MO-88903_96932_CA_LSA_20230509

Phase I Limited Site Assessment

Former Atlantic Coast Fire Truck Facility
4718 Mountain Creek Avenue, Suite B
Denver, North Carolina

DEQ Incident No. 96932
H&H Job No. ACF-001
May 9, 2023

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Table of Contents

Section Page No.
1.0 Executive Summary and Recommendations ........................................................................1 
2.0 Introduction and Site History ................................................................................................4 
3.0 Receptor Information and Risk Characterization ...............................................................6 
3.1 Receptor Information .............................................................................................................6 
3.1.1 Water Supply Wells ........................................................................................................6 
3.1.2 Surface Water ..................................................................................................................6 
3.1.3 Subsurface Structures ......................................................................................................7 
3.1.4 Property Owners and Land Use ......................................................................................7 
3.1.5 Wellhead Protection Areas ...............................................................................................7 
3.2 Risk and Land Use Characterization .....................................................................................7 
4.0 Geology and Hydrogeology ....................................................................................................8 
4.1 Regional Geology and Hydrogeology ...................................................................................8 
4.2 Site Hydrogeology .................................................................................................................8 
5.0 Soil and Groundwater Sampling ...........................................................................................9 
5.1 Soil and Groundwater Assessment Activities .......................................................................9 
5.2 Soil and Groundwater Analytical Results ...........................................................................11 
6.0 Summary and Recommendations ........................................................................................13 

List of Tables

Table 1 Summary of Phase I LSA Soil Sample Results
Table 2 Summary of Phase I LSA Temporary Monitoring Well Construction
Table 3 Summary of Phase I LSA Groundwater Sample Results
Table 4 Summary of Phase I LSA Groundwater Sample Results - TICs

List of Figures

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Sample Location Map
Figure 4 Receptor Survey Map

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List of Appendices

Appendix A Risk Classification and Land Use Form
Appendix B Boring Log and Well Completion and Abandonment Records
Appendix C Laboratory Analytical Reports and Low-Flow Form
Appendix D Prior Assessment Results
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Phase I Limited Site Assessment
Former Atlantic Coast Fire Trucks Facility
Denver, North Carolina
H&H Job No. ACF-001

1.0 Executive Summary and Recommendations

This Phase I Limited Site Assessment (LSA) report describes assessment activities related to a
surficial (non-UST) release of petroleum at the former Atlantic Coast Fire Truck (ACFT) facility
located at 4718 Mountain Creek Avenue Suite B in Denver, Catawba County, North Carolina
(Site). The Site is approximately 1.04 acres in area and contains an approximately 8,750 ft2
commercial warehouse that is split into two separate tenant suites. ACTF reportedly operated
out of Suite B from approximately 2015 to 2020. ACTF operations included servicing and
maintenance of firetrucks and other related first responder vehicles.

In March 2022, Highland Environmental Solutions, Inc. (HES) was contracted by the property
owner to conduct assessment in areas of apparent staining observed on the interior concrete slab
and exterior gravel area of the ACTF facility. In response, ACTF contracted with Civil &
Environmental Consultants, Inc. (CEC) to confirm the results of HES’s assessment. HES’s and
CEC’s assessment generally included the collection of soil samples from multiple interior and
exterior locations in areas of apparent staining. Following CEC’s assessment, a second
“supplemental” assessment was conducted by HES at the request of the property owner. The
supplemental assessment activities conducted by HES included the removal of an approximate 1
ft by 1ft section of interior concrete slab, inspection and laboratory testing of the vapor barrier
below the removed portion of the slab, and the collection of soil samples from below the vapor
barrier. In summary, results of HES’s and CEC’s assessment activities indicated the presence of
total petroleum hydrocarbons diesel range organics (TPH-DRO) above the North Carolina
Department of Environmental Quality (NCDEQ) UST Action Level of 100 mg/kg in two (2)
sample locations ranging from 299.7 mg/kg to 1,300 mg/kg.

Based on the presence of TPH-DRO above action levels, the North Carolina Department of
Environmental Quality (DEQ) requested that ACTF conduct a Limited Site Assessment (LSA) in
a letter dated January 30, 2023.
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At the request of ACTF, H&H conducted a Phase I LSA at the Site in April 2023. The Phase I
LSA included the installation of one combination soil boring/temporary monitoring well in
previous sample location S-7/CEC-A1/CEC-A2 which indicated the highest concentration of
TPH-DRO detected during HES's and CEC’s prior assessments.

Land Use/Risk Characterization
As part of the LSA activities, H&H performed a site land use and risk characterization survey. The
land use/risk classification survey included a water-supply well receptor survey within a 1,500 ft
radius of the Site. H&H identified one potential WSW located approximately 1,300 ft
topographically upgradient/cross gradient to the Site. No other WSWs were identified and
remaining properties appear to have municipal water connections. According to the United States
Geological Survey (USGS) topographic map dated 2022, no surface water bodies are located
within 500 feet of the source area.

The zoning of the site is Planned Development (PD). The properties in the surrounding area are
primarily zoned as PD, Highway Commercial (HC), Residential (R-20), and Residential (R-40).
The nearest residentially zoned property is located approximately 500 ft north-northwest and
topographically upgradient of the source area.

Phase I LSA Sampling
On April 12, 2022, H&H oversaw the advancement of LSA soil boring HHSB-1, which was
subsequently converted into temporary monitoring well HHTMW-1. LSA boring HHSB-
1/HHTMW-1 was installed in the approximate location of prior soil borings S-7 and CEC-
A1/A2. In accordance with LSA guidelines, soil samples were collected from HHSB-1 in
approximate 10 ft intervals until groundwater was encountered.

Laboratory analytical results of the soil samples indicated the presence of C9-C22 aromatics
(97.0 mg/kg) above the Soil-to-Groundwater Maximum Soil Contamination Concentration
(MSCC) of 31 mg/kg at a depth of 0 ft to 2 ft below ground surface (bgs) in HHSB-1.
Concentrations of C9-C22 aromatics were not detected in soil above the MSCC in the deeper
samples collected (8 ft to 10 ft bgs, 18 ft to 20 ft bgs, and 28 to 30 ft bgs). Concentrations were
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not detected in the soil samples collected from HHSB-1 above Residential or
Industrial/Commercial MSCCs.

Laboratory analytical results of the groundwater sample collected from HHTMW-1 did not
indicate the presence of compounds above North Carolina Administrative Code 2L Standards
(2L Standards) or Gross Contamination Levels (GCLs).

Recommendations
Based upon the results of the LSA, H&H recommends that DEQ issue a no further action (NFA)
letter for this release incident.
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2.0 Introduction and Site History

This Phase I LSA report documents assessment activities related to a non-UST petroleum release
at the former ACFT facility located at 4718 Mountain Creek Avenue Suite B in Denver, Catawba
County, North Carolina.

The Site consists of one parcel (Parcel ID No. 368312962366) which is approximately 1.04 acres
in area and contains an approximately 8,750 ft2 commercial warehouse. The Site was reportedly
undeveloped land until the construction of the current commercial warehouse in approximately
2007. A Site location map is presented as Figure 1, and the Site map is depicted on Figure 2.

ACFT operated in the eastern portion of the on-Site building in Suite B, from 2015 to 2020,
performing fire truck maintenance activities. Highland Environmental Solutions, Inc. (HES)
conducted an initial visual inspection of the former ACFT leased space on October 5, 2021. The
initial inspection by HES identified staining on the interior concrete slab of the ACTF tenant
space and in an exterior gravel area on the south side of the building. Following the inspection,
soil assessment activities were conducted by HES on March 6, 2022. The soil assessment
activities included the collection of eight (8) soil samples in interior and exterior areas of
staining. Locations of HES’s soil samples are provided in Appendix D.

Laboratory analytical results of the soil samples collected by HES indicated the presence of total
petroleum hydrocarbons diesel-range organics (TPH-DRO) in sample SB-7 (202.5 mg/kg) above
North Carolina Department of Environmental Quality (NCDEQ) Action Level of 100 mg/kg. A
summary of the analytical results of HES’s soil assessment is provided in Appendix D.

Following HES’s assessment, Civil & Environmental Consultants, Inc. (CEC) was retained by
ACFT’s legal counsel to conduct further soil assessment at the Site. CECs assessment activities
were conducted on June 29, 2022 and included the collection of twelve (12) soil samples from
eleven (11) soil borings. The locations of CEC’s soil samples are provided in Appendix D.

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Laboratory analytical results of the soil samples collected by CEC indicated the presence of
TPH-DRO in samples CEC-A1 (150 mg/kg) and CEC-A2 (1,300 mg/kg) above the NCDEQ
Action Level of 100 mg/kg. Samples CEC-A1 and CEC-A2 were collected from the same
location as HES’s soil sample SB-7. A summary of the analytical results of CEC’s soil
assessment is provided in Appendix D.

Following CEC’s assessment, a second “supplemental” assessment was conducted by HES at the
request of the property owner in September 2022. The supplemental assessment activities
conducted by HES included the removal of an approximate 1 ft by 1ft section of interior concrete
slab, inspection and laboratory testing of the vapor barrier below the removed portion of the slab,
and the collection of a soil samples from below the vapor barrier. The location of the additional
samples collected by HES during the supplemental assessment is provided Appendix D.

Laboratory analytical results of the soil samples collected by HES indicated the presence of
TPH-DRO in sample SL-1 (299.7 mg/kg) above the NCDEQ Action Level of 100 mg/kg. A
summary of the analytical results of HES’s additional soil assessment is provided in Appendix
D.

Based upon the presence of TPH-DRO above NCDEQ Action Levels, DEQ requested that ACTF
conduct a Phase I LSA at the Site. H&H performed the Phase I LSA in April 2023. The methods
and results of the Phase I LSA are provided in the following sections.
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3.0 Receptor Information and Risk Characterization

As part of the Phase I LSA, H&H performed a site land use and risk characterization survey.
The LSA Risk Classification and Land Use Form is provided in Appendix A. A discussion of
potential receptors and land use is provided below.

3.1 Receptor Information

3.1.1 Water Supply Wells

H&H conducted a water supply well survey for the area within a 1,500-ft radius of the former
UST basin. The survey was conducted by performing area reconnaissance and checking for
municipal water connections. H&H also interviewed tenants and landowners of occupied
properties within 500 ft of the source area regarding their water usage.

Based on the water supply well survey, municipal water is available to all properties but one
within a 1,500-ft radius of the site. One water supply well was identified approximately 1,300 ft
from the source area (Figure 4). The water supply well is cross to upgradient of the Site. Further,
results of the Phase I LSA did not indicate the presence of groundwater impacts. As such, potential
impacts to the identified water-supply well from the Site is not a concern.

3.1.2 Surface Water

H&H conducted a visual survey for surface water bodies in the area during the receptor survey.
According to the USGS topographic map, no surface water bodies are located within 500 feet of the
source area. The closest surface water body is an unnamed tributary of Mundy Creek located
approximately 510 ft south-southeast of the source area (Figure 1). Mundy Creek is located
greater than 1,500 ft southeast of the source area.
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3.1.3 Subsurface Structures

Visual observations were made for potential subsurface contamination conduits in the immediate
vicinity of the HHBS-1/HHTMW-1 location. Based upon our review, there are no anticipated
subsurface contamination conduits of concern in the area.

3.1.4 Property Owners and Land Use

The site is currently developed and is not anticipated to be redeveloped in the near future.
Surrounding properties are used primarily for commercial and residential purposes.

The zoning of the site is Planned Development (PD). The properties in the surrounding area are
primarily zoned as PD, Highway Commercial (HC), Residential (R-20), and Residential (R-40).
The nearest residentially zoned property is located approximately 500 ft north-northwest and
upgradient of the source area.

3.1.5 Wellhead Protection Areas

Based on our review of the DEQ Wellhead Protection Program’s (WHPP) SWAP Info 2.0
mapping database, the site is not located in a wellhead protection area.

3.2 Risk and Land Use Characterization

Based upon the receptor data, as well as the Phase I LSA groundwater analytical data presented
in Section 5.0, the site qualifies for a low-risk designation. In addition, based upon the zoning of
the site and surrounding area, the site qualifies for an industrial/commercial land use
classification.
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4.0 Geology and Hydrogeology

4.1 Regional Geology and Hydrogeology

The subject property is located in the Piedmont Physiographic Province of North Carolina.
According to the Geologic Map of North Carolina dated 1985, the subject property lies within
the Late Paleozoic Intrusives terrane. In the site area, underlying bedrock is predominantly
composed of granites and granodiorites. The land surface of the area is generally characterized
as gently sloping, which may become moderately steep where intersected by streams.

In the Piedmont, the bedrock is overlain by a mantle of weathered rock termed saprolite or
residuum. The saprolite consists of unconsolidated clay, silt, and sand with lesser amounts of
rock fragments. Due to the range of parent rock types and their variable susceptibility to
weathering, the saprolite ranges widely in color, texture, and thickness. Generally, the saprolite
is thickest near interstream divides and thins toward streambeds. In profile, the saprolite
normally grades from clayey soils near the land surface to highly weathered rock above
competent bedrock.

The occurrence and movement of groundwater in the Piedmont is typically within two separate
but interconnected water-bearing zones. A shallow water-bearing zone occurs within the
saprolite, and a deeper water-bearing zone occurs within the underlying bedrock.

4.2 Site Hydrogeology

Soil samples collected during the Phase I LSA indicate that shallow soil in the source area
consists predominately of red to brown clayey silts with some sand to approximately 30 ft bgs.
DPT refusal was encountered at approximately 30 ft bgs. As such, logging of subsurface
lithology was not possible beyond 30 ft bgs. Based on topography, H&H expects that the
groundwater flow direction is to the south or southeast. Bedrock was not encountered during the
drilling actiivtes.
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5.0 Soil and Groundwater Sampling

5.1 Soil and Groundwater Assessment Activities

On April 12, 2023, H&H oversaw the advancement of LSA soil boring HHSB-1, which was
converted to temporary monitoring well HHTMW-1 in the approximate location of prior sample
S-7 and CEC-A1/CEC-A2. The location of boring HH-SB-1/HHTMW-1 is shown on Figure 3.
Soil and groundwater samples were collected in accordance with NCDEQ UST Section
guidelines.

Prior to drilling activities, H&H contacted North Carolina 811, the public utility locator, to mark
subsurface utilities at the Site. In addition, H&H also contracted with Sweetwater Utility
Exploration, LLC., a private utility locator, to screen the drilling location for subgrade utilities
not marked by the public utility locator. In addition, prior to boring advancement, a
decontaminated stainless-steel hand auger was used to clear the boring to a depth of
approximately 5 ft below ground surface (bgs) to further screen the location for the presence of
subsurface utilities.

H&H contracted with Innovative Environmental Technologies, Inc. (IET) of Concord, North
Carolina to install one co-located soil boring and temporary monitoring well. The soil boring log
and temporary monitoring well construction details are provided in Appendix B. IET utilized an
AMS Power Probe 9510 drill rig to advance HHSB-1 using direct-push technology (DPT)
methods to refusal. During boring advancement, continuous soil samples were recovered in 5 ft
Macro-Core acetate liners, logged for lithological description, and evaluated for evidence of
impacts by visual observations, presence of odors, staining, and organic vapors as measured
using a photo-ionization detector (PID).

Based on the depth to water and in accordance with NCDEQ UST Section guidelines, soil
samples were collected every 10 ft until groundwater is encountered. The soil samples from the
uppermost and lowermost intervals (0 ft to 2 ft and 28 ft to 30 ft bgs, respectively) were analyzed
for volatile organic compounds (VOCs) by EPA Method 8260B, semi-VOCs by EPA Method
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8270D, and volatile petroleum hydrocarbons (VPH) and Extractable Petroleum Hydrocarbons
(EPH) by the Massachusetts Department of Environmental Protection (MADEP) Methods.
Middle intervals (8 ft to 10 ft bgs and 18 ft to 20 ft bgs) were analyzed for VPH and EPH by the
MADEP Methods in accordance with NCDEQ UST section guidance. The soil samples were
submitted to Pace Analytical, a North Carolina-certified laboratory. Dedicated laboratory-
supplied sample kits and jars were used for sample collection and the samples were placed in an
iced cooler after collection. A chain-of-custody record was completed for the samples collected
and included the sample description, date collected, time collected, matrix, sample container
information, and analyses required. The chain-of-custody was signed by field personnel prior to
placement in the iced sample cooler for shipment to the laboratory. The chain-of-custody record
and laboratory analytical data report are provided in Appendix C. A summary of the soil
analytical results is provided on Table 1.

Following collection of the soil samples, IET utilized air rotary and hollow stem auger drilling
methods to advance the boring into the water table and construct temporary monitoring well
HHTMW-1. The temporary monitoring well was installed to a total depth of 43 ft bgs and
constructed using 2-inch diameter PVC riser with a 10 ft section of 0.010-inch slotted, pre-
packed, PVC screen set to bracket the surficial aquifer. A filter sand pack was then installed
from the bottom of the well boring to approximately two ft above the well screen, and an
approximate 2 ft bentonite seal was installed above the filter sand pack. A summary of the
temporary monitoring well construction details is provided on Table 2.

Prior to sampling, H&H developed the temporary monitoring well in accordance with standard
protocols. Following development, a groundwater sample was collected using a bladder pump
and “low flow” sampling methods. During sampling, the temporary well was purged until field
parameters of temperature, pH, specific conductivity, and oxidation reduction potential (ORP)
stabilized. Following stabilization of field parameters, groundwater samples were collected and
submitted for laboratory analysis of VOCs by EPA Method 6200, Bases Neutrals and Acids by
EPA Method 625 plus the 10 highest tentatively identified compounds (TICs), Lead and
Chromium by EPA Method 6020, and VPH and EPH by the MADEP Methods.

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The groundwater samples were submitted to Pace Analytical, a North Carolina-certified
laboratory. Dedicated laboratory-supplied sample kits and bottles were used for sample
collection and the samples were placed in an iced cooler after collection. A chain-of-custody
record was completed for the samples collected and included the sample description, date
collected, time collected, matrix, sample container information, and analyses required. The
chain-of-custody was signed by field personnel prior to placement in the iced sample cooler for
shipment to the laboratory. The chain-of-custody record and laboratory analytical data sheets are
provided in Appendix C. A summary of the groundwater analytical results is provided in Table 3
and Table 4.

Following the collection of the groundwater sample, the temporary monitoring well was
abandoned in accordance with North Carolina requirements. The abandonment record is
provided in Appendix B.

5.2 Soil and Groundwater Analytical Results

Laboratory analytical results of the soil samples indicated the presence of C9-C22 aromatics
(97.0 mg/kg) in HHSB-1 at the depth interval of 0 ft to 2 ft bgs above the Soil-to-Groundwater
MSCC of 31 mg/kg, respectively. In addition, a low-level concentration of methylene chloride
was detected in HHSB-1 at the depth interval of 0 ft to 2 ft bgs and 28 ft to 30 ft bgs above the
Soil-to Groundwater MSCC of 0.023 mg/kg. However, the detection of methylene chloride is
flagged as a laboratory contaminant (C9) by the laboratory. In addition, methylene chloride was
not detected in the previous sample collected by CEC at this location. As such, the methylene
chloride concentration is not considered to be representative of Site conditions and is a result of
laboratory contamination. No other compounds were detected above Soil-to-Groundwater
MSCCs and concentrations were not detected above Residential or Industrial/Commercial
MSCCs.

Laboratory analytical results of the groundwater sample did not indicate the presence of VPH,
EPH, VOCs, or SVOCs above laboratory reporting limits. Chromium and lead concentrations
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were detected, but the reported concentrations are well below their respective 2L standards and
are likely attributable to background concentrations.

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6.0 Summary and Recommendations

Based on the Phase I LSA, the site qualifies for a low risk industrial/commercial classification.
Results of Phase I LSA soil sampling indicate that compound concentrations are not present in
soil above Residential or Industrial MSCCs. A concentration of C9 – C22 aromatics is present in
shallow soil (0 ft to 2 ft bs), but deeper soil samples indicate that the concentrations C9 – C22
aromatics attenuate rapidly and do not pose a risk to groundwater. Further, results of the
groundwater sampling do not indicate the presence of compounds in groundwater at the Site
above the 2L Standards or GCLs.

Because compounds concentrations detected in soil do not exceed Residential/Commercial
MSCCs and the results of the soil and groundwater sampling do not indicate the potential for
groundwater impacts from this release, H&H requests that DEQ issue a NFA letter for the
incident.

Tables
Table 1Summary of Phase I LSA Soil Sample ResultsFormer ACFT Facility4718 Mountain Creek Avenue Suite BDenver, North CarolinaH&H Job. No. ACF.001MADEP MADEP MADEP MADEP MADEP MADEP MADEP MADEP 8260B 8270E 6020 6020Sample IDDate CollectedSource AreaSample Depth (ft)Incident Phase4/12/2023 0-2 LSA<14 <14 <62.4 BDL610<1497.097.00.111 C9ALL BDL26.1 21.14/12/2023 8-10 LSA<13 <13 <12.3 BDL79.1<1315.3 15.3NA NA NA NA4/12/2023 18-20 LSA<16 <16 <12.6 BDL51.3<16 <12.6 BDL NA NA NA NA4/12/2023 28-30 LSA<13 <13 <13.1 BDL <13.1 <13 <13.1 BDL0.122 C9ALL BDL38.8 18.468 NS NS 540 NS NS NS 31 0.023 varies 3.8 270625 NS NS 1,560 31,200 NS NS 469 93.8 varies 1.32 4009,340 NS NS 23,300 467,000 NS NS 7,000 1,400 varies 6.54 400Mean-- -- -- -- -- -- -- -- -- -- 65 16Range-- -- -- -- -- -- -- -- -- -- 7.0 - 300 ND - 50Notes:1 = Division of Waste Management Maximum Soil Contaminant Concentration Levels (MSCCs), September 2022.2 = Range and mean values of background metals for North Carolina soils published in Elements in North American Soils by Dragun and Chekiri, 2005.With the exception of VPH and EPH, only those compounds detected are shown.Concentrations are reported in milligrams per kilogram (mg/kg).Bold values exceed the Soil to Ground Water MSCC and the upper range of natually occuring regional background concentrations for metals C9 = concentration attributable to laboratory contaminationLSA = Limited Site Assessment; MADEP = Massachusetts Department of Environmental Protection; VPH = Volatile Petroleum Hydrocarbons; EPH = Extractable Petroleum Hydrocarbons SVOC = Semivolatile Organic Compound; BDL = Below Laboratory Detection Limit ; NA = Not Analyzed; N/A = Not Applicable; ND = Not Detected; NS = Not Specified LeadChromium (total)SouthernExterior GravelAreaSVOCsSoil to Ground Water MSCC (mg/kg)1Residential MSCC (mg/kg)1EPH C19-C36 Aliphatics VPH C9-C10 Aromatics EPH C11-C22 Aromatics Total C9-C22 AromaticsMethylene ChlorideEPH C9-C18 Aliphatics Total C9-C18 AliphaticsRegional Background Metals in Soil (mg/kg)2HHSB-1Analytical MethodContaminant of ConcernVPH C5-C8 Aliphatics VPH C9-C12 Aliphatics Industrial/Commercial MSCC (mg/kg)1https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Atlantic Coast Fire Trucks (ACF)/Tables/Data Tables5/9/2023Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Temporary Well ConstructionFormer ACFT Facility4718 Mountain Creek Avenue Suite BDenver, North CarolinaH&H Job No. ACF.001Well ID Date Installed Date AbandonedWell Diameter (in)Total Depth (ft bgs)Screen Interval(ft bgs)Depth to Water (ft TOC)HHTMW-1 4/12/2023 4/13/2023 2 43 33 - 43 34.21Notes:ft = feet; in = inches; bgs = below ground surface; TOC = top of casinghttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Atlantic Coast Fire Trucks (ACF)/Tables/Data Tables4/27/2023Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3Summary of Phase I LSA Groundwater Sample ResultsFormer ACFT Facility4718 Mountain Creek Avenue Suite BDenver, North CarolinaH&H Job. No. ACF.001MADEP MADEP MADEP MADEP MADEP MADEP MADEP MADEP 6200B 625 6020 6020Sample IDDate CollectedSource AreaIncident PhaseHHTMW-1 4/13/2023Southern Exterior Gravel AreaLSA<100 <100 <105 BDL <105 <100 <105 BDL ALL BDL ALL BDL2.3 1.4400 NS NS 700 10,000 NS NS 200varies varies 10 15NS NS NS NS NS NS NS NSvaries varies 10,000 15,000Notes:1 = Division of Waste Management 2L Groundwater Quality Standards (April 2022) and Gross Contamination Levels for Groundwater (GCLs; September 2022)With the exception of VPH and EPH, only those compounds detected are shown.Concentrations are reported in micrograms per liter (μg/L)LSA = Limited Site Assessment; MADEP = Massachusetts Department of Environmental Protection; VPH = Volatile Petroleum Hydrocarbons; EPH = Extractable Petroleum Hydrocarbons; VOC = Volatile Organic CompoundSVOC = Semivolatile Organic Compound; BDL = Below Laboratory Detection Limit; NS = Not Specified; N/A = Not ApplicableVPH C9-C12 Aliphatics EPH C9-C18 Aliphatics Total C9-C18 AliphaticsEPH C19-C36 Aliphatics VPH C9-C10 Aromatics EPH C11-C22 Aromatics Gross Contamination Level (µg/L)1Analytical MethodContaminant of ConcernVPH C5-C8 Aliphatics Total C9-C22 AromaticsLeadSVOCsChromium (total)VOCNorth Carolina 2L Groundwater Standard (µg/L)1https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Atlantic Coast Fire Trucks (ACF)/Tables/Data Tables4/27/2023Table 3 (Page 1 of 1)Hart & Hickman, PC
Table 4Summary of Phase I LSA Groundwater Sample Results - TICsFormer ACFT Facility4718 Mountain Creek Avenue Suite BDenver, North CarolinaH&H Job. No. ACF.001625 TIC 625 TIC 625 TIC 625 TIC 625 TIC 625 TIC 625 TIC 625 TIC 625 TIC 625 TICSample IDDate CollectedSource AreaIncident PhaseHHTMW-1 4/13/2023Southern Exterior Gravel AreaLSA 21.0 J 13.9 J 13.1 J 13.6 J 9.1 J 10.0 J 11.3 J 9.9 J 16.6 J 196 JNotes:Concentrations are reported in micrograms per liter (μg/L)LSA = Limited Site Assessment; TIC = Tentatively Identified Compound; J = Estimated concentration that is above the laboratory method detection limit but below the laboratory reporting limit Analytical MethodContaminant of ConcernTolueneNonanoic acidhexadecanoic acidUnknown ConstituentOctadecanoic acidUnknown Constituent2-methyl-DodecaneHeneicosaneHexatriacontaneUnknown Constituenthttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Atlantic Coast Fire Trucks (ACF)/Tables/Data Tables4/27/2023Table 4 (Page 1 of 1)Hart & Hickman, PC

