WS-10023_45185_CA_LSA_20200117_PhaseII

An Equal Opportunity Employer

January 17, 2020

Ms. Carin Kromm
NCDEQ-UST Section
Winston-Salem Regional Office
450 W. Hanes Mill Road
Suite 300
Winston-Salem, NC 27105

Re: Limited Site Assessment Report
Speedway #6934
566 Old Hollow Road
Winston-Salem, Forsyth County, NC
Incident Number: 45185
GRI Project Number: 4341

Dear Ms. Kromm,

Please find enclosed the referenced report for the above mentioned site. If you have any questions, please do
not hesitate to contact Joanna Alley E.I.T. and/or Nicole Long with Geological Resources, Inc. at 704-845-4010.

Sincerely,
Speedway, LLC.
Charles Chiara
Environmental Representative

Enclosure

Speedway LLC

Speedway Office
P.O. Box 1500
Springfield, OH 45501
Telephone [phone]

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Phase II Limited Site Assessment Report
Speedway #6934
566 Old Hollow Road
Winston-Salem, Forsyth County
North Carolina
Facility ID Number: 0-015480
Incident Number: 45185
GRI Project Number: 4341

Prepared for:

Charles Chiara
Speedway, LLC
500 Speedway Drive
Enon, Ohio 45323

January 13, 2020

Joanna Alley. E.I.T.
Project Manager
Nicole Long
Project Manager

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
i

EXECUTIVE SUMMARY
The Speedway #6934 site is located at 566 Old Hollow Road in Winston-Salem, Forsyth County, North
Carolina. The property operates as a petroleum retail facility and convenience store. The site is covered
by the building, concrete and asphalt. There are one 6,000-gallon gasoline, two 8,000-gallon gasoline and
one 3,000-gallon diesel USTs currently in use at the site with five associated gasoline and one diesel
dispenser islands. The surrounding properties are commercial/industrial and residential.

On November 12, 2018, a small leak was discovered in the RUL flex connector in dispenser 7/8 and on
January 28, 2019, GRI conducted a site check at the subject site. One soil boring was advanced below the
dispenser during repairs to a depth of approximately 2 feet below ground surface (bgs) and a soil sample
was collected from the boring (SB-1). The RAL, soil-to-water MCCs and/or residential SCLs were below the
concentrations of gasoline-range organics (GRO), benzene, toluene, ethylbenzene and xylenes reported
in soil sample SB-1. Site Check results identified a release at the site and a LSA was required.

A receptor survey was conducted on July 23, 2019. Fourteen non-potable water supply wells were
identified within a 1,500-foot radius of the site. One inactive non-potable water supply well was identified
within a 250-foot radius of the site. In addition, three suspected water supply wells (WSW-15 through
WSW-17) were identified; however their presence could not be confirmed. Public water is available to
the subject site and to all surrounding properties. All residence with water supply wells are connected to
public water. No surface water bodies were identified within a 500-foot radius of the site.

On July 23, 2019, one monitoring well (MW-1) was installed slightly downgradient of soil borings SB-1 and
the UST basin, the location of the soil contamination identified during previous environmental assessment
activities conducted in January 2019. Soil samples were collected at 10-foot intervals during the
installation of monitoring well MW-1. The soil-to-water MCC was below the concentration of benzene
reported in soil samples MW-1 (10’) and MW-1 (20’).

On July 23, 2019, a ground water sample was collected from MW-1. The MACs were below the
concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, isopropylbenzene, n-
propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, t-amyl alcohol, tert-butyl alcohol, EDB,
1-methylnapthalene, 2-methylnapthalene, C5-C8 aliphatic, 1,2,-dichloroethane, di-isopropyl ether and
TAME reported in the ground water sample collected from MW-1. The GCLs were below the
concentration of benzene, MTBE and tert-butyl alcohol reported in MW-1. Based on the reported ground
water contaminant concentrations and the presence of a water supply well within a 250-foot radius of
the site, a Phase II Limited Site Assessment was required to be completed at the site.

On December 19, 2019, three additional monitoring wells were installed at the site in order to determine
the ground water flow direction and delineate ground water contamination. A ground water sample was
collected from each well following installation. The MACs were below the concentrations of benzene,
toluene, ethylbenzene, xylenes, MTBE, naphthalene, n-propylbenzene, 1,2,4-trimethylbenzene, t-amyl
alcohol, tert-butyl alcohol, C5-C8 aliphatics and/or C9-C10 aromatics reported in the ground water
samples collected from MW-3 and MW-4. None of the reported concentrations were above the GCLs
during the December 2019 sampling event. No free product was observed at the site.

Based on the presence of a water supply well within 250 feet of the site, and the MACs and GCLs being

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
ii

below the reported contaminant concentrations, the site risk should be classified as high and a
Comprehensive Site Assessment should be conducted at the site. Please note that it is recommended to
attempt to abandon water supply well WSW-1 prior to the start of further assessment activities in order
to lower the risk of the site.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341

TABLE OF CONTENTS

1. RISK CHARACTERIZATION .....................................................................................................1
2. RECEPTOR INFORMATION .....................................................................................................4
3. SITE GEOLOGY AND HYDROGEOLOGY ...................................................................................5
4. SITE INVESTIGATION .............................................................................................................6
5. CONCLUSIONS AND RECOMMENDATIONS ............................................................................8
6. LIMITATIONS ........................................................................................................................9

FIGURES
Figure 1: Site Location Map
Figure 2: Site Vicinity Map
Figure 3: Site Map
Figure 4: Water Table Surface Map
Figure 5: Soil Quality Map
Figure 6: Ground Water Quality Map

TABLES
Table 1: UST Owner/Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Well Construction and Gauging Information
Table 6: Summary of Soil Sample Analytical Results
Table 7: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Water Use Questionnaire Forms
Appendix B: Forsyth County Property Cards
Appendix C: Well Construction Records and Subsurface Logs
Appendix D: State Correspondence
Appendix E: Laboratory Analytical Reports

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
1
1. RISK CHARACTERIZATION
Limited Site Assessment Risk Classification and Land Use Form
Part I – Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non-drinking
purposes? NO

2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the
release? NO

3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling
water, filling swimming pools) located within 250 feet of the source area of the release?
YES

An inactive non-potable water supply well (WSW-1) is located approximately 180 feet to the west
of the site.

4. Does ground water within 500 feet of the source area of the release have the potential for future
use (there is no other source of water supply other than the groundwater)? NO

Public water is available to the site and surrounding properties.

5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a
confined space or pose any other serious threat to public health, public safety or the
environment?
NO

6. Are there any other factors that would cause the release to pose an imminent danger to public
health, public safety, or the environment? NO
If YES, explain:

Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release? NO

If YES, does the maximum groundwater contaminant concentration exceed the surface water
quality standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? N/A

8. Is the source area of the release located within an approved or planned wellhead protection area
as defined in 42 USC 300h-7(e)? NO

9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled
“Geology of North Carolina” published by the Department in 1985? NO

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
2
10. If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of
drinking water? N/A
If YES, describe.
11. Do the levels of ground water contamination for any contaminant exceed the gross contamination
levels established by the Department? YES

The gross contamination levels (GCLs) were below the concentrations of benzene, MTBE and tert-
butyl alcohol reported in MW-1.

Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or
temporary)? NO
Explain:
The subject property is an active convenience store and petroleum retail facility.

2. Does the property contain a school, daycare center, hospital, playground, park, recreation area,
church, nursing home, or other place of public assembly? NO
Explain:

The subject property is an active convenience store and petroleum retail facility.

3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or
industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
Explain:

The subject property is an active convenience store and petroleum retail facility.

4. Do children visit the property? YES
Explain:

The site is currently a convenience store and children would likely visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security
personnel or both)? NO
Explain:
The property is easily accessible to pedestrian and vehicular traffic.
6. Do pavement, buildings, or other structures cap the contaminated soil? YES

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
3
Explain:
The site is currently covered with the building, concrete and asphalt.

If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil
will remain capped in the foreseeable future?
The site may be removed as part of road widening project in the future.
7. What is the zoning status of the property?
According to the City of Winston-Salem Official Zoning Map, the site is zoned H-B (Highway-
Business).
8. Is the use of the property likely to change in the next 20 years? YES
Explain:

North Carolina Department of Transportation (NCDOT) reportedly may take most of the site
during road widening activities in the futures.

Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes
property containing source area of the release):

9. What is the distance from the source area of the release to the nearest primary or secondary
residence (permanent or temporary)?

The closest primary residence is 563 Old Hollow Road located approximately 240 feet northwest
of the UST basin.

10. What is the distance from the source area of the release to the nearest school, daycare center,
hospital, playground, park, recreation area, church, nursing home or other place of public
assembly?

Bethany Baptist Church is located at 600 Old Hollow Road, approximately 300 feet southeast of
the source area at the site.

11. What is the zoning status of properties in the surrounding area?

According to the Forsyth County Tax Parcel Viewer Map, the surrounding areas are zoned Highway
and Limited Business (HB & LB), and/or Residential (RS-9).

12. Briefly characterize the use and activities of the land in the surrounding area.

The area surrounding the site is a mixture of commercial, business and residential such as a former
gas station, a church, used car lot and heating/cooling repair services and residential properties.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
4

2. RECEPTOR INFORMATION
1. Water Supply Wells:
A receptor survey was conducted on July 23, 2019. Fourteen non-potable water supply wells were
identified within a 1,500-foot radius of the site. Of the fourteen non-potable water supply wells,
one inactive water supply well (WSW-1) is located within a 250-foot radius of the site. The status
of several wells could not be confirmed; however active water meters were identified at all
properties. In addition three suspected water supply wells (WSW-15 through WSW-17) were
identified; however, their presence could not be confirmed. A Site Location Map is provided as
Figure 1 and a Site Vicinity Map showing property boundaries for the site and surrounding
properties has been included as Figure 2. Water supply well information has been provided in
Table 3. Returned water use questionnaire forms are attached as Appendix A

2. Public Water Supplies:
Are public water supplies available within 1,500 feet of the source area of the release? YES
If yes, where is the location of the nearest public water lines and the source(s) of the public water
supply. Explain:
Municipal water is available to the site and the surrounding properties. Water lines run along the
public streets in the area. Public water is supplied by the Winston-Salem/Forsyth County utilities.

3. Surface Water:
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) within 1,500 feet of the
source area of the release. This information must be shown on the USGS topographic map.
Two ponds were identified approximately 1,200 feet to the north and 1,400 feet to the south-
southwest of the site. A small creek named Ogburn Branch starts about 600 feet southeast of the
site and flows to the southwest-south.

4. Wellhead Protection Areas:
Identify all planned or approved wellhead protection areas in the vicinity of the source area. This
information must be shown on the USGS topographic map. Wellhead protection areas are defined
in 42 USC 300h-7(e).
On January 6, 2020, GRI personnel accessed the NCDEQ Source Water Assessment and Protection
(SWAP) Program’s website to identify wellhead protection areas in the vicinity of the subject site.
The site is not located within a wellhead protection area.

5. Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not located in the Coastal Plain Physiographic Region.

6. Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. The water main
and other underground utilities run along Old Hollow Road and Germantown Road and several

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
5
underground utility lines were observed on the property.

7. Property Owners and Occupants:
The names and addresses of the owners of properties adjacent to the site are presented in Table
4. Property boundaries are shown on Figure 2. Property cards for the adjacent property owners
and water supply well owners are attached as Appendix B.
3. SITE GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is located in the Charlotte Belt. The
bedrock is generally described as foliated to massive metamorphosed biotite gnesis and schist. The soil
samples collected during well installation activities were brown to red silts. The depth to ground water
during the December 19, 2019 gauging event ranged from 25.91 to 31.07 feet below the top of well casing.
A copy of the well construction records and subsurface logs have been included as Appendix C. A Site
Map is included as Figure 3. Well construction and gauging information is presented in Table 5. Photos
of the newly installed monitoring wells are shown below:

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
6
4. SITE INVESTIGATION
On November 12, 2018, a small leak was discovered in the RUL flex connector in dispenser 7/8 and on
January 28, 2019, GRI conducted a site check at the subject site. One soil boring was advanced below the
dispenser during repairs to a depth of approximately 2 feet below ground surface (bgs) and a soil sample
was collected from the boring (SB-1). The regulatory action level (RAL), soil-to-water maximum
contaminant concentrations (MCCs) and/or residential Soil Cleanup Levels (SCLs) were below the
concentrations of gasoline-range organics (GRO), benzene, toluene, ethylbenzene and xylenes reported
in soil sample SB-1. Based on these results, a Limited Site Assessment (LSA) was recommended in the Site
Check.

In accordance with the Notice of Regulatory Requirements (NORR) dated July 11, 2019, one monitoring
well (MW-1) was installed by a North Carolina licensed well contractor on July 23, 2019 to assess the
identified release at the site. MW-1 was installed to a total depth of 40 feet bgs with a 20-foot screened
interval set to bracket the water table at the time of installation. Monitoring well MW-1 was installed
slightly downgradient of soil borings SB-1 and UST basin, the location of the soil contamination identified
during previous environmental assessment activities conducted in January 2019. A copy of the NORR and
the approved Task Authorization (TA) form have been included in Appendix D.

Based on the ground water contaminant concentrations in the sample collected from MW-1, and the
presence of a water supply well within a 250-foot radius of the site, three additional monitoring wells
were required to be installed at the site in order to determine the ground water flow direction.
Monitoring wells MW-2 through MW-4 were installed at the site on December 19, 2019 to total depths
ranging between 30 to 35 feet bgs, with a screened interval of 15 feet. A copy of the approved TA form
for additional monitoring has been included in Appendix D.

Monitoring wells MW-1 through MW-4 were gauged on December 19, 2019. The depth to ground water
ranged from 25.91 to 31.07 feet. The ground water elevation ranged from 68.91 to 72.90 feet during the
December 19, 2019 ground water gauging event. Ground water flow was generally towards the south
with a horizontal gradient of 0.03 feet per foot. A Water Table Surface Map has been included as Figure
4. Gauging data from the December 2019 gauging event has been included in Table 5. A summary of the
current gauging data is shown below:

Well ID DATE
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Groundwater
Elevation
(ft.)
MW-1 07/23/19 20 - 40 40 100.00 27.71 72.29
12/19/19 28.56 71.44
MW-2 12/19/19 20 - 35 35 98.81 25.91 72.90
MW-3 12/19/19 20 - 35 35 101.75 31.07 70.68
MW-4 12/19/19 15 - 30 30 97.73 28.82 68.91

1. Soil Sampling:
Soil sample (SB-1) was collected on January 28, 2019 during Site Check activities, and submitted for
laboratory analyses of total petroleum hydrocarbons (TPH) GRO by EPA Method 8015D and BTEX by
EPA Method 8260B. The applicable RAL, soil-to-water MCCs and/or SCLs were below the

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
7
concentrations of GRO, benzene, toluene, ethylbenzene and xylenes reported in the soil sample
collected from SB-1. No free product was noted at the site.

On July 23, 2019, two soil samples (MW-1 (10’) and MW-1 (20’)) were collected at 10-foot intervals
during the installation of monitoring well MW-1. The soil samples were submitted for analysis of
volatile organic compounds (VOCs) by EPA Method 8260D, semi-VOCs (SVOCs) by 8270E, volatile
petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons by (EPH) by the MADEP
methods.

The soil-to-water MCC was below the concentration of benzene reported in soil samples MW-1 (10’)
and MW-1 (20’). A Soil Quality Map has been included as Figure 5. A summary of the soil sample
analytical results is presented in Table 6. A copy of the laboratory analytical report from the July 2019
soil sampling event has been included in Appendix E. A copy of the current soil sampling data
collected during the LSA activities is shown below:
Sample ID Sample Depth (ft-BGS) Benzene Toluene Ethylbenzene Total Xylenes MTBE Naphthalene Soil to Water MCC (mg/kg) 0.0056 4.3 4.9 4.6 0.091 0.16
Residential SCLs (mg/kg) 18 1,200 1,560 3,129 350 313
MW-1 (10') 10 0.00650 <0.00679 <0.00339 <0.00882 0.00944 <0.0170
MW-1 (20') 20 0.00641 <0.00766 <0.00383 <0.00996 0.0386 <0.0192

2. Ground Water Sampling:
On July 23, 2019, MW-1 was gauged, purged, and sampled. The ground water sample was submitted
for analysis of VOCs by EPA Method 6200B plus oxygenates and ethanol, SVOCs by 625.1 plus 10 TICs,
EDB by EPA Method 504.1, total lead by EPA Method 6010 and VPH and EPH by the MADEP Methods.
The maximum allowable concentrations (MACs) specified in T15A NCAC 2L.0202 were below the
concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, isopropylbenzene,
n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-trimethylbenzene, t-amyl alcohol, tert-butyl alcohol,
EDB, 1-methylnapthalene, 2-methylnapthalene, C5-C8 aliphatics, 1,2-dichloroethane, di-isopropyl
ether and TAME reported in the ground water sample collected from MW-1. The GCLs were below
the concentration of benzene, MTBE and tert-butyl alcohol reported in MW-1.

On December 19, 2019, monitoring wells MW-2 through MW-4 were gauged, purged and sampled.
Monitoring well MW-1 was only gauged for depth to water to determine depth of new wells. The
ground water samples were submitted for analysis of VOCs plus oxygenates and ethanol, EDB, total
lead and VPH. The MACs were below the concentrations of benzene, toluene, ethylbenzene, xylenes,
MTBE, naphthalene, n-propylbenzene, 1,2,4-trimethylbenzene, t-amyl alcohol, tert-butyl alcohol, C5-
C8 aliphatics and/or C9-C10 aromatics reported in the ground water samples collected from MW-3
and MW-4. None of the reported concentrations were above the GCLs during the December 2019
sampling event. No free product was observed at the site. A Ground Water Quality Map has been
included as Figure 6. A summary of the ground water analytical data has been included in Table 7.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
8
Copies of the laboratory analytical reports have been included in Appendix E. A summary of the
current ground water sampling data is shown below:

Contaminant
of Concern
 Date Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MAC (µg/l) 1 600 600 500 20 6
GCL (µg/l) 5,000 260,000 84,500 85,500 20,000 6,000
MW-1 7/23/19 18,600 40,600 3,960 19,300 107,000 661
12/19/19 NS NS NS NS NS NS
MW-2 12/19/19 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00
MW-3 12/19/19 2,970 26,700 1,580 10,200 70.9 189
MW-4 12/19/19 <1.00 2.94 <1.00 <3.00 <1.00 <5.00

3. Quality Control:
The soil and ground water samples were immediately placed in laboratory-supplied containers after
collection, which were then placed in iced coolers. New disposable bailers were used to sample the
monitoring well and new nitrile gloves were worn during soil and ground water sampling. Samples
were logged using proper chain-of-custody procedures. The samples were transported to a North
Carolina certified laboratory for analysis. A laboratory supplied trip blank was included in the sample
cooler. No detectable concentrations of requested method constituents were reported in the trip
blank.

5. CONCLUSIONS AND RECOMMENDATIONS
 The site is an active convenience store and petroleum retail facility. Land use in the area consists
of commercial, industrial and residential properties. NCDOT may take most of the site during road
widening activities.
 A receptor survey was conducted on July 23, 2019. Fourteen non-potable water supply wells were
identified within a 1,500-foot radius of the site. One non-potable inactive water supply well was
identified within a 250-foot radius of the site. In addition, three suspected water supply wells
(WSW-15 through WSW-17) were identified; however, their presence could not be confirmed.
Public water is available to the subject site and to all surrounding properties.
 No surface water bodies were identified within a 500-foot radius of the site.
 On July 23, 2019, one monitoring well (MW-1) was installed slightly downgradient of soil borings
SB-1 and UST basin.
 Soil samples were collected at 10-foot intervals during the installation of monitoring well MW-1.
The soil-to-water MCC was below the concentration of benzene reported in soil samples MW-1
(10’) and MW-1 (20’).
 On July 23, 2019, a ground water sample was collected from MW-1 following monitoring well
installation. The MACs were below the concentrations of benzene, toluene, ethylbenzene,
xylenes, MTBE, naphthalene, isopropylbenzene, n-propylbenzene, 1,2,4-trimethylbenzene, 1,3,5-
trimethylbenzene, t-amyl alcohol, tert-butyl alcohol, EDB, 1-methylnapthalene, 2-

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Phase II Limited Site Assessment Report
Prepared on: January 13, 2020 Speedway #6934
Project Manager: Joanna Alley. E.I.T. GRI Project No. 4341
9
methylnapthalene, C5-C8 aliphatics, 1,2-dichloroethane, di-isopropyl ether and TAME reported in
the ground water sample collected from MW-1.
 The GCLs were below the concentration of benzene, MTBE and tert-butyl alcohol reported in MW-
1 collected during the July 23, 2019 sampling event.
 On December 19, 2019, three additional monitoring wells were installed at the site in order to
determine the ground water flow direction and to delineate ground water contamination. A
ground water sample was collected from each well following installation. The MACs were below
the concentrations of benzene, toluene, ethylbenzene, xylenes, MTBE, naphthalene, n-
propylbenzene, 1,2,4-trimethylbenzene, t-amyl alcohol, tert-butyl alcohol, C5-C8 aliphatics
and/or C9-C10 aromatics reported in the ground water samples collected from MW-3 and MW-
4.
 None of the reported concentrations were above the GCLs during the December 19, 2019
sampling event.
 No free product was observed at the site during the December 19, 2019 sampling event.
 Based on the presence of a water supply well within 250 feet of the site, and the MACs and GCLs
being below the reported contaminant concentrations, the site risk should be classified as high
and a Comprehensive Site Assessment should be conducted at the site. Please note that it is
recommended to attempt to abandon water supply well WSW-1 prior to the start of further
assessment activities in order to lower the risk of the site.

6. LIMITATIONS
This report has been prepared for the exclusive use of Speedway, LLC. and the NCDEQ for specific
application to the referenced site in Forsyth County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by NCDEQ and with resources adequate only for
that scope of work. Our findings have been developed in accordance with generally accepted standards
of geology and hydrogeology practices in the State of North Carolina, available information and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data.

FIGURES
SITE LOCATION
Figure 1
Site Location
Speedway #6934
566 Old Hollow Road Winston-
Salem Forsyth County, NC
Incident No. 45185
GRI Project No. 4341500 M
2000 FT
Date: 01/08/2020 Location: 36.194573° N 80.255148° W
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SITE
6829-91-9827.0006829-92-2389.0006829-92-5347.0006829-82-8386.0006839-02-0630.000
6829-92-5083.000
6829-92-1776.000
6829-92-9226.0006829-92-4328.0006829-91-6760.000
6829-92-7205.000
6829-91-8160.0006829-92-1047.0006829-91-4982.000
6829-81-8952.0006829-81-5968.0006829-92-4023.0006829-82-4466.0006829-91-4700.000
6829-81-7023.000
6829-82-9861.000
OGBURN BRANCH 86WSW-17
WSW-16
WSW-15
WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-2
WSW-1
WSW-14
WSW-13 WSW-12
WSW-11 WSW-10
OLD HOLLOW RD GERMANTON RDPUGH DR
MERRY DALE DRWINDY HILL DRHUNSFORD DRPLANTATION DRROCK SPRING DR
TWIN OAK DRBROWNWOOD DRVANCLAIR DR JUTLAND DRWHITE OAK DRHOLLY RIDGE DRROSCOE VAUGHN DRCRESTRIDGE LNSTONEWAY CT FIGURE 2: SITE VICINITY MAPSPEEDWAY #6934566 OLD HOLLOW ROADWINSTON-SALEM, FORSYTH COUNTYNORTH CAROLINAINCIDENT NO. 45185GRI PROJECT NO. 4341
PREPARED BY:GEOLOGICAL RESOURCES, INC.JULY 19, 2019
³
0 300150Feet
1 inch = 300 feet
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
1,500-FOOT RADIUS
LEGEND
"J Water Supply Well
!P Possible Well
Pond
streets
Adjacent Properties and Well Owners
Parcels
Streams

