WS-96299_96999_CA_SAR_20230505

7343 West Friendly Avenue, Suite J, Greensboro, NC 27410 [phone] Fax: [phone] www.envirotrac.com
Offices in CT, FL, GA, MA, NC, NH, NJ, NY, OH, PA, VA, WV

May 5, 2023
Mr. Gene Mao Guilford County Department of Health and Human Services 400 W. Market Street, Suite 300 Greensboro, North Carolina 27401
Reference: Still Room Soil Investigation
Gilbarco
7300 West Friendly Avenue
Greensboro, North Carolina
Dear Mr. Mao:
In July 2021 Gilbarco believes that approximately 300 gallons of Exxsol D60 Fluid was released from a UST system beneath the building (Figure 1). The UST system provides fluid for testing
equipment in the meter assembly calibration area of the plant (Figure 2). The UST system consists of two 2,000-gallon USTs and product piping from the USTs to the meter assembly calibration area. The bottom of both USTs is a depth of 8 feet below the floor slab. The bottom of the concrete
chases enclosing the piping is a depth of approximately 3 feet below the floor slab (Figures 3). Soil borings SS-1 through SS-11 and a temporary well were installed to assess the subsurface. Information from this investigation was previously reported in a letter dated October 22, 2021. Results of the previous soil sample analytical testing are included on Table 1. The laboratory report from the groundwater sample from temporary well TW-12 are included on Table 2. Although the investigation did not show evidence of a release on the order of 300 gallons, Gilbarco replaced product piping between the two product tanks and pumps with above ground piping. In October 2022, during a routine transfer of product from the supply tank to the working tank, it was suspected that approximately 100 gallons of Exxsol D60 was lost based on inventory control records. Gilbarco took the following actions:
1. Immediately took offline an underground transfer line of concern and replaced it with an above ground line (this lines’ integrity was later assessed and found to be a non-issue).
2. Replaced the existing TLS-350 tank monitoring system with a TLS-450 and replaced tank gauges in the tanks. 3. Began a process of pressure testing underground pressure lines which identified another
line of concern in January of 2023. 4. Immediately took the second underground line offline and have begun steps to have it replaced with an above ground line.
5. Once lines of concern were identified, scheduled soil borings and sampling to identify and isolate the suspected release.
7343 West Friendly Avenue, Suite J, Greensboro, NC 27410 [phone] Fax: [phone] www.envirotrac.com
Offices in CT, FL, GA, MA, NC, NH, NJ, NY, OH, PA, VA, WV
A summary of the soil sampling and analytical results is provided below. After the whole of the actions taken above and the results of the pressure testing and soil borings, Gilbarco now believes that the suspected product inventory losses were due to the older inventory control
equipment. No evidence of a release on the order of 100 gallons was found during the investigation conducted.
On January 23, 2023, one soil boring (SS-12) was installed adjacent to the Exxsol D60 working tank located in the Still Room. Six soil borings (SS-13, SS-14, SS-15, SS-16, SS-17, and SS-18 were installed along the product piping from the USTs to the testing equipment. The concrete floor slab was cored to access subsurface soil. The product lines are enclosed in concrete. Soil borings SS-14 encountered refusal at 40 inches. SS-16 encountered refusal at 30 inches due to a pipe and concrete. SS-17 encountered refusal at eight inches below the floor slab, believed to have occurred from encountering the concrete encasing the product piping. A hand auger was used to complete six borings (SS-12 through SS-16, and SS-18). Soil boring SS-12 was terminated at an approximate depth of 3 feet below the floor slab. Soil recovered from the boring included sand with silt and clay fill. Soil boring SS-13 was terminated at an approximate depth of 5 feet below the floor slab. Soil recovered from the boring included fine to medium sand fill and
poorly weathered rock at two feet below the slab floor. Soil boring SS-14 encountered refusal at an approximate depth of 40 inches below the floor slab. Soil recovered from the boring included firm fine to coarse sand with silt fill and a strong odor. Soil boring SS-15 was terminated at an
approximate depth of 5.11 feet below the floor slab. Soil recovered from the boring included fine to coarse sand with clay fill. Soil boring SS-16 encountered refusal at an approximate depth of 30 inches on a pipe surrounded by concrete. Soil recovered from the boring included fine to
coarse sand with silt fill. Soil boring SS-18 was terminated at an approximate depth of 5 feet below the floor slab. Soil recovered from the boring included fine to medium sand with silt fill. Groundwater was not encountered within the soil borings.
Two soil samples were collected from soil boring SS-1 (50 and 107 inches), SS-4 (68 and 131 inches), and SS-5 (99 and 132 inches) below the floor slab. One soil sample was collected from soil boring SS-2 (48 inches), SS-3 (78 inches), SS-7 (74 inches), SS-9 (73 inches), SS-10 (72 inches), SS-11 (73 inches), SS-12 (36 inches), SS-13 (60 inches), SS-14 (40 inches), SS-15 (59 inches), SS-16 (30 inches), and SS-18 (60 inches) below the floor slab. Soil samples were analyzed for volatile organic compounds (VOC) by EPA Method 8260. Samples were placed in laboratory prepared containers, labeled, preserved, and maintained under chain-of-custody until delivered to Pace Analytical Services, LLC (Pace) in Huntersville, North Carolina via laboratory courier. A Chain-of-Custody document was utilized throughout the collection and transportation of the samples.
Soil analytical results are summarized in Table 1 and the complete laboratory reports are enclosed. The results indicate that p-isopropyltoluene was detected in SS-1 at 50 and 107 inches, SS-4 at 68 and 131 inches, SS-5 at 132 inches and SS-11 at 73 inches at levels above
the Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs), and below the Residential MSCCs and Industrial MSCCs. Methylene Chloride was detected in SS-1 at 50 inches, SS-2 at 48 inches, SS-4 at 68 inches, SS-5 at 132 inches, SS-12 at 36 inches, SS-13 at 60 inches, SS-14 at 40 inches, SS-15 at 59 inches, SS-16 at 30 inches, and SS-18 at 60 inches above the Soil-to-Groundwater MSCC, and below the Residential MSCC and Industrial MSCC.
7343 West Friendly Avenue, Suite J, Greensboro, NC 27410 [phone] Fax: [phone] www.envirotrac.com
Offices in CT, FL, GA, MA, NC, NH, NJ, NY, OH, PA, VA, WV
Naphthalene was detected in SS-1 at 50 inches, SS-3 at 78 inches, SS-11 at 73 inches, SS-12
at 36 inches, and SS-13 at 60 inches above the Soil-to-Groundwater MSCC, and SS-4 at 68 inches was detected above the Residential MSCC and below the Industrial MSCC. 1,2,4-Trimethylbenzene was detected in SS-5 at 132 inches and SS-11 at 73 inches above the Soil-
to-Groundwater MSCC, and below the Residential MSCC and Industrial MSCC. N-Butylbenzene, sec-Butylbenzene, 4-methyl-2-pentanone and 1,3,5-timethylbenzene were detected in SS-11 at 73 inches above the Soil-to-Groundwater MSCC, and below the Residential MSCC and Industrial MSCC. Chloroform was detected in SS-12 at 36 inches, SS-13 at 60 inches, SS-14 at 40 inches, and SS-18 at 60 inches above the Soil-to-Groundwater MSCCs. Toluene was detected in SS-12 at 36 inches, SS-13 at 60 inches, SS-15 at 59 inches, and SS-18 at 60 inches above the Soil-to-Groundwater MSCCs. The remainder of the soil analytical results were below the Soil-to-Groundwater MSCCs or below the laboratory detection limits. Acetone and methylene chloride detected in the soil samples are believed to have originated from the laboratory. The laboratory analytical report is enclosed.
The week of March 27, 2023 Gilbarco identified a significant increase in Exxsol D60 usage. In reviewing operations, a calibration stand was brought online in early February. Gilbarco believes changes in calibration system supply line pressures resulted in losses of up to 1500
gallons between February through March 2023. Gilbarco shut down calibration system operations and has constructed and above ground supply line to service the calibration stands. Gilbarco has resolved integrity issues with the meter calibration supply system.
On April 3, 2023, seven soil borings were installed in the calibration area. Three soil borings (MAINLINE CORNER UNIT 8, MAINLINE DRAIN TO 7, and UNIT 4/6 MAINLINE SUPPLY AND
DRAIN) were installed along the product mainline piping. Four soil borings were installed perpendicular to the mainline (UNIT 7/8 SUPPLY UNIT 8 DRAIN, UNIT 7 DRAIN, UNUSED SUPPLY, UNIT 4/6 SUPPLY AND DRAIN, and UNIT 2 SUPPLY). A hand auger was used to complete the seven borings to a range in depth from 57-inches to 94-inches bgs. Soil encountered was consistent with previous soil borings. Groundwater was not encountered within the soil borings.
One soil sample was collected from soil boring UNIT 7/8 SUPPLY UNIT 8 DRAIN (82 inches), UNIT 7 DRAIN, UNUSED SUPPLY (94 inches), UNIT 2 SUPPLY (77 inches), MAINLINE CORNER UNIT 8 (57 inches), MAINLINE DRAIN TO 7 (74 inches), UNIT 4/6 SUPPLY AND DRAIN (78 inches), and UNIT 4/6 MAINLINE SUPPLY AND DRAIN (82 inches) below the floor slab. Soil samples were analyzed for volatile organic compounds (VOCs) by EPA Method 8260. Samples were placed in laboratory prepared containers, labeled, preserved, and maintained under chain-of-custody until delivered to Pace Analytical Services, LLC (Pace) in Huntersville,
North Carolina via laboratory courier. A Chain-of-Custody document was utilized throughout the collection and transportation of the samples.
Soil analytical results are summarized in Table 1 and the complete laboratory reports are
enclosed. The results indicate that p-isopropyltoluene was detected in MAINLINE CORNER UNIT 8 at 57 inches at levels above the Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCCs), and below the Residential MSCCs and Industrial MSCCs. Methylene Chloride was detected in UNIT 7/8 SUPPLY UNIT 8 DRAIN at 82 inches, UNIT 7 DRAIN, UNUSED SUPPLY at 94 inches, UNIT 2 SUPPLY at 77 inches, MAINLINE DRAIN TO 7 at 74
7343 West Friendly Avenue, Suite J, Greensboro, NC 27410 [phone] Fax: [phone] www.envirotrac.com
Offices in CT, FL, GA, MA, NC, NH, NJ, NY, OH, PA, VA, WV
inches, UNIT 4/6 SUPPLY AND DRAIN at 78 inches, and UNIT 4/6 MAINLINE SUPPLY AND
DRAIN at 82 inches above the Soil-to-Groundwater MSCC, and below the Residential MSCC and Industrial MSCC. P-Isopropyltoluene, 4-Methyl-2-pentanone, and 1,2,4-Trimethylbenzene were detected in MAINLINE CORNER UNIT 8 at 57 inches above the Soil-to-Groundwater
MSCC, and below the Residential MSCCs and Industrial MSCCs. The remainder of the soil analytical results were below the Soil-to-Groundwater MSCCs or below the laboratory detection limits. Acetone and methylene chloride detected in the soil samples are believed to have originated from the laboratory. The laboratory analytical report is enclosed.
EnviroTrac concludes that evidence of a release from the Exxsol D60 USTs and piping on the order of 100 gallons and the release of 1500 gallon in the calibration area were not observed or evident from the soil sample analytical results. EnviroTrac recommends that the product system and new inventory control equipment be monitored closely to ensure proper function.
EnviroTrac Ltd.
Christopher W. Hay, EI, RSM Principal
Enclosed: Table 1 – Soil Sample Analytical Results Table 2 – Groundwater Sample Analytical Results Figure 1 – Site Location Map Figure 2 – Still Room Location Map
Figure 3 – Sample Location Map Figure 4 – Sample Location Map 2 Analytical Laboratory Reports and Chain-of-Custodies
Cc: Mr. John Burke – Gilbarco
TABLES
TABLE 1: SOIL SAMPLE ANALYTICAL RESULTSAcetonen-Butylbenzenesec-Butylbenzene2-Butanone (MEK)ChloroformEthylbenzeneIsoopropylbenzenep-IsopropyltolueneMethylene Chloride4-Methyl-2-pentanone (MIBK)Methyl-tert-butyl ether (MTBE)Napthalenen-PropylbenzeneToluene1,2,4- Trimethylbenzene1,3.5- TrimethylbenzeneXylene (Total)24 2.4 2.2 16 0.37 8.0 1.7 0.12 0.023 0.42 0.085 0.2 1.4 5.4 6.6 6.6 6.014,000 782 1,560 9,380 20 60.3 1,564 1,560 93.8 1,250.0 156 5.5 1,560 1,250 156 156 3,120210,000 11,600 23,300 140,000 180 297 40,880 23,300 1,400 18,600 1,810 27 23,300 18,600 2,330 2,330 46,700Sample IDCollection Depth (inches bgs)Collection DateSS-1 50"50"07/08/212.30 BDL 0.694 0.761 BDL BDL BDL1.33 0.341BDL BDL0.308BDL BDL 1.77 1.16 0.282SS-1 107"107"07/08/210.261 BDL BDL BDL BDL BDL BDL0.133BDL BDL BDL 0.0269 BDL BDL BDL 0.103 0.0217SS-2 48 "48"07/08/21BDL BDL BDL BDL BDL BDL BDL BDL0.405BDL BDL 0.0844 BDL BDL BDL BDL BDLSS-3 7878"08/05/21BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL5.95BDL BDL BDL BDL BDLSS-4 6868"08/05/210.386 1.98 BDL BDL BDL BDL BDL2.06 0.160BDL BDL6.99BDL 0.09 2.32 0.702 0.105SS-4 131131"08/05/21BDL BDL BDL BDL BDL BDL BDL2.58BDL BDL BDL BDL BDL BDL BDL 2.71 BDLSS-5 9999"08/05/21BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0156SS-5 13213208/05/21BDL BDL 1.53 BDL BDL 0.15 BDL2.41 0.09770.258 BDL 0.155 0.795 BDL8.122.98 0.272SS-7 @ 6'274"09/03/21BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.029 BDL BDL BDL BDL BDL BDLSS-9 @ 6'173"09/03/21BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDLSS-10 @ 6'72"09/03/21BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.0204 BDL BDL BDL BDL BDL BDLSS-11 @ 6'173"09/03/21BDL7.56 11.1BDL BDL 0.535 BDL15.6BDL5.48BDL1.27BDL BDL43.5 18.53.01SS-12 @ 3'36"01/23/23BDL BDL BDL BDL0.624BDL BDL BDL3.15BDL BDL0.788BDL18.3BDL BDL BDLSS-13 @ 5'60"01/23/2312.3 BDL BDL BDL0.688BDL BDL BDL1.59BDL BDL0.494BDL10.9BDL BDL BDLSS-14 @ 40"40"01/23/23BDL BDL BDL BDL0.593BDL BDL BDL2.83BDL BDL BDL BDL14.8BDL BDL BDLSS-15 @ 59"59"01/23/23BDL BDL BDL BDL BDL BDL BDL BDL0.0946BDLBDL BDL BDL0.422 BDL BDL BDLSS-16 @ 30"30"01/23/23BDL BDL BDL BDL BDL BDL BDL BDL0.0533BDL BDL BDL BDL 0.197 BDL BDL BDLSS-18 @ 5'60"01/23/23BDL BDL BDL BDL0.684BDL BDL BDL2.49BDL BDL BDL BDL13.5BDL BDL BDLUnit 7/8 Supply Unit 8 Drain82"04/03/23BDL BDL 0.0127 BDL BDL BDL BDL BDL0.579BDL BDL BDL BDL BDL 0.0676 0.029 BDLUnit 7 Drain, Unused Supply94"04/03/23BDL BDL BDL BDL BDL BDL BDL BDL0.97BDL BDL BDL BDL BDL BDL BDL BDLUnit 2 Supply77"04/03/23BDL BDL BDL BDL BDL BDL BDL BDL1.21BDL BDL BDL BDL BDL BDL BDL BDLMainline Corner Unit 857"04/03/23BDL BDL4.42BDL BDL BDL 0.6455.57BDL4.6BDL BDL BDL BDL7.856.21 BDLMainline Drain to 774"04/03/23BDL BDL BDL BDL BDL BDL BDL BDL0.423BDL BDL BDL BDL BDL BDL BDL 0.0166Unit 4/6 Supply and Drain78"04/03/230.252 BDL BDL BDL BDL BDL BDL BDL0.234BDL BDL BDL BDL BDL BDL BDL BDLUnit 4/6 Mainline Supply & Drain82"04/03/23BDL BDL BDL BDL BDL BDL BDL BDL0.253BDL BDL BDL BDL BDL BDL BDL BDLNotes:Results presented in milligrams per kilogram (mg/kg)MSCC = Maximum Soil Contaminant Concentration inches bgs = inches below ground surfaceBold denotes concentration is greater than the comparison criteriaBDL = Not detected at or above laboratory detection limitVOCs by EPA Method 8260D (mg/kg)COMPARISON CRITERIAParameterAnalytical MethodIndustrial MSCCResidential MSCCSoil-to-Groundwater MSCC11.990009.001 of 1May 2023
TABLE 2: GROUNDWATER SAMPLE ANALYTICAL RESULTS
Volatile Organic Compounds by Standard Method 8260(µg/L)
Ethyl-
benzene
p-Isopropyl-
toluene
Naph-
thalene
Toluene Total Xylenes
600 NE 6 600 500
TW-12 01/12/22 6.1 18.2 4.6 2.5 10.7
NOTES:
2L Standard = North Carolina Groundwater Standard (15A NCAC 2L .0202), effective April 1, 2013.
μg/L = Micrograms per liter, analogous to parts per billion
BOLD = Concentration exceeds the 2L Standard
Well ID Collection
Date
2L Standard
11.990009.00 1 of 1 May 2023
The groundwater depth for TM-12 was 17 feet bgs.
FIGURES

ANALYTICAL LABORATORY REPORTS AND
CHAIN-OF-CUSTODIES

#=CL#
July 14, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92548694
92548694
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
GILBARO
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on July 09, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lindsey N Wooten
[e-mail]
Project Manager
[phone]
Enclosures
cc: Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92548694
GILBARO
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92548694
GILBARO
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92548694001 SS-1 50"EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92548694002 SS-1 107"EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92548694003 SS-2 48"EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92548694
GILBARO
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92548694001 SS-1 50"
Acetone 2300 ug/kg 07/13/21 05:22735EPA 8260D
2-Butanone (MEK)761 ug/kg 07/13/21 05:22735EPA 8260D
sec-Butylbenzene 694 ug/kg 07/13/21 05:2236.8EPA 8260D
p-Isopropyltoluene 1330 ug/kg 07/13/21 05:2236.8EPA 8260D
Methylene Chloride 341 ug/kg 07/13/21 05:22147EPA 8260D
Naphthalene 308 ug/kg 07/13/21 05:2236.8EPA 8260D
1,2,4-Trimethylbenzene 1770 ug/kg 07/13/21 05:2236.8EPA 8260D
1,3,5-Trimethylbenzene 1160 ug/kg 07/13/21 05:2236.8EPA 8260D
Xylene (Total)282 ug/kg 07/13/21 05:2273.5EPA 8260D
m&p-Xylene 137 ug/kg 07/13/21 05:2273.5EPA 8260D
o-Xylene 145 ug/kg 07/13/21 05:2236.8EPA 8260D
Percent Moisture 17.5 %07/09/21 17:04 N20.10SW-846
92548694002 SS-1 107"
Acetone 261 ug/kg 07/13/21 13:43245EPA 8260D
p-Isopropyltoluene 133 ug/kg 07/13/21 13:4312.3EPA 8260D
Naphthalene 26.9 ug/kg 07/13/21 13:4312.3EPA 8260D
1,3,5-Trimethylbenzene 103 ug/kg 07/13/21 13:4312.3EPA 8260D
o-Xylene 21.7 ug/kg 07/13/21 13:4312.3EPA 8260D
Percent Moisture 33.7 %07/09/21 17:05 N20.10SW-846
92548694003 SS-2 48"
Methylene Chloride 405 ug/kg 07/13/21 05:59154EPA 8260D
Naphthalene 84.4 ug/kg 07/13/21 05:5938.6EPA 8260D
Percent Moisture 11.1 %07/09/21 17:05 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548694
GILBARO
Sample: SS-1 50"Lab ID: 92548694001 Collected: 07/08/21 11:25 Received: 07/09/21 13:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 2300 ug/kg 07/13/21 05:22 67-64-107/12/21 14:10735 4
Benzene ND ug/kg 07/13/21 05:22 71-43-207/12/21 14:1036.8 4
Bromobenzene ND ug/kg 07/13/21 05:22 108-86-107/12/21 14:1036.8 4
Bromochloromethane ND ug/kg 07/13/21 05:22 74-97-507/12/21 14:1036.8 4
Bromodichloromethane ND ug/kg 07/13/21 05:22 75-27-407/12/21 14:1036.8 4
Bromoform ND ug/kg 07/13/21 05:22 75-25-207/12/21 14:1036.8 4
Bromomethane ND ug/kg 07/13/21 05:22 74-83-9 IK07/12/21 14:1073.5 4
2-Butanone (MEK)761 ug/kg 07/13/21 05:22 78-93-307/12/21 14:10735 4
n-Butylbenzene ND ug/kg 07/13/21 05:22 104-51-807/12/21 14:1036.8 4
sec-Butylbenzene 694 ug/kg 07/13/21 05:22 135-98-807/12/21 14:1036.8 4
tert-Butylbenzene ND ug/kg 07/13/21 05:22 98-06-607/12/21 14:1036.8 4
Carbon tetrachloride ND ug/kg 07/13/21 05:22 56-23-507/12/21 14:1036.8 4
Chlorobenzene ND ug/kg 07/13/21 05:22 108-90-707/12/21 14:1036.8 4
Chloroethane ND ug/kg 07/13/21 05:22 75-00-307/12/21 14:1073.5 4
Chloroform ND ug/kg 07/13/21 05:22 67-66-307/12/21 14:1036.8 4
Chloromethane ND ug/kg 07/13/21 05:22 74-87-307/12/21 14:1073.5 4
2-Chlorotoluene ND ug/kg 07/13/21 05:22 95-49-807/12/21 14:1036.8 4
4-Chlorotoluene ND ug/kg 07/13/21 05:22 106-43-407/12/21 14:1036.8 4
1,2-Dibromo-3-chloropropane ND ug/kg 07/13/21 05:22 96-12-807/12/21 14:1036.8 4
Dibromochloromethane ND ug/kg 07/13/21 05:22 124-48-107/12/21 14:1036.8 4
1,2-Dibromoethane (EDB)ND ug/kg 07/13/21 05:22 106-93-407/12/21 14:1036.8 4
Dibromomethane ND ug/kg 07/13/21 05:22 74-95-307/12/21 14:1036.8 4
1,2-Dichlorobenzene ND ug/kg 07/13/21 05:22 95-50-107/12/21 14:1036.8 4
1,3-Dichlorobenzene ND ug/kg 07/13/21 05:22 541-73-107/12/21 14:1036.8 4
1,4-Dichlorobenzene ND ug/kg 07/13/21 05:22 106-46-707/12/21 14:1036.8 4
Dichlorodifluoromethane ND ug/kg 07/13/21 05:22 75-71-807/12/21 14:1073.5 4
1,1-Dichloroethane ND ug/kg 07/13/21 05:22 75-34-307/12/21 14:1036.8 4
1,2-Dichloroethane ND ug/kg 07/13/21 05:22 107-06-207/12/21 14:1036.8 4
1,1-Dichloroethene ND ug/kg 07/13/21 05:22 75-35-407/12/21 14:1036.8 4
cis-1,2-Dichloroethene ND ug/kg 07/13/21 05:22 156-59-207/12/21 14:1036.8 4
trans-1,2-Dichloroethene ND ug/kg 07/13/21 05:22 156-60-507/12/21 14:1036.8 4
1,2-Dichloropropane ND ug/kg 07/13/21 05:22 78-87-507/12/21 14:1036.8 4
1,3-Dichloropropane ND ug/kg 07/13/21 05:22 142-28-907/12/21 14:1036.8 4
2,2-Dichloropropane ND ug/kg 07/13/21 05:22 594-20-707/12/21 14:1036.8 4
1,1-Dichloropropene ND ug/kg 07/13/21 05:22 563-58-607/12/21 14:1036.8 4
cis-1,3-Dichloropropene ND ug/kg 07/13/21 05:22 10061-01-507/12/21 14:1036.8 4
trans-1,3-Dichloropropene ND ug/kg 07/13/21 05:22 10061-02-607/12/21 14:1036.8 4
Diisopropyl ether ND ug/kg 07/13/21 05:22 108-20-307/12/21 14:1036.8 4
Ethylbenzene ND ug/kg 07/13/21 05:22 100-41-407/12/21 14:1036.8 4
Hexachloro-1,3-butadiene ND ug/kg 07/13/21 05:22 87-68-307/12/21 14:1073.5 4
2-Hexanone ND ug/kg 07/13/21 05:22 591-78-607/12/21 14:10368 4
Isopropylbenzene (Cumene)ND ug/kg 07/13/21 05:22 98-82-807/12/21 14:1036.8 4
p-Isopropyltoluene 1330 ug/kg 07/13/21 05:22 99-87-607/12/21 14:1036.8 4
Methylene Chloride 341 ug/kg 07/13/21 05:22 75-09-207/12/21 14:10147 4
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/13/21 05:22 108-10-107/12/21 14:10368 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548694
GILBARO
Sample: SS-1 50"Lab ID: 92548694001 Collected: 07/08/21 11:25 Received: 07/09/21 13:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 07/13/21 05:22 1634-04-407/12/21 14:1036.8 4
Naphthalene 308 ug/kg 07/13/21 05:22 91-20-307/12/21 14:1036.8 4
n-Propylbenzene ND ug/kg 07/13/21 05:22 103-65-107/12/21 14:1036.8 4
Styrene ND ug/kg 07/13/21 05:22 100-42-507/12/21 14:1036.8 4
1,1,1,2-Tetrachloroethane ND ug/kg 07/13/21 05:22 630-20-607/12/21 14:1036.8 4
1,1,2,2-Tetrachloroethane ND ug/kg 07/13/21 05:22 79-34-507/12/21 14:1036.8 4
Tetrachloroethene ND ug/kg 07/13/21 05:22 127-18-407/12/21 14:1036.8 4
Toluene ND ug/kg 07/13/21 05:22 108-88-307/12/21 14:1036.8 4
1,2,3-Trichlorobenzene ND ug/kg 07/13/21 05:22 87-61-607/12/21 14:1036.8 4
1,2,4-Trichlorobenzene ND ug/kg 07/13/21 05:22 120-82-107/12/21 14:1036.8 4
1,1,1-Trichloroethane ND ug/kg 07/13/21 05:22 71-55-607/12/21 14:1036.8 4
1,1,2-Trichloroethane ND ug/kg 07/13/21 05:22 79-00-507/12/21 14:1036.8 4
Trichloroethene ND ug/kg 07/13/21 05:22 79-01-607/12/21 14:1036.8 4
Trichlorofluoromethane ND ug/kg 07/13/21 05:22 75-69-407/12/21 14:1036.8 4
1,2,3-Trichloropropane ND ug/kg 07/13/21 05:22 96-18-407/12/21 14:1036.8 4
1,2,4-Trimethylbenzene 1770 ug/kg 07/13/21 05:22 95-63-607/12/21 14:1036.8 4
1,3,5-Trimethylbenzene 1160 ug/kg 07/13/21 05:22 108-67-807/12/21 14:1036.8 4
Vinyl acetate ND ug/kg 07/13/21 05:22 108-05-407/12/21 14:10368 4
Vinyl chloride ND ug/kg 07/13/21 05:22 75-01-407/12/21 14:1073.5 4
Xylene (Total)282 ug/kg 07/13/21 05:22 1330-20-707/12/21 14:1073.5 4
m&p-Xylene 137 ug/kg 07/13/21 05:22 179601-23-107/12/21 14:1073.5 4
o-Xylene 145 ug/kg 07/13/21 05:22 95-47-607/12/21 14:1036.8 4
Surrogates
Toluene-d8 (S)103 %07/13/21 05:22 2037-26-5 D307/12/21 14:1070-130 4
4-Bromofluorobenzene (S)123 %07/13/21 05:22 460-00-407/12/21 14:1069-134 4
1,2-Dichloroethane-d4 (S)110 %07/13/21 05:22 17060-07-007/12/21 14:1070-130 4
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.5 %07/09/21 17:04 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548694
GILBARO
Sample: SS-1 107"Lab ID: 92548694002 Collected: 07/08/21 11:36 Received: 07/09/21 13:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 261 ug/kg 07/13/21 13:43 67-64-107/13/21 10:49245 1
Benzene ND ug/kg 07/13/21 13:43 71-43-207/13/21 10:4912.3 1
Bromobenzene ND ug/kg 07/13/21 13:43 108-86-107/13/21 10:4912.3 1
Bromochloromethane ND ug/kg 07/13/21 13:43 74-97-507/13/21 10:4912.3 1
Bromodichloromethane ND ug/kg 07/13/21 13:43 75-27-407/13/21 10:4912.3 1
Bromoform ND ug/kg 07/13/21 13:43 75-25-207/13/21 10:4912.3 1
Bromomethane ND ug/kg 07/13/21 13:43 74-83-9 IK07/13/21 10:4924.5 1
2-Butanone (MEK)ND ug/kg 07/13/21 13:43 78-93-307/13/21 10:49245 1
n-Butylbenzene ND ug/kg 07/13/21 13:43 104-51-807/13/21 10:4912.3 1
sec-Butylbenzene ND ug/kg 07/13/21 13:43 135-98-807/13/21 10:4912.3 1
tert-Butylbenzene ND ug/kg 07/13/21 13:43 98-06-607/13/21 10:4912.3 1
Carbon tetrachloride ND ug/kg 07/13/21 13:43 56-23-507/13/21 10:4912.3 1
Chlorobenzene ND ug/kg 07/13/21 13:43 108-90-707/13/21 10:4912.3 1
Chloroethane ND ug/kg 07/13/21 13:43 75-00-307/13/21 10:4924.5 1
Chloroform ND ug/kg 07/13/21 13:43 67-66-307/13/21 10:4912.3 1
Chloromethane ND ug/kg 07/13/21 13:43 74-87-307/13/21 10:4924.5 1
2-Chlorotoluene ND ug/kg 07/13/21 13:43 95-49-807/13/21 10:4912.3 1
4-Chlorotoluene ND ug/kg 07/13/21 13:43 106-43-407/13/21 10:4912.3 1
1,2-Dibromo-3-chloropropane ND ug/kg 07/13/21 13:43 96-12-8 v207/13/21 10:4912.3 1
Dibromochloromethane ND ug/kg 07/13/21 13:43 124-48-107/13/21 10:4912.3 1
1,2-Dibromoethane (EDB)ND ug/kg 07/13/21 13:43 106-93-407/13/21 10:4912.3 1
Dibromomethane ND ug/kg 07/13/21 13:43 74-95-307/13/21 10:4912.3 1
1,2-Dichlorobenzene ND ug/kg 07/13/21 13:43 95-50-107/13/21 10:4912.3 1
1,3-Dichlorobenzene ND ug/kg 07/13/21 13:43 541-73-107/13/21 10:4912.3 1
1,4-Dichlorobenzene ND ug/kg 07/13/21 13:43 106-46-707/13/21 10:4912.3 1
Dichlorodifluoromethane ND ug/kg 07/13/21 13:43 75-71-807/13/21 10:4924.5 1
1,1-Dichloroethane ND ug/kg 07/13/21 13:43 75-34-307/13/21 10:4912.3 1
1,2-Dichloroethane ND ug/kg 07/13/21 13:43 107-06-207/13/21 10:4912.3 1
1,1-Dichloroethene ND ug/kg 07/13/21 13:43 75-35-407/13/21 10:4912.3 1
cis-1,2-Dichloroethene ND ug/kg 07/13/21 13:43 156-59-207/13/21 10:4912.3 1
trans-1,2-Dichloroethene ND ug/kg 07/13/21 13:43 156-60-507/13/21 10:4912.3 1
1,2-Dichloropropane ND ug/kg 07/13/21 13:43 78-87-507/13/21 10:4912.3 1
1,3-Dichloropropane ND ug/kg 07/13/21 13:43 142-28-907/13/21 10:4912.3 1
2,2-Dichloropropane ND ug/kg 07/13/21 13:43 594-20-707/13/21 10:4912.3 1
1,1-Dichloropropene ND ug/kg 07/13/21 13:43 563-58-607/13/21 10:4912.3 1
cis-1,3-Dichloropropene ND ug/kg 07/13/21 13:43 10061-01-507/13/21 10:4912.3 1
trans-1,3-Dichloropropene ND ug/kg 07/13/21 13:43 10061-02-607/13/21 10:4912.3 1
Diisopropyl ether ND ug/kg 07/13/21 13:43 108-20-307/13/21 10:4912.3 1
Ethylbenzene ND ug/kg 07/13/21 13:43 100-41-407/13/21 10:4912.3 1
Hexachloro-1,3-butadiene ND ug/kg 07/13/21 13:43 87-68-307/13/21 10:4924.5 1
2-Hexanone ND ug/kg 07/13/21 13:43 591-78-607/13/21 10:49123 1
Isopropylbenzene (Cumene)ND ug/kg 07/13/21 13:43 98-82-807/13/21 10:4912.3 1
p-Isopropyltoluene 133 ug/kg 07/13/21 13:43 99-87-607/13/21 10:4912.3 1
Methylene Chloride ND ug/kg 07/13/21 13:43 75-09-207/13/21 10:4949.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/13/21 13:43 108-10-107/13/21 10:49123 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548694
GILBARO
Sample: SS-1 107"Lab ID: 92548694002 Collected: 07/08/21 11:36 Received: 07/09/21 13:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 07/13/21 13:43 1634-04-407/13/21 10:4912.3 1
Naphthalene 26.9 ug/kg 07/13/21 13:43 91-20-307/13/21 10:4912.3 1
n-Propylbenzene ND ug/kg 07/13/21 13:43 103-65-107/13/21 10:4912.3 1
Styrene ND ug/kg 07/13/21 13:43 100-42-507/13/21 10:4912.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 07/13/21 13:43 630-20-607/13/21 10:4912.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 07/13/21 13:43 79-34-507/13/21 10:4912.3 1
Tetrachloroethene ND ug/kg 07/13/21 13:43 127-18-407/13/21 10:4912.3 1
Toluene ND ug/kg 07/13/21 13:43 108-88-307/13/21 10:4912.3 1
1,2,3-Trichlorobenzene ND ug/kg 07/13/21 13:43 87-61-607/13/21 10:4912.3 1
1,2,4-Trichlorobenzene ND ug/kg 07/13/21 13:43 120-82-107/13/21 10:4912.3 1
1,1,1-Trichloroethane ND ug/kg 07/13/21 13:43 71-55-607/13/21 10:4912.3 1
1,1,2-Trichloroethane ND ug/kg 07/13/21 13:43 79-00-507/13/21 10:4912.3 1
Trichloroethene ND ug/kg 07/13/21 13:43 79-01-607/13/21 10:4912.3 1
Trichlorofluoromethane ND ug/kg 07/13/21 13:43 75-69-407/13/21 10:4912.3 1
1,2,3-Trichloropropane ND ug/kg 07/13/21 13:43 96-18-407/13/21 10:4912.3 1
1,2,4-Trimethylbenzene ND ug/kg 07/13/21 13:43 95-63-607/13/21 10:4912.3 1
1,3,5-Trimethylbenzene 103 ug/kg 07/13/21 13:43 108-67-807/13/21 10:4912.3 1
Vinyl acetate ND ug/kg 07/13/21 13:43 108-05-407/13/21 10:49123 1
Vinyl chloride ND ug/kg 07/13/21 13:43 75-01-407/13/21 10:4924.5 1
Xylene (Total)ND ug/kg 07/13/21 13:43 1330-20-707/13/21 10:4924.5 1
m&p-Xylene ND ug/kg 07/13/21 13:43 179601-23-107/13/21 10:4924.5 1
o-Xylene 21.7 ug/kg 07/13/21 13:43 95-47-607/13/21 10:4912.3 1
Surrogates
Toluene-d8 (S)101 %07/13/21 13:43 2037-26-507/13/21 10:4970-130 1
4-Bromofluorobenzene (S)123 %07/13/21 13:43 460-00-407/13/21 10:4969-134 1
1,2-Dichloroethane-d4 (S)104 %07/13/21 13:43 17060-07-007/13/21 10:4970-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 33.7 %07/09/21 17:05 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548694
GILBARO
Sample: SS-2 48"Lab ID: 92548694003 Collected: 07/08/21 14:50 Received: 07/09/21 13:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 07/13/21 05:59 67-64-107/12/21 14:10771 4
Benzene ND ug/kg 07/13/21 05:59 71-43-207/12/21 14:1038.6 4
Bromobenzene ND ug/kg 07/13/21 05:59 108-86-107/12/21 14:1038.6 4
Bromochloromethane ND ug/kg 07/13/21 05:59 74-97-507/12/21 14:1038.6 4
Bromodichloromethane ND ug/kg 07/13/21 05:59 75-27-407/12/21 14:1038.6 4
Bromoform ND ug/kg 07/13/21 05:59 75-25-207/12/21 14:1038.6 4
Bromomethane ND ug/kg 07/13/21 05:59 74-83-9 IK07/12/21 14:1077.1 4
2-Butanone (MEK)ND ug/kg 07/13/21 05:59 78-93-307/12/21 14:10771 4
n-Butylbenzene ND ug/kg 07/13/21 05:59 104-51-807/12/21 14:1038.6 4
sec-Butylbenzene ND ug/kg 07/13/21 05:59 135-98-807/12/21 14:1038.6 4
tert-Butylbenzene ND ug/kg 07/13/21 05:59 98-06-607/12/21 14:1038.6 4
Carbon tetrachloride ND ug/kg 07/13/21 05:59 56-23-507/12/21 14:1038.6 4
Chlorobenzene ND ug/kg 07/13/21 05:59 108-90-707/12/21 14:1038.6 4
Chloroethane ND ug/kg 07/13/21 05:59 75-00-307/12/21 14:1077.1 4
Chloroform ND ug/kg 07/13/21 05:59 67-66-307/12/21 14:1038.6 4
Chloromethane ND ug/kg 07/13/21 05:59 74-87-307/12/21 14:1077.1 4
2-Chlorotoluene ND ug/kg 07/13/21 05:59 95-49-807/12/21 14:1038.6 4
4-Chlorotoluene ND ug/kg 07/13/21 05:59 106-43-407/12/21 14:1038.6 4
1,2-Dibromo-3-chloropropane ND ug/kg 07/13/21 05:59 96-12-807/12/21 14:1038.6 4
Dibromochloromethane ND ug/kg 07/13/21 05:59 124-48-107/12/21 14:1038.6 4
1,2-Dibromoethane (EDB)ND ug/kg 07/13/21 05:59 106-93-407/12/21 14:1038.6 4
Dibromomethane ND ug/kg 07/13/21 05:59 74-95-307/12/21 14:1038.6 4
1,2-Dichlorobenzene ND ug/kg 07/13/21 05:59 95-50-107/12/21 14:1038.6 4
1,3-Dichlorobenzene ND ug/kg 07/13/21 05:59 541-73-107/12/21 14:1038.6 4
1,4-Dichlorobenzene ND ug/kg 07/13/21 05:59 106-46-707/12/21 14:1038.6 4
Dichlorodifluoromethane ND ug/kg 07/13/21 05:59 75-71-807/12/21 14:1077.1 4
1,1-Dichloroethane ND ug/kg 07/13/21 05:59 75-34-307/12/21 14:1038.6 4
1,2-Dichloroethane ND ug/kg 07/13/21 05:59 107-06-207/12/21 14:1038.6 4
1,1-Dichloroethene ND ug/kg 07/13/21 05:59 75-35-407/12/21 14:1038.6 4
cis-1,2-Dichloroethene ND ug/kg 07/13/21 05:59 156-59-207/12/21 14:1038.6 4
trans-1,2-Dichloroethene ND ug/kg 07/13/21 05:59 156-60-507/12/21 14:1038.6 4
1,2-Dichloropropane ND ug/kg 07/13/21 05:59 78-87-507/12/21 14:1038.6 4
1,3-Dichloropropane ND ug/kg 07/13/21 05:59 142-28-907/12/21 14:1038.6 4
2,2-Dichloropropane ND ug/kg 07/13/21 05:59 594-20-707/12/21 14:1038.6 4
1,1-Dichloropropene ND ug/kg 07/13/21 05:59 563-58-607/12/21 14:1038.6 4
cis-1,3-Dichloropropene ND ug/kg 07/13/21 05:59 10061-01-507/12/21 14:1038.6 4
trans-1,3-Dichloropropene ND ug/kg 07/13/21 05:59 10061-02-607/12/21 14:1038.6 4
Diisopropyl ether ND ug/kg 07/13/21 05:59 108-20-307/12/21 14:1038.6 4
Ethylbenzene ND ug/kg 07/13/21 05:59 100-41-407/12/21 14:1038.6 4
Hexachloro-1,3-butadiene ND ug/kg 07/13/21 05:59 87-68-307/12/21 14:1077.1 4
2-Hexanone ND ug/kg 07/13/21 05:59 591-78-607/12/21 14:10386 4
Isopropylbenzene (Cumene)ND ug/kg 07/13/21 05:59 98-82-807/12/21 14:1038.6 4
p-Isopropyltoluene ND ug/kg 07/13/21 05:59 99-87-607/12/21 14:1038.6 4
Methylene Chloride 405 ug/kg 07/13/21 05:59 75-09-207/12/21 14:10154 4
4-Methyl-2-pentanone (MIBK)ND ug/kg 07/13/21 05:59 108-10-107/12/21 14:10386 4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92548694
GILBARO
Sample: SS-2 48"Lab ID: 92548694003 Collected: 07/08/21 14:50 Received: 07/09/21 13:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 07/13/21 05:59 1634-04-407/12/21 14:1038.6 4
Naphthalene 84.4 ug/kg 07/13/21 05:59 91-20-307/12/21 14:1038.6 4
n-Propylbenzene ND ug/kg 07/13/21 05:59 103-65-107/12/21 14:1038.6 4
Styrene ND ug/kg 07/13/21 05:59 100-42-507/12/21 14:1038.6 4
1,1,1,2-Tetrachloroethane ND ug/kg 07/13/21 05:59 630-20-607/12/21 14:1038.6 4
1,1,2,2-Tetrachloroethane ND ug/kg 07/13/21 05:59 79-34-507/12/21 14:1038.6 4
Tetrachloroethene ND ug/kg 07/13/21 05:59 127-18-407/12/21 14:1038.6 4
Toluene ND ug/kg 07/13/21 05:59 108-88-307/12/21 14:1038.6 4
1,2,3-Trichlorobenzene ND ug/kg 07/13/21 05:59 87-61-607/12/21 14:1038.6 4
1,2,4-Trichlorobenzene ND ug/kg 07/13/21 05:59 120-82-107/12/21 14:1038.6 4
1,1,1-Trichloroethane ND ug/kg 07/13/21 05:59 71-55-607/12/21 14:1038.6 4
1,1,2-Trichloroethane ND ug/kg 07/13/21 05:59 79-00-507/12/21 14:1038.6 4
Trichloroethene ND ug/kg 07/13/21 05:59 79-01-607/12/21 14:1038.6 4
Trichlorofluoromethane ND ug/kg 07/13/21 05:59 75-69-407/12/21 14:1038.6 4
1,2,3-Trichloropropane ND ug/kg 07/13/21 05:59 96-18-407/12/21 14:1038.6 4
1,2,4-Trimethylbenzene ND ug/kg 07/13/21 05:59 95-63-607/12/21 14:1038.6 4
1,3,5-Trimethylbenzene ND ug/kg 07/13/21 05:59 108-67-807/12/21 14:1038.6 4
Vinyl acetate ND ug/kg 07/13/21 05:59 108-05-407/12/21 14:10386 4
Vinyl chloride ND ug/kg 07/13/21 05:59 75-01-407/12/21 14:1077.1 4
Xylene (Total)ND ug/kg 07/13/21 05:59 1330-20-707/12/21 14:1077.1 4
m&p-Xylene ND ug/kg 07/13/21 05:59 179601-23-107/12/21 14:1077.1 4
o-Xylene ND ug/kg 07/13/21 05:59 95-47-607/12/21 14:1038.6 4
Surrogates
Toluene-d8 (S)102 %07/13/21 05:59 2037-26-5 D307/12/21 14:1070-130 4
4-Bromofluorobenzene (S)122 %07/13/21 05:59 460-00-407/12/21 14:1069-134 4
1,2-Dichloroethane-d4 (S)108 %07/13/21 05:59 17060-07-007/12/21 14:1070-130 4
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.1 %07/09/21 17:05 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632773
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92548694001, 92548694003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3324054
Associated Lab Samples:92548694001, 92548694003
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/12/21 23:31
1,1,1-Trichloroethane ug/kg ND 5.0 07/12/21 23:31
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/12/21 23:31
