25077_Raleigh Ice_Phase II_20110708

(Page 1 of 75)
enviroassessments
env Iroassessmen ts.cam
:B13&T ESA083038
BB&T Aect, Name: Biedermann Realty
Phase II Environmental Site Assessment
BIEDERMANN REALTY
912 West Hodges Street
Raleigh, Wake County, North Carolina
Prepared For:
Branch 3anking & Trust Company
5130 Parkway Plaza Boulevard
Charlotte, North Carolina 28217
[phone]
Prepared by:
EnviroAssessments
9307 Monroe Road, Suite K
Charlotte, North Carolina 28270
EA Project No. 08-7690.2
[phone]
July 8, 2011
I certify that this report and all attachments were prepared under my direction in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information
submitted. The information submitted is, to the best of my knowledge and belief,
true, accurate, and complete.
Michael P. McDermott Jr.
Environmental Scientist
CA����y
SfAt �
1$ l;g .�.► Cliff R. Lundgren, P.G.
Aift �� Senior Project Manager
!9;

TABLE OF CONTENTS
I
Pace Number
1.0 EXECUTIVE SUMMARY .......................................... ... ........... ...................... ............ „I ............... ......... ..1
2.0 INTRODUCTION ..................................... „...............................................................................................
,.3
3.0 BACKGROUND..........................................................................................................................................4
4.0 PHASE 11 ESA ACTIVITIES....................................................................................................................5
5.0 LABORATORY ANALYTICAL RESULTS...........................................................................................12
6.0 DISCUSSION OF FINDINGS AND CONCLUSIONS........................................................................„. 15
7.0 SIGNATURES OF ENVIRONMENTAL PROFESSIONALS................................................... „......... 116
Figures
Figure 1: Site Location Map
Figure 2: Site Plan
Tables
Table 1: Soil Sampling Analytical Results
Table 2: Groundwater Sampling Analytical Results
Appendices
Appendix 1: Laboratory Analytical Results and Chain of Custody Forms
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Phase lI Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
1.0 EXECUTIVE SUMMARY
EnviroAssessments (EA) has performed a Phase II Environmental Site Assessment (ESA) in conformance
with the scope and limitations ofthe American Society for Testing and Materials (ASTM) Practice E 1903-97
of the Biedermann Realty property (the "Project") located at 912 West Hodges Street in Raleigh, Wake
County, North Carolina.
The Project consists of three irregular -shaped parcels of land which total approximately 11.36 acres and is
identified as Parcel Identification Numbers (PIN Numbers) 1715211211, 1715114091 and 1715116336
according to the Wake County Tax Assessor. The Project is accessible via Hodges Street to the north. PIN
number 1715211211 is approximately 2.79 acres and currently improved with a deck hockey rink, lacrosse
field, and an asphalt parking area. PIN number 1715114091 is approximately 2.88 acres and exists primarily
as a wetland area and a pond. Drainage culverts run north along the eastern property line of this parcel, then
east along the southern property line of PIN I715116336, north through PIN 1715211211 between the deck
hockey rink and the asphalt parking area, and under West Hodges Street before discharging into Crabtree
Creek. PIN number 1715116336 is approximately 5.69 acres in size and is laterally bisected by Hodges
Street, which runs east -west through the parcel. The southern portion of the parcel is improved with one
single -story, approximately 33,750 square foot building originally constructed in 1979 and currently
operating as RecZone, an ice skating rink. The skating rink is kept frozen via a closed -loop cooling tower and
compression system. A cooling tower cools gaseous R-22 Freon to a liquid state that lowers the temperature
of a saltwater mixture (brine) below 32 degrees Fahrenheit. The brine is then pumped through approximately
five miles of piping located beneath the skating rink to keep the ice frozen. Moisture within the ambient air of
the skating rink area is regulated by a dehumidifier, while the remaining portions of the building utilize roof -
mounted split systems to regulate temperature. Domestic hot water is supplied by gas -fired and electric water
heaters. The Project is provided with municipal water and sewer services by the City of Raleigh. EA
personnel did not note any water supply or groundwater monitor wells at the Project; however, the facility
utilizes a "snow melt pit" located along the eastern elevation of the Project building. According to Mr.
Biedermann, the Project owner, the ice scraped offthe skating rink by the zamboni machine is dumped in the
pit and allowed to melt. From which point, the melt is discharged to the municipal sewer system. Natural gas
service by PSNC Energy and electrical service is supplied by Carolina Power & Light Company (CP&L).
Additional improvements include paved parking areas, drive aisles, sidewalks, and equipment pads, an
ancillary storage shed and landscaped areas.
Prior to construction of the current improvements in 1979, the Project reportedly existed as undeveloped land.
According to the USGS Topographic Quadrangle Map of Raleigh East, North Carolina (Figure 1), the
original topography of the Project is located approximately 185 to 200 feet above mean sea level (MSL). The
Project sloped gently to the north towards Crabtree Creek. However, according to Mr. Biedermann, the
Project owner, the western portions of parcel number 1715116336 and the northern portion of parcel number
1715114091 of the Project has been and/or is actively being filled with approximately 10 to 15 feet of
material from old construction sites of downtown Raleigh. Block and anchor retaining wall systems are
positioned at various locations in the western portions of the Project to maintain the structural integrity of the
fill material.

Phase 11 Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
2
Historically, the Project improvements have operated as a roller skating rink (1979—1989), nightclub (1989 —
2001) and ice skating rink from approximately 2001 until the present time.
A prior Transaction Screen conducted by EA (dated October 9, 2008 and prepared for BB&T) identified the
following on -site issues of potential environmental concern:
• Prior to construction of the current structural improvements in 1979, the Project appears to have
existed as undeveloped land and/or wetlands since at least 1958. During which time, areas of the
Project (specifically, the western portion of parcel number 1715116336 and the northern portion of
parcel number 1715114091) have been filled with unknown materials from unknown sources, and
graded to an elevation approximately 10 to 15 feet above the original topography. A prior Phase I
ESA conducted by Withers and Ravenel Engineering & Surveying dated June 1, 2000 identified two
areas of de minimis surface staining south of the Project building. At the time of this assessment no
staining was observed; however, according to Mr. Biedermann, the Project owner, the northern
portion of parcel number 1715114091(south of the Project building) is actively being filled with FloId
construction materials from downtown Raleigh.
The Client (BB&T) authorized EA to complete this Phase II ESA to evaluate the site in order to detern
potential impact to the Project from the on -site fill material which originated from an unknown source.
Phase I1 assessment activities were performed by EA and its subcontractors on June 6, 2011, which consisted
of the advancing and screening six (6) soil borings (S-1 through S-6) for the presence of potentially
contaminated fill material, the collection and sampling of one (1) on -site soil sample (S-2-23), the installation
of three (3) temporary groundwater piezometer wells (TMW-1 though TMW-3) and the collection and
sampling of three (3) groundwater samples (TMW-1, TMW-2 and TWM-3).
In summary, no concentrations of target analytes detected in soil sample 5-2-23 exceeded eitherlthe
Preliminary Health -Based PSRGs or the Protection of Groundwater PSRGs. However, groundwater samples
TMW-1, TMW-2 and TMW-3 revealed concentrations of several target analytes which exceed their
respective NCAC 2L Groundwater Quality Standards. Laboratory analysis revealed concentrations of
Arsenic (20.1 ug/L), Barium (5,040 ug/L), Cadmium (37.7 ug/L), Chromium (634 ug/L), Lead (320 ug/L)�and
Mercury (1.1 ug/L) in groundwater sample TMW-1, all of which exceeded their NCAC 2L Groundwater
Quality Standards, respectively. Groundwater sample TMW-2 revealed concentrations of Chromium (52.7
ug/L), Lead (16.8 ug/L), 1,2-Dichloroethane (4.7 ug/L) and MTBE (163 ug/L); all exceeding the 2L
Groundwater Quality Standards. Groundwater sample TMW-3 revealed concentrations of 1,2-Dichloroethane
(4.8 ug/L) and MTBE (171 ug/L); exceeding the 2L Groundwater Quality Standards. Several other target
analytes were detected in TMW-1, TMW-2 and TMW-3; however, at levels below their respective 2L
Groundwater Standards.
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(Page 5 of 75)
Phase II Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
2.0 INTRODUCTION
2.1 Purpose
The purpose of this Phase II Environmental Site Assessment (ESA) is to evaluate the environmental
conditions identified in the Phase I ESA (Practice E 1527) or Transaction Screen (Practice E 1528) process
for the purpose of providing sufficient information regarding the nature and extent of contamination to assist
in making informed business decisions about the property; and where applicable, providing the level of
knowledge necessary to satisfy the innocent purchaser defense under Comprehensive Environmental
Response Compensation and Liability Act (CERCLA).
2.2 Limitations and Exceptions of Assessment
There may be additional issues or conditions at the property as noted by the legal analysis of Appendix X1 of
Practices E 1527-05 and ASTM E 1528 which may be present on property in quantities and under conditions
that may lead to contamination of the property or of nearby properties but are not included in CERCLA's
definition of hazardous substances (42 USC L 9601(14)) or do not otherwise present potential CERCLA
liability. Parties may wish to assess these issues in connection with commercial property transactions;
however, they are beyond the scope of this report.
As stipulated by the ASTM E 1903-97 (Reapproved 2002) Process, this ESA does not formally address
certain non -scope issues including, but not limited to the following:
Asbestos -containing Materials
Mold Growth in Structures
Radon
Lead -based Paint
Lead in Drinking Water
Wetlands
Endangered Species
Indoor Air Quality
No implication is intended as to the relative importance of such considerations, nor is this list intended to be
all-inclusive.
2.3 Reliance
Branch Banking and Trust Company (BB&T) (the Client) (the "Relying Party") may rely on the contents of
the ESA subject to the limitations placed on the scope, nature and type of EA's services as stated in the ESA
and subject to those Terms and Conditions as stated in EA's contract with the Client. The Relying Party is
the only party to whom EA grants the right to rely upon the ESA. No other third party may rely on the ESA
unless the express written consent of EA is first obtained.

Phase If Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
3.0 BACKGROUND
3.1 Project Description
The Project consists of three irregular -shaped parcels of land which total approximately 11.36 acres and is
identified as Parcel Identification Numbers (PIN Numbers) 1715211211, 1715114091 and 1715116336
according to the Wake County Tax Assessor. The Project is accessible via Hodges Street to the north. PIN
number 1715211211 is approximately 2.79 acres and currently improved with a deck hockey rink, lacrosse
field, and an asphalt parking area. PIN number 1715114091 is approximately 2.88 acres and exists primarily
as a wetland area and a pond. Drainage culverts run north along the eastern property line of this parcel, then
I
east along the southern property line of PIN 1715116336, north through PIN 1715211211 between the deck
hockey rink and the asphalt parking area, and under West Hodges Street before discharging into Crabee
Creek. PIN number 1715116336 is approximately 5.69 acres in size and is laterally bisected by Hodges
Street, which runs east -west through the parcel. The southern portion of the parcel is improved with one
single -story, approximately 33,750 square foot building originally constructed in 1979 and currently
operating as RecZone, an ice skating rink. The skating rink is kept frozen via a closed -loop cooling tower and
compression system. A cooling tower cools gaseous R-22 Freon to a liquid state that lowers the temperature
of a saltwater mixture (brine) below 32 degrees Fahrenheit. The brine is then pumped through approximately
five miles of piping located beneath the skating rink to keep the ice frozen. Moisture within the ambient aii of
the skating rink area is regulated by a dehumidifier, while the remaining portions of the building utilize rdof-
mounted split systems to regulate temperature. Domestic hot water is supplied by gas -fired and electric water
heaters. The Project is provided with municipal water and sewer services by the City of Raleigh. 'I!A
personnel did not note any water supply or groundwater monitor wells at the Project; however, the facie ity
utilizes a "snow melt pit" located along the eastern elevation of the Project building. According to Mr.
Biedermann, the Project owner, the ice scraped off the skating rink by the zamboni machine is dumped inthe
pit and allowed to melt. From which point, the melt is discharged to the municipal sewer system. Natural,gas
service by PSNC Energy and electrical service is supplied by Carolina Power & Light Company (CP&L).
Additional improvements include paved parking areas, drive aisles, sidewalks, and equipment pads an
ancillary storage shed and landscaped areas.
Prior to construction of the current improvements in 1979, the Project reportedly existed as undeveloped l
According to the USGS Topographic Quadrangle Map of Raleigh East, North Carolina (Figure 1),
original topography of the Project is located approximately 185 to 200 feet above mean sea level (MSL).
Project sloped gently to the north towards Crabtree Creek. However, according to Mr. Biedermann
Project owner, the western portions of parcel number 1715116336 and the northern portion of parcel nut
1715114091 of the Project has been and/or is actively being filled with approximately 10 to 15 fe,
material from old construction sites of downtown Raleigh. Block and anchor retaining wall system;
positioned at various locations in the western portions of the Project to maintain the structural integrity c
fill material.
the
the
: of
are
(9L 90 9 aBa3)

(Page 7 of 75)
Phase I1 Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
Historically, the Project improvements have operated as a roller skating rink (1979—1989), nightclub (1989 —
2001) and ice skating rink from approximately 2001 until the present time. A Site Location Map (Figure 1)
and a Site Plan (Figure 2) are attached.
3.2 Physical Setting
The topographic, geologic and hydrogeologic settings of a site are considered of interest since they may
provide information related to the direction and physical mechanisms of contaminant migration, if present,
from on -site and off -site sources. EA personnel have reviewed information from the following sources with
regard to the topography, geology and hydrogeology of the site and surrounding area:
• United States Geologic Survey (USGS) Topographic Quadrangle Map of Raleigh East, North
Carolina, dated 1968 (photorevised 1987);
• Geologic Map of North Carolina, North Carolina Geologic Survey, 1985;
• USDA Web Soil Survey, http://webaoilsurvey.nres.tisda.gov/app/, dated 2007;
3.2.1 Geologic Settin
The Project is located in the Raleigh Belt of the Piedmont Physiographic Province of North Carolina. The
geology in the vicinity of the Project consists of Pennsylvanian to Permian aged mega-crystic to equigranular
granitic rock.
The soil profile at the Project is comprised of three main soils: Chewacla sandy loam, zero to two percent
slopes, frequently flooded (CmA); Faceville sandy loam, two to six percent slopes, moderately eroded
(FaB2): and Wake-Wateree complex, ten to twenty-five percent slopes, very rocky (WkE). Chewacla soils are
The southwestern, wooded portion of the Project contains Fairview Sandy Clay Loam (FeD2) with I5-25%
slope. Fairview Sandy Clay Loam is well drained with moderate available water capacity and moderately
high to high permeability. The northwestern wooded portion of the Project contains Udorthents (Ud) soil
with 0-IS% slope. Udothents is well drained with moderate available water capacity and very low to high
permeability. The developed portion of the Project is characterized by Urban Land (Ur) made up of
impervious layers over human transported material.
3.2.2 Topographic Settin
According to the USGS Topographic Quadrangle Map of Raleigh East, North Carolina (Figure 1), the
Project elevation is approximately 200 feet above mean sea level (MSL). The Project slopes to the north
towards Crabtree Creek. In the absence of any other obvious significant structural or geomorphic drainage
features, surface drainage is suspected to be influenced primarily by the surface topography.

Phase II Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
3.2.3 Hvdroaeoloaic Settin
Groundwater generally occurs as a result of infiltration of both meteoric and surface water through
relatively permeable overburden. Fractures, joints, bedding planes and other discontinuities in the underly
rock can affect the groundwater conditions. Site -specific groundwater flow may also be influenced by
proximity of nearby drainage features, sinkholes, creeks, swamps, and pumped groundwater we
Groundwater levels and flow directions are typically site specific. In this setting, the surface of
groundwater table is expected to be a subdued replica of the ground surface. Groundwater may occur a
near the soil/rock interface or it may be contained within the bedrock. Based on EA's review of
topographic map, the Project's groundwater flow direction is interpreted to be generally to the north towa
Crabtree Creek. The topography and hydrology in the site vicinity are variable and several local compone
of groundwater flow may exist.
3.3 Summary of Previous Assessments
A prior Phase 1 Environmental Site Assessment conducted by Withers and Ravenel Engineering & Surve3
Inc. and dated June 1, 2000 identified the following on -site issues of potential environmental concern:
6
or
• According to this report, Project was originally utilized as a roller skating rink for a short perio of
time beginning in 1979 before being converted into a nightclub. Prior to the development of the
original improvements in 1979, the Project appears to have existed only as undeveloped land since at
least 1958. The prior Phase I ESA report did not identify any potential environmental concerns likely
to have impacted the Project; however several items of note were identified.
Surficial staining was observed in soils in the vicinity of one empty 55-gallon drum located E
the nightclub building. The drum appeared to have previously contained motor oil; however
time of the site visit the drum was found to be upside down and the cap to the fill spout was mi
The drum was resting on asphalt with approximately one inch of soil on top of the w
According to the prior Phase I ESA report, no staining or odors were noted in soils 1(
approximately one foot from the drum.
Another surface oil stain, with an approximate three foot radius, was noted near the wooded ar 'a at
the southern portion of PIN number 1715211211. The staining was reportedly likely caused as a
result of equipment maintenance being conducted on machinery utilized in the construction Of a
residential subdivision located to the south of this parcel. During the site visit a shovel was used to
inspect the stained area. According to the prior Phase I ESA report, odors and staining were fourid to
dissipate at a depth of approximately one foot below the surface; therefore, the affects of the observed
staining were considered minimal.
In addition to the stufrcial staining noted above, a few minor areas of household debris I and
miscellaneous solid waste were noted at the Project. Household debris and solid waste inc
washer, trashcan and a construction barrel were noted near the wetland pond area. Also,
ra
of
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(Page 9 of 75)
Phase 11 Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
concrete, gravel, asphalt, tires, culverts, hoses, bricks, carpet and siding were observed on the
southern portion of PIN number 1715211211, near the area of surfical staining noted above. These
materials were reported by Mr. Glen Russell, the Controller of the Project, to have been placed on the
subject property by the construction company developing the subdivision located to the south of PIN
number 1715211211.
The prior Phase I ESA report did no: identify any other on -site items of note. In addition, no off -site
potential environmental concerns likely to have impacted the Project were identified. The prior
Phase I ESA report recommended that efforts be enacted to limit the placement of uncontrolled waste
on the Project and that all solid wastes be removed from the Project for proper disposal.
A prior Transaction Screen conducted by EA (dated October 9, 2008 and prepared for BB&T) identified the
following on -site issues of potential environmental concern:
Prior to construction of the current structural improvements in 1979, the Project appears to have
existed as undeveloped land and/or wetlands since at least 1958. During which time, areas of the
Project (specifically, the western portion of parcel number 1715116336 and the northern portion of
parcel number 1715114091) have been filled with unknown materials from unknown sources, and
graded to an elevation approximately 10 to 15 feet above the original topography. A prior Phase I
ESA conducted by Withers and Ravenel Engineering & Surveying dated June 1, 2000 identified two
areas of de minimis surface staining south ofthe Project building. At the time of this assessment, no
staining was observed: however, according to Mr. Biedermann, the Project owner, the northern
portion of parcel number 1715114091 (south of the Project building) is actively being filled with old
construction materials from downtown Raleigh.
As part of the prior Transaction Screen of the Project conducted by EA (dated October 9, 2008 and prepared
for BB&T) EA reviewed the following regulatory files for the Tops Exxon Mart #4 off -site listed property
located at 2408 Wake Forest Drive in Raleigh, North Carolina (Facility ID Number 0-006353, Incident
Number 26744) that are identified and summarized below.
Underground Storage Tank Closure Report — Tops Exxon Mart #4 — SEI Engineering & Geological Services,
P.C. — January 2005.
Review of an Underground Storage Tank (UST) Assessment Report dated January 2005 and prepared
by SEI Engineering & Geological Service, P.C. and obtained from the NCDENR office in Raleigh,
North Carolina indicates that 5 petroleum USTs ranging from 10,000- to 12,000-gallons were
permanently closed via removal from the ground in November and December of 2004. At the time of
the tank closure, approximately 25 gallons of liquid petroleum, sludge and waste waters from the 5
USTs was removed and transported by Garco Environmental, Industrial & Recycling Services Inc. to
a recycling facility in Asheboro, North Carolina. Approximately 2,746.73 tons of suspected
contaminated soil was removed from around the former tank basins, pump islands, and product lines
at the site. Approximately 241.8 of clean stone and 2,155 tons of clean soil were used to backfill the

Phase 11 Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
excavation, In addition, soil samples from beneath the USTs, product lines and dispenser islands
were taken and analyzed for total petroleum hydrocarbons (TPH) as gasoline range organics (GRO)
or diesel range organics (DRO) using EPA Method 8015; volatile organic compounds (VOC) using
EPA Method 826013; semi -volatile organic compounds using EPA Method 8270C; and/or MADO
Methods for volatile petroleum hydrocarbons (VPH) and extractable petroleum hydrocarbons (EP .
Analytical results detected TPH as GRO concentration exceeding NCDENR 2L groundwater qua ity
standards in 2 of 25 soil samples taken during tank closure events, and numerous petroleum
constituents above Soil -to Groundwater maximum soil contaminant concentrations (MSCCs) in 9 of
14 soil samples taken during over -excavation events.
Limited Site Assessment Report — Tops Exxon Mart #4 — SEl Engineering & Geological Services, P.C. —
January 24, 2005.
• Review of a Limited Site Assessment Report dated January 2005 prepared by SEI Engineering &
Geological Service, P.C. and obtained from the NCDENR office in Raleigh, North Carolina indicates
that 5 groundwater monitoring wells (MW-1 through MW-4, and DW-1) were installed at the
property in December of 2004 and January of 2005. Groundwater was determined to flow north
towards Crabtree Creek, parallel to and away from the Project. Additionally, groundwater saris Iles
were collected from each well and analyzed using EPA Methods 601, 602 (with IPE and MTBE), 625
(with BNA and TICS), 504.1 for EDB, 3030C for Lead, and/or MADEP Methods for VPH and EPH.
Target constituents were detected at concentrations above the 15A NCAC 2L groundwater standards
in three (MW-1, MW-2 and DW-I) of the five monitoring wells; however, all concentrations were
below Gross Contamination Levels (GCLs). In addition, a 1,000-foot radius search did not re eai
any water supply wells in the surrounding area, and no planned or approved wellhead protec ion
areas were located with 1,500 feet of the source area. Therefore, it was recommended the sit be
considered "low risk" and issued a letter of "No Further Action".
The Client (BB&T) authorized EA to complete this Phase II ESA to evaluate the site in order to
potential impact to the Project from the on -site fill material which originated from an unknown
4.0 PHASE II ESA ACTIVITIES
4.1 Scope of Services
The ESA was conducted in substantial compliance with ASTM Designation: E 1903-97 - Standard Guic
Environmental Site Assessments: Phase II Environmental Site Assessment Process. The intention c
ASTM E 1903-97 practice is "to provide assistance to users in satisfying the appropriate inquiry eleme
CERCLA's innocent purchaser defense as defined in 42 USC D 9601(35)(B), where a previous assess
satisfying that element identified recognized environmental conditions" Specifically, this Phase 11
included the following Quality Assurance/Quality Control (QA/QC) scope of services:
the
t of
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(Page 11 of 75)
Phase II Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
(A) Site and Vicinity Reconnaissance - EA conducted a site and vicinity reconnaissance using readily
available information; the objective of which was to determine the existence and establish the
characteristics of the previously identified existing and/or pre-existing "recognized environmental
condition" or "potential environmental condition" in connection with the subject property, as defined
in ASTM E-1527-05 and ASTM E-1528. Additionally, the evaluation included site and vicinity
reconnaissance with respect to structural improvements, utility locations, topography, easements and
property boundaries in order to determine optimal sampling locations while preserving the integrity
of the aforementioned property attributes, as well as the health and safety of those parties involved.
(B) Field Methods — The work description included personnel health and safety precautions to be
followed in accordance with applicable federal, state or local laws, and requirements imposed by the
owner or occupant of the property or by the user. EA's field methods and sampling protocol was
designed to provide collection of the potentially contaminated environmental media at locations in which
they are most likely to occur. EA has taken into consideration the properties, behaviors, fate and transport
characteristics, and the likely distribution of the potential contaminants in the given setting. Samples
were selected for analysis using qualitative and/or quantitative field analytical techniques, and were
manually collected using clean sample retrieval, collection and storage devices. Each sample container
was labeled with the project name and number, the sampler's name, and the time and date of sample
collection. The filled sample containers were appropriately packaged and stored while acknowledging
preservation, temperature and hold time requirements prior to submittal for laboratory analysis. A
completed chain of custody form was maintained with the samples.
(C) LaboratoryAnalysis — Prior to engaging services, EA verified the certification or licensing ofthe
analytical laboratory chosen to allow precision and accuracy of the data it generates. The chosen
analytical method was designed to detect the contaminants suspected to be present in the samples
collected, as well as being appropriate for the sample medium and laboratory detection limits for the
recognized environmental conditions. When appropriate, the preparation and analysis of trip blanks,
equipment blanks, duplicate samples and background samples will be used to verify the data quality.
The findings reported in the analytical data will influence the conclusions of the investigation
regarding the environmental condition.
4.2 Deviations
This Phase I1 ESA substantially complies with the scope of services and ASTM E 1903-97 (Reapproved
2002), as amended, except for exceptions and/or limiting conditions as discussed in Section 2.2.
4.3 Field Explorations & Observations
4.3.1 Subsurface Utility Locating
EA personnel contacted the North Carolina One Call Center and requested that the local utility services
conduct an Electromagnetic (EM) Survey in the area of concern at the Project to determine the orientation and