TABLES
UST ID Number 1-4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 1-2 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 3 Facility ID Number
Owner or Operator?
Owner/OperatorUnknown 04/17/1984 - 04/18/1986
Address Telephone Number
Unknown Unknown
Unknown Unknown
0-015480
Name of Owner or Operator Dates of Ownership / Operation
Name of Owner or Operator Dates of Ownership / Operation
Unknown 04/21/1970 - 04/18/1986
Address Telephone Number
Address Telephone Number
5446 University Parkway, Winston-Salem, NC 27105 1-336-767-6280
0-015480
0-015480
Name of Owner or Operator Dates of Ownership / Operation
A. T. Williams Oil Company 01/30/1991 - 04/02/2001
500 Speedway Drive, Enon, Ohio 45323 1-919-516-8069
Name of Owner or Operator Dates of Ownership / Operation
Speedway, LLC. 01/01/2016 - Current
Address Telephone Number
0-015480
TABLE 1
UST OWNER/OPERATOR INFORMATION
SPEEDWAY #6934
INICDENT NO. 45185
Address Telephone Number
5446 University Parkway, Winston-Salem, NC 27105 1-336-767-6280
0-015480
Name of Owner or Operator Dates of Ownership / Operation
A. T. Williams Oil Company 04/18/1986 - 04/02/2001
Address Telephone Number
5446 University Parkway, Winston-Salem, NC 27105-1366 1-800-642-0945
0-015480
Name of Owner or Operator Dates of Ownership / Operation
WilcoHess, LLC. 04/02/2001 - 01/01/2016
Page 1 of 1
Date: 01/07/2020
Was
Release
Associated
with UST
System?
(Yes / No)
1 Diesel NA 3,000 4/21/1970 Single Wall Steel 64" x 18'
Single Wall
FRP Current No
2 Gasoline NA 6,000 4/21/1970 Single Wall Steel 8' x 16'
Single Wall
FRP Current Yes
3 Gasoline NA 8,000 4/17/1984 Single Wall Steel 8' x 21' 4"
Single Wall
FRP Current Yes
4 Gasoline NA 8,000 1/30/1991 Single Wall Steel 8' x 21' 4"
Single Wall
FRP Current Yes
TABLE 2
UST SYSTEM INFORMATION
SPEEDWAY #6934
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Tank
Dimensions
Description
of
Associated
Product
Piping
and
Pumps
Status
of
UST
Facility ID #: 0-015480
INCIDENT NO. 45185
Page 1 of 1
Date: 01/07/2020 Facility ID #: 0-015480
Well ID Parcel ID No. Well Owner Mailing Address Well Location Address
Well Use
(Potable/
Agriculture, etc.)
Public Water
Connected
Distance from
source area of
release
(ft.)
WSW-1 6829-92-4023
Pamela H. Bowles and Carolyn N.
Collins
PO Box 480,
Germantown, NC 27019
564 Old Hollow Road
Winston-Salem, NC 27105 Not in Use Yes 180 W
WSW-2 6829-92-4328 Ann D. Lawson
547 Old Hollow Road
Winston-Salem, NC 27105
547 Old Hollow Road
Winston-Salem, NC 27105
Status not
confirmed Yes 360 NW
WSW-3 6829-92-1047 Jan R. Littell
544 Old Hollow Road
Winston-Salem, NC 27105
544 Old Hollow Road
Winston-Salem, NC 27105
Status not
confirmed Yes 465 W
WSW-4 6829-91-6760 Robert N. & Teresa Y. Bias
5655 Germantown Road,
Winston-Salem, NC 27105
5655 Germantown Road,
Winston-Salem, NC 27105
Not in Use
(no pump or
power)
Yes 345 S
WSW-5 6829-81-8952 Michael L. & Rita Y. Lewis
947 Rock Spring Drive
Winston-Salem, NC 27105
947 Rock Spring Drive
Winston-Salem, NC 27105 Irrigational Yes 810 W
WSW-6 6829-81-5968 Stanley C. & Deborah C. Taylor
929 Rock Spring Drive
Winston-Salem, NC 27105
929 Rock Spring Drive
Winston-Salem, NC 27105
Status not
confirmed Yes 1,080 W
WSW-7 6829-91-4700 Claude A. Whittington
5650 Germantown Road,
Winston-Salem, NC 27105
5650 Germantown Road,
Winston-Salem, NC 27105 Not in Use Yes 450 SW
WSW-8 6829-91-8160 James R. Myers
1137 Twin Oak Drive
Winston-Salem, NC 27105
1137 Twin Oak Drive
Winston-Salem, NC 27105
Status not
confirmed Yes 950 S
WSW-9 6829-81-7023 Guy A. & Teresa Cowell
5651 Plantation Drive
Winston-Salem, NC 27105
5651 Plantation Drive
Winston-Salem, NC 27105 Not in Use Yes 1,375 SW
WSW-10
&
WSW-11
6829-82-8386 John Southard, Inc.
2601 Reynolds Drive
Winston-Salem, NC 27104
535 Old Hollow Road
Winston-Salem, NC 27105 Not in Use Yes
740 NW
790 NW
WSW-12 6829-92-1776 Russell G. & Paula B. Stop
5735 White Oaks Drive
Winston-Salem, NC 27105
5735 White Oaks Drive
Winston-Salem, NC 27105
Status not
confirmed Yes 870 NW
WSW-13 6829-82-9861 David Caudill
1185 Lowvalley Court
Rural Hill, NC 27045
5736 White Oaks Drive
Winston-Salem, NC 27105
Status not
confirmed Yes 1,015 NW
WSW-14 6829-82-4466 Billy J. Deboard
515 Old Hollow Road
Winston-Salem, NC 27105
515 Old Hollow Road
Winston-Salem, NC 27105 Not in Use Yes 1,200 NW
WSW-15 6839-02-0630 US Bank National Association
4801 Frederica Street
Owensboro, KY 42301
5721 Germantown Road,
Winston-Salem, NC 27105
Status not
confirmed Yes 720 NE
WSW-16
&
WSW-17
6829-92-2389 Shirley T. Cook 3000 Tesh Road
Germantown, NC 27019
545 Old Hollow Road,
Winston-Salem, NC 27105
Status not
confirmed Yes 465 NW
Notes:
• Water supply wells are shown on Figure 2
• Ft. BGS : Feet below ground surface
TABLE 3
WATER SUPPLY WELL INFORMATION
SPEEDWAY #6934 (INCIDENT NO. 45185)
Page 1 of 1
Date: 01/07/2020 Facility ID #: 0-015480
PIN Number Property Owner Name Property Owner Address
6829-92-5083 (site) Nancy W. Downing
1829 Shoreham Dr.
Charlotte, NC 28211
6829-92-7205 John H. Spainhour & Sons Grading
Co.
8530 Chipboard Road
Rural Hill, NC 27045
6829-91-9827 Bethany Baptist Church Uw
600 Old Hollow Road,
Winston-Salem, NC 27105
6829-91-4982 George D. & Susan W. Carter
5012 Klondike Road,
Walkertown, NC 27051
6829-92-4023 Pamela H. Bowles and Carolyn N.
Collins
PO Box 480,
Germantown, NC 27019
6829-92-5347 Shirley T. Cook
3000 Tesh Road,
Germantown, NC 27019
Note:
• Properties are keyed to Figure 2.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
SPEEDWAY #6934 (INCIDENT NO. 45185)
Page 1 of 1
Date: 01/07/2020 Facility ID #: 0-015480
Well ID Date Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(ft.)
Free Product
Thickness
(ft.)
Groundwater
Elevation
(ft.)
Comments
07/23/19 27.71 ---72.29
12/19/19 28.56 ---71.44
MW-2 12/19/19 12/19/19 20 20 - 35 35 98.81 25.91 ---72.90
MW-3 12/19/19 12/19/19 20 20 - 35 35 101.75 31.07 ---70.68
MW-4 12/19/19 12/19/19 15 15 - 30 30 97.73 28.82 ---68.91
Notes:
• ft BGS : feet below ground surface.
TABLE 5
WELL CONSTRUCTION AND GAUGING INFORMATION
SPEEDWAY #6934 (INCIDENT NO. 45185)
100.004020 - 402007/23/19MW-1
Page 1 of 1
Date: 01/07/2020
Sample IDDate Collected (mm/dd/yy)Sample Depth(ft-BGS)BenzeneTolueneEthylbenzeneTotal XylenesMTBENaphthalene1-Methylnaphthalene2-MethylnaphthaleneAdjusted C5-C8 AliphaticsAdjusted C9-C12 AliphaticsUnadjusted C9-C10 AromaticsUnadjusted C9-C18 AliphaticsUnadjusted C19-C36 AliphaticsAdjusted C11-C22 AromaticsNE NE NE NE NE NE NE NE NE NE NE NE NE NE
0.0056 4.3 4.9 4.6 0.091 0.16 0.004 3.6 68 540 31 540 NE 31
18 1,200 1,560 3,129 350 313 20 63 939 1,500 469 1,500 31,000 469
MW-1 (10') 07/23/19 10 0.00650 <0.00679 <0.00339 <0.00882 0.00944 <0.0170 <0.419 <0.419 <6.79 <6.79 <6.79 <8.17 <8.17 <8.17
MW-1 (20') 07/23/19 20 0.00641 <0.00766 <0.00383 <0.00996 0.0386 <0.0192 <0.418 <0.418 <7.66 <7.66 <7.66 <8.17 <8.17 <8.17
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• Trip Blank results reported in ug/l (micrograms per liter)
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• < : Less than the method detection limit specified in the laboratory report
• Concentrations in bold face type indicate the soil to water MCCs were below the reported concentrations.
• Concentrations in italic type indicate the Residential SCLs were below the reported concentrations.
• NE: Not Established
• NR: Not Requested.
Residential SCLs (mg/kg)
RAL (mg/kg)
Soil to Water MCC (mg/kg)
Analytical Method →EPA Methods 8260D and 8270E
TABLE 6
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
SPEEDWAY #6934 (INCIDENT NO. 45185)
Facility ID #: 0-015480
MADEP EPHMADEP VPH
Page 1 of 1
Date: 01/07/2020 Facility ID # : 0-015480
EPA
504.1 EPA 6010
Well
ID
Date Sampled
(mm/dd/yy)
1 600 600 500 20 6 70 70 400 400 40 10 0.02 1 30 15 400 700 200 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 25,000 30,000 28,500 25,000 40,000 10,000 50 1,000 12,500 15,000 NE NE NE NE NE NE
07/23/19 18,600 40,600 3,960 19,300 107,000 661 128 380 2,590 680 28,500 73,800 10.6 51.3 99.0 10.6 11,800 <10,000 <10,000 <125 <125 <125
12/19/19 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
MW-2 12/19/19 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <50.0 <5.0 <0.0100 NR NR <5.00 <100 <100 <100 NR NR NR
MW-3 12/19/19 2,970 26,700 1,580 10,200 70.9 189 <20.0 132 1,170 375 16,100 648 <0.0100 NR NR 5.29 20,000 <500 4,620 NR NR NR
MW-4 12/19/19 <1.00 2.94 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 <50.0 75.7 <0.0100 NR NR 5.94 129 <100 <100 NR NR NR
07/23/19 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR NR NR NR NR NR NR NR NR
12/19/19 <1.00 <1.00 <1.00 <3.00 <1.00 <5.00 <1.00 <1.00 <1.00 <1.00 NR NR NR NR NR NR NR NR NR NR NR NR
Notes:
• Results reported in micrograms per liter (µg/l).
• MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202.
• < : Less than the method detection limit specified in the laboratory report.
• GCL: Gross contamination level.
• Concentrations in bold face type indicate the MAC was below the reported concentration.
• Results in italics indicate the GCLs were below the reported concentrations.
• J: Estimated value.
• NE: Not established.
• S: Toxicity exceeds solubility, no visible sheen or free product in water or on sediment or shoreline per 15A NCAC 02B .0211 & .0220
• NR: Not reported.
• Other reported compounds above the MACs; 07/23/19: 1,2-dichloroethane, di-isopropyl ether and TAME in MW-1, 12/19/19: chloroform in MW-3. C9-C12 AliphaticsAjusted C11-C22 AromaticsUnadjusted C9-C10 AromaticsLeadGCL (μg/l)
Trip Blank
• Refer to laboratory report for other detectable concentrations which did not exceed the MACs.
EPA 625
1-Methylnaphthalene2-MethylnaphthaleneMW-1 EDBMAC (μg/l)MTBENaphthaleneIsopropylbenzenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
SPEEDWAY #6934 (INCIDENT NO. 45185)
Analytical Method

Contaminant of Concern
BenzeneTolueneEthylbenzeneXylenesMADEP VPH MADEP EPH
Unadjusted C9-C18 AliphaticsUnadjusted C19-C36 Aliphaticst-Amyl AlcoholEPA 6200B + 5 Oxygenates
tert-Butyl alcoholC5-C8 AliphaticsPage 1 of 1

APPENDICES

APPENDIX A
Water Use Questionnaire Forms

APPENDIX B
Forsyth County Property Cards

Site
MapForsyth, Forsyth County Tax AdministrationSources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, EsriJapan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, andthe GIS User Community
Address Points
Forsyth County Boundary
Streets
Parcels
Parcels - Mailing Labels
Tax Municipal Polygon
Winston-Salem
Red: Band_1
Green: Band_2
Blue: Band_3
1/20/2020, 10:14:29 AM
0 0.015 0.030.0075 mi
0 0.03 0.060.015 km
1:1,128
Forsyth County Tax AdministrationForsyth County Tax Administration
Adjacent Property
MapForsyth, Forsyth County Tax AdministrationSources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, EsriJapan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, andthe GIS User Community
Address Points
Forsyth County Boundary
Streets
Parcels
Parcels - Mailing Labels
Tax Municipal Polygon
Winston-Salem
Red: Band_1
Green: Band_2
Blue: Band_3
1/20/2020, 10:16:07 AM
0 0.015 0.030.0075 mi
0 0.03 0.060.015 km
1:1,128
Forsyth County Tax AdministrationForsyth County Tax Administration
Adjacent Property
MapForsyth, Forsyth County Tax AdministrationSources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, EsriJapan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, andthe GIS User Community
Address Points
Forsyth County Boundary
Streets
Parcels
Parcels - Mailing Labels
Tax Municipal Polygon
Winston-Salem
Red: Band_1
Green: Band_2
Blue: Band_3
1/20/2020, 10:17:23 AM
0 0.035 0.070.0175 mi
0 0.06 0.120.03 km
1:2,257
Forsyth County Tax AdministrationForsyth County Tax Administration
Adjacent Property
MapForsyth, Forsyth County Tax AdministrationSources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, EsriJapan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, andthe GIS User Community
Address Points
Forsyth County Boundary
Streets
Parcels
Parcels - Mailing Labels
Tax Municipal Polygon
Winston-Salem
Red: Band_1
Green: Band_2
Blue: Band_3
1/20/2020, 10:15:36 AM
0 0.015 0.030.0075 mi
0 0.03 0.060.015 km
1:1,128
Forsyth County Tax AdministrationForsyth County Tax Administration
Adjacent Property
MapForsyth, Forsyth County Tax AdministrationSources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, EsriJapan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, andthe GIS User Community
Address Points
Forsyth County Boundary
Streets
Parcels
Parcels - Mailing Labels
Tax Municipal Polygon
Winston-Salem
Red: Band_1
Green: Band_2
Blue: Band_3
1/20/2020, 10:19:05 AM
0 0.035 0.070.0175 mi
0 0.06 0.120.03 km
1:2,257
Forsyth County Tax AdministrationForsyth County Tax Administration
Adjacent Property
MapForsyth, Forsyth County Tax AdministrationSources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, EsriJapan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, andthe GIS User Community
Address Points
Forsyth County Boundary
Streets
Parcels
Parcels - Mailing Labels
Tax Municipal Polygon
Winston-Salem
Red: Band_1
Green: Band_2
Blue: Band_3
1/20/2020, 10:18:29 AM
0 0.035 0.070.0175 mi
0 0.06 0.120.03 km
1:2,257
Forsyth County Tax AdministrationForsyth County Tax Administration
WSW-1
MapForsyth, Forsyth County Tax AdministrationSources: Esri, HERE, Garmin, Intermap, increment P Corp., GEBCO, USGS,FAO, NPS, NRCAN, GeoBase, IGN, Kadaster NL, Ordnance Survey, EsriJapan, METI, Esri China (Hong Kong), (c) OpenStreetMap contributors, andthe GIS User Community
Address Points
Forsyth County Boundary
Streets
Parcels
Parcels - Mailing Labels
Tax Municipal Polygon
Winston-Salem
Red: Band_1
Green: Band_2
Blue: Band_3
1/20/2020, 10:20:43 AM
0 0.0095 0.0190.00475 mi
0 0.015 0.030.0075 km
1:564
Forsyth County Tax AdministrationForsyth County Tax Administration
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APPENDIX C
Well Construction Records and Subsurface Logs
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:

Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:

Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Corey N. Buchanan
4417-B
Geological Resources, Inc.
NA
07/23/19 MW-1
Speedway #6934 / Speedway, LLC.0-015480
566 Old Hollow Road, Winston-Salem, 27105
Forsyth 6829-92-5083
36.194573 80.255148
40
27.71
6
Auger
08/06/19
27.71 40 Saturated
0 20 2 SCH 40 PVC
20 40 2 0.010 SCH 40 PVC
0
16
18
16
18
40
Grout
Bentonite 3/8" chips
Sand GP #3 Pour
Pour
0
0.1
6
23
0.1
6
23
40
Asphalt
Air knife, no lithology logged
Brown silt
Red silt
Finished with flush mounted manhole and pad.
Pour
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #6934
Address 566 Old Hollow Road, Winston-Salem, NC
Boring Number MW-1 Date Drilled
Sample Method Grab Drilling Method 6" solid stem augers
Completion DetailsWell installed at completion to a total depth of 40 feet with a 20 foot screened interval
Driller Geological Resources, Inc.Log By Corey Buchanan
Lab Sample PIDDepthSampleInterval(ft)ppm LITHOLOGY
0
3
5 13.8
6
9
MW-1 (10') 10 30.1
12
15 15 55.4

18
MW-1 (20') 20 32.9
21
24
25 283.9
27
30 30 898.6
33
35 463.0
36
39
40 557.2
42

45
48
51

54
Odors at 10'
Strong odors between 15' to 40'
07/23/19
0'-0.1' Asphalt
0.1'-6' Preclear with airknife, no lithology returned
6'-23' Brown silt
Moist at 30-35'
Wet at 35-40'
Well set at 40'
23'-40' Red silt
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:

Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:

Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Sam Bowers
3220-A
Geological Resources, Inc.
NA
12/19/19 MW-2
Speedway #6934 / Speedway, LLC.0-015480
566 Old Hollow Road, Winston-Salem, 27105
Forsyth 6829-92-5083
36.194573 80.255148
35
25.91
6
Auger
12/30/19
25.91 35 Saturated
0 20 2 SCH 40 PVC
20 35 2 0.010 SCH 40 PVC
0
16
18
16
18
35
Grout
Bentonite 3/8" chips
Sand GP #2 Pour
Pour
0
6
6
35
Air knife, no lithology logged
Red silt
Finished with flush mounted manhole and pad.
Pour
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #6934
Address 566 Old Hollow Road, Winston-Salem, NC
Boring Number MW-2 Date Drilled
Sample Method Grab Drilling Method 6" solid stem augers
Completion DetailsWell installed to a total depth of 35 feet with a 15 foot screened interval
Driller Geological Resources, Inc.Log By Alex Lin
Lab Sample PIDDepthSampleInterval(ft)ppm LITHOLOGY
0
3
6
9
10 0.3
12
15

18
20 0.0
21
24

27
30
33

36
39
42

45
48
51

54
Well set at 35'
12/19/19
0'-6' Preclear with airknife, no lithology returned
6'-35' Red silt, moist at 30'
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:

Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:

Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Sam Bowers
3220-A
Geological Resources, Inc.
NA
12/19/19 MW-3
Speedway #6934 / Speedway, LLC.0-015480
566 Old Hollow Road, Winston-Salem, 27105
Forsyth 6829-92-5083
36.194573 80.255148
35
31.07
6
Auger
12/30/19
31.07 35 Saturated
0 20 2 SCH 40 PVC
20 35 2 0.010 SCH 40 PVC
0
16
18
16
18
35
Grout
Bentonite 3/8" chips
Sand GP #2 Pour
Pour
0
6
8
6
8
35
Air knife, no lithology logged
Reddish brown silt
Brown silt with minor clay, slight odor at 30'
Finished with flush mounted manhole and pad.
Pour
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #6934
Address 566 Old Hollow Road, Winston-Salem, NC
Boring Number MW-3 Date Drilled
Sample Method Grab Drilling Method 6" solid stem augers
Completion DetailsWell installed to a total depth of 35 feet with a 15 foot screened interval
Driller Geological Resources, Inc.Log By Alex Lin
Lab Sample PIDDepthSampleInterval(ft)ppm LITHOLOGY
0
3
6
9
10 0.0
12
15 15 0.0

18
20 0.8
21
24
25 39.8
27
30 30 25.9
33
35 17.4
36
39
42

45
48
51

54
Well set at 35'
6'-8' Redish brown silt
8'-35' Brown silt with minor clay, moist and slight odor at 30'
12/19/19
0'-6' Preclear with airknife, no lithology returned
WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:
Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)
3. Well Use (check well use):
Water Supply Well:
Agricultural Municipal/Public
Geothermal (Heating/Cooling Supply) Residential Water Supply (single)
Industrial/Commercial Residential Water Supply (shared)
Irrigation
Non-Water Supply Well:
Monitoring Recovery
Injection Well:
Aquifer Recharge Groundwater Remediation
Aquifer Storage and Recovery Salinity Barrier
Aquifer Test Stormwater Drainage
Experimental Technology Subsidence Control
Geothermal (Closed Loop) Tracer
Geothermal (Heating/Cooling Return) Other (explain under #21 Remarks)
4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
6. Is(are) the well(s): Permanent or Temporary
7. Is this a repair to an existing well: Yes or No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:
9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- )
10. Static water level below top of casing: (ft.)
If water level is above casing,
11. Borehole diameter: (in.)
12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)
FOR WATER SUPPLY WELLS ONLY:
13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:

Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:

Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Sam Bowers
3220-A
Geological Resources, Inc.
NA
12/19/19 MW-4
Speedway #6934 / Speedway, LLC.0-015480
566 Old Hollow Road, Winston-Salem, 27105
Forsyth 6829-92-5083
36.194573 80.255148
30
28.82
6
Auger
12/30/19
28.82 30 Saturated
0 15 2 SCH 40 PVC
15 30 2 0.010 SCH 40 PVC
0
11
13
11
13
30
Grout
Bentonite 3/8" chips
Sand GP #2 Pour
Pour
0
6
6
30
Air knife, no lithology logged
Reddish brown silt with minor clay
Finished with flush mounted manhole and pad.
Pour
Geological Resources, Inc.Phone:[phone]
3502 Hayes Road Fax:[phone]
Monroe, NC 28110
SUBSURFACE LOG
Project Speedway #6934
Address 566 Old Hollow Road, Winston-Salem, NC
Boring Number MW-4 Date Drilled
Sample Method Grab Drilling Method 6" solid stem augers
Completion DetailsWell installed to a total depth of 30 feet with a 15 foot screened interval
Driller Geological Resources, Inc.Log By Alex Lin
Lab Sample PID
Depth Sample Interval(ft)ppm LITHOLOGY
0
3
6
9
10 1.3
12
15

18
20 1.7
21
24

27
30 30 1.3
33

36
39
42

45
48
51

54
Well set at 30'
6'-30' Redish brown silt with minor clay, moist at 22'
12/19/19
0'-6' Preclear with airknife, no lithology returned

APPENDIX D
State Correspondence

Site Name City / County /Forsyth Incident #45185
Resp Pty Name / Contact Incident Mgr Region WS
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #1
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:1 ChangeOrd:1
Project Mgr Email Site Risk / Rank / Abatement:RRA Date:
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (T/F)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
w Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode
RO AuthProposed
Rate/Price
(Consultant)CO AuthProposed Task
Subtotal
(Consultant)
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
2.610 1 /site Y $7,089.00 y $7,089.00 $7,089.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed3
TOTAL:$7,089.00 $7,089.00 TOTAL:
Total Standard Costs (Not Third Party)$7,089.00 $7,089.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:8/21/19 by:(PM)(Reserved for RO)
RO Review:8/26/19 by:(IM)Joint UST Preapproval Confirmed By:Date1 8/27/2019
CO Review:8/26/19 by:(STF)RP or Designee Receipt Confirmation By:Date 4 8/27/2019
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supercede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be rembursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supercede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all appliable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA Ver.4/10/2019
JRA
Proposed
Units / Type
(Consultant)
Christina Schroeter
ActiveTRUE
19-444 September 2019
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
Yes
Speedway, LLC.
Geological Resources, Inc.
DIRECTED COSTS
Winston-Salem
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Speedway #6934
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be attached to
elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,you discover that
unexpected tasks must be performed,incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request designated as a "Change
Order"in the provided space above prior to conducting those tasks.Include a copy of the prior ePATAform for confirmation.Please attach this form tothe cover of the corresponding
claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been completed within 12 months of the
completion date of the FIRST completed task to remain within the Statute of Limitations.All ePATAs submitted within a claim are closed with that claim,and may not be re-used in a
separate submittal,even for costsor tasks that werenotoriginally claimed.Final reimbursementof costs associated withthe Total Claimed amount belowmay be affected by the eligibility
status of the site (i.e., deductibles, apportionment, etc.), and the documentary validation of incurred costs as reasonable and necessary expenses per 15A NCAC 2P .0402 and .0404.
CGS
HB
(Initials)
Christina Schroeter
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management

APPENDIX E
Laboratory Analytical Reports

ANALYTICAL REPORT
August 08, 2019
Geological Resources- NC Speedway
Sample Delivery Group:L1121787
Samples Received:07/24/2019
Project Number:4341
Description:Speedway 6934
Site:6934
Report To:Ms. Nicole Long
3502 Hayes Rd.
Charlotte, NC 28110
Entire Report Reviewed By:
August 08, 2019
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 1 of 53
August 08, 2019
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 1 of 53
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TRIP BLANK L1121787-01 5
MW-1 L1121787-02 7
MW-1 (10') L1121787-03 11
MW-1 (20') L1121787-04 14
Qc: Quality Control Summary 17
Total Solids by Method 2540 G-2011 17
Metals (ICP) by Method 6010D 18
Volatile Petroleum Hydrocarbons by Method MADEPV 19
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 21
Volatile Organic Compounds (GC/MS) by Method 8260D 26
EDB / DBCP by Method 504.1 28
TPH by Method MADEPE 29
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 32
Semi Volatile Organic Compounds (GC/MS) by Method 8270E 37
Gl: Glossary of Terms 43
Al: Accreditations & Locations 44
Sc: Sample Chain of Custody 45
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 2 of 53
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TRIP BLANK L1121787-01 GW Corey N. Buchanan 07/23/19 08:40 07/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1317486 1 07/25/19 19:34 07/25/19 19:34 JHH Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 L1121787-02 GW Corey N. Buchanan 07/23/19 15:12 07/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG1317099 1 07/25/19 10:56 07/26/19 13:58 CCE Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1318211 100 07/26/19 20:05 07/26/19 20:05 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1317486 50 07/25/19 21:52 07/25/19 21:52 JHH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1318206 2000 07/27/19 18:43 07/27/19 18:43 JAH Mt. Juliet, TN
EDB / DBCP by Method 504.1 WG1317171 50 07/25/19 08:46 07/26/19 11:38 KLM Mt. Juliet, TN
TPH by Method MADEPE WG1318081 1.25 07/26/19 07:29 07/27/19 11:47 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1318081 1.25 07/26/19 07:29 07/27/19 12:09 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1318962 1.43 07/30/19 06:08 07/30/19 14:57 JNJ Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1318962 7.15 07/30/19 06:08 07/30/19 18:43 JNJ Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 (10') L1121787-03 Solid Corey N. Buchanan 07/23/19 10:56 07/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1319285 1 07/30/19 11:09 07/30/19 11:18 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1318991 54 07/29/19 12:07 07/29/19 12:07 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1319377 1.08 07/23/19 10:56 07/29/19 16:06 GLN Mt. Juliet, TN
TPH by Method MADEPE WG1320617 1 07/30/19 15:28 08/01/19 16:51 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1320617 1 07/30/19 15:28 08/02/19 00:09 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1318945 1 07/28/19 16:39 07/29/19 03:07 LEL Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-1 (20') L1121787-04 Solid Corey N. Buchanan 07/23/19 11:06 07/24/19 08:45
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Total Solids by Method 2540 G-2011 WG1319285 1 07/30/19 11:09 07/30/19 11:18 KBC Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1318991 61 07/29/19 12:47 07/29/19 12:47 BMB Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D WG1319377 1.22 07/23/19 11:06 07/29/19 16:28 GLN Mt. Juliet, TN
TPH by Method MADEPE WG1320617 1 07/30/19 15:28 08/01/19 17:14 SHG Mt. Juliet, TN
TPH by Method MADEPE WG1320617 1 07/30/19 15:28 08/01/19 23:46 SHG Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1318945 1 07/28/19 16:39 07/29/19 03:26 LEL Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 3 of 53
ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
Project Narrative
Due to multiple preparation procedures, calculated analytes are not reported in the quality control samples for EPH and VPH
Methods.