Figures
REVISION NO. 0
FIGURE NO. 2
SITE MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
NOTES:
1. AERIAL IMAGERY OBTAINED FROM BING IMAGING
SERVICES (2023).
2. BASE DATA OBTAINED FROM NC ONEMAP (2023).
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
JOB NO. ACF-001
DATE: 4-12-23
FORMER ATLANTIC COAST FIRE TRUCKS
4718 MOUNTAIN CREEK AVENUE SUITE B
DENVER, NORTH CAROLINAMOUNTA
IN
CR
EEK
AV
ENUE
NC-1
5
0
S:\AAA-Master Projects\Atlantic Coast Fire Trucks (ACF)\Figures\RS-ACF-230412.dwg, FIG 2, 4/20/2023 3:44:28 PM, kmckinney
REVISION NO. 0
FIGURE NO. 3
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
CO-LOCATED SOIL BORING AND
TEMPORARY MONITORING WELL
NOTES:
1. AERIAL IMAGERY OBTAINED FROM BING IMAGING
SERVICES (2023).
2. BASE DATA OBTAINED FROM NC ONEMAP (2023).
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
JOB NO. ACF-001
DATE: 4-20-23
FORMER ATLANTIC COAST FIRE TRUCKS
4718 MOUNTAIN CREEK AVENUE SUITE B
DENVER, NORTH CAROLINAMOUNTA
IN
CR
EEK
AV
ENUE
NC-1
5
0
HHSB-1/HHTMW-1
S:\AAA-Master Projects\Atlantic Coast Fire Trucks (ACF)\Figures\RS-ACF-230412.dwg, FIG 3, 4/20/2023 3:44:46 PM, kmckinney
REVISION NO. 0
JOB NO. ACF-001
DATE: 4-12-23
FIGURE NO. 4
FORMER ATLANTIC COAST FIRE TRUCKS
4718 MOUNTAIN CREEK AVENUE SUITE B
DENVER, NORTH CAROLINA
RECEPTOR SURVEY MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL LINE
WATER SUPPLY WELL
NOTES:
1.AERIAL IMAGERY OBTAINED FROM BING IMAGING
SERVICES (2023).
2.BASE DATA OBTAINED FROM NC ONEMAP (2023).
3.NO WATER SUPPLY WELLS IDENTIFIED IN THE SURVEY
RADIUS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
1,500 FT
S:\AAA-Master Projects\Atlantic Coast Fire Trucks (ACF)\Figures\RS-ACF-230412.dwg, FIG 4, 4/20/2023 3:45:02 PM, kmckinney

Appendix A

Risk Classification and Land Use Form
1
Limited Site Assessment Risk Classification and Land Use Form
Part I - Groundwater/Surface Water/Vapor Impacts High Risk 1. Has the discharge or release contaminated any water supply well including any used for non-drinking purposes?

The discharge or release has not resulted in known contaminated water wells in the site
area. 2. Is a water supply well used for drinking water located within 1,000 feet of the source
area of the discharge or release?

Water supply wells used for drinking water were not identified within 1,000 ft of the source area.
3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial
cooling water, filling swimming pools) located within 250 feet of the source area of the release or discharge? Water supply wells used for any purpose were not identified within 250 ft of the source
area.
4. Does groundwater within 500 feet of the source area of the discharge or release have the potential for future use in that there is no other source of water supply other than the groundwater?

The subject site and surrounding properties are served by the municipal water supply. 5. Do vapors from the discharge or release pose a threat of explosion because of accumulation of the vapors in a confined space, or pose any other serious threat to public
health, public safety or the environment?

Vapors from the discharge or release do not pose a threat of explosion and do not pose a serious threat to public health, public safety, or the environment.
6. Are there any other factors that would cause the discharge or release to pose an
imminent danger to public health, public safety, or the environment? No other factors would cause the discharge or release to pose an imminent danger to public health, public safety, or the environment.
2
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the discharge or
release? According to the USGS topographic map, no surface water bodies are located within 500 feet of the source area. The closest surface water body is an unnamed tributary of
Mundy Creek located approximately 510 ft south-southeast of the source area.
8. Is the source area of the discharge or release located within a designated wellhead protection area as defined in 42 USC 300h-7(e)?
The source area is not located within a designated wellhead protection area.
9. Is the discharge or release located in the Coastal Plain physiographic region as designated on a map entitled "Geology of North Carolina" published by the Department in 1985? If yes, is the source area of the discharge or release located in an area in which
there is recharge to an unconfined or semi-confined deeper aquifer that is being used or
may be used as a source of drinking water? The discharge or release is not located in the Coastal Plain physiographic region.
10. Do the levels of groundwater contamination for any contaminant exceed the gross
contamination levels established (see Table 3) by the Department? Detected concentrations do not exceed gross contamination levels.
Part II - Land Use Property Containing Source Area of Discharge or Release 1. Does the property contain one or more primary or secondary residences (permanent or temporary)?

The property does not contain a primary or secondary residence. 2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly?

The property does not contain a place of public assembly.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial (e.g., manufacturing, utilities, industrial research and development,
chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped?
3
The property is currently developed with one warehouse used for business/commercial operations. Prior to the existing structure having been built the property was
undeveloped.
4. Do children visit the property? Children currently do not visit the property.

5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or both)? Access to rear of the property currently is restricted with a locked chain link fence..

6. Do pavement, buildings, or other structures cap the contaminated soil? The area of the UST release is currently partially capped with asphalt and/or concrete and is anticipated to be capped with asphalt and/or concrete during site redevelopment.

7. What is the zoning status of the property? The property is zoned as Planned Development (PD).
8. Is the use of the property likely to change in the next 20 years?

The use of the site property is not likely to change in the next 20 years.
Property Surrounding Source Area of Discharge or Release
The questions below pertain to the area within 1500 feet of the source area of the discharge or release (excludes property containing source area of the release): 9. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?

The nearest residentially zoned parcel is approximately 500 ft north-northwest of the source area.
10. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly? Kids in Motion daycare is located approximately 1,250 ft west-southwest of the source
area.
11. What is the zoning status of properties in the surrounding area?
4
The properties in the surrounding area are primarily zoned as PD, Highway Commercial (HC), Residential (R-20), and Residential (R-40).

12. Briefly characterize the use and activities of the land in the surrounding area. The primary land use in the immediate vicinity of the site is commercial and residential.

Appendix B

Boring Log and Well Completion and Abandonment Records
NOTES:Boring cleared to 5' bgs via hand auger.
Client:
Project:
Address:
Atlantic Coast Fire Trucks
ACF-001
4718 Mountain Creek Avenue SuiteB, Denver, NC
WELL LOG
Well No.
Page:
HHSB-1/HHTMW-1
1 of 2
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/12/2023
4/12/2023
IET
Hollow Stem Auger
AMS Power Probe 9510
Mike Tynan
Adam Michalak
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
49.0
8.25
DP, GR
45.0
34.0
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
49.0
2.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips/Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
Temporary monitoring well stickup
GR
DP
DP
DP
DP
5.00
5.00
4.00
3.75
4.00
(0') Poorly graded GRAVEL (GP); loose, dry, gray
(0.2') SILT with sand (ML); little fine sand, little clay, soft, moist, reddish-brown
(2.5') Sandy SILT (ML); some fine sand, soft, moist, brown-grey, slight petroleum
odor
(3') SILT (ML); few medium sand, trace clay, soft, moist, reddish-brown, no odor
(5.5') SILT (ML); few fine sand, medium stiff, moist, reddish-brown
(10') Poorly graded SAND (SP); mostly fine-coarse grained sand, trace silt, loose,
dry, light brown with white
(11') SILT (ML); trace clay, medium stiff, dry, reddish-brown
(15') SILT (ML); few fine-coarse sand, medium stiff, dry, light brown with brown and
white, micaceous
(18') SILT (ML); few clay, medium stiff, dry, reddish-brown with slight white
(20') Sandy SILT (ML); some fine-medium sand, few clay, medium stiff, dry, light
brown with brown, white, and yellow, micaceous
4.4
39.9
5.1
5.7
6.7
7.3
9.6
10.3
6.2
9.9
8.8
13.2
6.1
HHSB-1 (0-2)
HHSB-1 (8-10)
HHSB-1 (18-20)
0
5
10
15
20
25
NOTES:
Client:
Project:
Address:
Atlantic Coast Fire Trucks
ACF-001
4718 Mountain Creek Avenue SuiteB, Denver, NC
WELL LOG
Well No.
Page:
HHSB-1/HHTMW-1
2 of 2
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
4/12/2023
4/12/2023
IET
Hollow Stem Auger
AMS Power Probe 9510
Mike Tynan
Adam Michalak
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
49.0
8.25
DP, GR
45.0
34.0
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Pack:
49.0
2.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips/Bent. Chips
Sand Pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)25
30
35
40
45
50
DP 4.00 (25') As Above
(30') 30' and below logged from hollow stem auger cuttings--SILT (ML); few
fine-medium sand, soft, dry, medium brown, powdery
(35') As Above: color change to dark brown, micaceous
(45') As Above: wet at 45'
(49') Boring terminated
0.0
8.1
6.5 HHSB-1 (28-30)
25
30
35
40
45
50
Boring cleared to 5' bgs via hand auger.

WELL CONSTRUCTION RECORD (GW-1) For Internal Use Only:

Form GW-1 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name

2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.)

3. Well Use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)

4. Date Well(s) Completed: Well ID#
5a. Well Location:

Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip

County Parcel Identification No. (PIN)

5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)

N W

6. Is(are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.

8. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
construction, only 1 GW-1 is needed. Indicate TOTAL NUMBER of wells
drilled:

9. Total well depth below land surface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10. Static water level below top of casing: (ft.)
If water level is above casing, use “+”
11. Borehole diameter: (in.)

12. Well construction method:
(i.e. auger, rotary, cable, direct push, etc.)

FOR WATER SUPPLY WELLS ONLY:

13a. Yield (gpm) Method of test:
13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN
FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary)
FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:

Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a
copy of this record has been provided to the well owner.
23. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
construction details. You may also attach additional pages if necessary.

SUBMITTAL INSTRUCTIONS

24a. For All Wells: Submit this form within 30 days of completion of well
construction to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells: In addition to sending the form to the address in 24a
above, also submit one copy of this form within 30 days of completion of well
construction to the following:

Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells: In addition to sending the form to
the address(es) above, also submit one copy of this form within 30 days of
completion of well construction to the county health department of the county
where constructed.
Mike Tynan
2725-A
IET
4/12/2023 TMW-1
Former ACTF Facility
4718 Mountain Creek Ave, Denver 28037
Catawba
35 33 48.510 -81 03 13.187
43
34
8.25
Auger/air
4/14/2023
34 44 silty sand, pwr
0 33 2 Sch40 PVC
33 43 2 0.010 Sch40 PVC prepacked
26
30
30
45
bentonite
#2 silica sand pour through augers
pour
See consultant's log
Well abandoned after sampling (4/13/23)
Print Form
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1. Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2. Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3. Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s):(gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8. Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9. Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
Mike Tynan
2725-A <2
IET
~50 lbs Hole Plug
4/13/23
Removed all PVC screen and riser. Filled borehole
completely with bentonite.
Former ACTF Facility
4718 Mountain Creek Ave, Denver 28037 4/14/2023
Catawba
35 33 48.510 -81 03 13.187
TMW-1
43
8.25
34
33
10