Phase 11 Environmental Site Assessment to
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
location of underground utility lines for optimal sampling locations. At the time of the assessment, ;all
underground utility lines appeared to be marked up to the Project boundaries. However, public utilities are
not authorized to locate underground lines on private property.
On June 4, 2011, EA subcontractor, Taylor Wiseman & Taylor (TWT), conducted an on -site Electromagnetic
(EM) and Ground Penetrating Radar (GPR) Survey at the Project to determine the orientation and location of
the on -site subsurface utilities in order to determine optimal sampling locations. All items located were
marked directly on the surface using paint. EA and its subcontractor identified several subsurface utilities
near the proposed sampling locations.
4.3.2 Soil Assessment
On June 6, 2011, EA and its subcontractor utilized a Geoprobe® sampling device to advance soil borings at
six (6) locations (S-1 through S-6) at the Project, to evaluate on -site fill material for evidence of poten�ial
contamination. Each of the soil borings were screened for the presence of Volatile Organic Compounds
(VOCs) at two -foot intervals using a Photo Ionization Detector (PID) and visual and olfactory indicators.
One (1) soil sample (5-2-23) was collected from the depth of probe refusal (23 feet below grade) from soil
boring S-2. No VOC concentrations were detected in any of the soil borings (S-1 through S-6), therefore no
additional soil samples were collected. The soil boring locations are depicted on the attached Figure 2,
Soil boring S-1 was advanced adjacent to a wash pit located to the east of the Project building to adept of
twenty (20) feet below grade (BG). Soils consisted consisting of orange and brown silty clay and sandfill
material at depths of 0-4 feet BG underlain by dark brown sand and silt at depths of 4-8 feet BG, dark brown
and grey sand and silt at depths of 8-12 feet BG, grey and orange micaceous sand and silt at depths of 12-16
feet BG and dark brown micaceous silt at depths of 16-20 feet BG. No VOC concentrations were detected
throughout soil boring S-1; therefore, a soil sample was not collected from this location.
Soil boring S-2 was advanced to the southeast of the Project building to the point of probe refusal at a d(
of twenty-three (23) feet BG. Soils consisted of tan sand and silt fill material at depths of 0-4 feet
underlain by brown and orange micaceous sand and silt fill material at depths of 4-12 feet BG, red and i
micaceous sand and silt fill material at depths of 12-16 feet BG, dark grey and brown micaceous silt at del
of 16-20 feet BG and dark grey and brown micaceous silt and saprolite at depths of 20-23 feet BG. No V
concentrations were detected throughout soil boring S-2. EA attempted to advance soil boring S-2 to
groundwater table; however probe refusal was encountered at a depth of twenty-three (23) feet BG. One
sample (5-2-23) was collected from soil boring S-2 at a depth of twenty-three (23) feet BG.
Soil boring S-3 was advanced in the vicinity of on -site garbage dumpsters located to the south of the Pro
building to a depth of sixteen (16) feet BG. Soils consisted of red micaceous silty clay at depths of 0-8
BG underlain by red and brown micaceous silty clay at depths of 8-12 feet BG and red and grey sand and
at depths of 12-16 feet BG. No VOC concentrations were detected throughout soil boring S-3; therefore, a
sample was not collected from this location.
silt
(SL 90 ZT abed)

(Page 13 of 75)
Phase lI Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
11
Soil boring S-4 was advanced to the southwest of the Project building to a depth of sixteen (16) feet BG.
Soils consisted of orange and tan micaceous sand and silt fill material at depths of 0-4 feet BG underlain by
orange and brown micaceous sand and silt fill material at depths of4-14 feet BG and dark brown micaceous
silt at depths of 14-16 feet BG. No VOC concentrations were detected throughout soil boring S-4; therefore, a
soil sample was not collected from this location.
Soil boring S-5 was advanced on the southern portion of the project to the point of probe refusal at a depth of
twenty-eight (28) feet BG. Soils consisted oftan and brown micaceous sand and silt fill material at depths of
0-4 feet BG underlain by brown micaceous sand and silt fill material at depths of 4-8 feet BG, brown and grey
sand and silt fill material intermingled with black deposits (suspected asphalt) at depths of8-17 feet BG, dark
brown micaceous clay at depths of 17-20 feet BG, brown and grey sand and silt fill material intermingled with
black deposits (suspected asphalt) at depths of 20-23.5 feet BG, grey clay at depths of 23.5-24 feet BG and
brown and grey sand and silt fill material intermingled with black deposits (suspected asphalt) at depths of 24-
28 feet BG, with a layer of wet grey sand at a depth of approximately 26 feet BG. Probe refusal was
encountered in soil boring S-5 at a depth of 29 feet BG. No VOC concentrations were detected throughout
soil boring S-5; therefore, a soil sample was not collected from this location.
Soil boring S-6 was advanced on the southern portion ofthe Project, and to the northeast of soil boring S-5, to
a depth of sixteen (16) feet BG. Soils consisted of tan and red micaceous fill material at depths of 0-4 feet BG
underlain by brown fill material intermingled with asphalt and gravel at depths of 4-12 feet BG and saturated
red and brown sand and silt fill material at depths of 12-16 feet BG. No VOC concentrations were detected
throughout soil boring S-6; therefore, a soil sample was not collected from this location.
Soil sample S-2-23 was placed into appropriate sample containers and labeled with the project name, time and
date of collection, and analysis to be performed. The filled sample containers were placed in a cooler
containing ice and transported to PACE Analytical in Huntersville, North Carolina(allorth Carolina -certified
laboratory). A chain -of -custody form was maintained with the samples. All soil samples were submitted and
analyzed for Volatile Organic Compounds (VOCs) by EPA Method 8260, Polynuclear Aromatic
Hydrocarbons (PAH) by EPA Method 8270 and RCRA 8 Metals by EPA Method 6010. A copy of the
laboratory analytical report is attached as Appendix 1. The laboratory results are discussed in Section 5.0 of
this report.
4.3.3 Surface Water and/or Groundwater A§sessment
According Flood Insurance Rate Map #3720171500J dated May 2, 2006, the Project is located in Flood Zone
AE, an area inundated by 100-year flooding, for which base flood elevations (BFEs) have been determined.
In addition, according to the map in the attached EDR report and the U.S. Fish and Wildlife Service Wetlands
Mapper (http://www.fws. ov/nwi�, the majority of the total deeded 2.88 acres of Project parcel number
1715114091 is designated as federal wetland area which constitutes approximately 25%of the total property.
However, in order to confirm the boundaries and extent of wetlands on any property, a formal wetlands
survey would be required.

Phase I1 Environmental Site Assessment 12
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
No groundwater monitoring wells or water supply wells were observed on the Project at the time of
investigation.
On June 6, 2010, EA and its subcontractor installed one -inch diameter temporary groundwater piezometer
wells in three (3) locations at the Project depicted on the attached Figure 2. Soil boring S-5 was converted to
temporary groundwater piezometer well (TMW-1). In addition, temporary groundwater piezometer well
TMW-2 was installed on the southern portion of the Project to a depth of twenty-eight (28) feet BG and
temporary groundwater piezometer well TMW-3 was installed on the northern portion of the Project to a
depth of twenty-five (25) feet BG. Depths to groundwater were measured to be 18.54 feet BG in TM -1,
22.10 feet BG in TMW-2 and 11.3 feet BG in TMW-3. Each of the temporary groundwater piezometer wells
were developed/purged of at least three (3) well volumes of groundwater prior to the collection of
groundwater samples from each well. Low -flow sampling techniques were utilized to collect the groundwater
samples in an attempt to limit turbidity, however, groundwater samples collected from TMW-1 and TMW-2
appeared turbid at the time of collection.
The groundwater samples were placed into appropriate sample containers and labeled with the project naive,
time and date of collection, and analysis to be performed. The filled sample containers were placed in a
cooler containing ice and transported to PACE Analytical in Huntersville, North Carolina (a North Carolina -
certified laboratory). A chain -of -custody form was maintained with the samples. The groundwater saml ies
were submitted and analyzed for Volatile Organic Compounds (VOCs) by EPA Method 8260, Polynuclear
Aromatic Hydrocarbons (PAH) by EPA Method 9270 and RCRA 8 Metals by EPA Method 6010. A copy of
the laboratory analytical report is attached as Appendix 1. The laboratory results are discussed in Section 5.0
of this report.
5.0 LABORATORY ANALYTICAL RESULTS
5.1 Soil Assessment
EA collected a total of one (1) soil sample for laboratory analysis (S-2-23). A copy of the laboratory
analytical report is attached as Appendix 1. A summary of the soil analytical results is presented in Table 1.
i
Laboratory analysis of soil sample S-2-23 revealed an Acetone concentration of 0.0338J mg/kg, which does
not exceed the Inactive Hazardous Sites Branch (IHSB) Protection of Groundwater Preliminary �5011
Remediation Goal (PSRG) of 24 mg/kg or the Health -Based PSRG of 12,000 mg/kg for Acetone. Soil ple
S-2-23 also revealed a Methylene Chloride concentration of 0.0096 J mg/kg, which does not excee the
Protection of Groundwater PSRG of 0.023 mg/kg or the Health -Based PSRG of I 1 mg/kg for Methy ene
Chloride. The "J" value indicates an estimated concentration above adjusted laboratory detection limits and
below adjusted laboratory reporting limits. Low concentrations of Arsenic, Barium, Chromium, Leadand
Mercury were also detected in soil sample S-2-23; all of which were below the Protection of Groundwater
PSRGs and the Health -Based PSRGs. No other target analytes were detected in soil sample S-1-2.
A copy of the laboratory analytical report is attached as Appendix 1 and the soil sampling
are
(SL 90 VT abed)

(Page 15 of 75)
Phase It Environmental Site Assessment
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
summarized in Table 1 and on Figure 2.
980103% 01-
CI3AaV
dlNV.L*
13

Phase 11 Environmental Site Assessment 14
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
5.2 Surface Water and/or Groundwater Assessment
EA collected a total of three (3) groundwater samples for laboratory analysis (TMW-1, TMW-2 and TMW -3).
A copy of the laboratory analytical report is attached as Appendix 1. A summary of the groundwater
analytical results is presented in Table 2.
Laboratory analysis oftemporary groundwater piezometer well TMW-1 revealed an Arsenic concentration of
20.1 micrograms per Liter (ug/L), exceeding the 2L Groundwater Standard of 10 ug/L for Arsenic. Barium
was detected at a concentration of 5,040 ug/L, exceeding the 2L Groundwater Standard of 700 ug/L for
Barium. Cadmium was detected at a concentration of 37.7 ug/L, exceeding the 2L Groundwater Standard of 2
ug/L for Cadmium. Chromium was detected in TMW-1 at 634 ug/L, exceeding the 2L Groundwater Standard
of 10 ug/L for Chromium. Lead was also detected at a concentration of 320 ug/L, exceeding its respective 2L
Groundwater Standard of 15 ug/L. Mercury was detected at a concentration of 1.1 ugiL, slightly exceeding
the 2L Groundwater Standard of 1 ug/L for Mercury. Several other target analytes were detected in TMW-1
at levels below their respective 2L Groundwattr Standards.
I
Laboratory analysis of temporary groundwater pizometer well :TMW-2 revealed a 1,2-Dichloroett
concentration of 4.7 ug/L, exceeding the 2L Groundwater itaard of 0.4 ug/L for 1,2-Dichloroeth
Groundwater sample TMW-2 also revealed a Methyl tert-butyl ether (MTBE) concentration of 163 u
exceeding the 2L Groundwater Standard of 20 ug/L for MTBE. Chromium was detected in TMW-2 at
ug/L, exceeding the 2L Groundwater Standard of 10 ug/L for Chromium. A Lead concentration of 16.81
was also detected in TMW-2, exceeding the 2L Groundwater Standard of 15 ug/L for Lead. Arsenic, Bar
and several other volatile organic compounds were also detected in TMW-2, all of which were below 1
respective NCAC 2L Groundwater Standards.
Laboratory analysis of temporary groundwater piezometer well TMW-3 revealed a 1,2-Dichloroethane
concentration of 4.8 ug/L, exceeding the 2L Groundwater Standard of 0.4 ug/L for 1,2-Dichloroethane.
Groundwater sample TMW-3 also revealed a MTBE concentration of 171 ug/L, exceeding the 2L
Groundwater Standard of 20 ug/L for MTBE. Barium, Chromium and several other volatile org is
compounds were also detected in TMW-3, all of which were below their respective NCAC 2L Groundwater
Standards.
A copy of the laboratory analytical report is attached as Appendix 1 and the groundwater sampling
summarized in Table 2 and on Figure 2.
are
(SL 3o 91 abEd)

(Page 17 of 75)
Phase 11 Environmental Site Assessment 15
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
6.9 DISCUSSION OF FINDINGS AND CONCLUSIONS
6.1 Findings
In summary, no concentrations of target analytes detected in soil sample S-2-23 exceeded either the
Preliminary Health -Based PSRGs or the Protection of Groundwater PSRGs. However, groundwater samples
TMW-1, TMW-2 and TMW-3 revealed concentrations of several target analytes which exceed their
respective NCAC 2L Groundwater Quality Standards. Laboratory analysis revealed concentrations of
Arsenic (20.1 ug/L), Barium (5,040 ug/L), Cadmium (37.7 ug/L), Chromium (634 ug/L), Lead (320 ug/L) and
Mercury (1.1 ugtL) in groundwater sample TMW-1, all of which exceeded their NCAC 2L Groundwater
Quality Standards, respectively. Groundwater sample TMW-2 revealed concentrations of Chromium (52.7
ug/L), Lead (16.8 ug/L), 1,2-Dichloroethane (4.7 ug/L) and MTBE (163 ug/L); all exceeding the 21,
Groundwater Quality Standards. Groundwater sample TMW-3 revealed concentrations of 1,2-Dichloroethane
(4.8 ug/L) and MTBE (171 ug/L); exceeding the 2L Groundwater Quality Standards. Several other target
analytes were detected in TMW-1, TMW-2 and TMW-3; however, at levels below their respective 2L
Groundwater Standards.
A copy of the laboratory analytical report is attached as Appendix 1. A summary ofthe soil sampling results
is attached as Table 1 and a summary of the groundwater analytical results is attached as Table 2.
6.2 Conclusions
EA has performed a Phase 1I ESA in conformance with the scope and limitations of ASTM Practice E 1903-
97 (Reapproved 2002) of Biedermann Realty property (the "Project") located 912 West Hodges Street in
Raleigh, Wake County, North Carolina. Any exceptions to, or deletions from, this practice are described in
Section 2.2 of this report. This assessment has revealed no evidence of contamination from the suspected on -
site potential environmental conditions in connection with the Project, with the exception of the following:
• The Project contains significant amounts of undocumented and uncontrolled landfill material
reportedly originating from old construction sites of downtown Raleigh. Based on recent soil
borings, the landfill material is generally described as clayey, sandy and silty soils with gravel,
concrete, rock, asphalt, and organic (trees/stumps) debris. The description of the material appears to
be consistent with typical "construction/demolition" debris.
• Laboratory analysis revealed concentrations of several target analytes exceeding NCDENRNCAC
2L Groundwater Quality Standards in groundwater samples TMW-1, TMW-2 and TMW-3.
• No concentrations of target analytes were detected in soil sample 5-2-23 that exceeded either the
Preliminary Health -Based PSRGs or the Protection of Groundwater PSRGs as established by the
IHSB.
•' The specific source and extent of the metals, petroleum- and solvent -related groundwater

Phase lI Environmental Site Assessment J 6
Biedermann Realty
912 West Hodges Street
Raleigh, Wake County, North Carolina
EA Project No. 08-7690.2— BB&T ESA083038
July 8, 2011
contamination identified at the Project is unknown. The elevated metals concentrations in
groundwater samples TMW-1 and TMW-2 may be due to the turbidity of the samples at time; of
collection and not indicative of actual groundwater conditions.
7.0 SIGNATURES OF ENVIRONMENTAL PROFESSIONALS
We declare that, to the best of our professional knowledge and belief, we meet the definition i of
Environmental Professional as defined in §312.10 of 40 CFR 312" and we have the specific qualifications
based on education, training, and experience to assess a property of the nature, history, and setting of the
subject property. We have developed and performed the all appropriate inquiries in conformance with ;the
standards and practices set forth in 40 CFR Part 312.
i
EA appreciates the opportunity to be of service on this project. Please call the undersigned at [phone]
or [phone] if you desire additional information.
Sincerely,
EnviroAssessments
CA
CEIYs4
Cliff R. Lundgren, P.G. p i359 SEAL
'
Senior Project Manager C� (r
Attachments NS.,
(SL 90 81 abEg)

(Page 19 of 75)
V;) '00. LE
8 nideL AlFA31L
a3aad
�llwvls
FIGURES

71

(Page 21 of 75)
Figure 2 — Site Plan
4307 MwMe Road. S' ,1 t K
Chartatte. tdurth Carg—,� 23270
T 706.866,8$92 F 70a.n.:6.:tz71
% w
70 envlroassessments
Scale: 1" =100' N t
Site Name: Biedermarm Realty
912 West Hodges Street
Raleigh, North Carolina
Project Number: 08-7690.2
BBBT Project Number: ESA083038

TABLES
(SL 90 ZZ abed)

(Page 23 of 75)
TABLE 1
SOIL ANALYTICAL RESULTS
BIEDERMANN REALTY
912 WEST HODGES STREET
RALEIGH, WAKE COUNTY, NORTH CAROLINA
ENVIROASSESSMENTS, PLLC PROJECT NO.08-7690.2
ems:;:.'
Sample 1D
Analytical
Method
8260B
.' • y . - ,....,., , .:...¢ .<'Y v
S-2-23
Preliminary
Health -Based
PSRG
12000
Protection of
Groundwater PSRG
24
Sample Depth (ft b s
' g)
23
Collection Date
Acetone
6/6/2011
0.0338J
Methylene Chloride
8260B
0.00961
11
0.023
Benzo
jalpyrene
8270C
ND
0.015
0.059
Benzo[b]fluoranthene
8270C
ND
0.15
0.6
Benzo[ ,h,i] eryiene
8270C
ND
NIA
360
Benzo[k]fluoranthene
8270C
ND
1.5
5.9
Fluoranthene
8270C
ND
460
330
Ftuorene
8270C
ND
460
56
Pyrene
8270C
ND
340
220
Arsenic
6010
0.58
4.4
5.8
Barium
60 00
80.9
3100
580
Cadmium
6010
ND
14
3
Chromium
6010
14.3
23000
360000
Lead
6010
1.7
400
270
jMercury
6010
0.0034J
4.7
1
Selenium
6010
FND
78
2.1
Silver
6010
ND
78 1
3.4
Notes:
All concentrations are reported in milligrams per kilogram (mg/kg).
Unless otherwise noted, PSRG values were obtained from the Guidelines for Assessment and Cleanup by the State of North
Carolina, Department of Environment and Natural Resources, Division of Waste Management, Superfund
Section, Inactive Hazardous Sites Branch; January 20W.
PSRG - Preliminary Soil Remediation Goals
BOLD results exceed their respective Preliminary
ft, bgs - feet below ground surface
ND - Not Detected

TABLE 2
GROUNDWATER ANALYTICAL RESULTS
BIEDEMMANN REALTY
912 WEST HODGES STREET
RALEIGH, WAKE COUNTY, NORTH CAROLINA
ENVIROASSESSMENTS, PLLC PROJECT NO.08-7690.2
Analytical
Method
TMW-1
TMW-2
TMW-3
North Carolina2L Groundwater
Quality Standards
Gross Co�nnination Levels
for Groundwater
u
p1bomene
616/2011
6/6/2011
6/6/20i1
8260B
ND
ND
ND
1
5000
82608
ND
ND
ND
6W
260000
8260B
ND
ND
ND600
94500
-)
8260B
ND
ND
ND
500
85500
Acetone
8260E
5.1.1
5.21
3.1J
6000
6000000
is-1,2-Dichloroethene
8260B
0.453
ND
ND
70
70000
hloromethane
9260B
ND
0.20J
ND
3
3000
1,2-Dichtoroethane
8260E
ND
4.7
4.8
0.4
400
DiisoproZil ether
8260E
ND
1.4
1.5
70
70000
ethyl tert-butyl ether (MTBE)
8260E
ND
163
171
20
20000
retie
8270C
ND
ND
ND
200
200
enz a Anthracene
8270C
ND
ND
ND
0.05
4.7
gene
8270C
ND
ND
ND
5
5
o(b Fluorantheae
8270C
ND
ND
ND
0.05
0.75
enzo(lr) Fluoranthene
8270C
ND
ND
ND
0.5
0.5
enzo(a) Pyrene
9270C
ND
ND
ND
0.005
0.81
ndeno 1,2,3-CD rene
9270C
ND
ND
ND
0.05
0.05
enzo (G Hj)Perylene
9270C
I.IJ
ND
NO
200
200
enic
60103
20.1
5.1
ND
10
NE
arium
6010B
5040
301
110
700
700000
Cadmium
601013
37.7
ND
ND
2
NE
bromium
6010B
634
52.7
9.7
10
10000
cad
6010B
320
16.8
ND
15
15000
crcury
6010E
1.1
ND
ND
I
NE
lenium
6010E
14.9
ND
ND
20
WE
ilver
6010B
5
ND
ND
20
20000
Notes:
All concentrations are reported in micrograms per liter (ug/L).
ND - Not Detected
- .._. NT - NotTested-- -- ------...— ------ ._ .
NE - Not Established

(Page 25 of 75)
APPENDICES

APPENDIX I
LABORATORY ANALYTICAL RESULTS
AND CHAIN OF CUSTODY FORMS
(SL 90 9Z abed)

(Page 27 of 75)
aeeftlxii a e
wwwpactlabs com
.tune 16, 2011
i Mr. Gary Sawyer
EnviroAssessments
9307 Monroe Rd. Ste. K
Charlotte, NC 28270
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Pace Analytical Services, Inc.
2225 Riverside Or,
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
Dear Mr. Sawyer:
Enclosed are the analytical results for sample(s) received by the laboratory on June 07, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brandon Helton
brandon,[e-mail]
Project Manager
Enclosures
cc: Mr, Cliff Lundgren, EnviroAssessments
Mr, Mike McDermott, EnviroAssessments
Ms. Amanda Petoskey, EnviroAssessments
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 47

aceAnalydcal'
irmpecalleba.com
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 26804
[phone] [phone]
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Charlotte Certification IDs
9800 Kfncey Ave. Ste 100, Huntersviile, NC 28078
Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 6342
North Carolina Wastewater Certification #:12
Pennsylvania Certification #: 68-00784
South Carolina Certification V. 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification* PH-0 IN
Florida)NELAP Certification #: E87648
Massachusetts Certification #: M-NCO30
New Jersey Certification #: NC011
North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
South Carolina Drinking Water Cert. #: 99006003
Virginia Certification #: 00213
Connecticut Certification #: PH-0104
Florida)NELAP Certlfication #: E87627
Kentucky UST Certification #: 84
Louisiana DHH Drinking Water # LA 100031
West Virginia Certification #: 357
Pace Analytical Services, Inc.
9800 KinceylAve. Suite 100
Hunter villa, NC 280-18
North Carolina Wastewater Certification #: 40
Pennsylvania Certlfrcation M 68-03578
South Carolina Bloassay Certification #: 99030002
South Carolina Certification #: 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
I
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wriaen consent of Pace Analytical Services, Inc..
Ll1�.j=
Page 2 of 47
(SL 90 8Z ab2d)

(Page 29 of 75)
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
�G�MalytlCal 206 East Meadow Road - Suits A 2225 Riverside Dr.
www.pace4 com Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
SAMPLE SUMMARY
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Lab ID
Sample ID
filatrlx
Date Collected
Date Received
9295688001
5-2-23
Solid
06/06/1110:30
06107/1115:33
9295688002
TMW-1
Water
06106/1115:45
06/07/1115:33
9295688003
TMW-2
Water
06/0611116:15
06/07/1115:33
9296680004
TMW-3
Water
06/06/1117:30
06/0711115:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analy0cal Services, Inc.
9800 lancey Ave, Suite 100
Huntersvil e, NC 28078
[phone]
Page 3 of 47

•
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical, Services, Inc.
Analytical
205 East Meadow Road - Suite A
2225 Riverside Or.
9800 Kincey
Ave. Suite 100
Eden, NO 27288
Asheville, NO 28804
Hunters
'Me, NO 28078
mM►Psoatthaw"
[phone]
(828)254-71767D4)875-9092
SAMPLE ANALYTE COUNT
Project:
BIEDERMANN REALTY 08-7690.2
Pace Project No.:
9295688
Anslytes
Lab ID
Sample ID
Method
Analysts
Reported i,
aborstory
9295688001
3-2-23
EPA6010
JMW
7
PASI-A
EPA 7471
SHB
1
PASI-A
EPA 8270
PPM
74
PAST-C
EPA 8260
DLK
71
PASI-C
ASTM D2974-87
TNM
1
PASI-C
9295688002
TMW-1
EPA6010
JMW
7
PASI-A
EPA 7470
SHB
1
PASI-A
EPA 8270
PPM
74
PASI-C
I
EPA 8260
MCK
63
PASI-C
9295688003
TMW-2
EPA6010
JMW
7
PASI-A
EPA 7470
SHB
1
PASI-A
EPA 8270
PPM
74
j PASI-C
EPA 8260
MCK
63
PASI-C
9295688004
TMW-3
EPA6010
JMW
7
PASI-A
EPA 7470
SHB
1
! PASI-A
EPA 8270
PPM
74
PASI-C
EPA 8260
MCK
63
PAW-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 47
(5L 30 OE abed)