1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 4 of 53
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 4 of 53
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1121787
TRIP BLANK
Collected date/time: 07/23/19 08:40
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 07/25/2019 19:34 WG1317486
1,1,1-Trichloroethane ND 1.00 1 07/25/2019 19:34 WG1317486
1,1,2,2-Tetrachloroethane ND 1.00 1 07/25/2019 19:34 WG1317486
1,1,2-Trichloroethane ND 1.00 1 07/25/2019 19:34 WG1317486
1,1-Dichloroethane ND 1.00 1 07/25/2019 19:34 WG1317486
1,1-Dichloroethene ND 1.00 1 07/25/2019 19:34 WG1317486
1,1-Dichloropropene ND 1.00 1 07/25/2019 19:34 WG1317486
1,2,3-Trichlorobenzene ND 1.00 1 07/25/2019 19:34 WG1317486
1,2,3-Trichloropropane ND 2.50 1 07/25/2019 19:34 WG1317486
1,2,3-Trimethylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
1,2,4-Trichlorobenzene ND 1.00 1 07/25/2019 19:34 WG1317486
1,2,4-Trimethylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
1,2-Dibromo-3-Chloropropane ND 5.00 1 07/25/2019 19:34 WG1317486
1,2-Dibromoethane ND 1.00 1 07/25/2019 19:34 WG1317486
1,2-Dichlorobenzene ND 1.00 1 07/25/2019 19:34 WG1317486
1,2-Dichloroethane ND 1.00 1 07/25/2019 19:34 WG1317486
1,2-Dichloropropane ND 1.00 1 07/25/2019 19:34 WG1317486
1,3,5-Trimethylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
1,3-Dichlorobenzene ND 1.00 1 07/25/2019 19:34 WG1317486
1,3-Dichloropropane ND 1.00 1 07/25/2019 19:34 WG1317486
1,4-Dichlorobenzene ND 1.00 1 07/25/2019 19:34 WG1317486
2,2-Dichloropropane ND 1.00 1 07/25/2019 19:34 WG1317486
Benzene ND 1.00 1 07/25/2019 19:34 WG1317486
Bromobenzene ND 1.00 1 07/25/2019 19:34 WG1317486
Bromochloromethane ND 1.00 1 07/25/2019 19:34 WG1317486
Bromodichloromethane ND 1.00 1 07/25/2019 19:34 WG1317486
Bromoform ND 1.00 1 07/25/2019 19:34 WG1317486
Carbon tetrachloride ND 1.00 1 07/25/2019 19:34 WG1317486
Chlorobenzene ND 1.00 1 07/25/2019 19:34 WG1317486
Chloroethane ND 5.00 1 07/25/2019 19:34 WG1317486
Chloroform ND 5.00 1 07/25/2019 19:34 WG1317486
Chlorodibromomethane ND 1.00 1 07/25/2019 19:34 WG1317486
Dichlorodifluoromethane ND 5.00 1 07/25/2019 19:34 WG1317486
Di-isopropyl ether ND 1.00 1 07/25/2019 19:34 WG1317486
Ethylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
Hexachloro-1,3-butadiene ND 1.00 1 07/25/2019 19:34 WG1317486
Isopropylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
Bromomethane ND 5.00 1 07/25/2019 19:34 WG1317486
Chloromethane ND 2.50 1 07/25/2019 19:34 WG1317486
Methyl tert-butyl ether ND 1.00 1 07/25/2019 19:34 WG1317486
Dibromomethane ND 1.00 1 07/25/2019 19:34 WG1317486
Methylene Chloride ND 5.00 1 07/25/2019 19:34 WG1317486
Naphthalene ND 5.00 1 07/25/2019 19:34 WG1317486
Styrene ND 1.00 1 07/25/2019 19:34 WG1317486
Tetrachloroethene ND 1.00 1 07/25/2019 19:34 WG1317486
Toluene ND 1.00 1 07/25/2019 19:34 WG1317486
Trichloroethene ND 1.00 1 07/25/2019 19:34 WG1317486
Trichlorofluoromethane ND 5.00 1 07/25/2019 19:34 WG1317486
Vinyl chloride ND 1.00 1 07/25/2019 19:34 WG1317486
Total Xylenes ND 3.00 1 07/25/2019 19:34 WG1317486
cis-1,2-Dichloroethene ND 1.00 1 07/25/2019 19:34 WG1317486
cis-1,3-Dichloropropene ND 1.00 1 07/25/2019 19:34 WG1317486
n-Butylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
n-Propylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
2-Chlorotoluene ND 1.00 1 07/25/2019 19:34 WG1317486
p-Isopropyltoluene ND 1.00 1 07/25/2019 19:34 WG1317486
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 5 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 5 of 53
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1121787
TRIP BLANK
Collected date/time: 07/23/19 08:40
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
4-Chlorotoluene ND 1.00 1 07/25/2019 19:34 WG1317486
sec-Butylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
tert-Butylbenzene ND 1.00 1 07/25/2019 19:34 WG1317486
trans-1,2-Dichloroethene ND 1.00 1 07/25/2019 19:34 WG1317486
trans-1,3-Dichloropropene ND 1.00 1 07/25/2019 19:34 WG1317486
(S) Toluene-d8 107 80.0-120 07/25/2019 19:34 WG1317486
(S) 4-Bromofluorobenzene 98.7 77.0-126 07/25/2019 19:34 WG1317486
(S) 1,2-Dichloroethane-d4 104 70.0-130 07/25/2019 19:34 WG1317486
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 6 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 6 of 53
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1121787
MW-1
Collected date/time: 07/23/19 15:12
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Lead 10.6 B 5.00 1 07/26/2019 13:58 WG1317099
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 178000 10000 100 07/26/2019 20:05 WG1318211
Unadjusted C9-C12 Aliphatics 40900 10000 100 07/26/2019 20:05 WG1318211
Unadjusted C9-C10 Aromatics ND 10000 100 07/26/2019 20:05 WG1318211
Adjusted C5-C8 Aliphatics 11800 10000 100 07/26/2019 20:05 WG1318211
Adjusted C9-C12 Aliphatics ND 10000 100 07/26/2019 20:05 WG1318211
Total VPH 227000 20000 100 07/26/2019 20:05 WG1318211
Total Purgeable Hydrocarbons C5-C12 220000 20000 100 07/26/2019 20:05 WG1318211
(S) 2,5-Dibromotoluene(FID)90.5 70.0-130 07/26/2019 20:05 WG1318211
(S) 2,5-Dibromotoluene(PID)83.0 70.0-130 07/26/2019 20:05 WG1318211
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 50.0 50 07/25/2019 21:52 WG1317486
1,1,1-Trichloroethane ND 50.0 50 07/25/2019 21:52 WG1317486
1,1,2,2-Tetrachloroethane ND 50.0 50 07/25/2019 21:52 WG1317486
1,1,2-Trichloroethane ND 50.0 50 07/25/2019 21:52 WG1317486
1,1-Dichloroethane ND 50.0 50 07/25/2019 21:52 WG1317486
1,1-Dichloroethene ND 50.0 50 07/25/2019 21:52 WG1317486
1,1-Dichloropropene ND 50.0 50 07/25/2019 21:52 WG1317486
1,2,3-Trichlorobenzene ND 50.0 50 07/25/2019 21:52 WG1317486
1,2,3-Trichloropropane ND 125 50 07/25/2019 21:52 WG1317486
1,2,3-Trimethylbenzene 930 50.0 50 07/25/2019 21:52 WG1317486
1,2,4-Trichlorobenzene ND 50.0 50 07/25/2019 21:52 WG1317486
1,2,4-Trimethylbenzene 2590 50.0 50 07/25/2019 21:52 WG1317486
1,2-Dibromo-3-Chloropropane ND 250 50 07/25/2019 21:52 WG1317486
1,2-Dibromoethane ND 50.0 50 07/25/2019 21:52 WG1317486
1,2-Dichlorobenzene ND 50.0 50 07/25/2019 21:52 WG1317486
1,2-Dichloroethane 56.8 50.0 50 07/25/2019 21:52 WG1317486
1,2-Dichloropropane ND 50.0 50 07/25/2019 21:52 WG1317486
1,3,5-Trimethylbenzene 680 50.0 50 07/25/2019 21:52 WG1317486
1,3-Dichlorobenzene ND 50.0 50 07/25/2019 21:52 WG1317486
1,3-Dichloropropane ND 50.0 50 07/25/2019 21:52 WG1317486
1,4-Dichlorobenzene ND 50.0 50 07/25/2019 21:52 WG1317486
2,2-Dichloropropane ND 50.0 50 07/25/2019 21:52 WG1317486
Benzene 18600 2000 2000 07/27/2019 18:43 WG1318206
Bromobenzene ND 50.0 50 07/25/2019 21:52 WG1317486
Bromochloromethane ND 50.0 50 07/25/2019 21:52 WG1317486
Bromodichloromethane ND 50.0 50 07/25/2019 21:52 WG1317486
Bromoform ND 50.0 50 07/25/2019 21:52 WG1317486
Carbon tetrachloride ND 50.0 50 07/25/2019 21:52 WG1317486
Chlorobenzene ND 50.0 50 07/25/2019 21:52 WG1317486
Chloroethane ND 250 50 07/25/2019 21:52 WG1317486
Chloroform ND 250 50 07/25/2019 21:52 WG1317486
Chlorodibromomethane ND 50.0 50 07/25/2019 21:52 WG1317486
Dichlorodifluoromethane ND 250 50 07/25/2019 21:52 WG1317486
Di-isopropyl ether 300 50.0 50 07/25/2019 21:52 WG1317486
Ethanol ND 5000 50 07/25/2019 21:52 WG1317486
Ethylbenzene 3960 50.0 50 07/25/2019 21:52 WG1317486
Hexachloro-1,3-butadiene ND 50.0 50 07/25/2019 21:52 WG1317486
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 7 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 7 of 53
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1121787
MW-1
Collected date/time: 07/23/19 15:12
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isopropylbenzene 128 50.0 50 07/25/2019 21:52 WG1317486
Bromomethane ND 250 50 07/25/2019 21:52 WG1317486
Chloromethane ND 125 50 07/25/2019 21:52 WG1317486
Methyl tert-butyl ether 107000 2000 2000 07/27/2019 18:43 WG1318206
Dibromomethane ND 50.0 50 07/25/2019 21:52 WG1317486
Methylene Chloride ND 250 50 07/25/2019 21:52 WG1317486
Naphthalene 661 250 50 07/25/2019 21:52 WG1317486
Styrene ND 50.0 50 07/25/2019 21:52 WG1317486
Tetrachloroethene ND 50.0 50 07/25/2019 21:52 WG1317486
Toluene 40600 2000 2000 07/27/2019 18:43 WG1318206
Trichloroethene ND 50.0 50 07/25/2019 21:52 WG1317486
Trichlorofluoromethane ND 250 50 07/25/2019 21:52 WG1317486
Vinyl chloride ND 50.0 50 07/25/2019 21:52 WG1317486
Total Xylenes 19300 150 50 07/25/2019 21:52 WG1317486
cis-1,2-Dichloroethene ND 50.0 50 07/25/2019 21:52 WG1317486
cis-1,3-Dichloropropene ND 50.0 50 07/25/2019 21:52 WG1317486
n-Butylbenzene ND 50.0 50 07/25/2019 21:52 WG1317486
n-Propylbenzene 380 50.0 50 07/25/2019 21:52 WG1317486
2-Chlorotoluene ND 50.0 50 07/25/2019 21:52 WG1317486
p-Isopropyltoluene ND 50.0 50 07/25/2019 21:52 WG1317486
4-Chlorotoluene ND 50.0 50 07/25/2019 21:52 WG1317486
sec-Butylbenzene ND 50.0 50 07/25/2019 21:52 WG1317486
tert-Butylbenzene ND 50.0 50 07/25/2019 21:52 WG1317486
trans-1,2-Dichloroethene ND 50.0 50 07/25/2019 21:52 WG1317486
trans-1,3-Dichloropropene ND 50.0 50 07/25/2019 21:52 WG1317486
Ethyl tert-butyl ether ND 50.0 50 07/25/2019 21:52 WG1317486
t-Amyl Alcohol 28500 2500 50 07/25/2019 21:52 WG1317486
tert-Butyl alcohol 73800 10000 2000 07/27/2019 18:43 WG1318206
tert-Amyl Methyl Ether 642 50.0 50 07/25/2019 21:52 WG1317486
Tert-Amyl Ethyl Ether ND 50.0 50 07/25/2019 21:52 WG1317486
tert-Butyl Formate ND 1000 50 07/25/2019 21:52 WG1317486
(S) Toluene-d8 109 80.0-120 07/25/2019 21:52 WG1317486
(S) Toluene-d8 106 80.0-120 07/27/2019 18:43 WG1318206
(S) 1,2-Dichloroethane-d4 110 70.0-130 07/25/2019 21:52 WG1317486
(S) 1,2-Dichloroethane-d4 113 70.0-130 07/27/2019 18:43 WG1318206
(S) 4-Bromofluorobenzene 96.8 77.0-126 07/25/2019 21:52 WG1317486
(S) 4-Bromofluorobenzene 96.6 77.0-126 07/27/2019 18:43 WG1318206
EDB / DBCP by Method 504.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ethylene Dibromide 10.6 0.500 50 07/26/2019 11:38 WG1317171
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C9-C18 Aliphatics ND 125 1.25 07/27/2019 11:47 WG1318081
Unadjusted C19-C36 Aliphatics ND 125 1.25 07/27/2019 11:47 WG1318081
Unadjusted C11-C22 Aromatics 920 125 1.25 07/27/2019 12:09 WG1318081
Unadjusted Total Petroleum Hydrocarbons 974 125 1.25 07/27/2019 12:09 WG1318081
Adjusted C11-C22 Aromatics ND 125 1.25 07/27/2019 12:09 WG1318081
Adjusted Total Petroleum Hydrocarbons ND 125 1.25 07/27/2019 12:09 WG1318081
(S) o-Terphenyl 66.6 40.0-140 07/27/2019 12:09 WG1318081
(S) 1-Chloro-octadecane 72.6 40.0-140 07/27/2019 11:47 WG1318081
(S) 2-Fluorobiphenyl 88.7 40.0-140 07/27/2019 12:09 WG1318081
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 8 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 8 of 53
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1121787
MW-1
Collected date/time: 07/23/19 15:12
TPH by Method MADEPE
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
(S) 2-Bromonaphthalene 84.4 40.0-140 07/27/2019 12:09 WG1318081
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1-Methylnaphthalene 51.3 J4 1.43 1.43 07/30/2019 14:57 WG1318962
2,4,6-Trichlorophenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
2,4-Dichlorophenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
2,4-Dimethylphenol 37.8 14.3 1.43 07/30/2019 14:57 WG1318962
2,4-Dinitrophenol ND 71.5 1.43 07/30/2019 14:57 WG1318962
2,4-Dinitrotoluene ND 14.3 1.43 07/30/2019 14:57 WG1318962
2,6-Dinitrotoluene ND 14.3 1.43 07/30/2019 14:57 WG1318962
2-Chloronaphthalene ND J4 1.43 1.43 07/30/2019 14:57 WG1318962
2-Chlorophenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
2-Methylnaphthalene 99.0 J4 1.43 1.43 07/30/2019 14:57 WG1318962
2-Methylphenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
2-Nitrophenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
3,3-Dichlorobenzidine ND 14.3 1.43 07/30/2019 14:57 WG1318962
3&4-Methyl Phenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
4,6-Dinitro-2-methylphenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
4-Bromophenyl-phenylether ND J4 14.3 1.43 07/30/2019 14:57 WG1318962
4-Chloro-3-methylphenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
4-Chloroaniline ND J4 14.3 1.43 07/30/2019 14:57 WG1318962
4-Chlorophenyl-phenylether ND 14.3 1.43 07/30/2019 14:57 WG1318962
4-Nitrophenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
Acenaphthene ND J4 1.43 1.43 07/30/2019 14:57 WG1318962
Acenaphthylene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Anthracene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Benzo(a)anthracene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Benzo(a)pyrene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Benzo(b)fluoranthene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Benzo(g,h,i)perylene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Benzo(k)fluoranthene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Benzoic acid ND J4 14.3 1.43 07/30/2019 14:57 WG1318962
Bis(2-chlorethoxy)methane ND 14.3 1.43 07/30/2019 14:57 WG1318962
Bis(2-chloroisopropyl)ether ND J4 14.3 1.43 07/30/2019 14:57 WG1318962
Bis(2-ethylhexyl)phthalate ND 4.29 1.43 07/30/2019 14:57 WG1318962
Benzylbutyl phthalate ND 4.29 1.43 07/30/2019 14:57 WG1318962
Chrysene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Di-n-butyl phthalate ND 4.29 1.43 07/30/2019 14:57 WG1318962
Di-n-octyl phthalate ND 4.29 1.43 07/30/2019 14:57 WG1318962
Dibenz(a,h)anthracene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Dibenzofuran ND J4 14.3 1.43 07/30/2019 14:57 WG1318962
Diethyl phthalate ND 4.29 1.43 07/30/2019 14:57 WG1318962
Dimethyl phthalate ND 4.29 1.43 07/30/2019 14:57 WG1318962
Fluoranthene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Fluorene ND J4 1.43 1.43 07/30/2019 14:57 WG1318962
Hexachlorobenzene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Hexachloro-1,3-butadiene ND 14.3 1.43 07/30/2019 14:57 WG1318962
Hexachlorocyclopentadiene ND 14.3 1.43 07/30/2019 14:57 WG1318962
Hexachloroethane ND J4 14.3 1.43 07/30/2019 14:57 WG1318962
Indeno(1,2,3-cd)pyrene ND 1.43 1.43 07/30/2019 14:57 WG1318962
Isophorone ND 14.3 1.43 07/30/2019 14:57 WG1318962
n-Nitrosodi-n-propylamine ND 14.3 1.43 07/30/2019 14:57 WG1318962
n-Nitrosodiphenylamine ND 14.3 1.43 07/30/2019 14:57 WG1318962
Naphthalene 405 7.15 7.15 07/30/2019 18:43 WG1318962
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 9 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 9 of 53
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1121787
MW-1
Collected date/time: 07/23/19 15:12
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Nitrobenzene ND 14.3 1.43 07/30/2019 14:57 WG1318962
Pentachlorophenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
Phenanthrene ND J4 1.43 1.43 07/30/2019 14:57 WG1318962
Phenol ND 14.3 1.43 07/30/2019 14:57 WG1318962
Pyrene ND J4 1.43 1.43 07/30/2019 14:57 WG1318962
(S) 2-Fluorophenol 36.7 10.0-120 07/30/2019 14:57 WG1318962
(S) 2-Fluorophenol 44.4 10.0-120 07/30/2019 18:43 WG1318962
(S) Phenol-d5 0.000 J2 8.00-424 07/30/2019 14:57 WG1318962
(S) Phenol-d5 0.000 J2 8.00-424 07/30/2019 18:43 WG1318962
(S) Nitrobenzene-d5 44.5 15.0-314 07/30/2019 14:57 WG1318962
(S) Nitrobenzene-d5 28.7 15.0-314 07/30/2019 18:43 WG1318962
(S) 2-Fluorobiphenyl 39.9 22.0-127 07/30/2019 18:43 WG1318962
(S) 2-Fluorobiphenyl 50.3 22.0-127 07/30/2019 14:57 WG1318962
(S) 2,4,6-Tribromophenol 48.6 10.0-153 07/30/2019 18:43 WG1318962
(S) 2,4,6-Tribromophenol 59.1 10.0-153 07/30/2019 14:57 WG1318962
(S) p-Terphenyl-d14 55.5 29.0-141 07/30/2019 14:57 WG1318962
(S) p-Terphenyl-d14 42.7 29.0-141 07/30/2019 18:43 WG1318962
Sample Narrative:
L1121787-02 WG1318962: Duplicate analysis was performed.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier RDL Dilution Analysis Batch CAS #
Analyte ug/l ug/l date / time
2-Pentanol, 2-Methyl-848 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000590-36-3
Toluene 5040 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000108-88-3
P-Xylene 1900 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000106-42-3
Unknown-02 845 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000064-04-0
2-Pentanol, 2-Methyl-1720 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000590-36-3
Benzene, 1,3-Dimethyl-723 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000108-38-3
Unknown-01 706 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000077-74-7
Unknown-01 1440 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000077-74-7
Benzene, 1,3,5-Trimethyl-584 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000108-67-8
Ethylbenzene 1220 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000100-41-4
Cyclopentanol, 1-Methyl-1210 J N 0.000 7.15 07/30/2019 18:43 WG1318962 001462-03-9
Cyclopentanol, 1-Methyl-548 J N 0.000 1.43 07/30/2019 14:57 WG1318962 001462-03-9
Benzene, 1-Ethyl-3-Methyl-1120 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000620-14-4
Ethylbenzene 465 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000100-41-4
Benzene, 1-Ethyl-2-Methyl-348 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000611-14-3
3-Hexanol, 3-Methyl-336 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000597-96-6
Unknown-02 679 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000625-23-0
3-Hexanol, 3-Methyl-672 J N 0.000 7.15 07/30/2019 18:43 WG1318962 000597-96-6
Unknown-03 322 J N 0.000 1.43 07/30/2019 14:57 WG1318962 000625-23-0
2-Cyclopenten-1-One, 2-Methyl-587 J N 0.000 7.15 07/30/2019 18:43 WG1318962 001120-73-6
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICs are identified and quantitated using individual standards. TIC
listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is
accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is
10% or more of that of the nearest internal standard.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 10 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1121787
MW-1 (10')
Collected date/time: 07/23/19 10:56
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.5 1 07/30/2019 11:18 WG1319285
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics ND 6.79 54 07/29/2019 12:07 WG1318991
Unadjusted C9-C12 Aliphatics ND 6.79 54 07/29/2019 12:07 WG1318991
Unadjusted C9-C10 Aromatics ND 6.79 54 07/29/2019 12:07 WG1318991
Adjusted C5-C8 Aliphatics ND 6.79 54 07/29/2019 12:07 WG1318991
Adjusted C9-C12 Aliphatics ND 6.79 54 07/29/2019 12:07 WG1318991
Total VPH ND 13.6 54 07/29/2019 12:07 WG1318991
Total Purgeable Hydrocarbons C5-C12 ND 13.6 54 07/29/2019 12:07 WG1318991
(S) 2,5-Dibromotoluene(FID)99.5 70.0-130 07/29/2019 12:07 WG1318991
(S) 2,5-Dibromotoluene(PID)104 70.0-130 07/29/2019 12:07 WG1318991
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,2,3-Trichlorobenzene ND 0.00339 1.08 07/29/2019 16:06 WG1319377
1,2,4-Trichlorobenzene ND 0.0170 1.08 07/29/2019 16:06 WG1319377
1,2,4-Trimethylbenzene ND 0.00679 1.08 07/29/2019 16:06 WG1319377
1,2-Dibromoethane ND 0.00339 1.08 07/29/2019 16:06 WG1319377
1,2-Dichloroethane ND 0.00339 1.08 07/29/2019 16:06 WG1319377
1,3,5-Trimethylbenzene ND 0.00679 1.08 07/29/2019 16:06 WG1319377
2-Butanone (MEK)0.515 0.0339 1.08 07/29/2019 16:06 WG1319377
Acetone 0.249 0.0339 1.08 07/29/2019 16:06 WG1319377
Benzene 0.00650 0.00136 1.08 07/29/2019 16:06 WG1319377
Di-isopropyl ether ND 0.00136 1.08 07/29/2019 16:06 WG1319377
Ethylbenzene ND 0.00339 1.08 07/29/2019 16:06 WG1319377
Isopropylbenzene ND 0.00339 1.08 07/29/2019 16:06 WG1319377
Methyl tert-butyl ether 0.00944 0.00136 1.08 07/29/2019 16:06 WG1319377
Methylene Chloride ND 0.0339 1.08 07/29/2019 16:06 WG1319377
Naphthalene ND 0.0170 1.08 07/29/2019 16:06 WG1319377
Styrene ND 0.0170 1.08 07/29/2019 16:06 WG1319377
Toluene ND 0.00679 1.08 07/29/2019 16:06 WG1319377
Xylenes, Total ND 0.00882 1.08 07/29/2019 16:06 WG1319377
n-Butylbenzene ND 0.0170 1.08 07/29/2019 16:06 WG1319377
n-Propylbenzene ND 0.00679 1.08 07/29/2019 16:06 WG1319377
sec-Butylbenzene ND 0.0170 1.08 07/29/2019 16:06 WG1319377
tert-Butylbenzene ND 0.00679 1.08 07/29/2019 16:06 WG1319377
(S) Toluene-d8 104 75.0-131 07/29/2019 16:06 WG1319377
(S) 4-Bromofluorobenzene 97.8 67.0-138 07/29/2019 16:06 WG1319377
(S) 1,2-Dichloroethane-d4 103 70.0-130 07/29/2019 16:06 WG1319377
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics ND 8.17 1 08/01/2019 16:51 WG1320617
Unadjusted C19-C36 Aliphatics ND 8.17 1 08/01/2019 16:51 WG1320617
Unadjusted C11-C22 Aromatics ND 8.17 1 08/02/2019 00:09 WG1320617
Unadjusted Total Petroleum Hydrocarbons ND 8.17 1 08/01/2019 16:51 WG1320617
Adjusted C11-C22 Aromatics ND 8.17 1 08/02/2019 00:09 WG1320617
Adjusted Total Petroleum Hydrocarbons ND 8.17 1 08/01/2019 16:51 WG1320617
(S) o-Terphenyl 54.9 40.0-140 08/02/2019 00:09 WG1320617
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1121787
MW-1 (10')
Collected date/time: 07/23/19 10:56
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
(S) 1-Chloro-octadecane 53.4 40.0-140 08/01/2019 16:51 WG1320617
(S) 2-Fluorobiphenyl 81.4 40.0-140 08/02/2019 00:09 WG1320617
(S) 2-Bromonaphthalene 79.5 40.0-140 08/02/2019 00:09 WG1320617
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0419 1 07/29/2019 03:07 WG1318945
Acenaphthylene ND 0.0419 1 07/29/2019 03:07 WG1318945
Anthracene ND 0.0419 1 07/29/2019 03:07 WG1318945
Benzo(a)anthracene ND 0.0419 1 07/29/2019 03:07 WG1318945
Benzo(b)fluoranthene ND 0.0419 1 07/29/2019 03:07 WG1318945
Benzo(k)fluoranthene ND 0.0419 1 07/29/2019 03:07 WG1318945
Benzo(g,h,i)perylene ND 0.0419 1 07/29/2019 03:07 WG1318945
Benzo(a)pyrene ND 0.0419 1 07/29/2019 03:07 WG1318945
Bis(2-chlorethoxy)methane ND 0.419 1 07/29/2019 03:07 WG1318945
Bis(2-chloroethyl)ether ND 0.419 1 07/29/2019 03:07 WG1318945
Bis(2-chloroisopropyl)ether ND 0.419 1 07/29/2019 03:07 WG1318945
4-Bromophenyl-phenylether ND 0.419 1 07/29/2019 03:07 WG1318945
4-Chloroaniline ND 0.419 1 07/29/2019 03:07 WG1318945
2-Chloronaphthalene ND 0.0419 1 07/29/2019 03:07 WG1318945
4-Chlorophenyl-phenylether ND 0.419 1 07/29/2019 03:07 WG1318945
Chrysene ND 0.0419 1 07/29/2019 03:07 WG1318945
Dibenz(a,h)anthracene ND 0.0419 1 07/29/2019 03:07 WG1318945
Dibenzofuran ND 0.419 1 07/29/2019 03:07 WG1318945
3,3-Dichlorobenzidine ND 0.419 1 07/29/2019 03:07 WG1318945
2,4-Dinitrotoluene ND 0.419 1 07/29/2019 03:07 WG1318945
2,6-Dinitrotoluene ND 0.419 1 07/29/2019 03:07 WG1318945
Fluoranthene ND 0.0419 1 07/29/2019 03:07 WG1318945
Fluorene ND 0.0419 1 07/29/2019 03:07 WG1318945
Hexachlorobenzene ND 0.419 1 07/29/2019 03:07 WG1318945
Hexachloro-1,3-butadiene ND 0.419 1 07/29/2019 03:07 WG1318945
Hexachlorocyclopentadiene ND 0.419 1 07/29/2019 03:07 WG1318945
Hexachloroethane ND 0.419 1 07/29/2019 03:07 WG1318945
Indeno(1,2,3-cd)pyrene ND 0.0419 1 07/29/2019 03:07 WG1318945
Isophorone ND 0.419 1 07/29/2019 03:07 WG1318945
1-Methylnaphthalene ND 0.419 1 07/29/2019 03:07 WG1318945
2-Methylnaphthalene ND 0.419 1 07/29/2019 03:07 WG1318945
Naphthalene ND 0.0419 1 07/29/2019 03:07 WG1318945
Nitrobenzene ND 0.419 1 07/29/2019 03:07 WG1318945
n-Nitrosodiphenylamine ND 0.419 1 07/29/2019 03:07 WG1318945
n-Nitrosodi-n-propylamine ND 0.419 1 07/29/2019 03:07 WG1318945
Phenanthrene ND 0.0419 1 07/29/2019 03:07 WG1318945
Benzylbutyl phthalate ND 0.419 1 07/29/2019 03:07 WG1318945
Bis(2-ethylhexyl)phthalate ND 0.419 1 07/29/2019 03:07 WG1318945
Di-n-butyl phthalate ND 0.419 1 07/29/2019 03:07 WG1318945
Diethyl phthalate ND 0.419 1 07/29/2019 03:07 WG1318945
Dimethyl phthalate ND 0.419 1 07/29/2019 03:07 WG1318945
Di-n-octyl phthalate ND 0.419 1 07/29/2019 03:07 WG1318945
Pyrene ND 0.0419 1 07/29/2019 03:07 WG1318945
Benzoic acid ND 0.419 1 07/29/2019 03:07 WG1318945
4-Chloro-3-methylphenol ND 0.419 1 07/29/2019 03:07 WG1318945
2-Chlorophenol ND 0.419 1 07/29/2019 03:07 WG1318945
2-Methylphenol ND 0.419 1 07/29/2019 03:07 WG1318945
3&4-Methyl Phenol ND 0.419 1 07/29/2019 03:07 WG1318945
2,4-Dichlorophenol ND 0.419 1 07/29/2019 03:07 WG1318945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1121787
MW-1 (10')
Collected date/time: 07/23/19 10:56
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2,4-Dimethylphenol ND 0.419 1 07/29/2019 03:07 WG1318945
4,6-Dinitro-2-methylphenol ND 0.419 1 07/29/2019 03:07 WG1318945
