25 ug/l J
74-83-9 Methyl bromide ND 1.3 0.39 ug/l
74-87-3 Methyl chloride ND 1.3 0.27 ug/l
74-95-3 Methylene bromide ND 1.3 0.25 ug/l
75-09-2 Methylene chloride ND 5.0 2.5 ug/l
1634-04-4 Methyl Tert Butyl Ether 104 1.3 0.25 ug/l
91-20-3 Naphthalene 57.1 1.3 0.37 ug/l
103-65-1 n-Propylbenzene 0.36 1.3 0.25 ug/l J
100-42-5 Styrene ND 1.3 0.25 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.3 0.25 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.3 0.25 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.3 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.3 0.25 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 1.3 0.25 ug/l
96-18-4 1,2,3-Trichloropropane ND 1.3 0.25 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 1.3 0.25 ug/l
95-63-6 1,2,4-Trimethylbenzene 17.2 1.3 0.25 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.4 1.3 0.25 ug/l
127-18-4 Tetrachloroethylene ND 1.3 0.25 ug/l
108-88-3 Toluene 1.8 1.3 0.25 ug/l
79-01-6 Trichloroethylene ND 1.3 0.25 ug/l
75-69-4 Trichlorofluoromethane ND 1.3 0.25 ug/l
75-01-4 Vinyl chloride ND 1.3 0.25 ug/l
1330-20-7 Xylene (total)4.1 3.8 0.54 ug/l
m,p-Xylene 3.5 2.5 0.29 ug/l
95-47-6 o-Xylene 0.51 1.3 0.25 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 54
FA9570 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-3
Lab Sample ID:FA9570-3 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183634.D 1 11/04/13 TD n/a n/a VA1367
Run #2 A0183676.D 2 11/05/13 TD n/a n/a VA1368
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.72 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.70 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene 0.31 0.50 0.10 ug/l J
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 54
FA9570 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-3
Lab Sample ID:FA9570-3 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride ND 0.50 0.11 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 54.1 b 1.0 0.20 ug/l
91-20-3 Naphthalene 3.7 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.35 0.50 0.10 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%100%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%98%70-130%
2037-26-5 Toluene-D8 99%101%70-130%
460-00-4 4-Bromofluorobenzene 104%102%70-130%
(a) Associated BS recovery outside control limits.
(b) Result is from Run# 2
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 54
FA9570 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA9570-4 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183677.D 200 11/05/13 TD n/a n/a VA1368
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 2200 100 20 ug/l
108-86-1 Bromobenzene ND 100 20 ug/l
74-97-5 Bromochloromethane ND 100 20 ug/l
75-27-4 Bromodichloromethane ND 100 20 ug/l
75-25-2 Bromoform ND 100 20 ug/l
104-51-8 n-Butylbenzene ND 100 20 ug/l
135-98-8 sec-Butylbenzene ND 100 20 ug/l
98-06-6 tert-Butylbenzene ND 100 20 ug/l
108-90-7 Chlorobenzene ND 100 20 ug/l
75-00-3 Chloroethane ND 100 26 ug/l
67-66-3 Chloroform ND 100 20 ug/l
95-49-8 o-Chlorotoluene ND 100 20 ug/l
106-43-4 p-Chlorotoluene ND 100 20 ug/l
56-23-5 Carbon tetrachloride ND 100 25 ug/l
75-34-3 1,1-Dichloroethane ND 100 20 ug/l
75-35-4 1,1-Dichloroethylene ND 100 20 ug/l
563-58-6 1,1-Dichloropropene ND 100 20 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 100 33 ug/l
106-93-4 1,2-Dibromoethane ND 100 20 ug/l
107-06-2 1,2-Dichloroethane ND 100 20 ug/l
78-87-5 1,2-Dichloropropane ND 100 20 ug/l
142-28-9 1,3-Dichloropropane ND 100 20 ug/l
108-20-3 Di-Isopropyl ether 1240 100 20 ug/l
594-20-7 2,2-Dichloropropane ND 100 20 ug/l
124-48-1 Dibromochloromethane ND 100 20 ug/l
75-71-8 Dichlorodifluoromethane ND 100 20 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 100 20 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 100 20 ug/l
541-73-1 m-Dichlorobenzene ND 100 20 ug/l
95-50-1 o-Dichlorobenzene ND 100 20 ug/l
106-46-7 p-Dichlorobenzene ND 100 22 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 100 20 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 54
FA9570 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-4R
Lab Sample ID:FA9570-4 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 100 20 ug/l
100-41-4 Ethylbenzene 512 100 20 ug/l
87-68-3 Hexachlorobutadiene ND 100 20 ug/l
98-82-8 Isopropylbenzene 30.0 100 20 ug/l J
99-87-6 p-Isopropyltoluene ND 100 20 ug/l
74-83-9 Methyl bromide ND 100 31 ug/l
74-87-3 Methyl chloride ND 100 21 ug/l
74-95-3 Methylene bromide ND 100 20 ug/l
75-09-2 Methylene chloride ND 400 200 ug/l
1634-04-4 Methyl Tert Butyl Ether 7130 100 20 ug/l
91-20-3 Naphthalene 119 100 30 ug/l
103-65-1 n-Propylbenzene 82.5 100 20 ug/l J
100-42-5 Styrene ND 100 20 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 100 20 ug/l
71-55-6 1,1,1-Trichloroethane ND 100 20 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 100 20 ug/l
79-00-5 1,1,2-Trichloroethane ND 100 20 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 100 20 ug/l
96-18-4 1,2,3-Trichloropropane ND 100 20 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 100 20 ug/l
95-63-6 1,2,4-Trimethylbenzene 558 100 20 ug/l
108-67-8 1,3,5-Trimethylbenzene 133 100 20 ug/l
127-18-4 Tetrachloroethylene ND 100 20 ug/l
108-88-3 Toluene 2300 100 20 ug/l
79-01-6 Trichloroethylene ND 100 20 ug/l
75-69-4 Trichlorofluoromethane ND 100 20 ug/l