(Page 31 of 75)
acemalytical e
t+'*W4&0/abacom
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NO 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite 100
Huntersvi8e, NO 28075
[phone]
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Sample: S-2-23 Lab ID: 9296688001 Collected: 06106111 10:30 Received: 06/07111 1623 Matrix: Solid
Results reported on a "dry -weight" basis
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Oual
8010 MET ICP
Analytical Method: EPA6010 Preparation Method: EPA 3050
Arsenic
0.68 mg/kg
0.40
0.26
1
06/09/11 15.30
06/10111 22:33
7440-38-2
Barium
80.9 mg/kg
0.40
0.016
1
06/09/11 16:30
06/10/11 22:33
7440-39-3
Cadmium
NO mg/kg
0,079
0.047
1
06/09/11 15:30
0611011122:33
7440-43-9
Chromium
14.3 mg/kg
0.40
0.024
1
06/09/11 15:30
06/10/11 22:33
7440-47-3
Lead
1.7 mg/kg
0.40
0.38
1
06/09/11 15:30
06/10/11 22:33
7439-92-1
Selenium
NO mg/kg
0.79
0.30
1
06/09/11 15:30
06/13/11 12:55
7782-49-2
Silver
NO mg/kg
0.40
0.024
1
06/09/11 16:30
06/10/11 22:33
7440-22-4
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.0034.11 mg/kg
0.0042
0.000083
1
06/09/11 15:20
06/09/11 17:28
7439-97-6
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
Acenaphthene
NO ug/kg
376
86.6
1
06/08/11 13:10
06/10/11 17:06
83-32-9
Acenapht"ene
NO ug/kg
376
88.9
1
06108111 1310
06110111 17:06
208-96-8
Aniline
NO ugikg
376
101
1
06/08/11 13:10
06/10/11 17:06
62-53-3
Anthracene
NO ug/kg
376
84.3
1
06/06/11 13710
06110111 17:06
120-12-i
Benzo(a)anthracene
NO ug/kg
376
69.5
1
06/08/11 13:10
06/10/11 17:06
66-55-3
Senzo(a)pyrene
NO ug/kg
376
71.8
1
06/08/11 13:10
06/10/11 17:06
50-32-8
Benzo(b)fluoranthene
NO ug/kg
376
64.9
1
06/08/11 13:10
06/10/11 17:06
205-99-2
Benzo(g,h,t)perylene
NO ug/kg
376
95.7
1
06/08111 13:10
06/10/11 17:06
191-24-2
Benzo(k)fluoranlhene
NO ug/kg
376
74.1
1
06/08/11 13:10
06/10/11 17:06
207-08-9
Benzoic Acid
NO ug/kg
1880
68.4
1
06/08/11 13:10
06/10/11 17:06
65-85-0
Benzyl alcohol
NO ug/kg
752
75.2
1
06/08/11 13:10
06/10/11 17:06
100-51-6
4-Bromophenylphenyl ether
NO ug/kg
376
68.4
1
06/08/11 13:10
06/10111 17:06
101-55-3
Butylbenzytphthalate
NO ugikg
376
79.8
1
08/08111 13:10
06/10111 17:06
85-68-7
4-Chloro-3-methylphenol
NO ug/kg
752
77.5
1
06/08/11 13:10
06110/11 17:06
59-50-7
4-Chtoroaniine
NO ug/kg
1880
105
1
06/0B111 13:10
06110111 17:06
106.47-8
bis(2-Chloroethoxy)methane
NO ug/kg
376
87.7
1
06/08/11 13:10
06/10111 17:06
111-91-1
bis(2-Chloroethyl) ether
NO ug/kg
376
95.7
1
06/08/11 13:10
06/10/11 17:06
111-44-4
bis(2-Chioroisopropyl) ether
NO ug/kg
376
100
1
06/08/11 13:10
06/10/11 17:06
108-60-1
2-Chloronaphthalene
NO uglkg
376
74.1
1
06/08111 13:10
06/10/11 17:06
91-58-7
2-Chlorophenol
NO ug/kg
376
103
1
06/08/11 13:10
06/10/11 17:06
95-57-8
4-Chlorophenylphenyi ether
NO ug/kg
376
77.5
1
06/08/11 13:10
06/10/11 17:06
7005-72-3
Chrysene
NO ug/kg
376
50.1
1
06/08MI 13:10
06/10/11 17:06
218-01-9
Dibenz(a,h)anthracene
NO ug/kg
376
79.8
1
06/08/11 13:10
06/10/11 17:06
53-70-3
Dibenzofuran
NO ug/kg
376
61.5
1
OBID8111 13:10
06110/11 17:06
132-64-9
1,2-Dichlorobenzene
NO ug/kg
376
100
1
06/08/11 13:10
06110/11 17:06
95-50-1
1,3-Oichlorobenzena
NO ugikg
376
85.5
1
06108111 13:10
06110111 17:06
541-73-1
1,4-Dichlorobenzene
NO ug/kg
376
106
1
06/08/11 13:10
06/10111 17:06
10646-7
3,3'-Dichlorobenzidine
NO ugikg
1880
82.0
1
06/08/11 13:10
06/10/11 17:06
91-94-1
2,4-Dichlorophenol
NO ug/kg
376
82.0
1
06/08/11 13:10
06/10/11 17:06
120-83-2
Diethylphthalate
NO ug/kg
376
58.1
1
06/08/11 13:10
06/10/11 17:06
84-66-2
2,4-Dimethylphenol
NO ug/kg
376
148
1
00/08111 13:10
06/10/11 17:06
105-67-9
Dimethylphthalate
NO ug/kg
376
76.3
1
06/08/11 13:10
06/10/11 17:06
131-11-3
DI-n-butylphthalate
NO ug/kg
376
61.5
1
06/08/11 13:10
06/10/11 17:06
84-74-2
Date: 06/1612011 03:13 PM
REPORT OF LABORATORY ANALYSIS
Page 5 of 47
This report shall hot be reproduced, except in full,
without the written consent of
Pace Analytical Services, Inc..
ova

• Pace Analytical Services, Inc. Pace Analytical Services, Inc.
AnalXici f 205 East Meadow Road - SuReA 2225 Riverside Dr.
7' emm:psodatrtrnm Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9296688
Pace Analytical,
9600 Kincey
Hunters
Services, Inc.
`pve. Suite 100
Hie, NC 28078
[phone]
I
i I
Sample: S-2-23
Lab ID: 9295688001 Collected: 06/06/11
10:30
Received: 06/07/11 15:33 Matrix: Solid
Results reported on a "dry -weight" basis
j
Report
I
Parameters
Results Units Limit
MDL
OF
Prepared
Analyzed CAS No.
Qual
8270 MSSV Microwave
Analytical Method: EPA 8270 Preparation Method: EPA 3546
4,6-Dinitro-2-methylphenol
NO ugfkg
752
75.2
1
06/08/11 13:10
06/10/11 17:06 534-52-1
2,4-Dinitrophenol
ND ug/kg
1880
61.5
1
06/08111 13:10
O6/10/11 17:06 51-28-5
2,4-Dinitrotoluene
ND ug/kg
376
70.6
1
06/08/11 13:10
06/10/11 17:06 121-14-21
1
2,6-Dinitrototuene
NO ug/kg
376
78.6
1
06108(11 13:10
06MOIll 17:06 606-20-21
DI-n-octylphthalate
NO ug/kg
376
78.6
1
06/08111 13:10
06110111 17:06 117-84-0
bis(2-Ethylhexyl)phthalate
ND ug/kg
376
103
1
06/08/11 113:10
06/10111 17:06 117-81-7I
Fluoranthene
NO uglkg
376
54.7
1
06/08/11 13:10
06/10/11 17:00 206.44-0'
Fluorene
NO ug/kg
376
77.5
1
06/08/11 13:10
06/10/11 17:06 86-73-7
Hexachloro-1,3-butadiene
ND ug/kg
376
64.9
1
06108/11 13:10
06110/11 17:06 87-68-3
Hexachlorobenzene
NO ugfkg
376
47.9
1
06/08/11 13:10
06/10/11 17:06 118-74-1
Hexachiorocydopentadiene
ND ug/kg
376
69.5
1
06/08/1i 13:10
06/10/11 17:06 77-47-4
Hexachioroelhane
ND ug/kg
376
99.1
1
06/08/11 13:10
06/10/11 17:06 67-72-1
!
Indeno(1,2,3-cd)pyrene
ND ug/kg
376
77.5
1
06/08/11 13:10
06/10/11 17:06 193-39-5
Isophorone
NO ug/kg
376
84.3
1
06/08111 13:10
06/10/11 17:06 78-59-1
1-Methylnaphthalene
ND ugfkg
376
98.0
1
06/08/11 13:10
06/10/11 17:06 90-12-0
2-Methylnaphthalene
ND ugfkg
376
80.9
1
06/08/11 13:10
06I10/11 17:06 91-57-6
2-Methylphenol(o-Cresol)
NO ug/kg
376
114
1
06/08/11 13:10
06/10/11 17:06 95-48-7
3&4-Methylphenol(m&p Cresol)
NO uglkg
376
148
1
06/08(11 13:10
06/10/11 17:06
Naphthalene
ND ug/kg
376
92.3
1
06/08/11 13:10
06/10/11 17:06 91-20-3
2-Nitroadline
ND ug/kg
1880
116
1
06/08/11 13:10
06/10/11 17:06 88-744
3-Nitroaniline
ND ug/kg
1880
103
1
06/08/11 13:10
06/10/11 17:Oe 99-09-2
4-Nitroaniline
NO ugfkg
752
106
1
06/08/11 13:10
06110/11 17:06 100-01-E
1
Nitrobenzene
ND ug/kg
376
103
1
06/08/11 13:10
06110111 17:06 98-95-3
2-Nitrophenol
ND ug/kg
376
91.2
1
06/08/11 13:10
06/10/11 17:06 88-76-5
4-Nftrophenof
NO ug/kg
1880
67.2
1
06/08111 13:10
06/10/11 17:06 100-02-7
N-Nitrosodimethylantine
NO ug/kg
376
122
1
06/08/11 13:10
06110/11 17:06 62-75-9
N-Nitroso-di-n-propylamine
ND ugfkg
376
71.8
1
06/08/11 113:10
06/10/11 17:06 621-64-1
N-Nitrosodiphenylamine
ND uglkg
376
112
1
061081111310
06/10111 17:06 86-30-6
Pentachlorophenol
NO ug/kg
1880
68.4
1
06/08/11 13:10
06110/11 17:06 87-86-5
Phenanthrene
ND uglkg
376
62.7
1
06/08/11 13:10
06/10/11 17:06 85-01-8
Phenol
NO ug/kg
376
113
1
06/08111 13:10
06/10/11 17:06 108-95-2
Pyrene
NO ug/kg
376
63.8
1
06/08/11 13:10
06/10/il 17:06 129-00-0
17:06 120-82-1
1,2,4-Trichlorobenzene
NO ugfkg
376
72.9
1
06/0811i 13:10
06/10/11
2,4,5-Trichloroptienol
NO ugfkg
376
116
1
06/08111 13:10
06/10111 17:06 95-95 4
2,4,6-Tdchlorophenol
ND ug/kg
376
83.2
1
06/08/11 13:10
06/1Oil 1 17:06 88-06-2
Nitrobenzene-d5 (S)
43 %
23-110
1
06/08111 13:10
06/10111 17:06 4165-60r0
2-Fluorobiphenyl (S)
46 %
30-110
1
06/08/il 13:10
06110/ll 17:06 321-60-8
Terphenyl-d14 (S)
61 %
28-110
1
06/08/11 13:10
06/10/11 17:06 1718-51r0
4
Phenof-66 (S)
40 %
22-110
1
06/08/11 13:10
06/10/11 17:06 13127-8
1
2-Fluorophenol(S)
42 %
13-110
1
06/08/11 13:10
06/10/11 17:06 367-12-�
2,4,6-Tribromophenol (S)
104 %
27-110
1
06/08111 13:10
06/10111 17:06 118-79�
826015036A Volatile Organics
Analytical Method: EPA 8260
Acetone
33.8J uglkg
105
10.5
1
06/15/11 14:18 67-64-1
Benzene
ND uglkg
5.2
1.7
1
06/15/11 14:18 71-43-2
I
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
Page 6 of 47
This report shall not be
reproduced, except
In full,
without the written consent of Pace Analytical
Services, Inc.,
(5L 3o Z£ abpd)
ace

(Page 33 of 75)
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr.
wanpe cabUcom Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Project: BIEDERMANN REALTY08-7690.2
Pace Analytical Services, Inc.
9800 Knceygve. Suite too
Huntersvifle, NC 28078
[phone]
Pace Project No.: 9295688
Sample: S-2-23 Lab ID: 9295608001 Collected: 06/06/11 10:30 Received: 06/07/11 15:33 Matrix: Solid
Results reported on a "dry-welght" basis
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
826015035A Volatile Organics
Analytical Method: EPA 8260
Bromobenzene
Bromochloromethane
ND ug/kg
5.2
2.1
1
06/15/11 14:18
108-86-1
Bromodichloromethane
ND ug/kg
NO ug/kg
5.2
5.2
1.8
1
06/15/11 14:18
74-97-5
Bromoform
ND ug/kg
5.2
2.0
2.4
1
1
06/15/11 14:18
75-27-4
Bromomethane
NO ug/kg
10.5
2.6
1
06/15/11 14:18
75-25.2
2-Butanone (MEK)
ND ug/kg
105
3.0
1
06/15/11 14:18
74-83-9
n-Butylbenzene
NO ug/kg
5.2
1.9
1
06/15/11 14:18
78-93-3
sec-Butylbenzene
NO ug/kg
5.2
1.7
1
06/15111 14:18
104-51-8
tert-Butylbenzene
ND uglkg
5.2
2.1
1
06/15/11 14:18
135-98-8
Carbon tetrachloride
ND ug/kg
5.2
2.7
1
06/15/11 14:18
98-06-6
Chlorobenzene
NO ug/kg
5.2
2.0
1
06/15/11 14:18
56-23-5
Chloreethane
ND ug/kg
10.6
2.5
1
06/15/11 14:18
108-90-7
Chloroform
NO ug/kg
5.2
1.7
1
06/15/11 14:18
75-00-3
Chloromethane
ND ug/kg
10.5
2.5
1
06/15/11 14:18
67-66-3
2-Chlorotoluene
NO ug/kg
5.2
1.8
1
06/15/11 14:18
74-87-3
4-Chlorotoluene
NO ug/kg
5.2
1.9
1
06/15/11 14:18
95-49-8
1,2-Dibromo-3-chloropropane
NO uglkg
5.2
3.8
1
06/15/11 14:18
106.43-4
Dibromochloromethane
NO ug/kg
5.2
1.9
1
06/15/11 14:18
96-12-8
1,2-Dibromoethane (ED8)
NO ug/kg
5.2
1.9
1
08/15/11 14:18
124-48-1
Dibromomethane
NO ug/kg
5.2
2.6
1
06/15/11 14:18
106-93-4
1,2-Dichlorobenzene
NO ug/kg
5.2
2.0
1
06/15/11 14:18
74-95-3
1,3-Dichlorobenzene
ND ug/kg
5.2
2.1
1
06/15/11 14:18
95-50-1
1,4-Dichlorobenzene
NO uglkg
5.2
1.8
1
06/15/11 14:18
541-73-1
DichlorodiFluoromethane
NO ug/kg
10.5
3.8
1
06/15/11 14:18
108-46-7
1,1-Dichloroethene
ND ug/kg
5.2
1.6
1
06/15/11 14:18
75-71-8
1,2-Dichloroethane
NO ug/kg
5.2
2.3
1
06/15/11 14:18
75-34-3
1,1-Dichloroethene
ND ug/kg
5.2
1.9
1
05115/11 14:18
107-06-2
cis-1,2-Dichloroethene
ND ug/kg
5.2
1.5
1
06/15/11 14:18
75-35-4
trans-1,2-Dichloroethene
ND uglkg
5.2
2.0
1
06/15/11 14:18
156-59-2
1,2-Dichloropropane
NO ug/kg
5.2
1.8
1
06/15/11 14:18
156-60-5
1,3-Dichloropropane
ND ug/kg
5.2
2.0
1
06/15/11 14:18
78-87-5
2,2-Dichloropropane
NO ug/kg
5.2
1.8
1
06/15/11 14:18
06/15/11 14:18
142-28-9
594-20-7
1,1-Dichloropropene
NO ug/kg
5.2
1.6
1
06/15/11 14:18
563.58-6
cis- 1, 3-Dichloropropene
NO uglkg
5.2
1.9
1
06/15/11 14,18
10061-01-5
trans-1,3-Dichloropropene
NO ug/kg
5.2
1.6
1
06116/11 14:18
10061-02-6
Diisopropyi ether
NO ug/kg
5.2
1.8
1
06/15/11 14:18
108-20-3
Ethylbenzene
NO uglkg
5.2
1.9
1
06/15/11 14:18
100-41-4
Hexachloro-1,3-butadiene
ND uglkg
5.2
2.1
1
06/15/11 14:18
87-68-3
2-Hexanone
ND uglkg
52.3
4.1
1
06/15/11 14:18
591-78-6
Isopropylbenzene (Cumene)
NO ug/kg
6.2
2.0
1
06/15/11 14:18
98-82-8
p-Isopropyltoluene
NO ug/kg
5.2
1.8
1
06/15/11 14:18
99-87-6
Methylene Chloride
9.8J ug/kg
20.9
3.1
1
06/15/11 14:18
75-09-2
4-Methyl-2-pentanone (MIBK)
NO ug/kg
52.3
3.9
1
06115/11 14:18
108-10-1
Methyl-tert-butyl ether
ND ug/kg
5.2
1.6
1
06/15/11 14:18
1634-04-4
Naphthalene
ND ug/kg
5.2
1.3
1
06/15/11 14:18
91-20-3
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 7 of 47
This report shall not be reproduced, except In full,
without thewnttcn conse
ntof Pace Analytical Services, Inc,.

Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical services, Inc.
q,, j•
205 East Meadow Road - Suite A
2225 Riverside Dr.
980010ncey Ave. Suite 100
!it IL�nJtiCL' I
Eden, NC 27288
Asheville, NC 23504
tiuntersvilte, NC 28078
xwwpocambLo
[phone]
[phone]
[phone]
ANALYTICAL RESULTS
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Sample: S-2-23
Lab ID: 9296688001 Collected: 06/06/11 10:30 Received: 06/07/11 15:33 Matrix: Solid,
Results reported on a dry -weight" basis
Report
Parameters
Results Units Limit
MDL OF Prepared
Analyzed CAS No. Qua]
826015035A Volatile Organics
Analytical Method: EPA 8260
n-Propylbenzene
NO ug/kg
5.2
1.8 1
06/15/11 14:18 103-65-1
Styrene
NO ug/kg
5.2
1.9 1
06/15/11 14:18 100-42-5
1, 1, 1,2-Tetrachloroethane
NO ug/kg
5.2
2.2 1
06/15/11 14:18 630-20-6
1,1,2,2-Tetrachloroethane
NO ugikg
5.2
2.0 1
06/15/11 14:18 79-34-5
Telrachloroethene
NO ug/kg
5.2
1.8 1
06/16/11 14:18 127-18-4
Toluene
NO ug/kg
5.2
5.2
1.9 1
2.3 1
06/15/11 14:18 108-88-3
06/15/11 14:18 87-61-6
11
1,2,3-Trichlorobenzene
ND ugtkg
1,2,4-Trichlorobenzene
NO ugtkg
5.2
1.7 1
06/1511i 14:18 120-82-1
1,1,1-Trichloroethane
ND ug/kg
5.2
1.9 1
06/15/11 14:18 71-55-6'
1,1,2-Trichloroethane
NO ugtkg
5.2
2.2 1
06/15111 14:18 79-00-5I
Trichloroethene
NO ug/kg
5.2
2.2 1
06/15/11 14:18 79-01-61
Trichlorofluoromethane
NO ug/kg
5.2
2.3 1
06/15111 i4:18 75- "
1,2.3-Trichicropropane
NO ug/kg
5.2
1.7 1
06/15/11 14:18 96-18-41
1.2,4-Trimethylbenzene
NO ug/kg
5.2
2.1 1
06/15/11 14:18 9"3-6
1,3,5-Trimethylbenzene
NO ug/kg
5.2
1.9 1
06/15/11 14:18 108-67
14:18 108-05-�
Vinyl acetate
NO ug/kg
52.3
9.2 1
06/15/11
Vinyl chloride
ND ug/kg
10.5
1.9 1
06/15/11 14:18 75-01-4I
Xylene (Total)
NO ug/kg
10.5
3.8 1
06/15/11 14:18 1330-20-7
m&p-Xylene
NO uglkg
10.5
3.8 1
06/15/11 14:18 179601123-1
o-Xylene
NO ug/kg
5.2
2.0 1
06/15/11 14:18 95-47-6I
Dibromofluoromethane IS)
98 %
70-130
1
06/15/11 14:18 1888-53-7
Toluene-d8 (S)
102 %
70-130
70-130
1
1
06/15111 14:18 2037-26-5
06/15/11 14:18 460 004
4-Bromofluorobenzene (S)
92 %
1,2-13ichloroethane-& (S)
94 %
70-132
1
06/15/11 14:18 17060-07-0
I
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
12.2 %
0.10
0.10 1
06109/11 13:49
Sample: TMW-1
Lab ID: 9295688002 Collected: 06/06111 15:45 Received: 06/07111 15:33 Matrix: Water
Report
Parameters
Results Units Limit
MOILDF Prepared
Analyzed CAS�10.
Qual
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Arsenic
20A ug/L
5.0
2.7 1 08/11/11 12:15
06/14/11 00:14 7440-38-2
06/14/11 00:14 7440-36-3
Barium
5040 ug/L
5.0
2.5 1 06/11/11 12:15
Cadmium
37.7 ug/L
1.0
0.50 1 06/11/11 12:15
06/14/11 00:14 744049
Chromium
634 ug/L
5.0
2.0 1 06/11/11 12:15
06/14/11 00:14 7440-4
-3
Lead
320 ug/L
5.0
4.0 1 06/11/11 12:15
06/14/11 00:14 7439-9
-1
Selenium
14.9 ug/L
10.0
5.0 1 06/11/11 12:15
06/14/11 00:14 7782-4,
2
4
Silver
5.0 ug/L
5.0
2.5 1 06/11/11 12:15
06114/11 00:14 7440-2
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
1.1 ug/L
0.20
0,10 1 06/0911110:15
06/09/1115:44 7439-97-6
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
Page 8 of 47
This report shall not be reproduced, except In full,
1
without the written consenntt Pace Analytical Services, Inc..
1
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1
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(Page 35 of 75)
acemalw cal
WWW.Pft1&U .coat
Pace Analytical Services, Inc- Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Project: BIEDERMANN REALTY 08-7690.2
Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Pace Project No.: 9296688
Sample. TMW-1 Lab 10; 9295988002 Collected: 06106111 15:45 Received: 06/07111 15:33 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270 MSSV S911Rivolatile Organic:
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
Acenaphthylene
ND ug/L
10.0
0.25
1
06/13/11 15:00
06/15/11 13:02
83-32-9
Aniline
ND ug/L
10.0
0.21
1
06/13/11 15:00
06/15/11 13:02
208-96-8
Anthracene
ND ug/L
ND ug/L
10.0
2.0
1
06/13/11 15:00
06/15/11 13:02
62-53-3
Benzo(a)anthracene
ND ug/L
10.0
0.14
1
06/13111 15:00
06/15/11 13:02
120-12-7
Benzo(a)pyrene
ND ug/L
10.0
0.33
1
06113/11 15:00
06/15/11 13:02
56-55-3
Benzo(b)fluoranthene
ND ug/L
10.0
10.0
0.30
1
06/13/11 15:00
06/15/11 13:02
50-32-8
Benzo(g,h,i)perylene
1.1J ug/L
10.0
0.28
1
06/13/11 15:00
06/15/11 13:02
205-99-2
Benzo(k)fluoranthene
ND ug/L
10.0
0.38
0.43
1
06/13/11 15:00
06/16/11 13:02
191-24-2
Benzoic Acid
ND ug/L
50.0
1
06/13/11 15:00
06/15/11 13:02
207-08-9
Benzyl alcohol
ND ug/L
20.0
11.5
1
06/13111 15:00
06/15111 13:02
65-85-0
4-Bromophenylphenyl ether
ND ug/L
10.0
2.4
0.82
1
06113/11 15:00
06/15111 13:02
100-51-6
Butylbenzylphthalate
ND ug/L
10.0
0.79
1
06/13/11 15:00
06/15/11 13:02
101-55-3
4-Chloro-3-methylphenol
ND ug/L
20.0
3.7
1
06/13/11 15:00
06/15/11 13:02
85-68-7
4-Chloroaniline
ND ug/L
20.0
1
06/13/11 15:00
06116/11 13:02
59-50-7
bis(2-Chloroethoxy)methane
ND ug/L
10.0
2.8
0.92
1
06/13/11 15:00
06/15/11 13:02
106.47-8
bis(2-Chloroethyl) ether
ND ug/L
10.0
1.0
1
06/13/11 15:00
06/15/11 13:02
111-91-1
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
0.95
1
1
06/13/11 15:00
06/15/11 13:02
111-44-4
2-Chloronaphthalene
ND uglL
10.0
0.98
1
06/13/11 15:00
06/15/11 13:02
108-60-1
2-Chlorophenol
ND ug/L
10.0
1.3
06/13/11 15:00
06/15/11 13:02
91-58-7
4-Chlorophenylphenyl ether
ND ug/L
10.0
0.87
1
06/13111 15:00
06/15111 13:02
95-57-8
Chrysene
ND ug/L
10.0
0.21
1
06/13/11 15:00
06/15/11 13:02
7005-72-3
Dibenz(a,h)anthracene
ND ug/L
10.0
0.55
1
1
06/13/11 15:00
06/15/11 13:02
218-01-9
Dibenzofuran
ND ug/L
10.0
06/13/11 15:00
06/15/11 13:02
53-70-3
1,2-Dichlorobenzene
ND ug/L
10.0
0.89
0.88
1
1
06/13/11 15:00
05/15/11 13:02
132-64-9
1,3-Dichlorobenzene
ND ug/L
10.0
0.81
06/13/11 15:00
06115/11 13:02
95-50-1
1,4-Dichlorobenzene
ND ug/L
10.0
0.95
1
1
06/13/11 15:00
06/13/11 15:00
06/15/11 13:02
06/15/11 13:02
541-73-1
106.46-7
3,3'-Dictllorobenzidine
ND ug/L
20.0
2.1
1
06/13/11 15:00
D6115111 13:02
91-94-1
2,4-Dichlorophenol
Diethylphthalate
ND ug/L
10.0
1.7
1
06/13/11 15:00
06/15/11 13:02
120-83-2
2,4-Dimethylphenol
ND ug/L
ND ug/L
10.0
10.0
0.58
1
06/13111 15:00
06115/11 13:02
84-66-2
Dimethyiphthalate
ND ug/L
10.0
1.2
1
06/13/11 15:00
06/15/11 13:02
105-67-9
Di-n-butylphthalate
ND ug/L
10.0
0.76
0,75
1
06/13/11 15:00
06/16/11 13:02
131-11-3
4,6-Dinitro-2-methylphenol
ND ug/L
20.0
2.6
1
1
06/13111 15:00
06/13/11 15:00
06/15/11 13:02
06/15/11 13:02
84-74-2
534-52-1
2,4-Dinitrophenol
ND ug/L
50.0
9.0
1
06/13/11 15:00
06/15/11 13:02
51-28-5
2,4-Dinitrotoluene
ND ug/L
10.0
0.90
1
06/13/11 15:00
06/15/11 13:02
121-14-2
2,6-Dinitrotoluene
ND ug/L
10.0
0.98
1
06/13/11 15:00
06115111 13:02
606-20-2
Di-n-octylphthalate
ND ug/L
10.0
0.66
1
06/13/11 15:00
06/15/11 13:02
117-84-0
bis(2-Ethylhexyl)phthalate
ND ug/L
6.0
0.79
1
06/13/11 15:00
06/15/11 13:02
117-81-7
Fluoranthene
ND ug/L
10.0
0.21
1
06/1311115:00
06115/11 13:02
206-44-0
Fluorene
ND ug/L
10.0
0.21
1
06/13/11 15:00
06/15/11 13:02
86-73-7
Hexachloro-1,3-butadlene
ND ug/L
10.0
0.94
1
06/13/11 15:00
06/15/11 13:02
87-68-3
Hexachlorobenzene
ND ug/L
10.0
0.72
1
06/13/11 15:00
06/15/11 13:02
118-74.1
Hexachlorocyclopentadiene
ND ug/L
10.0
0.88
1
06/13/11 15:00
06/15/11 13:02
77-47-4
Hexachloroethane
ND ug/L
10.0
1.1
1
06/13/11 15:00
06/15/11 13:02
67-72-1
Indeno(1,2,3-cd)pyrene
ND ug1L
10.0
0.29
1
06/13/11 15:00
06/15/11 13:02
193-39-5
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 9 of 47
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc..