2,4-Dinitrophenol ND 0.419 1 07/29/2019 03:07 WG1318945
2-Nitrophenol ND 0.419 1 07/29/2019 03:07 WG1318945
4-Nitrophenol ND 0.419 1 07/29/2019 03:07 WG1318945
Pentachlorophenol ND 0.419 1 07/29/2019 03:07 WG1318945
Phenol ND 0.419 1 07/29/2019 03:07 WG1318945
2,4,6-Trichlorophenol ND 0.419 1 07/29/2019 03:07 WG1318945
(S) 2-Fluorophenol 63.2 12.0-120 07/29/2019 03:07 WG1318945
(S) Phenol-d5 55.7 10.0-120 07/29/2019 03:07 WG1318945
(S) Nitrobenzene-d5 47.9 10.0-122 07/29/2019 03:07 WG1318945
(S) 2-Fluorobiphenyl 58.7 15.0-120 07/29/2019 03:07 WG1318945
(S) 2,4,6-Tribromophenol 96.2 10.0-127 07/29/2019 03:07 WG1318945
(S) p-Terphenyl-d14 66.6 10.0-120 07/29/2019 03:07 WG1318945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1121787
MW-1 (20')
Collected date/time: 07/23/19 11:06
Total Solids by Method 2540 G-2011
Result Qualifier Dilution Analysis Batch
Analyte %date / time
Total Solids 79.6 1 07/30/2019 11:18 WG1319285
Volatile Petroleum Hydrocarbons by Method MADEPV
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C5-C8 Aliphatics ND 7.66 61 07/29/2019 12:47 WG1318991
Unadjusted C9-C12 Aliphatics ND 7.66 61 07/29/2019 12:47 WG1318991
Unadjusted C9-C10 Aromatics ND 7.66 61 07/29/2019 12:47 WG1318991
Adjusted C5-C8 Aliphatics ND 7.66 61 07/29/2019 12:47 WG1318991
Adjusted C9-C12 Aliphatics ND 7.66 61 07/29/2019 12:47 WG1318991
Total VPH ND 15.3 61 07/29/2019 12:47 WG1318991
Total Purgeable Hydrocarbons C5-C12 ND 15.3 61 07/29/2019 12:47 WG1318991
(S) 2,5-Dibromotoluene(FID)101 70.0-130 07/29/2019 12:47 WG1318991
(S) 2,5-Dibromotoluene(PID)105 70.0-130 07/29/2019 12:47 WG1318991
Volatile Organic Compounds (GC/MS) by Method 8260D
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
1,2,3-Trichlorobenzene ND 0.00383 1.22 07/29/2019 16:28 WG1319377
1,2,4-Trichlorobenzene ND 0.0192 1.22 07/29/2019 16:28 WG1319377
1,2,4-Trimethylbenzene ND 0.00766 1.22 07/29/2019 16:28 WG1319377
1,2-Dibromoethane ND 0.00383 1.22 07/29/2019 16:28 WG1319377
1,2-Dichloroethane ND 0.00383 1.22 07/29/2019 16:28 WG1319377
1,3,5-Trimethylbenzene ND 0.00766 1.22 07/29/2019 16:28 WG1319377
2-Butanone (MEK)0.603 0.0383 1.22 07/29/2019 16:28 WG1319377
Acetone 0.456 0.0383 1.22 07/29/2019 16:28 WG1319377
Benzene 0.00641 0.00153 1.22 07/29/2019 16:28 WG1319377
Di-isopropyl ether ND 0.00153 1.22 07/29/2019 16:28 WG1319377
Ethylbenzene ND 0.00383 1.22 07/29/2019 16:28 WG1319377
Isopropylbenzene ND 0.00383 1.22 07/29/2019 16:28 WG1319377
Methyl tert-butyl ether 0.0386 0.00153 1.22 07/29/2019 16:28 WG1319377
Methylene Chloride ND 0.0383 1.22 07/29/2019 16:28 WG1319377
Naphthalene ND 0.0192 1.22 07/29/2019 16:28 WG1319377
Styrene ND 0.0192 1.22 07/29/2019 16:28 WG1319377
Toluene ND 0.00766 1.22 07/29/2019 16:28 WG1319377
Xylenes, Total ND 0.00996 1.22 07/29/2019 16:28 WG1319377
n-Butylbenzene ND 0.0192 1.22 07/29/2019 16:28 WG1319377
n-Propylbenzene ND 0.00766 1.22 07/29/2019 16:28 WG1319377
sec-Butylbenzene ND 0.0192 1.22 07/29/2019 16:28 WG1319377
tert-Butylbenzene ND 0.00766 1.22 07/29/2019 16:28 WG1319377
(S) Toluene-d8 105 75.0-131 07/29/2019 16:28 WG1319377
(S) 4-Bromofluorobenzene 98.4 67.0-138 07/29/2019 16:28 WG1319377
(S) 1,2-Dichloroethane-d4 103 70.0-130 07/29/2019 16:28 WG1319377
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Unadjusted C9-C18 Aliphatics ND 8.17 1 08/01/2019 17:14 WG1320617
Unadjusted C19-C36 Aliphatics ND 8.17 1 08/01/2019 17:14 WG1320617
Unadjusted C11-C22 Aromatics ND 8.17 1 08/01/2019 23:46 WG1320617
Unadjusted Total Petroleum Hydrocarbons ND 8.17 1 08/01/2019 17:14 WG1320617
Adjusted C11-C22 Aromatics ND 8.17 1 08/01/2019 23:46 WG1320617
Adjusted Total Petroleum Hydrocarbons ND 8.17 1 08/01/2019 17:14 WG1320617
(S) o-Terphenyl 57.9 40.0-140 08/01/2019 23:46 WG1320617
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1121787
MW-1 (20')
Collected date/time: 07/23/19 11:06
TPH by Method MADEPE
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
(S) 1-Chloro-octadecane 55.8 40.0-140 08/01/2019 17:14 WG1320617
(S) 2-Fluorobiphenyl 82.7 40.0-140 08/01/2019 23:46 WG1320617
(S) 2-Bromonaphthalene 80.8 40.0-140 08/01/2019 23:46 WG1320617
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Acenaphthene ND 0.0418 1 07/29/2019 03:26 WG1318945
Acenaphthylene ND 0.0418 1 07/29/2019 03:26 WG1318945
Anthracene ND 0.0418 1 07/29/2019 03:26 WG1318945
Benzo(a)anthracene ND 0.0418 1 07/29/2019 03:26 WG1318945
Benzo(b)fluoranthene ND 0.0418 1 07/29/2019 03:26 WG1318945
Benzo(k)fluoranthene ND 0.0418 1 07/29/2019 03:26 WG1318945
Benzo(g,h,i)perylene ND 0.0418 1 07/29/2019 03:26 WG1318945
Benzo(a)pyrene ND 0.0418 1 07/29/2019 03:26 WG1318945
Bis(2-chlorethoxy)methane ND 0.418 1 07/29/2019 03:26 WG1318945
Bis(2-chloroethyl)ether ND 0.418 1 07/29/2019 03:26 WG1318945
Bis(2-chloroisopropyl)ether ND 0.418 1 07/29/2019 03:26 WG1318945
4-Bromophenyl-phenylether ND 0.418 1 07/29/2019 03:26 WG1318945
4-Chloroaniline ND 0.418 1 07/29/2019 03:26 WG1318945
2-Chloronaphthalene ND 0.0418 1 07/29/2019 03:26 WG1318945
4-Chlorophenyl-phenylether ND 0.418 1 07/29/2019 03:26 WG1318945
Chrysene ND 0.0418 1 07/29/2019 03:26 WG1318945
Dibenz(a,h)anthracene ND 0.0418 1 07/29/2019 03:26 WG1318945
Dibenzofuran ND 0.418 1 07/29/2019 03:26 WG1318945
3,3-Dichlorobenzidine ND 0.418 1 07/29/2019 03:26 WG1318945
2,4-Dinitrotoluene ND 0.418 1 07/29/2019 03:26 WG1318945
2,6-Dinitrotoluene ND 0.418 1 07/29/2019 03:26 WG1318945
Fluoranthene ND 0.0418 1 07/29/2019 03:26 WG1318945
Fluorene ND 0.0418 1 07/29/2019 03:26 WG1318945
Hexachlorobenzene ND 0.418 1 07/29/2019 03:26 WG1318945
Hexachloro-1,3-butadiene ND 0.418 1 07/29/2019 03:26 WG1318945
Hexachlorocyclopentadiene ND 0.418 1 07/29/2019 03:26 WG1318945
Hexachloroethane ND 0.418 1 07/29/2019 03:26 WG1318945
Indeno(1,2,3-cd)pyrene ND 0.0418 1 07/29/2019 03:26 WG1318945
Isophorone ND 0.418 1 07/29/2019 03:26 WG1318945
1-Methylnaphthalene ND 0.418 1 07/29/2019 03:26 WG1318945
2-Methylnaphthalene ND 0.418 1 07/29/2019 03:26 WG1318945
Naphthalene ND 0.0418 1 07/29/2019 03:26 WG1318945
Nitrobenzene ND 0.418 1 07/29/2019 03:26 WG1318945
n-Nitrosodiphenylamine ND 0.418 1 07/29/2019 03:26 WG1318945
n-Nitrosodi-n-propylamine ND 0.418 1 07/29/2019 03:26 WG1318945
Phenanthrene ND 0.0418 1 07/29/2019 03:26 WG1318945
Benzylbutyl phthalate ND 0.418 1 07/29/2019 03:26 WG1318945
Bis(2-ethylhexyl)phthalate ND 0.418 1 07/29/2019 03:26 WG1318945
Di-n-butyl phthalate ND 0.418 1 07/29/2019 03:26 WG1318945
Diethyl phthalate ND 0.418 1 07/29/2019 03:26 WG1318945
Dimethyl phthalate ND 0.418 1 07/29/2019 03:26 WG1318945
Di-n-octyl phthalate ND 0.418 1 07/29/2019 03:26 WG1318945
Pyrene ND 0.0418 1 07/29/2019 03:26 WG1318945
Benzoic acid 0.921 0.418 1 07/29/2019 03:26 WG1318945
4-Chloro-3-methylphenol ND 0.418 1 07/29/2019 03:26 WG1318945
2-Chlorophenol ND 0.418 1 07/29/2019 03:26 WG1318945
2-Methylphenol ND 0.418 1 07/29/2019 03:26 WG1318945
3&4-Methyl Phenol ND 0.418 1 07/29/2019 03:26 WG1318945
2,4-Dichlorophenol ND 0.418 1 07/29/2019 03:26 WG1318945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1121787
MW-1 (20')
Collected date/time: 07/23/19 11:06
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result (dry)Qualifier RDL (dry)Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
2,4-Dimethylphenol ND 0.418 1 07/29/2019 03:26 WG1318945
4,6-Dinitro-2-methylphenol ND 0.418 1 07/29/2019 03:26 WG1318945
2,4-Dinitrophenol ND 0.418 1 07/29/2019 03:26 WG1318945
2-Nitrophenol ND 0.418 1 07/29/2019 03:26 WG1318945
4-Nitrophenol ND 0.418 1 07/29/2019 03:26 WG1318945
Pentachlorophenol ND 0.418 1 07/29/2019 03:26 WG1318945
Phenol ND 0.418 1 07/29/2019 03:26 WG1318945
2,4,6-Trichlorophenol ND 0.418 1 07/29/2019 03:26 WG1318945
(S) 2-Fluorophenol 60.5 12.0-120 07/29/2019 03:26 WG1318945
(S) Phenol-d5 52.6 10.0-120 07/29/2019 03:26 WG1318945
(S) Nitrobenzene-d5 45.5 10.0-122 07/29/2019 03:26 WG1318945
(S) 2-Fluorobiphenyl 53.0 15.0-120 07/29/2019 03:26 WG1318945
(S) 2,4,6-Tribromophenol 89.8 10.0-127 07/29/2019 03:26 WG1318945
(S) p-Terphenyl-d14 59.1 10.0-120 07/29/2019 03:26 WG1318945
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1319285
Total Solids by Method 2540 G-2011 L1121787-03,04
Method Blank (MB)
(MB) R3435876-1 07/30/19 11:18
MB Result MB Qualifier MB MDL MB RDL
Analyte %%%
Total Solids 0.00100
L1121793-04 Original Sample (OS) • Duplicate (DUP)
(OS) L1121793-04 07/30/19 11:18 • (DUP) R3435876-3 07/30/19 11:18
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte %%%%
Total Solids 96.6 96.2 1 0.353 10
Laboratory Control Sample (LCS)
(LCS) R3435876-2 07/30/19 11:18
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte %%%%
Total Solids 50.0 50.0 100 85.0-115
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1317099
Metals (ICP) by Method 6010D L1121787-02
Method Blank (MB)
(MB) R3434765-1 07/26/19 13:23
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Lead 2.66 J 1.90 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3434765-2 07/26/19 13:25 • (LCSD) R3434765-3 07/26/19 13:27
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Lead 1000 966 951 96.6 95.1 80.0-120 1.52 20
L1121888-23 Original Sample (OS) • Matrix Spike (MS)
(OS) L1121888-23 07/26/19 13:30 • (MS) R3434765-5 07/26/19 13:35
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Lead 1000 ND 973 97.0 1 75.0-125
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318211
Volatile Petroleum Hydrocarbons by Method MADEPV L1121787-02
Method Blank (MB)
(MB) R3434969-3 07/26/19 13:34
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Adjusted C5-C8 Aliphatics U 33.3 100
Adjusted C9-C12 Aliphatics U 33.3 100
Total VPH U 66.7 200
Total Purgeable Hydrocarbons
C5-C12 U 66.7 200
(S) 2,5-Dibromotoluene(FID)94.6 70.0-130
(S) 2,5-Dibromotoluene(PID)86.2 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3434969-1 07/26/19 11:22 • (LCSD) R3434969-2 07/26/19 11:55
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1040 1150 86.4 96.0 70.0-130 10.5 50
Unadjusted C9-C12 Aliphatics 1400 1410 1540 101 110 70.0-130 8.80 50
Unadjusted C9-C10 Aromatics 200 177 187 88.7 93.7 70.0-130 5.57 50
Total VPH 2800 2630 2880 93.8 103 70.0-130 9.08 50
Total Purgeable Hydrocarbons
C5-C12 2800 2670 2920 95.3 104 70.0-130 8.86 50
(S) 2,5-Dibromotoluene(FID) 93.6 95.9 70.0-130
(S) 2,5-Dibromotoluene(PID) 87.6 90.2 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318991
Volatile Petroleum Hydrocarbons by Method MADEPV L1121787-03,04
Method Blank (MB)
(MB) R3435385-3 07/28/19 15:45
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C5-C8 Aliphatics 2.28 J 1.67 5.00
Unadjusted C9-C12 Aliphatics U 1.67 5.00
Unadjusted C9-C10 Aromatics 1.95 J 1.67 5.00
Adjusted C5-C8 Aliphatics 2.26 J 1.67 5.00
Adjusted C9-C12 Aliphatics U 1.67 5.00
Total VPH 4.23 J 3.34 10.0
Total Purgeable Hydrocarbons
C5-C12 4.37 J 0.335 10.0
(S) 2,5-Dibromotoluene(FID)102 70.0-130
(S) 2,5-Dibromotoluene(PID)105 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3435385-1 07/28/19 12:10 • (LCSD) R3435385-2 07/28/19 12:50
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 1.20 1.10 1.02 92.0 85.4 70.0-130 7.51 50
Unadjusted C9-C12 Aliphatics 1.40 1.25 1.17 89.4 83.4 70.0-130 7.03 50
Unadjusted C9-C10 Aromatics 0.200 0.188 0.173 93.8 86.3 70.0-130 8.26 50
Total VPH 2.80 2.54 2.36 90.6 84.4 70.0-130 7.14 50
Total Purgeable Hydrocarbons
C5-C12 2.80 2.67 2.48 95.5 88.6 70.0-130 7.48 50
(S) 2,5-Dibromotoluene(FID) 102 105 70.0-130
(S) 2,5-Dibromotoluene(PID) 108 111 70.0-130
L1121454-38 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1121454-38 07/28/19 19:11 • (MS) R3435385-4 07/29/19 13:27 • (MSD) R3435385-5 07/29/19 14:07
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C5-C8 Aliphatics 1.50 ND 26.0 47.6 31.5 60.4 50 70.0-130 J6 J3 J6 58.7 50
Unadjusted C9-C12 Aliphatics 1.75 ND 35.6 74.9 40.8 85.7 50 70.0-130 J6 J3 71.0 50
Unadjusted C9-C10 Aromatics 0.250 ND 5.80 11.5 14.5 60.1 50 70.0-130 J6 J3 J6 65.8 50
Total VPH 3.49 ND 67.3 134 38.5 76.6 50 70.0-130 J6 J3 66.2 50
Total Purgeable Hydrocarbons C5-C12 3.49 12.5 75.6 142 36.1 73.9 50 70.0-130 J6 J3 60.9 50
(S) 2,5-Dibromotoluene(FID) 102 102 70.0-130
(S) 2,5-Dibromotoluene(PID) 107 109 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1317486
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1121787-01,02
Method Blank (MB)
(MB) R3434647-4 07/25/19 11:26
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromochloromethane U 0.520 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride 0.400 J 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.419 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Ethanol U 42.0 100
Hexachloro-1,3-butadiene U 0.256 1.00
Isopropylbenzene U 0.326 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1317486
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1121787-01,02
Method Blank (MB)
(MB) R3434647-4 07/25/19 11:26
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
p-Isopropyltoluene U 0.350 1.00
Methylene Chloride U 1.00 5.00
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,2,3-Trichlorobenzene U 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene U 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,3-Trimethylbenzene U 0.355 1.00
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl chloride U 0.259 1.00
Xylenes, Total U 1.06 3.00
tert-Amyl Methyl Ether U 0.260 1.00
Ethyl tert-butyl ether U 0.270 1.00
t-Amyl Alcohol U 4.90 50.0
tert-Butyl formate U 3.30 20.0
Tert-Amyl Ethyl Ether U 0.401 1.00
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 97.0 77.0-126
(S) 1,2-Dichloroethane-d4 104 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3434647-1 07/25/19 10:06 • (LCSD) R3434647-2 07/25/19 10:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 23.1 23.0 92.3 92.0 70.0-123 0.284 20
Bromobenzene 25.0 22.4 21.7 89.5 86.7 73.0-121 3.18 20
Bromodichloromethane 25.0 25.3 25.5 101 102 75.0-120 0.717 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1317486
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1121787-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3434647-1 07/25/19 10:06 • (LCSD) R3434647-2 07/25/19 10:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Bromochloromethane 25.0 24.1 24.3 96.4 97.3 76.0-122 0.922 20
Bromoform 25.0 24.1 23.9 96.4 95.4 68.0-132 1.02 20
Bromomethane 25.0 25.3 25.3 101 101 10.0-160 0.190 25
n-Butylbenzene 25.0 25.3 24.8 101 99.2 73.0-125 2.05 20
sec-Butylbenzene 25.0 24.3 23.9 97.1 95.4 75.0-125 1.79 20
tert-Butylbenzene 25.0 24.5 24.2 97.9 96.7 76.0-124 1.26 20
Carbon tetrachloride 25.0 27.1 26.6 108 106 68.0-126 2.03 20
Chlorobenzene 25.0 24.1 23.6 96.3 94.6 80.0-121 1.77 20
Chlorodibromomethane 25.0 26.0 25.3 104 101 77.0-125 3.09 20
Chloroethane 25.0 25.9 25.5 103 102 47.0-150 1.26 20
Chloroform 25.0 22.5 22.5 90.0 90.0 73.0-120 0.0438 20
Chloromethane 25.0 27.0 27.2 108 109 41.0-142 0.475 20
2-Chlorotoluene 25.0 24.9 24.7 99.8 98.6 76.0-123 1.16 20
4-Chlorotoluene 25.0 24.4 23.8 97.5 95.4 75.0-122 2.21 20
1,2-Dibromo-3-Chloropropane 25.0 20.9 20.5 83.8 82.1 58.0-134 2.00 20
1,2-Dibromoethane 25.0 25.8 25.5 103 102 80.0-122 1.13 20
Dibromomethane 25.0 24.5 24.3 98.1 97.4 80.0-120 0.766 20
1,2-Dichlorobenzene 25.0 23.8 23.7 95.3 94.7 79.0-121 0.589 20
1,3-Dichlorobenzene 25.0 23.8 23.7 95.4 94.6 79.0-120 0.772 20
1,4-Dichlorobenzene 25.0 23.2 22.9 92.7 91.7 79.0-120 1.12 20
Dichlorodifluoromethane 25.0 27.4 27.1 109 108 51.0-149 0.939 20
1,1-Dichloroethane 25.0 23.9 24.2 95.5 96.8 70.0-126 1.26 20
1,2-Dichloroethane 25.0 23.0 23.3 92.0 93.1 70.0-128 1.08 20
1,1-Dichloroethene 25.0 23.8 24.2 95.1 96.7 71.0-124 1.64 20
cis-1,2-Dichloroethene 25.0 23.0 23.0 91.8 91.8 73.0-120 0.00353 20
trans-1,2-Dichloroethene 25.0 23.4 23.4 93.5 93.7 73.0-120 0.233 20
1,2-Dichloropropane 25.0 25.3 25.4 101 101 77.0-125 0.355 20
1,1-Dichloropropene 25.0 25.2 25.4 101 102 74.0-126 0.539 20
1,3-Dichloropropane 25.0 26.2 25.6 105 102 80.0-120 2.45 20
cis-1,3-Dichloropropene 25.0 26.8 26.6 107 106 80.0-123 0.692 20
trans-1,3-Dichloropropene 25.0 26.3 26.1 105 105 78.0-124 0.502 20
2,2-Dichloropropane 25.0 24.6 24.8 98.4 99.2 58.0-130 0.771 20
Di-isopropyl ether 25.0 24.6 24.9 98.5 99.6 58.0-138 1.18 20
Ethylbenzene 25.0 24.5 24.1 98.1 96.5 79.0-123 1.68 20
Hexachloro-1,3-butadiene 25.0 24.2 24.5 96.7 98.0 54.0-138 1.23 20
Isopropylbenzene 25.0 24.2 23.9 96.7 95.7 76.0-127 1.09 20
p-Isopropyltoluene 25.0 24.5 23.9 98.1 95.8 76.0-125 2.37 20
Methylene Chloride 25.0 22.6 22.6 90.3 90.4 67.0-120 0.130 20
Methyl tert-butyl ether 25.0 19.3 19.3 77.4 77.3 68.0-125 0.0971 20
Naphthalene 25.0 22.4 22.6 89.7 90.2 54.0-135 0.562 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1317486
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1121787-01,02
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3434647-1 07/25/19 10:06 • (LCSD) R3434647-2 07/25/19 10:26
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
n-Propylbenzene 25.0 24.9 24.4 99.5 97.6 77.0-124 1.87 20
Styrene 25.0 25.2 24.9 101 99.5 73.0-130 1.14 20
1,1,1,2-Tetrachloroethane 25.0 22.5 22.3 90.2 89.1 75.0-125 1.18 20
1,1,2,2-Tetrachloroethane 25.0 22.4 22.2 89.6 88.9 65.0-130 0.762 20
Tetrachloroethene 25.0 26.1 25.7 104 103 72.0-132 1.65 20
Toluene 25.0 23.5 23.2 94.1 92.7 79.0-120 1.43 20
1,2,3-Trichlorobenzene 25.0 24.1 24.1 96.3 96.5 50.0-138 0.271 20
1,2,4-Trichlorobenzene 25.0 24.6 24.1 98.3 96.6 57.0-137 1.82 20
1,1,1-Trichloroethane 25.0 25.6 25.8 103 103 73.0-124 0.865 20
1,1,2-Trichloroethane 25.0 26.1 25.6 104 102 80.0-120 1.80 20
Trichloroethene 25.0 25.1 25.1 101 100 78.0-124 0.321 20
Trichlorofluoromethane 25.0 25.7 26.0 103 104 59.0-147 0.853 20
1,2,3-Trichloropropane 25.0 23.1 23.4 92.3 93.7 73.0-130 1.51 20
1,2,3-Trimethylbenzene 25.0 23.7 23.5 95.0 94.0 77.0-120 1.02 20
1,2,4-Trimethylbenzene 25.0 23.4 23.0 93.5 92.1 76.0-121 1.52 20
1,3,5-Trimethylbenzene 25.0 24.0 23.6 95.9 94.3 76.0-122 1.66 20
Vinyl chloride 25.0 26.7 26.8 107 107 67.0-131 0.192 20
Xylenes, Total 75.0 70.0 70.0 93.3 93.3 79.0-123 0.000 20
Tert-Amyl Ethyl Ether 25.0 23.3 23.4 93.2 93.4 70.0-130 0.209 20
ethanol 1250 1020 1180 81.8 94.1 10.0-160 14.0 30
(S) Toluene-d8 108 106 80.0-120
(S) 4-Bromofluorobenzene 99.5 99.3 77.0-126
(S) 1,2-Dichloroethane-d4 108 107 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3434647-3 07/25/19 10:46
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl Formate 100 85.8 85.8 10.0-160
(S) Toluene-d8 107 80.0-120
(S) 4-Bromofluorobenzene 97.0 77.0-126
(S) 1,2-Dichloroethane-d4 105 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318206
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1121787-02
Method Blank (MB)
(MB) R3435045-4 07/27/19 17:06
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.331 1.00
Methyl tert-butyl ether U 0.367 1.00
Toluene U 0.412 1.00
tert-Butyl alcohol U 2.40 5.00
(S) Toluene-d8 105 80.0-120
(S) 4-Bromofluorobenzene 95.9 77.0-126
(S) 1,2-Dichloroethane-d4 109 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3435045-1 07/27/19 15:45 • (LCSD) R3435045-2 07/27/19 16:04
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Benzene 25.0 24.8 24.1 99.4 96.2 70.0-123 3.26 20
Methyl tert-butyl ether 25.0 21.3 21.4 85.1 85.5 68.0-125 0.517 20
Toluene 25.0 24.5 24.3 98.1 97.1 79.0-120 1.03 20
tert-Butyl alcohol 125 126 127 101 101 27.0-160 0.157 30
(S) Toluene-d8 105 108 80.0-120
(S) 4-Bromofluorobenzene 96.8 97.8 77.0-126
(S) 1,2-Dichloroethane-d4 115 111 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1319377
Volatile Organic Compounds (GC/MS) by Method 8260D L1121787-03,04
Method Blank (MB)
(MB) R3435416-2 07/29/19 11:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acetone U 0.0137 0.0250
Benzene U 0.000400 0.00100
n-Butylbenzene U 0.00384 0.0125
sec-Butylbenzene U 0.00253 0.0125
tert-Butylbenzene U 0.00155 0.00500
1,2-Dibromoethane U 0.000525 0.00250
1,2-Dichloroethane U 0.000475 0.00250
Di-isopropyl ether U 0.000350 0.00100
Ethylbenzene U 0.000530 0.00250
Isopropylbenzene U 0.000863 0.00250
2-Butanone (MEK)0.0254 0.0125 0.0250
Methylene Chloride 0.00982 J 0.00664 0.0250
Methyl tert-butyl ether U 0.000295 0.00100
Naphthalene U 0.00312 0.0125
n-Propylbenzene U 0.00118 0.00500
Styrene U 0.00273 0.0125
Toluene U 0.00125 0.00500
1,2,3-Trichlorobenzene U 0.000625 0.00250
1,2,4-Trichlorobenzene U 0.00482 0.0125
1,2,4-Trimethylbenzene U 0.00116 0.00500
1,3,5-Trimethylbenzene U 0.00108 0.00500
Xylenes, Total U 0.00478 0.00650
(S) Toluene-d8 104 75.0-131
(S) 4-Bromofluorobenzene 97.9 67.0-138
(S) 1,2-Dichloroethane-d4 104 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3435416-1 07/29/19 10:28
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acetone 0.625 0.642 103 10.0-160
Benzene 0.125 0.122 97.5 70.0-123
n-Butylbenzene 0.125 0.112 89.8 68.0-135
sec-Butylbenzene 0.125 0.113 90.2 74.0-130
tert-Butylbenzene 0.125 0.115 91.6 75.0-127
1,2-Dibromoethane 0.125 0.140 112 74.0-128
1,2-Dichloroethane 0.125 0.126 101 65.0-131
Di-isopropyl ether 0.125 0.106 85.0 60.0-136
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1319377
Volatile Organic Compounds (GC/MS) by Method 8260D L1121787-03,04
Laboratory Control Sample (LCS)
(LCS) R3435416-1 07/29/19 10:28
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Ethylbenzene 0.125 0.123 98.1 74.0-126
Isopropylbenzene 0.125 0.125 99.8 72.0-127
2-Butanone (MEK)0.625 0.728 116 30.0-160
Methylene Chloride 0.125 0.127 102 68.0-123
Methyl tert-butyl ether 0.125 0.114 91.0 66.0-132
Naphthalene 0.125 0.126 100 59.0-130
n-Propylbenzene 0.125 0.118 94.8 74.0-126
Styrene 0.125 0.126 101 72.0-127
Toluene 0.125 0.125 99.6 75.0-121
1,2,3-Trichlorobenzene 0.125 0.119 95.5 59.0-139
1,2,4-Trichlorobenzene 0.125 0.115 91.9 62.0-137
1,2,4-Trimethylbenzene 0.125 0.120 96.0 70.0-126
1,3,5-Trimethylbenzene 0.125 0.113 90.6 73.0-127
Xylenes, Total 0.375 0.375 100 72.0-127
(S) Toluene-d8 106 75.0-131
(S) 4-Bromofluorobenzene 100 67.0-138
(S) 1,2-Dichloroethane-d4 107 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1317171
EDB / DBCP by Method 504.1 L1121787-02
Method Blank (MB)
(MB) R3434541-1 07/25/19 16:04
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ethylene Dibromide U 0.00240 0.0100
L1121421-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1121421-01 07/25/19 16:53 • (DUP) R3434541-3 07/25/19 16:41
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/l ug/l %%
Ethylene Dibromide ND 0.000 1 0.000 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3434541-4 07/25/19 18:55 • (LCSD) R3434541-5 07/25/19 21:20
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ethylene Dibromide 0.250 0.236 0.242 94.4 96.8 70.0-130 2.51 20
Laboratory Control Sample (LCS)
(LCS) R3434624-1 07/26/19 12:02
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Ethylene Dibromide 0.250 0.231 92.4 70.0-130
L1121789-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1121789-01 07/25/19 16:29 • (MS) R3434541-2 07/25/19 16:17
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ethylene Dibromide 0.100 ND 0.106 106 1 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318081
TPH by Method MADEPE L1121787-02
Method Blank (MB)
(MB) R3435036-1 07/27/19 06:42
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C9-C18 Aliphatics U 33.0 100
Unadjusted C19-C36 Aliphatics U 33.0 100
(S) 1-Chloro-octadecane 73.6 40.0-140
Method Blank (MB)
(MB) R3435036-4 07/27/19 07:47
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C11-C22 Aromatics 34.7 J 33.0 100
(S) o-Terphenyl 85.8 40.0-140
(S) 2-Fluorobiphenyl 89.0 40.0-140
(S) 2-Bromonaphthalene 84.6 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3435036-2 07/27/19 07:04 • (LCSD) R3435036-3 07/27/19 07:25
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C9-C18 Aliphatics 600 374 374 62.3 62.3 40.0-140 0.000 25
Unadjusted C19-C36 Aliphatics 800 706 686 88.2 85.8 40.0-140 2.87 25
(S) 1-Chloro-octadecane 72.2 63.2 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3435036-5 07/27/19 08:09 • (LCSD) R3435036-6 07/27/19 08:31
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C11-C22 Aromatics 1700 1480 1470 87.1 86.5 40.0-140 0.678 25
(S) o-Terphenyl 85.0 82.5 40.0-140
(S) 2-Fluorobiphenyl 93.6 92.6 40.0-140