1,1,2-Trichloroethane ug/kg ND 5.0 07/12/21 23:31
1,1-Dichloroethane ug/kg ND 5.0 07/12/21 23:31
1,1-Dichloroethene ug/kg ND 5.0 07/12/21 23:31
1,1-Dichloropropene ug/kg ND 5.0 07/12/21 23:31
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/12/21 23:31
1,2,3-Trichloropropane ug/kg ND 5.0 07/12/21 23:31
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/12/21 23:31
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/12/21 23:31
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 07/12/21 23:31
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/12/21 23:31
1,2-Dichlorobenzene ug/kg ND 5.0 07/12/21 23:31
1,2-Dichloroethane ug/kg ND 5.0 07/12/21 23:31
1,2-Dichloropropane ug/kg ND 5.0 07/12/21 23:31
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/12/21 23:31
1,3-Dichlorobenzene ug/kg ND 5.0 07/12/21 23:31
1,3-Dichloropropane ug/kg ND 5.0 07/12/21 23:31
1,4-Dichlorobenzene ug/kg ND 5.0 07/12/21 23:31
2,2-Dichloropropane ug/kg ND 5.0 07/12/21 23:31
2-Butanone (MEK)ug/kg ND 100 07/12/21 23:31
2-Chlorotoluene ug/kg ND 5.0 07/12/21 23:31
2-Hexanone ug/kg ND 50.0 07/12/21 23:31
4-Chlorotoluene ug/kg ND 5.0 07/12/21 23:31
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/12/21 23:31
Acetone ug/kg ND 100 07/12/21 23:31
Benzene ug/kg ND 5.0 07/12/21 23:31
Bromobenzene ug/kg ND 5.0 07/12/21 23:31
Bromochloromethane ug/kg ND 5.0 07/12/21 23:31
Bromodichloromethane ug/kg ND 5.0 07/12/21 23:31
Bromoform ug/kg ND 5.0 07/12/21 23:31
Bromomethane ug/kg ND 10.0 IK07/12/21 23:31
Carbon tetrachloride ug/kg ND 5.0 07/12/21 23:31
Chlorobenzene ug/kg ND 5.0 07/12/21 23:31
Chloroethane ug/kg ND 10.0 07/12/21 23:31
Chloroform ug/kg ND 5.0 07/12/21 23:31
Chloromethane ug/kg ND 10.0 07/12/21 23:31
cis-1,2-Dichloroethene ug/kg ND 5.0 07/12/21 23:31
cis-1,3-Dichloropropene ug/kg ND 5.0 07/12/21 23:31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3324054
Associated Lab Samples:92548694001, 92548694003
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 07/12/21 23:31
Dibromomethane ug/kg ND 5.0 07/12/21 23:31
Dichlorodifluoromethane ug/kg ND 10.0 07/12/21 23:31
Diisopropyl ether ug/kg ND 5.0 07/12/21 23:31
Ethylbenzene ug/kg ND 5.0 07/12/21 23:31
Hexachloro-1,3-butadiene ug/kg ND 10.0 07/12/21 23:31
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/12/21 23:31
m&p-Xylene ug/kg ND 10.0 07/12/21 23:31
Methyl-tert-butyl ether ug/kg ND 5.0 07/12/21 23:31
Methylene Chloride ug/kg ND 20.0 07/12/21 23:31
n-Butylbenzene ug/kg ND 5.0 07/12/21 23:31
n-Propylbenzene ug/kg ND 5.0 07/12/21 23:31
Naphthalene ug/kg ND 5.0 07/12/21 23:31
o-Xylene ug/kg ND 5.0 07/12/21 23:31
p-Isopropyltoluene ug/kg ND 5.0 07/12/21 23:31
sec-Butylbenzene ug/kg ND 5.0 07/12/21 23:31
Styrene ug/kg ND 5.0 07/12/21 23:31
tert-Butylbenzene ug/kg ND 5.0 07/12/21 23:31
Tetrachloroethene ug/kg ND 5.0 07/12/21 23:31
Toluene ug/kg ND 5.0 07/12/21 23:31
trans-1,2-Dichloroethene ug/kg ND 5.0 07/12/21 23:31
trans-1,3-Dichloropropene ug/kg ND 5.0 07/12/21 23:31
Trichloroethene ug/kg ND 5.0 07/12/21 23:31
Trichlorofluoromethane ug/kg ND 5.0 07/12/21 23:31
Vinyl acetate ug/kg ND 50.0 07/12/21 23:31
Vinyl chloride ug/kg ND 10.0 07/12/21 23:31
Xylene (Total)ug/kg ND 10.0 07/12/21 23:31
1,2-Dichloroethane-d4 (S)%112 70-130 07/12/21 23:31
4-Bromofluorobenzene (S)%99 69-134 07/12/21 23:31
Toluene-d8 (S)%100 70-130 07/12/21 23:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324055LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11301250 91 70-130
1,1,1-Trichloroethane ug/kg 11101250 88 70-130
1,1,2,2-Tetrachloroethane ug/kg 10501250 84 70-130
1,1,2-Trichloroethane ug/kg 10601250 85 70-130
1,1-Dichloroethane ug/kg 12301250 98 70-130
1,1-Dichloroethene ug/kg 12101250 97 70-130
1,1-Dichloropropene ug/kg 11901250 95 70-130
1,2,3-Trichlorobenzene ug/kg 10801250 86 65-130
1,2,3-Trichloropropane ug/kg 10901250 87 70-130
1,2,4-Trichlorobenzene ug/kg 10801250 86 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324055LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 10801250 86 70-130
1,2-Dibromo-3-chloropropane ug/kg 10601250 85 70-130
1,2-Dibromoethane (EDB)ug/kg 11201250 90 70-130
1,2-Dichlorobenzene ug/kg 10801250 86 70-130
1,2-Dichloroethane ug/kg 11201250 89 63-130
1,2-Dichloropropane ug/kg 11601250 92 70-130
1,3,5-Trimethylbenzene ug/kg 11001250 88 70-130
1,3-Dichlorobenzene ug/kg 10801250 87 70-130
1,3-Dichloropropane ug/kg 11301250 90 70-130
1,4-Dichlorobenzene ug/kg 10801250 86 70-130
2,2-Dichloropropane ug/kg 10401250 83 66-130
2-Butanone (MEK)ug/kg 23002500 92 70-130
2-Chlorotoluene ug/kg 11501250 92 70-130
2-Hexanone ug/kg 22702500 91 70-130
4-Chlorotoluene ug/kg 10601250 85 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 22602500 90 70-130
Acetone ug/kg 24202500 97 69-130
Benzene ug/kg 11501250 92 70-130
Bromobenzene ug/kg 11501250 92 70-130
Bromochloromethane ug/kg 12301250 98 70-130
Bromodichloromethane ug/kg 10301250 83 69-130
Bromoform ug/kg 10901250 87 70-130
Bromomethane ug/kg 1400 IK1250112 52-130
Carbon tetrachloride ug/kg 11801250 94 70-130
Chlorobenzene ug/kg 11401250 91 70-130
Chloroethane ug/kg 12501250 100 65-130
Chloroform ug/kg 12801250 102 70-130
Chloromethane ug/kg 11101250 89 55-130
cis-1,2-Dichloroethene ug/kg 11901250 95 70-130
cis-1,3-Dichloropropene ug/kg 11301250 90 70-130
Dibromochloromethane ug/kg 11101250 88 70-130
Dibromomethane ug/kg 11601250 93 70-130
Dichlorodifluoromethane ug/kg 12101250 97 45-156
Diisopropyl ether ug/kg 11101250 89 70-130
Ethylbenzene ug/kg 12301250 98 70-130
Hexachloro-1,3-butadiene ug/kg 10901250 87 66-130
Isopropylbenzene (Cumene)ug/kg 11401250 92 70-130
m&p-Xylene ug/kg 22602500 90 70-130
Methyl-tert-butyl ether ug/kg 11201250 89 70-130
Methylene Chloride ug/kg 12601250 101 65-130
n-Butylbenzene ug/kg 11301250 90 67-130
n-Propylbenzene ug/kg 11501250 92 70-130
Naphthalene ug/kg 10501250 84 70-130
o-Xylene ug/kg 11401250 91 70-130
p-Isopropyltoluene ug/kg 11001250 88 67-130
sec-Butylbenzene ug/kg 11001250 88 69-130
Styrene ug/kg 11301250 90 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324055LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 10501250 84 67-130
Tetrachloroethene ug/kg 10601250 85 70-130
Toluene ug/kg 11101250 88 70-130
trans-1,2-Dichloroethene ug/kg 12101250 97 70-130
trans-1,3-Dichloropropene ug/kg 11301250 90 68-130
Trichloroethene ug/kg 11701250 93 70-130
Trichlorofluoromethane ug/kg 11601250 93 70-130
Vinyl acetate ug/kg 25502500 102 70-130
Vinyl chloride ug/kg 12001250 96 61-130
Xylene (Total)ug/kg 34003750 91 70-130
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%102 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3324057MATRIX SPIKE SAMPLE:
MSSpike
Result
92548792005
1,1,1,2-Tetrachloroethane ug/kg 484537 90 70-131ND
1,1,1-Trichloroethane ug/kg 463537 86 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 430537 80 66-130ND
1,1,2-Trichloroethane ug/kg 446537 83 66-133ND
1,1-Dichloroethane ug/kg 513537 96 65-130ND
1,1-Dichloroethene ug/kg 512537 95 10-158ND
1,1-Dichloropropene ug/kg 513537 95 68-133ND
1,2,3-Trichlorobenzene ug/kg 486537 90 27-138ND
1,2,3-Trichloropropane ug/kg 437537 81 67-130ND
1,2,4-Trichlorobenzene ug/kg 485537 90 51-134ND
1,2,4-Trimethylbenzene ug/kg 470537 88 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 407537 76 32-130ND
1,2-Dibromoethane (EDB)ug/kg 480537 89 70-130ND
1,2-Dichlorobenzene ug/kg 468537 87 69-130ND
1,2-Dichloroethane ug/kg 476537 89 59-130ND
1,2-Dichloropropane ug/kg 503537 94 70-130ND
1,3,5-Trimethylbenzene ug/kg 474537 88 65-137ND
1,3-Dichlorobenzene ug/kg 480537 89 70-130ND
1,3-Dichloropropane ug/kg 495537 92 70-130ND
1,4-Dichlorobenzene ug/kg 465537 87 68-130ND
2,2-Dichloropropane ug/kg 397537 74 32-130ND
2-Butanone (MEK)ug/kg 8201070 76 10-136ND
2-Chlorotoluene ug/kg 487537 91 69-141ND
2-Hexanone ug/kg 8351070 78 10-144ND
4-Chlorotoluene ug/kg 464537 86 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 8621070 80 25-143ND
Acetone ug/kg 7321070 68 10-130ND
Benzene ug/kg 503537 94 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3324057MATRIX SPIKE SAMPLE:
MSSpike
Result
92548792005
Bromobenzene ug/kg 484537 90 70-130ND
Bromochloromethane ug/kg 488537 91 69-134ND
Bromodichloromethane ug/kg 424537 79 64-130ND
Bromoform ug/kg 408537 76 62-130ND
Bromomethane ug/kg 372 IK53769 20-176ND
Carbon tetrachloride ug/kg 488537 91 65-140ND
Chlorobenzene ug/kg 510537 95 70-130ND
Chloroethane ug/kg 181537 34 10-130ND
Chloroform ug/kg 529537 99 63-130ND
Chloromethane ug/kg 496537 92 58-130ND
cis-1,2-Dichloroethene ug/kg 500537 93 66-130ND
cis-1,3-Dichloropropene ug/kg 460537 86 67-130ND
Dibromochloromethane ug/kg 454537 85 67-130ND
Dibromomethane ug/kg 489537 91 63-131ND
Dichlorodifluoromethane ug/kg 473537 88 44-180ND
Diisopropyl ether ug/kg 462537 86 63-130ND
Ethylbenzene ug/kg 562537 105 66-130ND
Hexachloro-1,3-butadiene ug/kg 497537 93 64-150ND
Isopropylbenzene (Cumene)ug/kg 527537 98 69-135ND
m&p-Xylene ug/kg 10501070 98 60-133ND
Methyl-tert-butyl ether ug/kg 458537 85 65-130ND
Methylene Chloride ug/kg 539537 100 61-130ND
n-Butylbenzene ug/kg 496537 92 65-140ND
n-Propylbenzene ug/kg 504537 94 67-140ND
Naphthalene ug/kg 450537 84 15-145ND
o-Xylene ug/kg 508537 95 66-133ND
p-Isopropyltoluene ug/kg 483537 90 56-147ND
sec-Butylbenzene ug/kg 497537 92 65-139ND
Styrene ug/kg 494537 92 70-132ND
tert-Butylbenzene ug/kg 485537 90 62-135ND
Tetrachloroethene ug/kg 471537 88 70-135ND
Toluene ug/kg 484537 90 67-130ND
trans-1,2-Dichloroethene ug/kg 516537 96 69-130ND
trans-1,3-Dichloropropene ug/kg 454537 85 62-130ND
Trichloroethene ug/kg 516537 96 70-135ND
Trichlorofluoromethane ug/kg 145537 27 10-130ND
Vinyl acetate ug/kg 9881070 92 53-130ND
Vinyl chloride ug/kg 488537 91 61-148ND
Xylene (Total)ug/kg 15601610 97 63-132ND
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92548792004
3324056SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 6J6.1J
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92548792004
3324056SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg 3.6J3.1J
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg 11.3 410.9
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%107108
4-Bromofluorobenzene (S)%10199
Toluene-d8 (S)%102101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 07/14/2021 01:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
633014
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92548694002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3324940
Associated Lab Samples:92548694002
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 07/13/21 12:47
1,1,1-Trichloroethane ug/kg ND 5.0 07/13/21 12:47
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 07/13/21 12:47
1,1,2-Trichloroethane ug/kg ND 5.0 07/13/21 12:47
1,1-Dichloroethane ug/kg ND 5.0 07/13/21 12:47
1,1-Dichloroethene ug/kg ND 5.0 07/13/21 12:47
1,1-Dichloropropene ug/kg ND 5.0 07/13/21 12:47
1,2,3-Trichlorobenzene ug/kg ND 5.0 07/13/21 12:47
1,2,3-Trichloropropane ug/kg ND 5.0 07/13/21 12:47
1,2,4-Trichlorobenzene ug/kg ND 5.0 07/13/21 12:47
1,2,4-Trimethylbenzene ug/kg ND 5.0 07/13/21 12:47
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 v207/13/21 12:47
1,2-Dibromoethane (EDB)ug/kg ND 5.0 07/13/21 12:47
1,2-Dichlorobenzene ug/kg ND 5.0 07/13/21 12:47
1,2-Dichloroethane ug/kg ND 5.0 07/13/21 12:47
1,2-Dichloropropane ug/kg ND 5.0 07/13/21 12:47
1,3,5-Trimethylbenzene ug/kg ND 5.0 07/13/21 12:47
1,3-Dichlorobenzene ug/kg ND 5.0 07/13/21 12:47
1,3-Dichloropropane ug/kg ND 5.0 07/13/21 12:47
1,4-Dichlorobenzene ug/kg ND 5.0 07/13/21 12:47
2,2-Dichloropropane ug/kg ND 5.0 07/13/21 12:47
2-Butanone (MEK)ug/kg ND 100 07/13/21 12:47
2-Chlorotoluene ug/kg ND 5.0 07/13/21 12:47
2-Hexanone ug/kg ND 50.0 07/13/21 12:47
4-Chlorotoluene ug/kg ND 5.0 07/13/21 12:47
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 07/13/21 12:47
Acetone ug/kg ND 100 07/13/21 12:47
Benzene ug/kg ND 5.0 07/13/21 12:47
Bromobenzene ug/kg ND 5.0 07/13/21 12:47
Bromochloromethane ug/kg ND 5.0 07/13/21 12:47
Bromodichloromethane ug/kg ND 5.0 07/13/21 12:47
Bromoform ug/kg ND 5.0 07/13/21 12:47
Bromomethane ug/kg ND 10.0 IK07/13/21 12:47
Carbon tetrachloride ug/kg ND 5.0 07/13/21 12:47
Chlorobenzene ug/kg ND 5.0 07/13/21 12:47
Chloroethane ug/kg ND 10.0 07/13/21 12:47
Chloroform ug/kg ND 5.0 07/13/21 12:47
Chloromethane ug/kg ND 10.0 07/13/21 12:47
cis-1,2-Dichloroethene ug/kg ND 5.0 07/13/21 12:47
cis-1,3-Dichloropropene ug/kg ND 5.0 07/13/21 12:47
REPORT OF LABORATORY ANALYSIS
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Page 18 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3324940
Associated Lab Samples:92548694002
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 07/13/21 12:47
Dibromomethane ug/kg ND 5.0 07/13/21 12:47
Dichlorodifluoromethane ug/kg ND 10.0 07/13/21 12:47
Diisopropyl ether ug/kg ND 5.0 07/13/21 12:47
Ethylbenzene ug/kg ND 5.0 07/13/21 12:47
Hexachloro-1,3-butadiene ug/kg ND 10.0 07/13/21 12:47
Isopropylbenzene (Cumene)ug/kg ND 5.0 07/13/21 12:47
m&p-Xylene ug/kg ND 10.0 07/13/21 12:47
Methyl-tert-butyl ether ug/kg ND 5.0 07/13/21 12:47
Methylene Chloride ug/kg ND 20.0 07/13/21 12:47
n-Butylbenzene ug/kg ND 5.0 07/13/21 12:47
n-Propylbenzene ug/kg ND 5.0 07/13/21 12:47
Naphthalene ug/kg ND 5.0 07/13/21 12:47
o-Xylene ug/kg ND 5.0 07/13/21 12:47
p-Isopropyltoluene ug/kg ND 5.0 07/13/21 12:47
sec-Butylbenzene ug/kg ND 5.0 07/13/21 12:47
Styrene ug/kg ND 5.0 07/13/21 12:47
tert-Butylbenzene ug/kg ND 5.0 07/13/21 12:47
Tetrachloroethene ug/kg ND 5.0 07/13/21 12:47
Toluene ug/kg ND 5.0 07/13/21 12:47
trans-1,2-Dichloroethene ug/kg ND 5.0 07/13/21 12:47
trans-1,3-Dichloropropene ug/kg ND 5.0 07/13/21 12:47
Trichloroethene ug/kg ND 5.0 07/13/21 12:47
Trichlorofluoromethane ug/kg ND 5.0 07/13/21 12:47
Vinyl acetate ug/kg ND 50.0 07/13/21 12:47
Vinyl chloride ug/kg ND 10.0 07/13/21 12:47
Xylene (Total)ug/kg ND 10.0 07/13/21 12:47
1,2-Dichloroethane-d4 (S)%111 70-130 07/13/21 12:47
4-Bromofluorobenzene (S)%99 69-134 07/13/21 12:47
Toluene-d8 (S)%100 70-130 07/13/21 12:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324941LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11401250 91 70-130
1,1,1-Trichloroethane ug/kg 10801250 86 70-130
1,1,2,2-Tetrachloroethane ug/kg 10501250 84 70-130
1,1,2-Trichloroethane ug/kg 10701250 85 70-130
1,1-Dichloroethane ug/kg 12001250 96 70-130
1,1-Dichloroethene ug/kg 12101250 96 70-130
1,1-Dichloropropene ug/kg 11701250 94 70-130
1,2,3-Trichlorobenzene ug/kg 11501250 92 65-130
1,2,3-Trichloropropane ug/kg 11001250 88 70-130
1,2,4-Trichlorobenzene ug/kg 11501250 92 68-130
REPORT OF LABORATORY ANALYSIS
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Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324941LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11001250 88 70-130
1,2-Dibromo-3-chloropropane ug/kg 1050 v3125084 70-130
1,2-Dibromoethane (EDB)ug/kg 11401250 91 70-130
1,2-Dichlorobenzene ug/kg 11101250 89 70-130
1,2-Dichloroethane ug/kg 11001250 88 63-130
1,2-Dichloropropane ug/kg 11601250 92 70-130
1,3,5-Trimethylbenzene ug/kg 11301250 90 70-130
1,3-Dichlorobenzene ug/kg 11001250 88 70-130
1,3-Dichloropropane ug/kg 11501250 92 70-130
1,4-Dichlorobenzene ug/kg 10901250 87 70-130
2,2-Dichloropropane ug/kg 11001250 88 66-130
2-Butanone (MEK)ug/kg 22502500 90 70-130
2-Chlorotoluene ug/kg 11501250 92 70-130
2-Hexanone ug/kg 21902500 88 70-130
4-Chlorotoluene ug/kg 11001250 88 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 22302500 89 70-130
Acetone ug/kg 22702500 91 69-130
Benzene ug/kg 11501250 92 70-130
Bromobenzene ug/kg 11501250 92 70-130
Bromochloromethane ug/kg 12201250 97 70-130
Bromodichloromethane ug/kg 10401250 84 69-130
Bromoform ug/kg 11001250 88 70-130
Bromomethane ug/kg 1290 IK1250104 52-130
Carbon tetrachloride ug/kg 11801250 94 70-130
Chlorobenzene ug/kg 11601250 93 70-130
Chloroethane ug/kg 12201250 97 65-130
Chloroform ug/kg 12501250 100 70-130
Chloromethane ug/kg 10701250 85 55-130
cis-1,2-Dichloroethene ug/kg 11501250 92 70-130
cis-1,3-Dichloropropene ug/kg 11401250 92 70-130
Dibromochloromethane ug/kg 11201250 90 70-130
Dibromomethane ug/kg 11701250 94 70-130
Dichlorodifluoromethane ug/kg 11501250 92 45-156
Diisopropyl ether ug/kg 10801250 87 70-130
Ethylbenzene ug/kg 12501250 100 70-130
Hexachloro-1,3-butadiene ug/kg 12001250 96 66-130
Isopropylbenzene (Cumene)ug/kg 11801250 94 70-130
m&p-Xylene ug/kg 23202500 93 70-130
Methyl-tert-butyl ether ug/kg 11201250 90 70-130
Methylene Chloride ug/kg 12101250 97 65-130
n-Butylbenzene ug/kg 12101250 97 67-130
n-Propylbenzene ug/kg 11701250 94 70-130
Naphthalene ug/kg 10701250 85 70-130
o-Xylene ug/kg 11401250 91 70-130
p-Isopropyltoluene ug/kg 11601250 93 67-130
sec-Butylbenzene ug/kg 11601250 93 69-130
Styrene ug/kg 11601250 93 70-130
REPORT OF LABORATORY ANALYSIS
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Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3324941LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 10901250 88 67-130
Tetrachloroethene ug/kg 11001250 88 70-130
Toluene ug/kg 11201250 90 70-130
trans-1,2-Dichloroethene ug/kg 12001250 96 70-130
trans-1,3-Dichloropropene ug/kg 11501250 92 68-130
Trichloroethene ug/kg 11801250 95 70-130
Trichlorofluoromethane ug/kg 11301250 91 70-130
Vinyl acetate ug/kg 25102500 100 70-130
Vinyl chloride ug/kg 11501250 92 61-130
Xylene (Total)ug/kg 34703750 92 70-130
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3324943MATRIX SPIKE SAMPLE:
MSSpike
Result
92548792002
1,1,1,2-Tetrachloroethane ug/kg 652692 94 70-131ND
1,1,1-Trichloroethane ug/kg 634692 92 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 593692 86 66-130ND
1,1,2-Trichloroethane ug/kg 593692 86 66-133ND
1,1-Dichloroethane ug/kg 697692 101 65-130ND
1,1-Dichloroethene ug/kg 738692 107 10-158ND
1,1-Dichloropropene ug/kg 705692 102 68-133ND
1,2,3-Trichlorobenzene ug/kg 703692 102 27-138ND
1,2,3-Trichloropropane ug/kg 599692 87 67-130ND
1,2,4-Trichlorobenzene ug/kg 702692 102 51-134ND
1,2,4-Trimethylbenzene ug/kg 739692 106 63-1366.6J
1,2-Dibromo-3-chloropropane ug/kg 563 v369281 32-130ND
1,2-Dibromoethane (EDB)ug/kg 639692 92 70-130ND
1,2-Dichlorobenzene ug/kg 658692 95 69-130ND
1,2-Dichloroethane ug/kg 637692 92 59-130ND
1,2-Dichloropropane ug/kg 684692 99 70-130ND
1,3,5-Trimethylbenzene ug/kg 703692 102 65-137ND
1,3-Dichlorobenzene ug/kg 661692 96 70-130ND
1,3-Dichloropropane ug/kg 694692 100 70-130ND
1,4-Dichlorobenzene ug/kg 678692 98 68-130ND
2,2-Dichloropropane ug/kg 566692 82 32-130ND
2-Butanone (MEK)ug/kg 11301390 82 10-136ND
2-Chlorotoluene ug/kg 695692 101 69-141ND
2-Hexanone ug/kg 11401390 83 10-144ND
4-Chlorotoluene ug/kg 666692 96 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 11901390 86 25-143ND
Acetone ug/kg 9851390 71 10-130ND
Benzene ug/kg 678692 98 67-130ND
REPORT OF LABORATORY ANALYSIS
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Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3324943MATRIX SPIKE SAMPLE:
MSSpike
Result
92548792002
Bromobenzene ug/kg 683692 99 70-130ND
Bromochloromethane ug/kg 665692 96 69-134ND
Bromodichloromethane ug/kg 560692 81 64-130ND
Bromoform ug/kg 547692 79 62-130ND
Bromomethane ug/kg 434 IK69263 20-176ND
Carbon tetrachloride ug/kg 647692 94 65-140ND
Chlorobenzene ug/kg 693692 100 70-130ND
Chloroethane ug/kg 218692 31 10-130ND
Chloroform ug/kg 708692 102 63-130ND
Chloromethane ug/kg 681692 98 58-130ND
cis-1,2-Dichloroethene ug/kg 673692 97 66-130ND
cis-1,3-Dichloropropene ug/kg 742692 107 67-130ND
Dibromochloromethane ug/kg 599692 87 67-130ND
Dibromomethane ug/kg 647692 94 63-131ND
Dichlorodifluoromethane ug/kg 644692 93 44-180ND
Diisopropyl ether ug/kg 626692 90 63-130ND
Ethylbenzene ug/kg 790692 114 66-130ND
Hexachloro-1,3-butadiene ug/kg 745692 108 64-150ND
Isopropylbenzene (Cumene)ug/kg 727692 105 69-135ND
m&p-Xylene ug/kg 15001390 108 60-133ND
Methyl-tert-butyl ether ug/kg 623692 90 65-130ND
Methylene Chloride ug/kg 690692 100 61-130ND
n-Butylbenzene ug/kg 745692 108 65-140ND
n-Propylbenzene ug/kg 730692 106 67-140ND
Naphthalene ug/kg 716692 103 15-1454.6J
o-Xylene ug/kg 718692 104 66-133ND
p-Isopropyltoluene ug/kg 718692 104 56-147ND
sec-Butylbenzene ug/kg 710692 103 65-139ND
Styrene ug/kg 668692 97 70-132ND
tert-Butylbenzene ug/kg 692692 100 62-135ND
Tetrachloroethene ug/kg 671692 97 70-135ND
Toluene ug/kg 701692 101 67-130ND
trans-1,2-Dichloroethene ug/kg 712692 103 69-130ND
trans-1,3-Dichloropropene ug/kg 609692 88 62-130ND
Trichloroethene ug/kg 701692 101 70-135ND
Trichlorofluoromethane ug/kg 174692 25 10-130ND
Vinyl acetate ug/kg 13401390 97 53-130ND
Vinyl chloride ug/kg 672692 97 61-148ND
Xylene (Total)ug/kg 22102070 107 63-132ND
1,2-Dichloroethane-d4 (S)%118 70-130
4-Bromofluorobenzene (S)%98 69-134
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
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Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92548792001
3324942SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 107 5102
1,2-Dibromo-3-chloropropane ug/kg ND v2ND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg 42.9 441.1
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg 21.9 221.4
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg ND IKND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 50.8 151.5
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg 9.6J10J
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92548792001
3324942SAMPLE DUPLICATE:
m&p-Xylene ug/kg 26.5 624.8
Methyl-tert-butyl ether ug/kg 22.0 723.6
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg 35.6 135.1
Naphthalene ug/kg 95.1 1383.8
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg ND6.0J
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg 26.5 624.8
1,2-Dichloroethane-d4 (S)%105107
4-Bromofluorobenzene (S)%99100
Toluene-d8 (S)%101102
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92548694
GILBARO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
632523
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92548694001, 92548694002, 92548694003
Parameter Units
Dup
Result QualifiersRPDResult
92548100001
3322659SAMPLE DUPLICATE:
Percent Moisture %12.4 N2711.6
Parameter Units
Dup
Result QualifiersRPDResult
92548694003
3322945SAMPLE DUPLICATE:
Percent Moisture %10.5 N2611.1
REPORT OF LABORATORY ANALYSIS
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Page 25 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92548694
GILBARO
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 26 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92548694
GILBARO
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92548694001 632773 632804SS-1 50"EPA 5035A/5030B EPA 8260D
92548694002 633014 633026SS-1 107"EPA 5035A/5030B EPA 8260D
92548694003 632773 632804SS-2 48"EPA 5035A/5030B EPA 8260D
92548694001 632523SS-1 50"SW-846
92548694002 632523SS-1 107"SW-846
92548694003 632523SS-2 48"SW-846
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[phone]
Page 27 of 30
Page 28 of 30
Page 29 of 30
Page 30 of 30
#=CL#
August 11, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92554053
92554053
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
GILBARCO 11.990009.00
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on August 06, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lindsey N Wooten
[e-mail]
Project Manager
[phone]
Enclosures
cc: Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 1 of 32
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92554053001 SS-3 78 EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92554053002 SS-4 68 EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92554053003 SS-4 131 EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92554053004 SS-5 99 EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92554053005 SS-5 132 EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 32
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92554053001 SS-3 78
Naphthalene 5950 ug/kg 08/09/21 20:18789EPA 8260D
Percent Moisture 5.2 %08/09/21 13:05 N20.10SW-846
92554053002 SS-4 68
Acetone 368 ug/kg 08/10/21 13:26333EPA 8260D
n-Butylbenzene 1980 ug/kg 08/10/21 13:2616.7EPA 8260D
p-Isopropyltoluene 2060 ug/kg 08/10/21 13:2616.7EPA 8260D
Methylene Chloride 160 ug/kg 08/10/21 13:2666.7EPA 8260D
Naphthalene 6990 ug/kg 08/10/21 13:2616.7EPA 8260D
Toluene 90.0 ug/kg 08/10/21 13:2616.7EPA 8260D
1,2,4-Trimethylbenzene 2320 ug/kg 08/10/21 13:2616.7EPA 8260D
1,3,5-Trimethylbenzene 702 ug/kg 08/10/21 13:2616.7EPA 8260D
Xylene (Total)105 ug/kg 08/10/21 13:2633.3EPA 8260D
m&p-Xylene 76.9 ug/kg 08/10/21 13:2633.3EPA 8260D
o-Xylene 28.4 ug/kg 08/10/21 13:2616.7EPA 8260D
Percent Moisture 10.8 %08/09/21 13:05 N20.10SW-846
92554053003 SS-4 131
p-Isopropyltoluene 2580 ug/kg 08/09/21 20:531250EPA 8260D
1,3,5-Trimethylbenzene 2710 ug/kg 08/09/21 20:531250EPA 8260D
Percent Moisture 21.5 %08/09/21 13:05 N20.10SW-846
92554053004 SS-5 99
o-Xylene 15.6 ug/kg 08/10/21 12:519.6EPA 8260D
Percent Moisture 11.0 %08/09/21 13:05 N20.10SW-846
92554053005 SS-5 132
sec-Butylbenzene 1530 ug/kg 08/10/21 14:0120.8EPA 8260D
Ethylbenzene 150 ug/kg 08/10/21 14:0120.8EPA 8260D
p-Isopropyltoluene 2410 ug/kg 08/10/21 14:0120.8EPA 8260D
Methylene Chloride 97.7 ug/kg 08/10/21 14:0183.2EPA 8260D
4-Methyl-2-pentanone (MIBK)258 ug/kg 08/10/21 14:01208EPA 8260D
Naphthalene 155 ug/kg 08/10/21 14:0120.8EPA 8260D
n-Propylbenzene 795 ug/kg 08/10/21 14:0120.8EPA 8260D
1,2,4-Trimethylbenzene 8120 ug/kg 08/10/21 14:0120.8EPA 8260D
1,3,5-Trimethylbenzene 2980 ug/kg 08/10/21 14:0120.8EPA 8260D
Xylene (Total)272 ug/kg 08/10/21 14:0141.6EPA 8260D
m&p-Xylene 272 ug/kg 08/10/21 14:0141.6EPA 8260D
Percent Moisture 19.2 %08/09/21 13:05 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-3 78 Lab ID: 92554053001 Collected: 08/05/21 10:45 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/09/21 20:18 67-64-108/09/21 15:0615800 50
Benzene ND ug/kg 08/09/21 20:18 71-43-208/09/21 15:06789 50
Bromobenzene ND ug/kg 08/09/21 20:18 108-86-108/09/21 15:06789 50
Bromochloromethane ND ug/kg 08/09/21 20:18 74-97-508/09/21 15:06789 50
Bromodichloromethane ND ug/kg 08/09/21 20:18 75-27-408/09/21 15:06789 50
Bromoform ND ug/kg 08/09/21 20:18 75-25-208/09/21 15:06789 50
Bromomethane ND ug/kg 08/09/21 20:18 74-83-908/09/21 15:061580 50
2-Butanone (MEK)ND ug/kg 08/09/21 20:18 78-93-308/09/21 15:0615800 50
n-Butylbenzene ND ug/kg 08/09/21 20:18 104-51-808/09/21 15:06789 50
sec-Butylbenzene ND ug/kg 08/09/21 20:18 135-98-808/09/21 15:06789 50
tert-Butylbenzene ND ug/kg 08/09/21 20:18 98-06-608/09/21 15:06789 50
Carbon tetrachloride ND ug/kg 08/09/21 20:18 56-23-508/09/21 15:06789 50
Chlorobenzene ND ug/kg 08/09/21 20:18 108-90-708/09/21 15:06789 50
Chloroethane ND ug/kg 08/09/21 20:18 75-00-308/09/21 15:061580 50
Chloroform ND ug/kg 08/09/21 20:18 67-66-308/09/21 15:06789 50
Chloromethane ND ug/kg 08/09/21 20:18 74-87-308/09/21 15:061580 50
2-Chlorotoluene ND ug/kg 08/09/21 20:18 95-49-808/09/21 15:06789 50
4-Chlorotoluene ND ug/kg 08/09/21 20:18 106-43-408/09/21 15:06789 50
1,2-Dibromo-3-chloropropane ND ug/kg 08/09/21 20:18 96-12-808/09/21 15:06789 50
Dibromochloromethane ND ug/kg 08/09/21 20:18 124-48-108/09/21 15:06789 50
1,2-Dibromoethane (EDB)ND ug/kg 08/09/21 20:18 106-93-408/09/21 15:06789 50
Dibromomethane ND ug/kg 08/09/21 20:18 74-95-308/09/21 15:06789 50
1,2-Dichlorobenzene ND ug/kg 08/09/21 20:18 95-50-108/09/21 15:06789 50
1,3-Dichlorobenzene ND ug/kg 08/09/21 20:18 541-73-108/09/21 15:06789 50
1,4-Dichlorobenzene ND ug/kg 08/09/21 20:18 106-46-708/09/21 15:06789 50
Dichlorodifluoromethane ND ug/kg 08/09/21 20:18 75-71-808/09/21 15:061580 50
1,1-Dichloroethane ND ug/kg 08/09/21 20:18 75-34-308/09/21 15:06789 50
1,2-Dichloroethane ND ug/kg 08/09/21 20:18 107-06-208/09/21 15:06789 50
1,1-Dichloroethene ND ug/kg 08/09/21 20:18 75-35-408/09/21 15:06789 50
cis-1,2-Dichloroethene ND ug/kg 08/09/21 20:18 156-59-208/09/21 15:06789 50
trans-1,2-Dichloroethene ND ug/kg 08/09/21 20:18 156-60-508/09/21 15:06789 50
1,2-Dichloropropane ND ug/kg 08/09/21 20:18 78-87-508/09/21 15:06789 50
1,3-Dichloropropane ND ug/kg 08/09/21 20:18 142-28-908/09/21 15:06789 50
2,2-Dichloropropane ND ug/kg 08/09/21 20:18 594-20-708/09/21 15:06789 50
1,1-Dichloropropene ND ug/kg 08/09/21 20:18 563-58-608/09/21 15:06789 50
cis-1,3-Dichloropropene ND ug/kg 08/09/21 20:18 10061-01-508/09/21 15:06789 50
trans-1,3-Dichloropropene ND ug/kg 08/09/21 20:18 10061-02-608/09/21 15:06789 50
Diisopropyl ether ND ug/kg 08/09/21 20:18 108-20-308/09/21 15:06789 50
Ethylbenzene ND ug/kg 08/09/21 20:18 100-41-408/09/21 15:06789 50
Hexachloro-1,3-butadiene ND ug/kg 08/09/21 20:18 87-68-308/09/21 15:061580 50
2-Hexanone ND ug/kg 08/09/21 20:18 591-78-608/09/21 15:067890 50
Isopropylbenzene (Cumene)ND ug/kg 08/09/21 20:18 98-82-808/09/21 15:06789 50
p-Isopropyltoluene ND ug/kg 08/09/21 20:18 99-87-608/09/21 15:06789 50
Methylene Chloride ND ug/kg 08/09/21 20:18 75-09-208/09/21 15:063160 50
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/09/21 20:18 108-10-108/09/21 15:067890 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-3 78 Lab ID: 92554053001 Collected: 08/05/21 10:45 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 08/09/21 20:18 1634-04-408/09/21 15:06789 50
Naphthalene 5950 ug/kg 08/09/21 20:18 91-20-308/09/21 15:06789 50
n-Propylbenzene ND ug/kg 08/09/21 20:18 103-65-108/09/21 15:06789 50
Styrene ND ug/kg 08/09/21 20:18 100-42-508/09/21 15:06789 50
1,1,1,2-Tetrachloroethane ND ug/kg 08/09/21 20:18 630-20-608/09/21 15:06789 50
1,1,2,2-Tetrachloroethane ND ug/kg 08/09/21 20:18 79-34-508/09/21 15:06789 50
Tetrachloroethene ND ug/kg 08/09/21 20:18 127-18-408/09/21 15:06789 50
Toluene ND ug/kg 08/09/21 20:18 108-88-308/09/21 15:06789 50
1,2,3-Trichlorobenzene ND ug/kg 08/09/21 20:18 87-61-608/09/21 15:06789 50
1,2,4-Trichlorobenzene ND ug/kg 08/09/21 20:18 120-82-108/09/21 15:06789 50
1,1,1-Trichloroethane ND ug/kg 08/09/21 20:18 71-55-608/09/21 15:06789 50
1,1,2-Trichloroethane ND ug/kg 08/09/21 20:18 79-00-508/09/21 15:06789 50
Trichloroethene ND ug/kg 08/09/21 20:18 79-01-608/09/21 15:06789 50
Trichlorofluoromethane ND ug/kg 08/09/21 20:18 75-69-408/09/21 15:06789 50
1,2,3-Trichloropropane ND ug/kg 08/09/21 20:18 96-18-408/09/21 15:06789 50
1,2,4-Trimethylbenzene ND ug/kg 08/09/21 20:18 95-63-608/09/21 15:06789 50
1,3,5-Trimethylbenzene ND ug/kg 08/09/21 20:18 108-67-808/09/21 15:06789 50
Vinyl acetate ND ug/kg 08/09/21 20:18 108-05-408/09/21 15:067890 50
Vinyl chloride ND ug/kg 08/09/21 20:18 75-01-408/09/21 15:061580 50
Xylene (Total)ND ug/kg 08/09/21 20:18 1330-20-708/09/21 15:061580 50
m&p-Xylene ND ug/kg 08/09/21 20:18 179601-23-108/09/21 15:061580 50
o-Xylene ND ug/kg 08/09/21 20:18 95-47-608/09/21 15:06789 50
Surrogates
Toluene-d8 (S)101 %08/09/21 20:18 2037-26-5 D308/09/21 15:0670-130 50
4-Bromofluorobenzene (S)106 %08/09/21 20:18 460-00-408/09/21 15:0669-134 50
1,2-Dichloroethane-d4 (S)103 %08/09/21 20:18 17060-07-008/09/21 15:0670-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 5.2 %08/09/21 13:05 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-4 68 Lab ID: 92554053002 Collected: 08/05/21 14:50 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 368 ug/kg 08/10/21 13:26 67-64-108/10/21 10:38333 2
Benzene ND ug/kg 08/10/21 13:26 71-43-208/10/21 10:3816.7 2
Bromobenzene ND ug/kg 08/10/21 13:26 108-86-108/10/21 10:3816.7 2
Bromochloromethane ND ug/kg 08/10/21 13:26 74-97-508/10/21 10:3816.7 2
Bromodichloromethane ND ug/kg 08/10/21 13:26 75-27-408/10/21 10:3816.7 2
Bromoform ND ug/kg 08/10/21 13:26 75-25-208/10/21 10:3816.7 2
Bromomethane ND ug/kg 08/10/21 13:26 74-83-9 v108/10/21 10:3833.3 2
2-Butanone (MEK)ND ug/kg 08/10/21 13:26 78-93-308/10/21 10:38333 2
n-Butylbenzene 1980 ug/kg 08/10/21 13:26 104-51-808/10/21 10:3816.7 2
sec-Butylbenzene ND ug/kg 08/10/21 13:26 135-98-808/10/21 10:3816.7 2
tert-Butylbenzene ND ug/kg 08/10/21 13:26 98-06-608/10/21 10:3816.7 2
Carbon tetrachloride ND ug/kg 08/10/21 13:26 56-23-508/10/21 10:3816.7 2
Chlorobenzene ND ug/kg 08/10/21 13:26 108-90-708/10/21 10:3816.7 2
Chloroethane ND ug/kg 08/10/21 13:26 75-00-308/10/21 10:3833.3 2
Chloroform ND ug/kg 08/10/21 13:26 67-66-308/10/21 10:3816.7 2
Chloromethane ND ug/kg 08/10/21 13:26 74-87-308/10/21 10:3833.3 2
2-Chlorotoluene ND ug/kg 08/10/21 13:26 95-49-808/10/21 10:3816.7 2
4-Chlorotoluene ND ug/kg 08/10/21 13:26 106-43-408/10/21 10:3816.7 2
1,2-Dibromo-3-chloropropane ND ug/kg 08/10/21 13:26 96-12-808/10/21 10:3816.7 2
Dibromochloromethane ND ug/kg 08/10/21 13:26 124-48-108/10/21 10:3816.7 2
1,2-Dibromoethane (EDB)ND ug/kg 08/10/21 13:26 106-93-408/10/21 10:3816.7 2
Dibromomethane ND ug/kg 08/10/21 13:26 74-95-308/10/21 10:3816.7 2
1,2-Dichlorobenzene ND ug/kg 08/10/21 13:26 95-50-108/10/21 10:3816.7 2
1,3-Dichlorobenzene ND ug/kg 08/10/21 13:26 541-73-108/10/21 10:3816.7 2
1,4-Dichlorobenzene ND ug/kg 08/10/21 13:26 106-46-708/10/21 10:3816.7 2
Dichlorodifluoromethane ND ug/kg 08/10/21 13:26 75-71-8 v108/10/21 10:3833.3 2
1,1-Dichloroethane ND ug/kg 08/10/21 13:26 75-34-308/10/21 10:3816.7 2
1,2-Dichloroethane ND ug/kg 08/10/21 13:26 107-06-208/10/21 10:3816.7 2
1,1-Dichloroethene ND ug/kg 08/10/21 13:26 75-35-408/10/21 10:3816.7 2
cis-1,2-Dichloroethene ND ug/kg 08/10/21 13:26 156-59-208/10/21 10:3816.7 2
trans-1,2-Dichloroethene ND ug/kg 08/10/21 13:26 156-60-508/10/21 10:3816.7 2
1,2-Dichloropropane ND ug/kg 08/10/21 13:26 78-87-508/10/21 10:3816.7 2
1,3-Dichloropropane ND ug/kg 08/10/21 13:26 142-28-908/10/21 10:3816.7 2
2,2-Dichloropropane ND ug/kg 08/10/21 13:26 594-20-708/10/21 10:3816.7 2
1,1-Dichloropropene ND ug/kg 08/10/21 13:26 563-58-608/10/21 10:3816.7 2
cis-1,3-Dichloropropene ND ug/kg 08/10/21 13:26 10061-01-508/10/21 10:3816.7 2
trans-1,3-Dichloropropene ND ug/kg 08/10/21 13:26 10061-02-608/10/21 10:3816.7 2
Diisopropyl ether ND ug/kg 08/10/21 13:26 108-20-308/10/21 10:3816.7 2
Ethylbenzene ND ug/kg 08/10/21 13:26 100-41-408/10/21 10:3816.7 2
Hexachloro-1,3-butadiene ND ug/kg 08/10/21 13:26 87-68-308/10/21 10:3833.3 2
2-Hexanone ND ug/kg 08/10/21 13:26 591-78-608/10/21 10:38167 2
Isopropylbenzene (Cumene)ND ug/kg 08/10/21 13:26 98-82-808/10/21 10:3816.7 2
p-Isopropyltoluene 2060 ug/kg 08/10/21 13:26 99-87-608/10/21 10:3816.7 2
Methylene Chloride 160 ug/kg 08/10/21 13:26 75-09-208/10/21 10:3866.7 2
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/10/21 13:26 108-10-108/10/21 10:38167 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-4 68 Lab ID: 92554053002 Collected: 08/05/21 14:50 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 08/10/21 13:26 1634-04-408/10/21 10:3816.7 2
Naphthalene 6990 ug/kg 08/10/21 13:26 91-20-308/10/21 10:3816.7 2
n-Propylbenzene ND ug/kg 08/10/21 13:26 103-65-108/10/21 10:3816.7 2