75-01-4 Vinyl chloride ND 100 20 ug/l
m,p-Xylene 1180 200 23 ug/l
95-47-6 o-Xylene 829 100 20 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 97%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 54
FA9570 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-5
Lab Sample ID:FA9570-5 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183636.D 1 11/04/13 TD n/a n/a VA1367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 54
FA9570 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-5
Lab Sample ID:FA9570-5 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride 0.40 0.50 0.11 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.29 0.50 0.10 ug/l J
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 103%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 95%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 54
FA9570 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-6
Lab Sample ID:FA9570-6 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183637.D 1 11/04/13 TD n/a n/a VA1367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 54
FA9570 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-6
Lab Sample ID:FA9570-6 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride 0.23 0.50 0.11 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 102%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 54
FA9570 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-7
Lab Sample ID:FA9570-7 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183638.D 1 11/04/13 TD n/a n/a VA1367
Run #2 A0183678.D 10 11/05/13 TD n/a n/a VA1368
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 239 a 5.0 1.0 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 2.0 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane b ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 54
FA9570 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-7
Lab Sample ID:FA9570-7 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene 22.4 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene 0.75 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride ND 0.50 0.11 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 10.4 0.50 0.10 ug/l
91-20-3 Naphthalene 0.27 0.50 0.15 ug/l J
103-65-1 n-Propylbenzene 0.76 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.97 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene 0.28 0.50 0.10 ug/l J
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 2.7 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)11.4 1.5 0.22 ug/l
m,p-Xylene 7.1 1.0 0.12 ug/l
95-47-6 o-Xylene 4.3 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%101%70-130%
2037-26-5 Toluene-D8 99%102%70-130%
460-00-4 4-Bromofluorobenzene 104%102%70-130%
(a) Result is from Run# 2
(b) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 54
FA9570 33.7
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-8
Lab Sample ID:FA9570-8 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183639.D 1 11/04/13 TD n/a n/a VA1367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 0.29 0.50 0.10 ug/l J
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene 0.17 0.50 0.10 ug/l J
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether 0.16 0.50 0.10 ug/l J
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 54
FA9570 33.8
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-8
Lab Sample ID:FA9570-8 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride 0.18 0.50 0.11 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 3.3 0.50 0.10 ug/l
91-20-3 Naphthalene 0.70 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene 1.1 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene 0.12 1.0 0.12 ug/l J
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 101%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 54
FA9570 33.8
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-9
Lab Sample ID:FA9570-9 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183640.D 1 11/04/13 TD n/a n/a VA1367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 54
FA9570 33.9
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-9
Lab Sample ID:FA9570-9 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride 0.14 0.50 0.11 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 54
FA9570 33.9
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-10
Lab Sample ID:FA9570-10 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183641.D 1 11/04/13 TD n/a n/a VA1367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 54
FA9570 33.10
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-10
Lab Sample ID:FA9570-10 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride ND 0.50 0.11 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 54
FA9570 33.10
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-11
Lab Sample ID:FA9570-11 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183642.D 1000 11/04/13 TD n/a n/a VA1367
Run #2 A0183679.D 2000 11/05/13 TD n/a n/a VA1368
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 12300 500 100 ug/l
108-86-1 Bromobenzene ND 500 100 ug/l
74-97-5 Bromochloromethane ND 500 100 ug/l
75-27-4 Bromodichloromethane ND 500 100 ug/l
75-25-2 Bromoform ND 500 100 ug/l
104-51-8 n-Butylbenzene ND 500 100 ug/l
135-98-8 sec-Butylbenzene ND 500 100 ug/l
98-06-6 tert-Butylbenzene ND 500 100 ug/l
108-90-7 Chlorobenzene ND 500 100 ug/l