(S) 2-Bromonaphthalene 89.0 88.9 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1320617
TPH by Method MADEPE L1121787-03,04
Method Blank (MB)
(MB) R3436988-1 08/01/19 14:33
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C9-C18 Aliphatics U 2.17 6.50
Unadjusted C19-C36 Aliphatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) 1-Chloro-octadecane 70.9 40.0-140
Method Blank (MB)
(MB) R3436988-4 08/01/19 15:42
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Unadjusted C11-C22 Aromatics U 2.17 6.50
Unadjusted Total Petroleum
Hydrocarbons U 2.17 6.50
(S) o-Terphenyl 70.3 40.0-140
(S) 2-Fluorobiphenyl 78.8 40.0-140
(S) 2-Bromonaphthalene 77.1 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3436988-2 08/01/19 14:56 • (LCSD) R3436988-3 08/01/19 15:19
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 39.9 26.2 27.6 65.7 69.2 40.0-140 5.20 25
Unadjusted C19-C36 Aliphatics 53.2 40.7 41.6 76.5 78.2 40.0-140 2.19 25
(S) 1-Chloro-octadecane 68.0 68.2 40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3436988-5 08/01/19 16:05 • (LCSD) R3436988-6 08/01/19 16:28
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 113 74.7 77.0 66.1 68.1 40.0-140 3.03 25
(S) o-Terphenyl 71.2 70.1 40.0-140
(S) 2-Fluorobiphenyl 82.9 82.9 40.0-140
(S) 2-Bromonaphthalene 81.4 81.8 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1320617
TPH by Method MADEPE L1121787-03,04
L1121787-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1121787-04 08/01/19 17:14 • (MS) R3436988-7 08/01/19 17:37 • (MSD) R3436988-8 08/01/19 18:01
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C9-C18 Aliphatics 50.1 ND 32.5 33.3 64.9 66.4 1 40.0-140 2.29 50
Unadjusted C19-C36 Aliphatics 66.8 ND 46.6 47.0 69.7 70.3 1 40.0-140 0.805 50
(S) 1-Chloro-octadecane 60.2 60.9 40.0-140
L1121787-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1121787-04 08/01/19 17:14 • (MS) R3436988-10 08/01/19 23:23 • (MSD) R3436988-9 08/01/19 23:00
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Unadjusted C11-C22 Aromatics 142 ND 79.8 86.9 56.2 61.2 1 40.0-140 8.59 50
(S) o-Terphenyl 57.7 62.2 40.0-140
(S) 2-Fluorobiphenyl 77.8 80.8 40.0-140
(S) 2-Bromonaphthalene 76.9 79.3 40.0-140
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318962
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1121787-02
Method Blank (MB)
(MB) R3435805-2 07/30/19 15:01
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Acenaphthene U 0.316 1.00
Acenaphthylene U 0.309 1.00
Anthracene U 0.291 1.00
Benzo(a)anthracene U 0.0975 1.00
Benzo(b)fluoranthene U 0.0896 1.00
Benzo(k)fluoranthene U 0.355 1.00
Benzo(g,h,i)perylene U 0.161 1.00
Benzo(a)pyrene U 0.340 1.00
Bis(2-chlorethoxy)methane U 0.329 10.0
Bis(2-chloroisopropyl)ether U 0.445 10.0
4-Bromophenyl-phenylether U 0.335 10.0
2-Chloronaphthalene U 0.330 1.00
4-Chlorophenyl-phenylether U 0.303 10.0
Chrysene U 0.332 1.00
Dibenz(a,h)anthracene U 0.279 1.00
3,3-Dichlorobenzidine U 2.02 10.0
2,4-Dinitrotoluene U 1.65 10.0
2,6-Dinitrotoluene U 0.279 10.0
Fluoranthene U 0.310 1.00
Fluorene U 0.323 1.00
Hexachlorobenzene U 0.341 1.00
Hexachloro-1,3-butadiene U 0.329 10.0
Hexachlorocyclopentadiene U 2.33 10.0
Hexachloroethane U 0.365 10.0
Indeno(1,2,3-cd)pyrene U 0.279 1.00
Isophorone U 0.272 10.0
Naphthalene U 0.372 1.00
Nitrobenzene U 0.367 10.0
n-Nitrosodiphenylamine U 1.19 10.0
n-Nitrosodi-n-propylamine U 0.403 10.0
Phenanthrene U 0.366 1.00
Benzylbutyl phthalate U 0.275 3.00
Bis(2-ethylhexyl)phthalate U 0.709 3.00
Di-n-butyl phthalate U 0.266 3.00
Diethyl phthalate U 0.282 3.00
Dimethyl phthalate U 0.283 3.00
Di-n-octyl phthalate U 0.278 3.00
Pyrene U 0.330 1.00
Benzoic Acid U 4.40 10.0
4-Chloroaniline U 0.382 10.0
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318962
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1121787-02
Method Blank (MB)
(MB) R3435805-2 07/30/19 15:01
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
4-Chloro-3-methylphenol U 0.263 10.0
2-Chlorophenol U 0.283 10.0
2-Nitrophenol U 0.320 10.0
4-Nitrophenol U 2.01 10.0
Pentachlorophenol U 0.313 10.0
Phenol U 0.334 10.0
2,4,6-Trichlorophenol U 0.297 10.0
Dibenzofuran U 0.380 10.0
2,4-Dichlorophenol U 0.284 10.0
2,4-Dimethylphenol U 0.624 10.0
4,6-Dinitro-2-methylphenol U 2.66 10.0
2,4-Dinitrophenol U 3.25 50.0
2-Methylnaphthalene U 0.311 1.00
2-Methylphenol U 3.12 10.0
3&4-Methyl Phenol U 0.266 10.0
1-Methylnaphthalene U 0.332 1.00
(S) Nitrobenzene-d5 35.0 15.0-314
(S) 2-Fluorobiphenyl 44.5 22.0-127
(S) p-Terphenyl-d14 44.9 29.0-141
(S) Phenol-d5 10.3 8.00-424
(S) 2-Fluorophenol 18.8 10.0-120
(S) 2,4,6-Tribromophenol 36.9 10.0-153
Laboratory Control Sample (LCS)
(LCS) R3435805-1 07/30/19 14:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Acenaphthene 50.0 18.1 36.2 47.0-145 J4
Acenaphthylene 50.0 19.7 39.4 33.0-145
Anthracene 50.0 21.0 42.0 27.0-133
Benzo(a)anthracene 50.0 23.3 46.6 33.0-143
Benzo(b)fluoranthene 50.0 25.2 50.4 24.0-159
Benzo(k)fluoranthene 50.0 25.3 50.6 11.0-162
Benzo(g,h,i)perylene 50.0 27.1 54.2 1.00-219
Benzo(a)pyrene 50.0 24.4 48.8 17.0-163
Bis(2-chlorethoxy)methane 50.0 22.0 44.0 1.00-219
Bis(2-chloroisopropyl)ether 50.0 16.0 32.0 36.0-166 J4
4-Bromophenyl-phenylether 50.0 19.8 39.6 53.0-127 J4
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318962
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1121787-02
Laboratory Control Sample (LCS)
(LCS) R3435805-1 07/30/19 14:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
2-Chloronaphthalene 50.0 17.5 35.0 60.0-120 J4
4-Chlorophenyl-phenylether 50.0 20.3 40.6 25.0-158
Chrysene 50.0 24.3 48.6 17.0-168
Dibenz(a,h)anthracene 50.0 27.0 54.0 1.00-227
3,3-Dichlorobenzidine 100 43.9 43.9 1.00-262
2,4-Dinitrotoluene 50.0 29.0 58.0 39.0-139
2,6-Dinitrotoluene 50.0 27.8 55.6 50.0-158
Fluoranthene 50.0 23.6 47.2 26.0-137
Fluorene 50.0 20.8 41.6 59.0-121 J4
Hexachlorobenzene 50.0 21.0 42.0 1.00-152
Hexachloro-1,3-butadiene 50.0 14.5 29.0 24.0-120
Hexachlorocyclopentadiene 50.0 10.8 21.6 10.0-120
Hexachloroethane 50.0 13.2 26.4 40.0-120 J4
Indeno(1,2,3-cd)pyrene 50.0 26.5 53.0 1.00-171
Isophorone 50.0 20.8 41.6 21.0-196
Naphthalene 50.0 15.2 30.4 21.0-133
Nitrobenzene 50.0 18.8 37.6 35.0-180
n-Nitrosodiphenylamine 50.0 22.2 44.4 44.0-120
n-Nitrosodi-n-propylamine 50.0 20.4 40.8 1.00-230
Phenanthrene 50.0 20.4 40.8 54.0-120 J4
Benzylbutyl phthalate 50.0 23.2 46.4 1.00-152
Bis(2-ethylhexyl)phthalate 50.0 23.5 47.0 8.00-158
Di-n-butyl phthalate 50.0 24.0 48.0 1.00-120
Diethyl phthalate 50.0 27.2 54.4 1.00-120
Dimethyl phthalate 50.0 27.9 55.8 1.00-120
Di-n-octyl phthalate 50.0 24.0 48.0 4.00-146
Pyrene 50.0 22.2 44.4 52.0-120 J4
Benzoic Acid 100 ND 0.000 10.0-120 J4
4-Chloroaniline 50.0 7.15 14.3 23.0-120 J4
4-Chloro-3-methylphenol 50.0 21.2 42.4 22.0-147
2-Chlorophenol 50.0 18.1 36.2 23.0-134
Dibenzofuran 50.0 19.7 39.4 42.0-120 J4
2,4-Dichlorophenol 50.0 21.2 42.4 39.0-135
2,4-Dimethylphenol 50.0 20.0 40.0 32.0-120
4,6-Dinitro-2-methylphenol 50.0 24.7 49.4 1.00-181
2,4-Dinitrophenol 50.0 22.4 44.8 1.00-191
2-Methylnaphthalene 50.0 15.1 30.2 35.0-120 J4
2-Methylphenol 50.0 16.1 32.2 26.0-120
3&4-Methyl Phenol 50.0 15.8 31.6 27.0-120
2-Nitrophenol 50.0 22.6 45.2 29.0-182
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318962
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1121787-02
Laboratory Control Sample (LCS)
(LCS) R3435805-1 07/30/19 14:40
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
4-Nitrophenol 50.0 7.48 15.0 1.00-132
Pentachlorophenol 50.0 16.0 32.0 14.0-176
Phenol 50.0 6.27 12.5 5.00-120
2,4,6-Trichlorophenol 50.0 23.1 46.2 37.0-144
1-Methylnaphthalene 50.0 15.7 31.4 33.0-120 J4
(S) Nitrobenzene-d5 29.8 15.0-314
(S) 2-Fluorobiphenyl 34.8 22.0-127
(S) p-Terphenyl-d14 45.7 29.0-141
(S) Phenol-d5 11.3 8.00-424
(S) 2-Fluorophenol 18.5 10.0-120
(S) 2,4,6-Tribromophenol 46.7 10.0-153
L1122176-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1122176-03 07/30/19 17:42 • (MS) R3435779-1 07/30/19 18:02 • (MSD) R3435779-2 07/30/19 18:22
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Acenaphthene 50.0 U 13.9 14.8 27.8 29.6 1 47.0-145 J6 J6 6.27 48
Acenaphthylene 50.0 U 14.8 15.8 29.6 31.6 1 33.0-145 J6 J6 6.54 74
Anthracene 50.0 U 16.2 17.0 32.4 34.0 1 27.0-133 4.82 66
Benzo(a)anthracene 50.0 U 18.2 18.2 36.4 36.4 1 33.0-143 0.000 53
Benzo(b)fluoranthene 50.0 U 18.8 19.2 37.6 38.4 1 24.0-159 2.11 71
Benzo(k)fluoranthene 50.0 U 18.5 18.5 37.0 37.0 1 11.0-162 0.000 63
Benzo(g,h,i)perylene 50.0 U 18.4 18.5 36.8 37.0 1 1.00-219 0.542 97
Benzo(a)pyrene 50.0 U 19.2 19.0 38.4 38.0 1 17.0-163 1.05 72
Bis(2-chlorethoxy)methane 50.0 U 12.0 13.6 24.0 27.2 1 33.0-184 J6 J6 12.5 54
Bis(2-chloroisopropyl)ether 50.0 U 10.3 11.6 20.6 23.2 1 36.0-166 J6 J6 11.9 76
4-Bromophenyl-phenylether 50.0 U 15.6 16.6 31.2 33.2 1 53.0-127 J6 J6 6.21 43
2-Chloronaphthalene 50.0 U 13.4 14.4 26.8 28.8 1 60.0-120 J6 J6 7.19 24
4-Chlorophenyl-phenylether 50.0 U 15.2 16.7 30.4 33.4 1 25.0-158 9.40 61
Chrysene 50.0 U 18.0 18.1 36.0 36.2 1 17.0-168 0.554 87
Dibenz(a,h)anthracene 50.0 U 18.0 18.0 36.0 36.0 1 1.00-227 0.000 126
3,3-Dichlorobenzidine 100 U 16.2 19.1 16.2 19.1 1 1.00-262 16.4 108
2,4-Dinitrotoluene 50.0 U 17.7 19.8 35.4 39.6 1 39.0-139 J6 11.2 42
2,6-Dinitrotoluene 50.0 0.562 16.8 18.9 32.5 36.7 1 50.0-158 J6 J6 11.8 48
Fluoranthene 50.0 U 17.7 17.8 35.4 35.6 1 26.0-137 0.563 66
Fluorene 50.0 U 15.6 17.1 31.2 34.2 1 59.0-121 J6 J6 9.17 38
Hexachlorobenzene 50.0 U 15.1 16.3 30.2 32.6 1 1.00-152 7.64 55
Hexachloro-1,3-butadiene 50.0 U 10.6 11.7 21.2 23.4 1 24.0-120 J6 J6 9.87 62
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318962
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1121787-02
L1122176-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1122176-03 07/30/19 17:42 • (MS) R3435779-1 07/30/19 18:02 • (MSD) R3435779-2 07/30/19 18:22
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Hexachlorocyclopentadiene 50.0 U 8.22 8.62 16.4 17.2 1 10.0-146 4.75 34
Hexachloroethane 50.0 U 9.58 10.4 19.2 20.8 1 40.0-120 J6 J6 8.21 52
Indeno(1,2,3-cd)pyrene 50.0 U 18.6 18.7 37.2 37.4 1 1.00-171 0.536 99
Isophorone 50.0 U 12.5 13.5 25.0 27.0 1 21.0-196 7.69 93
Naphthalene 50.0 U 10.7 11.3 21.4 22.6 1 21.0-133 5.45 65
Nitrobenzene 50.0 U 11.5 12.5 23.0 25.0 1 35.0-180 J6 J6 8.33 62
n-Nitrosodiphenylamine 50.0 U 16.4 17.3 32.8 34.6 1 16.0-160 5.34 28
n-Nitrosodi-n-propylamine 50.0 U 13.4 15.0 26.8 30.0 1 1.00-230 11.3 87
Phenanthrene 50.0 U 16.0 16.8 32.0 33.6 1 54.0-120 J6 J6 4.88 39
Benzylbutyl phthalate 50.0 U 19.6 19.6 39.2 39.2 1 1.00-152 0.000 60
Bis(2-ethylhexyl)phthalate 50.0 1.68 19.7 20.2 36.0 37.0 1 8.00-158 2.51 82
Di-n-butyl phthalate 50.0 U 18.6 18.9 37.2 37.8 1 1.00-120 1.60 47
Diethyl phthalate 50.0 U 17.3 18.8 34.6 37.6 1 1.00-120 8.31 100
Dimethyl phthalate 50.0 U 16.8 18.1 33.6 36.2 1 1.00-120 7.45 183
Di-n-octyl phthalate 50.0 U 19.0 19.2 38.0 38.4 1 4.00-146 1.05 69
Pyrene 50.0 U 18.3 18.3 36.6 36.6 1 52.0-120 J6 J6 0.000 49
Benzoic Acid 100 U 18.2 18.2 18.2 18.2 1 10.0-120 0.000 40
4-Chloroaniline 50.0 U 4.70 4.26 9.40 8.52 1 10.0-137 J6 J6 9.82 33
4-Chloro-3-methylphenol 50.0 U 15.9 17.5 31.8 35.0 1 22.0-147 9.58 73
2-Chlorophenol 50.0 U 10.2 11.7 20.4 23.4 1 23.0-134 J6 13.7 61
Dibenzofuran 50.0 U 14.8 15.9 29.6 31.8 1 17.0-150 7.17 27
2,4-Dichlorophenol 50.0 U 13.7 15.2 27.4 30.4 1 39.0-135 J6 J6 10.4 50
2,4-Dimethylphenol 50.0 U 12.5 13.9 25.0 27.8 1 32.0-120 J6 J6 10.6 58
4,6-Dinitro-2-methylphenol 50.0 U 17.1 17.7 34.2 35.4 1 1.00-181 3.45 203
2,4-Dinitrophenol 50.0 U 15.1 15.9 30.2 31.8 1 1.00-191 5.16 132
2-Methylnaphthalene 50.0 U 11.7 12.7 23.4 25.4 1 13.0-142 8.20 29
2-Methylphenol 50.0 U 10.4 11.6 20.8 23.2 1 14.0-120 10.9 29
3&4-Methyl Phenol 50.0 0.447 11.4 12.6 21.9 24.3 1 13.0-124 10.0 26
2-Nitrophenol 50.0 U 12.1 13.9 24.2 27.8 1 29.0-182 J6 J6 13.8 55
4-Nitrophenol 50.0 U 8.32 8.99 16.6 18.0 1 1.00-132 7.74 131
Pentachlorophenol 50.0 U 14.0 13.8 28.0 27.6 1 14.0-176 1.44 86
Phenol 50.0 U 5.99 6.60 12.0 13.2 1 5.00-120 9.69 64
2,4,6-Trichlorophenol 50.0 U 16.3 17.2 32.6 34.4 1 37.0-144 J6 J6 5.37 58
1-Methylnaphthalene 50.0 U 12.2 13.1 24.4 26.2 1 33.0-120 J6 J6 7.11 23
(S) Nitrobenzene-d5 20.8 24.0 15.0-314
(S) 2-Fluorobiphenyl 25.1 26.9 22.0-127
(S) p-Terphenyl-d14 34.6 33.3 29.0-141
(S) Phenol-d5 9.95 10.6 8.00-424
(S) 2-Fluorophenol 13.6 14.6 10.0-120
(S) 2,4,6-Tribromophenol 32.0 32.9 10.0-153
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1121787-03,04
Method Blank (MB)
(MB) R3435408-1 07/29/19 00:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Acenaphthene U 0.00642 0.0333
Acenaphthylene U 0.00671 0.0333
Anthracene U 0.00632 0.0333
Benzo(a)anthracene U 0.00428 0.0333
Benzo(b)fluoranthene U 0.00695 0.0333
Benzo(k)fluoranthene U 0.00582 0.0333
Benzo(g,h,i)perylene U 0.00721 0.0333
Benzo(a)pyrene U 0.00548 0.0333
Bis(2-chlorethoxy)methane U 0.00770 0.333
Bis(2-chloroethyl)ether U 0.00896 0.333
Bis(2-chloroisopropyl)ether U 0.00760 0.333
4-Bromophenyl-phenylether U 0.0114 0.333
4-Chloroaniline U 0.0363 0.333
2-Chloronaphthalene U 0.00639 0.0333
4-Chlorophenyl-phenylether U 0.00627 0.333
Chrysene U 0.00555 0.0333
Dibenz(a,h)anthracene U 0.00821 0.0333
Dibenzofuran U 0.00518 0.333
3,3-Dichlorobenzidine U 0.0794 0.333
2,4-Dinitrotoluene U 0.00607 0.333
2,6-Dinitrotoluene U 0.00737 0.333
Fluoranthene U 0.00496 0.0333
Fluorene U 0.00682 0.0333
Hexachlorobenzene U 0.00856 0.333
Hexachloro-1,3-butadiene U 0.0100 0.333
Hexachlorocyclopentadiene U 0.0587 0.333
Hexachloroethane U 0.0134 0.333
Indeno(1,2,3-cd)pyrene U 0.00772 0.0333
Isophorone U 0.00522 0.333
1-Methylnaphthalene U 0.0110 0.333
2-Methylnaphthalene U 0.0260 0.333
Naphthalene U 0.00889 0.0333
Nitrobenzene U 0.00695 0.333
n-Nitrosodiphenylamine U 0.0900 0.333
n-Nitrosodi-n-propylamine U 0.00906 0.333
Phenanthrene U 0.00528 0.0333
Benzylbutyl phthalate U 0.0103 0.333
Bis(2-ethylhexyl)phthalate U 0.0120 0.333
Di-n-butyl phthalate U 0.0109 0.333
Diethyl phthalate U 0.00691 0.333
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1121787-03,04
Method Blank (MB)
(MB) R3435408-1 07/29/19 00:34
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Dimethyl phthalate U 0.00540 0.333
Di-n-octyl phthalate U 0.00907 0.333
Pyrene U 0.0123 0.0333
Benzoic Acid U 0.111 0.333
4-Chloro-3-methylphenol U 0.00477 0.333
2-Chlorophenol U 0.00831 0.333
2-Methylphenol U 0.0330 0.333
3&4-Methyl Phenol U 0.0329 0.333
2,4-Dichlorophenol U 0.00746 0.333
2,4-Dimethylphenol U 0.0471 0.333
4,6-Dinitro-2-methylphenol U 0.124 0.333
2,4-Dinitrophenol U 0.0980 0.333
2-Nitrophenol U 0.0130 0.333
4-Nitrophenol U 0.0525 0.333
Pentachlorophenol U 0.0480 0.333
Phenol U 0.00695 0.333
2,4,6-Trichlorophenol U 0.00779 0.333
(S) Nitrobenzene-d5 54.4 10.0-122
(S) 2-Fluorobiphenyl 65.2 15.0-120
(S) p-Terphenyl-d14 71.5 10.0-120
(S) Phenol-d5 61.1 10.0-120
(S) 2-Fluorophenol 68.9 12.0-120
(S) 2,4,6-Tribromophenol 88.0 10.0-127
Laboratory Control Sample (LCS)
(LCS) R3435408-2 07/29/19 00:53
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Acenaphthene 0.666 0.423 63.5 38.0-120
Acenaphthylene 0.666 0.439 65.9 40.0-120
Anthracene 0.666 0.469 70.4 42.0-120
Benzo(a)anthracene 0.666 0.516 77.5 44.0-120
Benzo(b)fluoranthene 0.666 0.500 75.1 43.0-120
Benzo(k)fluoranthene 0.666 0.511 76.7 44.0-120
Benzo(g,h,i)perylene 0.666 0.514 77.2 43.0-120
Benzo(a)pyrene 0.666 0.501 75.2 45.0-120
Bis(2-chlorethoxy)methane 0.666 0.302 45.3 20.0-120
Bis(2-chloroethyl)ether 0.666 0.378 56.8 16.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1121787-03,04
Laboratory Control Sample (LCS)
(LCS) R3435408-2 07/29/19 00:53
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
Bis(2-chloroisopropyl)ether 0.666 0.340 51.1 23.0-120
4-Bromophenyl-phenylether 0.666 0.519 77.9 40.0-120
4-Chloroaniline 0.666 0.308 46.2 18.0-120
2-Chloronaphthalene 0.666 0.431 64.7 35.0-120
4-Chlorophenyl-phenylether 0.666 0.487 73.1 40.0-120
Chrysene 0.666 0.485 72.8 43.0-120
Dibenz(a,h)anthracene 0.666 0.506 76.0 44.0-120
Dibenzofuran 0.666 0.451 67.7 44.0-120
3,3-Dichlorobenzidine 1.33 0.991 74.5 28.0-120
2,4-Dinitrotoluene 0.666 0.530 79.6 45.0-120
2,6-Dinitrotoluene 0.666 0.509 76.4 42.0-120
Fluoranthene 0.666 0.493 74.0 44.0-120
Fluorene 0.666 0.447 67.1 41.0-120
Hexachlorobenzene 0.666 0.532 79.9 39.0-120
Hexachloro-1,3-butadiene 0.666 0.375 56.3 15.0-120
Hexachlorocyclopentadiene 0.666 0.424 63.7 15.0-120
Hexachloroethane 0.666 0.339 50.9 17.0-120
Indeno(1,2,3-cd)pyrene 0.666 0.511 76.7 45.0-120
Isophorone 0.666 0.312 46.8 23.0-120
1-Methylnaphthalene 0.666 0.349 52.4 34.0-120
2-Methylnaphthalene 0.666 0.331 49.7 34.0-120
Naphthalene 0.666 0.310 46.5 18.0-120
Nitrobenzene 0.666 0.297 44.6 17.0-120
n-Nitrosodiphenylamine 0.666 0.456 68.5 40.0-120
n-Nitrosodi-n-propylamine 0.666 0.358 53.8 26.0-120
Phenanthrene 0.666 0.455 68.3 42.0-120
Benzylbutyl phthalate 0.666 0.505 75.8 40.0-120
Bis(2-ethylhexyl)phthalate 0.666 0.481 72.2 41.0-120
Di-n-butyl phthalate 0.666 0.495 74.3 43.0-120
Diethyl phthalate 0.666 0.494 74.2 43.0-120
Dimethyl phthalate 0.666 0.470 70.6 43.0-120
Di-n-octyl phthalate 0.666 0.512 76.9 40.0-120
Pyrene 0.666 0.472 70.9 41.0-120
Benzoic Acid 1.33 0.277 20.8 10.0-120
4-Chloro-3-methylphenol 0.666 0.392 58.9 28.0-120
2-Chlorophenol 0.666 0.419 62.9 28.0-120
2-Methylphenol 0.666 0.408 61.3 35.0-120
3&4-Methyl Phenol 0.666 0.472 70.9 42.0-120
2,4-Dichlorophenol 0.666 0.411 61.7 25.0-120
2,4-Dimethylphenol 0.666 0.346 52.0 15.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1121787-03,04
Laboratory Control Sample (LCS)
(LCS) R3435408-2 07/29/19 00:53
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg %%
4,6-Dinitro-2-methylphenol 0.666 0.525 78.8 16.0-120
2,4-Dinitrophenol 0.666 0.426 64.0 10.0-120
2-Nitrophenol 0.666 0.404 60.7 20.0-120
4-Nitrophenol 0.666 0.491 73.7 27.0-120
Pentachlorophenol 0.666 0.542 81.4 29.0-120
Phenol 0.666 0.378 56.8 28.0-120
2,4,6-Trichlorophenol 0.666 0.541 81.2 37.0-120
(S) Nitrobenzene-d5 51.1 10.0-122
(S) 2-Fluorobiphenyl 67.6 15.0-120
(S) p-Terphenyl-d14 80.5 10.0-120
(S) Phenol-d5 63.8 10.0-120
(S) 2-Fluorophenol 68.5 12.0-120
(S) 2,4,6-Tribromophenol 105 10.0-127
L1121552-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1121552-01 07/29/19 01:12 • (MS) R3435408-3 07/29/19 01:32 • (MSD) R3435408-4 07/29/19 01:51
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
Acenaphthene 0.783 U 0.370 0.464 47.3 59.3 1 18.0-120 22.5 32
Acenaphthylene 0.783 U 0.373 0.466 47.6 59.5 1 25.0-120 22.2 32
Anthracene 0.783 U 0.374 0.497 47.7 63.5 1 22.0-120 28.3 29
4-Chloroaniline 0.783 U 0.266 0.348 33.9 44.4 1 10.0-120 26.8 36
Benzo(a)anthracene 0.783 U 0.401 0.534 51.2 68.2 1 25.0-120 28.4 29
Benzo(b)fluoranthene 0.783 U 0.390 0.519 49.8 66.2 1 19.0-122 28.2 31
Benzo(k)fluoranthene 0.783 U 0.390 0.536 49.8 68.5 1 23.0-120 J3 31.5 30
Benzo(g,h,i)perylene 0.783 U 0.399 0.516 50.9 65.9 1 10.0-120 25.7 33
Benzo(a)pyrene 0.783 U 0.389 0.527 49.7 67.3 1 24.0-120 30.0 30
Dibenzofuran 0.783 U 0.390 0.488 49.8 62.3 1 24.0-120 22.2 30
Bis(2-chlorethoxy)methane 0.783 U 0.281 0.341 35.9 43.5 1 10.0-120 19.3 34
Bis(2-chloroethyl)ether 0.783 U 0.376 0.441 48.0 56.3 1 10.0-120 15.8 40
Bis(2-chloroisopropyl)ether 0.783 U 0.341 0.404 43.5 51.7 1 10.0-120 17.0 40
4-Bromophenyl-phenylether 0.783 U 0.439 0.561 56.0 71.6 1 27.0-120 24.5 30
2-Chloronaphthalene 0.783 U 0.384 0.466 49.1 59.5 1 20.0-120 19.1 32
4-Chlorophenyl-phenylether 0.783 U 0.415 0.523 53.0 66.8 1 24.0-120 23.1 29
Chrysene 0.783 U 0.382 0.509 48.8 65.0 1 21.0-120 28.5 29
Dibenz(a,h)anthracene 0.783 U 0.392 0.527 50.0 67.3 1 10.0-120 29.4 32
1-Methylnaphthalene 0.783 U 0.333 0.393 42.5 50.2 1 10.0-120 16.5 36
2-Methylnaphthalene 0.783 U 0.317 0.377 40.5 48.2 1 10.0-120 17.3 37
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1121787-03,04
L1121552-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1121552-01 07/29/19 01:12 • (MS) R3435408-3 07/29/19 01:32 • (MSD) R3435408-4 07/29/19 01:51
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
3,3-Dichlorobenzidine 1.56 U 0.770 1.05 49.2 66.9 1 10.0-120 30.4 34
2,4-Dinitrotoluene 0.783 U 0.407 0.561 52.0 71.6 1 30.0-120 J3 31.8 31
2,6-Dinitrotoluene 0.783 U 0.408 0.548 52.1 70.0 1 25.0-120 29.3 31
Fluoranthene 0.783 U 0.377 0.520 48.2 66.4 1 18.0-126 31.7 32
Fluorene 0.783 U 0.376 0.496 48.0 63.4 1 25.0-120 27.5 30
Hexachlorobenzene 0.783 U 0.467 0.580 59.6 74.0 1 27.0-120 21.6 28
Hexachloro-1,3-butadiene 0.783 U 0.415 0.434 53.0 55.4 1 10.0-120 4.43 38
Hexachlorocyclopentadiene 0.783 U 0.393 0.462 50.2 59.0 1 10.0-120 16.2 40
Hexachloroethane 0.783 U 0.388 0.409 49.5 52.3 1 10.0-120 5.31 40
Indeno(1,2,3-cd)pyrene 0.783 U 0.394 0.520 50.3 66.4 1 10.0-120 27.5 32
Isophorone 0.783 U 0.285 0.343 36.3 43.8 1 13.0-120 18.7 34
Naphthalene 0.783 U 0.319 0.359 40.7 45.8 1 10.0-120 11.8 35
Nitrobenzene 0.783 U 0.299 0.345 38.1 44.0 1 10.0-120 14.3 36
Benzoic Acid 1.56 U 0.302 0.353 19.3 22.6 1 10.0-152 15.4 40
n-Nitrosodiphenylamine 0.783 U 0.355 0.473 45.3 60.4 1 17.0-120 28.4 29
n-Nitrosodi-n-propylamine 0.783 U 0.316 0.407 40.4 52.0 1 10.0-120 25.0 37
Phenanthrene 0.783 U 0.374 0.490 47.7 62.6 1 17.0-120 26.9 31
Benzylbutyl phthalate 0.783 U 0.383 0.537 48.9 68.6 1 23.0-120 J3 33.5 30
Bis(2-ethylhexyl)phthalate 0.783 U 0.363 0.503 46.4 64.3 1 17.0-126 J3 32.3 30
Di-n-butyl phthalate 0.783 U 0.372 0.520 47.4 66.4 1 30.0-120 J3 33.2 29
Diethyl phthalate 0.783 U 0.382 0.529 48.8 67.6 1 26.0-120 J3 32.3 28
Dimethyl phthalate 0.783 U 0.377 0.511 48.2 65.3 1 25.0-120 J3 30.2 29
Di-n-octyl phthalate 0.783 U 0.382 0.542 48.8 69.2 1 21.0-123 J3 34.6 29
Pyrene 0.783 U 0.376 0.501 48.0 64.0 1 16.0-121 28.4 32
4-Chloro-3-methylphenol 0.783 U 0.327 0.429 41.7 54.8 1 15.0-120 27.1 30
2-Chlorophenol 0.783 U 0.366 0.460 46.7 58.7 1 15.0-120 22.8 37
2-Methylphenol 0.783 U 0.330 0.450 42.2 57.5 1 11.0-120 30.7 40
3&4-Methyl Phenol 0.783 U 0.376 0.495 48.0 63.2 1 12.0-123 27.3 38
2,4-Dichlorophenol 0.783 U 0.345 0.446 44.0 56.9 1 20.0-120 25.6 31
2,4-Dimethylphenol 0.783 U 0.229 0.342 29.3 43.7 1 10.0-120 J3 39.5 33
4,6-Dinitro-2-methylphenol 0.783 U 0.466 0.620 59.5 79.1 1 10.0-120 28.4 39
2,4-Dinitrophenol 0.783 U 0.460 0.613 58.7 78.2 1 10.0-121 28.5 40
2-Nitrophenol 0.783 U 0.372 0.464 47.4 59.3 1 12.0-120 22.2 39
4-Nitrophenol 0.783 U 0.341 0.507 43.5 64.7 1 10.0-137 J3 39.1 32
Pentachlorophenol 0.783 U 0.335 0.468 42.8 59.8 1 10.0-160 J3 33.1 31
Phenol 0.783 U 0.335 0.430 42.8 55.0 1 12.0-120 24.9 38
2,4,6-Trichlorophenol 0.783 U 0.380 0.528 48.5 67.4 1 19.0-120 J3 32.6 32
(S) Nitrobenzene-d5 42.6 48.0 10.0-122
(S) 2-Fluorobiphenyl 51.4 59.8 15.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1318945
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1121787-03,04
L1121552-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1121552-01 07/29/19 01:12 • (MS) R3435408-3 07/29/19 01:32 • (MSD) R3435408-4 07/29/19 01:51
Spike Amount
(dry)
Original Result
(dry)MS Result (dry)MSD Result
(dry)MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg mg/kg mg/kg mg/kg %%%%%
(S) p-Terphenyl-d14 53.2 69.1 10.0-120
(S) Phenol-d5 46.5 58.7 10.0-120
(S) 2-Fluorophenol 53.0 65.0 12.0-120
(S) 2,4,6-Tribromophenol 61.7 78.8 10.0-127
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry)Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
RDL (dry)Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J2 Surrogate recovery limits have been exceeded; values are outside lower control limits.
J3 The associated batch QC was outside the established quality control range for precision.
J4 The associated batch QC was outside the established quality control range for accuracy.
J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low.
N The analyte is tentatively identified and the associated numerical value may not be consistent with the actual concentration present in the sample.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 43 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 43 of 53
ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 15:59 44 of 53
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1121787 08/08/19 16:09 44 of 53
Page 1 of 3