Styrene ND ug/kg 08/10/21 13:26 100-42-508/10/21 10:3816.7 2
1,1,1,2-Tetrachloroethane ND ug/kg 08/10/21 13:26 630-20-608/10/21 10:3816.7 2
1,1,2,2-Tetrachloroethane ND ug/kg 08/10/21 13:26 79-34-508/10/21 10:3816.7 2
Tetrachloroethene ND ug/kg 08/10/21 13:26 127-18-408/10/21 10:3816.7 2
Toluene 90.0 ug/kg 08/10/21 13:26 108-88-308/10/21 10:3816.7 2
1,2,3-Trichlorobenzene ND ug/kg 08/10/21 13:26 87-61-608/10/21 10:3816.7 2
1,2,4-Trichlorobenzene ND ug/kg 08/10/21 13:26 120-82-108/10/21 10:3816.7 2
1,1,1-Trichloroethane ND ug/kg 08/10/21 13:26 71-55-608/10/21 10:3816.7 2
1,1,2-Trichloroethane ND ug/kg 08/10/21 13:26 79-00-508/10/21 10:3816.7 2
Trichloroethene ND ug/kg 08/10/21 13:26 79-01-608/10/21 10:3816.7 2
Trichlorofluoromethane ND ug/kg 08/10/21 13:26 75-69-408/10/21 10:3816.7 2
1,2,3-Trichloropropane ND ug/kg 08/10/21 13:26 96-18-408/10/21 10:3816.7 2
1,2,4-Trimethylbenzene 2320 ug/kg 08/10/21 13:26 95-63-608/10/21 10:3816.7 2
1,3,5-Trimethylbenzene 702 ug/kg 08/10/21 13:26 108-67-808/10/21 10:3816.7 2
Vinyl acetate ND ug/kg 08/10/21 13:26 108-05-408/10/21 10:38167 2
Vinyl chloride ND ug/kg 08/10/21 13:26 75-01-408/10/21 10:3833.3 2
Xylene (Total)105 ug/kg 08/10/21 13:26 1330-20-708/10/21 10:3833.3 2
m&p-Xylene 76.9 ug/kg 08/10/21 13:26 179601-23-108/10/21 10:3833.3 2
o-Xylene 28.4 ug/kg 08/10/21 13:26 95-47-608/10/21 10:3816.7 2
Surrogates
Toluene-d8 (S)100 %08/10/21 13:26 2037-26-508/10/21 10:3870-130 2
4-Bromofluorobenzene (S)106 %08/10/21 13:26 460-00-408/10/21 10:3869-134 2
1,2-Dichloroethane-d4 (S)103 %08/10/21 13:26 17060-07-008/10/21 10:3870-130 2
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.8 %08/09/21 13:05 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-4 131 Lab ID: 92554053003 Collected: 08/05/21 15:00 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/09/21 20:53 67-64-108/09/21 15:0625100 50
Benzene ND ug/kg 08/09/21 20:53 71-43-208/09/21 15:061250 50
Bromobenzene ND ug/kg 08/09/21 20:53 108-86-108/09/21 15:061250 50
Bromochloromethane ND ug/kg 08/09/21 20:53 74-97-508/09/21 15:061250 50
Bromodichloromethane ND ug/kg 08/09/21 20:53 75-27-408/09/21 15:061250 50
Bromoform ND ug/kg 08/09/21 20:53 75-25-208/09/21 15:061250 50
Bromomethane ND ug/kg 08/09/21 20:53 74-83-908/09/21 15:062510 50
2-Butanone (MEK)ND ug/kg 08/09/21 20:53 78-93-308/09/21 15:0625100 50
n-Butylbenzene ND ug/kg 08/09/21 20:53 104-51-808/09/21 15:061250 50
sec-Butylbenzene ND ug/kg 08/09/21 20:53 135-98-808/09/21 15:061250 50
tert-Butylbenzene ND ug/kg 08/09/21 20:53 98-06-608/09/21 15:061250 50
Carbon tetrachloride ND ug/kg 08/09/21 20:53 56-23-508/09/21 15:061250 50
Chlorobenzene ND ug/kg 08/09/21 20:53 108-90-708/09/21 15:061250 50
Chloroethane ND ug/kg 08/09/21 20:53 75-00-308/09/21 15:062510 50
Chloroform ND ug/kg 08/09/21 20:53 67-66-308/09/21 15:061250 50
Chloromethane ND ug/kg 08/09/21 20:53 74-87-308/09/21 15:062510 50
2-Chlorotoluene ND ug/kg 08/09/21 20:53 95-49-808/09/21 15:061250 50
4-Chlorotoluene ND ug/kg 08/09/21 20:53 106-43-408/09/21 15:061250 50
1,2-Dibromo-3-chloropropane ND ug/kg 08/09/21 20:53 96-12-808/09/21 15:061250 50
Dibromochloromethane ND ug/kg 08/09/21 20:53 124-48-108/09/21 15:061250 50
1,2-Dibromoethane (EDB)ND ug/kg 08/09/21 20:53 106-93-408/09/21 15:061250 50
Dibromomethane ND ug/kg 08/09/21 20:53 74-95-308/09/21 15:061250 50
1,2-Dichlorobenzene ND ug/kg 08/09/21 20:53 95-50-108/09/21 15:061250 50
1,3-Dichlorobenzene ND ug/kg 08/09/21 20:53 541-73-108/09/21 15:061250 50
1,4-Dichlorobenzene ND ug/kg 08/09/21 20:53 106-46-708/09/21 15:061250 50
Dichlorodifluoromethane ND ug/kg 08/09/21 20:53 75-71-808/09/21 15:062510 50
1,1-Dichloroethane ND ug/kg 08/09/21 20:53 75-34-308/09/21 15:061250 50
1,2-Dichloroethane ND ug/kg 08/09/21 20:53 107-06-208/09/21 15:061250 50
1,1-Dichloroethene ND ug/kg 08/09/21 20:53 75-35-408/09/21 15:061250 50
cis-1,2-Dichloroethene ND ug/kg 08/09/21 20:53 156-59-208/09/21 15:061250 50
trans-1,2-Dichloroethene ND ug/kg 08/09/21 20:53 156-60-508/09/21 15:061250 50
1,2-Dichloropropane ND ug/kg 08/09/21 20:53 78-87-508/09/21 15:061250 50
1,3-Dichloropropane ND ug/kg 08/09/21 20:53 142-28-908/09/21 15:061250 50
2,2-Dichloropropane ND ug/kg 08/09/21 20:53 594-20-708/09/21 15:061250 50
1,1-Dichloropropene ND ug/kg 08/09/21 20:53 563-58-608/09/21 15:061250 50
cis-1,3-Dichloropropene ND ug/kg 08/09/21 20:53 10061-01-508/09/21 15:061250 50
trans-1,3-Dichloropropene ND ug/kg 08/09/21 20:53 10061-02-608/09/21 15:061250 50
Diisopropyl ether ND ug/kg 08/09/21 20:53 108-20-308/09/21 15:061250 50
Ethylbenzene ND ug/kg 08/09/21 20:53 100-41-408/09/21 15:061250 50
Hexachloro-1,3-butadiene ND ug/kg 08/09/21 20:53 87-68-308/09/21 15:062510 50
2-Hexanone ND ug/kg 08/09/21 20:53 591-78-608/09/21 15:0612500 50
Isopropylbenzene (Cumene)ND ug/kg 08/09/21 20:53 98-82-808/09/21 15:061250 50
p-Isopropyltoluene 2580 ug/kg 08/09/21 20:53 99-87-608/09/21 15:061250 50
Methylene Chloride ND ug/kg 08/09/21 20:53 75-09-208/09/21 15:065020 50
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/09/21 20:53 108-10-108/09/21 15:0612500 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-4 131 Lab ID: 92554053003 Collected: 08/05/21 15:00 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 08/09/21 20:53 1634-04-408/09/21 15:061250 50
Naphthalene ND ug/kg 08/09/21 20:53 91-20-308/09/21 15:061250 50
n-Propylbenzene ND ug/kg 08/09/21 20:53 103-65-108/09/21 15:061250 50
Styrene ND ug/kg 08/09/21 20:53 100-42-508/09/21 15:061250 50
1,1,1,2-Tetrachloroethane ND ug/kg 08/09/21 20:53 630-20-608/09/21 15:061250 50
1,1,2,2-Tetrachloroethane ND ug/kg 08/09/21 20:53 79-34-508/09/21 15:061250 50
Tetrachloroethene ND ug/kg 08/09/21 20:53 127-18-408/09/21 15:061250 50
Toluene ND ug/kg 08/09/21 20:53 108-88-308/09/21 15:061250 50
1,2,3-Trichlorobenzene ND ug/kg 08/09/21 20:53 87-61-608/09/21 15:061250 50
1,2,4-Trichlorobenzene ND ug/kg 08/09/21 20:53 120-82-108/09/21 15:061250 50
1,1,1-Trichloroethane ND ug/kg 08/09/21 20:53 71-55-608/09/21 15:061250 50
1,1,2-Trichloroethane ND ug/kg 08/09/21 20:53 79-00-508/09/21 15:061250 50
Trichloroethene ND ug/kg 08/09/21 20:53 79-01-608/09/21 15:061250 50
Trichlorofluoromethane ND ug/kg 08/09/21 20:53 75-69-408/09/21 15:061250 50
1,2,3-Trichloropropane ND ug/kg 08/09/21 20:53 96-18-408/09/21 15:061250 50
1,2,4-Trimethylbenzene ND ug/kg 08/09/21 20:53 95-63-608/09/21 15:061250 50
1,3,5-Trimethylbenzene 2710 ug/kg 08/09/21 20:53 108-67-808/09/21 15:061250 50
Vinyl acetate ND ug/kg 08/09/21 20:53 108-05-408/09/21 15:0612500 50
Vinyl chloride ND ug/kg 08/09/21 20:53 75-01-408/09/21 15:062510 50
Xylene (Total)ND ug/kg 08/09/21 20:53 1330-20-708/09/21 15:062510 50
m&p-Xylene ND ug/kg 08/09/21 20:53 179601-23-108/09/21 15:062510 50
o-Xylene ND ug/kg 08/09/21 20:53 95-47-608/09/21 15:061250 50
Surrogates
Toluene-d8 (S)98 %08/09/21 20:53 2037-26-5 D308/09/21 15:0670-130 50
4-Bromofluorobenzene (S)105 %08/09/21 20:53 460-00-408/09/21 15:0669-134 50
1,2-Dichloroethane-d4 (S)104 %08/09/21 20:53 17060-07-008/09/21 15:0670-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.5 %08/09/21 13:05 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-5 99 Lab ID: 92554053004 Collected: 08/05/21 15:40 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/10/21 12:51 67-64-108/10/21 10:38193 1
Benzene ND ug/kg 08/10/21 12:51 71-43-208/10/21 10:389.6 1
Bromobenzene ND ug/kg 08/10/21 12:51 108-86-108/10/21 10:389.6 1
Bromochloromethane ND ug/kg 08/10/21 12:51 74-97-508/10/21 10:389.6 1
Bromodichloromethane ND ug/kg 08/10/21 12:51 75-27-408/10/21 10:389.6 1
Bromoform ND ug/kg 08/10/21 12:51 75-25-208/10/21 10:389.6 1
Bromomethane ND ug/kg 08/10/21 12:51 74-83-9 v108/10/21 10:3819.3 1
2-Butanone (MEK)ND ug/kg 08/10/21 12:51 78-93-308/10/21 10:38193 1
n-Butylbenzene ND ug/kg 08/10/21 12:51 104-51-808/10/21 10:389.6 1
sec-Butylbenzene ND ug/kg 08/10/21 12:51 135-98-808/10/21 10:389.6 1
tert-Butylbenzene ND ug/kg 08/10/21 12:51 98-06-608/10/21 10:389.6 1
Carbon tetrachloride ND ug/kg 08/10/21 12:51 56-23-508/10/21 10:389.6 1
Chlorobenzene ND ug/kg 08/10/21 12:51 108-90-708/10/21 10:389.6 1
Chloroethane ND ug/kg 08/10/21 12:51 75-00-308/10/21 10:3819.3 1
Chloroform ND ug/kg 08/10/21 12:51 67-66-308/10/21 10:389.6 1
Chloromethane ND ug/kg 08/10/21 12:51 74-87-308/10/21 10:3819.3 1
2-Chlorotoluene ND ug/kg 08/10/21 12:51 95-49-808/10/21 10:389.6 1
4-Chlorotoluene ND ug/kg 08/10/21 12:51 106-43-408/10/21 10:389.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 08/10/21 12:51 96-12-808/10/21 10:389.6 1
Dibromochloromethane ND ug/kg 08/10/21 12:51 124-48-108/10/21 10:389.6 1
1,2-Dibromoethane (EDB)ND ug/kg 08/10/21 12:51 106-93-408/10/21 10:389.6 1
Dibromomethane ND ug/kg 08/10/21 12:51 74-95-308/10/21 10:389.6 1
1,2-Dichlorobenzene ND ug/kg 08/10/21 12:51 95-50-108/10/21 10:389.6 1
1,3-Dichlorobenzene ND ug/kg 08/10/21 12:51 541-73-108/10/21 10:389.6 1
1,4-Dichlorobenzene ND ug/kg 08/10/21 12:51 106-46-708/10/21 10:389.6 1
Dichlorodifluoromethane ND ug/kg 08/10/21 12:51 75-71-8 v108/10/21 10:3819.3 1
1,1-Dichloroethane ND ug/kg 08/10/21 12:51 75-34-308/10/21 10:389.6 1
1,2-Dichloroethane ND ug/kg 08/10/21 12:51 107-06-208/10/21 10:389.6 1
1,1-Dichloroethene ND ug/kg 08/10/21 12:51 75-35-408/10/21 10:389.6 1
cis-1,2-Dichloroethene ND ug/kg 08/10/21 12:51 156-59-208/10/21 10:389.6 1
trans-1,2-Dichloroethene ND ug/kg 08/10/21 12:51 156-60-508/10/21 10:389.6 1
1,2-Dichloropropane ND ug/kg 08/10/21 12:51 78-87-508/10/21 10:389.6 1
1,3-Dichloropropane ND ug/kg 08/10/21 12:51 142-28-908/10/21 10:389.6 1
2,2-Dichloropropane ND ug/kg 08/10/21 12:51 594-20-708/10/21 10:389.6 1
1,1-Dichloropropene ND ug/kg 08/10/21 12:51 563-58-608/10/21 10:389.6 1
cis-1,3-Dichloropropene ND ug/kg 08/10/21 12:51 10061-01-508/10/21 10:389.6 1
trans-1,3-Dichloropropene ND ug/kg 08/10/21 12:51 10061-02-608/10/21 10:389.6 1
Diisopropyl ether ND ug/kg 08/10/21 12:51 108-20-308/10/21 10:389.6 1
Ethylbenzene ND ug/kg 08/10/21 12:51 100-41-408/10/21 10:389.6 1
Hexachloro-1,3-butadiene ND ug/kg 08/10/21 12:51 87-68-308/10/21 10:3819.3 1
2-Hexanone ND ug/kg 08/10/21 12:51 591-78-608/10/21 10:3896.4 1
Isopropylbenzene (Cumene)ND ug/kg 08/10/21 12:51 98-82-808/10/21 10:389.6 1
p-Isopropyltoluene ND ug/kg 08/10/21 12:51 99-87-608/10/21 10:389.6 1
Methylene Chloride ND ug/kg 08/10/21 12:51 75-09-208/10/21 10:3838.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 08/10/21 12:51 108-10-108/10/21 10:3896.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-5 99 Lab ID: 92554053004 Collected: 08/05/21 15:40 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 08/10/21 12:51 1634-04-408/10/21 10:389.6 1
Naphthalene ND ug/kg 08/10/21 12:51 91-20-308/10/21 10:389.6 1
n-Propylbenzene ND ug/kg 08/10/21 12:51 103-65-108/10/21 10:389.6 1
Styrene ND ug/kg 08/10/21 12:51 100-42-508/10/21 10:389.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 08/10/21 12:51 630-20-608/10/21 10:389.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 08/10/21 12:51 79-34-508/10/21 10:389.6 1
Tetrachloroethene ND ug/kg 08/10/21 12:51 127-18-408/10/21 10:389.6 1
Toluene ND ug/kg 08/10/21 12:51 108-88-308/10/21 10:389.6 1
1,2,3-Trichlorobenzene ND ug/kg 08/10/21 12:51 87-61-608/10/21 10:389.6 1
1,2,4-Trichlorobenzene ND ug/kg 08/10/21 12:51 120-82-108/10/21 10:389.6 1
1,1,1-Trichloroethane ND ug/kg 08/10/21 12:51 71-55-608/10/21 10:389.6 1
1,1,2-Trichloroethane ND ug/kg 08/10/21 12:51 79-00-508/10/21 10:389.6 1
Trichloroethene ND ug/kg 08/10/21 12:51 79-01-608/10/21 10:389.6 1
Trichlorofluoromethane ND ug/kg 08/10/21 12:51 75-69-408/10/21 10:389.6 1
1,2,3-Trichloropropane ND ug/kg 08/10/21 12:51 96-18-408/10/21 10:389.6 1
1,2,4-Trimethylbenzene ND ug/kg 08/10/21 12:51 95-63-608/10/21 10:389.6 1
1,3,5-Trimethylbenzene ND ug/kg 08/10/21 12:51 108-67-808/10/21 10:389.6 1
Vinyl acetate ND ug/kg 08/10/21 12:51 108-05-408/10/21 10:3896.4 1
Vinyl chloride ND ug/kg 08/10/21 12:51 75-01-408/10/21 10:3819.3 1
Xylene (Total)ND ug/kg 08/10/21 12:51 1330-20-708/10/21 10:3819.3 1
m&p-Xylene ND ug/kg 08/10/21 12:51 179601-23-108/10/21 10:3819.3 1
o-Xylene 15.6 ug/kg 08/10/21 12:51 95-47-608/10/21 10:389.6 1
Surrogates
Toluene-d8 (S)99 %08/10/21 12:51 2037-26-508/10/21 10:3870-130 1
4-Bromofluorobenzene (S)99 %08/10/21 12:51 460-00-408/10/21 10:3869-134 1
1,2-Dichloroethane-d4 (S)101 %08/10/21 12:51 17060-07-008/10/21 10:3870-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.0 %08/09/21 13:05 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-5 132 Lab ID: 92554053005 Collected: 08/05/21 15:50 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 08/10/21 14:01 67-64-108/10/21 10:38416 2.5
Benzene ND ug/kg 08/10/21 14:01 71-43-208/10/21 10:3820.8 2.5
Bromobenzene ND ug/kg 08/10/21 14:01 108-86-108/10/21 10:3820.8 2.5
Bromochloromethane ND ug/kg 08/10/21 14:01 74-97-508/10/21 10:3820.8 2.5
Bromodichloromethane ND ug/kg 08/10/21 14:01 75-27-408/10/21 10:3820.8 2.5
Bromoform ND ug/kg 08/10/21 14:01 75-25-208/10/21 10:3820.8 2.5
Bromomethane ND ug/kg 08/10/21 14:01 74-83-9 v108/10/21 10:3841.6 2.5
2-Butanone (MEK)ND ug/kg 08/10/21 14:01 78-93-308/10/21 10:38416 2.5
n-Butylbenzene ND ug/kg 08/10/21 14:01 104-51-808/10/21 10:3820.8 2.5
sec-Butylbenzene 1530 ug/kg 08/10/21 14:01 135-98-808/10/21 10:3820.8 2.5
tert-Butylbenzene ND ug/kg 08/10/21 14:01 98-06-608/10/21 10:3820.8 2.5
Carbon tetrachloride ND ug/kg 08/10/21 14:01 56-23-508/10/21 10:3820.8 2.5
Chlorobenzene ND ug/kg 08/10/21 14:01 108-90-708/10/21 10:3820.8 2.5
Chloroethane ND ug/kg 08/10/21 14:01 75-00-308/10/21 10:3841.6 2.5
Chloroform ND ug/kg 08/10/21 14:01 67-66-308/10/21 10:3820.8 2.5
Chloromethane ND ug/kg 08/10/21 14:01 74-87-308/10/21 10:3841.6 2.5
2-Chlorotoluene ND ug/kg 08/10/21 14:01 95-49-808/10/21 10:3820.8 2.5
4-Chlorotoluene ND ug/kg 08/10/21 14:01 106-43-408/10/21 10:3820.8 2.5
1,2-Dibromo-3-chloropropane ND ug/kg 08/10/21 14:01 96-12-808/10/21 10:3820.8 2.5
Dibromochloromethane ND ug/kg 08/10/21 14:01 124-48-108/10/21 10:3820.8 2.5
1,2-Dibromoethane (EDB)ND ug/kg 08/10/21 14:01 106-93-408/10/21 10:3820.8 2.5
Dibromomethane ND ug/kg 08/10/21 14:01 74-95-308/10/21 10:3820.8 2.5
1,2-Dichlorobenzene ND ug/kg 08/10/21 14:01 95-50-108/10/21 10:3820.8 2.5
1,3-Dichlorobenzene ND ug/kg 08/10/21 14:01 541-73-108/10/21 10:3820.8 2.5
1,4-Dichlorobenzene ND ug/kg 08/10/21 14:01 106-46-708/10/21 10:3820.8 2.5
Dichlorodifluoromethane ND ug/kg 08/10/21 14:01 75-71-8 v108/10/21 10:3841.6 2.5
1,1-Dichloroethane ND ug/kg 08/10/21 14:01 75-34-308/10/21 10:3820.8 2.5
1,2-Dichloroethane ND ug/kg 08/10/21 14:01 107-06-208/10/21 10:3820.8 2.5
1,1-Dichloroethene ND ug/kg 08/10/21 14:01 75-35-408/10/21 10:3820.8 2.5
cis-1,2-Dichloroethene ND ug/kg 08/10/21 14:01 156-59-208/10/21 10:3820.8 2.5
trans-1,2-Dichloroethene ND ug/kg 08/10/21 14:01 156-60-508/10/21 10:3820.8 2.5
1,2-Dichloropropane ND ug/kg 08/10/21 14:01 78-87-508/10/21 10:3820.8 2.5
1,3-Dichloropropane ND ug/kg 08/10/21 14:01 142-28-908/10/21 10:3820.8 2.5
2,2-Dichloropropane ND ug/kg 08/10/21 14:01 594-20-708/10/21 10:3820.8 2.5
1,1-Dichloropropene ND ug/kg 08/10/21 14:01 563-58-608/10/21 10:3820.8 2.5
cis-1,3-Dichloropropene ND ug/kg 08/10/21 14:01 10061-01-508/10/21 10:3820.8 2.5
trans-1,3-Dichloropropene ND ug/kg 08/10/21 14:01 10061-02-608/10/21 10:3820.8 2.5
Diisopropyl ether ND ug/kg 08/10/21 14:01 108-20-308/10/21 10:3820.8 2.5
Ethylbenzene 150 ug/kg 08/10/21 14:01 100-41-408/10/21 10:3820.8 2.5
Hexachloro-1,3-butadiene ND ug/kg 08/10/21 14:01 87-68-308/10/21 10:3841.6 2.5
2-Hexanone ND ug/kg 08/10/21 14:01 591-78-608/10/21 10:38208 2.5
Isopropylbenzene (Cumene)ND ug/kg 08/10/21 14:01 98-82-808/10/21 10:3820.8 2.5
p-Isopropyltoluene 2410 ug/kg 08/10/21 14:01 99-87-608/10/21 10:3820.8 2.5
Methylene Chloride 97.7 ug/kg 08/10/21 14:01 75-09-208/10/21 10:3883.2 2.5
4-Methyl-2-pentanone (MIBK)258 ug/kg 08/10/21 14:01 108-10-108/10/21 10:38208 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 32
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Sample: SS-5 132 Lab ID: 92554053005 Collected: 08/05/21 15:50 Received: 08/06/21 10:59 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 08/10/21 14:01 1634-04-408/10/21 10:3820.8 2.5
Naphthalene 155 ug/kg 08/10/21 14:01 91-20-308/10/21 10:3820.8 2.5
n-Propylbenzene 795 ug/kg 08/10/21 14:01 103-65-108/10/21 10:3820.8 2.5
Styrene ND ug/kg 08/10/21 14:01 100-42-508/10/21 10:3820.8 2.5
1,1,1,2-Tetrachloroethane ND ug/kg 08/10/21 14:01 630-20-608/10/21 10:3820.8 2.5
1,1,2,2-Tetrachloroethane ND ug/kg 08/10/21 14:01 79-34-508/10/21 10:3820.8 2.5
Tetrachloroethene ND ug/kg 08/10/21 14:01 127-18-408/10/21 10:3820.8 2.5
Toluene ND ug/kg 08/10/21 14:01 108-88-308/10/21 10:3820.8 2.5
1,2,3-Trichlorobenzene ND ug/kg 08/10/21 14:01 87-61-608/10/21 10:3820.8 2.5
1,2,4-Trichlorobenzene ND ug/kg 08/10/21 14:01 120-82-108/10/21 10:3820.8 2.5
1,1,1-Trichloroethane ND ug/kg 08/10/21 14:01 71-55-608/10/21 10:3820.8 2.5
1,1,2-Trichloroethane ND ug/kg 08/10/21 14:01 79-00-508/10/21 10:3820.8 2.5
Trichloroethene ND ug/kg 08/10/21 14:01 79-01-608/10/21 10:3820.8 2.5
Trichlorofluoromethane ND ug/kg 08/10/21 14:01 75-69-408/10/21 10:3820.8 2.5
1,2,3-Trichloropropane ND ug/kg 08/10/21 14:01 96-18-408/10/21 10:3820.8 2.5
1,2,4-Trimethylbenzene 8120 ug/kg 08/10/21 14:01 95-63-608/10/21 10:3820.8 2.5
1,3,5-Trimethylbenzene 2980 ug/kg 08/10/21 14:01 108-67-808/10/21 10:3820.8 2.5
Vinyl acetate ND ug/kg 08/10/21 14:01 108-05-408/10/21 10:38208 2.5
Vinyl chloride ND ug/kg 08/10/21 14:01 75-01-408/10/21 10:3841.6 2.5
Xylene (Total)272 ug/kg 08/10/21 14:01 1330-20-708/10/21 10:3841.6 2.5
m&p-Xylene 272 ug/kg 08/10/21 14:01 179601-23-108/10/21 10:3841.6 2.5
o-Xylene ND ug/kg 08/10/21 14:01 95-47-608/10/21 10:3820.8 2.5
Surrogates
Toluene-d8 (S)101 %08/10/21 14:01 2037-26-508/10/21 10:3870-130 2.5
4-Bromofluorobenzene (S)137 %08/10/21 14:01 460-00-4 S208/10/21 10:3869-134 2.5
1,2-Dichloroethane-d4 (S)103 %08/10/21 14:01 17060-07-008/10/21 10:3870-130 2.5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.2 %08/09/21 13:05 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
638973
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92554053001, 92554053003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3354543
Associated Lab Samples:92554053001, 92554053003
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/09/21 16:48
1,1,1-Trichloroethane ug/kg ND 5.0 08/09/21 16:48
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/09/21 16:48
1,1,2-Trichloroethane ug/kg ND 5.0 08/09/21 16:48
1,1-Dichloroethane ug/kg ND 5.0 08/09/21 16:48
1,1-Dichloroethene ug/kg ND 5.0 08/09/21 16:48
1,1-Dichloropropene ug/kg ND 5.0 08/09/21 16:48
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/09/21 16:48
1,2,3-Trichloropropane ug/kg ND 5.0 08/09/21 16:48
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/09/21 16:48
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/09/21 16:48
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/09/21 16:48
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/09/21 16:48
1,2-Dichlorobenzene ug/kg ND 5.0 08/09/21 16:48
1,2-Dichloroethane ug/kg ND 5.0 08/09/21 16:48
1,2-Dichloropropane ug/kg ND 5.0 08/09/21 16:48
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/09/21 16:48
1,3-Dichlorobenzene ug/kg ND 5.0 08/09/21 16:48
1,3-Dichloropropane ug/kg ND 5.0 08/09/21 16:48
1,4-Dichlorobenzene ug/kg ND 5.0 08/09/21 16:48
2,2-Dichloropropane ug/kg ND 5.0 08/09/21 16:48
2-Butanone (MEK)ug/kg ND 100 08/09/21 16:48
2-Chlorotoluene ug/kg ND 5.0 08/09/21 16:48
2-Hexanone ug/kg ND 50.0 08/09/21 16:48
4-Chlorotoluene ug/kg ND 5.0 08/09/21 16:48
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/09/21 16:48
Acetone ug/kg ND 100 08/09/21 16:48
Benzene ug/kg ND 5.0 08/09/21 16:48
Bromobenzene ug/kg ND 5.0 08/09/21 16:48
Bromochloromethane ug/kg ND 5.0 08/09/21 16:48
Bromodichloromethane ug/kg ND 5.0 08/09/21 16:48
Bromoform ug/kg ND 5.0 08/09/21 16:48
Bromomethane ug/kg ND 10.0 08/09/21 16:48
Carbon tetrachloride ug/kg ND 5.0 08/09/21 16:48
Chlorobenzene ug/kg ND 5.0 08/09/21 16:48
Chloroethane ug/kg ND 10.0 08/09/21 16:48
Chloroform ug/kg ND 5.0 08/09/21 16:48
Chloromethane ug/kg ND 10.0 08/09/21 16:48
cis-1,2-Dichloroethene ug/kg ND 5.0 08/09/21 16:48
cis-1,3-Dichloropropene ug/kg ND 5.0 08/09/21 16:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3354543
Associated Lab Samples:92554053001, 92554053003
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 08/09/21 16:48
Dibromomethane ug/kg ND 5.0 08/09/21 16:48
Dichlorodifluoromethane ug/kg ND 10.0 08/09/21 16:48
Diisopropyl ether ug/kg ND 5.0 08/09/21 16:48
Ethylbenzene ug/kg ND 5.0 08/09/21 16:48
Hexachloro-1,3-butadiene ug/kg ND 10.0 08/09/21 16:48
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/09/21 16:48
m&p-Xylene ug/kg ND 10.0 08/09/21 16:48
Methyl-tert-butyl ether ug/kg ND 5.0 08/09/21 16:48
Methylene Chloride ug/kg ND 20.0 08/09/21 16:48
n-Butylbenzene ug/kg ND 5.0 08/09/21 16:48
n-Propylbenzene ug/kg ND 5.0 08/09/21 16:48
Naphthalene ug/kg ND 5.0 08/09/21 16:48
o-Xylene ug/kg ND 5.0 08/09/21 16:48
p-Isopropyltoluene ug/kg ND 5.0 08/09/21 16:48
sec-Butylbenzene ug/kg ND 5.0 08/09/21 16:48
Styrene ug/kg ND 5.0 08/09/21 16:48
tert-Butylbenzene ug/kg ND 5.0 08/09/21 16:48
Tetrachloroethene ug/kg ND 5.0 08/09/21 16:48
Toluene ug/kg ND 5.0 08/09/21 16:48
trans-1,2-Dichloroethene ug/kg ND 5.0 08/09/21 16:48
trans-1,3-Dichloropropene ug/kg ND 5.0 08/09/21 16:48
Trichloroethene ug/kg ND 5.0 08/09/21 16:48
Trichlorofluoromethane ug/kg ND 5.0 08/09/21 16:48
Vinyl acetate ug/kg ND 50.0 08/09/21 16:48
Vinyl chloride ug/kg ND 10.0 08/09/21 16:48
Xylene (Total)ug/kg ND 10.0 08/09/21 16:48
1,2-Dichloroethane-d4 (S)%101 70-130 08/09/21 16:48
4-Bromofluorobenzene (S)%101 69-134 08/09/21 16:48
Toluene-d8 (S)%100 70-130 08/09/21 16:48
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3354544LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12501250 100 70-130
1,1,1-Trichloroethane ug/kg 11701250 93 70-130
1,1,2,2-Tetrachloroethane ug/kg 12001250 96 70-130
1,1,2-Trichloroethane ug/kg 12101250 97 70-130
1,1-Dichloroethane ug/kg 12501250 100 70-130
1,1-Dichloroethene ug/kg 12801250 102 70-130
1,1-Dichloropropene ug/kg 11701250 93 70-130
1,2,3-Trichlorobenzene ug/kg 13101250 105 65-130
1,2,3-Trichloropropane ug/kg 12701250 101 70-130
1,2,4-Trichlorobenzene ug/kg 12901250 103 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3354544LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12201250 97 70-130
1,2-Dibromo-3-chloropropane ug/kg 13001250 104 70-130
1,2-Dibromoethane (EDB)ug/kg 12401250 99 70-130
1,2-Dichlorobenzene ug/kg 13201250 106 70-130
1,2-Dichloroethane ug/kg 12201250 97 63-130
1,2-Dichloropropane ug/kg 12501250 100 70-130
1,3,5-Trimethylbenzene ug/kg 12101250 96 70-130
1,3-Dichlorobenzene ug/kg 13001250 104 70-130
1,3-Dichloropropane ug/kg 12401250 99 70-130
1,4-Dichlorobenzene ug/kg 12401250 99 70-130
2,2-Dichloropropane ug/kg 12301250 99 66-130
2-Butanone (MEK)ug/kg 22202500 89 70-130
2-Chlorotoluene ug/kg 12301250 98 70-130
2-Hexanone ug/kg 23602500 94 70-130
4-Chlorotoluene ug/kg 11901250 95 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 23802500 95 70-130
Acetone ug/kg 24802500 99 69-130
Benzene ug/kg 12201250 98 70-130
Bromobenzene ug/kg 12701250 101 70-130
Bromochloromethane ug/kg 13501250 108 70-130
Bromodichloromethane ug/kg 12301250 98 69-130
Bromoform ug/kg 12601250 101 70-130
Bromomethane ug/kg 16001250 128 52-130
Carbon tetrachloride ug/kg 12601250 101 70-130
Chlorobenzene ug/kg 12401250 99 70-130
Chloroethane ug/kg 15001250 120 65-130
Chloroform ug/kg 12701250 102 70-130
Chloromethane ug/kg 11901250 95 55-130
cis-1,2-Dichloroethene ug/kg 12501250 100 70-130
cis-1,3-Dichloropropene ug/kg 12001250 96 70-130
Dibromochloromethane ug/kg 13101250 104 70-130
Dibromomethane ug/kg 13201250 106 70-130
Dichlorodifluoromethane ug/kg 15701250 126 45-156
Diisopropyl ether ug/kg 11101250 89 70-130
Ethylbenzene ug/kg 13101250 105 70-130
Hexachloro-1,3-butadiene ug/kg 11401250 92 66-130
Isopropylbenzene (Cumene)ug/kg 12201250 98 70-130
m&p-Xylene ug/kg 24302500 97 70-130
Methyl-tert-butyl ether ug/kg 11601250 92 70-130
Methylene Chloride ug/kg 12801250 102 65-130
n-Butylbenzene ug/kg 12601250 101 67-130
n-Propylbenzene ug/kg 12101250 97 70-130
Naphthalene ug/kg 12501250 100 70-130
o-Xylene ug/kg 12201250 97 70-130
p-Isopropyltoluene ug/kg 11901250 95 67-130
sec-Butylbenzene ug/kg 11501250 92 69-130
Styrene ug/kg 12401250 100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3354544LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11801250 94 67-130
Tetrachloroethene ug/kg 12301250 99 70-130
Toluene ug/kg 12101250 97 70-130
trans-1,2-Dichloroethene ug/kg 12701250 102 70-130
trans-1,3-Dichloropropene ug/kg 13101250 105 68-130
Trichloroethene ug/kg 12001250 96 70-130
Trichlorofluoromethane ug/kg 12301250 99 70-130
Vinyl acetate ug/kg 26002500 104 70-130
Vinyl chloride ug/kg 14601250 117 61-130
Xylene (Total)ug/kg 36503750 97 70-130
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%100 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3354546MATRIX SPIKE SAMPLE:
MSSpike
Result
92554125002
1,1,1,2-Tetrachloroethane ug/kg 436495 88 70-131ND
1,1,1-Trichloroethane ug/kg 498495 101 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 406495 82 66-130ND
1,1,2-Trichloroethane ug/kg 403495 82 66-133ND
1,1-Dichloroethane ug/kg 485495 98 65-130ND
1,1-Dichloroethene ug/kg 527495 107 10-158ND
1,1-Dichloropropene ug/kg 507495 103 68-133ND
1,2,3-Trichlorobenzene ug/kg 493495 100 27-138ND
1,2,3-Trichloropropane ug/kg 408495 83 67-130ND
1,2,4-Trichlorobenzene ug/kg 493495 100 51-134ND
1,2,4-Trimethylbenzene ug/kg 458495 93 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 418495 85 32-130ND
1,2-Dibromoethane (EDB)ug/kg 420495 85 70-130ND
1,2-Dichlorobenzene ug/kg 467495 95 69-130ND
1,2-Dichloroethane ug/kg 465495 94 59-130ND
1,2-Dichloropropane ug/kg 454495 92 70-130ND
1,3,5-Trimethylbenzene ug/kg 448495 91 65-137ND
1,3-Dichlorobenzene ug/kg 467495 95 70-130ND
1,3-Dichloropropane ug/kg 434495 88 70-130ND
1,4-Dichlorobenzene ug/kg 448495 91 68-130ND
2,2-Dichloropropane ug/kg 463495 94 32-130ND
2-Butanone (MEK)ug/kg 751988 76 10-136ND
2-Chlorotoluene ug/kg 440495 89 69-141ND
2-Hexanone ug/kg 719988 73 10-144ND
4-Chlorotoluene ug/kg 424495 86 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 719988 73 25-143ND
Acetone ug/kg 756988 77 10-130ND
Benzene ug/kg 466495 94 67-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3354546MATRIX SPIKE SAMPLE:
MSSpike
Result
92554125002
Bromobenzene ug/kg 448495 91 70-130ND
Bromochloromethane ug/kg 473495 96 69-134ND
Bromodichloromethane ug/kg 420495 85 64-130ND
Bromoform ug/kg 381495 77 62-130ND
Bromomethane ug/kg 373495 76 20-176ND
Carbon tetrachloride ug/kg 466495 94 65-140ND
Chlorobenzene ug/kg 460495 93 70-130ND
Chloroethane ug/kg 296495 60 10-130ND
Chloroform ug/kg 499495 101 63-130ND
Chloromethane ug/kg 534495 108 58-130ND
cis-1,2-Dichloroethene ug/kg 496495 100 66-130ND
cis-1,3-Dichloropropene ug/kg 404495 82 67-130ND
Dibromochloromethane ug/kg 429495 87 67-130ND
Dibromomethane ug/kg 434495 88 63-131ND
Dichlorodifluoromethane ug/kg 632495 128 44-180ND
Diisopropyl ether ug/kg 434495 88 63-130ND
Ethylbenzene ug/kg 510495 103 66-130ND
Hexachloro-1,3-butadiene ug/kg 489495 99 64-150ND
Isopropylbenzene (Cumene)ug/kg 475495 96 69-135ND
m&p-Xylene ug/kg 935988 95 60-133ND
Methyl-tert-butyl ether ug/kg 429495 87 65-130ND
Methylene Chloride ug/kg 493495 100 61-130ND
n-Butylbenzene ug/kg 486495 98 65-140ND
n-Propylbenzene ug/kg 448495 91 67-140ND
Naphthalene ug/kg 434495 88 15-145ND
o-Xylene ug/kg 464495 94 66-133ND
p-Isopropyltoluene ug/kg 460495 93 56-147ND
sec-Butylbenzene ug/kg 446495 90 65-139ND
Styrene ug/kg 452495 91 70-132ND
tert-Butylbenzene ug/kg 454495 92 62-135ND
Tetrachloroethene ug/kg 521495 106 70-135ND
Toluene ug/kg 464495 94 67-130ND
trans-1,2-Dichloroethene ug/kg 520495 105 69-130ND
trans-1,3-Dichloropropene ug/kg 429495 87 62-130ND
Trichloroethene ug/kg 462495 94 70-135ND
Trichlorofluoromethane ug/kg 282495 57 10-130ND
Vinyl acetate ug/kg 905988 92 53-130ND
Vinyl chloride ug/kg 605495 123 61-148ND
Xylene (Total)ug/kg 14001490 94 63-132ND
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92554125001
3354545SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92554125001
3354545SAMPLE DUPLICATE:
m&p-Xylene ug/kg 5.3J0.0055J
mg/kg
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg ND0.015J mg/kg
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 4.8J0.0048J
mg/kg
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg ND0.0055J
mg/kg
1,2-Dichloroethane-d4 (S)%9999
4-Bromofluorobenzene (S)%9798
Toluene-d8 (S)%100100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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Huntersville, NC 28078
[phone]
Page 21 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
639155
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92554053002, 92554053004, 92554053005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3355228
Associated Lab Samples:92554053002, 92554053004, 92554053005
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 08/10/21 12:33
1,1,1-Trichloroethane ug/kg ND 5.0 08/10/21 12:33
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 08/10/21 12:33
1,1,2-Trichloroethane ug/kg ND 5.0 08/10/21 12:33
1,1-Dichloroethane ug/kg ND 5.0 08/10/21 12:33
1,1-Dichloroethene ug/kg ND 5.0 08/10/21 12:33
1,1-Dichloropropene ug/kg ND 5.0 08/10/21 12:33
1,2,3-Trichlorobenzene ug/kg ND 5.0 08/10/21 12:33
1,2,3-Trichloropropane ug/kg ND 5.0 08/10/21 12:33
1,2,4-Trichlorobenzene ug/kg ND 5.0 08/10/21 12:33
1,2,4-Trimethylbenzene ug/kg ND 5.0 08/10/21 12:33
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 08/10/21 12:33
1,2-Dibromoethane (EDB)ug/kg ND 5.0 08/10/21 12:33
1,2-Dichlorobenzene ug/kg ND 5.0 08/10/21 12:33
1,2-Dichloroethane ug/kg ND 5.0 08/10/21 12:33
1,2-Dichloropropane ug/kg ND 5.0 08/10/21 12:33
1,3,5-Trimethylbenzene ug/kg ND 5.0 08/10/21 12:33
1,3-Dichlorobenzene ug/kg ND 5.0 08/10/21 12:33
1,3-Dichloropropane ug/kg ND 5.0 08/10/21 12:33
1,4-Dichlorobenzene ug/kg ND 5.0 08/10/21 12:33
2,2-Dichloropropane ug/kg ND 5.0 08/10/21 12:33
2-Butanone (MEK)ug/kg ND 100 08/10/21 12:33
2-Chlorotoluene ug/kg ND 5.0 08/10/21 12:33
2-Hexanone ug/kg ND 50.0 08/10/21 12:33
4-Chlorotoluene ug/kg ND 5.0 08/10/21 12:33
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 08/10/21 12:33
Acetone ug/kg ND 100 08/10/21 12:33
Benzene ug/kg ND 5.0 08/10/21 12:33
Bromobenzene ug/kg ND 5.0 08/10/21 12:33
Bromochloromethane ug/kg ND 5.0 08/10/21 12:33
Bromodichloromethane ug/kg ND 5.0 08/10/21 12:33
Bromoform ug/kg ND 5.0 08/10/21 12:33
Bromomethane ug/kg ND 10.0 v108/10/21 12:33
Carbon tetrachloride ug/kg ND 5.0 08/10/21 12:33
Chlorobenzene ug/kg ND 5.0 08/10/21 12:33
Chloroethane ug/kg ND 10.0 08/10/21 12:33
Chloroform ug/kg ND 5.0 08/10/21 12:33
Chloromethane ug/kg ND 10.0 08/10/21 12:33
cis-1,2-Dichloroethene ug/kg ND 5.0 08/10/21 12:33
cis-1,3-Dichloropropene ug/kg ND 5.0 08/10/21 12:33
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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Page 22 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3355228
Associated Lab Samples:92554053002, 92554053004, 92554053005
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 08/10/21 12:33
Dibromomethane ug/kg ND 5.0 08/10/21 12:33
Dichlorodifluoromethane ug/kg ND 10.0 v108/10/21 12:33
Diisopropyl ether ug/kg ND 5.0 08/10/21 12:33
Ethylbenzene ug/kg ND 5.0 08/10/21 12:33
Hexachloro-1,3-butadiene ug/kg ND 10.0 08/10/21 12:33
Isopropylbenzene (Cumene)ug/kg ND 5.0 08/10/21 12:33
m&p-Xylene ug/kg ND 10.0 08/10/21 12:33
Methyl-tert-butyl ether ug/kg ND 5.0 08/10/21 12:33
Methylene Chloride ug/kg ND 20.0 08/10/21 12:33
n-Butylbenzene ug/kg ND 5.0 08/10/21 12:33
n-Propylbenzene ug/kg ND 5.0 08/10/21 12:33
Naphthalene ug/kg ND 5.0 08/10/21 12:33
o-Xylene ug/kg ND 5.0 08/10/21 12:33
p-Isopropyltoluene ug/kg ND 5.0 08/10/21 12:33
sec-Butylbenzene ug/kg ND 5.0 08/10/21 12:33
Styrene ug/kg ND 5.0 08/10/21 12:33
tert-Butylbenzene ug/kg ND 5.0 08/10/21 12:33
Tetrachloroethene ug/kg ND 5.0 08/10/21 12:33
Toluene ug/kg ND 5.0 08/10/21 12:33
trans-1,2-Dichloroethene ug/kg ND 5.0 08/10/21 12:33
trans-1,3-Dichloropropene ug/kg ND 5.0 08/10/21 12:33
Trichloroethene ug/kg ND 5.0 08/10/21 12:33
Trichlorofluoromethane ug/kg ND 5.0 08/10/21 12:33
Vinyl acetate ug/kg ND 50.0 08/10/21 12:33
Vinyl chloride ug/kg ND 10.0 08/10/21 12:33
Xylene (Total)ug/kg ND 10.0 08/10/21 12:33
1,2-Dichloroethane-d4 (S)%106 70-130 08/10/21 12:33
4-Bromofluorobenzene (S)%101 69-134 08/10/21 12:33
Toluene-d8 (S)%100 70-130 08/10/21 12:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355229LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11001250 88 70-130
1,1,1-Trichloroethane ug/kg 11501250 92 70-130
1,1,2,2-Tetrachloroethane ug/kg 10501250 84 70-130
1,1,2-Trichloroethane ug/kg 10901250 87 70-130
1,1-Dichloroethane ug/kg 12201250 98 70-130
1,1-Dichloroethene ug/kg 12401250 99 70-130
1,1-Dichloropropene ug/kg 11401250 91 70-130
1,2,3-Trichlorobenzene ug/kg 11701250 93 65-130
1,2,3-Trichloropropane ug/kg 11001250 88 70-130
1,2,4-Trichlorobenzene ug/kg 11801250 94 68-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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Huntersville, NC 28078
[phone]
Page 23 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355229LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11201250 89 70-130
1,2-Dibromo-3-chloropropane ug/kg 10901250 87 70-130
1,2-Dibromoethane (EDB)ug/kg 10801250 86 70-130
1,2-Dichlorobenzene ug/kg 11801250 94 70-130
1,2-Dichloroethane ug/kg 11601250 92 63-130
1,2-Dichloropropane ug/kg 11401250 91 70-130
1,3,5-Trimethylbenzene ug/kg 11001250 88 70-130
1,3-Dichlorobenzene ug/kg 12001250 96 70-130
1,3-Dichloropropane ug/kg 10901250 87 70-130
1,4-Dichlorobenzene ug/kg 11101250 89 70-130
2,2-Dichloropropane ug/kg 12001250 96 66-130
2-Butanone (MEK)ug/kg 20502500 82 70-130
2-Chlorotoluene ug/kg 11101250 89 70-130
2-Hexanone ug/kg 20002500 80 70-130
4-Chlorotoluene ug/kg 10701250 86 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 20802500 83 70-130
Acetone ug/kg 22702500 91 69-130
Benzene ug/kg 11201250 90 70-130
Bromobenzene ug/kg 11301250 91 70-130
Bromochloromethane ug/kg 12901250 103 70-130
Bromodichloromethane ug/kg 11001250 88 69-130
Bromoform ug/kg 10901250 87 70-130
Bromomethane ug/kg 1590 v11250127 52-130
Carbon tetrachloride ug/kg 11501250 92 70-130
Chlorobenzene ug/kg 11101250 89 70-130
Chloroethane ug/kg 14501250 116 65-130
Chloroform ug/kg 12201250 97 70-130
Chloromethane ug/kg 11801250 94 55-130
cis-1,2-Dichloroethene ug/kg 12101250 97 70-130