Appendix C

Laboratory Analytical Reports and Low-Flow Form
#=CL#
April 26, 2023
LIMS USE: FR - JOHN LOPEZ
LIMS OBJECT ID: 92662294
92662294
Project:
Pace Project No.:
RE:
John Lopez
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
ACF-001
Dear John Lopez:
Enclosed are the analytical results for sample(s) received by the laboratory on April 14, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
• Pace Analytical Services - Minneapolis
This report was revised on April 25, 2023, to remove 6020B copper and report chromium on all Pace samples.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 70
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92662294
ACF-001
Pace Analytical Services, LLC - Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414
A2LA Certification #: 2926.01
Alabama Certification #: 40770
Alaska Contaminated Sites Certification #: 17-009
Alaska DW Certification #: MN00064
Arizona Certification #: AZ0014
Arkansas DW Certification #: MN00064
Arkansas WW Certification #: 88-0680
California Certification #: 2929
Colorado Certification #: MN00064
Connecticut Certification #: PH-0256
EPA Region 8 Tribal Water Systems+Wyoming DW
Certification #: via MN 027-053-137
Florida Certification #: E87605
Georgia Certification #: 959
GMP+ Certification #: GMP050884
Hawaii Certification #: MN00064
Idaho Certification #: MN00064
Illinois Certification #: 200011
Indiana Certification #: C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky DW Certification #: 90062
Kentucky WW Certification #: 90062
Louisiana DEQ Certification #: AI-03086
Louisiana DW Certification #: MN00064
Maine Certification #: MN00064
Maryland Certification #: 322
Michigan Certification #: 9909
Minnesota Certification #: 027-053-137
Minnesota Dept of Ag Approval: via MN 027-053-137
Minnesota Petrofund Registration #: 1240
Mississippi Certification #: MN00064
Missouri Certification #: 10100
Montana Certification #: CERT0092
Nebraska Certification #: NE-OS-18-06
Nevada Certification #: MN00064
New Hampshire Certification #: 2081
New Jersey Certification #: MN002
New York Certification #: 11647
North Carolina DW Certification #: 27700
North Carolina WW Certification #: 530
North Dakota Certification (A2LA) #: R-036
North Dakota Certification (MN) #: R-036
Ohio DW Certification #: 41244
Ohio VAP Certification (1700) #: CL101
Oklahoma Certification #: 9507
Oregon Primary Certification #: MN300001
Oregon Secondary Certification #: MN200001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification #: MN00064
South Carolina Certification #:74003001
Tennessee Certification #: TN02818
Texas Certification #: T104704192
Utah Certification #: MN00064
Vermont Certification #: VT-027053137
Virginia Certification #: 460163
Washington Certification #: C486
West Virginia DEP Certification #: 382
West Virginia DW Certification #: 9952 C
Wisconsin Certification #: 999407970
Wyoming UST Certification #: via A2LA 2926.01
USDA Permit #: P330-19-00208
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 70
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92662294
ACF-001
Lab ID Sample ID Matrix Date Collected Date Received
92662294001 HHSB-1 (0-2)Solid 04/12/23 14:10 04/14/23 09:29
92662294002 HHSB-1 (28-30)Solid 04/12/23 14:55 04/14/23 09:29
92662294003 HHSB-1 (8-10)Solid 04/12/23 14:25 04/14/23 09:29
92662294004 HHSB-1 (18-20)Solid 04/12/23 14:40 04/14/23 09:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 70
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92662294
ACF-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92662294001 HHSB-1 (0-2)MADEP EPH 7 PASI-CBAJ, NND
EPA 6020B 2 PASI-MNN2
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92662294002 HHSB-1 (28-30)MADEP EPH 7 PASI-CBAJ, NND
EPA 6020B 2 PASI-MNN2
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
SW-846 1 PASI-CKDF
92662294003 HHSB-1 (8-10)MADEP EPH 7 PASI-CBAJ, NND
SW-846 1 PASI-CKDF
92662294004 HHSB-1 (18-20)MADEP EPH 7 PASI-CBAJ, NND
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
PASI-M = Pace Analytical Services - Minneapolis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 70
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662294
ACF-001
Method:
Client:Hart & Hickman
MADEP EPH
Date:April 26, 2023
Description:MADEP EPH NC Soil
General Information:
4 samples were analyzed for MADEP EPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition
with any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the endof this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 768569
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).
• HHSB-1 (0-2) (Lab ID: 92662294001)
• 1-Chlorooctadecane (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 70
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662294
ACF-001
Method:
Client:Hart & Hickman
EPA 6020B
Date:April 26, 2023
Description:6020B MET ICPMS
General Information:
2 samples were analyzed for EPA 6020B by Pace Analytical Services Minneapolis. All samples were received in acceptable condition
with any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the endof this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3050B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 70
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662294
ACF-001
Method:
Client:Hart & Hickman
EPA 8270E
Date:April 26, 2023
Description:8270E MSSV Microwave
General Information:
2 samples were analyzed for EPA 8270E by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 769298
v2: The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated
samples and the sensitivity of the instrument was verified with a reporting limit check standard.
• BLANK (Lab ID: 3994086)
• Hexachlorocyclopentadiene
• DUP (Lab ID: 3994089)
• Hexachlorocyclopentadiene
• HHSB-1 (28-30) (Lab ID: 92662294002)
• Hexachlorocyclopentadiene
v3: The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated
samples may have low bias.
• LCS (Lab ID: 3994087)
• Hexachlorocyclopentadiene
• MS (Lab ID: 3994088)
• Hexachlorocyclopentadiene
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 70
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662294
ACF-001
Method:
Client:Hart & Hickman
EPA 8270E
Date:April 26, 2023
Description:8270E MSSV Microwave
QC Batch: 768315
L2: Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samples
may be biased low.
• LCS (Lab ID: 3989137)
• Benzoic Acid
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 769298
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92661946006
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3994088)
• Benzoic Acid
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
Analyte Comments:
QC Batch: 768315
D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.
• DUP (Lab ID: 3989140)
• Nitrobenzene-d5 (S)
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 70
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662294
ACF-001
Method:
Client:Hart & Hickman
EPA 8260D
Date:April 26, 2023
Description:8260D/5035A/5030B Volatiles
General Information:
2 samples were analyzed for EPA 8260D by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A/5030B with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 768510
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 3990169)
• 1,2,3-Trichlorobenzene
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• Vinyl chloride
• DUP (Lab ID: 3990172)
• 1,2,3-Trichlorobenzene
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• Vinyl chloride
• HHSB-1 (0-2) (Lab ID: 92662294001)
• 1,2,3-Trichlorobenzene
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• Vinyl chloride
• HHSB-1 (28-30) (Lab ID: 92662294002)
• 1,2,3-Trichlorobenzene
• Chloroethane
• Chloromethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 70
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662294
ACF-001
Method:
Client:Hart & Hickman
EPA 8260D
Date:April 26, 2023
Description:8260D/5035A/5030B Volatiles
QC Batch: 768510
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• Vinyl chloride
• LCS (Lab ID: 3990170)
• 1,2,3-Trichlorobenzene
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• Vinyl chloride
• MS (Lab ID: 3990171)
• 1,2,3-Trichlorobenzene
• Chloroethane
• Chloromethane
• Dichlorodifluoromethane
• Hexachloro-1,3-butadiene
• Vinyl chloride
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 768510
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samplesmay be biased high.
• LCS (Lab ID: 3990170)
• Chloromethane
• Dichlorodifluoromethane
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 70
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662294
ACF-001
Method:
Client:Hart & Hickman
EPA 8260D
Date:April 26, 2023
Description:8260D/5035A/5030B Volatiles
Additional Comments:
Analyte Comments:
QC Batch: 768510
C9: Common Laboratory Contaminant.
• DUP (Lab ID: 3990172)
• Methylene Chloride
• HHSB-1 (0-2) (Lab ID: 92662294001)
• Methylene Chloride
• HHSB-1 (28-30) (Lab ID: 92662294002)
• Methylene Chloride
• MS (Lab ID: 3990171)
• Methylene Chloride
• BLANK (Lab ID: 3990169)
• 1,2,3-Trichloropropane
• DUP (Lab ID: 3990172)
• 1,2,3-Trichloropropane
• HHSB-1 (0-2) (Lab ID: 92662294001)
• Vinyl acetate
• HHSB-1 (28-30) (Lab ID: 92662294002)
• 1,2,4-Trimethylbenzene
• LCS (Lab ID: 3990170)
• 1,2,3-Trichloropropane
• MS (Lab ID: 3990171)
• 1,2,3-Trichloropropane
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (0-2)Lab ID:92662294001 Collected:04/12/23 14:10 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/20/23 13:17 N204/18/23 08:2862.4 62.4 5
Aliphatic (C19-C36)610 mg/kg 04/20/23 13:17 N204/18/23 08:2862.4 62.4 5
Aromatic (C11-C22)97.0 mg/kg 04/19/23 16:34 N204/18/23 08:2812.5 12.5 1
Surrogates
1-Chlorooctadecane (S)227 %04/20/23 13:17 3386-33-2 S504/18/23 08:2840-140 5
o-Terphenyl (S)132 %04/19/23 16:34 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)100 %04/19/23 16:34 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)110 %04/19/23 16:34 580-13-204/18/23 08:2840-140 1
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Chromium 26.1 mg/kg 04/19/23 13:06 7440-47-304/19/23 08:232.5 0.48 1
Lead 21.1 mg/kg 04/19/23 13:06 7439-92-104/19/23 08:230.62 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/16/23 13:50 83-32-904/15/23 15:464231491
Acenaphthylene ND ug/kg 04/16/23 13:50 208-96-804/15/23 15:464231491
Aniline ND ug/kg 04/16/23 13:50 62-53-304/15/23 15:464231651
Anthracene ND ug/kg 04/16/23 13:50 120-12-704/15/23 15:464231381
Benzo(a)anthracene ND ug/kg 04/16/23 13:50 56-55-304/15/23 15:464231411
Benzo(a)pyrene ND ug/kg 04/16/23 13:50 50-32-804/15/23 15:464231461
Benzo(b)fluoranthene ND ug/kg 04/16/23 13:50 205-99-204/15/23 15:464231411
Benzo(g,h,i)perylene ND ug/kg 04/16/23 13:50 191-24-204/15/23 15:464231641
Benzo(k)fluoranthene ND ug/kg 04/16/23 13:50 207-08-904/15/23 15:464231491
Benzoic Acid ND ug/kg 04/16/23 13:50 65-85-0 L204/15/23 15:4621109091
Benzyl alcohol ND ug/kg 04/16/23 13:50 100-51-604/15/23 15:468463201
4-Bromophenylphenyl ether ND ug/kg 04/16/23 13:50 101-55-304/15/23 15:464231631
Butylbenzylphthalate ND ug/kg 04/16/23 13:50 85-68-704/15/23 15:464231781
4-Chloro-3-methylphenol ND ug/kg 04/16/23 13:50 59-50-704/15/23 15:468462971
4-Chloroaniline ND ug/kg 04/16/23 13:50 106-47-804/15/23 15:468463321
bis(2-Chloroethoxy)methane ND ug/kg 04/16/23 13:50 111-91-104/15/23 15:464231761
bis(2-Chloroethyl) ether ND ug/kg 04/16/23 13:50 111-44-404/15/23 15:464231591
2-Chloronaphthalene ND ug/kg 04/16/23 13:50 91-58-704/15/23 15:464231681
2-Chlorophenol ND ug/kg 04/16/23 13:50 95-57-804/15/23 15:464231591
4-Chlorophenylphenyl ether ND ug/kg 04/16/23 13:50 7005-72-304/15/23 15:464231581
Chrysene ND ug/kg 04/16/23 13:50 218-01-904/15/23 15:464231541
Dibenz(a,h)anthracene ND ug/kg 04/16/23 13:50 53-70-304/15/23 15:464231631
Dibenzofuran ND ug/kg 04/16/23 13:50 132-64-904/15/23 15:464231531
1,2-Dichlorobenzene ND ug/kg 04/16/23 13:50 95-50-104/15/23 15:464231531
1,3-Dichlorobenzene ND ug/kg 04/16/23 13:50 541-73-104/15/23 15:464231501
1,4-Dichlorobenzene ND ug/kg 04/16/23 13:50 106-46-704/15/23 15:464231611
3,3'-Dichlorobenzidine ND ug/kg 04/16/23 13:50 91-94-104/15/23 15:468462861
2,4-Dichlorophenol ND ug/kg 04/16/23 13:50 120-83-204/15/23 15:464231651
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (0-2)Lab ID:92662294001 Collected:04/12/23 14:10 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Diethylphthalate ND ug/kg 04/16/23 13:50 84-66-204/15/23 15:464231551
2,4-Dimethylphenol ND ug/kg 04/16/23 13:50 105-67-904/15/23 15:464231761
Dimethylphthalate ND ug/kg 04/16/23 13:50 131-11-304/15/23 15:464231541
Di-n-butylphthalate ND ug/kg 04/16/23 13:50 84-74-204/15/23 15:464231421
4,6-Dinitro-2-methylphenol ND ug/kg 04/16/23 13:50 534-52-104/15/23 15:468463951
2,4-Dinitrophenol ND ug/kg 04/16/23 13:50 51-28-504/15/23 15:46211013101
2,4-Dinitrotoluene ND ug/kg 04/16/23 13:50 121-14-204/15/23 15:464231631
2,6-Dinitrotoluene ND ug/kg 04/16/23 13:50 606-20-204/15/23 15:464231551
Di-n-octylphthalate ND ug/kg 04/16/23 13:50 117-84-004/15/23 15:464231671
bis(2-Ethylhexyl)phthalate ND ug/kg 04/16/23 13:50 117-81-704/15/23 15:464231641
Fluoranthene ND ug/kg 04/16/23 13:50 206-44-004/15/23 15:464231451
Fluorene ND ug/kg 04/16/23 13:50 86-73-704/15/23 15:464231491
Hexachloro-1,3-butadiene ND ug/kg 04/16/23 13:50 87-68-304/15/23 15:464231831
Hexachlorobenzene ND ug/kg 04/16/23 13:50 118-74-104/15/23 15:464231651
Hexachlorocyclopentadiene ND ug/kg 04/16/23 13:50 77-47-404/15/23 15:464232421
Hexachloroethane ND ug/kg 04/16/23 13:50 67-72-104/15/23 15:464231611
Indeno(1,2,3-cd)pyrene ND ug/kg 04/16/23 13:50 193-39-504/15/23 15:464231671
Isophorone ND ug/kg 04/16/23 13:50 78-59-104/15/23 15:464231881
1-Methylnaphthalene ND ug/kg 04/16/23 13:50 90-12-004/15/23 15:464231491
2-Methylnaphthalene ND ug/kg 04/16/23 13:50 91-57-604/15/23 15:464231691
2-Methylphenol(o-Cresol)ND ug/kg 04/16/23 13:50 95-48-704/15/23 15:464231731
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/16/23 13:50 15831-10-404/15/23 15:464231701
Naphthalene ND ug/kg 04/16/23 13:50 91-20-304/15/23 15:464231441
2-Nitroaniline ND ug/kg 04/16/23 13:50 88-74-404/15/23 15:4621103461
3-Nitroaniline ND ug/kg 04/16/23 13:50 99-09-204/15/23 15:4621103321
4-Nitroaniline ND ug/kg 04/16/23 13:50 100-01-604/15/23 15:468463221
Nitrobenzene ND ug/kg 04/16/23 13:50 98-95-304/15/23 15:464231961
2-Nitrophenol ND ug/kg 04/16/23 13:50 88-75-504/15/23 15:464231831
4-Nitrophenol ND ug/kg 04/16/23 13:50 100-02-704/15/23 15:4621108181
N-Nitrosodimethylamine ND ug/kg 04/16/23 13:50 62-75-904/15/23 15:464231421
N-Nitroso-di-n-propylamine ND ug/kg 04/16/23 13:50 621-64-704/15/23 15:464231591
N-Nitrosodiphenylamine ND ug/kg 04/16/23 13:50 86-30-604/15/23 15:464231501
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/16/23 13:50 108-60-104/15/23 15:464232011
Pentachlorophenol ND ug/kg 04/16/23 13:50 87-86-504/15/23 15:468464141
Phenanthrene ND ug/kg 04/16/23 13:50 85-01-804/15/23 15:464231381
Phenol ND ug/kg 04/16/23 13:50 108-95-204/15/23 15:464231881
Pyrene ND ug/kg 04/16/23 13:50 129-00-004/15/23 15:464231721
Pyridine ND ug/kg 04/16/23 13:50 110-86-104/15/23 15:464231331
1,2,4-Trichlorobenzene ND ug/kg 04/16/23 13:50 120-82-104/15/23 15:464231671
2,4,5-Trichlorophenol ND ug/kg 04/16/23 13:50 95-95-404/15/23 15:464231941
2,4,6-Trichlorophenol ND ug/kg 04/16/23 13:50 88-06-204/15/23 15:464231741
Surrogates
Nitrobenzene-d5 (S)40 %04/16/23 13:50 4165-60-004/15/23 15:4610-130 1
2-Fluorobiphenyl (S)31 %04/16/23 13:50 321-60-804/15/23 15:4610-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (0-2)Lab ID:92662294001 Collected:04/12/23 14:10 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Terphenyl-d14 (S)58 %04/16/23 13:50 1718-51-004/15/23 15:4610-130 1
Phenol-d6 (S)41 %04/16/23 13:50 13127-88-304/15/23 15:4610-130 1
2-Fluorophenol (S)39 %04/16/23 13:50 367-12-404/15/23 15:4610-130 1
2,4,6-Tribromophenol (S)36 %04/16/23 13:50 118-79-604/15/23 15:4610-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/18/23 22:56 67-64-104/17/23 17:0116051.3 1
Benzene ND ug/kg 04/18/23 22:56 71-43-204/17/23 17:018.0 3.2 1
Bromobenzene ND ug/kg 04/18/23 22:56 108-86-104/17/23 17:018.0 2.6 1
Bromochloromethane ND ug/kg 04/18/23 22:56 74-97-504/17/23 17:018.0 2.4 1
Bromodichloromethane ND ug/kg 04/18/23 22:56 75-27-404/17/23 17:018.0 3.1 1
Bromoform ND ug/kg 04/18/23 22:56 75-25-204/17/23 17:018.0 2.8 1
Bromomethane ND ug/kg 04/18/23 22:56 74-83-904/17/23 17:0131.9 24.8 1
2-Butanone (MEK)ND ug/kg 04/18/23 22:56 78-93-304/17/23 17:0116038.3 1
n-Butylbenzene ND ug/kg 04/18/23 22:56 104-51-804/17/23 17:018.0 5.0 1
sec-Butylbenzene ND ug/kg 04/18/23 22:56 135-98-804/17/23 17:018.0 3.5 1
tert-Butylbenzene ND ug/kg 04/18/23 22:56 98-06-604/17/23 17:018.0 2.8 1
Carbon tetrachloride ND ug/kg 04/18/23 22:56 56-23-504/17/23 17:018.0 3.0 1
Chlorobenzene ND ug/kg 04/18/23 22:56 108-90-704/17/23 17:018.0 4.6 1
Chloroethane ND ug/kg 04/18/23 22:56 75-00-3 IH,v104/17/23 17:0116.0 6.2 1
Chloroform ND ug/kg 04/18/23 22:56 67-66-304/17/23 17:018.0 6.7 1
Chloromethane ND ug/kg 04/18/23 22:56 74-87-3 IH,L1,
v104/17/23 17:0116.0 6.7 1
2-Chlorotoluene ND ug/kg 04/18/23 22:56 95-49-804/17/23 17:018.0 2.8 1
4-Chlorotoluene ND ug/kg 04/18/23 22:56 106-43-404/17/23 17:018.0 4.4 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/18/23 22:56 96-12-804/17/23 17:018.0 3.1 1
Dibromochloromethane ND ug/kg 04/18/23 22:56 124-48-104/17/23 17:018.0 4.5 1
1,2-Dibromoethane (EDB)ND ug/kg 04/18/23 22:56 106-93-404/17/23 17:018.0 3.5 1
Dibromomethane ND ug/kg 04/18/23 22:56 74-95-304/17/23 17:018.0 1.7 1
1,2-Dichlorobenzene ND ug/kg 04/18/23 22:56 95-50-104/17/23 17:018.0 2.9 1
1,3-Dichlorobenzene ND ug/kg 04/18/23 22:56 541-73-104/17/23 17:018.0 2.5 1
1,4-Dichlorobenzene ND ug/kg 04/18/23 22:56 106-46-704/17/23 17:018.0 2.1 1
Dichlorodifluoromethane ND ug/kg 04/18/23 22:56 75-71-8 IH,L1,
v104/17/23 17:0116.0 8.1 1
1,1-Dichloroethane ND ug/kg 04/18/23 22:56 75-34-304/17/23 17:018.0 3.3 1
1,2-Dichloroethane ND ug/kg 04/18/23 22:56 107-06-204/17/23 17:018.0 5.3 1
1,1-Dichloroethene ND ug/kg 04/18/23 22:56 75-35-404/17/23 17:018.0 3.3 1
cis-1,2-Dichloroethene ND ug/kg 04/18/23 22:56 156-59-204/17/23 17:018.0 2.7 1
trans-1,2-Dichloroethene ND ug/kg 04/18/23 22:56 156-60-504/17/23 17:018.0 6.8 1
1,2-Dichloropropane ND ug/kg 04/18/23 22:56 78-87-504/17/23 17:018.0 2.4 1
1,3-Dichloropropane ND ug/kg 04/18/23 22:56 142-28-904/17/23 17:018.0 2.5 1
2,2-Dichloropropane ND ug/kg 04/18/23 22:56 594-20-704/17/23 17:018.0 6.1 1
1,1-Dichloropropene ND ug/kg 04/18/23 22:56 563-58-604/17/23 17:018.0 3.8 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (0-2)Lab ID:92662294001 Collected:04/12/23 14:10 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND ug/kg 04/18/23 22:56 10061-01-504/17/23 17:018.0 2.2 1
trans-1,3-Dichloropropene ND ug/kg 04/18/23 22:56 10061-02-604/17/23 17:018.0 2.7 1
Diisopropyl ether ND ug/kg 04/18/23 22:56 108-20-304/17/23 17:018.0 2.2 1
Ethylbenzene ND ug/kg 04/18/23 22:56 100-41-404/17/23 17:018.0 3.7 1
Hexachloro-1,3-butadiene ND ug/kg 04/18/23 22:56 87-68-3 v104/17/23 17:0116.0 13.1 1
2-Hexanone ND ug/kg 04/18/23 22:56 591-78-604/17/23 17:0179.9 7.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/18/23 22:56 98-82-804/17/23 17:018.0 2.7 1
p-Isopropyltoluene ND ug/kg 04/18/23 22:56 99-87-604/17/23 17:018.0 3.9 1
Methylene Chloride 111 ug/kg 04/18/23 22:56 75-09-2 C904/17/23 17:0131.9 21.9 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/18/23 22:56 108-10-104/17/23 17:0179.9 7.7 1
Methyl-tert-butyl ether ND ug/kg 04/18/23 22:56 1634-04-404/17/23 17:018.0 3.0 1
Naphthalene ND ug/kg 04/18/23 22:56 91-20-304/17/23 17:018.0 4.2 1
n-Propylbenzene ND ug/kg 04/18/23 22:56 103-65-104/17/23 17:018.0 2.8 1
Styrene ND ug/kg 04/18/23 22:56 100-42-504/17/23 17:018.0 2.1 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/18/23 22:56 630-20-604/17/23 17:018.0 3.1 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/18/23 22:56 79-34-504/17/23 17:018.0 2.1 1
Tetrachloroethene ND ug/kg 04/18/23 22:56 127-18-404/17/23 17:018.0 2.5 1
Toluene ND ug/kg 04/18/23 22:56 108-88-304/17/23 17:018.0 5.5 1
1,2,3-Trichlorobenzene ND ug/kg 04/18/23 22:56 87-61-6 v104/17/23 17:018.0 6.5 1
1,2,4-Trichlorobenzene ND ug/kg 04/18/23 22:56 120-82-104/17/23 17:018.0 6.7 1
1,1,1-Trichloroethane ND ug/kg 04/18/23 22:56 71-55-604/17/23 17:018.0 4.2 1