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006934 Facility ID 0000015480
Address:566 Old Hollow Rd
City:Winston-Salem State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:180345 Work Order #:1103241108

COC ID # 00051527
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Nicole Long
Address:3502 Hayes Road, Monroe, NC 28110
Phone #:Fax #:
Sampler:Corey Buchanan
Shipped:FedExp
Tracking #:100259868672
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-1 07/23/2019 03:12pm W 5 1LG HCL U&A MADEP EPH TC #342 MADEP EPH
VOA HCL BTEX by 6200B NC task code 2726200B
VOA NA2S2O3 EDB 504.1 NC Task Code 280 504.1
VOA HCL TAEE-Oxygenate 6200B
VOA HCL U&A MADEP VPH TC #341 MADEP VPH
1LAG COOL 625 10 TICS NC Task Code 301 625
VOA HCL TBF-Oxygenate- TC #240 6200B
VOA HCL 4 Oxygenates + Ethanol TC 240 6200B
250 ML HNO3 Lead 6010 6010
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/3 https://www.speedway-ids.com
Page 2 of 3

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006934 Facility ID 0000015480
Address:566 Old Hollow Rd
City:Winston-Salem State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:180345 Work Order #:1103241108

COC ID # 00051527
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Nicole Long
Address:3502 Hayes Road, Monroe, NC 28110
Phone #:Fax #:
Sampler:Corey Buchanan
Shipped:FedExp
Tracking #:100259868672
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-1 (10')07/23/2019 10:56am S 5 4 OZ COOL Total Solids 2540 G
VOA MEOH U&A MADEP VPH TC #421 MADEP VPH
4 OZ COOL U&A MADEP EPH TC #422 MADEP EPH
8 OZ JAR COOL SVOCs(R)-8270E-TC #410 8270E
VOA MEOH/NAHSO4VOC's- TC#409 8260D
MW-1 (20')07/23/2019 11:06am S 5 4 OZ COOL Total Solids 2540 G
VOA MEOH U&A MADEP VPH TC #421 MADEP VPH
4 OZ COOL U&A MADEP EPH TC #422 MADEP EPH
8 OZ JAR COOL SVOCs(R)-8270E-TC #410 8270E
VOA MEOH/NAHSO4VOC's- TC#409 8260D
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.2/3 https://www.speedway-ids.com
Page 3 of 3

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006934 Facility ID 0000015480
Address:566 Old Hollow Rd
City:Winston-Salem State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:180345 Work Order #:1103241108

COC ID # 00051527
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Nicole Long
Address:3502 Hayes Road, Monroe, NC 28110
Phone #:Fax #:
Sampler:Corey Buchanan
Shipped:FedExp
Tracking #:100259868672
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
TRIP BLANK 07/23/2019 08:40am W 1 VOA HCL BTEX by 6200B NC task code 2726200B
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.3/3 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51527 Printed: 09/23/2019
Analysis Name: 4 Oxygenates + Ethanol TC 240 ( Water )
Analysis Description / Method:4 Oxygenates + Ethanol TC 240 / 6200B
Container Type / Preservative:VOA / HCL
Analytes: Ethanol ug/L, Ethyl tert-butyl ether ug/L, t-Butyl alcohol ug/L, tert-Amyl alcohol ug/L, tert-Amyl methyl ether ug/L

Analysis Name: 625 10 TICS NC Task Code 301 ( Water )
Analysis Description / Method:625 10 TICS / 625
Container Type / Preservative:1LAG / COOL
Analytes: 1-Methylnaphthalene ug/L, 2,4,6-Trichlorophenol ug/L, 2,4-Dichlorophenol ug/L, 2,4-Dimethylphenol ug/L, 2,4-Dinitrophenol ug/L, 2,4-Dinitrotoluene ug/L, 2,6-Dinitrotoluene ug/L, 2-Chloronaphthalene ug/L,
2-Chlorophenol ug/L, 2-Methylnaphthalene ug/L, 2-Methylphenol ug/L, 2-Nitrophenol ug/L, 3,3'-Dichlorobenzidine ug/L, 3- & 4-Methylphenol ug/L, 4,6-Dinitro-o-cresol ug/L, 4-Bromophenyl phenyl ether ug/L,
4-Chloro-3-methylphenol ug/L, 4-Chloroaniline ug/L, 4-Chlorophenyl phenyl ether ug/L, 4-Nitrophenol ug/L, Acenaphthene ug/L, Acenaphthylene ug/L, Anthracene ug/L, Benzo(a)anthracene ug/L, Benzo(a)pyrene ug/L,
Benzo(b)fluoranthene ug/L, Benzo(g,h,I)perylene ug/L, Benzo(k)fluoranthene ug/L, Benzoic acid ug/L, Bis(2-chloroethoxy)methane ug/L, Bis(2-chloroisopropyl)ether ug/L, Bis(2-ethylhexyl)phthalate ug/L, Butyl benzyl
phthalate ug/L, Chrysene ug/L, Di-n-butyl phthalate ug/L, Di-n-octyl phthalate ug/L, Dibenzo(a,h)anthracene ug/L, Dibenzofuran ug/L, Diethyl phthalate ug/L, Dimethyl phthalate ug/L, Fluoranthene ug/L, Fluorene ug/L,
Hexachlorobenzene ug/L, Hexachlorobutadiene ug/L, Hexachlorocyclopentadiene ug/L, Hexachloroethane ug/L, Indeno(1,2,3-cd)pyrene ug/L, Isophorone ug/L, N-Nitroso-di-n-propylamine ug/L, N-Nitrosodiphenylamine
ug/L, Naphthalene ug/L, Nitrobenzene ug/L, Pentachlorophenol ug/L, Phenanthrene ug/L, Phenol ug/L, Pyrene ug/L

Analysis Name: BTEX by 6200B NC task code 272 ( Water )
Analysis Description / Method:6200B / 6200B
Container Type / Preservative:VOA / HCL
Analytes: 1,1,1,2-Tetrachloroethane ug/L, 1,1,1-Trichloroethane ug/L, 1,1,2,2-Tetrachloroethane ug/L, 1,1,2-Trichloroethane ug/L, 1,1-Dichloroethane ug/L, 1,1-Dichloroethylene ug/L, 1,1-Dichloropropene ug/L,
1,2,3-Trichlorobenzene ug/L, 1,2,3-Trichloropropane ug/L, 1,2,3-Trimethylbenzene ug/L, 1,2,4-Trichlorobenzene ug/L, 1,2,4-Trimethylbenzene ug/L, 1,2-Dibromo-3-chloropropane ug/L, 1,2-Dibromoethane ug/L,
Speedway LLC.1/5 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51527 Printed: 09/23/2019
1,2-Dichlorobenzene ug/L, 1,2-Dichloroethane ug/L, 1,2-Dichloropropane ug/L, 1,3,5-Trimethylbenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,3-Dichloropropane ug/L, 1,4-Dichlorobenzene ug/L, 2,2-Dichloropropane ug/L,
Benzene ug/L, Bromobenzene ug/L, Bromochloromethane ug/L, Bromodichloromethane ug/L, Bromoform ug/L, Carbon tetrachloride ug/L, Chlorobenzene ug/L, Chloroethane ug/L, Chloroform ug/L,
Dibromochloromethane ug/L, Dichlorodifluoromethane ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Hexachlorobutadiene ug/L, Isopropylbenzene ug/L, Methyl bromide ug/L, Methyl chloride ug/L, Methyl tert butyl
ether ug/L, Methylene bromide ug/L, Methylene chloride ug/L, Naphthalene ug/L, Styrene ug/L, Tetrachloroethyllene ug/L, Toluene ug/L, Trichloroethylene ug/L, Trichlorofluoromethane ug/L, Vinyl chloride ug/L, Xylene
ug/L, cis-1,2-Dichloroethylene ug/L, cis-1,3-Dichloropropene ug/L, n-Butylbenzene ug/L, n-Propylbenzene ug/L, o-Chlorotoluene ug/L, p-Isopropyltoluene ug/L, p-chlorotoluene ug/L, sec-Butylbenzene ug/L,
tert-Butylbenzene ug/L, trans-1,2-Dichloroethylene ug/L, trans-1,3-Dichloropropene ug/L

Analysis Name: EDB 504.1 NC Task Code 280 ( Water )
Analysis Description / Method:EDB by 504.1 / 504.1
Container Type / Preservative:VOA / NA2S2O3
Analytes: 1,2-Dibromoethane ug/L

Analysis Name: Lead 6010 ( Water )
Analysis Description / Method:Lead 6010 / 6010
Container Type / Preservative:250 ML / HNO3
Analytes: Lead ug/L

Analysis Name: SVOCs(R)-8270E-TC #410 ( Soil )
Analysis Description / Method:SVOCs(R)-8270E-TC #410 / 8270E
Container Type / Preservative:8 OZ JAR / COOL
Analytes: 1-Methylnaphthalene mg/Kg, 2,4,6-Trichlorophenol mg/Kg, 2,4-Dichlorophenol mg/Kg, 2,4-Dimethylphenol mg/Kg, 2,4-Dinitrophenol mg/Kg, 2,4-Dinitrotoluene mg/Kg, 2,6-Dinitrotoluene mg/Kg,
2-Chloronaphthalene mg/Kg, 2-Chlorophenol mg/Kg, 2-Methylnaphthalene mg/Kg, 2-Methylphenol mg/Kg, 2-Nitrophenol mg/Kg, 3,3'-Dichlorobenzidine mg/Kg, 3- & 4-Methylphenol mg/Kg, 4,6-Dinitro-o-cresol mg/Kg,
4-Bromophenyl phenyl ether mg/Kg, 4-Chloro-3-methylphenol mg/Kg, 4-Chloroaniline mg/Kg, 4-Chlorophenyl phenyl ether mg/Kg, 4-Nitrophenol mg/Kg, Acenaphthene mg/Kg, Acenaphthylene mg/Kg, Anthracene mg/Kg,
Speedway LLC.2/5 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51527 Printed: 09/23/2019
Benzo(a)anthracene mg/Kg, Benzo(a)pyrene mg/Kg, Benzo(b)fluoranthene mg/Kg, Benzo(g,h,I)perylene mg/Kg, Benzo(k)fluoranthene mg/Kg, Benzoic acid mg/Kg, Bis(2-chloroethoxy)methane mg/Kg,
Bis(2-chloroisopropyl)ether mg/Kg, Bis(2-ethylhexyl)phthalate mg/Kg, Butyl benzyl phthalate mg/Kg, Chrysene mg/Kg, Di-n-butyl phthalate mg/Kg, Di-n-octyl phthalate mg/Kg, Dibenz(a,h)anthracene mg/Kg, Dibenzofuran
mg/Kg, Diethyl phthalate mg/Kg, Dimethyl phthalate mg/Kg, Fluoranthene mg/Kg, Fluorene mg/Kg, Hexachlorobenzene mg/Kg, Hexachlorobutadiene mg/Kg, Hexachlorocyclopentadiene mg/Kg, Hexachloroethane mg/Kg,
Indeno(1,2,3-cd)pyrene mg/Kg, Isophorone mg/Kg, N-Nitroso-di-n-propylamine mg/Kg, N-Nitrosodiphenylamine mg/Kg, Naphthalene mg/Kg, Nitrobenzene mg/Kg, Pentachlorophenol mg/Kg, Phenanthrene mg/Kg, Phenol
mg/Kg, Pyrene mg/Kg, bis(2-Chloroethyl)ether mg/Kg

Analysis Name: TAEE-Oxygenate ( Water )
Analysis Description / Method:TAEE-Oxygenate / 6200B
Container Type / Preservative:VOA / HCL
Analytes: TERT-AMYL ETHYL ETHER ug/L

Analysis Name: TBF-Oxygenate- TC #240 ( Water )
Analysis Description / Method:TBF-Oxygenate- TC #240 / 6200B
Container Type / Preservative:VOA / HCL
Analytes: tert-Butyl formate ug/L

Analysis Name: Total Solids ( Soil )
Analysis Description / Method:Total Solids / 2540 G
Container Type / Preservative:4 OZ / COOL
Analytes: Solids,Total %

Analysis Name: U&A MADEP EPH TC #342 ( Water )
Analysis Description / Method:U&A MADEP EPH TC #342 / MADEP EPH
Container Type / Preservative:1LG / HCL
Speedway LLC.3/5 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51527 Printed: 09/23/2019
Analytes: Adjusted Total Petroleum hydrocarbon ug/L, C11-C22 Aromatics ug/L, C11-C22 aromatics (unadjusted) ug/L, Unadjusted C19-C36 Aliphatics ug/L, Unadjusted C9-C18 Aliphatics ug/L, Unadjusted Total
Petroleum hydrocarbon ug/L

Analysis Name: U&A MADEP EPH TC #422 ( Soil )
Analysis Description / Method:U&A MADEP EPH TC #422 / MADEP EPH
Container Type / Preservative:4 OZ / COOL
Analytes: Adjusted Total Petroleum hydrocarbon mg/Kg, C11-C22 Aromatics mg/Kg, C11-C22 aromatics (unadjusted) mg/Kg, Unadjusted C19-C36 Aliphatics mg/Kg, Unadjusted C9-C18 Aliphatics mg/Kg, Unadjusted
Total Petroleum hydrocarbon mg/Kg

Analysis Name: U&A MADEP VPH TC #341 ( Water )
Analysis Description / Method:U&A MADEP VPH TC #341 / MADEP VPH
Container Type / Preservative:VOA / HCL
Analytes: C5-C8 Aliphatics ug/L, C5-C8 aliphatics (unadjusted) ug/L, C9-C10 aromatics (unadjusted) ug/L, C9-C12 Aliphatics ug/L, C9-C12 aliphatics (unadjusted) ug/L, Total Purgeable Hydrocarbons ug/L, Total VPH
ug/L

Analysis Name: U&A MADEP VPH TC #421 ( Soil )
Analysis Description / Method:U&A MADEP VPH Task Code #421 / MADEP VPH
Container Type / Preservative:VOA / MEOH
Analytes: C5-C8 Aliphatics mg/Kg, C5-C8 aliphatics (unadjusted) mg/Kg, C9-C10 aromatics (unadjusted) mg/Kg, C9-C12 Aliphatics mg/Kg, C9-C12 aliphatics (unadjusted) mg/Kg, Total Purgeable Hydrocarbons mg/Kg,
Total VPH mg/Kg

Analysis Name: VOC's- TC#409 ( Soil )
Analysis Description / Method:VOC'S- TC#409 / 8260D
Container Type / Preservative:VOA / MEOH/NAHSO4
Speedway LLC.4/5 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 51527 Printed: 09/23/2019
Analytes: 1,2,3-Trichlorobenzene mg/Kg, 1,2,4-Trichlorobenzene mg/Kg, 1,2,4-Trimethylbenzene mg/Kg, 1,2-Dibromoethane mg/Kg, 1,2-Dichloroethane mg/Kg, 1,3,5-Trimethylbenzene mg/Kg, 2-Butanone mg/Kg,
Acetone mg/Kg, Benzene mg/Kg, Diisopropyl ether mg/Kg, Ethylbenzene mg/Kg, Isopropylbenzene mg/Kg, Methyl tert butyl ether mg/Kg, Methylene chloride mg/Kg, Naphthalene mg/Kg, Styrene mg/Kg, Toluene mg/Kg,
Total Xylenes mg/Kg, n-Butylbenzene mg/Kg, n-Propylbenzene mg/Kg, sec-Butylbenzene mg/Kg, tert-Butylbenzene mg/Kg

Speedway LLC.5/5 https://www.speedway-ids.com
ANALYTICAL REPORT
December 30, 2019
Geological Resources- NC Speedway
Sample Delivery Group:L1173221
Samples Received:12/20/2019
Project Number:4341
Description:Speedway 6934
Site:6934
Report To:Ms. Nicole Long
3502 Hayes Rd.
Charlotte, NC 28110
Entire Report Reviewed By:
December 30, 2019
[Preliminary Report]
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received.
12065 Lebanon Rd Mount Juliet, TN 37122 615-758-5858 800-767-5859 www.pacenational.com
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 12/30/19 15:15 1 of 28
January 02, 2020
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 01/02/20 15:25 1 of 28
ONE LAB. NATIONWIDE.TABLE OF CONTENTS
Cp: Cover Page 1
Tc: Table of Contents 2
Ss: Sample Summary 3
Cn: Case Narrative 4
Sr: Sample Results 5
TRIP BLANK L1173221-01 5
MW-2 L1173221-02 7
MW-3 L1173221-03 9
MW-4 L1173221-04 11
Qc: Quality Control Summary 13
Metals (ICP) by Method 6010D 13
Volatile Petroleum Hydrocarbons by Method MADEPV 14
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 15
EDB / DBCP by Method 504.1 20
Gl: Glossary of Terms 22
Al: Accreditations & Locations 23
Sc: Sample Chain of Custody 24
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 12/30/19 15:15 2 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 01/02/20 15:25 2 of 28
ONE LAB. NATIONWIDE.SAMPLE SUMMARY
Collected by Collected date/time Received date/time
TRIP BLANK L1173221-01 GW Corey Buchanan 12/19/19 09:10 12/20/19 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1402647 1 12/26/19 13:19 12/26/19 13:19 DWR Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-2 L1173221-02 GW Corey Buchanan 12/19/19 12:41 12/20/19 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG1400665 1 12/23/19 06:09 12/24/19 18:59 TRB Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1400735 1 12/21/19 17:35 12/21/19 17:35 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997 WG1403302 1 12/30/19 13:11 12/30/19 13:11 JAH Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1402647 1 12/26/19 18:23 12/26/19 18:23 DWR Mt. Juliet, TN
EDB / DBCP by Method 504.1 WG1402506 1 12/26/19 10:03 12/26/19 19:45 KLM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-3 L1173221-03 GW Corey Buchanan 12/19/19 13:43 12/20/19 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG1400665 1 12/23/19 06:09 12/24/19 19:02 TRB Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1400735 5 12/21/19 18:08 12/21/19 18:08 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1402647 20 12/26/19 18:43 12/26/19 18:43 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1403302 500 12/30/19 13:32 12/30/19 13:32 JAH Mt. Juliet, TN
EDB / DBCP by Method 504.1 WG1402506 1 12/26/19 10:03 12/26/19 19:56 KLM Mt. Juliet, TN
Collected by Collected date/time Received date/time
MW-4 L1173221-04 GW Corey Buchanan 12/19/19 14:40 12/20/19 09:30
Method Batch Dilution Preparation Analysis Analyst Location
date/time date/time
Metals (ICP) by Method 6010D WG1400665 1 12/23/19 06:09 12/24/19 19:04 TRB Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV WG1400735 1 12/21/19 18:40 12/21/19 18:40 ACG Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1402647 1 12/26/19 19:03 12/26/19 19:03 DWR Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 WG1403302 1 12/30/19 13:53 12/30/19 13:53 JAH Mt. Juliet, TN
EDB / DBCP by Method 504.1 WG1403039 1 12/27/19 09:15 12/27/19 21:47 LEL Mt. Juliet, TN
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
[Preliminary Report]
T. Alan Harvill
Project Manager
Project Narrative
Due to multiple preparation procedures, calculated analytes are not reported in the quality control samples for EPH and VPH
Methods.