cis-1,3-Dichloropropene ug/kg 10901250 87 70-130
Dibromochloromethane ug/kg 11401250 92 70-130
Dibromomethane ug/kg 11701250 94 70-130
Dichlorodifluoromethane ug/kg 1510 v11250121 45-156
Diisopropyl ether ug/kg 10801250 86 70-130
Ethylbenzene ug/kg 11701250 94 70-130
Hexachloro-1,3-butadiene ug/kg 10901250 87 66-130
Isopropylbenzene (Cumene)ug/kg 11001250 88 70-130
m&p-Xylene ug/kg 22002500 88 70-130
Methyl-tert-butyl ether ug/kg 10801250 87 70-130
Methylene Chloride ug/kg 12301250 99 65-130
n-Butylbenzene ug/kg 11401250 91 67-130
n-Propylbenzene ug/kg 11001250 88 70-130
Naphthalene ug/kg 11001250 88 70-130
o-Xylene ug/kg 11001250 88 70-130
p-Isopropyltoluene ug/kg 11001250 88 67-130
sec-Butylbenzene ug/kg 10501250 84 69-130
Styrene ug/kg 11101250 89 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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Huntersville, NC 28078
[phone]
Page 24 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3355229LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 10701250 86 67-130
Tetrachloroethene ug/kg 11201250 90 70-130
Toluene ug/kg 11101250 89 70-130
trans-1,2-Dichloroethene ug/kg 12301250 98 70-130
trans-1,3-Dichloropropene ug/kg 11801250 95 68-130
Trichloroethene ug/kg 11201250 90 70-130
Trichlorofluoromethane ug/kg 12101250 97 70-130
Vinyl acetate ug/kg 24402500 98 70-130
Vinyl chloride ug/kg 14101250 113 61-130
Xylene (Total)ug/kg 33003750 88 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%97 69-134
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3355230MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92553871004
3355231
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 10300 97 70-13195 210300<103 10000 9830
1,1,1-Trichloroethane ug/kg 10300 102 65-13398 410300<103 10500 10100
1,1,2,2-Tetrachloroethane ug/kg 10300 96 66-13095 010300<103 9850 9830
1,1,2-Trichloroethane ug/kg 10300 100 66-13395 610300<103 10400 9800
1,1-Dichloroethane ug/kg 10300 108 65-130102 610300<103 11100 10500
1,1-Dichloroethene ug/kg 10300 113 10-158108 410300<103 11600 11100
1,1-Dichloropropene ug/kg 10300 104 68-133100 410300<103 10700 10300
1,2,3-Trichlorobenzene ug/kg 10300 97 27-13896 110300<103 9980 9880
1,2,3-Trichloropropane ug/kg 10300 94 67-13098 410300<103 9690 10100
1,2,4-Trichlorobenzene ug/kg 10300 98 51-13496 310300<103 10100 9850
1,2,4-Trimethylbenzene ug/kg 10300 85 63-13694 2103003970048500 49300
1,2-Dibromo-3-chloropropane ug/kg 10300 97 32-13098 110300<103 9970 10100
1,2-Dibromoethane (EDB)ug/kg 10300 96 70-13096 010300<103 9860 9870
1,2-Dichlorobenzene ug/kg 10300 100 69-13097 310300<103 10300 9960
1,2-Dichloroethane ug/kg 10300 100 59-13096 410300<103 10300 9860
1,2-Dichloropropane ug/kg 10300 102 70-13096 710300<103 10600 9850
1,3,5-Trimethylbenzene ug/kg 10300 100 65-13792 4103001200022300 21500
1,3-Dichlorobenzene ug/kg 10300 102 70-13096 510300<103 10500 9930
1,3-Dichloropropane ug/kg 10300 95 70-13095 010300<103 9800 9790
1,4-Dichlorobenzene ug/kg 10300 94 68-13092 110300<103 9680 9540
2,2-Dichloropropane ug/kg 10300 88 32-13083 610300<103 9100 8560
2-Butanone (MEK)ug/kg 20600 90 10-13691 0206001320J19900 20000
2-Chlorotoluene ug/kg 10300 107 69-141104 210300<103 11000 10700
2-Hexanone ug/kg 20600 94 10-14499 520600<1030 19500 20500
4-Chlorotoluene ug/kg 10300 93 70-13293 010300<103 9570 9610
4-Methyl-2-pentanone (MIBK) ug/kg 20600 94 25-14392 220600126020700 20300
Acetone ug/kg 20600 97 10-13099 220600250022600 23000
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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Huntersville, NC 28078
[phone]
Page 25 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3355230MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92553871004
3355231
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Benzene ug/kg 10300 103 67-13098 51030062711200 10700
Bromobenzene ug/kg 10300 98 70-13092 610300<103 10100 9490
Bromochloromethane ug/kg 10300 112 69-134103 810300<103 11500 10600
Bromodichloromethane ug/kg 10300 97 64-13093 510300<103 10000 9560
Bromoform ug/kg 10300 92 62-13091 110300<103 9490 9430
Bromomethane ug/kg v11030010520-176107 210300<206 10800 11000
Carbon tetrachloride ug/kg 10300 105 65-140100 510300<103 10800 10300
Chlorobenzene ug/kg 10300 99 70-13098 110300<103 10200 10100
Chloroethane ug/kg 10300 129 10-130119 810300<206 13300 12300
Chloroform ug/kg 10300 108 63-130102 61030086.0J 11200 10600
Chloromethane ug/kg 10300 107 58-130100 610300<206 11000 10300
cis-1,2-Dichloroethene ug/kg 10300 104 66-130101 310300<103 10700 10400
cis-1,3-Dichloropropene ug/kg 10300 91 67-13086 610300<103 9420 8900
Dibromochloromethane ug/kg 10300 98 67-13097 210300<103 10100 9950
Dibromomethane ug/kg 10300 104 63-13198 610300<103 10700 10100
Dichlorodifluoromethane ug/kg v11030014344-180135 510300<206 14700 14000
Diisopropyl ether ug/kg 10300 92 63-13088 410300<103 9480 9090
Ethylbenzene ug/kg 10300 105 66-130109 210300864019400 19900
Hexachloro-1,3-butadiene ug/kg 10300 96 64-15097 210300<206 9900 10100
Isopropylbenzene (Cumene) ug/kg 10300 117 69-135116 110300<103 12100 12000
m&p-Xylene ug/kg 20600 96 60-133104 3206003300052700 54400
Methyl-tert-butyl ether ug/kg 10300 92 65-13088 410300174011200 10800
Methylene Chloride ug/kg 10300 107 61-130100 710300<412 11200 10500
n-Butylbenzene ug/kg 10300 135 65-140137 110300<103 14000 14100
n-Propylbenzene ug/kg M11030014667-140145 010300<103 15000 15000
Naphthalene ug/kg 10300 89 15-14595 3103001050019700 20300
o-Xylene ug/kg 10300 99 66-133102 1103001550025700 26000
p-Isopropyltoluene ug/kg 10300 115 56-147114 110300<103 11800 11700
sec-Butylbenzene ug/kg 10300 100 65-139100 010300<103 10300 10300
Styrene ug/kg 10300 99 70-13297 21030046510700 10500
tert-Butylbenzene ug/kg 10300 103 62-13598 510300<103 10600 10100
Tetrachloroethene ug/kg 10300 100 70-13599 110300<103 10400 10200
Toluene ug/kg 10300 100 67-13096 210300941019700 19300
trans-1,2-Dichloroethene ug/kg 10300 110 69-130105 510300<103 11400 10800
trans-1,3-Dichloropropene ug/kg 10300 99 62-13095 410300<103 10200 9780
Trichloroethene ug/kg 10300 101 70-13595 510300<103 10400 9850
Trichlorofluoromethane ug/kg 10300 111 10-130105 510300<103 11400 10800
Vinyl acetate ug/kg 20600 97 53-13094 320600<1030 19900 19300
Vinyl chloride ug/kg 10300 129 61-148123 510300<206 13400 12700
Xylene (Total)ug/kg 30900 97 63-132103 3309004850078400 80400
1,2-Dichloroethane-d4 (S)%95 70-13094
4-Bromofluorobenzene (S)%101 69-134103
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 32
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
638921
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92554053001, 92554053002, 92554053003, 92554053004, 92554053005
Parameter Units
Dup
Result QualifiersRPDResult
92553871001
3354296SAMPLE DUPLICATE:
Percent Moisture %19.9 N2420.7
Parameter Units
Dup
Result QualifiersRPDResult
92554017001
3354297SAMPLE DUPLICATE:
Percent Moisture %25.7 N21730.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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Huntersville, NC 28078
[phone]
Page 27 of 32
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from samplere-analysis).S2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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[phone]
Page 28 of 32
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92554053
GILBARCO 11.990009.00
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92554053001 638973 638983SS-3 78 EPA 5035A/5030B EPA 8260D
92554053002 639155 639181SS-4 68 EPA 5035A/5030B EPA 8260D
92554053003 638973 638983SS-4 131 EPA 5035A/5030B EPA 8260D
92554053004 639155 639181SS-5 99 EPA 5035A/5030B EPA 8260D
92554053005 639155 639181SS-5 132 EPA 5035A/5030B EPA 8260D
92554053001 638921SS-3 78 SW-846
92554053002 638921SS-4 68 SW-846
92554053003 638921SS-4 131 SW-846
92554053004 638921SS-5 99 SW-846
92554053005 638921SS-5 132 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/11/2021 11:02 AM
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[phone]
Page 29 of 32
Page 30 of 32
Page 31 of 32
Page 32 of 32
#=CL#
September 13, 2021
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92559777
92559777
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
GILBARCO/11.990009.00
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on September 07, 2021. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lindsey N Wooten
[e-mail]
Project Manager
[phone]
Enclosures
cc: Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92559777001 SS-7 @ 6'2 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92559777002 SS-9 @ 6'1 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92559777003 SS-10 @ 6'EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92559777004 SS-11 @ 6'1 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 28
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92559777001 SS-7 @ 6'2
Methyl-tert-butyl ether 29.0 ug/kg 09/09/21 16:00 C711.9EPA 8260D
Percent Moisture 28.2 %09/08/21 12:45 N20.10SW-846
92559777002 SS-9 @ 6'1
Percent Moisture 17.6 %09/08/21 12:45 N20.10SW-846
92559777003 SS-10 @ 6'
Methyl-tert-butyl ether 20.4 ug/kg 09/09/21 16:35 C7,D67.1EPA 8260D
Percent Moisture 13.8 %09/08/21 12:45 N20.10SW-846
92559777004 SS-11 @ 6'1
n-Butylbenzene 7560 ug/kg 09/09/21 09:08 M1314EPA 8260D
sec-Butylbenzene 11100 ug/kg 09/09/21 09:08314EPA 8260D
Ethylbenzene 535 ug/kg 09/09/21 09:08314EPA 8260D
p-Isopropyltoluene 15600 ug/kg 09/09/21 09:08314EPA 8260D
4-Methyl-2-pentanone (MIBK)5480 ug/kg 09/09/21 09:083140EPA 8260D
Naphthalene 1270 ug/kg 09/09/21 09:08314EPA 8260D
1,2,4-Trimethylbenzene 43500 ug/kg 09/09/21 09:08314EPA 8260D
1,3,5-Trimethylbenzene 18500 ug/kg 09/09/21 09:08314EPA 8260D
Xylene (Total)3010 ug/kg 09/09/21 09:08628EPA 8260D
m&p-Xylene 3010 ug/kg 09/09/21 09:08628EPA 8260D
Percent Moisture 14.4 %09/08/21 12:45 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-7 @ 6'2 Lab ID: 92559777001 Collected: 09/03/21 11:18 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 09/09/21 16:00 67-64-1 v209/09/21 13:33237 1
Benzene ND ug/kg 09/09/21 16:00 71-43-209/09/21 13:3311.9 1
Bromobenzene ND ug/kg 09/09/21 16:00 108-86-109/09/21 13:3311.9 1
Bromochloromethane ND ug/kg 09/09/21 16:00 74-97-509/09/21 13:3311.9 1
Bromodichloromethane ND ug/kg 09/09/21 16:00 75-27-409/09/21 13:3311.9 1
Bromoform ND ug/kg 09/09/21 16:00 75-25-209/09/21 13:3311.9 1
Bromomethane ND ug/kg 09/09/21 16:00 74-83-909/09/21 13:3323.7 1
2-Butanone (MEK)ND ug/kg 09/09/21 16:00 78-93-3 v209/09/21 13:33237 1
n-Butylbenzene ND ug/kg 09/09/21 16:00 104-51-809/09/21 13:3311.9 1
sec-Butylbenzene ND ug/kg 09/09/21 16:00 135-98-809/09/21 13:3311.9 1
tert-Butylbenzene ND ug/kg 09/09/21 16:00 98-06-609/09/21 13:3311.9 1
Carbon tetrachloride ND ug/kg 09/09/21 16:00 56-23-509/09/21 13:3311.9 1
Chlorobenzene ND ug/kg 09/09/21 16:00 108-90-709/09/21 13:3311.9 1
Chloroethane ND ug/kg 09/09/21 16:00 75-00-309/09/21 13:3323.7 1
Chloroform ND ug/kg 09/09/21 16:00 67-66-309/09/21 13:3311.9 1
Chloromethane ND ug/kg 09/09/21 16:00 74-87-309/09/21 13:3323.7 1
2-Chlorotoluene ND ug/kg 09/09/21 16:00 95-49-809/09/21 13:3311.9 1
4-Chlorotoluene ND ug/kg 09/09/21 16:00 106-43-409/09/21 13:3311.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/09/21 16:00 96-12-809/09/21 13:3311.9 1
Dibromochloromethane ND ug/kg 09/09/21 16:00 124-48-109/09/21 13:3311.9 1
1,2-Dibromoethane (EDB)ND ug/kg 09/09/21 16:00 106-93-409/09/21 13:3311.9 1
Dibromomethane ND ug/kg 09/09/21 16:00 74-95-309/09/21 13:3311.9 1
1,2-Dichlorobenzene ND ug/kg 09/09/21 16:00 95-50-109/09/21 13:3311.9 1
1,3-Dichlorobenzene ND ug/kg 09/09/21 16:00 541-73-109/09/21 13:3311.9 1
1,4-Dichlorobenzene ND ug/kg 09/09/21 16:00 106-46-709/09/21 13:3311.9 1
Dichlorodifluoromethane ND ug/kg 09/09/21 16:00 75-71-809/09/21 13:3323.7 1
1,1-Dichloroethane ND ug/kg 09/09/21 16:00 75-34-309/09/21 13:3311.9 1
1,2-Dichloroethane ND ug/kg 09/09/21 16:00 107-06-209/09/21 13:3311.9 1
1,1-Dichloroethene ND ug/kg 09/09/21 16:00 75-35-409/09/21 13:3311.9 1
cis-1,2-Dichloroethene ND ug/kg 09/09/21 16:00 156-59-209/09/21 13:3311.9 1
trans-1,2-Dichloroethene ND ug/kg 09/09/21 16:00 156-60-509/09/21 13:3311.9 1
1,2-Dichloropropane ND ug/kg 09/09/21 16:00 78-87-509/09/21 13:3311.9 1
1,3-Dichloropropane ND ug/kg 09/09/21 16:00 142-28-909/09/21 13:3311.9 1
2,2-Dichloropropane ND ug/kg 09/09/21 16:00 594-20-709/09/21 13:3311.9 1
1,1-Dichloropropene ND ug/kg 09/09/21 16:00 563-58-609/09/21 13:3311.9 1
cis-1,3-Dichloropropene ND ug/kg 09/09/21 16:00 10061-01-509/09/21 13:3311.9 1
trans-1,3-Dichloropropene ND ug/kg 09/09/21 16:00 10061-02-609/09/21 13:3311.9 1
Diisopropyl ether ND ug/kg 09/09/21 16:00 108-20-309/09/21 13:3311.9 1
Ethylbenzene ND ug/kg 09/09/21 16:00 100-41-409/09/21 13:3311.9 1
Hexachloro-1,3-butadiene ND ug/kg 09/09/21 16:00 87-68-309/09/21 13:3323.7 1
2-Hexanone ND ug/kg 09/09/21 16:00 591-78-6 v209/09/21 13:33119 1
Isopropylbenzene (Cumene)ND ug/kg 09/09/21 16:00 98-82-809/09/21 13:3311.9 1
p-Isopropyltoluene ND ug/kg 09/09/21 16:00 99-87-609/09/21 13:3311.9 1
Methylene Chloride ND ug/kg 09/09/21 16:00 75-09-209/09/21 13:3347.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/09/21 16:00 108-10-1 v209/09/21 13:33119 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-7 @ 6'2 Lab ID: 92559777001 Collected: 09/03/21 11:18 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether 29.0 ug/kg 09/09/21 16:00 1634-04-4 C709/09/21 13:3311.9 1
Naphthalene ND ug/kg 09/09/21 16:00 91-20-309/09/21 13:3311.9 1
n-Propylbenzene ND ug/kg 09/09/21 16:00 103-65-109/09/21 13:3311.9 1
Styrene ND ug/kg 09/09/21 16:00 100-42-509/09/21 13:3311.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/09/21 16:00 630-20-609/09/21 13:3311.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/09/21 16:00 79-34-509/09/21 13:3311.9 1
Tetrachloroethene ND ug/kg 09/09/21 16:00 127-18-409/09/21 13:3311.9 1
Toluene ND ug/kg 09/09/21 16:00 108-88-309/09/21 13:3311.9 1
1,2,3-Trichlorobenzene ND ug/kg 09/09/21 16:00 87-61-609/09/21 13:3311.9 1
1,2,4-Trichlorobenzene ND ug/kg 09/09/21 16:00 120-82-109/09/21 13:3311.9 1
1,1,1-Trichloroethane ND ug/kg 09/09/21 16:00 71-55-609/09/21 13:3311.9 1
1,1,2-Trichloroethane ND ug/kg 09/09/21 16:00 79-00-509/09/21 13:3311.9 1
Trichloroethene ND ug/kg 09/09/21 16:00 79-01-609/09/21 13:3311.9 1
Trichlorofluoromethane ND ug/kg 09/09/21 16:00 75-69-409/09/21 13:3311.9 1
1,2,3-Trichloropropane ND ug/kg 09/09/21 16:00 96-18-409/09/21 13:3311.9 1
1,2,4-Trimethylbenzene ND ug/kg 09/09/21 16:00 95-63-609/09/21 13:3311.9 1
1,3,5-Trimethylbenzene ND ug/kg 09/09/21 16:00 108-67-809/09/21 13:3311.9 1
Vinyl acetate ND ug/kg 09/09/21 16:00 108-05-409/09/21 13:33119 1
Vinyl chloride ND ug/kg 09/09/21 16:00 75-01-409/09/21 13:3323.7 1
Xylene (Total)ND ug/kg 09/09/21 16:00 1330-20-709/09/21 13:3323.7 1
m&p-Xylene ND ug/kg 09/09/21 16:00 179601-23-109/09/21 13:3323.7 1
o-Xylene ND ug/kg 09/09/21 16:00 95-47-609/09/21 13:3311.9 1
Surrogates
Toluene-d8 (S)99 %09/09/21 16:00 2037-26-509/09/21 13:3370-130 1
4-Bromofluorobenzene (S)99 %09/09/21 16:00 460-00-409/09/21 13:3369-134 1
1,2-Dichloroethane-d4 (S)93 %09/09/21 16:00 17060-07-009/09/21 13:3370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 28.2 %09/08/21 12:45 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-9 @ 6'1 Lab ID: 92559777002 Collected: 09/03/21 11:37 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 09/09/21 16:18 67-64-1 v209/09/21 13:33161 1
Benzene ND ug/kg 09/09/21 16:18 71-43-209/09/21 13:338.0 1
Bromobenzene ND ug/kg 09/09/21 16:18 108-86-109/09/21 13:338.0 1
Bromochloromethane ND ug/kg 09/09/21 16:18 74-97-509/09/21 13:338.0 1
Bromodichloromethane ND ug/kg 09/09/21 16:18 75-27-409/09/21 13:338.0 1
Bromoform ND ug/kg 09/09/21 16:18 75-25-209/09/21 13:338.0 1
Bromomethane ND ug/kg 09/09/21 16:18 74-83-909/09/21 13:3316.1 1
2-Butanone (MEK)ND ug/kg 09/09/21 16:18 78-93-3 v209/09/21 13:33161 1
n-Butylbenzene ND ug/kg 09/09/21 16:18 104-51-809/09/21 13:338.0 1
sec-Butylbenzene ND ug/kg 09/09/21 16:18 135-98-809/09/21 13:338.0 1
tert-Butylbenzene ND ug/kg 09/09/21 16:18 98-06-609/09/21 13:338.0 1
Carbon tetrachloride ND ug/kg 09/09/21 16:18 56-23-509/09/21 13:338.0 1
Chlorobenzene ND ug/kg 09/09/21 16:18 108-90-709/09/21 13:338.0 1
Chloroethane ND ug/kg 09/09/21 16:18 75-00-309/09/21 13:3316.1 1
Chloroform ND ug/kg 09/09/21 16:18 67-66-309/09/21 13:338.0 1
Chloromethane ND ug/kg 09/09/21 16:18 74-87-309/09/21 13:3316.1 1
2-Chlorotoluene ND ug/kg 09/09/21 16:18 95-49-809/09/21 13:338.0 1
4-Chlorotoluene ND ug/kg 09/09/21 16:18 106-43-409/09/21 13:338.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/09/21 16:18 96-12-809/09/21 13:338.0 1
Dibromochloromethane ND ug/kg 09/09/21 16:18 124-48-109/09/21 13:338.0 1
1,2-Dibromoethane (EDB)ND ug/kg 09/09/21 16:18 106-93-409/09/21 13:338.0 1
Dibromomethane ND ug/kg 09/09/21 16:18 74-95-309/09/21 13:338.0 1
1,2-Dichlorobenzene ND ug/kg 09/09/21 16:18 95-50-109/09/21 13:338.0 1
1,3-Dichlorobenzene ND ug/kg 09/09/21 16:18 541-73-109/09/21 13:338.0 1
1,4-Dichlorobenzene ND ug/kg 09/09/21 16:18 106-46-709/09/21 13:338.0 1
Dichlorodifluoromethane ND ug/kg 09/09/21 16:18 75-71-809/09/21 13:3316.1 1
1,1-Dichloroethane ND ug/kg 09/09/21 16:18 75-34-309/09/21 13:338.0 1
1,2-Dichloroethane ND ug/kg 09/09/21 16:18 107-06-209/09/21 13:338.0 1
1,1-Dichloroethene ND ug/kg 09/09/21 16:18 75-35-409/09/21 13:338.0 1
cis-1,2-Dichloroethene ND ug/kg 09/09/21 16:18 156-59-209/09/21 13:338.0 1
trans-1,2-Dichloroethene ND ug/kg 09/09/21 16:18 156-60-509/09/21 13:338.0 1
1,2-Dichloropropane ND ug/kg 09/09/21 16:18 78-87-509/09/21 13:338.0 1
1,3-Dichloropropane ND ug/kg 09/09/21 16:18 142-28-909/09/21 13:338.0 1
2,2-Dichloropropane ND ug/kg 09/09/21 16:18 594-20-709/09/21 13:338.0 1
1,1-Dichloropropene ND ug/kg 09/09/21 16:18 563-58-609/09/21 13:338.0 1
cis-1,3-Dichloropropene ND ug/kg 09/09/21 16:18 10061-01-509/09/21 13:338.0 1
trans-1,3-Dichloropropene ND ug/kg 09/09/21 16:18 10061-02-609/09/21 13:338.0 1
Diisopropyl ether ND ug/kg 09/09/21 16:18 108-20-309/09/21 13:338.0 1
Ethylbenzene ND ug/kg 09/09/21 16:18 100-41-409/09/21 13:338.0 1
Hexachloro-1,3-butadiene ND ug/kg 09/09/21 16:18 87-68-309/09/21 13:3316.1 1
2-Hexanone ND ug/kg 09/09/21 16:18 591-78-6 v209/09/21 13:3380.3 1
Isopropylbenzene (Cumene)ND ug/kg 09/09/21 16:18 98-82-809/09/21 13:338.0 1
p-Isopropyltoluene ND ug/kg 09/09/21 16:18 99-87-609/09/21 13:338.0 1
Methylene Chloride ND ug/kg 09/09/21 16:18 75-09-209/09/21 13:3332.1 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/09/21 16:18 108-10-1 v209/09/21 13:3380.3 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-9 @ 6'1 Lab ID: 92559777002 Collected: 09/03/21 11:37 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 09/09/21 16:18 1634-04-409/09/21 13:338.0 1
Naphthalene ND ug/kg 09/09/21 16:18 91-20-309/09/21 13:338.0 1
n-Propylbenzene ND ug/kg 09/09/21 16:18 103-65-109/09/21 13:338.0 1
Styrene ND ug/kg 09/09/21 16:18 100-42-509/09/21 13:338.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/09/21 16:18 630-20-609/09/21 13:338.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/09/21 16:18 79-34-509/09/21 13:338.0 1
Tetrachloroethene ND ug/kg 09/09/21 16:18 127-18-409/09/21 13:338.0 1
Toluene ND ug/kg 09/09/21 16:18 108-88-309/09/21 13:338.0 1
1,2,3-Trichlorobenzene ND ug/kg 09/09/21 16:18 87-61-609/09/21 13:338.0 1
1,2,4-Trichlorobenzene ND ug/kg 09/09/21 16:18 120-82-109/09/21 13:338.0 1
1,1,1-Trichloroethane ND ug/kg 09/09/21 16:18 71-55-609/09/21 13:338.0 1
1,1,2-Trichloroethane ND ug/kg 09/09/21 16:18 79-00-509/09/21 13:338.0 1
Trichloroethene ND ug/kg 09/09/21 16:18 79-01-609/09/21 13:338.0 1
Trichlorofluoromethane ND ug/kg 09/09/21 16:18 75-69-409/09/21 13:338.0 1
1,2,3-Trichloropropane ND ug/kg 09/09/21 16:18 96-18-409/09/21 13:338.0 1
1,2,4-Trimethylbenzene ND ug/kg 09/09/21 16:18 95-63-609/09/21 13:338.0 1
1,3,5-Trimethylbenzene ND ug/kg 09/09/21 16:18 108-67-809/09/21 13:338.0 1
Vinyl acetate ND ug/kg 09/09/21 16:18 108-05-409/09/21 13:3380.3 1
Vinyl chloride ND ug/kg 09/09/21 16:18 75-01-409/09/21 13:3316.1 1
Xylene (Total)ND ug/kg 09/09/21 16:18 1330-20-709/09/21 13:3316.1 1
m&p-Xylene ND ug/kg 09/09/21 16:18 179601-23-109/09/21 13:3316.1 1
o-Xylene ND ug/kg 09/09/21 16:18 95-47-609/09/21 13:338.0 1
Surrogates
Toluene-d8 (S)101 %09/09/21 16:18 2037-26-509/09/21 13:3370-130 1
4-Bromofluorobenzene (S)100 %09/09/21 16:18 460-00-409/09/21 13:3369-134 1
1,2-Dichloroethane-d4 (S)95 %09/09/21 16:18 17060-07-009/09/21 13:3370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.6 %09/08/21 12:45 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-10 @ 6'Lab ID: 92559777003 Collected: 09/03/21 13:32 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 09/09/21 16:35 67-64-1 v209/09/21 13:33142 1
Benzene ND ug/kg 09/09/21 16:35 71-43-209/09/21 13:337.1 1
Bromobenzene ND ug/kg 09/09/21 16:35 108-86-109/09/21 13:337.1 1
Bromochloromethane ND ug/kg 09/09/21 16:35 74-97-509/09/21 13:337.1 1
Bromodichloromethane ND ug/kg 09/09/21 16:35 75-27-409/09/21 13:337.1 1
Bromoform ND ug/kg 09/09/21 16:35 75-25-209/09/21 13:337.1 1
Bromomethane ND ug/kg 09/09/21 16:35 74-83-909/09/21 13:3314.2 1
2-Butanone (MEK)ND ug/kg 09/09/21 16:35 78-93-3 v209/09/21 13:33142 1
n-Butylbenzene ND ug/kg 09/09/21 16:35 104-51-809/09/21 13:337.1 1
sec-Butylbenzene ND ug/kg 09/09/21 16:35 135-98-809/09/21 13:337.1 1
tert-Butylbenzene ND ug/kg 09/09/21 16:35 98-06-609/09/21 13:337.1 1
Carbon tetrachloride ND ug/kg 09/09/21 16:35 56-23-509/09/21 13:337.1 1
Chlorobenzene ND ug/kg 09/09/21 16:35 108-90-709/09/21 13:337.1 1
Chloroethane ND ug/kg 09/09/21 16:35 75-00-309/09/21 13:3314.2 1
Chloroform ND ug/kg 09/09/21 16:35 67-66-309/09/21 13:337.1 1
Chloromethane ND ug/kg 09/09/21 16:35 74-87-309/09/21 13:3314.2 1
2-Chlorotoluene ND ug/kg 09/09/21 16:35 95-49-809/09/21 13:337.1 1
4-Chlorotoluene ND ug/kg 09/09/21 16:35 106-43-409/09/21 13:337.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/09/21 16:35 96-12-809/09/21 13:337.1 1
Dibromochloromethane ND ug/kg 09/09/21 16:35 124-48-109/09/21 13:337.1 1
1,2-Dibromoethane (EDB)ND ug/kg 09/09/21 16:35 106-93-409/09/21 13:337.1 1
Dibromomethane ND ug/kg 09/09/21 16:35 74-95-309/09/21 13:337.1 1
1,2-Dichlorobenzene ND ug/kg 09/09/21 16:35 95-50-109/09/21 13:337.1 1
1,3-Dichlorobenzene ND ug/kg 09/09/21 16:35 541-73-109/09/21 13:337.1 1
1,4-Dichlorobenzene ND ug/kg 09/09/21 16:35 106-46-709/09/21 13:337.1 1
Dichlorodifluoromethane ND ug/kg 09/09/21 16:35 75-71-809/09/21 13:3314.2 1
1,1-Dichloroethane ND ug/kg 09/09/21 16:35 75-34-309/09/21 13:337.1 1
1,2-Dichloroethane ND ug/kg 09/09/21 16:35 107-06-209/09/21 13:337.1 1
1,1-Dichloroethene ND ug/kg 09/09/21 16:35 75-35-409/09/21 13:337.1 1
cis-1,2-Dichloroethene ND ug/kg 09/09/21 16:35 156-59-209/09/21 13:337.1 1
trans-1,2-Dichloroethene ND ug/kg 09/09/21 16:35 156-60-509/09/21 13:337.1 1
1,2-Dichloropropane ND ug/kg 09/09/21 16:35 78-87-509/09/21 13:337.1 1
1,3-Dichloropropane ND ug/kg 09/09/21 16:35 142-28-909/09/21 13:337.1 1
2,2-Dichloropropane ND ug/kg 09/09/21 16:35 594-20-709/09/21 13:337.1 1
1,1-Dichloropropene ND ug/kg 09/09/21 16:35 563-58-609/09/21 13:337.1 1
cis-1,3-Dichloropropene ND ug/kg 09/09/21 16:35 10061-01-509/09/21 13:337.1 1
trans-1,3-Dichloropropene ND ug/kg 09/09/21 16:35 10061-02-609/09/21 13:337.1 1
Diisopropyl ether ND ug/kg 09/09/21 16:35 108-20-309/09/21 13:337.1 1
Ethylbenzene ND ug/kg 09/09/21 16:35 100-41-409/09/21 13:337.1 1
Hexachloro-1,3-butadiene ND ug/kg 09/09/21 16:35 87-68-309/09/21 13:3314.2 1
2-Hexanone ND ug/kg 09/09/21 16:35 591-78-6 v209/09/21 13:3370.8 1
Isopropylbenzene (Cumene)ND ug/kg 09/09/21 16:35 98-82-809/09/21 13:337.1 1
p-Isopropyltoluene ND ug/kg 09/09/21 16:35 99-87-609/09/21 13:337.1 1
Methylene Chloride ND ug/kg 09/09/21 16:35 75-09-209/09/21 13:3328.3 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/09/21 16:35 108-10-1 v209/09/21 13:3370.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-10 @ 6'Lab ID: 92559777003 Collected: 09/03/21 13:32 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether 20.4 ug/kg 09/09/21 16:35 1634-04-4 C7,D609/09/21 13:337.1 1
Naphthalene ND ug/kg 09/09/21 16:35 91-20-309/09/21 13:337.1 1
n-Propylbenzene ND ug/kg 09/09/21 16:35 103-65-109/09/21 13:337.1 1
Styrene ND ug/kg 09/09/21 16:35 100-42-509/09/21 13:337.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/09/21 16:35 630-20-609/09/21 13:337.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/09/21 16:35 79-34-509/09/21 13:337.1 1
Tetrachloroethene ND ug/kg 09/09/21 16:35 127-18-409/09/21 13:337.1 1
Toluene ND ug/kg 09/09/21 16:35 108-88-309/09/21 13:337.1 1
1,2,3-Trichlorobenzene ND ug/kg 09/09/21 16:35 87-61-609/09/21 13:337.1 1
1,2,4-Trichlorobenzene ND ug/kg 09/09/21 16:35 120-82-109/09/21 13:337.1 1
1,1,1-Trichloroethane ND ug/kg 09/09/21 16:35 71-55-609/09/21 13:337.1 1
1,1,2-Trichloroethane ND ug/kg 09/09/21 16:35 79-00-509/09/21 13:337.1 1
Trichloroethene ND ug/kg 09/09/21 16:35 79-01-609/09/21 13:337.1 1
Trichlorofluoromethane ND ug/kg 09/09/21 16:35 75-69-409/09/21 13:337.1 1
1,2,3-Trichloropropane ND ug/kg 09/09/21 16:35 96-18-409/09/21 13:337.1 1
1,2,4-Trimethylbenzene ND ug/kg 09/09/21 16:35 95-63-609/09/21 13:337.1 1
1,3,5-Trimethylbenzene ND ug/kg 09/09/21 16:35 108-67-809/09/21 13:337.1 1
Vinyl acetate ND ug/kg 09/09/21 16:35 108-05-409/09/21 13:3370.8 1
Vinyl chloride ND ug/kg 09/09/21 16:35 75-01-409/09/21 13:3314.2 1
Xylene (Total)ND ug/kg 09/09/21 16:35 1330-20-709/09/21 13:3314.2 1
m&p-Xylene ND ug/kg 09/09/21 16:35 179601-23-109/09/21 13:3314.2 1
o-Xylene ND ug/kg 09/09/21 16:35 95-47-609/09/21 13:337.1 1
Surrogates
Toluene-d8 (S)102 %09/09/21 16:35 2037-26-509/09/21 13:3370-130 1
4-Bromofluorobenzene (S)96 %09/09/21 16:35 460-00-409/09/21 13:3369-134 1
1,2-Dichloroethane-d4 (S)95 %09/09/21 16:35 17060-07-009/09/21 13:3370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.8 %09/08/21 12:45 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-11 @ 6'1 Lab ID: 92559777004 Collected: 09/03/21 13:52 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 09/09/21 09:08 67-64-109/08/21 16:586280 50
Benzene ND ug/kg 09/09/21 09:08 71-43-209/08/21 16:58314 50
Bromobenzene ND ug/kg 09/09/21 09:08 108-86-109/08/21 16:58314 50
Bromochloromethane ND ug/kg 09/09/21 09:08 74-97-509/08/21 16:58314 50
Bromodichloromethane ND ug/kg 09/09/21 09:08 75-27-409/08/21 16:58314 50
Bromoform ND ug/kg 09/09/21 09:08 75-25-209/08/21 16:58314 50
Bromomethane ND ug/kg 09/09/21 09:08 74-83-909/08/21 16:58628 50
2-Butanone (MEK)ND ug/kg 09/09/21 09:08 78-93-309/08/21 16:586280 50
n-Butylbenzene 7560 ug/kg 09/09/21 09:08 104-51-8 M109/08/21 16:58314 50
sec-Butylbenzene 11100 ug/kg 09/09/21 09:08 135-98-809/08/21 16:58314 50
tert-Butylbenzene ND ug/kg 09/09/21 09:08 98-06-609/08/21 16:58314 50
Carbon tetrachloride ND ug/kg 09/09/21 09:08 56-23-509/08/21 16:58314 50
Chlorobenzene ND ug/kg 09/09/21 09:08 108-90-709/08/21 16:58314 50
Chloroethane ND ug/kg 09/09/21 09:08 75-00-309/08/21 16:58628 50
Chloroform ND ug/kg 09/09/21 09:08 67-66-309/08/21 16:58314 50
Chloromethane ND ug/kg 09/09/21 09:08 74-87-309/08/21 16:58628 50
2-Chlorotoluene ND ug/kg 09/09/21 09:08 95-49-809/08/21 16:58314 50
4-Chlorotoluene ND ug/kg 09/09/21 09:08 106-43-409/08/21 16:58314 50
1,2-Dibromo-3-chloropropane ND ug/kg 09/09/21 09:08 96-12-809/08/21 16:58314 50
Dibromochloromethane ND ug/kg 09/09/21 09:08 124-48-109/08/21 16:58314 50
1,2-Dibromoethane (EDB)ND ug/kg 09/09/21 09:08 106-93-409/08/21 16:58314 50
Dibromomethane ND ug/kg 09/09/21 09:08 74-95-309/08/21 16:58314 50
1,2-Dichlorobenzene ND ug/kg 09/09/21 09:08 95-50-109/08/21 16:58314 50
1,3-Dichlorobenzene ND ug/kg 09/09/21 09:08 541-73-109/08/21 16:58314 50
1,4-Dichlorobenzene ND ug/kg 09/09/21 09:08 106-46-709/08/21 16:58314 50
Dichlorodifluoromethane ND ug/kg 09/09/21 09:08 75-71-809/08/21 16:58628 50
1,1-Dichloroethane ND ug/kg 09/09/21 09:08 75-34-309/08/21 16:58314 50
1,2-Dichloroethane ND ug/kg 09/09/21 09:08 107-06-209/08/21 16:58314 50
1,1-Dichloroethene ND ug/kg 09/09/21 09:08 75-35-409/08/21 16:58314 50
cis-1,2-Dichloroethene ND ug/kg 09/09/21 09:08 156-59-209/08/21 16:58314 50
trans-1,2-Dichloroethene ND ug/kg 09/09/21 09:08 156-60-509/08/21 16:58314 50
1,2-Dichloropropane ND ug/kg 09/09/21 09:08 78-87-509/08/21 16:58314 50
1,3-Dichloropropane ND ug/kg 09/09/21 09:08 142-28-909/08/21 16:58314 50
2,2-Dichloropropane ND ug/kg 09/09/21 09:08 594-20-709/08/21 16:58314 50
1,1-Dichloropropene ND ug/kg 09/09/21 09:08 563-58-609/08/21 16:58314 50
cis-1,3-Dichloropropene ND ug/kg 09/09/21 09:08 10061-01-509/08/21 16:58314 50
trans-1,3-Dichloropropene ND ug/kg 09/09/21 09:08 10061-02-609/08/21 16:58314 50
Diisopropyl ether ND ug/kg 09/09/21 09:08 108-20-309/08/21 16:58314 50
Ethylbenzene 535 ug/kg 09/09/21 09:08 100-41-409/08/21 16:58314 50
Hexachloro-1,3-butadiene ND ug/kg 09/09/21 09:08 87-68-3 M109/08/21 16:58628 50
2-Hexanone ND ug/kg 09/09/21 09:08 591-78-609/08/21 16:583140 50
Isopropylbenzene (Cumene)ND ug/kg 09/09/21 09:08 98-82-809/08/21 16:58314 50
p-Isopropyltoluene 15600 ug/kg 09/09/21 09:08 99-87-609/08/21 16:58314 50
Methylene Chloride ND ug/kg 09/09/21 09:08 75-09-209/08/21 16:581260 50
4-Methyl-2-pentanone (MIBK)5480 ug/kg 09/09/21 09:08 108-10-109/08/21 16:583140 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Sample: SS-11 @ 6'1 Lab ID: 92559777004 Collected: 09/03/21 13:52 Received: 09/07/21 10:54 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 09/09/21 09:08 1634-04-409/08/21 16:58314 50
Naphthalene 1270 ug/kg 09/09/21 09:08 91-20-309/08/21 16:58314 50
n-Propylbenzene ND ug/kg 09/09/21 09:08 103-65-109/08/21 16:58314 50
Styrene ND ug/kg 09/09/21 09:08 100-42-509/08/21 16:58314 50
1,1,1,2-Tetrachloroethane ND ug/kg 09/09/21 09:08 630-20-609/08/21 16:58314 50
1,1,2,2-Tetrachloroethane ND ug/kg 09/09/21 09:08 79-34-5 M109/08/21 16:58314 50
Tetrachloroethene ND ug/kg 09/09/21 09:08 127-18-409/08/21 16:58314 50
Toluene ND ug/kg 09/09/21 09:08 108-88-309/08/21 16:58314 50
1,2,3-Trichlorobenzene ND ug/kg 09/09/21 09:08 87-61-609/08/21 16:58314 50
1,2,4-Trichlorobenzene ND ug/kg 09/09/21 09:08 120-82-109/08/21 16:58314 50
1,1,1-Trichloroethane ND ug/kg 09/09/21 09:08 71-55-6 v2,v309/08/21 16:58314 50
1,1,2-Trichloroethane ND ug/kg 09/09/21 09:08 79-00-509/08/21 16:58314 50
Trichloroethene ND ug/kg 09/09/21 09:08 79-01-609/08/21 16:58314 50
Trichlorofluoromethane ND ug/kg 09/09/21 09:08 75-69-409/08/21 16:58314 50
1,2,3-Trichloropropane ND ug/kg 09/09/21 09:08 96-18-409/08/21 16:58314 50
1,2,4-Trimethylbenzene 43500 ug/kg 09/09/21 09:08 95-63-609/08/21 16:58314 50
1,3,5-Trimethylbenzene 18500 ug/kg 09/09/21 09:08 108-67-809/08/21 16:58314 50
Vinyl acetate ND ug/kg 09/09/21 09:08 108-05-409/08/21 16:583140 50
Vinyl chloride ND ug/kg 09/09/21 09:08 75-01-409/08/21 16:58628 50
Xylene (Total)3010 ug/kg 09/09/21 09:08 1330-20-709/08/21 16:58628 50
m&p-Xylene 3010 ug/kg 09/09/21 09:08 179601-23-109/08/21 16:58628 50
o-Xylene ND ug/kg 09/09/21 09:08 95-47-609/08/21 16:58314 50
Surrogates
Toluene-d8 (S)99 %09/09/21 09:08 2037-26-5 D309/08/21 16:5870-130 50
4-Bromofluorobenzene (S)134 %09/09/21 09:08 460-00-409/08/21 16:5869-134 50
1,2-Dichloroethane-d4 (S)101 %09/09/21 09:08 17060-07-009/08/21 16:5870-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.4 %09/08/21 12:45 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
645905
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92559777004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3388059
Associated Lab Samples:92559777004
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/09/21 00:30
1,1,1-Trichloroethane ug/kg ND 5.0 v209/09/21 00:30
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/09/21 00:30
1,1,2-Trichloroethane ug/kg ND 5.0 09/09/21 00:30
1,1-Dichloroethane ug/kg ND 5.0 09/09/21 00:30
1,1-Dichloroethene ug/kg ND 5.0 09/09/21 00:30
1,1-Dichloropropene ug/kg ND 5.0 09/09/21 00:30
1,2,3-Trichlorobenzene ug/kg ND 5.0 09/09/21 00:30
1,2,3-Trichloropropane ug/kg ND 5.0 09/09/21 00:30
1,2,4-Trichlorobenzene ug/kg ND 5.0 09/09/21 00:30
1,2,4-Trimethylbenzene ug/kg ND 5.0 09/09/21 00:30
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/09/21 00:30
1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/09/21 00:30
1,2-Dichlorobenzene ug/kg ND 5.0 09/09/21 00:30
1,2-Dichloroethane ug/kg ND 5.0 09/09/21 00:30
1,2-Dichloropropane ug/kg ND 5.0 09/09/21 00:30
1,3,5-Trimethylbenzene ug/kg ND 5.0 09/09/21 00:30
1,3-Dichlorobenzene ug/kg ND 5.0 09/09/21 00:30
1,3-Dichloropropane ug/kg ND 5.0 09/09/21 00:30
1,4-Dichlorobenzene ug/kg ND 5.0 09/09/21 00:30
2,2-Dichloropropane ug/kg ND 5.0 09/09/21 00:30
2-Butanone (MEK)ug/kg ND 100 09/09/21 00:30
2-Chlorotoluene ug/kg ND 5.0 09/09/21 00:30
2-Hexanone ug/kg ND 50.0 09/09/21 00:30
4-Chlorotoluene ug/kg ND 5.0 09/09/21 00:30
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/09/21 00:30
Acetone ug/kg ND 100 09/09/21 00:30
Benzene ug/kg ND 5.0 09/09/21 00:30
Bromobenzene ug/kg ND 5.0 09/09/21 00:30
Bromochloromethane ug/kg ND 5.0 09/09/21 00:30
Bromodichloromethane ug/kg ND 5.0 09/09/21 00:30
Bromoform ug/kg ND 5.0 09/09/21 00:30
Bromomethane ug/kg ND 10.0 09/09/21 00:30
Carbon tetrachloride ug/kg ND 5.0 09/09/21 00:30
Chlorobenzene ug/kg ND 5.0 09/09/21 00:30
Chloroethane ug/kg ND 10.0 09/09/21 00:30
Chloroform ug/kg ND 5.0 09/09/21 00:30
Chloromethane ug/kg ND 10.0 09/09/21 00:30
cis-1,2-Dichloroethene ug/kg ND 5.0 09/09/21 00:30
cis-1,3-Dichloropropene ug/kg ND 5.0 09/09/21 00:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3388059
Associated Lab Samples:92559777004
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 09/09/21 00:30
Dibromomethane ug/kg ND 5.0 09/09/21 00:30
Dichlorodifluoromethane ug/kg ND 10.0 09/09/21 00:30
Diisopropyl ether ug/kg ND 5.0 09/09/21 00:30
Ethylbenzene ug/kg ND 5.0 09/09/21 00:30
Hexachloro-1,3-butadiene ug/kg ND 10.0 09/09/21 00:30
Isopropylbenzene (Cumene)ug/kg ND 5.0 09/09/21 00:30
m&p-Xylene ug/kg ND 10.0 09/09/21 00:30
Methyl-tert-butyl ether ug/kg ND 5.0 09/09/21 00:30
Methylene Chloride ug/kg ND 20.0 09/09/21 00:30
n-Butylbenzene ug/kg ND 5.0 09/09/21 00:30
n-Propylbenzene ug/kg ND 5.0 09/09/21 00:30
Naphthalene ug/kg ND 5.0 09/09/21 00:30
o-Xylene ug/kg ND 5.0 09/09/21 00:30
p-Isopropyltoluene ug/kg ND 5.0 09/09/21 00:30
sec-Butylbenzene ug/kg ND 5.0 09/09/21 00:30
Styrene ug/kg ND 5.0 09/09/21 00:30
tert-Butylbenzene ug/kg ND 5.0 09/09/21 00:30
Tetrachloroethene ug/kg ND 5.0 09/09/21 00:30
Toluene ug/kg ND 5.0 09/09/21 00:30
trans-1,2-Dichloroethene ug/kg ND 5.0 09/09/21 00:30
trans-1,3-Dichloropropene ug/kg ND 5.0 09/09/21 00:30
Trichloroethene ug/kg ND 5.0 09/09/21 00:30
Trichlorofluoromethane ug/kg ND 5.0 09/09/21 00:30