75-00-3 Chloroethane ND 500 130 ug/l
67-66-3 Chloroform ND 500 100 ug/l
95-49-8 o-Chlorotoluene ND 500 100 ug/l
106-43-4 p-Chlorotoluene ND 500 100 ug/l
56-23-5 Carbon tetrachloride ND 500 130 ug/l
75-34-3 1,1-Dichloroethane ND 500 100 ug/l
75-35-4 1,1-Dichloroethylene ND 500 100 ug/l
563-58-6 1,1-Dichloropropene ND 500 100 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 500 160 ug/l
106-93-4 1,2-Dibromoethane ND 500 100 ug/l
107-06-2 1,2-Dichloroethane ND 500 100 ug/l
78-87-5 1,2-Dichloropropane ND 500 100 ug/l
142-28-9 1,3-Dichloropropane ND 500 100 ug/l
108-20-3 Di-Isopropyl ether 4820 500 100 ug/l
594-20-7 2,2-Dichloropropane ND 500 100 ug/l
124-48-1 Dibromochloromethane ND 500 100 ug/l
75-71-8 Dichlorodifluoromethane a ND 500 100 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 500 100 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 500 100 ug/l
541-73-1 m-Dichlorobenzene ND 500 100 ug/l
95-50-1 o-Dichlorobenzene ND 500 100 ug/l
106-46-7 p-Dichlorobenzene ND 500 110 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 500 100 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 54
FA9570 33.11
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-11
Lab Sample ID:FA9570-11 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 500 100 ug/l
100-41-4 Ethylbenzene 1870 500 100 ug/l
87-68-3 Hexachlorobutadiene ND 500 100 ug/l
98-82-8 Isopropylbenzene ND 500 100 ug/l
99-87-6 p-Isopropyltoluene ND 500 100 ug/l
74-83-9 Methyl bromide ND 500 150 ug/l
74-87-3 Methyl chloride ND 500 110 ug/l
74-95-3 Methylene bromide ND 500 100 ug/l
75-09-2 Methylene chloride 1410 2000 1000 ug/l J
1634-04-4 Methyl Tert Butyl Ether 52700 b 1000 200 ug/l
91-20-3 Naphthalene 230 500 150 ug/l J
103-65-1 n-Propylbenzene 161 500 100 ug/l J
100-42-5 Styrene ND 500 100 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 500 100 ug/l
71-55-6 1,1,1-Trichloroethane ND 500 100 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 500 100 ug/l
79-00-5 1,1,2-Trichloroethane ND 500 100 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 500 100 ug/l
96-18-4 1,2,3-Trichloropropane ND 500 100 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 500 100 ug/l
95-63-6 1,2,4-Trimethylbenzene 1030 500 100 ug/l
108-67-8 1,3,5-Trimethylbenzene 362 500 100 ug/l J
127-18-4 Tetrachloroethylene ND 500 100 ug/l
108-88-3 Toluene 42300 500 100 ug/l
79-01-6 Trichloroethylene ND 500 100 ug/l
75-69-4 Trichlorofluoromethane ND 500 100 ug/l
75-01-4 Vinyl chloride ND 500 100 ug/l
1330-20-7 Xylene (total)11100 1500 220 ug/l
m,p-Xylene 6750 1000 120 ug/l
95-47-6 o-Xylene 4350 500 100 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%98%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%99%70-130%
2037-26-5 Toluene-D8 103%104%70-130%
460-00-4 4-Bromofluorobenzene 104%105%70-130%
(a) Associated BS recovery outside control limits.
(b) Result is from Run# 2
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 54
FA9570 33.11
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-12
Lab Sample ID:FA9570-12 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183643.D 1 11/04/13 TD n/a n/a VA1367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 54
FA9570 33.12
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-12
Lab Sample ID:FA9570-12 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride ND 0.50 0.11 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 0.13 0.50 0.10 ug/l J
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 104%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 54
FA9570 33.12
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-13
Lab Sample ID:FA9570-13 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a A0183663.D 1 11/05/13 TD n/a n/a VA1368
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 54
FA9570 33.13
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-13
Lab Sample ID:FA9570-13 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride ND 0.50 0.11 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride 1.4 2.0 1.0 ug/l J
1634-04-4 Methyl Tert Butyl Ether 0.15 0.50 0.10 ug/l J
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene 0.13 0.50 0.10 ug/l J
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 100%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 103%70-130%
460-00-4 4-Bromofluorobenzene 105%70-130%
(a) Sample vial(s) contained significant headspace; reported results are considered minimum values.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 54
FA9570 33.13
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:TW-1
Lab Sample ID:FA9570-14 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0183644.D 1 11/04/13 TD n/a n/a VA1367
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane a ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 54
FA9570 33.14
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:TW-1
Lab Sample ID:FA9570-14 Date Sampled:10/28/13
Matrix:AQ - Ground Water Date Received:10/31/13
Method:SM 6200B Percent Solids:n/a
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride 0.15 0.50 0.11 ug/l J
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether 0.44 0.50 0.10 ug/l J
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%70-130%
2037-26-5 Toluene-D8 90%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
(a) Associated BS recovery outside control limits.
