FA-610_11196_CA_SCH_20210908

 
WithersRavenel
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115 MacKenan Drive | Cary, NC 27511 
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C‐0832 
Asheville | Cary | Greensboro | Pittsboro | Raleigh | Wilmington 

SITE CHECK REPORT 

Former C.C. Newell Store 
NCDEQ Incident #11196 
UST # FA‐610 
216 Camp Easter Road, Unit A 
Carthage, Moore County, North Carolina 
WithersRavenel Project No. 02172214.97 

Prepared for: 
State of North Carolina 
Department of Environmental Quality 
Division of Waste Management  
Underground Storage Tank Section 
Federal & State Lead Program 
1646 Mail Service Center 
Raleigh, North Carolina 27699‐1646 

Prepared by:
WithersRavenel
115 MacKenan Drive 
Cary, North Carolina 27511 
North Carolina Firm License No. C‐0832 
October 8, 2021
WithersRavenel
Our People. Your Success. 

Former C.C. Newell Store WR Project # 02172214.97 
Site Check Report October 2021 
ii 

October 8, 2021 

State of North Carolina 
Department of Environmental Quality 
Federal & State Lead Program 
Division of Waste Management‐Underground Storage Tank Section 
1646 Mail Service Center 
Raleigh, North Carolina 27699‐1646 

Attn:  Mr. Hassan Osman 

Re:  Site Check Report  
Former C.C. Newell Store 
216 Camp Easter Road 
Carthage, Moore County, North Carolina 
Groundwater Incident Number: 11196 
UST Number: FA‐610 
WR Project Number:  02172214.97 

Mr. Osman, 
WithersRavenel, Inc. (WR) has completed this Site Check Report to document soil, groundwater, 
and sub‐slab vapor sampling activities completed at the site in association with our proposal, 
numbered TA‐03 and associated change orders, for the above referenced site, approved by the 
Federal & State Lead Program on August 4, 2021.   

The enclosed report summarizes results of the recently completed monitoring activities.    

WR appreciates the opportunity to be of service to the Federal & State Lead Program.  Should you 
have any questions regarding the attached, please contact Matthew James at (919) 469‐3340. 

Cordially, 
WithersRavenel 
  David Vail G. Matthew James, PG 
Environmental Staff Professional I Senior Geologist 

WithersRavenel
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Former C.C. Newell Store WR Project # 02172214.97 
Site Check Report October 2021 
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TABLE OF CONTENTS 

SECTION A: SITE INFORMATION ..................................................................................................................... 1 
SECTION B. EXECUTIVE SUMMARY ................................................................................................................ 3 
SECTION C.  SITE HISTORY AND CHARACTERIZATION ........................................................................... 6 
SECTION D.  SOIL, GROUNDWATER, & SUB‐SLAB VAPOR ASSESSMENT – JULY‐AUG 2021 ..... 9 
SECTION E.  CONCLUSIONS AND RECOMMENDATIONS .................................................................... 12 

FIGURES  
Figure 1 General Location Map 
Figure 2 Site Map 
Figure 3A Soil Analytical Results – July 2021 
Figure 3B Groundwater Analytical Results – July & August 2021 
Figure 3C Sub‐Slab Vapor Analytical Results – July 2021 
Figure 4 Receptor Map 

TABLES  
Table B‐1 Site History: UST/AST System & Other Release Information 
Table B‐3 Summary of Soil Analytical Results  
Table B‐4 Summary of Groundwater Analytical Results 
Table B‐5A Public & Private Water Supply Well Information 
Table B‐5B Additional Receptor Information 
Table B‐5C Adjacent Property Information 
Table B‐7 Monitoring & Remediation Well Construction Information 
Table B‐10 Summary of Indoor Air Vapor Analytical Results 
Table B‐11 Summary of Sub‐Slab Vapor Analytical Results 

APPENDICES  
Appendix A Boring Log & Well Construction Record  
Appendix B Laboratory Analytical Reports and Chains‐of‐Custody  
Appendix C Field Notes and Photographic Record 
Appendix D NCDEQ Risk Calculator 
Appendix E Standard Operating Procedures 

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Former C.C. Newell Store WR Project # 02172214.97 
Site Check Report October 2021 
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SECTION A: SITE INFORMATION  
1. Site Identification 
Date of Report:  October 8, 2021 
Facility I.D.: 00‐0‐0000033411 
Incident No.: 11196 
Site Risk: Intermediate  
Site Rank: I190D 
Land Use Category: Business (Moore County Zoning B‐2) 
Site Name: Former C.C. Newell Store 
Site Location: 216 Camp Easter Road, Unit A 
Nearest City/Town: Carthage 
County: Moore 
Description of Geographical Data Point:  Center of Former Pump Island 
Location Method:  Google Earth 
Latitude: 35.241181° 
Longitude: ‐79.306578° 
2. Contact Information 
Responsible Party: Unknown 

Property Owner 216 CER Holding, LLC 
Address: 175 W. New Hampshire Ave 
Southern Pines, NC 28387 
Phone: 910‐692‐9771 

Property Occupant: VTG Canine Sports Medicine & Rehab Mobile Clinic 
Address: 216 Camp Easter Road, Unit A 
Carthage, NC  
Phone: 910‐818‐8436 

Consultant/Contractor: WithersRavenel 
Address:  115 MacKenan Drive, Cary, NC 27511 
Phone:  919‐469‐3340 

Analytical Laboratory: Waypoint Analytical, LLC  
State Certification Number: ENV402 
Address: 449 Springbrook Rd., Charlotte, NC 28217 
Phone: 704‐529‐6364 

Analytical Laboratory: Con‐Test  
State Certification Number: ENV652 
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Address: 39 Spruce Street, East Longmeadow, MA 01028 
Phone: 413‐525‐2332 
Analytical Laboratory: Eurofins Air Toxics LLC  
State Certification Number: ‐‐‐ 
Address: 180 Blue Ravine Rd, Suite B, Folsom, CA 95630 
Phone: 916‐985‐1000 
3.Release Information
Date Discovered:  December 1993 
Estimated Quantity of Release:  Unknown 
Cause of Release:  Compromised UST or Delivery System 
Source of Release: UST or Delivery System 
Type of Material Release Occurred: Petroleum 
Criteria Used to Classify Risk: Surface Water Body within 100‐feet, 
Potential for Vapor Intrusion 
Sizes & Contents of UST System(s) from which 
Release Occurred: 
(2)4,000‐gallon gasoline, (1) 2,000‐gallon gasoline,
(1)550‐gallon gasoline and (1) 550‐gallon kerosene
USTs
4.Information about Monitoring Report
Date(s) of Assessment/Monitoring Event(s):July 1, July 2, July 21, & August 17, 2021 
5.Certification
I, G. Matthew James, a Licensed Geologist for 
WithersRavenel, do certify that the information 
contained in this report is correct and accurate to 
the best of my knowledge. 
WithersRavenel, is licensed to practice 
geology/engineering in North Carolina.  
The certification numbers are C‐293 (Geology) and 
C‐0451 (Engineering). 
10-8-21
WithersRavenel
Our People. Your Success. 

Former C.C. Newell Store WR Project # 02172214.97 
Site Check Report October 2021 
3 

SECTION B. EXECUTIVE SUMMARY 

1. Summary of Activities Associated with Current TA 

WithersRavenel, Inc. (WR) conducted soil, groundwater and sub‐slab vapor sampling activities, as 
well as monitoring well installation at the Former C.C. Newell Store site located at 216 Camp 
Easter Road, Unit A in Carthage, Moore County, North Carolina in association with TA‐03 under 
NCDEQ Contract #N122019B.   

2. Soil, Groundwater, Free Product, Indoor Air, and Sub‐Slab Vapor Assessment Information 

Soils 
Previous site work between the dates of March 29 to April 3, 2021, included collecting soil samples 
from four soil borings (B‐1, B‐2, B‐3 and B‐4) during the installation of monitoring wells MW‐2, 
MW‐3, MW‐4 and MW‐5, respectively. The soil samples showed diesel range organics (DRO) as 
total petroleum hydrocarbons (TPH) in each sample.  Levels of DRO TPH in the sample from boring 
B‐2 (MW‐3) were reported in excess of the NCDEQ Action Level.  Gasoline range organics (GRO) 
as TPH were reported in three of the four samples.  Levels of GRO TPH in samples from B‐2 (MW‐
3) and B‐3 (MW‐4) were in excess of the NCDEQ Action Level.   

Soil samples associated with this TA were obtained on July 1, 2021, from sub‐slab sample locations 
within the building footprint (WR‐1, WR‐2, WR‐3) as well as from locations between the building 
and former pump island (WR‐4 and WR‐5). On July 21, 2021, WR collected soil samples from sub‐
slab sample locations within the former oil change bay room inside the building footprint (WR‐6, 
WR‐8, and WR‐9). WR‐7 was located in the center of the former mechanic’s trench but was not 
sampled as the soils were completely saturated.  

Each soil sample collected on July 1 and July 21, 2021, was analyzed by Environmental Protection 
Agency (EPA) Methods 8260D, 8270E, MADEP (Massachusetts Department of Environmental 
Protection) Extractable Petroleum Hydrocarbons (EPH) and MADEP Volatile Petroleum 
Hydrocarbons (VPH). Samples WR‐1, WR‐2, WR‐6, WR‐8, and WR‐9 were also analyzed by EPA 
Method 6020B (Chromium and Lead). Analytical results indicated that WR‐1 contained Chromium 
at levels above the Commercial / Industrial cleanup levels. WR‐2 contained Chromium at levels 
above the Commercial / Industrial cleanup levels and Naphthalene and Aromatic C9‐C10 at levels 
above the Soil‐to‐Groundwater Maximum Soil Contaminant Concentration Levels (MSCCs), but 
below the Residential MSCCs. WR‐3, WR‐4 and WR‐5 did not have any detections above the Soil‐
to‐Groundwater MSCCs. WR‐6, WR‐8, and WR‐9 were found to have detections of Chromium in 
excess of the Commercial / Industrial cleanup levels. 

Groundwater  
During the course of this TA, WR obtained groundwater samples from monitoring wells MW‐1, 
MW‐2, MW‐3, MW‐4, MW‐5, and MW‐6, as well as from the temporary wells that were installed 
in the soil borings WR‐6 (Temporary Well ‐ TW), WR‐7 (TW), WR‐8 (TW), and WR‐9 (TW) that 
were advanced into the water table, and from WSW‐1 (located at 216 Camp Easter Road, Unit B). 
MW‐1 to MW‐5 were gauged, purged, and sampled on July 1, 2021. An attempt to install MW‐6 
with a hand auger was made on this day. The pre‐packed well screen and riser pipe were set and 
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the void space around the screen and riser were filled with #2 well sand. No water entered the 
well, and WR returned on July 2, 2021, to check the depth to water in the well. During the night 
or July 1 and the morning of July 2, strong storms passed through the area and inundated the area 
east of the building, flooding the well.  The water level was approximately 0.7’ below the top of 
the casing, and just as much water was present outside of the casing, above the screen pack. It 
was determined that this water in the well was likely not groundwater and instead was rainwater. 
Due to the lack of water encountered at a depth of 8.5 feet Below Ground Surface (BGS), the 
inundation of the surrounding area and likely cross contamination from rainwater in this boring, a 
drill rig was utilized on July 21, 2021, to install the well in a nearby location. The well was installed 
to a depth of 26 feet BGS, with first water being encountered in the soils between 23‐24 feet 
BGS. The well went dry during development and did not recharge on this day. On August 17, 2021, 
WR re‐mobilized to the site to collect groundwater samples from WSW‐1 (located at 216 Camp 
Easter Road, Unit B), gauge, purge, and sample MW‐6, and install temporary wells WR‐6 (TW), 
WR‐7 (TW), WR‐8 (TW), and WR‐9 (TW), and gauge, develop, sample, and abandon the temporary 
wells. MW‐1 to MW‐6 and WSW‐1 were analyzed by SM 6200B, WR‐6 (TW) to WR‐9 (TW) were 
analyzed by SM 6200B, 625.1, MADEP EPH, and MADEP VPH.    

Laboratory results for the samples indicated the presence of one or more compounds targeted by 
SM6200B in MW‐1, MW‐3, MW‐4, MW‐5, WR‐6 (TW), and WR‐9 (TW). Concentrations of 
benzene (MW‐3 and MW‐4), 1,2‐dichloroethane (MW‐1), and Methyl‐tert‐Butyl Ether (MTBE) 
(MW‐1) were reported in excess of their respective 2L Standards. Benzene was detected at levels 
ten times the NC Surface Water 2B Standards in MW‐3 in the July 1, 2021, sample.  None of the 
compounds reported in any of the samples were at concentrations exceeding their respective 
GCLs.  There were no detections of compounds targeted by Method 625.1, MADEP EPH or VPH. 
MW‐2, MW‐6, WR‐7 (TW), WR‐8 (TW), and WSW‐1 were not found to have targeted compounds 
at levels above the minimum laboratory detection limits. 

Free Product 
No free product was measured in any of the permanent or temporary monitoring wells sampled 
on July 1, 2021, July 21, 2021, or August 17, 2021.   

Indoor Air 
Previously completed assessment included an 8‐hour indoor air sample (IAS‐1) obtained from 
within the site structure on April 3, 2021, that indicated the presence of numerous chemical 
compounds.  Several of the compounds reported in the sample were in excess of their respective 
Indoor Air/Crawlspace Residential Vapor Intrusion Screening Levels (NCDEQ, January 2021).  
Indoor air results were also inserted in the NCDEQ Risk Calculator and Indoor Air exceeded the 
carcinogenic risk for both Residential and Non‐Residential air. 

Sub‐Slab Vapor 
On July 1, 2021, WR installed two vapor pins through the slab of the building for assessing the 
sub‐slab vapors present below the building. Two one‐liter stainless steel, batch certified summa 
canisters with <100 mL/hr flow controllers (approximately 10‐minute flow controllers) were 
utilized to collect the samples. The vapor pins and the summa canisters/flow controllers were 
connected utilizing Teflon tubing.  

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The samples were analyzed by analytical method TO‐15. The analytical results indicated several 
low‐level detections of targeted constituents in both samples (SSV‐1 and SSV‐2). All of the 
compounds reported in the samples were below their respective Non‐Residential Vapor Intrusion 
Screening Levels (NCDEQ, January 2021). Sub‐Slab Vapor results were also inserted in the 
NCDEQ Risk Calculator, and the results indicated that there were no risk exceedances for 
Residential or Non‐Residential workers from the soil gas to indoor air pathway under the present 
scenario or future scenarios at the site.  

3.       Receptor Information 

Although no receptor survey was completed by WR in association with this TA, WR identified the 
presence of a Freshwater Forested/Shrub Wetland (PFO4B) located immediately northeast of the 
site and a Lake Habitat (L1UBHh) located immediately west of the site.  Each of these wetland 
features are indexed by the US Fish & Wildlife Service (FWS), National Wetlands Inventory.  

In addition, while conversing with neighboring property owners, it was revealed to WR that there 
are two water supply wells (WSWs) located on the northern adjoining property. One well is 
completely inactive and does not have power to the pump. The other well (WSW‐1) is located 
approximately 100’ north of the source area. The well is a 35‐foot deep, approximately 18‐inch 
wide, bored well.  The well is not used for drinking but is used for the restrooms in the adjoining 
building.  

4. Remediation Activities 

Five petroleum USTs were reportedly removed from the location in December 1993.  NCDEQ 
records state that soil samples obtained in association with UST closures indicated a release, 
however, no physical records of assessment at the location were made available to WR.   NCDEQ 
stated that one UST was abandoned in‐place adjacent to the former dispenser island. 

5. Recommendations 

Based on the results of assessment and monitoring activities conducted at the site in association 
with this TA, WR recommends having the property owner remove building materials impacted by 
the petroleum impacted water and retesting the indoor air.  If indoor air concentrations continue 
to exceed non‐residential carcinogenic risk, the installation of an active mitigation or passive 
venting system to deplete contaminant concentrations in the structure may be needed. 

WithersRavenel
Our People. Your Success. 

Former C.C. Newell Store WR Project # 02172214.97 
Site Check Report October 2021 
6 

SECTION C.  SITE HISTORY AND CHARACTERIZATION 

WR has completed assessment and sampling activities at the referenced site in association with 
TA‐03.  The following information summarizes the site history and characterization.   

1. UST Information 

The site is located within an incorporated area of Carthage, Moore County, NC (Figure 1), 
addressed as 216 Camp Easter Road, Unit A.  Five petroleum USTs, identified as (2) 4,000‐gallon 
(gal) gasoline, (1) 2,000‐gal gasoline, (1) 550‐gal gasoline and (1) 550‐gal kerosene tanks were 
reportedly removed from the property in December 1993 (Table B‐1). Additional review of 
historical files indicates that only four certificates of disposal exist for the five USTs, and that there 
seems to be one 550‐gallon tank unaccounted for. No information is presently available regarding 
the ownership or operation of the UST systems.   

Research of the Facility ID Number (00‐0‐0000033411) associated with the property through the 
NCDEQ Excel databases “tblAllTanks” and “tblUSTDB” identify the RP Company as “CC Newell 
Store” and RP as Linda Oldham.  Soil samples obtained from the site at the time of the UST closures 
“indicated a release”.     

2.       Description of Release/General Assessment History 

The following summary of the assessment history is based on WR’s review of historical files for 
the subject incident: 

 Five petroleum USTs were permanently closed through removal during December 1993.  WR 
was not provided any records relating to the closure of the UST systems (e.g., Closure Report). 
o It is WR’s understanding that one UST was close in‐place adjacent to the former 
dispenser island.  
 In February 2021, the NCDEQ received a complaint about petroleum vapor intrusion in the 
on‐site building. DEQ staff visited the site and confirmed the strong petroleum odor and 
noticed LNAPL seeping out around the foundation at the front of the building. The source of 
the petroleum was not able to be identified.  

No additional records of any assessment at the property are available through NCDEQ Laserfiche, 
however a permanent monitoring well (MW‐1) had been installed on the property at some point 
in time.   

3.  Brief Description of Site Characteristics 

The property is located at 216 Camp Easter Road, Unit A in Carthage, Moore County, North 
Carolina (Figure 2).  The property includes a single‐story block structure.  The structure shares a 
common wall with the adjoining property – 216 Camp Easter Road, Unit B (owned by James S. & 
Kimberly Von Cannon).   

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The subject property includes 0.17 acres of land, approximately 1/2 of which is developed with 
structures and/or concrete and asphalt paved areas.  The remainder of the parcel is covered with 
moderate to dense tree/shrub growth.  The Moore County parcel ID for the property is 00037218, 
while the NC PIN is 950416825805.   

Surface drainage through the area generally follows topography or is channeled through wet 
weather ditches running parallel to primary and secondary roadways.  Near the source location, 
surface drainage flows to the west, towards Crystal Lake (approximately 100’ away) and south 
towards the outfall of Crystal Lake (Mill Creek – approximately 350’ away).  Mill Creek drains to 
the east to the Little River within the Cape Fear River drainage basin.     

4.       Information on Receptors/Potential Receptors 

Although no receptor survey was completed by WR in association with this TA, WR identified the 
presence of a Freshwater Forested/Shrub Wetland located immediately northeast of the site and 
a Lake Habitat located immediately west of the site.  Each of these wetland features are indexed 
by the US FWS, National Wetlands Inventory. 

 Freshwater Forested/Shrub Wetland (PFO4B) ‐ Paulustrine, Forested, Needle‐Leaved 
Evergreen, Seasonally Saturated. 
 Lake Habitat (L1UBHh) ‐ Lacustrine, Limnetic, Unconsolidated Bottom, Permanently Flooded, 
Diked/Impounded. 

While WR did not complete a receptor survey under the current TA, WR personnel recognized the 
presence of several supply wells (of confirmed use) located on properties to the north of the site.  
While municipal water is available to the site and surrounding properties, the potential exists for 
the use of one or more potable supply wells in the vicinity of the site.  It was reported to WR by 
the neighboring property owner of 216 Camp Easter Road Unit B, that one of the wells is inactive 
and not utilized, and the other well (WSW‐1) is utilized for non‐potable sources (restrooms), and 
that they rely on bottled water for drinking. 

The site and surrounding properties are serviced by the municipal water supply system, however, 
WR made no attempt at verifying the use of private supply wells while at the location.  The NC 
Source Water Assessment Program (SWAP) does not identify any community supply wells or 
wellhead protection areas within a one‐mile radius of the site.   

The site is located in the western portion of the Coastal Plain Physiographic Province of North 
Carolina and situated in a location characterized by sediments of Cretaceous age within the Cape 
Fear Formation.  Underlying materials are described as “Sandstone and sandy mudstone, yellowish 
gray to bluish gray, mottled red to yellowish orange, indurated, grading and laterally continuous 
bedding, blocky clay, faint cross‐bedding, feldspar and mica common”.       

Additional receptors in the vicinity of the site include Crystal Lake, located approximately 100 feet 
west of the source of the release and the dam/outfall of the lake, Mill Creek, located approximately 
350 feet south of the source of the release. The NCDEQ NC Surface Water Classifications website 
identifies Crystal Lake as Water Supply III (WS‐III), Class B; High Quality Waters (HQW) and Mill 
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Creek below the Crystal Lake dam as WS‐III; HQW. WS‐III is defined by the NC Surface Water 
Classification website as water used as sources of water supply for drinking, culinary, or food 
processing purposes where a more protective WS‐I or II classification is not feasible. These waters 
are also protected for Class C uses. WS‐III waters are generally in low to moderately developed 
watersheds. Class B waters are defined as waters protected for all Class C uses (secondary 
recreation, fishing, wildlife, fish consumption, aquatic life including propagation, survival, and 
maintenance of biological integrity, and agriculture. Secondary recreation includes wading, 
boating, and other uses involving human body contact with water where such activities take place 
in an infrequent, unorganized, or incidental manner.), in addition to primary recreation. Primary 
recreational activities include swimming, skin diving, water skiing, and similar uses involving human 
body contact with water where such activities take place in an organized manner or on a frequent 
basis. HQW is a supplemental classification intended to protect waters which are rated excellent 
based on biological and physical/chemical characteristics through Division monitoring or special 
studies, primary nursery areas designated by the Marine Fisheries Commission, and other 
functional nursery areas designated by the Marine Fisheries Commission.  

5.        Interviews with Neighboring Property Owners 

During the assessment period associated with this TA, WR had the opportunity to interview two 
of the neighboring property owners. On July 1, 2021, Mr. Freddie McKenzie, the long‐time owner 
of the southern adjacent property located at 202 Camp Easter Road, visited the site. Mr. McKenzie 
reported that the southern end of the on‐site building was formerly utilized as a mechanic’s shop 
and performed oil changes. The former mechanic’s bay/oil change bay formerly had an 
approximately six‐foot‐deep trench through the center of the bay to allow a mechanic to stand up 
beneath the vehicle that was being worked on. Mr. McKenzie reported that he could remember 
there being plenty of oil that spilled in the trench during oil changes, and other times when the 
mechanics had to stand on milkcrates in the trench due to groundwater being present in the 
trench. He reported that the shop wasn’t very busy and was used more periodically than regularly. 
In addition to this information regarding the on‐site building, Mr. McKenzie shared additional 
information about his property to the south of the site. He stated that in the 1970’s he had a well 
drilled on the southeast end of his building. The water was deemed “swamp water” and had a 
sheen on it, so he couldn’t use the well. He reported that the whole swamp southeast of him has 
had a sheen in the past.  

On this same day, the northern adjoining property owner James (Jim) Von Canon, who owns 216 
Camp Easter Rd, Unit B came to discuss the site with WR staff and DEQ staff. Mr. Von Canon 
stated that there was formerly a 4‐ to 5‐foot‐wide concrete octagon located behind (east) of the 
site building (216 Camp Easter Rd Unit A). He reported that there was a 6‐ to 8‐inch‐wide 
terracotta pipe in the center of the octagon that extended down into the earth an unknown depth 
and was formerly used as an “oil dump” for waste oil to be discarded. Mr. Von Canon reported that 
this “oil dump” was in place until recently, when the current property owner re‐graded the area 
behind the building and installed two new septic holding tanks.  

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On July 21, 2021, Mr. Von Canon reported to WR that he has two water supply wells on his 
property.  He reported that the closest well (WSW‐1) was connected to the restrooms in the 
apartment unit in 216 Camp Easter Rd Unit B, and that the second well (WSW‐2), while currently 
inactive, has just been used for washing cars in recent years.  

SECTION D.  SOIL, GROUNDWATER & SUB‐SLAB VAPOR ASSESSMENT – JULY ‐ AUGUST 
2021 

On July 1, 2021, WR personnel mobilized to the subject property to perform soil, groundwater, 
and sub‐slab vapor assessment activities at the facility in association with TA‐03 under NCDEQ 
Contract # N122019B. WR returned to the site on July 2, 2021, to check the water level in the 
newly installed MW‐6, however, heavy rains had inundated the area and filled the well boring and 
well with rainwater. WR returned to the location on July 21, 2021, for the purposes of obtaining 
additional soil samples, and overseeing the installation of a Type II groundwater monitoring well 
(MW‐6) with a drill rig.  On August 17, 2021, WR returned to the site again for the purposes of 
installing four temporary monitoring wells, collecting groundwater samples from the temporary 
wells, and collecting groundwater samples from WSW‐1 and from MW‐6. The following 
paragraphs describe the sampling activities and associated laboratory analytical results.  

D.1. SOIL BORINGS AND MONITORING WELL INSTALLATIONS/SAMPLING 

On July 1, 2021, WR advanced five soil borings (WR‐1, WR‐2, WR‐3, WR‐4, and WR‐5) at the site. 
The soils were characterized, screened with a Photoinization Detector (PID), and placed in 
laboratory supplied/prepared sample containers. In addition to these soil samples collected on this 
day, WR gauged MW‐1 to MW‐5 with an electronic water level indicator prior to purging and 
sampling using a peristaltic pump and virgin polyethylene (PE) tubing. WR also advanced boring 
for MW‐6 to a depth of 8.5 feet BGS, however the well did not produce water. On July 2, 2021, 
WR revisited the site to check the depth to water in MW‐6, however, significant rainfall had 
inundated the area and filled the well and boring with rainwater. On July 21, 2021, WR mobilized 
to the site to witness the installation of one permanent Type‐II monitoring well (MW‐6) and to 
advance four soil borings (WR‐6, WR‐7, WR‐8, and WR‐9). On August 17, 2021, the soil borings 
WR‐6, WR‐7, WR‐8, and WR‐9 were then converted into temporary monitoring wells (WR‐6 (TW), 
WR‐7 (TW), WR‐8 (TW), and WR‐9 (TW)). During this site visit, WR also sampled WSW‐1 and 
gauged and purged MW‐6 (Figure 2). Samples WR‐1, WR‐2, WR‐3, WR‐6, WR‐8, and WR‐9 were 
collected from beneath the slab within the building footprint. Samples WR‐4 and WR‐5 were 
collected from locations beneath the concrete pavement between the building and former pump 
island. WR‐7 was not sampled as the soils were completely saturated. Each of the borings were 
advanced using a decontaminated hand auger after using a hammer drill to core the slab in each 
location.   

During advancement of soil borings, samples were obtained from each boring for screening and 
characterization. The depth intervals from each boring that exhibited the highest PID readings was 
collected as a single soil sample and submitted to Waypoint Analytical for laboratory analysis by 
EPA Methods 8260D, 8270E, MADEP EPH and VPH. Samples WR‐1, WR‐2, WR‐6, WR‐8, and 
WR‐9 were also analyzed by EPA Method 6020B (Chromium and Lead).  Results of this testing are 
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discussed in Section D.2, below. Due to the varying depth to groundwater, the depth of the borings 
and samples ranged from 2.0 feet below ground surface (BGS) to 3.0 feet BGS.  

Monitoring well MW‐6 was installed on July 21, 2021, by Quantex, Inc. The well was installed with 
a Geoprobe track‐mounted rig utilizing six‐inch augers. The well was constructed with two‐inch 
PVC Sch 40 screen with a slot size of 0.010 from 11 to 26 feet and two‐inch PVC Sch 40 riser pipe 
from 0 to 11 feet. The void space surrounding the PVC well screen and riser pipe was backfilled 
with #2 well sand from 9 to 26 feet, bentonite from 7 to 9 feet, and neat cement from 0 to 7 feet. 
The well was finished with a standard size flush‐mount manhole cover set in a concrete pad. 

Soil borings WR‐6, WR‐7, WR‐8, and WR‐9 were advanced below the water table after soil 
samples were collected so that the borings could later be converted to temporary monitoring wells.  
Each temporary well (WR‐6 (TW), WR‐7 (TW), WR‐8 (TW), and WR‐9 (TW)) was constructed with 
5‐ft of 1‐inch (in) diameter (dia) slotted PVC well screen, with the exception of WR‐7 (TW) where 
a 2” screen was utilized.  Following installation, the well screen was surrounded with #2 well sand 
extending to approximately 6‐in above the water table.  After the sampling was completed, the 
screens were removed and the holes were backfilled with #2 well sand, followed by bentonite, and 
a cement to patch the slab.   

Following installation, each well was gauged with an electronic water level indicator and 
developed/purged using a peristaltic pump using virgin polyethylene (PE) tubing, or a dedicated 
polyethylene bailer where possible (MW‐6).  Water levels as measured on July 1 and August 17, 
2021, are shown in Table B‐7, ranging from 1.05 to 12.76‐ft beneath the top of well casings.  
Following development/purging, each well was sampled using laboratory prepared sample 
containers including chemical preservatives specific to the analysis requested.  All of the samples 
collected were transferred to Waypoint Analytical under Chain‐of‐Custody procedures.  MW‐1 to 
MW‐6 and WSW‐1 were analyzed by SM 6200B, WR‐6 (TW) to WR‐9 (TW) were analyzed by SM 
6200B, 625.1, MADEP EPH, and MADEP VPH.    

D.2. LABORATORY RESULTS – SOIL AND GROUNDWATER SAMPLES 

Laboratory Results – Soil Samples 
Analytical results for the soil sample obtained from borings WR‐1 to WR‐9 (with the exception of 
WR‐7 – not sampled) showed the following: 
 EPA‐6020B (Chromium and Lead) – Chromium was reported in WR‐1, WR‐2, WR‐6, WR‐8, 
and WR‐9 at levels that exceeded the Commercial / Industrial Cleanup Levels. Lead was 
detected in these same samples, but below the Soil‐to‐Groundwater MSCC. No other samples 
were analyzed for Chromium and Lead.      
 EPA‐8260D – There were no detections above the laboratory minimum detection limits for 
this analysis for soil samples WR‐1, WR‐3, WR‐4, WR‐6, WR‐8, and WR‐9. Sample WR‐2 and 
5 both had several detections of target constituents above the minimum laboratory detection 
limits, but below the Soil‐to‐Groundwater MSCCs. WR‐2 also contained Naphthalene at a 
concentration above the Soil‐to‐Groundwater MSCC, but below the Residential soil cleanup 
levels.  
 EPA‐8270E – There were no detections above the laboratory minimum detection limits for 
this analysis for soil samples WR‐1, WR‐2, WR‐3, WR‐4, WR‐5, WR‐6, WR‐8, and WR‐9. 
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 MADEP EPH – There were no detections above the laboratory minimum detection limits for 
this analysis for soil samples WR‐1, WR‐2, WR‐3, WR‐4, WR‐5, WR‐6, WR‐8, and WR‐9. 
MADEP VPH – There were no detections above the laboratory minimum detection limits for 
this analysis for soil samples WR‐1, WR‐3, WR‐4, WR‐5, WR‐6, WR‐8, and WR‐9. Sample WR‐
2 contained Aliphatic C5‐C8 and Aliphatic C9‐C12 at concentrations above the minimum 
laboratory detection limits, but below the Soil‐to‐Groundwater MSCCs, and Aromatic C9‐C10 
at a concentration above the Soil‐to‐Groundwater MSCC, but below the Residential Soil 
Cleanup Levels.       

These results are illustrated on Figure 3A included in Table B‐3, while the laboratory report is 
included in Appendix B.  Field notes and site photographs are included in Appendix C.   

Laboratory Results – Groundwater Samples 
Analytical results for the groundwater samples obtained from MW‐1, MW‐2, MW‐3, MW‐4, MW‐
5, MW‐6, WR‐6 (TW), WR‐7 (TW), WR‐8 (TW), WR‐9 (TW), and WSW‐1 showed the following: 
 SM6200B – One or more compounds were reported in samples MW‐1, MW‐3, MW‐4, MW‐
5, WR‐6 (TW), and WR‐9 (TW).  
o Concentrations of benzene (MW‐3 and MW‐4), 1,2‐dichloroethane (MW‐1), and 
Methyl‐tert‐Butyl Ether (MTBE) (MW‐1) were reported in excess of their 
respective 2L Standards.  
o Benzene was detected at levels ten times the NC Surface Water 2B Standards in 
MW‐3 in the July 1, 2021, sample.  
o None of the compounds reported in any of the samples were at concentrations 
exceeding their respective GCLs.   
 625.1 – There were no detections of target compounds above the minimum laboratory 
detection limits for this analysis. 
 MADEP EPH – There were no detections of target compounds above the minimum laboratory 
detection limits for this analysis. 
 MADEP VPH – There were no detections of target compounds above the minimum laboratory 
detection limits for this analysis. 

These results are included in Table B‐4 and shown on Figure 3B, while the laboratory report is 
included in Appendix B.  Field notes and site photographs are included in Appendix C.   

D.3. SUB‐SLAB VAPOR SAMPLING 

On July 1, 2021, WR installed two vapor pins through the slab of the building utilizing a hammer 
drill for assessing the sub‐slab vapors present below the building. Two one‐liter stainless steel, 
batch certified summa canisters with <100 mL/hr flow controllers (approximately 10‐minute flow 
controllers) were utilized to collect the samples. The vapor pins and the summa canisters/flow 
controllers were connected utilizing Teflon tubing.  

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D.4. LABORATORY RESULTS – SUB‐SLAB VAPOR SAMPLE 

Laboratory Results – Sub‐Slab Vapor Sample 
Analytical results for indoor air sample TO‐15 indicated the presence of several low‐level 
detections of targeted constituents in both samples (SSV‐1 and SSV‐2). All the compounds 
reported in the samples were below their respective Non‐Residential Vapor Intrusion Screening 
Levels (NCDEQ, January 2021). Sub‐Slab Vapor results were also inserted in the NCDEQ Risk 
Calculator, and the results indicated that there were no risk exceedances for Residential or Non‐
Residential workers from the soil gas to indoor air pathway under the present scenario or future 
scenarios at the site. 

These data are shown on Figure 3C, and included in Table B‐11, while the laboratory report is 
included in Appendix B.  Field notes and site photographs are included in Appendix C.  The NCDEQ 
Risk Calculator is provided in Appendix D. 

SECTION E.  CONCLUSIONS AND RECOMMENDATIONS 

This report documents the results of field activities conducted at the site for TA‐03, which included 
the installation of nine soil borings, collection and analysis of a soil sample from each of the borings 
except WR‐7, installation and sampling of one permanent Type II monitoring well, and four 
temporary Type II monitoring wells, sampling of a water supply well, and collection of two sub‐
slab vapor samples, as well as repairing damaged to the floor where soils samples were collected.  
Conclusions based on observations, analytical data and research relating to the release at the site 
combined with historical information include the following: 

 The property is currently unoccupied.   
 It was reported in historical documents that five petroleum USTs were removed from the 
location in December 1993, however only four certificates of disposal exist, and one is missing 
for a 550‐gallon UST.  Results for one or more soil samples collected in association with the 
UST closures indicated that a release had occurred. 
 The site and all surrounding properties appear to be provided potable water through the local 
municipal supply system, however, WR personnel observed several supply wells within a 
1,000‐ft radius of the site. The wells on the adjoining property 216 Camp Easter Rd, Unit B, 
are utilized for non‐potable purposes.  
 No wellhead protection areas or source water intakes were identified within 1‐mile of the site. 
 WR identified the presence of a Freshwater Forested/Shrub Wetland located immediately 
northeast of the site and a Lake Habitat located immediately west of the site.  Each of these 
wetland features are indexed by the US FWS, National Wetlands Inventory and are located 
within 100‐ft of the site. 
 WR identified two surface water bodies within 500 feet of the site. Crystal Lake, a WS‐III, 
Class B, HQW surface water, and Mill Creek below the Crystal Lake dam, a WS‐III, HQW 
surface water.  
 Laboratory results for soil samples obtained from borings installed in association with this 
assessment showed exceedances of the Soil‐to‐Groundwater MSCCs in WR‐2 for naphthalene 
(EPA Method 8260D) and Aromatic C‐9‐C10 (MADEP VPH). In addition, laboratory results for 
WithersRavenel
Our People. Your Success. 

Former C.C. Newell Store WR Project # 02172214.97 
Site Check Report October 2021 
13 

soil samples WR‐1, WR‐2, WR‐6, WR‐8, WR‐9 showed exceedances of the Commercial / 
Industrial soil cleanup levels for chromium by EPA Method 6020B.  
 Laboratory data for groundwater samples obtained from wells MW‐1, MW‐3, MW‐4, MW‐5, 
WR‐6 (TW), and WR‐9 (TW) showed one or more compounds in each of the samples. 
Concentrations of benzene (MW‐3 and MW‐4), 1,2‐dichloroethane (MW‐1), and Methyl‐tert‐
Butyl Ether (MTBE) (MW‐1) were reported in excess of their respective 2L Standards. Benzene 
was detected at levels ten times the NC Surface Water 2B Standards in MW‐3 in the July 1, 
2021, sample.  None of the compounds reported in any of the samples were at concentrations 
exceeding their respective GCLs.  
 Analytical results for the sub‐slab vapor samples analyzed by TO‐15 indicated the presence of 
presence of several low‐level detections of targeted constituents in both samples (SSV‐1 and 
SSV‐2). All the compounds reported in the samples were below their respective Non‐
Residential Vapor Intrusion Screening Levels (NCDEQ, January 2021).  
 Sub‐Slab Vapor results were also inserted in the NCDEQ Risk Calculator, and the results 
indicated that there were no risk exceedances for Residential or Non‐Residential workers from 
the soil gas to indoor air pathway under the present scenario or future scenarios at the site.  

Based on the results of assessment and monitoring activities conducted at the site in association 
with this TA, WR recommends having the property owner remove building materials impacted by 
the petroleum impacted water and retesting the indoor air.  If indoor air concentrations continue 
to exceed non‐residential carcinogenic risk, the installation of an active mitigation or passive 
venting system to deplete contaminant concentrations in the structure will be needed. 

WR appreciates the opportunity to be of service in the completion of these assessment activities.  
Should you have questions, comments, or require additional information, please contact WR at 
your earliest convenience. 

Cordially, 
WithersRavenel 

David Vail G. Matthew James, PG 
Environmental Staff Professional I Senior Geologist 

FIGURES 

KBB
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SUBJECT SITE
±0.143 ACRE
SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
GENERAL LOCATION MAP
WithersRavenel
Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 |www.withersravenel.com
1"=500 '
GRAPHIC SCALE
1 inch = 500 ft.
0 500250 1000
FORMER C.C. NEWELL STORE(INCIDENT #11196)216 CAMP EASTER ROAD, UNIT ACARTHAGE, MOORE COUNTY, NC
CAMP EASTER ROADPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)MW-1CRYSTALLAKEMW-2MW-3MW-4MW-6IAS-1WR-2WR-1WR-3MW-5WR-4WR-5WR-6WR-7WR-8WR-9SSV-1SSV-2FORMERDISPENSERISLANDDV
MJ
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SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:SITE MAPWithersRavenel
Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 |www.withersravenel.com
1"=20 'LEGENDPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)TYPE II MONITORING WELL LOCATIONINDOOR AIR SAMPLE LOCATIONSUB SLAB VAPOR SAMPLE LOCATIONSOIL SAMPLE LOCATIONSOIL BORING CONVERTED TOTEMPORARY MONITORING WELLNOTES: 1.) AERIAL OBTAINED FROM NC ONE MAP.GRAPHIC SCALE1 inch = 20 ft.0201040FORMER C.C. NEWELL STORE(INCIDENT #11196)216 CAMP EASTER ROAD, UNIT ACARTHAGE, MOORE COUNTY, NC
CAMP EASTER ROADPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)CRYSTALLAKEWR-2WR-1WR-3WR-4WR-5WR-6WR-7WR-8WR-9FORMERDISPENSERISLANDLEGENDPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)SOIL SAMPLE LOCATIONSOIL SAMPLE CONVERTED TOTEMPORARY MONITORING WELLNOTES: 1.) AERIAL OBTAINED FROM NC ONE MAP.FORMER C.C. NEWELL STORE(INCIDENT #11196)
216 CAMP EASTER ROAD, UNIT ACARTHAGE, MOORE COUNTY, NC GRAPHIC SCALE1 inch = 20 ft.0201040DCV
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3A
SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
SITE MAP
WITH SOIL SAMPLE ANALYTICALRESULTS - JULY 2021
WithersRavenel
Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 |www.withersravenel.com
1"=20 '
CAMP EASTER ROADPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)MW-1MW-2MW-3MW-4MW-6MW-5WR-6WR-7WR-8WR-9FORMERDISPENSERISLAND12LEGENDPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)TYPE II MONITORING WELL LOCATIONSOIL BORING CONVERTED TOTEMPORARY MONITORING WELLACTIVE, NON-POTABLE WATER SUPPLY WELLINACTIVE WATER SUPPLY WELLNOTES: 1.) AERIAL OBTAINED FROM NC ONE MAP.FORMER C.C. NEWELL STORE(INCIDENT #11196)
216 CAMP EASTER ROAD, UNIT ACARTHAGE, MOORE COUNTY, NC GRAPHIC SCALE1 inch = 20 ft.0201040DCV
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3B
SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
SITE MAPWITH GROUNDWATERANALYTICAL RESULTS -JULY & AUGUST 2021
WithersRavenel
Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 |www.withersravenel.com
1"=20 '12
CAMP EASTER ROADPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)SSV-1SSV-2FORMERDISPENSERISLANDLEGENDPOSSIBLE FORMER UST LOCATION (BASED ON GPR SURVEY)SUB-SLAB VAPOR SAMPLE LOCATIONNOTES: 1.) AERIAL OBTAINED FROM NC ONE MAP.FORMER C.C. NEWELL STORE(INCIDENT #11196)
216 CAMP EASTER ROAD, UNIT ACARTHAGE, MOORE COUNTY, NC GRAPHIC SCALE1 inch = 20 ft.0201040DCV
MJ
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3C
SCALE:FIGURE NO.:
PROJECT NO.:DATE:APPROVED BY:
SITE MAP
WITH MONITORING WELL &INDOOR AIR SAMPLE LOCATIONSSHOWN
WithersRavenel
Engineers | Planners | Surveyors
115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 |www.withersravenel.com
1"=20 '