1,1,2-Trichloroethane ND ug/kg 04/18/23 22:56 79-00-504/17/23 17:018.0 2.7 1
Trichloroethene ND ug/kg 04/18/23 22:56 79-01-604/17/23 17:018.0 6.4 1
Trichlorofluoromethane ND ug/kg 04/18/23 22:56 75-69-404/17/23 17:018.0 4.4 1
1,2,3-Trichloropropane ND ug/kg 04/18/23 22:56 96-18-404/17/23 17:018.0 4.0 1
1,2,4-Trimethylbenzene ND ug/kg 04/18/23 22:56 95-63-604/17/23 17:018.0 4.7 1
1,3,5-Trimethylbenzene ND ug/kg 04/18/23 22:56 108-67-804/17/23 17:018.0 2.7 1
Vinyl acetate ND ug/kg 04/18/23 22:56 108-05-404/17/23 17:0179.9 16.4 1
Vinyl chloride ND ug/kg 04/18/23 22:56 75-01-4 IH,v104/17/23 17:0116.0 4.1 1
Xylene (Total)ND ug/kg 04/18/23 22:56 1330-20-704/17/23 17:0116.0 4.6 1
m&p-Xylene ND ug/kg 04/18/23 22:56 179601-23-104/17/23 17:0116.0 5.5 1
o-Xylene ND ug/kg 04/18/23 22:56 95-47-604/17/23 17:018.0 3.5 1
Surrogates
Toluene-d8 (S)101 %04/18/23 22:56 2037-26-504/17/23 17:0170-130 1
4-Bromofluorobenzene (S)104 %04/18/23 22:56 460-00-404/17/23 17:0170-130 1
1,2-Dichloroethane-d4 (S)104 %04/18/23 22:56 17060-07-004/17/23 17:0170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 21.2 %04/14/23 13:44 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (28-30)Lab ID:92662294002 Collected:04/12/23 14:55 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/19/23 16:59 N204/18/23 08:2813.1 13.1 1
Aliphatic (C19-C36)ND mg/kg 04/19/23 16:59 N204/18/23 08:2813.1 13.1 1
Aromatic (C11-C22)ND mg/kg 04/19/23 16:59 N204/18/23 08:2813.1 13.1 1
Surrogates
1-Chlorooctadecane (S)98 %04/19/23 16:59 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)79 %04/19/23 16:59 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)103 %04/19/23 16:59 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)108 %04/19/23 16:59 580-13-204/18/23 08:2840-140 1
Analytical Method: EPA 6020B Preparation Method: EPA 3050B
Pace Analytical Services - Minneapolis
6020B MET ICPMS
Chromium 38.8 mg/kg 04/19/23 13:21 7440-47-304/19/23 08:232.6 0.50 1
Lead 18.4 mg/kg 04/19/23 13:21 7439-92-104/19/23 08:230.64 0.12 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 04/21/23 12:29 83-32-904/20/23 16:514231491
Acenaphthylene ND ug/kg 04/21/23 12:29 208-96-804/20/23 16:514231491
Aniline ND ug/kg 04/21/23 12:29 62-53-304/20/23 16:514231651
Anthracene ND ug/kg 04/21/23 12:29 120-12-704/20/23 16:514231391
Benzo(a)anthracene ND ug/kg 04/21/23 12:29 56-55-304/20/23 16:514231411
Benzo(a)pyrene ND ug/kg 04/21/23 12:29 50-32-804/20/23 16:514231461
Benzo(b)fluoranthene ND ug/kg 04/21/23 12:29 205-99-204/20/23 16:514231411
Benzo(g,h,i)perylene ND ug/kg 04/21/23 12:29 191-24-204/20/23 16:514231641
Benzo(k)fluoranthene ND ug/kg 04/21/23 12:29 207-08-904/20/23 16:514231491
Benzoic Acid ND ug/kg 04/21/23 12:29 65-85-004/20/23 16:5121209091
Benzyl alcohol ND ug/kg 04/21/23 12:29 100-51-604/20/23 16:518463211
4-Bromophenylphenyl ether ND ug/kg 04/21/23 12:29 101-55-304/20/23 16:514231631
Butylbenzylphthalate ND ug/kg 04/21/23 12:29 85-68-704/20/23 16:514231781
4-Chloro-3-methylphenol ND ug/kg 04/21/23 12:29 59-50-704/20/23 16:518462981
4-Chloroaniline ND ug/kg 04/21/23 12:29 106-47-804/20/23 16:518463321
bis(2-Chloroethoxy)methane ND ug/kg 04/21/23 12:29 111-91-104/20/23 16:514231761
bis(2-Chloroethyl) ether ND ug/kg 04/21/23 12:29 111-44-404/20/23 16:514231591
2-Chloronaphthalene ND ug/kg 04/21/23 12:29 91-58-704/20/23 16:514231681
2-Chlorophenol ND ug/kg 04/21/23 12:29 95-57-804/20/23 16:514231591
4-Chlorophenylphenyl ether ND ug/kg 04/21/23 12:29 7005-72-304/20/23 16:514231581
Chrysene ND ug/kg 04/21/23 12:29 218-01-904/20/23 16:514231541
Dibenz(a,h)anthracene ND ug/kg 04/21/23 12:29 53-70-304/20/23 16:514231631
Dibenzofuran ND ug/kg 04/21/23 12:29 132-64-904/20/23 16:514231531
1,2-Dichlorobenzene ND ug/kg 04/21/23 12:29 95-50-104/20/23 16:514231531
1,3-Dichlorobenzene ND ug/kg 04/21/23 12:29 541-73-104/20/23 16:514231501
1,4-Dichlorobenzene ND ug/kg 04/21/23 12:29 106-46-704/20/23 16:514231621
3,3'-Dichlorobenzidine ND ug/kg 04/21/23 12:29 91-94-104/20/23 16:518462861
2,4-Dichlorophenol ND ug/kg 04/21/23 12:29 120-83-204/20/23 16:514231651
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (28-30)Lab ID:92662294002 Collected:04/12/23 14:55 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Diethylphthalate ND ug/kg 04/21/23 12:29 84-66-204/20/23 16:514231551
2,4-Dimethylphenol ND ug/kg 04/21/23 12:29 105-67-904/20/23 16:514231761
Dimethylphthalate ND ug/kg 04/21/23 12:29 131-11-304/20/23 16:514231541
Di-n-butylphthalate ND ug/kg 04/21/23 12:29 84-74-204/20/23 16:514231421
4,6-Dinitro-2-methylphenol ND ug/kg 04/21/23 12:29 534-52-104/20/23 16:518463951
2,4-Dinitrophenol ND ug/kg 04/21/23 12:29 51-28-504/20/23 16:51212013101
2,4-Dinitrotoluene ND ug/kg 04/21/23 12:29 121-14-204/20/23 16:514231631
2,6-Dinitrotoluene ND ug/kg 04/21/23 12:29 606-20-204/20/23 16:514231551
Di-n-octylphthalate ND ug/kg 04/21/23 12:29 117-84-004/20/23 16:514231671
bis(2-Ethylhexyl)phthalate ND ug/kg 04/21/23 12:29 117-81-704/20/23 16:514231641
Fluoranthene ND ug/kg 04/21/23 12:29 206-44-004/20/23 16:514231451
Fluorene ND ug/kg 04/21/23 12:29 86-73-704/20/23 16:514231491
Hexachloro-1,3-butadiene ND ug/kg 04/21/23 12:29 87-68-304/20/23 16:514231831
Hexachlorobenzene ND ug/kg 04/21/23 12:29 118-74-104/20/23 16:514231651
Hexachlorocyclopentadiene ND ug/kg 04/21/23 12:29 77-47-4 v204/20/23 16:514232421
Hexachloroethane ND ug/kg 04/21/23 12:29 67-72-104/20/23 16:514231621
Indeno(1,2,3-cd)pyrene ND ug/kg 04/21/23 12:29 193-39-504/20/23 16:514231671
Isophorone ND ug/kg 04/21/23 12:29 78-59-104/20/23 16:514231891
1-Methylnaphthalene ND ug/kg 04/21/23 12:29 90-12-004/20/23 16:514231491
2-Methylnaphthalene ND ug/kg 04/21/23 12:29 91-57-604/20/23 16:514231691
2-Methylphenol(o-Cresol)ND ug/kg 04/21/23 12:29 95-48-704/20/23 16:514231731
3&4-Methylphenol(m&p Cresol)ND ug/kg 04/21/23 12:29 15831-10-404/20/23 16:514231711
Naphthalene ND ug/kg 04/21/23 12:29 91-20-304/20/23 16:514231441
2-Nitroaniline ND ug/kg 04/21/23 12:29 88-74-404/20/23 16:5121203461
3-Nitroaniline ND ug/kg 04/21/23 12:29 99-09-204/20/23 16:5121203321
4-Nitroaniline ND ug/kg 04/21/23 12:29 100-01-604/20/23 16:518463221
Nitrobenzene ND ug/kg 04/21/23 12:29 98-95-304/20/23 16:514231961
2-Nitrophenol ND ug/kg 04/21/23 12:29 88-75-504/20/23 16:514231831
4-Nitrophenol ND ug/kg 04/21/23 12:29 100-02-704/20/23 16:5121208181
N-Nitrosodimethylamine ND ug/kg 04/21/23 12:29 62-75-904/20/23 16:514231421
N-Nitroso-di-n-propylamine ND ug/kg 04/21/23 12:29 621-64-704/20/23 16:514231591
N-Nitrosodiphenylamine ND ug/kg 04/21/23 12:29 86-30-604/20/23 16:514231501
2,2'-Oxybis(1-chloropropane)ND ug/kg 04/21/23 12:29 108-60-104/20/23 16:514232011
Pentachlorophenol ND ug/kg 04/21/23 12:29 87-86-504/20/23 16:518464141
Phenanthrene ND ug/kg 04/21/23 12:29 85-01-804/20/23 16:514231391
Phenol ND ug/kg 04/21/23 12:29 108-95-204/20/23 16:514231891
Pyrene ND ug/kg 04/21/23 12:29 129-00-004/20/23 16:514231721
Pyridine ND ug/kg 04/21/23 12:29 110-86-104/20/23 16:514231331
1,2,4-Trichlorobenzene ND ug/kg 04/21/23 12:29 120-82-104/20/23 16:514231671
2,4,5-Trichlorophenol ND ug/kg 04/21/23 12:29 95-95-404/20/23 16:514231941
2,4,6-Trichlorophenol ND ug/kg 04/21/23 12:29 88-06-204/20/23 16:514231741
Surrogates
Nitrobenzene-d5 (S)56 %04/21/23 12:29 4165-60-004/20/23 16:5110-130 1
2-Fluorobiphenyl (S)58 %04/21/23 12:29 321-60-804/20/23 16:5110-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (28-30)Lab ID:92662294002 Collected:04/12/23 14:55 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
Terphenyl-d14 (S)79 %04/21/23 12:29 1718-51-004/20/23 16:5110-130 1
Phenol-d6 (S)54 %04/21/23 12:29 13127-88-304/20/23 16:5110-130 1
2-Fluorophenol (S)54 %04/21/23 12:29 367-12-404/20/23 16:5110-130 1
2,4,6-Tribromophenol (S)66 %04/21/23 12:29 118-79-604/20/23 16:5110-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 04/18/23 23:14 67-64-104/17/23 17:0114044.9 1
Benzene ND ug/kg 04/18/23 23:14 71-43-204/17/23 17:017.0 2.8 1
Bromobenzene ND ug/kg 04/18/23 23:14 108-86-104/17/23 17:017.0 2.3 1
Bromochloromethane ND ug/kg 04/18/23 23:14 74-97-504/17/23 17:017.0 2.1 1
Bromodichloromethane ND ug/kg 04/18/23 23:14 75-27-404/17/23 17:017.0 2.7 1
Bromoform ND ug/kg 04/18/23 23:14 75-25-204/17/23 17:017.0 2.5 1
Bromomethane ND ug/kg 04/18/23 23:14 74-83-904/17/23 17:0128.0 21.7 1
2-Butanone (MEK)ND ug/kg 04/18/23 23:14 78-93-304/17/23 17:0114033.6 1
n-Butylbenzene ND ug/kg 04/18/23 23:14 104-51-804/17/23 17:017.0 4.4 1
sec-Butylbenzene ND ug/kg 04/18/23 23:14 135-98-804/17/23 17:017.0 3.1 1
tert-Butylbenzene ND ug/kg 04/18/23 23:14 98-06-604/17/23 17:017.0 2.5 1
Carbon tetrachloride ND ug/kg 04/18/23 23:14 56-23-504/17/23 17:017.0 2.6 1
Chlorobenzene ND ug/kg 04/18/23 23:14 108-90-704/17/23 17:017.0 4.0 1
Chloroethane ND ug/kg 04/18/23 23:14 75-00-3 IH,v104/17/23 17:0114.0 5.4 1
Chloroform ND ug/kg 04/18/23 23:14 67-66-304/17/23 17:017.0 5.9 1
Chloromethane ND ug/kg 04/18/23 23:14 74-87-3 IH,L1,
v104/17/23 17:0114.0 5.9 1
2-Chlorotoluene ND ug/kg 04/18/23 23:14 95-49-804/17/23 17:017.0 2.5 1
4-Chlorotoluene ND ug/kg 04/18/23 23:14 106-43-404/17/23 17:017.0 3.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 04/18/23 23:14 96-12-804/17/23 17:017.0 2.7 1
Dibromochloromethane ND ug/kg 04/18/23 23:14 124-48-104/17/23 17:017.0 3.9 1
1,2-Dibromoethane (EDB)ND ug/kg 04/18/23 23:14 106-93-404/17/23 17:017.0 3.1 1
Dibromomethane ND ug/kg 04/18/23 23:14 74-95-304/17/23 17:017.0 1.5 1
1,2-Dichlorobenzene ND ug/kg 04/18/23 23:14 95-50-104/17/23 17:017.0 2.5 1
1,3-Dichlorobenzene ND ug/kg 04/18/23 23:14 541-73-104/17/23 17:017.0 2.2 1
1,4-Dichlorobenzene ND ug/kg 04/18/23 23:14 106-46-704/17/23 17:017.0 1.8 1
Dichlorodifluoromethane ND ug/kg 04/18/23 23:14 75-71-8 IH,L1,
v104/17/23 17:0114.0 7.1 1
1,1-Dichloroethane ND ug/kg 04/18/23 23:14 75-34-304/17/23 17:017.0 2.9 1
1,2-Dichloroethane ND ug/kg 04/18/23 23:14 107-06-204/17/23 17:017.0 4.6 1
1,1-Dichloroethene ND ug/kg 04/18/23 23:14 75-35-404/17/23 17:017.0 2.9 1
cis-1,2-Dichloroethene ND ug/kg 04/18/23 23:14 156-59-204/17/23 17:017.0 2.4 1
trans-1,2-Dichloroethene ND ug/kg 04/18/23 23:14 156-60-504/17/23 17:017.0 6.0 1
1,2-Dichloropropane ND ug/kg 04/18/23 23:14 78-87-504/17/23 17:017.0 2.1 1
1,3-Dichloropropane ND ug/kg 04/18/23 23:14 142-28-904/17/23 17:017.0 2.2 1
2,2-Dichloropropane ND ug/kg 04/18/23 23:14 594-20-704/17/23 17:017.0 5.3 1
1,1-Dichloropropene ND ug/kg 04/18/23 23:14 563-58-604/17/23 17:017.0 3.4 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
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Huntersville, NC 28078
[phone]
Page 18 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (28-30)Lab ID:92662294002 Collected:04/12/23 14:55 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
cis-1,3-Dichloropropene ND ug/kg 04/18/23 23:14 10061-01-504/17/23 17:017.0 1.9 1
trans-1,3-Dichloropropene ND ug/kg 04/18/23 23:14 10061-02-604/17/23 17:017.0 2.4 1
Diisopropyl ether ND ug/kg 04/18/23 23:14 108-20-304/17/23 17:017.0 1.9 1
Ethylbenzene ND ug/kg 04/18/23 23:14 100-41-404/17/23 17:017.0 3.3 1
Hexachloro-1,3-butadiene ND ug/kg 04/18/23 23:14 87-68-3 v104/17/23 17:0114.0 11.5 1
2-Hexanone ND ug/kg 04/18/23 23:14 591-78-604/17/23 17:0170.0 6.7 1
Isopropylbenzene (Cumene)ND ug/kg 04/18/23 23:14 98-82-804/17/23 17:017.0 2.4 1
p-Isopropyltoluene ND ug/kg 04/18/23 23:14 99-87-604/17/23 17:017.0 3.4 1
Methylene Chloride 122 ug/kg 04/18/23 23:14 75-09-2 C904/17/23 17:0128.0 19.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 04/18/23 23:14 108-10-104/17/23 17:0170.0 6.7 1
Methyl-tert-butyl ether ND ug/kg 04/18/23 23:14 1634-04-404/17/23 17:017.0 2.6 1
Naphthalene ND ug/kg 04/18/23 23:14 91-20-304/17/23 17:017.0 3.7 1
n-Propylbenzene ND ug/kg 04/18/23 23:14 103-65-104/17/23 17:017.0 2.5 1
Styrene ND ug/kg 04/18/23 23:14 100-42-504/17/23 17:017.0 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 04/18/23 23:14 630-20-604/17/23 17:017.0 2.7 1
1,1,2,2-Tetrachloroethane ND ug/kg 04/18/23 23:14 79-34-504/17/23 17:017.0 1.8 1
Tetrachloroethene ND ug/kg 04/18/23 23:14 127-18-404/17/23 17:017.0 2.2 1
Toluene ND ug/kg 04/18/23 23:14 108-88-304/17/23 17:017.0 4.8 1
1,2,3-Trichlorobenzene ND ug/kg 04/18/23 23:14 87-61-6 v104/17/23 17:017.0 5.7 1
1,2,4-Trichlorobenzene ND ug/kg 04/18/23 23:14 120-82-104/17/23 17:017.0 5.9 1
1,1,1-Trichloroethane ND ug/kg 04/18/23 23:14 71-55-604/17/23 17:017.0 3.6 1
1,1,2-Trichloroethane ND ug/kg 04/18/23 23:14 79-00-504/17/23 17:017.0 2.3 1
Trichloroethene ND ug/kg 04/18/23 23:14 79-01-604/17/23 17:017.0 5.6 1
Trichlorofluoromethane ND ug/kg 04/18/23 23:14 75-69-404/17/23 17:017.0 3.9 1
1,2,3-Trichloropropane ND ug/kg 04/18/23 23:14 96-18-404/17/23 17:017.0 3.5 1
1,2,4-Trimethylbenzene ND ug/kg 04/18/23 23:14 95-63-604/17/23 17:017.0 4.2 1
1,3,5-Trimethylbenzene ND ug/kg 04/18/23 23:14 108-67-804/17/23 17:017.0 2.4 1
Vinyl acetate ND ug/kg 04/18/23 23:14 108-05-404/17/23 17:0170.0 14.4 1
Vinyl chloride ND ug/kg 04/18/23 23:14 75-01-4 IH,v104/17/23 17:0114.0 3.6 1
Xylene (Total)ND ug/kg 04/18/23 23:14 1330-20-704/17/23 17:0114.0 4.0 1
m&p-Xylene ND ug/kg 04/18/23 23:14 179601-23-104/17/23 17:0114.0 4.8 1
o-Xylene ND ug/kg 04/18/23 23:14 95-47-604/17/23 17:017.0 3.1 1
Surrogates
Toluene-d8 (S)100 %04/18/23 23:14 2037-26-504/17/23 17:0170-130 1
4-Bromofluorobenzene (S)106 %04/18/23 23:14 460-00-404/17/23 17:0170-130 1
1,2-Dichloroethane-d4 (S)104 %04/18/23 23:14 17060-07-004/17/23 17:0170-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 23.1 %04/14/23 13:44 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (8-10)Lab ID:92662294003 Collected:04/12/23 14:25 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/19/23 17:25 N204/18/23 08:2812.3 12.3 1
Aliphatic (C19-C36)79.1 mg/kg 04/19/23 17:25 N204/18/23 08:2812.3 12.3 1
Aromatic (C11-C22)15.3 mg/kg 04/19/23 17:25 N204/18/23 08:2812.3 12.3 1
Surrogates
1-Chlorooctadecane (S)102 %04/19/23 17:25 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)75 %04/19/23 17:25 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)91 %04/19/23 17:25 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)93 %04/19/23 17:25 580-13-204/18/23 08:2840-140 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 18.6 %04/14/23 13:44 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 70
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662294
ACF-001
Sample:HHSB-1 (18-20)Lab ID:92662294004 Collected:04/12/23 14:40 Received:04/14/23 09:29 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 04/19/23 17:50 N204/18/23 08:2812.6 12.6 1
Aliphatic (C19-C36)51.3 mg/kg 04/19/23 17:50 N204/18/23 08:2812.6 12.6 1
Aromatic (C11-C22)ND mg/kg 04/19/23 17:50 N204/18/23 08:2812.6 12.6 1
Surrogates
1-Chlorooctadecane (S)109 %04/19/23 17:50 3386-33-204/18/23 08:2840-140 1
o-Terphenyl (S)75 %04/19/23 17:50 84-15-104/18/23 08:2840-140 1
2-Fluorobiphenyl (S)94 %04/19/23 17:50 321-60-804/18/23 08:2840-140 1
2-Bromonaphthalene (S)95 %04/19/23 17:50 580-13-204/18/23 08:2840-140 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 22.2 %04/14/23 13:45 N20.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
876278
EPA 3050B
EPA 6020B
6020B Solids UPD5
Laboratory:Pace Analytical Services - Minneapolis
Associated Lab Samples:92662294001, 92662294002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4620895
Associated Lab Samples:92662294001, 92662294002
Matrix:Solid
AnalyzedMDL
Chromium mg/kg ND 2.0 04/19/23 13:000.38
Lead mg/kg ND 0.49 04/19/23 13:000.092
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4620896LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium mg/kg 52.349.1 106 80-120
Lead mg/kg 49.949.1 102 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4620897MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662294001
4620898
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium mg/kg 61.4 113 75-125110 1 206226.1 95.6 94.3
Lead mg/kg 61.4 108 75-125104 2 206221.1 87.4 85.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768510
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662294001, 92662294002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3990169
Associated Lab Samples:92662294001, 92662294002
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 04/18/23 14:581.9
1,1,1-Trichloroethane ug/kg ND 5.0 04/18/23 14:582.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 04/18/23 14:581.3
1,1,2-Trichloroethane ug/kg ND 5.0 04/18/23 14:581.7
1,1-Dichloroethane ug/kg ND 5.0 04/18/23 14:582.1
1,1-Dichloroethene ug/kg ND 5.0 04/18/23 14:582.1
1,1-Dichloropropene ug/kg ND 5.0 04/18/23 14:582.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 v104/18/23 14:584.0
1,2,3-Trichloropropane ug/kg ND 5.0 04/18/23 14:582.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 04/18/23 14:584.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 04/18/23 14:583.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 04/18/23 14:581.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 04/18/23 14:582.2
1,2-Dichlorobenzene ug/kg ND 5.0 04/18/23 14:581.8
1,2-Dichloroethane ug/kg ND 5.0 04/18/23 14:583.3
1,2-Dichloropropane ug/kg ND 5.0 04/18/23 14:581.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 04/18/23 14:581.7
1,3-Dichlorobenzene ug/kg ND 5.0 04/18/23 14:581.6
1,3-Dichloropropane ug/kg ND 5.0 04/18/23 14:581.6
1,4-Dichlorobenzene ug/kg ND 5.0 04/18/23 14:581.3
2,2-Dichloropropane ug/kg ND 5.0 04/18/23 14:583.8
2-Butanone (MEK)ug/kg ND 100 04/18/23 14:5824.0
2-Chlorotoluene ug/kg ND 5.0 04/18/23 14:581.8
2-Hexanone ug/kg ND 50.0 04/18/23 14:584.8
4-Chlorotoluene ug/kg ND 5.0 04/18/23 14:582.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 04/18/23 14:584.8
Acetone ug/kg ND 100 04/18/23 14:5832.1
Benzene ug/kg ND 5.0 04/18/23 14:582.0
Bromobenzene ug/kg ND 5.0 04/18/23 14:581.6
Bromochloromethane ug/kg ND 5.0 04/18/23 14:581.5
Bromodichloromethane ug/kg ND 5.0 04/18/23 14:581.9
Bromoform ug/kg ND 5.0 04/18/23 14:581.8
Bromomethane ug/kg ND 20.0 04/18/23 14:5815.5
Carbon tetrachloride ug/kg ND 5.0 04/18/23 14:581.9
Chlorobenzene ug/kg ND 5.0 04/18/23 14:582.9
Chloroethane ug/kg ND 10.0 IH,v104/18/23 14:583.9
Chloroform ug/kg 8.6 5.0 04/18/23 14:584.2
Chloromethane ug/kg ND 10.0 IH,v104/18/23 14:584.2
cis-1,2-Dichloroethene ug/kg ND 5.0 04/18/23 14:581.7
cis-1,3-Dichloropropene ug/kg ND 5.0 04/18/23 14:581.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3990169
Associated Lab Samples:92662294001, 92662294002
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 04/18/23 14:582.8
Dibromomethane ug/kg ND 5.0 04/18/23 14:581.1
Dichlorodifluoromethane ug/kg ND 10.0 IH,v104/18/23 14:585.1
Diisopropyl ether ug/kg ND 5.0 04/18/23 14:581.4
Ethylbenzene ug/kg ND 5.0 04/18/23 14:582.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 v104/18/23 14:588.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 04/18/23 14:581.7
m&p-Xylene ug/kg ND 10.0 04/18/23 14:583.4
Methyl-tert-butyl ether ug/kg ND 5.0 04/18/23 14:581.9
Methylene Chloride ug/kg ND 20.0 04/18/23 14:5813.7
n-Butylbenzene ug/kg 5.1 5.0 04/18/23 14:583.2
n-Propylbenzene ug/kg ND 5.0 04/18/23 14:581.8
Naphthalene ug/kg ND 5.0 04/18/23 14:582.6
o-Xylene ug/kg ND 5.0 04/18/23 14:582.2
p-Isopropyltoluene ug/kg ND 5.0 04/18/23 14:582.5
sec-Butylbenzene ug/kg 3.0J 5.0 04/18/23 14:582.2
Styrene ug/kg ND 5.0 04/18/23 14:581.3
tert-Butylbenzene ug/kg ND 5.0 04/18/23 14:581.8
Tetrachloroethene ug/kg ND 5.0 04/18/23 14:581.6
Toluene ug/kg ND 5.0 04/18/23 14:583.4
trans-1,2-Dichloroethene ug/kg ND 5.0 04/18/23 14:584.2
trans-1,3-Dichloropropene ug/kg ND 5.0 04/18/23 14:581.7
Trichloroethene ug/kg ND 5.0 04/18/23 14:584.0
Trichlorofluoromethane ug/kg ND 5.0 04/18/23 14:582.8
Vinyl acetate ug/kg ND 50.0 04/18/23 14:5810.3
Vinyl chloride ug/kg ND 10.0 IH,v104/18/23 14:582.5
Xylene (Total)ug/kg ND 10.0 04/18/23 14:582.8
1,2-Dichloroethane-d4 (S)%104 70-130 04/18/23 14:58
4-Bromofluorobenzene (S)%97 70-130 04/18/23 14:58
Toluene-d8 (S)%100 70-130 04/18/23 14:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3990170LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 513500 103 70-130
1,1,1-Trichloroethane ug/kg 514500 103 70-130
1,1,2,2-Tetrachloroethane ug/kg 474500 95 70-130
1,1,2-Trichloroethane ug/kg 496500 99 70-130
1,1-Dichloroethane ug/kg 476500 95 70-130
1,1-Dichloroethene ug/kg 543500 109 70-130
1,1-Dichloropropene ug/kg 541500 108 70-130