ND = Not detected MDL - Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 54
FA9570 33.14
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
38 of 54
FA9570 4
FA9570: Chain of Custody
Page 1 of 3
39 of 54
FA9570 44.1
FA9570: Chain of Custody
Page 2 of 3
40 of 54
FA9570 44.1
FA9570: Chain of Custody
Page 3 of 3
41 of 54
FA9570 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
42 of 54
FA9570 5
Method Blank Summary Page 1 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1367-MB A0183616.D 1 11/04/13 TD n/a n/a VA1367
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-3, FA9570-5, FA9570-6, FA9570-7, FA9570-8, FA9570-9, FA9570-10, FA9570-11, FA9570-12,
FA9570-14
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
43 of 54
FA9570 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1367-MB A0183616.D 1 11/04/13 TD n/a n/a VA1367
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-3, FA9570-5, FA9570-6, FA9570-7, FA9570-8, FA9570-9, FA9570-10, FA9570-11, FA9570-12,
FA9570-14
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride ND 0.50 0.11 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 101%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
44 of 54
FA9570 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1368-MB A0183662.D 1 11/05/13 TD n/a n/a VA1368
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-2, FA9570-3, FA9570-4, FA9570-7, FA9570-11, FA9570-13
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.10 ug/l
108-86-1 Bromobenzene ND 0.50 0.10 ug/l
74-97-5 Bromochloromethane ND 0.50 0.10 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.10 ug/l
75-25-2 Bromoform ND 0.50 0.10 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.10 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.10 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.10 ug/l
108-90-7 Chlorobenzene ND 0.50 0.10 ug/l
75-00-3 Chloroethane ND 0.50 0.13 ug/l
67-66-3 Chloroform ND 0.50 0.10 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.10 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.10 ug/l
56-23-5 Carbon tetrachloride ND 0.50 0.13 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.10 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.10 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.10 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.16 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.10 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.10 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.10 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.10 ug/l
108-20-3 Di-Isopropyl ether ND 0.50 0.10 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.10 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.10 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.10 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.10 ug/l
541-73-1 m-Dichlorobenzene ND 0.50 0.10 ug/l
95-50-1 o-Dichlorobenzene ND 0.50 0.10 ug/l
106-46-7 p-Dichlorobenzene ND 0.50 0.11 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.10 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.10 ug/l
100-41-4 Ethylbenzene ND 0.50 0.10 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.10 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.10 ug/l
45 of 54
FA9570 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1368-MB A0183662.D 1 11/05/13 TD n/a n/a VA1368
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-2, FA9570-3, FA9570-4, FA9570-7, FA9570-11, FA9570-13
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.10 ug/l
74-83-9 Methyl bromide ND 0.50 0.15 ug/l
74-87-3 Methyl chloride ND 0.50 0.11 ug/l
74-95-3 Methylene bromide ND 0.50 0.10 ug/l
75-09-2 Methylene chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.10 ug/l
91-20-3 Naphthalene ND 0.50 0.15 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.10 ug/l
100-42-5 Styrene ND 0.50 0.10 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.10 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.10 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.10 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.10 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.10 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.10 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.10 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.10 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.10 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.10 ug/l
108-88-3 Toluene ND 0.50 0.10 ug/l
79-01-6 Trichloroethylene ND 0.50 0.10 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.10 ug/l
75-01-4 Vinyl chloride ND 0.50 0.10 ug/l
1330-20-7 Xylene (total)ND 1.5 0.22 ug/l
m,p-Xylene ND 1.0 0.12 ug/l
95-47-6 o-Xylene ND 0.50 0.10 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 99%70-130%
17060-07-0 1,2-Dichloroethane-D4 99%70-130%
2037-26-5 Toluene-D8 104%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
46 of 54
FA9570 55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1367-BS A0183614.D 1 11/04/13 TD n/a n/a VA1367
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-3, FA9570-5, FA9570-6, FA9570-7, FA9570-8, FA9570-9, FA9570-10, FA9570-11, FA9570-12,
FA9570-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.4 104 70-130
108-86-1 Bromobenzene 10 10.5 105 70-130
74-97-5 Bromochloromethane 10 9.6 96 70-130
75-27-4 Bromodichloromethane 10 10.2 102 70-130
75-25-2 Bromoform 10 9.0 90 70-130
104-51-8 n-Butylbenzene 10 9.1 91 70-130
135-98-8 sec-Butylbenzene 10 10.6 106 70-130
98-06-6 tert-Butylbenzene 10 10.2 102 70-130
108-90-7 Chlorobenzene 10 11.1 111 70-130
75-00-3 Chloroethane 10 9.6 96 60-140
67-66-3 Chloroform 10 10.1 101 70-130
95-49-8 o-Chlorotoluene 10 11.1 111 70-130
106-43-4 p-Chlorotoluene 10 10.5 105 70-130
56-23-5 Carbon tetrachloride 10 10.7 107 70-130
75-34-3 1,1-Dichloroethane 10 10.1 101 70-130
75-35-4 1,1-Dichloroethylene 10 10.6 106 70-130
563-58-6 1,1-Dichloropropene 10 10.4 104 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.8 88 70-130
106-93-4 1,2-Dibromoethane 10 10.8 108 70-130
107-06-2 1,2-Dichloroethane 10 10.1 101 70-130
78-87-5 1,2-Dichloropropane 10 10.2 102 70-130
142-28-9 1,3-Dichloropropane 10 10.4 104 70-130
108-20-3 Di-Isopropyl ether 10 8.4 84 70-130
594-20-7 2,2-Dichloropropane 10 10.8 108 70-130
124-48-1 Dibromochloromethane 10 10.3 103 70-130
75-71-8 Dichlorodifluoromethane 10 14.2 142*60-140
156-59-2 cis-1,2-Dichloroethylene 10 10.7 107 70-130
10061-01-5 cis-1,3-Dichloropropene 10 9.3 93 70-130
541-73-1 m-Dichlorobenzene 10 11.6 116 70-130
95-50-1 o-Dichlorobenzene 10 11.3 113 70-130
106-46-7 p-Dichlorobenzene 10 10.2 102 70-130
156-60-5 trans-1,2-Dichloroethylene 10 10.1 101 70-130
10061-02-6 trans-1,3-Dichloropropene 10 10.1 101 70-130
100-41-4 Ethylbenzene 10 10.5 105 70-130
87-68-3 Hexachlorobutadiene 10 11.5 115 70-130
98-82-8 Isopropylbenzene 10 10.7 107 70-130
* = Outside of Control Limits.