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 KincelAve. Suite 100
pacaiebs�m Eden, NC 27288 Asheville, NC 28804 Huntereville, NC 28078
[phone] [phone] i(704)875-9092
Project:
Pace Project No.:
Sample: TMW-1
BIEDERMANN REALTY 08-7690.2
9295688
Parameters
8270 MSSV Semtvolatlie Organic
Isophorone
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenot
N-Nitrosodimethylamine
N-Nilroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV Low Level
Acetone
Benzene
Bromobenzene
Bromochloromelhane
Bromodichloromethane
Bromoform
Bromomethene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chioromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-chloropropane
Date: 06/16/2011 03:13 PM
ANALYTICAL RESULTS
Lab ID• 9295688002 Collected: 06/06111 15,45 Received: 06/07/11 15:33 Matrix:
Report
Results Units Limit MDL OF Prepared
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Analyzed CAS I
ND ug/L
10.0
0.89
1
06113111 15:00
06/15/11 13:02
78-59-1
NO ug/L
10.0
0.32
1
06/13/11 15:00
06/15/11 13:02
90-12-0
NO ug/L
10.0
0.28
1
06/13/11 16:00
06/15/11 13:02
91-57-6
NO ug/L
10.0
1.6
1
06/13/11 15:00
06/15/11 13:02
95-48-7 1
NO ug/L
10.0
2.0
1
06113/11 15:00
06/15/11 13:02
1
NO ug/L
10.0
0.34
1
06/13/11 15:00
05/15/11 13:02
91-20-31
NO ug/L
50.0
2.0
1
06/13/11 15:00
06/15111 13:02
88-74-4
ND ug1L
50.0
2.0
1
06/13/11 15:00
06/15/11 13:02
99-09-2
ND ug/L
20.0
2.1
1
06/13/11 15:00
06/15/11 13:02
100-01-6
ND ug1L
10.0
1.1
1
06113/11 15:00
06/15/11 13:02
98-95-31
NO ug/L
10.0
0.91
1
06/13111 15:00
06/15/11 13:02
88-75-51
ND ug/L
50.0
4.1
1
06/13/11 15:00
06/15/11 13:02
100-02-7
NO ug/L
10.0
0.91
1
06/13/11 15:00
06/15/11 13:02
62-75-91
ND ug/L
10.0
0.99
1
06/13/11 15:00
05/15/11 13:02
621-64-7
NO ug/L
10.0
1.0
1
06/13/11 15:00
06/15/11 13:02
86-30-61
ND ug/L
25.0
4.6
1
06/13/11 15:00
06/15111 13:02
87-86-5
NO ug/L
10.0
0.22
1
06/13/11 15:00
06/15/11 13:02
85-01-8
NO ug/L
10.0
1.9
1
06/13/11 15:00
06/15/11 13:02
108-95-2
NO ug/L
10.0
0.19
1
06/13/11 15:00
06/15/11 13:02
129-00-0
NO ug/L
10.0
0.98
1
06/13/11 15:00
06/15/11 13:02
120-82-1
NO ug/L
10.0
0.92
1
06/13/11 15:00
06/16/11 1102
95-9541
ND ug/L
10.0
1.3
1
05/13/11 15:00
06/15/11 13:02
88-06-21
66 %
21-110
1
06/13/11 15:00
06115/11 13:02
4165-6 -0
63 %
27-110
1
06/13/11 15:00
06115/11 13:02
321-60-8
90 %
31-107
1
06/13/11 15.00
06/15/11 13:02
1718-5' -0
29 %
10-110
1
06/13/11 15:00
06/15/11 13:02
13127-88-
41 %
12-110
1
06/13/11 15:00
06/15111 13:02
367-12-4
87 %
27-110
4
06/13/11 15:00
06/15/11 13:02
118-79-6
Analytical Method: EPA 8260
SAJ ug/L
25.0
2.2
1
06/09/11 08:14 67-64-
NO ug/L
1.0
0.25
1
06/09/11 08:14
71-43-
NO ug/L
1.0
0.30
1
06/09/11 08:14
108-81
NO ug/L
1.0
0.17
1
06/09/11 08:14
74-97-
NO ug/L
1.0
0.18
1
06/09111 08:14
75-27-
NO ug/L
1.0
0.26
1
06/09111 08:14
75-25,
NO ug/L
2.0
0.29
1
06/09111 08:14
74-83
NO ug/L
5.0
0.96
1
06/09111 08:14
78-93
NO ug/L
1.0
0.25
1
06/09/11 08:14
56-23
NO ug/L
1.0
0.23
1
06/09/11 08:14
108-9'
NO ug/L
1.0
0.54
1
06/09/11 08:14
75-00
NO ug/L
1.0
0.14
1
06/09/11 08:14
67-68
NO ug/L
1.0
0.11
1
06/09/11 08:14
74-87
NO ug/L
1.0
0.35
1
06/09/11 08:14
95-49
NO ug/L
1.0
0.31
1
06/09/11 08:14
106.4
NO ug/L
5.0
2.5
1
06/09/11 08:14
96-12
REPORT OF LABORATORY
ANALYSIS
This report shell not be reproduced, except in full,
without the written consent of PsceAnalytical
Services, Inc..
Qual
Page 10 of 47
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(Page 37 of 75)
m Pace Analytical Servlc4s, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalXical 205 East Meadow Roed - Suite A 2225 Riverside Dr. 9800 Kncey Ave. Suite 100
MvwpecelaW.can Eden. NC 27288 Asheville, NC 26804 Huntersviae, NC 28078
[phone] [phone]
[phone]
ANAI*YTICAL RESULTS
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
oampie: I mvY-1
Lab ID: 9298688002
Collected: 06/06/11 15:45
Received: 06/07/11 15:33 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
OF
Prepared Analyzed
CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
Dibromochlorometh8ne
NO ug/L
1.0
0.21
1
06/09/11 08:14
124-48-1
1,2-Dibromoethane (EDB)
NO ug/L
1.0
0.27
1
06/09/11 08:14
106-93-4
Dibromomethane
NO ug/L
1.0
0.21
1
06/09/11 08:14
74-95-3
1,2-Dichlorobenzene
NO ug/L
1.0
0.30
1
06/09/11 08:14
95-50-1
1,3-Dichlorobenzene
ND ug/L
1.0
0.24
1
06/09/11 08:14
541-73-1
1,4-Dichlorobenzene
NO ug/L
1.0
0.33
1
06/09/11 08:14
106-46-7
Dichlorodifluoromethane
ND ug/L
1.0
0.21
1
06/09/11 08:14
75-71-8
1, 1 -Dichloroethane
NO ug/L
1.0
0.32
1
06/09/11 08:14
75-34-3
1,2-Dichloroethane
NO ug/L
1.0
0.12
1
06/09/11 08:14
107-06-2
1,1-Dichloroethene
ND ug/L
1.0
0.56
1
06/09/11 08:14
75-35.4
cis-1,2-Dichloroethene
0.45.1 ug/L
1.0
0.19
1
06109/11 08:14
156-59-2
trans-1,2-Dichloroethene
ND ug/L
1.0
0.49
1
06/09/11 08:14
156-60-5
1,2-Dichloropropane
NO ug/L
1.0
0.27
1
06/09/11 08:14
78-87-5
1,3-Dichloropropane
ND ug/L
1.0
0.28
1
06/09/11 08:14
142-28.9
2,2-Dichloropropane
NO ug/L
1.0
0.13
1
06/09111 08:14
594-20.7
1,1-Dichloropropene
NO ug/L
1.0
0.49
1
06/09/11 08:14
563-58-6
cls-1,3-Dichloropropene
ND ug/L
1.0
0.13
1
06/09/11 08:14
10061-01-5
trans-1,3-Dichloropropene
NO ug/L
1.0
0.26
1
06/09/11 08:14
10061-02-6
Diisopropyl ether
NO ug/L
1.0
0.12
1
06/09/11 08:14
108-20-3
Ethylbenzene
ND ug/L
1.0
0.30
1
06109/11 06:14
100-41-4
Hexachloro-1,3-butadiene
NO ug/L
1.0
0.71
1
06/09/11 08:14
87-68-3
2-Hexanone
NO ug/L
5.0
0.46
1
06/09/11 08:14
591-78-6
p-Isopropyitoluene
NO ug/L
1.0
0.31
1
06/09/11 08:14
99-87-6
Methylene Chloride
ND ug/L
2.0
0.97
1
06/09/11 08:14
75-09-2
4-Methyl-2-penlanone (MIBK)
NO ug/L
5.0
0.33
1
06/09/11 08:14
108-10-1
Methyl-terl-butyl ether
NO ug/L
1.0
0.21
1
06/09/11 08:14
1634-04-4
Naphthalene
ND ug/L
1.0
0.24
1
06/09/11 08:14
91-20-3
Styrene
NO ug/L
1.0
0.26
1
06/09/11 08:14
100-42-5
1, 1. 1,2-Tetrachloroethane
NO ug/L
1.0
0.33
1
06/09/11 08:14
630-20-6
1,1,2,2-Tetrachloroelhane
NO ug/L
1.0
0.40
1
06/09/11 08:14
79-34-5
Tetrachloroethene
NO ug/L
1.0
0.46
1
06/09/11 08:14
127-18-4
Toluene
NO ug/L
1.0
0.26
1
06/09/11 08:14
108-88-3
1,2,3-Trichlorobenzene
NO ug/L
1.0
0.33
1
06/09/11 08:14
87-61-6
1,2,4-Trichlorobenzene
NO ug/L
1.0
0.35
1
06/09/11 08:14
120-82-1
1, 1. 1 -Trichloroethane
ND ug/L
1.0
0.48
1
06/09/11 08:14
71-55-6
1,1,2-Trichloroethane
ND ug/L
1.0
0.29
1
06/09/11 08:14
79-00-5
Trichloroethene
NO ug/L
1.0
0.47
1
06/09/11 08:14
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
06/09/11 08:14
75-69-4
1,2,3-Trichloropropane
ND ug/L
1.0
0.41
1
08/09/11 08:14
96-18-4
Vinyl acetate
ND ug/L
2.0
0.35
1
06/09/11 08:14
108-05-4
Vinyl chloride
NO ug/L
1.0
0.62
1
06/09/11 08:14
75-01-4
m&p-Xylene
ND ug/L
2.0
0.66
1
06109/11 08:14
17%01-23-1
o-Xylene
ND ug/L
1.0
0.23
1
06/09/11 08:14
95-47-6
4-Bromofluorobenzene (S)
100 %
70-130
1
06/09/11 08:14
460-00-4
Dibromofluoromethane (S)
102 %
70-130
1
06/09/11 08:14
1868-53-7
1,2-Dichloroethane-d4 (S)
99 %
70-130
1
06/09/11 08:14
17060-07-0
Date: 06/1612011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 11 of 47
This report shall not t+e reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
:s

Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
/:l lai) /t14G(
``��
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kincey Ave, Suite 100
Hunteraville, NC 28078
��1 a1
Eden,
NC 27288
Asheville, NC 28804
[phone]
[phone]
i(704)875.9092
ANALYTICAL RESULTS
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Sample: TMW-1
Lab ID: 9295688002 Collected: 06/06/11 15:45
Received: 06/07/11 15:33 Matrix: Water
Report
Parameters
Results Units
Limit
MDL OF
Prepared
Analyzed CAS No. Qual
8260 MSV Low Level
Analytical Method: EPA 8260
i
i
Toluene-d8 (S)
96 %
70.130
1
06/09/11 08:14 2037-26I5
Sample: TMW-2
Lab ID: 9295668003 Collected: 06/06/11 16:15
Received: 06/07/11 15:33 Matrix: Water
Report
Parameters
Results Units
Limit
MDL OF
Prepared
Analyzed CAS No. Quaff
6010 MET ICP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
i
i
Arsenic
5.1 ug/L
5.0
2.7 1
06/11/11 12:15
06/14/11 00:29 7440-38& 2
Barium
301 ug/L
5.0
2.5 1
06/11/11 12:15
05/14/11 00:29 1440-39 3
Cadmium
ND ug/L
1.0
0.50 1
06/11/11 12:15
06/14111 00:29 7440-43i-9
Chromium
52.7 ug/L
5.0
2.0 1
06/11/11 12:15
08/14/11 00:29 1440-473
Lead
16.8 ug/L
5.0
4.0 1
06/11/11 12:15
06/14/11 00:29 7439-92-1
778249-2
Selenium
NO ug/L
10.0
5.0 1
06/11/11 12:15
06/14/11 00:29
Silver
NO ug/L
5.0
2.5 1
06/11/11 12:15
06/14/11 00:20 7440-22 4
7470 Mercury
Analytical Method:
EPA7470 Preparation Method: EPA7470
Mercury
NO ug/L
0.20
0.10 1
06/09/11 10:15
06/09/11 15:47 7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method:
EPA 8270 Preparation Method: EPA 3510
Acenaphthene
NO ug/L
10.0
0,25 1
06113/11 1&00
06115111 13:29 83-32-9II
Acenaphthylene
NO ug/L
10.0
0.21 1
2.0 1
06/13/11 15:00
06/13/11 15:00
06/15/11 13:29 208-96-8
06/15/11 13:29 62-,'
Aniline
ND ug/L
10.0
1
Anthracene
ND ug/L
10.0
0,14 1
06/13/11 15:00
06/15/11 13:29 120-12-7
Benzo(a)anthracene
ND ug/L
10.0
0.33 1
06/13/11 15:00
06/15/11 13:29 56-55-3.
Benzo(a)pyrene
NO ug/L
10.0
0.30 1
06/13111 15:00
06/15/11 13:29 50-32-8
Benzo(b)fluoranthene
ND ug/L
10.0
0.28 1
06/13/11 15:00
06/15/11 13:29 205-99.2
Benzo(g,h,i)perylene
ND ug/L
10.0
0.38 1
06/13/11 15:00
06/15/11 13:29 191-24 2
Benzo(k)fluoranthene
ND ug/L
1010
0.43 1
06/13/11 15.00
06/15/11 13:29 207-0819
Benzoic Acid
ND ug/L
50.0
11.5 1
06/13/11 15:00
05/15/11 13:29 65-85-0
Benzyl alcohol
ND ug/L
20.0
2.4 1
06/13l11 15:00
06/15/11 13:29 100-5116
4-Bromophenylphenyl ether
NO ug/L
10.0
0.82 1
06/13111 15:00
06/15/11 13:29 101-5513
Butylbenzylphthalate
NO ug/L
10.0
0.79 1
06/13/11 15:00
06/15/11 13:29 85-68-7
4-Chloro-3-methyiphenol
ND ug/L
20.0
3.7 1
06/13/11 15:00
06/15/11 13:29 59-50-7
4-Chloroaniline
NO ug/L
20.0
2.8 1
06/13/11 15:00
06/15/11 13:29 106-47 8
bis(2-Chloroethoxy)methane
ND ug/L
10.0
0.92 1
06/13/11 15:00
06/16/11 13:29 111-91.1
bis(2-Chloroethyl) ether
NO ug/L
10.0
1.0 1
06/13/11 15:00
06/15/11 13:29 111-44.4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
0.95 1
06/13/11 15:00
06115/11 13:29 108 6011
2-Chloronaphthalene
ND ug/L
10.0
0.98 1
06/13/11 15:00
06/15/11 13:29 91-58-7
2-Chlorophenol
NO ug/L
10.0
1.3 1
06/13/11 15:00
06/15/11 13:29 95-57-8
4-Chlorophenylphenyl ether
ND ug/L
10.0
0.87 1
06/13/11 15:00
05-72 3
06/15/11 13:29 7019
13:29 218-011
Chrysene
ND ug/L
10.0
0.21 1
06/13/11 15:00
06/15/11
Dibenz(a,h)anthracene
ND ug/L
10.0
0.55 1
06/13/11 15:00
06/16111 13:29 53-70-3
Dibenzoturan
ND ug/L
10.0
0.89 1
06113111 15:00
06115/i1 13:29 132-64L9
1,2-Dichlorobenzene
NO ug/L
10.0
0.88 1
06/13/11 15:00
06/15/11 13:29 95-50-1
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
Page 12 of 47
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc
Y M •c0o�0
7�
(SL 30 SE abed)

(Page 39 of 75)
aCeAwlytrcal
»ww.pacelleftoorn
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suits A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
(336)62"921 [phone]
ANALYTICAL RESULTS
Project: BIEDERMANN REALTY 08-7690.2
Pace Analytical Services, Inc,
9800 Klncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Project No.: 9295688
Sample: TMW-2 Lab ID: 9296888003 Collected: 06/06111 16:15 Received: 06/07/11 15:33 Matrix: Water
Report
Parameters Results Units Limit MDL OF Prepared Analyzed CAS No. Qual
8270 MSSV Semivolatile Organic
Analytical Method: EPA8270 Preparation Method: EPA 3510
1,3-Dichlorobenzene
1,4-Dichlorobenzene
NO ug/L
10.0
0.81
1
06/13/11 15:00
06/16/11 13:29
3,3'-Dichiorobenzidine
ND ug/L
NO ug/L
10.0
0.95
1
06/13/11 15:00
06/15/11 13:29
2,4-Dichlorophencl
NO ug/L
20.0
10.0
2.1
1
06/13111 15:00
06/15/11 13:29
Diethylphthalate
ND ug/L
10.0
1.7
0.58
1
06/13/11 15:00
06/15/11 13:29
2,4-Dimethylphenol
NO ug/L
10.0
1
06/13/11 15:00
06/15/11 13:29
Dimethylphthalate
NO ug/L
10.0
1.2
0.76
1
06/13111 15:00
06/15/11 13:29
Di-n-butylphthalate
ND ug/L
10.0
0.75
1
06/13/11 15:00
06/15/11 13:29
4,6-Dinitro 2 methylphenol
ND ug/L
20.0
2.6
1
06/13/11 15:00
06/15/11 13:29
2,4-Dinitrophenol
ND ug/L
50.0
1
06/13/11 15:00
06115/11 13:29
2,4-Dinitrotoluene
NO ug/L
10.0
9.0
0.90
1
06/13/11 15:00
06115/11 13:29
2,6 Dinitrotoluene
ND ug/L
10.0
1
06J13/11 15:00
06l15/11 13:29
Di-n-octylphthalats
NO ug/L
10.0
0.98
0.66
1
06/13/11 15:00
06/15/11 13:29
bis(2-Ethylhexyl)pnthalate
NO ug/L
6.0
0.79
1
06/13/11 15:00
06/15/11 13:29
Fluoranthene
NO ug/L
10.0
1
06/13/11 16:00
06/15/11 13:29
Fluorene
NO ug/L
0.21
1
06/13111 15:00
06/15/11 13:29
Hexachloro-1,3-butadiene
NO ug/L
10.0
0.21
1
06/13/11 15:00
06/15/11 13:29
Hexachlorobenzerte
NO ug/L
10.0
10.0
0.94
1
06/13/11 15:00
06/15/11 13:29
Hexachlorocyclopentadiene
ND ug/L
10.0
0.72
0.88
1
1
06/13/11 15:00
06/15/11 13:29
Hexachloroethane
ND ug/L
10.0
1.1
1
06113111 15:00
06f15111 13:29
Indeno(1,2,3-cd)pyrene
NO ug/L
10.0
0.29
1
06/13/11 15:00
06/15/11 13:29
Isophorone
NO ug/L
10.0
0.89
1
06/13/11 15:00
06/15/11 13:29
1-Methylnaphthalene
ND ug/L
10.0
0.32
1
06/13/11 15:00
06/13/11 15:00
06/15/11 13:29
06/15/11 13:29
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
ND ug/L
10.0
0.28
1
06/13/11 16:00
06/15/11 13:29
3&4-Methylphenol(m&p Cresol)
ND ug/L
NO ug/L
10.0
10.0
1.6
1
06/13/11 15:00
06/15/11 13:29
Naphthalene
NO ug/L
10.0
2.0
0.34
1
06/13/11 15:00
06/15/11 13:29
2-Nitroaniline
NO ug/L
50.0
1
06/13/11 15:00
06/15111 13:29
3-Nitroaniline
NO ug/L
50.0
2.0
2.0
1
06/13/11 15:00
06/15/11 13:29
4-Nitroaniline
ND ug/L
20.0
2.1
1
1
06/13/11 15:00
06/13/11 15:00
06115/11 13:29
06/15/11 13:29
Nitrobenzene
2-Nitrophenol
ND ug/L
10.0
1.1
1
06/13/11 15:00
06/15/11 13:29
4-Nitrophenol
ND ug/L
ND ug/L
10.0
0.91
1
06/13/11 15:00
O6/15/11 13:29
N-Nitrosodimethylamine
NO ug/L
50.0
10.0
4.1
0.91
1
1
06/13/11 15:00
06113/11 15:00
06/15/11 13:29
06/15/11 13:29
N-Nitroso-dl-n-propylamine
ND ug/L
10.0
0.99
1
06/13/11 15:00
06/15/11 13:29
N-Nitrosodiphenylamine
ND ug/L
10.0
1.0
1
06/13/11 15:00
06/15/11 13:29
Pentachlorophenoi
NO ug/L
25.0
4.6
1
06/13/11 15:00
00/15/11 13:29
Phenanthrene
ND ug/L
10.0
0.22
1
06/13/11 15:00
06/15/11 13:29
Phenol
NO ugiL
10.0
1.9
1
06/13/11 16:00
06/15/11 13:29
Pyrene
NO ug/L
10.0
0.19
1
06/13/11 15:00
06/15/11 13:29
1,2,4-Trichlorobenxene
ND ug/L
10.0
0.98
1
06113/1115:00
06115/11 13:29
2,4,5-Trichlorophe/iol
ND ug/L
10.0
0.92
1
06/13/11 16:00
06/16/11 13:29
2,4,6-Trichlorophenol
NO ug/L
10.0
1.3
1
06/13/11 15:00
06/15/11 13:29
Nitrobenzene-d5 (S)
53 %
21-110
1
06/13/11 15:00
06/15/11 13:29
2-Fluorobiphenyl ($)
55 %
27-110
1
06/13/11 15:00
06/15/11 13:29
Terphenyl-dl4 (S)
Be %
31-107
1
06/13/11 15:00
06/15/11 13:29
Date: 06/1612011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in
fun,
without the written consent of Pace Analytical
Services, Inc..
o�e-
641-73-1
106-46-7
91-94-1
120-83-2
84-66-2
106-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39.5
78-59-1
90-12-0
91-57-6
95-48-7
91-20-3
88-7"
99-09-2
100-01.6
98-95-3
88-75-5
100.02-7
62-75-9
621-64-7
86-30.6
87.86-5
85-01-8
108-95-2
129-00-0
120-82-1
95-95-4
M06-2
4165-60-0
321.60-8
1718-51-0
Page 13 of 47

s Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
��acl
Analytiitial 205 East Meadow Road - Suite 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 26804 Huntar*08, NC 28078
wwwpaceftftcom
[phone] [phone] [phone]
i
ANALYTICAL RESULTS
i
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688 1
Sample: TMW-2
Lab ID: 9295688003
Collected: 06/08/11 16.15 Received: 06/07/11 15:33 Matrix: Water
Report
Parameters
Results Units
Limit
MOIL
OF Prepared
Analyzed CAS No,
Qual
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Phenol-d6 (S)
24 %
10-110
1 06/13/11 16:00
06/15/11 13:29 13127-88-3
2-Fluorophenol (S)
33 %
12-110
1 06/13/11 15:00
06/15/11 13:29 367-12-4
214,6-Tribromophenol (S)
82 %
27-110
1 06/13/11 15:00
06/15/11 13:29 118-79.6
8260 MSV Low Level
Analytical Method: EPA
8260
Acetone
5.2J ug/L
25.0
2.2
1
06/09/11 08:40 67-64-1
Benzene
NO ug/L
1.0
0.25
1
06/09/11 08AC 71-43-2
Bromobenzene
NO ug/L
1.0
0.30
1
06/09/11 08:40 108-86-1
Bromochloromethane
ND ug/L
1.0
0.17
1
06/09/11 08:40 74-97-5I
Bromodichloromethane
ND ug/L
1.0
0.18
1
06/09/11 08:40 75-27-41
Bromoform
ND ug/L
1.0
0.26
1
06/09/11 08:40 75-25-21
Bromomethane
ND ug/L
2.0
0.29
1
06/09/11 08:40 74-83-9
2-Butanone (MEK)
ND ug/L
5.0
0.96
1
06/09/11 08:40 78-93-31
Carbon tetrachloride
NO ug/L
1.0
0.25
1
06/09/11 08:40 56-23-5
Chlorobenzene
ND ug/L
1.0
0.23
1
06/09/11 08:40 108-90-
Chloroethane
ND ug1L
1.0
0.54
1
06/09/11 08:40 7"0-3
Chloroform
NO ug/L
1.0
0.14
1
06109/11 08:40 67-66-3
Chloromethane
0.20J ug/L
1.0
0.11
1
06/09/11 08:40 74-87-3
2-Chiorotoluene
ND ug/L
1.0
0.35
1
06/09/11 08:40 95.49-8
4-Chlorotoluene
NO ug/L
1.0
0.31
1
06/09/11 08AO 106A3.4
1,2-Dibromo-3-chloropropane
NO ug/L
5.0
2.5
1
06109/11 08:40 96-12-8
Dibromochloromethane
NO ug/L
1.0
0.21
1
06l09/11 08,40 124-48-1
1,2-Dibromoethane (EDB)
ND ug/L
1.0
0.27
1
06/09/11 08:40 106-9314
Dibromomethane
ND ug/L
1.0
0.21
1
06/09/11 08AO 74-95-3
1,2-Dichlorobenzene
ND ug/L
1.0
0.30
1
06/09111 08:40 95-50-1
1,3-Dichlorobenzene
NO ug/L
1.0
0.24
1
06/09/11 08:40 541-7
1
1,4-Dichlorobenzene
NO ug/L
1.0
0.33
0.21
1
1
06/09/11 08:40 106 461117
06/09/11 08:40 75 711
Dichlorodifluoromethane
ND ug/L
NO ug/L
1.0
1.0
0.32
1
06/09/11 08:40 75-34 3
1,1-Dichloroethane
1,2-Dichloroethane
4.7 ug/L
1.0
0.12
1
06/09/11 08:40 107-06I2
06/09111 08:40 75-35-4
1,1-Dichloroethene
ND ug1L
1.0
1.0
0.56
0.19
1
1
06/09/11 08*40 156-59.2
cis- 1, 2-Dichloroethene
ND ug/L
ND ug/L
1.0
0.49
1
06109/11 08,40 156-60
5
trans-1,2-Dichloroethene
ND ug/L
1.0
0.27
1
06/09/11 08:40 78-87-5
1,2-Dlchloropropane
NO, ug/L
1.0
0.28
1
06/09/11 08'40 142-2819
1,3-Dlchloropropane
ND ug/L
1.0
0.13
1
06/09111 08.40 594 2017
2,2-Diohloropropane
ND ug/L
1.0
0.49
1
06/09/11 08:40 563 58-6
1,1-Dichloropropene
NO ug/L
1.0
0.13
1
06/0911108.40 10061-01-5
cis-1,3-Dichloropropene
ND ug/L
1 0
0.26
1
06/09111 08:40 10081-02-6
trans-1,3-Dichloropropene
Diisopropyl ether
1A ug/L
1.0
0.12
1
06/09111 08:40 108-20-3
Ethylbenzene
ND ug/L
1.0
0.30
1
06/09/11 08:40 100-41-4
06/09/11 08:40 87-68
Hexachloro-1,3-buladiene
ND ug/L
1.0
5.0
0.71
0.46
1
1
06/09/11 08:40 591-7 1-6
2-Hexanone
NO ug/L
NO ug/L
1.0
0.31
1
06/09/11 08:40 99-87
6
p-Isopropyltoluene
ND ug/L
2.0
0.97
1
06l09111 08:40 75-09-2
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
ND ug/L
5.0
0.33
1
06/09/11 08:40 108-1
-1
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shag not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
age 14 of 47
(SL 30 0V abed)