Vinyl acetate ug/kg ND 50.0 09/09/21 00:30
Vinyl chloride ug/kg ND 10.0 09/09/21 00:30
Xylene (Total)ug/kg ND 10.0 09/09/21 00:30
1,2-Dichloroethane-d4 (S)%104 70-130 09/09/21 00:30
4-Bromofluorobenzene (S)%101 69-134 09/09/21 00:30
Toluene-d8 (S)%98 70-130 09/09/21 00:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3388060LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 11901250 95 70-130
1,1,1-Trichloroethane ug/kg 1010 v3125081 70-130
1,1,2,2-Tetrachloroethane ug/kg 11301250 90 70-130
1,1,2-Trichloroethane ug/kg 10301250 83 70-130
1,1-Dichloroethane ug/kg 11301250 90 70-130
1,1-Dichloroethene ug/kg 11801250 94 70-130
1,1-Dichloropropene ug/kg 11601250 93 70-130
1,2,3-Trichlorobenzene ug/kg 11901250 95 65-130
1,2,3-Trichloropropane ug/kg 11801250 94 70-130
1,2,4-Trichlorobenzene ug/kg 11901250 95 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3388060LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 11201250 89 70-130
1,2-Dibromo-3-chloropropane ug/kg 12401250 99 70-130
1,2-Dibromoethane (EDB)ug/kg 11701250 94 70-130
1,2-Dichlorobenzene ug/kg 11901250 95 70-130
1,2-Dichloroethane ug/kg 11501250 92 63-130
1,2-Dichloropropane ug/kg 11601250 93 70-130
1,3,5-Trimethylbenzene ug/kg 11101250 89 70-130
1,3-Dichlorobenzene ug/kg 11801250 95 70-130
1,3-Dichloropropane ug/kg 11801250 94 70-130
1,4-Dichlorobenzene ug/kg 11901250 96 70-130
2,2-Dichloropropane ug/kg 11101250 89 66-130
2-Butanone (MEK)ug/kg 22002500 88 70-130
2-Chlorotoluene ug/kg 12001250 96 70-130
2-Hexanone ug/kg 22802500 91 70-130
4-Chlorotoluene ug/kg 11601250 93 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 22102500 89 70-130
Acetone ug/kg 21702500 87 69-130
Benzene ug/kg 11401250 91 70-130
Bromobenzene ug/kg 12101250 97 70-130
Bromochloromethane ug/kg 12201250 97 70-130
Bromodichloromethane ug/kg 10101250 80 69-130
Bromoform ug/kg 11501250 92 70-130
Bromomethane ug/kg 10501250 84 52-130
Carbon tetrachloride ug/kg 11401250 91 70-130
Chlorobenzene ug/kg 12001250 96 70-130
Chloroethane ug/kg 11301250 90 65-130
Chloroform ug/kg 11501250 92 70-130
Chloromethane ug/kg 10701250 86 55-130
cis-1,2-Dichloroethene ug/kg 11001250 88 70-130
cis-1,3-Dichloropropene ug/kg 11701250 93 70-130
Dibromochloromethane ug/kg 11901250 95 70-130
Dibromomethane ug/kg 12601250 101 70-130
Dichlorodifluoromethane ug/kg 14201250 114 45-156
Diisopropyl ether ug/kg 10101250 80 70-130
Ethylbenzene ug/kg 11001250 88 70-130
Hexachloro-1,3-butadiene ug/kg 12301250 98 66-130
Isopropylbenzene (Cumene)ug/kg 11601250 93 70-130
m&p-Xylene ug/kg 23002500 92 70-130
Methyl-tert-butyl ether ug/kg 10301250 83 70-130
Methylene Chloride ug/kg 10601250 85 65-130
n-Butylbenzene ug/kg 11301250 90 67-130
n-Propylbenzene ug/kg 11501250 92 70-130
Naphthalene ug/kg 11801250 94 70-130
o-Xylene ug/kg 11701250 94 70-130
p-Isopropyltoluene ug/kg 11501250 92 67-130
sec-Butylbenzene ug/kg 11301250 90 69-130
Styrene ug/kg 11901250 95 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3388060LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 11101250 89 67-130
Tetrachloroethene ug/kg 12401250 99 70-130
Toluene ug/kg 11601250 93 70-130
trans-1,2-Dichloroethene ug/kg 11401250 91 70-130
trans-1,3-Dichloropropene ug/kg 11501250 92 68-130
Trichloroethene ug/kg 12301250 99 70-130
Trichlorofluoromethane ug/kg 11701250 94 70-130
Vinyl acetate ug/kg 23002500 92 70-130
Vinyl chloride ug/kg 11201250 90 61-130
Xylene (Total)ug/kg 34703750 93 70-130
1,2-Dichloroethane-d4 (S)%90 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3389514MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92559777004
3389515
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 31400 114 70-131119 431400ND35900 37300
1,1,1-Trichloroethane ug/kg v3314009865-13392 731400ND30900 28800
1,1,2,2-Tetrachloroethane ug/kg M13140018866-130211 1131400ND59100 66300
1,1,2-Trichloroethane ug/kg 31400 98 66-13398 131400ND30800 30600
1,1-Dichloroethane ug/kg 31400 104 65-130100 431400ND32600 31400
1,1-Dichloroethene ug/kg 31400 111 10-158106 531400ND34900 33400
1,1-Dichloropropene ug/kg 31400 111 68-133106 531400ND35000 33200
1,2,3-Trichlorobenzene ug/kg 31400 113 27-138126 1031400ND35600 39500
1,2,3-Trichloropropane ug/kg 31400 102 67-130110 731400ND32000 34500
1,2,4-Trichlorobenzene ug/kg 31400 114 51-134125 931400ND35700 39200
1,2,4-Trimethylbenzene ug/kg 31400 98 63-136135 15314004350074200 86100
1,2-Dibromo-3-chloropropane ug/kg 31400 106 32-130116 931400ND33200 36500
1,2-Dibromoethane (EDB)ug/kg 31400 108 70-130115 631400ND34000 36200
1,2-Dichlorobenzene ug/kg 31400 109 69-130120 1031400ND34300 37800
1,2-Dichloroethane ug/kg 31400 102 59-13098 431400ND32000 30800
1,2-Dichloropropane ug/kg 31400 109 70-130103 631400ND34300 32400
1,3,5-Trimethylbenzene ug/kg 31400 105 65-137124 11314001850051500 57600
1,3-Dichlorobenzene ug/kg 31400 110 70-130122 1131400ND34400 38400
1,3-Dichloropropane ug/kg 31400 109 70-130116 731400ND34200 36600
1,4-Dichlorobenzene ug/kg 31400 110 68-130121 931400ND34600 37900
2,2-Dichloropropane ug/kg 31400 109 32-130102 631400ND34100 32000
2-Butanone (MEK)ug/kg 62800 95 10-13690 662800ND59900 56300
2-Chlorotoluene ug/kg 31400 116 69-141133 1331400ND36400 41700
2-Hexanone ug/kg 62800 98 10-144104 662800ND61400 65500
4-Chlorotoluene ug/kg 31400 109 70-132121 1031400ND34200 37900
4-Methyl-2-pentanone (MIBK) ug/kg 62800 96 25-14393 262800548065500 64100
Acetone ug/kg 62800 88 10-13082 662800ND55100 51700
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3389514MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92559777004
3389515
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
Benzene ug/kg 31400 108 67-130105 331400ND34000 33100
Bromobenzene ug/kg 31400 112 70-130125 1031400ND35300 39100
Bromochloromethane ug/kg 31400 110 69-134105 531400ND34600 32900
Bromodichloromethane ug/kg 31400 91 64-13089 231400ND28500 28000
Bromoform ug/kg 31400 101 62-130109 731400ND31800 34200
Bromomethane ug/kg 31400 89 20-17691 231400ND27900 28500
Carbon tetrachloride ug/kg 31400 109 65-140108 231400ND34400 33900
Chlorobenzene ug/kg 31400 114 70-130124 831400ND35900 39000
Chloroethane ug/kg 31400 102 10-13099 231400ND31900 31200
Chloroform ug/kg 31400 109 63-130101 731400ND34200 31900
Chloromethane ug/kg 31400 97 58-13093 531400ND30600 29100
cis-1,2-Dichloroethene ug/kg 31400 102 66-13096 631400ND31900 30100
cis-1,3-Dichloropropene ug/kg 31400 110 67-130105 531400ND34600 32800
Dibromochloromethane ug/kg 31400 108 67-130117 831400ND34000 36700
Dibromomethane ug/kg 31400 117 63-131113 431400ND36800 35400
Dichlorodifluoromethane ug/kg 31400 138 44-180133 431400ND43400 41700
Diisopropyl ether ug/kg 31400 91 63-13086 631400ND28600 27000
Ethylbenzene ug/kg 31400 106 66-130113 73140053533700 36000
Hexachloro-1,3-butadiene ug/kg M13140018164-150198 931400ND56800 62300
Isopropylbenzene (Cumene) ug/kg 31400 118 69-135129 931400ND37000 40600
m&p-Xylene ug/kg 62800 109 60-133120 962800301071700 78200
Methyl-tert-butyl ether ug/kg 31400 92 65-13087 631400ND29000 27300
Methylene Chloride ug/kg 31400 92 61-13087 631400ND29000 27300
n-Butylbenzene ug/kg M13140012665-140145 1231400756047100 53100
n-Propylbenzene ug/kg 31400 120 67-140133 1031400ND37600 41700
Naphthalene ug/kg 31400 107 15-145117 931400127034900 38100
o-Xylene ug/kg 31400 117 66-133124 631400ND36600 39000
p-Isopropyltoluene ug/kg 31400 115 56-147135 11314001560051700 58000
sec-Butylbenzene ug/kg 31400 109 65-139125 11314001110045300 50400
Styrene ug/kg 31400 113 70-132118 431400ND35600 37000
tert-Butylbenzene ug/kg 31400 115 62-135128 1131400ND36000 40300
Tetrachloroethene ug/kg 31400 115 70-135128 1031400ND36200 40200
Toluene ug/kg 31400 113 67-130110 331400ND35500 34600
trans-1,2-Dichloroethene ug/kg 31400 105 69-130100 531400ND33000 31300
trans-1,3-Dichloropropene ug/kg 31400 106 62-130102 431400ND33400 32100
Trichloroethene ug/kg 31400 122 70-135117 431400ND38300 36600
Trichlorofluoromethane ug/kg 31400 113 10-130109 431400ND35500 34100
Vinyl acetate ug/kg 62800 98 53-13093 662800ND61800 58300
Vinyl chloride ug/kg 31400 104 61-148101 331400ND32500 31600
Xylene (Total)ug/kg 94200 112 63-132121 8942003010108000 117000
1,2-Dichloroethane-d4 (S)%92 70-13079
4-Bromofluorobenzene (S)%S013469-134138
Toluene-d8 (S)%99 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
646193
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92559777001, 92559777002, 92559777003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3389560
Associated Lab Samples:92559777001, 92559777002, 92559777003
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/09/21 13:06
1,1,1-Trichloroethane ug/kg ND 5.0 09/09/21 13:06
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/09/21 13:06
1,1,2-Trichloroethane ug/kg ND 5.0 09/09/21 13:06
1,1-Dichloroethane ug/kg ND 5.0 09/09/21 13:06
1,1-Dichloroethene ug/kg ND 5.0 09/09/21 13:06
1,1-Dichloropropene ug/kg ND 5.0 09/09/21 13:06
1,2,3-Trichlorobenzene ug/kg ND 5.0 09/09/21 13:06
1,2,3-Trichloropropane ug/kg ND 5.0 09/09/21 13:06
1,2,4-Trichlorobenzene ug/kg ND 5.0 09/09/21 13:06
1,2,4-Trimethylbenzene ug/kg ND 5.0 09/09/21 13:06
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/09/21 13:06
1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/09/21 13:06
1,2-Dichlorobenzene ug/kg ND 5.0 09/09/21 13:06
1,2-Dichloroethane ug/kg ND 5.0 09/09/21 13:06
1,2-Dichloropropane ug/kg ND 5.0 09/09/21 13:06
1,3,5-Trimethylbenzene ug/kg ND 5.0 09/09/21 13:06
1,3-Dichlorobenzene ug/kg ND 5.0 09/09/21 13:06
1,3-Dichloropropane ug/kg ND 5.0 09/09/21 13:06
1,4-Dichlorobenzene ug/kg ND 5.0 09/09/21 13:06
2,2-Dichloropropane ug/kg ND 5.0 09/09/21 13:06
2-Butanone (MEK)ug/kg ND 100 v209/09/21 13:06
2-Chlorotoluene ug/kg ND 5.0 09/09/21 13:06
2-Hexanone ug/kg ND 50.0 v209/09/21 13:06
4-Chlorotoluene ug/kg ND 5.0 09/09/21 13:06
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 v209/09/21 13:06
Acetone ug/kg ND 100 v209/09/21 13:06
Benzene ug/kg ND 5.0 09/09/21 13:06
Bromobenzene ug/kg ND 5.0 09/09/21 13:06
Bromochloromethane ug/kg ND 5.0 09/09/21 13:06
Bromodichloromethane ug/kg ND 5.0 09/09/21 13:06
Bromoform ug/kg ND 5.0 09/09/21 13:06
Bromomethane ug/kg ND 10.0 09/09/21 13:06
Carbon tetrachloride ug/kg ND 5.0 09/09/21 13:06
Chlorobenzene ug/kg ND 5.0 09/09/21 13:06
Chloroethane ug/kg ND 10.0 09/09/21 13:06
Chloroform ug/kg ND 5.0 09/09/21 13:06
Chloromethane ug/kg ND 10.0 09/09/21 13:06
cis-1,2-Dichloroethene ug/kg ND 5.0 09/09/21 13:06
cis-1,3-Dichloropropene ug/kg ND 5.0 09/09/21 13:06
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3389560
Associated Lab Samples:92559777001, 92559777002, 92559777003
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 09/09/21 13:06
Dibromomethane ug/kg ND 5.0 09/09/21 13:06
Dichlorodifluoromethane ug/kg ND 10.0 09/09/21 13:06
Diisopropyl ether ug/kg ND 5.0 09/09/21 13:06
Ethylbenzene ug/kg ND 5.0 09/09/21 13:06
Hexachloro-1,3-butadiene ug/kg ND 10.0 09/09/21 13:06
Isopropylbenzene (Cumene)ug/kg ND 5.0 09/09/21 13:06
m&p-Xylene ug/kg ND 10.0 09/09/21 13:06
Methyl-tert-butyl ether ug/kg ND 5.0 09/09/21 13:06
Methylene Chloride ug/kg ND 20.0 09/09/21 13:06
n-Butylbenzene ug/kg ND 5.0 09/09/21 13:06
n-Propylbenzene ug/kg ND 5.0 09/09/21 13:06
Naphthalene ug/kg ND 5.0 09/09/21 13:06
o-Xylene ug/kg ND 5.0 09/09/21 13:06
p-Isopropyltoluene ug/kg ND 5.0 09/09/21 13:06
sec-Butylbenzene ug/kg ND 5.0 09/09/21 13:06
Styrene ug/kg ND 5.0 09/09/21 13:06
tert-Butylbenzene ug/kg ND 5.0 09/09/21 13:06
Tetrachloroethene ug/kg ND 5.0 09/09/21 13:06
Toluene ug/kg ND 5.0 09/09/21 13:06
trans-1,2-Dichloroethene ug/kg ND 5.0 09/09/21 13:06
trans-1,3-Dichloropropene ug/kg ND 5.0 09/09/21 13:06
Trichloroethene ug/kg ND 5.0 09/09/21 13:06
Trichlorofluoromethane ug/kg ND 5.0 09/09/21 13:06
Vinyl acetate ug/kg ND 50.0 09/09/21 13:06
Vinyl chloride ug/kg ND 10.0 09/09/21 13:06
Xylene (Total)ug/kg ND 10.0 09/09/21 13:06
1,2-Dichloroethane-d4 (S)%99 70-130 09/09/21 13:06
4-Bromofluorobenzene (S)%102 69-134 09/09/21 13:06
Toluene-d8 (S)%100 70-130 09/09/21 13:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3389561LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 12601250 100 70-130
1,1,1-Trichloroethane ug/kg 12501250 100 70-130
1,1,2,2-Tetrachloroethane ug/kg 11701250 93 70-130
1,1,2-Trichloroethane ug/kg 11501250 92 70-130
1,1-Dichloroethane ug/kg 12401250 99 70-130
1,1-Dichloroethene ug/kg 12601250 101 70-130
1,1-Dichloropropene ug/kg 12601250 101 70-130
1,2,3-Trichlorobenzene ug/kg 12301250 98 65-130
1,2,3-Trichloropropane ug/kg 11101250 89 70-130
1,2,4-Trichlorobenzene ug/kg 12501250 100 68-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3389561LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 12401250 99 70-130
1,2-Dibromo-3-chloropropane ug/kg 10901250 87 70-130
1,2-Dibromoethane (EDB)ug/kg 12101250 97 70-130
1,2-Dichlorobenzene ug/kg 12701250 101 70-130
1,2-Dichloroethane ug/kg 11501250 92 63-130
1,2-Dichloropropane ug/kg 12001250 96 70-130
1,3,5-Trimethylbenzene ug/kg 12101250 97 70-130
1,3-Dichlorobenzene ug/kg 12401250 99 70-130
1,3-Dichloropropane ug/kg 11901250 95 70-130
1,4-Dichlorobenzene ug/kg 12901250 103 70-130
2,2-Dichloropropane ug/kg 12301250 99 66-130
2-Butanone (MEK)ug/kg 1920 v3250077 70-130
2-Chlorotoluene ug/kg 13001250 104 70-130
2-Hexanone ug/kg 2010 v3250080 70-130
4-Chlorotoluene ug/kg 12801250 102 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 2050 v3250082 70-130
Acetone ug/kg 1960 v3250078 69-130
Benzene ug/kg 12301250 98 70-130
Bromobenzene ug/kg 12901250 104 70-130
Bromochloromethane ug/kg 12501250 100 70-130
Bromodichloromethane ug/kg 11901250 95 69-130
Bromoform ug/kg 12401250 99 70-130
Bromomethane ug/kg 15601250 125 52-130
Carbon tetrachloride ug/kg 13001250 104 70-130
Chlorobenzene ug/kg 13001250 104 70-130
Chloroethane ug/kg 12401250 99 65-130
Chloroform ug/kg 12401250 99 70-130
Chloromethane ug/kg 11501250 92 55-130
cis-1,2-Dichloroethene ug/kg 12101250 97 70-130
cis-1,3-Dichloropropene ug/kg 12401250 99 70-130
Dibromochloromethane ug/kg 13501250 108 70-130
Dibromomethane ug/kg 12601250 101 70-130
Dichlorodifluoromethane ug/kg 16001250 128 45-156
Diisopropyl ether ug/kg 10801250 86 70-130
Ethylbenzene ug/kg 12301250 99 70-130
Hexachloro-1,3-butadiene ug/kg 12701250 101 66-130
Isopropylbenzene (Cumene)ug/kg 13201250 105 70-130
m&p-Xylene ug/kg 25702500 103 70-130
Methyl-tert-butyl ether ug/kg 11201250 89 70-130
Methylene Chloride ug/kg 11001250 88 65-130
n-Butylbenzene ug/kg 13001250 104 67-130
n-Propylbenzene ug/kg 12801250 102 70-130
Naphthalene ug/kg 11901250 96 70-130
o-Xylene ug/kg 12501250 100 70-130
p-Isopropyltoluene ug/kg 12601250 101 67-130
sec-Butylbenzene ug/kg 12801250 102 69-130
Styrene ug/kg 13101250 105 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3389561LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 12701250 102 67-130
Tetrachloroethene ug/kg 12801250 102 70-130
Toluene ug/kg 12801250 103 70-130
trans-1,2-Dichloroethene ug/kg 11901250 95 70-130
trans-1,3-Dichloropropene ug/kg 12001250 96 68-130
Trichloroethene ug/kg 12401250 100 70-130
Trichlorofluoromethane ug/kg 12501250 100 70-130
Vinyl acetate ug/kg 24802500 99 70-130
Vinyl chloride ug/kg 13301250 106 61-130
Xylene (Total)ug/kg 38203750 102 70-130
1,2-Dichloroethane-d4 (S)%85 70-130
4-Bromofluorobenzene (S)%102 69-134
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3389562MATRIX SPIKE SAMPLE:
MSSpike
Result
92559777002
1,1,1,2-Tetrachloroethane ug/kg 807802 101 70-131ND
1,1,1-Trichloroethane ug/kg 696 v380287 65-133ND
1,1,2,2-Tetrachloroethane ug/kg 725802 90 66-130ND
1,1,2-Trichloroethane ug/kg 675802 84 66-133ND
1,1-Dichloroethane ug/kg 744802 93 65-130ND
1,1-Dichloroethene ug/kg 799802 100 10-158ND
1,1-Dichloropropene ug/kg 812802 101 68-133ND
1,2,3-Trichlorobenzene ug/kg 890802 111 27-138ND
1,2,3-Trichloropropane ug/kg 735802 92 67-130ND
1,2,4-Trichlorobenzene ug/kg 899802 112 51-134ND
1,2,4-Trimethylbenzene ug/kg 814802 101 63-136ND
1,2-Dibromo-3-chloropropane ug/kg 696802 87 32-130ND
1,2-Dibromoethane (EDB)ug/kg 777802 97 70-130ND
1,2-Dichlorobenzene ug/kg 854802 106 69-130ND
1,2-Dichloroethane ug/kg 735802 92 59-130ND
1,2-Dichloropropane ug/kg 791802 99 70-130ND
1,3,5-Trimethylbenzene ug/kg 821802 102 65-137ND
1,3-Dichlorobenzene ug/kg 848802 106 70-130ND
1,3-Dichloropropane ug/kg 806802 100 70-130ND
1,4-Dichlorobenzene ug/kg 867802 108 68-130ND
2,2-Dichloropropane ug/kg 671802 84 32-130ND
2-Butanone (MEK)ug/kg 11701600 73 10-136ND
2-Chlorotoluene ug/kg 860802 107 69-141ND
2-Hexanone ug/kg 12501600 78 10-144ND
4-Chlorotoluene ug/kg 833802 104 70-132ND
4-Methyl-2-pentanone (MIBK)ug/kg 12901600 80 25-143ND
Acetone ug/kg 8421600 52 10-130ND
Benzene ug/kg 803802 100 67-130ND
REPORT OF LABORATORY ANALYSIS
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Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3389562MATRIX SPIKE SAMPLE:
MSSpike
Result
92559777002
Bromobenzene ug/kg 843802 105 70-130ND
Bromochloromethane ug/kg 745802 93 69-134ND
Bromodichloromethane ug/kg 635802 79 64-130ND
Bromoform ug/kg 667802 83 62-130ND
Bromomethane ug/kg 224802 28 20-176ND
Carbon tetrachloride ug/kg 796802 99 65-140ND
Chlorobenzene ug/kg 867802 108 70-130ND
Chloroethane ug/kg 85.7802 11 10-130ND
Chloroform ug/kg 760802 95 63-130ND
Chloromethane ug/kg 744802 93 58-130ND
cis-1,2-Dichloroethene ug/kg 738802 92 66-130ND
cis-1,3-Dichloropropene ug/kg 742802 92 67-130ND
Dibromochloromethane ug/kg 727802 91 67-130ND
Dibromomethane ug/kg 809802 101 63-131ND
Dichlorodifluoromethane ug/kg 971802 121 44-180ND
Diisopropyl ether ug/kg 665802 83 63-130ND
Ethylbenzene ug/kg 816802 102 66-130ND
Hexachloro-1,3-butadiene ug/kg 963802 120 64-150ND
Isopropylbenzene (Cumene)ug/kg 885802 110 69-135ND
m&p-Xylene ug/kg 17101600 106 60-133ND
Methyl-tert-butyl ether ug/kg 683802 85 65-130ND
Methylene Chloride ug/kg 697802 87 61-130ND
n-Butylbenzene ug/kg 854802 106 65-140ND
n-Propylbenzene ug/kg 843802 105 67-140ND
Naphthalene ug/kg 823802 103 15-145ND
o-Xylene ug/kg 852802 106 66-133ND
p-Isopropyltoluene ug/kg 875802 109 56-147ND
sec-Butylbenzene ug/kg 860802 107 65-139ND
Styrene ug/kg 822802 102 70-132ND
tert-Butylbenzene ug/kg 829802 103 62-135ND
Tetrachloroethene ug/kg 902802 112 70-135ND
Toluene ug/kg 829802 103 67-130ND
trans-1,2-Dichloroethene ug/kg 765802 95 69-130ND
trans-1,3-Dichloropropene ug/kg 722802 90 62-130ND
Trichloroethene ug/kg 879802 109 70-135ND
Trichlorofluoromethane ug/kg 84.1802 10 10-130ND
Vinyl acetate ug/kg 13701600 86 53-130ND
Vinyl chloride ug/kg 759802 95 61-148ND
Xylene (Total)ug/kg 25602400 106 63-132ND
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%99 69-134
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92559777003
3389563SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg ND v2ND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg ND v2ND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg ND v2ND
Acetone ug/kg ND v2ND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg NDND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
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Page 23 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92559777003
3389563SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg 12.6 C7,D64720.4
Methylene Chloride ug/kg NDND
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%9595
4-Bromofluorobenzene (S)%9796
Toluene-d8 (S)%100102
REPORT OF LABORATORY ANALYSIS
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Page 24 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
645788
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92559777001, 92559777002, 92559777003, 92559777004
Parameter Units
Dup
Result QualifiersRPDResult
92559716001
3387351SAMPLE DUPLICATE:
Percent Moisture %8.6 N287.9
Parameter Units
Dup
Result QualifiersRPDResult
92559831002
3387352SAMPLE DUPLICATE:
Percent Moisture %15.6 N2015.5
REPORT OF LABORATORY ANALYSIS
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Page 25 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte is a possible laboratory contaminant (not present in method blank).C7
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Page 26 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92559777
GILBARCO/11.990009.00
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92559777001 646193 646208SS-7 @ 6'2 EPA 5035A/5030B EPA 8260D
92559777002 646193 646208SS-9 @ 6'1 EPA 5035A/5030B EPA 8260D
92559777003 646193 646208SS-10 @ 6'EPA 5035A/5030B EPA 8260D
92559777004 645905 645937SS-11 @ 6'1 EPA 5035A/5030B EPA 8260D
92559777001 645788SS-7 @ 6'2 SW-846
92559777002 645788SS-9 @ 6'1 SW-846
92559777003 645788SS-10 @ 6'SW-846
92559777004 645788SS-11 @ 6'1 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/13/2021 10:42 AM
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Page 27 of 28
Page 28 of 28
#=CL#
January 27, 2023
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92648387
92648387
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
GILBARCO
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on January 24, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sara Poulson
[e-mail]
Project Manager
[phone]
Enclosures
cc:Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92648387
GILBARCO
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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Page 2 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92648387
GILBARCO
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92648387001 SS-12@3'EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92648387002 SS-13@5'EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92648387003 SS-14@40'EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92648387004 SS-15@59'EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92648387005 SS-16@30'EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
92648387006 SS-18@5'EPA 8260D 70 PASI-CSAS
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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Page 3 of 28
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92648387
GILBARCO
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92648387001 SS-12@3'
Chloroform 624 ug/kg 01/25/23 06:01 B292EPA 8260D
Methylene Chloride 3150 ug/kg 01/25/23 06:011170EPA 8260D
Naphthalene 788 ug/kg 01/25/23 06:01292EPA 8260D
Toluene 18300 ug/kg 01/25/23 06:01292EPA 8260D
Percent Moisture 2.4 %01/24/23 15:32 N20.10SW-846
92648387002 SS-13@5'
Acetone 12300 ug/kg 01/25/23 06:197170EPA 8260D
Chloroform 688 ug/kg 01/25/23 06:19 B358EPA 8260D
Methylene Chloride 1590 ug/kg 01/25/23 06:191430EPA 8260D
Naphthalene 494 ug/kg 01/25/23 06:19358EPA 8260D
Toluene 10900 ug/kg 01/25/23 06:19358EPA 8260D
Percent Moisture 5.0 %01/24/23 15:32 N20.10SW-846
92648387003 SS-14@40'
Chloroform 593 ug/kg 01/25/23 06:54 B337EPA 8260D
Methylene Chloride 2830 ug/kg 01/25/23 06:541350EPA 8260D
Toluene 14800 ug/kg 01/25/23 06:54337EPA 8260D
Percent Moisture 5.8 %01/24/23 15:32 N20.10SW-846
92648387004 SS-15@59'
Methylene Chloride 94.6 ug/kg 01/25/23 02:1239.6EPA 8260D
Toluene 422 ug/kg 01/25/23 02:129.9EPA 8260D
Percent Moisture 30.5 %01/24/23 15:32 N20.10SW-846
92648387005 SS-16@30'
Methylene Chloride 53.3 ug/kg 01/25/23 02:3020.7EPA 8260D
Toluene 197 ug/kg 01/25/23 02:305.2EPA 8260D
Percent Moisture 4.2 %01/24/23 15:32 N20.10SW-846
92648387006 SS-18@5'
Chloroform 684 ug/kg 01/25/23 06:36 B368EPA 8260D
Methylene Chloride 2490 ug/kg 01/25/23 06:361470EPA 8260D
Toluene 13500 ug/kg 01/25/23 06:36368EPA 8260D
Percent Moisture 22.5 %01/24/23 15:32 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
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Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-12@3'Lab ID: 92648387001 Collected: 01/23/23 13:50 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 01/25/23 06:01 67-64-101/24/23 16:475850 50
Benzene ND ug/kg 01/25/23 06:01 71-43-201/24/23 16:47292 50
Bromobenzene ND ug/kg 01/25/23 06:01 108-86-101/24/23 16:47292 50
Bromochloromethane ND ug/kg 01/25/23 06:01 74-97-501/24/23 16:47292 50
Bromodichloromethane ND ug/kg 01/25/23 06:01 75-27-4 v101/24/23 16:47292 50
Bromoform ND ug/kg 01/25/23 06:01 75-25-2 v101/24/23 16:47292 50
Bromomethane ND ug/kg 01/25/23 06:01 74-83-901/24/23 16:47585 50
2-Butanone (MEK)ND ug/kg 01/25/23 06:01 78-93-301/24/23 16:475850 50
n-Butylbenzene ND ug/kg 01/25/23 06:01 104-51-801/24/23 16:47292 50
sec-Butylbenzene ND ug/kg 01/25/23 06:01 135-98-801/24/23 16:47292 50
tert-Butylbenzene ND ug/kg 01/25/23 06:01 98-06-601/24/23 16:47292 50
Carbon tetrachloride ND ug/kg 01/25/23 06:01 56-23-501/24/23 16:47292 50
Chlorobenzene ND ug/kg 01/25/23 06:01 108-90-701/24/23 16:47292 50
Chloroethane ND ug/kg 01/25/23 06:01 75-00-301/24/23 16:47585 50
Chloroform 624 ug/kg 01/25/23 06:01 67-66-3 B01/24/23 16:47292 50
Chloromethane ND ug/kg 01/25/23 06:01 74-87-301/24/23 16:47585 50
2-Chlorotoluene ND ug/kg 01/25/23 06:01 95-49-801/24/23 16:47292 50
4-Chlorotoluene ND ug/kg 01/25/23 06:01 106-43-4 v101/24/23 16:47292 50
1,2-Dibromo-3-chloropropane ND ug/kg 01/25/23 06:01 96-12-8 IK01/24/23 16:47292 50
Dibromochloromethane ND ug/kg 01/25/23 06:01 124-48-1 v101/24/23 16:47292 50
1,2-Dibromoethane (EDB)ND ug/kg 01/25/23 06:01 106-93-401/24/23 16:47292 50
Dibromomethane ND ug/kg 01/25/23 06:01 74-95-301/24/23 16:47292 50
1,2-Dichlorobenzene ND ug/kg 01/25/23 06:01 95-50-101/24/23 16:47292 50
1,3-Dichlorobenzene ND ug/kg 01/25/23 06:01 541-73-101/24/23 16:47292 50
1,4-Dichlorobenzene ND ug/kg 01/25/23 06:01 106-46-701/24/23 16:47292 50
Dichlorodifluoromethane ND ug/kg 01/25/23 06:01 75-71-8 IH01/24/23 16:47585 50
1,1-Dichloroethane ND ug/kg 01/25/23 06:01 75-34-301/24/23 16:47292 50
1,2-Dichloroethane ND ug/kg 01/25/23 06:01 107-06-201/24/23 16:47292 50
1,1-Dichloroethene ND ug/kg 01/25/23 06:01 75-35-401/24/23 16:47292 50
cis-1,2-Dichloroethene ND ug/kg 01/25/23 06:01 156-59-201/24/23 16:47292 50
trans-1,2-Dichloroethene ND ug/kg 01/25/23 06:01 156-60-501/24/23 16:47292 50
1,2-Dichloropropane ND ug/kg 01/25/23 06:01 78-87-501/24/23 16:47292 50
1,3-Dichloropropane ND ug/kg 01/25/23 06:01 142-28-901/24/23 16:47292 50
2,2-Dichloropropane ND ug/kg 01/25/23 06:01 594-20-701/24/23 16:47292 50
1,1-Dichloropropene ND ug/kg 01/25/23 06:01 563-58-601/24/23 16:47292 50
cis-1,3-Dichloropropene ND ug/kg 01/25/23 06:01 10061-01-501/24/23 16:47292 50
trans-1,3-Dichloropropene ND ug/kg 01/25/23 06:01 10061-02-601/24/23 16:47292 50
Diisopropyl ether ND ug/kg 01/25/23 06:01 108-20-301/24/23 16:47292 50
Ethylbenzene ND ug/kg 01/25/23 06:01 100-41-401/24/23 16:47292 50
Hexachloro-1,3-butadiene ND ug/kg 01/25/23 06:01 87-68-301/24/23 16:47585 50
2-Hexanone ND ug/kg 01/25/23 06:01 591-78-6 IK01/24/23 16:472920 50
Isopropylbenzene (Cumene)ND ug/kg 01/25/23 06:01 98-82-801/24/23 16:47292 50
p-Isopropyltoluene ND ug/kg 01/25/23 06:01 99-87-601/24/23 16:47292 50
Methylene Chloride 3150 ug/kg 01/25/23 06:01 75-09-201/24/23 16:471170 50
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/25/23 06:01 108-10-101/24/23 16:472920 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-12@3'Lab ID: 92648387001 Collected: 01/23/23 13:50 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 01/25/23 06:01 1634-04-401/24/23 16:47292 50
Naphthalene 788 ug/kg 01/25/23 06:01 91-20-301/24/23 16:47292 50
n-Propylbenzene ND ug/kg 01/25/23 06:01 103-65-101/24/23 16:47292 50
Styrene ND ug/kg 01/25/23 06:01 100-42-501/24/23 16:47292 50
1,1,1,2-Tetrachloroethane ND ug/kg 01/25/23 06:01 630-20-601/24/23 16:47292 50
1,1,2,2-Tetrachloroethane ND ug/kg 01/25/23 06:01 79-34-501/24/23 16:47292 50
Tetrachloroethene ND ug/kg 01/25/23 06:01 127-18-401/24/23 16:47292 50
Toluene 18300 ug/kg 01/25/23 06:01 108-88-301/24/23 16:47292 50
1,2,3-Trichlorobenzene ND ug/kg 01/25/23 06:01 87-61-601/24/23 16:47292 50
1,2,4-Trichlorobenzene ND ug/kg 01/25/23 06:01 120-82-101/24/23 16:47292 50
1,1,1-Trichloroethane ND ug/kg 01/25/23 06:01 71-55-601/24/23 16:47292 50
1,1,2-Trichloroethane ND ug/kg 01/25/23 06:01 79-00-501/24/23 16:47292 50
Trichloroethene ND ug/kg 01/25/23 06:01 79-01-601/24/23 16:47292 50
Trichlorofluoromethane ND ug/kg 01/25/23 06:01 75-69-401/24/23 16:47292 50
1,2,3-Trichloropropane ND ug/kg 01/25/23 06:01 96-18-401/24/23 16:47292 50
1,2,4-Trimethylbenzene ND ug/kg 01/25/23 06:01 95-63-601/24/23 16:47292 50
1,3,5-Trimethylbenzene ND ug/kg 01/25/23 06:01 108-67-8 v101/24/23 16:47292 50
Vinyl acetate ND ug/kg 01/25/23 06:01 108-05-401/24/23 16:472920 50
Vinyl chloride ND ug/kg 01/25/23 06:01 75-01-401/24/23 16:47585 50
Xylene (Total)ND ug/kg 01/25/23 06:01 1330-20-701/24/23 16:47585 50
m&p-Xylene ND ug/kg 01/25/23 06:01 179601-23-101/24/23 16:47585 50
o-Xylene ND ug/kg 01/25/23 06:01 95-47-601/24/23 16:47292 50
Surrogates
Toluene-d8 (S)104 %01/25/23 06:01 2037-26-5 D301/24/23 16:4770-130 50
4-Bromofluorobenzene (S)108 %01/25/23 06:01 460-00-401/24/23 16:4770-130 50
1,2-Dichloroethane-d4 (S)110 %01/25/23 06:01 17060-07-001/24/23 16:4770-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 2.4 %01/24/23 15:32 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-13@5'Lab ID: 92648387002 Collected: 01/23/23 14:10 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 12300 ug/kg 01/25/23 06:19 67-64-101/24/23 16:477170 50
Benzene ND ug/kg 01/25/23 06:19 71-43-201/24/23 16:47358 50
Bromobenzene ND ug/kg 01/25/23 06:19 108-86-101/24/23 16:47358 50
Bromochloromethane ND ug/kg 01/25/23 06:19 74-97-501/24/23 16:47358 50
Bromodichloromethane ND ug/kg 01/25/23 06:19 75-27-4 v101/24/23 16:47358 50
Bromoform ND ug/kg 01/25/23 06:19 75-25-2 v101/24/23 16:47358 50
Bromomethane ND ug/kg 01/25/23 06:19 74-83-901/24/23 16:47717 50
2-Butanone (MEK)ND ug/kg 01/25/23 06:19 78-93-301/24/23 16:477170 50
n-Butylbenzene ND ug/kg 01/25/23 06:19 104-51-801/24/23 16:47358 50
sec-Butylbenzene ND ug/kg 01/25/23 06:19 135-98-801/24/23 16:47358 50
tert-Butylbenzene ND ug/kg 01/25/23 06:19 98-06-601/24/23 16:47358 50
Carbon tetrachloride ND ug/kg 01/25/23 06:19 56-23-501/24/23 16:47358 50
Chlorobenzene ND ug/kg 01/25/23 06:19 108-90-701/24/23 16:47358 50
Chloroethane ND ug/kg 01/25/23 06:19 75-00-301/24/23 16:47717 50
Chloroform 688 ug/kg 01/25/23 06:19 67-66-3 B01/24/23 16:47358 50
Chloromethane ND ug/kg 01/25/23 06:19 74-87-301/24/23 16:47717 50
2-Chlorotoluene ND ug/kg 01/25/23 06:19 95-49-801/24/23 16:47358 50
4-Chlorotoluene ND ug/kg 01/25/23 06:19 106-43-4 v101/24/23 16:47358 50
1,2-Dibromo-3-chloropropane ND ug/kg 01/25/23 06:19 96-12-8 IK01/24/23 16:47358 50
Dibromochloromethane ND ug/kg 01/25/23 06:19 124-48-1 v101/24/23 16:47358 50
1,2-Dibromoethane (EDB)ND ug/kg 01/25/23 06:19 106-93-401/24/23 16:47358 50
Dibromomethane ND ug/kg 01/25/23 06:19 74-95-301/24/23 16:47358 50
1,2-Dichlorobenzene ND ug/kg 01/25/23 06:19 95-50-101/24/23 16:47358 50
1,3-Dichlorobenzene ND ug/kg 01/25/23 06:19 541-73-101/24/23 16:47358 50
1,4-Dichlorobenzene ND ug/kg 01/25/23 06:19 106-46-701/24/23 16:47358 50
Dichlorodifluoromethane ND ug/kg 01/25/23 06:19 75-71-8 IH01/24/23 16:47717 50
1,1-Dichloroethane ND ug/kg 01/25/23 06:19 75-34-301/24/23 16:47358 50
1,2-Dichloroethane ND ug/kg 01/25/23 06:19 107-06-201/24/23 16:47358 50
1,1-Dichloroethene ND ug/kg 01/25/23 06:19 75-35-401/24/23 16:47358 50
cis-1,2-Dichloroethene ND ug/kg 01/25/23 06:19 156-59-201/24/23 16:47358 50
trans-1,2-Dichloroethene ND ug/kg 01/25/23 06:19 156-60-501/24/23 16:47358 50
1,2-Dichloropropane ND ug/kg 01/25/23 06:19 78-87-501/24/23 16:47358 50
1,3-Dichloropropane ND ug/kg 01/25/23 06:19 142-28-901/24/23 16:47358 50
2,2-Dichloropropane ND ug/kg 01/25/23 06:19 594-20-701/24/23 16:47358 50
1,1-Dichloropropene ND ug/kg 01/25/23 06:19 563-58-601/24/23 16:47358 50
cis-1,3-Dichloropropene ND ug/kg 01/25/23 06:19 10061-01-501/24/23 16:47358 50
trans-1,3-Dichloropropene ND ug/kg 01/25/23 06:19 10061-02-601/24/23 16:47358 50
Diisopropyl ether ND ug/kg 01/25/23 06:19 108-20-301/24/23 16:47358 50
Ethylbenzene ND ug/kg 01/25/23 06:19 100-41-401/24/23 16:47358 50
Hexachloro-1,3-butadiene ND ug/kg 01/25/23 06:19 87-68-301/24/23 16:47717 50
2-Hexanone ND ug/kg 01/25/23 06:19 591-78-6 IK01/24/23 16:473580 50
Isopropylbenzene (Cumene)ND ug/kg 01/25/23 06:19 98-82-801/24/23 16:47358 50
p-Isopropyltoluene ND ug/kg 01/25/23 06:19 99-87-601/24/23 16:47358 50
Methylene Chloride 1590 ug/kg 01/25/23 06:19 75-09-201/24/23 16:471430 50
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/25/23 06:19 108-10-101/24/23 16:473580 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-13@5'Lab ID: 92648387002 Collected: 01/23/23 14:10 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 01/25/23 06:19 1634-04-401/24/23 16:47358 50
Naphthalene 494 ug/kg 01/25/23 06:19 91-20-301/24/23 16:47358 50
n-Propylbenzene ND ug/kg 01/25/23 06:19 103-65-101/24/23 16:47358 50
Styrene ND ug/kg 01/25/23 06:19 100-42-501/24/23 16:47358 50
1,1,1,2-Tetrachloroethane ND ug/kg 01/25/23 06:19 630-20-601/24/23 16:47358 50
1,1,2,2-Tetrachloroethane ND ug/kg 01/25/23 06:19 79-34-501/24/23 16:47358 50
Tetrachloroethene ND ug/kg 01/25/23 06:19 127-18-401/24/23 16:47358 50
Toluene 10900 ug/kg 01/25/23 06:19 108-88-301/24/23 16:47358 50
1,2,3-Trichlorobenzene ND ug/kg 01/25/23 06:19 87-61-601/24/23 16:47358 50
1,2,4-Trichlorobenzene ND ug/kg 01/25/23 06:19 120-82-101/24/23 16:47358 50
1,1,1-Trichloroethane ND ug/kg 01/25/23 06:19 71-55-601/24/23 16:47358 50
1,1,2-Trichloroethane ND ug/kg 01/25/23 06:19 79-00-501/24/23 16:47358 50
Trichloroethene ND ug/kg 01/25/23 06:19 79-01-601/24/23 16:47358 50
Trichlorofluoromethane ND ug/kg 01/25/23 06:19 75-69-401/24/23 16:47358 50
1,2,3-Trichloropropane ND ug/kg 01/25/23 06:19 96-18-401/24/23 16:47358 50
1,2,4-Trimethylbenzene ND ug/kg 01/25/23 06:19 95-63-601/24/23 16:47358 50
1,3,5-Trimethylbenzene ND ug/kg 01/25/23 06:19 108-67-8 v101/24/23 16:47358 50
Vinyl acetate ND ug/kg 01/25/23 06:19 108-05-401/24/23 16:473580 50
Vinyl chloride ND ug/kg 01/25/23 06:19 75-01-401/24/23 16:47717 50
Xylene (Total)ND ug/kg 01/25/23 06:19 1330-20-701/24/23 16:47717 50
m&p-Xylene ND ug/kg 01/25/23 06:19 179601-23-101/24/23 16:47717 50
o-Xylene ND ug/kg 01/25/23 06:19 95-47-601/24/23 16:47358 50
Surrogates
Toluene-d8 (S)103 %01/25/23 06:19 2037-26-5 D301/24/23 16:4770-130 50
4-Bromofluorobenzene (S)120 %01/25/23 06:19 460-00-401/24/23 16:4770-130 50
1,2-Dichloroethane-d4 (S)113 %01/25/23 06:19 17060-07-001/24/23 16:4770-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 5.0 %01/24/23 15:32 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-14@40'Lab ID: 92648387003 Collected: 01/23/23 14:19 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 01/25/23 06:54 67-64-101/24/23 16:476730 50
Benzene ND ug/kg 01/25/23 06:54 71-43-201/24/23 16:47337 50
Bromobenzene ND ug/kg 01/25/23 06:54 108-86-101/24/23 16:47337 50