TABLES 

UST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofUSTWas release associated with UST System? (Y/N)1Gasoline Not Listed 4,000 Single‐Wall Steel Not Listed Unknown1/1/1983 RemovedY2Gasoline Not Listed 4,000 Single‐Wall Steel Not Listed Unknown1/1/1983 RemovedY3Gasoline Not Listed 2,000 Single‐Wall Steel Not Listed Unknown1/1/1983 RemovedY4Gasoline Not Listed 550 Single‐Wall Steel Not Listed Unknown1/1/1983 RemovedY5Kerosene Not Listed 550 Single‐Wall Steel Not Listed Unknown1/1/1983 RemovedYAST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofASTWas release associated with AST System? (Y/N)N/AIncidentNumberMaterialReleasedDateofReleaseIncident # 11196 Petrolueum UnknownNotes:1)2) Description of release from NCDEQ Summary prepared 03/16/2021.UST Information from NCDEQ "tblAllTanks" Excel database.Incident # 11196Description of ReleaseTable B‐1Site History:  UST/AST System & Other Release InformationFormer C.C. Newell StoreFive USTs were removed from the property during 1993.  Soil samples obtained in association with closure confirmed release(s).  Groundwater was not thought to have been impacted.N/A216 Camp Easter RoadCarthage, Moore County, NCPage 1 of 1
ChromiumLead n‐ButylbenzeneEthylbenzeneNaphthalenen‐PropylbenzeneToluenem,p‐Xyleneo‐XyleneXylene (Total)n‐HexaneAcenaphthene1,2‐Dichlorobenzene1,3‐DichlorobenzeneHexachlorobenzeneNaphthalene1,2,4‐Trichlorobenzene2,4,6‐TrichlorophenolAliphatic C19‐C36Aliphatic C9‐C18Aromatic C11‐C22Aliphatic C5‐C8Aliphatic C9‐C12Aromatic C9‐C107440‐47‐3 7439‐92‐1 104‐51‐8 100‐41‐491‐20‐3 103‐65‐1 108‐88‐3179601‐23‐95‐47‐6 1330‐20‐7 110‐54‐383‐32‐995‐50‐1 541‐73‐1 118‐74‐191‐20‐3 120‐82‐188‐06‐2 C19‐C36 C9‐C18 C11‐C22 C5‐C8 C9‐C12 C9‐C10B‐13/29/20210.83<0.26 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NAB‐23/29/2021180.7 69.4NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NAB‐33/29/202180.4 75.1NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NAB‐43/29/20217.8 6.1NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NAWR‐17/1/2021NA NA9.02 7.74<0.005 <0.005 <0.011 <0.005 <0.005 <0.011 <0.005 <0.005 <0.011 <0.771 <0.771 <0.771 <0.771 <0.771 <0.771 <0.771 <57.5 <57.5 <57.5 <9.33 <9.33 <9.33WR‐27/1/2021NA NA9.77 7.43 0.207 0.281 0.814 0.419 0.252 1.56 0.647 2.21<0.300 <0.793 <0.793 <0.793 <0.793 <0.793 <0.793 <0.793 <60.2 <60.2 <60.226.2 91.8 35.3WR‐37/1/2021NA NA NA NA <0.005 <0.005 <0.010 <0.005 <0.005 <0.010 <0.005 <0.005 <0.010 <0.661 <0.661 <0.661 <0.661 <0.661 <0.661 <0.661 <51.3 <51.3 <51.3 <8.00 <8.00 <8.00WR‐47/1/2021NANANANA <0.005 <0.005 <0.011 <0.005 <0.005 <0.011 <0.005 <0.005 <0.011 <0.768 <0.768 <0.768 <0.768 <0.768 <0.768 <0.768 <59.6 <59.6 <59.6 <9.21 <9.21 <9.21WR‐57/1/2021NA NA NA NA <0.0050.018<0.0110.012<0.0050.021<0.0050.021<0.011 <0.767 <0.767 <0.767 <0.767 <0.767 <0.767 <0.767 <58.7 <58.7 <58.7 <9.30 <9.30 <9.30WR‐67/21/2021NA NA7.33 8.21<0.006 <0.006 <0.012 <0.006 <0.006 <0.012 <0.006 <0.006 <0.012 <0.815 <0.815 <0.815 <0.815 <0.815 <0.815 <0.815 <62.9 <62.9 <62.9 <9.89 <9.89 <9.89WR‐87/21/2021NA NA9.23 5.47<0.005 <0.005 <0.011 <0.005 <0.005 <0.011 <0.005 <0.005 <0.011 <0.773 <0.773 <0.773 <0.773 <0.773 <0.773 <0.773 <58.1 <58.1 <58.1 <9.38 <9.38 <9.38WR‐97/21/2021NA NA9.56 7.46<0.006 <0.006 <0.012 <0.006 <0.006 <0.012 <0.006 <0.006 <0.012 <0.811 <0.811 <0.811 <0.811 <0.811 <0.811 <0.811 <62.1 <62.1 <62.1 <9.82 <9.82 <9.82 100 50 N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/A N/AN/A N/A 360,000 270 2.4 8 0.2 1.4 5.4 6 6 6 NL 8.3 0.23 7.6 NL 0.2 2.1 0.15 # 540 31 68 540 31N/A N/A 1.32 400 782 60.3 5.5 1,560 1,250 3,120 3,120 3,120 NL 930 1,400 460 NL 5.5 22.8 15.6 31,200 1,560 469 625 1,560 469N/A N/A 6.54 400 11,600 297 27 23,300 18,600 46,700 46,700 46,700 NL 14,000 21,000 7000 NL 27 112 233 467,000 23,300 7,000 9,340 23,300 7,000Notes:1)2)ResultResultResultResultResultTABLE B‐3SUMMARY OF SOIL ANALYTICAL RESULTSFormer C.C. Newell StoreIncident # 11196= Result Exceeds State Action LevelEPA Method 8270EAnalytical Method EPA Method 8015CSampleIDDateCollectedDiesel Range OrganicsGasoline Range OrganicsResidential MSCCCommercial / Industrial MSCCEPA Method 6020BState Action LevelMADEP EPHMADEP VPH216 Camp Easter RoadCarthage, Moore County, NC= Result Exceeds Soil‐to‐Groundwater Maximum Soil Contaminant Concentration Level= Result Exceeds Residential Soil Cleanup Levels= Result Exceeds Commercial / Industrial Soil Cleanup LevelsAll results provided in mg/kg (milligrams per kilogram) or parts per millionWR‐7 not collected as all soils encountered were completely saturatedEPA Method 8260D= Result Exceeds Laboratory Detection LimitsSoil‐to‐Groundwater MSCCPage 1 of 1
Benzene Butylbenzene, n‐Butylbenzene, sec‐ Di‐Isopropyl Ether Dichloroethane, 1,2‐ Ethylbenzene MBK, Methyl Butyl Ketone (2‐Hexanone) Isopropylbenzene (Cumene) Methyl‐tert‐Butyl Ether Naphthalene Propylbenzene, n‐Toluene Trimethylbenzene, 1,2,4‐ Trimethylbenzene, 1,3,5‐Xylene, m,p‐ Xylenes, o‐Total XylenesAcenaphtheneNaphthalenePhenolPyrene1,2,4‐Trichlorobenzene2,4,6‐TrichlorophenolAliphatic C9‐C18Aliphatic C19‐C36Aromatic C11‐C22Aliphatic C5‐C8Aliphatic C9‐C12Aromatic C9‐C1071‐43‐2 104‐51‐8 135‐98‐8 108‐20‐3 107‐06‐2 100‐41‐4 591‐78‐698‐82‐81634‐04‐491‐20‐3 103‐65‐1 108‐88‐395‐63‐6 108‐67‐895‐47‐6108‐38‐3/106‐42‐31330‐20‐783‐32‐991‐20‐3 108‐95‐2 129‐00‐0 120‐82‐188‐06‐2C9‐C18 C19‐C36 C11‐C22 C5‐C8 C9‐C12 C9‐C103/1/2021<0.5 <0.5 <0.515 2.2<0.5 NR <0.527<0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5NA NA NA NA NA NA NA NA NA NA NA NA7/1/2021<0.500 <0.500 <0.50018.7 2.11<0.500 <1.00 <0.50030.8<1.00 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500NA NA NA NA NA NA NA NA NA NA NA NA3/29/2021<0.500 <0.500 <0.500 <0.500 <0.500 <0.5001.92<0.500 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500NA NA NA NA NA NA NA NA NA NA NA NA7/1/2021<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500NA NA NA NA NA NA NA NA NA NA NA NA3/29/202119.11.30 0.774<0.500 <0.50020.2<1.002.63<1.008.18 8.26 88.9 54.6 15.7 46.7 100 147NA NA NA NA NA NA NA NA NA NA NA NA7/1/2021110.0<0.500 <0.500 <0.500 <0.50019.4<1.001.02<1.003.73 1.33 0.6 12.1 7.5 3.7 3.05 6.76NA NA NA NA NA NA NA NA NA NA NA NA3/29/20211.12<0.500 <0.500 <0.500 <0.5003.61<1.000.651<1.001.88 1.16 9.43 11.6 3.26 9.14 20.2 29.3NA NA NA NA NA NA NA NA NA NA NA NA7/1/20211.60<0.500 <0.500 <0.500 <0.5001.53<1.00 <0.500 <1.00 <1.00 <0.500 <0.5001.3<0.5001.30<0.5001.3NA NA NA NA NA NA NA NA NA NA NA NA3/29/2021<0.500 <0.500 <0.500 <0.500 <0.5006.46<1.001.19<1.001.25 2.34 10.9 11.2 2.78 10.2 27.9 38.1NA NA NA NA NA NA NA NA NA NA NA NA7/1/2021<0.500 <0.500 <0.500 <0.500 <0.5001.98<1.000.56<1.00 <1.000.67<0.5004.1<0.5002.5<0.5002.5NA NA NA NA NA NA NA NA NA NA NA NAMW‐6 8/17/2021<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500NA NA NA NA NA NA NA NA NA NA NA NAWR‐6 (TW) 8/17/2021<0.500 <0.500 <0.500 <0.500 <0.5001.73<1.00 <0.500 <1.00 <1.00 <0.500 <0.5000.7<0.500 <1.00 <0.500 <0.500<10.3 <10.3 <10.3 <10.3 <10.3 <20.6 <372 <532 <266 <50.0 <50.0 <50.0WR‐7 (TW) 8/17/2021<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500<10.3 <10.3 <10.3 <10.3 <10.3 <20.6 <368 <526 <263 <50.0 <50.0 <50.0WR‐8 (TW) 8/17/2021<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500<11.1 <11.1 <11.1 <11.1 <11.1 <22.2 NA NA NA <50.0 <50.0 <50.0WR‐9 (TW) 8/17/2021<0.500 <0.500 <0.5000.616<0.5001.73<1.00 <0.5002.69<1.00 <0.500 <0.5001.4<0.5001.6<0.5001.6<10.2 <10.2 <10.2 <10.2 <10.2 <20.4 <350 <500 <250 <50.0 <50.0 <50.0Neighbor WSW (WSW‐1)8/17/2021<0.500 <0.500 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <1.00 <1.00 <0.500 <0.500 <0.500 <0.500 <1.00 <0.500 <0.500 NA NA NA NA NA NA NA NA NA NA NA NA170 70 70 0.4 600 40 70 20 670 600 400 400 500 500 500 80 6 30 200 70 4 700 10,000 200 400 700 2001.19 420** NL NL 9.9*** 68*** NL 2700** 19 400** 1,500** 57*** NL 130** 6,200** 6,200** 6,200** 70*** 400** 4,000*** 20*** 488 1.0 3000** NL 830** 600** 3000** 830**11.9 4,200** NL NL 99*** 680*** NL 27,000** 190 4,000** 15,000** 570*** NL 1,300** 62,000** 62,000** 62,000** 700*** 4,000** 40,000*** 200*** 4,880 10 30000** NL 8,300** 6,000** 30,000** 8,300**5,000 5,900 8,800 70,000 400 80,000 40,000 30,500 20,000 6,000 26,100 260,000 28,500 24,100 50,000 50,000 50,000 1,950 6,000 30,000 200 24,500 4,000 NLNLNLNLNLNLNotes:1) All results provided in ug/L (micrograms per liter) or parts per billion.2) Compounds analyzed for by laboratory but not listed were not found above laboratory detection limits. See the laboratory report included  in  Appendix for a full list of constituents. 3) NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L.4)5)*) Chemical not listed in 2B Surface Water Standards, Class B In‐Stream Target Value used.**) Chemical not listed in 2B Surface Water Standards, Class WS I‐V In‐Stream Target Value used.***) Chemical not listed in 2B Surface Water Standards, EPA National Recommended Water Quality Criteria Class WS I‐V value used.NL =  No Regulatory Limit EstablishedNA / NR = Not Analyzed or Not ReportedRESULT= Result Exceeds Laboratory Detection LimitsRESULT= Result Exceeds NC 2L StandardResult= Result Exceeds Ten Times the NC Surface Water StandardsRESULT= Result Exceeds GCLMADEP ‐ VPHTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSFormer C.C. Newell StoreIncident # 11196216 Camp Easter RoadCarthage, Moore County, NC625.1 ‐ Semi Volatile Organic CompoundsAnalytical MethodSampleIDMADEP ‐ EPHGCLs for Groundwater6200B ‐ Volatile Organic CompoundsMW‐4GCLs for Groundwater = NCDEQ Gross Contamination Levels (GCLs) for Groundwater.North Carolina Surface Water Standards obtained from the June 19, 2019 Standards for Class C Freshwater Standards.  NC 2L Standard DateCollectedMW‐1MW‐2MW‐3North Carolina Surface Water 2B Standards (10X)North Carolina Surface Water 2B StandardsMW‐5Page 1 of 1
WSW‐1
Referred to as  
"Neighbor 
WSW" in analytical data
950416825944 216 Camp Easter Road Unit B Moore James R. Von Canon, Jr. PO Box 129
Lakeview, NC 28350
Active (Connected to restrooms, non‐
potable), bottled 
water for cooking and drinking
~35'Unk 100 Upgradinet
WSW‐2 950416825944 216 Camp Easter Road Unit B Moore James R. Von Canon, Jr. PO Box 129
Lakeview, NC 28351 Inactive Unk Unk 180 Cross‐gradient
Notes: 
       2.)  Information regarding the water supply well's use and location was obtained from historical reports.
       3.)  Well distance from source area values was provided in historical reports.
Well Screen 
Interval(feet)Well UseWell ID Property Owner AddressProperty Address  County Well Depth
(feet)Property Owner
Well Distance 
from Source Area(feet)PIN
Location Relative 
to Groundwater Flow
TABLE B‐5APUBLIC & PRIVATE WATER SUPPLY WELL INFORMATION
Former C.C. Newell Store
216 Camp Easter RoadCarthage, Moore County, NC
UST #: FA‐610Incident Number: Incident # 11196
Page 1 of 1
EastingNorthing1Crystal LakeWestCrystal Lake Support, Inc. PO Box 485Southern Pines, NC 28388Recreational100 Cross‐Gradient 1908358.45 542837.692Mill CreekSoutheastN/ARecreational310 Down‐Gradient 1908755.05 542633.00Receptor IDTABLE B‐5BADDITIONAL RECEPTOR INFORMATIONFormer C.C. Newell Store216 Camp Easter RoadCarthage, Moore County, NCLocation of Significant Points(NC State Plane NAD 83 Feet)Incident Number: Incident # 11196ContactInformationDescriptionUST #: FA‐610LocationDistance from Source Area(feet)Location Relative to Groundwater FlowUsagePage 1 of 1
216 Camp Easter Rd, Unit A216 CER Holding LLCLakeview, NC 28350175 West New Hampshire AveSouthern Pines, NC 28387216 Camp Easter Rd, Unit B James R & Kimberly S Von CanonLakeview, NC 28350PO Box 129Lakeview, NC 283500 Camp Easter Rd216 CER Holding LLCLakeview, NC 28350175 West New Hampshire AveSouthern Pines, NC 283870 Camp Easter RdFrederick McKenzieLakeview, NC 28350PO Box 41Lakeview, NC 28350202 Camp Easter RdSue B. McKenzieLakeview, NC 28350PO Box 233Lakeview, NC 28350240 Camp Easter RdFrank H AleoLakeview, NC 28350PO Box 366Lakeview, NC 28350116 Lone Pine RdMark Walker & Vera FrancesLakeview, NC 28350PO Box 224Lakeview, NC 283500 US HWY 1Carolyn D McCaskillWoodedLakeview, NC 283502369 Everett Dowdy RdSanford, NC 273300 Camp Easter RdCrystal Lake Support, Inc.Recreational LakeLakeview, NC 28350PO Box 485Southern Pines, NC 28387       1)W&R has not performed a receptor survey in association with the subject property and thus the information provided above has not been verified. 2)3)4)Moore County Zoning Codes:B‐2 = Highway Commercial DistrictRA‐40 = Residential and Agricultural ‐ 40 District 8RA‐4070'Down‐gradientRA‐20 = Residential and Agricultural ‐ 20 District Carthage, Moore County, NCNotes: Property owner information from the Moore County GIS Service, data current as ofSeptember 10, 2021. See Figure 4 for corresponding map information.Distances shown from source area are measured from location of monitoring well MW‐1 and the nearest property boundary of the adjacent property.6Occupied ResidenceRA‐20255'Up‐gradient7RA‐20185'Down‐gradient4Vacant BuildingB‐290'Down‐gradinet5Occupied ResidenceRA‐20182'Up‐gradientDown‐gradient3Gravel Parking LotB‐225'Down‐gradient1Apartment / Storage / ShopB‐240'Up‐gradient2WoodedB‐2105'Location Relative to Groundwater FlowSITEVacantB‐2‐‐‐‐‐‐Property IDProperty AddressProperty Owner & AddressUsageZoningDistance/Direction from Source AreaTABLE B‐5CADJACENT PROPERTY INFORMATIONFormer C.C. Newell StoreIncident Number: Incident # 11196UST #: FA‐610216 Camp Easter Road
    BenzeneCyclohexaneDibromochloromethaneEthanolEthylbenzene4‐EthyltolueneHeptanen‐HexaneIsopropanolNaphthaleneToluene1,2,4‐Trimethylbenzene1,3,5‐Trimethylbenzenem&p‐Xyleneo‐Xylene71‐43‐2 110‐82‐7 124‐48‐164‐17‐5 100‐41‐4 622‐96‐8 142‐82‐5 110‐54‐398‐82‐891‐20‐3 108‐88‐395‐63‐6 108‐67‐8 1330‐20‐795‐47‐6IAS‐1 4/3/202111018 2.1 554003701801705214013001,6004602,1009500.36 1,300 NL NL 1.1 NL 83 150 42 NL 1,000 13 13 21 21Notes:1)2)3)NLResultResult= Not Listed= Result Exceeds Laboratory Detection Limits= Result exceeds Indoor Air/Crawlspace Residential Vapor Intrusion Screening Levels, NCDEQ, January 2021 (Based on November 2020 US EPA Regional Screening Tables).TO‐15IASL (µg/m3)All results provided in µg/m3 (micrograms per cubic meter).Analytical MethodSampleIDDateCollectedCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included  in the Appendix for a full list of constituents. IASL=Indoor Air Screening Level (Indoor Air/Crawlspace Residential Vapor Intrusion Screening Levels, NCDEQ, January 2021 (Based on November 2020 US EPA Regional Screening Tables).SUMMARY OF INDOOR AIR VAPOR ANALYTICAL RESULTSTABLE B‐10Former C.C. Newell StoreIncident # 11196216 Camp Easter RoadCarthage, Moore County, NC

  Acetone2‐Butanone (Methyl Ethyl Ketone)Carbon DisulfideEthanol4‐Methyl‐2‐pentanone2‐Propanol67‐64‐178‐93‐375‐15‐064‐17‐5 108‐10‐167‐63‐0
SSV‐1 7/1/2021 250 46 <4.0 310 5.3 240
SSV‐2 7/1/2021 170 14 21 140 <0.99 110
2,700,000 440,000 61,000 NL 260,000 18,000
Notes:
1)
2)
3)
NL
Result
Result
All results provided in µg/m3 (micrograms per cubic meter).
TO‐15
TABLE B‐11
SUMMARY OF SUB SLAB VAPOR ANALYTICAL RESULTS
Former C.C. Newell Store
Incident # 11196
216 Camp Easter Road
Carthage, Moore County, NC
Analytical Method
Sample
ID
Compounds analyzed for by laboratory but not listed were not detected above 
laboratory detection limits. See the laboratory report included  in the Appendix for a full 
list of constituents. 
Non‐Residential VISL =  Vapor Intrusion Screening Levels for Non‐Residential Structures, NCDEQ, January 2021 (Based on November 2020 US EPA Regional 
Screening Tables).
= Result exceeds Vapor Intrusion Screening Levels for Non‐Residential Structures, 
NCDEQ, January 2021 (Based on November 2020 US EPA Regional Screening Tables).
= Not Listed
= Result Exceeds Laboratory Detection Limits
Date
Collected
Non‐Residential VISLs 
(µg/m3)

APPENDIX A 
 BORING LOG, WELL CONSTRUCTION RECORD 

Well ID:Job Name:
Date:Site Loc.:
W&R Rep:Driller:
Notes:
WELL CONSTRUCTION LOG
MW-6 Former C.C. Newell Store Job #:02172214.97
July 21, 2021 Carthage, NC TOC EL:NM
S. Powell Quantex, Inc.GW EL:NM
542870.70
Depth in
Feet Soil Description
(Field USCS Classification)
Well Construction
0 Ground Surface
1.0
2.0
3.0
7 - 9 ft Bentonite
NC NAD83 Easting:1908510.32 NC NAD83 Northing:
17.0
18.0
4.0
5.0
6.0
7.0
8.0
9.0
10.0
11.0
12.0
13.0
14.0
15.0
16.0
19.0
20.0
21.0
22.0
23.0
24.0
25.0
26.0
27.0
28.0
29.0
30.0
1.) Boring Terminated at 26' BLS
2.) BLS - Below Land Surface = Groundwater Level (Measured Beneath TOC), 07/21/2021
3.) TOC - Top of Casing
0 - 7 ft Neat Cement
Tan, brown moist silty clay
Red, brown moist silty clay
Red silt
Page 1 of 1
115 MacKenan Drive Cary, North Carolina 27511 tel:[phone] fax:[phone] www.withersravenel.com
11 - 26 ft 2" Dia.
0.010-Slot PVC
Well Screen
0-11 ft- 2" Dia.
PVC Casing
9 - 26 ft #2 Clean-
Washed Torpedo Sand
Boring Terminated at 26' BLS
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By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.



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James D. Barker
3106-A
Quantex, Inc.
NA
✔
7/21/21 MW-6
Former CC Newell Store NA
216 Camp Easter Road, Lakeview, NC 28350
Moore NA
35.241312 79.306304
✔
✔
1
26'
~24'
6"
Auger
23 24 Red SILT
0112"Sch 40 PVC
11 26 2"0.010 Sch 40 PVC
0 7 Neat Cement 140 lbs. Poured
7 9 Bentonite 3/8" Pellets 35 lbs.
9 26 #2 silica sand pour
0 5 Orange Tan Moist Clay
5 19 Reddish Dark Grey CLAY
19 26 Red SILT
7/21/21

APPENDIX B 
 LABORATORY ANALYTICAL REPORT & CHAIN OF CUSTODY 

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

7/13/2021
Withers & Ravenel Kevin Buchanan
115 Mackenan Dr. BUILDING 117 Cary, NC, 27511
Ref: Analytical Testing
Lab Report Number: 21-183-0032 Client Project Description: Former CC Newell Store
02172214.97
Dear Kevin Buchanan:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/2/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 104
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202137735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202199012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-183-0032
Page 2 of 104
Report Number:
Sample Summary Table
Client Project Description:
21-183-0032
Former CC Newell Store
02172214.97
Lab No Client Sample ID Matrix Date Collected Date Received
07/01/2021 09:15Aqueous 90920 MW-1 07/02/2021 14:55
07/01/2021 13:55Aqueous 90921 MW-2 07/02/2021 14:55
07/01/2021 14:15Aqueous 90922 MW-3 07/02/2021 14:55
07/01/2021 09:35Aqueous 90923 MW-4 07/02/2021 14:55
07/01/2021 09:30Aqueous 90924 MW-5 07/02/2021 14:55
07/01/2021 10:50Solids 90925 WR-1 07/02/2021 14:55
07/01/2021 11:30Solids 90926 WR-2 07/02/2021 14:55
07/01/2021 12:00Solids 90927 WR-3 07/02/2021 14:55
07/01/2021 12:45Solids 90928 WR-4 07/02/2021 14:55
07/01/2021 13:30Solids 90929 WR-5 07/02/2021 14:55
Page 3 of 104
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-183-0032
Report Limit
Project:Former CC Newell Store
V 90920MW-1
18.7 07/08/2021 15:396200BDi-Isopropyl Ether (DIPE)µg/L 0.500
2.11 07/08/2021 15:396200B1,2-Dichloroethane µg/L 0.500
30.8 07/08/2021 15:396200BMethyl tert-butyl ether (MTBE)µg/L 1.00
V 90922MW-3
10.1 07/08/2021 16:036200BAcetoneµg/L 10.0
110 07/08/2021 16:286200BBenzeneµg/L 5.00
19.4 07/08/2021 16:036200BEthylbenzeneµg/L 0.500
1.02 07/08/2021 16:036200BIsopropylbenzeneµg/L 0.500
3.73 07/08/2021 16:036200BNaphthaleneµg/L 1.00
1.33 07/08/2021 16:036200Bn-Propylbenzene µg/L 0.500
0.628 07/08/2021 16:036200BTolueneµg/L 0.500
12.1 07/08/2021 16:036200B1,2,4-Trimethylbenzene µg/L 0.500
7.46 07/08/2021 16:036200B1,3,5-Trimethylbenzene µg/L 0.500
3.05 07/08/2021 16:036200Bo-Xylene µg/L 0.500
3.71 07/08/2021 16:036200Bm,p-Xylene µg/L 1.00
6.76 07/08/2021 16:036200BXylene (Total)µg/L 0.500
V 90923MW-4
1.60 07/08/2021 14:506200BBenzeneµg/L 0.500
1.53 07/08/2021 14:506200BEthylbenzeneµg/L 0.500
1.32 07/08/2021 14:506200B1,2,4-Trimethylbenzene µg/L 0.500
1.30 07/08/2021 14:506200Bm,p-Xylene µg/L 1.00
1.30 07/08/2021 14:506200BXylene (Total)µg/L 0.500
V 90924MW-5
1.98 07/08/2021 15:146200BEthylbenzeneµg/L 0.500
0.561 07/08/2021 15:146200BIsopropylbenzeneµg/L 0.500
0.665 07/08/2021 15:146200Bn-Propylbenzene µg/L 0.500
4.14 07/08/2021 15:146200B1,2,4-Trimethylbenzene µg/L 0.500
2.46 07/08/2021 15:146200Bm,p-Xylene µg/L 1.00
2.46 07/08/2021 15:146200BXylene (Total)µg/L 0.500
V 90925WR-1
9.02 07/09/2021 00:406020BChromiummg/Kg - dry 1.17
7.74 07/09/2021 00:406020BLeadmg/Kg - dry 1.17
14.3 07/07/2021 16:45SW-DRYWT Moisture %
Page 4 of 104
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-183-0032
Report Limit
Project:Former CC Newell Store
V 90926WR-2
9.77 07/09/2021 02:376020BChromiummg/Kg - dry 1.20
7.43 07/09/2021 02:376020BLeadmg/Kg - dry 1.20
0.207 07/06/2021 15:148260Dn-Butylbenzene mg/Kg - dry 0.150
0.281 07/06/2021 15:148260DEthylbenzenemg/Kg - dry 0.150
0.814 07/06/2021 15:148260DNaphthalenemg/Kg - dry 0.300
0.419 07/06/2021 15:148260Dn-Propylbenzene mg/Kg - dry 0.150
0.252 07/06/2021 15:148260DToluenemg/Kg - dry 0.150
0.647 07/06/2021 15:148260Do-Xylene mg/Kg - dry 0.150
1.56 07/06/2021 15:148260Dm,p-Xylene mg/Kg - dry 0.300
2.21 07/06/2021 15:148260DXylene (Total)mg/Kg - dry 0.150
26.2 07/07/2021 08:06MADEP-VPH Aliphatic C5-C8 mg/Kg - dry 9.62
91.8 07/07/2021 08:06MADEP-VPH Aliphatic C9-C12 mg/Kg - dry 9.62
35.3 07/07/2021 08:06MADEP-VPH Aromatic C9-C10 mg/Kg - dry 9.62
16.8 07/07/2021 16:45SW-DRYWT Moisture %
V 90928WR-4
13.1 07/07/2021 16:45SW-DRYWT Moisture %
V 90929WR-5
0.018 07/06/2021 13:158260DEthylbenzenemg/Kg - dry 0.005
0.012 07/06/2021 13:158260Dn-Propylbenzene mg/Kg - dry 0.005
0.021 07/06/2021 13:158260Dm,p-Xylene mg/Kg - dry 0.011
0.021 07/06/2021 13:158260DXylene (Total)mg/Kg - dry 0.005
14.0 07/08/2021 14:25SW-DRYWT Moisture %
Page 5 of 104

Client: Withers & Ravenel CASE NARRATIVE
Project: Former CC Newell Store Lab Report Number: 21-183-0032
Date: 7/13/2021
Massachusetts EPH Method MADEP-EPH Analyte: Aliphatic C9-C18 QC Batch No: V6364/V6175
Analyte was flagged for 0% recovery in the LCS and/or LCSD due to the result being below the MQL. The actual result was 168.853 ug/mL which calculates to a recovery of 56.3% which is within the acceptable recovery range.
Sample 90926 (WR-2)
Analyte: Aliphatic C9-C18 QC Batch No: V6364/V6175
Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual result was 182.237 ug/mL which calculates to a recovery of 60.7% which is within the acceptable recovery range.
Analyte: Aliphatic C9-C18
QC Batch No: V6364/V6175 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 160.586 ug/mL which calculates to a recovery of 53.5% which is within the acceptable recovery range. Massachusetts VPH Method MADEP-VPH Sample 90925 (WR-1)
Analyte: 2,5-Dibromotoluene (FID) QC Batch No: V6157/V6156 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all
showed surrogates within QC limits.
Sample 90928 (WR-4) Analyte: 2,5-Dibromotoluene (FID)
QC Batch No: V6157/V6156 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 90929 (WR-5)
Analyte: 2,5-Dibromotoluene (FID) QC Batch No: V6157/V6156 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Sample 90928 (WR-4) Analyte: 2,5-Dibromotoluene (PID) QC Batch No: V6157/V6156 Surrogate(s) exhibited a high bias in this project sample where no target analytes were detected. The high recovery(s) had no impact on the data. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits.
Page 6 of 104

Metals Analyses Method 6020B Sample 90925 (WR-1)
Analyte: Chromium QC Batch No: V6315/V6306
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Semivolatile Organic Compounds - GC/MS Method 8270E Sample 90830 Analyte: 2,4,6-Tribromophenol
QC Batch No: V6348/V6173 MS Surrogate recovery is above range.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V6348/V6173 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 342
ug/kg which calculates to a recovery of 20% which is below the acceptable recovery range.
Analyte: Benzo(a)pyrene QC Batch No: V6348/V6173
Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Analyte: Benzoic Acid QC Batch No: V6348/V6173
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 1580 ug/kg which calculates to a recovery of 94% which is above the acceptable recovery range. Analyte: Benzoic Acid QC Batch No: V6348/V6173 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the
batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable.
Sample 90830 Analyte: Benzoic Acid QC Batch No: V6348/V6173 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1520 ug/kg which calculates to a recovery of 91% which is above the acceptable recovery range.
Analyte: Pentachlorophenol QC Batch No: V6348/V6173 Recovery for the LCS exceeded the upper acceptance limit. However, all sample results associated with the batch are below the MQL, so this high bias had no impact upon the client data. The results are considered to be acceptable. Sample 90830 Analyte: Pyridine QC Batch No: V6348/V6173 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was 87.1 ug/kg which calculates to a recovery of 5% which is below the acceptable recovery range.
Page 7 of 104