(Page 41 of 75)
V /Ql ifvGl a Pace Analytical Services, Inc. Pace Anatytical Services, Inc. Pace Analytical Services, Inc,
vG 205 5ast Meadow Road - Suite A 2225 Riverside or. 9800 Kincey Ave. Suite 100
"W Pecslabacom Eden, Na 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
ANALYTICAL RESULTS
Project: BIEDERMAN14 REALTY W7690.2
Pace Project No.: 9295688
Sample: TMW-2
Lab ID: 9295688003 Collected: 06/06/11 16:15
Received: 06/07/11 15:33 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
0260 MSV Low Level
Analytical Method:
EPA 8260
Methyl-tert-butyl ether
Naphthalene
163 ug/L
1.0
0.21
1
06/09111 08:40
1634-04.4
Styrene
ND ug/L
1.0
0.24
1
06/09/11 08:40
91-20-3
1, 1, 1,2-Tetrachloroethane
ND ug/L
ND ug/L
1.0
1.0
0.26
1
06/09/11 08:40
100.42-5
1,1,2,2-Tetrachloroethane
ND ug/L
1.0
0.33
0.40
1
1
06/0911108:40
630.20.E
Tetrachloroethene
ND ug/L
1.0
0.46
1
06/09/11 08:40
79-34-5
Toluene
ND ug/L
1.0
0.26
1
06/09/11 08:40
06/0911108:40
127-18-4
108-88.3
1,2,3-Trichlorobenzene
NO ug/L
1.0
0.33
1
06/09/11 08:40
87-61-6
1,2,4-Trichlorobenzene
ND ug1L
1.0
0.35
1
06/0911108:40
120-82-1
1,1,1-Trichloroethane
ND ug/L
1.0
0.48
1
06/09111 08:40
71-55-6
1.1,2-Tdchloroethane
ND uglL
1.0
0.29
1
06/09/11 08:40
79-00-5
Trichloroethene
ND ug/L
1.0
0.47
1
06/09/11 08.40
79-01-6
Trichlorofluoromethane
ND ug/L
1.0
0.20
1
06109/11 08:40
75-69-4
1,2,3-Trfchloropropane
ND ug/L
1.0
0.41
1
06/09/11 08:40
96-184
Vinyl acetate
Vinyl chloride
ND ug/L
2.0
0.35
1
06/09/11 08:40
108-05-4
m8p-Xylene
ND ug/L
1.0
0.62
1
06/09/11 08.40
75-014
o-Xylene
ND ug1L
2.0
0.66
1
06109111 08:40
179601-23-1
4-Sromofluorobenzene (S)
ND ug/L
100 °A
1.0
70-130
0.23
1
1
06/09/11 08:40
95-47-6
Dlbromofluoromethane (S)
103 %
70-130
1
O6/09/11 08:40
06/09/11 08:40
460-00.4
1868-53-7
1,2-Dichioroethane-d4 (S)
99 °%
70-130
1
06/09/11 08:40
17060.07-0
Toluene-d8 (6)
97 °%
90-130
1
06109/11 08:40
2037-26.5
satnpie: TMW-3
Lab ID: 9226688004
Collected: 06/06111 17:30
Received: 06l07/11 16:33 Matrix: water
Report
Parameters
Results Units
Limit
MDL
DF
Prepared
Analyzed
CAS No. Qual
6010 MET ICP
Analytical Method: EPA 601 D Preparation Method: EPA 3010
Arsenic
ND ug/L
5.0
2.7
1
06/11/11 12:15
06/14/11 00:36
7440-38-2
Barium
110 ug/L
5.0
2.5
1
06111/11 12:15
06/14/11 00:36
7440-39-3
Cadmium
ND ug/L
1.0
0.50
1
06/11/11 12:15
06/14/11 00:36
7440-43-9
Chromium
9.7 ug/L
5.0
2.0
1
06/11/11 12:15
06/14/11 00:36
7440.47-3
Lead
ND ug/L
5.0
4.0
1
06/11/11 12:15
06/14/11 00:36
7439-92-1
Selenium
ND ug/L
10.0
5.0
1
06111/11 12:15
06/14/11 00:36
7782-49-2
Silver
ND uglL
5.0
2.5
1
06/11/11 12:15
06/14/11 00:36
7440-22-4
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND ug/L
0.20
0.10
1
06/09/11 10:15
06/09/11 15:49
7439-97-6
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
ND ug/L
10.0
0.26
1
06/13/11 15:00
06/15/11 13:57
83-32-9
Acenaphthylene
ND ug/L
10.0
0.21
1
06/13/11 15:00
06/15/11 13:57
208-96-8
Aniline
ND ug/L
10.0
2.0
1
06/13/11 15:00
06/15/11 13:57
62-53-3
Anthracene
ND ug/L
10.0
0.14
1
06/13/11 16:00
06/15/11 13:57
120-12-7
Date: 0611612011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 15 of 47
This report shall not be reproduced, except In full,
without the writte i consent of Pace Analytical Services, Inc..
c�O�O•
Y�:

IC,
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
(f/tj'' f 205 East Meadow Road - Suite 2225 Riverside Dr.
Mrnt oca Eden, NC 27288 Asheville. NC 28804
[phone] [phone]
ANALYTICAL RESULTS
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Pace AnatyticaI Services, Inc.
9800 KinceyPAvs. Suite 100
HuntersIvllle, NC 28078
[phone]
Sample: TMW-3
Lab ID: 9295688004 Collected: 06/06/11 17:30
Received: 06/07/11 15:33 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
OF
Prepared
Analyzed CAS No. Qual
8270 MSSV Semlvolatiie Organic
Analytical Method: EPA 8270 Preparation Method: EPA 3510
i
i
Benzo(a)anlhracene
NO ug/L
10.0
0.33
1
06/13111 15:00
06115/11 13:57 56-55-3
Benzo(a)pyrene
ND ug/L
10.0
0.30
1
06/13/11 15:00
06/15/11 13:57 50-32-8
Benzo(b)fluoranthene
NO ug/L
10.0
0.28
1
06/13/11 15:00
06/15111 13:57 205-99-2
Benzo(g,h,i)perylene
NO ug/L
10.0
0.38
1
06/13/11 15:00
06/15/11 13:57 191-24-2
Benzo(k)fluoranthene
ND ug/L
10.0
0.43
1
06/13111 15:00
06/15111 13:57 207-08-9
BenzoicAcid
ND ug1L
50.0
11.5
1
06/13/11 15:00
06/16/11 13:57 65-85-0 j
Benzyl alcohol
NO ug/L
20.0
2.4
1
06/13/11 15:00
06/15/11 13:57 100-51-6
4-Bromophenylphenyl ether
NO ug/L
10.0
0.82
1
06113/11 15:00
06115/11 13:67 101-55-3
Butylbenzylphthalate
ND ug/L
10.0
0.79
1
06/13111 15:00
06/15/11 13:57 85-68-7
4-Chloro-3-methylphenol
NO ug/L
20.0
3.7
1
06/13/11 15:00
06/15/11 13:57 59-50-7
4-Chloroaniiine
NO ug/L
20.0
2.8
1
06/13/11 15:00
06/15/11 13:57 106-47-8
bis(2-Chloroethoxy)methane
NO ug/L
10.0
0.92
1
06/13/11 15:00
08/15111 13:57 111-91-1I
bfs(2-Chioroethyl) ether
NO ug/L
10.0
1.0
1
06/13111 15:00
06/15/11 13:67 111-44-4
bis(2-Chloroisopropyl) ether
ND ug/L
10.0
0.95
1
06/13/11 15:00
06/15/11 13:57 108-60-
2-Chioronaphthalene
NO ug/L
10.0
0.98
1
06/13/11 15:00
06/15/11 13:57 91-58-71
2-Chlorophenol
ND ug/L
10.0
1.3
1
o6/13111 15.00
06/15/11 13:57 95-57-8
4-Chlorophenyiphenyl ether
ND uglL
10.0
0.87
1
06113111 15:00
06115/11 13:57 7005-72i 3
Chrysene
NO ug/L
10.0
0.21
1
06113111 15:00
06/15/11 13:57 218-01-
Dibenz(a,h)anthracene
NO ug/L
10.0
0.55
1
06/13/11 15:00
06/15/11 13:57 53-70-31
Dibenzofuran
NO ug/L
10.0
0.89
1
06/13/11 15:00
06/16/11 13:57 132-64-
1,2-Dichlorobenzene
NO ug/L
10.0
0.88
1
06/13/11 15:00
06/15/11 13:57 95-50-1
1,3-Dichlorobenzene
NO ug/L
10.0
0.81
1
06/13/1115:00
06/15/11 13:57 641-73-1
1,4-Dichlorobenzene
ND ug/L
10.0
0.95
1
06/13/11 15:00
06/15/11 13:57 106.46-7
3,3'-Dichlorobenzidine
ND uglL
20.0
2.1
1
06/13/11 15:00
06115/11 13:57 91-94-11
2,4-Dichlorophenol
ND ug/L
10.0
1.7
1
06/13/11 15:00
06/15/11 13:57 120-83-2
Diethylphthalate
ND ug/L
10.0
0.68
1
06/13/11 15:00
06/15/11 13:57 84 66 2�
2,4-Dimethylphenol
ND ug/L
10.0
1.2
1
06113/11 15:00
06115/11 13:57 105 67-
Dimethylphthalate
ND ug/L
10.0
0.76
1
06/13/11 15:00
06/15111 13:57 131-11-3
13:57 84 74-2
Di-n-butylphthalate
ND ug/L
10.0
0.75
1
06/13/11 15:00
06115/11
4,6-Dinitro-2-methylphenol
ND ug/L
20.0
2.6
1
06/13/11 15:00
06115111 13:57 534-52-�1
2,4-Dinitrophenol
ND ug/L
50.0
9.0
1
06/13/11 15:00
06/15/11 13:57 51-28.5,
2,4-Dinitrotoluene
ND ug/L
10.0
0.90
1
06/13/11 15:00
06/15/11 13:57 121-14-
2,6-Dinitrotoluene
NO ug/L
10.0
0.98
1
06/13/11 15:00
06115111 13:67 606-20-i
Di-n-octyiphthalate
ND ug/L
10.0
0.66
1
06/13/11 15:00
06/15/11 13:57 117-84-I0
bis(2-Ethyihexyl)phthaiate
ND ug/L
6.0
0.79
0,21
1
1
06/13111 15:00
06/13/11 15:00
06/15/11 13:57 117-81-7
06/15111 13:57 206.44 0
Fluoranthene
NO ug/L
ND ug/L
10.0
10.0
0.21
1
06/13/11 15:00
06/15/11 13:57 86-73-71I
Fluorene
Hexachloro-1,3-butadiene
ND ug/L
10.0
0.94
1
06/13/11 15:00
06/16/11 13:57 87-68-3
118-7441
Hexachlorobenzene
NO ug/L
10.0
0.72
1
06/13/11 15:00
06115111 1157
Hexachlorocyciopentadiene
ND ug/L
10.0
0,88
1
06/13/11 15:00
06/13/11 15:00
06/15111 13:57 77147
06/15111 13:57 67-72-1
Hexachloroethane
NO ug/L
ND ug/L
10.0
10.0
1.1
0.29
1
1
06/13/11 15:00
06/15/11 13:57 193-3 I19-5
Indeno(1,2,3-cd)pyrene
NO ug/L
10.0
0,89
1
06/13/11 15:00
06/15/11 13:57 78-59-1
Isophorone
1-Methyinaphthalene
NO ug/L
10.0
0.32
1
06/13111 15:00
06115/11 13:57 90 12-b
2-Methylnaphthalene
NO ug/L
10.0
0.28
1
06/13/11 16:00
06/15111 13:57 91-57-e
2-Methylphenol(o-Cresol)
NO ug/L
10.0
1,6
1
06/13/11 15:00
06/15/11 13:57 95-48-
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 16 of 47
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.,
�Cl�s
(SL 40 Zb abed)

(Page 43 of 75)
7
aceArralytical a
Pace Analytical Services, Inc,
205 East Meadow Road
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
- Suite A
2225 Riverside Dr.
9800 Kincey Ave. Suite 10o
wwNprcals com
Eden. NC 27288
Asheville, NC 28804
Hunteraville, NC 28078
[phone]
[phone]
[phone]
ANALYTICAL
RESULTS
Project: BIEDERMANN
REALTY 08-7690.2
Pace Project No.: 9295688
Sample. TN W-3
Lab 10: 9295688004 Collected: 06/06/11 17:30
Received: 06/07111 15:33 Matrix: Water
Report
Parameters
Results Units
Limit
MDL
OF
Prepared
Analyzed
CAS No. Qual
8270 MSSV Semlvolatile Organic
Analytical Method: EPA 8270 Preparation Method: EPA 3510
3&4-Methylphenol(m&p Cresol)
Naphthalene
NO ug/L
10.0
2.0
1
06/13/11 15:00
06/15111 13:57
2-Nitroaniline
NO ug/L
NO ug/L
10.0
0.34
1
06/13/11 15:00
06/15/11 13:57
91-20-3
3-Nitroaniiine
NO ug/L
50.0
2.0
1
06/13/11 15:00
06/15/11 13:57
88-74-4
4-Nitroaniline
NO ug/L
50.0
20.0
2.0
1
06/13/11 15:00
06/15/11 13:57
99-09-2
Nitrobenzene
NO ug/L
10.0
2.1
1
06/13111 15:00
06/15/11 13:57
100-01-6
2-Nitrophenol
ND ug/L
10.0
1.1
1
06/13111 15:00
06/15l11 13:57
98-95 3
4-Nitrophenot
NO ug/L
50.0
0.91
1
06113/11 15:00
06115/11 13:57
88-75-5
N-Nitrosodimethylamine
NO ug/L
10.0
4.1
1
06/13/11 15:00
06115/11 13:57
100-02-7
N-Nitroso-di-n-propylamine
NO ug/L
10.0
0,91
1
06/13/11 15:00
06/15/11 13:57
62-75-9
N-Nitrosodiphenylamine
NO ug/L
10.0
0.99
1
06/13/11 15:00
06/15/11 13:57
621-64-7
Pentachlorophenol
ND ug/L
25.0
1.0
4.6
1
06/13/11 15:00
06/15/11 13:57
86-30-6
Phenanthrene
NO ug/L
10.0
1
06/13/11 15:00
06/15/11 13:57
87-86.5
Phenol
NO ug/L
10.0
0.22
1
06/13/11 15:00
06/16/11 13:57
85-01-8
Pyrene
ND ug/L
10.0
1.9
1
06/13/11 15:00
06/15/11 13:57
108-95-2
1,2,4-Trichlorobenzene
NO ug/L
10.0
0.19
1
06/13/11 15:00
06/15/11 13:57
129-00.0
2,4,5-Trichlorophenol
NO ug/L
10.0
0.98
1
06/13/11 15:00
06/15/11 13:57
120-82-1
2,4,6-Trichlorophenol
ND ug/L
10.0
0.92
1
06/13/11 15:00
06/15/11 13:57
95-95-4
Nitrobenzene-d5 (S)
50 %
1.3
1
06/13/11 15:00
06/15/11 13:57
88-06-2
2-Fluorobiphenyl (S)
49 %
21-110
1
06/13/11 15:00
06/15/11 13:57
4165-60-0
Terphenyl-d14 (S)
74 %
27-110
31-107
1
06/13/11 15:00
06/15/11 13:57
321-60-8
Phenol-d6 (S)
19 %
1
06/13/11 15:00
06/15/11 13:57
1718-51-0
2-Fluorophenol (S)
30 %
10-110
1
05/13/11 15:00
06/15/11 13:57
13127-88-3
2,4,6-Tribromophenol (S)
75 %
12-110
1
06/13/11 15:00
06/15/11 13:57
367-12-4
27-110
1
06/13/11 15:00
06/15/11 13:57
118-79-6
8260 MSV Low Level
Analytical Method: EPA 8260
Acetone
Benzene
3.1J ug/L
25.0 2.2
1
06/09/11 09:05 67-64-1
Bromobenzene
NO ug/L
NO ug/L
1.0 0.25
1.0
1
06/09/11 09:05
71-43-2
Bromochloromethane
NO ug/L
0.30
1.0 0.17
1
1
06/09/11 09:05
108-86-1
Bromodichloromethane
NO ug/L
1.0 0.18
1
06/09/11 09:05
74-97-5
Bromoform
NO ug/L
1.0 0.26
1
06/09/11 09:05
75-27-4
Bromomethane
NO ug/L
2.0 0.29
1
06/09111 09:05
75-25-2
2-Butanone (MEK)
NO ug/L
5.0 0.96
1
06/09/11 09:05
74-83-9
Carbon tetrachloride
NO ug/L
1.0 0.25
1
06/09/11 09:05
78-93-3
Chlorobenzene
NO ug/L
1.0 0.23
1
06/09/11 09:05
W23-5
Chloroethane
NO ug/L
1.0 0.54
1
06/09/11 09:05
108-90-7
Chloroform
NO ug/L
1.0 0.14
1
06/09/11 09:05
06/09/11 09:05
75-00-3
67-66-3
Chloromethane
NO ug/L
1.D 0.11
1
06/09/11 09:05
74-87-3
2-Chlorotoluene
NO ug/L
1.0 0.35
1
06/09/11 09:05
95-49-8
4-Chlorotoluene
NO ug/L
1.0 0.31
1
06/09/11 09:05
106-43-4
1,2-Dibromo-3-chloropropane
ND ug/L
5.0 2.5
1
06/09/11 09:06
96-12-8
Dibromochloromethane
NO ug/L
1.0 0.21
1
06/09/11 09:05
124-48-1
1,2-Dibromoethane (EDB)
NO ug/L
1.0 0.27
1
06/09/11 09:05
106-93-4
Dibromomelhane
NO ug/L
1.0 0.21
1
06/09/11 09:05
74-95-3
1,2-Dichlorobenzene
NO ug/L
1.0 0.30
1
06/09/11 09:05
95-50-1
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
Page 17 of 47
This report shall not be reproduced, except in full,
without the wrlttcn consent of Pace Analytical Services, Inc..

e
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Anstytica11 Services, Inc.
nJt�� f
205 East Meadow Road - Suits A
2225 Riverside Dr.
9800 KlnceyjAve. Suite 100
Eden. NC 27288
Asheville, NC 28804
Huntersvilie, NC 28078
a�wFa`�
I(704)875-9092
[phone]
[phone]
ANALYTICAL RESULTS
I
j
Project: BIEDERMANN
REALTY 08-7690.2
Pace Project No.: 9295688
Sample: TMW-3
Lab ID: 9295688004 Collected: 06/06/11 17:30
Received: 06/07/11 15:33 Matrix: Water
Report
Parameters
Results Units Limit MDL OF
Prepared
Analyzed CAS No. Qual
an
8260 MSV Low Level
Analytical Method: EPA 8260
1,3-Dichlorobenzene
ND ug/L
1,4-Dichlorobenzene
NO ug/L
Dichlorodifluoromethane
ND ug/L
1,1-Dichloroethane
ND ug/L
1,2-Dichloroethane
4.8 ug/L
1,1-Dichloroethene
ND ug/L
cis-1,2-Dichloroethene
NO ug/L
trans-1,2-Dichloroethene
ND ug/L
1,2-Dichloropropane
NO ug/L
1,3-Dichloropropane
NO ug/L
2,2-Dichloropropane
NO ug/L
1,1-Dichloropropene
NO ug/L
cis-1,3-Dichloropropene
NO ug/L
trans-1,3-Dichloropropene
NO ug/L
Dlisopropyl ether
1.5 ug/L
Ethylbenzene
NO ug/L
Hexachloro-1,3-butadiene
NO ug/L
2-Hexanone
NO ug/L
p-Isopropyltoluene
NO ug/L
Methylene Chloride
ND ug/L
4-Methyl-2-pentanone (MIRK)
ND ug/L
Methyl-tert-butyl ether
171 ug/L
Naphthalene
ND ug/L
Styrene
ND ug/L
1,1,1,2-Tetrachloroethane
ND ug/L
1,1,2,2-Tetrachioroethane
NO ug/L
Tetrachloroethene
ND ug/L
Toluene
NO ug/L
1,2,3-Trichlorobenzene
ND ug/L
1,2,4-Trichlorobenzene
ND ug/L
1,1,1-Trichooroethane
NO ug/L
1,1,2-Trichloroethane
NO ug/L
Trichloroethene
NO ug/L
Trichlorofluoromethane
NO ug/L
1,2,3-Trichioropropane
ND ug/L
Vinyl acetate
NO ug/L
Vinyl chloride
NO ug/L
m&p-Xyiene
NO ug/L
o-Xyiene
NO ug/L
4-Bromofluorobenzene (S)
98 %
Dibromofluoromethane (S)
98 %
1,2-Dichloroethane-d4 (S)
97 %
Toluene-d8 (S)
94 %
Date: 06/16/2011 03:13 PM
1.0
0.24
1
06109/1109:05 541-73-
1.0
0.33
1
0610911109:05 106-46-
1.0
0.21
1
06/0911109'05 75-71-8
1.0
0.32
1
06/0911109:05 75-34-3
1.0
0.12
1
06109/1109:05 107-06-
1.0
0.56
1
06/09/1109:05 75-35-4
1.0
0.19
1
06109/1109:05 156-59-
1.0
0.49
1
06109/1109:05 156-60-
1.0
0.27
1
06109/1109:05 78-87-5
1.0
0.28
1
06/0911109:05 142-28-
1.0
0.13
1
0610911109.05 594-20-
1.0
0.49
1
06109/1109:05 563-58-
1.0
0.13
1
0610911109:05 100614
1.0
0.26
1
06/0911109:05 10061-1
1.0
0.12
1
0810911109.05 108-20
1.0
0.30
1
06/09/1109:05 100-41
1.0
0.71
1
06/0911109:05 87-68-i
5.0
0.46
1
05/09/1109:05 591-78
1.0
0.31
1
06/09/1109:05 99-87-(
2.0
0.97
1
06/09/1109:05 75-09-:
5.0
0.33
1
06/09/1109:05 108-10
1.0
0.21
1
06/09/11 09:06 1634-0
1.0
0.24
1
06109/1109:05 91-20-:
1.0
0.26
1
06/09/1109:05 100-42
1.0
0.33
1
0610911109:05 630-20
1.0
0.40
1
06/0911109:05 79-34-1
1.0
0.46
1
06/09/1109:05 127-18
1.0
0.26
1
06JWJ1109:05 108-88
1.0
0.33
1
0610911109:05 87-61-1
1.0
0.35
1
06/09/1109:05 120-82
1.0
0.48
1
0610911109:05 71-55-
1.0
0.29
1
06/09/11 09:05 79-00-
1.0
0.47
1
06/09MI09:05 79-01-
1.0
0.20
1
06/0911109:05 75-69-
1.0
0.41
1
06/0911109:05 96-18-
2.0
0.35
1
06/0911109:05 108-01
1.0
0.62
1
06/0911109:05 75-01-
2.0
0.66
1
0610911109:05 17960
1.0
0.23
1
06/09/1109:05 95-47-
70-130
1
06/0911109:05 460-01
70-130
1
0610911109:05 1868-1
70-130
1
06/09/11 09.05 17060
70-130
1
0610911109.05 20372.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Sefvioes, Inc..
`LL�1
age 18 of 47
(SL 3o V4 abed)

(Page 45 of 75)
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc,
aeel4TiafWimi a 205 East Meadow Ro2d - Suite A 2225 Riverside Dr. 9aDD Kincey Ave. Suite 100
rrwnpece Ihmom Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] (8281254-7176 [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
QC Batch: MPRP/8519 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 9295688001
METHOD BLANK: 618170 Matrix: Solid
Associated Lab Samples: 9295688001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Arsenic
mg/kg
ND
0.50
06/10/1120:42
Barium
mg/kg
ND
0.50
0611011120:42
Cadmium
mg/kg
ND
0.10
06110/1120:42
Chromium
mg/kg
0,0765
0.50
06IWI20:42
Lead
mg/kg
ND
0.60
06110/1120:42
Selenium
mg/kg
ND
1.0
06/10/1120:42
Silver
mg/kg
ND
0.50
06/10/1120:42
t^rsvKAI UK 1.UN I KUL SAMPLE:
Parameter
618171
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
47.7
95
80-120
Barium
mg/k9
50
47.2
94
80-120
Cadmium
mg/kg
50
49.8
100
80-120
Chromium
mg/kg
50
49.9
100
80-120
Lead
mg/kg
50
49.3
99
80-120
Selenium
mg/kg
50
46.2
92
80-120
Silver
mg/kg
25
24.6
98
80-120
MATRIX SPIKE SAMPLE:
618172
9295549001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
mg/kg
2.3
52.9
51.3
93
75-125
Barium
mg/kg
24.1
52.9
83.8
113
75-125
Cadmium
mg/kg
0.20
52,9
50.8
96
75-126
Chromium
mg/kg
14.0
52.9
64.5
96
75-125
Lead
mg/kg
11.6
52,9
59.8
91
75-125
Selenium
mg/kg
1.2
52.9
45.7
84
75-125
Silver
mg/kg
ND
26.4
26.7
101
75-125
SAMPLE DUPLICATE: 618173
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Date: 06/16/2011 03:13 PM
9295549002 Dup
Units Result Result RPD
mg/kg 1.8 1.1 45
mg/kg 5.0 5.0 1
mglkg 0.85 1.2 37
mg/kg 57.2 45.5 23
mg/kg 11.9 12.2 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Max
RPD Qualifiers
20 R1
20
20 R1
20 R1
20
Page 19 of 47