47 of 54
FA9570 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1367-BS A0183614.D 1 11/04/13 TD n/a n/a VA1367
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-3, FA9570-5, FA9570-6, FA9570-7, FA9570-8, FA9570-9, FA9570-10, FA9570-11, FA9570-12,
FA9570-14
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 10.2 102 70-130
74-83-9 Methyl bromide 10 9.0 90 60-140
74-87-3 Methyl chloride 10 10.1 101 60-140
74-95-3 Methylene bromide 10 10.1 101 70-130
75-09-2 Methylene chloride 10 10.0 100 70-130
1634-04-4 Methyl Tert Butyl Ether 10 9.4 94 70-130
91-20-3 Naphthalene 10 9.6 96 70-130
103-65-1 n-Propylbenzene 10 10.5 105 70-130
100-42-5 Styrene 10 9.1 91 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.6 106 70-130
71-55-6 1,1,1-Trichloroethane 10 10.5 105 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 9.3 93 70-130
79-00-5 1,1,2-Trichloroethane 10 10.0 100 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.1 111 70-130
96-18-4 1,2,3-Trichloropropane 10 9.8 98 70-130
120-82-1 1,2,4-Trichlorobenzene 10 9.7 97 70-130
95-63-6 1,2,4-Trimethylbenzene 10 9.4 94 70-130
108-67-8 1,3,5-Trimethylbenzene 10 9.3 93 70-130
127-18-4 Tetrachloroethylene 10 11.5 115 70-130
108-88-3 Toluene 10 10.5 105 70-130
79-01-6 Trichloroethylene 10 10.7 107 70-130
75-69-4 Trichlorofluoromethane 10 8.9 89 60-140
75-01-4 Vinyl chloride 10 10.7 107 60-140
1330-20-7 Xylene (total)30 31.2 104 70-130
m,p-Xylene 20 20.8 104 70-130
95-47-6 o-Xylene 10 10.3 103 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 98%70-130%
17060-07-0 1,2-Dichloroethane-D4 95%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
* = Outside of Control Limits.
48 of 54
FA9570 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1368-BS A0183660.D 1 11/05/13 TD n/a n/a VA1368
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-2, FA9570-3, FA9570-4, FA9570-7, FA9570-11, FA9570-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 8.7 87 70-130
108-86-1 Bromobenzene 10 9.4 94 70-130
74-97-5 Bromochloromethane 10 7.8 78 70-130
75-27-4 Bromodichloromethane 10 8.7 87 70-130
75-25-2 Bromoform 10 8.8 88 70-130
104-51-8 n-Butylbenzene 10 7.8 78 70-130
135-98-8 sec-Butylbenzene 10 9.1 91 70-130
98-06-6 tert-Butylbenzene 10 8.8 88 70-130
108-90-7 Chlorobenzene 10 9.8 98 70-130
75-00-3 Chloroethane 10 9.7 97 60-140
67-66-3 Chloroform 10 8.5 85 70-130
95-49-8 o-Chlorotoluene 10 10.2 102 70-130
106-43-4 p-Chlorotoluene 10 9.2 92 70-130
56-23-5 Carbon tetrachloride 10 8.8 88 70-130
75-34-3 1,1-Dichloroethane 10 8.6 86 70-130
75-35-4 1,1-Dichloroethylene 10 8.5 85 70-130
563-58-6 1,1-Dichloropropene 10 9.4 94 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 8.5 85 70-130
106-93-4 1,2-Dibromoethane 10 9.3 93 70-130
107-06-2 1,2-Dichloroethane 10 8.7 87 70-130
78-87-5 1,2-Dichloropropane 10 8.8 88 70-130
142-28-9 1,3-Dichloropropane 10 9.0 90 70-130
108-20-3 Di-Isopropyl ether 10 7.8 78 70-130
594-20-7 2,2-Dichloropropane 10 8.8 88 70-130
124-48-1 Dibromochloromethane 10 9.2 92 70-130
75-71-8 Dichlorodifluoromethane 10 12.4 124 60-140
156-59-2 cis-1,2-Dichloroethylene 10 8.8 88 70-130
10061-01-5 cis-1,3-Dichloropropene 10 7.6 76 70-130
541-73-1 m-Dichlorobenzene 10 10.2 102 70-130
95-50-1 o-Dichlorobenzene 10 9.9 99 70-130
106-46-7 p-Dichlorobenzene 10 9.0 90 70-130
156-60-5 trans-1,2-Dichloroethylene 10 8.3 83 70-130
10061-02-6 trans-1,3-Dichloropropene 10 8.6 86 70-130
100-41-4 Ethylbenzene 10 9.1 91 70-130
87-68-3 Hexachlorobutadiene 10 9.9 99 70-130
98-82-8 Isopropylbenzene 10 8.8 88 70-130
* = Outside of Control Limits.