Bromochloromethane ND ug/kg 01/25/23 06:54 74-97-501/24/23 16:47337 50
Bromodichloromethane ND ug/kg 01/25/23 06:54 75-27-4 v101/24/23 16:47337 50
Bromoform ND ug/kg 01/25/23 06:54 75-25-2 v101/24/23 16:47337 50
Bromomethane ND ug/kg 01/25/23 06:54 74-83-901/24/23 16:47673 50
2-Butanone (MEK)ND ug/kg 01/25/23 06:54 78-93-301/24/23 16:476730 50
n-Butylbenzene ND ug/kg 01/25/23 06:54 104-51-801/24/23 16:47337 50
sec-Butylbenzene ND ug/kg 01/25/23 06:54 135-98-801/24/23 16:47337 50
tert-Butylbenzene ND ug/kg 01/25/23 06:54 98-06-601/24/23 16:47337 50
Carbon tetrachloride ND ug/kg 01/25/23 06:54 56-23-501/24/23 16:47337 50
Chlorobenzene ND ug/kg 01/25/23 06:54 108-90-701/24/23 16:47337 50
Chloroethane ND ug/kg 01/25/23 06:54 75-00-301/24/23 16:47673 50
Chloroform 593 ug/kg 01/25/23 06:54 67-66-3 B01/24/23 16:47337 50
Chloromethane ND ug/kg 01/25/23 06:54 74-87-301/24/23 16:47673 50
2-Chlorotoluene ND ug/kg 01/25/23 06:54 95-49-801/24/23 16:47337 50
4-Chlorotoluene ND ug/kg 01/25/23 06:54 106-43-4 v101/24/23 16:47337 50
1,2-Dibromo-3-chloropropane ND ug/kg 01/25/23 06:54 96-12-8 IK01/24/23 16:47337 50
Dibromochloromethane ND ug/kg 01/25/23 06:54 124-48-1 v101/24/23 16:47337 50
1,2-Dibromoethane (EDB)ND ug/kg 01/25/23 06:54 106-93-401/24/23 16:47337 50
Dibromomethane ND ug/kg 01/25/23 06:54 74-95-301/24/23 16:47337 50
1,2-Dichlorobenzene ND ug/kg 01/25/23 06:54 95-50-101/24/23 16:47337 50
1,3-Dichlorobenzene ND ug/kg 01/25/23 06:54 541-73-101/24/23 16:47337 50
1,4-Dichlorobenzene ND ug/kg 01/25/23 06:54 106-46-701/24/23 16:47337 50
Dichlorodifluoromethane ND ug/kg 01/25/23 06:54 75-71-8 IH01/24/23 16:47673 50
1,1-Dichloroethane ND ug/kg 01/25/23 06:54 75-34-301/24/23 16:47337 50
1,2-Dichloroethane ND ug/kg 01/25/23 06:54 107-06-201/24/23 16:47337 50
1,1-Dichloroethene ND ug/kg 01/25/23 06:54 75-35-401/24/23 16:47337 50
cis-1,2-Dichloroethene ND ug/kg 01/25/23 06:54 156-59-201/24/23 16:47337 50
trans-1,2-Dichloroethene ND ug/kg 01/25/23 06:54 156-60-501/24/23 16:47337 50
1,2-Dichloropropane ND ug/kg 01/25/23 06:54 78-87-501/24/23 16:47337 50
1,3-Dichloropropane ND ug/kg 01/25/23 06:54 142-28-901/24/23 16:47337 50
2,2-Dichloropropane ND ug/kg 01/25/23 06:54 594-20-701/24/23 16:47337 50
1,1-Dichloropropene ND ug/kg 01/25/23 06:54 563-58-601/24/23 16:47337 50
cis-1,3-Dichloropropene ND ug/kg 01/25/23 06:54 10061-01-501/24/23 16:47337 50
trans-1,3-Dichloropropene ND ug/kg 01/25/23 06:54 10061-02-601/24/23 16:47337 50
Diisopropyl ether ND ug/kg 01/25/23 06:54 108-20-301/24/23 16:47337 50
Ethylbenzene ND ug/kg 01/25/23 06:54 100-41-401/24/23 16:47337 50
Hexachloro-1,3-butadiene ND ug/kg 01/25/23 06:54 87-68-301/24/23 16:47673 50
2-Hexanone ND ug/kg 01/25/23 06:54 591-78-6 IK01/24/23 16:473370 50
Isopropylbenzene (Cumene)ND ug/kg 01/25/23 06:54 98-82-801/24/23 16:47337 50
p-Isopropyltoluene ND ug/kg 01/25/23 06:54 99-87-601/24/23 16:47337 50
Methylene Chloride 2830 ug/kg 01/25/23 06:54 75-09-201/24/23 16:471350 50
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/25/23 06:54 108-10-101/24/23 16:473370 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-14@40'Lab ID: 92648387003 Collected: 01/23/23 14:19 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 01/25/23 06:54 1634-04-401/24/23 16:47337 50
Naphthalene ND ug/kg 01/25/23 06:54 91-20-301/24/23 16:47337 50
n-Propylbenzene ND ug/kg 01/25/23 06:54 103-65-101/24/23 16:47337 50
Styrene ND ug/kg 01/25/23 06:54 100-42-501/24/23 16:47337 50
1,1,1,2-Tetrachloroethane ND ug/kg 01/25/23 06:54 630-20-601/24/23 16:47337 50
1,1,2,2-Tetrachloroethane ND ug/kg 01/25/23 06:54 79-34-501/24/23 16:47337 50
Tetrachloroethene ND ug/kg 01/25/23 06:54 127-18-401/24/23 16:47337 50
Toluene 14800 ug/kg 01/25/23 06:54 108-88-301/24/23 16:47337 50
1,2,3-Trichlorobenzene ND ug/kg 01/25/23 06:54 87-61-601/24/23 16:47337 50
1,2,4-Trichlorobenzene ND ug/kg 01/25/23 06:54 120-82-101/24/23 16:47337 50
1,1,1-Trichloroethane ND ug/kg 01/25/23 06:54 71-55-601/24/23 16:47337 50
1,1,2-Trichloroethane ND ug/kg 01/25/23 06:54 79-00-501/24/23 16:47337 50
Trichloroethene ND ug/kg 01/25/23 06:54 79-01-601/24/23 16:47337 50
Trichlorofluoromethane ND ug/kg 01/25/23 06:54 75-69-401/24/23 16:47337 50
1,2,3-Trichloropropane ND ug/kg 01/25/23 06:54 96-18-401/24/23 16:47337 50
1,2,4-Trimethylbenzene ND ug/kg 01/25/23 06:54 95-63-601/24/23 16:47337 50
1,3,5-Trimethylbenzene ND ug/kg 01/25/23 06:54 108-67-8 v101/24/23 16:47337 50
Vinyl acetate ND ug/kg 01/25/23 06:54 108-05-401/24/23 16:473370 50
Vinyl chloride ND ug/kg 01/25/23 06:54 75-01-401/24/23 16:47673 50
Xylene (Total)ND ug/kg 01/25/23 06:54 1330-20-701/24/23 16:47673 50
m&p-Xylene ND ug/kg 01/25/23 06:54 179601-23-101/24/23 16:47673 50
o-Xylene ND ug/kg 01/25/23 06:54 95-47-601/24/23 16:47337 50
Surrogates
Toluene-d8 (S)102 %01/25/23 06:54 2037-26-5 D301/24/23 16:4770-130 50
4-Bromofluorobenzene (S)111 %01/25/23 06:54 460-00-401/24/23 16:4770-130 50
1,2-Dichloroethane-d4 (S)110 %01/25/23 06:54 17060-07-001/24/23 16:4770-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 5.8 %01/24/23 15:32 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-15@59'Lab ID: 92648387004 Collected: 01/23/23 14:58 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 01/25/23 02:12 67-64-101/24/23 16:47198 1
Benzene ND ug/kg 01/25/23 02:12 71-43-201/24/23 16:479.9 1
Bromobenzene ND ug/kg 01/25/23 02:12 108-86-101/24/23 16:479.9 1
Bromochloromethane ND ug/kg 01/25/23 02:12 74-97-501/24/23 16:479.9 1
Bromodichloromethane ND ug/kg 01/25/23 02:12 75-27-4 v101/24/23 16:479.9 1
Bromoform ND ug/kg 01/25/23 02:12 75-25-2 v101/24/23 16:479.9 1
Bromomethane ND ug/kg 01/25/23 02:12 74-83-901/24/23 16:4719.8 1
2-Butanone (MEK)ND ug/kg 01/25/23 02:12 78-93-301/24/23 16:47198 1
n-Butylbenzene ND ug/kg 01/25/23 02:12 104-51-801/24/23 16:479.9 1
sec-Butylbenzene ND ug/kg 01/25/23 02:12 135-98-801/24/23 16:479.9 1
tert-Butylbenzene ND ug/kg 01/25/23 02:12 98-06-601/24/23 16:479.9 1
Carbon tetrachloride ND ug/kg 01/25/23 02:12 56-23-501/24/23 16:479.9 1
Chlorobenzene ND ug/kg 01/25/23 02:12 108-90-701/24/23 16:479.9 1
Chloroethane ND ug/kg 01/25/23 02:12 75-00-301/24/23 16:4719.8 1
Chloroform ND ug/kg 01/25/23 02:12 67-66-301/24/23 16:479.9 1
Chloromethane ND ug/kg 01/25/23 02:12 74-87-301/24/23 16:4719.8 1
2-Chlorotoluene ND ug/kg 01/25/23 02:12 95-49-801/24/23 16:479.9 1
4-Chlorotoluene ND ug/kg 01/25/23 02:12 106-43-4 v101/24/23 16:479.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/25/23 02:12 96-12-8 IK01/24/23 16:479.9 1
Dibromochloromethane ND ug/kg 01/25/23 02:12 124-48-1 v101/24/23 16:479.9 1
1,2-Dibromoethane (EDB)ND ug/kg 01/25/23 02:12 106-93-401/24/23 16:479.9 1
Dibromomethane ND ug/kg 01/25/23 02:12 74-95-301/24/23 16:479.9 1
1,2-Dichlorobenzene ND ug/kg 01/25/23 02:12 95-50-101/24/23 16:479.9 1
1,3-Dichlorobenzene ND ug/kg 01/25/23 02:12 541-73-101/24/23 16:479.9 1
1,4-Dichlorobenzene ND ug/kg 01/25/23 02:12 106-46-701/24/23 16:479.9 1
Dichlorodifluoromethane ND ug/kg 01/25/23 02:12 75-71-8 IH01/24/23 16:4719.8 1
1,1-Dichloroethane ND ug/kg 01/25/23 02:12 75-34-301/24/23 16:479.9 1
1,2-Dichloroethane ND ug/kg 01/25/23 02:12 107-06-201/24/23 16:479.9 1
1,1-Dichloroethene ND ug/kg 01/25/23 02:12 75-35-401/24/23 16:479.9 1
cis-1,2-Dichloroethene ND ug/kg 01/25/23 02:12 156-59-201/24/23 16:479.9 1
trans-1,2-Dichloroethene ND ug/kg 01/25/23 02:12 156-60-501/24/23 16:479.9 1
1,2-Dichloropropane ND ug/kg 01/25/23 02:12 78-87-501/24/23 16:479.9 1
1,3-Dichloropropane ND ug/kg 01/25/23 02:12 142-28-901/24/23 16:479.9 1
2,2-Dichloropropane ND ug/kg 01/25/23 02:12 594-20-701/24/23 16:479.9 1
1,1-Dichloropropene ND ug/kg 01/25/23 02:12 563-58-601/24/23 16:479.9 1
cis-1,3-Dichloropropene ND ug/kg 01/25/23 02:12 10061-01-501/24/23 16:479.9 1
trans-1,3-Dichloropropene ND ug/kg 01/25/23 02:12 10061-02-601/24/23 16:479.9 1
Diisopropyl ether ND ug/kg 01/25/23 02:12 108-20-301/24/23 16:479.9 1
Ethylbenzene ND ug/kg 01/25/23 02:12 100-41-401/24/23 16:479.9 1
Hexachloro-1,3-butadiene ND ug/kg 01/25/23 02:12 87-68-301/24/23 16:4719.8 1
2-Hexanone ND ug/kg 01/25/23 02:12 591-78-6 IK01/24/23 16:4799.0 1
Isopropylbenzene (Cumene)ND ug/kg 01/25/23 02:12 98-82-801/24/23 16:479.9 1
p-Isopropyltoluene ND ug/kg 01/25/23 02:12 99-87-601/24/23 16:479.9 1
Methylene Chloride 94.6 ug/kg 01/25/23 02:12 75-09-201/24/23 16:4739.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/25/23 02:12 108-10-101/24/23 16:4799.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-15@59'Lab ID: 92648387004 Collected: 01/23/23 14:58 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 01/25/23 02:12 1634-04-401/24/23 16:479.9 1
Naphthalene ND ug/kg 01/25/23 02:12 91-20-301/24/23 16:479.9 1
n-Propylbenzene ND ug/kg 01/25/23 02:12 103-65-101/24/23 16:479.9 1
Styrene ND ug/kg 01/25/23 02:12 100-42-501/24/23 16:479.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/25/23 02:12 630-20-601/24/23 16:479.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/25/23 02:12 79-34-501/24/23 16:479.9 1
Tetrachloroethene ND ug/kg 01/25/23 02:12 127-18-401/24/23 16:479.9 1
Toluene 422 ug/kg 01/25/23 02:12 108-88-301/24/23 16:479.9 1
1,2,3-Trichlorobenzene ND ug/kg 01/25/23 02:12 87-61-601/24/23 16:479.9 1
1,2,4-Trichlorobenzene ND ug/kg 01/25/23 02:12 120-82-101/24/23 16:479.9 1
1,1,1-Trichloroethane ND ug/kg 01/25/23 02:12 71-55-601/24/23 16:479.9 1
1,1,2-Trichloroethane ND ug/kg 01/25/23 02:12 79-00-501/24/23 16:479.9 1
Trichloroethene ND ug/kg 01/25/23 02:12 79-01-601/24/23 16:479.9 1
Trichlorofluoromethane ND ug/kg 01/25/23 02:12 75-69-401/24/23 16:479.9 1
1,2,3-Trichloropropane ND ug/kg 01/25/23 02:12 96-18-401/24/23 16:479.9 1
1,2,4-Trimethylbenzene ND ug/kg 01/25/23 02:12 95-63-601/24/23 16:479.9 1
1,3,5-Trimethylbenzene ND ug/kg 01/25/23 02:12 108-67-8 v101/24/23 16:479.9 1
Vinyl acetate ND ug/kg 01/25/23 02:12 108-05-401/24/23 16:4799.0 1
Vinyl chloride ND ug/kg 01/25/23 02:12 75-01-401/24/23 16:4719.8 1
Xylene (Total)ND ug/kg 01/25/23 02:12 1330-20-701/24/23 16:4719.8 1
m&p-Xylene ND ug/kg 01/25/23 02:12 179601-23-101/24/23 16:4719.8 1
o-Xylene ND ug/kg 01/25/23 02:12 95-47-601/24/23 16:479.9 1
Surrogates
Toluene-d8 (S)100 %01/25/23 02:12 2037-26-5 D301/24/23 16:4770-130 1
4-Bromofluorobenzene (S)103 %01/25/23 02:12 460-00-401/24/23 16:4770-130 1
1,2-Dichloroethane-d4 (S)110 %01/25/23 02:12 17060-07-001/24/23 16:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 30.5 %01/24/23 15:32 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-16@30'Lab ID: 92648387005 Collected: 01/23/23 15:10 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 01/25/23 02:30 67-64-101/24/23 16:47103 1
Benzene ND ug/kg 01/25/23 02:30 71-43-201/24/23 16:475.2 1
Bromobenzene ND ug/kg 01/25/23 02:30 108-86-101/24/23 16:475.2 1
Bromochloromethane ND ug/kg 01/25/23 02:30 74-97-5 v101/24/23 16:475.2 1
Bromodichloromethane ND ug/kg 01/25/23 02:30 75-27-4 v101/24/23 16:475.2 1
Bromoform ND ug/kg 01/25/23 02:30 75-25-2 v101/24/23 16:475.2 1
Bromomethane ND ug/kg 01/25/23 02:30 74-83-901/24/23 16:4710.3 1
2-Butanone (MEK)ND ug/kg 01/25/23 02:30 78-93-301/24/23 16:47103 1
n-Butylbenzene ND ug/kg 01/25/23 02:30 104-51-801/24/23 16:475.2 1
sec-Butylbenzene ND ug/kg 01/25/23 02:30 135-98-801/24/23 16:475.2 1
tert-Butylbenzene ND ug/kg 01/25/23 02:30 98-06-601/24/23 16:475.2 1
Carbon tetrachloride ND ug/kg 01/25/23 02:30 56-23-501/24/23 16:475.2 1
Chlorobenzene ND ug/kg 01/25/23 02:30 108-90-701/24/23 16:475.2 1
Chloroethane ND ug/kg 01/25/23 02:30 75-00-301/24/23 16:4710.3 1
Chloroform ND ug/kg 01/25/23 02:30 67-66-301/24/23 16:475.2 1
Chloromethane ND ug/kg 01/25/23 02:30 74-87-301/24/23 16:4710.3 1
2-Chlorotoluene ND ug/kg 01/25/23 02:30 95-49-801/24/23 16:475.2 1
4-Chlorotoluene ND ug/kg 01/25/23 02:30 106-43-4 v101/24/23 16:475.2 1
1,2-Dibromo-3-chloropropane ND ug/kg 01/25/23 02:30 96-12-8 IK01/24/23 16:475.2 1
Dibromochloromethane ND ug/kg 01/25/23 02:30 124-48-101/24/23 16:475.2 1
1,2-Dibromoethane (EDB)ND ug/kg 01/25/23 02:30 106-93-401/24/23 16:475.2 1
Dibromomethane ND ug/kg 01/25/23 02:30 74-95-301/24/23 16:475.2 1
1,2-Dichlorobenzene ND ug/kg 01/25/23 02:30 95-50-101/24/23 16:475.2 1
1,3-Dichlorobenzene ND ug/kg 01/25/23 02:30 541-73-101/24/23 16:475.2 1
1,4-Dichlorobenzene ND ug/kg 01/25/23 02:30 106-46-701/24/23 16:475.2 1
Dichlorodifluoromethane ND ug/kg 01/25/23 02:30 75-71-8 IH01/24/23 16:4710.3 1
1,1-Dichloroethane ND ug/kg 01/25/23 02:30 75-34-301/24/23 16:475.2 1
1,2-Dichloroethane ND ug/kg 01/25/23 02:30 107-06-201/24/23 16:475.2 1
1,1-Dichloroethene ND ug/kg 01/25/23 02:30 75-35-401/24/23 16:475.2 1
cis-1,2-Dichloroethene ND ug/kg 01/25/23 02:30 156-59-201/24/23 16:475.2 1
trans-1,2-Dichloroethene ND ug/kg 01/25/23 02:30 156-60-501/24/23 16:475.2 1
1,2-Dichloropropane ND ug/kg 01/25/23 02:30 78-87-501/24/23 16:475.2 1
1,3-Dichloropropane ND ug/kg 01/25/23 02:30 142-28-901/24/23 16:475.2 1
2,2-Dichloropropane ND ug/kg 01/25/23 02:30 594-20-701/24/23 16:475.2 1
1,1-Dichloropropene ND ug/kg 01/25/23 02:30 563-58-601/24/23 16:475.2 1
cis-1,3-Dichloropropene ND ug/kg 01/25/23 02:30 10061-01-501/24/23 16:475.2 1
trans-1,3-Dichloropropene ND ug/kg 01/25/23 02:30 10061-02-601/24/23 16:475.2 1
Diisopropyl ether ND ug/kg 01/25/23 02:30 108-20-301/24/23 16:475.2 1
Ethylbenzene ND ug/kg 01/25/23 02:30 100-41-401/24/23 16:475.2 1
Hexachloro-1,3-butadiene ND ug/kg 01/25/23 02:30 87-68-301/24/23 16:4710.3 1
2-Hexanone ND ug/kg 01/25/23 02:30 591-78-6 IK01/24/23 16:4751.7 1
Isopropylbenzene (Cumene)ND ug/kg 01/25/23 02:30 98-82-801/24/23 16:475.2 1
p-Isopropyltoluene ND ug/kg 01/25/23 02:30 99-87-601/24/23 16:475.2 1
Methylene Chloride 53.3 ug/kg 01/25/23 02:30 75-09-201/24/23 16:4720.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/25/23 02:30 108-10-101/24/23 16:4751.7 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-16@30'Lab ID: 92648387005 Collected: 01/23/23 15:10 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 01/25/23 02:30 1634-04-401/24/23 16:475.2 1
Naphthalene ND ug/kg 01/25/23 02:30 91-20-301/24/23 16:475.2 1
n-Propylbenzene ND ug/kg 01/25/23 02:30 103-65-101/24/23 16:475.2 1
Styrene ND ug/kg 01/25/23 02:30 100-42-501/24/23 16:475.2 1
1,1,1,2-Tetrachloroethane ND ug/kg 01/25/23 02:30 630-20-601/24/23 16:475.2 1
1,1,2,2-Tetrachloroethane ND ug/kg 01/25/23 02:30 79-34-501/24/23 16:475.2 1
Tetrachloroethene ND ug/kg 01/25/23 02:30 127-18-401/24/23 16:475.2 1
Toluene 197 ug/kg 01/25/23 02:30 108-88-301/24/23 16:475.2 1
1,2,3-Trichlorobenzene ND ug/kg 01/25/23 02:30 87-61-601/24/23 16:475.2 1
1,2,4-Trichlorobenzene ND ug/kg 01/25/23 02:30 120-82-101/24/23 16:475.2 1
1,1,1-Trichloroethane ND ug/kg 01/25/23 02:30 71-55-601/24/23 16:475.2 1
1,1,2-Trichloroethane ND ug/kg 01/25/23 02:30 79-00-501/24/23 16:475.2 1
Trichloroethene ND ug/kg 01/25/23 02:30 79-01-601/24/23 16:475.2 1
Trichlorofluoromethane ND ug/kg 01/25/23 02:30 75-69-401/24/23 16:475.2 1
1,2,3-Trichloropropane ND ug/kg 01/25/23 02:30 96-18-401/24/23 16:475.2 1
1,2,4-Trimethylbenzene ND ug/kg 01/25/23 02:30 95-63-601/24/23 16:475.2 1
1,3,5-Trimethylbenzene ND ug/kg 01/25/23 02:30 108-67-8 v101/24/23 16:475.2 1
Vinyl acetate ND ug/kg 01/25/23 02:30 108-05-401/24/23 16:4751.7 1
Vinyl chloride ND ug/kg 01/25/23 02:30 75-01-401/24/23 16:4710.3 1
Xylene (Total)ND ug/kg 01/25/23 02:30 1330-20-701/24/23 16:4710.3 1
m&p-Xylene ND ug/kg 01/25/23 02:30 179601-23-101/24/23 16:4710.3 1
o-Xylene ND ug/kg 01/25/23 02:30 95-47-601/24/23 16:475.2 1
Surrogates
Toluene-d8 (S)101 %01/25/23 02:30 2037-26-5 D301/24/23 16:4770-130 1
4-Bromofluorobenzene (S)92 %01/25/23 02:30 460-00-401/24/23 16:4770-130 1
1,2-Dichloroethane-d4 (S)112 %01/25/23 02:30 17060-07-001/24/23 16:4770-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 4.2 %01/24/23 15:32 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-18@5'Lab ID: 92648387006 Collected: 01/23/23 15:20 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 01/25/23 06:36 67-64-101/24/23 16:477370 50
Benzene ND ug/kg 01/25/23 06:36 71-43-201/24/23 16:47368 50
Bromobenzene ND ug/kg 01/25/23 06:36 108-86-101/24/23 16:47368 50
Bromochloromethane ND ug/kg 01/25/23 06:36 74-97-501/24/23 16:47368 50
Bromodichloromethane ND ug/kg 01/25/23 06:36 75-27-4 v101/24/23 16:47368 50
Bromoform ND ug/kg 01/25/23 06:36 75-25-2 v101/24/23 16:47368 50
Bromomethane ND ug/kg 01/25/23 06:36 74-83-901/24/23 16:47737 50
2-Butanone (MEK)ND ug/kg 01/25/23 06:36 78-93-301/24/23 16:477370 50
n-Butylbenzene ND ug/kg 01/25/23 06:36 104-51-801/24/23 16:47368 50
sec-Butylbenzene ND ug/kg 01/25/23 06:36 135-98-801/24/23 16:47368 50
tert-Butylbenzene ND ug/kg 01/25/23 06:36 98-06-601/24/23 16:47368 50
Carbon tetrachloride ND ug/kg 01/25/23 06:36 56-23-501/24/23 16:47368 50
Chlorobenzene ND ug/kg 01/25/23 06:36 108-90-701/24/23 16:47368 50
Chloroethane ND ug/kg 01/25/23 06:36 75-00-301/24/23 16:47737 50
Chloroform 684 ug/kg 01/25/23 06:36 67-66-3 B01/24/23 16:47368 50
Chloromethane ND ug/kg 01/25/23 06:36 74-87-301/24/23 16:47737 50
2-Chlorotoluene ND ug/kg 01/25/23 06:36 95-49-801/24/23 16:47368 50
4-Chlorotoluene ND ug/kg 01/25/23 06:36 106-43-4 v101/24/23 16:47368 50
1,2-Dibromo-3-chloropropane ND ug/kg 01/25/23 06:36 96-12-8 IK01/24/23 16:47368 50
Dibromochloromethane ND ug/kg 01/25/23 06:36 124-48-1 v101/24/23 16:47368 50
1,2-Dibromoethane (EDB)ND ug/kg 01/25/23 06:36 106-93-401/24/23 16:47368 50
Dibromomethane ND ug/kg 01/25/23 06:36 74-95-301/24/23 16:47368 50
1,2-Dichlorobenzene ND ug/kg 01/25/23 06:36 95-50-101/24/23 16:47368 50
1,3-Dichlorobenzene ND ug/kg 01/25/23 06:36 541-73-101/24/23 16:47368 50
1,4-Dichlorobenzene ND ug/kg 01/25/23 06:36 106-46-701/24/23 16:47368 50
Dichlorodifluoromethane ND ug/kg 01/25/23 06:36 75-71-8 IH01/24/23 16:47737 50
1,1-Dichloroethane ND ug/kg 01/25/23 06:36 75-34-301/24/23 16:47368 50
1,2-Dichloroethane ND ug/kg 01/25/23 06:36 107-06-201/24/23 16:47368 50
1,1-Dichloroethene ND ug/kg 01/25/23 06:36 75-35-401/24/23 16:47368 50
cis-1,2-Dichloroethene ND ug/kg 01/25/23 06:36 156-59-201/24/23 16:47368 50
trans-1,2-Dichloroethene ND ug/kg 01/25/23 06:36 156-60-501/24/23 16:47368 50
1,2-Dichloropropane ND ug/kg 01/25/23 06:36 78-87-501/24/23 16:47368 50
1,3-Dichloropropane ND ug/kg 01/25/23 06:36 142-28-901/24/23 16:47368 50
2,2-Dichloropropane ND ug/kg 01/25/23 06:36 594-20-701/24/23 16:47368 50
1,1-Dichloropropene ND ug/kg 01/25/23 06:36 563-58-601/24/23 16:47368 50
cis-1,3-Dichloropropene ND ug/kg 01/25/23 06:36 10061-01-501/24/23 16:47368 50
trans-1,3-Dichloropropene ND ug/kg 01/25/23 06:36 10061-02-601/24/23 16:47368 50
Diisopropyl ether ND ug/kg 01/25/23 06:36 108-20-301/24/23 16:47368 50
Ethylbenzene ND ug/kg 01/25/23 06:36 100-41-401/24/23 16:47368 50
Hexachloro-1,3-butadiene ND ug/kg 01/25/23 06:36 87-68-301/24/23 16:47737 50
2-Hexanone ND ug/kg 01/25/23 06:36 591-78-6 IK01/24/23 16:473680 50
Isopropylbenzene (Cumene)ND ug/kg 01/25/23 06:36 98-82-801/24/23 16:47368 50
p-Isopropyltoluene ND ug/kg 01/25/23 06:36 99-87-601/24/23 16:47368 50
Methylene Chloride 2490 ug/kg 01/25/23 06:36 75-09-201/24/23 16:471470 50
4-Methyl-2-pentanone (MIBK)ND ug/kg 01/25/23 06:36 108-10-101/24/23 16:473680 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92648387
GILBARCO
Sample: SS-18@5'Lab ID: 92648387006 Collected: 01/23/23 15:20 Received: 01/24/23 10:34 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 01/25/23 06:36 1634-04-401/24/23 16:47368 50
Naphthalene ND ug/kg 01/25/23 06:36 91-20-301/24/23 16:47368 50
n-Propylbenzene ND ug/kg 01/25/23 06:36 103-65-101/24/23 16:47368 50
Styrene ND ug/kg 01/25/23 06:36 100-42-501/24/23 16:47368 50
1,1,1,2-Tetrachloroethane ND ug/kg 01/25/23 06:36 630-20-601/24/23 16:47368 50
1,1,2,2-Tetrachloroethane ND ug/kg 01/25/23 06:36 79-34-501/24/23 16:47368 50
Tetrachloroethene ND ug/kg 01/25/23 06:36 127-18-401/24/23 16:47368 50
Toluene 13500 ug/kg 01/25/23 06:36 108-88-301/24/23 16:47368 50
1,2,3-Trichlorobenzene ND ug/kg 01/25/23 06:36 87-61-601/24/23 16:47368 50
1,2,4-Trichlorobenzene ND ug/kg 01/25/23 06:36 120-82-101/24/23 16:47368 50
1,1,1-Trichloroethane ND ug/kg 01/25/23 06:36 71-55-601/24/23 16:47368 50
1,1,2-Trichloroethane ND ug/kg 01/25/23 06:36 79-00-501/24/23 16:47368 50
Trichloroethene ND ug/kg 01/25/23 06:36 79-01-601/24/23 16:47368 50
Trichlorofluoromethane ND ug/kg 01/25/23 06:36 75-69-401/24/23 16:47368 50
1,2,3-Trichloropropane ND ug/kg 01/25/23 06:36 96-18-401/24/23 16:47368 50
1,2,4-Trimethylbenzene ND ug/kg 01/25/23 06:36 95-63-601/24/23 16:47368 50
1,3,5-Trimethylbenzene ND ug/kg 01/25/23 06:36 108-67-8 v101/24/23 16:47368 50
Vinyl acetate ND ug/kg 01/25/23 06:36 108-05-401/24/23 16:473680 50
Vinyl chloride ND ug/kg 01/25/23 06:36 75-01-401/24/23 16:47737 50
Xylene (Total)ND ug/kg 01/25/23 06:36 1330-20-701/24/23 16:47737 50
m&p-Xylene ND ug/kg 01/25/23 06:36 179601-23-101/24/23 16:47737 50
o-Xylene ND ug/kg 01/25/23 06:36 95-47-601/24/23 16:47368 50
Surrogates
Toluene-d8 (S)102 %01/25/23 06:36 2037-26-5 D301/24/23 16:4770-130 50
4-Bromofluorobenzene (S)108 %01/25/23 06:36 460-00-401/24/23 16:4770-130 50
1,2-Dichloroethane-d4 (S)111 %01/25/23 06:36 17060-07-001/24/23 16:4770-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.5 %01/24/23 15:32 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751489
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92648387001, 92648387002, 92648387003, 92648387004, 92648387005, 92648387006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3905175
Associated Lab Samples:92648387001, 92648387002, 92648387003, 92648387004, 92648387005, 92648387006
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 01/24/23 22:58
1,1,1-Trichloroethane ug/kg ND 5.0 01/24/23 22:58
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 01/24/23 22:58
1,1,2-Trichloroethane ug/kg ND 5.0 01/24/23 22:58
1,1-Dichloroethane ug/kg ND 5.0 01/24/23 22:58
1,1-Dichloroethene ug/kg ND 5.0 01/24/23 22:58
1,1-Dichloropropene ug/kg ND 5.0 01/24/23 22:58
1,2,3-Trichlorobenzene ug/kg ND 5.0 01/24/23 22:58
1,2,3-Trichloropropane ug/kg ND 5.0 01/24/23 22:58
1,2,4-Trichlorobenzene ug/kg ND 5.0 01/24/23 22:58
1,2,4-Trimethylbenzene ug/kg ND 5.0 01/24/23 22:58
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 IK01/24/23 22:58
1,2-Dibromoethane (EDB)ug/kg ND 5.0 01/24/23 22:58
1,2-Dichlorobenzene ug/kg ND 5.0 01/24/23 22:58
1,2-Dichloroethane ug/kg ND 5.0 01/24/23 22:58
1,2-Dichloropropane ug/kg ND 5.0 01/24/23 22:58
1,3,5-Trimethylbenzene ug/kg ND 5.0 v101/24/23 22:58
1,3-Dichlorobenzene ug/kg ND 5.0 01/24/23 22:58
1,3-Dichloropropane ug/kg ND 5.0 01/24/23 22:58
1,4-Dichlorobenzene ug/kg ND 5.0 01/24/23 22:58
2,2-Dichloropropane ug/kg ND 5.0 01/24/23 22:58
2-Butanone (MEK)ug/kg ND 100 01/24/23 22:58
2-Chlorotoluene ug/kg ND 5.0 01/24/23 22:58
2-Hexanone ug/kg ND 50.0 IK01/24/23 22:58
4-Chlorotoluene ug/kg ND 5.0 v101/24/23 22:58
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 01/24/23 22:58
Acetone ug/kg ND 100 01/24/23 22:58
Benzene ug/kg ND 5.0 01/24/23 22:58
Bromobenzene ug/kg ND 5.0 01/24/23 22:58
Bromochloromethane ug/kg ND 5.0 01/24/23 22:58
Bromodichloromethane ug/kg ND 5.0 v101/24/23 22:58
Bromoform ug/kg ND 5.0 v101/24/23 22:58
Bromomethane ug/kg ND 10.0 01/24/23 22:58
Carbon tetrachloride ug/kg ND 5.0 01/24/23 22:58
Chlorobenzene ug/kg ND 5.0 01/24/23 22:58
Chloroethane ug/kg ND 10.0 01/24/23 22:58
Chloroform ug/kg 9.0 5.0 01/24/23 22:58
Chloromethane ug/kg ND 10.0 01/24/23 22:58
cis-1,2-Dichloroethene ug/kg ND 5.0 01/24/23 22:58
cis-1,3-Dichloropropene ug/kg ND 5.0 01/24/23 22:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3905175
Associated Lab Samples:92648387001, 92648387002, 92648387003, 92648387004, 92648387005, 92648387006
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 v101/24/23 22:58
Dibromomethane ug/kg ND 5.0 01/24/23 22:58
Dichlorodifluoromethane ug/kg ND 10.0 IH01/24/23 22:58
Diisopropyl ether ug/kg ND 5.0 01/24/23 22:58
Ethylbenzene ug/kg ND 5.0 01/24/23 22:58
Hexachloro-1,3-butadiene ug/kg ND 10.0 01/24/23 22:58
Isopropylbenzene (Cumene)ug/kg ND 5.0 01/24/23 22:58
m&p-Xylene ug/kg ND 10.0 01/24/23 22:58
Methyl-tert-butyl ether ug/kg ND 5.0 01/24/23 22:58
Methylene Chloride ug/kg ND 20.0 01/24/23 22:58
n-Butylbenzene ug/kg ND 5.0 01/24/23 22:58
n-Propylbenzene ug/kg ND 5.0 01/24/23 22:58
Naphthalene ug/kg ND 5.0 01/24/23 22:58
o-Xylene ug/kg ND 5.0 01/24/23 22:58
p-Isopropyltoluene ug/kg ND 5.0 01/24/23 22:58
sec-Butylbenzene ug/kg ND 5.0 01/24/23 22:58
Styrene ug/kg ND 5.0 01/24/23 22:58
tert-Butylbenzene ug/kg ND 5.0 01/24/23 22:58
Tetrachloroethene ug/kg ND 5.0 01/24/23 22:58
Toluene ug/kg ND 5.0 01/24/23 22:58
trans-1,2-Dichloroethene ug/kg ND 5.0 01/24/23 22:58
trans-1,3-Dichloropropene ug/kg ND 5.0 01/24/23 22:58
Trichloroethene ug/kg ND 5.0 01/24/23 22:58
Trichlorofluoromethane ug/kg ND 5.0 01/24/23 22:58
Vinyl acetate ug/kg ND 50.0 01/24/23 22:58
Vinyl chloride ug/kg ND 10.0 01/24/23 22:58
Xylene (Total)ug/kg ND 10.0 01/24/23 22:58
1,2-Dichloroethane-d4 (S)%111 70-130 01/24/23 22:58
4-Bromofluorobenzene (S)%101 70-130 01/24/23 22:58
Toluene-d8 (S)%100 70-130 01/24/23 22:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905176LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 577500 115 70-130
1,1,1-Trichloroethane ug/kg 573500 115 70-130
1,1,2,2-Tetrachloroethane ug/kg 483500 97 70-130
1,1,2-Trichloroethane ug/kg 526500 105 70-130
1,1-Dichloroethane ug/kg 516500 103 70-130
1,1-Dichloroethene ug/kg 552500 110 70-130
1,1-Dichloropropene ug/kg 541500 108 70-130
1,2,3-Trichlorobenzene ug/kg 490500 98 70-130
1,2,3-Trichloropropane ug/kg 495500 99 70-130
1,2,4-Trichlorobenzene ug/kg 530500 106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905176LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 546500 109 70-130
1,2-Dibromo-3-chloropropane ug/kg 584 IK500117 67-130
1,2-Dibromoethane (EDB)ug/kg 525500 105 70-130
1,2-Dichlorobenzene ug/kg 529500 106 70-130
1,2-Dichloroethane ug/kg 562500 112 70-130
1,2-Dichloropropane ug/kg 558500 112 70-130
1,3,5-Trimethylbenzene ug/kg 577 v1500115 70-130
1,3-Dichlorobenzene ug/kg 521500 104 70-130
1,3-Dichloropropane ug/kg 509500 102 70-130
1,4-Dichlorobenzene ug/kg 544500 109 70-130
2,2-Dichloropropane ug/kg 566500 113 67-130
2-Butanone (MEK)ug/kg 9761000 98 66-130
2-Chlorotoluene ug/kg 569500 114 70-130
2-Hexanone ug/kg 1060 IK1000106 70-130
4-Chlorotoluene ug/kg 585 v1500117 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 10501000 105 70-130
Acetone ug/kg 9431000 94 67-130
Benzene ug/kg 517500 103 70-130
Bromobenzene ug/kg 538500 108 70-130
Bromochloromethane ug/kg 482500 96 70-130
Bromodichloromethane ug/kg 601 v1500120 70-130
Bromoform ug/kg 565 v1500113 70-130
Bromomethane ug/kg 561500 112 53-175
Carbon tetrachloride ug/kg 641500 128 70-130
Chlorobenzene ug/kg 516500 103 70-130
Chloroethane ug/kg 502500 100 70-135
Chloroform ug/kg 508500 102 70-130
Chloromethane ug/kg 596500 119 64-130
cis-1,2-Dichloroethene ug/kg 557500 111 70-130
cis-1,3-Dichloropropene ug/kg 569500 114 70-130
Dibromochloromethane ug/kg 576 v1500115 70-130
Dibromomethane ug/kg 576500 115 70-130
Dichlorodifluoromethane ug/kg 672 IH500134 63-145
Diisopropyl ether ug/kg 511500 102 68-130
Ethylbenzene ug/kg 505500 101 70-130
Hexachloro-1,3-butadiene ug/kg 552500 110 70-130
Isopropylbenzene (Cumene)ug/kg 539500 108 70-130
m&p-Xylene ug/kg 10901000 109 70-130
Methyl-tert-butyl ether ug/kg 521500 104 70-130
Methylene Chloride ug/kg 500500 100 67-130
n-Butylbenzene ug/kg 563500 113 70-130
n-Propylbenzene ug/kg 574500 115 70-130
Naphthalene ug/kg 465500 93 70-130
o-Xylene ug/kg 521500 104 70-130
p-Isopropyltoluene ug/kg 573500 115 70-130
sec-Butylbenzene ug/kg 551500 110 70-130
Styrene ug/kg 541500 108 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3905176LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 530500 106 64-130
Tetrachloroethene ug/kg 563500 113 70-130
Toluene ug/kg 536500 107 70-130
trans-1,2-Dichloroethene ug/kg 560500 112 70-130
trans-1,3-Dichloropropene ug/kg 591500 118 70-130
Trichloroethene ug/kg 601500 120 70-130
Trichlorofluoromethane ug/kg 517500 103 70-130
Vinyl acetate ug/kg 11301000 113 70-134
Vinyl chloride ug/kg 524500 105 68-130
Xylene (Total)ug/kg 16101500 107 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3905177MATRIX SPIKE SAMPLE:
MSSpike
Result
92648146003
1,1,1,2-Tetrachloroethane ug/kg 13101170 112 58-140ND
1,1,1-Trichloroethane ug/kg 13801170 118 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 11601170 99 52-139ND
1,1,2-Trichloroethane ug/kg 12901170 110 56-140ND
1,1-Dichloroethane ug/kg 13601170 116 58-145ND
1,1-Dichloroethene ug/kg 15301170 130 57-158ND
1,1-Dichloropropene ug/kg 14001170 119 58-151ND
1,2,3-Trichlorobenzene ug/kg 8121170 69 48-149ND
1,2,3-Trichloropropane ug/kg 11301170 96 54-132ND
1,2,4-Trichlorobenzene ug/kg 10701170 91 51-151ND
1,2,4-Trimethylbenzene ug/kg 11701170 100 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 998 v1117085 44-134ND
1,2-Dibromoethane (EDB)ug/kg 12701170 108 60-138ND
1,2-Dichlorobenzene ug/kg 11901170 101 59-147ND
1,2-Dichloroethane ug/kg 13901170 119 57-139ND
1,2-Dichloropropane ug/kg 13601170 116 62-145ND
1,3,5-Trimethylbenzene ug/kg 1290 v11170110 47-159ND
1,3-Dichlorobenzene ug/kg 12201170 104 58-144ND
1,3-Dichloropropane ug/kg 12701170 108 60-142ND
1,4-Dichlorobenzene ug/kg 12401170 106 57-143ND
2,2-Dichloropropane ug/kg 12401170 106 37-144ND
2-Butanone (MEK)ug/kg 24802340 106 28-146ND
2-Chlorotoluene ug/kg 12701170 108 55-158ND
2-Hexanone ug/kg 2290 v1234098 44-141ND
4-Chlorotoluene ug/kg 1310 v11170112 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 23802340 101 50-138ND
Acetone ug/kg 20602340 88 20-136ND
Benzene ug/kg 12601170 108 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3905177MATRIX SPIKE SAMPLE:
MSSpike
Result
92648146003
Bromobenzene ug/kg 12301170 105 59-145ND
Bromochloromethane ug/kg 12301170 105 57-143ND
Bromodichloromethane ug/kg 1330 v11170114 53-133ND
Bromoform ug/kg 1210 v11170104 48-133ND
Bromomethane ug/kg 6941170 59 10-167ND
Carbon tetrachloride ug/kg 10101170 86 57-147ND
Chlorobenzene ug/kg 12201170 104 61-144ND
Chloroethane ug/kg 5901170 50 10-153ND
Chloroform ug/kg 13401170 112 58-14120.7
Chloromethane ug/kg 15501170 133 54-165ND
cis-1,2-Dichloroethene ug/kg 14401170 123 59-144ND
cis-1,3-Dichloropropene ug/kg 13301170 113 56-137ND
Dibromochloromethane ug/kg 1330 v11170113 53-139ND
Dibromomethane ug/kg 13601170 116 60-136ND
Dichlorodifluoromethane ug/kg 1900 IH1170162 49-177ND
Diisopropyl ether ug/kg 13401170 114 53-136ND
Ethylbenzene ug/kg 11901170 101 53-150ND
Hexachloro-1,3-butadiene ug/kg 16301170 139 42-186ND
Isopropylbenzene (Cumene)ug/kg 13001170 111 62-154ND
m&p-Xylene ug/kg 25902340 110 49-156ND
Methyl-tert-butyl ether ug/kg 12901170 110 54-133ND
Methylene Chloride ug/kg 14701170 120 50-15354.9
n-Butylbenzene ug/kg 13001170 111 44-174ND
n-Propylbenzene ug/kg 12501170 107 52-157ND
Naphthalene ug/kg 7071170 60 37-150ND
o-Xylene ug/kg 12101170 104 54-150ND
p-Isopropyltoluene ug/kg 12901170 110 50-164ND
sec-Butylbenzene ug/kg 13001170 111 58-161ND
Styrene ug/kg 12601170 107 60-148ND
tert-Butylbenzene ug/kg 12301170 105 44-151ND
Tetrachloroethene ug/kg 12901170 110 53-151ND
Toluene ug/kg 17501170 99 52-148589
trans-1,2-Dichloroethene ug/kg 14501170 123 60-148ND
trans-1,3-Dichloropropene ug/kg 13601170 116 55-133ND
Trichloroethene ug/kg 13901170 119 60-148ND
Trichlorofluoromethane ug/kg 6961170 59 10-154ND
Vinyl acetate ug/kg 26802340 115 50-149ND
Vinyl chloride ug/kg 14901170 127 57-157ND
Xylene (Total)ug/kg 38003520 108 52-153ND
1,2-Dichloroethane-d4 (S)%113 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92648146004
3905178SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg ND IKND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg ND v1ND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg ND IKND
4-Chlorotoluene ug/kg ND v1ND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg 5.8JND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg ND v1ND
Bromoform ug/kg ND v1ND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg 18.3 2614.1
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg ND v1ND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND IHND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 7.9JND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92648146004
3905178SAMPLE DUPLICATE:
m&p-Xylene ug/kg 7.8JND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg 72.8 D682174
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 668 D659365
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%113110
4-Bromofluorobenzene (S)%102103
Toluene-d8 (S)%102100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
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Page 23 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92648387
GILBARCO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
751455
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92648387001, 92648387002, 92648387003, 92648387004, 92648387005, 92648387006
Parameter Units
Dup
Result QualifiersRPDResult
92648142001
3905010SAMPLE DUPLICATE:
Percent Moisture %7.7 N207.7
Parameter Units
Dup
Result QualifiersRPDResult
92648381002
3905011SAMPLE DUPLICATE:
Percent Moisture %20.3 N2321.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 24 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92648387
GILBARCO
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
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Page 25 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92648387
GILBARCO
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92648387001 751489 751587SS-12@3'EPA 5035A/5030B EPA 8260D
92648387002 751489 751587SS-13@5'EPA 5035A/5030B EPA 8260D
92648387003 751489 751587SS-14@40'EPA 5035A/5030B EPA 8260D
92648387004 751489 751587SS-15@59'EPA 5035A/5030B EPA 8260D
92648387005 751489 751587SS-16@30'EPA 5035A/5030B EPA 8260D
92648387006 751489 751587SS-18@5'EPA 5035A/5030B EPA 8260D
92648387001 751455SS-12@3'SW-846
92648387002 751455SS-13@5'SW-846
92648387003 751455SS-14@40'SW-846
92648387004 751455SS-15@59'SW-846
92648387005 751455SS-16@30'SW-846
92648387006 751455SS-18@5'SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 01/27/2023 12:23 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 28
Page 27 of 28
Page 28 of 28
#=CL#
April 11, 2023
LIMS USE: FR - CHRIS HAY
LIMS OBJECT ID: 92660640
92660640
Project:
Pace Project No.:
RE:
Chris Hay
EnviroTrac
7343 W. Friendly Avenue
Suite J
Greensboro, NC 27410
GILBARRO
Dear Chris Hay:
Enclosed are the analytical results for sample(s) received by the laboratory on April 05, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sara Poulson
[e-mail]
Project Manager
[phone]
Enclosures
cc: Annamarie Blauser, EnviroTrac Ltd
Gail Hay, EnviroTrac, Ltd.