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
e
Malyd al 205 East Meadow Road - Suite A 2225 Riverside Dr.
IeC,
.
smWpacam(ucorrr Eden. NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
i I .
PaceAnalytica I Services, Inc.
9800 KinceyAve. Suite 100
Kunterswlle, NC 28078
[phone]
47
;o 9r abaa)

(Page 47 of 75)
n�ng %/��% e
GGl
Pace Analytical Services, Inc,
Pace Analytical Services, Inc.
U (GL�t1iR[
205 East Meadow Rard - Suite A
2225 Riverside Dr,
mm-psoafeba.com
Eden. NC 27288
Asheville, NC 28604
[phone]
[phone]
QUALITY CONTROL
DATA
i
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
QC Batch: MPRP/8527
Analysis Method:
EPA 6010
QC Batch Method: EPA 3010
Analysis Description:
6010 MET
I Associated Lab Samples: 9295688002, 9295688003, 9295688004
METHOD BLANK: 618926
Matrix: Water
Associated Lab Samples: 92g5688OO2, 929%88003, 9295688004
Blank Reporting
Parameter
Units Result Limit
Analyzed Qualifiers
Arsenic
ug/L
ND
5.0 06/1411100:06
Barium
ug/L
ND
5.0 06/1411100:06
Cadmium
ug1L
ND
1.0 06/14111 MOB
Chromium
ug/L
ND
5.0 06114/1100:06
Lead
ug/L
ND
5.0 06/1411100:06
Selenium
ug/L
ND
10.0 06114/1100:06
Silver
ug/L
ND
5.0 06/1411100:06
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 1o0
Hunteraville, NC 28078
[phone]
UNDUKA I tJKY t;UN I KUL SAMPLE:
618927
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
ug/L
500
489
98
80-120
Barium
ug/L
500
497
99
80-120
Cadmium
ug/L
500
465
93
80-120
Chromium
ug/L
500
465
93
80-120
Lead
ug/L
500
478
96
80-120
Selenium
ug/L
500
484
97
80-120
Silver
ug/L
250
235
94
80.120
MAI KIA SPIKE SAMPLE:
618928
9295688002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Arsenic
ug/L
20.1
500
334
63
75-125 Mo
Barium
ug/L
5040
500
5220
36
75-125 MO
Cadmium
ug/L
37.7
Soo
347
62
75-125 MO
Chromium
ug/L
634
Soo
931
59
75-125 MO
Lead
ug/L
320
500
589
54
75-125 Mo
Selenium
ug/L
14.9
500
302
57
75-125 MO
Silver
uglL
5.0
250
201
78
75-125
SAMPLE DUPLICATE: 618929
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Date: 06/1612011 03:13 PM
9295688003 Dup
Units Result Result RPD
ug/L 5.1 ND
ug/L 301 293 3
ug/L ND ND
ug/L $2.7 50.7 4
U9& 16.8 14.6 14
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written cohsent of Pace Analytical Services, Inc..
Max
RPD Qualifiers
20
20
20
20
20
Page 21 of 47

a
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
9800 Kincey, qve. Suite 100
aCG �a1 �/t�4Rl
205 East Meadow Road - Suite A
2225 Riverside Dr.
Hunters Ale, NC 28078
P scam
Www(336)623-8921
Eden, NC 27288
Asheville, NC 28804
[phone]
[phone]
QUALITY CONTROL DATA
Project: BIEDERMANN
REALTY 08-7590.2
Pace Project No.: 9295688
SAMPLE DUPLICATE: 618929
9295688003 Dup
Max
Parameter
Units Result Result
RPD RPD
Qualifiers
Selenium
ugfL ND ND
20
Silver
ug/L ND ND
20
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 22 of 47
(5L 90 85 abEd)

(Page 49 of 75)
aceAna1 cal
m►» Pece46acom
Pace Analytcat Services, Inc. Pace Analytical services, inc. Pace Analytical Services, Inc.
205 East Meadow Rord - Suite 2225 Riverside Dr. 9800 KinceyAve. Suite too
Eden. Na 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
(704)8759092
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
QC Batch: MERP13541
Analysis Method: EPA7470
QC Batch Method: EPA 7470
Analysis
Description: 7470 Mercury
Associated Lab Samples: 9295688002, 9295688003, 9295688004
METHOD BLANK: 618051
Matrix: Water
Associated Lab Samples: 9295688002, 9295688003, 9295688004
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Mercury ug/L
ND 0.20
06/0911114:32
LABORATORY CONTROL SAMPLE: 618052
Spike
LCS
LCS
% Rec
Parameter Units
Cone.
Result
% Rec
Limits Qualifiers
Mercury ug/L
2.5
2.6
100
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 618053
618054
MS
MSD
9295374002
Spike
Spike MS
MSD
MS MSD % Rec Max
Parameter Units Result
Cone,
Cone. Result
Result
% Rec % Rec Limits RPD RPD Qual
Mercury uglL 0.19J
2.5
2.5 2.0
2.0
74 72 75-125 2 25 MO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 618055
618056
MS
MSD
9295509001
Spike
Spike MS
MSD
MS MSD % Rec Max
Parameter Units Result
Cone.
Cone, Result
Result
% Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND
2.5
2.5 2.4
2.4
95 94 75-125 1 25
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 23 of 47
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalyflcal'
wrra:Fscatrbaeomm
Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100
Eden, NC 27288 Asheville, NC 28804 Hunters I. Ile, NC 28078
[phone] [phone] i704)875-9092
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
QC Batch: MERP13539 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 9295688001
METHOD BLANK: 618041
Matrix: Solid
Associated Lab Samples: 9295688001
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
Mercury
mg/kg
0.00061J 0.0050
06109/1116:35
LABORATORY CONTROL SAMPLE:
618042
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Mercury
mg/kg
.067 0.066
100
80-120
MATRIX SPIKE SAMPLE:
618043
9295733001 Spike
MS
MS % Rec
Parameter
Units
Result Conc.
Result
% Rec Limits
Mercury
mg/kg
0.12 .083
0.15
39 75-125 k
SAMPLE DUPLICATE: 618044
9295733002 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Mercury mglkg 0.0061 0.0027J 20
Date: 06/1612011 03:13 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
y 5
Page 24 of 47
(9L 90 09 abed)

(Page 51 of 75)
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalX cad 205 East Meadow Road - Suite A 2226 Riverside Dr.
rrarepacelabscom Eden. NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
•••• ••••.�, ., vv.1r 1Jove
QC Batch Method: EPA 3546
Analysis Method: EPA 8270
Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 929568800i
METHOD BLANK: 617486 Matrix: Solid
Associated Lab Samples: 9295688001
Parameter
Blank
Units Result
Reporting
Limit
Analyzed Qualifiers
1,2,4-Trichlorobenzene
ug/kg
NO
330
910911112:50
1,2-Dichlorobenzene
uglkg
ND
330
0610911112:50
1,3-Dichlorobenzene
ug/kg
NO
330
W0911112:50
1,4-Dichlorobenzene
ug/kg
NO
330
06/09/11 12:50
1-Methylnaphthalene
ug/kg
NO
330
06/09/11 12:50
2,45-Trfchiorophenol
ug/kg
NO
330
06/09/11 12:50
2,4,6-Trichlorophenoi
uglkg
NO
330
OW0911112:50
2,4-Dichlorophenol
ug/kg
NO
330
06/09/11 12:50
2,4-Dimethylphenol
ug/kg
NO
330
06/0911112:50
2,4-Dinitrophenol
ug/kg
NO
1650
0610911112:50
2,4-Dinitrotoluene
ug/kg
NO
330
06/0911112:50
2,6-Dinitrotoluene
uglkg
NO
330
06109/1112:50
2-Chloronsphthalene
ug/kg
NO
330
06/0911112:50
2-Chlorophenol
ug/kg
ND
330
06/09/11 12:50
2-Methyl naphthalene
ug/kg
NO
330
06109/1112:60
2-Methylphenol(o-Cresol)
ug/kg
NO
330
06/09M112:50
2-Nitroaniline
ug/kg
NO
1650
06/09/11 12:50
2-Nitrophenol
uglkg
ND
330
06/09/11 12:50
3&4-Methylphenol(m&p Cresol)
ug/kg
NO
330
06109/11 12:50
3,3'-Dichlorobenzidine
ug/kg
NO
1650
06109/1112:50
3-Nitroaniline
ug/kg
NO
1650
06/09/11 12:50
4,6-Dinitro-2-methylphenol
ug/kg
NO
660
0610911112:50
4-Bromophenylphenyi ether
ug/kg
NO
330
06M9/11 12:50
4-Chloro-3-methylphenol
ug/kg
NO
660
06/09/11 12:50
4-Chloroaniline
ug/kg
NO
1650
06109/1112:50
4-Chlorophenylphenyl ether
ug/kg
NO
330
06/09/11 12:50
4-Nitroaniline
ug/kg
NO
660
06109/1112:50
4-Nitrophanol
ug/kg
ND
1650
0610911112:50
Acenaphthene
ug/kg
NO
330
06/0911112:60
Acenaphthyiene
uglkg
ND
330
0610911112:50
Aniline
ug/kg
NO
330
06/0911112:50
Anthracene
ug/kg
NO
330
06/09/11 12:50
Benzo(a)anthracene
ug/kg
NO
330
06/0911112:50
Benzo(a)pyrene
ug/kg
ND
330
06/0911112:50
Benzo(b)tluoranthene
uglkg
NO
330
0610911112:50
Benzo(g,h,i)perylene
ug/kg
NO
330
06/09/11 12:50
Benzo(k)fluoranthene
ug/kg
ND
330
06/09/11 12:50
Benzoic Acid
uglkg
NO
1860
06/09/11 12:50
Benzyl alcohol
ug/kg
NO
660
06/09/11 12:50
bis(2-Chloroethoxy)methane
uglkg
NO
330
06109(1112:50
bls(2-Chloroethyl) ether
ug/kg
NO
330
06/09/11 12:50
bis(2-Chloroisopropyl) ether
ug/kg
NO
330
06/09/11 12:50
bIs(2-Ethyihexyl)phthalate
ug/kg
NO
330
06/09/11 12:50
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wdttan colssent of
Pace Analytical Services, Inc..
_ �
r
Pace Ans"cal Services, Inc.
9800 KinoeyAve. Suite too
Huntersville, NC 28070
[phone]
Page 25 at 47

i
e Pace Analytical Services, Inc. Pace Analyticat Services, Ina
eft(Ut! 'ar 205 East Meadow Road - Suite A 2225 Riverside Dr.
wmpeowftcom Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
METHOD BLANK: 617486
Associated Lab Samples:
Parameter
9296688001
Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Butyibenzylphthelate
ug/kg
NO
330
06/09/1112:50
Chrysene
ugikg
NO
330
0610911112:50
Oi-n-butylphthalate
ugikg
NO
330
0610911112:50
Di-n-octylphthalate
ugikg
NO
330
0610911112:50
Dibenz(a,h)anthracene
ug/kg
NO
330
06/0911112:50
Dibenzofuran
ug/kg
NO
330
06/0911112:50
Diethylphthalate
ug/kg
NO
330
W09/11 12:50
Dimethylphthalate
ug/kg
NO
330
06/0911112:50
Fluorenthene
ug/kg
NO
330
06109/1112:50
Fluorene
ug/kg
NO
330
06/0911112:50
Hexachloro-1,3-butadiene
ug/kg
NO
330
06/09/1112:50
Hexachlorobenzene
ug/kg
NO
330
06/09/1112:50
Hexachlorocyclopentadlene
ugikg
NO
330
06/0911112:50
Hexachloroethane
ugikg
ND
330
06109/1112:50
indeno(1,2,3-od)pyrene
ugikg
NO
330
0610911112:50
Isophorone
ugikg
NO
330
06109/1112:50
N-Nitroso-di-n-propylamine
ug/kg
NO
330
06/0911112:50
N-Nitrosodimethytarrine
ug/kg
NO
330
06109/1112:50
N-Nitrosodiphenylamine
ugikg
NO
330
06109/1112:50
Naphthalene
ugikg
NO
330
08/0911112:50
Nitrobenzene
ug/kg
NO
330
06109/1112:50
Pentachlorophenol
ugikg
NO
1650
06109/1112:50
Phenanthrene
ug/kg
NO
330
0610911112:50
Phenol
ugikg
ND
330
06109/il12:60
1kg
NO
330
0610911112:50
2 4,6-Tribromophenol (S)
%ene
52
27-110
06/09/11 12:50
2-Fluorobiphenyl (S)
%
72
30-110
06/09/11 12:50
2-Fluorophenol (S)
%
63
13-110
06/09111 12:50
Nitrobenzene-d5 (S)
%
76
23-110
06/09/11 12:50
Phenol-d6 (S)
%
62
22-110
06/09/11 12:50
TerphenyI-d14 (S)
°%
79
28-110
06109/11 12:50
LABORATORY CONTROL SAMPLE: 617487
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimelhylphenol
2,4-Dinitrophenol
Date: 06/16/2011 03:13 PM
Spike
LCS
LCS
Units
Conc.
Result
% Rec
ugikg
1670
1160
69
ugikg
1670
1070
64
ug/kg
1670
1090
65
ug/kg
1670
1070
64
ugikg
1670
1290
77
ugikg
1670
1060
63
ugikg
1670
1130
68
ug/kg
1670
1270
76
ugikg
1670
1150
69
ug/kg
8330
5260
63
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
ceo,re
Qualifiers
% Rec
Limits
39-101
36-110
35-110
35-110
45-105
48-109
45-111
51-116
42-103
28-103
Pace Ar
9800
Qualifiers
I SerAces, Inc.
Aw. Suite 100
ville, NC 28078
Page 26 of 47
(SL 90 Z5 a62d)

(Page 53 of 75)
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalXical 205 East Meadow Rord - Suite A 2225 Riverside Dr.
e�r+►Pecommoom Eden, NO 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
vMovr%Mrvr« %,W%4tKULZiAMFI-t:
Parameter
517487
Units
Spike
Conc.
LCS
Result
2,4-Dinitrotoluene
ug/kg
1670
1330
2,6-Dinitrotoluene
ug/kg
1670
1270
2-Chloronaphthalene
ug/kg
1670
1090
2-Chlorophenol
ug/kg
1670
979
2-Methylnaphthatene
ug/kg
1670
1230
2-Methylphenol(o-Cresol)
ug/kg
1670
1010
2-Nitroanffine
ug/k9
3330
2730
2-Nitrophenol
ug/kg
1670
1010
3&4-Methylphenol(m&p Cresol)
ug/kg
1670
1040
3,W-Dichlorobenzidine,
ug/kg
3330
2340
3-Nitroanillne
ug/kg
3330
2310
4,6-Dinitro-2-methylphenol
ug/kg
3330
2340
4-Bromophenylphenyt ether
ug/kg
1670
1100
4-Chloro-3-methylphenol
ug/kg
3330
3110
4-Chloroaniline
ug/kg
3330
2260
4-Chlorophenytphenyt ether
ug/kg
1670
1190
4-Nitroaniline
ug/kg
3330
2470
4-Nltrophenol
ug/kg
8330
8170
Acenaphthene
ug/kg
1670
1240
Acenaphthylene
ug/kg
1670
1130
Aniline
ug/kg
1670
912
Anthracene
ug/kg
1670
1330
Senzo(a)anthracene
ug/kg
1670
1310
Benzo(a)pyrene
ug/kg
1670
1220
Benzo(b)fluoranthene
ug/kg
1670
1230
Benzo(g,h,f)perylene
ug/kg
1670
1240
Benzo(k)fluoranthene
ug/kg
1670
1380
Benzoic Acid
ug/kg
8330
3520
Benzyl alcohol
ug/kg
3330
2180
bis(2-Chloroethoxy)methane
ug/kg
1670
1050
bls(2-Chloroethyl) ether
ug/kg
1670
992
bis(2-Chloroisopropyl) ether
ug/kg
1670
896
bis(2-Ethyihexyl)phthaiate
ug/kg
1670
1160
Butylbenzylphthalate
ug/kg
1670
1150
Chrysene
ug/kg
1670
1340
Df-n-butylphthalate
ug/kg
1670
1220
Di-n-octylphlhalate
ug/kg
1670
1110
Dibenz(a,h)anthracene
ug/kg
1670
1230
Dibenzofuran
ug/kg
1670
1240
Diethylphthalate
ug/kg
1670
1320
Dimethylphthalate
ug/kg
1670
1250
Fluoranthene
ug/kg
1670
1460
Fluorene
ug/kg
1670
1300
Hexachlora-1,3-butadlene
ug/kg
1670
1110
Hexachlorobenzene
ug/kg
1670
1190
Hexachlorocyclopentadiene
ug/kg
1670
607
Hexachioroethane
ug/kg
1670
1050
Indeno(1,2,3-cd)pyrene
ug/kg
1670
1260
Date: 06/16(2011 03:13 PM
LCS
% Rea
% Rea
Limits
60 46-114
76 48-112
65 44-105
59 36-110
74 39-112
60 39-101
82 44-111
61 41-100
62 43-103
70 10-150
69 35-110
70 38-118
66 47-115
93 43-127
68 34-109
71 44-115
74 37-111
98 21-152
74 38-117
68 46-107
55 29-110
80 50-110
79 47-116
73 47-106
74 47-109
74 39-115
83 45-117
42 16-110
65 38-105
63 39-110
60 19-119
54 21-110
70 35-116
69 38-110
81 49.110
73 43-109
66 37-109
74 43-116
75 45-106
79 4i-114
75 43-110
88 50-114
78 46-114
67 28-111
71 46-120
36 18-119
63 33-110
76 42-115
REPORT OF LABORATORY ANALYSIS
This report rhal' not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 wncey Ave. Suite 100
Huntersville, NC 28078
Qualifiers
[phone]
Page 27 of 47

Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
Pace Analyttca' Services, Inc.
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kinsey Pve. Suite 100
Eden, NC 27288
Asheville, NC 28804
Hunters iMile, NC 28078
[phone]
[phone]
1VO4)875-9092
QUALITY CONTROL DATA
I
ANN REALTY 08-7690.2
MPLE:
617487
Spike
LCS LCS
°% Rec
Units
Conc. Result % Rec
Limits
Qualifiers
uglkg
1670
1370
82
44-109
ug/kg
1670
1140
69
43-104
uglkg
1670
1050
63
29-110
uglkg
1670
1290
77
48-113
ug/kg
1670
1100
66
41-110
ug/kg
1670
1150
69
38-110
ug/kg
3330
2160
65
32-128
ug/kg
1670
1300
78
50-110
uglkg
1670
1100
66
28-106
ug/kg
1670
1220
73
45-114
%
70
27A10
u%
64
30-110
%
61
13-110
%
72
23-110
o%
60
22-110
y(
71
28-110
j
I
PIKE DUPLICATE: 617489
617490
aceAnalytrcal
anrw4sce ebLoom
Project: BIEDERM
Pace Project No.: 9295688
LABORATORY CONTROL SA
Parameter
Isophorone
N-N itroso-di-n-propylamine
N-Nitrosodimethylamine
N-Nitrosod Iphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2Afr-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
MATRIX SPIKE & MATRIX S
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methyinaphlhalene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimelhylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methyinaphthalene
2-Methylphenol(o-Cresol)
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol(m&p
Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dindro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
MS
MSD
9295694003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD ( RPD
Qual
uglkg
<401
2030
2030
1180
1350
58
67
18-119
13
30
ug/kg
<401
2030
2030
1140
1280
56
63
50-110
11
30
ug/kg
<401
2030
2030
1120
1290
56
64
27-110
14
30
ug/kg
<401
2030
2030
1110
1270
55
63
28-110
14
30
uglkg
<401
2030
2030
1150
1250
57
62
24-116
8
30
ug/kg
<401
2030
2030
1190
1410
59
70
28-110
17
30
UPg
<401
2030
2030
1250
1510
62
75
17-117
19
30
uglkg
<401
2030
2030
1230
1370
61
68
21-128
101
30
ug/kg
<401
2030
2030
1070
1230
53
61
10-120
13
30
uglkg
<2000
10100
10100
3930
5610
39
55
10 107
33�
30 R1
ug/kg
<401
2030
2030
1240
1560
61
77
36-109
23i
30
ug/kg
<401
2030
2030
1210
1530
60
75
32-110
23i
30
ug/kg
<401
2030
2030
1090
1270
54
63
30-107
15
30
ug/kg
<401
2030
2030
1080
1210
53
60
14-106
12
30
ug/kg
<401
2030
2030
1100
1190
54
59
10.135
H
30
uglkg
<401
2030
2030
1010
1130
50
56
10.124
11
30
ug/kg
<2000
4040
4040
19901
2470
49
61
26-116
(
30
uglkg
<401
2030
2030
1180
1350
58
67
28-103
14
30
ug/kg
<401
2030
2030
1020
1140
50
56
10A 09
111
30
uglkg
<2000
4040
4040
2260
2990
56
74
10-150
28
30
uglkg
<2000
4040
4040
2160
2570
53
63
22-110
17
30
uglkg
<801
4040
4040
1880
2560
47
63
13-121
30
30
ug/kg
<401
2030
2030
1050
1310
52
85
31-109
21
30
ug/kg
<801
4040
4040
2340
2600
58
64
13-128
1Q
30
uglkg
<2000
4040
4040
2010
2100
50
52
18-102
5
30
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 28 of 47
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. Inc..
(SL 3o b5 abed)

(Page 55 of 75)
aceAnalytical a Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Nwn.A+taiabtcom Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite Ioo
Hunterevise, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 617489
9295694003
Parameter Units Result
MS
Spike
Cone.
MSD
Spike
Cone.
617490
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
Max
RPD RPD Oual
4-Chlorophenylphenyl ether
4-Nitroaniline
ug/kg
ugikg
<401
<801
2030
2030
1110
1350
55
6.7
29-112
20
30
4-Nitrophenol
ug/kg
<2000
4040
10100
4040
10100
2310
2680
57
66
16-111
15
30
Acenaphthene
ugikg
<401
2030
2030
4970
6180
49
61
14-135
22
30
Acenaphthylene
ug/kg
<401
2030
2030
1140
1140
1340
1340
56
56
66
26-114
16
30
Aniline
ug/kg
<401
2030
2030
831
943
41
66
47
32-108
10-107
16
13
30
30
Anthracene
Benzo(a)anthracene
ugikg
<401
2030
2030
1160
1390
57
69
32-111
18
30
Senze(a)pyrene
ug/kg
ug/kg
<401
<401
2030
2030
1080
1390
53
69
25-117
25
30
Benzo(b)fluoranthene
ug/kg
<401
2030
2030
2030
2030
1030
1030
1330
51
66
25-106
25
30
Benzo(g,h,l)perylene
ugikg
<401
2030
2030
1150
1360
1420
51
57
67
70
24-110
19-112
28
21
30
Benzo(k)ffuoranthene
ug/kg
<401
2030
2030
1020
1330
50
66
24-114
27
30
30
Benzoic Acid
ug/kg
<2000
101100
10100
1670J
15001
16
15
10-110
30
Benzyl alcohol
bis(2-Chloroethoxy)methane
ug/kg
uglkg
<801
<401
4040
4040
2240
2490
55
62
24-106
11
30
bis(2-Chloroethyl) ether
ug/kg
<401
2030
2030
2030
2030
956
1030
1070
47
53
13-119
11
30
bis(2-Chloroisopropyi) ether
ug/kg
<401
2030
2030
961
1170
1070
51
58
10-134
13
30
bis(2-Ethylhexyl)phthalate
ug/kg
<401
2030
2030
999
1300
47
49
53
64
10-113
10-125
11
26
30
30
Butylbenzylphthalate
ug/kg
<401
2030
2030
1130
1450
56
72
18-110
24
30
Chrysene
ugikg
<401
2030
2030
1110
1430
55
71
30-110
25
30
Di-n-buylphthalate
ug/kg
<401
2030
2030
1040
1280
51
63
19-112
21
30
Oi-n-octylphthalate
ug/kg
<401
2030
2030
1290
1600
64
79
17-105
22
30
Dibenz(a,h)anthracene
ugikg
<401
2030
2030
1180
1470
58
73
23-111
22
30
Dibenzofuran
ug/kg
<401
2030
2030
1160
1360
57
67
35-103
16
30
Diethylphthaiate
ug/kg
<401
2030
2030
1100
1370
55
68
27-113
21
30
Dimethylphthalate
ugikg
<401
2030
2030
1110
1380
55
68
26-111
22
30
Fluoranthene
ug/kg
<401
2030
2030
1160
1390
57
68
33-109
18
30
Fluorene
ug/kg
<401
2030
2030
1200
1420
59
70
32-113
16
30
Hexachloro-1,3-butadiene
ug/kg
<401
2030
2030
1200
1370
59
68
16-116
13
30
Hexachlorobenzene
ug/kg
<401
2030
2030
1190
1510
59
75
27-12D
24
30
Hexachlorocyclopentadlene
ug/kg
<401
2030
2030
768
1040
38
51
10-108
30
30
Hexachloroethane
ug/kg
<401
2030
2030
1040
1160
52
57
10-117
11
30
Indeno(1,2,3-cd)pyrene
ugikg
<401
2030
2030
1150
1420
57
70
10-122
21
30
Isophorone
ug/kg
<401
2030
2030
1080
1240
53
61
28-114
14
30
N-Nitroso-di-n-propylamine
ug/kg
<401
2030
2030
1010
1130
50
56
27-113
11
30
N-Nltrosodimethylemine
ugikg
<401
2030
2030
933
1120
46
56
10-109
19
30
N-Nitrosodiphenylamine
ug/kg
<401
2030
2030
1120
1320
55
65
10-128
17
30
Naphthalene
ug/kg
<401
2030
2030
1070
1220
53
60
25-110
13
30
Nitrobenzene
ug/kg
<401
2030
2030
979
1120
48
56
18-114
14
30
Pentachlorophenol
ug/kg
<2000
4040
4040
2100
2940
52
73
10-122
33
30 R1
Phenanthrene
ug/kg
<401
2030
2030
1100
1340
54
66
30-114
20
30
Phenol
ug/kg
<401
2030
2030
1160
1260
57
62
11-102
9
30
Pyrene
ugikg
<401
2030
2030
1090
1480
54
73
25-116
30
30
2,4,6-Tribromophenol (S)
%
60
76
27-110
2-Fluorobiphenyl (S)
%
50
57
30-110
2-Fluoraphenol(S)
%
50
59
13-110
Nitrobenzene-d5 (S)
%
50
55
23-110
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report chat not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 29 of 47