49 of 54
FA9570 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1368-BS A0183660.D 1 11/05/13 TD n/a n/a VA1368
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-2, FA9570-3, FA9570-4, FA9570-7, FA9570-11, FA9570-13
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 8.6 86 70-130
74-83-9 Methyl bromide 10 9.4 94 60-140
74-87-3 Methyl chloride 10 9.8 98 60-140
74-95-3 Methylene bromide 10 8.6 86 70-130
75-09-2 Methylene chloride 10 7.9 79 70-130
1634-04-4 Methyl Tert Butyl Ether 10 7.6 76 70-130
91-20-3 Naphthalene 10 7.7 77 70-130
103-65-1 n-Propylbenzene 10 10.6 106 70-130
100-42-5 Styrene 10 7.6 76 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 9.4 94 70-130
71-55-6 1,1,1-Trichloroethane 10 8.8 88 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 8.9 89 70-130
79-00-5 1,1,2-Trichloroethane 10 8.9 89 70-130
87-61-6 1,2,3-Trichlorobenzene 10 9.5 95 70-130
96-18-4 1,2,3-Trichloropropane 10 9.1 91 70-130
120-82-1 1,2,4-Trichlorobenzene 10 7.9 79 70-130
95-63-6 1,2,4-Trimethylbenzene 10 8.1 81 70-130
108-67-8 1,3,5-Trimethylbenzene 10 8.1 81 70-130
127-18-4 Tetrachloroethylene 10 9.6 96 70-130
108-88-3 Toluene 10 9.3 93 70-130
79-01-6 Trichloroethylene 10 8.9 89 70-130
75-69-4 Trichlorofluoromethane 10 8.5 85 60-140
75-01-4 Vinyl chloride 10 9.9 99 60-140
1330-20-7 Xylene (total)30 28.6 95 70-130
m,p-Xylene 20 20.0 100 70-130
95-47-6 o-Xylene 10 8.6 86 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 96%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 103%70-130%
* = Outside of Control Limits.
50 of 54
FA9570 55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9569-14MS A0183628.D 50 11/04/13 TD n/a n/a VA1367
FA9569-14MSD A0183629.D 50 11/04/13 TD n/a n/a VA1367
FA9569-14 A0183631.D 50 11/04/13 TD n/a n/a VA1367
FA9569-14 A0183622.D 200 11/04/13 TD n/a n/a VA1367
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-3, FA9570-5, FA9570-6, FA9570-7, FA9570-8, FA9570-9, FA9570-10, FA9570-11, FA9570-12,
FA9570-14
FA9569-14 Spike MS MS MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene 1020 500 1590 114 1590 114 0 70-130/20
108-86-1 Bromobenzene ND 500 478 96 489 98 2 70-130/20
74-97-5 Bromochloromethane ND 500 458 92 451 90 2 70-130/20
75-27-4 Bromodichloromethane ND 500 461 92 450 90 2 70-130/20
75-25-2 Bromoform ND 500 298 60*307 61*3 70-130/20
104-51-8 n-Butylbenzene 16.0 J 500 445 86 471 91 6 70-130/20
135-98-8 sec-Butylbenzene 15.5 J 500 485 94 519 101 7 70-130/20
98-06-6 tert-Butylbenzene ND 500 461 92 495 99 7 70-130/20
108-90-7 Chlorobenzene ND 500 518 104 522 104 1 70-130/20
75-00-3 Chloroethane ND 500 556 111 520 104 7 60-140/20
67-66-3 Chloroform ND 500 474 95 469 94 1 70-130/20
95-49-8 o-Chlorotoluene ND 500 542 108 561 112 3 70-130/20
106-43-4 p-Chlorotoluene ND 500 480 96 492 98 2 70-130/20
56-23-5 Carbon tetrachloride ND 500 463 93 469 94 1 70-130/20
75-34-3 1,1-Dichloroethane ND 500 468 94 467 93 0 70-130/20
75-35-4 1,1-Dichloroethylene ND 500 480 96 485 97 1 70-130/20
563-58-6 1,1-Dichloropropene ND 500 453 91 460 92 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 500 441 88 468 94 6 70-130/20
106-93-4 1,2-Dibromoethane ND 500 478 96 487 97 2 70-130/20
107-06-2 1,2-Dichloroethane ND 500 482 96 471 94 2 70-130/20
78-87-5 1,2-Dichloropropane ND 500 494 99 482 96 2 70-130/20
142-28-9 1,3-Dichloropropane ND 500 481 96 480 96 0 70-130/20
108-20-3 Di-Isopropyl ether ND 500 420 84 414 83 1 70-130/20
594-20-7 2,2-Dichloropropane ND 500 486 97 483 97 1 70-130/20
124-48-1 Dibromochloromethane ND 500 402 80 412 82 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 500 758 152*783 157*3 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 500 486 97 477 95 2 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 500 437 87 418 84 4 70-130/20
541-73-1 m-Dichlorobenzene ND 500 515 103 530 106 3 70-130/20
95-50-1 o-Dichlorobenzene ND 500 515 103 524 105 2 70-130/20
106-46-7 p-Dichlorobenzene ND 500 471 94 480 96 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 500 462 92 450 90 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 500 462 92 454 91 2 70-130/20
100-41-4 Ethylbenzene 2780 a 500 3290 102 3380 120 3 70-130/20
87-68-3 Hexachlorobutadiene ND 500 474 95 510 102 7 70-130/20
98-82-8 Isopropylbenzene 149 500 644 99 667 104 4 70-130/20
* = Outside of Control Limits.