Sample 90927/WR-3 – The sample jar was broken prior to the % moisture and metals analyses being performed.
Data is reported on an “as received” or “wet” basis.
Page 8 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-1
90920 Matrix:
7/1/2021 9:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Benzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Bromobenzene 1 07/08/21 15:39 6200BJLB
<1.00 µg/L 1.00Bromochloromethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/08/21 15:39 6200BJLB
<5.00 µg/L 5.00Bromoform 1 07/08/21 15:39 6200BJLB
<1.00 µg/L 1.00Bromomethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/08/21 15:39 6200BJLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Chlorobenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/08/21 15:39 6200BJLB
<1.00 µg/L 1.00Chloroethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Chloroform 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Chloromethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/08/21 15:39 6200BJLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Dibromomethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/08/21 15:39 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 9 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-1
90920 Matrix:
7/1/2021 9:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/08/21 15:39 6200BJLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/08/21 15:39 6200BJLB
2.11 µg/L 0.5001,2-Dichloroethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/08/21 15:39 6200BJLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/08/21 15:39 6200BJLB
<200 µg/L 200Ethanol 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Ethylbenzene 1 07/08/21 15:39 6200BJLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/08/21 15:39 6200BJLB
18.7 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Isopropylbenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/08/21 15:39 6200BJLB
<1.00 µg/L 1.002-Hexanone 1 07/08/21 15:39 6200BJLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/08/21 15:39 6200BJLB
<2.00 µg/L 2.00Methylene Chloride 1 07/08/21 15:39 6200BJLB
30.8 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/08/21 15:39 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 10 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-1
90920 Matrix:
7/1/2021 9:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/08/21 15:39 6200BJLB
<1.00 µg/L 1.00Naphthalene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500n-Propylbenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Styrene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Toluene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Trichloroethene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/08/21 15:39 6200BJLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/08/21 15:39 6200BJLB
<1.00 µg/L 1.00m,p-Xylene 1 07/08/21 15:39 6200BJLB
<0.500 µg/L 0.500o-Xylene 1 07/08/21 15:39 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 11 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-1
90920 Matrix:
7/1/2021 9:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 07/08/21 15:39 6200B
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/08/21 15:391 JLB V6335
Surrogate: Dibromofluoromethane 102 Limits: 70-130%07/08/21 15:391 JLB V6335
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%07/08/21 15:391 JLB V6335
Surrogate: Toluene-d8 100 Limits: 70-130%07/08/21 15:391 JLB V6335
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 12 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-2
90921 Matrix:
7/1/2021 13:55
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Benzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Bromobenzene 1 07/08/21 14:25 6200BJLB
<1.00 µg/L 1.00Bromochloromethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/08/21 14:25 6200BJLB
<5.00 µg/L 5.00Bromoform 1 07/08/21 14:25 6200BJLB
<1.00 µg/L 1.00Bromomethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/08/21 14:25 6200BJLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Chlorobenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/08/21 14:25 6200BJLB
<1.00 µg/L 1.00Chloroethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Chloroform 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Chloromethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/08/21 14:25 6200BJLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Dibromomethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/08/21 14:25 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 13 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-2
90921 Matrix:
7/1/2021 13:55
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/08/21 14:25 6200BJLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/08/21 14:25 6200BJLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/08/21 14:25 6200BJLB
<200 µg/L 200Ethanol 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Ethylbenzene 1 07/08/21 14:25 6200BJLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Isopropylbenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/08/21 14:25 6200BJLB
<1.00 µg/L 1.002-Hexanone 1 07/08/21 14:25 6200BJLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/08/21 14:25 6200BJLB
<2.00 µg/L 2.00Methylene Chloride 1 07/08/21 14:25 6200BJLB
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/08/21 14:25 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 14 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-2
90921 Matrix:
7/1/2021 13:55
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/08/21 14:25 6200BJLB
<1.00 µg/L 1.00Naphthalene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500n-Propylbenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Styrene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Toluene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Trichloroethene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/08/21 14:25 6200BJLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/08/21 14:25 6200BJLB
<1.00 µg/L 1.00m,p-Xylene 1 07/08/21 14:25 6200BJLB
<0.500 µg/L 0.500o-Xylene 1 07/08/21 14:25 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 15 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-2
90921 Matrix:
7/1/2021 13:55
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 07/08/21 14:25 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/08/21 14:251 JLB V6335
Surrogate: Dibromofluoromethane 102 Limits: 70-130%07/08/21 14:251 JLB V6335
Surrogate: 1,2-Dichloroethane - d4 99.0 Limits: 70-130%07/08/21 14:251 JLB V6335
Surrogate: Toluene-d8 99.6 Limits: 70-130%07/08/21 14:251 JLB V6335
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 16 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-3
90922 Matrix:
7/1/2021 14:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
10.1 µg/L 10.0Acetone 1 07/08/21 16:03 6200BJLB
110 µg/L 5.00Benzene 10 07/08/21 16:28 6200BJLB
<0.500 µg/L 0.500Bromobenzene 1 07/08/21 16:03 6200BJLB
<1.00 µg/L 1.00Bromochloromethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/08/21 16:03 6200BJLB
<5.00 µg/L 5.00Bromoform 1 07/08/21 16:03 6200BJLB
<1.00 µg/L 1.00Bromomethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/08/21 16:03 6200BJLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Chlorobenzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/08/21 16:03 6200BJLB
<1.00 µg/L 1.00Chloroethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Chloroform 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Chloromethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/08/21 16:03 6200BJLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Dibromomethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/08/21 16:03 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 17 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-3
90922 Matrix:
7/1/2021 14:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/08/21 16:03 6200BJLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/08/21 16:03 6200BJLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/08/21 16:03 6200BJLB
<200 µg/L 200Ethanol 1 07/08/21 16:03 6200BJLB
19.4 µg/L 0.500Ethylbenzene 1 07/08/21 16:03 6200BJLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/08/21 16:03 6200BJLB
1.02 µg/L 0.500Isopropylbenzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/08/21 16:03 6200BJLB
<1.00 µg/L 1.002-Hexanone 1 07/08/21 16:03 6200BJLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/08/21 16:03 6200BJLB
<2.00 µg/L 2.00Methylene Chloride 1 07/08/21 16:03 6200BJLB
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/08/21 16:03 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 18 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-3
90922 Matrix:
7/1/2021 14:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/08/21 16:03 6200BJLB
3.73 µg/L 1.00Naphthalene 1 07/08/21 16:03 6200BJLB
1.33 µg/L 0.500n-Propylbenzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Styrene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/08/21 16:03 6200BJLB
0.628 µg/L 0.500Toluene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Trichloroethene 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/08/21 16:03 6200BJLB
12.1 µg/L 0.5001,2,4-Trimethylbenzene 1 07/08/21 16:03 6200BJLB
7.46 µg/L 0.5001,3,5-Trimethylbenzene 1 07/08/21 16:03 6200BJLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/08/21 16:03 6200BJLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/08/21 16:03 6200BJLB
3.71 µg/L 1.00m,p-Xylene 1 07/08/21 16:03 6200BJLB
3.05 µg/L 0.500o-Xylene 1 07/08/21 16:03 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 19 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-3
90922 Matrix:
7/1/2021 14:15
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
6.76 µg/L 0.500Xylene (Total)1 07/08/21 16:03 6200B
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/08/21 16:031 JLB V6335
Surrogate: Dibromofluoromethane 101 Limits: 70-130%07/08/21 16:031 JLB V6335
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 70-130%07/08/21 16:031 JLB V6335
Surrogate: Toluene-d8 99.4 Limits: 70-130%07/08/21 16:031 JLB V6335
Surrogate: 4-Bromofluorobenzene 103 Limits: 70-130%07/08/21 16:2810 JLB V6335
Surrogate: Dibromofluoromethane 101 Limits: 70-130%07/08/21 16:2810 JLB V6335
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%07/08/21 16:2810 JLB V6335
Surrogate: Toluene-d8 99.8 Limits: 70-130%07/08/21 16:2810 JLB V6335
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 20 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-4
90923 Matrix:
7/1/2021 9:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 07/08/21 14:50 6200BJLB
1.60 µg/L 0.500Benzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Bromobenzene 1 07/08/21 14:50 6200BJLB
<1.00 µg/L 1.00Bromochloromethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/08/21 14:50 6200BJLB
<5.00 µg/L 5.00Bromoform 1 07/08/21 14:50 6200BJLB
<1.00 µg/L 1.00Bromomethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/08/21 14:50 6200BJLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Chlorobenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/08/21 14:50 6200BJLB
<1.00 µg/L 1.00Chloroethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Chloroform 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Chloromethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/08/21 14:50 6200BJLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Dibromomethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/08/21 14:50 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 21 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-4
90923 Matrix:
7/1/2021 9:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/08/21 14:50 6200BJLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/08/21 14:50 6200BJLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/08/21 14:50 6200BJLB
<200 µg/L 200Ethanol 1 07/08/21 14:50 6200BJLB
1.53 µg/L 0.500Ethylbenzene 1 07/08/21 14:50 6200BJLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Isopropylbenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/08/21 14:50 6200BJLB
<1.00 µg/L 1.002-Hexanone 1 07/08/21 14:50 6200BJLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/08/21 14:50 6200BJLB
<2.00 µg/L 2.00Methylene Chloride 1 07/08/21 14:50 6200BJLB
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/08/21 14:50 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 22 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-4
90923 Matrix:
7/1/2021 9:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/08/21 14:50 6200BJLB
<1.00 µg/L 1.00Naphthalene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500n-Propylbenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Styrene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Toluene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Trichloroethene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/08/21 14:50 6200BJLB
1.32 µg/L 0.5001,2,4-Trimethylbenzene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/08/21 14:50 6200BJLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/08/21 14:50 6200BJLB
1.30 µg/L 1.00m,p-Xylene 1 07/08/21 14:50 6200BJLB
<0.500 µg/L 0.500o-Xylene 1 07/08/21 14:50 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 23 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-4
90923 Matrix:
7/1/2021 9:35
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
1.30 µg/L 0.500Xylene (Total)1 07/08/21 14:50 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%07/08/21 14:501 JLB V6335
Surrogate: Dibromofluoromethane 102 Limits: 70-130%07/08/21 14:501 JLB V6335
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 70-130%07/08/21 14:501 JLB V6335
Surrogate: Toluene-d8 101 Limits: 70-130%07/08/21 14:501 JLB V6335
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 24 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-5
90924 Matrix:
7/1/2021 9:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Benzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Bromobenzene 1 07/08/21 15:14 6200BJLB
<1.00 µg/L 1.00Bromochloromethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Bromodichloromethane 1 07/08/21 15:14 6200BJLB
<5.00 µg/L 5.00Bromoform 1 07/08/21 15:14 6200BJLB
<1.00 µg/L 1.00Bromomethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500n-Butylbenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500sec-Butyl benzene 1 07/08/21 15:14 6200BJLB
<2.00 µg/L 2.00tert-Butyl benzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Carbon Tetrachloride 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Chlorobenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Chlorodibromomethane 1 07/08/21 15:14 6200BJLB
<1.00 µg/L 1.00Chloroethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Chloroform 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Chloromethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5002-Chlorotoluene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5004-Chlorotoluene 1 07/08/21 15:14 6200BJLB
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,2-Dibromoethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Dibromomethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 07/08/21 15:14 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 25 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-5
90924 Matrix:
7/1/2021 9:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 07/08/21 15:14 6200BJLB
<5.00 µg/L 5.00Dichlorodifluoromethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,2-Dichloroethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,1-Dichloroethene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,2-Dichloropropane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,3-Dichloropropane 1 07/08/21 15:14 6200BJLB
<2.00 µg/L 2.002,2-Dichloropropane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,1-Dichloropropene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 07/08/21 15:14 6200BJLB
<200 µg/L 200Ethanol 1 07/08/21 15:14 6200BJLB
1.98 µg/L 0.500Ethylbenzene 1 07/08/21 15:14 6200BJLB
<3.00 µg/L 3.00Hexachlorobutadiene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 07/08/21 15:14 6200BJLB
0.561 µg/L 0.500Isopropylbenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5004-Isopropyl toluene 1 07/08/21 15:14 6200BJLB
<1.00 µg/L 1.002-Hexanone 1 07/08/21 15:14 6200BJLB
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 07/08/21 15:14 6200BJLB
<2.00 µg/L 2.00Methylene Chloride 1 07/08/21 15:14 6200BJLB
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 07/08/21 15:14 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 26 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-5
90924 Matrix:
7/1/2021 9:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 07/08/21 15:14 6200BJLB
<1.00 µg/L 1.00Naphthalene 1 07/08/21 15:14 6200BJLB
0.665 µg/L 0.500n-Propylbenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Styrene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Tetrachloroethene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Toluene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Trichloroethene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Trichlorofluoromethane 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 07/08/21 15:14 6200BJLB
4.14 µg/L 0.5001,2,4-Trimethylbenzene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 07/08/21 15:14 6200BJLB
<5.00 µg/L 5.00Vinyl Acetate 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500Vinyl Chloride 1 07/08/21 15:14 6200BJLB
2.46 µg/L 1.00m,p-Xylene 1 07/08/21 15:14 6200BJLB
<0.500 µg/L 0.500o-Xylene 1 07/08/21 15:14 6200BJLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 27 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:MW-5
90924 Matrix:
7/1/2021 9:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
2.46 µg/L 0.500Xylene (Total)1 07/08/21 15:14 6200B
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/08/21 15:141 JLB V6335
Surrogate: Dibromofluoromethane 101 Limits: 70-130%07/08/21 15:141 JLB V6335
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%07/08/21 15:141 JLB V6335
Surrogate: Toluene-d8 99.4 Limits: 70-130%07/08/21 15:141 JLB V6335
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 28 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<57.5 mg/Kg - dry 57.5Aliphatic C19-C36 1 07/09/21 16:04 MADEP-EPHZRC
<9.33 mg/Kg - dry 9.33Aliphatic C5-C8 100 07/06/21 15:54 MADEP-VPHTBL
<9.33 mg/Kg - dry 9.33Aliphatic C9-C12 100 07/06/21 15:54 MADEP-VPHTBL
<57.5 mg/Kg - dry 57.5Aliphatic C9-C18 1 07/09/21 16:04 MADEP-EPHZRC
<57.5 mg/Kg - dry 57.5Aromatic C11-C22 1 07/09/21 16:04 MADEP-EPHZRC
<9.33 mg/Kg - dry 9.33Aromatic C9-C10 100 07/06/21 15:54 MADEP-VPHTBL
<0.023 mg/Kg - dry 0.023Acetone 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Benzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromobenzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromochloromethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromodichloromethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromoform 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Bromomethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005n-Butylbenzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005sec-Butyl benzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005tert-Butyl benzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Carbon Tetrachloride 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorobenzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorodibromomethane 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Chloroethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Chloroform 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Chloromethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0052-Chlorotoluene 1 07/06/21 13:45 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 29 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Chlorotoluene 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.0111,2-Dibromo-3-Chloropropane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dibromoethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Dibromomethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichlorobenzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichlorobenzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,4-Dichlorobenzene 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Dichlorodifluoromethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloroethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,2-Dichloroethene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,2-Dichloroethene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloropropane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichloropropane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0052,2-Dichloropropane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloropropene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,3-Dichloropropene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,3-Dichloropropene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Ethylbenzene 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Hexachlorobutadiene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Di-Isopropyl Ether (DIPE)1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Isopropylbenzene 1 07/06/21 13:45 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 30 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Isopropyl toluene 1 07/06/21 13:45 8260DTBL
<0.023 mg/Kg - dry 0.0232-Hexanone 1 07/06/21 13:45 8260DTBL
<0.023 mg/Kg - dry 0.023Methyl Ethyl Ketone (MEK)1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Methylene Chloride 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Methyl tert-butyl ether (MTBE)1 07/06/21 13:45 8260DTBL
<0.023 mg/Kg - dry 0.0234-Methyl-2-Pentanone 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Naphthalene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005n-Propylbenzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Styrene 1 07/06/21 13:45 8260DTBL
<0.058 mg/Kg - dry 0.058Ethyl Tertiary Butyl Ether (ETBE)1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1,2-Tetrachloroethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2,2-Tetrachloroethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Tetrachloroethene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Toluene 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.0111,2,3-Trichlorobenzene 1 07/06/21 13:45 8260DTBL
14.3 %Moisture 1 07/07/21 16:45 SW-DRYWTEDV
<0.011 mg/Kg - dry 0.0111,2,4-Trichlorobenzene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1-Trichloroethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2-Trichloroethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Trichloroethene 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Trichlorofluoromethane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2,3-Trichloropropane 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,3,5-Trimethylbenzene 1 07/06/21 13:45 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 31 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.011 mg/Kg - dry 0.011Vinyl Acetate 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011Vinyl Chloride 1 07/06/21 13:45 8260DTBL
<0.011 mg/Kg - dry 0.011m,p-Xylene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005o-Xylene 1 07/06/21 13:45 8260DTBL
<0.005 mg/Kg - dry 0.005Xylene (Total)1 07/06/21 13:45 8260D
9.02 mg/Kg - dry 1.17Chromium 10 07/09/21 00:40 6020BEDV
7.74 mg/Kg - dry 1.17Lead 10 07/09/21 00:40 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 32 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V6201 07/06/21 08:00
<0.023 mg/Kg - dry 0.023Acrolein 1 07/06/21 13:45 V6202TBL
<0.023 mg/Kg - dry 0.023Acrylonitrile 1 07/06/21 13:45 V6202TBL
<0.005 mg/Kg - dry 0.005Carbon Disulfide 1 07/06/21 13:45 V6202TBL
<0.011 mg/Kg - dry 0.011n-Hexane 1 07/06/21 13:45 V6202TBL
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%07/06/21 13:451 TBL V6202
Surrogate: Dibromofluoromethane 101 Limits: 84-123%07/06/21 13:451 TBL V6202
Surrogate: Toluene-d8 97.5 Limits: 76-129%07/06/21 13:451 TBL V6202
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.771 mg/Kg - dry 0.771Acenaphthene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Acenaphthylene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Aniline 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Anthracene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Benzo(a)anthracene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Benzo(a)pyrene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Benzo(b)fluoranthene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Benzo(g,h,i)perylene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Benzo(k)fluoranthene 1 07/08/21 21:32 V6348JMV
<2.33 mg/Kg - dry 2.33Benzoic Acid 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Benzyl alcohol 1 07/08/21 21:32 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 33 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.771 mg/Kg - dry 0.771Bis(2-Chloroethoxy)methane 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Bis(2-Chloroethyl)ether 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.385Bis(2-Chloroisopropyl)ether 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Bis(2-ethylhexyl)phthalate 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7714-Bromophenyl phenyl ether 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.385Butyl benzyl phthalate 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7714-Chloro-3-methylphenol 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.3854-Chloroaniline 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712-Chloronaphthalene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712-Chlorophenol 1 07/08/21 21:32 V6348JMV
<1.17 mg/Kg - dry 1.174-Chlorophenyl phenyl ether 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Chrysene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Dibenz(a,h)anthracene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Dibenzofuran 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7711,2-Dichlorobenzene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7711,3-Dichlorobenzene 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.3851,4-Dichlorobenzene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7713,3'-Dichlorobenzidine 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712,4-Dichlorophenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Diethyl phthalate 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Dimethyl phthalate 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.3852,4-Dimethylphenol 1 07/08/21 21:32 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 34 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.771 mg/Kg - dry 0.771Di-n-butyl phthalate 1 07/08/21 21:32 V6348JMV
<1.75 mg/Kg - dry 1.754,6-Dinitro-2-methylphenol 1 07/08/21 21:32 V6348JMV
<1.75 mg/Kg - dry 1.752,4-Dinitrophenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712,4-Dinitrotoluene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712,6-Dinitrotoluene 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.385Di-n-Octyl Phthalate 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Fluoranthene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Fluorene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Hexachlorobenzene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Hexachlorobutadiene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Hexachlorocyclopentadiene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Hexachloroethane 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Indeno(1,2,3-cd)pyrene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Isophorone 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7711-Methylnaphthalene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712-Methylnaphthalene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712-Methylphenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7713&4 Methylphenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Naphthalene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712-Nitroaniline 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7713-Nitroaniline 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.3854-Nitroaniline 1 07/08/21 21:32 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 35 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-1
90925 Matrix:
7/1/2021 10:50
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.385 mg/Kg - dry 0.385Nitrobenzene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712-Nitrophenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7714-Nitrophenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771N-Nitrosodimethylamine 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771N-Nitrosodiphenylamine 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771N-Nitroso-di-n-propylamine 1 07/08/21 21:32 V6348JMV
<1.17 mg/Kg - dry 1.17Pentachlorophenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Phenanthrene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Phenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.771Pyrene 1 07/08/21 21:32 V6348JMV
<0.385 mg/Kg - dry 0.385Pyridine 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7711,2,4-Trichlorobenzene 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712,4,5-Trichlorophenol 1 07/08/21 21:32 V6348JMV
<0.771 mg/Kg - dry 0.7712,4,6-Trichlorophenol 1 07/08/21 21:32 V6348JMV
Surrogate: Phenol-d5 78.4 Limits: 34-121%07/08/21 21:321 JMV V6348
Surrogate: 2-Fluorobiphenyl 97.6 Limits: 44-115%07/08/21 21:321 JMV V6348
Surrogate: 2-Fluorophenol 80.5 Limits: 35-115%07/08/21 21:321 JMV V6348
Surrogate: Nitrobenzene-d5 80.2 Limits: 37-122%07/08/21 21:321 JMV V6348
Surrogate: 4-Terphenyl-d14 99.4 Limits: 54-127%07/08/21 21:321 JMV V6348
Surrogate: 2,4,6-Tribromophenol 121 Limits: 39-132%07/08/21 21:321 JMV V6348
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 36 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<60.2 mg/Kg - dry 60.2Aliphatic C19-C36 1 07/09/21 16:40 MADEP-EPHZRC
26.2 mg/Kg - dry 9.62Aliphatic C5-C8 100 07/07/21 08:06 MADEP-VPHTBL
91.8 mg/Kg - dry 9.62Aliphatic C9-C12 100 07/07/21 08:06 MADEP-VPHTBL
<60.2 mg/Kg - dry 60.2Aliphatic C9-C18 1 07/09/21 16:40 MADEP-EPHZRC
<60.2 mg/Kg - dry 60.2Aromatic C11-C22 1 07/09/21 16:40 MADEP-EPHZRC
35.3 mg/Kg - dry 9.62Aromatic C9-C10 100 07/07/21 08:06 MADEP-VPHTBL
<0.600 mg/Kg - dry 0.600Acetone 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Benzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Bromobenzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Bromochloromethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Bromodichloromethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Bromoform 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.300Bromomethane 50 07/06/21 15:14 8260DTBL
0.207 mg/Kg - dry 0.150n-Butylbenzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150sec-Butyl benzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150tert-Butyl benzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Carbon Tetrachloride 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Chlorobenzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Chlorodibromomethane 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.300Chloroethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Chloroform 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.300Chloromethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1502-Chlorotoluene 50 07/06/21 15:14 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 37 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.150 mg/Kg - dry 0.1504-Chlorotoluene 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.3001,2-Dibromo-3-Chloropropane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,2-Dibromoethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Dibromomethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,2-Dichlorobenzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,3-Dichlorobenzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,4-Dichlorobenzene 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.300Dichlorodifluoromethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,1-Dichloroethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,2-Dichloroethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,1-Dichloroethene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150cis-1,2-Dichloroethene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150trans-1,2-Dichloroethene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,2-Dichloropropane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,3-Dichloropropane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1502,2-Dichloropropane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,1-Dichloropropene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150cis-1,3-Dichloropropene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150trans-1,3-Dichloropropene 50 07/06/21 15:14 8260DTBL
0.281 mg/Kg - dry 0.150Ethylbenzene 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.300Hexachlorobutadiene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Di-Isopropyl Ether (DIPE)50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Isopropylbenzene 50 07/06/21 15:14 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 38 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.150 mg/Kg - dry 0.1504-Isopropyl toluene 50 07/06/21 15:14 8260DTBL
<0.600 mg/Kg - dry 0.6002-Hexanone 50 07/06/21 15:14 8260DTBL
<0.600 mg/Kg - dry 0.600Methyl Ethyl Ketone (MEK)50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Methylene Chloride 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Methyl tert-butyl ether (MTBE)50 07/06/21 15:14 8260DTBL
<0.030 mg/Kg - dry 0.0304-Methyl-2-Pentanone 50 07/06/21 15:14 8260DTBL
0.814 mg/Kg - dry 0.300Naphthalene 50 07/06/21 15:14 8260DTBL
0.419 mg/Kg - dry 0.150n-Propylbenzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Styrene 50 07/06/21 15:14 8260DTBL
<3.00 mg/Kg - dry 3.00Ethyl Tertiary Butyl Ether (ETBE)50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,1,1,2-Tetrachloroethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,1,2,2-Tetrachloroethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Tetrachloroethene 50 07/06/21 15:14 8260DTBL
0.252 mg/Kg - dry 0.150Toluene 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.3001,2,3-Trichlorobenzene 50 07/06/21 15:14 8260DTBL
16.8 %Moisture 1 07/07/21 16:45 SW-DRYWTEDV
<0.300 mg/Kg - dry 0.3001,2,4-Trichlorobenzene 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,1,1-Trichloroethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,1,2-Trichloroethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.150Trichloroethene 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.300Trichlorofluoromethane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,2,3-Trichloropropane 50 07/06/21 15:14 8260DTBL
<0.150 mg/Kg - dry 0.1501,3,5-Trimethylbenzene 50 07/06/21 15:14 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 39 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.300 mg/Kg - dry 0.300Vinyl Acetate 50 07/06/21 15:14 8260DTBL
<0.300 mg/Kg - dry 0.300Vinyl Chloride 50 07/06/21 15:14 8260DTBL
1.56 mg/Kg - dry 0.300m,p-Xylene 50 07/06/21 15:14 8260DTBL
0.647 mg/Kg - dry 0.150o-Xylene 50 07/06/21 15:14 8260DTBL
2.21 mg/Kg - dry 0.150Xylene (Total)50 07/06/21 15:14 8260D
9.77 mg/Kg - dry 1.20Chromium 10 07/09/21 02:37 6020BEDV
7.43 mg/Kg - dry 1.20Lead 10 07/09/21 02:37 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 40 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 MED
8260D Prep Batch(es):V6203 07/06/21 08:00
<0.600 mg/Kg - dry 0.600Acrolein 50 07/06/21 15:14 V6204TBL
<0.600 mg/Kg - dry 0.600Acrylonitrile 50 07/06/21 15:14 V6204TBL
<0.150 mg/Kg - dry 0.150Carbon Disulfide 50 07/06/21 15:14 V6204TBL
<0.300 mg/Kg - dry 0.300n-Hexane 50 07/06/21 15:14 V6204TBL
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%07/06/21 15:1450 TBL V6204
Surrogate: Dibromofluoromethane 98.0 Limits: 70-130%07/06/21 15:1450 TBL V6204
Surrogate: Toluene-d8 98.0 Limits: 76-129%07/06/21 15:1450 TBL V6204
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.793 mg/Kg - dry 0.793Acenaphthene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Acenaphthylene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Aniline 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Anthracene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Benzo(a)anthracene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Benzo(a)pyrene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Benzo(b)fluoranthene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Benzo(g,h,i)perylene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Benzo(k)fluoranthene 1 07/08/21 21:55 V6348JMV
<2.40 mg/Kg - dry 2.40Benzoic Acid 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Benzyl alcohol 1 07/08/21 21:55 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 41 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.793 mg/Kg - dry 0.793Bis(2-Chloroethoxy)methane 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Bis(2-Chloroethyl)ether 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.396Bis(2-Chloroisopropyl)ether 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Bis(2-ethylhexyl)phthalate 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7934-Bromophenyl phenyl ether 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.396Butyl benzyl phthalate 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7934-Chloro-3-methylphenol 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.3964-Chloroaniline 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932-Chloronaphthalene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932-Chlorophenol 1 07/08/21 21:55 V6348JMV
<1.20 mg/Kg - dry 1.204-Chlorophenyl phenyl ether 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Chrysene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Dibenz(a,h)anthracene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Dibenzofuran 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7931,2-Dichlorobenzene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7931,3-Dichlorobenzene 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.3961,4-Dichlorobenzene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7933,3'-Dichlorobenzidine 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932,4-Dichlorophenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Diethyl phthalate 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Dimethyl phthalate 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.3962,4-Dimethylphenol 1 07/08/21 21:55 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 42 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.793 mg/Kg - dry 0.793Di-n-butyl phthalate 1 07/08/21 21:55 V6348JMV
<1.80 mg/Kg - dry 1.804,6-Dinitro-2-methylphenol 1 07/08/21 21:55 V6348JMV
<1.80 mg/Kg - dry 1.802,4-Dinitrophenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932,4-Dinitrotoluene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932,6-Dinitrotoluene 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.396Di-n-Octyl Phthalate 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Fluoranthene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Fluorene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Hexachlorobenzene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Hexachlorobutadiene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Hexachlorocyclopentadiene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Hexachloroethane 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Indeno(1,2,3-cd)pyrene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Isophorone 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7931-Methylnaphthalene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932-Methylnaphthalene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932-Methylphenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7933&4 Methylphenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Naphthalene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932-Nitroaniline 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7933-Nitroaniline 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.3964-Nitroaniline 1 07/08/21 21:55 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 43 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-2
90926 Matrix:
7/1/2021 11:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.396 mg/Kg - dry 0.396Nitrobenzene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932-Nitrophenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7934-Nitrophenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793N-Nitrosodimethylamine 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793N-Nitrosodiphenylamine 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793N-Nitroso-di-n-propylamine 1 07/08/21 21:55 V6348JMV
<1.20 mg/Kg - dry 1.20Pentachlorophenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Phenanthrene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Phenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.793Pyrene 1 07/08/21 21:55 V6348JMV
<0.396 mg/Kg - dry 0.396Pyridine 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7931,2,4-Trichlorobenzene 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932,4,5-Trichlorophenol 1 07/08/21 21:55 V6348JMV
<0.793 mg/Kg - dry 0.7932,4,6-Trichlorophenol 1 07/08/21 21:55 V6348JMV
Surrogate: Phenol-d5 81.6 Limits: 34-121%07/08/21 21:551 JMV V6348
Surrogate: 2-Fluorobiphenyl 99.4 Limits: 44-115%07/08/21 21:551 JMV V6348
Surrogate: 2-Fluorophenol 85.8 Limits: 35-115%07/08/21 21:551 JMV V6348
Surrogate: Nitrobenzene-d5 86.1 Limits: 37-122%07/08/21 21:551 JMV V6348
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%07/08/21 21:551 JMV V6348
Surrogate: 2,4,6-Tribromophenol 115 Limits: 39-132%07/08/21 21:551 JMV V6348
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 44 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<51.3 mg/Kg 51.3Aliphatic C19-C36 1 07/09/21 17:17 MADEP-EPHZRC
<8.00 mg/Kg 8.00Aliphatic C5-C8 100 07/06/21 16:22 MADEP-VPHTBL
<8.00 mg/Kg 8.00Aliphatic C9-C12 100 07/06/21 16:22 MADEP-VPHTBL
<51.3 mg/Kg 51.3Aliphatic C9-C18 1 07/09/21 17:17 MADEP-EPHZRC
<51.3 mg/Kg 51.3Aromatic C11-C22 1 07/09/21 17:17 MADEP-EPHZRC
<8.00 mg/Kg 8.00Aromatic C9-C10 100 07/06/21 16:22 MADEP-VPHTBL
<0.020 mg/Kg 0.020Acetone 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Benzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Bromobenzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Bromochloromethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Bromodichloromethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Bromoform 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Bromomethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005n-Butylbenzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005sec-Butyl benzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005tert-Butyl benzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Carbon Tetrachloride 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Chlorobenzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Chlorodibromomethane 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Chloroethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Chloroform 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Chloromethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0052-Chlorotoluene 1 07/06/21 14:15 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 45 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg 0.0054-Chlorotoluene 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.0101,2-Dibromo-3-Chloropropane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,2-Dibromoethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Dibromomethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,2-Dichlorobenzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,3-Dichlorobenzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,4-Dichlorobenzene 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Dichlorodifluoromethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,1-Dichloroethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,2-Dichloroethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,1-Dichloroethene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005cis-1,2-Dichloroethene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005trans-1,2-Dichloroethene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,2-Dichloropropane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,3-Dichloropropane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0052,2-Dichloropropane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,1-Dichloropropene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005cis-1,3-Dichloropropene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005trans-1,3-Dichloropropene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Ethylbenzene 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Hexachlorobutadiene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Di-Isopropyl Ether (DIPE)1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Isopropylbenzene 1 07/06/21 14:15 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 46 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg 0.0054-Isopropyl toluene 1 07/06/21 14:15 8260DTBL
<0.020 mg/Kg 0.0202-Hexanone 1 07/06/21 14:15 8260DTBL
<0.020 mg/Kg 0.020Methyl Ethyl Ketone (MEK)1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Methylene Chloride 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Methyl tert-butyl ether (MTBE)1 07/06/21 14:15 8260DTBL
<0.020 mg/Kg 0.0204-Methyl-2-Pentanone 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Naphthalene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005n-Propylbenzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Styrene 1 07/06/21 14:15 8260DTBL
<0.050 mg/Kg 0.050Ethyl Tertiary Butyl Ether (ETBE)1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,1,1,2-Tetrachloroethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,1,2,2-Tetrachloroethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Tetrachloroethene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Toluene 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.0101,2,3-Trichlorobenzene 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.0101,2,4-Trichlorobenzene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,1,1-Trichloroethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,1,2-Trichloroethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Trichloroethene 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Trichlorofluoromethane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,2,3-Trichloropropane 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.0051,3,5-Trimethylbenzene 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010Vinyl Acetate 1 07/06/21 14:15 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 47 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.010 mg/Kg 0.010Vinyl Chloride 1 07/06/21 14:15 8260DTBL
<0.010 mg/Kg 0.010m,p-Xylene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005o-Xylene 1 07/06/21 14:15 8260DTBL
<0.005 mg/Kg 0.005Xylene (Total)1 07/06/21 14:15 8260D
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/06/21 14:151 TBL V6202
Surrogate: Dibromofluoromethane 101 Limits: 84-123%07/06/21 14:151 TBL V6202
Surrogate: Toluene-d8 97.7 Limits: 76-129%07/06/21 14:151 TBL V6202
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 48 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V6201 07/06/21 08:00
<0.020 mg/Kg 0.020Acrolein 1 07/06/21 14:15 V6202TBL
<0.020 mg/Kg 0.020Acrylonitrile 1 07/06/21 14:15 V6202TBL
<0.005 mg/Kg 0.005Carbon Disulfide 1 07/06/21 14:15 V6202TBL
<0.010 mg/Kg 0.010n-Hexane 1 07/06/21 14:15 V6202TBL
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%07/06/21 14:151 TBL V6202
Surrogate: Dibromofluoromethane 101 Limits: 84-123%07/06/21 14:151 TBL V6202
Surrogate: Toluene-d8 97.7 Limits: 76-129%07/06/21 14:151 TBL V6202
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.661 mg/Kg 0.661Acenaphthene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Acenaphthylene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Aniline 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Anthracene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Benzo(a)anthracene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Benzo(a)pyrene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Benzo(b)fluoranthene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Benzo(g,h,i)perylene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Benzo(k)fluoranthene 1 07/08/21 22:18 V6348JMV
<2.00 mg/Kg 2.00Benzoic Acid 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Benzyl alcohol 1 07/08/21 22:18 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 49 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.661 mg/Kg 0.661Bis(2-Chloroethoxy)methane 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Bis(2-Chloroethyl)ether 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.331Bis(2-Chloroisopropyl)ether 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Bis(2-ethylhexyl)phthalate 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6614-Bromophenyl phenyl ether 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.331Butyl benzyl phthalate 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6614-Chloro-3-methylphenol 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.3314-Chloroaniline 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612-Chloronaphthalene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612-Chlorophenol 1 07/08/21 22:18 V6348JMV
<1.00 mg/Kg 1.004-Chlorophenyl phenyl ether 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Chrysene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Dibenz(a,h)anthracene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Dibenzofuran 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6611,2-Dichlorobenzene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6611,3-Dichlorobenzene 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.3311,4-Dichlorobenzene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6613,3'-Dichlorobenzidine 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612,4-Dichlorophenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Diethyl phthalate 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Dimethyl phthalate 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.3312,4-Dimethylphenol 1 07/08/21 22:18 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 50 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.661 mg/Kg 0.661Di-n-butyl phthalate 1 07/08/21 22:18 V6348JMV
<1.50 mg/Kg 1.504,6-Dinitro-2-methylphenol 1 07/08/21 22:18 V6348JMV
<1.50 mg/Kg 1.502,4-Dinitrophenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612,4-Dinitrotoluene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612,6-Dinitrotoluene 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.331Di-n-Octyl Phthalate 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Fluoranthene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Fluorene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Hexachlorobenzene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Hexachlorobutadiene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Hexachlorocyclopentadiene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Hexachloroethane 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Indeno(1,2,3-cd)pyrene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Isophorone 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6611-Methylnaphthalene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612-Methylnaphthalene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612-Methylphenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6613&4 Methylphenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Naphthalene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612-Nitroaniline 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6613-Nitroaniline 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.3314-Nitroaniline 1 07/08/21 22:18 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 51 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-3
90927 Matrix:
7/1/2021 12:00
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.331 mg/Kg 0.331Nitrobenzene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612-Nitrophenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6614-Nitrophenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661N-Nitrosodimethylamine 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661N-Nitrosodiphenylamine 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661N-Nitroso-di-n-propylamine 1 07/08/21 22:18 V6348JMV
<1.00 mg/Kg 1.00Pentachlorophenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Phenanthrene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Phenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.661Pyrene 1 07/08/21 22:18 V6348JMV
<0.331 mg/Kg 0.331Pyridine 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6611,2,4-Trichlorobenzene 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612,4,5-Trichlorophenol 1 07/08/21 22:18 V6348JMV
<0.661 mg/Kg 0.6612,4,6-Trichlorophenol 1 07/08/21 22:18 V6348JMV
Surrogate: Phenol-d5 76.0 Limits: 34-121%07/08/21 22:181 JMV V6348
Surrogate: 2-Fluorobiphenyl 95.2 Limits: 44-115%07/08/21 22:181 JMV V6348
Surrogate: 2-Fluorophenol 79.0 Limits: 35-115%07/08/21 22:181 JMV V6348
Surrogate: Nitrobenzene-d5 78.4 Limits: 37-122%07/08/21 22:181 JMV V6348
Surrogate: 4-Terphenyl-d14 101 Limits: 54-127%07/08/21 22:181 JMV V6348
Surrogate: 2,4,6-Tribromophenol 116 Limits: 39-132%07/08/21 22:181 JMV V6348
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 52 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<59.6 mg/Kg - dry 59.6Aliphatic C19-C36 1 07/09/21 18:30 MADEP-EPHZRC
<9.21 mg/Kg - dry 9.21Aliphatic C5-C8 100 07/06/21 16:51 MADEP-VPHTBL
<9.21 mg/Kg - dry 9.21Aliphatic C9-C12 100 07/06/21 16:51 MADEP-VPHTBL
<59.6 mg/Kg - dry 59.6Aliphatic C9-C18 1 07/09/21 18:30 MADEP-EPHZRC
<59.6 mg/Kg - dry 59.6Aromatic C11-C22 1 07/09/21 18:30 MADEP-EPHZRC
<9.21 mg/Kg - dry 9.21Aromatic C9-C10 100 07/06/21 16:51 MADEP-VPHTBL
<0.023 mg/Kg - dry 0.023Acetone 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Benzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromobenzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromochloromethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromodichloromethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Bromoform 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Bromomethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005n-Butylbenzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005sec-Butyl benzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005tert-Butyl benzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Carbon Tetrachloride 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorobenzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorodibromomethane 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Chloroethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Chloroform 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Chloromethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0052-Chlorotoluene 1 07/06/21 14:45 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 53 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Chlorotoluene 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.0111,2-Dibromo-3-Chloropropane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dibromoethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Dibromomethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichlorobenzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichlorobenzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,4-Dichlorobenzene 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Dichlorodifluoromethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloroethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,2-Dichloroethene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,2-Dichloroethene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloropropane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichloropropane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0052,2-Dichloropropane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloropropene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,3-Dichloropropene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,3-Dichloropropene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Ethylbenzene 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Hexachlorobutadiene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Di-Isopropyl Ether (DIPE)1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Isopropylbenzene 1 07/06/21 14:45 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 54 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Isopropyl toluene 1 07/06/21 14:45 8260DTBL
<0.023 mg/Kg - dry 0.0232-Hexanone 1 07/06/21 14:45 8260DTBL
<0.023 mg/Kg - dry 0.023Methyl Ethyl Ketone (MEK)1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Methylene Chloride 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Methyl tert-butyl ether (MTBE)1 07/06/21 14:45 8260DTBL
<0.023 mg/Kg - dry 0.0234-Methyl-2-Pentanone 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Naphthalene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005n-Propylbenzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Styrene 1 07/06/21 14:45 8260DTBL
<0.057 mg/Kg - dry 0.057Ethyl Tertiary Butyl Ether (ETBE)1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1,2-Tetrachloroethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2,2-Tetrachloroethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Tetrachloroethene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Toluene 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.0111,2,3-Trichlorobenzene 1 07/06/21 14:45 8260DTBL
13.1 %Moisture 1 07/07/21 16:45 SW-DRYWTEDV
<0.011 mg/Kg - dry 0.0111,2,4-Trichlorobenzene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1-Trichloroethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2-Trichloroethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Trichloroethene 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Trichlorofluoromethane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,2,3-Trichloropropane 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.0051,3,5-Trimethylbenzene 1 07/06/21 14:45 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 55 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.011 mg/Kg - dry 0.011Vinyl Acetate 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011Vinyl Chloride 1 07/06/21 14:45 8260DTBL
<0.011 mg/Kg - dry 0.011m,p-Xylene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005o-Xylene 1 07/06/21 14:45 8260DTBL
<0.005 mg/Kg - dry 0.005Xylene (Total)1 07/06/21 14:45 8260D
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/06/21 14:451 TBL V6202
Surrogate: Dibromofluoromethane 102 Limits: 84-123%07/06/21 14:451 TBL V6202
Surrogate: Toluene-d8 98.2 Limits: 76-129%07/06/21 14:451 TBL V6202
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 56 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V6201 07/06/21 08:00
<0.023 mg/Kg - dry 0.023Acrolein 1 07/06/21 14:45 V6202TBL
<0.023 mg/Kg - dry 0.023Acrylonitrile 1 07/06/21 14:45 V6202TBL
<0.005 mg/Kg - dry 0.005Carbon Disulfide 1 07/06/21 14:45 V6202TBL
<0.011 mg/Kg - dry 0.011n-Hexane 1 07/06/21 14:45 V6202TBL
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/06/21 14:451 TBL V6202
Surrogate: Dibromofluoromethane 102 Limits: 84-123%07/06/21 14:451 TBL V6202
Surrogate: Toluene-d8 98.2 Limits: 76-129%07/06/21 14:451 TBL V6202
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.768 mg/Kg - dry 0.768Acenaphthene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Acenaphthylene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Aniline 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Anthracene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Benzo(a)anthracene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Benzo(a)pyrene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Benzo(b)fluoranthene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Benzo(g,h,i)perylene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Benzo(k)fluoranthene 1 07/08/21 22:41 V6348JMV
<2.32 mg/Kg - dry 2.32Benzoic Acid 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Benzyl alcohol 1 07/08/21 22:41 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 57 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.768 mg/Kg - dry 0.768Bis(2-Chloroethoxy)methane 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Bis(2-Chloroethyl)ether 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.384Bis(2-Chloroisopropyl)ether 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Bis(2-ethylhexyl)phthalate 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7684-Bromophenyl phenyl ether 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.384Butyl benzyl phthalate 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7684-Chloro-3-methylphenol 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.3844-Chloroaniline 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682-Chloronaphthalene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682-Chlorophenol 1 07/08/21 22:41 V6348JMV
<1.16 mg/Kg - dry 1.164-Chlorophenyl phenyl ether 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Chrysene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Dibenz(a,h)anthracene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Dibenzofuran 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7681,2-Dichlorobenzene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7681,3-Dichlorobenzene 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.3841,4-Dichlorobenzene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7683,3'-Dichlorobenzidine 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682,4-Dichlorophenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Diethyl phthalate 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Dimethyl phthalate 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.3842,4-Dimethylphenol 1 07/08/21 22:41 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 58 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.768 mg/Kg - dry 0.768Di-n-butyl phthalate 1 07/08/21 22:41 V6348JMV
<1.75 mg/Kg - dry 1.754,6-Dinitro-2-methylphenol 1 07/08/21 22:41 V6348JMV
<1.75 mg/Kg - dry 1.752,4-Dinitrophenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682,4-Dinitrotoluene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682,6-Dinitrotoluene 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.384Di-n-Octyl Phthalate 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Fluoranthene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Fluorene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Hexachlorobenzene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Hexachlorobutadiene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Hexachlorocyclopentadiene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Hexachloroethane 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Indeno(1,2,3-cd)pyrene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Isophorone 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7681-Methylnaphthalene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682-Methylnaphthalene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682-Methylphenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7683&4 Methylphenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Naphthalene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682-Nitroaniline 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7683-Nitroaniline 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.3844-Nitroaniline 1 07/08/21 22:41 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 59 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-4
90928 Matrix:
7/1/2021 12:45
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.384 mg/Kg - dry 0.384Nitrobenzene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682-Nitrophenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7684-Nitrophenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768N-Nitrosodimethylamine 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768N-Nitrosodiphenylamine 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768N-Nitroso-di-n-propylamine 1 07/08/21 22:41 V6348JMV
<1.16 mg/Kg - dry 1.16Pentachlorophenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Phenanthrene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Phenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.768Pyrene 1 07/08/21 22:41 V6348JMV
<0.384 mg/Kg - dry 0.384Pyridine 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7681,2,4-Trichlorobenzene 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682,4,5-Trichlorophenol 1 07/08/21 22:41 V6348JMV
<0.768 mg/Kg - dry 0.7682,4,6-Trichlorophenol 1 07/08/21 22:41 V6348JMV
Surrogate: Phenol-d5 85.2 Limits: 34-121%07/08/21 22:411 JMV V6348
Surrogate: 2-Fluorobiphenyl 101 Limits: 44-115%07/08/21 22:411 JMV V6348
Surrogate: 2-Fluorophenol 88.4 Limits: 35-115%07/08/21 22:411 JMV V6348
Surrogate: Nitrobenzene-d5 85.2 Limits: 37-122%07/08/21 22:411 JMV V6348
Surrogate: 4-Terphenyl-d14 104 Limits: 54-127%07/08/21 22:411 JMV V6348
Surrogate: 2,4,6-Tribromophenol 120 Limits: 39-132%07/08/21 22:411 JMV V6348
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 60 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<58.7 mg/Kg - dry 58.7Aliphatic C19-C36 1 07/09/21 19:06 MADEP-EPHZRC
<9.30 mg/Kg - dry 9.30Aliphatic C5-C8 100 07/06/21 17:20 MADEP-VPHTBL
<9.30 mg/Kg - dry 9.30Aliphatic C9-C12 100 07/06/21 17:20 MADEP-VPHTBL
<58.7 mg/Kg - dry 58.7Aliphatic C9-C18 1 07/09/21 19:06 MADEP-EPHZRC
<58.7 mg/Kg - dry 58.7Aromatic C11-C22 1 07/09/21 19:06 MADEP-EPHZRC
<9.30 mg/Kg - dry 9.30Aromatic C9-C10 100 07/06/21 17:20 MADEP-VPHTBL
<0.023 mg/Kg - dry 0.023Acetone 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Benzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Bromobenzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Bromochloromethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Bromodichloromethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Bromoform 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Bromomethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005n-Butylbenzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005sec-Butyl benzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005tert-Butyl benzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Carbon Tetrachloride 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorobenzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorodibromomethane 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Chloroethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Chloroform 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Chloromethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0052-Chlorotoluene 1 07/06/21 13:15 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 61 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Chlorotoluene 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.0111,2-Dibromo-3-Chloropropane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dibromoethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Dibromomethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichlorobenzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichlorobenzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,4-Dichlorobenzene 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Dichlorodifluoromethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloroethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,2-Dichloroethene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,2-Dichloroethene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloropropane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichloropropane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0052,2-Dichloropropane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloropropene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,3-Dichloropropene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,3-Dichloropropene 1 07/06/21 13:15 8260DTBL
0.018 mg/Kg - dry 0.005Ethylbenzene 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Hexachlorobutadiene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Di-Isopropyl Ether (DIPE)1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Isopropylbenzene 1 07/06/21 13:15 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 62 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Isopropyl toluene 1 07/06/21 13:15 8260DTBL
<0.023 mg/Kg - dry 0.0232-Hexanone 1 07/06/21 13:15 8260DTBL
<0.023 mg/Kg - dry 0.023Methyl Ethyl Ketone (MEK)1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Methylene Chloride 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Methyl tert-butyl ether (MTBE)1 07/06/21 13:15 8260DTBL
<0.023 mg/Kg - dry 0.0234-Methyl-2-Pentanone 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Naphthalene 1 07/06/21 13:15 8260DTBL
0.012 mg/Kg - dry 0.005n-Propylbenzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Styrene 1 07/06/21 13:15 8260DTBL
<0.058 mg/Kg - dry 0.058Ethyl Tertiary Butyl Ether (ETBE)1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1,2-Tetrachloroethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2,2-Tetrachloroethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Tetrachloroethene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Toluene 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.0111,2,3-Trichlorobenzene 1 07/06/21 13:15 8260DTBL
14.0 %Moisture 1 07/08/21 14:25 SW-DRYWTEDV
<0.011 mg/Kg - dry 0.0111,2,4-Trichlorobenzene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1-Trichloroethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2-Trichloroethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005Trichloroethene 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Trichlorofluoromethane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,2,3-Trichloropropane 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.0051,3,5-Trimethylbenzene 1 07/06/21 13:15 8260DTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 63 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.011 mg/Kg - dry 0.011Vinyl Acetate 1 07/06/21 13:15 8260DTBL
<0.011 mg/Kg - dry 0.011Vinyl Chloride 1 07/06/21 13:15 8260DTBL
0.021 mg/Kg - dry 0.011m,p-Xylene 1 07/06/21 13:15 8260DTBL
<0.005 mg/Kg - dry 0.005o-Xylene 1 07/06/21 13:15 8260DTBL
0.021 mg/Kg - dry 0.005Xylene (Total)1 07/06/21 13:15 8260D
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/06/21 13:151 TBL V6202
Surrogate: Dibromofluoromethane 101 Limits: 84-123%07/06/21 13:151 TBL V6202
Surrogate: Toluene-d8 97.6 Limits: 76-129%07/06/21 13:151 TBL V6202
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 64 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V6201 07/06/21 08:00
<0.023 mg/Kg - dry 0.023Acrolein 1 07/06/21 13:15 V6202TBL
<0.023 mg/Kg - dry 0.023Acrylonitrile 1 07/06/21 13:15 V6202TBL
<0.005 mg/Kg - dry 0.005Carbon Disulfide 1 07/06/21 13:15 V6202TBL
<0.011 mg/Kg - dry 0.011n-Hexane 1 07/06/21 13:15 V6202TBL
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%07/06/21 13:151 TBL V6202
Surrogate: Dibromofluoromethane 101 Limits: 84-123%07/06/21 13:151 TBL V6202
Surrogate: Toluene-d8 97.6 Limits: 76-129%07/06/21 13:151 TBL V6202
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.767 mg/Kg - dry 0.767Acenaphthene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Acenaphthylene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Aniline 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Anthracene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Benzo(a)anthracene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Benzo(a)pyrene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Benzo(b)fluoranthene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Benzo(g,h,i)perylene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Benzo(k)fluoranthene 1 07/08/21 23:05 V6348JMV