1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 12/30/19 15:15 4 of 28
T. Alan Harvill
Project Manager
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1173221
TRIP BLANK
Collected date/time: 12/19/19 09:10
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/2019 13:19 WG1402647
1,1,1-Trichloroethane ND 1.00 1 12/26/2019 13:19 WG1402647
1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/2019 13:19 WG1402647
1,1,2-Trichloroethane ND 1.00 1 12/26/2019 13:19 WG1402647
1,1-Dichloroethane ND 1.00 1 12/26/2019 13:19 WG1402647
1,1-Dichloroethene ND 1.00 1 12/26/2019 13:19 WG1402647
1,1-Dichloropropene ND 1.00 1 12/26/2019 13:19 WG1402647
1,2,3-Trichlorobenzene ND 1.00 1 12/26/2019 13:19 WG1402647
1,2,3-Trichloropropane ND 2.50 1 12/26/2019 13:19 WG1402647
1,2,3-Trimethylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
1,2,4-Trichlorobenzene ND 1.00 1 12/26/2019 13:19 WG1402647
1,2,4-Trimethylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/2019 13:19 WG1402647
1,2-Dibromoethane ND 1.00 1 12/26/2019 13:19 WG1402647
1,2-Dichlorobenzene ND 1.00 1 12/26/2019 13:19 WG1402647
1,2-Dichloroethane ND 1.00 1 12/26/2019 13:19 WG1402647
1,2-Dichloropropane ND 1.00 1 12/26/2019 13:19 WG1402647
1,3,5-Trimethylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
1,3-Dichlorobenzene ND 1.00 1 12/26/2019 13:19 WG1402647
1,3-Dichloropropane ND 1.00 1 12/26/2019 13:19 WG1402647
1,4-Dichlorobenzene ND 1.00 1 12/26/2019 13:19 WG1402647
2,2-Dichloropropane ND 1.00 1 12/26/2019 13:19 WG1402647
Benzene ND 1.00 1 12/26/2019 13:19 WG1402647
Bromobenzene ND 1.00 1 12/26/2019 13:19 WG1402647
Bromochloromethane ND 1.00 1 12/26/2019 13:19 WG1402647
Bromodichloromethane ND 1.00 1 12/26/2019 13:19 WG1402647
Bromoform ND 1.00 1 12/26/2019 13:19 WG1402647
Carbon tetrachloride ND 1.00 1 12/26/2019 13:19 WG1402647
Chlorobenzene ND 1.00 1 12/26/2019 13:19 WG1402647
Chloroethane ND 5.00 1 12/26/2019 13:19 WG1402647
Chloroform ND 5.00 1 12/26/2019 13:19 WG1402647
Chlorodibromomethane ND 1.00 1 12/26/2019 13:19 WG1402647
Dichlorodifluoromethane ND 5.00 1 12/26/2019 13:19 WG1402647
Di-isopropyl ether ND 1.00 1 12/26/2019 13:19 WG1402647
Ethylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
Hexachloro-1,3-butadiene ND 1.00 1 12/26/2019 13:19 WG1402647
Isopropylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
Bromomethane ND 5.00 1 12/26/2019 13:19 WG1402647
Chloromethane ND 2.50 1 12/26/2019 13:19 WG1402647
Methyl tert-butyl ether ND 1.00 1 12/26/2019 13:19 WG1402647
Dibromomethane ND 1.00 1 12/26/2019 13:19 WG1402647
Methylene Chloride ND 5.00 1 12/26/2019 13:19 WG1402647
Naphthalene ND 5.00 1 12/26/2019 13:19 WG1402647
Styrene ND 1.00 1 12/26/2019 13:19 WG1402647
Tetrachloroethene ND 1.00 1 12/26/2019 13:19 WG1402647
Toluene ND 1.00 1 12/26/2019 13:19 WG1402647
Trichloroethene ND J4 1.00 1 12/26/2019 13:19 WG1402647
Trichlorofluoromethane ND 5.00 1 12/26/2019 13:19 WG1402647
Vinyl chloride ND 1.00 1 12/26/2019 13:19 WG1402647
Total Xylenes ND 3.00 1 12/26/2019 13:19 WG1402647
cis-1,2-Dichloroethene ND 1.00 1 12/26/2019 13:19 WG1402647
cis-1,3-Dichloropropene ND 1.00 1 12/26/2019 13:19 WG1402647
n-Butylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
n-Propylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
2-Chlorotoluene ND 1.00 1 12/26/2019 13:19 WG1402647
p-Isopropyltoluene ND 1.00 1 12/26/2019 13:19 WG1402647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 01
L1173221
TRIP BLANK
Collected date/time: 12/19/19 09:10
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
4-Chlorotoluene ND 1.00 1 12/26/2019 13:19 WG1402647
sec-Butylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
tert-Butylbenzene ND 1.00 1 12/26/2019 13:19 WG1402647
trans-1,2-Dichloroethene ND 1.00 1 12/26/2019 13:19 WG1402647
trans-1,3-Dichloropropene ND 1.00 1 12/26/2019 13:19 WG1402647
(S) Toluene-d8 107 80.0-120 12/26/2019 13:19 WG1402647
(S) 4-Bromofluorobenzene 99.1 77.0-126 12/26/2019 13:19 WG1402647
(S) 1,2-Dichloroethane-d4 96.8 70.0-130 12/26/2019 13:19 WG1402647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1173221
MW-2
Collected date/time: 12/19/19 12:41
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Lead ND 5.00 1 12/24/2019 18:59 WG1400665
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics ND 100 1 12/21/2019 17:35 WG1400735
Unadjusted C9-C12 Aliphatics ND 100 1 12/21/2019 17:35 WG1400735
Unadjusted C9-C10 Aromatics ND 100 1 12/21/2019 17:35 WG1400735
Adjusted C5-C8 Aliphatics ND 100 1 12/21/2019 17:35 WG1400735
Adjusted C9-C12 Aliphatics ND J 100 1 12/21/2019 17:35 WG1400735
Total VPH ND 200 1 12/21/2019 17:35 WG1400735
Total Purgeable Hydrocarbons C5-C12 ND 200 1 12/21/2019 17:35 WG1400735
(S) 2,5-Dibromotoluene(FID)97.1 70.0-130 12/21/2019 17:35 WG1400735
(S) 2,5-Dibromotoluene(PID)84.8 70.0-130 12/21/2019 17:35 WG1400735
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/2019 18:23 WG1402647
1,1,1-Trichloroethane ND 1.00 1 12/26/2019 18:23 WG1402647
1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/2019 18:23 WG1402647
1,1,2-Trichloroethane ND 1.00 1 12/26/2019 18:23 WG1402647
1,1-Dichloroethane ND 1.00 1 12/26/2019 18:23 WG1402647
1,1-Dichloroethene ND 1.00 1 12/26/2019 18:23 WG1402647
1,1-Dichloropropene ND 1.00 1 12/26/2019 18:23 WG1402647
1,2,3-Trichlorobenzene ND 1.00 1 12/26/2019 18:23 WG1402647
1,2,3-Trichloropropane ND 2.50 1 12/26/2019 18:23 WG1402647
1,2,3-Trimethylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
1,2,4-Trichlorobenzene ND 1.00 1 12/26/2019 18:23 WG1402647
1,2,4-Trimethylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/2019 18:23 WG1402647
1,2-Dibromoethane ND 1.00 1 12/26/2019 18:23 WG1402647
1,2-Dichlorobenzene ND 1.00 1 12/26/2019 18:23 WG1402647
1,2-Dichloroethane ND 1.00 1 12/26/2019 18:23 WG1402647
1,2-Dichloropropane ND 1.00 1 12/26/2019 18:23 WG1402647
1,3,5-Trimethylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
1,3-Dichlorobenzene ND 1.00 1 12/26/2019 18:23 WG1402647
1,3-Dichloropropane ND 1.00 1 12/26/2019 18:23 WG1402647
1,4-Dichlorobenzene ND 1.00 1 12/26/2019 18:23 WG1402647
2,2-Dichloropropane ND 1.00 1 12/26/2019 18:23 WG1402647
Benzene ND 1.00 1 12/26/2019 18:23 WG1402647
Bromobenzene ND 1.00 1 12/26/2019 18:23 WG1402647
Bromochloromethane ND 1.00 1 12/26/2019 18:23 WG1402647
Bromodichloromethane ND 1.00 1 12/26/2019 18:23 WG1402647
Bromoform ND 1.00 1 12/26/2019 18:23 WG1402647
Carbon tetrachloride ND 1.00 1 12/26/2019 18:23 WG1402647
Chlorobenzene ND 1.00 1 12/26/2019 18:23 WG1402647
Chloroethane ND 5.00 1 12/26/2019 18:23 WG1402647
Chloroform ND 5.00 1 12/26/2019 18:23 WG1402647
Chlorodibromomethane ND 1.00 1 12/26/2019 18:23 WG1402647
Dichlorodifluoromethane ND 5.00 1 12/26/2019 18:23 WG1402647
Di-isopropyl ether ND 1.00 1 12/26/2019 18:23 WG1402647
Ethanol ND 100 1 12/26/2019 18:23 WG1402647
Ethylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
Hexachloro-1,3-butadiene ND 1.00 1 12/26/2019 18:23 WG1402647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 01/02/20 15:25 7 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 02
L1173221
MW-2
Collected date/time: 12/19/19 12:41
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isopropylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
Bromomethane ND 5.00 1 12/26/2019 18:23 WG1402647
Chloromethane ND 2.50 1 12/26/2019 18:23 WG1402647
Methyl tert-butyl ether ND 1.00 1 12/26/2019 18:23 WG1402647
Dibromomethane ND 1.00 1 12/26/2019 18:23 WG1402647
Methylene Chloride ND 5.00 1 12/26/2019 18:23 WG1402647
Naphthalene ND 5.00 1 12/26/2019 18:23 WG1402647
Styrene ND 1.00 1 12/26/2019 18:23 WG1402647
Tetrachloroethene ND 1.00 1 12/26/2019 18:23 WG1402647
Toluene ND 1.00 1 12/26/2019 18:23 WG1402647
Trichloroethene ND J4 1.00 1 12/26/2019 18:23 WG1402647
Trichlorofluoromethane ND 5.00 1 12/26/2019 18:23 WG1402647
Vinyl chloride ND 1.00 1 12/26/2019 18:23 WG1402647
Total Xylenes ND 3.00 1 12/26/2019 18:23 WG1402647
cis-1,2-Dichloroethene ND 1.00 1 12/26/2019 18:23 WG1402647
cis-1,3-Dichloropropene ND 1.00 1 12/26/2019 18:23 WG1402647
n-Butylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
n-Propylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
2-Chlorotoluene ND 1.00 1 12/26/2019 18:23 WG1402647
p-Isopropyltoluene ND 1.00 1 12/26/2019 18:23 WG1402647
4-Chlorotoluene ND 1.00 1 12/26/2019 18:23 WG1402647
sec-Butylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
tert-Butylbenzene ND 1.00 1 12/26/2019 18:23 WG1402647
trans-1,2-Dichloroethene ND 1.00 1 12/26/2019 18:23 WG1402647
trans-1,3-Dichloropropene ND 1.00 1 12/26/2019 18:23 WG1402647
Ethyl tert-butyl ether ND 1.00 1 12/26/2019 18:23 WG1402647
t-Amyl Alcohol ND 50.0 1 12/26/2019 18:23 WG1402647
tert-Butyl alcohol ND 5.00 1 12/26/2019 18:23 WG1402647
tert-Amyl Methyl Ether ND 1.00 1 12/26/2019 18:23 WG1402647
Tert-Amyl Ethyl Ether ND 1.00 1 12/26/2019 18:23 WG1402647
tert-Butyl Formate ND 20.0 1 12/30/2019 13:11 WG1403302
(S) Toluene-d8 107 80.0-120 12/26/2019 18:23 WG1402647
(S) Toluene-d8 99.1 80.0-120 12/30/2019 13:11 WG1403302
(S) 1,2-Dichloroethane-d4 97.1 70.0-130 12/26/2019 18:23 WG1402647
(S) 1,2-Dichloroethane-d4 95.9 70.0-130 12/30/2019 13:11 WG1403302
(S) 4-Bromofluorobenzene 99.4 77.0-126 12/26/2019 18:23 WG1402647
(S) 4-Bromofluorobenzene 95.6 77.0-126 12/30/2019 13:11 WG1403302
EDB / DBCP by Method 504.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ethylene Dibromide ND 0.0100 1 12/26/2019 19:45 WG1402506
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 12/30/19 15:15 8 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 01/02/20 15:25 8 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1173221
MW-3
Collected date/time: 12/19/19 13:43
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Lead 5.29 5.00 1 12/24/2019 19:02 WG1400665
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 49700 500 5 12/21/2019 18:08 WG1400735
Unadjusted C9-C12 Aliphatics 25400 500 5 12/21/2019 18:08 WG1400735
Unadjusted C9-C10 Aromatics 4620 500 5 12/21/2019 18:08 WG1400735
Adjusted C5-C8 Aliphatics 20000 500 5 12/21/2019 18:08 WG1400735
Adjusted C9-C12 Aliphatics ND 500 5 12/21/2019 18:08 WG1400735
Total VPH 79700 1000 5 12/21/2019 18:08 WG1400735
Total Purgeable Hydrocarbons C5-C12 79000 1000 5 12/21/2019 18:08 WG1400735
(S) 2,5-Dibromotoluene(FID)113 70.0-130 12/21/2019 18:08 WG1400735
(S) 2,5-Dibromotoluene(PID)92.2 70.0-130 12/21/2019 18:08 WG1400735
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 20.0 20 12/26/2019 18:43 WG1402647
1,1,1-Trichloroethane ND 20.0 20 12/26/2019 18:43 WG1402647
1,1,2,2-Tetrachloroethane ND 20.0 20 12/26/2019 18:43 WG1402647
1,1,2-Trichloroethane ND 20.0 20 12/26/2019 18:43 WG1402647
1,1-Dichloroethane ND 20.0 20 12/26/2019 18:43 WG1402647
1,1-Dichloroethene ND 20.0 20 12/26/2019 18:43 WG1402647
1,1-Dichloropropene ND 20.0 20 12/26/2019 18:43 WG1402647
1,2,3-Trichlorobenzene ND 20.0 20 12/26/2019 18:43 WG1402647
1,2,3-Trichloropropane ND 50.0 20 12/26/2019 18:43 WG1402647
1,2,3-Trimethylbenzene 496 20.0 20 12/26/2019 18:43 WG1402647
1,2,4-Trichlorobenzene ND 20.0 20 12/26/2019 18:43 WG1402647
1,2,4-Trimethylbenzene 1170 20.0 20 12/26/2019 18:43 WG1402647
1,2-Dibromo-3-Chloropropane ND 100 20 12/26/2019 18:43 WG1402647
1,2-Dibromoethane ND 20.0 20 12/26/2019 18:43 WG1402647
1,2-Dichlorobenzene ND 20.0 20 12/26/2019 18:43 WG1402647
1,2-Dichloroethane ND 20.0 20 12/26/2019 18:43 WG1402647
1,2-Dichloropropane ND 20.0 20 12/26/2019 18:43 WG1402647
1,3,5-Trimethylbenzene 375 20.0 20 12/26/2019 18:43 WG1402647
1,3-Dichlorobenzene ND 20.0 20 12/26/2019 18:43 WG1402647
1,3-Dichloropropane ND 20.0 20 12/26/2019 18:43 WG1402647
1,4-Dichlorobenzene ND 20.0 20 12/26/2019 18:43 WG1402647
2,2-Dichloropropane ND 20.0 20 12/26/2019 18:43 WG1402647
Benzene 2970 20.0 20 12/26/2019 18:43 WG1402647
Bromobenzene ND 20.0 20 12/26/2019 18:43 WG1402647
Bromochloromethane ND 20.0 20 12/26/2019 18:43 WG1402647
Bromodichloromethane ND 20.0 20 12/26/2019 18:43 WG1402647
Bromoform ND 20.0 20 12/26/2019 18:43 WG1402647
Carbon tetrachloride ND 20.0 20 12/26/2019 18:43 WG1402647
Chlorobenzene ND 20.0 20 12/26/2019 18:43 WG1402647
Chloroethane ND 100 20 12/26/2019 18:43 WG1402647
Chloroform 132 100 20 12/26/2019 18:43 WG1402647
Chlorodibromomethane ND 20.0 20 12/26/2019 18:43 WG1402647
Dichlorodifluoromethane ND 100 20 12/26/2019 18:43 WG1402647
Di-isopropyl ether 45.1 20.0 20 12/26/2019 18:43 WG1402647
Ethanol ND 2000 20 12/26/2019 18:43 WG1402647
Ethylbenzene 1580 20.0 20 12/26/2019 18:43 WG1402647
Hexachloro-1,3-butadiene ND 20.0 20 12/26/2019 18:43 WG1402647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 12/30/19 15:15 9 of 28
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
Geological Resources- NC Speedway 4341 L1173221 01/02/20 15:25 9 of 28
ONE LAB. NATIONWIDE.SAMPLE RESULTS - 03
L1173221
MW-3
Collected date/time: 12/19/19 13:43
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isopropylbenzene ND 20.0 20 12/26/2019 18:43 WG1402647
Bromomethane ND 100 20 12/26/2019 18:43 WG1402647
Chloromethane ND 50.0 20 12/26/2019 18:43 WG1402647
Methyl tert-butyl ether 70.9 20.0 20 12/26/2019 18:43 WG1402647
Dibromomethane ND 20.0 20 12/26/2019 18:43 WG1402647
Methylene Chloride ND 100 20 12/26/2019 18:43 WG1402647
Naphthalene 189 100 20 12/26/2019 18:43 WG1402647
Styrene ND 20.0 20 12/26/2019 18:43 WG1402647
Tetrachloroethene ND 20.0 20 12/26/2019 18:43 WG1402647
Toluene 26700 500 500 12/30/2019 13:32 WG1403302
Trichloroethene ND J4 20.0 20 12/26/2019 18:43 WG1402647
Trichlorofluoromethane ND 100 20 12/26/2019 18:43 WG1402647
Vinyl chloride ND 20.0 20 12/26/2019 18:43 WG1402647
Total Xylenes 10200 60.0 20 12/26/2019 18:43 WG1402647
cis-1,2-Dichloroethene ND 20.0 20 12/26/2019 18:43 WG1402647
cis-1,3-Dichloropropene ND 20.0 20 12/26/2019 18:43 WG1402647
n-Butylbenzene ND 20.0 20 12/26/2019 18:43 WG1402647
n-Propylbenzene 132 20.0 20 12/26/2019 18:43 WG1402647
2-Chlorotoluene ND 20.0 20 12/26/2019 18:43 WG1402647
p-Isopropyltoluene ND 20.0 20 12/26/2019 18:43 WG1402647
4-Chlorotoluene ND 20.0 20 12/26/2019 18:43 WG1402647
sec-Butylbenzene ND 20.0 20 12/26/2019 18:43 WG1402647
tert-Butylbenzene ND 20.0 20 12/26/2019 18:43 WG1402647
trans-1,2-Dichloroethene ND 20.0 20 12/26/2019 18:43 WG1402647
trans-1,3-Dichloropropene ND 20.0 20 12/26/2019 18:43 WG1402647
Ethyl tert-butyl ether ND 20.0 20 12/26/2019 18:43 WG1402647
t-Amyl Alcohol 16100 1000 20 12/26/2019 18:43 WG1402647
tert-Butyl alcohol 648 100 20 12/26/2019 18:43 WG1402647
tert-Amyl Methyl Ether ND 20.0 20 12/26/2019 18:43 WG1402647
Tert-Amyl Ethyl Ether ND 20.0 20 12/26/2019 18:43 WG1402647
tert-Butyl Formate ND 10000 500 12/30/2019 13:32 WG1403302
(S) Toluene-d8 107 80.0-120 12/26/2019 18:43 WG1402647
(S) Toluene-d8 101 80.0-120 12/30/2019 13:32 WG1403302
(S) 1,2-Dichloroethane-d4 98.6 70.0-130 12/26/2019 18:43 WG1402647
(S) 1,2-Dichloroethane-d4 94.1 70.0-130 12/30/2019 13:32 WG1403302
(S) 4-Bromofluorobenzene 94.5 77.0-126 12/26/2019 18:43 WG1402647
(S) 4-Bromofluorobenzene 96.8 77.0-126 12/30/2019 13:32 WG1403302
EDB / DBCP by Method 504.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ethylene Dibromide ND 0.0100 1 12/26/2019 19:56 WG1402506
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1173221
MW-4
Collected date/time: 12/19/19 14:40
Metals (ICP) by Method 6010D
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Lead 5.94 5.00 1 12/24/2019 19:04 WG1400665
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Unadjusted C5-C8 Aliphatics 133 100 1 12/21/2019 18:40 WG1400735
Unadjusted C9-C12 Aliphatics ND 100 1 12/21/2019 18:40 WG1400735
Unadjusted C9-C10 Aromatics ND 100 1 12/21/2019 18:40 WG1400735
Adjusted C5-C8 Aliphatics 129 100 1 12/21/2019 18:40 WG1400735
Adjusted C9-C12 Aliphatics ND J 100 1 12/21/2019 18:40 WG1400735
Total VPH 204 200 1 12/21/2019 18:40 WG1400735
Total Purgeable Hydrocarbons C5-C12 225 B 200 1 12/21/2019 18:40 WG1400735
(S) 2,5-Dibromotoluene(FID)94.5 70.0-130 12/21/2019 18:40 WG1400735
(S) 2,5-Dibromotoluene(PID)81.9 70.0-130 12/21/2019 18:40 WG1400735
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
1,1,1,2-Tetrachloroethane ND 1.00 1 12/26/2019 19:03 WG1402647
1,1,1-Trichloroethane ND 1.00 1 12/26/2019 19:03 WG1402647
1,1,2,2-Tetrachloroethane ND 1.00 1 12/26/2019 19:03 WG1402647
1,1,2-Trichloroethane ND 1.00 1 12/26/2019 19:03 WG1402647
1,1-Dichloroethane ND 1.00 1 12/26/2019 19:03 WG1402647
1,1-Dichloroethene ND 1.00 1 12/26/2019 19:03 WG1402647
1,1-Dichloropropene ND 1.00 1 12/26/2019 19:03 WG1402647
1,2,3-Trichlorobenzene ND 1.00 1 12/26/2019 19:03 WG1402647
1,2,3-Trichloropropane ND 2.50 1 12/26/2019 19:03 WG1402647
1,2,3-Trimethylbenzene ND 1.00 1 12/26/2019 19:03 WG1402647
1,2,4-Trichlorobenzene ND 1.00 1 12/26/2019 19:03 WG1402647
1,2,4-Trimethylbenzene ND 1.00 1 12/30/2019 13:53 WG1403302
1,2-Dibromo-3-Chloropropane ND 5.00 1 12/26/2019 19:03 WG1402647
1,2-Dibromoethane ND 1.00 1 12/26/2019 19:03 WG1402647
1,2-Dichlorobenzene ND 1.00 1 12/26/2019 19:03 WG1402647
1,2-Dichloroethane ND 1.00 1 12/26/2019 19:03 WG1402647
1,2-Dichloropropane ND 1.00 1 12/26/2019 19:03 WG1402647
1,3,5-Trimethylbenzene ND 1.00 1 12/30/2019 13:53 WG1403302
1,3-Dichlorobenzene ND 1.00 1 12/26/2019 19:03 WG1402647
1,3-Dichloropropane ND 1.00 1 12/26/2019 19:03 WG1402647
1,4-Dichlorobenzene ND 1.00 1 12/26/2019 19:03 WG1402647
2,2-Dichloropropane ND 1.00 1 12/26/2019 19:03 WG1402647
Benzene ND 1.00 1 12/26/2019 19:03 WG1402647
Bromobenzene ND 1.00 1 12/26/2019 19:03 WG1402647
Bromochloromethane ND 1.00 1 12/26/2019 19:03 WG1402647
Bromodichloromethane ND 1.00 1 12/26/2019 19:03 WG1402647
Bromoform ND 1.00 1 12/26/2019 19:03 WG1402647
Carbon tetrachloride ND 1.00 1 12/26/2019 19:03 WG1402647
Chlorobenzene ND 1.00 1 12/26/2019 19:03 WG1402647
Chloroethane ND 5.00 1 12/26/2019 19:03 WG1402647
Chloroform ND 5.00 1 12/26/2019 19:03 WG1402647
Chlorodibromomethane ND 1.00 1 12/26/2019 19:03 WG1402647
Dichlorodifluoromethane ND 5.00 1 12/26/2019 19:03 WG1402647
Di-isopropyl ether ND 1.00 1 12/26/2019 19:03 WG1402647
Ethanol ND 100 1 12/26/2019 19:03 WG1402647
Ethylbenzene ND 1.00 1 12/26/2019 19:03 WG1402647
Hexachloro-1,3-butadiene ND 1.00 1 12/26/2019 19:03 WG1402647
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.SAMPLE RESULTS - 04
L1173221
MW-4
Collected date/time: 12/19/19 14:40
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Isopropylbenzene ND 1.00 1 12/26/2019 19:03 WG1402647
Bromomethane ND 5.00 1 12/26/2019 19:03 WG1402647
Chloromethane ND 2.50 1 12/26/2019 19:03 WG1402647
Methyl tert-butyl ether ND 1.00 1 12/26/2019 19:03 WG1402647
Dibromomethane ND 1.00 1 12/26/2019 19:03 WG1402647
Methylene Chloride ND 5.00 1 12/26/2019 19:03 WG1402647
Naphthalene ND 5.00 1 12/26/2019 19:03 WG1402647
Styrene ND 1.00 1 12/26/2019 19:03 WG1402647
Tetrachloroethene ND 1.00 1 12/26/2019 19:03 WG1402647
Toluene 2.94 1.00 1 12/30/2019 13:53 WG1403302
Trichloroethene ND J4 1.00 1 12/26/2019 19:03 WG1402647
Trichlorofluoromethane ND 5.00 1 12/26/2019 19:03 WG1402647
Vinyl chloride ND 1.00 1 12/26/2019 19:03 WG1402647
Total Xylenes ND 3.00 1 12/30/2019 13:53 WG1403302
cis-1,2-Dichloroethene ND 1.00 1 12/26/2019 19:03 WG1402647
cis-1,3-Dichloropropene ND 1.00 1 12/26/2019 19:03 WG1402647
n-Butylbenzene ND 1.00 1 12/26/2019 19:03 WG1402647
n-Propylbenzene ND 1.00 1 12/26/2019 19:03 WG1402647
2-Chlorotoluene ND 1.00 1 12/26/2019 19:03 WG1402647
p-Isopropyltoluene ND 1.00 1 12/26/2019 19:03 WG1402647
4-Chlorotoluene ND 1.00 1 12/26/2019 19:03 WG1402647
sec-Butylbenzene ND 1.00 1 12/26/2019 19:03 WG1402647
tert-Butylbenzene ND 1.00 1 12/26/2019 19:03 WG1402647
trans-1,2-Dichloroethene ND 1.00 1 12/26/2019 19:03 WG1402647
trans-1,3-Dichloropropene ND 1.00 1 12/26/2019 19:03 WG1402647
Ethyl tert-butyl ether ND 1.00 1 12/26/2019 19:03 WG1402647
t-Amyl Alcohol ND 50.0 1 12/26/2019 19:03 WG1402647
tert-Butyl alcohol 75.7 5.00 1 12/26/2019 19:03 WG1402647
tert-Amyl Methyl Ether ND 1.00 1 12/26/2019 19:03 WG1402647
Tert-Amyl Ethyl Ether ND 1.00 1 12/26/2019 19:03 WG1402647
tert-Butyl Formate ND 20.0 1 12/30/2019 13:53 WG1403302
(S) Toluene-d8 107 80.0-120 12/26/2019 19:03 WG1402647
(S) Toluene-d8 98.8 80.0-120 12/30/2019 13:53 WG1403302
(S) 1,2-Dichloroethane-d4 96.2 70.0-130 12/26/2019 19:03 WG1402647
(S) 1,2-Dichloroethane-d4 93.7 70.0-130 12/30/2019 13:53 WG1403302
(S) 4-Bromofluorobenzene 101 77.0-126 12/26/2019 19:03 WG1402647
(S) 4-Bromofluorobenzene 95.8 77.0-126 12/30/2019 13:53 WG1403302
EDB / DBCP by Method 504.1
Result Qualifier RDL Dilution Analysis Batch
Analyte ug/l ug/l date / time
Ethylene Dibromide ND 0.0100 1 12/27/2019 21:47 WG1403039
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1400665
Metals (ICP) by Method 6010D L1173221-02,03,04
Method Blank (MB)
(MB) R3485805-1 12/24/19 17:39
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Lead U 1.90 5.00
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3485805-2 12/24/19 17:42 • (LCSD) R3485805-3 12/24/19 17:44
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Lead 1000 975 976 97.5 97.6 80.0-120 0.117 20
L1172972-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1172972-01 12/24/19 17:47 • (MS) R3485805-5 12/24/19 17:52 • (MSD) R3485805-6 12/24/19 17:54
Spike Amount Original Result MS Result MSD Result MS Rec.MSD Rec.Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l ug/l %%%%%
Lead 1000 U 955 957 95.5 95.7 1 75.0-125 0.206 20
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1400735
Volatile Petroleum Hydrocarbons by Method MADEPV L1173221-02,03,04
Method Blank (MB)
(MB) R3484990-2 12/21/19 13:11
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Unadjusted C5-C8 Aliphatics U 33.3 100
Unadjusted C9-C12 Aliphatics U 33.3 100
Unadjusted C9-C10 Aromatics U 33.3 100
Adjusted C5-C8 Aliphatics U 33.3 100
Total VPH U 66.7 200
Adjusted C9-C12 Aliphatics U 33.3 100
Total Purgeable Hydrocarbons
C5-C12 79.2 J 66.7 200
(S) 2,5-Dibromotoluene(FID)85.8 70.0-130
(S) 2,5-Dibromotoluene(PID)76.9 70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3484990-1 12/21/19 10:07 • (LCSD) R3484990-3 12/22/19 03:27
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Unadjusted C5-C8 Aliphatics 1200 1140 1180 95.0 98.3 70.0-130 3.45 50
Unadjusted C9-C12 Aliphatics 1400 1410 1600 101 114 70.0-130 12.6 50
Unadjusted C9-C10 Aromatics 200 170 186 85.0 93.0 70.0-130 8.99 50
Total VPH 2800 2720 2970 97.1 106 70.0-130 8.79 50
Total Purgeable Hydrocarbons
C5-C12 2800 2910 3160 104 113 70.0-130 8.24 50
(S) 2,5-Dibromotoluene(FID) 97.5 102 70.0-130
(S) 2,5-Dibromotoluene(PID) 86.2 88.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402647
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1173221-01,02,03,04
Method Blank (MB)
(MB) R3486388-2 12/26/19 12:07
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Benzene U 0.331 1.00
Bromobenzene U 0.352 1.00
Bromodichloromethane U 0.380 1.00
Bromochloromethane U 0.520 1.00
Bromoform U 0.469 1.00
Bromomethane U 0.866 5.00
n-Butylbenzene U 0.361 1.00
sec-Butylbenzene U 0.365 1.00
tert-Butylbenzene U 0.399 1.00
Carbon tetrachloride U 0.379 1.00
Chlorobenzene U 0.348 1.00
Chlorodibromomethane U 0.327 1.00
Chloroethane U 0.453 5.00
Chloroform U 0.324 5.00
Chloromethane U 0.276 2.50
2-Chlorotoluene U 0.375 1.00
4-Chlorotoluene U 0.351 1.00
1,2-Dibromo-3-Chloropropane U 1.33 5.00
1,2-Dibromoethane U 0.381 1.00
Dibromomethane U 0.346 1.00
1,2-Dichlorobenzene U 0.349 1.00
1,3-Dichlorobenzene U 0.220 1.00
1,4-Dichlorobenzene U 0.274 1.00
Dichlorodifluoromethane U 0.551 5.00
1,1-Dichloroethane U 0.259 1.00
1,2-Dichloroethane U 0.361 1.00
1,1-Dichloroethene U 0.398 1.00
cis-1,2-Dichloroethene U 0.260 1.00
trans-1,2-Dichloroethene U 0.396 1.00
1,2-Dichloropropane U 0.306 1.00
1,1-Dichloropropene U 0.352 1.00
1,3-Dichloropropane U 0.366 1.00
cis-1,3-Dichloropropene U 0.419 1.00
trans-1,3-Dichloropropene U 0.419 1.00
2,2-Dichloropropane U 0.321 1.00
Di-isopropyl ether U 0.320 1.00
Ethylbenzene U 0.384 1.00
Ethanol U 42.0 100
Hexachloro-1,3-butadiene 0.399 J 0.256 1.00
Isopropylbenzene U 0.326 1.00
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402647
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1173221-01,02,03,04
Method Blank (MB)
(MB) R3486388-2 12/26/19 12:07
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
p-Isopropyltoluene U 0.350 1.00
Methylene Chloride U 1.00 5.00
Methyl tert-butyl ether U 0.367 1.00
Naphthalene U 1.00 5.00
n-Propylbenzene U 0.349 1.00
Styrene U 0.307 1.00
1,1,1,2-Tetrachloroethane U 0.385 1.00
1,1,2,2-Tetrachloroethane U 0.130 1.00
Tetrachloroethene U 0.372 1.00
Toluene U 0.412 1.00
1,2,3-Trichlorobenzene 0.279 J 0.230 1.00
1,2,4-Trichlorobenzene U 0.355 1.00
1,1,1-Trichloroethane U 0.319 1.00
1,1,2-Trichloroethane U 0.383 1.00
Trichloroethene 0.404 J 0.398 1.00
Trichlorofluoromethane U 1.20 5.00
1,2,3-Trichloropropane U 0.807 2.50
1,2,3-Trimethylbenzene U 0.355 1.00
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Vinyl chloride U 0.259 1.00
Xylenes, Total U 1.06 3.00
tert-Amyl Methyl Ether U 0.260 1.00
Ethyl tert-butyl ether U 0.270 1.00
tert-Butyl alcohol U 2.40 5.00
t-Amyl Alcohol U 4.90 50.0
Tert-Amyl Ethyl Ether U 0.401 1.00
(S) Toluene-d8 108 80.0-120
(S) 4-Bromofluorobenzene 99.4 77.0-126
(S) 1,2-Dichloroethane-d4 96.6 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3486388-1 12/26/19 11:47
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Benzene 5.00 5.06 101 70.0-123
Bromobenzene 5.00 4.53 90.6 73.0-121
Bromodichloromethane 5.00 4.65 93.0 75.0-120
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402647
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1173221-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R3486388-1 12/26/19 11:47
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Bromochloromethane 5.00 4.97 99.4 76.0-122
Bromoform 5.00 4.71 94.2 68.0-132
Bromomethane 5.00 5.51 110 10.0-160
n-Butylbenzene 5.00 4.78 95.6 73.0-125
sec-Butylbenzene 5.00 4.58 91.6 75.0-125
tert-Butylbenzene 5.00 4.31 86.2 76.0-124
Carbon tetrachloride 5.00 4.73 94.6 68.0-126
Chlorobenzene 5.00 5.04 101 80.0-121
Chlorodibromomethane 5.00 4.67 93.4 77.0-125
Chloroethane 5.00 4.59 91.8 47.0-150
Chloroform 5.00 5.08 102 73.0-120
Chloromethane 5.00 5.10 102 41.0-142
2-Chlorotoluene 5.00 4.64 92.8 76.0-123
4-Chlorotoluene 5.00 4.62 92.4 75.0-122
1,2-Dibromo-3-Chloropropane 5.00 4.58 91.6 58.0-134
1,2-Dibromoethane 5.00 4.98 99.6 80.0-122
Dibromomethane 5.00 4.85 97.0 80.0-120
1,2-Dichlorobenzene 5.00 4.87 97.4 79.0-121
1,3-Dichlorobenzene 5.00 4.83 96.6 79.0-120
1,4-Dichlorobenzene 5.00 4.96 99.2 79.0-120
Dichlorodifluoromethane 5.00 6.52 130 51.0-149
1,1-Dichloroethane 5.00 4.91 98.2 70.0-126
1,2-Dichloroethane 5.00 4.79 95.8 70.0-128
1,1-Dichloroethene 5.00 5.07 101 71.0-124
cis-1,2-Dichloroethene 5.00 5.22 104 73.0-120
trans-1,2-Dichloroethene 5.00 5.27 105 73.0-120
1,2-Dichloropropane 5.00 5.07 101 77.0-125
1,1-Dichloropropene 5.00 5.10 102 74.0-126
1,3-Dichloropropane 5.00 5.03 101 80.0-120
cis-1,3-Dichloropropene 5.00 4.74 94.8 80.0-123
trans-1,3-Dichloropropene 5.00 4.80 96.0 78.0-124
2,2-Dichloropropane 5.00 5.20 104 58.0-130
Di-isopropyl ether 5.00 4.80 96.0 58.0-138
Ethylbenzene 5.00 4.90 98.0 79.0-123
Hexachloro-1,3-butadiene 5.00 5.29 106 54.0-138
Isopropylbenzene 5.00 4.96 99.2 76.0-127
p-Isopropyltoluene 5.00 4.49 89.8 76.0-125
Methylene Chloride 5.00 5.10 102 67.0-120
Methyl tert-butyl ether 5.00 4.74 94.8 68.0-125
Naphthalene 5.00 4.72 94.4 54.0-135
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402647
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1173221-01,02,03,04
Laboratory Control Sample (LCS)
(LCS) R3486388-1 12/26/19 11:47
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
n-Propylbenzene 5.00 4.54 90.8 77.0-124
Styrene 5.00 4.69 93.8 73.0-130
1,1,1,2-Tetrachloroethane 5.00 4.85 97.0 75.0-125
1,1,2,2-Tetrachloroethane 5.00 4.98 99.6 65.0-130
Tetrachloroethene 5.00 5.11 102 72.0-132
Toluene 5.00 5.36 107 79.0-120
1,2,3-Trichlorobenzene 5.00 5.06 101 50.0-138
1,2,4-Trichlorobenzene 5.00 5.15 103 57.0-137
1,1,1-Trichloroethane 5.00 4.88 97.6 73.0-124
1,1,2-Trichloroethane 5.00 5.29 106 80.0-120
Trichloroethene 5.00 6.30 126 78.0-124 J4
Trichlorofluoromethane 5.00 5.55 111 59.0-147
1,2,3-Trichloropropane 5.00 4.82 96.4 73.0-130
1,2,3-Trimethylbenzene 5.00 4.58 91.6 77.0-120
1,2,4-Trimethylbenzene 5.00 4.32 86.4 76.0-121
1,3,5-Trimethylbenzene 5.00 4.45 89.0 76.0-122
Vinyl chloride 5.00 4.74 94.8 67.0-131
Xylenes, Total 15.0 14.8 98.7 79.0-123
Tert-Amyl Ethyl Ether 5.00 4.62 92.4 70.0-130
ethanol 250 237 94.8 10.0-160
tert-Butyl alcohol 25.0 23.6 94.4 27.0-160
tert-Amyl Methyl Ether 5.00 4.67 93.4 66.0-125
Ethyl tert-butyl ether 5.00 4.80 96.0 63.0-138
(S) Toluene-d8 107 80.0-120
(S) 4-Bromofluorobenzene 99.8 77.0-126
(S) 1,2-Dichloroethane-d4 97.8 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1403302
Volatile Organic Compounds (GC/MS) by Method 6200B-1997/6200B-2011 L1173221-02,03,04
Method Blank (MB)
(MB) R3486993-3 12/30/19 11:52
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Toluene U 0.412 1.00
1,2,4-Trimethylbenzene U 0.373 1.00
1,3,5-Trimethylbenzene U 0.387 1.00
Xylenes, Total U 1.06 3.00
tert-Butyl formate U 3.30 20.0
(S) Toluene-d8 99.2 80.0-120
(S) 4-Bromofluorobenzene 94.0 77.0-126
(S) 1,2-Dichloroethane-d4 96.3 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3486993-1 12/30/19 10:52
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Toluene 5.00 5.78 116 79.0-120
1,2,4-Trimethylbenzene 5.00 5.30 106 76.0-121
1,3,5-Trimethylbenzene 5.00 5.34 107 76.0-122
Xylenes, Total 15.0 16.4 109 79.0-123
(S) Toluene-d8 99.0 80.0-120
(S) 4-Bromofluorobenzene 96.6 77.0-126
(S) 1,2-Dichloroethane-d4 95.3 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3486993-2 12/30/19 11:12
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
tert-Butyl Formate 100 109 109 10.0-160
(S) Toluene-d8 99.2 80.0-120
(S) 4-Bromofluorobenzene 97.1 77.0-126
(S) 1,2-Dichloroethane-d4 89.7 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1402506
EDB / DBCP by Method 504.1 L1173221-02,03
Method Blank (MB)
(MB) R3486244-1 12/26/19 16:48
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ethylene Dibromide U 0.00240 0.0100
L1173144-14 Original Sample (OS) • Duplicate (DUP)
(OS) L1173144-14 12/26/19 17:32 • (DUP) R3486244-3 12/26/19 17:21
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/l ug/l %%
Ethylene Dibromide ND 0.000 1.01 0.000 20
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3486244-4 12/26/19 19:23 • (LCSD) R3486244-5 12/26/19 21:47
Spike Amount LCS Result LCSD Result LCS Rec.LCSD Rec.Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte ug/l ug/l ug/l %%%%%
Ethylene Dibromide 0.250 0.253 0.252 101 101 70.0-130 0.396 20
L1173449-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1173449-01 12/26/19 17:10 • (MS) R3486244-2 12/26/19 16:59
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ethylene Dibromide 0.102 U 0.114 112 1.02 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
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ONE LAB. NATIONWIDE.QUALITY CONTROL SUMMARYWG1403039
EDB / DBCP by Method 504.1 L1173221-04
Method Blank (MB)
(MB) R3486658-1 12/27/19 20:52
MB Result MB Qualifier MB MDL MB RDL
Analyte ug/l ug/l ug/l
Ethylene Dibromide U 0.00240 0.0100
L1173302-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1173302-01 12/27/19 21:36 • (DUP) R3486658-3 12/27/19 21:25
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte ug/l ug/l %%
Ethylene Dibromide ND 0.000 1.02 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3486658-4 12/27/19 23:27
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Ethylene Dibromide 0.250 0.261 104 70.0-130
Laboratory Control Sample (LCS)
(LCS) R3486658-5 12/28/19 01:50
Spike Amount LCS Result LCS Rec.Rec. Limits LCS Qualifier
Analyte ug/l ug/l %%
Ethylene Dibromide 0.250 0.263 105 70.0-130
L1173302-03 Original Sample (OS) • Matrix Spike (MS)
(OS) L1173302-03 12/27/19 21:14 • (MS) R3486658-2 12/27/19 21:03
Spike Amount Original Result MS Result MS Rec.Dilution Rec. Limits MS Qualifier
Analyte ug/l ug/l ug/l %%
Ethylene Dibromide 0.102 ND 0.108 106 1.02 70.0-130
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On-Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec.Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
(S)
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
Dilution
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
Limits
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non-spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
Qualifier
This column provides a letter and/or number designation that corresponds to additional information concerning the result
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
Result
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state “ND” (Not Detected) or “BDL”
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)Confidence level of 2 sigma.
Case Narrative (Cn)
A brief discussion about the included sample results, including a discussion of any non-conformances to protocol
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
Summary (Qc)
This section of the report includes the results of the laboratory quality control analyses required by procedure or
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
Sample Chain of
Custody (Sc)
This is the document created in the field when your samples were initially collected. This is used to verify the time and
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
Sample Results (Sr)
This section of your report will provide the results of all testing performed on your samples. These results are provided
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
B The same analyte is found in the associated blank.
J The identification of the analyte is acceptable; the reported value is an estimate.
J4 The associated batch QC was outside the established quality control range for accuracy.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn-around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
* Not all certifications held by the laboratory are applicable to the results reported in the attached report.
* Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.