51 of 54
FA9570 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9569-14MS A0183628.D 50 11/04/13 TD n/a n/a VA1367
FA9569-14MSD A0183629.D 50 11/04/13 TD n/a n/a VA1367
FA9569-14 A0183631.D 50 11/04/13 TD n/a n/a VA1367
FA9569-14 A0183622.D 200 11/04/13 TD n/a n/a VA1367
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-3, FA9570-5, FA9570-6, FA9570-7, FA9570-8, FA9570-9, FA9570-10, FA9570-11, FA9570-12,
FA9570-14
FA9569-14 Spike MS MS MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 500 445 89 476 95 7 70-130/20
74-83-9 Methyl bromide ND 500 489 98 479 96 2 60-140/20
74-87-3 Methyl chloride ND 500 586 117 553 111 6 60-140/20
74-95-3 Methylene bromide ND 500 478 96 466 93 3 70-130/20
75-09-2 Methylene chloride ND 500 530 106 506 101 5 70-130/20
1634-04-4 Methyl Tert Butyl Ether 8.7 J 500 470 92 454 89 3 70-130/20
91-20-3 Naphthalene 656 500 1100 89 1200 109 9 70-130/20
103-65-1 n-Propylbenzene 399 500 898 100 947 110 5 70-130/20
100-42-5 Styrene ND 500 413 83 410 82 1 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 500 482 96 481 96 0 70-130/20
71-55-6 1,1,1-Trichloroethane ND 500 471 94 473 95 0 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 500 439 88 462 92 5 70-130/20
79-00-5 1,1,2-Trichloroethane ND 500 463 93 461 92 0 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 500 466 93 505 101 8 70-130/20
96-18-4 1,2,3-Trichloropropane ND 500 451 90 465 93 3 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 500 424 85 461 92 8 70-130/20
95-63-6 1,2,4-Trimethylbenzene 1230 500 1730 100 1800 114 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 191 500 635 89 666 95 5 70-130/20
127-18-4 Tetrachloroethylene ND 500 468 94 494 99 5 70-130/20
108-88-3 Toluene 1180 500 1690 102 1730 110 2 70-130/20
79-01-6 Trichloroethylene ND 500 463 93 463 93 0 70-130/20
75-69-4 Trichlorofluoromethane ND 500 482 96 466 93 3 60-140/20
75-01-4 Vinyl chloride ND 500 613 123 567 113 8 60-140/20
1330-20-7 Xylene (total)4910 1500 6430 101 6550 109 2 70-130/20
m,p-Xylene 4350 1000 5340 99 5440 109 2 70-130/20
95-47-6 o-Xylene 556 500 1090 107 1110 111 2 70-130/20
CAS No.Surrogate Recoveries MS MSD FA9569-14 FA9569-14 Limits
1868-53-7 Dibromofluoromethane 101%99%95%97%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%98%97%98%70-130%
2037-26-5 Toluene-D8 98%100%100%99%70-130%
460-00-4 4-Bromofluorobenzene 101%102%102%102%70-130%
(a) Result is from Run #2.
* = Outside of Control Limits.
52 of 54
FA9570 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9542-3MS A0183672.D 1 11/05/13 TD n/a n/a VA1368
FA9542-3MSD A0183673.D 1 11/05/13 TD n/a n/a VA1368
FA9542-3 A0183666.D 1 11/05/13 TD n/a n/a VA1368
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-2, FA9570-3, FA9570-4, FA9570-7, FA9570-11, FA9570-13
FA9542-3 Spike MS MS MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l %RPD Rec/RPD
71-43-2 Benzene ND 10 11.1 111 11.0 110 1 70-130/20
108-86-1 Bromobenzene ND 10 11.3 113 11.1 111 2 70-130/20
74-97-5 Bromochloromethane ND 10 10.1 101 9.9 99 2 70-130/20
75-27-4 Bromodichloromethane ND 10 11.2 112 10.6 106 6 70-130/20
75-25-2 Bromoform ND 10 9.9 99 9.9 99 0 70-130/20
104-51-8 n-Butylbenzene ND 10 9.1 91 9.6 96 5 70-130/20
135-98-8 sec-Butylbenzene ND 10 10.5 105 11.1 111 6 70-130/20
98-06-6 tert-Butylbenzene ND 10 10.6 106 10.8 108 2 70-130/20
108-90-7 Chlorobenzene ND 10 11.9 119 11.9 119 0 70-130/20
75-00-3 Chloroethane ND 10 12.9 129 11.8 118 9 60-140/20
67-66-3 Chloroform ND 10 10.9 109 10.7 107 2 70-130/20
95-49-8 o-Chlorotoluene ND 10 12.0 120 12.2 122 2 70-130/20
106-43-4 p-Chlorotoluene ND 10 10.9 109 11.1 111 2 70-130/20
56-23-5 Carbon tetrachloride ND 10 10.7 107 10.7 107 0 70-130/20
75-34-3 1,1-Dichloroethane ND 10 10.9 109 11.3 113 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 10 10.9 109 11.2 112 3 70-130/20