Elizabeth Taccone, Envirotrac - NC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 38
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92660640
GILBARRO
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 38
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92660640
GILBARRO
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92660640001 UNIT 7/8 SUPPLY UNIT 7 DRAIN EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92660640002 UNIT 8 DRAIN, UNUSED SUPPLY EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92660640003 UNIT 2 SUPPLY EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92660640004 MAIN LINE COOLENT UNIT EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92660640005 MAINLINE DRAIN TO 7 EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92660640006 UNIT 4/6 SUPPLY AND DRAIN EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92660640007 UNIT 4/6 MAINLINE SUPPLY AND D EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
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[phone]
Page 3 of 38
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92660640
GILBARRO
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92660640001 UNIT 7/8 SUPPLY UNIT 7 DRAIN
sec-Butylbenzene 12.7 ug/kg 04/11/23 02:4210.4EPA 8260D
Methylene Chloride 579 ug/kg 04/11/23 02:42 IK41.5EPA 8260D
1,2,4-Trimethylbenzene 67.6 ug/kg 04/11/23 02:4210.4EPA 8260D
1,3,5-Trimethylbenzene 29.0 ug/kg 04/11/23 02:4210.4EPA 8260D
Percent Moisture 19.7 %04/06/23 17:54 N20.10SW-846
92660640002 UNIT 8 DRAIN, UNUSED SUPPLY
Methylene Chloride 970 ug/kg 04/08/23 06:41 L231.8EPA 8260D
Percent Moisture 19.3 %04/06/23 17:54 N20.10SW-846
92660640003 UNIT 2 SUPPLY
Methylene Chloride 1210 ug/kg 04/08/23 06:58 L259.6EPA 8260D
Percent Moisture 19.3 %04/06/23 17:55 N20.10SW-846
92660640004 MAIN LINE COOLENT UNIT
sec-Butylbenzene 4420 ug/kg 04/08/23 14:58391EPA 8260D
Isopropylbenzene (Cumene)645 ug/kg 04/08/23 14:58391EPA 8260D
p-Isopropyltoluene 5570 ug/kg 04/08/23 14:58391EPA 8260D
4-Methyl-2-pentanone (MIBK)4600 ug/kg 04/08/23 14:583910EPA 8260D
1,2,4-Trimethylbenzene 7850 ug/kg 04/08/23 14:58391EPA 8260D
1,3,5-Trimethylbenzene 6210 ug/kg 04/08/23 14:58391EPA 8260D
Percent Moisture 10.5 %04/06/23 17:55 N20.10SW-846
92660640005 MAINLINE DRAIN TO 7
Methylene Chloride 423 ug/kg 04/08/23 07:34 L251.9EPA 8260D
o-Xylene 16.6 ug/kg 04/08/23 07:3413.0EPA 8260D
Percent Moisture 20.0 %04/06/23 17:55 N20.10SW-846
92660640006 UNIT 4/6 SUPPLY AND DRAIN
Acetone 252 ug/kg 04/08/23 07:52150EPA 8260D
Methylene Chloride 234 ug/kg 04/08/23 07:52 L230.0EPA 8260D
Percent Moisture 10 %04/06/23 17:55 N20.10SW-846
92660640007 UNIT 4/6 MAINLINE SUPPLY AND
D
Methylene Chloride 253 ug/kg 04/08/23 08:09 L232.5EPA 8260D
Percent Moisture 17.6 %04/06/23 17:55 N20.10SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 4 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 7/8 SUPPLY UNIT 7
DRAIN
Lab ID: 92660640001 Collected: 04/03/23 15:34 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/11/23 02:42 67-64-104/06/23 00:03207 1
Benzene ND ug/kg 04/11/23 02:42 71-43-204/06/23 00:0310.4 1
Bromobenzene ND ug/kg 04/11/23 02:42 108-86-104/06/23 00:0310.4 1
Bromochloromethane ND ug/kg 04/11/23 02:42 74-97-504/06/23 00:0310.4 1
Bromodichloromethane ND ug/kg 04/11/23 02:42 75-27-404/06/23 00:0310.4 1
Bromoform ND ug/kg 04/11/23 02:42 75-25-2 IK04/06/23 00:0310.4 1
Bromomethane ND ug/kg 04/11/23 02:42 74-83-904/06/23 00:0341.5 1
2-Butanone (MEK)ND ug/kg 04/11/23 02:42 78-93-304/06/23 00:03207 1
n-Butylbenzene ND ug/kg 04/11/23 02:42 104-51-804/06/23 00:0310.4 1
sec-Butylbenzene 12.7 ug/kg 04/11/23 02:42 135-98-804/06/23 00:0310.4 1
tert-Butylbenzene ND ug/kg 04/11/23 02:42 98-06-604/06/23 00:0310.4 1
Carbon tetrachloride ND ug/kg 04/11/23 02:42 56-23-504/06/23 00:0310.4 1
Chlorobenzene ND ug/kg 04/11/23 02:42 108-90-704/06/23 00:0310.4 1
Chloroethane ND ug/kg 04/11/23 02:42 75-00-304/06/23 00:0320.7 1
Chloroform ND ug/kg 04/11/23 02:42 67-66-304/06/23 00:0310.4 1
Chloromethane ND ug/kg 04/11/23 02:42 74-87-304/06/23 00:0320.7 1
2-Chlorotoluene ND ug/kg 04/11/23 02:42 95-49-804/06/23 00:0310.4 1
4-Chlorotoluene ND ug/kg 04/11/23 02:42 106-43-404/06/23 00:0310.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/11/23 02:42 96-12-804/06/23 00:0310.4 1
Dibromochloromethane ND ug/kg 04/11/23 02:42 124-48-104/06/23 00:0310.4 1
1,2-Dibromoethane (EDB)ND ug/kg 04/11/23 02:42 106-93-404/06/23 00:0310.4 1
Dibromomethane ND ug/kg 04/11/23 02:42 74-95-304/06/23 00:0310.4 1
1,2-Dichlorobenzene ND ug/kg 04/11/23 02:42 95-50-104/06/23 00:0310.4 1
1,3-Dichlorobenzene ND ug/kg 04/11/23 02:42 541-73-104/06/23 00:0310.4 1
1,4-Dichlorobenzene ND ug/kg 04/11/23 02:42 106-46-704/06/23 00:0310.4 1
Dichlorodifluoromethane ND ug/kg 04/11/23 02:42 75-71-8 v104/06/23 00:0320.7 1
1,1-Dichloroethane ND ug/kg 04/11/23 02:42 75-34-304/06/23 00:0310.4 1
1,2-Dichloroethane ND ug/kg 04/11/23 02:42 107-06-204/06/23 00:0310.4 1
1,1-Dichloroethene ND ug/kg 04/11/23 02:42 75-35-404/06/23 00:0310.4 1
cis-1,2-Dichloroethene ND ug/kg 04/11/23 02:42 156-59-204/06/23 00:0310.4 1
trans-1,2-Dichloroethene ND ug/kg 04/11/23 02:42 156-60-504/06/23 00:0310.4 1
1,2-Dichloropropane ND ug/kg 04/11/23 02:42 78-87-504/06/23 00:0310.4 1
1,3-Dichloropropane ND ug/kg 04/11/23 02:42 142-28-904/06/23 00:0310.4 1
2,2-Dichloropropane ND ug/kg 04/11/23 02:42 594-20-704/06/23 00:0310.4 1
1,1-Dichloropropene ND ug/kg 04/11/23 02:42 563-58-604/06/23 00:0310.4 1
cis-1,3-Dichloropropene ND ug/kg 04/11/23 02:42 10061-01-504/06/23 00:0310.4 1
trans-1,3-Dichloropropene ND ug/kg 04/11/23 02:42 10061-02-604/06/23 00:0310.4 1
Diisopropyl ether ND ug/kg 04/11/23 02:42 108-20-304/06/23 00:0310.4 1
Ethylbenzene ND ug/kg 04/11/23 02:42 100-41-404/06/23 00:0310.4 1
Hexachloro-1,3-butadiene ND ug/kg 04/11/23 02:42 87-68-304/06/23 00:0320.7 1
2-Hexanone ND ug/kg 04/11/23 02:42 591-78-6 v104/06/23 00:03104 1
Isopropylbenzene (Cumene)ND ug/kg 04/11/23 02:42 98-82-804/06/23 00:0310.4 1
p-Isopropyltoluene ND ug/kg 04/11/23 02:42 99-87-604/06/23 00:0310.4 1
Methylene Chloride 579 ug/kg 04/11/23 02:42 75-09-2 IK04/06/23 00:0341.5 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
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Page 5 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 7/8 SUPPLY UNIT 7
DRAIN
Lab ID: 92660640001 Collected: 04/03/23 15:34 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/11/23 02:42 108-10-104/06/23 00:03104 1
Methyl-tert-butyl ether ND ug/kg 04/11/23 02:42 1634-04-404/06/23 00:0310.4 1
Naphthalene ND ug/kg 04/11/23 02:42 91-20-3 v104/06/23 00:0310.4 1
n-Propylbenzene ND ug/kg 04/11/23 02:42 103-65-104/06/23 00:0310.4 1
Styrene ND ug/kg 04/11/23 02:42 100-42-504/06/23 00:0310.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/11/23 02:42 630-20-604/06/23 00:0310.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/11/23 02:42 79-34-504/06/23 00:0310.4 1
Tetrachloroethene ND ug/kg 04/11/23 02:42 127-18-404/06/23 00:0310.4 1
Toluene ND ug/kg 04/11/23 02:42 108-88-304/06/23 00:0310.4 1
1,2,3-Trichlorobenzene ND ug/kg 04/11/23 02:42 87-61-604/06/23 00:0310.4 1
1,2,4-Trichlorobenzene ND ug/kg 04/11/23 02:42 120-82-104/06/23 00:0310.4 1
1,1,1-Trichloroethane ND ug/kg 04/11/23 02:42 71-55-604/06/23 00:0310.4 1
1,1,2-Trichloroethane ND ug/kg 04/11/23 02:42 79-00-504/06/23 00:0310.4 1
Trichloroethene ND ug/kg 04/11/23 02:42 79-01-604/06/23 00:0310.4 1
Trichlorofluoromethane ND ug/kg 04/11/23 02:42 75-69-404/06/23 00:0310.4 1
1,2,3-Trichloropropane ND ug/kg 04/11/23 02:42 96-18-404/06/23 00:0310.4 1
1,2,4-Trimethylbenzene 67.6 ug/kg 04/11/23 02:42 95-63-604/06/23 00:0310.4 1
1,3,5-Trimethylbenzene 29.0 ug/kg 04/11/23 02:42 108-67-804/06/23 00:0310.4 1
Vinyl acetate ND ug/kg 04/11/23 02:42 108-05-404/06/23 00:03104 1
Vinyl chloride ND ug/kg 04/11/23 02:42 75-01-404/06/23 00:0320.7 1
Xylene (Total)ND ug/kg 04/11/23 02:42 1330-20-704/06/23 00:0320.7 1
m&p-Xylene ND ug/kg 04/11/23 02:42 179601-23-104/06/23 00:0320.7 1
o-Xylene ND ug/kg 04/11/23 02:42 95-47-604/06/23 00:0310.4 1
Surrogates
Toluene-d8 (S)101 %04/11/23 02:42 2037-26-504/06/23 00:0370-130 1
4-Bromofluorobenzene (S)108 %04/11/23 02:42 460-00-404/06/23 00:0370-130 1
1,2-Dichloroethane-d4 (S)110 %04/11/23 02:42 17060-07-004/06/23 00:0370-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.7 %04/06/23 17:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
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Page 6 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 8 DRAIN, UNUSED
SUPPLY
Lab ID: 92660640002 Collected: 04/03/23 15:54 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/08/23 06:41 67-64-104/06/23 15:16159 1
Benzene ND ug/kg 04/08/23 06:41 71-43-204/06/23 15:167.9 1
Bromobenzene ND ug/kg 04/08/23 06:41 108-86-104/06/23 15:167.9 1
Bromochloromethane ND ug/kg 04/08/23 06:41 74-97-504/06/23 15:167.9 1
Bromodichloromethane ND ug/kg 04/08/23 06:41 75-27-404/06/23 15:167.9 1
Bromoform ND ug/kg 04/08/23 06:41 75-25-204/06/23 15:167.9 1
Bromomethane ND ug/kg 04/08/23 06:41 74-83-904/06/23 15:1631.8 1
2-Butanone (MEK)ND ug/kg 04/08/23 06:41 78-93-304/06/23 15:16159 1
n-Butylbenzene ND ug/kg 04/08/23 06:41 104-51-804/06/23 15:167.9 1
sec-Butylbenzene ND ug/kg 04/08/23 06:41 135-98-804/06/23 15:167.9 1
tert-Butylbenzene ND ug/kg 04/08/23 06:41 98-06-604/06/23 15:167.9 1
Carbon tetrachloride ND ug/kg 04/08/23 06:41 56-23-504/06/23 15:167.9 1
Chlorobenzene ND ug/kg 04/08/23 06:41 108-90-704/06/23 15:167.9 1
Chloroethane ND ug/kg 04/08/23 06:41 75-00-304/06/23 15:1615.9 1
Chloroform ND ug/kg 04/08/23 06:41 67-66-304/06/23 15:167.9 1
Chloromethane ND ug/kg 04/08/23 06:41 74-87-304/06/23 15:1615.9 1
2-Chlorotoluene ND ug/kg 04/08/23 06:41 95-49-804/06/23 15:167.9 1
4-Chlorotoluene ND ug/kg 04/08/23 06:41 106-43-404/06/23 15:167.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/08/23 06:41 96-12-804/06/23 15:167.9 1
Dibromochloromethane ND ug/kg 04/08/23 06:41 124-48-104/06/23 15:167.9 1
1,2-Dibromoethane (EDB)ND ug/kg 04/08/23 06:41 106-93-404/06/23 15:167.9 1
Dibromomethane ND ug/kg 04/08/23 06:41 74-95-304/06/23 15:167.9 1
1,2-Dichlorobenzene ND ug/kg 04/08/23 06:41 95-50-104/06/23 15:167.9 1
1,3-Dichlorobenzene ND ug/kg 04/08/23 06:41 541-73-104/06/23 15:167.9 1
1,4-Dichlorobenzene ND ug/kg 04/08/23 06:41 106-46-704/06/23 15:167.9 1
Dichlorodifluoromethane ND ug/kg 04/08/23 06:41 75-71-804/06/23 15:1615.9 1
1,1-Dichloroethane ND ug/kg 04/08/23 06:41 75-34-304/06/23 15:167.9 1
1,2-Dichloroethane ND ug/kg 04/08/23 06:41 107-06-204/06/23 15:167.9 1
1,1-Dichloroethene ND ug/kg 04/08/23 06:41 75-35-404/06/23 15:167.9 1
cis-1,2-Dichloroethene ND ug/kg 04/08/23 06:41 156-59-204/06/23 15:167.9 1
trans-1,2-Dichloroethene ND ug/kg 04/08/23 06:41 156-60-504/06/23 15:167.9 1
1,2-Dichloropropane ND ug/kg 04/08/23 06:41 78-87-504/06/23 15:167.9 1
1,3-Dichloropropane ND ug/kg 04/08/23 06:41 142-28-904/06/23 15:167.9 1
2,2-Dichloropropane ND ug/kg 04/08/23 06:41 594-20-704/06/23 15:167.9 1
1,1-Dichloropropene ND ug/kg 04/08/23 06:41 563-58-604/06/23 15:167.9 1
cis-1,3-Dichloropropene ND ug/kg 04/08/23 06:41 10061-01-504/06/23 15:167.9 1
trans-1,3-Dichloropropene ND ug/kg 04/08/23 06:41 10061-02-604/06/23 15:167.9 1
Diisopropyl ether ND ug/kg 04/08/23 06:41 108-20-304/06/23 15:167.9 1
Ethylbenzene ND ug/kg 04/08/23 06:41 100-41-404/06/23 15:167.9 1
Hexachloro-1,3-butadiene ND ug/kg 04/08/23 06:41 87-68-304/06/23 15:1615.9 1
2-Hexanone ND ug/kg 04/08/23 06:41 591-78-604/06/23 15:1679.4 1
Isopropylbenzene (Cumene)ND ug/kg 04/08/23 06:41 98-82-804/06/23 15:167.9 1
p-Isopropyltoluene ND ug/kg 04/08/23 06:41 99-87-604/06/23 15:167.9 1
Methylene Chloride 970 ug/kg 04/08/23 06:41 75-09-2 L204/06/23 15:1631.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 8 DRAIN, UNUSED
SUPPLY
Lab ID: 92660640002 Collected: 04/03/23 15:54 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/08/23 06:41 108-10-104/06/23 15:1679.4 1
Methyl-tert-butyl ether ND ug/kg 04/08/23 06:41 1634-04-404/06/23 15:167.9 1
Naphthalene ND ug/kg 04/08/23 06:41 91-20-304/06/23 15:167.9 1
n-Propylbenzene ND ug/kg 04/08/23 06:41 103-65-104/06/23 15:167.9 1
Styrene ND ug/kg 04/08/23 06:41 100-42-504/06/23 15:167.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/08/23 06:41 630-20-604/06/23 15:167.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/08/23 06:41 79-34-504/06/23 15:167.9 1
Tetrachloroethene ND ug/kg 04/08/23 06:41 127-18-404/06/23 15:167.9 1
Toluene ND ug/kg 04/08/23 06:41 108-88-304/06/23 15:167.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/08/23 06:41 87-61-604/06/23 15:167.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/08/23 06:41 120-82-104/06/23 15:167.9 1
1,1,1-Trichloroethane ND ug/kg 04/08/23 06:41 71-55-604/06/23 15:167.9 1
1,1,2-Trichloroethane ND ug/kg 04/08/23 06:41 79-00-504/06/23 15:167.9 1
Trichloroethene ND ug/kg 04/08/23 06:41 79-01-604/06/23 15:167.9 1
Trichlorofluoromethane ND ug/kg 04/08/23 06:41 75-69-404/06/23 15:167.9 1
1,2,3-Trichloropropane ND ug/kg 04/08/23 06:41 96-18-404/06/23 15:167.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/08/23 06:41 95-63-604/06/23 15:167.9 1
1,3,5-Trimethylbenzene ND ug/kg 04/08/23 06:41 108-67-804/06/23 15:167.9 1
Vinyl acetate ND ug/kg 04/08/23 06:41 108-05-404/06/23 15:1679.4 1
Vinyl chloride ND ug/kg 04/08/23 06:41 75-01-404/06/23 15:1615.9 1
Xylene (Total)ND ug/kg 04/08/23 06:41 1330-20-704/06/23 15:1615.9 1
m&p-Xylene ND ug/kg 04/08/23 06:41 179601-23-104/06/23 15:1615.9 1
o-Xylene ND ug/kg 04/08/23 06:41 95-47-604/06/23 15:167.9 1
Surrogates
Toluene-d8 (S)102 %04/08/23 06:41 2037-26-504/06/23 15:1670-130 1
4-Bromofluorobenzene (S)102 %04/08/23 06:41 460-00-404/06/23 15:1670-130 1
1,2-Dichloroethane-d4 (S)104 %04/08/23 06:41 17060-07-004/06/23 15:1670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.3 %04/06/23 17:54 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 2 SUPPLY Lab ID: 92660640003 Collected: 04/03/23 16:24 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/08/23 06:58 67-64-104/06/23 15:16298 1
Benzene ND ug/kg 04/08/23 06:58 71-43-204/06/23 15:1614.9 1
Bromobenzene ND ug/kg 04/08/23 06:58 108-86-104/06/23 15:1614.9 1
Bromochloromethane ND ug/kg 04/08/23 06:58 74-97-504/06/23 15:1614.9 1
Bromodichloromethane ND ug/kg 04/08/23 06:58 75-27-404/06/23 15:1614.9 1
Bromoform ND ug/kg 04/08/23 06:58 75-25-204/06/23 15:1614.9 1
Bromomethane ND ug/kg 04/08/23 06:58 74-83-904/06/23 15:1659.6 1
2-Butanone (MEK)ND ug/kg 04/08/23 06:58 78-93-304/06/23 15:16298 1
n-Butylbenzene ND ug/kg 04/08/23 06:58 104-51-804/06/23 15:1614.9 1
sec-Butylbenzene ND ug/kg 04/08/23 06:58 135-98-804/06/23 15:1614.9 1
tert-Butylbenzene ND ug/kg 04/08/23 06:58 98-06-604/06/23 15:1614.9 1
Carbon tetrachloride ND ug/kg 04/08/23 06:58 56-23-504/06/23 15:1614.9 1
Chlorobenzene ND ug/kg 04/08/23 06:58 108-90-704/06/23 15:1614.9 1
Chloroethane ND ug/kg 04/08/23 06:58 75-00-304/06/23 15:1629.8 1
Chloroform ND ug/kg 04/08/23 06:58 67-66-304/06/23 15:1614.9 1
Chloromethane ND ug/kg 04/08/23 06:58 74-87-304/06/23 15:1629.8 1
2-Chlorotoluene ND ug/kg 04/08/23 06:58 95-49-804/06/23 15:1614.9 1
4-Chlorotoluene ND ug/kg 04/08/23 06:58 106-43-404/06/23 15:1614.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/08/23 06:58 96-12-804/06/23 15:1614.9 1
Dibromochloromethane ND ug/kg 04/08/23 06:58 124-48-104/06/23 15:1614.9 1
1,2-Dibromoethane (EDB)ND ug/kg 04/08/23 06:58 106-93-404/06/23 15:1614.9 1
Dibromomethane ND ug/kg 04/08/23 06:58 74-95-304/06/23 15:1614.9 1
1,2-Dichlorobenzene ND ug/kg 04/08/23 06:58 95-50-104/06/23 15:1614.9 1
1,3-Dichlorobenzene ND ug/kg 04/08/23 06:58 541-73-104/06/23 15:1614.9 1
1,4-Dichlorobenzene ND ug/kg 04/08/23 06:58 106-46-704/06/23 15:1614.9 1
Dichlorodifluoromethane ND ug/kg 04/08/23 06:58 75-71-804/06/23 15:1629.8 1
1,1-Dichloroethane ND ug/kg 04/08/23 06:58 75-34-304/06/23 15:1614.9 1
1,2-Dichloroethane ND ug/kg 04/08/23 06:58 107-06-204/06/23 15:1614.9 1
1,1-Dichloroethene ND ug/kg 04/08/23 06:58 75-35-404/06/23 15:1614.9 1
cis-1,2-Dichloroethene ND ug/kg 04/08/23 06:58 156-59-204/06/23 15:1614.9 1
trans-1,2-Dichloroethene ND ug/kg 04/08/23 06:58 156-60-504/06/23 15:1614.9 1
1,2-Dichloropropane ND ug/kg 04/08/23 06:58 78-87-504/06/23 15:1614.9 1
1,3-Dichloropropane ND ug/kg 04/08/23 06:58 142-28-904/06/23 15:1614.9 1
2,2-Dichloropropane ND ug/kg 04/08/23 06:58 594-20-704/06/23 15:1614.9 1
1,1-Dichloropropene ND ug/kg 04/08/23 06:58 563-58-604/06/23 15:1614.9 1
cis-1,3-Dichloropropene ND ug/kg 04/08/23 06:58 10061-01-504/06/23 15:1614.9 1
trans-1,3-Dichloropropene ND ug/kg 04/08/23 06:58 10061-02-604/06/23 15:1614.9 1
Diisopropyl ether ND ug/kg 04/08/23 06:58 108-20-304/06/23 15:1614.9 1
Ethylbenzene ND ug/kg 04/08/23 06:58 100-41-404/06/23 15:1614.9 1
Hexachloro-1,3-butadiene ND ug/kg 04/08/23 06:58 87-68-304/06/23 15:1629.8 1
2-Hexanone ND ug/kg 04/08/23 06:58 591-78-604/06/23 15:16149 1
Isopropylbenzene (Cumene)ND ug/kg 04/08/23 06:58 98-82-804/06/23 15:1614.9 1
p-Isopropyltoluene ND ug/kg 04/08/23 06:58 99-87-604/06/23 15:1614.9 1
Methylene Chloride 1210 ug/kg 04/08/23 06:58 75-09-2 L204/06/23 15:1659.6 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/08/23 06:58 108-10-104/06/23 15:16149 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 2 SUPPLY Lab ID: 92660640003 Collected: 04/03/23 16:24 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 04/08/23 06:58 1634-04-404/06/23 15:1614.9 1
Naphthalene ND ug/kg 04/08/23 06:58 91-20-304/06/23 15:1614.9 1
n-Propylbenzene ND ug/kg 04/08/23 06:58 103-65-104/06/23 15:1614.9 1
Styrene ND ug/kg 04/08/23 06:58 100-42-504/06/23 15:1614.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/08/23 06:58 630-20-604/06/23 15:1614.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/08/23 06:58 79-34-504/06/23 15:1614.9 1
Tetrachloroethene ND ug/kg 04/08/23 06:58 127-18-404/06/23 15:1614.9 1
Toluene ND ug/kg 04/08/23 06:58 108-88-304/06/23 15:1614.9 1
1,2,3-Trichlorobenzene ND ug/kg 04/08/23 06:58 87-61-604/06/23 15:1614.9 1
1,2,4-Trichlorobenzene ND ug/kg 04/08/23 06:58 120-82-104/06/23 15:1614.9 1
1,1,1-Trichloroethane ND ug/kg 04/08/23 06:58 71-55-604/06/23 15:1614.9 1
1,1,2-Trichloroethane ND ug/kg 04/08/23 06:58 79-00-504/06/23 15:1614.9 1
Trichloroethene ND ug/kg 04/08/23 06:58 79-01-604/06/23 15:1614.9 1
Trichlorofluoromethane ND ug/kg 04/08/23 06:58 75-69-404/06/23 15:1614.9 1
1,2,3-Trichloropropane ND ug/kg 04/08/23 06:58 96-18-404/06/23 15:1614.9 1
1,2,4-Trimethylbenzene ND ug/kg 04/08/23 06:58 95-63-604/06/23 15:1614.9 1
1,3,5-Trimethylbenzene ND ug/kg 04/08/23 06:58 108-67-804/06/23 15:1614.9 1
Vinyl acetate ND ug/kg 04/08/23 06:58 108-05-404/06/23 15:16149 1
Vinyl chloride ND ug/kg 04/08/23 06:58 75-01-404/06/23 15:1629.8 1
Xylene (Total)ND ug/kg 04/08/23 06:58 1330-20-704/06/23 15:1629.8 1
m&p-Xylene ND ug/kg 04/08/23 06:58 179601-23-104/06/23 15:1629.8 1
o-Xylene ND ug/kg 04/08/23 06:58 95-47-604/06/23 15:1614.9 1
Surrogates
Toluene-d8 (S)100 %04/08/23 06:58 2037-26-504/06/23 15:1670-130 1
4-Bromofluorobenzene (S)106 %04/08/23 06:58 460-00-404/06/23 15:1670-130 1
1,2-Dichloroethane-d4 (S)104 %04/08/23 06:58 17060-07-004/06/23 15:1670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 19.3 %04/06/23 17:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: MAIN LINE COOLENT UNIT Lab ID: 92660640004 Collected: 04/03/23 16:41 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/08/23 14:58 67-64-104/06/23 15:167820 50
Benzene ND ug/kg 04/08/23 14:58 71-43-204/06/23 15:16391 50
Bromobenzene ND ug/kg 04/08/23 14:58 108-86-104/06/23 15:16391 50
Bromochloromethane ND ug/kg 04/08/23 14:58 74-97-504/06/23 15:16391 50
Bromodichloromethane ND ug/kg 04/08/23 14:58 75-27-404/06/23 15:16391 50
Bromoform ND ug/kg 04/08/23 14:58 75-25-204/06/23 15:16391 50
Bromomethane ND ug/kg 04/08/23 14:58 74-83-904/06/23 15:161560 50
2-Butanone (MEK)ND ug/kg 04/08/23 14:58 78-93-304/06/23 15:167820 50
n-Butylbenzene ND ug/kg 04/08/23 14:58 104-51-804/06/23 15:16391 50
sec-Butylbenzene 4420 ug/kg 04/08/23 14:58 135-98-804/06/23 15:16391 50
tert-Butylbenzene ND ug/kg 04/08/23 14:58 98-06-604/06/23 15:16391 50
Carbon tetrachloride ND ug/kg 04/08/23 14:58 56-23-504/06/23 15:16391 50
Chlorobenzene ND ug/kg 04/08/23 14:58 108-90-704/06/23 15:16391 50
Chloroethane ND ug/kg 04/08/23 14:58 75-00-304/06/23 15:16782 50
Chloroform ND ug/kg 04/08/23 14:58 67-66-304/06/23 15:16391 50
Chloromethane ND ug/kg 04/08/23 14:58 74-87-304/06/23 15:16782 50
2-Chlorotoluene ND ug/kg 04/08/23 14:58 95-49-804/06/23 15:16391 50
4-Chlorotoluene ND ug/kg 04/08/23 14:58 106-43-404/06/23 15:16391 50
1,2-Dibromo-3-chloropropane ND ug/kg 04/08/23 14:58 96-12-804/06/23 15:16391 50
Dibromochloromethane ND ug/kg 04/08/23 14:58 124-48-104/06/23 15:16391 50
1,2-Dibromoethane (EDB)ND ug/kg 04/08/23 14:58 106-93-404/06/23 15:16391 50
Dibromomethane ND ug/kg 04/08/23 14:58 74-95-304/06/23 15:16391 50
1,2-Dichlorobenzene ND ug/kg 04/08/23 14:58 95-50-104/06/23 15:16391 50
1,3-Dichlorobenzene ND ug/kg 04/08/23 14:58 541-73-104/06/23 15:16391 50
1,4-Dichlorobenzene ND ug/kg 04/08/23 14:58 106-46-704/06/23 15:16391 50
Dichlorodifluoromethane ND ug/kg 04/08/23 14:58 75-71-804/06/23 15:16782 50
1,1-Dichloroethane ND ug/kg 04/08/23 14:58 75-34-304/06/23 15:16391 50
1,2-Dichloroethane ND ug/kg 04/08/23 14:58 107-06-204/06/23 15:16391 50
1,1-Dichloroethene ND ug/kg 04/08/23 14:58 75-35-404/06/23 15:16391 50
cis-1,2-Dichloroethene ND ug/kg 04/08/23 14:58 156-59-204/06/23 15:16391 50
trans-1,2-Dichloroethene ND ug/kg 04/08/23 14:58 156-60-504/06/23 15:16391 50
1,2-Dichloropropane ND ug/kg 04/08/23 14:58 78-87-504/06/23 15:16391 50
1,3-Dichloropropane ND ug/kg 04/08/23 14:58 142-28-904/06/23 15:16391 50
2,2-Dichloropropane ND ug/kg 04/08/23 14:58 594-20-704/06/23 15:16391 50
1,1-Dichloropropene ND ug/kg 04/08/23 14:58 563-58-604/06/23 15:16391 50
cis-1,3-Dichloropropene ND ug/kg 04/08/23 14:58 10061-01-504/06/23 15:16391 50
trans-1,3-Dichloropropene ND ug/kg 04/08/23 14:58 10061-02-604/06/23 15:16391 50
Diisopropyl ether ND ug/kg 04/08/23 14:58 108-20-304/06/23 15:16391 50
Ethylbenzene ND ug/kg 04/08/23 14:58 100-41-404/06/23 15:16391 50
Hexachloro-1,3-butadiene ND ug/kg 04/08/23 14:58 87-68-304/06/23 15:16782 50
2-Hexanone ND ug/kg 04/08/23 14:58 591-78-604/06/23 15:163910 50
Isopropylbenzene (Cumene)645 ug/kg 04/08/23 14:58 98-82-804/06/23 15:16391 50
p-Isopropyltoluene 5570 ug/kg 04/08/23 14:58 99-87-604/06/23 15:16391 50
Methylene Chloride ND ug/kg 04/08/23 14:58 75-09-2 L204/06/23 15:161560 50
4-Methyl-2-pentanone (MIBK)4600 ug/kg 04/08/23 14:58 108-10-104/06/23 15:163910 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: MAIN LINE COOLENT UNIT Lab ID: 92660640004 Collected: 04/03/23 16:41 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 04/08/23 14:58 1634-04-404/06/23 15:16391 50
Naphthalene ND ug/kg 04/08/23 14:58 91-20-304/06/23 15:16391 50
n-Propylbenzene ND ug/kg 04/08/23 14:58 103-65-104/06/23 15:16391 50
Styrene ND ug/kg 04/08/23 14:58 100-42-504/06/23 15:16391 50
1,1,1,2-Tetrachloroethane ND ug/kg 04/08/23 14:58 630-20-604/06/23 15:16391 50
1,1,2,2-Tetrachloroethane ND ug/kg 04/08/23 14:58 79-34-504/06/23 15:16391 50
Tetrachloroethene ND ug/kg 04/08/23 14:58 127-18-404/06/23 15:16391 50
Toluene ND ug/kg 04/08/23 14:58 108-88-304/06/23 15:16391 50
1,2,3-Trichlorobenzene ND ug/kg 04/08/23 14:58 87-61-604/06/23 15:16391 50
1,2,4-Trichlorobenzene ND ug/kg 04/08/23 14:58 120-82-104/06/23 15:16391 50
1,1,1-Trichloroethane ND ug/kg 04/08/23 14:58 71-55-604/06/23 15:16391 50
1,1,2-Trichloroethane ND ug/kg 04/08/23 14:58 79-00-504/06/23 15:16391 50
Trichloroethene ND ug/kg 04/08/23 14:58 79-01-604/06/23 15:16391 50
Trichlorofluoromethane ND ug/kg 04/08/23 14:58 75-69-404/06/23 15:16391 50
1,2,3-Trichloropropane ND ug/kg 04/08/23 14:58 96-18-404/06/23 15:16391 50
1,2,4-Trimethylbenzene 7850 ug/kg 04/08/23 14:58 95-63-604/06/23 15:16391 50
1,3,5-Trimethylbenzene 6210 ug/kg 04/08/23 14:58 108-67-804/06/23 15:16391 50
Vinyl acetate ND ug/kg 04/08/23 14:58 108-05-404/06/23 15:163910 50
Vinyl chloride ND ug/kg 04/08/23 14:58 75-01-404/06/23 15:16782 50
Xylene (Total)ND ug/kg 04/08/23 14:58 1330-20-704/06/23 15:16782 50
m&p-Xylene ND ug/kg 04/08/23 14:58 179601-23-104/06/23 15:16782 50
o-Xylene ND ug/kg 04/08/23 14:58 95-47-604/06/23 15:16391 50
Surrogates
Toluene-d8 (S)102 %04/08/23 14:58 2037-26-504/06/23 15:1670-130 50
4-Bromofluorobenzene (S)133 %04/08/23 14:58 460-00-4 S004/06/23 15:1670-130 50
1,2-Dichloroethane-d4 (S)108 %04/08/23 14:58 17060-07-004/06/23 15:1670-130 50
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10.5 %04/06/23 17:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: MAINLINE DRAIN TO 7 Lab ID: 92660640005 Collected: 04/03/23 16:57 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/08/23 07:34 67-64-104/06/23 15:16260 1
Benzene ND ug/kg 04/08/23 07:34 71-43-204/06/23 15:1613.0 1
Bromobenzene ND ug/kg 04/08/23 07:34 108-86-104/06/23 15:1613.0 1
Bromochloromethane ND ug/kg 04/08/23 07:34 74-97-504/06/23 15:1613.0 1
Bromodichloromethane ND ug/kg 04/08/23 07:34 75-27-404/06/23 15:1613.0 1
Bromoform ND ug/kg 04/08/23 07:34 75-25-204/06/23 15:1613.0 1
Bromomethane ND ug/kg 04/08/23 07:34 74-83-904/06/23 15:1651.9 1
2-Butanone (MEK)ND ug/kg 04/08/23 07:34 78-93-304/06/23 15:16260 1
n-Butylbenzene ND ug/kg 04/08/23 07:34 104-51-804/06/23 15:1613.0 1
sec-Butylbenzene ND ug/kg 04/08/23 07:34 135-98-804/06/23 15:1613.0 1
tert-Butylbenzene ND ug/kg 04/08/23 07:34 98-06-604/06/23 15:1613.0 1
Carbon tetrachloride ND ug/kg 04/08/23 07:34 56-23-504/06/23 15:1613.0 1
Chlorobenzene ND ug/kg 04/08/23 07:34 108-90-704/06/23 15:1613.0 1
Chloroethane ND ug/kg 04/08/23 07:34 75-00-304/06/23 15:1626.0 1
Chloroform ND ug/kg 04/08/23 07:34 67-66-304/06/23 15:1613.0 1
Chloromethane ND ug/kg 04/08/23 07:34 74-87-304/06/23 15:1626.0 1
2-Chlorotoluene ND ug/kg 04/08/23 07:34 95-49-804/06/23 15:1613.0 1
4-Chlorotoluene ND ug/kg 04/08/23 07:34 106-43-404/06/23 15:1613.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/08/23 07:34 96-12-804/06/23 15:1613.0 1
Dibromochloromethane ND ug/kg 04/08/23 07:34 124-48-104/06/23 15:1613.0 1
1,2-Dibromoethane (EDB)ND ug/kg 04/08/23 07:34 106-93-404/06/23 15:1613.0 1
Dibromomethane ND ug/kg 04/08/23 07:34 74-95-304/06/23 15:1613.0 1
1,2-Dichlorobenzene ND ug/kg 04/08/23 07:34 95-50-104/06/23 15:1613.0 1
1,3-Dichlorobenzene ND ug/kg 04/08/23 07:34 541-73-104/06/23 15:1613.0 1
1,4-Dichlorobenzene ND ug/kg 04/08/23 07:34 106-46-704/06/23 15:1613.0 1
Dichlorodifluoromethane ND ug/kg 04/08/23 07:34 75-71-804/06/23 15:1626.0 1
1,1-Dichloroethane ND ug/kg 04/08/23 07:34 75-34-304/06/23 15:1613.0 1
1,2-Dichloroethane ND ug/kg 04/08/23 07:34 107-06-204/06/23 15:1613.0 1
1,1-Dichloroethene ND ug/kg 04/08/23 07:34 75-35-404/06/23 15:1613.0 1
cis-1,2-Dichloroethene ND ug/kg 04/08/23 07:34 156-59-204/06/23 15:1613.0 1
trans-1,2-Dichloroethene ND ug/kg 04/08/23 07:34 156-60-504/06/23 15:1613.0 1
1,2-Dichloropropane ND ug/kg 04/08/23 07:34 78-87-504/06/23 15:1613.0 1
1,3-Dichloropropane ND ug/kg 04/08/23 07:34 142-28-904/06/23 15:1613.0 1
2,2-Dichloropropane ND ug/kg 04/08/23 07:34 594-20-704/06/23 15:1613.0 1
1,1-Dichloropropene ND ug/kg 04/08/23 07:34 563-58-604/06/23 15:1613.0 1
cis-1,3-Dichloropropene ND ug/kg 04/08/23 07:34 10061-01-504/06/23 15:1613.0 1
trans-1,3-Dichloropropene ND ug/kg 04/08/23 07:34 10061-02-604/06/23 15:1613.0 1
Diisopropyl ether ND ug/kg 04/08/23 07:34 108-20-304/06/23 15:1613.0 1
Ethylbenzene ND ug/kg 04/08/23 07:34 100-41-404/06/23 15:1613.0 1
Hexachloro-1,3-butadiene ND ug/kg 04/08/23 07:34 87-68-304/06/23 15:1626.0 1
2-Hexanone ND ug/kg 04/08/23 07:34 591-78-604/06/23 15:16130 1
Isopropylbenzene (Cumene)ND ug/kg 04/08/23 07:34 98-82-804/06/23 15:1613.0 1
p-Isopropyltoluene ND ug/kg 04/08/23 07:34 99-87-604/06/23 15:1613.0 1
Methylene Chloride 423 ug/kg 04/08/23 07:34 75-09-2 L204/06/23 15:1651.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/08/23 07:34 108-10-104/06/23 15:16130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: MAINLINE DRAIN TO 7 Lab ID: 92660640005 Collected: 04/03/23 16:57 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Methyl-tert-butyl ether ND ug/kg 04/08/23 07:34 1634-04-404/06/23 15:1613.0 1
Naphthalene ND ug/kg 04/08/23 07:34 91-20-304/06/23 15:1613.0 1
n-Propylbenzene ND ug/kg 04/08/23 07:34 103-65-104/06/23 15:1613.0 1
Styrene ND ug/kg 04/08/23 07:34 100-42-504/06/23 15:1613.0 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/08/23 07:34 630-20-604/06/23 15:1613.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/08/23 07:34 79-34-504/06/23 15:1613.0 1
Tetrachloroethene ND ug/kg 04/08/23 07:34 127-18-404/06/23 15:1613.0 1
Toluene ND ug/kg 04/08/23 07:34 108-88-304/06/23 15:1613.0 1
1,2,3-Trichlorobenzene ND ug/kg 04/08/23 07:34 87-61-604/06/23 15:1613.0 1
1,2,4-Trichlorobenzene ND ug/kg 04/08/23 07:34 120-82-104/06/23 15:1613.0 1
1,1,1-Trichloroethane ND ug/kg 04/08/23 07:34 71-55-604/06/23 15:1613.0 1
1,1,2-Trichloroethane ND ug/kg 04/08/23 07:34 79-00-504/06/23 15:1613.0 1
Trichloroethene ND ug/kg 04/08/23 07:34 79-01-604/06/23 15:1613.0 1
Trichlorofluoromethane ND ug/kg 04/08/23 07:34 75-69-404/06/23 15:1613.0 1
1,2,3-Trichloropropane ND ug/kg 04/08/23 07:34 96-18-404/06/23 15:1613.0 1
1,2,4-Trimethylbenzene ND ug/kg 04/08/23 07:34 95-63-604/06/23 15:1613.0 1
1,3,5-Trimethylbenzene ND ug/kg 04/08/23 07:34 108-67-804/06/23 15:1613.0 1
Vinyl acetate ND ug/kg 04/08/23 07:34 108-05-404/06/23 15:16130 1
Vinyl chloride ND ug/kg 04/08/23 07:34 75-01-404/06/23 15:1626.0 1
Xylene (Total)ND ug/kg 04/08/23 07:34 1330-20-704/06/23 15:1626.0 1
m&p-Xylene ND ug/kg 04/08/23 07:34 179601-23-104/06/23 15:1626.0 1
o-Xylene 16.6 ug/kg 04/08/23 07:34 95-47-604/06/23 15:1613.0 1
Surrogates
Toluene-d8 (S)102 %04/08/23 07:34 2037-26-504/06/23 15:1670-130 1
4-Bromofluorobenzene (S)104 %04/08/23 07:34 460-00-404/06/23 15:1670-130 1
1,2-Dichloroethane-d4 (S)108 %04/08/23 07:34 17060-07-004/06/23 15:1670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 20.0 %04/06/23 17:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 4/6 SUPPLY AND
DRAIN
Lab ID: 92660640006 Collected: 04/04/23 08:17 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 252 ug/kg 04/08/23 07:52 67-64-104/06/23 15:16150 1
Benzene ND ug/kg 04/08/23 07:52 71-43-204/06/23 15:167.5 1
Bromobenzene ND ug/kg 04/08/23 07:52 108-86-104/06/23 15:167.5 1
Bromochloromethane ND ug/kg 04/08/23 07:52 74-97-504/06/23 15:167.5 1
Bromodichloromethane ND ug/kg 04/08/23 07:52 75-27-404/06/23 15:167.5 1
Bromoform ND ug/kg 04/08/23 07:52 75-25-204/06/23 15:167.5 1
Bromomethane ND ug/kg 04/08/23 07:52 74-83-904/06/23 15:1630.0 1
2-Butanone (MEK)ND ug/kg 04/08/23 07:52 78-93-304/06/23 15:16150 1
n-Butylbenzene ND ug/kg 04/08/23 07:52 104-51-804/06/23 15:167.5 1
sec-Butylbenzene ND ug/kg 04/08/23 07:52 135-98-804/06/23 15:167.5 1
tert-Butylbenzene ND ug/kg 04/08/23 07:52 98-06-604/06/23 15:167.5 1
Carbon tetrachloride ND ug/kg 04/08/23 07:52 56-23-504/06/23 15:167.5 1
Chlorobenzene ND ug/kg 04/08/23 07:52 108-90-704/06/23 15:167.5 1
Chloroethane ND ug/kg 04/08/23 07:52 75-00-304/06/23 15:1615.0 1
Chloroform ND ug/kg 04/08/23 07:52 67-66-304/06/23 15:167.5 1
Chloromethane ND ug/kg 04/08/23 07:52 74-87-304/06/23 15:1615.0 1
2-Chlorotoluene ND ug/kg 04/08/23 07:52 95-49-804/06/23 15:167.5 1
4-Chlorotoluene ND ug/kg 04/08/23 07:52 106-43-404/06/23 15:167.5 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/08/23 07:52 96-12-804/06/23 15:167.5 1
Dibromochloromethane ND ug/kg 04/08/23 07:52 124-48-104/06/23 15:167.5 1
1,2-Dibromoethane (EDB)ND ug/kg 04/08/23 07:52 106-93-404/06/23 15:167.5 1
Dibromomethane ND ug/kg 04/08/23 07:52 74-95-304/06/23 15:167.5 1
1,2-Dichlorobenzene ND ug/kg 04/08/23 07:52 95-50-104/06/23 15:167.5 1
1,3-Dichlorobenzene ND ug/kg 04/08/23 07:52 541-73-104/06/23 15:167.5 1
1,4-Dichlorobenzene ND ug/kg 04/08/23 07:52 106-46-704/06/23 15:167.5 1
Dichlorodifluoromethane ND ug/kg 04/08/23 07:52 75-71-804/06/23 15:1615.0 1
1,1-Dichloroethane ND ug/kg 04/08/23 07:52 75-34-304/06/23 15:167.5 1
1,2-Dichloroethane ND ug/kg 04/08/23 07:52 107-06-204/06/23 15:167.5 1
1,1-Dichloroethene ND ug/kg 04/08/23 07:52 75-35-404/06/23 15:167.5 1
cis-1,2-Dichloroethene ND ug/kg 04/08/23 07:52 156-59-204/06/23 15:167.5 1
trans-1,2-Dichloroethene ND ug/kg 04/08/23 07:52 156-60-504/06/23 15:167.5 1
1,2-Dichloropropane ND ug/kg 04/08/23 07:52 78-87-504/06/23 15:167.5 1
1,3-Dichloropropane ND ug/kg 04/08/23 07:52 142-28-904/06/23 15:167.5 1
2,2-Dichloropropane ND ug/kg 04/08/23 07:52 594-20-704/06/23 15:167.5 1
1,1-Dichloropropene ND ug/kg 04/08/23 07:52 563-58-604/06/23 15:167.5 1
cis-1,3-Dichloropropene ND ug/kg 04/08/23 07:52 10061-01-504/06/23 15:167.5 1
trans-1,3-Dichloropropene ND ug/kg 04/08/23 07:52 10061-02-604/06/23 15:167.5 1
Diisopropyl ether ND ug/kg 04/08/23 07:52 108-20-304/06/23 15:167.5 1
Ethylbenzene ND ug/kg 04/08/23 07:52 100-41-404/06/23 15:167.5 1
Hexachloro-1,3-butadiene ND ug/kg 04/08/23 07:52 87-68-304/06/23 15:1615.0 1
2-Hexanone ND ug/kg 04/08/23 07:52 591-78-604/06/23 15:1675.0 1
Isopropylbenzene (Cumene)ND ug/kg 04/08/23 07:52 98-82-804/06/23 15:167.5 1
p-Isopropyltoluene ND ug/kg 04/08/23 07:52 99-87-604/06/23 15:167.5 1
Methylene Chloride 234 ug/kg 04/08/23 07:52 75-09-2 L204/06/23 15:1630.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 4/6 SUPPLY AND