1,2,3-Trichlorobenzene ug/kg 548 v150011070-130
1,2,3-Trichloropropane ug/kg 468500 94 70-130
1,2,4-Trichlorobenzene ug/kg 551500 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3990170LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 540500 108 70-130
1,2-Dibromo-3-chloropropane ug/kg 459500 92 67-130
1,2-Dibromoethane (EDB)ug/kg 456500 91 70-130
1,2-Dichlorobenzene ug/kg 518500 104 70-130
1,2-Dichloroethane ug/kg 487500 97 70-130
1,2-Dichloropropane ug/kg 449500 90 70-130
1,3,5-Trimethylbenzene ug/kg 512500 102 70-130
1,3-Dichlorobenzene ug/kg 502500 100 70-130
1,3-Dichloropropane ug/kg 480500 96 70-130
1,4-Dichlorobenzene ug/kg 472500 94 70-130
2,2-Dichloropropane ug/kg 403500 81 67-130
2-Butanone (MEK)ug/kg 9591000 96 66-130
2-Chlorotoluene ug/kg 521500 104 70-130
2-Hexanone ug/kg 9991000 100 70-130
4-Chlorotoluene ug/kg 522500 104 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 10001000 100 70-130
Acetone ug/kg 9741000 97 67-130
Benzene ug/kg 457500 91 70-130
Bromobenzene ug/kg 485500 97 70-130
Bromochloromethane ug/kg 485500 97 70-130
Bromodichloromethane ug/kg 491500 98 70-130
Bromoform ug/kg 452500 90 70-130
Bromomethane ug/kg 459500 92 53-175
Carbon tetrachloride ug/kg 510500 102 70-130
Chlorobenzene ug/kg 496500 99 70-130
Chloroethane ug/kg 602 IH,v150012070-135
Chloroform ug/kg 495500 99 70-130
Chloromethane ug/kg 807 IH,L1,v150016164-130
cis-1,2-Dichloroethene ug/kg 503500 101 70-130
cis-1,3-Dichloropropene ug/kg 481500 96 70-130
Dibromochloromethane ug/kg 474500 95 70-130
Dibromomethane ug/kg 494500 99 70-130
Dichlorodifluoromethane ug/kg 862 IH,L1,v150017263-145
Diisopropyl ether ug/kg 500500 100 68-130
Ethylbenzene ug/kg 481500 96 70-130
Hexachloro-1,3-butadiene ug/kg 574 v150011570-130
Isopropylbenzene (Cumene)ug/kg 527500 105 70-130
m&p-Xylene ug/kg 10301000 103 70-130
Methyl-tert-butyl ether ug/kg 469500 94 70-130
Methylene Chloride ug/kg 508500 102 67-130
n-Butylbenzene ug/kg 529500 106 70-130
n-Propylbenzene ug/kg 529500 106 70-130
Naphthalene ug/kg 495500 99 70-130
o-Xylene ug/kg 533500 107 70-130
p-Isopropyltoluene ug/kg 533500 107 70-130
sec-Butylbenzene ug/kg 535500 107 70-130
Styrene ug/kg 488500 98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3990170LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 480500 96 64-130
Tetrachloroethene ug/kg 513500 103 70-130
Toluene ug/kg 501500 100 70-130
trans-1,2-Dichloroethene ug/kg 514500 103 70-130
trans-1,3-Dichloropropene ug/kg 473500 95 70-130
Trichloroethene ug/kg 543500 109 70-130
Trichlorofluoromethane ug/kg 543500 109 70-130
Vinyl acetate ug/kg 9731000 97 70-134
Vinyl chloride ug/kg 642 IH,v150012868-130
Xylene (Total)ug/kg 15701500 104 70-130
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3990171MATRIX SPIKE SAMPLE:
MSSpike
Result
92662091006
1,1,1,2-Tetrachloroethane ug/kg 791826 96 58-140ND
1,1,1-Trichloroethane ug/kg 793826 96 58-144ND
1,1,2,2-Tetrachloroethane ug/kg 782826 95 52-139ND
1,1,2-Trichloroethane ug/kg 796826 96 56-140ND
1,1-Dichloroethane ug/kg 830826 101 58-145ND
1,1-Dichloroethene ug/kg 848826 103 57-158ND
1,1-Dichloropropene ug/kg 788826 95 58-151ND
1,2,3-Trichlorobenzene ug/kg 547 v18266648-149ND
1,2,3-Trichloropropane ug/kg 753826 91 54-132ND
1,2,4-Trichlorobenzene ug/kg 611826 74 51-151ND
1,2,4-Trimethylbenzene ug/kg 760826 92 38-170ND
1,2-Dibromo-3-chloropropane ug/kg 561826 68 44-134ND
1,2-Dibromoethane (EDB)ug/kg 745826 90 60-138ND
1,2-Dichlorobenzene ug/kg 758826 92 59-147ND
1,2-Dichloroethane ug/kg 774826 94 57-139ND
1,2-Dichloropropane ug/kg 766826 93 62-145ND
1,3,5-Trimethylbenzene ug/kg 731826 89 47-159ND
1,3-Dichlorobenzene ug/kg 697826 84 58-144ND
1,3-Dichloropropane ug/kg 817826 99 60-142ND
1,4-Dichlorobenzene ug/kg 658826 80 57-143ND
2,2-Dichloropropane ug/kg 539826 65 37-144ND
2-Butanone (MEK)ug/kg 15101650 91 28-146ND
2-Chlorotoluene ug/kg 771826 93 55-158ND
2-Hexanone ug/kg 14801650 90 44-141ND
4-Chlorotoluene ug/kg 735826 89 55-146ND
4-Methyl-2-pentanone (MIBK)ug/kg 15101650 91 50-138ND
Acetone ug/kg 16601650 100 20-136ND
Benzene ug/kg 735826 89 60-145ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3990171MATRIX SPIKE SAMPLE:
MSSpike
Result
92662091006
Bromobenzene ug/kg 716826 87 59-145ND
Bromochloromethane ug/kg 767826 93 57-143ND
Bromodichloromethane ug/kg 744826 90 53-133ND
Bromoform ug/kg 690826 84 48-133ND
Bromomethane ug/kg 616826 75 10-167ND
Carbon tetrachloride ug/kg 759826 92 57-147ND
Chlorobenzene ug/kg 770826 93 61-144ND
Chloroethane ug/kg 706 IH,v18268510-153ND
Chloroform ug/kg 783826 95 58-141ND
Chloromethane ug/kg 1100 IH,v182613354-165ND
cis-1,2-Dichloroethene ug/kg 810826 98 59-144ND
cis-1,3-Dichloropropene ug/kg 765826 93 56-137ND
Dibromochloromethane ug/kg 735826 89 53-139ND
Dibromomethane ug/kg 773826 94 60-136ND
Dichlorodifluoromethane ug/kg 1190 IH,v182614349-177ND
Diisopropyl ether ug/kg 785826 95 53-136ND
Ethylbenzene ug/kg 731826 88 53-150ND
Hexachloro-1,3-butadiene ug/kg 611 v18267442-186ND
Isopropylbenzene (Cumene)ug/kg 785826 95 62-154ND
m&p-Xylene ug/kg 15301650 92 49-156ND
Methyl-tert-butyl ether ug/kg 752826 91 54-133ND
Methylene Chloride ug/kg 916 C98269650-153125
n-Butylbenzene ug/kg 703826 85 44-174ND
n-Propylbenzene ug/kg 737826 89 52-157ND
Naphthalene ug/kg 509826 62 37-150ND
o-Xylene ug/kg 797826 95 54-1509.3
p-Isopropyltoluene ug/kg 714826 85 50-16411.3
sec-Butylbenzene ug/kg 752826 91 58-161ND
Styrene ug/kg 732826 89 60-148ND
tert-Butylbenzene ug/kg 726826 88 44-151ND
Tetrachloroethene ug/kg 683826 83 53-151ND
Toluene ug/kg 773826 93 52-148ND
trans-1,2-Dichloroethene ug/kg 749826 91 60-148ND
trans-1,3-Dichloropropene ug/kg 731826 89 55-133ND
Trichloroethene ug/kg 751826 91 60-148ND
Trichlorofluoromethane ug/kg 484826 59 10-154ND
Vinyl acetate ug/kg 11501650 69 50-149ND
Vinyl chloride ug/kg 997 IH,v182612157-157ND
Xylene (Total)ug/kg 23302470 94 52-153ND
1,2-Dichloroethane-d4 (S)%95 70-130
4-Bromofluorobenzene (S)%106 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662091007
3990172SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND v130ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg ND 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg 4.9J 30ND
Chloroethane ug/kg ND IH,v130ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND IH,v130ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND IH,v130ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 6.0J 30ND
Hexachloro-1,3-butadiene ug/kg ND v130ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662091007
3990172SAMPLE DUPLICATE:
m&p-Xylene ug/kg 10.2J 30ND
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg 181 C91930219
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg 10.2 19 308.4
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 6.0J 30ND
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND IH,v130ND
Xylene (Total)ug/kg 10.2J 30ND
1,2-Dichloroethane-d4 (S)%104104
4-Bromofluorobenzene (S)%108104
Toluene-d8 (S)%101102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768315
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662294001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3989138
Associated Lab Samples:92662294001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 331 04/16/23 09:11130
1,2-Dichlorobenzene ug/kg ND 331 04/16/23 09:11119
1,3-Dichlorobenzene ug/kg ND 331 04/16/23 09:11117
1,4-Dichlorobenzene ug/kg ND 331 04/16/23 09:11126
1-Methylnaphthalene ug/kg ND 331 04/16/23 09:11116
2,2'-Oxybis(1-chloropropane)ug/kg ND 331 04/16/23 09:11158
2,4,5-Trichlorophenol ug/kg ND 331 04/16/23 09:11152
2,4,6-Trichlorophenol ug/kg ND 331 04/16/23 09:11136
2,4-Dichlorophenol ug/kg ND 331 04/16/23 09:11129
2,4-Dimethylphenol ug/kg ND 331 04/16/23 09:11137
2,4-Dinitrophenol ug/kg ND 1660 04/16/23 09:111020
2,4-Dinitrotoluene ug/kg ND 331 04/16/23 09:11127
2,6-Dinitrotoluene ug/kg ND 331 04/16/23 09:11121
2-Chloronaphthalene ug/kg ND 331 04/16/23 09:11131
2-Chlorophenol ug/kg ND 331 04/16/23 09:11124
2-Methylnaphthalene ug/kg ND 331 04/16/23 09:11132
2-Methylphenol(o-Cresol)ug/kg ND 331 04/16/23 09:11135
2-Nitroaniline ug/kg ND 1660 04/16/23 09:11271
2-Nitrophenol ug/kg ND 331 04/16/23 09:11143
3&4-Methylphenol(m&p Cresol)ug/kg ND 331 04/16/23 09:11133
3,3'-Dichlorobenzidine ug/kg ND 662 04/16/23 09:11224
3-Nitroaniline ug/kg ND 1660 04/16/23 09:11260
4,6-Dinitro-2-methylphenol ug/kg ND 662 04/16/23 09:11309
4-Bromophenylphenyl ether ug/kg ND 331 04/16/23 09:11127
4-Chloro-3-methylphenol ug/kg ND 662 04/16/23 09:11233
4-Chloroaniline ug/kg ND 662 04/16/23 09:11260
4-Chlorophenylphenyl ether ug/kg ND 331 04/16/23 09:11123
4-Nitroaniline ug/kg ND 662 04/16/23 09:11252
4-Nitrophenol ug/kg ND 1660 04/16/23 09:11640
Acenaphthene ug/kg ND 331 04/16/23 09:11116
Acenaphthylene ug/kg ND 331 04/16/23 09:11116
Aniline ug/kg ND 331 04/16/23 09:11129
Anthracene ug/kg ND 331 04/16/23 09:11108
Benzo(a)anthracene ug/kg ND 331 04/16/23 09:11110
Benzo(a)pyrene ug/kg ND 331 04/16/23 09:11114
Benzo(b)fluoranthene ug/kg ND 331 04/16/23 09:11110
Benzo(g,h,i)perylene ug/kg ND 331 04/16/23 09:11128
Benzo(k)fluoranthene ug/kg ND 331 04/16/23 09:11116
Benzoic Acid ug/kg ND 1660 04/16/23 09:11711
Benzyl alcohol ug/kg ND 662 04/16/23 09:11251
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3989138
Associated Lab Samples:92662294001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 331 04/16/23 09:11137
bis(2-Chloroethyl) ether ug/kg ND 331 04/16/23 09:11124
bis(2-Ethylhexyl)phthalate ug/kg ND 331 04/16/23 09:11128
Butylbenzylphthalate ug/kg ND 331 04/16/23 09:11139
Chrysene ug/kg ND 331 04/16/23 09:11120
Di-n-butylphthalate ug/kg ND 331 04/16/23 09:11111
Di-n-octylphthalate ug/kg ND 331 04/16/23 09:11130
Dibenz(a,h)anthracene ug/kg ND 331 04/16/23 09:11127
Dibenzofuran ug/kg ND 331 04/16/23 09:11119
Diethylphthalate ug/kg ND 331 04/16/23 09:11121
Dimethylphthalate ug/kg ND 331 04/16/23 09:11120
Fluoranthene ug/kg ND 331 04/16/23 09:11113
Fluorene ug/kg ND 331 04/16/23 09:11116
Hexachloro-1,3-butadiene ug/kg ND 331 04/16/23 09:11143
Hexachlorobenzene ug/kg ND 331 04/16/23 09:11129
Hexachlorocyclopentadiene ug/kg ND 331 04/16/23 09:11190
Hexachloroethane ug/kg ND 331 04/16/23 09:11126
Indeno(1,2,3-cd)pyrene ug/kg ND 331 04/16/23 09:11130
Isophorone ug/kg ND 331 04/16/23 09:11147
N-Nitroso-di-n-propylamine ug/kg ND 331 04/16/23 09:11124
N-Nitrosodimethylamine ug/kg ND 331 04/16/23 09:11111
N-Nitrosodiphenylamine ug/kg ND 331 04/16/23 09:11117
Naphthalene ug/kg ND 331 04/16/23 09:11112
Nitrobenzene ug/kg ND 331 04/16/23 09:11154
Pentachlorophenol ug/kg ND 662 04/16/23 09:11324
Phenanthrene ug/kg ND 331 04/16/23 09:11108
Phenol ug/kg ND 331 04/16/23 09:11147
Pyrene ug/kg ND 331 04/16/23 09:11134
Pyridine ug/kg ND 331 04/16/23 09:11104
2,4,6-Tribromophenol (S)%59 10-131 04/16/23 09:11
2-Fluorobiphenyl (S)%60 10-130 04/16/23 09:11
2-Fluorophenol (S)%54 10-130 04/16/23 09:11
Nitrobenzene-d5 (S)%57 10-130 04/16/23 09:11
Phenol-d6 (S)%54 10-130 04/16/23 09:11
Terphenyl-d14 (S)%70 10-130 04/16/23 09:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989137LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 11301670 68 43-130
1,2-Dichlorobenzene ug/kg 11101670 66 43-130
1,3-Dichlorobenzene ug/kg 10901670 65 43-130
1,4-Dichlorobenzene ug/kg 10901670 65 44-130
1-Methylnaphthalene ug/kg 12001670 72 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989137LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 9851670 59 29-130
2,4,5-Trichlorophenol ug/kg 12301670 73 47-130
2,4,6-Trichlorophenol ug/kg 12401670 74 47-130
2,4-Dichlorophenol ug/kg 12701670 76 45-130
2,4-Dimethylphenol ug/kg 17201670 103 45-130
2,4-Dinitrophenol ug/kg 38608360 46 27-140
2,4-Dinitrotoluene ug/kg 12101670 72 46-130
2,6-Dinitrotoluene ug/kg 12301670 73 48-130
2-Chloronaphthalene ug/kg 11401670 68 46-130
2-Chlorophenol ug/kg 11801670 71 43-130
2-Methylnaphthalene ug/kg 11301670 68 47-130
2-Methylphenol(o-Cresol)ug/kg 12201670 73 42-130
2-Nitroaniline ug/kg 22403340 67 41-130
2-Nitrophenol ug/kg 11601670 69 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 11801670 71 39-130
3,3'-Dichlorobenzidine ug/kg 20303340 61 41-130
3-Nitroaniline ug/kg 20003340 60 37-130
4,6-Dinitro-2-methylphenol ug/kg 22203340 66 38-141
4-Bromophenylphenyl ether ug/kg 11701670 70 47-130
4-Chloro-3-methylphenol ug/kg 24303340 73 44-130
4-Chloroaniline ug/kg 22003340 66 41-130
4-Chlorophenylphenyl ether ug/kg 11601670 69 45-130
4-Nitroaniline ug/kg 21703340 65 42-130
4-Nitrophenol ug/kg 59808360 72 39-131
Acenaphthene ug/kg 11701670 70 49-130
Acenaphthylene ug/kg 12001670 72 50-130
Aniline ug/kg 9761670 58 38-130
Anthracene ug/kg 11301670 67 49-130
Benzo(a)anthracene ug/kg 12201670 73 51-130
Benzo(a)pyrene ug/kg 13001670 78 51-130
Benzo(b)fluoranthene ug/kg 12901670 77 49-130
Benzo(g,h,i)perylene ug/kg 14001670 84 48-140
Benzo(k)fluoranthene ug/kg 13601670 81 51-130
Benzoic Acid ug/kg 834J L283601022-130
Benzyl alcohol ug/kg 21803340 65 43-130
bis(2-Chloroethoxy)methane ug/kg 10601670 64 43-130
bis(2-Chloroethyl) ether ug/kg 10501670 63 42-130
bis(2-Ethylhexyl)phthalate ug/kg 12001670 72 43-130
Butylbenzylphthalate ug/kg 12201670 73 44-131
Chrysene ug/kg 12401670 74 51-130
Di-n-butylphthalate ug/kg 11501670 69 46-130
Di-n-octylphthalate ug/kg 11701670 70 45-130
Dibenz(a,h)anthracene ug/kg 13801670 82 48-130
Dibenzofuran ug/kg 11701670 70 10-130
Diethylphthalate ug/kg 11901670 71 48-130
Dimethylphthalate ug/kg 11801670 70 48-130
Fluoranthene ug/kg 11801670 71 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989137LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 12001670 72 48-130
Hexachloro-1,3-butadiene ug/kg 11001670 66 39-130
Hexachlorobenzene ug/kg 11501670 69 47-130
Hexachlorocyclopentadiene ug/kg 12301670 74 17-130
Hexachloroethane ug/kg 11001670 66 40-130
Indeno(1,2,3-cd)pyrene ug/kg 14301670 85 50-130
Isophorone ug/kg 11301670 68 41-130
N-Nitroso-di-n-propylamine ug/kg 10801670 64 36-130
N-Nitrosodimethylamine ug/kg 10901670 65 34-130
N-Nitrosodiphenylamine ug/kg 11801670 70 48-130
Naphthalene ug/kg 11301670 68 46-130
Nitrobenzene ug/kg 10801670 65 39-130
Pentachlorophenol ug/kg 21803340 65 42-130
Phenanthrene ug/kg 12001670 72 50-130
Phenol ug/kg 12601670 76 42-130
Pyrene ug/kg 12701670 76 50-130
Pyridine ug/kg 8671670 52 26-130
2,4,6-Tribromophenol (S)%72 10-131
2-Fluorobiphenyl (S)%68 10-130
2-Fluorophenol (S)%68 10-130
Nitrobenzene-d5 (S)%65 10-130
Phenol-d6 (S)%67 10-130
Terphenyl-d14 (S)%75 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3989139MATRIX SPIKE SAMPLE:
MSSpike
Result
92661774001
1,2,4-Trichlorobenzene ug/kg 10801830 59 16-130ND
1,2-Dichlorobenzene ug/kg 10001830 55 19-130ND
1,3-Dichlorobenzene ug/kg 9821830 53 19-130ND
1,4-Dichlorobenzene ug/kg 9951830 54 20-130ND
1-Methylnaphthalene ug/kg 10401830 57 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 8941830 49 10-130ND
2,4,5-Trichlorophenol ug/kg 10701830 58 19-130ND
2,4,6-Trichlorophenol ug/kg 11501830 63 18-130ND
2,4-Dichlorophenol ug/kg 11901830 65 16-130ND
2,4-Dimethylphenol ug/kg 17401830 95 10-130ND
2,4-Dinitrophenol ug/kg 52709190 57 10-143ND
2,4-Dinitrotoluene ug/kg 8131830 44 19-130ND
2,6-Dinitrotoluene ug/kg 11701830 64 22-130ND
2-Chloronaphthalene ug/kg 9271830 50 18-130ND
2-Chlorophenol ug/kg 10601830 58 20-130ND
2-Methylnaphthalene ug/kg 9751830 53 18-130ND
2-Methylphenol(o-Cresol)ug/kg 10601830 58 13-130ND
2-Nitroaniline ug/kg 19203670 52 18-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3989139MATRIX SPIKE SAMPLE:
MSSpike
Result
92661774001
2-Nitrophenol ug/kg 12001830 65 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 10401830 57 13-130ND
3,3'-Dichlorobenzidine ug/kg 17003670 46 10-130ND
3-Nitroaniline ug/kg 1590J3670 43 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 22703670 62 10-144ND
4-Bromophenylphenyl ether ug/kg 11601830 63 18-130ND
4-Chloro-3-methylphenol ug/kg 20103670 55 16-130ND
4-Chloroaniline ug/kg 18503670 50 17-130ND
4-Chlorophenylphenyl ether ug/kg 10601830 58 17-130ND
4-Nitroaniline ug/kg 16903670 46 21-130ND
4-Nitrophenol ug/kg 50309190 55 13-131ND
Acenaphthene ug/kg 9621830 52 20-130ND
Acenaphthylene ug/kg 10101830 55 21-130ND
Aniline ug/kg 7721830 42 10-130ND
Anthracene ug/kg 9921830 54 19-130ND
Benzo(a)anthracene ug/kg 10801830 59 17-130ND
Benzo(a)pyrene ug/kg 11501830 63 14-130ND
Benzo(b)fluoranthene ug/kg 12101830 66 11-134ND
Benzo(g,h,i)perylene ug/kg 10001830 55 12-130ND
Benzo(k)fluoranthene ug/kg 12701830 69 15-130ND
Benzoic Acid ug/kg 48109190 52 10-130ND
Benzyl alcohol ug/kg 18603670 51 20-130ND
bis(2-Chloroethoxy)methane ug/kg 9801830 53 16-130ND
bis(2-Chloroethyl) ether ug/kg 9611830 52 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 10801830 59 11-130ND
Butylbenzylphthalate ug/kg 10201830 56 10-130ND
Chrysene ug/kg 11101830 61 17-130ND
Di-n-butylphthalate ug/kg 10101830 55 16-130ND
Di-n-octylphthalate ug/kg 10101830 55 16-130ND
Dibenz(a,h)anthracene ug/kg 10301830 56 13-130ND
Dibenzofuran ug/kg 10401830 57 19-130ND
Diethylphthalate ug/kg 9531830 52 22-130ND
Dimethylphthalate ug/kg 8161830 44 23-130ND
Fluoranthene ug/kg 11701830 64 14-130ND
Fluorene ug/kg 9611830 52 19-130ND
Hexachloro-1,3-butadiene ug/kg 11101830 61 12-130ND
Hexachlorobenzene ug/kg 12601830 68 17-130ND
Hexachlorocyclopentadiene ug/kg 11901830 65 10-130ND
Hexachloroethane ug/kg 10201830 55 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 10701830 58 13-130ND
Isophorone ug/kg 9761830 53 17-130ND
N-Nitroso-di-n-propylamine ug/kg 10001830 55 10-130ND
N-Nitrosodimethylamine ug/kg 9201830 50 16-130ND
N-Nitrosodiphenylamine ug/kg 15101830 82 19-130ND
Naphthalene ug/kg 10301830 56 18-130ND
Nitrobenzene ug/kg 10301830 56 15-130ND
Pentachlorophenol ug/kg 21903670 60 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3989139MATRIX SPIKE SAMPLE:
MSSpike
Result
92661774001
Phenanthrene ug/kg 10501830 57 17-130ND
Phenol ug/kg 11001830 60 15-130ND
Pyrene ug/kg 11101830 60 31-130ND
Pyridine ug/kg 6361830 35 10-130ND
2,4,6-Tribromophenol (S)%66 10-131
2-Fluorobiphenyl (S)%53 10-130
2-Fluorophenol (S)%52 10-130
Nitrobenzene-d5 (S)%56 10-130
Phenol-d6 (S)%51 10-130
Terphenyl-d14 (S)%63 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92661946008
3989140SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg 1290J 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92661946008
3989140SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg 2680 0 302.7 mg/kg
Benzo(a)anthracene ug/kg 8890 11 307.9 mg/kg
Benzo(a)pyrene ug/kg 7650 14 306.6 mg/kg
Benzo(b)fluoranthene ug/kg 11600 10 3010.5 mg/kg
Benzo(g,h,i)perylene ug/kg 5510 14 304.8 mg/kg
Benzo(k)fluoranthene ug/kg 4830 13 304.2 mg/kg
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg 9290 6 308.8 mg/kg
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg 1800J 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg 14900 4 3014.3 mg/kg
Fluorene ug/kg 1160J 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND 30ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg 5180 16 304.4 mg/kg
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg 12600 6 3013.3 mg/kg
Phenol ug/kg ND 30ND
Pyrene ug/kg 16200 8 3015.0 mg/kg
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%3937
2-Fluorobiphenyl (S)%3834
2-Fluorophenol (S)%3729
Nitrobenzene-d5 (S)%49 D347
Phenol-d6 (S)%4840
Terphenyl-d14 (S)%6361
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
769298
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662294002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3994086
Associated Lab Samples:92662294002
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 331 04/21/23 10:38130
1,2-Dichlorobenzene ug/kg ND 331 04/21/23 10:38119
1,3-Dichlorobenzene ug/kg ND 331 04/21/23 10:38117
1,4-Dichlorobenzene ug/kg ND 331 04/21/23 10:38126
1-Methylnaphthalene ug/kg ND 331 04/21/23 10:38116
2,2'-Oxybis(1-chloropropane)ug/kg ND 331 04/21/23 10:38158
2,4,5-Trichlorophenol ug/kg ND 331 04/21/23 10:38152
2,4,6-Trichlorophenol ug/kg ND 331 04/21/23 10:38136
2,4-Dichlorophenol ug/kg ND 331 04/21/23 10:38129
2,4-Dimethylphenol ug/kg ND 331 04/21/23 10:38137
2,4-Dinitrophenol ug/kg ND 1660 04/21/23 10:381020
2,4-Dinitrotoluene ug/kg ND 331 04/21/23 10:38127
2,6-Dinitrotoluene ug/kg ND 331 04/21/23 10:38121
2-Chloronaphthalene ug/kg ND 331 04/21/23 10:38131
2-Chlorophenol ug/kg ND 331 04/21/23 10:38124
2-Methylnaphthalene ug/kg ND 331 04/21/23 10:38132