<2.33 mg/Kg - dry 2.33Benzoic Acid 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Benzyl alcohol 1 07/08/21 23:05 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 65 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.767 mg/Kg - dry 0.767Bis(2-Chloroethoxy)methane 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Bis(2-Chloroethyl)ether 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.383Bis(2-Chloroisopropyl)ether 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Bis(2-ethylhexyl)phthalate 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7674-Bromophenyl phenyl ether 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.383Butyl benzyl phthalate 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7674-Chloro-3-methylphenol 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.3834-Chloroaniline 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672-Chloronaphthalene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672-Chlorophenol 1 07/08/21 23:05 V6348JMV
<1.16 mg/Kg - dry 1.164-Chlorophenyl phenyl ether 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Chrysene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Dibenz(a,h)anthracene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Dibenzofuran 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7671,2-Dichlorobenzene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7671,3-Dichlorobenzene 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.3831,4-Dichlorobenzene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7673,3'-Dichlorobenzidine 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672,4-Dichlorophenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Diethyl phthalate 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Dimethyl phthalate 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.3832,4-Dimethylphenol 1 07/08/21 23:05 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 66 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.767 mg/Kg - dry 0.767Di-n-butyl phthalate 1 07/08/21 23:05 V6348JMV
<1.74 mg/Kg - dry 1.744,6-Dinitro-2-methylphenol 1 07/08/21 23:05 V6348JMV
<1.74 mg/Kg - dry 1.742,4-Dinitrophenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672,4-Dinitrotoluene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672,6-Dinitrotoluene 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.383Di-n-Octyl Phthalate 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Fluoranthene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Fluorene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Hexachlorobenzene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Hexachlorobutadiene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Hexachlorocyclopentadiene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Hexachloroethane 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Indeno(1,2,3-cd)pyrene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Isophorone 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7671-Methylnaphthalene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672-Methylnaphthalene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672-Methylphenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7673&4 Methylphenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Naphthalene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672-Nitroaniline 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7673-Nitroaniline 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.3834-Nitroaniline 1 07/08/21 23:05 V6348JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 67 of 104
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-183-0032
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Kevin Buchanan
Cary
02172214.97 Received : 07/02/2021
Former CC Newell Store
Report Date : 07/13/2021
Sample ID :
Lab No :
Sampled:WR-5
90929 Matrix:
7/1/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V6173 07/06/21 09:00
<0.383 mg/Kg - dry 0.383Nitrobenzene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672-Nitrophenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7674-Nitrophenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767N-Nitrosodimethylamine 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767N-Nitrosodiphenylamine 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767N-Nitroso-di-n-propylamine 1 07/08/21 23:05 V6348JMV
<1.16 mg/Kg - dry 1.16Pentachlorophenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Phenanthrene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Phenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.767Pyrene 1 07/08/21 23:05 V6348JMV
<0.383 mg/Kg - dry 0.383Pyridine 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7671,2,4-Trichlorobenzene 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672,4,5-Trichlorophenol 1 07/08/21 23:05 V6348JMV
<0.767 mg/Kg - dry 0.7672,4,6-Trichlorophenol 1 07/08/21 23:05 V6348JMV
Surrogate: Phenol-d5 75.4 Limits: 34-121%07/08/21 23:051 JMV V6348
Surrogate: 2-Fluorobiphenyl 91.0 Limits: 44-115%07/08/21 23:051 JMV V6348
Surrogate: 2-Fluorophenol 76.3 Limits: 35-115%07/08/21 23:051 JMV V6348
Surrogate: Nitrobenzene-d5 71.3 Limits: 37-122%07/08/21 23:051 JMV V6348
Surrogate: 4-Terphenyl-d14 92.2 Limits: 54-127%07/08/21 23:051 JMV V6348
Surrogate: 2,4,6-Tribromophenol 94.3 Limits: 39-132%07/08/21 23:051 JMV V6348
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 68 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Metals Analyses
6020B
V6315QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V6306
Associated Lab Samples: 90925, 90926
LRB-V6306 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
07/08/21 17:221.00<1.00mg/KgChromium
07/08/21 17:221.00<1.00mg/KgLead
LCS-V6306Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10513.112.5mg/KgChromium 80-120
10513.112.5mg/KgLead 80-120
V 90925-MS-V6306 V 90925-MSD-V6306Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
23.0 12223.512.512.57.73mg/KgChromium 126*75-125 2.1 20
20.0 10720.212.512.56.63mg/KgLead 109 75-125 0.9 20
V 90925-PDS-V6306Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/09/21 01:1210116.6mg/KgChromium
07/09/21 01:1210115.9mg/KgLead
Page 1 of 33* QC Fail Date:07/13/2021 12:09 PM
Page 69 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V6335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V6334
Associated Lab Samples: 90920, 90921, 90922, 90923, 90924
LRB-V6334 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/08/21 13:3610.0< 10.0µg/LAcetone
07/08/21 13:360.500< 0.500µg/LBenzene
07/08/21 13:360.500< 0.500µg/LBromobenzene
07/08/21 13:361.00< 1.00µg/LBromochloromethane
07/08/21 13:360.500< 0.500µg/LBromodichloromethane
07/08/21 13:365.00< 5.00µg/LBromoform
07/08/21 13:361.00< 1.00µg/LBromomethane
07/08/21 13:360.500< 0.500µg/Ln-Butylbenzene
07/08/21 13:360.500< 0.500µg/Lsec-Butyl benzene
07/08/21 13:362.00< 2.00µg/Ltert-Butyl benzene
07/08/21 13:360.500< 0.500µg/LCarbon Tetrachloride
07/08/21 13:360.500< 0.500µg/LChlorobenzene
07/08/21 13:360.500< 0.500µg/LChlorodibromomethane
07/08/21 13:361.00< 1.00µg/LChloroethane
07/08/21 13:360.500< 0.500µg/LChloroform
07/08/21 13:360.500< 0.500µg/LChloromethane
07/08/21 13:360.500< 0.500µg/L2-Chlorotoluene
07/08/21 13:360.500< 0.500µg/L4-Chlorotoluene
07/08/21 13:362.00< 2.00µg/L1,2-Dibromo-3-Chloropropane
07/08/21 13:360.500< 0.500µg/L1,2-Dibromoethane
07/08/21 13:360.500< 0.500µg/LDibromomethane
07/08/21 13:360.500< 0.500µg/L1,2-Dichlorobenzene
07/08/21 13:360.500< 0.500µg/L1,3-Dichlorobenzene
07/08/21 13:360.500< 0.500µg/L1,4-Dichlorobenzene
07/08/21 13:365.00< 5.00µg/LDichlorodifluoromethane
07/08/21 13:360.500< 0.500µg/L1,1-Dichloroethane
07/08/21 13:360.500< 0.500µg/L1,2-Dichloroethane
Page 2 of 33Date:07/13/2021 12:09 PM
Page 70 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V6335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V6334
Associated Lab Samples: 90920, 90921, 90922, 90923, 90924
LRB-V6334 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/08/21 13:360.500< 0.500µg/L1,1-Dichloroethene
07/08/21 13:360.500< 0.500µg/Lcis-1,2-Dichloroethene
07/08/21 13:360.500< 0.500µg/Ltrans-1,2-Dichloroethene
07/08/21 13:360.500< 0.500µg/L1,2-Dichloropropane
07/08/21 13:360.500< 0.500µg/L1,3-Dichloropropane
07/08/21 13:362.00< 2.00µg/L2,2-Dichloropropane
07/08/21 13:360.500< 0.500µg/L1,1-Dichloropropene
07/08/21 13:360.500< 0.500µg/Lcis-1,3-Dichloropropene
07/08/21 13:360.500< 0.500µg/Ltrans-1,3-Dichloropropene
07/08/21 13:36200< 200µg/LEthanol
07/08/21 13:360.500< 0.500µg/LEthylbenzene
07/08/21 13:363.00< 3.00µg/LHexachlorobutadiene
07/08/21 13:360.500< 0.500µg/LDi-Isopropyl Ether (DIPE)
07/08/21 13:360.500< 0.500µg/LIsopropylbenzene
07/08/21 13:360.500< 0.500µg/L4-Isopropyl toluene
07/08/21 13:361.00< 1.00µg/L2-Hexanone
07/08/21 13:365.00< 5.00µg/LMethyl Ethyl Ketone (MEK)
07/08/21 13:362.00< 2.00µg/LMethylene Chloride
07/08/21 13:361.00< 1.00µg/LMethyl tert-butyl ether (MTBE)
07/08/21 13:361.00< 1.00µg/L4-Methyl-2-Pentanone
07/08/21 13:361.00< 1.00µg/LNaphthalene
07/08/21 13:360.500< 0.500µg/Ln-Propylbenzene
07/08/21 13:360.500< 0.500µg/LStyrene
07/08/21 13:360.500< 0.500µg/L1,1,1,2-Tetrachloroethane
07/08/21 13:360.500< 0.500µg/L1,1,2,2-Tetrachloroethane
07/08/21 13:360.500< 0.500µg/LTetrachloroethene
07/08/21 13:360.500< 0.500µg/LToluene
Page 3 of 33Date:07/13/2021 12:09 PM
Page 71 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V6335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V6334
Associated Lab Samples: 90920, 90921, 90922, 90923, 90924
LRB-V6334 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/08/21 13:360.500< 0.500µg/L1,2,3-Trichlorobenzene
07/08/21 13:360.500< 0.500µg/L1,2,4-Trichlorobenzene
07/08/21 13:360.500< 0.500µg/L1,1,1-Trichloroethane
07/08/21 13:360.500< 0.500µg/L1,1,2-Trichloroethane
07/08/21 13:360.500< 0.500µg/LTrichloroethene
07/08/21 13:360.500< 0.500µg/LTrichlorofluoromethane
07/08/21 13:360.500< 0.500µg/L1,2,3-Trichloropropane
07/08/21 13:360.500< 0.500µg/L1,2,4-Trimethylbenzene
07/08/21 13:360.500< 0.500µg/L1,3,5-Trimethylbenzene
07/08/21 13:365.00< 5.00µg/LVinyl Acetate
07/08/21 13:360.500< 0.500µg/LVinyl Chloride
07/08/21 13:361.00< 1.00µg/Lm,p-Xylene
07/08/21 13:360.500< 0.500µg/Lo-Xylene
07/08/21 13:364-Bromofluorobenzene (S)100 70-130
07/08/21 13:36Dibromofluoromethane (S)102 70-130
07/08/21 13:361,2-Dichloroethane - d4 (S)99.6 70-130
07/08/21 13:36Toluene-d8 (S)99.6 70-130
LCS-V6334 LCSD-V6334Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.9 99.794.537.840.0µg/LAcetone 40-160 5.4 20.0
20.3 10210420.820.0µg/LBenzene 70-130 2.4 20.0
20.3 10210320.520.0µg/LBromobenzene 70-130 0.9 20.0
20.9 10510821.620.0µg/LBromochloromethane 70-130 3.2 20.0
23.0 11511623.120.0µg/LBromodichloromethane 70-130 0.4 20.0
Page 4 of 33Date:07/13/2021 12:09 PM
Page 72 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V6335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V6334
LCS-V6334 LCSD-V6334Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.1 10610320.620.0µg/LBromoform 70-130 2.3 20.0
23.1 11611723.320.0µg/LBromomethane 60-140 0.8 20.0
21.0 10510821.620.0µg/Ln-Butylbenzene 70-130 2.8 20.0
21.0 10510621.220.0µg/Lsec-Butyl benzene 70-130 0.9 20.0
20.4 10210320.620.0µg/Ltert-Butyl benzene 70-130 0.9 20.0
20.8 10410921.720.0µg/LCarbon Tetrachloride 70-130 4.2 20.0
20.6 10310420.720.0µg/LChlorobenzene 70-130 0.4 20.0
20.4 10210220.320.0µg/LChlorodibromomethane 70-130 0.4 20.0
22.9 11512024.020.0µg/LChloroethane 60-140 4.6 20.0
19.0 95.098.019.620.0µg/LChloroform 70-130 3.1 20.0
16.9 84.586.517.320.0µg/LChloromethane 60-140 2.3 20.0
20.9 10596.519.320.0µg/L2-Chlorotoluene 70-130 7.9 20.0
20.1 10110420.720.0µg/L4-Chlorotoluene 70-130 2.9 20.0
20.8 10410721.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 2.8 20.0
20.2 10110020.020.0µg/L1,2-Dibromoethane 70-130 0.9 20.0
21.0 10510621.120.0µg/LDibromomethane 70-130 0.4 20.0
20.5 10310420.720.0µg/L1,2-Dichlorobenzene 70-130 0.9 20.0
20.3 10210320.520.0µg/L1,3-Dichlorobenzene 70-130 0.9 20.0
19.9 99.510120.120.0µg/L1,4-Dichlorobenzene 70-130 1.0 20.0
18.6 93.094.018.820.0µg/LDichlorodifluoromethane 60-140 1.0 20.0
21.2 10611021.920.0µg/L1,1-Dichloroethane 70-130 3.2 20.0
20.8 10410520.920.0µg/L1,2-Dichloroethane 70-130 0.4 20.0
20.3 10210921.820.0µg/L1,1-Dichloroethene 70-130 7.1 20.0
20.9 10510520.920.0µg/Lcis-1,2-Dichloroethene 70-130 0.0 20.0
20.8 10410821.520.0µg/Ltrans-1,2-Dichloroethene 70-130 3.3 20.0
21.4 10710821.620.0µg/L1,2-Dichloropropane 70-130 0.9 20.0
Page 5 of 33Date:07/13/2021 12:09 PM
Page 73 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V6335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V6334
LCS-V6334 LCSD-V6334Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.6 10310220.420.0µg/L1,3-Dichloropropane 70-130 0.9 20.0
25.1 12612424.820.0µg/L2,2-Dichloropropane 70-130 1.2 20.0
20.5 10310621.220.0µg/L1,1-Dichloropropene 70-130 3.3 20.0
22.9 11511923.720.0µg/Lcis-1,3-Dichloropropene 70-130 3.4 20.0
22.9 11511823.520.0µg/Ltrans-1,3-Dichloropropene 70-130 2.5 20.0
592 118121605500µg/LEthanol 60-140 2.1 20.0
20.2 10110220.420.0µg/LEthylbenzene 70-130 0.9 20.0
20.6 10310621.220.0µg/LHexachlorobutadiene 70-130 2.8 20.0
21.2 10610721.320.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.4 20.0
20.3 10210621.120.0µg/LIsopropylbenzene 70-130 3.8 20.0
20.7 10410621.220.0µg/L4-Isopropyl toluene 70-130 2.3 20.0
22.4 11210821.520.0µg/L2-Hexanone 60-140 4.1 20.0
19.3 96.596.019.220.0µg/LMethyl Ethyl Ketone (MEK)60-140 0.5 20.0
20.1 10110320.520.0µg/LMethylene Chloride 70-130 1.9 20.0
22.0 11010721.420.0µg/LMethyl tert-butyl ether (MTBE)70-130 2.7 20.0
21.6 10810420.820.0µg/L4-Methyl-2-Pentanone 60-140 3.7 20.0
20.9 10511723.420.0µg/LNaphthalene 70-130 11.2 20.0
20.4 10210420.820.0µg/Ln-Propylbenzene 70-130 1.9 20.0
20.9 10510721.420.0µg/LStyrene 70-130 2.3 20.0
20.4 10210120.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.4 20.0
21.9 11010520.920.0µg/L1,1,2,2-Tetrachloroethane 70-130 4.6 20.0
20.6 10310320.620.0µg/LTetrachloroethene 70-130 0.0 20.0
20.3 10210320.620.0µg/LToluene 70-130 1.4 20.0
19.3 96.510521.020.0µg/L1,2,3-Trichlorobenzene 70-130 8.4 20.0
21.3 10711322.620.0µg/L1,2,4-Trichlorobenzene 70-130 5.9 20.0
22.3 11211523.020.0µg/L1,1,1-Trichloroethane 70-130 3.0 20.0
Page 6 of 33Date:07/13/2021 12:09 PM
Page 74 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V6335QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V6334
LCS-V6334 LCSD-V6334Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
21.4 10710621.120.0µg/L1,1,2-Trichloroethane 70-130 1.4 20.0
20.4 10210420.820.0µg/LTrichloroethene 70-130 1.9 20.0
21.3 10711022.020.0µg/LTrichlorofluoromethane 60-140 3.2 20.0
21.2 10610220.320.0µg/L1,2,3-Trichloropropane 70-130 4.3 20.0
20.7 10410520.920.0µg/L1,2,4-Trimethylbenzene 70-130 0.9 20.0
20.7 10410521.020.0µg/L1,3,5-Trimethylbenzene 70-130 1.4 20.0
25.0 12512224.320.0µg/LVinyl Acetate 60-140 2.8 20.0
20.5 10310721.320.0µg/LVinyl Chloride 60-140 3.8 20.0
42.1 10510642.240.0µg/Lm,p-Xylene 70-130 0.2 20.0
20.6 10310420.720.0µg/Lo-Xylene 70-130 0.4 20.0
99.61004-Bromofluorobenzene (S)70-130
101102Dibromofluoromethane (S)70-130
1031031,2-Dichloroethane - d4 (S)70-130
99.899.0Toluene-d8 (S)70-130
Page 7 of 33Date:07/13/2021 12:09 PM
Page 75 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6202QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6201
Associated Lab Samples: 90925, 90927, 90928, 90929
LRB-V6201 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/21 11:450.020<0.020mg/KgAcetone
07/06/21 11:450.005<0.005mg/KgBenzene
07/06/21 11:450.005<0.005mg/KgBromobenzene
07/06/21 11:450.005<0.005mg/KgBromochloromethane
07/06/21 11:450.005<0.005mg/KgBromodichloromethane
07/06/21 11:450.005<0.005mg/KgBromoform
07/06/21 11:450.010<0.010mg/KgBromomethane
07/06/21 11:450.005<0.005mg/Kgn-Butylbenzene
07/06/21 11:450.005<0.005mg/Kgsec-Butyl benzene
07/06/21 11:450.005<0.005mg/Kgtert-Butyl benzene
07/06/21 11:450.005<0.005mg/KgCarbon Tetrachloride
07/06/21 11:450.005<0.005mg/KgChlorobenzene
07/06/21 11:450.005<0.005mg/KgChlorodibromomethane
07/06/21 11:450.010<0.010mg/KgChloroethane
07/06/21 11:450.005<0.005mg/KgChloroform
07/06/21 11:450.010<0.010mg/KgChloromethane
07/06/21 11:450.005<0.005mg/Kg2-Chlorotoluene
07/06/21 11:450.005<0.005mg/Kg4-Chlorotoluene
07/06/21 11:450.010<0.010mg/Kg1,2-Dibromo-3-Chloropropane
07/06/21 11:450.005<0.005mg/Kg1,2-Dibromoethane
07/06/21 11:450.005<0.005mg/KgDibromomethane
07/06/21 11:450.005<0.005mg/Kg1,2-Dichlorobenzene
07/06/21 11:450.005<0.005mg/Kg1,3-Dichlorobenzene
07/06/21 11:450.005<0.005mg/Kg1,4-Dichlorobenzene
07/06/21 11:450.010<0.010mg/KgDichlorodifluoromethane
07/06/21 11:450.005<0.005mg/Kg1,1-Dichloroethane
07/06/21 11:450.005<0.005mg/Kg1,2-Dichloroethane
Page 8 of 33Date:07/13/2021 12:09 PM
Page 76 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6202QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6201
Associated Lab Samples: 90925, 90927, 90928, 90929
LRB-V6201 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/21 11:450.005<0.005mg/Kg1,1-Dichloroethene
07/06/21 11:450.005<0.005mg/Kgcis-1,2-Dichloroethene
07/06/21 11:450.005<0.005mg/Kgtrans-1,2-Dichloroethene
07/06/21 11:450.005<0.005mg/Kg1,2-Dichloropropane
07/06/21 11:450.005<0.005mg/Kg1,3-Dichloropropane
07/06/21 11:450.005<0.005mg/Kg2,2-Dichloropropane
07/06/21 11:450.005<0.005mg/Kg1,1-Dichloropropene
07/06/21 11:450.005<0.005mg/Kgcis-1,3-Dichloropropene
07/06/21 11:450.005<0.005mg/Kgtrans-1,3-Dichloropropene
07/06/21 11:450.005<0.005mg/KgEthylbenzene
07/06/21 11:450.010<0.010mg/KgHexachlorobutadiene
07/06/21 11:450.005<0.005mg/KgDi-Isopropyl Ether (DIPE)
07/06/21 11:450.005<0.005mg/KgIsopropylbenzene
07/06/21 11:450.005<0.005mg/Kg4-Isopropyl toluene
07/06/21 11:450.020<0.020mg/Kg2-Hexanone
07/06/21 11:450.020<0.020mg/KgMethyl Ethyl Ketone (MEK)
07/06/21 11:450.010<0.010mg/KgMethylene Chloride
07/06/21 11:450.005<0.005mg/KgMethyl tert-butyl ether (MTBE)
07/06/21 11:450.020<0.020mg/Kg4-Methyl-2-Pentanone
07/06/21 11:450.010<0.010mg/KgNaphthalene
07/06/21 11:450.005<0.005mg/Kgn-Propylbenzene
07/06/21 11:450.005<0.005mg/KgStyrene
07/06/21 11:450.050<0.050mg/KgEthyl Tertiary Butyl Ether (ETBE)
07/06/21 11:450.005<0.005mg/Kg1,1,1,2-Tetrachloroethane
07/06/21 11:450.005<0.005mg/Kg1,1,2,2-Tetrachloroethane
07/06/21 11:450.005<0.005mg/KgTetrachloroethene
07/06/21 11:450.005<0.005mg/KgToluene
Page 9 of 33Date:07/13/2021 12:09 PM
Page 77 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6202QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6201
Associated Lab Samples: 90925, 90927, 90928, 90929
LRB-V6201 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/21 11:450.010<0.010mg/Kg1,2,3-Trichlorobenzene
07/06/21 11:450.010<0.010mg/Kg1,2,4-Trichlorobenzene
07/06/21 11:450.005<0.005mg/Kg1,1,1-Trichloroethane
07/06/21 11:450.005<0.005mg/Kg1,1,2-Trichloroethane
07/06/21 11:450.005<0.005mg/KgTrichloroethene
07/06/21 11:450.010<0.010mg/KgTrichlorofluoromethane
07/06/21 11:450.005<0.005mg/Kg1,2,3-Trichloropropane
07/06/21 11:450.005<0.005mg/Kg1,3,5-Trimethylbenzene
07/06/21 11:450.010<0.010mg/KgVinyl Acetate
07/06/21 11:450.010<0.010mg/KgVinyl Chloride
07/06/21 11:450.010<0.010mg/Kgm,p-Xylene
07/06/21 11:450.005<0.005mg/Kgo-Xylene
07/06/21 11:450.020<0.020mg/KgAcrolein
07/06/21 11:450.020<0.020mg/KgAcrylonitrile
07/06/21 11:450.005<0.005mg/KgCarbon Disulfide
07/06/21 11:450.010<0.010mg/Kgn-Hexane
07/06/21 11:454-Bromofluorobenzene (S)99.6 70-130
07/06/21 11:45Dibromofluoromethane (S)99.6 84-123
07/06/21 11:45Toluene-d8 (S)98.4 76-129
LCS-V6201 LCSD-V6201Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.094.10.0940.100mg/KgAcetone 29-198 1.1 20
0.051 1021060.0520.050mg/KgBenzene 74-127 3.0 20
0.049 99.21010.0500.050mg/KgBromobenzene 73-125 1.6 20
Page 10 of 33Date:07/13/2021 12:09 PM
Page 78 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6202QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6201
LCS-V6201 LCSD-V6201Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031040.0510.050mg/KgBromochloromethane 72-134 0.9 20
0.051 1031050.0520.050mg/KgBromodichloromethane 75-122 1.1 20
0.053 1061070.0530.050mg/KgBromoform 66-135 1.1 20
0.038 77.680.20.0400.050mg/KgBromomethane 20-180 3.2 20
0.050 1011070.0530.050mg/Kgn-Butylbenzene 65-135 5.1 20
0.050 1011060.0530.050mg/Kgsec-Butyl benzene 66-131 4.8 20
0.049 99.81040.0520.050mg/Kgtert-Butyl benzene 67-132 4.5 20
0.049 99.21040.0510.050mg/KgCarbon Tetrachloride 64-143 4.5 20
0.051 1021040.0520.050mg/KgChlorobenzene 74-118 1.7 20
0.051 1031050.0520.050mg/KgChlorodibromomethane 73-122 1.5 20
0.044 88.497.00.0480.050mg/KgChloroethane 33-149 9.2 20
0.050 1001020.0510.050mg/KgChloroform 73-127 2.3 20
0.039 78.482.20.0410.050mg/KgChloromethane 45-143 4.7 20
0.050 1001040.0510.050mg/Kg2-Chlorotoluene 67-124 3.3 20
0.050 1001040.0510.050mg/Kg4-Chlorotoluene 71-126 3.1 20
0.049 98.61030.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.3 20
0.051 1021030.0510.050mg/Kg1,2-Dibromoethane 70-132 0.3 20
0.053 1061060.0520.050mg/KgDibromomethane 74-133 0.3 20
0.050 1001020.0500.050mg/Kg1,2-Dichlorobenzene 72-123 1.3 20
0.050 1001030.0510.050mg/Kg1,3-Dichlorobenzene 71-120 2.7 20
0.050 1011030.0510.050mg/Kg1,4-Dichlorobenzene 71-123 1.5 20
0.041 82.488.20.0440.050mg/KgDichlorodifluoromethane 26-146 6.7 20
0.051 1021040.0520.050mg/Kg1,1-Dichloroethane 74-127 2.3 20
0.050 1011010.0500.050mg/Kg1,2-Dichloroethane 68-128 0.1 20
0.049 99.41060.0520.050mg/Kg1,1-Dichloroethene 67-149 6.2 20
0.051 1021040.0520.050mg/Kgcis-1,2-Dichloroethene 76-134 1.7 20
Page 11 of 33Date:07/13/2021 12:09 PM
Page 79 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6202QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6201
LCS-V6201 LCSD-V6201Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1021050.0520.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.2 20
0.051 1031030.0510.050mg/Kg1,2-Dichloropropane 73-130 0.3 20
0.050 1021010.0500.050mg/Kg1,3-Dichloropropane 75-124 0.5 20
0.049 98.21050.0520.050mg/Kg2,2-Dichloropropane 50-142 6.8 20
0.050 1011070.0530.050mg/Kg1,1-Dichloropropene 71-130 5.5 20
0.052 1041040.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20
0.052 1051040.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.3 20
0.050 1021040.0520.050mg/KgEthylbenzene 74-128 2.1 20
0.049 99.81050.0520.050mg/KgHexachlorobutadiene 64-125 4.6 20
0.052 1051050.0520.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.5 20
0.050 1011040.0520.050mg/KgIsopropylbenzene 68-126 3.5 20
0.050 1001050.0520.050mg/Kg4-Isopropyl toluene 68-129 4.8 20
0.049 99.81010.0500.050mg/Kg2-Hexanone 61-157 0.9 20
0.047 95.498.00.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.6 20
0.049 98.01010.0500.050mg/KgMethylene Chloride 74-129 2.6 20
0.051 1041030.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.7 20
0.050 1021020.0510.050mg/Kg4-Methyl-2-Pentanone 57-162 0.5 20
0.052 1061100.0540.050mg/KgNaphthalene 57-157 3.7 20
0.050 1011050.0520.050mg/Kgn-Propylbenzene 67-130 3.8 20
0.052 1041060.0520.050mg/KgStyrene 77-121 1.5 20
0.106 1061050.1050.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.051 1021030.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.1 20
0.049 99.81020.0510.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.5 20
0.050 1021060.0520.050mg/KgTetrachloroethene 68-130 3.6 20
0.050 1011050.0520.050mg/KgToluene 71-129 3.1 20
0.052 1041060.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.1 20
Page 12 of 33Date:07/13/2021 12:09 PM
Page 80 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6202QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6201
LCS-V6201 LCSD-V6201Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031060.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.1 20
0.050 1011070.0530.050mg/Kg1,1,1-Trichloroethane 67-131 5.1 20
0.051 1031020.0510.050mg/Kg1,1,2-Trichloroethane 70-133 0.7 20
0.051 1021050.0520.050mg/KgTrichloroethene 75-133 2.5 20
0.044 89.895.00.0470.050mg/KgTrichlorofluoromethane 44-146 5.6 20
0.049 98.698.80.0490.050mg/Kg1,2,3-Trichloropropane 60-137 0.2 20
0.050 1011040.0520.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.5 20
0.052 1051060.0520.050mg/KgVinyl Acetate 85-161 0.1 20
0.043 86.492.40.0460.050mg/KgVinyl Chloride 48-147 6.7 20
0.104 1041070.1070.100mg/Kgm,p-Xylene 75-124 2.8 20
0.051 1021040.0520.050mg/Kgo-Xylene 74-126 1.9 20
0.102 1021040.1040.100mg/KgAcrolein 70-130 1.9 20
0.098 98.41010.1010.100mg/KgAcrylonitrile 65-134 2.6 20
0.050 1001040.0520.050mg/KgCarbon Disulfide 61-129 4.3 20
0.052 1051140.0560.050mg/Kgn-Hexane 70-130 7.6 20
99.21004-Bromofluorobenzene (S)70-130
10098.2Dibromofluoromethane (S)84-123
99.097.8Toluene-d8 (S)76-129
Page 13 of 33Date:07/13/2021 12:09 PM
Page 81 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6204QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V6203
Associated Lab Samples: 90926
LRB-V6203 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/21 11:450.020<0.020mg/KgAcetone
07/06/21 11:450.005<0.005mg/KgBenzene
07/06/21 11:450.005<0.005mg/KgBromobenzene
07/06/21 11:450.005<0.005mg/KgBromochloromethane
07/06/21 11:450.005<0.005mg/KgBromodichloromethane
07/06/21 11:450.005<0.005mg/KgBromoform
07/06/21 11:450.010<0.010mg/KgBromomethane
07/06/21 11:450.005<0.005mg/Kgn-Butylbenzene
07/06/21 11:450.005<0.005mg/Kgsec-Butyl benzene
07/06/21 11:450.005<0.005mg/Kgtert-Butyl benzene
07/06/21 11:450.005<0.005mg/KgCarbon Tetrachloride
07/06/21 11:450.005<0.005mg/KgChlorobenzene
07/06/21 11:450.005<0.005mg/KgChlorodibromomethane
07/06/21 11:450.010<0.010mg/KgChloroethane
07/06/21 11:450.005<0.005mg/KgChloroform
07/06/21 11:450.010<0.010mg/KgChloromethane
07/06/21 11:450.005<0.005mg/Kg2-Chlorotoluene
07/06/21 11:450.005<0.005mg/Kg4-Chlorotoluene
07/06/21 11:450.010<0.010mg/Kg1,2-Dibromo-3-Chloropropane
07/06/21 11:450.005<0.005mg/Kg1,2-Dibromoethane
07/06/21 11:450.005<0.005mg/KgDibromomethane
07/06/21 11:450.005<0.005mg/Kg1,2-Dichlorobenzene
07/06/21 11:450.005<0.005mg/Kg1,3-Dichlorobenzene
07/06/21 11:450.005<0.005mg/Kg1,4-Dichlorobenzene
07/06/21 11:450.010<0.010mg/KgDichlorodifluoromethane
07/06/21 11:450.005<0.005mg/Kg1,1-Dichloroethane
07/06/21 11:450.005<0.005mg/Kg1,2-Dichloroethane
Page 14 of 33Date:07/13/2021 12:09 PM
Page 82 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6204QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V6203
Associated Lab Samples: 90926
LRB-V6203 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/21 11:450.005<0.005mg/Kg1,1-Dichloroethene
07/06/21 11:450.005<0.005mg/Kgcis-1,2-Dichloroethene
07/06/21 11:450.005<0.005mg/Kgtrans-1,2-Dichloroethene
07/06/21 11:450.005<0.005mg/Kg1,2-Dichloropropane
07/06/21 11:450.005<0.005mg/Kg1,3-Dichloropropane
07/06/21 11:450.005<0.005mg/Kg2,2-Dichloropropane
07/06/21 11:450.005<0.005mg/Kg1,1-Dichloropropene
07/06/21 11:450.005<0.005mg/Kgcis-1,3-Dichloropropene
07/06/21 11:450.005<0.005mg/Kgtrans-1,3-Dichloropropene
07/06/21 11:450.005<0.005mg/KgEthylbenzene
07/06/21 11:450.010<0.010mg/KgHexachlorobutadiene
07/06/21 11:450.005<0.005mg/KgDi-Isopropyl Ether (DIPE)
07/06/21 11:450.005<0.005mg/KgIsopropylbenzene
07/06/21 11:450.005<0.005mg/Kg4-Isopropyl toluene
07/06/21 11:450.020<0.020mg/Kg2-Hexanone
07/06/21 11:450.020<0.020mg/KgMethyl Ethyl Ketone (MEK)
07/06/21 11:450.005<0.005mg/KgMethylene Chloride
07/06/21 11:450.005<0.005mg/KgMethyl tert-butyl ether (MTBE)
07/06/21 11:450.010<0.010mg/KgNaphthalene
07/06/21 11:450.005<0.005mg/Kgn-Propylbenzene
07/06/21 11:450.005<0.005mg/KgStyrene
07/06/21 11:450.100<0.100mg/KgEthyl Tertiary Butyl Ether (ETBE)
07/06/21 11:450.005<0.005mg/Kg1,1,1,2-Tetrachloroethane
07/06/21 11:450.005<0.005mg/Kg1,1,2,2-Tetrachloroethane
07/06/21 11:450.005<0.005mg/KgTetrachloroethene
07/06/21 11:450.005<0.005mg/KgToluene
07/06/21 11:450.010<0.010mg/Kg1,2,3-Trichlorobenzene
Page 15 of 33Date:07/13/2021 12:09 PM
Page 83 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6204QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V6203
Associated Lab Samples: 90926
LRB-V6203 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/21 11:450.010<0.010mg/Kg1,2,4-Trichlorobenzene
07/06/21 11:450.005<0.005mg/Kg1,1,1-Trichloroethane
07/06/21 11:450.005<0.005mg/Kg1,1,2-Trichloroethane
07/06/21 11:450.005<0.005mg/KgTrichloroethene
07/06/21 11:450.010<0.010mg/KgTrichlorofluoromethane
07/06/21 11:450.005<0.005mg/Kg1,2,3-Trichloropropane
07/06/21 11:450.005<0.005mg/Kg1,3,5-Trimethylbenzene
07/06/21 11:450.010<0.010mg/KgVinyl Acetate
07/06/21 11:450.010<0.010mg/KgVinyl Chloride
07/06/21 11:450.010<0.010mg/Kgm,p-Xylene
07/06/21 11:450.005<0.005mg/Kgo-Xylene
07/06/21 11:450.020<0.020mg/KgAcrolein
07/06/21 11:450.020<0.020mg/KgAcrylonitrile
07/06/21 11:450.005<0.005mg/KgCarbon Disulfide
07/06/21 11:450.010<0.010mg/Kgn-Hexane
07/06/21 11:454-Bromofluorobenzene (S)99.6 70-130
07/06/21 11:45Dibromofluoromethane (S)99.6 70-130
07/06/21 11:45Toluene-d8 (S)98.4 76-129
LCS-V6203 LCSD-V6203Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.093 93.094.10.0940.100mg/KgAcetone 29-198 1.1 20
0.051 1021060.0520.050mg/KgBenzene 74-127 3.0 20
0.049 99.21010.0500.050mg/KgBromobenzene 73-125 1.6 20
0.051 1031040.0510.050mg/KgBromochloromethane 72-134 0.9 20
Page 16 of 33Date:07/13/2021 12:09 PM
Page 84 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6204QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V6203
LCS-V6203 LCSD-V6203Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031050.0520.050mg/KgBromodichloromethane 75-122 1.1 20
0.053 1061070.0530.050mg/KgBromoform 66-135 1.1 20
0.038 77.680.20.0400.050mg/KgBromomethane 20-180 3.2 20
0.050 1011070.0530.050mg/Kgn-Butylbenzene 65-135 5.1 20
0.050 1011060.0530.050mg/Kgsec-Butyl benzene 66-131 4.8 20
0.049 99.81040.0520.050mg/Kgtert-Butyl benzene 67-132 4.5 20
0.049 99.21040.0510.050mg/KgCarbon Tetrachloride 64-143 4.5 20
0.051 1021040.0520.050mg/KgChlorobenzene 74-118 1.7 20
0.051 1031050.0520.050mg/KgChlorodibromomethane 73-122 1.5 20
0.044 88.497.00.0480.050mg/KgChloroethane 33-149 9.2 20
0.050 1001020.0510.050mg/KgChloroform 73-127 2.3 20
0.039 78.482.20.0410.050mg/KgChloromethane 45-143 4.7 20
0.050 1001040.0510.050mg/Kg2-Chlorotoluene 67-124 3.3 20
0.050 1001040.0510.050mg/Kg4-Chlorotoluene 71-126 3.1 20
0.049 98.61030.0510.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 4.3 20
0.051 1021030.0510.050mg/Kg1,2-Dibromoethane 70-132 0.3 20
0.053 1061060.0520.050mg/KgDibromomethane 74-133 0.3 20
0.050 1001020.0500.050mg/Kg1,2-Dichlorobenzene 72-123 1.3 20
0.050 1001030.0510.050mg/Kg1,3-Dichlorobenzene 71-120 2.7 20
0.050 1011030.0510.050mg/Kg1,4-Dichlorobenzene 71-123 1.5 20
0.041 82.488.20.0440.050mg/KgDichlorodifluoromethane 26-146 6.7 20
0.051 1021040.0520.050mg/Kg1,1-Dichloroethane 74-127 2.3 20
0.050 1011010.0500.050mg/Kg1,2-Dichloroethane 68-128 0.1 20
0.049 99.41060.0520.050mg/Kg1,1-Dichloroethene 67-149 6.2 20
0.051 1021040.0520.050mg/Kgcis-1,2-Dichloroethene 76-134 1.7 20
0.051 1021050.0520.050mg/Kgtrans-1,2-Dichloroethene 73-132 3.2 20
Page 17 of 33Date:07/13/2021 12:09 PM
Page 85 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6204QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V6203
LCS-V6203 LCSD-V6203Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031030.0510.050mg/Kg1,2-Dichloropropane 73-130 0.3 20
0.050 1021010.0500.050mg/Kg1,3-Dichloropropane 75-124 0.5 20
0.049 98.21050.0520.050mg/Kg2,2-Dichloropropane 50-142 6.8 20
0.050 1011070.0530.050mg/Kg1,1-Dichloropropene 71-130 5.5 20
0.052 1041040.0510.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20
0.052 1051040.0510.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.3 20
0.050 1021040.0520.050mg/KgEthylbenzene 74-128 2.1 20
0.049 99.81050.0520.050mg/KgHexachlorobutadiene 64-125 4.6 20
0.052 1051050.0520.050mg/KgDi-Isopropyl Ether (DIPE)59-159 0.5 20
0.050 1011040.0520.050mg/KgIsopropylbenzene 68-126 3.5 20
0.050 1001050.0520.050mg/Kg4-Isopropyl toluene 68-129 4.8 20
0.049 99.81010.0500.050mg/Kg2-Hexanone 61-157 0.9 20
0.047 95.498.00.0490.050mg/KgMethyl Ethyl Ketone (MEK)63-149 2.6 20
0.049 98.01010.0500.050mg/KgMethylene Chloride 74-129 2.6 20
0.051 1041030.0510.050mg/KgMethyl tert-butyl ether (MTBE)70-130 0.7 20
0.052 1061100.0540.050mg/KgNaphthalene 57-157 3.7 20
0.050 1011050.0520.050mg/Kgn-Propylbenzene 67-130 3.8 20
0.052 1041060.0520.050mg/KgStyrene 77-121 1.5 20
0.106 1061050.1050.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.9 20
0.051 1021030.0510.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.1 20
0.049 99.81020.0510.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 2.5 20
0.050 1021060.0520.050mg/KgTetrachloroethene 68-130 3.6 20
0.050 1011050.0520.050mg/KgToluene 71-129 3.1 20
0.052 1041060.0520.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.1 20
0.051 1031060.0520.050mg/Kg1,2,4-Trichlorobenzene 66-125 2.1 20
0.050 1011070.0530.050mg/Kg1,1,1-Trichloroethane 67-131 5.1 20
Page 18 of 33Date:07/13/2021 12:09 PM
Page 86 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6204QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 MED
QC Prep:V6203
LCS-V6203 LCSD-V6203Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031020.0510.050mg/Kg1,1,2-Trichloroethane 70-133 0.7 20
0.051 1021050.0520.050mg/KgTrichloroethene 75-133 2.5 20
0.044 89.895.00.0470.050mg/KgTrichlorofluoromethane 44-146 5.6 20
0.049 98.698.80.0490.050mg/Kg1,2,3-Trichloropropane 60-137 0.2 20
0.050 1011040.0520.050mg/Kg1,3,5-Trimethylbenzene 69-128 3.5 20
0.052 1051060.0520.050mg/KgVinyl Acetate 85-161 0.1 20
0.043 86.492.40.0460.050mg/KgVinyl Chloride 48-147 6.7 20
0.104 1041070.1070.100mg/Kgm,p-Xylene 75-124 2.8 20
0.051 1021040.0520.050mg/Kgo-Xylene 74-126 1.9 20
0.102 1021040.1040.100mg/KgAcrolein 70-130 1.9 20
0.098 98.41010.1010.100mg/KgAcrylonitrile 65-134 2.6 20
0.050 1001040.0520.050mg/KgCarbon Disulfide 61-129 4.3 20
0.052 1051140.0560.050mg/Kgn-Hexane 70-130 7.6 20
99.21004-Bromofluorobenzene (S)70-130
10098.2Dibromofluoromethane (S)70-130
99.097.8Toluene-d8 (S)76-129
Page 19 of 33Date:07/13/2021 12:09 PM
Page 87 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
Associated Lab Samples: 90925, 90926, 90927, 90928, 90929
LRB-V6173 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/08/21 12:170.660<0.660mg/KgAcenaphthene
07/08/21 12:170.660<0.660mg/KgAcenaphthylene
07/08/21 12:170.660<0.660mg/KgAniline
07/08/21 12:170.660<0.660mg/KgAnthracene
07/08/21 12:170.660<0.660mg/KgBenzo(a)anthracene
07/08/21 12:170.660<0.660mg/KgBenzo(a)pyrene
07/08/21 12:170.660<0.660mg/KgBenzo(b)fluoranthene
07/08/21 12:170.660<0.660mg/KgBenzo(g,h,i)perylene
07/08/21 12:170.660<0.660mg/KgBenzo(k)fluoranthene
07/08/21 12:172.00<2.00mg/KgBenzoic Acid
07/08/21 12:170.660<0.660mg/KgBenzyl alcohol
07/08/21 12:170.660<0.660mg/KgBis(2-Chloroethoxy)methane
07/08/21 12:170.660<0.660mg/KgBis(2-Chloroethyl)ether
07/08/21 12:170.330<0.330mg/KgBis(2-Chloroisopropyl)ether
07/08/21 12:170.660<0.660mg/KgBis(2-ethylhexyl)phthalate
07/08/21 12:170.660<0.660mg/Kg4-Bromophenyl phenyl ether
07/08/21 12:170.330<0.330mg/KgButyl benzyl phthalate
07/08/21 12:170.660<0.660mg/Kg4-Chloro-3-methylphenol
07/08/21 12:170.330<0.330mg/Kg4-Chloroaniline
07/08/21 12:170.660<0.660mg/Kg2-Chloronaphthalene
07/08/21 12:170.660<0.660mg/Kg2-Chlorophenol
07/08/21 12:171.00<1.00mg/Kg4-Chlorophenyl phenyl ether
07/08/21 12:170.660<0.660mg/KgChrysene
07/08/21 12:170.660<0.660mg/KgDibenz(a,h)anthracene
07/08/21 12:170.660<0.660mg/KgDibenzofuran
07/08/21 12:170.660<0.660mg/Kg1,2-Dichlorobenzene
07/08/21 12:170.660<0.660mg/Kg1,3-Dichlorobenzene
Page 20 of 33Date:07/13/2021 12:09 PM
Page 88 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
Associated Lab Samples: 90925, 90926, 90927, 90928, 90929
LRB-V6173 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/08/21 12:170.330<0.330mg/Kg1,4-Dichlorobenzene
07/08/21 12:170.660<0.660mg/Kg3,3'-Dichlorobenzidine
07/08/21 12:170.660<0.660mg/Kg2,4-Dichlorophenol
07/08/21 12:170.660<0.660mg/KgDiethyl phthalate
07/08/21 12:170.660<0.660mg/KgDimethyl phthalate
07/08/21 12:170.330<0.330mg/Kg2,4-Dimethylphenol
07/08/21 12:170.660<0.660mg/KgDi-n-butyl phthalate
07/08/21 12:171.50<1.50mg/Kg4,6-Dinitro-2-methylphenol
07/08/21 12:171.50<1.50mg/Kg2,4-Dinitrophenol
07/08/21 12:170.660<0.660mg/Kg2,4-Dinitrotoluene
07/08/21 12:170.660<0.660mg/Kg2,6-Dinitrotoluene
07/08/21 12:170.330<0.330mg/KgDi-n-Octyl Phthalate
07/08/21 12:170.660<0.660mg/KgFluoranthene
07/08/21 12:170.660<0.660mg/KgFluorene
07/08/21 12:170.660<0.660mg/KgHexachlorobenzene
07/08/21 12:170.660<0.660mg/KgHexachlorobutadiene
07/08/21 12:170.660<0.660mg/KgHexachlorocyclopentadiene
07/08/21 12:170.660<0.660mg/KgHexachloroethane
07/08/21 12:170.660<0.660mg/KgIndeno(1,2,3-cd)pyrene
07/08/21 12:170.660<0.660mg/KgIsophorone
07/08/21 12:170.660<0.660mg/Kg1-Methylnaphthalene
07/08/21 12:170.660<0.660mg/Kg2-Methylnaphthalene
07/08/21 12:170.660<0.660mg/Kg2-Methylphenol
07/08/21 12:170.660<0.660mg/Kg3&4 Methylphenol
07/08/21 12:170.660<0.660mg/KgNaphthalene
07/08/21 12:170.660<0.660mg/Kg2-Nitroaniline
07/08/21 12:170.660<0.660mg/Kg3-Nitroaniline
Page 21 of 33Date:07/13/2021 12:09 PM
Page 89 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
Associated Lab Samples: 90925, 90926, 90927, 90928, 90929
LRB-V6173 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/08/21 12:170.330<0.330mg/Kg4-Nitroaniline
07/08/21 12:170.330<0.330mg/KgNitrobenzene
07/08/21 12:170.660<0.660mg/Kg2-Nitrophenol
07/08/21 12:170.660<0.660mg/Kg4-Nitrophenol
07/08/21 12:170.660<0.660mg/KgN-Nitrosodimethylamine
07/08/21 12:170.660<0.660mg/KgN-Nitrosodiphenylamine
07/08/21 12:170.660<0.660mg/KgN-Nitroso-di-n-propylamine
07/08/21 12:171.00<1.00mg/KgPentachlorophenol
07/08/21 12:170.660<0.660mg/KgPhenanthrene
07/08/21 12:170.660<0.660mg/KgPhenol
07/08/21 12:170.660<0.660mg/KgPyrene
07/08/21 12:170.330<0.330mg/KgPyridine
07/08/21 12:170.660<0.660mg/Kg1,2,4-Trichlorobenzene
07/08/21 12:170.660<0.660mg/Kg2,4,5-Trichlorophenol
07/08/21 12:170.660<0.660mg/Kg2,4,6-Trichlorophenol
07/08/21 12:172-Fluorobiphenyl (S)110 44-115
07/08/21 12:172-Fluorophenol (S)94.8 35-115
07/08/21 12:17Nitrobenzene-d5 (S)98.2 37-122
07/08/21 12:174-Terphenyl-d14 (S)104 54-127
07/08/21 12:172,4,6-Tribromophenol (S)122 39-132
07/08/21 12:17Phenol-d5 (S)93.6 34-121
LCS-V6173Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1081.801.67mg/KgAcenaphthene 40-123
1091.821.67mg/KgAcenaphthylene 32-132
Page 22 of 33Date:07/13/2021 12:09 PM
Page 90 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
LCS-V6173Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.21.541.67mg/KgAniline 12-197
1101.831.67mg/KgAnthracene 47-123
1071.791.67mg/KgBenzo(a)anthracene 49-126
135*2.251.67mg/KgBenzo(a)pyrene 45-129
1222.031.67mg/KgBenzo(b)fluoranthene 45-132
1171.951.67mg/KgBenzo(g,h,i)perylene 43-134
1171.961.67mg/KgBenzo(k)fluoranthene 47-132
0.0*0.5801.67mg/KgBenzoic Acid 10-83
1001.671.67mg/KgBenzyl alcohol 29-122
96.41.611.67mg/KgBis(2-Chloroethoxy)methane 36-121
87.41.461.67mg/KgBis(2-Chloroethyl)ether 31-120
92.81.551.67mg/KgBis(2-Chloroisopropyl)ether 33-131
1101.831.67mg/KgBis(2-ethylhexyl)phthalate 51-133
1171.951.67mg/Kg4-Bromophenyl phenyl ether 46-124
1041.741.67mg/KgButyl benzyl phthalate 48-132
1011.691.67mg/Kg4-Chloro-3-methylphenol 45-122
81.41.361.67mg/Kg4-Chloroaniline 17-106
1051.761.67mg/Kg2-Chloronaphthalene 41-114
1011.691.67mg/Kg2-Chlorophenol 34-121
1202.011.67mg/Kg4-Chlorophenyl phenyl ether 45-121
1111.851.67mg/KgChrysene 50-124
95.81.601.67mg/KgDibenz(a,h)anthracene 45-134
1101.841.67mg/KgDibenzofuran 44-120
93.41.561.67mg/Kg1,2-Dichlorobenzene 33-117
92.21.541.67mg/Kg1,3-Dichlorobenzene 30-115
89.81.501.67mg/Kg1,4-Dichlorobenzene 31-115
1071.781.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 23 of 33* QC Fail Date:07/13/2021 12:09 PM
Page 91 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
LCS-V6173Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1011.681.67mg/Kg2,4-Dichlorophenol 40-122
1131.881.67mg/KgDiethyl phthalate 50-124
1111.861.67mg/KgDimethyl phthalate 48-124
1001.671.67mg/Kg2,4-Dimethylphenol 30-127
1171.951.67mg/KgDi-n-butyl phthalate 51-128
1131.891.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
1272.121.67mg/Kg2,4-Dinitrophenol 27-129
1222.041.67mg/Kg2,4-Dinitrotoluene 48-126
1171.961.67mg/Kg2,6-Dinitrotoluene 46-124
1071.791.67mg/KgDi-n-Octyl Phthalate 45-140
1151.921.67mg/KgFluoranthene 50-127
1111.851.67mg/KgFluorene 43-125
1212.021.67mg/KgHexachlorobenzene 45-122
1021.701.67mg/KgHexachlorobutadiene 32-123
88.61.481.67mg/KgHexachlorocyclopentadiene 32-117
89.21.491.67mg/KgHexachloroethane 28-117
1151.921.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
85.61.431.67mg/KgIsophorone 30-122
88.61.481.67mg/Kg1-Methylnaphthalene 40-119
88.61.481.67mg/Kg2-Methylnaphthalene 38-122
1021.711.67mg/Kg2-Methylphenol 32-122
88.01.471.67mg/Kg3&4 Methylphenol 34-119
85.01.421.67mg/KgNaphthalene 35-123
1041.731.67mg/Kg2-Nitroaniline 44-127
99.41.661.67mg/Kg3-Nitroaniline 33-119
1212.021.67mg/Kg4-Nitroaniline 63-147
83.21.391.67mg/KgNitrobenzene 34-122
Page 24 of 33Date:07/13/2021 12:09 PM
Page 92 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
LCS-V6173Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
87.41.461.67mg/Kg2-Nitrophenol 36-123
1252.081.67mg/Kg4-Nitrophenol 30-132
61.61.031.67mg/KgN-Nitrosodimethylamine 10-146
1252.091.67mg/KgN-Nitrosodiphenylamine 38-127
95.21.591.67mg/KgN-Nitroso-di-n-propylamine 36-120
143*2.391.67mg/KgPentachlorophenol 25-133
1111.861.67mg/KgPhenanthrene 50-121
96.41.611.67mg/KgPhenol 34-121
1141.901.67mg/KgPyrene 47-127
44.00.7361.67mg/KgPyridine 10-80
89.81.501.67mg/Kg1,2,4-Trichlorobenzene 34-118
1131.891.67mg/Kg2,4,5-Trichlorophenol 41-124
1171.951.67mg/Kg2,4,6-Trichlorophenol 39-126
1062-Fluorobiphenyl (S)44-115
95.42-Fluorophenol (S)35-115
80.8Nitrobenzene-d5 (S)37-122
1094-Terphenyl-d14 (S)54-127
1292,4,6-Tribromophenol (S)39-132
92.1Phenol-d5 (S)34-121
V 90830-MS-V6173 V 90830-MSD-V6173Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.94 1151.601.671.68<0.665mg/KgAcenaphthene 95.8 40-123 19.2 20
1.97 1171.651.671.68<0.665mg/KgAcenaphthylene 98.8 32-132 17.6 20
0.900 53.50.8021.671.68<0.665mg/KgAniline 48.0 12-197 11.5 20
Page 25 of 33* QC Fail Date:07/13/2021 12:09 PM
Page 93 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
V 90830-MS-V6173 V 90830-MSD-V6173Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.94 1151.571.671.68<0.665mg/KgAnthracene 94.0 47-123 21.0*20
1.91 1141.571.671.68<0.665mg/KgBenzo(a)anthracene 94.0 49-126 19.5 20
2.29 136*1.861.671.68<0.665mg/KgBenzo(a)pyrene 111 45-129 20.7*20
2.00 1191.661.671.68<0.665mg/KgBenzo(b)fluoranthene 99.4 45-132 18.5 20
1.99 1181.601.671.68<0.665mg/KgBenzo(g,h,i)perylene 95.8 43-134 21.7*20
1.94 1151.631.671.68<0.665mg/KgBenzo(k)fluoranthene 97.6 47-132 17.3 20
2.37 141*1.521.671.68<2.01mg/KgBenzoic Acid 0.0*10-83 16.9 20
1.74 1041.391.671.68<0.665mg/KgBenzyl alcohol 83.2 29-122 22.3*20
1.72 1021.451.671.68<0.665mg/KgBis(2-Chloroethoxy)methane 86.8 36-121 17.0 20
1.75 1041.451.671.68<0.665mg/KgBis(2-Chloroethyl)ether 86.8 31-120 18.7 20
1.66 98.81.331.671.68<0.332mg/KgBis(2-Chloroisopropyl)ether 79.6 33-131 22.0*20
1.90 1131.561.671.68<0.665mg/KgBis(2-ethylhexyl)phthalate 93.4 51-133 19.6 20
2.09 124*1.661.671.68<0.665mg/Kg4-Bromophenyl phenyl ether 99.4 46-124 22.9*20
1.78 1061.471.671.68<0.332mg/KgButyl benzyl phthalate 88.0 48-132 19.0 20
1.81 1081.511.671.68<0.665mg/Kg4-Chloro-3-methylphenol 90.4 45-122 18.0 20
1.36 80.91.181.671.68<0.332mg/Kg4-Chloroaniline 70.6 17-106 14.1 20
1.91 1141.591.671.68<0.665mg/Kg2-Chloronaphthalene 95.2 41-114 18.2 20
1.83 1091.491.671.68<0.665mg/Kg2-Chlorophenol 89.2 34-121 20.4*20
2.10 125*1.781.671.68<1.01mg/Kg4-Chlorophenyl phenyl ether 107 45-121 16.4 20
1.92 1141.581.671.68<0.665mg/KgChrysene 94.6 50-124 19.4 20
1.78 1061.371.671.68<0.665mg/KgDibenz(a,h)anthracene 82.0 45-134 26.0*20
1.98 1181.631.671.68<0.665mg/KgDibenzofuran 97.6 44-120 19.3 20
1.71 1021.381.671.68<0.665mg/Kg1,2-Dichlorobenzene 82.6 33-117 21.3*20
1.68 1001.371.671.68<0.665mg/Kg1,3-Dichlorobenzene 82.0 30-115 20.3*20
1.69 1011.361.671.68<0.332mg/Kg1,4-Dichlorobenzene 81.4 31-115 21.6*20
1.47 87.51.331.671.68<0.665mg/Kg3,3'-Dichlorobenzidine 79.6 22-121 10.0 20
Page 26 of 33* QC Fail Date:07/13/2021 12:09 PM
Page 94 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
V 90830-MS-V6173 V 90830-MSD-V6173Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.83 1091.491.671.68<0.665mg/Kg2,4-Dichlorophenol 89.2 40-122 20.4*20
1.98 1181.621.671.68<0.665mg/KgDiethyl phthalate 97.0 50-124 20.0 20
1.97 1171.621.671.68<0.665mg/KgDimethyl phthalate 97.0 48-124 19.4 30
1.86 1111.541.671.68<0.332mg/Kg2,4-Dimethylphenol 92.2 30-127 18.8 20
2.03 1211.651.671.68<0.665mg/KgDi-n-butyl phthalate 98.8 51-128 20.6*20
0.342 0.0*0.3021.671.68<1.51mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
2.29 136*1.871.671.68<1.51mg/Kg2,4-Dinitrophenol 112 27-129 20.1*20
2.08 1241.701.671.68<0.665mg/Kg2,4-Dinitrotoluene 102 48-126 20.1*20
2.04 1211.691.671.68<0.665mg/Kg2,6-Dinitrotoluene 101 46-124 18.7 20
1.82 1081.501.671.68<0.332mg/KgDi-n-Octyl Phthalate 89.8 45-140 19.2 20
2.03 1211.631.671.68<0.665mg/KgFluoranthene 97.6 50-127 21.8*20
2.01 1201.661.671.68<0.665mg/KgFluorene 99.4 43-125 19.0 20
2.16 129*1.731.671.68<0.665mg/KgHexachlorobenzene 104 45-122 22.1*20
1.93 1151.551.671.68<0.665mg/KgHexachlorobutadiene 92.8 32-123 21.8*20
1.74 1041.441.671.68<0.665mg/KgHexachlorocyclopentadiene 86.2 32-117 18.8 20
1.69 1011.341.671.68<0.665mg/KgHexachloroethane 80.2 28-117 23.1*20
1.91 1141.571.671.68<0.665mg/KgIndeno(1,2,3-cd)pyrene 94.0 45-133 19.5 20
1.53 91.01.271.671.68<0.665mg/KgIsophorone 76.0 30-122 18.5 20
1.62 96.41.341.671.68<0.665mg/Kg1-Methylnaphthalene 80.2 40-119 18.9 20
1.62 96.41.371.671.68<0.665mg/Kg2-Methylnaphthalene 82.0 38-122 16.7 20
1.91 1141.561.671.68<0.665mg/Kg2-Methylphenol 93.4 32-122 20.1*20
1.60 95.21.311.671.68<0.665mg/Kg3&4 Methylphenol 78.4 34-119 19.9 20
1.54 91.61.261.671.68<0.665mg/KgNaphthalene 75.4 35-123 20.0 20
1.88 1121.521.671.68<0.665mg/Kg2-Nitroaniline 91.0 44-127 21.1*20
1.77 1051.491.671.68<0.665mg/Kg3-Nitroaniline 89.2 33-119 17.1 20
2.06 1231.661.671.68<0.332mg/Kg4-Nitroaniline 99.4 63-147 21.5*20
Page 27 of 33* QC Fail Date:07/13/2021 12:09 PM
Page 95 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V6348QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V6173
V 90830-MS-V6173 V 90830-MSD-V6173Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.54 91.61.241.671.68<0.332mg/KgNitrobenzene 74.2 34-122 21.5*20
1.64 97.61.361.671.68<0.665mg/Kg2-Nitrophenol 81.4 32-123 18.6 20
2.18 1301.741.671.68<0.665mg/Kg4-Nitrophenol 104 30-132 22.4*20
1.01 60.11.071.671.68<0.665mg/KgN-Nitrosodimethylamine 64.0 10-146 5.7 30
2.20 131*1.791.671.68<0.665mg/KgN-Nitrosodiphenylamine 107 38-127 20.5*20
1.74 1041.391.671.68<0.665mg/KgN-Nitroso-di-n-propylamine 83.2 36-120 22.3*20
2.55 152*2.021.671.68<1.01mg/KgPentachlorophenol 121 25-133 23.1*20
1.95 1161.551.671.68<0.665mg/KgPhenanthrene 92.8 50-121 22.8*20
1.76 1051.411.671.68<0.665mg/KgPhenol 84.4 34-121 22.0*20
1.95 1161.591.671.68<0.665mg/KgPyrene 95.2 47-127 20.3*20
0.087 0.0*0.0791.671.68<0.332mg/KgPyridine 0.0*10-80 0.0 20
1.68 1001.381.671.68<0.665mg/Kg1,2,4-Trichlorobenzene 82.6 34-118 19.6 20
2.00 1191.631.671.68<0.665mg/Kg2,4,5-Trichlorophenol 97.6 41-124 20.3*20
2.17 129*1.771.671.68<0.665mg/Kg2,4,6-Trichlorophenol 106 39-126 20.3*20
1142-Fluorobiphenyl (S)94.6 44-115
1022-Fluorophenol (S)84.0 35-115
88.0Nitrobenzene-d5 (S)74.2 37-122
1214-Terphenyl-d14 (S)101 54-127
138*2,4,6-Tribromophenol (S)117 39-132
97.0Phenol-d5 (S)80.7 34-121
Page 28 of 33* QC Fail Date:07/13/2021 12:09 PM
Page 96 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V6364QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V6175
Associated Lab Samples: 90925, 90926, 90927, 90928, 90929
LRB-V6175 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/09/21 10:3650.0<50.0mg/KgAliphatic C19-C36
07/09/21 10:3650.0<50.0mg/KgAliphatic C9-C18
07/09/21 10:3650.0<50.0mg/KgAromatic C11-C22
07/09/21 10:362-Fluorobiphenyl (S)79.7 40-140
07/09/21 10:362-Bromonaphthalene (S)76.2 40-140
07/09/21 10:36Chlorooctadecane (S)75.0 40-140
07/09/21 10:36OTP Surrogate (S)65.0 40-140
LCS-V6175Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
81.365.180.0mg/KgAliphatic C19-C36 40-140
0.0*9.2060.0mg/KgAliphatic C9-C18 40-140
92.9158170mg/KgAromatic C11-C22 40-140
97.02-Fluorobiphenyl (S)40-140
1022-Bromonaphthalene (S)40-140
75.5Chlorooctadecane (S)40-140
87.0OTP Surrogate (S)40-140
V 90926-MS-V6175 V 90926-MSD-V6175Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
65.9 81.065.979.981.3<50.8mg/KgAliphatic C19-C36 82.4 40-140 0.0 50
9.35 0.0*9.2059.961.0<50.8mg/KgAliphatic C9-C18 0.0*40-140 0.0 50
152 87.8143170173<50.8mg/KgAromatic C11-C22 84.1 40-140 6.1 50
1002-Fluorobiphenyl (S)93.7 40-140
Page 29 of 33* QC Fail Date:07/13/2021 12:09 PM
Page 97 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V6364QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V6175
V 90926-MS-V6175 V 90926-MSD-V6175Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1052-Bromonaphthalene (S)98.5 40-140
71.4Chlorooctadecane (S)68.0 40-140
79.3OTP Surrogate (S)78.0 40-140
Page 30 of 33Date:07/13/2021 12:09 PM
Page 98 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V6157QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V6156
Associated Lab Samples: 90925, 90926, 90927, 90928, 90929
LRB-V6156 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/06/21 13:008.00<8.00mg/KgAliphatic C5-C8
07/06/21 13:008.00<8.00mg/KgAliphatic C9-C12
07/06/21 13:008.00<8.00mg/KgAromatic C9-C10
07/06/21 13:002,5-Dibromotoluene (FID) (S)93.4 70-130
07/06/21 13:002,5-Dibromotoluene (PID) (S)88.4 70-130
LCS-V6156 LCSD-V6156Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
32.8 10397.831.332.0mg/KgAliphatic C5-C8 70-130 4.6 50
34.4 10810333.132.0mg/KgAliphatic C9-C12 70-130 3.8 50
12.9 12190.19.6510.7mg/KgAromatic C9-C10 70-130 28.8 50
93.290.62,5-Dibromotoluene (FID) (S)70-130
88.586.12,5-Dibromotoluene (PID) (S)70-130
Page 31 of 33Date:07/13/2021 12:09 PM
Page 99 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
Dry Weight Determination
SW-DRYWT
V6242QC Analytical Batch:
Analysis Method:
Analysis Description:
V 90916-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/07/21 16:454.814.014.7%Moisture
V 90985-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/07/21 16:455.610.310.9%Moisture
Page 32 of 33Date:07/13/2021 12:09 PM
Page 100 of 104
Quality Control Data
21-183-0032Report No:
Project Description:
Client ID:Withers & Ravenel
Former CC Newell Store
Dry Weight Determination
SW-DRYWT
V6304QC Analytical Batch:
Analysis Method:
Analysis Description:
V 90892-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/08/21 14:253.735.634.3%Moisture
V 90994-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/08/21 14:254.324.926.0%Moisture
Page 33 of 33Date:07/13/2021 12:09 PM
Page 101 of 104
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-183-0032
Withers & Ravenel
01221
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.4C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Talon J Yelton Date & Time:07/02/2021 15:03:29
Special precautions or instructions included?
Comments:
Page 102 of 104
Page 103 of 104
Page 104 of 104
7/19/2021
Mr. Matt James
Withers Ravenel Inc.
115 Mackenan Drive
Cary NC 27511
Project Name: CC Newell Store
Project #: 02172214.97
Dear Mr. Matt James
The following report includes the data for the above referenced project for sample(s)
received on 7/6/2021 at Eurofins Air Toxics LLC.
The data and associated QC analyzed by TO-15 are compliant with the project
requirements or laboratory criteria with the exception of the deviations noted in the
attached case narrative.
Thank you for choosing Eurofins Air Toxics LLC. for your air analysis needs. Eurofins Air
Toxics Inc. is committed to providing accurate data of the highest quality. Please feel free
to contact the Project Manager: Brian Whittaker at 916-985-1000 if you have any
questions regarding the data in this report.
Regards,
Brian Whittaker
Project Manager
Workorder #: 2107120
Page 1 of 16
Mr. Matt James
Withers Ravenel Inc.
115 Mackenan Drive
Cary, NC 27511
WORK ORDER #: 2107120
CLIENT:BILL TO:
PHONE:
Mr. Matt James
Withers Ravenel Inc.
115 Mackenan Drive
Cary, NC 27511
919.469.3340
919.467.6008
07/06/2021
DATE COMPLETED:07/19/2021
P.O. #
PROJECT #02172214.97 CC Newell Store
Work Order Summary
FAX:
DATE RECEIVED:CONTACT:Brian Whittaker
NAMEFRACTION #TEST VAC./PRES.
RECEIPT
PRESSURE
FINAL
01A SSV-1 TO-15 4.5 "Hg 10 psi
02A SSV-2 TO-15 4.5 "Hg 10 psi
03A Lab Blank TO-15 NA NA
04A CCV TO-15 NA NA
05A LCS TO-15 NA NA
05AA LCSD TO-15 NA NA
CERTIFIED BY:
Technical Director
DATE: 07/19/21
Page 2 of 16
Certification numbers: AZ Licensure AZ0775, FL NELAP – E87680, LA NELAP – 02089, NH NELAP - 209220, NJ NELAP - CA016,
NY NELAP - 11291, TX NELAP - T104704434-20-16, UT NELAP – CA009332020-12, VA NELAP - 10615, WA NELAP - C935
Name of Accreditation Body: NELAP/ORELAP (Oregon Environmental Laboratory Accreditation Program)
Accreditation number: CA300005-014, Effective date: 10/18/2020, Expiration date: 10/17/2021.
Eurofins Air Toxics, LLC certifies that the test results contained in this report meet all requirements of the NELAC standards
This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, LLC.
180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630
[phone] . [phone] . FAX [phone]
LABORATORY NARRATIVE
EPA Method TO-15
Withers Ravenel Inc.
Workorder# 2107120
Two 1 Liter Summa Canister samples were received on July 06, 2021. The laboratory performed analysis
via EPA Method TO-15 using GC/MS in the full scan mode.
There were no receiving discrepancies.
Receiving Notes
All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag is defined
at the bottom of this Case Narrative and on each Sample Result Summary page.
Analytical Notes
Ten qualifiers may have been used on the data analysis sheets and indicates as follows:
B - Compound present in laboratory blank greater than reporting limit (background subtraction not
performed).
J - Estimated value.
E - Exceeds instrument calibration range.
S - Saturated peak.
Q - Exceeds quality control limits.
U - Compound analyzed for but not detected above the reporting limit, LOD, or MDL value. See
data page for project specific U-flag definition.
UJ- Non-detected compound associated with low bias in the CCV
N - The identification is based on presumptive evidence.
M - Reported value may be biased due to apparent matrix interferences.
CN - See Case Narrative.
File extensions may have been used on the data analysis sheets and indicates
as follows:
a-File was requantified
b-File was quantified by a second column and detector
r1-File was requantified for the purpose of reissue
Definition of Data Qualifying Flags
Page 3 of 16
EPA METHOD TO-15 GC/MS FULL SCAN
Summary of Detected Compounds
Client Sample ID: SSV-1
Lab ID#: 2107120-01A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
9.9 170 19 310Ethanol
9.9 100 24 250Acetone
4.0 96 9.7 2402-Propanol
4.0 16 12 462-Butanone (Methyl Ethyl Ketone)
0.99 1.3 4.0 5.34-Methyl-2-pentanone
Client Sample ID: SSV-2
Lab ID#: 2107120-02A
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
9.9 76 19 140Ethanol
9.9 72 24 170Acetone
4.0 45 9.7 1102-Propanol
4.0 6.6 12 21Carbon Disulfide
4.0 4.6 12 142-Butanone (Methyl Ethyl Ketone)
Page 4 of 16
Client Sample ID: SSV-1
Lab ID#: 2107120-01A
EPA METHOD TO-15 GC/MS FULL SCAN
a071417File Name:
Dil. Factor:1.98
Date of Collection: 7/1/21 12:51:00 PM
Date of Analysis: 7/14/21 07:46 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.99 Not Detected 4.9 Not DetectedFreon 12
0.99 Not Detected 6.9 Not DetectedFreon 114
9.9 Not Detected 20 Not DetectedChloromethane
0.99 Not Detected 2.5 Not DetectedVinyl Chloride
0.99 Not Detected 2.2 Not Detected1,3-Butadiene
9.9 Not Detected 38 Not DetectedBromomethane
4.0 Not Detected 10 Not DetectedChloroethane
0.99 Not Detected 5.6 Not DetectedFreon 11
9.9 170 19 310Ethanol
0.99 Not Detected 7.6 Not DetectedFreon 113
0.99 Not Detected 3.9 Not Detected1,1-Dichloroethene
9.9 100 24 250Acetone
4.0 96 9.7 2402-Propanol
4.0 Not Detected 12 Not DetectedCarbon Disulfide
4.0 Not Detected 12 Not Detected3-Chloropropene
9.9 Not Detected 34 Not DetectedMethylene Chloride
4.0 Not Detected 14 Not DetectedMethyl tert-butyl ether
0.99 Not Detected 3.9 Not Detectedtrans-1,2-Dichloroethene
0.99 Not Detected 3.5 Not DetectedHexane
0.99 Not Detected 4.0 Not Detected1,1-Dichloroethane
4.0 16 12 462-Butanone (Methyl Ethyl Ketone)
0.99 Not Detected 3.9 Not Detectedcis-1,2-Dichloroethene
0.99 Not Detected 2.9 Not DetectedTetrahydrofuran
0.99 Not Detected 4.8 Not DetectedChloroform
0.99 Not Detected 5.4 Not Detected1,1,1-Trichloroethane
0.99 Not Detected 3.4 Not DetectedCyclohexane
0.99 Not Detected 6.2 Not DetectedCarbon Tetrachloride
0.99 Not Detected 4.6 Not Detected2,2,4-Trimethylpentane
0.99 Not Detected 3.2 Not DetectedBenzene
0.99 Not Detected 4.0 Not Detected1,2-Dichloroethane
0.99 Not Detected 4.0 Not DetectedHeptane
0.99 Not Detected 5.3 Not DetectedTrichloroethene
0.99 Not Detected 4.6 Not Detected1,2-Dichloropropane
4.0 Not Detected 14 Not Detected1,4-Dioxane
0.99 Not Detected 6.6 Not DetectedBromodichloromethane
0.99 Not Detected 4.5 Not Detectedcis-1,3-Dichloropropene
0.99 1.3 4.0 5.34-Methyl-2-pentanone
0.99 Not Detected 3.7 Not DetectedToluene
0.99 Not Detected 4.5 Not Detectedtrans-1,3-Dichloropropene
0.99 Not Detected 5.4 Not Detected1,1,2-Trichloroethane
0.99 Not Detected 6.7 Not DetectedTetrachloroethene
4.0 Not Detected 16 Not Detected2-Hexanone
Page 5 of 16
Client Sample ID: SSV-1
Lab ID#: 2107120-01A
EPA METHOD TO-15 GC/MS FULL SCAN
a071417File Name:
Dil. Factor:1.98
Date of Collection: 7/1/21 12:51:00 PM
Date of Analysis: 7/14/21 07:46 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.99 Not Detected 8.4 Not DetectedDibromochloromethane
0.99 Not Detected 7.6 Not Detected1,2-Dibromoethane (EDB)
0.99 Not Detected 4.6 Not DetectedChlorobenzene
0.99 Not Detected 4.3 Not DetectedEthyl Benzene
0.99 Not Detected 4.3 Not Detectedm,p-Xylene
0.99 Not Detected 4.3 Not Detectedo-Xylene
0.99 Not Detected 4.2 Not DetectedStyrene
0.99 Not Detected 10 Not DetectedBromoform
0.99 Not Detected 4.9 Not DetectedCumene
0.99 Not Detected 6.8 Not Detected1,1,2,2-Tetrachloroethane
0.99 Not Detected 4.9 Not DetectedPropylbenzene
0.99 Not Detected 4.9 Not Detected4-Ethyltoluene
0.99 Not Detected 4.9 Not Detected1,3,5-Trimethylbenzene
0.99 Not Detected 4.9 Not Detected1,2,4-Trimethylbenzene
0.99 Not Detected 6.0 Not Detected1,3-Dichlorobenzene
0.99 Not Detected 6.0 Not Detected1,4-Dichlorobenzene
0.99 Not Detected 5.1 Not Detectedalpha-Chlorotoluene
0.99 Not Detected 6.0 Not Detected1,2-Dichlorobenzene
4.0 Not Detected 29 Not Detected1,2,4-Trichlorobenzene
4.0 Not Detected 42 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
99 70-130Toluene-d8
92 70-1301,2-Dichloroethane-d4
101 70-1304-Bromofluorobenzene
Page 6 of 16
Client Sample ID: SSV-2
Lab ID#: 2107120-02A
EPA METHOD TO-15 GC/MS FULL SCAN
a071415File Name:
Dil. Factor:1.98
Date of Collection: 7/1/21 12:54:00 PM
Date of Analysis: 7/14/21 06:23 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.99 Not Detected 4.9 Not DetectedFreon 12
0.99 Not Detected 6.9 Not DetectedFreon 114
9.9 Not Detected 20 Not DetectedChloromethane
0.99 Not Detected 2.5 Not DetectedVinyl Chloride
0.99 Not Detected 2.2 Not Detected1,3-Butadiene
9.9 Not Detected 38 Not DetectedBromomethane
4.0 Not Detected 10 Not DetectedChloroethane
0.99 Not Detected 5.6 Not DetectedFreon 11
9.9 76 19 140Ethanol
0.99 Not Detected 7.6 Not DetectedFreon 113
0.99 Not Detected 3.9 Not Detected1,1-Dichloroethene
9.9 72 24 170Acetone
4.0 45 9.7 1102-Propanol
4.0 6.6 12 21Carbon Disulfide
4.0 Not Detected 12 Not Detected3-Chloropropene
9.9 Not Detected 34 Not DetectedMethylene Chloride
4.0 Not Detected 14 Not DetectedMethyl tert-butyl ether
0.99 Not Detected 3.9 Not Detectedtrans-1,2-Dichloroethene
0.99 Not Detected 3.5 Not DetectedHexane
0.99 Not Detected 4.0 Not Detected1,1-Dichloroethane
4.0 4.6 12 142-Butanone (Methyl Ethyl Ketone)
0.99 Not Detected 3.9 Not Detectedcis-1,2-Dichloroethene
0.99 Not Detected 2.9 Not DetectedTetrahydrofuran
0.99 Not Detected 4.8 Not DetectedChloroform
0.99 Not Detected 5.4 Not Detected1,1,1-Trichloroethane
0.99 Not Detected 3.4 Not DetectedCyclohexane
0.99 Not Detected 6.2 Not DetectedCarbon Tetrachloride
0.99 Not Detected 4.6 Not Detected2,2,4-Trimethylpentane
0.99 Not Detected 3.2 Not DetectedBenzene
0.99 Not Detected 4.0 Not Detected1,2-Dichloroethane
0.99 Not Detected 4.0 Not DetectedHeptane
0.99 Not Detected 5.3 Not DetectedTrichloroethene
0.99 Not Detected 4.6 Not Detected1,2-Dichloropropane
4.0 Not Detected 14 Not Detected1,4-Dioxane
0.99 Not Detected 6.6 Not DetectedBromodichloromethane
0.99 Not Detected 4.5 Not Detectedcis-1,3-Dichloropropene
0.99 Not Detected 4.0 Not Detected4-Methyl-2-pentanone
0.99 Not Detected 3.7 Not DetectedToluene
0.99 Not Detected 4.5 Not Detectedtrans-1,3-Dichloropropene
0.99 Not Detected 5.4 Not Detected1,1,2-Trichloroethane
0.99 Not Detected 6.7 Not DetectedTetrachloroethene
4.0 Not Detected 16 Not Detected2-Hexanone
Page 7 of 16
Client Sample ID: SSV-2
Lab ID#: 2107120-02A
EPA METHOD TO-15 GC/MS FULL SCAN
a071415File Name:
Dil. Factor:1.98
Date of Collection: 7/1/21 12:54:00 PM
Date of Analysis: 7/14/21 06:23 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.99 Not Detected 8.4 Not DetectedDibromochloromethane
0.99 Not Detected 7.6 Not Detected1,2-Dibromoethane (EDB)
0.99 Not Detected 4.6 Not DetectedChlorobenzene
0.99 Not Detected 4.3 Not DetectedEthyl Benzene
0.99 Not Detected 4.3 Not Detectedm,p-Xylene
0.99 Not Detected 4.3 Not Detectedo-Xylene
0.99 Not Detected 4.2 Not DetectedStyrene
0.99 Not Detected 10 Not DetectedBromoform
0.99 Not Detected 4.9 Not DetectedCumene
0.99 Not Detected 6.8 Not Detected1,1,2,2-Tetrachloroethane
0.99 Not Detected 4.9 Not DetectedPropylbenzene
0.99 Not Detected 4.9 Not Detected4-Ethyltoluene
0.99 Not Detected 4.9 Not Detected1,3,5-Trimethylbenzene
0.99 Not Detected 4.9 Not Detected1,2,4-Trimethylbenzene
0.99 Not Detected 6.0 Not Detected1,3-Dichlorobenzene
0.99 Not Detected 6.0 Not Detected1,4-Dichlorobenzene
0.99 Not Detected 5.1 Not Detectedalpha-Chlorotoluene
0.99 Not Detected 6.0 Not Detected1,2-Dichlorobenzene
4.0 Not Detected 29 Not Detected1,2,4-Trichlorobenzene
4.0 Not Detected 42 Not DetectedHexachlorobutadiene
Container Type: 1 Liter Summa Canister
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
90 70-1301,2-Dichloroethane-d4
102 70-1304-Bromofluorobenzene
Page 8 of 16
Client Sample ID: Lab Blank
Lab ID#: 2107120-03A
EPA METHOD TO-15 GC/MS FULL SCAN
a071405File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 01:06 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 2.5 Not DetectedFreon 12
0.50 Not Detected 3.5 Not DetectedFreon 114
5.0 Not Detected 10 Not DetectedChloromethane
0.50 Not Detected 1.3 Not DetectedVinyl Chloride
0.50 Not Detected 1.1 Not Detected1,3-Butadiene
5.0 Not Detected 19 Not DetectedBromomethane
2.0 Not Detected 5.3 Not DetectedChloroethane
0.50 Not Detected 2.8 Not DetectedFreon 11
5.0 Not Detected 9.4 Not DetectedEthanol
0.50 Not Detected 3.8 Not DetectedFreon 113
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethene
5.0 Not Detected 12 Not DetectedAcetone
2.0 Not Detected 4.9 Not Detected2-Propanol
2.0 Not Detected 6.2 Not DetectedCarbon Disulfide
2.0 Not Detected 6.3 Not Detected3-Chloropropene
5.0 Not Detected 17 Not DetectedMethylene Chloride
2.0 Not Detected 7.2 Not DetectedMethyl tert-butyl ether
0.50 Not Detected 2.0 Not Detectedtrans-1,2-Dichloroethene
0.50 Not Detected 1.8 Not DetectedHexane
0.50 Not Detected 2.0 Not Detected1,1-Dichloroethane
2.0 Not Detected 5.9 Not Detected2-Butanone (Methyl Ethyl Ketone)
0.50 Not Detected 2.0 Not Detectedcis-1,2-Dichloroethene
0.50 Not Detected 1.5 Not DetectedTetrahydrofuran
0.50 Not Detected 2.4 Not DetectedChloroform
0.50 Not Detected 2.7 Not Detected1,1,1-Trichloroethane
0.50 Not Detected 1.7 Not DetectedCyclohexane
0.50 Not Detected 3.1 Not DetectedCarbon Tetrachloride
0.50 Not Detected 2.3 Not Detected2,2,4-Trimethylpentane
0.50 Not Detected 1.6 Not DetectedBenzene
0.50 Not Detected 2.0 Not Detected1,2-Dichloroethane
0.50 Not Detected 2.0 Not DetectedHeptane
0.50 Not Detected 2.7 Not DetectedTrichloroethene
0.50 Not Detected 2.3 Not Detected1,2-Dichloropropane
2.0 Not Detected 7.2 Not Detected1,4-Dioxane
0.50 Not Detected 3.4 Not DetectedBromodichloromethane
0.50 Not Detected 2.3 Not Detectedcis-1,3-Dichloropropene
0.50 Not Detected 2.0 Not Detected4-Methyl-2-pentanone
0.50 Not Detected 1.9 Not DetectedToluene
0.50 Not Detected 2.3 Not Detectedtrans-1,3-Dichloropropene
0.50 Not Detected 2.7 Not Detected1,1,2-Trichloroethane
0.50 Not Detected 3.4 Not DetectedTetrachloroethene
2.0 Not Detected 8.2 Not Detected2-Hexanone
Page 9 of 16
Client Sample ID: Lab Blank
Lab ID#: 2107120-03A
EPA METHOD TO-15 GC/MS FULL SCAN
a071405File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 01:06 PM
(ug/m3)(ug/m3)(ppbv)(ppbv)Compound
AmountRpt. LimitAmountRpt. Limit
0.50 Not Detected 4.2 Not DetectedDibromochloromethane
0.50 Not Detected 3.8 Not Detected1,2-Dibromoethane (EDB)
0.50 Not Detected 2.3 Not DetectedChlorobenzene
0.50 Not Detected 2.2 Not DetectedEthyl Benzene
0.50 Not Detected 2.2 Not Detectedm,p-Xylene
0.50 Not Detected 2.2 Not Detectedo-Xylene
0.50 Not Detected 2.1 Not DetectedStyrene
0.50 Not Detected 5.2 Not DetectedBromoform
0.50 Not Detected 2.4 Not DetectedCumene
0.50 Not Detected 3.4 Not Detected1,1,2,2-Tetrachloroethane
0.50 Not Detected 2.4 Not DetectedPropylbenzene
0.50 Not Detected 2.4 Not Detected4-Ethyltoluene
0.50 Not Detected 2.4 Not Detected1,3,5-Trimethylbenzene
0.50 Not Detected 2.4 Not Detected1,2,4-Trimethylbenzene
0.50 Not Detected 3.0 Not Detected1,3-Dichlorobenzene
0.50 Not Detected 3.0 Not Detected1,4-Dichlorobenzene
0.50 Not Detected 2.6 Not Detectedalpha-Chlorotoluene
0.50 Not Detected 3.0 Not Detected1,2-Dichlorobenzene
2.0 Not Detected 15 Not Detected1,2,4-Trichlorobenzene
2.0 Not Detected 21 Not DetectedHexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
96 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 10 of 16
Client Sample ID: CCV
Lab ID#: 2107120-04A
EPA METHOD TO-15 GC/MS FULL SCAN
a071402File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 11:16 AM
%RecoveryCompound
97Freon 12
101Freon 114
91Chloromethane
94Vinyl Chloride
791,3-Butadiene
92Bromomethane
93Chloroethane
100Freon 11
90Ethanol
99Freon 113
911,1-Dichloroethene
88Acetone
872-Propanol
92Carbon Disulfide
933-Chloropropene
92Methylene Chloride
93Methyl tert-butyl ether
91trans-1,2-Dichloroethene
91Hexane
941,1-Dichloroethane
942-Butanone (Methyl Ethyl Ketone)
94cis-1,2-Dichloroethene
88Tetrahydrofuran
89Chloroform
901,1,1-Trichloroethane
90Cyclohexane
97Carbon Tetrachloride
922,2,4-Trimethylpentane
98Benzene
1011,2-Dichloroethane
88Heptane
101Trichloroethene
951,2-Dichloropropane
1011,4-Dioxane
94Bromodichloromethane
98cis-1,3-Dichloropropene
934-Methyl-2-pentanone
98Toluene
101trans-1,3-Dichloropropene
1001,1,2-Trichloroethane
107Tetrachloroethene
952-Hexanone
Page 11 of 16
Client Sample ID: CCV
Lab ID#: 2107120-04A
EPA METHOD TO-15 GC/MS FULL SCAN
a071402File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 11:16 AM
%RecoveryCompound
104Dibromochloromethane
1071,2-Dibromoethane (EDB)
105Chlorobenzene
102Ethyl Benzene
101m,p-Xylene
101o-Xylene
102Styrene
108Bromoform
104Cumene
981,1,2,2-Tetrachloroethane
104Propylbenzene
1044-Ethyltoluene
991,3,5-Trimethylbenzene
1061,2,4-Trimethylbenzene
1041,3-Dichlorobenzene
1031,4-Dichlorobenzene
97alpha-Chlorotoluene
1021,2-Dichlorobenzene
931,2,4-Trichlorobenzene
97Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
97 70-130Toluene-d8
92 70-1301,2-Dichloroethane-d4
99 70-1304-Bromofluorobenzene
Page 12 of 16
Client Sample ID: LCS
Lab ID#: 2107120-05A
EPA METHOD TO-15 GC/MS FULL SCAN
a071403File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 11:41 AM
Limits%RecoveryCompound
Method
100 70-130Freon 12
104 70-130Freon 114
92 70-130Chloromethane
97 70-130Vinyl Chloride
82 70-1301,3-Butadiene
92 70-130Bromomethane
92 70-130Chloroethane
103 70-130Freon 11
79 70-130Ethanol
102 70-130Freon 113
95 70-1301,1-Dichloroethene
91 70-130Acetone
95 70-1302-Propanol
94 70-130Carbon Disulfide
95 70-1303-Chloropropene
95 70-130Methylene Chloride
95 70-130Methyl tert-butyl ether
92 70-130trans-1,2-Dichloroethene
94 70-130Hexane
96 70-1301,1-Dichloroethane
96 70-1302-Butanone (Methyl Ethyl Ketone)
96 70-130cis-1,2-Dichloroethene
94 70-130Tetrahydrofuran
92 70-130Chloroform
93 70-1301,1,1-Trichloroethane
93 70-130Cyclohexane
101 70-130Carbon Tetrachloride
93 70-1302,2,4-Trimethylpentane
100 70-130Benzene
105 70-1301,2-Dichloroethane
90 70-130Heptane
105 70-130Trichloroethene
97 70-1301,2-Dichloropropane
106 70-1301,4-Dioxane
97 70-130Bromodichloromethane
101 70-130cis-1,3-Dichloropropene
98 70-1304-Methyl-2-pentanone
99 70-130Toluene
104 70-130trans-1,3-Dichloropropene
100 70-1301,1,2-Trichloroethane
104 70-130Tetrachloroethene
102 70-1302-Hexanone
Page 13 of 16
Client Sample ID: LCS
Lab ID#: 2107120-05A
EPA METHOD TO-15 GC/MS FULL SCAN
a071403File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 11:41 AM
Limits%RecoveryCompound
Method
104 70-130Dibromochloromethane
107 70-1301,2-Dibromoethane (EDB)
104 70-130Chlorobenzene
100 70-130Ethyl Benzene
100 70-130m,p-Xylene
100 70-130o-Xylene
103 70-130Styrene
107 70-130Bromoform
101 70-130Cumene
100 70-1301,1,2,2-Tetrachloroethane
102 70-130Propylbenzene
102 70-1304-Ethyltoluene
98 70-1301,3,5-Trimethylbenzene
107 70-1301,2,4-Trimethylbenzene
104 70-1301,3-Dichlorobenzene
102 70-1301,4-Dichlorobenzene
105 70-130alpha-Chlorotoluene
102 70-1301,2-Dichlorobenzene
125 70-1301,2,4-Trichlorobenzene
128 70-130Hexachlorobutadiene
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
99 70-1301,2-Dichloroethane-d4
97 70-1304-Bromofluorobenzene
Page 14 of 16
Client Sample ID: LCSD
Lab ID#: 2107120-05AA
EPA METHOD TO-15 GC/MS FULL SCAN
a071404File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 12:05 PM
Limits%RecoveryCompound
Method
100 70-130Freon 12
104 70-130Freon 114
90 70-130Chloromethane
96 70-130Vinyl Chloride
80 70-1301,3-Butadiene
92 70-130Bromomethane
92 70-130Chloroethane
103 70-130Freon 11
80 70-130Ethanol
102 70-130Freon 113
94 70-1301,1-Dichloroethene
89 70-130Acetone
94 70-1302-Propanol
94 70-130Carbon Disulfide
94 70-1303-Chloropropene
94 70-130Methylene Chloride
95 70-130Methyl tert-butyl ether
92 70-130trans-1,2-Dichloroethene
93 70-130Hexane
95 70-1301,1-Dichloroethane
99 70-1302-Butanone (Methyl Ethyl Ketone)
96 70-130cis-1,2-Dichloroethene
95 70-130Tetrahydrofuran
91 70-130Chloroform
93 70-1301,1,1-Trichloroethane
93 70-130Cyclohexane
100 70-130Carbon Tetrachloride
92 70-1302,2,4-Trimethylpentane
98 70-130Benzene
104 70-1301,2-Dichloroethane
89 70-130Heptane
104 70-130Trichloroethene
95 70-1301,2-Dichloropropane
104 70-1301,4-Dioxane
97 70-130Bromodichloromethane
101 70-130cis-1,3-Dichloropropene
98 70-1304-Methyl-2-pentanone
98 70-130Toluene
106 70-130trans-1,3-Dichloropropene
102 70-1301,1,2-Trichloroethane
106 70-130Tetrachloroethene
106 70-1302-Hexanone
Page 15 of 16
Client Sample ID: LCSD
Lab ID#: 2107120-05AA
EPA METHOD TO-15 GC/MS FULL SCAN
a071404File Name:
Dil. Factor:1.00
Date of Collection: NA
Date of Analysis: 7/14/21 12:05 PM
Limits%RecoveryCompound
Method
106 70-130Dibromochloromethane
108 70-1301,2-Dibromoethane (EDB)
105 70-130Chlorobenzene
103 70-130Ethyl Benzene
101 70-130m,p-Xylene
101 70-130o-Xylene
106 70-130Styrene
108 70-130Bromoform
103 70-130Cumene
101 70-1301,1,2,2-Tetrachloroethane
102 70-130Propylbenzene
104 70-1304-Ethyltoluene
99 70-1301,3,5-Trimethylbenzene
109 70-1301,2,4-Trimethylbenzene
105 70-1301,3-Dichlorobenzene
104 70-1301,4-Dichlorobenzene
106 70-130alpha-Chlorotoluene
103 70-1301,2-Dichlorobenzene
131 Q 70-1301,2,4-Trichlorobenzene
134 Q 70-130Hexachlorobutadiene
Q = Exceeds Quality Control limits.
Container Type: NA - Not Applicable
Limits%RecoverySurrogates
Method
98 70-130Toluene-d8
100 70-1301,2-Dichloroethane-d4
97 70-1304-Bromofluorobenzene
Page 16 of 16