563-58-6 1,1-Dichloropropene ND 10 11.5 115 11.7 117 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10 10.0 100 10.2 102 2 70-130/20
106-93-4 1,2-Dibromoethane ND 10 11.4 114 11.6 116 2 70-130/20
107-06-2 1,2-Dichloroethane ND 10 11.3 113 11.1 111 2 70-130/20
78-87-5 1,2-Dichloropropane ND 10 11.5 115 11.1 111 4 70-130/20
142-28-9 1,3-Dichloropropane ND 10 11.2 112 11.2 112 0 70-130/20
108-20-3 Di-Isopropyl ether ND 10 9.0 90 9.0 90 0 70-130/20
594-20-7 2,2-Dichloropropane ND 10 11.2 112 11.1 111 1 70-130/20
124-48-1 Dibromochloromethane ND 10 10.8 108 10.6 106 2 70-130/20
75-71-8 Dichlorodifluoromethane ND 10 15.9 159*16.3 163*2 60-140/20
156-59-2 cis-1,2-Dichloroethylene ND 10 11.2 112 11.1 111 1 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10 8.8 88 8.2 82 7 70-130/20
541-73-1 m-Dichlorobenzene ND 10 12.2 122 12.5 125 2 70-130/20
95-50-1 o-Dichlorobenzene ND 10 12.1 121 12.1 121 0 70-130/20
106-46-7 p-Dichlorobenzene ND 10 10.9 109 11.0 110 1 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10 10.5 105 10.8 108 3 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10 10.1 101 9.9 99 2 70-130/20
100-41-4 Ethylbenzene ND 10 11.0 110 11.4 114 4 70-130/20
87-68-3 Hexachlorobutadiene ND 10 10.7 107 11.4 114 6 70-130/20
98-82-8 Isopropylbenzene ND 10 10.6 106 11.1 111 5 70-130/20
* = Outside of Control Limits.
53 of 54
FA9570 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA9570
Account:GRINCC GRI (Geological Resources Inc.)
Project:Handee Hugo 5; 1210 N Main St, Bladenboro, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA9542-3MS A0183672.D 1 11/05/13 TD n/a n/a VA1368
FA9542-3MSD A0183673.D 1 11/05/13 TD n/a n/a VA1368
FA9542-3 A0183666.D 1 11/05/13 TD n/a n/a VA1368
The QC reported here applies to the following samples:Method: SM 6200B
FA9570-1, FA9570-2, FA9570-3, FA9570-4, FA9570-7, FA9570-11, FA9570-13
FA9542-3 Spike MS MS MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10 10 100 10.7 107 7 70-130/20
74-83-9 Methyl bromide ND 10 12.0 120 11.3 113 6 60-140/20
74-87-3 Methyl chloride 0.18 J 10 12.6 124 12.4 122 2 60-140/20
74-95-3 Methylene bromide ND 10 11.1 111 11.0 110 1 70-130/20
75-09-2 Methylene chloride ND 10 10.4 104 10.3 103 1 70-130/20
1634-04-4 Methyl Tert Butyl Ether 10 10 20.6 106 21.2 112 3 70-130/20
91-20-3 Naphthalene ND 10 9.4 94 10 100 6 70-130/20
103-65-1 n-Propylbenzene ND 10 12.3 123 12.5 125 2 70-130/20
100-42-5 Styrene ND 10 9.6 96 9.4 94 2 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10 11.4 114 11.2 112 2 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10 11.0 110 11.1 111 1 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10 10.5 105 10.9 109 4 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10 11.0 110 11.1 111 1 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10 11.5 115 12.1 121 5 70-130/20
96-18-4 1,2,3-Trichloropropane ND 10 10.6 106 11.0 110 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10 9.7 97 10.1 101 4 70-130/20
95-63-6 1,2,4-Trimethylbenzene ND 10 9.9 99 10.0 100 1 70-130/20
108-67-8 1,3,5-Trimethylbenzene ND 10 9.4 94 9.7 97 3 70-130/20
127-18-4 Tetrachloroethylene ND 10 10.9 109 11.3 113 4 70-130/20
108-88-3 Toluene ND 10 11.0 110 11.2 112 2 70-130/20
79-01-6 Trichloroethylene ND 10 10.9 109 10.9 109 0 70-130/20
75-69-4 Trichlorofluoromethane ND 10 11.1 111 10.7 107 4 60-140/20
75-01-4 Vinyl chloride ND 10 12.8 128 12.6 126 2 60-140/20
1330-20-7 Xylene (total)0.51 J 30 35.8 118 36.1 119 1 70-130/20
m,p-Xylene 0.17 J 20 24.3 121 24.7 123 2 70-130/20
95-47-6 o-Xylene 0.33 J 10 11.5 112 11.4 111 1 70-130/20
CAS No.Surrogate Recoveries MS MSD FA9542-3 Limits
1868-53-7 Dibromofluoromethane 103%100%99%70-130%
17060-07-0 1,2-Dichloroethane-D4 103%102%100%70-130%
2037-26-5 Toluene-D8 99%100%102%70-130%
460-00-4 4-Bromofluorobenzene 101%101%103%70-130%
* = Outside of Control Limits.
54 of 54
FA9570 55.3.2