2-Methylphenol(o-Cresol)ug/kg ND 331 04/21/23 10:38135
2-Nitroaniline ug/kg ND 1660 04/21/23 10:38271
2-Nitrophenol ug/kg ND 331 04/21/23 10:38143
3&4-Methylphenol(m&p Cresol)ug/kg ND 331 04/21/23 10:38133
3,3'-Dichlorobenzidine ug/kg ND 662 04/21/23 10:38224
3-Nitroaniline ug/kg ND 1660 04/21/23 10:38260
4,6-Dinitro-2-methylphenol ug/kg ND 662 04/21/23 10:38309
4-Bromophenylphenyl ether ug/kg ND 331 04/21/23 10:38127
4-Chloro-3-methylphenol ug/kg ND 662 04/21/23 10:38233
4-Chloroaniline ug/kg ND 662 04/21/23 10:38260
4-Chlorophenylphenyl ether ug/kg ND 331 04/21/23 10:38123
4-Nitroaniline ug/kg ND 662 04/21/23 10:38252
4-Nitrophenol ug/kg ND 1660 04/21/23 10:38640
Acenaphthene ug/kg ND 331 04/21/23 10:38116
Acenaphthylene ug/kg ND 331 04/21/23 10:38116
Aniline ug/kg ND 331 04/21/23 10:38129
Anthracene ug/kg ND 331 04/21/23 10:38108
Benzo(a)anthracene ug/kg ND 331 04/21/23 10:38110
Benzo(a)pyrene ug/kg ND 331 04/21/23 10:38114
Benzo(b)fluoranthene ug/kg ND 331 04/21/23 10:38110
Benzo(g,h,i)perylene ug/kg ND 331 04/21/23 10:38128
Benzo(k)fluoranthene ug/kg ND 331 04/21/23 10:38116
Benzoic Acid ug/kg ND 1660 04/21/23 10:38711
Benzyl alcohol ug/kg ND 662 04/21/23 10:38251
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3994086
Associated Lab Samples:92662294002
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 331 04/21/23 10:38137
bis(2-Chloroethyl) ether ug/kg ND 331 04/21/23 10:38124
bis(2-Ethylhexyl)phthalate ug/kg ND 331 04/21/23 10:38128
Butylbenzylphthalate ug/kg ND 331 04/21/23 10:38139
Chrysene ug/kg ND 331 04/21/23 10:38120
Di-n-butylphthalate ug/kg ND 331 04/21/23 10:38111
Di-n-octylphthalate ug/kg ND 331 04/21/23 10:38130
Dibenz(a,h)anthracene ug/kg ND 331 04/21/23 10:38127
Dibenzofuran ug/kg ND 331 04/21/23 10:38119
Diethylphthalate ug/kg ND 331 04/21/23 10:38121
Dimethylphthalate ug/kg ND 331 04/21/23 10:38120
Fluoranthene ug/kg ND 331 04/21/23 10:38113
Fluorene ug/kg ND 331 04/21/23 10:38116
Hexachloro-1,3-butadiene ug/kg ND 331 04/21/23 10:38143
Hexachlorobenzene ug/kg ND 331 04/21/23 10:38129
Hexachlorocyclopentadiene ug/kg ND 331 v204/21/23 10:38190
Hexachloroethane ug/kg ND 331 04/21/23 10:38126
Indeno(1,2,3-cd)pyrene ug/kg ND 331 04/21/23 10:38130
Isophorone ug/kg ND 331 04/21/23 10:38147
N-Nitroso-di-n-propylamine ug/kg ND 331 04/21/23 10:38124
N-Nitrosodimethylamine ug/kg ND 331 04/21/23 10:38111
N-Nitrosodiphenylamine ug/kg ND 331 04/21/23 10:38117
Naphthalene ug/kg ND 331 04/21/23 10:38112
Nitrobenzene ug/kg ND 331 04/21/23 10:38154
Pentachlorophenol ug/kg ND 662 04/21/23 10:38324
Phenanthrene ug/kg ND 331 04/21/23 10:38108
Phenol ug/kg ND 331 04/21/23 10:38147
Pyrene ug/kg ND 331 04/21/23 10:38134
Pyridine ug/kg ND 331 04/21/23 10:38104
2,4,6-Tribromophenol (S)%63 10-131 04/21/23 10:38
2-Fluorobiphenyl (S)%64 10-130 04/21/23 10:38
2-Fluorophenol (S)%57 10-130 04/21/23 10:38
Nitrobenzene-d5 (S)%60 10-130 04/21/23 10:38
Phenol-d6 (S)%57 10-130 04/21/23 10:38
Terphenyl-d14 (S)%86 10-130 04/21/23 10:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3994087LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 9871660 59 43-130
1,2-Dichlorobenzene ug/kg 9661660 58 43-130
1,3-Dichlorobenzene ug/kg 9271660 56 43-130
1,4-Dichlorobenzene ug/kg 9391660 57 44-130
1-Methylnaphthalene ug/kg 11201660 68 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3994087LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 8111660 49 29-130
2,4,5-Trichlorophenol ug/kg 12501660 75 47-130
2,4,6-Trichlorophenol ug/kg 12201660 73 47-130
2,4-Dichlorophenol ug/kg 10901660 65 45-130
2,4-Dimethylphenol ug/kg 15401660 92 45-130
2,4-Dinitrophenol ug/kg 52808310 64 27-140
2,4-Dinitrotoluene ug/kg 12601660 76 46-130
2,6-Dinitrotoluene ug/kg 12601660 76 48-130
2-Chloronaphthalene ug/kg 11001660 66 46-130
2-Chlorophenol ug/kg 9841660 59 43-130
2-Methylnaphthalene ug/kg 10401660 63 47-130
2-Methylphenol(o-Cresol)ug/kg 10201660 62 42-130
2-Nitroaniline ug/kg 22903320 69 41-130
2-Nitrophenol ug/kg 10601660 64 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 10401660 62 39-130
3,3'-Dichlorobenzidine ug/kg 23103320 69 41-130
3-Nitroaniline ug/kg 23003320 69 37-130
4,6-Dinitro-2-methylphenol ug/kg 23403320 70 38-141
4-Bromophenylphenyl ether ug/kg 12301660 74 47-130
4-Chloro-3-methylphenol ug/kg 24003320 72 44-130
4-Chloroaniline ug/kg 20303320 61 41-130
4-Chlorophenylphenyl ether ug/kg 11901660 71 45-130
4-Nitroaniline ug/kg 23703320 71 42-130
4-Nitrophenol ug/kg 61808310 74 39-131
Acenaphthene ug/kg 11801660 71 49-130
Acenaphthylene ug/kg 12001660 73 50-130
Aniline ug/kg 8021660 48 38-130
Anthracene ug/kg 12001660 72 49-130
Benzo(a)anthracene ug/kg 12901660 77 51-130
Benzo(a)pyrene ug/kg 13601660 82 51-130
Benzo(b)fluoranthene ug/kg 14201660 85 49-130
Benzo(g,h,i)perylene ug/kg 14601660 88 48-140
Benzo(k)fluoranthene ug/kg 14601660 88 51-130
Benzoic Acid ug/kg 41408310 50 22-130
Benzyl alcohol ug/kg 19003320 57 43-130
bis(2-Chloroethoxy)methane ug/kg 9371660 56 43-130
bis(2-Chloroethyl) ether ug/kg 8911660 54 42-130
bis(2-Ethylhexyl)phthalate ug/kg 14401660 87 43-130
Butylbenzylphthalate ug/kg 14901660 90 44-131
Chrysene ug/kg 13001660 79 51-130
Di-n-butylphthalate ug/kg 12101660 73 46-130
Di-n-octylphthalate ug/kg 13601660 82 45-130
Dibenz(a,h)anthracene ug/kg 14501660 87 48-130
Dibenzofuran ug/kg 11901660 72 10-130
Diethylphthalate ug/kg 12101660 73 48-130
Dimethylphthalate ug/kg 12001660 72 48-130
Fluoranthene ug/kg 12501660 76 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3994087LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 12401660 74 48-130
Hexachloro-1,3-butadiene ug/kg 9161660 55 39-130
Hexachlorobenzene ug/kg 12301660 74 47-130
Hexachlorocyclopentadiene ug/kg 769 v316604617-130
Hexachloroethane ug/kg 8821660 53 40-130
Indeno(1,2,3-cd)pyrene ug/kg 14801660 89 50-130
Isophorone ug/kg 10701660 64 41-130
N-Nitroso-di-n-propylamine ug/kg 9831660 59 36-130
N-Nitrosodimethylamine ug/kg 9061660 55 34-130
N-Nitrosodiphenylamine ug/kg 12401660 75 48-130
Naphthalene ug/kg 10101660 61 46-130
Nitrobenzene ug/kg 9641660 58 39-130
Pentachlorophenol ug/kg 24203320 73 42-130
Phenanthrene ug/kg 12801660 77 50-130
Phenol ug/kg 10801660 65 42-130
Pyrene ug/kg 15101660 91 50-130
Pyridine ug/kg 7081660 43 26-130
2,4,6-Tribromophenol (S)%76 10-131
2-Fluorobiphenyl (S)%63 10-130
2-Fluorophenol (S)%54 10-130
Nitrobenzene-d5 (S)%56 10-130
Phenol-d6 (S)%56 10-130
Terphenyl-d14 (S)%88 10-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3994088MATRIX SPIKE SAMPLE:
MSSpike
Result
92661946006
1,2,4-Trichlorobenzene ug/kg 9841900 52 16-130ND
1,2-Dichlorobenzene ug/kg 9471900 50 19-130ND
1,3-Dichlorobenzene ug/kg 9171900 48 19-130ND
1,4-Dichlorobenzene ug/kg 9351900 49 20-130ND
1-Methylnaphthalene ug/kg 10401900 55 19-130ND
2,2'-Oxybis(1-chloropropane)ug/kg 8111900 43 10-130ND
2,4,5-Trichlorophenol ug/kg 12201900 64 19-130ND
2,4,6-Trichlorophenol ug/kg 11601900 61 18-130ND
2,4-Dichlorophenol ug/kg 10701900 56 16-130ND
2,4-Dimethylphenol ug/kg 8371900 44 10-130ND
2,4-Dinitrophenol ug/kg 20009530 21 10-143ND
2,4-Dinitrotoluene ug/kg 12301900 64 19-130ND
2,6-Dinitrotoluene ug/kg 12301900 65 22-130ND
2-Chloronaphthalene ug/kg 10801900 57 18-130ND
2-Chlorophenol ug/kg 9401900 49 20-130ND
2-Methylnaphthalene ug/kg 9991900 52 18-130ND
2-Methylphenol(o-Cresol)ug/kg 7621900 40 13-130ND
2-Nitroaniline ug/kg 22003810 58 18-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
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Page 40 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3994088MATRIX SPIKE SAMPLE:
MSSpike
Result
92661946006
2-Nitrophenol ug/kg 10401900 55 19-130ND
3&4-Methylphenol(m&p Cresol)ug/kg 8051900 42 13-130ND
3,3'-Dichlorobenzidine ug/kg 17503810 46 10-130ND
3-Nitroaniline ug/kg 23303810 61 22-130ND
4,6-Dinitro-2-methylphenol ug/kg 18303810 48 10-144ND
4-Bromophenylphenyl ether ug/kg 11901900 62 18-130ND
4-Chloro-3-methylphenol ug/kg 21503810 56 16-130ND
4-Chloroaniline ug/kg 18603810 49 17-130ND
4-Chlorophenylphenyl ether ug/kg 11001900 58 17-130ND
4-Nitroaniline ug/kg 23203810 61 21-130ND
4-Nitrophenol ug/kg 59509530 62 13-131ND
Acenaphthene ug/kg 11101900 58 20-130ND
Acenaphthylene ug/kg 11401900 60 21-130ND
Aniline ug/kg 5941900 31 10-130ND
Anthracene ug/kg 11001900 58 19-130ND
Benzo(a)anthracene ug/kg 11801900 62 17-130ND
Benzo(a)pyrene ug/kg 12701900 67 14-130ND
Benzo(b)fluoranthene ug/kg 12801900 67 11-134ND
Benzo(g,h,i)perylene ug/kg 13901900 68 12-130ND
Benzo(k)fluoranthene ug/kg 13601900 71 15-130ND
Benzoic Acid ug/kg ND M19530210-130ND
Benzyl alcohol ug/kg 18703810 49 20-130ND
bis(2-Chloroethoxy)methane ug/kg 9091900 48 16-130ND
bis(2-Chloroethyl) ether ug/kg 8801900 46 18-130ND
bis(2-Ethylhexyl)phthalate ug/kg 13701900 72 11-130ND
Butylbenzylphthalate ug/kg 13601900 72 10-130ND
Chrysene ug/kg 12101900 64 17-130ND
Di-n-butylphthalate ug/kg 11301900 60 16-130ND
Di-n-octylphthalate ug/kg 12101900 63 16-130ND
Dibenz(a,h)anthracene ug/kg 13701900 72 13-130ND
Dibenzofuran ug/kg 11201900 59 19-130ND
Diethylphthalate ug/kg 11701900 61 22-130ND
Dimethylphthalate ug/kg 11701900 61 23-130ND
Fluoranthene ug/kg 10501900 55 14-130ND
Fluorene ug/kg 11501900 60 19-130ND
Hexachloro-1,3-butadiene ug/kg 9071900 48 12-130ND
Hexachlorobenzene ug/kg 12001900 63 17-130ND
Hexachlorocyclopentadiene ug/kg 575 v319003010-130ND
Hexachloroethane ug/kg 8671900 45 14-130ND
Indeno(1,2,3-cd)pyrene ug/kg 14201900 75 13-130ND
Isophorone ug/kg 9941900 52 17-130ND
N-Nitroso-di-n-propylamine ug/kg 9391900 49 10-130ND
N-Nitrosodimethylamine ug/kg 9011900 47 16-130ND
N-Nitrosodiphenylamine ug/kg 10801900 57 19-130ND
Naphthalene ug/kg 9861900 52 18-130ND
Nitrobenzene ug/kg 9291900 49 15-130ND
Pentachlorophenol ug/kg 22403810 59 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3994088MATRIX SPIKE SAMPLE:
MSSpike
Result
92661946006
Phenanthrene ug/kg 12001900 63 17-130ND
Phenol ug/kg 9651900 51 15-130ND
Pyrene ug/kg 14001900 71 31-130ND
Pyridine ug/kg 8001900 42 10-130ND
2,4,6-Tribromophenol (S)%50 10-131
2-Fluorobiphenyl (S)%50 10-130
2-Fluorophenol (S)%34 10-130
Nitrobenzene-d5 (S)%50 10-130
Phenol-d6 (S)%41 10-130
Terphenyl-d14 (S)%77 10-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662294002
3994089SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
1-Methylnaphthalene ug/kg ND 30ND
2,2'-Oxybis(1-chloropropane)ug/kg ND 30ND
2,4,5-Trichlorophenol ug/kg ND 30ND
2,4,6-Trichlorophenol ug/kg ND 30ND
2,4-Dichlorophenol ug/kg ND 30ND
2,4-Dimethylphenol ug/kg ND 30ND
2,4-Dinitrophenol ug/kg ND 30ND
2,4-Dinitrotoluene ug/kg ND 30ND
2,6-Dinitrotoluene ug/kg ND 30ND
2-Chloronaphthalene ug/kg ND 30ND
2-Chlorophenol ug/kg ND 30ND
2-Methylnaphthalene ug/kg ND 30ND
2-Methylphenol(o-Cresol)ug/kg ND 30ND
2-Nitroaniline ug/kg ND 30ND
2-Nitrophenol ug/kg ND 30ND
3&4-Methylphenol(m&p Cresol)ug/kg ND 30ND
3,3'-Dichlorobenzidine ug/kg ND 30ND
3-Nitroaniline ug/kg ND 30ND
4,6-Dinitro-2-methylphenol ug/kg ND 30ND
4-Bromophenylphenyl ether ug/kg ND 30ND
4-Chloro-3-methylphenol ug/kg ND 30ND
4-Chloroaniline ug/kg ND 30ND
4-Chlorophenylphenyl ether ug/kg ND 30ND
4-Nitroaniline ug/kg ND 30ND
4-Nitrophenol ug/kg ND 30ND
Acenaphthene ug/kg ND 30ND
Acenaphthylene ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662294002
3994089SAMPLE DUPLICATE:
Aniline ug/kg ND 30ND
Anthracene ug/kg ND 30ND
Benzo(a)anthracene ug/kg ND 30ND
Benzo(a)pyrene ug/kg ND 30ND
Benzo(b)fluoranthene ug/kg ND 30ND
Benzo(g,h,i)perylene ug/kg ND 30ND
Benzo(k)fluoranthene ug/kg ND 30ND
Benzoic Acid ug/kg ND 30ND
Benzyl alcohol ug/kg ND 30ND
bis(2-Chloroethoxy)methane ug/kg ND 30ND
bis(2-Chloroethyl) ether ug/kg ND 30ND
bis(2-Ethylhexyl)phthalate ug/kg ND 30ND
Butylbenzylphthalate ug/kg ND 30ND
Chrysene ug/kg ND 30ND
Di-n-butylphthalate ug/kg ND 30ND
Di-n-octylphthalate ug/kg ND 30ND
Dibenz(a,h)anthracene ug/kg ND 30ND
Dibenzofuran ug/kg ND 30ND
Diethylphthalate ug/kg ND 30ND
Dimethylphthalate ug/kg ND 30ND
Fluoranthene ug/kg ND 30ND
Fluorene ug/kg ND 30ND
Hexachloro-1,3-butadiene ug/kg ND 30ND
Hexachlorobenzene ug/kg ND 30ND
Hexachlorocyclopentadiene ug/kg ND v230ND
Hexachloroethane ug/kg ND 30ND
Indeno(1,2,3-cd)pyrene ug/kg ND 30ND
Isophorone ug/kg ND 30ND
N-Nitroso-di-n-propylamine ug/kg ND 30ND
N-Nitrosodimethylamine ug/kg ND 30ND
N-Nitrosodiphenylamine ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
Nitrobenzene ug/kg ND 30ND
Pentachlorophenol ug/kg ND 30ND
Phenanthrene ug/kg ND 30ND
Phenol ug/kg ND 30ND
Pyrene ug/kg ND 30ND
Pyridine ug/kg ND 30ND
2,4,6-Tribromophenol (S)%6566
2-Fluorobiphenyl (S)%5758
2-Fluorophenol (S)%5454
Nitrobenzene-d5 (S)%5756
Phenol-d6 (S)%5554
Terphenyl-d14 (S)%7579
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768569
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662294001, 92662294002, 92662294003, 92662294004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3990298
Associated Lab Samples:92662294001, 92662294002, 92662294003, 92662294004
Matrix:Solid
AnalyzedMDL
Aliphatic (C09-C18)mg/kg ND 10.1 N204/19/23 08:3110.1
Aliphatic (C19-C36)mg/kg ND 10.1 N204/19/23 08:3110.1
Aromatic (C11-C22)mg/kg ND 10.1 N204/19/23 08:3110.1
1-Chlorooctadecane (S)%114 40-140 04/19/23 08:31
2-Bromonaphthalene (S)%90 40-140 04/19/23 08:31
2-Fluorobiphenyl (S)%85 40-140 04/19/23 08:31
o-Terphenyl (S)%85 40-140 04/19/23 08:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3990299LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3990300
Aliphatic (C09-C18)mg/kg ND N210.1 77 40-14078ND 50
Aliphatic (C19-C36)mg/kg 17.7 N213.5 131 40-14013618.0 2 50
Aromatic (C11-C22)mg/kg 27.1 N228.7 94 40-1409426.5 2 50
1-Chlorooctadecane (S)%121 40-140124
2-Bromonaphthalene (S)%95 40-14095
2-Fluorobiphenyl (S)%90 40-14089
o-Terphenyl (S)%93 40-14090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 70
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662294
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768197
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662294001, 92662294002, 92662294003, 92662294004
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92661748005
3988459SAMPLE DUPLICATE:
Percent Moisture %16.1 N252517.1
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92662205002
3988460SAMPLE DUPLICATE:
Percent Moisture %92.0 N202592.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
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9800 Kincey Ave. Suite 100
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[phone]
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92662294
ACF-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Common Laboratory Contaminant.C9
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 46 of 70
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92662294
ACF-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92662294001 768569 768765HHSB-1 (0-2)MADEP EPH MADEP EPH
92662294002 768569 768765HHSB-1 (28-30)MADEP EPH MADEP EPH
92662294003 768569 768765HHSB-1 (8-10)MADEP EPH MADEP EPH
92662294004 768569 768765HHSB-1 (18-20)MADEP EPH MADEP EPH
92662294001 876278 876392HHSB-1 (0-2)EPA 3050B EPA 6020B
92662294002 876278 876392HHSB-1 (28-30)EPA 3050B EPA 6020B
92662294001 768315 768346HHSB-1 (0-2)EPA 3546 EPA 8270E
92662294002 769298 769492HHSB-1 (28-30)EPA 3546 EPA 8270E
92662294001 768510 768907HHSB-1 (0-2)EPA 5035A/5030B EPA 8260D
92662294002 768510 768907HHSB-1 (28-30)EPA 5035A/5030B EPA 8260D
92662294001 768197HHSB-1 (0-2)SW-846
92662294002 768197HHSB-1 (28-30)SW-846
92662294003 768197HHSB-1 (8-10)SW-846
92662294004 768197HHSB-1 (18-20)SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:41 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 47 of 70
Page 48 of 70
Page 49 of 70
Page 50 of 70
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 21, 2023
Taylor Cannon
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: ACF-001
Client Job Number:
Project Number: 92662294
Laboratory Work Order Number: 23D1950
Enclosed are results of analyses for samples as received by the laboratory on April 18, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 20
Table of Contents
Page 51 of 70
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23D1950-01 5
23D1950-02 7
23D1950-03 9
23D1950-04 11
Sample Preparation Information 13
QC Data 14
Petroleum Hydrocarbons Analyses - VPH 14
B337638 14
Flag/Qualifier Summary 16
Certifications 17
Chain of Custody/Sample Receipt 18
Page 2 of 20
Table of Contents
Page 52 of 70
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/21/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Taylor Cannon
92662294
23D1950
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
ACF-001
HHSB-1 (0-2)23D1950-01 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
HHSB-1 (28-30)23D1950-02 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
HHSB-1 (8-10)23D1950-03 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
HHSB-1 (18-20)23D1950-04 Soil MADEP-VPH-Feb
2018 Rev 2.1
SM 2540G
[TOC_1]Sample Summary[TOC]
Page 3 of 20
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
SM 2540G
Qualifications:
Sample was extracted past the recommended holding time.
Analyte & Samples(s) Qualified:
H-06
% Solids
23D1950-01[HHSB-1 (0-2)], 23D1950-02[HHSB-1 (28-30)], 23D1950-03[HHSB-1 (8-10)], 23D1950-04[HHSB-1 (18-20)]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 4 of 20
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-01
Field Sample #: HHSB-1 (0-2)
Sample Matrix: Soil
Sampled: 4/12/2023 14:10
[TOC_2]23D1950-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.10
Petroleum Hydrocarbons Analyses - VPH
ND 14 4/19/23 13:46 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 14 4/19/23 13:46 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 14 4/19/23 13:46 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 14 4/19/23 13:46 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 14 4/19/23 13:46 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)102 4/19/23 13:4670-130
2,5-Dibromotoluene (PID)101 4/19/23 13:4670-130
[TOC_1]Sample Results[TOC]
Page 5 of 20
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-01
Field Sample #: HHSB-1 (0-2)
Sample Matrix: Soil
Sampled: 4/12/2023 14:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.1 4/20/23 6:34 WDC% Wt 4/20/23SM 2540G1H-06% Solids
Page 6 of 20
Table of Contents
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-02
Field Sample #: HHSB-1 (28-30)
Sample Matrix: Soil
Sampled: 4/12/2023 14:55
[TOC_2]23D1950-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.14
Petroleum Hydrocarbons Analyses - VPH
ND 13 4/19/23 14:16 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 13 4/19/23 14:16 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 13 4/19/23 14:16 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 13 4/19/23 14:16 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 13 4/19/23 14:16 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)101 4/19/23 14:1670-130
2,5-Dibromotoluene (PID)99.7 4/19/23 14:1670-130
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Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-02
Field Sample #: HHSB-1 (28-30)
Sample Matrix: Soil
Sampled: 4/12/2023 14:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.7 4/20/23 6:34 WDC% Wt 4/20/23SM 2540G1H-06% Solids
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Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-03
Field Sample #: HHSB-1 (8-10)
Sample Matrix: Soil
Sampled: 4/12/2023 14:25
[TOC_2]23D1950-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.20
Petroleum Hydrocarbons Analyses - VPH
ND 13 4/19/23 14:45 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 13 4/19/23 14:45 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 13 4/19/23 14:45 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 13 4/19/23 14:45 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 13 4/19/23 14:45 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)95.6 4/19/23 14:4570-130
2,5-Dibromotoluene (PID)96.9 4/19/23 14:4570-130
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Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-03
Field Sample #: HHSB-1 (8-10)
Sample Matrix: Soil
Sampled: 4/12/2023 14:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.6 4/20/23 6:34 WDC% Wt 4/20/23SM 2540G1H-06% Solids
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Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-04