Pace Analytical Services, Inc.
Pace Analytcal Services, Inc.
Pace Analytical
Services, Inc.
aCEA�alytical
205 East Meadow Road - Suits
2226 Riverside Dr.
9800 Kncey
kve. Suite 100
Edan. NC 27288
Asheville, NC 28804
Hunters
ills, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
i
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 617489
617490
j
MS MSD
9295694003 Spike Spike
MS MSD MS MSD
% Rec
Max
Parameter
Units Result Cone. Cone.
Result Result %Rec %Rec
Limits RPD
RPD oual
Phenol-d6 (S) % 49 54
22-110
Terphenyl-d14 (S)
%
53 71
28-110
Date: 06/16/2011 03:13 PM
I
i
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without thewdtien consent of Pace Analytical Services, Inc..
`s
Page 30 of 47
(SL 90 99 abpd)

(Page 57 of 75)
flaPace Analytical Services, Inc. Pace Analytical Services, Inc.
aUP AnalXical ! 205 East Meadow Rord - Suite A 2225 Riverside or.
W++pecs"Loorn Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
,-v r+naiygis Method: EPA8270
QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV
Associated Lab Samples: 9295688002, 9295688003, 9295688004
METHOD BLANK: 619947 Matrix: Water
Associated Lab Samples: 9295688002, 9295688003, 9295688004
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifier;
1,2,4-Trichlorobenzene
uglL
NO
10.0
0611511112:35
1,2-Dichlorobenzene
ug/L
NO
10.0
06/1511112:35
1,3-Dichlorobenzene
ug/L
NO
10.0
0611511112:35
1,4-Dichlorobenzene
ug/L
NO
10.0
0611511112:35
1-Methyinaphthalene
ug/L
NO
10.0
06/15/11 12:35
2,4,5-Tiichlorophenol
ug/L
NO
10.0
06M5/1112:35
2,4,6-Tfichlorophenol
ug/L
NO
10.0
0611511112:35
2,4-Dichlorophenol
ug/L
NO
10.0
06/15/11 12:35
2,4-Dimethylphenol
ug/L
NO
10.0
06/1511112:35
2,4-Dinitrophenol
ug/L
NO
50.0
06/15/11 12:35
2,4-Dinitrotoluene
ug/L
NO
10.0
06/15/11 12:35
2,6-Dinitrotoluene
ug/L
NO
10.0
06115111112:35
2-Chloronaphthalene
ug/L
NO
10.0
0611511112:35
2-Chlorophenol
ug/L
NO
10.0
06/1611112:35
2-Methyinaphthalene
ug/L
ND
10.0
06115[1112:35
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
06/15/11 12:35
2-Nitroaniline
ug/L
NO
50.0
06/1511112:35
2-Nitrophenol
ug/L
NO
10.0
0611511112:35
3&4-Methylphenol(m&p Cresol)
ug/L
NO
10.0
06/15/11 12:35
3,3'-Dichlorobenzidine
ug/L
NO
20.0
06/15/11 12:35
3-Nitroaniline
ug/L
NO
50.0
06/15/11 12:35
4,6-Dinitro-2-methylphenol
ug/L
NO
20.0
06/1511112:35
4-Bromophenylphenyl ether
ug/L
NO
10.0
06/15/11 12:35
4-Chioro-3-methylphenol
ug/L
NO
20.0
06115/1112:35
4-Chloroaniiine
ug/L
ND
20.0
0611611112:35
4-Chiorophenylphenyl ether
ug/L
NO
10.0
06/15111 12:35
4-Nitroaniline
ug/L
NO
20.0
06115/1112:35
4-Nitrophenol
ug/L
NO
50.0
06115/1112:35
Acenaphthene
ug/L
NO
10.0
06/1611112:35
Acenaphthylene
ug/L
NO
10.0
06/1511112:35
Aniline
ug/L
NO
10.0
06/15/11 12:35
Anthracene
ug/L
NO
10.0
06/15/11 12:35
Senzo(a)anthraoene
ug/L
NO
10.0
06/1511112:35
Benzo(a)pyrene
ug/L
NO
10.0
06/15/11 12:35
Benzo(b)fluoranthens
ug/L
ND
10.0
06/15/11 12:35
Benzo(g,h,l)perylene
ug/L
NO
10.0
06/15/11 12:35
Benzo(k)fluoranthene
ug/L
NO
10.0
0611511112:35
Benzoic Acid
ug/L
NO
50.0
06/15/11 12:35
Benzyl alcohol
ug/L
NO
20.0
06/15/11 12:35
bis(2-Ch)oroethoxy)methane
ug1L
NO
10.0
06/'1511112:35
bis(2-ChlorcethyD ether
ug/L
NO
10.0
06/15/11 12:35
bis(2-Chloroisopropyl) ether
ug/L
NO
10.0
06/15/11 12:35
bls(2-Ethylhexyl)phthalate
ug/L
NO
6.0
06115/1112:35
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
w
Pace analytical services, Inc.
9800 KinceyAve. Suite too
Hunteraw7le, NC 28078
[phone]
Page 31 of 47

• Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
aeeAnalytica!
stivwsn Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
METHOD BLANK: 619947
Matrix: Water
Associated Lab Samples:
9296688002, 9295688003, 9295688004
Blank
Reporting
Parameter
Units Result
Limit
Analyzed
Butylbenzylph"ate
ug/L
ND
10.0
W1511112:35
Chrysene
ug/L
ND
10.0
06115/1112:35
Di-n-butylphthalate
ug/L
ND
10.0
06115/1112:35
Di-n-octyiphthalate
ug/L
ND
10.0
0611511112:35
Dibenz(a,h)anthracene
ug/L
ND
10.0
06115/1112:35
Dibenzofuran
ug1L
ND
10.0
0611511112:35
Diethylphthalate
ug/L
ND
10.0
06/15/11 '12:35
Dimethyiphthalate
ug/L
ND
10.0
06/1511112:35
Fluoranthene
ug/L
ND
10.0
06/1511112:35
Fluorene
ug/L
ND
10.0
06/1511112:35
Hexachloro-1,3-butadlene
ug/L
ND
10.0
06/1511112:35
Hexachlorobenzene
ug/L
ND
10.0
0611511112:35
Hexachlorocyclopentadiene
ug/L
ND
10.0
06/15/11 12:35
Hexachloroethane
ug/L
ND
10.0
06115/1112:35
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
0611611112:35
Isophorone
ug/L
ND
10.0
06/1511112:35
N-Nltroso-di-n-propylamine
ug/L
ND
10.0
06/1511112:35
N-Nitmsodimethylamine
ug/L
ND
10.0
06/1511112:35
N-Nitrosodiphenylamine
ug/L
ND
10.0
06/15/11 12:35
Naphthalene
ug/L
ND
10.0
06/15/11 12:35
Nitrobenzene
ug/L
ND
10.0
06/1511112:35
Pentachlorophenol
ug/L
ND
25.0
06116/1112:35
Phenanthrene
ug/L
ND
10.0
0611511112:35
Phenol
ug/L
ND
10.0
0611511112:35
Pyrene
ug/L
ND
10.0
06115/1112:35
2,4,6-Tribromophenol (S)
%
62
27-110
06/15111 12:35
2-Fluombiphenyl (S)
%
41
27-110
06/15/11 12:35
2-Fluorophenol (S)
%
26
12-110
06/15/11 12:35
Nitrobenzene-d5 (S)
%
47
21-110
06/15/11 12:35
Phenol-d6 (S)
%
16
10-110
06/15/11 12:35
Terphenyl-d14 (S)
%
65
31-107
06/15/11 12:35
LABORATORY CONTROL SAMPLE: 619948
Parameter
1,2,4-Trichlorobenzene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
1-Methylnaphthalene
2,4, 5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethyiphenoi
2,4-Dinitrophenol
Date: 06/16/2011 03:13 PM
Spike
LCS
Units
Conc.
Result
ug/L
50
28.6
ug/L
50
24.2
ug/L
50
21.8
ug/L
50
22.9
ug/L
50
30.7
ug/L
50
36.5
ug/L
50
41.8
ug/L
50
36.6
ug/L
50
33.2
ug/L
250
193
Qualifiers
LCS
% Rea
% Rea
Limits
57
10-110
48
10-110
44
10-110
46
10-110
61
21.110
73
23-116
84
21-114
73
22-120
66
15-109
77
10-103
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent
�of Pace Analytical Services, Inc..
Pace Ar
9800
Qualifiers
Services, Inc.
We. suite 100
Mile, NC 28078
[phone]
Page 32 of 47
(SL 90 89 abed)

(Page 59 of 75)
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceAnalXieal 205 East Meadow Road - Suite A 2225 Riverside Dr.
www.pac&%M.com Eden, NG 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
LABORATORY CONTROL SAMPLE: 619948
Pace Analytical Services, Inc.
9800 KlnceyAve. Suite 100
Huntersviils, NC 28078
Parameter
Spike
Units Conc.
LCS LCS
Result % Rec
% Rec
Limits Qualifiers
2,4-Dinitrotoluene
ug/L
50
40.4
81
24-119
2,6-Dinitrotoluene
ug/L
50
41.0
82
25-116
2-Chloronaphihalene
ug/L
50
34,8
70
18-110
2-Chlorophenoi
ug)L
50
33.3
67
10-104
2-Methylnaphthalene
ug/L
50
30.7
61
16-110
2-Methylphenol(o-Cresol)
ug/L
50
28.4
57
13-110
2-Nitroaniline
ug/L
100
83.1
83
20-117
2-Nitrophenol
ug/L
50
35.3
71
16-108
3&4-Methylphenol(m&p Cresol)
ug/L
50
26.4
53
14-110
3,3'-Dichlorobenzidine
ug/L
100
91.8
92
13-131
3-Nitroaniline
ug/L
100
83.6
84
15-117
4,6-Dinitro-2-methylphenol
ug/L
100
84.3
84
13-119
4-Bromophenylphenyl ether
ug/L
50
38.0
76
23-120
4-Chloro-3-methylphenol
ug/L
100
74.1
74
21-119
4-ChloroaniUne
ug/L
100
76.3
76
10-122
4-Chlorophenylphenyl ether
ug/L
50
37.2
74
22-112
4-Nitroaniline
ug/L
100
76.9
77
14-118
4-Nitrophenol
ug/L
250
89.6
36
10-110
Acenaphthene
ug/L
50
34.6
69
20-105
Acenaphthylene
ug/L
5o
33.3
67
23-106
Aniline
Anthracene
ug/L
50
31.7
63
10-110
Benzo(a)anthracene
ug/L
ug/L
50
50
40.9
82
25-12D
Benzo(a)pyrene
uglL
50
42.6
40.4
85
81
21-128
25-116
Benzo(b)fluoranthens
ug/L
50
40.1
80
23-117
Benzo(g,h,i)perylene
ug/L
50
40.5
81
17-128
Benzo(k)fluoranthene
ug/L
50
41.6
83
25-127
Benzoic Acid
ug/L
250
22.3J
9
10-110 L2
Benzyl alcohol
ug/L
100
70.8
71
IG-101
bis(2-Chloroethoxy)methane
ug/L
50
33.0
66
19-107
bis(2-Chloroethyl) ether
ug/L
50
31.9
64
10-108
bis(2-Chlorolsopropyl) ether
ug/L
50
29A
60
10-108
bis(2-E1hy)hexyi)phthalate
ug1L
50
46.6
93
16-123
Butylbenzylphthalate
ug/L
50
41.9
84
20-118
Chrysene
ug/L
50
41.8
84
24-125
Di-n-butylphthalate
ug/L
50
41.3
83
23-115
Di-n-octylphthalate
ug/L
50
46.4
93
20-115
Dibenz(a,h)anthracene
ug/L
50
42.0
84
18-131
Dibenzofuran
ug/L
50
35.8
72
23-106
Diethylphthalate
ug1L
50
37.4
75
24-115
Dimethylphthalate
ug/L
50
39.6
79
22-113
Fluoranthene
ug/L
50
39.7
79
24-125
Fiuorene
ug/L
50
35.6
71
24-114
Hexachloro-1,3-butadiene
ug/L
50
23.7
47
10-110
Hexachlorobenzene
ug/L
50
38.3
77
22-127
Hexachlorocyclopentadiene
ug/L
50
32.8
66
10-110
Hexachloroethane
ug/L
50
19.8
40
10-110
Indeno(1,2,3-cd)pyrene
ug/L
50
41.6
83
18-130
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the writter, consent of Pace Analytical Services, Inc..
[phone]
Page 33 of 47

Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ceMalytical 205 East Meadow Road - Suite A 2225 Riverside Dr.
rrWWPOtabbaa M Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Pace Analytical�Servlces, Inc.
9800 Kincay Ave. Suits 100
Huntersville, NC 28078
LABORATORY CONTROL SAMPLE:
Parameter
619948
Units
Spike LCS LCS
Cone. Result % Rae
% Rec If
Limits Qualifiers
Isophorone
ug/L
50 37.0 74
23-114
N-Nitroso-di-n-propylamine
ug/L
50 35.1 70
21-114
N-Nitrosodimethyiamine
ug/L
50 21.3 43
10110
N-Nitrosodiphenylamine
ug/L
50 39.0 78
24-123
Naphthalene
ug/L
50 29.5 59
14-110
Nitrobenzene
ug/L
50 35.2 70
16-106
Pentachlorophenol
ug/L
100 86.7 87
10-123
Phenanthrene
ug/L
50 38.7 77
25-119
Phenol
ug/L
50 14.5 29
10-110
Pyrene
ug/L
50 37.7 75
22-127
2,4,6-Tribromophenol (S)
%
85
27-110
2-Fluorobiphenyl(S)
%
56
27-110
2-Fluorophenol (8)
%
40
12410
Nitrobenzene-d5 (S)
%
67
21-110
Phenol-d6 (S)
%
27
10-110
Terphenyl-d14 (S)
I
%
76
31-107
I
I
i
I
I
i
I
Date: 06116/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
I
!I
Page 34 of 47
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
(5L 30 09 95ed)

(Page 61 of 75)
l e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
(-,1k6Ant71Xb1205 East Meadow Road - Suite A 2225 Riverside Dr.
WAwpocalsbsoom Eden, NO 27288 Asheville, NO 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
wu tiatcn: MSWI5572 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 9295688002, 9295688003, 92956880D4
nic r nvu OWlvn: bi ititii Matrix: Water
Associated Lab Samples: 9295688002, 9295688003, 9295688004
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ugiL
NO
1.0
06109/1102:19
1,1,1-TOchloroethane
ug/L
NO
1.0
0610911102:19
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/09/1102:19
1,1,2-Tdchloroethane
ug/L
ND
1.0
06/09/1102:19
1,1-Dichloroethane
ug/L
ND
1.0
06/09/1102:19
1,1-Dichloroethene
ug/L
ND
1.0
06/09/1102:19
1,1-Dichloropropene
ug/L
NO
1.0
06/09/1102:19
1,2,3-Trichlorobenzene
ug/L
NO
1.0
06109/1102:19
1,2,3-Trichloropropane
ug/L
ND
1.0
06/09/1102:19
1,2,4-Trichlorobenzene
ug/L
ND
1.0
06109/1102:19
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
06/09/1102:19
1,2-Dlbromoethane (EDB)
ug/L
ND
1.0
06109/11 D2:19
1,2-Dichlorobenzene
ug/L
NO
1.0
06/09/1102:19
1,2-Dichloroethane
ug/L
ND
1.0
06/09/1102:19
1,2-Dichloropropane
ug1L
NO
1.0
06/0911102:19
1,3-Dichlorobenzene
ug/L
NO
1.0
06/0911102:19
1,3-Dichloropropane
ug/L
NO
1.0
06109/1102:19
1,4-Dichiorobenzene
ug/L
NO
1.0
06/09/1102:19
2,2-Dichloropropane
ug1L
NO
1.0
06109/1102:19
2-Butanone (MEK)
ug/L
ND
5.0
06/09/1102:19
2-Chlorotoluene
ug/L
ND
1.0
06/09/1102:19
2-Hexanone
ug/L
ND
5.0
06/09/1102:19
4-Chlorotoluene
ug/L
NO
1.0
06109/1102:19
4-Methyl-2-pentanone (MIRK)
ug/L
NO
5.0
06/09/11 02:19
Acetone
ug/L
NO
25.0
06/0911102:19
Benzene
ug1L
NO
1.0
06/0911102:19
Bromobenzene
ug1L
ND
1.0
0610911102:19
Bromochioromethane
ug/L
ND
1.0
05109/1102:19
Bromodichloromethane
ug1L
ND
1.0
06/09/1102:19
Bromoform
ug/L
ND
1.0
06/09/1102-19
Bromomethane
ug/L
ND
2.0
0610911102:19
Carbon tetrachloride
ug/L
NO
1.0
06/09/1102:19
Chlorobenzene
ug1L
NO
1.0
06/09/1102:19
Chloroethane
ug/L
ND
1.0
06/09/1102:19
Chloroform
ug1L
ND
1.0
06/09/1102:19
Chloromelhane
ug/L
NO
1.0
0610911102:19
cis-1,2-Dichloroethene
ug/L
NO
1.0
06109/1102:19
cis-1,3-Dichloropropane
ugiL
NO
1.0
06/09/1102:19
Dibromochloromethane
ug/L
NO
1.0
06/0911102:19
Dibromomethane
ug/L
ND
1.0
06109/1102:19
DichlorodiNuoromethane
ug1L
NO
1.0
06/0911102:19
Diisopropyl ether
ug/L
ND
1.0
06109/1102:19
Ethylbenzene
ug/L
NO
1.0
06/09/1102:19
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report char not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
":
Pace Analytical Services, Inc.
9800 KmceyAve. Suite 100
Hunterav0le, NC 28078
[phone]
Page 35 of 47

e Pace Analytical Services, Inc. Pace Analytical Services. Inc.
(�55'aeMaOcal 205 East Meadow Road - Suite A 2225 Riverside Dr.
xavw.pecNaba.carr Eden, NC 27288 Asheville, NC 26604
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Pace Analytical Services, Inc.
9800 Kincey�ve. Suite 100
Huntent, ills, NC 28078
METHOD BLANK: 617667
Associated Lab Samples:
Parameter
Matrix: Water
9295688002, 9295688003, 9295688004
Blank Reporting
Units Result Limit
Analyzed Qualifiers
Hexachloro-1,3-butadiene
ug/L
0.74J
1.0
06109/1102:19
m&p-Xylene
ug/L
NO
2.0
06/0911102:19
Methyl-terl-butyl ether
ug/L
NO
1.0
06/09/11 02:19
Methylene Chloride
ug/L
NO
2.0
06/09/11 02:19
Naphthalene
ug/L
NO
1.0
06/09/1102:19
o-Xylene
ug/L
NO
1.0
06/09/1102:19
p-Isopropyltoluene
uglL
NO
1.0
06/09/1102:19
Styrene
ug/L
ND
1.0
06/09/1102:19
Tetrachloroethene
ug/L
ND
1.0
06/09/1102:19
Toluene
ug/L
NO
1.0
06109/1102:19
trans-1,2-Dichloroethene
ug/L
NO
1.0
05109/1102:19
trans-1,3-Dichloropropene
ug/L
NO
1.0
06/0911102:19
Trichloroelhene
ug/L
NO
1.0
06109/1102:19
Tdchlorofluoromethane
ug/L
ND
1.0
06109/1102:19
Vinyl acetate
ug/L
ND
2.0
06109/1102:19
Vinyl chloride
ug/L
NO
1.0
06109/1102:19
1,2-Dichloroethane-d4 (S)
%
99
70-130
06/09/1102:19
4-Bromofluorobenzene (S)
%
98
70-130
06/09111 02:19
Dibromofluoromethane (S)
%
101
70-130
06/09/11 02:19
Toluene-d8 (S)
%
97
70.130
06/09/1102:19
LABORATORY CONTROL SAMPLE:
Parameter
617668
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,11,2-Tetrachloroethane
ug/L
50
57.4
115
70130
1,1,1-Trichloroethane
ug/L
50
53.9
108
70-130
1,1,2,2-Tetrachloroethane
ug/L
5o
59.4
119
70-130
11,2-Trichloroethane
ug1L
50
56.4
113
70A30
1,1-Dichloroethane
ug/L
50
54.5
109
70-130
1,1-Dichloroethene
ug/L
50
55.0
110
70-132
1,1-Dichloropropene
ug/L
50
50.6
101
70-130
1,2,3-Trichlorobenzene
ug/L
50
63.3
107
70-135
1,2,3-Trichloropropane
ug/L
50
58.7
117
70-130
1,2,4-Trichlorobenzene
ug/L
50
54.4
109
70-134
1,2-Dibromo-3-chloropropane
ug/L
50
41.4
83
70-130
1,2-Dibromoethane (EDB)
ug/L
50
58.1
116
70-130
1,2-Dichlorobenzene
ug/L
50
53.2
106
106
70-130
70-130
1,2-Dichloroethane
ug/L
50
52.9
53.0
106
70-130
1,2-Dichloropropane
ug/L
50
50
52.0
104
70-130
1,3-Dichlorobenzene
ug/L
50
53.2
106
70-130
1,3-Dichloropropane
ug/L
50
50.7
101
70-130
1,4-Dichiorobenzene
ug/L
50
44.2
88
58-145
2,2-Dichloropropene
ug/L
100
106
106
70-145
2-Butanone (MEK)
ug/L
50
52.3
105
M130
2-Chiorotoluene
ug/L
Date: 06/0/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced,
except in full,
without the written consent of Pace Analytical Services, Inc..
Y=
Page 36 of 47
(SL 30 Z9 ebea)

(Page 63 of 75)
e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aW nalX cal 205 East Meadow Road - Suite A 2225 Riverside Or.
awe pacaWcom Eden, NO 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
v DUMM 1 UK r I UN r KUL SAMPLE:
Parameter
617668
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits
2-Hexanone
ug/L
00
107
107
70-144
4-Chtorotoluene
ug/L
50
52.6
105
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
108
108
70-140
Acetone
ug/L
100
103
103
50-175
Benzene
ug/L
50
49.7
99
70-130
Bromobenzene
ug/L
50
49.4
99
70-130
Bromochloromethane
ug/L
50
$2.3
105
70-130
Bromodichloromethane
ug/L
50
58.1
116
70-130
Bromoform
ug/L
50
49.6
99
70-130
Bromomethane
ug/L
50
51.9
104
54-130
Carbon tetrachloride
ug/L
50
56.5
113
70-132
Chlorobenzene
ug/L
50
64.5
109
70-130
Chloroethane
ug/L
50
58.1
116
64-134
Chloroform
ug/L
50
64.3
109
70-130
Chloromethane
ug/L
50
49.3
99
64-130
cis-1,2-Dichloroethene
ug/L
50
52.9
106
70-131
cis-1,3-Dichioropropene
ug/L
50
47.0
94
70-130
Dibromochloromethane
ug/L
50
51.8.
104
70-130
Dibromomethane
ug/L
50
56.0
112
70-131
Dichlorodifluoromethane
ug/L
50
52.1
104
56-130
Dlisopropyl ether
ug/L
50
51.6
103
70-130
Ethylbenzene
ug/L
50
54.1
108
70-130
Hexachloro-1,3-butadiene
ug/L
50
53.8
108
70-130
m&p-Xylene
ug/L
100
109
109
70-130
Methyl-tert-butyl ether
ug/L
50
66.9
114
70-130
Methylene Chloride
ug/L
50
50.7
101
63-130
Naphthalene
ug/L
50
51.3
103
70-138
o-Xylene
ug/L
50
57.5
115
70-130
p-Isopropyltoluene
ug/L
50
55.4
111
70-130
Styrene
ug/L
50
53.6
107
70-130
Tetrachloroethene
ug/L
50
56.7
113
70-130
Toluene
ug/L
50
50.6
101
70-130
trans-1,2-Dichloroethene
ug/L
50
53.4
107
70-130
trans- 1, 3-Dichloropropene
ug/L
50
45.0
90
70-132
Trichloroethene
ug1L
50
54.6
109
70-130
Trichlorofluoromethane
ug/L
50
59.4
119
62-133
Vinyl acetate
ug/L
100
84.9
85
66-157
Vinyl chloride
ug/L
50
62.4
125
69-130
1,2-Dichloroethane-d4 (S)
%
95
70-130
4-Bromofluorobenzene (S)
%
106
70-130
Dibromofluoromethane (S)
%
97
70-130
Toluene-d8 (S)
%
101
70-130
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 10o
Huntersville, NC 2807a
[phone]
Qualifiers
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 37 of 47
This report &halt not be reproduced, except in futt,
without the written consent of Pace Analytical Services, Inc..
Y a

Pace AnaWcal Services, Inc.
Pace
Analytical Services, Inc.
Pace Anatytieai:Sarvices, Inc.
aceAnaOcal
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Kinney
Ave. Suite 100
Eden, NC 27288
Asheville, NC 28804
Huntersville,
NC 28078
nww.psoslaWont
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 617669
617670
MS MSD
9295489001
Spike Spike
MS
MSD MS
MSD
% Rae
flax
Parameter
Units
Result
Cone. Cone.
Result
Result % Rae
% Rae
Limits
RPD RPD Qual
1,1-Dichloroethene
ug&
ND
50 50
50.7
49.4 101
99
70166
2 j 30
Benzene
ug/L
ND
50 50
55.0
55.3 110
111
70-148
1 30
Chiorobenzene
u91L
ND
50 50
59.1
58.2 118
116
70-146
2 30
Toluene
ug/L
ND
50 50
62.7
51.0 105
102
70-155
3 30
Trichloroethene
ug/L
ND
50 50
55.5
53.7 111
107
69-151
3 30
1,2-Dichloroethane-d4 (S)
°%
98
97
70-130
4-Bromofluorobenzene(S)
%
101
99
70-130
Dibromofluorometharie (S)
%
99
95
70-130
Toluene-d8 (S)
i
%
91
91
70-130
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 38 of 47
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
(9L 90 b9 abed)