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

8/6/2021
Withers & Ravenel David Vail
115 Mackenan Dr. BUILDING 117 Cary, NC, 27511
Ref: Analytical Testing
Lab Report Number: 21-204-0040 Client Project Description: CC Newell Store
02172214.97
Dear David Vail:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/23/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 52
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202199012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-204-0040
Page 2 of 52
Report Number:
Sample Summary Table
Client Project Description:
21-204-0040
CC Newell Store
02172214.97
Lab No Client Sample ID Matrix Date Collected Date Received
07/21/2021 13:30Solids 92315 WR-6 07/23/2021 14:58
07/21/2021 13:35Solids 92316 WR-8 07/23/2021 14:58
07/21/2021 13:40Solids 92317 WR-9 07/23/2021 14:58
Page 3 of 52
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-204-0040
Report Limit
Project:CC Newell Store
V 92315WR-6
7.33 07/29/2021 16:386020BChromiummg/Kg - dry 1.24
8.21 07/29/2021 16:386020BLeadmg/Kg - dry 1.24
19.1 07/28/2021 17:13SW-DRYWT Moisture %
V 92316WR-8
9.23 07/29/2021 16:456020BChromiummg/Kg - dry 1.17
5.47 07/29/2021 16:456020BLeadmg/Kg - dry 1.17
14.7 07/28/2021 17:13SW-DRYWT Moisture %
V 92317WR-9
9.56 07/29/2021 16:516020BChromiummg/Kg - dry 1.23
7.46 07/29/2021 16:516020BLeadmg/Kg - dry 1.23
18.5 07/28/2021 17:13SW-DRYWT Moisture %
Page 4 of 52

Client: Withers & Ravenel CASE NARRATIVE
Project: CC Newell Store Lab Report Number: 21-204-0040
Date: 8/6/2021
Massachusetts EPH Method MADEP-EPH Sample 92202 Analyte: Aliphatic C9-C18
QC Batch No: V7110/V7020 Analyte was flagged for 0% recovery in the MS and/or MSD due to the result being below the MQL. The actual
result was 154.690 ug/mL which calculates to a recovery of 51.6% which is within the acceptable recovery range. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: 2,4-Dinitrophenol
QC Batch No: V7307/V7186 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
1310 ug/kg which calculates to a recovery of 78% which is within the acceptable recovery range.
Sample 92274 Analyte: 2,4-Dinitrophenol
QC Batch No: V7307/V7186 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1370 ug/kg which calculates to a recovery of 81.8% which is within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol QC Batch No: V7307/V7186 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1410 ug/kg which calculates to a recovery of 84.8% which is within the acceptable recovery range.
Analyte: 3,3`-Dichlorobenzidine
QC Batch No: V7307/V7186 Analyte did not recover in the MS.
Analyte: 3,3`-Dichlorobenzidine QC Batch No: V7307/V7186 Analyter did not recover in the MSD.
Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V7307/V7186 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 1340 ug/kg which calculates to a recovery of 80.4% which is within the acceptable recovery range. Sample 92274 Analyte: 4,6-Dinitro-2-methylphenol
QC Batch No: V7307/V7186 Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1450 ug/kg which calculates to a recovery of 87% which is within the acceptable recovery range. Analyte: 4,6-Dinitro-2-methylphenol QC Batch No: V7307/V7186
Page 5 of 52

Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1410 ug/kg which calculates to a recovery of 84.6% which is within the acceptable recovery range.
Analyte: Benzoic Acid QC Batch No: V7307/V7186
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 1390 ug/kg which calculates to a recovery of 83% which is within the acceptable recovery range.
Sample 92274
Analyte: Benzoic Acid QC Batch No: V7307/V7186
Analyte was flagged for 0% recovery in the MSD due to the result being below the MQL. The actual result was 1670 ug/kg which calculates to a recovery of 100% which is above the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V7307/V7186 Analyte was flagged for 0% recovery in the MS due to the result being below the MQL. The actual result was
1560 ug/kg which calculates to a recovery of 93.6% which is above the acceptable recovery range.
Analyte: Dibenz(a,h)anthracene QC Batch No: V7307/V7186
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits for MS/MSD.
Page 6 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<62.9 mg/Kg - dry 62.9Aliphatic C19-C36 1 07/30/21 05:17 MADEP-EPHZRC
<9.89 mg/Kg - dry 9.89Aliphatic C5-C8 100 07/26/21 14:29 MADEP-VPHTBL
<9.89 mg/Kg - dry 9.89Aliphatic C9-C12 100 07/26/21 14:29 MADEP-VPHTBL
<62.9 mg/Kg - dry 62.9Aliphatic C9-C18 1 07/30/21 05:17 MADEP-EPHZRC
<62.9 mg/Kg - dry 62.9Aromatic C11-C22 1 07/30/21 05:17 MADEP-EPHZRC
<9.89 mg/Kg - dry 9.89Aromatic C9-C10 100 07/26/21 14:29 MADEP-VPHTBL
<0.024 mg/Kg - dry 0.024Acetone 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Benzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Bromobenzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Bromochloromethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Bromodichloromethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Bromoform 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Bromomethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006n-Butylbenzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006sec-Butyl benzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006tert-Butyl benzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Carbon Tetrachloride 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Chlorobenzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Chlorodibromomethane 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Chloroethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Chloroform 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Chloromethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0062-Chlorotoluene 1 07/27/21 17:06 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.006 mg/Kg - dry 0.0064-Chlorotoluene 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.0121,2-Dibromo-3-Chloropropane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dibromoethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Dibromomethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dichlorobenzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,3-Dichlorobenzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,4-Dichlorobenzene 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Dichlorodifluoromethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,1-Dichloroethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dichloroethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,1-Dichloroethene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006cis-1,2-Dichloroethene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006trans-1,2-Dichloroethene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dichloropropane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,3-Dichloropropane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0062,2-Dichloropropane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,1-Dichloropropene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006cis-1,3-Dichloropropene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006trans-1,3-Dichloropropene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Ethylbenzene 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Hexachlorobutadiene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Di-Isopropyl Ether (DIPE)1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Isopropylbenzene 1 07/27/21 17:06 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.006 mg/Kg - dry 0.0064-Isopropyl toluene 1 07/27/21 17:06 8260DTBL
<0.024 mg/Kg - dry 0.0242-Hexanone 1 07/27/21 17:06 8260DTBL
<0.024 mg/Kg - dry 0.024Methyl Ethyl Ketone (MEK)1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Methylene Chloride 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Methyl tert-butyl ether (MTBE)1 07/27/21 17:06 8260DTBL
<0.024 mg/Kg - dry 0.0244-Methyl-2-Pentanone 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Naphthalene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006n-Propylbenzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Styrene 1 07/27/21 17:06 8260DTBL
<0.061 mg/Kg - dry 0.061Ethyl Tertiary Butyl Ether (ETBE)1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,1,2-Tetrachloroethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,2,2-Tetrachloroethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Tetrachloroethene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Toluene 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.0121,2,3-Trichlorobenzene 1 07/27/21 17:06 8260DTBL
19.1 %Moisture 1 07/28/21 17:13 SW-DRYWTEDV
<0.012 mg/Kg - dry 0.0121,2,4-Trichlorobenzene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,1-Trichloroethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,2-Trichloroethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Trichloroethene 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Trichlorofluoromethane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,2,3-Trichloropropane 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.0061,3,5-Trimethylbenzene 1 07/27/21 17:06 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.012 mg/Kg - dry 0.012Vinyl Acetate 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012Vinyl Chloride 1 07/27/21 17:06 8260DTBL
<0.012 mg/Kg - dry 0.012m,p-Xylene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006o-Xylene 1 07/27/21 17:06 8260DTBL
<0.006 mg/Kg - dry 0.006Xylene (Total)1 07/27/21 17:06 8260D
7.33 mg/Kg - dry 1.24Chromium 10 07/29/21 16:38 6020BEDV
8.21 mg/Kg - dry 1.24Lead 10 07/29/21 16:38 6020BEDV
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V6973 07/27/21 08:00
<0.024 mg/Kg - dry 0.024Acrolein 1 07/27/21 17:06 V6974TBL
<0.024 mg/Kg - dry 0.024Acrylonitrile 1 07/27/21 17:06 V6974TBL
<0.006 mg/Kg - dry 0.006Carbon Disulfide 1 07/27/21 17:06 V6974TBL
<0.012 mg/Kg - dry 0.012n-Hexane 1 07/27/21 17:06 V6974TBL
Surrogate: 4-Bromofluorobenzene 98.8 Limits: 70-130%07/27/21 17:061 TBL V6974
Surrogate: Dibromofluoromethane 103 Limits: 84-123%07/27/21 17:061 TBL V6974
Surrogate: Toluene-d8 89.9 Limits: 76-129%07/27/21 17:061 TBL V6974
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.815 mg/Kg - dry 0.815Acenaphthene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Acenaphthylene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Aniline 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Anthracene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Benzo(a)anthracene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Benzo(a)pyrene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Benzo(b)fluoranthene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Benzo(g,h,i)perylene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Benzo(k)fluoranthene 1 08/03/21 16:32 V7307JMV
<2.47 mg/Kg - dry 2.47Benzoic Acid 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Benzyl alcohol 1 08/03/21 16:32 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 11 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.815 mg/Kg - dry 0.815Bis(2-Chloroethoxy)methane 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Bis(2-Chloroethyl)ether 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.407Bis(2-Chloroisopropyl)ether 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Bis(2-ethylhexyl)phthalate 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8154-Bromophenyl phenyl ether 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.407Butyl benzyl phthalate 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8154-Chloro-3-methylphenol 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.4074-Chloroaniline 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152-Chloronaphthalene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152-Chlorophenol 1 08/03/21 16:32 V7307JMV
<1.24 mg/Kg - dry 1.244-Chlorophenyl phenyl ether 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Chrysene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Dibenz(a,h)anthracene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Dibenzofuran 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8151,2-Dichlorobenzene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8151,3-Dichlorobenzene 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.4071,4-Dichlorobenzene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8153,3'-Dichlorobenzidine 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152,4-Dichlorophenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Diethyl phthalate 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Dimethyl phthalate 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.4072,4-Dimethylphenol 1 08/03/21 16:32 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 12 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.815 mg/Kg - dry 0.815Di-n-butyl phthalate 1 08/03/21 16:32 V7307JMV
<1.85 mg/Kg - dry 1.854,6-Dinitro-2-methylphenol 1 08/03/21 16:32 V7307JMV
<1.85 mg/Kg - dry 1.852,4-Dinitrophenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152,4-Dinitrotoluene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152,6-Dinitrotoluene 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.407Di-n-Octyl Phthalate 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Fluoranthene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Fluorene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Hexachlorobenzene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Hexachlorobutadiene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Hexachlorocyclopentadiene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Hexachloroethane 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Indeno(1,2,3-cd)pyrene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Isophorone 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8151-Methylnaphthalene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152-Methylnaphthalene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152-Methylphenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8153&4 Methylphenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Naphthalene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152-Nitroaniline 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8153-Nitroaniline 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.4074-Nitroaniline 1 08/03/21 16:32 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 13 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-6
92315 Matrix:
7/21/2021 13:30
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.407 mg/Kg - dry 0.407Nitrobenzene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152-Nitrophenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8154-Nitrophenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815N-Nitrosodimethylamine 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815N-Nitrosodiphenylamine 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815N-Nitroso-di-n-propylamine 1 08/03/21 16:32 V7307JMV
<1.24 mg/Kg - dry 1.24Pentachlorophenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Phenanthrene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Phenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.815Pyrene 1 08/03/21 16:32 V7307JMV
<0.407 mg/Kg - dry 0.407Pyridine 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8151,2,4-Trichlorobenzene 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152,4,5-Trichlorophenol 1 08/03/21 16:32 V7307JMV
<0.815 mg/Kg - dry 0.8152,4,6-Trichlorophenol 1 08/03/21 16:32 V7307JMV
Surrogate: Phenol-d5 76.3 Limits: 34-121%08/03/21 16:321 V7307
Surrogate: 2-Fluorobiphenyl 77.2 Limits: 44-115%08/03/21 16:321 V7307
Surrogate: 2-Fluorophenol 75.1 Limits: 35-115%08/03/21 16:321 V7307
Surrogate: Nitrobenzene-d5 67.1 Limits: 37-122%08/03/21 16:321 V7307
Surrogate: 4-Terphenyl-d14 95.2 Limits: 54-127%08/03/21 16:321 V7307
Surrogate: 2,4,6-Tribromophenol 93.1 Limits: 39-132%08/03/21 16:321 V7307
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 14 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<58.1 mg/Kg - dry 58.1Aliphatic C19-C36 1 07/30/21 05:53 MADEP-EPHZRC
<9.38 mg/Kg - dry 9.38Aliphatic C5-C8 100 07/26/21 14:58 MADEP-VPHTBL
<9.38 mg/Kg - dry 9.38Aliphatic C9-C12 100 07/26/21 14:58 MADEP-VPHTBL
<58.1 mg/Kg - dry 58.1Aliphatic C9-C18 1 07/30/21 05:53 MADEP-EPHZRC
<58.1 mg/Kg - dry 58.1Aromatic C11-C22 1 07/30/21 05:53 MADEP-EPHZRC
<9.38 mg/Kg - dry 9.38Aromatic C9-C10 100 07/26/21 14:58 MADEP-VPHTBL
<0.023 mg/Kg - dry 0.023Acetone 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Benzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Bromobenzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Bromochloromethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Bromodichloromethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Bromoform 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Bromomethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005n-Butylbenzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005sec-Butyl benzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005tert-Butyl benzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Carbon Tetrachloride 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorobenzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Chlorodibromomethane 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Chloroethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Chloroform 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Chloromethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0052-Chlorotoluene 1 07/27/21 16:06 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Chlorotoluene 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.0111,2-Dibromo-3-Chloropropane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dibromoethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Dibromomethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichlorobenzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichlorobenzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,4-Dichlorobenzene 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Dichlorodifluoromethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloroethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloroethene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,2-Dichloroethene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,2-Dichloroethene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,2-Dichloropropane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,3-Dichloropropane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0052,2-Dichloropropane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,1-Dichloropropene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005cis-1,3-Dichloropropene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005trans-1,3-Dichloropropene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Ethylbenzene 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Hexachlorobutadiene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Di-Isopropyl Ether (DIPE)1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Isopropylbenzene 1 07/27/21 16:06 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.005 mg/Kg - dry 0.0054-Isopropyl toluene 1 07/27/21 16:06 8260DTBL
<0.023 mg/Kg - dry 0.0232-Hexanone 1 07/27/21 16:06 8260DTBL
<0.023 mg/Kg - dry 0.023Methyl Ethyl Ketone (MEK)1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Methylene Chloride 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Methyl tert-butyl ether (MTBE)1 07/27/21 16:06 8260DTBL
<0.023 mg/Kg - dry 0.0234-Methyl-2-Pentanone 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Naphthalene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005n-Propylbenzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Styrene 1 07/27/21 16:06 8260DTBL
<0.058 mg/Kg - dry 0.058Ethyl Tertiary Butyl Ether (ETBE)1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1,2-Tetrachloroethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2,2-Tetrachloroethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Tetrachloroethene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Toluene 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.0111,2,3-Trichlorobenzene 1 07/27/21 16:06 8260DTBL
14.7 %Moisture 1 07/28/21 17:13 SW-DRYWTEDV
<0.011 mg/Kg - dry 0.0111,2,4-Trichlorobenzene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,1-Trichloroethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,1,2-Trichloroethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Trichloroethene 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Trichlorofluoromethane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,2,3-Trichloropropane 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.0051,3,5-Trimethylbenzene 1 07/27/21 16:06 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.011 mg/Kg - dry 0.011Vinyl Acetate 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011Vinyl Chloride 1 07/27/21 16:06 8260DTBL
<0.011 mg/Kg - dry 0.011m,p-Xylene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005o-Xylene 1 07/27/21 16:06 8260DTBL
<0.005 mg/Kg - dry 0.005Xylene (Total)1 07/27/21 16:06 8260D
9.23 mg/Kg - dry 1.17Chromium 10 07/29/21 16:45 6020BEDV
5.47 mg/Kg - dry 1.17Lead 10 07/29/21 16:45 6020BEDV
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V6973 07/27/21 08:00
<0.023 mg/Kg - dry 0.023Acrolein 1 07/27/21 16:06 V6974TBL
<0.023 mg/Kg - dry 0.023Acrylonitrile 1 07/27/21 16:06 V6974TBL
<0.005 mg/Kg - dry 0.005Carbon Disulfide 1 07/27/21 16:06 V6974TBL
<0.011 mg/Kg - dry 0.011n-Hexane 1 07/27/21 16:06 V6974TBL
Surrogate: 4-Bromofluorobenzene 98.6 Limits: 70-130%07/27/21 16:061 TBL V6974
Surrogate: Dibromofluoromethane 102 Limits: 84-123%07/27/21 16:061 TBL V6974
Surrogate: Toluene-d8 89.6 Limits: 76-129%07/27/21 16:061 TBL V6974
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.773 mg/Kg - dry 0.773Acenaphthene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Acenaphthylene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Aniline 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Anthracene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Benzo(a)anthracene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Benzo(a)pyrene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Benzo(b)fluoranthene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Benzo(g,h,i)perylene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Benzo(k)fluoranthene 1 08/03/21 16:54 V7307JMV
<2.34 mg/Kg - dry 2.34Benzoic Acid 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Benzyl alcohol 1 08/03/21 16:54 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 19 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.773 mg/Kg - dry 0.773Bis(2-Chloroethoxy)methane 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Bis(2-Chloroethyl)ether 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.386Bis(2-Chloroisopropyl)ether 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Bis(2-ethylhexyl)phthalate 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7734-Bromophenyl phenyl ether 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.386Butyl benzyl phthalate 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7734-Chloro-3-methylphenol 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.3864-Chloroaniline 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732-Chloronaphthalene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732-Chlorophenol 1 08/03/21 16:54 V7307JMV
<1.17 mg/Kg - dry 1.174-Chlorophenyl phenyl ether 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Chrysene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Dibenz(a,h)anthracene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Dibenzofuran 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7731,2-Dichlorobenzene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7731,3-Dichlorobenzene 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.3861,4-Dichlorobenzene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7733,3'-Dichlorobenzidine 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732,4-Dichlorophenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Diethyl phthalate 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Dimethyl phthalate 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.3862,4-Dimethylphenol 1 08/03/21 16:54 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 20 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.773 mg/Kg - dry 0.773Di-n-butyl phthalate 1 08/03/21 16:54 V7307JMV
<1.76 mg/Kg - dry 1.764,6-Dinitro-2-methylphenol 1 08/03/21 16:54 V7307JMV
<1.76 mg/Kg - dry 1.762,4-Dinitrophenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732,4-Dinitrotoluene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732,6-Dinitrotoluene 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.386Di-n-Octyl Phthalate 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Fluoranthene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Fluorene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Hexachlorobenzene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Hexachlorobutadiene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Hexachlorocyclopentadiene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Hexachloroethane 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Indeno(1,2,3-cd)pyrene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Isophorone 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7731-Methylnaphthalene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732-Methylnaphthalene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732-Methylphenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7733&4 Methylphenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Naphthalene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732-Nitroaniline 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7733-Nitroaniline 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.3864-Nitroaniline 1 08/03/21 16:54 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 21 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-8
92316 Matrix:
7/21/2021 13:35
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.386 mg/Kg - dry 0.386Nitrobenzene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732-Nitrophenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7734-Nitrophenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773N-Nitrosodimethylamine 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773N-Nitrosodiphenylamine 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773N-Nitroso-di-n-propylamine 1 08/03/21 16:54 V7307JMV
<1.17 mg/Kg - dry 1.17Pentachlorophenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Phenanthrene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Phenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.773Pyrene 1 08/03/21 16:54 V7307JMV
<0.386 mg/Kg - dry 0.386Pyridine 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7731,2,4-Trichlorobenzene 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732,4,5-Trichlorophenol 1 08/03/21 16:54 V7307JMV
<0.773 mg/Kg - dry 0.7732,4,6-Trichlorophenol 1 08/03/21 16:54 V7307JMV
Surrogate: Phenol-d5 73.6 Limits: 34-121%08/03/21 16:541 V7307
Surrogate: 2-Fluorobiphenyl 74.3 Limits: 44-115%08/03/21 16:541 V7307
Surrogate: 2-Fluorophenol 60.1 Limits: 35-115%08/03/21 16:541 V7307
Surrogate: Nitrobenzene-d5 71.3 Limits: 37-122%08/03/21 16:541 V7307
Surrogate: 4-Terphenyl-d14 83.2 Limits: 54-127%08/03/21 16:541 V7307
Surrogate: 2,4,6-Tribromophenol 63.7 Limits: 39-132%08/03/21 16:541 V7307
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 22 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<62.1 mg/Kg - dry 62.1Aliphatic C19-C36 1 07/30/21 07:06 MADEP-EPHZRC
<9.82 mg/Kg - dry 9.82Aliphatic C5-C8 100 07/26/21 15:26 MADEP-VPHTBL
<9.82 mg/Kg - dry 9.82Aliphatic C9-C12 100 07/26/21 15:26 MADEP-VPHTBL
<62.1 mg/Kg - dry 62.1Aliphatic C9-C18 1 07/30/21 07:06 MADEP-EPHZRC
<62.1 mg/Kg - dry 62.1Aromatic C11-C22 1 07/30/21 07:06 MADEP-EPHZRC
<9.82 mg/Kg - dry 9.82Aromatic C9-C10 100 07/26/21 15:26 MADEP-VPHTBL
<0.024 mg/Kg - dry 0.024Acetone 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Benzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Bromobenzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Bromochloromethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Bromodichloromethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Bromoform 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Bromomethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006n-Butylbenzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006sec-Butyl benzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006tert-Butyl benzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Carbon Tetrachloride 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Chlorobenzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Chlorodibromomethane 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Chloroethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Chloroform 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Chloromethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0062-Chlorotoluene 1 07/27/21 16:36 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.006 mg/Kg - dry 0.0064-Chlorotoluene 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.0121,2-Dibromo-3-Chloropropane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dibromoethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Dibromomethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dichlorobenzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,3-Dichlorobenzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,4-Dichlorobenzene 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Dichlorodifluoromethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,1-Dichloroethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dichloroethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,1-Dichloroethene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006cis-1,2-Dichloroethene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006trans-1,2-Dichloroethene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,2-Dichloropropane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,3-Dichloropropane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0062,2-Dichloropropane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,1-Dichloropropene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006cis-1,3-Dichloropropene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006trans-1,3-Dichloropropene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Ethylbenzene 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Hexachlorobutadiene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Di-Isopropyl Ether (DIPE)1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Isopropylbenzene 1 07/27/21 16:36 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.006 mg/Kg - dry 0.0064-Isopropyl toluene 1 07/27/21 16:36 8260DTBL
<0.024 mg/Kg - dry 0.0242-Hexanone 1 07/27/21 16:36 8260DTBL
<0.024 mg/Kg - dry 0.024Methyl Ethyl Ketone (MEK)1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Methylene Chloride 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Methyl tert-butyl ether (MTBE)1 07/27/21 16:36 8260DTBL
<0.024 mg/Kg - dry 0.0244-Methyl-2-Pentanone 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Naphthalene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006n-Propylbenzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Styrene 1 07/27/21 16:36 8260DTBL
<0.061 mg/Kg - dry 0.061Ethyl Tertiary Butyl Ether (ETBE)1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,1,2-Tetrachloroethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,2,2-Tetrachloroethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Tetrachloroethene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Toluene 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.0121,2,3-Trichlorobenzene 1 07/27/21 16:36 8260DTBL
18.5 %Moisture 1 07/28/21 17:13 SW-DRYWTEDV
<0.012 mg/Kg - dry 0.0121,2,4-Trichlorobenzene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,1-Trichloroethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,1,2-Trichloroethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Trichloroethene 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Trichlorofluoromethane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,2,3-Trichloropropane 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.0061,3,5-Trimethylbenzene 1 07/27/21 16:36 8260DTBL
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.012 mg/Kg - dry 0.012Vinyl Acetate 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012Vinyl Chloride 1 07/27/21 16:36 8260DTBL
<0.012 mg/Kg - dry 0.012m,p-Xylene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006o-Xylene 1 07/27/21 16:36 8260DTBL
<0.006 mg/Kg - dry 0.006Xylene (Total)1 07/27/21 16:36 8260D
9.56 mg/Kg - dry 1.23Chromium 10 07/29/21 16:51 6020BEDV
7.46 mg/Kg - dry 1.23Lead 10 07/29/21 16:51 6020BEDV
Qualifiers/
Definitions
Limit ExceededLDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035 LOW
8260D Prep Batch(es):V6973 07/27/21 08:00
<0.024 mg/Kg - dry 0.024Acrolein 1 07/27/21 16:36 V6974TBL
<0.024 mg/Kg - dry 0.024Acrylonitrile 1 07/27/21 16:36 V6974TBL
<0.006 mg/Kg - dry 0.006Carbon Disulfide 1 07/27/21 16:36 V6974TBL
<0.012 mg/Kg - dry 0.012n-Hexane 1 07/27/21 16:36 V6974TBL
Surrogate: 4-Bromofluorobenzene 97.3 Limits: 70-130%07/27/21 16:361 TBL V6974
Surrogate: Dibromofluoromethane 99.5 Limits: 84-123%07/27/21 16:361 TBL V6974
Surrogate: Toluene-d8 89.1 Limits: 76-129%07/27/21 16:361 TBL V6974
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.811 mg/Kg - dry 0.811Acenaphthene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Acenaphthylene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Aniline 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Anthracene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Benzo(a)anthracene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Benzo(a)pyrene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Benzo(b)fluoranthene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Benzo(g,h,i)perylene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Benzo(k)fluoranthene 1 08/03/21 17:17 V7307JMV
<2.45 mg/Kg - dry 2.45Benzoic Acid 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Benzyl alcohol 1 08/03/21 17:17 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 27 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.811 mg/Kg - dry 0.811Bis(2-Chloroethoxy)methane 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Bis(2-Chloroethyl)ether 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.404Bis(2-Chloroisopropyl)ether 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Bis(2-ethylhexyl)phthalate 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8114-Bromophenyl phenyl ether 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.404Butyl benzyl phthalate 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8114-Chloro-3-methylphenol 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.4044-Chloroaniline 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112-Chloronaphthalene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112-Chlorophenol 1 08/03/21 17:17 V7307JMV
<1.23 mg/Kg - dry 1.234-Chlorophenyl phenyl ether 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Chrysene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Dibenz(a,h)anthracene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Dibenzofuran 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8111,2-Dichlorobenzene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8111,3-Dichlorobenzene 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.4041,4-Dichlorobenzene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8113,3'-Dichlorobenzidine 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112,4-Dichlorophenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Diethyl phthalate 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Dimethyl phthalate 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.4042,4-Dimethylphenol 1 08/03/21 17:17 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 28 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.811 mg/Kg - dry 0.811Di-n-butyl phthalate 1 08/03/21 17:17 V7307JMV
<1.84 mg/Kg - dry 1.844,6-Dinitro-2-methylphenol 1 08/03/21 17:17 V7307JMV
<1.84 mg/Kg - dry 1.842,4-Dinitrophenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112,4-Dinitrotoluene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112,6-Dinitrotoluene 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.404Di-n-Octyl Phthalate 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Fluoranthene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Fluorene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Hexachlorobenzene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Hexachlorobutadiene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Hexachlorocyclopentadiene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Hexachloroethane 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Indeno(1,2,3-cd)pyrene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Isophorone 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8111-Methylnaphthalene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112-Methylnaphthalene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112-Methylphenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8113&4 Methylphenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Naphthalene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112-Nitroaniline 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8113-Nitroaniline 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.4044-Nitroaniline 1 08/03/21 17:17 V7307JMV
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 29 of 52
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-204-0040
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
David Vail
Cary
02172214.97 Received : 07/23/2021
CC Newell Store
Report Date : 08/06/2021
Sample ID :
Lab No :
Sampled:WR-9
92317 Matrix:
7/21/2021 13:40
Solids
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V7186 08/02/21 13:45
<0.404 mg/Kg - dry 0.404Nitrobenzene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112-Nitrophenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8114-Nitrophenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811N-Nitrosodimethylamine 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811N-Nitrosodiphenylamine 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811N-Nitroso-di-n-propylamine 1 08/03/21 17:17 V7307JMV
<1.23 mg/Kg - dry 1.23Pentachlorophenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Phenanthrene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Phenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.811Pyrene 1 08/03/21 17:17 V7307JMV
<0.404 mg/Kg - dry 0.404Pyridine 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8111,2,4-Trichlorobenzene 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112,4,5-Trichlorophenol 1 08/03/21 17:17 V7307JMV
<0.811 mg/Kg - dry 0.8112,4,6-Trichlorophenol 1 08/03/21 17:17 V7307JMV
Surrogate: Phenol-d5 71.9 Limits: 34-121%08/03/21 17:171 V7307
Surrogate: 2-Fluorobiphenyl 73.1 Limits: 44-115%08/03/21 17:171 V7307
Surrogate: 2-Fluorophenol 75.4 Limits: 35-115%08/03/21 17:171 V7307
Surrogate: Nitrobenzene-d5 69.5 Limits: 37-122%08/03/21 17:171 V7307
Surrogate: 4-Terphenyl-d14 83.8 Limits: 54-127%08/03/21 17:171 V7307
Surrogate: 2,4,6-Tribromophenol 79.0 Limits: 39-132%08/03/21 17:171 V7307
Qualifiers/
Definitions
Method Quantitation LimitMQLDilution FactorDF
Page 30 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Metals Analyses
6020B
V7096QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:V7024
Associated Lab Samples: 92315, 92316, 92317
LRB-V7024 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
07/29/21 14:411.00<1.00mg/KgChromium
07/29/21 14:411.00<1.00mg/KgLead
LCS-V7024Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
10212.712.5mg/KgChromium 80-120
10312.912.5mg/KgLead 80-120
V 92130-MS-V7024 V 92130-MSD-V7024Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
24.6 126*26.212.512.58.79mg/KgChromium 139*75-125 6.2 20
19.2 10019.912.512.56.73mg/KgLead 105 75-125 3.5 20
V 92130-PDS-V7024Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
07/29/21 15:1399.016.8mg/KgChromium
07/29/21 15:1398.015.5mg/KgLead
Page 1 of 20* QC Fail Date:08/06/2021 04:43 PM
Page 31 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6973
Associated Lab Samples: 92315, 92316, 92317
LRB-V6973 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/27/21 12:080.020<0.020mg/KgAcetone
07/27/21 12:080.005<0.005mg/KgBenzene
07/27/21 12:080.005<0.005mg/KgBromobenzene
07/27/21 12:080.005<0.005mg/KgBromochloromethane
07/27/21 12:080.005<0.005mg/KgBromodichloromethane
07/27/21 12:080.005<0.005mg/KgBromoform
07/27/21 12:080.010<0.010mg/KgBromomethane
07/27/21 12:080.005<0.005mg/Kgn-Butylbenzene
07/27/21 12:080.005<0.005mg/Kgsec-Butyl benzene
07/27/21 12:080.005<0.005mg/Kgtert-Butyl benzene
07/27/21 12:080.005<0.005mg/KgCarbon Tetrachloride
07/27/21 12:080.005<0.005mg/KgChlorobenzene
07/27/21 12:080.005<0.005mg/KgChlorodibromomethane
07/27/21 12:080.010<0.010mg/KgChloroethane
07/27/21 12:080.005<0.005mg/KgChloroform
07/27/21 12:080.010<0.010mg/KgChloromethane
07/27/21 12:080.005<0.005mg/Kg2-Chlorotoluene
07/27/21 12:080.005<0.005mg/Kg4-Chlorotoluene
07/27/21 12:080.010<0.010mg/Kg1,2-Dibromo-3-Chloropropane
07/27/21 12:080.005<0.005mg/Kg1,2-Dibromoethane
07/27/21 12:080.005<0.005mg/KgDibromomethane
07/27/21 12:080.005<0.005mg/Kg1,2-Dichlorobenzene
07/27/21 12:080.005<0.005mg/Kg1,3-Dichlorobenzene
07/27/21 12:080.005<0.005mg/Kg1,4-Dichlorobenzene
07/27/21 12:080.010<0.010mg/KgDichlorodifluoromethane
07/27/21 12:080.005<0.005mg/Kg1,1-Dichloroethane
07/27/21 12:080.005<0.005mg/Kg1,2-Dichloroethane
Page 2 of 20Date:08/06/2021 04:43 PM
Page 32 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6973
Associated Lab Samples: 92315, 92316, 92317
LRB-V6973 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/27/21 12:080.005<0.005mg/Kg1,1-Dichloroethene
07/27/21 12:080.005<0.005mg/Kgcis-1,2-Dichloroethene
07/27/21 12:080.005<0.005mg/Kgtrans-1,2-Dichloroethene
07/27/21 12:080.005<0.005mg/Kg1,2-Dichloropropane
07/27/21 12:080.005<0.005mg/Kg1,3-Dichloropropane
07/27/21 12:080.005<0.005mg/Kg2,2-Dichloropropane
07/27/21 12:080.005<0.005mg/Kg1,1-Dichloropropene
07/27/21 12:080.005<0.005mg/Kgcis-1,3-Dichloropropene
07/27/21 12:080.005<0.005mg/Kgtrans-1,3-Dichloropropene
07/27/21 12:080.005<0.005mg/KgEthylbenzene
07/27/21 12:080.010<0.010mg/KgHexachlorobutadiene
07/27/21 12:080.005<0.005mg/KgDi-Isopropyl Ether (DIPE)
07/27/21 12:080.005<0.005mg/KgIsopropylbenzene
07/27/21 12:080.005<0.005mg/Kg4-Isopropyl toluene
07/27/21 12:080.020<0.020mg/Kg2-Hexanone
07/27/21 12:080.020<0.020mg/KgMethyl Ethyl Ketone (MEK)
07/27/21 12:080.010<0.010mg/KgMethylene Chloride
07/27/21 12:080.005<0.005mg/KgMethyl tert-butyl ether (MTBE)
07/27/21 12:080.020<0.020mg/Kg4-Methyl-2-Pentanone
07/27/21 12:080.010<0.010mg/KgNaphthalene
07/27/21 12:080.005<0.005mg/Kgn-Propylbenzene
07/27/21 12:080.005<0.005mg/KgStyrene
07/27/21 12:080.050<0.050mg/KgEthyl Tertiary Butyl Ether (ETBE)
07/27/21 12:080.005<0.005mg/Kg1,1,1,2-Tetrachloroethane
07/27/21 12:080.005<0.005mg/Kg1,1,2,2-Tetrachloroethane
07/27/21 12:080.005<0.005mg/KgTetrachloroethene
07/27/21 12:080.005<0.005mg/KgToluene
Page 3 of 20Date:08/06/2021 04:43 PM
Page 33 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6973
Associated Lab Samples: 92315, 92316, 92317
LRB-V6973 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/27/21 12:080.010<0.010mg/Kg1,2,3-Trichlorobenzene
07/27/21 12:080.010<0.010mg/Kg1,2,4-Trichlorobenzene
07/27/21 12:080.005<0.005mg/Kg1,1,1-Trichloroethane
07/27/21 12:080.005<0.005mg/Kg1,1,2-Trichloroethane
07/27/21 12:080.005<0.005mg/KgTrichloroethene
07/27/21 12:080.010<0.010mg/KgTrichlorofluoromethane
07/27/21 12:080.005<0.005mg/Kg1,2,3-Trichloropropane
07/27/21 12:080.005<0.005mg/Kg1,3,5-Trimethylbenzene
07/27/21 12:080.010<0.010mg/KgVinyl Acetate
07/27/21 12:080.010<0.010mg/KgVinyl Chloride
07/27/21 12:080.010<0.010mg/Kgm,p-Xylene
07/27/21 12:080.005<0.005mg/Kgo-Xylene
07/27/21 12:080.020<0.020mg/KgAcrolein
07/27/21 12:080.020<0.020mg/KgAcrylonitrile
07/27/21 12:080.005<0.005mg/KgCarbon Disulfide
07/27/21 12:080.010<0.010mg/Kgn-Hexane
07/27/21 12:084-Bromofluorobenzene (S)99.8 70-130
07/27/21 12:08Dibromofluoromethane (S)99.4 84-123
07/27/21 12:08Toluene-d8 (S)90.6 76-129
LCS-V6973 LCSD-V6973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.099 99.099.20.0990.100mg/KgAcetone 29-198 0.2 20
0.052 1041100.0550.050mg/KgBenzene 74-127 5.4 20
0.043 87.290.60.0450.050mg/KgBromobenzene 73-125 3.8 20
Page 4 of 20Date:08/06/2021 04:43 PM
Page 34 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6973
LCS-V6973 LCSD-V6973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.052 1041090.0540.050mg/KgBromochloromethane 72-134 4.6 20
0.053 1061090.0540.050mg/KgBromodichloromethane 75-122 2.9 20
0.047 95.296.40.0480.050mg/KgBromoform 66-135 1.2 20
0.051 1021140.0570.050mg/KgBromomethane 20-180 10.9 20
0.043 87.293.80.0460.050mg/Kgn-Butylbenzene 65-135 7.2 20
0.043 87.094.00.0470.050mg/Kgsec-Butyl benzene 66-131 7.7 20
0.042 85.691.40.0450.050mg/Kgtert-Butyl benzene 67-132 6.5 20
0.049 99.01070.0530.050mg/KgCarbon Tetrachloride 64-143 7.9 20
0.046 93.498.40.0490.050mg/KgChlorobenzene 74-118 5.2 20
0.047 94.697.20.0480.050mg/KgChlorodibromomethane 73-122 2.7 20
0.045 90.496.40.0480.050mg/KgChloroethane 33-149 6.4 20
0.051 1021060.0530.050mg/KgChloroform 73-127 3.8 20
0.048 96.01080.0530.050mg/KgChloromethane 45-143 11.5 20
0.043 87.893.00.0460.050mg/Kg2-Chlorotoluene 67-124 5.7 20
0.044 88.293.40.0460.050mg/Kg4-Chlorotoluene 71-126 5.7 20
0.043 86.287.40.0430.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 1.3 20
0.047 94.896.40.0480.050mg/Kg1,2-Dibromoethane 70-132 1.6 20
0.054 1091080.0540.050mg/KgDibromomethane 74-133 0.5 20
0.044 88.492.60.0460.050mg/Kg1,2-Dichlorobenzene 72-123 4.6 20
0.043 87.492.20.0460.050mg/Kg1,3-Dichlorobenzene 71-120 5.3 20
0.044 88.291.40.0450.050mg/Kg1,4-Dichlorobenzene 71-123 3.5 20
0.046 92.61010.0500.050mg/KgDichlorodifluoromethane 26-146 8.4 20
0.052 1051110.0550.050mg/Kg1,1-Dichloroethane 74-127 5.7 20
0.053 1061080.0540.050mg/Kg1,2-Dichloroethane 68-128 2.0 20
0.051 1031100.0550.050mg/Kg1,1-Dichloroethene 67-149 6.7 20
0.052 1041100.0550.050mg/Kgcis-1,2-Dichloroethene 76-134 5.4 20
Page 5 of 20Date:08/06/2021 04:43 PM
Page 35 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6973
LCS-V6973 LCSD-V6973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.051 1031120.0550.050mg/Kgtrans-1,2-Dichloroethene 73-132 8.0 20
0.053 1061080.0540.050mg/Kg1,2-Dichloropropane 73-130 2.0 20
0.046 93.896.40.0480.050mg/Kg1,3-Dichloropropane 75-124 2.7 20
0.050 1001080.0540.050mg/Kg2,2-Dichloropropane 50-142 8.0 20
0.051 1021090.0540.050mg/Kg1,1-Dichloropropene 71-130 7.0 20
0.053 1071090.0540.050mg/Kgcis-1,3-Dichloropropene 71-125 1.8 20
0.053 1071090.0540.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.8 20
0.046 92.098.20.0490.050mg/KgEthylbenzene 74-128 6.5 20
0.042 85.092.80.0460.050mg/KgHexachlorobutadiene 64-125 8.7 20
0.054 1091130.0560.050mg/KgDi-Isopropyl Ether (DIPE)59-159 3.0 20
0.043 87.292.60.0460.050mg/KgIsopropylbenzene 68-126 6.0 20
0.043 86.893.20.0460.050mg/Kg4-Isopropyl toluene 68-129 7.1 20
0.044 89.290.80.0450.050mg/Kg2-Hexanone 61-157 1.7 20
0.050 1001010.0500.050mg/KgMethyl Ethyl Ketone (MEK)63-149 0.3 20
0.051 1021080.0530.050mg/KgMethylene Chloride 74-129 4.9 20
0.052 1051070.0530.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.8 20
0.052 1051050.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 0.0 20
0.043 86.286.20.0430.050mg/KgNaphthalene 57-157 0.0 20
0.043 87.893.40.0460.050mg/Kgn-Propylbenzene 67-130 6.1 20
0.047 94.899.00.0490.050mg/KgStyrene 77-121 4.3 20
0.111 1111130.1130.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 1.7 20
0.046 93.297.40.0480.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 4.4 20
0.044 89.290.60.0450.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 1.5 20
0.050 1001080.0540.050mg/KgTetrachloroethene 68-130 7.4 20
0.051 1021080.0530.050mg/KgToluene 71-129 5.1 20
0.045 90.892.60.0460.050mg/Kg1,2,3-Trichlorobenzene 68-130 1.9 20
Page 6 of 20Date:08/06/2021 04:43 PM
Page 36 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V6974QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035 LOW
QC Prep:V6973
LCS-V6973 LCSD-V6973Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.045 90.693.40.0460.050mg/Kg1,2,4-Trichlorobenzene 66-125 3.0 20
0.050 1021080.0540.050mg/Kg1,1,1-Trichloroethane 67-131 6.2 20
0.047 94.897.20.0480.050mg/Kg1,1,2-Trichloroethane 70-133 2.5 20
0.051 1031090.0540.050mg/KgTrichloroethene 75-133 6.2 20
0.047 95.01050.0520.050mg/KgTrichlorofluoromethane 44-146 10.1 20
0.045 90.089.80.0440.050mg/Kg1,2,3-Trichloropropane 60-137 0.2 20
0.043 87.292.60.0460.050mg/Kg1,3,5-Trimethylbenzene 69-128 6.0 20
0.054 1101110.0550.050mg/KgVinyl Acetate 85-161 1.6 20
0.049 99.41070.0530.050mg/KgVinyl Chloride 48-147 7.7 20
0.094 94.31010.1010.100mg/Kgm,p-Xylene 75-124 6.8 20
0.046 93.697.80.0480.050mg/Kgo-Xylene 74-126 4.3 20
0.111 1111110.1110.100mg/KgAcrolein 70-130 0.0 20
0.105 1051060.1060.100mg/KgAcrylonitrile 65-134 0.9 20
0.049 98.41070.0530.050mg/KgCarbon Disulfide 61-129 8.3 20
0.050 1011100.0540.050mg/Kgn-Hexane 70-130 8.3 20
97.697.84-Bromofluorobenzene (S)70-130
99.297.8Dibromofluoromethane (S)84-123
91.291.2Toluene-d8 (S)76-129
Page 7 of 20Date:08/06/2021 04:43 PM
Page 37 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
Associated Lab Samples: 92315, 92316, 92317
LRB-V7186 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/03/21 15:030.660<0.660mg/KgAcenaphthene
08/03/21 15:030.660<0.660mg/KgAcenaphthylene
08/03/21 15:030.660<0.660mg/KgAniline
08/03/21 15:030.660<0.660mg/KgAnthracene
08/03/21 15:030.660<0.660mg/KgBenzo(a)anthracene
08/03/21 15:030.660<0.660mg/KgBenzo(a)pyrene
08/03/21 15:030.660<0.660mg/KgBenzo(b)fluoranthene
08/03/21 15:030.660<0.660mg/KgBenzo(g,h,i)perylene
08/03/21 15:030.660<0.660mg/KgBenzo(k)fluoranthene
08/03/21 15:032.00<2.00mg/KgBenzoic Acid
08/03/21 15:030.660<0.660mg/KgBenzyl alcohol
08/03/21 15:030.660<0.660mg/KgBis(2-Chloroethoxy)methane
08/03/21 15:030.660<0.660mg/KgBis(2-Chloroethyl)ether
08/03/21 15:030.330<0.330mg/KgBis(2-Chloroisopropyl)ether
08/03/21 15:030.660<0.660mg/KgBis(2-ethylhexyl)phthalate
08/03/21 15:030.660<0.660mg/Kg4-Bromophenyl phenyl ether
08/03/21 15:030.330<0.330mg/KgButyl benzyl phthalate
08/03/21 15:030.660<0.660mg/Kg4-Chloro-3-methylphenol
08/03/21 15:030.330<0.330mg/Kg4-Chloroaniline
08/03/21 15:030.660<0.660mg/Kg2-Chloronaphthalene
08/03/21 15:030.660<0.660mg/Kg2-Chlorophenol
08/03/21 15:031.00<1.00mg/Kg4-Chlorophenyl phenyl ether
08/03/21 15:030.660<0.660mg/KgChrysene
08/03/21 15:030.660<0.660mg/KgDibenz(a,h)anthracene
08/03/21 15:030.660<0.660mg/KgDibenzofuran
08/03/21 15:030.660<0.660mg/Kg1,2-Dichlorobenzene
08/03/21 15:030.660<0.660mg/Kg1,3-Dichlorobenzene
Page 8 of 20Date:08/06/2021 04:43 PM
Page 38 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
Associated Lab Samples: 92315, 92316, 92317
LRB-V7186 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/03/21 15:030.330<0.330mg/Kg1,4-Dichlorobenzene
08/03/21 15:030.660<0.660mg/Kg3,3'-Dichlorobenzidine
08/03/21 15:030.660<0.660mg/Kg2,4-Dichlorophenol
08/03/21 15:030.660<0.660mg/KgDiethyl phthalate
08/03/21 15:030.660<0.660mg/KgDimethyl phthalate
08/03/21 15:030.330<0.330mg/Kg2,4-Dimethylphenol
08/03/21 15:030.660<0.660mg/KgDi-n-butyl phthalate
08/03/21 15:031.50<1.50mg/Kg4,6-Dinitro-2-methylphenol
08/03/21 15:031.50<1.50mg/Kg2,4-Dinitrophenol
08/03/21 15:030.660<0.660mg/Kg2,4-Dinitrotoluene
08/03/21 15:030.660<0.660mg/Kg2,6-Dinitrotoluene
08/03/21 15:030.330<0.330mg/KgDi-n-Octyl Phthalate
08/03/21 15:030.660<0.660mg/KgFluoranthene
08/03/21 15:030.660<0.660mg/KgFluorene
08/03/21 15:030.660<0.660mg/KgHexachlorobenzene
08/03/21 15:030.660<0.660mg/KgHexachlorobutadiene
08/03/21 15:030.660<0.660mg/KgHexachlorocyclopentadiene
08/03/21 15:030.660<0.660mg/KgHexachloroethane
08/03/21 15:030.660<0.660mg/KgIndeno(1,2,3-cd)pyrene
08/03/21 15:030.660<0.660mg/KgIsophorone
08/03/21 15:030.660<0.660mg/Kg1-Methylnaphthalene
08/03/21 15:030.660<0.660mg/Kg2-Methylnaphthalene
08/03/21 15:030.660<0.660mg/Kg2-Methylphenol
08/03/21 15:030.660<0.660mg/Kg3&4 Methylphenol
08/03/21 15:030.660<0.660mg/KgNaphthalene
08/03/21 15:030.660<0.660mg/Kg2-Nitroaniline
08/03/21 15:030.660<0.660mg/Kg3-Nitroaniline
Page 9 of 20Date:08/06/2021 04:43 PM
Page 39 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
Associated Lab Samples: 92315, 92316, 92317
LRB-V7186 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/03/21 15:030.330<0.330mg/Kg4-Nitroaniline
08/03/21 15:030.330<0.330mg/KgNitrobenzene
08/03/21 15:030.660<0.660mg/Kg2-Nitrophenol
08/03/21 15:030.660<0.660mg/Kg4-Nitrophenol
08/03/21 15:030.660<0.660mg/KgN-Nitrosodimethylamine
08/03/21 15:030.660<0.660mg/KgN-Nitrosodiphenylamine
08/03/21 15:030.660<0.660mg/KgN-Nitroso-di-n-propylamine
08/03/21 15:031.00<1.00mg/KgPentachlorophenol
08/03/21 15:030.660<0.660mg/KgPhenanthrene
08/03/21 15:030.660<0.660mg/KgPhenol
08/03/21 15:030.660<0.660mg/KgPyrene
08/03/21 15:030.330<0.330mg/KgPyridine
08/03/21 15:030.660<0.660mg/Kg1,2,4-Trichlorobenzene
08/03/21 15:030.660<0.660mg/Kg2,4,5-Trichlorophenol
08/03/21 15:030.660<0.660mg/Kg2,4,6-Trichlorophenol
08/03/21 15:032-Fluorobiphenyl (S)93.4 44-115
08/03/21 15:032-Fluorophenol (S)96.3 35-115
08/03/21 15:03Nitrobenzene-d5 (S)89.8 37-122
08/03/21 15:034-Terphenyl-d14 (S)108 54-127
08/03/21 15:032,4,6-Tribromophenol (S)102 39-132
08/03/21 15:03Phenol-d5 (S)93.3 34-121
LCS-V7186Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
82.01.371.67mg/KgAcenaphthene 40-123
88.01.471.67mg/KgAcenaphthylene 32-132
Page 10 of 20Date:08/06/2021 04:43 PM
Page 40 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
LCS-V7186Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
81.41.361.67mg/KgAniline 12-197
88.01.471.67mg/KgAnthracene 47-123
83.81.401.67mg/KgBenzo(a)anthracene 49-126
1031.721.67mg/KgBenzo(a)pyrene 45-129
95.21.591.67mg/KgBenzo(b)fluoranthene 45-132
89.81.501.67mg/KgBenzo(g,h,i)perylene 43-134
87.41.461.67mg/KgBenzo(k)fluoranthene 47-132
0.0*0.5801.67mg/KgBenzoic Acid 10-83
82.61.381.67mg/KgBenzyl alcohol 29-122
89.81.501.67mg/KgBis(2-Chloroethoxy)methane 36-121
69.41.161.67mg/KgBis(2-Chloroethyl)ether 31-120
77.81.301.67mg/KgBis(2-Chloroisopropyl)ether 33-131
96.41.611.67mg/KgBis(2-ethylhexyl)phthalate 51-133
83.21.391.67mg/Kg4-Bromophenyl phenyl ether 46-124
92.21.541.67mg/KgButyl benzyl phthalate 48-132
91.01.521.67mg/Kg4-Chloro-3-methylphenol 45-122
76.61.281.67mg/Kg4-Chloroaniline 17-106
83.21.391.67mg/Kg2-Chloronaphthalene 41-114
82.01.371.67mg/Kg2-Chlorophenol 34-121
86.81.451.67mg/Kg4-Chlorophenyl phenyl ether 45-121
88.01.471.67mg/KgChrysene 50-124
67.61.131.67mg/KgDibenz(a,h)anthracene 45-134
85.01.421.67mg/KgDibenzofuran 44-120
73.61.231.67mg/Kg1,2-Dichlorobenzene 33-117
72.41.211.67mg/Kg1,3-Dichlorobenzene 30-115
71.81.201.67mg/Kg1,4-Dichlorobenzene 31-115
84.41.411.67mg/Kg3,3'-Dichlorobenzidine 22-121
Page 11 of 20* QC Fail Date:08/06/2021 04:43 PM
Page 41 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
LCS-V7186Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
86.21.441.67mg/Kg2,4-Dichlorophenol 40-122
89.81.501.67mg/KgDiethyl phthalate 50-124
84.41.411.67mg/KgDimethyl phthalate 48-124
91.61.531.67mg/Kg2,4-Dimethylphenol 30-127
98.81.651.67mg/KgDi-n-butyl phthalate 51-128
0.0*0.2401.67mg/Kg4,6-Dinitro-2-methylphenol 29-132
0.0*0.5201.67mg/Kg2,4-Dinitrophenol 27-129
91.01.521.67mg/Kg2,4-Dinitrotoluene 48-126
91.61.531.67mg/Kg2,6-Dinitrotoluene 46-124
98.21.641.67mg/KgDi-n-Octyl Phthalate 45-140
90.41.511.67mg/KgFluoranthene 50-127
88.01.471.67mg/KgFluorene 43-125
85.61.431.67mg/KgHexachlorobenzene 45-122
75.41.261.67mg/KgHexachlorobutadiene 32-123
64.01.071.67mg/KgHexachlorocyclopentadiene 32-117
70.01.171.67mg/KgHexachloroethane 28-117
88.61.481.67mg/KgIndeno(1,2,3-cd)pyrene 45-133
73.01.221.67mg/KgIsophorone 30-122
80.81.351.67mg/Kg1-Methylnaphthalene 40-119
81.41.361.67mg/Kg2-Methylnaphthalene 38-122
84.41.411.67mg/Kg2-Methylphenol 32-122
75.41.261.67mg/Kg3&4 Methylphenol 34-119
77.21.291.67mg/KgNaphthalene 35-123
88.01.471.67mg/Kg2-Nitroaniline 44-127
84.41.411.67mg/Kg3-Nitroaniline 33-119
91.61.531.67mg/Kg4-Nitroaniline 63-147
76.01.271.67mg/KgNitrobenzene 34-122
Page 12 of 20* QC Fail Date:08/06/2021 04:43 PM
Page 42 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
LCS-V7186Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
77.21.291.67mg/Kg2-Nitrophenol 36-123
1041.741.67mg/Kg4-Nitrophenol 30-132
68.21.141.67mg/KgN-Nitrosodimethylamine 10-146
1021.711.67mg/KgN-Nitrosodiphenylamine 38-127
78.41.311.67mg/KgN-Nitroso-di-n-propylamine 36-120
77.81.301.67mg/KgPentachlorophenol 25-133
88.61.481.67mg/KgPhenanthrene 50-121
83.81.401.67mg/KgPhenol 34-121
88.61.481.67mg/KgPyrene 47-127
48.60.8121.67mg/KgPyridine 10-80
72.41.211.67mg/Kg1,2,4-Trichlorobenzene 34-118
82.01.371.67mg/Kg2,4,5-Trichlorophenol 41-124
85.01.421.67mg/Kg2,4,6-Trichlorophenol 39-126
82.02-Fluorobiphenyl (S)44-115
84.92-Fluorophenol (S)35-115
76.0Nitrobenzene-d5 (S)37-122
88.04-Terphenyl-d14 (S)54-127
90.32,4,6-Tribromophenol (S)39-132
82.2Phenol-d5 (S)34-121
V 92274-MS-V7186 V 92274-MSD-V7186Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.44 86.21.481.671.67<0.660mg/KgAcenaphthene 88.6 40-123 2.7 20
1.50 89.81.541.671.67<0.660mg/KgAcenaphthylene 92.2 32-132 2.6 20
0.868 51.90.8221.671.67<0.660mg/KgAniline 49.2 12-197 5.4 20
Page 13 of 20Date:08/06/2021 04:43 PM
Page 43 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
V 92274-MS-V7186 V 92274-MSD-V7186Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.53 91.61.541.671.67<0.660mg/KgAnthracene 92.2 47-123 0.6 20
1.45 86.81.491.671.67<0.660mg/KgBenzo(a)anthracene 89.2 49-126 2.7 20
1.75 1051.811.671.67<0.660mg/KgBenzo(a)pyrene 108 45-129 3.3 20
1.59 95.21.641.671.67<0.660mg/KgBenzo(b)fluoranthene 98.2 45-132 3.0 20
1.52 91.01.521.671.67<0.660mg/KgBenzo(g,h,i)perylene 91.0 43-134 0.0 20
1.54 92.21.581.671.67<0.660mg/KgBenzo(k)fluoranthene 94.6 47-132 2.5 20
1.56 0.0*1.671.671.67<2.00mg/KgBenzoic Acid 0.0*10-83 0.0 20
1.39 83.21.391.671.67<0.660mg/KgBenzyl alcohol 83.2 29-122 0.0 20
1.52 91.01.541.671.67<0.660mg/KgBis(2-Chloroethoxy)methane 92.2 36-121 1.3 20
1.30 77.81.291.671.67<0.660mg/KgBis(2-Chloroethyl)ether 77.2 31-120 0.7 20
1.28 76.61.271.671.67<0.330mg/KgBis(2-Chloroisopropyl)ether 76.0 33-131 0.7 20
1.67 1001.711.671.67<0.660mg/KgBis(2-ethylhexyl)phthalate 102 51-133 2.3 20
1.43 85.61.481.671.67<0.660mg/Kg4-Bromophenyl phenyl ether 88.6 46-124 3.4 20
1.59 95.21.631.671.67<0.330mg/KgButyl benzyl phthalate 97.6 48-132 2.4 20
1.52 91.01.581.671.67<0.660mg/Kg4-Chloro-3-methylphenol 94.6 45-122 3.8 20
0.979 58.61.011.671.67<0.330mg/Kg4-Chloroaniline 60.4 17-106 3.1 20
1.40 83.81.441.671.67<0.660mg/Kg2-Chloronaphthalene 86.2 41-114 2.8 20
1.35 80.81.301.671.67<0.660mg/Kg2-Chlorophenol 77.8 34-121 3.7 20
1.52 91.01.561.671.67<1.00mg/Kg4-Chlorophenyl phenyl ether 93.4 45-121 2.5 20
1.50 89.81.521.671.67<0.660mg/KgChrysene 91.0 50-124 1.3 20
1.66 99.41.271.671.67<0.660mg/KgDibenz(a,h)anthracene 76.0 45-134 26.6*20
1.45 86.81.511.671.67<0.660mg/KgDibenzofuran 90.4 44-120 4.0 20
1.21 72.41.171.671.67<0.660mg/Kg1,2-Dichlorobenzene 70.0 33-117 3.3 20
1.17 70.01.131.671.67<0.660mg/Kg1,3-Dichlorobenzene 67.6 30-115 3.4 20
1.16 69.41.101.671.67<0.330mg/Kg1,4-Dichlorobenzene 65.8 31-115 5.3 20
0.147 0.0*0.1471.671.67<0.660mg/Kg3,3'-Dichlorobenzidine 0.0*22-121 0.0 20
Page 14 of 20* QC Fail Date:08/06/2021 04:43 PM
Page 44 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
V 92274-MS-V7186 V 92274-MSD-V7186Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.47 88.01.491.671.67<0.660mg/Kg2,4-Dichlorophenol 89.2 40-122 1.3 20
1.50 89.81.551.671.67<0.660mg/KgDiethyl phthalate 92.8 50-124 3.2 20
1.44 86.21.501.671.67<0.660mg/KgDimethyl phthalate 89.8 48-124 4.0 30
1.57 94.01.621.671.67<0.330mg/Kg2,4-Dimethylphenol 97.0 30-127 3.1 20
1.66 99.41.711.671.67<0.660mg/KgDi-n-butyl phthalate 102 51-128 2.9 20
1.41 0.0*1.451.671.67<1.50mg/Kg4,6-Dinitro-2-methylphenol 0.0*29-132 0.0 20
1.37 0.0*1.411.671.67<1.50mg/Kg2,4-Dinitrophenol 0.0*27-129 0.0 20
1.52 91.01.591.671.67<0.660mg/Kg2,4-Dinitrotoluene 95.2 48-126 4.5 20
1.58 94.61.631.671.67<0.660mg/Kg2,6-Dinitrotoluene 97.6 46-124 3.1 20
1.72 1031.821.671.67<0.330mg/KgDi-n-Octyl Phthalate 109 45-140 5.6 20
1.51 90.41.571.671.67<0.660mg/KgFluoranthene 94.0 50-127 3.8 20
1.50 89.81.561.671.67<0.660mg/KgFluorene 93.4 43-125 3.9 20
1.47 88.01.501.671.67<0.660mg/KgHexachlorobenzene 89.8 45-122 2.0 20
1.30 77.81.331.671.67<0.660mg/KgHexachlorobutadiene 79.6 32-123 2.2 20
1.16 69.41.161.671.67<0.660mg/KgHexachlorocyclopentadiene 69.4 32-117 0.0 20
1.19 71.21.141.671.67<0.660mg/KgHexachloroethane 68.2 28-117 4.2 20
1.50 89.81.541.671.67<0.660mg/KgIndeno(1,2,3-cd)pyrene 92.2 45-133 2.6 20
1.25 74.81.271.671.67<0.660mg/KgIsophorone 76.0 30-122 1.5 20
1.33 79.61.361.671.67<0.660mg/Kg1-Methylnaphthalene 81.4 40-119 2.2 20
1.34 80.21.381.671.67<0.660mg/Kg2-Methylnaphthalene 82.6 38-122 2.9 20
1.42 85.01.411.671.67<0.660mg/Kg2-Methylphenol 84.4 32-122 0.7 20
1.24 74.21.251.671.67<0.660mg/Kg3&4 Methylphenol 74.8 34-119 0.8 20
1.30 77.81.321.671.67<0.660mg/KgNaphthalene 79.0 35-123 1.5 20
1.49 89.21.531.671.67<0.660mg/Kg2-Nitroaniline 91.6 44-127 2.6 20
1.10 65.81.191.671.67<0.660mg/Kg3-Nitroaniline 71.2 33-119 7.8 20
1.20 71.81.251.671.67<0.330mg/Kg4-Nitroaniline 74.8 63-147 4.0 20
Page 15 of 20* QC Fail Date:08/06/2021 04:43 PM
Page 45 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V7307QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V7186
V 92274-MS-V7186 V 92274-MSD-V7186Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
1.28 76.61.271.671.67<0.330mg/KgNitrobenzene 76.0 34-122 0.7 20
1.32 79.01.341.671.67<0.660mg/Kg2-Nitrophenol 80.2 32-123 1.5 20
1.76 1051.771.671.67<0.660mg/Kg4-Nitrophenol 106 30-132 0.5 20
0.895 53.50.9011.671.67<0.660mg/KgN-Nitrosodimethylamine 53.9 10-146 0.6 30
1.83 1101.871.671.67<0.660mg/KgN-Nitrosodiphenylamine 112 38-127 2.1 20
1.32 79.01.301.671.67<0.660mg/KgN-Nitroso-di-n-propylamine 77.8 36-120 1.5 20
1.64 98.21.641.671.67<1.00mg/KgPentachlorophenol 98.2 25-133 0.0 20
1.50 89.81.541.671.67<0.660mg/KgPhenanthrene 92.2 50-121 2.6 20
1.35 80.81.331.671.67<0.660mg/KgPhenol 79.6 34-121 1.4 20
1.52 91.01.581.671.67<0.660mg/KgPyrene 94.6 47-127 3.8 20
0.347 20.70.3581.671.67<0.330mg/KgPyridine 21.4 10-80 3.1 20
1.27 76.01.271.671.67<0.660mg/Kg1,2,4-Trichlorobenzene 76.0 34-118 0.0 20
1.44 86.21.491.671.67<0.660mg/Kg2,4,5-Trichlorophenol 89.2 41-124 3.4 20
1.47 88.01.511.671.67<0.660mg/Kg2,4,6-Trichlorophenol 90.4 39-126 2.6 20
81.42-Fluorobiphenyl (S)84.4 44-115
80.42-Fluorophenol (S)79.2 35-115
74.2Nitrobenzene-d5 (S)74.8 37-122
89.24-Terphenyl-d14 (S)93.4 54-127
95.72,4,6-Tribromophenol (S)98.4 39-132
78.0Phenol-d5 (S)77.7 34-121
Page 16 of 20Date:08/06/2021 04:43 PM
Page 46 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V7110QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V7020
Associated Lab Samples: 92315, 92316, 92317
LRB-V7020 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/29/21 16:3351.0<51.0mg/KgAliphatic C19-C36
07/29/21 16:3351.0<51.0mg/KgAliphatic C9-C18
07/29/21 16:3351.0<51.0mg/KgAromatic C11-C22
07/29/21 16:332-Fluorobiphenyl (S)88.7 40-140
07/29/21 16:332-Bromonaphthalene (S)87.0 40-140
07/29/21 16:33Chlorooctadecane (S)71.0 40-140
07/29/21 16:33OTP Surrogate (S)74.0 40-140
LCS-V7020Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
84.767.279.3mg/KgAliphatic C19-C36 40-140
0.0*9.1359.5mg/KgAliphatic C9-C18 40-140
83.3140168mg/KgAromatic C11-C22 40-140
96.72-Fluorobiphenyl (S)40-140
98.72-Bromonaphthalene (S)40-140
73.2Chlorooctadecane (S)40-140
84.3OTP Surrogate (S)40-140
V 92202-MS-V7020 V 92202-MSD-V7020Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
66.9 83.262.379.880.4<50.3mg/KgAliphatic C19-C36 78.0 40-140 7.1 50
9.26 0.0*9.1859.960.3<50.3mg/KgAliphatic C9-C18 0.0*40-140 0.0 50
136 79.5110170171<50.3mg/KgAromatic C11-C22 64.7 40-140 21.1 50
92.72-Fluorobiphenyl (S)82.2 40-140
Page 17 of 20* QC Fail Date:08/06/2021 04:43 PM
Page 47 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V7110QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V7020
V 92202-MS-V7020 V 92202-MSD-V7020Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
94.52-Bromonaphthalene (S)83.2 40-140
68.1Chlorooctadecane (S)64.0 40-140
79.6OTP Surrogate (S)66.0 40-140
Page 18 of 20Date:08/06/2021 04:43 PM
Page 48 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V6882QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V6881
Associated Lab Samples: 92315, 92316, 92317
LRB-V6881 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
07/26/21 12:048.00<8.00mg/KgAliphatic C5-C8
07/26/21 12:048.00<8.00mg/KgAliphatic C9-C12
07/26/21 12:048.00<8.00mg/KgAromatic C9-C10
07/26/21 12:042,5-Dibromotoluene (FID) (S)104 70-130
07/26/21 12:042,5-Dibromotoluene (PID) (S)84.8 70-130
LCS-V6881 LCSD-V6881Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
38.6 12111536.932.0mg/KgAliphatic C5-C8 70-130 4.5 50
39.7 12412239.132.0mg/KgAliphatic C9-C12 70-130 1.5 50
9.98 93.290.79.7110.7mg/KgAromatic C9-C10 70-130 2.7 50
1201192,5-Dibromotoluene (FID) (S)70-130
98.198.12,5-Dibromotoluene (PID) (S)70-130
Page 19 of 20Date:08/06/2021 04:43 PM
Page 49 of 52
Quality Control Data
21-204-0040Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
Dry Weight Determination
SW-DRYWT
V7025QC Analytical Batch:
Analysis Method:
Analysis Description:
V 92287-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/28/21 17:134.937.335.5%Moisture
V 92316-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 07/28/21 17:136.515.714.7%Moisture
Page 20 of 20Date:08/06/2021 04:43 PM
Page 50 of 52
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-204-0040
Withers & Ravenel
01221
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 4.1 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:07/23/2021 16:02:34
Special precautions or instructions included?
Comments:
Page 51 of 52
Page 52 of 52

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

8/26/2021
Withers & Ravenel Matt James
115 Mackenan Dr. BUILDING 117 Cary, NC, 27511
Ref: Analytical Testing
Lab Report Number: 21-231-0011 Client Project Description: CC Newell Store
02172214.97
Dear Matt James:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 8/19/2021 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 62
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2021402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202199012State ProgramSouth Carolina
Page 1 of 1 00016/21-231-0011
Page 2 of 62
Report Number:
Sample Summary Table
Client Project Description:
21-231-0011
CC Newell Store
02172214.97
Lab No Client Sample ID Matrix Date Collected Date Received
08/17/2021 12:30Aqueous 93863 WR-6(TW)08/19/2021 14:00
08/17/2021 13:30Aqueous 93864 WR-7(TW)08/19/2021 14:00
08/17/2021 14:00Aqueous 93865 WR-8(TW)08/19/2021 14:00
08/17/2021 13:00Aqueous 93866 WR-9(TW)08/19/2021 14:00
08/17/2021 11:30Aqueous 93867 MW-6 08/19/2021 14:00
08/17/2021 11:20Aqueous 93868 Neighbor WSW 08/19/2021 14:00
Page 3 of 62
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
21-231-0011
Report Limit
Project:CC Newell Store
V 93863WR-6(TW)
13.7 08/23/2021 13:486200BAcetoneµg/L 10.0
1.73 08/23/2021 13:486200BEthylbenzeneµg/L 0.500
0.661 08/23/2021 13:486200B1,2,4-Trimethylbenzene µg/L 0.500
V 93866WR-9(TW)
0.616 08/23/2021 15:006200BDi-Isopropyl Ether (DIPE)µg/L 0.500
1.73 08/23/2021 15:006200BEthylbenzeneµg/L 0.500
2.69 08/23/2021 15:006200BMethyl tert-butyl ether (MTBE)µg/L 1.00
1.41 08/23/2021 15:006200B1,2,4-Trimethylbenzene µg/L 0.500
1.59 08/23/2021 15:006200Bm,p-Xylene µg/L 1.00
1.59 08/23/2021 15:006200BXylene (Total)µg/L 0.500
Page 4 of 62