Field Sample #: HHSB-1 (18-20)
Sample Matrix: Soil
Sampled: 4/12/2023 14:40
[TOC_2]23D1950-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.15
Petroleum Hydrocarbons Analyses - VPH
ND 16 4/19/23 15:15 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 16 4/19/23 15:15 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 16 4/19/23 15:15 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 16 4/19/23 15:15 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 16 4/19/23 15:15 EEHmg/Kg dry 4/19/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)104 4/19/23 15:1570-130
2,5-Dibromotoluene (PID)99.3 4/19/23 15:1570-130
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Date Received: 4/18/2023
Work Order: 23D1950Sample Description:Project Location: ACF-001
Sample ID: 23D1950-04
Field Sample #: HHSB-1 (18-20)
Sample Matrix: Soil
Sampled: 4/12/2023 14:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
73.1 4/20/23 6:34 WDC% Wt 4/20/23SM 2540G1H-06% Solids
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Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B337638 04/19/2311.0 12.323D1950-01 [HHSB-1 (0-2)]
B337638 04/19/2311.4 12.023D1950-02 [HHSB-1 (28-30)]
B337638 04/19/2312.0 12.323D1950-03 [HHSB-1 (8-10)]
B337638 04/19/2311.5 13.123D1950-04 [HHSB-1 (18-20)]
Prep Method: % Solids Analytical Method: SM 2540G
Lab Number [Field ID]Batch Date
B337727 04/20/2323D1950-01 [HHSB-1 (0-2)]
B337727 04/20/2323D1950-02 [HHSB-1 (28-30)]
B337727 04/20/2323D1950-03 [HHSB-1 (8-10)]
B337727 04/20/2323D1950-04 [HHSB-1 (18-20)]
[TOC_1]Sample Preparation Information[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B337638 - MA VPH
[TOC_3]B337638[TOC]
Blank (B337638-BLK1) Prepared & Analyzed: 04/19/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)86.334.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)85.134.0
LCS (B337638-BS1) Prepared & Analyzed: 04/19/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 70-13095.27.14
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 70-13099.27.44
C9-C10 Aromatics mg/Kg wet10 2.50 70-1301042.61
Benzene mg/Kg wet0.050 2.50 70-1301092.72
Butylcyclohexane mg/Kg wet0.050 2.50 70-1301082.69
Decane mg/Kg wet0.050 2.50 70-13080.42.01
Ethylbenzene mg/Kg wet0.050 2.50 70-1301062.65
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 70-1301062.65
2-Methylpentane mg/Kg wet0.050 2.50 70-1301012.52
Naphthalene mg/Kg wet0.50 2.50 70-13078.01.95
Nonane mg/Kg wet0.050 2.50 30-1301092.73
Pentane mg/Kg wet0.050 2.50 70-13091.12.28
Toluene mg/Kg wet0.050 2.50 70-1301072.67
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 70-1301042.61
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 70-13093.92.35
m+p Xylene mg/Kg wet0.10 5.00 70-1301055.26
o-Xylene mg/Kg wet0.050 2.50 70-1301072.67
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10441.6
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10843.0
[TOC_1]QC Data[TOC]
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B337638 - MA VPH
LCS Dup (B337638-BSD1) Prepared & Analyzed: 04/19/23
Unadjusted C5-C8 Aliphatics mg/Kg wet10 7.50 2570-13094.5 0.8067.08
Unadjusted C9-C12 Aliphatics mg/Kg wet10 7.50 2570-13097.0 2.247.27
C9-C10 Aromatics mg/Kg wet10 2.50 2570-130105 0.9502.63
Benzene mg/Kg wet0.050 2.50 2570-130111 1.842.77
Butylcyclohexane mg/Kg wet0.050 2.50 2570-130105 2.242.63
Decane mg/Kg wet0.050 2.50 2570-13078.2 2.831.95
Ethylbenzene mg/Kg wet0.050 2.50 2570-130108 1.712.69
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050 2.50 2570-130106 0.5972.66
2-Methylpentane mg/Kg wet0.050 2.50 2570-130100 0.2432.51
Naphthalene mg/Kg wet0.50 2.50 2570-13080.5 3.202.01
Nonane mg/Kg wet0.050 2.50 2530-130107 1.812.68
Pentane mg/Kg wet0.050 2.50 2570-13090.1 1.082.25
Toluene mg/Kg wet0.050 2.50 2570-130108 1.232.70
1,2,4-Trimethylbenzene mg/Kg wet0.050 2.50 2570-130105 0.9502.63
2,2,4-Trimethylpentane mg/Kg wet0.050 2.50 2570-13092.8 1.152.32
m+p Xylene mg/Kg wet0.10 5.00 2570-130107 1.625.35
o-Xylene mg/Kg wet0.050 2.50 2570-130108 1.062.70
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10943.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11144.6
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Sample was extracted past the recommended holding time.H-06
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Soil
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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#=CL#
April 26, 2023
LIMS USE: FR - JOHN LOPEZ
LIMS OBJECT ID: 92662340
92662340
Project:
Pace Project No.:
RE:
John Lopez
Hart & Hickman
2923 S. Tryon St
Suite 100
Charlotte, NC 28203
ACF-001
Dear John Lopez:
Enclosed are the analytical results for sample(s) received by the laboratory on April 14, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 51
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92662340
ACF-001
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 51
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92662340
ACF-001
Lab ID Sample ID Matrix Date Collected Date Received
92662340001 HH TMW-1 Water 04/13/23 13:00 04/14/23 09:29
92662340002 TRIP BLANK Water 04/13/23 00:00 04/14/23 09:29
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 51
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92662340
ACF-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92662340001 HH TMW-1 MADEP EPH 7 PASI-CBAJ
EPA 6020B 2 PASI-AKRL
EPA 625.1 68 PASI-CPKS
SM 6200B 63 PASI-CLMB
92662340002 TRIP BLANK SM 6200B 63 PASI-CLMB
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 51
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662340
ACF-001
Method:
Client:Hart & Hickman
MADEP EPH
Date:April 26, 2023
Description:MADEP EPH NC Water
General Information:
1 sample was analyzed for MADEP EPH by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 51
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662340
ACF-001
Method:
Client:Hart & Hickman
EPA 6020B
Date:April 26, 2023
Description:6020 MET ICPMS
General Information:
1 sample was analyzed for EPA 6020B by Pace Analytical Services Asheville. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3010A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 51
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662340
ACF-001
Method:
Client:Hart & Hickman
EPA 625.1
Date:April 26, 2023
Description:625 RVE
General Information:
1 sample was analyzed for EPA 625.1 by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 625.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 768304
S0: Surrogate recovery outside laboratory control limits.
• LCS (Lab ID: 3989087)
• 2,4,6-Tribromophenol (S)
• Terphenyl-d14 (S)
• MS (Lab ID: 3989088)
• 2,4,6-Tribromophenol (S)
• Nitrobenzene-d5 (S)
• MSD (Lab ID: 3989089)
• 2,4,6-Tribromophenol (S)
• Nitrobenzene-d5 (S)
• Terphenyl-d14 (S)
S3: Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.
• BLANK (Lab ID: 3989086)
• Terphenyl-d14 (S)
• HH TMW-1 (Lab ID: 92662340001)
• Nitrobenzene-d5 (S)
• Terphenyl-d14 (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 51
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662340
ACF-001
Method:
Client:Hart & Hickman
EPA 625.1
Date:April 26, 2023
Description:625 RVE
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 768304
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samplesmay be biased high.
• LCS (Lab ID: 3989087)
• 2,4-Dimethylphenol
• Di-n-butylphthalate
• Diethylphthalate
• Dimethylphthalate
• Phenanthrene
• Pyrene
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 768304
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 35791132003
M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 3989088)
• 2,4-Dimethylphenol
• Di-n-butylphthalate
• Diethylphthalate
• Dimethylphthalate
• Phenanthrene
• Pyrene
• MSD (Lab ID: 3989089)
• 2,4-Dimethylphenol
• Di-n-butylphthalate
• Diethylphthalate
• Dimethylphthalate
• Phenanthrene
• Pyrene
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3989088)
• Fluoranthene
• MSD (Lab ID: 3989089)
• 2,4-Dinitrotoluene
• 4-Bromophenylphenyl ether
• 4-Chloro-3-methylphenol
• Benzo(a)anthracene
• Fluoranthene
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 51
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662340
ACF-001
Method:
Client:Hart & Hickman
SM 6200B
Date:April 26, 2023
Description:6200B MSV
General Information:
2 samples were analyzed for SM 6200B by Pace Analytical Services Charlotte. All samples were received in acceptable condition with
any exceptions noted below or on the chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end ofthis report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 768966
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92662032002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3992357)
• 1,1-Dichloroethene
• 1,1-Dichloropropene
• Methylene Chloride
• Naphthalene
• n-Butylbenzene
• trans-1,2-Dichloroethene
• MSD (Lab ID: 3992358)
• Naphthalene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 51
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92662340
ACF-001
Method:
Client:Hart & Hickman
SM 6200B
Date:April 26, 2023
Description:6200B MSV
QC Batch: 769533
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92662169004
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 3995247)
• Benzene
• Naphthalene
• n-Butylbenzene
• MSD (Lab ID: 3995248)
• Naphthalene
• n-Butylbenzene
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662340
ACF-001
Sample:HH TMW-1 Lab ID:92662340001 Collected:04/13/23 13:00 Received:04/14/23 09:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Pace Analytical Services - Charlotte
MADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 04/24/23 12:42 N204/23/23 13:221051051
Aliphatic (C19-C36)ND ug/L 04/24/23 12:42 N204/23/23 13:221051051
Aromatic (C11-C22)ND ug/L 04/24/23 12:42 N204/23/23 13:221051051
Surrogates
1-Chlorooctadecane (S)65 %04/24/23 12:42 3386-33-204/23/23 13:2240-140 1
o-Terphenyl (S)78 %04/24/23 12:42 84-15-104/23/23 13:2240-140 1
2-Fluorobiphenyl (S)83 %04/24/23 12:42 321-60-804/23/23 13:2240-140 1
2-Bromonaphthalene (S)85 %04/24/23 12:42 580-13-204/23/23 13:2240-140 1
Analytical Method: EPA 6020B Preparation Method: EPA 3010A
Pace Analytical Services - Asheville
6020 MET ICPMS
Chromium 2.3 ug/L 04/17/23 21:26 7440-47-304/16/23 16:381.0 0.50 1
Lead 1.4 ug/L 04/17/23 21:26 7439-92-104/16/23 16:381.0 0.077 1
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
Acenaphthene ND ug/L 04/18/23 23:04 83-32-904/15/23 01:205.0 2.0 1
Acenaphthylene ND ug/L 04/18/23 23:04 208-96-804/15/23 01:205.0 2.0 1
Anthracene ND ug/L 04/18/23 23:04 120-12-704/15/23 01:205.0 2.3 1
Benzo(a)anthracene ND ug/L 04/18/23 23:04 56-55-304/15/23 01:205.0 2.7 1
Benzo(a)pyrene ND ug/L 04/18/23 23:04 50-32-804/15/23 01:205.0 2.8 1
Benzo(b)fluoranthene ND ug/L 04/18/23 23:04 205-99-204/15/23 01:205.0 2.6 1
Benzo(g,h,i)perylene ND ug/L 04/18/23 23:04 191-24-204/15/23 01:205.0 2.8 1
Benzo(k)fluoranthene ND ug/L 04/18/23 23:04 207-08-904/15/23 01:205.0 2.7 1
4-Bromophenylphenyl ether ND ug/L 04/18/23 23:04 101-55-304/15/23 01:205.0 1.8 1
Butylbenzylphthalate ND ug/L 04/18/23 23:04 85-68-704/15/23 01:205.0 3.1 1
4-Chloro-3-methylphenol ND ug/L 04/18/23 23:04 59-50-704/15/23 01:205.0 3.3 1
bis(2-Chloroethoxy)methane ND ug/L 04/18/23 23:04 111-91-104/15/23 01:2010.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 04/18/23 23:04 111-44-404/15/23 01:205.0 1.9 1
2-Chloronaphthalene ND ug/L 04/18/23 23:04 91-58-704/15/23 01:205.0 1.7 1
2-Chlorophenol ND ug/L 04/18/23 23:04 95-57-804/15/23 01:205.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 04/18/23 23:04 7005-72-304/15/23 01:205.0 2.0 1
Chrysene ND ug/L 04/18/23 23:04 218-01-904/15/23 01:205.0 2.8 1
Dibenz(a,h)anthracene ND ug/L 04/18/23 23:04 53-70-304/15/23 01:205.0 3.0 1
3,3'-Dichlorobenzidine ND ug/L 04/18/23 23:04 91-94-104/15/23 01:2010.0 8.1 1
2,4-Dichlorophenol ND ug/L 04/18/23 23:04 120-83-204/15/23 01:205.0 1.4 1
Diethylphthalate ND ug/L 04/18/23 23:04 84-66-2 L104/15/23 01:205.0 2.0 1
2,4-Dimethylphenol ND ug/L 04/18/23 23:04 105-67-9 L104/15/23 01:2010.0 1.7 1
Dimethylphthalate ND ug/L 04/18/23 23:04 131-11-3 L104/15/23 01:205.0 2.1 1
Di-n-butylphthalate ND ug/L 04/18/23 23:04 84-74-2 L104/15/23 01:205.0 2.2 1
4,6-Dinitro-2-methylphenol ND ug/L 04/18/23 23:04 534-52-104/15/23 01:2010.0 7.8 1
2,4-Dinitrophenol ND ug/L 04/18/23 23:04 51-28-504/15/23 01:2050.0 26.0 1
2,4-Dinitrotoluene ND ug/L 04/18/23 23:04 121-14-204/15/23 01:205.0 1.6 1
2,6-Dinitrotoluene ND ug/L 04/18/23 23:04 606-20-204/15/23 01:205.0 1.7 1
Di-n-octylphthalate ND ug/L 04/18/23 23:04 117-84-004/15/23 01:205.0 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662340
ACF-001
Sample:HH TMW-1 Lab ID:92662340001 Collected:04/13/23 13:00 Received:04/14/23 09:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
Pace Analytical Services - Charlotte
625 RVE
bis(2-Ethylhexyl)phthalate ND ug/L 04/18/23 23:04 117-81-704/15/23 01:205.0 3.7 1
Fluoranthene ND ug/L 04/18/23 23:04 206-44-004/15/23 01:205.0 2.2 1
Fluorene ND ug/L 04/18/23 23:04 86-73-704/15/23 01:205.0 2.1 1
Hexachloro-1,3-butadiene ND ug/L 04/18/23 23:04 87-68-304/15/23 01:205.0 1.8 1
Hexachlorobenzene ND ug/L 04/18/23 23:04 118-74-104/15/23 01:205.0 2.2 1
Hexachlorocyclopentadiene ND ug/L 04/18/23 23:04 77-47-404/15/23 01:2010.0 1.6 1
Hexachloroethane ND ug/L 04/18/23 23:04 67-72-104/15/23 01:205.0 1.4 1
Indeno(1,2,3-cd)pyrene ND ug/L 04/18/23 23:04 193-39-504/15/23 01:205.0 2.9 1
Isophorone ND ug/L 04/18/23 23:04 78-59-104/15/23 01:2010.0 1.7 1
Naphthalene ND ug/L 04/18/23 23:04 91-20-304/15/23 01:205.0 2.1 1
Nitrobenzene ND ug/L 04/18/23 23:04 98-95-304/15/23 01:205.0 1.9 1
2-Nitrophenol ND ug/L 04/18/23 23:04 88-75-504/15/23 01:205.0 1.4 1
4-Nitrophenol ND ug/L 04/18/23 23:04 100-02-704/15/23 01:2010.0 6.6 1
N-Nitrosodimethylamine ND ug/L 04/18/23 23:04 62-75-904/15/23 01:205.0 1.9 1
N-Nitroso-di-n-propylamine ND ug/L 04/18/23 23:04 621-64-704/15/23 01:205.0 1.3 1
N-Nitrosodiphenylamine ND ug/L 04/18/23 23:04 86-30-604/15/23 01:2010.0 3.0 1
2,2'-Oxybis(1-chloropropane)ND ug/L 04/18/23 23:04 108-60-104/15/23 01:205.0 1.2 1
Pentachlorophenol ND ug/L 04/18/23 23:04 87-86-504/15/23 01:2010.0 3.8 1
Phenanthrene ND ug/L 04/18/23 23:04 85-01-8 L104/15/23 01:205.0 2.0 1
Phenol ND ug/L 04/18/23 23:04 108-95-204/15/23 01:205.0 1.4 1
Pyrene ND ug/L 04/18/23 23:04 129-00-0 L104/15/23 01:205.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 04/18/23 23:04 120-82-104/15/23 01:205.0 1.7 1
2,4,6-Trichlorophenol ND ug/L 04/18/23 23:04 88-06-204/15/23 01:2010.0 1.6 1
Surrogates
Nitrobenzene-d5 (S)129 %04/18/23 23:04 4165-60-0 S304/15/23 01:2010-120 1
2-Fluorobiphenyl (S)108 %04/18/23 23:04 321-60-804/15/23 01:2015-120 1
Terphenyl-d14 (S)137 %04/18/23 23:04 1718-51-0 S304/15/23 01:2011-131 1
Phenol-d6 (S)76 %04/18/23 23:04 13127-88-304/15/23 01:2010-120 1
2-Fluorophenol (S)91 %04/18/23 23:04 367-12-404/15/23 01:2010-120 1
2,4,6-Tribromophenol (S)132 %04/18/23 23:04 118-79-604/15/23 01:2010-137 1
Tentatively Identified Compounds
Toluene 21.0J ug/L 04/18/23 23:04 108-88-3 N04/15/23 01:201
Nonanoic acid 13.9J ug/L 04/18/23 23:04 112-05-0 N04/15/23 01:201
Hexadecanoic acid 13.1J ug/L 04/18/23 23:04 57-10-3 N04/15/23 01:201
Unknown 13.6J ug/L 04/18/23 23:0404/15/23 01:201
Octadecanoic acid 9.1J ug/L 04/18/23 23:04 57-11-4 N04/15/23 01:201
Unknown 10.0J ug/L 04/18/23 23:0404/15/23 01:201
Dodecane, 2-methyl-11.3J ug/L 04/18/23 23:04 1560-97-0 N04/15/23 01:201
Heneicosane 9.9J ug/L 04/18/23 23:04 629-94-7 N04/15/23 01:201
Hexatriacontane 16.6J ug/L 04/18/23 23:04 630-06-8 N04/15/23 01:201
Unknown 196J ug/L 04/18/23 23:0404/15/23 01:201
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/21/23 12:44 71-43-20.50 0.34 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662340
ACF-001
Sample:HH TMW-1 Lab ID:92662340001 Collected:04/13/23 13:00 Received:04/14/23 09:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Bromobenzene ND ug/L 04/21/23 12:44 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 04/21/23 12:44 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 04/21/23 12:44 75-27-40.50 0.31 1
Bromoform ND ug/L 04/21/23 12:44 75-25-20.50 0.34 1
Bromomethane ND ug/L 04/21/23 12:44 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 04/21/23 12:44 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 04/21/23 12:44 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 04/21/23 12:44 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 04/21/23 12:44 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 04/21/23 12:44 108-90-70.50 0.28 1
Chloroethane ND ug/L 04/21/23 12:44 75-00-31.0 0.65 1
Chloroform ND ug/L 04/21/23 12:44 67-66-30.50 0.43 1
Chloromethane ND ug/L 04/21/23 12:44 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/21/23 12:44 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 04/21/23 12:44 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/21/23 12:44 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 04/21/23 12:44 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/21/23 12:44 106-93-40.50 0.27 1
Dibromomethane ND ug/L 04/21/23 12:44 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 04/21/23 12:44 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 04/21/23 12:44 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 04/21/23 12:44 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 04/21/23 12:44 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 04/21/23 12:44 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 04/21/23 12:44 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 04/21/23 12:44 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 04/21/23 12:44 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/21/23 12:44 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 04/21/23 12:44 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 04/21/23 12:44 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 04/21/23 12:44 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 04/21/23 12:44 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/21/23 12:44 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/21/23 12:44 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 04/21/23 12:44 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 04/21/23 12:44 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/21/23 12:44 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 04/21/23 12:44 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 04/21/23 12:44 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 04/21/23 12:44 1634-04-40.50 0.42 1
Naphthalene ND ug/L 04/21/23 12:44 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 04/21/23 12:44 103-65-10.50 0.34 1
Styrene ND ug/L 04/21/23 12:44 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/21/23 12:44 630-20-60.50 0.31 1
1,1,2,2-Tetrachloroethane ND ug/L 04/21/23 12:44 79-34-50.50 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662340
ACF-001
Sample:HH TMW-1 Lab ID:92662340001 Collected:04/13/23 13:00 Received:04/14/23 09:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Tetrachloroethene ND ug/L 04/21/23 12:44 127-18-40.50 0.29 1
Toluene ND ug/L 04/21/23 12:44 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/21/23 12:44 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/21/23 12:44 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/21/23 12:44 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 04/21/23 12:44 79-00-50.50 0.32 1
Trichloroethene ND ug/L 04/21/23 12:44 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 04/21/23 12:44 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/21/23 12:44 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 04/21/23 12:44 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 04/21/23 12:44 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 04/21/23 12:44 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 04/21/23 12:44 179601-23-11.0 0.71 1
o-Xylene ND ug/L 04/21/23 12:44 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %04/21/23 12:44 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %04/21/23 12:44 460-00-470-130 1
Toluene-d8 (S)116 %04/21/23 12:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662340
ACF-001
Sample:TRIP BLANK Lab ID:92662340002 Collected:04/13/23 00:00 Received:04/14/23 09:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