State Accreditations
Alabama 40660 Nebraska NE-OS-15-05
Alaska 17-026 Nevada TN-03-2002-34
Arizona AZ0612 New Hampshire 2975
Arkansas 88-0469 New Jersey–NELAP TN002
California 2932 New Mexico ¹n/a
Colorado TN00003 New York 11742
Connecticut PH-0197 North Carolina Env375
Florida E87487 North Carolina ¹DW21704
Georgia NELAP North Carolina ³41
Georgia ¹923 North Dakota R-140
Idaho TN00003 Ohio–VAP CL0069
Illinois 200008 Oklahoma 9915
Indiana C-TN-01 Oregon TN200002
Iowa 364 Pennsylvania 68-02979
Kansas E-10277 Rhode Island LAO00356
Kentucky ¹ ⁶90010 South Carolina 84004
Kentucky ²16 South Dakota n/a
Louisiana AI30792 Tennessee ¹ ⁴2006
Louisiana ¹LA180010 Texas T104704245-18-15
Maine TN0002 Texas ⁵LAB0152
Maryland 324 Utah TN00003
Massachusetts M-TN003 Vermont VT2006
Michigan 9958 Virginia 460132
Minnesota 047-999-395 Washington C847
Mississippi TN00003 West Virginia 233
Missouri 340 Wisconsin 9980939910
Montana CERT0086 Wyoming A2LA

Third Party Federal Accreditations
A2LA – ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789
A2LA – ISO 17025 ⁵1461.02 DOD 1461.01
Canada 1461.01 USDA P330-15-00234
EPA–Crypto TN00003
ACCREDITATIONS & LOCATIONS

¹ Drinking Water ² Underground Storage Tanks ³ Aquatic Toxicity ⁴ Chemical/Microbiological ⁵ Mold ⁶ Wastewater n/a Accreditation not applicable

Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contactour main office. Pace National performs all testing at our central laboratory.
1 Cp
2Tc
3Ss
4Cn
5Sr
6Qc
7Gl
8Al
9Sc
ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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ACCOUNT:PROJECT:SDG:DATE/TIME:PAGE:
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Page 1 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006934 Facility ID 0000015480
Address:566 Old Hollow Rd
City:Winston-Salem State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190083 Work Order #:1103675080

COC ID # 00052417
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Joanna Alley
Address:3502 Hayes Road Monroe, NC 28110
Phone #:Fax #:
Sampler:Corey Buchanan
Shipped:FedExp
Tracking #:138248056227
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-2 12/19/2019 12:41pm W 10 VOA HCL BTEX by 6200B NC task code 2726200B
VOA NA2S2O3 EDB 504.1 NC Task Code 280 504.1
VOA HCL TAEE-Oxygenate 6200B
VOA HCL U&A MADEP VPH TC #341 MADEP VPH
VOA HCL 4 Oxygenates + Ethanol TC 240 6200B
VOA HCL TBF-Oxygenate- TC #240 6200B
250 ML HNO3 Lead 6010 6010
MW-3 12/19/2019 01:43pm W 10 VOA HCL BTEX by 6200B NC task code 2726200B
VOA NA2S2O3 EDB 504.1 NC Task Code 280 504.1
VOA HCL TAEE-Oxygenate 6200B
VOA HCL U&A MADEP VPH TC #341 MADEP VPH
VOA HCL 4 Oxygenates + Ethanol TC 240 6200B
VOA HCL TBF-Oxygenate- TC #240 6200B
250 ML HNO3 Lead 6010 6010
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.1/2 https://www.speedway-ids.com
Page 2 of 2

TURN AROUND TIME
STANDARD

Chain-of-Custody-Record
Speedway Project Information
Speedway Store #: C210006934 Facility ID 0000015480
Address:566 Old Hollow Rd
City:Winston-Salem State:NC
Phone #:Fax #:
Speedway Proj. Mgr: Charles Chiara **INVOICE TO SPEEDWAY**
AFE #:190083 Work Order #:1103675080

COC ID # 00052417
Lab Information
Lab:Pace Analytical Services (TN)
Consultant:Geological Resources, Inc. - Monroe, NC
Project Mgr: Joanna Alley
Address:3502 Hayes Road Monroe, NC 28110
Phone #:Fax #:
Sampler:Corey Buchanan
Shipped:FedExp
Tracking #:138248056227
Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks
MW-4 12/19/2019 02:40pm W 10 VOA HCL BTEX by 6200B NC task code 2726200B
VOA NA2S2O3 EDB 504.1 NC Task Code 280 504.1
VOA HCL TAEE-Oxygenate 6200B
VOA HCL U&A MADEP VPH TC #341 MADEP VPH
VOA HCL 4 Oxygenates + Ethanol TC 240 6200B
VOA HCL TBF-Oxygenate- TC #240 6200B
250 ML HNO3 Lead 6010 6010
TRIP BLANK 12/19/2019 09:10am W 1 VOA HCL BTEX by 6200B NC task code 2726200B
Relinquished by:Date Time Received by:Date Time
Relinquished by:Date Time Received by laboratory:Date Time
Special Reporting Requirements:Lab Notes:Temp
Speedway LLC.2/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 52417 Printed: 02/10/2020
Analysis Name: 4 Oxygenates + Ethanol TC 240 ( Water )
Analysis Description / Method:4 Oxygenates + Ethanol TC 240 / 6200B
Container Type / Preservative:VOA / HCL
Analytes: Ethanol ug/L, Ethyl tert-butyl ether ug/L, t-Butyl alcohol ug/L, tert-Amyl alcohol ug/L, tert-Amyl methyl ether ug/L

Analysis Name: BTEX by 6200B NC task code 272 ( Water )
Analysis Description / Method:6200B / 6200B
Container Type / Preservative:VOA / HCL
Analytes: 1,1,1,2-Tetrachloroethane ug/L, 1,1,1-Trichloroethane ug/L, 1,1,2,2-Tetrachloroethane ug/L, 1,1,2-Trichloroethane ug/L, 1,1-Dichloroethane ug/L, 1,1-Dichloroethylene ug/L, 1,1-Dichloropropene ug/L,
1,2,3-Trichlorobenzene ug/L, 1,2,3-Trichloropropane ug/L, 1,2,3-Trimethylbenzene ug/L, 1,2,4-Trichlorobenzene ug/L, 1,2,4-Trimethylbenzene ug/L, 1,2-Dibromo-3-chloropropane ug/L, 1,2-Dibromoethane ug/L,
1,2-Dichlorobenzene ug/L, 1,2-Dichloroethane ug/L, 1,2-Dichloropropane ug/L, 1,3,5-Trimethylbenzene ug/L, 1,3-Dichlorobenzene ug/L, 1,3-Dichloropropane ug/L, 1,4-Dichlorobenzene ug/L, 2,2-Dichloropropane ug/L,
Benzene ug/L, Bromobenzene ug/L, Bromochloromethane ug/L, Bromodichloromethane ug/L, Bromoform ug/L, Carbon tetrachloride ug/L, Chlorobenzene ug/L, Chloroethane ug/L, Chloroform ug/L,
Dibromochloromethane ug/L, Dichlorodifluoromethane ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Hexachlorobutadiene ug/L, Isopropylbenzene ug/L, Methyl bromide ug/L, Methyl chloride ug/L, Methyl tert butyl
ether ug/L, Methylene bromide ug/L, Methylene chloride ug/L, Naphthalene ug/L, Styrene ug/L, Tetrachloroethyllene ug/L, Toluene ug/L, Trichloroethylene ug/L, Trichlorofluoromethane ug/L, Vinyl chloride ug/L, Xylene
ug/L, cis-1,2-Dichloroethylene ug/L, cis-1,3-Dichloropropene ug/L, n-Butylbenzene ug/L, n-Propylbenzene ug/L, o-Chlorotoluene ug/L, p-Isopropyltoluene ug/L, p-chlorotoluene ug/L, sec-Butylbenzene ug/L,
tert-Butylbenzene ug/L, trans-1,2-Dichloroethylene ug/L, trans-1,3-Dichloropropene ug/L

Analysis Name: EDB 504.1 NC Task Code 280 ( Water )
Analysis Description / Method:EDB by 504.1 / 504.1
Container Type / Preservative:VOA / NA2S2O3
Analytes: 1,2-Dibromoethane ug/L

Speedway LLC.1/2 https://www.speedway-ids.com
Chain of Custody Analysis to be Performed Chain-of-Custody-Record
COC ID # 52417 Printed: 02/10/2020
Analysis Name: Lead 6010 ( Water )
Analysis Description / Method:Lead 6010 / 6010
Container Type / Preservative:250 ML / HNO3
Analytes: Lead ug/L

Analysis Name: TAEE-Oxygenate ( Water )
Analysis Description / Method:TAEE-Oxygenate / 6200B
Container Type / Preservative:VOA / HCL
Analytes: TERT-AMYL ETHYL ETHER ug/L

Analysis Name: TBF-Oxygenate- TC #240 ( Water )
Analysis Description / Method:TBF-Oxygenate- TC #240 / 6200B
Container Type / Preservative:VOA / HCL
Analytes: tert-Butyl formate ug/L

Analysis Name: U&A MADEP VPH TC #341 ( Water )
Analysis Description / Method:U&A MADEP VPH TC #341 / MADEP VPH
Container Type / Preservative:VOA / HCL
Analytes: C5-C8 Aliphatics ug/L, C5-C8 aliphatics (unadjusted) ug/L, C9-C10 aromatics (unadjusted) ug/L, C9-C12 Aliphatics ug/L, C9-C12 aliphatics (unadjusted) ug/L, Total Purgeable Hydrocarbons ug/L, Total VPH
ug/L

Speedway LLC.2/2 https://www.speedway-ids.com