Client: Withers & Ravenel CASE NARRATIVE
Project: CC Newell Store Lab Report Number: 21-231-0011
Date: 8/26/2021
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1 Sample 93864 (WR-7(TW)) QC Batch No: V8017/V7920
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory
Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix.
Sample 93865 (WR-8(TW))
QC Batch No: V8017/V7920 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due
to the sample matrix.
Analyte: Benzidine QC Batch No: V8017/V7920
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits for LCS/LCSD
Analyte: Benzoic Acid QC Batch No: V8017/V7920 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 11.9 ug/L which calculates to a recovery of 23.7% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V8017/V7920 Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was
13.7 ug/L which calculates to a recovery of 27.3% which is within the acceptable recovery range. Analyte: Hexachlorobutadiene QC Batch No: V8017/V7920
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 19.3 ug/L which calculates to a recovery of 38.5% which is within the acceptable recovery range.
Analyte: Hexachlorocyclopentadiene QC Batch No: V8017/V7920 Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 17.9 ug/L which calculates to a recovery of 34.8% which is within the acceptable recovery range.
Analyte: Hexachlorocyclopentadiene QC Batch No: V8017/V7920 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 17.0 ug/L which calculates to a recovery of 34% which is within the acceptable recovery range. Analyte: Pentachlorophenol
Page 5 of 62

QC Batch No: V8017/V7920
Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 41.4 ug/L which calculates to a recovery of 82.7% which is within the acceptable recovery range.
Analyte: Pentachlorophenol
QC Batch No: V8017/V7920 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
39.7 ug/L which calculates to a recovery of 79.3% which is within the acceptable recovery range.
Analyte: Phenol QC Batch No: V8017/V7920
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 8.98 ug/L which calculates to a recovery of 17.9% which is within the acceptable recovery range.
Massachusetts EPH Method MADEP-EPH QC Batch No: V8032 LCSD failed breakthrough test. Breakthrough was over 5%. However, LCS passed criteria. No further action
taken.
Analyte: 2-Bromonaphthalene QC Batch No: V8032/V7948
Surrogate recovery failed due to breakthrough on LCSD. LCS passed criteria. No further action taken. Sample 93863 (WR-6(TW)) Analyte: Chlorooctadecane
QC Batch No: V8032/V7948 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Sample 93864 (WR-7(TW)) Analyte: Chlorooctadecane
QC Batch No: V8032/V7948 Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix.
Page 6 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
13.7 µg/L 10.0Acetone 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Benzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Bromobenzene 1 08/23/21 13:48 6200BTBL
<1.00 µg/L 1.00Bromochloromethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Bromodichloromethane 1 08/23/21 13:48 6200BTBL
<5.00 µg/L 5.00Bromoform 1 08/23/21 13:48 6200BTBL
<1.00 µg/L 1.00Bromomethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500n-Butylbenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500sec-Butyl benzene 1 08/23/21 13:48 6200BTBL
<2.00 µg/L 2.00tert-Butyl benzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Carbon Tetrachloride 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Chlorobenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Chlorodibromomethane 1 08/23/21 13:48 6200BTBL
<1.00 µg/L 1.00Chloroethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Chloroform 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Chloromethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5002-Chlorotoluene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5004-Chlorotoluene 1 08/23/21 13:48 6200BTBL
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,2-Dibromoethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Dibromomethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 08/23/21 13:48 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 7 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 08/23/21 13:48 6200BTBL
<5.00 µg/L 5.00Dichlorodifluoromethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,2-Dichloroethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,2-Dichloropropane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,3-Dichloropropane 1 08/23/21 13:48 6200BTBL
<2.00 µg/L 2.002,2-Dichloropropane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,1-Dichloropropene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 08/23/21 13:48 6200BTBL
<200 µg/L 200Ethanol 1 08/23/21 13:48 6200BTBL
1.73 µg/L 0.500Ethylbenzene 1 08/23/21 13:48 6200BTBL
<3.00 µg/L 3.00Hexachlorobutadiene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Isopropylbenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5004-Isopropyl toluene 1 08/23/21 13:48 6200BTBL
<1.00 µg/L 1.002-Hexanone 1 08/23/21 13:48 6200BTBL
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 08/23/21 13:48 6200BTBL
<2.00 µg/L 2.00Methylene Chloride 1 08/23/21 13:48 6200BTBL
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 08/23/21 13:48 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 8 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 08/23/21 13:48 6200BTBL
<1.00 µg/L 1.00Naphthalene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500n-Propylbenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Styrene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Tetrachloroethene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Toluene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Trichloroethene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Trichlorofluoromethane 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 08/23/21 13:48 6200BTBL
0.661 µg/L 0.5001,2,4-Trimethylbenzene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 08/23/21 13:48 6200BTBL
<5.00 µg/L 5.00Vinyl Acetate 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500Vinyl Chloride 1 08/23/21 13:48 6200BTBL
<1.00 µg/L 1.00m,p-Xylene 1 08/23/21 13:48 6200BTBL
<0.500 µg/L 0.500o-Xylene 1 08/23/21 13:48 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 9 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 08/23/21 13:48 6200B
Surrogate: 4-Bromofluorobenzene 105 Limits: 70-130%08/23/21 13:481 TBL V7932
Surrogate: Dibromofluoromethane 98.4 Limits: 70-130%08/23/21 13:481 TBL V7932
Surrogate: 1,2-Dichloroethane - d4 95.6 Limits: 70-130%08/23/21 13:481 TBL V7932
Surrogate: Toluene-d8 99.8 Limits: 70-130%08/23/21 13:481 TBL V7932
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 10 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<10.3 µg/L 10.3Acenaphthene 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6Acenaphthylene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Anthracene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Benzidine 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Benzo(a)anthracene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Benzo(a)pyrene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Benzo(b)fluoranthene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Benzo(g,h,i)perylene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Benzo(k)fluoranthene 1 08/24/21 17:42 V8017JMV
<51.5 µg/L 51.5Benzoic Acid 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Benzyl alcohol 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Bis(2-Chloroethoxy)methane 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Bis(2-Chloroethyl)ether 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Bis(2-Chloroisopropyl)ether 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Bis(2-ethylhexyl)phthalate 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.64-Bromophenyl phenyl ether 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Butyl benzyl phthalate 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.34-Chloro-3-methylphenol 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.62-Chloronaphthalene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.32-Chlorophenol 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.64-Chlorophenyl phenyl ether 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Chrysene 1 08/24/21 17:42 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 11 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<20.6 µg/L 20.6Dibenz(a,h)anthracene 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6Dibenzofuran 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.31,2-Dichlorobenzene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.31,3-Dichlorobenzene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.31,4-Dichlorobenzene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.33,3'-Dichlorobenzidine 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.32,4-Dichlorophenol 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6Diethyl phthalate 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Dimethyl phthalate 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.62,4-Dimethylphenol 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Di-n-butyl phthalate 1 08/24/21 17:42 V8017JMV
<30.9 µg/L 30.94,6-Dinitro-2-methylphenol 1 08/24/21 17:42 V8017JMV
<30.9 µg/L 30.92,4-Dinitrophenol 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.32,4-Dinitrotoluene 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.62,6-Dinitrotoluene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Di-n-Octyl Phthalate 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Fluoranthene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Fluorene 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6Hexachlorobenzene 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6Hexachlorobutadiene 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6Hexachlorocyclopentadiene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Hexachloroethane 1 08/24/21 17:42 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 12 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<10.3 µg/L 10.3Indeno(1,2,3-cd)pyrene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Isophorone 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Naphthalene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Nitrobenzene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.32-Nitrophenol 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.34-Nitrophenol 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6N-Nitrosodiphenylamine 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.6N-Nitroso-di-n-propylamine 1 08/24/21 17:42 V8017JMV
<51.5 µg/L 51.5Pentachlorophenol 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Phenanthrene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Phenol 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.3Pyrene 1 08/24/21 17:42 V8017JMV
<10.3 µg/L 10.31,2,4-Trichlorobenzene 1 08/24/21 17:42 V8017JMV
<20.6 µg/L 20.62,4,6-Trichlorophenol 1 08/24/21 17:42 V8017JMV
Surrogate: Phenol-d5 19.1 Limits: 10-63%08/24/21 17:421 JMV V8017
Surrogate: 2-Fluorobiphenyl 57.9 Limits: 49-118%08/24/21 17:421 JMV V8017
Surrogate: 2-Fluorophenol 29.3 Limits: 22-84%08/24/21 17:421 JMV V8017
Surrogate: Nitrobenzene-d5 50.9 Limits: 43-123%08/24/21 17:421 JMV V8017
Surrogate: 4-Terphenyl-d14 88.9 Limits: 49-151%08/24/21 17:421 JMV V8017
Surrogate: 2,4,6-Tribromophenol 81.4 Limits: 31-144%08/24/21 17:421 JMV V8017
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 13 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-6(TW)
93863 Matrix:
8/17/2021 12:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V7948 08/24/21 09:45
<372 µg/L 372Aliphatic C9-C18 1 08/25/21 12:59 V8032ZRC
<532 µg/L 532Aliphatic C19-C36 1 08/25/21 12:59 V8032ZRC
<266 µg/L 266Aromatic C11-C22 1 08/25/21 12:59 V8032ZRC
Surrogate: 2-Bromonaphthalene 60.3 Limits: 40-140%08/25/21 12:591 ZRC V8032
Surrogate: Chlorooctadecane 37.7 *Limits: 40-140%08/25/21 12:591 ZRC V8032
Surrogate: OTP Surrogate 57.3 Limits: 40-140%08/25/21 12:591 ZRC V8032
Surrogate: 2-Fluorobiphenyl 83.3 Limits: 40-140%08/25/21 12:591 ZRC V8032
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V7802 08/20/21 08:00
<50.0 µg/L 50.0Aliphatic C5-C8 1 08/20/21 11:21 V7803TBL
<50.0 µg/L 50.0Aliphatic C9-C12 1 08/20/21 11:21 V7803TBL
<50.0 µg/L 50.0Aromatic C9-C10 1 08/20/21 11:21 V7803TBL
Surrogate: 2,5-Dibromotoluene (FID)105 Limits: 70-130%08/20/21 11:211 TBL V7803
Surrogate: 2,5-Dibromotoluene (PID)100 Limits: 70-130%08/20/21 11:211 TBL V7803
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 14 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Benzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Bromobenzene 1 08/23/21 14:12 6200BTBL
<1.00 µg/L 1.00Bromochloromethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Bromodichloromethane 1 08/23/21 14:12 6200BTBL
<5.00 µg/L 5.00Bromoform 1 08/23/21 14:12 6200BTBL
<1.00 µg/L 1.00Bromomethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500n-Butylbenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500sec-Butyl benzene 1 08/23/21 14:12 6200BTBL
<2.00 µg/L 2.00tert-Butyl benzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Carbon Tetrachloride 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Chlorobenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Chlorodibromomethane 1 08/23/21 14:12 6200BTBL
<1.00 µg/L 1.00Chloroethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Chloroform 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Chloromethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5002-Chlorotoluene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5004-Chlorotoluene 1 08/23/21 14:12 6200BTBL
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2-Dibromoethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Dibromomethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 08/23/21 14:12 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 15 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 08/23/21 14:12 6200BTBL
<5.00 µg/L 5.00Dichlorodifluoromethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2-Dichloroethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2-Dichloropropane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,3-Dichloropropane 1 08/23/21 14:12 6200BTBL
<2.00 µg/L 2.002,2-Dichloropropane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,1-Dichloropropene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 08/23/21 14:12 6200BTBL
<200 µg/L 200Ethanol 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Ethylbenzene 1 08/23/21 14:12 6200BTBL
<3.00 µg/L 3.00Hexachlorobutadiene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Isopropylbenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5004-Isopropyl toluene 1 08/23/21 14:12 6200BTBL
<1.00 µg/L 1.002-Hexanone 1 08/23/21 14:12 6200BTBL
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 08/23/21 14:12 6200BTBL
<2.00 µg/L 2.00Methylene Chloride 1 08/23/21 14:12 6200BTBL
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 08/23/21 14:12 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 16 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 08/23/21 14:12 6200BTBL
<1.00 µg/L 1.00Naphthalene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500n-Propylbenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Styrene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Tetrachloroethene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Toluene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Trichloroethene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Trichlorofluoromethane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 08/23/21 14:12 6200BTBL
<5.00 µg/L 5.00Vinyl Acetate 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500Vinyl Chloride 1 08/23/21 14:12 6200BTBL
<1.00 µg/L 1.00m,p-Xylene 1 08/23/21 14:12 6200BTBL
<0.500 µg/L 0.500o-Xylene 1 08/23/21 14:12 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 17 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 08/23/21 14:12 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%08/23/21 14:121 TBL V7932
Surrogate: Dibromofluoromethane 97.8 Limits: 70-130%08/23/21 14:121 TBL V7932
Surrogate: 1,2-Dichloroethane - d4 95.4 Limits: 70-130%08/23/21 14:121 TBL V7932
Surrogate: Toluene-d8 101 Limits: 70-130%08/23/21 14:121 TBL V7932
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 18 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<10.3 µg/L 10.3Acenaphthene 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6Acenaphthylene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Anthracene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Benzidine 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Benzo(a)anthracene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Benzo(a)pyrene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Benzo(b)fluoranthene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Benzo(g,h,i)perylene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Benzo(k)fluoranthene 1 08/24/21 18:26 V8017JMV
<51.5 µg/L 51.5Benzoic Acid 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Benzyl alcohol 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Bis(2-Chloroethoxy)methane 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Bis(2-Chloroethyl)ether 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Bis(2-Chloroisopropyl)ether 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Bis(2-ethylhexyl)phthalate 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.64-Bromophenyl phenyl ether 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Butyl benzyl phthalate 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.34-Chloro-3-methylphenol 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.62-Chloronaphthalene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.32-Chlorophenol 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.64-Chlorophenyl phenyl ether 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Chrysene 1 08/24/21 18:26 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 19 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<20.6 µg/L 20.6Dibenz(a,h)anthracene 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6Dibenzofuran 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.31,2-Dichlorobenzene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.31,3-Dichlorobenzene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.31,4-Dichlorobenzene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.33,3'-Dichlorobenzidine 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.32,4-Dichlorophenol 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6Diethyl phthalate 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Dimethyl phthalate 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.62,4-Dimethylphenol 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Di-n-butyl phthalate 1 08/24/21 18:26 V8017JMV
<30.9 µg/L 30.94,6-Dinitro-2-methylphenol 1 08/24/21 18:26 V8017JMV
<30.9 µg/L 30.92,4-Dinitrophenol 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.32,4-Dinitrotoluene 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.62,6-Dinitrotoluene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Di-n-Octyl Phthalate 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Fluoranthene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Fluorene 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6Hexachlorobenzene 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6Hexachlorobutadiene 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6Hexachlorocyclopentadiene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Hexachloroethane 1 08/24/21 18:26 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 20 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<10.3 µg/L 10.3Indeno(1,2,3-cd)pyrene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Isophorone 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Naphthalene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Nitrobenzene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.32-Nitrophenol 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.34-Nitrophenol 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6N-Nitrosodiphenylamine 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.6N-Nitroso-di-n-propylamine 1 08/24/21 18:26 V8017JMV
<51.5 µg/L 51.5Pentachlorophenol 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Phenanthrene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Phenol 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.3Pyrene 1 08/24/21 18:26 V8017JMV
<10.3 µg/L 10.31,2,4-Trichlorobenzene 1 08/24/21 18:26 V8017JMV
<20.6 µg/L 20.62,4,6-Trichlorophenol 1 08/24/21 18:26 V8017JMV
Surrogate: Phenol-d5 6.00 *Limits: 10-63%08/24/21 18:261 JMV V8017
Surrogate: 2-Fluorobiphenyl 34.4 *Limits: 49-118%08/24/21 18:261 JMV V8017
Surrogate: 2-Fluorophenol 8.69 *Limits: 22-84%08/24/21 18:261 JMV V8017
Surrogate: Nitrobenzene-d5 30.7 *Limits: 43-123%08/24/21 18:261 JMV V8017
Surrogate: 4-Terphenyl-d14 42.7 *Limits: 49-151%08/24/21 18:261 JMV V8017
Surrogate: 2,4,6-Tribromophenol 21.3 *Limits: 31-144%08/24/21 18:261 JMV V8017
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 21 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-7(TW)
93864 Matrix:
8/17/2021 13:30
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V7948 08/24/21 09:45
<368 µg/L 368Aliphatic C9-C18 1 08/25/21 13:35 V8032ZRC
<526 µg/L 526Aliphatic C19-C36 1 08/25/21 13:35 V8032ZRC
<263 µg/L 263Aromatic C11-C22 1 08/25/21 13:35 V8032ZRC
Surrogate: 2-Bromonaphthalene 77.9 Limits: 40-140%08/25/21 13:351 ZRC V8032
Surrogate: Chlorooctadecane 36.6 *Limits: 40-140%08/25/21 13:351 ZRC V8032
Surrogate: OTP Surrogate 78.7 Limits: 40-140%08/25/21 13:351 ZRC V8032
Surrogate: 2-Fluorobiphenyl 85.0 Limits: 40-140%08/25/21 13:351 ZRC V8032
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V7802 08/20/21 08:00
<50.0 µg/L 50.0Aliphatic C5-C8 1 08/20/21 11:46 V7803TBL
<50.0 µg/L 50.0Aliphatic C9-C12 1 08/20/21 11:46 V7803TBL
<50.0 µg/L 50.0Aromatic C9-C10 1 08/20/21 11:46 V7803TBL
Surrogate: 2,5-Dibromotoluene (FID)111 Limits: 70-130%08/20/21 11:461 TBL V7803
Surrogate: 2,5-Dibromotoluene (PID)107 Limits: 70-130%08/20/21 11:461 TBL V7803
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 22 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Benzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Bromobenzene 1 08/23/21 14:35 6200BTBL
<1.00 µg/L 1.00Bromochloromethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Bromodichloromethane 1 08/23/21 14:35 6200BTBL
<5.00 µg/L 5.00Bromoform 1 08/23/21 14:35 6200BTBL
<1.00 µg/L 1.00Bromomethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500n-Butylbenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500sec-Butyl benzene 1 08/23/21 14:35 6200BTBL
<2.00 µg/L 2.00tert-Butyl benzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Carbon Tetrachloride 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Chlorobenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Chlorodibromomethane 1 08/23/21 14:35 6200BTBL
<1.00 µg/L 1.00Chloroethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Chloroform 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Chloromethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5002-Chlorotoluene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5004-Chlorotoluene 1 08/23/21 14:35 6200BTBL
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2-Dibromoethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Dibromomethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 08/23/21 14:35 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 23 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 08/23/21 14:35 6200BTBL
<5.00 µg/L 5.00Dichlorodifluoromethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2-Dichloroethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2-Dichloropropane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,3-Dichloropropane 1 08/23/21 14:35 6200BTBL
<2.00 µg/L 2.002,2-Dichloropropane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,1-Dichloropropene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 08/23/21 14:35 6200BTBL
<200 µg/L 200Ethanol 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Ethylbenzene 1 08/23/21 14:35 6200BTBL
<3.00 µg/L 3.00Hexachlorobutadiene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Isopropylbenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5004-Isopropyl toluene 1 08/23/21 14:35 6200BTBL
<1.00 µg/L 1.002-Hexanone 1 08/23/21 14:35 6200BTBL
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 08/23/21 14:35 6200BTBL
<2.00 µg/L 2.00Methylene Chloride 1 08/23/21 14:35 6200BTBL
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 08/23/21 14:35 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 24 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 08/23/21 14:35 6200BTBL
<1.00 µg/L 1.00Naphthalene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500n-Propylbenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Styrene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Tetrachloroethene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Toluene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Trichloroethene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Trichlorofluoromethane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 08/23/21 14:35 6200BTBL
<5.00 µg/L 5.00Vinyl Acetate 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500Vinyl Chloride 1 08/23/21 14:35 6200BTBL
<1.00 µg/L 1.00m,p-Xylene 1 08/23/21 14:35 6200BTBL
<0.500 µg/L 0.500o-Xylene 1 08/23/21 14:35 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 25 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 08/23/21 14:35 6200B
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%08/23/21 14:351 TBL V7932
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%08/23/21 14:351 TBL V7932
Surrogate: 1,2-Dichloroethane - d4 95.8 Limits: 70-130%08/23/21 14:351 TBL V7932
Surrogate: Toluene-d8 101 Limits: 70-130%08/23/21 14:351 TBL V7932
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 26 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<11.1 µg/L 11.1Acenaphthene 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2Acenaphthylene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Anthracene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Benzidine 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Benzo(a)anthracene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Benzo(a)pyrene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Benzo(b)fluoranthene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Benzo(g,h,i)perylene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Benzo(k)fluoranthene 1 08/24/21 18:49 V8017JMV
<55.6 µg/L 55.6Benzoic Acid 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Benzyl alcohol 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Bis(2-Chloroethoxy)methane 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Bis(2-Chloroethyl)ether 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Bis(2-Chloroisopropyl)ether 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Bis(2-ethylhexyl)phthalate 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.24-Bromophenyl phenyl ether 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Butyl benzyl phthalate 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.14-Chloro-3-methylphenol 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.22-Chloronaphthalene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.12-Chlorophenol 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.24-Chlorophenyl phenyl ether 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Chrysene 1 08/24/21 18:49 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 27 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<22.2 µg/L 22.2Dibenz(a,h)anthracene 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2Dibenzofuran 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.11,2-Dichlorobenzene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.11,3-Dichlorobenzene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.11,4-Dichlorobenzene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.13,3'-Dichlorobenzidine 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.12,4-Dichlorophenol 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2Diethyl phthalate 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Dimethyl phthalate 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.22,4-Dimethylphenol 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Di-n-butyl phthalate 1 08/24/21 18:49 V8017JMV
<33.3 µg/L 33.34,6-Dinitro-2-methylphenol 1 08/24/21 18:49 V8017JMV
<33.3 µg/L 33.32,4-Dinitrophenol 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.12,4-Dinitrotoluene 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.22,6-Dinitrotoluene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Di-n-Octyl Phthalate 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Fluoranthene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Fluorene 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2Hexachlorobenzene 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2Hexachlorobutadiene 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2Hexachlorocyclopentadiene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Hexachloroethane 1 08/24/21 18:49 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 28 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<11.1 µg/L 11.1Indeno(1,2,3-cd)pyrene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Isophorone 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Naphthalene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Nitrobenzene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.12-Nitrophenol 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.14-Nitrophenol 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2N-Nitrosodiphenylamine 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.2N-Nitroso-di-n-propylamine 1 08/24/21 18:49 V8017JMV
<55.6 µg/L 55.6Pentachlorophenol 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Phenanthrene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Phenol 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.1Pyrene 1 08/24/21 18:49 V8017JMV
<11.1 µg/L 11.11,2,4-Trichlorobenzene 1 08/24/21 18:49 V8017JMV
<22.2 µg/L 22.22,4,6-Trichlorophenol 1 08/24/21 18:49 V8017JMV
Surrogate: Phenol-d5 3.41 *Limits: 10-63%08/24/21 18:491 JMV V8017
Surrogate: 2-Fluorobiphenyl 30.2 *Limits: 49-118%08/24/21 18:491 JMV V8017
Surrogate: 2-Fluorophenol 4.47 *Limits: 22-84%08/24/21 18:491 JMV V8017
Surrogate: Nitrobenzene-d5 25.5 *Limits: 43-123%08/24/21 18:491 JMV V8017
Surrogate: 4-Terphenyl-d14 37.6 *Limits: 49-151%08/24/21 18:491 JMV V8017
Surrogate: 2,4,6-Tribromophenol 11.4 *Limits: 31-144%08/24/21 18:491 JMV V8017
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 29 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-8(TW)
93865 Matrix:
8/17/2021 14:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V7802 08/20/21 08:00
<50.0 µg/L 50.0Aliphatic C5-C8 1 08/20/21 12:10 V7803TBL
<50.0 µg/L 50.0Aliphatic C9-C12 1 08/20/21 12:10 V7803TBL
<50.0 µg/L 50.0Aromatic C9-C10 1 08/20/21 12:10 V7803TBL
Surrogate: 2,5-Dibromotoluene (FID)92.8 Limits: 70-130%08/20/21 12:101 TBL V7803
Surrogate: 2,5-Dibromotoluene (PID)89.1 Limits: 70-130%08/20/21 12:101 TBL V7803
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 30 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Benzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Bromobenzene 1 08/23/21 15:00 6200BTBL
<1.00 µg/L 1.00Bromochloromethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Bromodichloromethane 1 08/23/21 15:00 6200BTBL
<5.00 µg/L 5.00Bromoform 1 08/23/21 15:00 6200BTBL
<1.00 µg/L 1.00Bromomethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500n-Butylbenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500sec-Butyl benzene 1 08/23/21 15:00 6200BTBL
<2.00 µg/L 2.00tert-Butyl benzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Carbon Tetrachloride 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Chlorobenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Chlorodibromomethane 1 08/23/21 15:00 6200BTBL
<1.00 µg/L 1.00Chloroethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Chloroform 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Chloromethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5002-Chlorotoluene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5004-Chlorotoluene 1 08/23/21 15:00 6200BTBL
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,2-Dibromoethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Dibromomethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 08/23/21 15:00 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 31 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 08/23/21 15:00 6200BTBL
<5.00 µg/L 5.00Dichlorodifluoromethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,2-Dichloroethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,2-Dichloropropane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,3-Dichloropropane 1 08/23/21 15:00 6200BTBL
<2.00 µg/L 2.002,2-Dichloropropane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,1-Dichloropropene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 08/23/21 15:00 6200BTBL
<200 µg/L 200Ethanol 1 08/23/21 15:00 6200BTBL
1.73 µg/L 0.500Ethylbenzene 1 08/23/21 15:00 6200BTBL
<3.00 µg/L 3.00Hexachlorobutadiene 1 08/23/21 15:00 6200BTBL
0.616 µg/L 0.500Di-Isopropyl Ether (DIPE)1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Isopropylbenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5004-Isopropyl toluene 1 08/23/21 15:00 6200BTBL
<1.00 µg/L 1.002-Hexanone 1 08/23/21 15:00 6200BTBL
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 08/23/21 15:00 6200BTBL
<2.00 µg/L 2.00Methylene Chloride 1 08/23/21 15:00 6200BTBL
2.69 µg/L 1.00Methyl tert-butyl ether (MTBE)1 08/23/21 15:00 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 32 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 08/23/21 15:00 6200BTBL
<1.00 µg/L 1.00Naphthalene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500n-Propylbenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Styrene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Tetrachloroethene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Toluene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Trichloroethene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Trichlorofluoromethane 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 08/23/21 15:00 6200BTBL
1.41 µg/L 0.5001,2,4-Trimethylbenzene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 08/23/21 15:00 6200BTBL
<5.00 µg/L 5.00Vinyl Acetate 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500Vinyl Chloride 1 08/23/21 15:00 6200BTBL
1.59 µg/L 1.00m,p-Xylene 1 08/23/21 15:00 6200BTBL
<0.500 µg/L 0.500o-Xylene 1 08/23/21 15:00 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 33 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
1.59 µg/L 0.500Xylene (Total)1 08/23/21 15:00 6200B
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%08/23/21 15:001 TBL V7932
Surrogate: Dibromofluoromethane 97.0 Limits: 70-130%08/23/21 15:001 TBL V7932
Surrogate: 1,2-Dichloroethane - d4 94.0 Limits: 70-130%08/23/21 15:001 TBL V7932
Surrogate: Toluene-d8 99.0 Limits: 70-130%08/23/21 15:001 TBL V7932
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 34 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<10.2 µg/L 10.2Acenaphthene 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4Acenaphthylene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Anthracene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Benzidine 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Benzo(a)anthracene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Benzo(a)pyrene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Benzo(b)fluoranthene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Benzo(g,h,i)perylene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Benzo(k)fluoranthene 1 08/24/21 18:04 V8017JMV
<51.0 µg/L 51.0Benzoic Acid 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Benzyl alcohol 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Bis(2-Chloroethoxy)methane 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Bis(2-Chloroethyl)ether 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Bis(2-Chloroisopropyl)ether 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Bis(2-ethylhexyl)phthalate 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.44-Bromophenyl phenyl ether 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Butyl benzyl phthalate 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.24-Chloro-3-methylphenol 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.42-Chloronaphthalene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.22-Chlorophenol 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.44-Chlorophenyl phenyl ether 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Chrysene 1 08/24/21 18:04 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 35 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<20.4 µg/L 20.4Dibenz(a,h)anthracene 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4Dibenzofuran 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.21,2-Dichlorobenzene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.21,3-Dichlorobenzene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.21,4-Dichlorobenzene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.23,3'-Dichlorobenzidine 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.22,4-Dichlorophenol 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4Diethyl phthalate 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Dimethyl phthalate 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.42,4-Dimethylphenol 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Di-n-butyl phthalate 1 08/24/21 18:04 V8017JMV
<30.6 µg/L 30.64,6-Dinitro-2-methylphenol 1 08/24/21 18:04 V8017JMV
<30.6 µg/L 30.62,4-Dinitrophenol 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.22,4-Dinitrotoluene 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.42,6-Dinitrotoluene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Di-n-Octyl Phthalate 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Fluoranthene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Fluorene 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4Hexachlorobenzene 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4Hexachlorobutadiene 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4Hexachlorocyclopentadiene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Hexachloroethane 1 08/24/21 18:04 V8017JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 36 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V7920 08/23/21 10:15
<10.2 µg/L 10.2Indeno(1,2,3-cd)pyrene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Isophorone 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Naphthalene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Nitrobenzene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.22-Nitrophenol 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.24-Nitrophenol 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4N-Nitrosodiphenylamine 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.4N-Nitroso-di-n-propylamine 1 08/24/21 18:04 V8017JMV
<51.0 µg/L 51.0Pentachlorophenol 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Phenanthrene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Phenol 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.2Pyrene 1 08/24/21 18:04 V8017JMV
<10.2 µg/L 10.21,2,4-Trichlorobenzene 1 08/24/21 18:04 V8017JMV
<20.4 µg/L 20.42,4,6-Trichlorophenol 1 08/24/21 18:04 V8017JMV
Surrogate: Phenol-d5 19.3 Limits: 10-63%08/24/21 18:041 JMV V8017
Surrogate: 2-Fluorobiphenyl 70.0 Limits: 49-118%08/24/21 18:041 JMV V8017
Surrogate: 2-Fluorophenol 30.0 Limits: 22-84%08/24/21 18:041 JMV V8017
Surrogate: Nitrobenzene-d5 60.8 Limits: 43-123%08/24/21 18:041 JMV V8017
Surrogate: 4-Terphenyl-d14 85.9 Limits: 49-151%08/24/21 18:041 JMV V8017
Surrogate: 2,4,6-Tribromophenol 86.0 Limits: 31-144%08/24/21 18:041 JMV V8017
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 37 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:WR-9(TW)
93866 Matrix:
8/17/2021 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V7948 08/24/21 09:45
<350 µg/L 350Aliphatic C9-C18 1 08/25/21 14:12 V8032ZRC
<500 µg/L 500Aliphatic C19-C36 1 08/25/21 14:12 V8032ZRC
<250 µg/L 250Aromatic C11-C22 1 08/25/21 14:12 V8032ZRC
Surrogate: 2-Bromonaphthalene 72.8 Limits: 40-140%08/25/21 14:121 ZRC V8032
Surrogate: Chlorooctadecane 53.0 Limits: 40-140%08/25/21 14:121 ZRC V8032
Surrogate: OTP Surrogate 63.5 Limits: 40-140%08/25/21 14:121 ZRC V8032
Surrogate: 2-Fluorobiphenyl 82.0 Limits: 40-140%08/25/21 14:121 ZRC V8032
Analytical Method:
Prep Method:
Test Results Units MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V7802 08/20/21 08:00
<50.0 µg/L 50.0Aliphatic C5-C8 1 08/20/21 12:34 V7803TBL
<50.0 µg/L 50.0Aliphatic C9-C12 1 08/20/21 12:34 V7803TBL
<50.0 µg/L 50.0Aromatic C9-C10 1 08/20/21 12:34 V7803TBL
Surrogate: 2,5-Dibromotoluene (FID)100 Limits: 70-130%08/20/21 12:341 TBL V7803
Surrogate: 2,5-Dibromotoluene (PID)96.0 Limits: 70-130%08/20/21 12:341 TBL V7803
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQL
Page 38 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:MW-6
93867 Matrix:
8/17/2021 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Benzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Bromobenzene 1 08/23/21 15:24 6200BTBL
<1.00 µg/L 1.00Bromochloromethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Bromodichloromethane 1 08/23/21 15:24 6200BTBL
<5.00 µg/L 5.00Bromoform 1 08/23/21 15:24 6200BTBL
<1.00 µg/L 1.00Bromomethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500n-Butylbenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500sec-Butyl benzene 1 08/23/21 15:24 6200BTBL
<2.00 µg/L 2.00tert-Butyl benzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Carbon Tetrachloride 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Chlorobenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Chlorodibromomethane 1 08/23/21 15:24 6200BTBL
<1.00 µg/L 1.00Chloroethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Chloroform 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Chloromethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5002-Chlorotoluene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5004-Chlorotoluene 1 08/23/21 15:24 6200BTBL
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2-Dibromoethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Dibromomethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 08/23/21 15:24 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 39 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:MW-6
93867 Matrix:
8/17/2021 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 08/23/21 15:24 6200BTBL
<5.00 µg/L 5.00Dichlorodifluoromethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2-Dichloroethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2-Dichloropropane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,3-Dichloropropane 1 08/23/21 15:24 6200BTBL
<2.00 µg/L 2.002,2-Dichloropropane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,1-Dichloropropene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 08/23/21 15:24 6200BTBL
<200 µg/L 200Ethanol 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Ethylbenzene 1 08/23/21 15:24 6200BTBL
<3.00 µg/L 3.00Hexachlorobutadiene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Isopropylbenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5004-Isopropyl toluene 1 08/23/21 15:24 6200BTBL
<1.00 µg/L 1.002-Hexanone 1 08/23/21 15:24 6200BTBL
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 08/23/21 15:24 6200BTBL
<2.00 µg/L 2.00Methylene Chloride 1 08/23/21 15:24 6200BTBL
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 08/23/21 15:24 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 40 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:MW-6
93867 Matrix:
8/17/2021 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 08/23/21 15:24 6200BTBL
<1.00 µg/L 1.00Naphthalene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500n-Propylbenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Styrene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Tetrachloroethene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Toluene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Trichloroethene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Trichlorofluoromethane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 08/23/21 15:24 6200BTBL
<5.00 µg/L 5.00Vinyl Acetate 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500Vinyl Chloride 1 08/23/21 15:24 6200BTBL
<1.00 µg/L 1.00m,p-Xylene 1 08/23/21 15:24 6200BTBL
<0.500 µg/L 0.500o-Xylene 1 08/23/21 15:24 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 41 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:MW-6
93867 Matrix:
8/17/2021 11:30
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 08/23/21 15:24 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%08/23/21 15:241 TBL V7932
Surrogate: Dibromofluoromethane 97.2 Limits: 70-130%08/23/21 15:241 TBL V7932
Surrogate: 1,2-Dichloroethane - d4 93.8 Limits: 70-130%08/23/21 15:241 TBL V7932
Surrogate: Toluene-d8 101 Limits: 70-130%08/23/21 15:241 TBL V7932
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 42 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:Neighbor WSW
93868 Matrix:
8/17/2021 11:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0Acetone 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Benzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Bromobenzene 1 08/23/21 15:48 6200BTBL
<1.00 µg/L 1.00Bromochloromethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Bromodichloromethane 1 08/23/21 15:48 6200BTBL
<5.00 µg/L 5.00Bromoform 1 08/23/21 15:48 6200BTBL
<1.00 µg/L 1.00Bromomethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500n-Butylbenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500sec-Butyl benzene 1 08/23/21 15:48 6200BTBL
<2.00 µg/L 2.00tert-Butyl benzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Carbon Tetrachloride 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Chlorobenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Chlorodibromomethane 1 08/23/21 15:48 6200BTBL
<1.00 µg/L 1.00Chloroethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Chloroform 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Chloromethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5002-Chlorotoluene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5004-Chlorotoluene 1 08/23/21 15:48 6200BTBL
<2.00 µg/L 2.001,2-Dibromo-3-Chloropropane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2-Dibromoethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Dibromomethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2-Dichlorobenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,3-Dichlorobenzene 1 08/23/21 15:48 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 43 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:Neighbor WSW
93868 Matrix:
8/17/2021 11:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.5001,4-Dichlorobenzene 1 08/23/21 15:48 6200BTBL
<5.00 µg/L 5.00Dichlorodifluoromethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2-Dichloroethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,1-Dichloroethene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500cis-1,2-Dichloroethene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500trans-1,2-Dichloroethene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2-Dichloropropane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,3-Dichloropropane 1 08/23/21 15:48 6200BTBL
<2.00 µg/L 2.002,2-Dichloropropane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,1-Dichloropropene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500cis-1,3-Dichloropropene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500trans-1,3-Dichloropropene 1 08/23/21 15:48 6200BTBL
<200 µg/L 200Ethanol 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Ethylbenzene 1 08/23/21 15:48 6200BTBL
<3.00 µg/L 3.00Hexachlorobutadiene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Di-Isopropyl Ether (DIPE)1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Isopropylbenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5004-Isopropyl toluene 1 08/23/21 15:48 6200BTBL
<1.00 µg/L 1.002-Hexanone 1 08/23/21 15:48 6200BTBL
<5.00 µg/L 5.00Methyl Ethyl Ketone (MEK)1 08/23/21 15:48 6200BTBL
<2.00 µg/L 2.00Methylene Chloride 1 08/23/21 15:48 6200BTBL
<1.00 µg/L 1.00Methyl tert-butyl ether (MTBE)1 08/23/21 15:48 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 44 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:Neighbor WSW
93868 Matrix:
8/17/2021 11:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.004-Methyl-2-Pentanone 1 08/23/21 15:48 6200BTBL
<1.00 µg/L 1.00Naphthalene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500n-Propylbenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Styrene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,1,1,2-Tetrachloroethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,1,2,2-Tetrachloroethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Tetrachloroethene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Toluene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichlorobenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2,4-Trichlorobenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,1,1-Trichloroethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,1,2-Trichloroethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Trichloroethene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Trichlorofluoromethane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2,3-Trichloropropane 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,2,4-Trimethylbenzene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.5001,3,5-Trimethylbenzene 1 08/23/21 15:48 6200BTBL
<5.00 µg/L 5.00Vinyl Acetate 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500Vinyl Chloride 1 08/23/21 15:48 6200BTBL
<1.00 µg/L 1.00m,p-Xylene 1 08/23/21 15:48 6200BTBL
<0.500 µg/L 0.500o-Xylene 1 08/23/21 15:48 6200BTBL
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 45 of 62
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 27511
21-231-0011
01221
Withers & Ravenel
115 Mackenan Dr. BUILDING 117
Matt James
Cary
02172214.97 Received : 08/19/2021
CC Newell Store
Report Date : 08/26/2021
Sample ID :
Lab No :
Sampled:Neighbor WSW
93868 Matrix:
8/17/2021 11:20
Aqueous
Test Results Units MQL By Analytical
Method
Date / Time
Analyzed
DF
<0.500 µg/L 0.500Xylene (Total)1 08/23/21 15:48 6200B
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%08/23/21 15:481 TBL V7932
Surrogate: Dibromofluoromethane 99.2 Limits: 70-130%08/23/21 15:481 TBL V7932
Surrogate: 1,2-Dichloroethane - d4 96.4 Limits: 70-130%08/23/21 15:481 TBL V7932
Surrogate: Toluene-d8 102 Limits: 70-130%08/23/21 15:481 TBL V7932
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLLimit ExceededL
Page 46 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V7932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V7931
Associated Lab Samples: 93863, 93864, 93865, 93866, 93867, 93868
LRB-V7931 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/23/21 12:3510.0< 10.0µg/LAcetone
08/23/21 12:350.500< 0.500µg/LBenzene
08/23/21 12:350.500< 0.500µg/LBromobenzene
08/23/21 12:351.00< 1.00µg/LBromochloromethane
08/23/21 12:350.500< 0.500µg/LBromodichloromethane
08/23/21 12:355.00< 5.00µg/LBromoform
08/23/21 12:351.00< 1.00µg/LBromomethane
08/23/21 12:350.500< 0.500µg/Ln-Butylbenzene
08/23/21 12:350.500< 0.500µg/Lsec-Butyl benzene
08/23/21 12:352.00< 2.00µg/Ltert-Butyl benzene
08/23/21 12:350.500< 0.500µg/LCarbon Tetrachloride
08/23/21 12:350.500< 0.500µg/LChlorobenzene
08/23/21 12:350.500< 0.500µg/LChlorodibromomethane
08/23/21 12:351.00< 1.00µg/LChloroethane
08/23/21 12:350.500< 0.500µg/LChloroform
08/23/21 12:350.500< 0.500µg/LChloromethane
08/23/21 12:350.500< 0.500µg/L2-Chlorotoluene
08/23/21 12:350.500< 0.500µg/L4-Chlorotoluene
08/23/21 12:352.00< 2.00µg/L1,2-Dibromo-3-Chloropropane
08/23/21 12:350.500< 0.500µg/L1,2-Dibromoethane
08/23/21 12:350.500< 0.500µg/LDibromomethane
08/23/21 12:350.500< 0.500µg/L1,2-Dichlorobenzene
08/23/21 12:350.500< 0.500µg/L1,3-Dichlorobenzene
08/23/21 12:350.500< 0.500µg/L1,4-Dichlorobenzene
08/23/21 12:355.00< 5.00µg/LDichlorodifluoromethane
08/23/21 12:350.500< 0.500µg/L1,1-Dichloroethane
08/23/21 12:350.500< 0.500µg/L1,2-Dichloroethane
Page 1 of 14Date:08/26/2021 02:39 PM
Page 47 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V7932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V7931
Associated Lab Samples: 93863, 93864, 93865, 93866, 93867, 93868
LRB-V7931 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/23/21 12:350.500< 0.500µg/L1,1-Dichloroethene
08/23/21 12:350.500< 0.500µg/Lcis-1,2-Dichloroethene
08/23/21 12:350.500< 0.500µg/Ltrans-1,2-Dichloroethene
08/23/21 12:350.500< 0.500µg/L1,2-Dichloropropane
08/23/21 12:350.500< 0.500µg/L1,3-Dichloropropane
08/23/21 12:352.00< 2.00µg/L2,2-Dichloropropane
08/23/21 12:350.500< 0.500µg/L1,1-Dichloropropene
08/23/21 12:350.500< 0.500µg/Lcis-1,3-Dichloropropene
08/23/21 12:350.500< 0.500µg/Ltrans-1,3-Dichloropropene
08/23/21 12:35200< 200µg/LEthanol
08/23/21 12:350.500< 0.500µg/LEthylbenzene
08/23/21 12:353.00< 3.00µg/LHexachlorobutadiene
08/23/21 12:350.500< 0.500µg/LDi-Isopropyl Ether (DIPE)
08/23/21 12:350.500< 0.500µg/LIsopropylbenzene
08/23/21 12:350.500< 0.500µg/L4-Isopropyl toluene
08/23/21 12:351.00< 1.00µg/L2-Hexanone
08/23/21 12:355.00< 5.00µg/LMethyl Ethyl Ketone (MEK)
08/23/21 12:352.00< 2.00µg/LMethylene Chloride
08/23/21 12:351.00< 1.00µg/LMethyl tert-butyl ether (MTBE)
08/23/21 12:351.00< 1.00µg/L4-Methyl-2-Pentanone
08/23/21 12:351.00< 1.00µg/LNaphthalene
08/23/21 12:350.500< 0.500µg/Ln-Propylbenzene
08/23/21 12:350.500< 0.500µg/LStyrene
08/23/21 12:350.500< 0.500µg/L1,1,1,2-Tetrachloroethane
08/23/21 12:350.500< 0.500µg/L1,1,2,2-Tetrachloroethane
08/23/21 12:350.500< 0.500µg/LTetrachloroethene
08/23/21 12:350.500< 0.500µg/LToluene
Page 2 of 14Date:08/26/2021 02:39 PM
Page 48 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V7932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V7931
Associated Lab Samples: 93863, 93864, 93865, 93866, 93867, 93868
LRB-V7931 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/23/21 12:350.500< 0.500µg/L1,2,3-Trichlorobenzene
08/23/21 12:350.500< 0.500µg/L1,2,4-Trichlorobenzene
08/23/21 12:350.500< 0.500µg/L1,1,1-Trichloroethane
08/23/21 12:350.500< 0.500µg/L1,1,2-Trichloroethane
08/23/21 12:350.500< 0.500µg/LTrichloroethene
08/23/21 12:350.500< 0.500µg/LTrichlorofluoromethane
08/23/21 12:350.500< 0.500µg/L1,2,3-Trichloropropane
08/23/21 12:350.500< 0.500µg/L1,2,4-Trimethylbenzene
08/23/21 12:350.500< 0.500µg/L1,3,5-Trimethylbenzene
08/23/21 12:355.00< 5.00µg/LVinyl Acetate
08/23/21 12:350.500< 0.500µg/LVinyl Chloride
08/23/21 12:351.00< 1.00µg/Lm,p-Xylene
08/23/21 12:350.500< 0.500µg/Lo-Xylene
08/23/21 12:354-Bromofluorobenzene (S)102 70-130
08/23/21 12:35Dibromofluoromethane (S)98.6 70-130
08/23/21 12:351,2-Dichloroethane - d4 (S)96.0 70-130
08/23/21 12:35Toluene-d8 (S)99.6 70-130
LCS-V7931 LCSD-V7931Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
58.7 14714156.340.0µg/LAcetone 40-160 4.1 20.0
20.8 10410621.120.0µg/LBenzene 70-130 1.4 20.0
19.1 95.595.519.120.0µg/LBromobenzene 70-130 0.0 20.0
20.3 10299.519.920.0µg/LBromochloromethane 70-130 1.9 20.0
18.1 90.590.518.120.0µg/LBromodichloromethane 70-130 0.0 20.0
Page 3 of 14Date:08/26/2021 02:39 PM
Page 49 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V7932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V7931
LCS-V7931 LCSD-V7931Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.0 90.090.518.120.0µg/LBromoform 70-130 0.5 20.0
17.7 88.583.016.620.0µg/LBromomethane 60-140 6.4 20.0
21.6 10810521.020.0µg/Ln-Butylbenzene 70-130 2.8 20.0
19.8 99.099.519.920.0µg/Lsec-Butyl benzene 70-130 0.5 20.0
19.8 99.096.519.320.0µg/Ltert-Butyl benzene 70-130 2.5 20.0
20.6 10310220.420.0µg/LCarbon Tetrachloride 70-130 0.9 20.0
20.1 10110020.020.0µg/LChlorobenzene 70-130 0.4 20.0
20.3 10299.519.920.0µg/LChlorodibromomethane 70-130 1.9 20.0
24.3 12211923.720.0µg/LChloroethane 60-140 2.5 20.0
19.3 96.599.019.820.0µg/LChloroform 70-130 2.5 20.0
22.9 11511623.120.0µg/LChloromethane 60-140 0.8 20.0
20.9 10510721.320.0µg/L2-Chlorotoluene 70-130 1.8 20.0
19.1 95.596.519.320.0µg/L4-Chlorotoluene 70-130 1.0 20.0
20.2 10192.018.420.0µg/L1,2-Dibromo-3-Chloropropane 70-130 9.3 20.0
19.3 96.593.518.720.0µg/L1,2-Dibromoethane 70-130 3.1 20.0
18.6 93.091.518.320.0µg/LDibromomethane 70-130 1.6 20.0
18.7 93.593.018.620.0µg/L1,2-Dichlorobenzene 70-130 0.5 20.0
18.9 94.595.019.020.0µg/L1,3-Dichlorobenzene 70-130 0.5 20.0
19.4 97.097.519.520.0µg/L1,4-Dichlorobenzene 70-130 0.5 20.0
21.6 10810521.020.0µg/LDichlorodifluoromethane 60-140 2.8 20.0
20.6 10310821.620.0µg/L1,1-Dichloroethane 70-130 4.7 20.0
18.2 91.090.518.120.0µg/L1,2-Dichloroethane 70-130 0.5 20.0
21.3 10710420.820.0µg/L1,1-Dichloroethene 70-130 2.3 20.0
19.7 98.599.519.920.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0
20.6 10310320.620.0µg/Ltrans-1,2-Dichloroethene 70-130 0.0 20.0
19.5 97.510520.920.0µg/L1,2-Dichloropropane 70-130 6.9 20.0
Page 4 of 14Date:08/26/2021 02:39 PM
Page 50 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V7932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V7931
LCS-V7931 LCSD-V7931Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.9 94.594.518.920.0µg/L1,3-Dichloropropane 70-130 0.0 20.0
23.3 11712023.920.0µg/L2,2-Dichloropropane 70-130 2.5 20.0
21.1 10610921.820.0µg/L1,1-Dichloropropene 70-130 3.2 20.0
19.2 96.098.519.720.0µg/Lcis-1,3-Dichloropropene 70-130 2.5 20.0
19.2 96.098.519.720.0µg/Ltrans-1,3-Dichloropropene 70-130 2.5 20.0
623 125114571500µg/LEthanol 60-140 8.7 20.0
19.4 97.010020.020.0µg/LEthylbenzene 70-130 3.0 20.0
23.3 11711723.320.0µg/LHexachlorobutadiene 70-130 0.0 20.0
19.9 99.598.019.620.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.5 20.0
20.2 10199.519.920.0µg/LIsopropylbenzene 70-130 1.4 20.0
20.1 10198.019.620.0µg/L4-Isopropyl toluene 70-130 2.5 20.0
20.1 10196.019.220.0µg/L2-Hexanone 60-140 4.5 20.0
23.3 11711022.020.0µg/LMethyl Ethyl Ketone (MEK)60-140 5.7 20.0
19.8 99.098.519.720.0µg/LMethylene Chloride 70-130 0.5 20.0
19.3 96.593.518.720.0µg/LMethyl tert-butyl ether (MTBE)70-130 3.1 20.0
19.8 99.095.019.020.0µg/L4-Methyl-2-Pentanone 60-140 4.1 20.0
19.8 99.095.519.120.0µg/LNaphthalene 70-130 3.5 20.0
19.9 99.598.519.720.0µg/Ln-Propylbenzene 70-130 1.0 20.0
19.4 97.097.519.520.0µg/LStyrene 70-130 0.5 20.0
19.7 98.599.519.920.0µg/L1,1,1,2-Tetrachloroethane 70-130 1.0 20.0
18.2 91.089.017.820.0µg/L1,1,2,2-Tetrachloroethane 70-130 2.2 20.0
19.4 97.010020.020.0µg/LTetrachloroethene 70-130 3.0 20.0
19.8 99.098.519.720.0µg/LToluene 70-130 0.5 20.0
20.9 10510320.620.0µg/L1,2,3-Trichlorobenzene 70-130 1.4 20.0
22.1 11110821.520.0µg/L1,2,4-Trichlorobenzene 70-130 2.7 20.0
20.7 10410420.820.0µg/L1,1,1-Trichloroethane 70-130 0.4 20.0
Page 5 of 14Date:08/26/2021 02:39 PM
Page 51 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V7932QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V7931
LCS-V7931 LCSD-V7931Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
18.6 93.091.518.320.0µg/L1,1,2-Trichloroethane 70-130 1.6 20.0
19.3 96.599.019.820.0µg/LTrichloroethene 70-130 2.5 20.0
21.0 10510120.220.0µg/LTrichlorofluoromethane 60-140 3.8 20.0
18.7 93.585.517.120.0µg/L1,2,3-Trichloropropane 70-130 8.9 20.0
20.0 10098.519.720.0µg/L1,2,4-Trimethylbenzene 70-130 1.5 20.0
19.7 98.599.019.820.0µg/L1,3,5-Trimethylbenzene 70-130 0.5 20.0
20.3 10210921.720.0µg/LVinyl Acetate 60-140 6.6 20.0
18.5 92.591.518.320.0µg/LVinyl Chloride 60-140 1.0 20.0
41.4 10410642.440.0µg/Lm,p-Xylene 70-130 2.3 20.0
19.5 97.598.519.720.0µg/Lo-Xylene 70-130 1.0 20.0
97.696.84-Bromofluorobenzene (S)70-130
97.897.0Dibromofluoromethane (S)70-130
97.498.41,2-Dichloroethane - d4 (S)70-130
100102Toluene-d8 (S)70-130
Page 6 of 14Date:08/26/2021 02:39 PM
Page 52 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V8017QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V7920
Associated Lab Samples: 93863, 93864, 93865, 93866
LRB-V7920 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/24/21 16:3510.0< 10.0µg/LAcenaphthene
08/24/21 16:3520.0< 20.0µg/LAcenaphthylene
08/24/21 16:3510.0< 10.0µg/LAnthracene
08/24/21 16:3510.0< 10.0µg/LBenzidine
08/24/21 16:3510.0< 10.0µg/LBenzo(a)anthracene
08/24/21 16:3510.0< 10.0µg/LBenzo(a)pyrene
08/24/21 16:3510.0< 10.0µg/LBenzo(b)fluoranthene
08/24/21 16:3510.0< 10.0µg/LBenzo(g,h,i)perylene
08/24/21 16:3510.0< 10.0µg/LBenzo(k)fluoranthene
08/24/21 16:3550.0< 50.0µg/LBenzoic Acid
08/24/21 16:3510.0< 10.0µg/LBenzyl alcohol
08/24/21 16:3510.0< 10.0µg/LBis(2-Chloroethoxy)methane
08/24/21 16:3510.0< 10.0µg/LBis(2-Chloroethyl)ether
08/24/21 16:3510.0< 10.0µg/LBis(2-Chloroisopropyl)ether
08/24/21 16:3510.0< 10.0µg/LBis(2-ethylhexyl)phthalate
08/24/21 16:3520.0< 20.0µg/L4-Bromophenyl phenyl ether
08/24/21 16:3510.0< 10.0µg/LButyl benzyl phthalate
08/24/21 16:3510.0< 10.0µg/L4-Chloro-3-methylphenol
08/24/21 16:3520.0< 20.0µg/L2-Chloronaphthalene
08/24/21 16:3510.0< 10.0µg/L2-Chlorophenol
08/24/21 16:3520.0< 20.0µg/L4-Chlorophenyl phenyl ether
08/24/21 16:3510.0< 10.0µg/LChrysene
08/24/21 16:3520.0< 20.0µg/LDibenz(a,h)anthracene
08/24/21 16:3520.0< 20.0µg/LDibenzofuran
08/24/21 16:3510.0< 10.0µg/L1,2-Dichlorobenzene
08/24/21 16:3510.0< 10.0µg/L1,3-Dichlorobenzene
08/24/21 16:3510.0< 10.0µg/L1,4-Dichlorobenzene
Page 7 of 14Date:08/26/2021 02:39 PM
Page 53 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V8017QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V7920
Associated Lab Samples: 93863, 93864, 93865, 93866
LRB-V7920 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/24/21 16:3510.0< 10.0µg/L3,3'-Dichlorobenzidine
08/24/21 16:3510.0< 10.0µg/L2,4-Dichlorophenol
08/24/21 16:3520.0< 20.0µg/LDiethyl phthalate
08/24/21 16:3510.0< 10.0µg/LDimethyl phthalate
08/24/21 16:3520.0< 20.0µg/L2,4-Dimethylphenol
08/24/21 16:3510.0< 10.0µg/LDi-n-butyl phthalate
08/24/21 16:3530.0< 30.0µg/L4,6-Dinitro-2-methylphenol
08/24/21 16:3530.0< 30.0µg/L2,4-Dinitrophenol
08/24/21 16:3510.0< 10.0µg/L2,4-Dinitrotoluene
08/24/21 16:3520.0< 20.0µg/L2,6-Dinitrotoluene
08/24/21 16:3510.0< 10.0µg/LDi-n-Octyl Phthalate
08/24/21 16:3510.0< 10.0µg/LFluoranthene
08/24/21 16:3510.0< 10.0µg/LFluorene
08/24/21 16:3520.0< 20.0µg/LHexachlorobenzene
08/24/21 16:3520.0< 20.0µg/LHexachlorobutadiene
08/24/21 16:3520.0< 20.0µg/LHexachlorocyclopentadiene
08/24/21 16:3510.0< 10.0µg/LHexachloroethane
08/24/21 16:3510.0< 10.0µg/LIndeno(1,2,3-cd)pyrene
08/24/21 16:3510.0< 10.0µg/LIsophorone
08/24/21 16:3510.0< 10.0µg/LNaphthalene
08/24/21 16:3510.0< 10.0µg/LNitrobenzene
08/24/21 16:3510.0< 10.0µg/L2-Nitrophenol
08/24/21 16:3510.0< 10.0µg/L4-Nitrophenol
08/24/21 16:3520.0< 20.0µg/LN-Nitrosodiphenylamine
08/24/21 16:3520.0< 20.0µg/LN-Nitroso-di-n-propylamine
08/24/21 16:3550.0< 50.0µg/LPentachlorophenol
08/24/21 16:3510.0< 10.0µg/LPhenanthrene
Page 8 of 14Date:08/26/2021 02:39 PM
Page 54 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V8017QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V7920
Associated Lab Samples: 93863, 93864, 93865, 93866
LRB-V7920 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/24/21 16:3510.0< 10.0µg/LPhenol
08/24/21 16:3510.0< 10.0µg/LPyrene
08/24/21 16:3510.0< 10.0µg/L1,2,4-Trichlorobenzene
08/24/21 16:3520.0< 20.0µg/L2,4,6-Trichlorophenol
08/24/21 16:352-Fluorobiphenyl (S)58.6 49-118
08/24/21 16:352-Fluorophenol (S)31.5 22-84
08/24/21 16:35Nitrobenzene-d5 (S)52.0 43-123
08/24/21 16:354-Terphenyl-d14 (S)89.6 49-151
08/24/21 16:352,4,6-Tribromophenol (S)77.8 31-144
08/24/21 16:35Phenol-d5 (S)20.3 10-63
LCS-V7920 LCSD-V7920Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
28.7 57.458.029.050.0µg/LAcenaphthene 47-145 1.0 20.0
30.0 60.059.429.750.0µg/LAcenaphthylene 33-145 1.0 20.0
38.2 76.471.835.950.0µg/LAnthracene 27-133 6.2 20.0
26.0 52.00.0*5.0850.0µg/LBenzidine 15-150 88.8*20.0
40.0 80.074.837.450.0µg/LBenzo(a)anthracene 33-143 6.7 20.0
56.2 11210854.150.0µg/LBenzo(a)pyrene 17-163 3.8 20.0
50.5 10196.448.250.0µg/LBenzo(b)fluoranthene 24-159 4.6 20.0
49.0 98.094.247.150.0µg/LBenzo(g,h,i)perylene 10-219 3.9 20.0
49.7 99.495.447.750.0µg/LBenzo(k)fluoranthene 11-162 4.1 20.0
11.5 0.0*0.0*11.550.0µg/LBenzoic Acid 10-125 0.0 20.0
19.4 38.836.618.350.0µg/LBenzyl alcohol 16-107 5.8 20.0
29.4 58.854.427.250.0µg/LBis(2-Chloroethoxy)methane 33-184 7.7 20.0
Page 9 of 14* QC Fail Date:08/26/2021 02:39 PM
Page 55 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V8017QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V7920
LCS-V7920 LCSD-V7920Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.7 41.437.618.850.0µg/LBis(2-Chloroethyl)ether 12-158 9.6 20.0
23.7 47.440.020.050.0µg/LBis(2-Chloroisopropyl)ether 36-166 16.9 20.0
47.8 95.692.046.050.0µg/LBis(2-ethylhexyl)phthalate 10-158 3.8 20.0
32.7 65.465.832.950.0µg/L4-Bromophenyl phenyl ether 53-127 0.6 20.0
43.1 86.281.640.850.0µg/LButyl benzyl phthalate 10-152 5.4 20.0
30.6 61.258.829.450.0µg/L4-Chloro-3-methylphenol 22-147 4.0 20.0
26.9 53.8*51.6*25.850.0µg/L2-Chloronaphthalene 60-118 4.1 20.0
22.8 45.640.620.350.0µg/L2-Chlorophenol 23-134 11.6 20.0
31.1 62.262.631.350.0µg/L4-Chlorophenyl phenyl ether 25-158 0.6 20.0
40.2 80.478.839.450.0µg/LChrysene 17-168 2.0 20.0
26.1 52.294.247.150.0µg/LDibenz(a,h)anthracene 10-227 57.3*20.0
30.0 60.059.829.950.0µg/LDibenzofuran 39-114 0.3 20.0
21.5 43.036.218.150.0µg/L1,2-Dichlorobenzene 32-129 17.1 20.0
21.1 42.234.817.450.0µg/L1,3-Dichlorobenzene 20-124 19.2 20.0
20.6 41.234.417.250.0µg/L1,4-Dichlorobenzene 20-124 17.9 20.0
42.9 85.873.436.750.0µg/L3,3'-Dichlorobenzidine 10-262 15.5 20.0
28.3 56.650.825.450.0µg/L2,4-Dichlorophenol 39-135 10.8 20.0
36.6 73.269.634.850.0µg/LDiethyl phthalate 10-114 5.0 20.0
32.5 65.063.831.950.0µg/LDimethyl phthalate 10-112 1.8 20.0
28.8 57.655.627.850.0µg/L2,4-Dimethylphenol 32-119 3.5 20.0
45.3 90.685.842.950.0µg/LDi-n-butyl phthalate 10-118 5.4 20.0
37.6 75.270.035.050.0µg/L4,6-Dinitro-2-methylphenol 10-181 7.1 20.0
37.1 74.268.434.250.0µg/L2,4-Dinitrophenol 10-191 8.1 20.0
37.0 74.069.034.550.0µg/L2,4-Dinitrotoluene 39-139 6.9 20.0
33.5 67.066.033.050.0µg/L2,6-Dinitrotoluene 50-158 1.5 20.0
54.9 11010653.250.0µg/LDi-n-Octyl Phthalate 10-146 3.1 20.0
Page 10 of 14* QC Fail Date:08/26/2021 02:39 PM
Page 56 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V8017QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V7920
LCS-V7920 LCSD-V7920Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.2 80.476.238.150.0µg/LFluoranthene 26-137 5.3 20.0
32.0 64.065.432.750.0µg/LFluorene 59-121 2.1 20.0
34.9 69.868.834.450.0µg/LHexachlorobenzene 10-152 1.4 20.0
21.8 43.60.0*5.8850.0µg/LHexachlorobutadiene 24-116 8.6 20.0
5.90 0.0*0.0*5.9050.0µg/LHexachlorocyclopentadiene 32-117 0.0 20.0
19.7 39.4*33.8*16.950.0µg/LHexachloroethane 40-113 15.3 20.0
47.7 95.491.045.550.0µg/LIndeno(1,2,3-cd)pyrene 10-171 4.7 20.0
23.2 46.442.421.250.0µg/LIsophorone 21-196 9.0 20.0
24.3 48.643.021.550.0µg/LNaphthalene 21-133 12.2 20.0
24.2 48.440.820.450.0µg/LNitrobenzene 35-180 17.0 20.0
25.0 50.045.822.950.0µg/L2-Nitrophenol 29-182 8.7 20.0
14.5 29.023.611.850.0µg/L4-Nitrophenol 10-132 20.5*20.0
41.3 82.681.840.950.0µg/LN-Nitrosodiphenylamine 69-152 0.9 20.0
24.9 49.844.622.350.0µg/LN-Nitroso-di-n-propylamine 10-230 11.0 20.0
9.73 0.0*0.0*9.7350.0µg/LPentachlorophenol 14-176 0.0 20.0
38.2 76.473.036.550.0µg/LPhenanthrene 54-120 4.5 20.0
10.8 21.60.0*2.8650.0µg/LPhenol 10-112 7.6 20.0
41.0 82.077.838.950.0µg/LPyrene 52-115 5.2 20.0
22.4 44.839.0*19.550.0µg/L1,2,4-Trichlorobenzene 44-142 13.8 20.0
28.7 57.456.428.250.0µg/L2,4,6-Trichlorophenol 37-144 1.7 20.0
54.452.42-Fluorobiphenyl (S)49-118
27.623.42-Fluorophenol (S)22-84
48.243.0Nitrobenzene-d5 (S)43-123
82.679.84-Terphenyl-d14 (S)49-151
74.872.72,4,6-Tribromophenol (S)31-144
Page 11 of 14* QC Fail Date:08/26/2021 02:39 PM
Page 57 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V8017QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V7920
LCS-V7920 LCSD-V7920Laboratory Control Sample & LCSD
LCSD
ResultParameter
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.815.8Phenol-d5 (S)10-63
Page 12 of 14Date:08/26/2021 02:39 PM
Page 58 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V8032QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V7948
Associated Lab Samples: 93863, 93864, 93866
LRB-V7948 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/25/21 11:10350< 350µg/LAliphatic C9-C18
08/25/21 11:10500< 500µg/LAliphatic C19-C36
08/25/21 11:10250< 250µg/LAromatic C11-C22
08/25/21 11:102-Fluorobiphenyl (S)81.0 40-140
08/25/21 11:102-Bromonaphthalene (S)67.7 40-140
08/25/21 11:10Chlorooctadecane (S)80.5 40-140
08/25/21 11:10OTP Surrogate (S)75.5 40-140
LCS-V7948 LCSD-V7948Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
381 63.565.5393600µg/LAliphatic C9-C18 40-140 3.1 50.0
674 84.299.5796800µg/LAliphatic C19-C36 40-140 16.5 50.0
1280 75.280.013601700µg/LAromatic C11-C22 40-140 6.0 50.0
82.587.52-Fluorobiphenyl (S)40-140
39.7*77.72-Bromonaphthalene (S)40-140
77.077.5Chlorooctadecane (S)40-140
72.577.0OTP Surrogate (S)40-140
Page 13 of 14* QC Fail Date:08/26/2021 02:39 PM
Page 59 of 62
Quality Control Data
21-231-0011Report No:
Project Description:
Client ID:Withers & Ravenel
CC Newell Store
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V7803QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V7802
Associated Lab Samples: 93863, 93864, 93865, 93866
LRB-V7802 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLBlank
ResultUnits
%
Recovery
% Rec
Limits
08/20/21 09:1750.0< 50.0µg/LAliphatic C5-C8
08/20/21 09:1750.0< 50.0µg/LAliphatic C9-C12
08/20/21 09:1750.0< 50.0µg/LAromatic C9-C10
08/20/21 09:172,5-Dibromotoluene (FID) (S)105 70-130
08/20/21 09:172,5-Dibromotoluene (PID) (S)101 70-130
LCS-V7802 LCSD-V7802Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
323 108120361300µg/LAliphatic C5-C8 70-130 11.1 50.0
342 114106317300µg/LAliphatic C9-C12 70-130 7.5 50.0
112 112109109100µg/LAromatic C9-C10 70-130 2.7 50.0
99.21012,5-Dibromotoluene (FID) (S)70-130
95.597.02,5-Dibromotoluene (PID) (S)70-130
Page 14 of 14Date:08/26/2021 02:39 PM
Page 60 of 62
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:21-231-0011
Withers & Ravenel
01221
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 5.8 C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)?Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Angela D Overcash Date & Time:08/19/2021 14:21:30
Special precautions or instructions included?
Comments:
Page 61 of 62
Page 62 of 62