(Page 65 of 75)
• Pace Anatytical Services, Inc. Pace Analytical Services, Inc,
ceAw y kal 205 East Meadow Road - Suite A 2225 Riverside Dr.
wwscpeeat,bmam Eden. NO 27288 Asheville, NO 28804
[phone] [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
QC Batch: MSV/15662 Analysis Method: EPA 8260
QC Balch Method: EPA 8260 Anaiysis Description: 8260 MSV 5035A Volatile Organics
Associated Lab Samples: 9295688001
METHOD BLANK: 620902
Associated Lab Samples: 9295688001
Parameter
Matrix! Solid
Blank Reporting
Units Result Lima
Analyzed Qualifiers
1, 1. 1, 2-Tetrachloroethane
ug/kg
NO
5.0
0611511110:18
1,1,1-Trichloroethane
ug/kg
NO
6.0
06/15/11 10:18
1,1,2,2-Tetrachloroethane
ug/kg
NO
6.0
06/15/11 10:18
1,1,2-Trichloroethane
ug/kg
NO
6.0
06/16/1110:18
1,1-Dichloroethane
ug/kg
NO
5.0
06/1611110:18
1,1-Dichloroethene
ugikg
NO
5.0
06115)1110:18
1, 1 -Dichloropropene
ug/kg
ND
5.0
06115/1110:18
1,2,3-Trichlorobenzene
ug/kg
NO
5.0
06/1511110:18
1.2,3-Trichloropropane
ugikg
NO
5.0
0611611110:18
1,2,4-Trichlorobenzene
ug/kg
NO
5.0
06/15/11 10:18
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
06115/1110:18
1,2-Dibromo-3-chloropropane
ug/kg
NO
5.0
06/15/11 10:18
1,2-Dibromoethane (EDB)
ug/kg
NO
5.0
06/15/11 10:18
1,2-Dlchlorobenzene
ug/kg
NO
5.0
06/1511110:18
1,2-Dichlorcethane
ug/kg
ND
5.0
06115/1110:18
1.2-Dichloropropane
ug/kg
ND
5.0
06115/1110:18
1,3,5-Trimethylbenzene
ugikg
ND
5.0
06M6/1110:18
1,3-Oichiorobenzene
ug/kg
ND
6.0
06115/1110:18
1,3-Dichloropropane
ug/kg
NO
5.0
06/15/11 10:18
1,4-Dichlorobenzene
ug/kg
NO
5.0
0611511110:18
2,2-Dichloropropane
ug/kg
ND
5.0
06115/1110:18
2-Butanone (MEK)
ugikg
NO
100
06/15/11 10:18
2-Chlorotoluene
ug/kg
NO
5.0
06/16/1110:18
2-Hexanone
ug/kg
NO
50.0
06/15/11 10:18
4-Chlorotoluene
ug/kg
NO
5.0
06/15/11 10:18
4-Methyl-2-pentanone (MIRK)
ug/kg
ND
50.0
06/15/11 10:18
Acetone
ug/kg
ND
100
0611511110:18
Benzene
ug/kg
NO
5.0
06/1511110:18
Bromobenzene
ug/kg
ND
5.0
06/i511110:18
Bromochloromethane
ug/kg
NO
5.0
06/1511110:19
Bromodichloromethane
ug/kg
NO
5.0
06/15/11 10:18
Bromoform
ugikg
ND
5.0
0611511110:18
Bromomethane
ug/kg
NO
10.0
06/15/11 10:18
Carbon tetrachloride
ug/kg
ND
5.0
06/15/11 10:18
Chlorobenzene
ug/kg
ND
5.0
06115/1110:18
Chloroethane
ug/kg
ND
10.0
06115/1110:18
Chloroform
ug/kg
ND
5.0
06115/1110:18
Chloromethane
ug/kg
NO
10.0
06/15/11 10:18
cis-1,2-Dichloroethene
ug/kg
NO
5.0
06/1511110:18
cis-1,3-Dichloropropene
ug/kg
ND
5.0
06116/1110:18
Dibromochloromethane
ug/kg
NO
5.0
0611511110:18
Dibromomethane
ugikg
ND
5.0
0611511110:18
Dichlorodifiuoromethane
ug/kg
NO
10.0
06115/1110:18
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shalt not be reproduced, except in full,
without the written consent of Pace Analytical
Services, Inc..
y
Pace Analytical Services, Inc.
9800 KlnoeyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 47

Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
aceMalytical 205 East Meadow Road - Suite 2225 Riverside Dr. 9800 Kinceyl ve. Suite 100
now.psoedebacsm Eden, NC 27288 Asheville, NC 28804 HunteisMile, NC 28078
[phone] [phone] 1(704)875-9092
I
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2 j
Pace Project No.: 9295688
METHOD BLANK: 620902 Matrix: Solid
Associated Lab Samples: 9295688001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
Diisopropyl ether
ug/kg
NO
5.0
06/15/11 10:18
Elhylbenzene
ug/kg
NO
5.0
0611511110:18
Hexachloro-1,3-butadiene
ug/kg
NO
5.0
06/1511110:18
Isopropylbenzene (Cumene)
ug/kg
NO
5.0
06/15/11 10:18
m&p-Xylene
ug/kg
NO
10.0
06/1511110*18
Methyl-tert-butyl ether
ug/kg
NO
5.0
06/15/11 10:18
Methylene Chloride
ug/kg
NO
20.0
06/15/11 10:18
n-Butylbenzene
ug/kg
NO
6.0
06/1511110:18
n-Propylbenzene
ug/kg
NO
5.0
06/15/11 10:18
Naphthalene
ug/kg
NO
5.0
06/15/11 10:18
o-Xylene
ug/kg
NO
5.0
06/1511110:18
p-Isopropyltoluene
ug/kg
NO
5.0
06/1511110:18
sec-Butylbenzene
ug/kg
NO
5.0
06/15/11 10:18
Styrene
ug/kg
NO
5.0
0611511110:18
tert-Butylbenzene
ug/kg
NO
6.0
0611511110:18
Tetrachloroethene
ug/kg
NO
5.0
0611511110:18
Toluene
ug/kg
NO
5.0
06/15/11 10:18
trans-1,2-Dichloroethene
ug/kg
NO
5.0
06/1511110:18
trans-1,3-Dichloropropene
ug/kg
NO
5.0
06/1511110:18
Trichloroethene
ug/kg
NO
5.0
06/15/11 10:18
Trichlorofluoromethane
ug/kg
NO
5.0
06115/1110:18
Vinyl acetate
ug/kg
NO
50.0
06/15/11 10:18
Vinyl chloride
ug/kg
NO
10.0
06/15111 10:18
Xylene (Total)
ug/kg
NO
10.0
06/15/11 10:18
1,2-Dichtoroethane-d4 (S)
%
98
70-132
06/16/11 10:18
4-Bromofluorobenzene (S)
%
96
70-130
06/15/11 10:18
Dibromofluoromethane (S)
%
97
70-130
06115/11 10:18
Toluene-d8 (S)
%
102
70-130
06/15/11 10:18
LABORATORY CONTROL SAMPLE:
Parameter
620903
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
56.1
112
70-131
1,1,1-Trichloroethane
ug/kg
50
52.2
104
70-141
1,1,2,2-Telrachloroethane
ug/kg
50
53.5
107
70-130
1,1,2-Trichloroethane
ug/kg
50
52.0
104
70-132
1,1-Dlchloroethane
ug/kg
50
50.3
101
70-143
1,1-Dichloroelhene
ug/kg
50
49.1
98
70-137
1,1-Dichloropropene
ug/kg
50
49.6
99
70-135
1,2,3-Trichlorobenzene
ug/kg
50
54.8
110
101
69-153
70-130
1,2,3-Tdchloropropane
ug/kg
50
50
50.4
64.7
109
55-171
1,2,4-Tdchlorobenzene
ug/kg
50
54.6
109
70-149
1,2,4-Trimethylbenzene
ug/kg
50
64.7
109
68-141
1,2-Dibromo-3-chloropropane
ug/kg
53.0
106
70.130
1,2-Dibromoethane (EDB)
ug/kg
50
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced,
except in full,
without the written consent of Pace Analytical Services, Inc..
y11��
Page 40 of 47
(SL 30 99 abEg)

(Page 67 of 75)
a
Ana'k
Pace Analytical Servlc$s, Inc.
Pace Analyttcal Services, Inc.
Pace Analytical Services, Inc.
!
205 East Meadow Road - Suite A
2225 Riverside Dr.
9800 Klneey Ave. Suite 100
wwM AecelBbicaom
Eden, NC 27288
Asheville, NC 28804
Huntersvills, NC 28070
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY
08-7690.2
Pace Project No.: 9295688
LABORATORY CONTROL SAMPLE:
620903
Parameter
Spilka LCS
knits Cone. Result
LCS
% Rec
% Rec
Limits
Qualifiers
1,2-Dichlorobenzene
1,2-Dichloroethane
ug/kg
50
53.8
108
70-140
1,2-Dichloropropane
ug/kg
ug/kg
50
49.1
98
70-137
1,3,5-Trimelhylbenzene
ugikg
50
50
52.4
54.5
105
70-133
1,3-Dichlorobenzene
ug/kg
50
53.6
109
70-143
1,3-Dichloropropane
ug/kg
50
52.6
107
70-144
1,4-Dichlorobenzene
ug/kg
50
53.4
105
107
70-132
2,2-Dichloropropane
ug/kg
50
54.2
108
70-142
68-152
2-Butanone (MEK)
2-Chlorotoluene
ug/kg
100
105
105
70-149
2-Hexanone
ug/kg
uglkg
50
100
53.8
108
70-141
4-Chlorotoluene
ug/kg
50
102
56.0
102
70-149
4-Methyl-2-pentanone (MIBK)
ug/kg
100
109
112
70-149
Acetone
ug/kg
100
109
109
109
70-153
70-157
Benzene
Bromobenzene
ug/kg
50
49.0
98
70-130
Bromochloromethane
ug/kg
ugikg
50
52.2
104
70-141
Bromodlchloromethane
ug/kg
50
50
49.6
99
70-149
Bromoform
ug/kg
5o
54.6
50.0
109
100
70-130
70-131
Bromomethane
Carbon tetrachloride
ug/kg
50
54.8
110
64-136
Chlorobenzene
ugikg
ug/kg
50
50
54.4
109
70-154
Chloroethane
ug/kg
50
53.0
57.9
106
70-135
Chloroform
ug/kg
50
52.3
116
105
68-151
70-130
Chloromethane
ugikg
5o
48.8
98
70-132
Cis- 1,2-Dichloroethene
ug/kg
50
49.4
99
70-140
cis- 1,3-Dichloropropane
ugikg
50
55.3
111
70-137
Dibromochloromethane
ug/kg
50
49.9
100
70-130
Dibromomethane
ug/kg
50
53.4
107
70-136
Dichlorodifluoromethane
ug/kg
50
49.4
99
36-148
Dilsopropyl ether
ug/kg
50
60.7
101
70-139
Ethylbenzene
ugikg
50
51.8
104
70-137
Hexachloro-1,3-butadiene
ug/kg
50
53.2
106
70-145
Isopropylbenzene (Cumene)
ug/kg
50
53.6
107
70-141
m&p-Xylene
ug/kg
00
106
106
70-140
Methyl-tert-butyl ether
ug/kg
50
50.6
101
45-150
Methylene Chloride
ug/kg
50
49.4
99
70-133
n-Butylbenzene
ugikg
50
56.7
113
65-155
n-Propylbenzene
ug/kg
50
55.8
112
70-148
Naphthalene
ug/kg
50
57.5
115
70-148
o-Xylene
ug/kg
50
52.1
104
70-141
p-Isopropyltoluene
ugikg
50
65.8
112
70-148
sec-Butylbenzene
ug/kg
50
55.1
110
70-145
Styrene
ugikg
50
55.3
111
70-138
tert-Butylbenzene
ugikg
50
54.8
110
70-143
Tetrachloroethene
ug/kg
5o
53.2
106
70-140
Toluene
ug/kg
5o
50.3
101
70-130
trans-1,2-0ichloroethene
ug/kg
50
49.4
99
70-136
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY
ANALYSIS
Page 41 of 47
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc

a
Pace Analytical Services, Inc,
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
e!lr iyfida
205 East Meadow
Road - Suite A
2225 Riverside
Dr.
9800 KinceyIAve. Suite 100
r
wMNavV4w1
Eden, NC 27288
Asheville, NC 28804
Huntersvllle, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
LABORATORY CONTROL SAMPLE:
620903
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
trans- 1, 3-Dichloropropene
ug/kg
50
60.5
101
70-138
Trichloroethene
ug/kg
50
52.3
105
70-132
Trichlorofluoromethane
ug/kg
50
47.9
96
69-134
Vinyl acetate
ug/kg
100
104
104
24-161
Vinyl chloride
ug/kg
50
51.5
103
55-140
Xylene (Total)
ug/kg
150
158
105
70-141
1,2-Dichloroethane-d4 (S)
%
95
70-132
4-Bromofluorobenzene(S)
%
97
70-130
Dibromofluoromethane (S)
%
100
70-130
Toluene-d8 (S)
%
101
70-130
MATRIX SPIKE SAMPLE:
621108
9295638024
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1, 1 -Dichloroethene
uglkg
NO
47.4
50.2
106
49-180
Benzene
ug/kg
ND
47.4
54.0
114
50-166
Chlorobenzene
ug/kg
NO
47.4
55.6
117
43-169
Toluene
ug/kg
NO
47.4
57.8
122
52-163
Trichloroethene
ug/kg
NO
47.4
52.1
110
49-167
1,2-Dichloroethane-d4 (S)
%
93
70-132
4-Bromofluorobenzene (S)
%
94
70-130
Dibromofluoromethane (S)
%
90
70-130
Toluene-d8 (S)
96
104
70-130
ac
SAMPLE DUPLICATE: 621107
Parameter
Units
9296174001 Dup
Result Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachioroethane
ug/kg
ND
30
1,1,1-Trichloroethane
ug/kg
NO ND
1,1,2,2-Tetrachloroethane
ug/kg
ND ND
30
1,1,2-Trichloroethane
uglkg
NO ND
30
30
1,1-Dichloroethene
ug/kg
NO NO
30
1,1-Dichloroethene
ug/kg
NO NO
1,1-Dichloropropene
ug/kg
ND
30
1,2,3-Trichiorobenzene
uglkg
ND NO
1,2,3-Trichloropropane
ug/kg
ND
30
12,4-Trichlorobenzene
ug/kg
NO ND
1,2,4-Trimethyibenzene
ug/kg
ND
30
1,2-Dibromo-3-chloropropane
ug/kg
NO ND
30
1,2-Dibromoethane (EDB)
ug/kg
NO ND
30
1,2-Dichlorobenzene
ug/kg
ND ND
30
1,2-Dichloroelhane
ug/kg
NO ND
30
1,2-Dichloropropane
ug/kg
NO ND
1,3,5-Trimethylbenzene
ug/kg
ND
30
1,3-Dichlorobenzene
ug/kg
NO ND
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
AC.O.n.
Page 42 of 47
(5L 90 29 abed)

(Page 69 of 75)
/1(!a'!{vGe(e P7ee Analytical Services, Inc. Pace Analytical Services, Inc,
205 East Meadow Road - Suite A 2225 Riverside Dr.
mmpscefabitoom Eden, NC 27288 Asheville, NC 28004
($36)623.8921 [phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE DUPLICATE: 621107
9296174.001 Dup
Max
I
Parameter
Units Resu'.t Result
RPD RPD
Qualifiers j
1,3-Dichloropropane
ug/k 9
ND
1,4-Dichlorobenzene
ug/kg
NO
ND
30
i
2,2-Dichloropropane
ug/kg
ND
2-Butanone (MEK)
uglkg
NO
NO
30
2-Chlorotoluene
ug/kg
ND
2-Hexanone
ug/kg
ND
NO
30
4-Chlorotoluene
ug/kg
ND
4-Methyl-2-pentanone (MIRK)
ug/kg
ND
ND
30
Acetone
uglkg
NO
ND
30
Benzene
ug/kg
NO
ND
30
Bromobenzene
ug/kg
NO
Bromochloromethane
uglkg
NO
ND
30
Bromodichloromethane
ug/kg
NO
ND
30
Bromoform
ug/kg
ND
ND
30
Bromomethane
uglkg
ND
ND
30
Carbon tetrachloride
uglkg
ND
NO
30
Chlorobenzene
ug/kg
ND
ND
30
Chloroethane
ug/kg
ND
ND
30
Chloroform
ug/kg
ND
ND
30
Chloromethane
ug/kg
ND
NO
30
cis-1,2-Dichloroethene
ug/kg
ND
ND
30
cis-1,3-Dichloropropene
ug/kg
NO,
ND
30
Dibromochloromethane
ug/kg
NO
NO
30
Dibromomethane
ug/kg
ND
Dichlorodifiuoromethane
ug/kg
ND
ND
30
Diisopropyl ether
uglkg
ND
Ethylbenzene
uglkg
NO
ND
30
Hexachloro-1,3-butadiene
ug/kg
NO
isopropylbenzene (Cumene)
ug/kg
ND
ND
30
m&p-Xytene
ug/kg
ND
ND
30
Methyl -ten -butyl ether
ug/kg
ND
NO
30
Methylene Chloride
ug/kg
NO
ND
30
n-Butylbenzene
uglkg
ND
n-Propylbenzene
uglkg
NO
Naphthalene
ug/kg
NO
o-Xylene
uglkg
ND
ND
30
p-isopropyltoiuene
ug/kg
ND
sec-Butylbenzene
ug/kg
ND
Styrene
ug/kg
NO
ND
30
tert-Butylbenzene
ug/kg
ND
Tetrachioroethene
ug/kg
ND
ND
30
Toluene
ug/kg
ND
NO
30
trans-1,2-Dichloroethene
ug/kg
ND
NO
30
trans- 1, 3-Dichloropropene
ug/kg
ND
ND
30
Trichloroethene
ug/kg
ND
ND
30
Trichicrofluoromethane
ug/kg
NO
ND
30
Vinyl acetate
ug/kg
NO
Vinyl chloride
ug/kg
ND
NO
30
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
Page 43 of 47 li
This report shall not be reproduced,
except In full,
without the written consent of Pace Analytical Services, Inc..

e Pace Analytical Services, Inc. Pace Anatyticat Services, Inc,
aceAnalytical 205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
m►w.Psahbaoom
[phone] [phone]
I
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
I Pace Project No.: 9295688
i
Pace Analytic* Services, Inc.
9800 KinceylAve. Suite 100
Hunteraville, NC 28078
(7o4)575-9092
i
SAMPLE DUPLICATE: 621107
9296174001
Dup
Max
Parameter
Units
Result
Result
RPD RPD Qualifiers
Xylene (Total)
ug/kg
ND
1,2-Dichloroethane-d4 (S)
%
88
95
3
4-Bromofluorobenzene(S)
%
92
95
1
Dibromofluoromethane (S)
%
91
101
7
Toluene-d8 (S)
%
99
99
4
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Ap�4
Page 44 of 47
(SL 30 OL abed)

(Page 71 of 75)
i
e
aeeAnatyl m1
Pace Analytical Servicos, Inc.
205 East Meadow Road Suite A
Pace Analytical ServIC6e, Inc.
Pace Analytical Services, Inc.
-
2225 Riverside Dr.
9800 Kinsey Ave. Suite 100
W#+t>acalBimcom
Eden, NO 272a8
Asheville, NC 26804
kuntersville, NC 28078
[phone]
[phone]
[phone]
QUALITY CONTROL DATA
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
QC Batch: PMST/3976
Analysis Method:
ASTM D2974-87
QC Batch Method: ASTM D2974-87
Analysis Description:
Dry Might/Percent Moisture
Associated tab Samples: 929566MI
SAMPLE DUPLICATE: 617984
I
9295733001 Dup
Max
Parameter
Units Result Result
RPD RPD
Quallfiers
Percent Moisture 96
19.5
18.4 6 25
SAMPLE DUPLICATE: 617985
0295714011 Dup
Max
1
Parameter
Units Result Result
RPD RPD
Qualifiers
Percent Moisture %
9.8
9.4 4 25
I
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 45 of 47
This report that not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
aee„e

e Pace Analytical Services, Inc. Pace Analytical Services, Inc.
lac,
MaOca! 206 East Meadow Road - Suite A 2226 Riverside Dr.
Warwpacabacom Eden, NO 27268 Asheville, NO 28804
[phone] [phone]
QUALIFIERS
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
DEFINITIONS
Pace Analytical; services. Inc.
9800 Kincey IAIve. Suite 100
Huntersir8le. NO 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited anatytes.
LABORATORIES
PAST -A Pace Analytical Services - Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this anWe in associated
samples may be biased low.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
R1 RPD value was outside control limits.
Date: 06/16/2011 03:13 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 46 of 47
(5L 30 ZL abed)

(Page 73 of 75)
UU17 lytical'
*wrpaasta wm
Pace Ane"cal Services, Inc.
205 East Meadow Rord - Suite A
Eden. NO 27288
[phone]
Pace Analyticat Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: BIEDERMANN REALTY 08-7690.2
Pace Project No.: 9295688
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntereville, NC 28078
[phone]
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
9295688001
5-2-23
EPA 3050
MPRP18519
EPA 6010
ICP17876
9295688002
TMW-1
EPA3010
MPRP/8527
EPA6010
ICP/7863
929568SW3
TMW-2
EPA3010
MPRP18527
EPA6010
ICP/7883
9295688004
TMW-3
EPA3010
MPRP/8527
EPA6010
ICP/7883
9295688002
TMW-1
EPA 7470
MERP13541
EPA 7470
MERC/3490
9295688003
TMW-2
EPA 7470
MERP13541
EPA 7470
MERC/3490
9295688004
TMW-3
EPA 7470
MERP/3541
EPA 7470
MERC/3490
9295688001
S-2.23
EPA7471
MERP/3539
EPA7471
MERC/3491
9295688001
S-2-23
EPA3546
0EXT/13852
EPA8270
MSSV/5032
9295688002
TMW-1
EPA 3510
0EXT/13900
EPA 8270
MSSVI5049
9296688003
TMW-2
EPA 3510
OEXT/13900
EPA 8270
MSSV15049
9295688004
TMW-3
EPA 3510
0EXT/13900
EPA 8270
MSSV/5049
9295688002
TMW-1
EPA 8260
MSW15572
9295688003
TMW-2
EPA 8260
MSV/15572
9295688004
TMW-3
EPA 8260
MSV/15572
9295688001
S-2-23
EPA 8260
MSV115662
9295688001
S-2-23
ASTM D2974-87
PMST/3976
Date: 06/16/2011 03:13 PM REPORT OF LABORATORY ANALYSIS Page 47 of 47
This report sha)I not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

Z)!Z�Ilao
Ra4aMd Cleru InWnubw:
I
CHAIN -OF -CUSTODY l Analytical Request Document
The Chabt *Custody is a LEGAL DOCUMENT, AN rWavwd Nelds moat be completed arxxlrab*.
Pape. 1 of
SeCNoa C e
----------------- Invaloe Irdarrnew : ---- -- --- --
raw, ea.nrlrror,,.u,, WTRZ C DE I
Drinkbrp waver OW
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COLLECTED
z
water WT
W b Wabr vw
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v
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a
ME
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SAMPLE ID Olt m
VV" WP
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(A-Z, 0-01; ! Air AR
p
w
I
Semple Ds MUST BE UNIQUE T"w TS
U
2
Dow07
X
U
!
a
a.
LL
C
DATE
TIME
GATE
TIME
I
ft
3523-7
Preservatives
S
19
SA1WLER NMIE AND SIGNATURE
ORIGINAL mtwNa1,.OfNA wm: VA 11
SIGNATURE d l
.k%Wbnt Nob: By slgn4V tlb loan yeu era accepUn Pace's NET 30 d" pryrn t time and ,0rae'r9 b rats awpes of 1.5% W MM1l1 for eny Wv0b s nor paid Wihn 30 days.
1473919
W--GULATOW MW CY
r NF'DES I"- GROUND WATER r DRINKING WATER
r UST (— RCRA i OTHER
t> w Locetbn , _ —
i>
utaly�Its Pilbiratl (Yfl�'
0
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U
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I W H
F-ALL-0-020rev.07, 15-WY-2D07

(Page 75 of 75)
ConditionSample p•Receipt
r �aceArlalyt/ial' .
Client Name: V ri wD Project # G2.95& rvT
Where Received: Huntersville ❑ Asheville ❑ Eden
Courier: ❑ Fed Ex ❑ UPS ❑ USPS ❑ Client ❑ Commercial Pace Other O' 't%naG:rx=
:.
Custody Seal on Cooler/Box Present: ❑ yss ,ETno Seals intact Elyes ❑ no fro]4�u':De
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None ❑Other
Thermometer Used: IR Gun : T1101 Type of lce: -a Blue None ATSamples on ice, cooling process has begun
Temp Correction Factor: Add / Subtract 0 •C
Corrected Looter Te C
Biolo (cal Tissue Is Frozen: Yes No
g
Date nd I Is pe
examining
Temp should be above fresh g 6-C
Comments:
con
Chain of Custody Present:
❑Yes I_No
❑WA
1.
Chain of Custody Filled Out:
Yes CNo
❑NIA
2.
Chain of Custody Relinquished:
es CNo
❑NIA
3.
Sampter Name & Signature on COC:
Yes ON,
❑NIA
4.
Sam les Arrived within Hold Time:
es ONO
❑NrA
5.
Short Hold Time Analysis <72hr :
OYe9'*6No
❑NIA
e,
Rush Turn Around Time Requested:
Oyes No
❑NIA
7,
Sufficient Volume:
Y s ONo
❑N/A
8.
Correct Containers Used:
❑Ye/Yeas [:]No
❑N/A
g,
-Pace Containers Used:
'DYes ONO
❑NIA
Containers Intact
es ❑No
❑NIA
10.
Filtered volume received for Dissolved tests
Oyes ONo
OM<
11.
Sample Labels match COC:
❑y ONO
❑N/A
12.
-Includes date/time/10/Anal sis Matrix:
All containers needing,preservation have been checked.
Yes ONO
OWA
13.
All Containers needing preservation are found to be in
compliance wHh EPA recommendation.
Yes []No
ON/A
exceptions: VOA, colfform, TOC, O&G, WI-DRO (water)
❑Yes ONO
N
Inival 4eA completed
Samples checked for dechlorination:
Dyes u<
r
Headspaee in VOA Vials >6mm :
Oyes CV1
15
Trip Blank Present:
Oyes ❑No
0
16.
Trip Blank Custody Seals Present
❑Yes ONO
❑N/A
Pace Trip Blank Lot # if purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted: Date/Time;
Comments/ Resolution:
SCURF Review: `a t.r-f Data: � 9 r I SRF Review: I —Zr" K Date: I G 7 I
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, Incorrect preservative, out of temp. Incorrect containers)
F-CH R-CS-003-rev.0313Apr2011