DRAIN
Lab ID: 92660640006 Collected: 04/04/23 08:17 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/08/23 07:52 108-10-104/06/23 15:1675.0 1
Methyl-tert-butyl ether ND ug/kg 04/08/23 07:52 1634-04-404/06/23 15:167.5 1
Naphthalene ND ug/kg 04/08/23 07:52 91-20-304/06/23 15:167.5 1
n-Propylbenzene ND ug/kg 04/08/23 07:52 103-65-104/06/23 15:167.5 1
Styrene ND ug/kg 04/08/23 07:52 100-42-504/06/23 15:167.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/08/23 07:52 630-20-604/06/23 15:167.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/08/23 07:52 79-34-504/06/23 15:167.5 1
Tetrachloroethene ND ug/kg 04/08/23 07:52 127-18-404/06/23 15:167.5 1
Toluene ND ug/kg 04/08/23 07:52 108-88-304/06/23 15:167.5 1
1,2,3-Trichlorobenzene ND ug/kg 04/08/23 07:52 87-61-604/06/23 15:167.5 1
1,2,4-Trichlorobenzene ND ug/kg 04/08/23 07:52 120-82-104/06/23 15:167.5 1
1,1,1-Trichloroethane ND ug/kg 04/08/23 07:52 71-55-604/06/23 15:167.5 1
1,1,2-Trichloroethane ND ug/kg 04/08/23 07:52 79-00-504/06/23 15:167.5 1
Trichloroethene ND ug/kg 04/08/23 07:52 79-01-604/06/23 15:167.5 1
Trichlorofluoromethane ND ug/kg 04/08/23 07:52 75-69-404/06/23 15:167.5 1
1,2,3-Trichloropropane ND ug/kg 04/08/23 07:52 96-18-404/06/23 15:167.5 1
1,2,4-Trimethylbenzene ND ug/kg 04/08/23 07:52 95-63-604/06/23 15:167.5 1
1,3,5-Trimethylbenzene ND ug/kg 04/08/23 07:52 108-67-804/06/23 15:167.5 1
Vinyl acetate ND ug/kg 04/08/23 07:52 108-05-404/06/23 15:1675.0 1
Vinyl chloride ND ug/kg 04/08/23 07:52 75-01-404/06/23 15:1615.0 1
Xylene (Total)ND ug/kg 04/08/23 07:52 1330-20-704/06/23 15:1615.0 1
m&p-Xylene ND ug/kg 04/08/23 07:52 179601-23-104/06/23 15:1615.0 1
o-Xylene ND ug/kg 04/08/23 07:52 95-47-604/06/23 15:167.5 1
Surrogates
Toluene-d8 (S)102 %04/08/23 07:52 2037-26-504/06/23 15:1670-130 1
4-Bromofluorobenzene (S)104 %04/08/23 07:52 460-00-404/06/23 15:1670-130 1
1,2-Dichloroethane-d4 (S)105 %04/08/23 07:52 17060-07-004/06/23 15:1670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 10 %04/06/23 17:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 4/6 MAINLINE
SUPPLY AND D
Lab ID: 92660640007 Collected: 04/04/23 08:57 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/08/23 08:09 67-64-104/06/23 15:16163 1
Benzene ND ug/kg 04/08/23 08:09 71-43-204/06/23 15:168.1 1
Bromobenzene ND ug/kg 04/08/23 08:09 108-86-104/06/23 15:168.1 1
Bromochloromethane ND ug/kg 04/08/23 08:09 74-97-504/06/23 15:168.1 1
Bromodichloromethane ND ug/kg 04/08/23 08:09 75-27-404/06/23 15:168.1 1
Bromoform ND ug/kg 04/08/23 08:09 75-25-204/06/23 15:168.1 1
Bromomethane ND ug/kg 04/08/23 08:09 74-83-904/06/23 15:1632.5 1
2-Butanone (MEK)ND ug/kg 04/08/23 08:09 78-93-304/06/23 15:16163 1
n-Butylbenzene ND ug/kg 04/08/23 08:09 104-51-804/06/23 15:168.1 1
sec-Butylbenzene ND ug/kg 04/08/23 08:09 135-98-804/06/23 15:168.1 1
tert-Butylbenzene ND ug/kg 04/08/23 08:09 98-06-604/06/23 15:168.1 1
Carbon tetrachloride ND ug/kg 04/08/23 08:09 56-23-504/06/23 15:168.1 1
Chlorobenzene ND ug/kg 04/08/23 08:09 108-90-704/06/23 15:168.1 1
Chloroethane ND ug/kg 04/08/23 08:09 75-00-304/06/23 15:1616.3 1
Chloroform ND ug/kg 04/08/23 08:09 67-66-304/06/23 15:168.1 1
Chloromethane ND ug/kg 04/08/23 08:09 74-87-304/06/23 15:1616.3 1
2-Chlorotoluene ND ug/kg 04/08/23 08:09 95-49-804/06/23 15:168.1 1
4-Chlorotoluene ND ug/kg 04/08/23 08:09 106-43-404/06/23 15:168.1 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/08/23 08:09 96-12-804/06/23 15:168.1 1
Dibromochloromethane ND ug/kg 04/08/23 08:09 124-48-104/06/23 15:168.1 1
1,2-Dibromoethane (EDB)ND ug/kg 04/08/23 08:09 106-93-404/06/23 15:168.1 1
Dibromomethane ND ug/kg 04/08/23 08:09 74-95-304/06/23 15:168.1 1
1,2-Dichlorobenzene ND ug/kg 04/08/23 08:09 95-50-104/06/23 15:168.1 1
1,3-Dichlorobenzene ND ug/kg 04/08/23 08:09 541-73-104/06/23 15:168.1 1
1,4-Dichlorobenzene ND ug/kg 04/08/23 08:09 106-46-704/06/23 15:168.1 1
Dichlorodifluoromethane ND ug/kg 04/08/23 08:09 75-71-804/06/23 15:1616.3 1
1,1-Dichloroethane ND ug/kg 04/08/23 08:09 75-34-304/06/23 15:168.1 1
1,2-Dichloroethane ND ug/kg 04/08/23 08:09 107-06-204/06/23 15:168.1 1
1,1-Dichloroethene ND ug/kg 04/08/23 08:09 75-35-404/06/23 15:168.1 1
cis-1,2-Dichloroethene ND ug/kg 04/08/23 08:09 156-59-204/06/23 15:168.1 1
trans-1,2-Dichloroethene ND ug/kg 04/08/23 08:09 156-60-504/06/23 15:168.1 1
1,2-Dichloropropane ND ug/kg 04/08/23 08:09 78-87-504/06/23 15:168.1 1
1,3-Dichloropropane ND ug/kg 04/08/23 08:09 142-28-904/06/23 15:168.1 1
2,2-Dichloropropane ND ug/kg 04/08/23 08:09 594-20-704/06/23 15:168.1 1
1,1-Dichloropropene ND ug/kg 04/08/23 08:09 563-58-604/06/23 15:168.1 1
cis-1,3-Dichloropropene ND ug/kg 04/08/23 08:09 10061-01-504/06/23 15:168.1 1
trans-1,3-Dichloropropene ND ug/kg 04/08/23 08:09 10061-02-604/06/23 15:168.1 1
Diisopropyl ether ND ug/kg 04/08/23 08:09 108-20-304/06/23 15:168.1 1
Ethylbenzene ND ug/kg 04/08/23 08:09 100-41-404/06/23 15:168.1 1
Hexachloro-1,3-butadiene ND ug/kg 04/08/23 08:09 87-68-304/06/23 15:1616.3 1
2-Hexanone ND ug/kg 04/08/23 08:09 591-78-604/06/23 15:1681.3 1
Isopropylbenzene (Cumene)ND ug/kg 04/08/23 08:09 98-82-804/06/23 15:168.1 1
p-Isopropyltoluene ND ug/kg 04/08/23 08:09 99-87-604/06/23 15:168.1 1
Methylene Chloride 253 ug/kg 04/08/23 08:09 75-09-2 L204/06/23 15:1632.5 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 38
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92660640
GILBARRO
Sample: UNIT 4/6 MAINLINE
SUPPLY AND D
Lab ID: 92660640007 Collected: 04/04/23 08:57 Received: 04/05/23 09:35 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/08/23 08:09 108-10-104/06/23 15:1681.3 1
Methyl-tert-butyl ether ND ug/kg 04/08/23 08:09 1634-04-404/06/23 15:168.1 1
Naphthalene ND ug/kg 04/08/23 08:09 91-20-304/06/23 15:168.1 1
n-Propylbenzene ND ug/kg 04/08/23 08:09 103-65-104/06/23 15:168.1 1
Styrene ND ug/kg 04/08/23 08:09 100-42-504/06/23 15:168.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/08/23 08:09 630-20-604/06/23 15:168.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/08/23 08:09 79-34-504/06/23 15:168.1 1
Tetrachloroethene ND ug/kg 04/08/23 08:09 127-18-404/06/23 15:168.1 1
Toluene ND ug/kg 04/08/23 08:09 108-88-304/06/23 15:168.1 1
1,2,3-Trichlorobenzene ND ug/kg 04/08/23 08:09 87-61-604/06/23 15:168.1 1
1,2,4-Trichlorobenzene ND ug/kg 04/08/23 08:09 120-82-104/06/23 15:168.1 1
1,1,1-Trichloroethane ND ug/kg 04/08/23 08:09 71-55-604/06/23 15:168.1 1
1,1,2-Trichloroethane ND ug/kg 04/08/23 08:09 79-00-504/06/23 15:168.1 1
Trichloroethene ND ug/kg 04/08/23 08:09 79-01-604/06/23 15:168.1 1
Trichlorofluoromethane ND ug/kg 04/08/23 08:09 75-69-404/06/23 15:168.1 1
1,2,3-Trichloropropane ND ug/kg 04/08/23 08:09 96-18-404/06/23 15:168.1 1
1,2,4-Trimethylbenzene ND ug/kg 04/08/23 08:09 95-63-604/06/23 15:168.1 1
1,3,5-Trimethylbenzene ND ug/kg 04/08/23 08:09 108-67-804/06/23 15:168.1 1
Vinyl acetate ND ug/kg 04/08/23 08:09 108-05-404/06/23 15:1681.3 1
Vinyl chloride ND ug/kg 04/08/23 08:09 75-01-404/06/23 15:1616.3 1
Xylene (Total)ND ug/kg 04/08/23 08:09 1330-20-704/06/23 15:1616.3 1
m&p-Xylene ND ug/kg 04/08/23 08:09 179601-23-104/06/23 15:1616.3 1
o-Xylene ND ug/kg 04/08/23 08:09 95-47-604/06/23 15:168.1 1
Surrogates
Toluene-d8 (S)100 %04/08/23 08:09 2037-26-504/06/23 15:1670-130 1
4-Bromofluorobenzene (S)105 %04/08/23 08:09 460-00-404/06/23 15:1670-130 1
1,2-Dichloroethane-d4 (S)106 %04/08/23 08:09 17060-07-004/06/23 15:1670-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 17.6 %04/06/23 17:55 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
766285
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92660640001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3978911
Associated Lab Samples:92660640001
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/11/23 01:14
1,1,1-Trichloroethane ug/kg ND 5.0 04/11/23 01:14
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/11/23 01:14
1,1,2-Trichloroethane ug/kg ND 5.0 04/11/23 01:14
1,1-Dichloroethane ug/kg ND 5.0 04/11/23 01:14
1,1-Dichloroethene ug/kg ND 5.0 04/11/23 01:14
1,1-Dichloropropene ug/kg ND 5.0 04/11/23 01:14
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/11/23 01:14
1,2,3-Trichloropropane ug/kg ND 5.0 04/11/23 01:14
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/11/23 01:14
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/11/23 01:14
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/11/23 01:14
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/11/23 01:14
1,2-Dichlorobenzene ug/kg ND 5.0 04/11/23 01:14
1,2-Dichloroethane ug/kg ND 5.0 04/11/23 01:14
1,2-Dichloropropane ug/kg ND 5.0 04/11/23 01:14
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/11/23 01:14
1,3-Dichlorobenzene ug/kg ND 5.0 04/11/23 01:14
1,3-Dichloropropane ug/kg ND 5.0 04/11/23 01:14
1,4-Dichlorobenzene ug/kg ND 5.0 04/11/23 01:14
2,2-Dichloropropane ug/kg ND 5.0 04/11/23 01:14
2-Butanone (MEK)ug/kg ND 100 04/11/23 01:14
2-Chlorotoluene ug/kg ND 5.0 04/11/23 01:14
2-Hexanone ug/kg ND 50.0 v104/11/23 01:14
4-Chlorotoluene ug/kg ND 5.0 04/11/23 01:14
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/11/23 01:14
Acetone ug/kg ND 100 04/11/23 01:14
Benzene ug/kg ND 5.0 04/11/23 01:14
Bromobenzene ug/kg ND 5.0 04/11/23 01:14
Bromochloromethane ug/kg ND 5.0 04/11/23 01:14
Bromodichloromethane ug/kg ND 5.0 04/11/23 01:14
Bromoform ug/kg ND 5.0 IK04/11/23 01:14
Bromomethane ug/kg ND 20.0 04/11/23 01:14
Carbon tetrachloride ug/kg ND 5.0 04/11/23 01:14
Chlorobenzene ug/kg ND 5.0 04/11/23 01:14
Chloroethane ug/kg ND 10.0 04/11/23 01:14
Chloroform ug/kg ND 5.0 04/11/23 01:14
Chloromethane ug/kg ND 10.0 04/11/23 01:14
cis-1,2-Dichloroethene ug/kg ND 5.0 04/11/23 01:14
cis-1,3-Dichloropropene ug/kg ND 5.0 04/11/23 01:14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3978911
Associated Lab Samples:92660640001
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 04/11/23 01:14
Dibromomethane ug/kg ND 5.0 04/11/23 01:14
Dichlorodifluoromethane ug/kg ND 10.0 v104/11/23 01:14
Diisopropyl ether ug/kg ND 5.0 04/11/23 01:14
Ethylbenzene ug/kg ND 5.0 04/11/23 01:14
Hexachloro-1,3-butadiene ug/kg ND 10.0 04/11/23 01:14
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/11/23 01:14
m&p-Xylene ug/kg ND 10.0 04/11/23 01:14
Methyl-tert-butyl ether ug/kg ND 5.0 04/11/23 01:14
Methylene Chloride ug/kg ND 20.0 IK04/11/23 01:14
n-Butylbenzene ug/kg ND 5.0 04/11/23 01:14
n-Propylbenzene ug/kg ND 5.0 04/11/23 01:14
Naphthalene ug/kg ND 5.0 v104/11/23 01:14
o-Xylene ug/kg ND 5.0 04/11/23 01:14
p-Isopropyltoluene ug/kg ND 5.0 04/11/23 01:14
sec-Butylbenzene ug/kg ND 5.0 04/11/23 01:14
Styrene ug/kg ND 5.0 04/11/23 01:14
tert-Butylbenzene ug/kg ND 5.0 04/11/23 01:14
Tetrachloroethene ug/kg ND 5.0 04/11/23 01:14
Toluene ug/kg ND 5.0 04/11/23 01:14
trans-1,2-Dichloroethene ug/kg ND 5.0 04/11/23 01:14
trans-1,3-Dichloropropene ug/kg ND 5.0 04/11/23 01:14
Trichloroethene ug/kg ND 5.0 04/11/23 01:14
Trichlorofluoromethane ug/kg ND 5.0 04/11/23 01:14
Vinyl acetate ug/kg ND 50.0 04/11/23 01:14
Vinyl chloride ug/kg ND 10.0 04/11/23 01:14
Xylene (Total)ug/kg ND 10.0 04/11/23 01:14
1,2-Dichloroethane-d4 (S)%118 70-130 04/11/23 01:14
4-Bromofluorobenzene (S)%98 70-130 04/11/23 01:14
Toluene-d8 (S)%100 70-130 04/11/23 01:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3978912LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 533500 107 70-130
1,1,1-Trichloroethane ug/kg 509500 102 70-130
1,1,2,2-Tetrachloroethane ug/kg 571500 114 70-130
1,1,2-Trichloroethane ug/kg 530500 106 70-130
1,1-Dichloroethane ug/kg 506500 101 70-130
1,1-Dichloroethene ug/kg 551500 110 70-130
1,1-Dichloropropene ug/kg 535500 107 70-130
1,2,3-Trichlorobenzene ug/kg 556500 111 70-130
1,2,3-Trichloropropane ug/kg 540500 108 70-130
1,2,4-Trichlorobenzene ug/kg 535500 107 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3978912LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 585500 117 70-130
1,2-Dibromo-3-chloropropane ug/kg 573500 115 67-130
1,2-Dibromoethane (EDB)ug/kg 535500 107 70-130
1,2-Dichlorobenzene ug/kg 551500 110 70-130
1,2-Dichloroethane ug/kg 522500 104 70-130
1,2-Dichloropropane ug/kg 469500 94 70-130
1,3,5-Trimethylbenzene ug/kg 577500 115 70-130
1,3-Dichlorobenzene ug/kg 552500 110 70-130
1,3-Dichloropropane ug/kg 542500 108 70-130
1,4-Dichlorobenzene ug/kg 533500 107 70-130
2,2-Dichloropropane ug/kg 484500 97 67-130
2-Butanone (MEK)ug/kg 10901000 109 66-130
2-Chlorotoluene ug/kg 579500 116 70-130
2-Hexanone ug/kg 1220 v11000122 70-130
4-Chlorotoluene ug/kg 549500 110 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 11301000 113 70-130
Acetone ug/kg 10901000 109 67-130
Benzene ug/kg 507500 101 70-130
Bromobenzene ug/kg 543500 109 70-130
Bromochloromethane ug/kg 513500 103 70-130
Bromodichloromethane ug/kg 514500 103 70-130
Bromoform ug/kg 457 IK50091 70-130
Bromomethane ug/kg 422500 84 53-175
Carbon tetrachloride ug/kg 546500 109 70-130
Chlorobenzene ug/kg 518500 104 70-130
Chloroethane ug/kg 525500 105 70-135
Chloroform ug/kg 484500 97 70-130
Chloromethane ug/kg 540500 108 64-130
cis-1,2-Dichloroethene ug/kg 499500 100 70-130
cis-1,3-Dichloropropene ug/kg 506500 101 70-130
Dibromochloromethane ug/kg 539500 108 70-130
Dibromomethane ug/kg 479500 96 70-130
Dichlorodifluoromethane ug/kg 643 v1500129 63-145
Diisopropyl ether ug/kg 473500 95 68-130
Ethylbenzene ug/kg 493500 99 70-130
Hexachloro-1,3-butadiene ug/kg 547500 109 70-130
Isopropylbenzene (Cumene)ug/kg 558500 112 70-130
m&p-Xylene ug/kg 11001000 110 70-130
Methyl-tert-butyl ether ug/kg 495500 99 70-130
Methylene Chloride ug/kg 528 IK500106 67-130
n-Butylbenzene ug/kg 555500 111 70-130
n-Propylbenzene ug/kg 560500 112 70-130
Naphthalene ug/kg 615 v1500123 70-130
o-Xylene ug/kg 546500 109 70-130
p-Isopropyltoluene ug/kg 546500 109 70-130
sec-Butylbenzene ug/kg 534500 107 70-130
Styrene ug/kg 549500 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3978912LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 529500 106 64-130
Tetrachloroethene ug/kg 522500 104 70-130
Toluene ug/kg 496500 99 70-130
trans-1,2-Dichloroethene ug/kg 525500 105 70-130
trans-1,3-Dichloropropene ug/kg 505500 101 70-130
Trichloroethene ug/kg 475500 95 70-130
Trichlorofluoromethane ug/kg 525500 105 70-130
Vinyl acetate ug/kg 10701000 107 70-134
Vinyl chloride ug/kg 450500 90 68-130
Xylene (Total)ug/kg 16401500 110 70-130
1,2-Dichloroethane-d4 (S)%110 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3978913MATRIX SPIKE SAMPLE:
MSSpike
Result
92660265004
1,1,1,2-Tetrachloroethane ug/kg 508708 72 58-140ND
1,1,1-Trichloroethane ug/kg 544708 77 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 559708 79 52-139ND
1,1,2-Trichloroethane ug/kg 509708 72 56-140ND
1,1-Dichloroethane ug/kg 509708 72 58-145ND
1,1-Dichloroethene ug/kg 576708 81 57-158ND
1,1-Dichloropropene ug/kg 549708 77 58-151ND
1,2,3-Trichlorobenzene ug/kg 416708 59 48-149ND
1,2,3-Trichloropropane ug/kg 487708 69 54-132ND
1,2,4-Trichlorobenzene ug/kg 471708 66 51-151ND
1,2,4-Trimethylbenzene ug/kg 628708 81 38-17052.7
1,2-Dibromo-3-chloropropane ug/kg 468708 66 44-134ND
1,2-Dibromoethane (EDB)ug/kg 516708 73 60-138ND
1,2-Dichlorobenzene ug/kg 525708 74 59-147ND
1,2-Dichloroethane ug/kg 529708 75 57-139ND
1,2-Dichloropropane ug/kg 480708 68 62-145ND
1,3,5-Trimethylbenzene ug/kg 583708 80 47-15916.5
1,3-Dichlorobenzene ug/kg 557708 79 58-144ND
1,3-Dichloropropane ug/kg 509708 72 60-142ND
1,4-Dichlorobenzene ug/kg 492708 69 57-143ND
2,2-Dichloropropane ug/kg 444708 63 37-144ND
2-Butanone (MEK)ug/kg 9131420 64 28-146ND
2-Chlorotoluene ug/kg 547708 77 55-158ND
2-Hexanone ug/kg 1010 v1142071 44-141ND
4-Chlorotoluene ug/kg 527708 74 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 10301420 73 50-138ND
Acetone ug/kg 8721420 62 20-136ND
Benzene ug/kg 502708 70 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3978913MATRIX SPIKE SAMPLE:
MSSpike
Result
92660265004
Bromobenzene ug/kg 507708 72 59-145ND
Bromochloromethane ug/kg 517708 73 57-143ND
Bromodichloromethane ug/kg 507708 72 53-133ND
Bromoform ug/kg 411 IK70858 48-133ND
Bromomethane ug/kg 386708 55 10-167ND
Carbon tetrachloride ug/kg 514708 73 57-147ND
Chlorobenzene ug/kg 515708 73 61-144ND
Chloroethane ug/kg 500708 71 10-153ND
Chloroform ug/kg 492708 69 58-141ND
Chloromethane ug/kg 558708 79 54-165ND
cis-1,2-Dichloroethene ug/kg 501708 71 59-144ND
cis-1,3-Dichloropropene ug/kg 493708 70 56-137ND
Dibromochloromethane ug/kg 504708 71 53-139ND
Dibromomethane ug/kg 478708 68 60-136ND
Dichlorodifluoromethane ug/kg 789 v1708111 49-177ND
Diisopropyl ether ug/kg 468708 66 53-136ND
Ethylbenzene ug/kg 504708 69 53-15013.7
Hexachloro-1,3-butadiene ug/kg 551708 78 42-186ND
Isopropylbenzene (Cumene)ug/kg 570708 80 62-154ND
m&p-Xylene ug/kg 11301420 77 49-15644.8
Methyl-tert-butyl ether ug/kg 480708 68 54-133ND
Methylene Chloride ug/kg 878708 124 50-153ND
n-Butylbenzene ug/kg 536708 76 44-174ND
n-Propylbenzene ug/kg 516708 72 52-157ND
Naphthalene ug/kg 444 v170861 37-15012.2
o-Xylene ug/kg 530708 74 54-150ND
p-Isopropyltoluene ug/kg 552708 78 50-164ND
sec-Butylbenzene ug/kg 541708 76 58-161ND
Styrene ug/kg 524708 74 60-148ND
tert-Butylbenzene ug/kg 522708 74 44-151ND
Tetrachloroethene ug/kg 481708 68 53-151ND
Toluene ug/kg 494708 70 52-148ND
trans-1,2-Dichloroethene ug/kg 536708 76 60-148ND
trans-1,3-Dichloropropene ug/kg 495708 70 55-133ND
Trichloroethene ug/kg 478708 67 60-148ND
Trichlorofluoromethane ug/kg 427708 60 10-154ND
Vinyl acetate ug/kg 9471420 67 50-149ND
Vinyl chloride ug/kg 500708 71 57-157ND
Xylene (Total)ug/kg 16602120 76 52-15344.8
1,2-Dichloroethane-d4 (S)%107 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 23 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92660265005
3978914SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg 727 D6661440
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg 223 D661419
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg ND v1ND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg ND10.6
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg ND IKND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg ND v1ND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 210 D655370
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg 16.5 D66833.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92660265005
3978914SAMPLE DUPLICATE:
m&p-Xylene ug/kg 1090 D6591990
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg ND IKND
n-Butylbenzene ug/kg 29.2 D69077.1
n-Propylbenzene ug/kg 59.2 D662112
Naphthalene ug/kg 222 D6,v151374
o-Xylene ug/kg 405 D657726
p-Isopropyltoluene ug/kg 30.9 D66560.8
sec-Butylbenzene ug/kg NDND
Styrene ug/kg 9.1J15.8
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg 40.9 D65370.2
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg 1490 582720
1,2-Dichloroethane-d4 (S)%113111
4-Bromofluorobenzene (S)%105104
Toluene-d8 (S)%10199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
766510
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92660640002, 92660640003, 92660640004, 92660640005, 92660640006, 92660640007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3980224
Associated Lab Samples:92660640002, 92660640003, 92660640004, 92660640005, 92660640006, 92660640007
Matrix: Solid
Analyzed
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/08/23 06:23
1,1,1-Trichloroethane ug/kg ND 5.0 04/08/23 06:23
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/08/23 06:23
1,1,2-Trichloroethane ug/kg ND 5.0 04/08/23 06:23
1,1-Dichloroethane ug/kg ND 5.0 04/08/23 06:23
1,1-Dichloroethene ug/kg ND 5.0 04/08/23 06:23
1,1-Dichloropropene ug/kg ND 5.0 04/08/23 06:23
1,2,3-Trichlorobenzene ug/kg ND 5.0 04/08/23 06:23
1,2,3-Trichloropropane ug/kg ND 5.0 04/08/23 06:23
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/08/23 06:23
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/08/23 06:23
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/08/23 06:23
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/08/23 06:23
1,2-Dichlorobenzene ug/kg ND 5.0 04/08/23 06:23
1,2-Dichloroethane ug/kg ND 5.0 04/08/23 06:23
1,2-Dichloropropane ug/kg ND 5.0 04/08/23 06:23
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/08/23 06:23
1,3-Dichlorobenzene ug/kg ND 5.0 04/08/23 06:23
1,3-Dichloropropane ug/kg ND 5.0 04/08/23 06:23
1,4-Dichlorobenzene ug/kg ND 5.0 04/08/23 06:23
2,2-Dichloropropane ug/kg ND 5.0 04/08/23 06:23
2-Butanone (MEK)ug/kg ND 100 04/08/23 06:23
2-Chlorotoluene ug/kg ND 5.0 04/08/23 06:23
2-Hexanone ug/kg ND 50.0 04/08/23 06:23
4-Chlorotoluene ug/kg ND 5.0 04/08/23 06:23
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/08/23 06:23
Acetone ug/kg ND 100 04/08/23 06:23
Benzene ug/kg ND 5.0 04/08/23 06:23
Bromobenzene ug/kg ND 5.0 04/08/23 06:23
Bromochloromethane ug/kg ND 5.0 04/08/23 06:23
Bromodichloromethane ug/kg ND 5.0 04/08/23 06:23
Bromoform ug/kg ND 5.0 04/08/23 06:23
Bromomethane ug/kg ND 20.0 04/08/23 06:23
Carbon tetrachloride ug/kg ND 5.0 04/08/23 06:23
Chlorobenzene ug/kg ND 5.0 04/08/23 06:23
Chloroethane ug/kg ND 10.0 04/08/23 06:23
Chloroform ug/kg ND 5.0 04/08/23 06:23
Chloromethane ug/kg ND 10.0 04/08/23 06:23
cis-1,2-Dichloroethene ug/kg ND 5.0 04/08/23 06:23
cis-1,3-Dichloropropene ug/kg ND 5.0 04/08/23 06:23
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 3980224
Associated Lab Samples:92660640002, 92660640003, 92660640004, 92660640005, 92660640006, 92660640007
Matrix: Solid
Analyzed
Dibromochloromethane ug/kg ND 5.0 04/08/23 06:23
Dibromomethane ug/kg ND 5.0 04/08/23 06:23
Dichlorodifluoromethane ug/kg ND 10.0 04/08/23 06:23
Diisopropyl ether ug/kg ND 5.0 04/08/23 06:23
Ethylbenzene ug/kg ND 5.0 04/08/23 06:23
Hexachloro-1,3-butadiene ug/kg ND 10.0 04/08/23 06:23
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/08/23 06:23
m&p-Xylene ug/kg ND 10.0 04/08/23 06:23
Methyl-tert-butyl ether ug/kg ND 5.0 04/08/23 06:23
Methylene Chloride ug/kg ND 20.0 04/08/23 06:23
n-Butylbenzene ug/kg ND 5.0 04/08/23 06:23
n-Propylbenzene ug/kg ND 5.0 04/08/23 06:23
Naphthalene ug/kg ND 5.0 04/08/23 06:23
o-Xylene ug/kg ND 5.0 04/08/23 06:23
p-Isopropyltoluene ug/kg ND 5.0 04/08/23 06:23
sec-Butylbenzene ug/kg ND 5.0 04/08/23 06:23
Styrene ug/kg ND 5.0 04/08/23 06:23
tert-Butylbenzene ug/kg ND 5.0 04/08/23 06:23
Tetrachloroethene ug/kg ND 5.0 04/08/23 06:23
Toluene ug/kg ND 5.0 04/08/23 06:23
trans-1,2-Dichloroethene ug/kg ND 5.0 04/08/23 06:23
trans-1,3-Dichloropropene ug/kg ND 5.0 04/08/23 06:23
Trichloroethene ug/kg ND 5.0 04/08/23 06:23
Trichlorofluoromethane ug/kg ND 5.0 04/08/23 06:23
Vinyl acetate ug/kg ND 50.0 04/08/23 06:23
Vinyl chloride ug/kg ND 10.0 04/08/23 06:23
Xylene (Total)ug/kg ND 10.0 04/08/23 06:23
1,2-Dichloroethane-d4 (S)%107 70-130 04/08/23 06:23
4-Bromofluorobenzene (S)%102 70-130 04/08/23 06:23
Toluene-d8 (S)%98 70-130 04/08/23 06:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3980225LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 479500 96 70-130
1,1,1-Trichloroethane ug/kg 496500 99 70-130
1,1,2,2-Tetrachloroethane ug/kg 547500 109 70-130
1,1,2-Trichloroethane ug/kg 492500 98 70-130
1,1-Dichloroethane ug/kg 498500 100 70-130
1,1-Dichloroethene ug/kg 534500 107 70-130
1,1-Dichloropropene ug/kg 540500 108 70-130
1,2,3-Trichlorobenzene ug/kg 536500 107 70-130
1,2,3-Trichloropropane ug/kg 513500 103 70-130
1,2,4-Trichlorobenzene ug/kg 484500 97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3980225LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 507500 101 70-130
1,2-Dibromo-3-chloropropane ug/kg 577500 115 67-130
1,2-Dibromoethane (EDB)ug/kg 490500 98 70-130
1,2-Dichlorobenzene ug/kg 488500 98 70-130
1,2-Dichloroethane ug/kg 507500 101 70-130
1,2-Dichloropropane ug/kg 459500 92 70-130
1,3,5-Trimethylbenzene ug/kg 517500 103 70-130
1,3-Dichlorobenzene ug/kg 480500 96 70-130
1,3-Dichloropropane ug/kg 502500 100 70-130
1,4-Dichlorobenzene ug/kg 476500 95 70-130
2,2-Dichloropropane ug/kg 480500 96 67-130
2-Butanone (MEK)ug/kg 11901000 119 66-130
2-Chlorotoluene ug/kg 532500 106 70-130
2-Hexanone ug/kg 12201000 122 70-130
4-Chlorotoluene ug/kg 497500 99 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 11301000 113 70-130
Acetone ug/kg 11701000 117 67-130
Benzene ug/kg 486500 97 70-130
Bromobenzene ug/kg 486500 97 70-130
Bromochloromethane ug/kg 500500 100 70-130
Bromodichloromethane ug/kg 475500 95 70-130
Bromoform ug/kg 511500 102 70-130
Bromomethane ug/kg 429500 86 53-175
Carbon tetrachloride ug/kg 528500 106 70-130
Chlorobenzene ug/kg 474500 95 70-130
Chloroethane ug/kg 500500 100 70-135
Chloroform ug/kg 476500 95 70-130
Chloromethane ug/kg 559500 112 64-130
cis-1,2-Dichloroethene ug/kg 484500 97 70-130
cis-1,3-Dichloropropene ug/kg 485500 97 70-130
Dibromochloromethane ug/kg 483500 97 70-130
Dibromomethane ug/kg 452500 90 70-130
Dichlorodifluoromethane ug/kg 714500 143 63-145
Diisopropyl ether ug/kg 470500 94 68-130
Ethylbenzene ug/kg 447500 89 70-130
Hexachloro-1,3-butadiene ug/kg 456500 91 70-130
Isopropylbenzene (Cumene)ug/kg 488500 98 70-130
m&p-Xylene ug/kg 9791000 98 70-130
Methyl-tert-butyl ether ug/kg 486500 97 70-130
Methylene Chloride ug/kg 319 L250064 67-130
n-Butylbenzene ug/kg 488500 98 70-130
n-Propylbenzene ug/kg 501500 100 70-130
Naphthalene ug/kg 628500 126 70-130
o-Xylene ug/kg 478500 96 70-130
p-Isopropyltoluene ug/kg 468500 94 70-130
sec-Butylbenzene ug/kg 482500 96 70-130
Styrene ug/kg 480500 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3980225LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 460500 92 64-130
Tetrachloroethene ug/kg 457500 91 70-130
Toluene ug/kg 465500 93 70-130
trans-1,2-Dichloroethene ug/kg 523500 105 70-130
trans-1,3-Dichloropropene ug/kg 472500 94 70-130
Trichloroethene ug/kg 447500 89 70-130
Trichlorofluoromethane ug/kg 540500 108 70-130
Vinyl acetate ug/kg 11201000 112 70-134
Vinyl chloride ug/kg 456500 91 68-130
Xylene (Total)ug/kg 14601500 97 70-130
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3980226MATRIX SPIKE SAMPLE:
MSSpike
Result
92660640002
1,1,1,2-Tetrachloroethane ug/kg 796794 100 58-140ND
1,1,1-Trichloroethane ug/kg 871794 110 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 922794 116 52-139ND
1,1,2-Trichloroethane ug/kg 833794 105 56-140ND
1,1-Dichloroethane ug/kg 815794 103 58-145ND
1,1-Dichloroethene ug/kg 929794 117 57-158ND
1,1-Dichloropropene ug/kg 841794 106 58-151ND
1,2,3-Trichlorobenzene ug/kg 682794 86 48-149ND
1,2,3-Trichloropropane ug/kg 815794 103 54-132ND
1,2,4-Trichlorobenzene ug/kg 652794 82 51-151ND
1,2,4-Trimethylbenzene ug/kg 754794 95 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 855794 108 44-134ND
1,2-Dibromoethane (EDB)ug/kg 803794 101 60-138ND
1,2-Dichlorobenzene ug/kg 786794 99 59-147ND
1,2-Dichloroethane ug/kg 858794 108 57-139ND
1,2-Dichloropropane ug/kg 787794 99 62-145ND
1,3,5-Trimethylbenzene ug/kg 753794 95 47-159ND
1,3-Dichlorobenzene ug/kg 728794 92 58-144ND
1,3-Dichloropropane ug/kg 844794 106 60-142ND
1,4-Dichlorobenzene ug/kg 661794 83 57-143ND
2,2-Dichloropropane ug/kg 588794 74 37-144ND
2-Butanone (MEK)ug/kg 18001590 113 28-146ND
2-Chlorotoluene ug/kg 775794 98 55-158ND
2-Hexanone ug/kg 18601590 117 44-141ND
4-Chlorotoluene ug/kg 708794 89 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 17801590 112 50-138ND
Acetone ug/kg 16601590 104 20-136ND
Benzene ug/kg 803794 101 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3980226MATRIX SPIKE SAMPLE:
MSSpike
Result
92660640002
Bromobenzene ug/kg 750794 95 59-145ND
Bromochloromethane ug/kg 877794 111 57-143ND
Bromodichloromethane ug/kg 828794 104 53-133ND
Bromoform ug/kg 841794 106 48-133ND
Bromomethane ug/kg 511794 64 10-167ND
Carbon tetrachloride ug/kg 754794 95 57-147ND
Chlorobenzene ug/kg 774794 98 61-144ND
Chloroethane ug/kg 770794 97 10-153ND
Chloroform ug/kg 824794 104 58-141ND
Chloromethane ug/kg 896794 113 54-165ND
cis-1,2-Dichloroethene ug/kg 852794 107 59-144ND
cis-1,3-Dichloropropene ug/kg 778794 98 56-137ND
Dibromochloromethane ug/kg 788794 99 53-139ND
Dibromomethane ug/kg 751794 95 60-136ND
Dichlorodifluoromethane ug/kg 926794 117 49-177ND
Diisopropyl ether ug/kg 798794 101 53-136ND
Ethylbenzene ug/kg 724794 91 53-150ND
Hexachloro-1,3-butadiene ug/kg 637794 80 42-186ND
Isopropylbenzene (Cumene)ug/kg 766794 96 62-154ND
m&p-Xylene ug/kg 15601590 98 49-156ND
Methyl-tert-butyl ether ug/kg 820794 103 54-133ND
Methylene Chloride ug/kg 1800794 104 50-153970
n-Butylbenzene ug/kg 648794 82 44-174ND
n-Propylbenzene ug/kg 714794 90 52-157ND
Naphthalene ug/kg 769794 97 37-150ND
o-Xylene ug/kg 797794 100 54-150ND
p-Isopropyltoluene ug/kg 699794 88 50-164ND
sec-Butylbenzene ug/kg 706794 89 58-161ND
Styrene ug/kg 788794 99 60-148ND
tert-Butylbenzene ug/kg 741794 93 44-151ND
Tetrachloroethene ug/kg 644794 81 53-151ND
Toluene ug/kg 782794 98 52-148ND
trans-1,2-Dichloroethene ug/kg 816794 103 60-148ND
trans-1,3-Dichloropropene ug/kg 746794 94 55-133ND
Trichloroethene ug/kg 751794 95 60-148ND
Trichlorofluoromethane ug/kg 521794 66 10-154ND
Vinyl acetate ug/kg 16101590 101 50-149ND
Vinyl chloride ug/kg 870794 110 57-157ND
Xylene (Total)ug/kg 23602380 99 52-153ND
1,2-Dichloroethane-d4 (S)%125 70-130
4-Bromofluorobenzene (S)%108 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92660640003
3980227SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg NDND
1,1,1-Trichloroethane ug/kg NDND
1,1,2,2-Tetrachloroethane ug/kg NDND
1,1,2-Trichloroethane ug/kg NDND
1,1-Dichloroethane ug/kg NDND
1,1-Dichloroethene ug/kg NDND
1,1-Dichloropropene ug/kg NDND
1,2,3-Trichlorobenzene ug/kg NDND
1,2,3-Trichloropropane ug/kg NDND
1,2,4-Trichlorobenzene ug/kg NDND
1,2,4-Trimethylbenzene ug/kg NDND
1,2-Dibromo-3-chloropropane ug/kg NDND
1,2-Dibromoethane (EDB)ug/kg NDND
1,2-Dichlorobenzene ug/kg NDND
1,2-Dichloroethane ug/kg NDND
1,2-Dichloropropane ug/kg NDND
1,3,5-Trimethylbenzene ug/kg NDND
1,3-Dichlorobenzene ug/kg NDND
1,3-Dichloropropane ug/kg NDND
1,4-Dichlorobenzene ug/kg NDND
2,2-Dichloropropane ug/kg NDND
2-Butanone (MEK)ug/kg NDND
2-Chlorotoluene ug/kg NDND
2-Hexanone ug/kg NDND
4-Chlorotoluene ug/kg NDND
4-Methyl-2-pentanone (MIBK)ug/kg NDND
Acetone ug/kg NDND
Benzene ug/kg NDND
Bromobenzene ug/kg NDND
Bromochloromethane ug/kg NDND
Bromodichloromethane ug/kg NDND
Bromoform ug/kg NDND
Bromomethane ug/kg NDND
Carbon tetrachloride ug/kg NDND
Chlorobenzene ug/kg NDND
Chloroethane ug/kg NDND
Chloroform ug/kg NDND
Chloromethane ug/kg NDND
cis-1,2-Dichloroethene ug/kg NDND
cis-1,3-Dichloropropene ug/kg NDND
Dibromochloromethane ug/kg NDND
Dibromomethane ug/kg NDND
Dichlorodifluoromethane ug/kg NDND
Diisopropyl ether ug/kg NDND
Ethylbenzene ug/kg 8.3JND
Hexachloro-1,3-butadiene ug/kg NDND
Isopropylbenzene (Cumene)ug/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92660640003
3980227SAMPLE DUPLICATE:
m&p-Xylene ug/kg NDND
Methyl-tert-butyl ether ug/kg NDND
Methylene Chloride ug/kg 913 281210
n-Butylbenzene ug/kg NDND
n-Propylbenzene ug/kg NDND
Naphthalene ug/kg NDND
o-Xylene ug/kg NDND
p-Isopropyltoluene ug/kg NDND
sec-Butylbenzene ug/kg NDND
Styrene ug/kg NDND
tert-Butylbenzene ug/kg NDND
Tetrachloroethene ug/kg NDND
Toluene ug/kg NDND
trans-1,2-Dichloroethene ug/kg NDND
trans-1,3-Dichloropropene ug/kg NDND
Trichloroethene ug/kg NDND
Trichlorofluoromethane ug/kg NDND
Vinyl acetate ug/kg NDND
Vinyl chloride ug/kg NDND
Xylene (Total)ug/kg NDND
1,2-Dichloroethane-d4 (S)%107104
4-Bromofluorobenzene (S)%103106
Toluene-d8 (S)%103100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 38
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92660640
GILBARRO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
766543
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples: 92660640001, 92660640002, 92660640003, 92660640004, 92660640005, 92660640006, 92660640007
Parameter Units
Dup
Result QualifiersRPDResult
92660612001
3980449SAMPLE DUPLICATE:
Percent Moisture %28.5 N2128.3
Parameter Units
Dup
Result QualifiersRPDResult
92660651012
3980450SAMPLE DUPLICATE:
Percent Moisture %10.9 N21412.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92660640
GILBARRO
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.IK
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 38
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92660640
GILBARRO
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92660640001 766285 766345UNIT 7/8 SUPPLY UNIT 7 DRAIN EPA 5035A/5030B EPA 8260D
92660640002 766510 767126UNIT 8 DRAIN, UNUSED SUPPLY EPA 5035A/5030B EPA 8260D
92660640003 766510 767126UNIT 2 SUPPLY EPA 5035A/5030B EPA 8260D
92660640004 766510 767126MAIN LINE COOLENT UNIT EPA 5035A/5030B EPA 8260D
92660640005 766510 767126MAINLINE DRAIN TO 7 EPA 5035A/5030B EPA 8260D
92660640006 766510 767126UNIT 4/6 SUPPLY AND DRAIN EPA 5035A/5030B EPA 8260D
92660640007 766510 767126UNIT 4/6 MAINLINE SUPPLY AND
D
EPA 5035A/5030B EPA 8260D
92660640001 766543UNIT 7/8 SUPPLY UNIT 7 DRAIN SW-846
92660640002 766543UNIT 8 DRAIN, UNUSED SUPPLY SW-846
92660640003 766543UNIT 2 SUPPLY SW-846
92660640004 766543MAIN LINE COOLENT UNIT SW-846
92660640005 766543MAINLINE DRAIN TO 7 SW-846
92660640006 766543UNIT 4/6 SUPPLY AND DRAIN SW-846
92660640007 766543UNIT 4/6 MAINLINE SUPPLY AND
D
SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/11/2023 04:42 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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