APPENDIX C 
 FIELD NOTES & PHOTOGRAPHIC RECORD 

WithersRavenel
Our People. Your Success.
Former C.C. Newell Store WR Project # 02172214.97 Site Check Report September 2021
WithersRavenel
Our People. Your Success.
Former C.C. Newell Store WR Project # 02172214.97 Site Check Report September 2021
WithersRavenel
Our People. Your Success.
Former C.C. Newell Store WR Project # 02172214.97 Site Check Report September 2021
WithersRavenel
Our People. Your Success.
Former C.C. Newell Store WR Project # 02172214.97 Site Check Report September 2021
WithersRavenel
Our People. Your Success.
Former C.C. Newell Store WR Project # 02172214.97 Site Check Report September 2021
WithersRavenel
Our People. Your Success.
Former C.C. Newell Store WR Project # 02172214.97 Site Check Report September 2021
Photographic Record
Project Name: Former CC Newell Store Project No. 02172214.97
Frame No. 1
Description: MW-1 in front of building.

Frame No. 2
Description: Typical monitoring well along front of building (MW-4 in photo)

Photographic Record
Project Name: Former CC Newell Store Project No. 02172214.97
Frame No. 3
Description: Soil boring through slab – note white powder spread on floor by owner.

Frame No. 4
Description: Sub-Slab Vapor sample 1 (SSV-1) located near center of building

Photographic Record
Project Name: Former CC Newell Store Project No. 02172214.97
Frame No. 5
Description: Installation of MW-6 at rear of building.
Frame No. 6

Description: Cored holes through slab in former oil change bay / mechanic’s bay in the southwestern corner
of the building. Soil boring WR-7 in center of frame, WR-8 in back right of frame. Later converted to
temporary wells

Photographic Record
Project Name: Former CC Newell Store Project No. 02172214.97
Frame No. 7
Description: WSW-1 located within wellhouse. 35’ deep 18” bored well.

Frame No. 8
Description: Sampling of WR-8 (TW)

APPENDIX D 
 NCDEQ RISK CALCULATOR 

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Prepared By:David Vail
WithersRavenel
North Carolina Department of Environmental Quality
Risk Calculator
CC Newell Store
216 Camp Easter Road
UST
11196
January 2021
November 2020 EPA RSL Table
North Carolina DEQ Risk Calculator
Table of Contents
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
Form No.
Input Form 1A Complete Exposure Pathways
Input Form 1B Exposure Factors and Target Risks
Input Form 1C Contaminant Migration Parameters
Input Form 1D Sample Statistics
Input Form 2A Soil Exposure Point Concentration Table
Input Form 2B Groundwater Exposure Point Concentration Table
Input Form 2C Surface Water Exposure Point Concentration Table
Input Form 2D Soil Gas Exposure Point Concentration Table
Input Form 2E Indoor Air Exposure Point Concentration Table
Output Form 1A Risk for Individual Pathways
Output Form 1B Sitewide Risk
Output Form 2A Resident Soil
Output Form 2B Resident Groundwater Use
Output Form 2C Non-Residential Worker Soil
Output Form 2D Non-Residential Worker Groundwater Use
Output Form 2E Construction Worker Soil
Output Form 2F Recreator/Trespasser Soil
Output Form 2G Recreator/Trespasser Surface Water
Output Form 3A Resident Groundwater to Indoor Air
Output Form 3B Resident Soil Gas to Indoor Air
Output Form 3C Resident Indoor Air
Output Form 3D Non-Residential Worker Groundwater to Indoor Air
Output Form 3E Non-Residential Worker Soil Gas to Indoor Air
Output Form 3F Non-Residential Worker Indoor Air
Output Form 4A Soil to Groundwater - Forward Mode
Output Form 4B Groundwater to Groundwater - Forward Mode
Output Form 4C Soil to Surface Water - Forward Mode
Output Form 4D Groundwater to Surface Water - Forward Mode
Output Form 4E Soil to Groundwater - Backward Mode
Output Form 4F Groundwater to Groundwater - Backward Mode
Output Form 4G Soil to Surface Water - Backward Mode
Output Form 4H Groundwater to Surface Water - Backward Mode
Output Section 4 - Contaminant Migration to Worksheets
Output Section 3 - Vapor Intrusion Calculators
TOC
Description
DATA INPUT SHEETS
Check box
if included
Input Section 1 - Exposure Pathways & Parameters
Input Section 2 - Exposure Point Concentrations
DATA OUTPUT SHEETS
Output Section 1 - Summary Output for All Calculators
Output Section 2 - Direct Contact Soil and Groundwater Calculators
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Factors and Target Risks
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Parameter Site Specific Value Justification
Target Cancer Risk (individual) 1.0E-06
Target Cancer Risk (cumulative) 1.0E-04
Target Hazard Index (individual) 2.0E-01
Target Hazard Index (cumulative) 1.0E+00
Lifetime (LT) (years)70
Body Weight (BW) (kg) 15
Exposure Duration (ED) (yr) 6
Exposure Frequency (EF) (d/yr) 350
Exposure Time (ET) (hr) 24
Skin Surface Area - Soil Exposure (SAs) (cm2)2373
Soil Adherence Factor (AF) (mg/cm2)0.2
Soil Ingestion Rate (IRS) (mg/day) 200
Skin Surface Area - Water Exposure (SAw) (cm2)6365
Water Ingestion Rate (IRW) (L/d) 0.78
Water Exposure Time (ETevent) (hr/event)0.54
Water Event Frequency (EV) (events/day) 1
Lifetime (LT) (years)70
Body Weight (BW) (kg) 80
Exposure Duration (ED) (yr) 20
Exposure Frequency (EF) (d/yr) 350
Exposure Time (ET) (hr) 24
Skin Surface Area - Soil Exposure (SAs) (cm2)6032
Soil Adherence Factor (AF) (mg/cm2)0.07
Soil Ingestion Rate (IRS) (mg/day) 100
Skin Surface Area - Water Exposure (SAw) (cm2)19652
Water Ingestion Rate (IRW) (L/d) 2.5
Water Exposure Time (ETevent) (hr/event)0.71
Water Event Frequency (EV) (events/day) 1
Lifetime (LT) (years)70
Body Weight (BW) (kg) 80
Exposure Duration (ED) (yr) 25
Exposure Frequency (EF) (d/yr) 250
Exposure Time (ET) (hr) 8
Skin Surface Area - Soil Exposure (SAs) (cm2)3527
Soil Adherence Factor (AF) (mg/cm2)0.12
Soil Ingestion Rate (IR) (mg/day) 100
Skin Surface Area - Water Exposure (SAw) (cm2)19652
Water Ingestion Rate (IRW) (L/d) 0.83
Water Exposure Time (ETevent) (hr/event)0.67
Water Event Frequency (EV) (events/day) 1
Lifetime (LT) (years)70
Body Weight (BW) (kg) 80
Working Weeks (EW) (wk/yr) 50
Exposure Duration (ED) (yr) 1
Exposure Frequency (EF) (d/yr) 250
Exposure Time (ET) (hr) 8
Skin Surface Area - Soil Exposure (SAs) (cm2)3527
Soil Adherence Factor (AF) (mg/cm2)0.3
Soil Ingestion Rate (IR) (mg/day) 330
1
70
80
330
1
250
8
3527
0.3
50
100
19652
2.5
0.71
1
20
350
24
6032
0.07
0.54
1
70
80
2373
0.2
200
6365
0.78
Input Form 1B
Exposure Unit ID:
Residential Child
General
Residential Adult
Default Value
1.0E-06
1.0E-04
2.0E-01
1.0E+00
70
15
6
350
24
Non-Residential Worker
Construction Worker
70
80
25
250
8
3527
0.12
100
19652
0.83
0.67
North Carolina DEQ Risk Calculator
Exposure Factors and Target Risks
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Parameter Site Specific Value Justification
Input Form 1B
Exposure Unit ID:
Default Value
Recreator Trespasser
Lifetime (LT) (years)70 NA 70
Averaging Time (AT) (days/yr) 365 NA 365
Body Weight (BW) (kg) 15 NA 15
Exposure Duration 0-2 (ED) (yr) 2 NA 2
Exposure Duration 2-6 (ED) (yr) 4 NA 4
Exposure Frequency (EF) (d/yr) 195 NA 195
Exposure Time (ET) (hr) 2 NA 2
Skin Surface Area - Soil Exposure (SAs) (cm2)2373 NA 2373
Soil Adherence Factor (AF) (mg/cm2)0.2 NA 0.2
Soil Ingestion Rate (IRS) (mg/day)200 NA 200
Skin Surface Area - Water Exposure (SAw) (cm2)6365 NA 6365
Water Ingestion Rate (IRW) (L/hr) 0.124 NA 0.124
Water Exposure Time (ETevent) (hr/event)2NA 2
Water Event Frequency (EV) (events/day) 1 NA 1
Recreator Trespasser
Lifetime (LT) (years)70 70 70
Body Weight (BW) (kg) 80 45 80
Exposure Duration 6-16 (ED) (yr) 10 10 10
Exposure Duration 16-26 (ED) (yr) 10 0 10
Exposure Frequency (EF) (d/yr) 195 90 195
Exposure Time (ET) (hr) 2 2 2
Skin Surface Area - Soil Exposure (SAs) (cm2)6032 6032 6032
Soil Adherence Factor (AF) (mg/cm2)0.07 0.2 0.07
Soil Ingestion Rate (IRS) (mg/day) 100 200 100
Skin Surface Area - Water Exposure (SAw) (cm2)19652 19652 19652
Water Ingestion Rate (IRW) (L/hr) 0.0985 0.071 0.0985
Water Exposure Time (ETevent) (hr/event)22 2
Water Event Frequency (EV) (events/day) 1 1 1
User Defined Child
User Defined Adult
North Carolina DEQ Risk Calculator
Contaminant Migration Parameters
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
Parameter Default Value
Site Specific
Value Justification
Distance to Protection of
Groundwater Point of
Exposure (POEgw) (feet)
00
Distance to Protection of
Surface Water Point of
Exposure (POEsw) (feet)
00
Depth to Base of Affected
Soils (ds) (cm)1244 1,244
Length of Affected Soil
Parallel to Assumed GW
Flow Direction (L) (cm)
Site-specific
value required
Areal extent of soil
contamination
range 0.5-500 (As) (acres)
0.5 0.5
Fraction of vegetative cover
(V) (unitless)0.5 0.5
0.15 (soil to
outdoor air
pathway)
0.15
0.3 (soil to
groundwater
pathway)
0.3
Provide justification for the contaminant migration parameters used.
Water Filled Soil Porosity
(θw) (unitless)
Input Form 1C
North Carolina DEQ Risk Calculator
Contaminant Migration Parameters
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
Parameter Default Value
Site Specific
Value Justification
Provide justification for the contaminant migration parameters used.
Input Form 1C
0.28 (soil to
outdoor air
pathway)
0.28
0.13 (soil to
groundwater
pathway)
0.13
Total Soil Porosity (n)
(unitless)0.43 0.43
Dry Soil Bulk Density (ρb)
(g/cm3)1.5 1.5
Net Infiltration Rate (I)
(cm/yr)66 66
0.006 (soil to
outdoor air
pathway)
0.006
0.002 (soil
leaching to
groundwater
pathway)
0.002
Aquifer Hydraulic
Conductivity (K) (cm/d)
Site-specific
value required
Hydraulic Gradient (i)
(unitless)
Site-specific
value required
Average Groundwater
Temperature (Tgw) (°C)25 25
Fraction Organic Carbon
(foc) (unitless)
Air Filled Soil Porosity (θa)
(unitless)
North Carolina DEQ Risk Calculator
Contaminant Migration Parameters
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
Parameter Default Value
Site Specific
Value Justification
Provide justification for the contaminant migration parameters used.
Input Form 1C
Aquifer Thickness (da) (cm)Site-specific
value required
Groundwater Source
Thickness (Sd) (cm)
Site-specific
value required
Groundwater Source Width
(Sw) (cm)
Site-specific
value required
Plume Thickness at GW/SW
Discharge (δsw) (cm)
Site-specific
value required
Plume Width at GW/SW
Discharge (Wgwsw) (cm)
Site-specific
value required
Surface Water Flowrate at
GW/SW Discharge (Qsw)
(cm3/d)
Site-specific
value required
North Carolina DEQ Risk Calculator
Sample StatisticsVersion Date: January 2021Basis: November 2020 EPA RSL TableSite ID: 11196Exposure Unit ID: #Sample IDConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab Qualifier1234567891011121314151617181920Note that the calculations in this sheet are for reference only and are not used in the calculators.SAMPLE DATA ENTRYMediaContaminant:Units:SAMPLE STATISTICSCountMinimumMaximumAverageStandard DeviationMedianMean - Standard DeviationMean + Standard Deviation95% PercentileInput Form 1D North Carolina DEQ Risk Calculator
Sample StatisticsVersion Date: January 2021Basis: November 2020 EPA RSL TableSite ID: 11196Exposure Unit ID: Note that the calculations in this sheet are for reference only and are not used in the calculators.Input Form 1D #Sample IDConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab QualifierConcentrationLab Qualifier1234567891011121314151617181920SAMPLE DATA ENTRYMediaContaminant:Units:SAMPLE STATISTICSCountMinimumAverageMaximumMedianStandard DeviationMean + Standard DeviationMean - Standard Deviation95% PercentileNorth Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2021Basis: November 2020 EPA RSL TableSite ID: 11196Exposure Unit ID: Description of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion250Highest Concentration67-64-1 Acetoneug/m3SSV-121Highest Concentration75-15-0 Carbon Disulfideug/m3SSV-2240Highest Concentration67-63-0 Isopropanolug/m3SSV-146Highest Concentration78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3SSV-15.3Highest Concentration108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m3SSV-1Input Form 2DSoil Gas Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator
Exposure Point ConcentrationsVersion Date: January 2021Basis: November 2020 EPA RSL TableSite ID: 11196Exposure Unit ID: Description of Exposure Point Concentration Selection:Exposure Point Concentration (ug/m3)Notes: CAS Number ChemicalMinimum Concentration (Qualifier)Maximum Concentration (Qualifier)UnitsLocation of Maximum ConcentrationDetection FrequencyRange of Detection LimitsConcentration Used for ScreeningBackground ValueScreening Toxicity Value (Screening Level) (n/c)Potential ARAR/TBC ValuePotential ARAR/TBC SourceCOPC Flag (Y/N)Rationale for Selection or Deletion110 71-43-2 Benzeneug/m318110-82-7Cyclohexaneug/m32.175-71-8Dichlorodifluoromethaneug/m355111-77-3Ethanol, 2-(2-methoxyethoxy)-ug/m3400100-41-4Ethylbenzeneug/m3180111-71-7Heptanal, n-ug/m3170110-54-3Hexane, N-ug/m35267-63-0Isopropanolug/m314091-20-3~Naphthaleneug/m31300108-88-3Tolueneug/m3160095-63-6Trimethylbenzene, 1,2,4-ug/m3460108-67-8Trimethylbenzene, 1,3,5-ug/m32100106-42-3Xylene, P-ug/m395095-47-6Xylene, o-ug/m3Input Form 2EIndoor Air Exposure Point Concentration TableNote: Chemicals highlighted in orange are non-volatile chemicals. Risks are calculated for these chemicals if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion.If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculationsNorth Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 0.0E+00 3.6E-02 NO
Indoor Air 2.4E-03 1.7E+02 YES
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 0.0E+00 2.9E-03 NO
Indoor Air 5.4E-04 4.0E+01 YES
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC
2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Sitewide RiskOutput Form 1BVersion Date: January 2021Basis: November 2020 EPA RSL TableSite ID: 11196Exposure Unit ID: ReceptorPathwayCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexCheck box to include in site-wide risk calculationsCarcinogenic RiskHazard IndexSoil NM NMNM NMGroundwater Use*NM NMNM NMSoil NMNMNM NMGroundwater Use*NMNMNM NMConstruction WorkerSoil NM NMSoil NMNMSurface Water Use*NMNMGroundwater to Indoor AirNM NMNM NMSoil Gas to Indoor Air0.0E+00 3.6E-020.0E+00 3.6E-02Indoor Air2.4E-03 1.7E+022.4E-03 1.7E+02Groundwater to Indoor AirNMNMNM NMSoil Gas to Indoor Air0.0E+00 2.9E-030.0E+00 2.9E-03Indoor Air5.4E-04 4.0E+015.4E-04 4.0E+012.4E-03 1.7E+022.4E-03 1.7E+025.4E-04 4.0E+015.4E-04 4.0E+010.0E+00 0.0E+000.0E+00 0.0E+003. NM = Not Modeled4. NC = Pathway not calculatedTOTAL SITEWIDE RISK FOR EACH RECEPTORNotes:1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based closure.ResidentNon-Residential WorkerResidentNon-Residential WorkerRecreator/TrespasserVAPOR INTRUSION CALCULATORSDIRECT CONTACT SOIL AND WATER CALCULATORSNon-Residential Worker - Future ScenarioConstruction WorkerRecreator/TrespasserResident - Current ScenarioResident - Future Scenario Non-Residential Worker - Current ScenarioNorth Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Indoor Air
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
CAS # Chemical Name:
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
71-43-2 Benzene 110 3.6E-01 6.3E+00 3.1E-04 3.5E+00
110-82-7 Cyclohexane 18 - 1.3E+03 2.9E-03
75-71-8 Dichlorodifluoromethane 2.1 - 2.1E+01 2.0E-02
111-77-3 Ethanol, 2-(2-methoxyethoxy)- 55 - -
100-41-4 Ethylbenzene 400 1.1E+00 2.1E+02 3.6E-04 3.8E-01
111-71-7 Heptanal, n- 180 - 6.3E-01 5.8E+01
110-54-3 Hexane, N- 170 - 1.5E+02 2.3E-01
67-63-0 Isopropanol 52 - 4.2E+01 2.5E-01
91-20-3 ~Naphthalene 140 8.3E-02 6.3E-01 1.7E-03 4.5E+01
108-88-3 Toluene 1300 - 1.0E+03 2.5E-01
95-63-6 Trimethylbenzene, 1,2,4- 1600 - 1.3E+01 2.6E+01
108-67-8 Trimethylbenzene, 1,3,5- 460 - 1.3E+01 7.4E+00
106-42-3 Xylene, P- 2100 - 2.1E+01 2.0E+01
95-47-6 Xylene, o- 950 - 2.1E+01 9.1E+00
Cumulative:2.4E-03 1.7E+02
All concentrations are in ug/m3
Output Form 3C
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic
risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 μg/m3.
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if
indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals
are likely not associated with vapor intrusion.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Resident Soil Gas to Indoor Air
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 250 7.5 -6.5E+03 2.3E-04
75-15-0 Carbon Disulfide 21 0.63 -1.5E+02 8.6E-04
67-63-0 Isopropanol 240 7.2 -4.2E+01 3.5E-02
78-93-3 Methyl Ethyl Ketone (2-Butanone)46 1.38 -1.0E+03 2.6E-04
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 5.3 0.159 -6.3E+02 5.1E-05
Cumulative: 0.0E+00 3.6E-02
All concentrations are in ug/m3
Output Form 3B
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Indoor Air
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
CAS # Chemical Name:
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
71-43-2 Benzene 110 1.6E+00 2.6E+01 7.0E-05 8.4E-01
110-82-7 Cyclohexane 18 - 5.3E+03 6.8E-04
75-71-8 Dichlorodifluoromethane 2.1 - 8.8E+01 4.8E-03
111-77-3 Ethanol, 2-(2-methoxyethoxy)-55 - -
100-41-4 Ethylbenzene 400 4.9E+00 8.8E+02 8.2E-05 9.1E-02
111-71-7 Heptanal, n-180 - 2.6E+00 1.4E+01
110-54-3 Hexane, N-170 - 6.1E+02 5.5E-02
67-63-0 Isopropanol 52 - 1.8E+02 5.9E-02
91-20-3 ~Naphthalene 140 3.6E-01 2.6E+00 3.9E-04 1.1E+01
108-88-3 Toluene 1300 - 4.4E+03 5.9E-02
95-63-6 Trimethylbenzene, 1,2,4-1600 - 5.3E+01 6.1E+00
108-67-8 Trimethylbenzene, 1,3,5-460 - 5.3E+01 1.8E+00
106-42-3 Xylene, P-2100 - 8.8E+01 4.8E+00
95-47-6 Xylene, o-950 - 8.8E+01 2.2E+00
Cumulative:5.4E-04 4.0E+01
All concentrations are in ug/m3
Output Form 3F
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic
risk or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 μg/m3.
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if
indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are
likely not associated with vapor intrusion.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: January 2021
Basis: November 2020 EPA RSL Table
Site ID: 11196
Exposure Unit ID:
CAS # Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 250 2.5 -2.7E+04 1.8E-05
75-15-0 Carbon Disulfide 21 0.21 -6.1E+02 6.8E-05
67-63-0 Isopropanol 240 2.4 -1.8E+02 2.7E-03
78-93-3 Methyl Ethyl Ketone (2-Butanone)46 0.46 -4.4E+03 2.1E-05
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone) 5.3 0.053 -2.6E+03 4.0E-06
Cumulative: 0.0E+00 2.9E-03
All concentrations are in ug/m3
Output For
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk,
no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
m3E
APPENDIX E
GENERAL OPERATING PROCEEDURES
Generalized Standard Operating Procedures (Not All Inclusive)

WithersRavenel
Our People. Your Success.
Soil Sampling, Soil Boring and Monitor Well Installation, Well Development Soil borings are installed utilizing a stainless-steel hand auger, direct-push hydraulic drill or auger rotary
drill using either a macro core™ sampler, hollow stem augers, or air rotary roller cone bit. Soil borings are
typically sampled at discrete intervals from the bucket of a clean stainless steel hand auger, direct push stainless steel sampler with acetate sleeve, or a split barrel sampler. When appropriate, soil samples may be collected from drill cuttings associated with the boring or well installation. Monitor wells are constructed within select soil borings of one, two, or four-inch inside diameter PVC
casing and machine slotted screen in accordance with NCAC Title 15A, Subchapter 02C (Well Construction Standards, Criteria and Standards Applicable to Water Supply and Certain Other Wells). Clean-washed “#2 Torpedo Sand” is typically utilized to fill the boring annulus surrounding the well screen, extending to a minimum of 1-foot above the well screen. A minimum 1-foot thick bentonite clay seal is emplaced above the sand pack and hydrated. Neat cement grout is placed in the remaining annulus
space from the upper portion of the bentonite seal to within 1-foot of surface grade. In coastal plain areas where shallow groundwater is encountered, a variance to construction standards may be employed to ensure the upper portion of the well screen intersects the upper aquifer surface. Wellheads may be completed with either concrete-set flush mounted traffic-bearing steel skirted manholes with bolt down covers or steel above-ground “stick-up” well protectors set in a concrete pad. The monitoring wells are
secured with locking caps. Temporary wells or piezometers may be completed with the PVC riser cut at or above grade, and are abandoned within 24-hours of their installation. Wells may be developed using a bailer, electric submersible pump, pneumatic pump, or peristaltic pump, dependent upon site conditions. When wells are developed by the driller, they may be developed with
any of the methods outlined above, in addition to air or water injection. Soil boring logs and well construction details are typically prepared for presentation in a report appendix. Borings completed in bedrock may be drilled using air rotary, coring, or sonic drilling methods. Groundwater Depth to Water Measurements

Groundwater level measurements are typically obtained using an electronic water level indicator which registers a tone and/or illuminated light when the probe contacts groundwater. Depth to groundwater measurements are obtained by lowering the probe attached to a cable usually marked in 0.01 foot intervals into the well until the probe of the meter intersects the water surface. The measurement from
the top of the riser pipe or top of casing (TOC) to the water level is recorded to the nearest 0.01 foot. The
electronic water level indicator probe and exposed probe cable is decontaminated between measurement locations.

Generalized Standard Operating Procedures (Not All Inclusive)

WithersRavenel
Our People. Your Success.
Free Product Level Measurements Light Non-Aqueous Phase Liquid (LNAPL) or “free product” present on the water table is measured using
an electronic oil/water interface probe. The interface probe has both an audible and illuminating light
that indicate when a liquid level is encountered. The oil/water interface probe registers a solid tone and solidly lit light when LNAPL petroleum product is encountered and a beeping tone flashing light when groundwater is encountered. Depth to LNAPL measurements are obtained by lowering the probe attached to a cable marked in 0.01 foot intervals into the well until the probe of the meter intersects the product or groundwater. The measurements from the top of the riser pipe or TOC to the liquid level are
recorded to the nearest 0.01 foot. The thickness of LNAPL is calculated by subtracting the depth to LNAPL measurement from the depth to groundwater measurement. The electronic interface probe is decontaminated between measurement locations. Soil Sampling and Field Screening
Soil sampling is performed in general accordance with ASTM: 1586-84 where applicable. Sampling procedures are followed to protect the chemical integrity of the soil samples and minimize the potential for cross contamination between sample locations, including discarding of the exterior of the sample which contacts the auger bucket, acetate sleeve, or split barrel sampler, the use of stainless steel sampling
equipment, and the thorough decontamination of sampling apparatus prior to use and between sample locations. Soil samples retained as a part of excavation or other intrusive “digging” activities may be collected from the bucket of excavation equipment or using a hand shovel, if appropriate. Care to collect soil samples
from excavation equipment includes retrieving native soil from material that has not made contact with the excavating equipment. Samples are collected in sealable bags or by directly filling sample containers as described above. Sampling is performed using new, disposable nitrile gloves for each sample location to ensure sample
integrity and minimize the potential for cross contamination or field personnel exposure to contaminants.
Sampling equipment such as hand auger extensions and buckets, direct push samplers, split spoons or shovels, are decontaminated prior to their use in the collection of samples. Samples are placed within laboratory grade sample containers provided by the laboratory to which the
samples are submitted, labeled, sealed, and placed in an ice filled cooler. An aliquot of the sample is
typically placed in a clean sealable bag and allowed to reach ambient air temperature for future screening of volatile vapor content with a photoionization detector (PID), flame-ionization detector (FID) or other portable screening device.
Screening of samples with a PID, FID or other field screening device is performed in accordance with
device manufacturer specifications for screening, following calibration of the instrument based on manufacturer recommended procedures.

Generalized Standard Operating Procedures (Not All Inclusive)

WithersRavenel
Our People. Your Success.
Groundwater Sampling Groundwater samples are generally collected using one of three standard methods – through the use of a
dedicated, disposable bailer, a peristaltic pump or submersible electric pump.
When sampling with a bailer, a minimum of three well volumes of groundwater are extracted from the well as a means of purging, unless the well is purged to a “dry” state prior to the removal of three volumes of water. Prior to collection of the groundwater sample with the bailer, the water level is allowed to recover to within 80% of the original level measured prior to purging.
When sampling with a peristaltic or submersible electric pump, polyethylene (PE) tubing (or equivalent) is emplaced into the screened section of the monitoring well, and the pump is used to extract water through the tubing. When using the either of these methods, general water quality measurements including but not limited to pH, temperature, dissolved oxygen (DO), oxygen reductive potential (ORP), specific
conductivity and turbidity may be used as methods for determining when an adequate purge of the well has been conducted. When water quality parameters are measured, the resulting data are included in well purge forms or field notes specific to each site and sampling point. Following the purging of three well volumes of groundwater (in the case of the bailed well) or stability of
monitored measurements (in the case of the peristaltic or submersible electric pump), the groundwater sample(s) are introduced directly into sample containers provided by the laboratory to which samples are ultimately submitted for analysis. Any samples requiring chemical preservation are contained in pre-preserved container(s) provided by the laboratory.
Sampling is performed using new, disposable nitrile gloves for each sample location to ensure sample integrity and minimize the potential for cross contamination of samples or field personnel exposure to contaminants. Water Supply Well Sampling

Sampling of water supply wells is accomplished through the collection of a representative sample from an in-line water tap or other point accessible for sampling. Where possible, the sample is collected from a point prior to any filtration or point of entry (POE) system which might be installed on a well. In some cases, samples will be collected from both pre and post-POE locations. Prior to the collection of samples
through an in-place sampling point, the tap or sampling port is cleaned with an Alconox® and deionized
water solution, rinsed with deionized water, and again with an isopropyl alcohol (IPA) rinse. In the case of active supply wells (e.g., a well with a useable well pump with an active power supply), the well pump is energized and allowed to run for a minimum of ten (10) minutes time, after which a sample is
contained in laboratory grade sample containers as described in the previous section. Water quality
parameters may be (but are not necessarily) measured in association with the well purging. Supply wells without active power supplies are not generally sampled, as the well seal cannot be compromised by individuals not certified as a well contractor. However, in the case of a well with no
power supply or pump installed, samples could be obtained through the use of a bailer, peristaltic pump or
electric submersible pump.
Generalized Standard Operating Procedures (Not All Inclusive)

WithersRavenel
Our People. Your Success.
Decontamination Procedures Decontamination procedures employed in the performance of field activities will vary dependent upon
the method(s) of sampling performed at any site, but will generally include the following:
• Remove excess soil/sludge from any sampling equipment as needed, • Wash and scrub the equipment with a phosphate-free detergent such as Alconox® or Liquinox® in a contaminant-free tap water solution. Use a brush to remove particulate matter and surface films as necessary,
• Rinse thoroughly with tap water, • Rinse thoroughly with analyte-free water (deionized water),
 Rinse thoroughly with isopropyl alcohol, • Allow the equipment to air dry,
• Prevent inadvertent contamination during storage and transport (accomplished through storage of equipment in foil or plastic bags/sheeting). In the case of disposable bailers and tubing utilized for the purging and sampling of wells, these items may be decontaminated prior to their disposal. In general, no decontamination of these items is necessary
prior to their use in sampling.