Benzene ND ug/L 04/21/23 00:12 71-43-20.50 0.34 1
Bromobenzene ND ug/L 04/21/23 00:12 108-86-10.50 0.29 1
Bromochloromethane ND ug/L 04/21/23 00:12 74-97-50.50 0.47 1
Bromodichloromethane ND ug/L 04/21/23 00:12 75-27-40.50 0.31 1
Bromoform ND ug/L 04/21/23 00:12 75-25-20.50 0.34 1
Bromomethane ND ug/L 04/21/23 00:12 74-83-95.0 1.7 1
n-Butylbenzene ND ug/L 04/21/23 00:12 104-51-80.50 0.49 1
sec-Butylbenzene ND ug/L 04/21/23 00:12 135-98-80.50 0.40 1
tert-Butylbenzene ND ug/L 04/21/23 00:12 98-06-60.50 0.32 1
Carbon tetrachloride ND ug/L 04/21/23 00:12 56-23-50.50 0.33 1
Chlorobenzene ND ug/L 04/21/23 00:12 108-90-70.50 0.28 1
Chloroethane ND ug/L 04/21/23 00:12 75-00-31.0 0.65 1
Chloroform ND ug/L 04/21/23 00:12 67-66-30.50 0.43 1
Chloromethane ND ug/L 04/21/23 00:12 74-87-31.0 0.54 1
2-Chlorotoluene ND ug/L 04/21/23 00:12 95-49-80.50 0.32 1
4-Chlorotoluene ND ug/L 04/21/23 00:12 106-43-40.50 0.32 1
1,2-Dibromo-3-chloropropane ND ug/L 04/21/23 00:12 96-12-81.0 0.34 1
Dibromochloromethane ND ug/L 04/21/23 00:12 124-48-10.50 0.36 1
1,2-Dibromoethane (EDB)ND ug/L 04/21/23 00:12 106-93-40.50 0.27 1
Dibromomethane ND ug/L 04/21/23 00:12 74-95-30.50 0.39 1
1,2-Dichlorobenzene ND ug/L 04/21/23 00:12 95-50-10.50 0.34 1
1,3-Dichlorobenzene ND ug/L 04/21/23 00:12 541-73-10.50 0.34 1
1,4-Dichlorobenzene ND ug/L 04/21/23 00:12 106-46-70.50 0.33 1
Dichlorodifluoromethane ND ug/L 04/21/23 00:12 75-71-80.50 0.35 1
1,1-Dichloroethane ND ug/L 04/21/23 00:12 75-34-30.50 0.37 1
1,2-Dichloroethane ND ug/L 04/21/23 00:12 107-06-20.50 0.32 1
1,1-Dichloroethene ND ug/L 04/21/23 00:12 75-35-40.50 0.35 1
cis-1,2-Dichloroethene ND ug/L 04/21/23 00:12 156-59-20.50 0.38 1
trans-1,2-Dichloroethene ND ug/L 04/21/23 00:12 156-60-50.50 0.40 1
1,2-Dichloropropane ND ug/L 04/21/23 00:12 78-87-50.50 0.36 1
1,3-Dichloropropane ND ug/L 04/21/23 00:12 142-28-90.50 0.28 1
2,2-Dichloropropane ND ug/L 04/21/23 00:12 594-20-70.50 0.39 1
1,1-Dichloropropene ND ug/L 04/21/23 00:12 563-58-60.50 0.43 1
cis-1,3-Dichloropropene ND ug/L 04/21/23 00:12 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene ND ug/L 04/21/23 00:12 10061-02-60.50 0.36 1
Diisopropyl ether ND ug/L 04/21/23 00:12 108-20-30.50 0.31 1
Ethylbenzene ND ug/L 04/21/23 00:12 100-41-40.50 0.30 1
Hexachloro-1,3-butadiene ND ug/L 04/21/23 00:12 87-68-32.0 1.5 1
Isopropylbenzene (Cumene)ND ug/L 04/21/23 00:12 98-82-80.50 0.33 1
Methylene Chloride ND ug/L 04/21/23 00:12 75-09-22.0 2.0 1
Methyl-tert-butyl ether ND ug/L 04/21/23 00:12 1634-04-40.50 0.42 1
Naphthalene ND ug/L 04/21/23 00:12 91-20-32.0 0.64 1
n-Propylbenzene ND ug/L 04/21/23 00:12 103-65-10.50 0.34 1
Styrene ND ug/L 04/21/23 00:12 100-42-50.50 0.29 1
1,1,1,2-Tetrachloroethane ND ug/L 04/21/23 00:12 630-20-60.50 0.31 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
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[phone]
Page 15 of 51
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92662340
ACF-001
Sample:TRIP BLANK Lab ID:92662340002 Collected:04/13/23 00:00 Received:04/14/23 09:29 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
6200B MSV
1,1,2,2-Tetrachloroethane ND ug/L 04/21/23 00:12 79-34-50.50 0.22 1
Tetrachloroethene ND ug/L 04/21/23 00:12 127-18-40.50 0.29 1
Toluene ND ug/L 04/21/23 00:12 108-88-30.50 0.24 1
1,2,3-Trichlorobenzene ND ug/L 04/21/23 00:12 87-61-62.0 0.81 1
1,2,4-Trichlorobenzene ND ug/L 04/21/23 00:12 120-82-12.0 0.64 1
1,1,1-Trichloroethane ND ug/L 04/21/23 00:12 71-55-60.50 0.33 1
1,1,2-Trichloroethane ND ug/L 04/21/23 00:12 79-00-50.50 0.32 1
Trichloroethene ND ug/L 04/21/23 00:12 79-01-60.50 0.38 1
Trichlorofluoromethane ND ug/L 04/21/23 00:12 75-69-41.0 0.30 1
1,2,3-Trichloropropane ND ug/L 04/21/23 00:12 96-18-40.50 0.26 1
1,2,4-Trimethylbenzene ND ug/L 04/21/23 00:12 95-63-60.50 0.50 1
1,3,5-Trimethylbenzene ND ug/L 04/21/23 00:12 108-67-80.50 0.33 1
Vinyl chloride ND ug/L 04/21/23 00:12 75-01-41.0 0.39 1
m&p-Xylene ND ug/L 04/21/23 00:12 179601-23-11.0 0.71 1
o-Xylene ND ug/L 04/21/23 00:12 95-47-60.50 0.34 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %04/21/23 00:12 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %04/21/23 00:12 460-00-470-130 1
Toluene-d8 (S)102 %04/21/23 00:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 16 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768326
EPA 3010A
EPA 6020B
6020 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92662340001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3989171
Associated Lab Samples:92662340001
Matrix:Water
AnalyzedMDL
Chromium ug/L ND 1.0 04/17/23 19:260.50
Lead ug/L ND 1.0 04/17/23 19:260.077
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989172LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium ug/L 51.450 103 80-120
Lead ug/L 50.350 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3989177MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662211001
3989178
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium ug/L 50 105 75-125104 0 20501.0 53.3 53.2
Lead ug/L 50 100 75-125101 1 20500.53J 50.7 51.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768966
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662340002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3992355
Associated Lab Samples:92662340002
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/20/23 23:540.31
1,1,1-Trichloroethane ug/L ND 0.50 04/20/23 23:540.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/20/23 23:540.22
1,1,2-Trichloroethane ug/L ND 0.50 04/20/23 23:540.32
1,1-Dichloroethane ug/L ND 0.50 04/20/23 23:540.37
1,1-Dichloroethene ug/L ND 0.50 04/20/23 23:540.35
1,1-Dichloropropene ug/L ND 0.50 04/20/23 23:540.43
1,2,3-Trichlorobenzene ug/L ND 2.0 04/20/23 23:540.81
1,2,3-Trichloropropane ug/L ND 0.50 04/20/23 23:540.26
1,2,4-Trichlorobenzene ug/L ND 2.0 04/20/23 23:540.64
1,2,4-Trimethylbenzene ug/L ND 0.50 04/20/23 23:540.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/20/23 23:540.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/20/23 23:540.27
1,2-Dichlorobenzene ug/L ND 0.50 04/20/23 23:540.34
1,2-Dichloroethane ug/L ND 0.50 04/20/23 23:540.32
1,2-Dichloropropane ug/L ND 0.50 04/20/23 23:540.36
1,3,5-Trimethylbenzene ug/L ND 0.50 04/20/23 23:540.33
1,3-Dichlorobenzene ug/L ND 0.50 04/20/23 23:540.34
1,3-Dichloropropane ug/L ND 0.50 04/20/23 23:540.28
1,4-Dichlorobenzene ug/L ND 0.50 04/20/23 23:540.33
2,2-Dichloropropane ug/L ND 0.50 04/20/23 23:540.39
2-Chlorotoluene ug/L ND 0.50 04/20/23 23:540.32
4-Chlorotoluene ug/L ND 0.50 04/20/23 23:540.32
Benzene ug/L ND 0.50 04/20/23 23:540.34
Bromobenzene ug/L ND 0.50 04/20/23 23:540.29
Bromochloromethane ug/L ND 0.50 04/20/23 23:540.47
Bromodichloromethane ug/L ND 0.50 04/20/23 23:540.31
Bromoform ug/L ND 0.50 04/20/23 23:540.34
Bromomethane ug/L ND 5.0 04/20/23 23:541.7
Carbon tetrachloride ug/L ND 0.50 04/20/23 23:540.33
Chlorobenzene ug/L ND 0.50 04/20/23 23:540.28
Chloroethane ug/L ND 1.0 04/20/23 23:540.65
Chloroform ug/L ND 0.50 04/20/23 23:540.43
Chloromethane ug/L ND 1.0 04/20/23 23:540.54
cis-1,2-Dichloroethene ug/L ND 0.50 04/20/23 23:540.38
cis-1,3-Dichloropropene ug/L ND 0.50 04/20/23 23:540.36
Dibromochloromethane ug/L ND 0.50 04/20/23 23:540.36
Dibromomethane ug/L ND 0.50 04/20/23 23:540.39
Dichlorodifluoromethane ug/L ND 0.50 04/20/23 23:540.35
Diisopropyl ether ug/L ND 0.50 04/20/23 23:540.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3992355
Associated Lab Samples:92662340002
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 04/20/23 23:540.30
Hexachloro-1,3-butadiene ug/L ND 2.0 04/20/23 23:541.5
Isopropylbenzene (Cumene)ug/L ND 0.50 04/20/23 23:540.33
m&p-Xylene ug/L ND 1.0 04/20/23 23:540.71
Methyl-tert-butyl ether ug/L ND 0.50 04/20/23 23:540.42
Methylene Chloride ug/L ND 2.0 04/20/23 23:542.0
n-Butylbenzene ug/L ND 0.50 04/20/23 23:540.49
n-Propylbenzene ug/L ND 0.50 04/20/23 23:540.34
Naphthalene ug/L ND 2.0 04/20/23 23:540.64
o-Xylene ug/L ND 0.50 04/20/23 23:540.34
sec-Butylbenzene ug/L ND 0.50 04/20/23 23:540.40
Styrene ug/L ND 0.50 04/20/23 23:540.29
tert-Butylbenzene ug/L ND 0.50 04/20/23 23:540.32
Tetrachloroethene ug/L ND 0.50 04/20/23 23:540.29
Toluene ug/L ND 0.50 04/20/23 23:540.24
trans-1,2-Dichloroethene ug/L ND 0.50 04/20/23 23:540.40
trans-1,3-Dichloropropene ug/L ND 0.50 04/20/23 23:540.36
Trichloroethene ug/L ND 0.50 04/20/23 23:540.38
Trichlorofluoromethane ug/L ND 1.0 04/20/23 23:540.30
Vinyl chloride ug/L ND 1.0 04/20/23 23:540.39
1,2-Dichloroethane-d4 (S)%99 70-130 04/20/23 23:54
4-Bromofluorobenzene (S)%101 70-130 04/20/23 23:54
Toluene-d8 (S)%102 70-130 04/20/23 23:54
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3992356LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 18.320 92 60-140
1,1,1-Trichloroethane ug/L 18.420 92 60-140
1,1,2,2-Tetrachloroethane ug/L 18.520 93 60-140
1,1,2-Trichloroethane ug/L 18.820 94 60-140
1,1-Dichloroethane ug/L 18.220 91 60-140
1,1-Dichloroethene ug/L 18.620 93 60-140
1,1-Dichloropropene ug/L 20.120 101 60-140
1,2,3-Trichlorobenzene ug/L 19.420 97 60-140
1,2,3-Trichloropropane ug/L 18.220 91 60-140
1,2,4-Trichlorobenzene ug/L 18.120 91 60-140
1,2,4-Trimethylbenzene ug/L 19.520 98 60-140
1,2-Dibromo-3-chloropropane ug/L 17.520 87 60-140
1,2-Dibromoethane (EDB)ug/L 19.120 95 60-140
1,2-Dichlorobenzene ug/L 18.820 94 60-140
1,2-Dichloroethane ug/L 17.820 89 60-140
1,2-Dichloropropane ug/L 18.820 94 60-140
1,3,5-Trimethylbenzene ug/L 19.420 97 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3992356LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 18.920 95 60-140
1,3-Dichloropropane ug/L 18.320 91 60-140
1,4-Dichlorobenzene ug/L 18.720 94 60-140
2,2-Dichloropropane ug/L 18.220 91 60-140
2-Chlorotoluene ug/L 18.420 92 60-140
4-Chlorotoluene ug/L 19.320 96 60-140
Benzene ug/L 18.420 92 60-140
Bromobenzene ug/L 18.220 91 60-140
Bromochloromethane ug/L 18.320 91 60-140
Bromodichloromethane ug/L 17.720 89 60-140
Bromoform ug/L 17.520 87 60-140
Bromomethane ug/L 12.820 64 60-140
Carbon tetrachloride ug/L 18.520 92 60-140
Chlorobenzene ug/L 18.520 92 60-140
Chloroethane ug/L 18.020 90 60-140
Chloroform ug/L 17.920 90 60-140
Chloromethane ug/L 17.520 88 60-140
cis-1,2-Dichloroethene ug/L 17.920 89 60-140
cis-1,3-Dichloropropene ug/L 18.720 94 60-140
Dibromochloromethane ug/L 18.220 91 60-140
Dibromomethane ug/L 18.320 91 60-140
Dichlorodifluoromethane ug/L 17.220 86 60-140
Diisopropyl ether ug/L 17.620 88 60-140
Ethylbenzene ug/L 18.420 92 60-140
Hexachloro-1,3-butadiene ug/L 18.320 92 60-140
Isopropylbenzene (Cumene)ug/L 19.420 97 60-140
m&p-Xylene ug/L 36.740 92 60-140
Methyl-tert-butyl ether ug/L 17.320 87 60-140
Methylene Chloride ug/L 19.620 98 60-140
n-Butylbenzene ug/L 19.420 97 60-140
n-Propylbenzene ug/L 18.320 91 60-140
Naphthalene ug/L 19.620 98 60-140
o-Xylene ug/L 18.520 93 60-140
sec-Butylbenzene ug/L 19.320 97 60-140
Styrene ug/L 19.220 96 60-140
tert-Butylbenzene ug/L 15.820 79 60-140
Tetrachloroethene ug/L 18.020 90 60-140
Toluene ug/L 17.620 88 60-140
trans-1,2-Dichloroethene ug/L 18.620 93 60-140
trans-1,3-Dichloropropene ug/L 18.320 91 60-140
Trichloroethene ug/L 19.220 96 60-140
Trichlorofluoromethane ug/L 17.220 86 60-140
Vinyl chloride ug/L 14.520 72 60-140
1,2-Dichloroethane-d4 (S)%102 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3992357MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662032002
3992358
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 126 60-140110 14 3020ND25.3 22.0
1,1,1-Trichloroethane ug/L 20 132 60-140116 13 3020ND26.4 23.2
1,1,2,2-Tetrachloroethane ug/L 20 129 60-140111 15 3020ND25.9 22.1
1,1,2-Trichloroethane ug/L 20 129 60-140114 12 3020ND25.8 22.8
1,1-Dichloroethane ug/L 20 139 60-140115 19 3020ND27.9 23.1
1,1-Dichloroethene ug/L M12014560-140128 13 3020ND29.0 25.5
1,1-Dichloropropene ug/L M12014460-140127 12 3020ND28.8 25.4
1,2,3-Trichlorobenzene ug/L 20 130 60-140123 6 3020ND26.0 24.6
1,2,3-Trichloropropane ug/L 20 124 60-140106 16 3020ND24.7 21.2
1,2,4-Trichlorobenzene ug/L 20 131 60-140132 1 3020ND26.2 26.5
1,2,4-Trimethylbenzene ug/L 20 133 60-140117 13 3020ND26.6 23.5
1,2-Dibromo-3-
chloropropane ug/L 20 115 60-140117 1 3020ND23.1 23.3
1,2-Dibromoethane (EDB)ug/L 20 130 60-140112 15 3020ND26.0 22.3
1,2-Dichlorobenzene ug/L 20 125 60-140124 1 3020ND25.1 24.7
1,2-Dichloroethane ug/L 20 124 60-140107 15 3020ND24.9 21.4
1,2-Dichloropropane ug/L 20 131 60-140115 12 3020ND26.1 23.1
1,3,5-Trimethylbenzene ug/L 20 133 60-140118 12 3020ND26.7 23.6
1,3-Dichlorobenzene ug/L 20 125 60-140111 12 3020ND25.0 22.2
1,3-Dichloropropane ug/L 20 126 60-140108 16 3020ND25.2 21.5
1,4-Dichlorobenzene ug/L 20 125 60-140109 14 3020ND25.0 21.8
2,2-Dichloropropane ug/L 20 134 60-140122 10 3020ND26.8 24.3
2-Chlorotoluene ug/L 20 125 60-140108 14 3020ND25.0 21.7
4-Chlorotoluene ug/L 20 128 60-140112 13 3020ND25.5 22.4
Benzene ug/L 20 128 60-140114 11 30200.64 26.2 23.5
Bromobenzene ug/L 20 119 60-140105 13 3020ND23.7 20.9
Bromochloromethane ug/L 20 127 60-140115 10 3020ND25.3 22.9
Bromodichloromethane ug/L 20 120 60-140108 10 3020ND23.9 21.6
Bromoform ug/L 20 120 60-140103 15 3020ND23.9 20.7
Bromomethane ug/L 20 65 60-14075 13 3020ND13.1 14.9
Carbon tetrachloride ug/L 20 130 60-140115 12 3020ND26.1 23.1
Chlorobenzene ug/L 20 126 60-140109 15 3020ND25.2 21.8
Chloroethane ug/L 20 130 60-140117 11 3020ND26.0 23.4
Chloroform ug/L 20 127 60-140112 13 3020ND25.4 22.4
Chloromethane ug/L 20 120 60-140116 4 3020ND24.1 23.1
cis-1,2-Dichloroethene ug/L 20 128 60-140113 12 3020ND25.6 22.6
cis-1,3-Dichloropropene ug/L 20 129 60-140112 14 3020ND25.9 22.5
Dibromochloromethane ug/L 20 126 60-140110 14 3020ND25.2 21.9
Dibromomethane ug/L 20 121 60-140111 9 3020ND24.2 22.2
Dichlorodifluoromethane ug/L 20 118 60-140104 13 3020ND23.6 20.8
Diisopropyl ether ug/L 20 133 60-140110 19 3020ND26.6 22.0
Ethylbenzene ug/L 20 136 60-140128 2 302053.2 80.5 78.8
Hexachloro-1,3-butadiene ug/L 20 135 60-140140 4 3020ND27.0 28.0
Isopropylbenzene(Cumene)ug/L 20 137 60-140123 9 30206.1 33.5 30.7
m&p-Xylene ug/L 40 122 60-140108 12 3040ND48.7 43.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3992357MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662032002
3992358
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 128 60-140104 21 3020ND25.5 20.7
Methylene Chloride ug/L M12014460-140121 17 3020ND28.8 24.2
n-Butylbenzene ug/L M12014160-140136 4 30201.6 29.8 28.7
n-Propylbenzene ug/L 20 124 60-140111 6 302022.6 47.4 44.7
Naphthalene ug/L M12016460-140189 4 302093.9 127 132
o-Xylene ug/L 20 123 60-140109 13 3020ND25.0 22.0
sec-Butylbenzene ug/L 20 134 60-140121 9 30201.7 28.4 26.0
Styrene ug/L 20 129 60-140111 14 3020ND25.7 22.2
tert-Butylbenzene ug/L 20 108 60-14098 10 3020ND21.6 19.6
Tetrachloroethene ug/L 20 123 60-140107 14 3020ND24.6 21.4
Toluene ug/L 20 121 60-140107 12 3020ND24.1 21.4
trans-1,2-Dichloroethene ug/L M12014460-140118 20 3020ND28.9 23.6
trans-1,3-Dichloropropene ug/L 20 127 60-140113 11 3020ND25.3 22.6
Trichloroethene ug/L 20 132 60-140118 11 3020ND26.3 23.6
Trichlorofluoromethane ug/L 20 134 60-140116 15 3020ND26.9 23.2
Vinyl chloride ug/L 20 116 60-140102 12 3020ND23.1 20.4
1,2-Dichloroethane-d4 (S)%104 70-130105
4-Bromofluorobenzene (S)%102 70-130101
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
769533
SM 6200B
SM 6200B
6200B MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662340001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3995245
Associated Lab Samples:92662340001
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 04/21/23 11:330.31
1,1,1-Trichloroethane ug/L ND 0.50 04/21/23 11:330.33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 04/21/23 11:330.22
1,1,2-Trichloroethane ug/L ND 0.50 04/21/23 11:330.32
1,1-Dichloroethane ug/L ND 0.50 04/21/23 11:330.37
1,1-Dichloroethene ug/L ND 0.50 04/21/23 11:330.35
1,1-Dichloropropene ug/L ND 0.50 04/21/23 11:330.43
1,2,3-Trichlorobenzene ug/L ND 2.0 04/21/23 11:330.81
1,2,3-Trichloropropane ug/L ND 0.50 04/21/23 11:330.26
1,2,4-Trichlorobenzene ug/L ND 2.0 04/21/23 11:330.64
1,2,4-Trimethylbenzene ug/L ND 0.50 04/21/23 11:330.50
1,2-Dibromo-3-chloropropane ug/L ND 1.0 04/21/23 11:330.34
1,2-Dibromoethane (EDB)ug/L ND 0.50 04/21/23 11:330.27
1,2-Dichlorobenzene ug/L ND 0.50 04/21/23 11:330.34
1,2-Dichloroethane ug/L ND 0.50 04/21/23 11:330.32
1,2-Dichloropropane ug/L ND 0.50 04/21/23 11:330.36
1,3,5-Trimethylbenzene ug/L ND 0.50 04/21/23 11:330.33
1,3-Dichlorobenzene ug/L ND 0.50 04/21/23 11:330.34
1,3-Dichloropropane ug/L ND 0.50 04/21/23 11:330.28
1,4-Dichlorobenzene ug/L ND 0.50 04/21/23 11:330.33
2,2-Dichloropropane ug/L ND 0.50 04/21/23 11:330.39
2-Chlorotoluene ug/L ND 0.50 04/21/23 11:330.32
4-Chlorotoluene ug/L ND 0.50 04/21/23 11:330.32
Benzene ug/L ND 0.50 04/21/23 11:330.34
Bromobenzene ug/L ND 0.50 04/21/23 11:330.29
Bromochloromethane ug/L ND 0.50 04/21/23 11:330.47
Bromodichloromethane ug/L ND 0.50 04/21/23 11:330.31
Bromoform ug/L ND 0.50 04/21/23 11:330.34
Bromomethane ug/L ND 5.0 04/21/23 11:331.7
Carbon tetrachloride ug/L ND 0.50 04/21/23 11:330.33
Chlorobenzene ug/L ND 0.50 04/21/23 11:330.28
Chloroethane ug/L ND 1.0 04/21/23 11:330.65
Chloroform ug/L ND 0.50 04/21/23 11:330.43
Chloromethane ug/L ND 1.0 04/21/23 11:330.54
cis-1,2-Dichloroethene ug/L ND 0.50 04/21/23 11:330.38
cis-1,3-Dichloropropene ug/L ND 0.50 04/21/23 11:330.36
Dibromochloromethane ug/L ND 0.50 04/21/23 11:330.36
Dibromomethane ug/L ND 0.50 04/21/23 11:330.39
Dichlorodifluoromethane ug/L ND 0.50 04/21/23 11:330.35
Diisopropyl ether ug/L ND 0.50 04/21/23 11:330.31
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
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[phone]
Page 23 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3995245
Associated Lab Samples:92662340001
Matrix:Water
AnalyzedMDL
Ethylbenzene ug/L ND 0.50 04/21/23 11:330.30
Hexachloro-1,3-butadiene ug/L ND 2.0 04/21/23 11:331.5
Isopropylbenzene (Cumene)ug/L ND 0.50 04/21/23 11:330.33
m&p-Xylene ug/L ND 1.0 04/21/23 11:330.71
Methyl-tert-butyl ether ug/L ND 0.50 04/21/23 11:330.42
Methylene Chloride ug/L ND 2.0 04/21/23 11:332.0
n-Butylbenzene ug/L ND 0.50 04/21/23 11:330.49
n-Propylbenzene ug/L ND 0.50 04/21/23 11:330.34
Naphthalene ug/L ND 2.0 04/21/23 11:330.64
o-Xylene ug/L ND 0.50 04/21/23 11:330.34
sec-Butylbenzene ug/L ND 0.50 04/21/23 11:330.40
Styrene ug/L ND 0.50 04/21/23 11:330.29
tert-Butylbenzene ug/L ND 0.50 04/21/23 11:330.32
Tetrachloroethene ug/L ND 0.50 04/21/23 11:330.29
Toluene ug/L ND 0.50 04/21/23 11:330.24
trans-1,2-Dichloroethene ug/L ND 0.50 04/21/23 11:330.40
trans-1,3-Dichloropropene ug/L ND 0.50 04/21/23 11:330.36
Trichloroethene ug/L ND 0.50 04/21/23 11:330.38
Trichlorofluoromethane ug/L ND 1.0 04/21/23 11:330.30
Vinyl chloride ug/L ND 1.0 04/21/23 11:330.39
1,2-Dichloroethane-d4 (S)%98 70-130 04/21/23 11:33
4-Bromofluorobenzene (S)%102 70-130 04/21/23 11:33
Toluene-d8 (S)%103 70-130 04/21/23 11:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3995246LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 19.220 96 60-140
1,1,1-Trichloroethane ug/L 19.320 97 60-140
1,1,2,2-Tetrachloroethane ug/L 19.520 98 60-140
1,1,2-Trichloroethane ug/L 20.720 104 60-140
1,1-Dichloroethane ug/L 19.220 96 60-140
1,1-Dichloroethene ug/L 21.020 105 60-140
1,1-Dichloropropene ug/L 21.120 106 60-140
1,2,3-Trichlorobenzene ug/L 19.320 97 60-140
1,2,3-Trichloropropane ug/L 18.320 91 60-140
1,2,4-Trichlorobenzene ug/L 18.320 91 60-140
1,2,4-Trimethylbenzene ug/L 20.220 101 60-140
1,2-Dibromo-3-chloropropane ug/L 16.920 85 60-140
1,2-Dibromoethane (EDB)ug/L 20.020 100 60-140
1,2-Dichlorobenzene ug/L 20.020 100 60-140
1,2-Dichloroethane ug/L 18.720 94 60-140
1,2-Dichloropropane ug/L 19.420 97 60-140
1,3,5-Trimethylbenzene ug/L 19.720 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3995246LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene ug/L 19.720 99 60-140
1,3-Dichloropropane ug/L 19.120 95 60-140
1,4-Dichlorobenzene ug/L 19.820 99 60-140
2,2-Dichloropropane ug/L 20.020 100 60-140
2-Chlorotoluene ug/L 18.720 94 60-140
4-Chlorotoluene ug/L 19.320 97 60-140
Benzene ug/L 19.120 95 60-140
Bromobenzene ug/L 18.820 94 60-140
Bromochloromethane ug/L 19.520 97 60-140
Bromodichloromethane ug/L 18.420 92 60-140
Bromoform ug/L 18.520 92 60-140
Bromomethane ug/L 15.220 76 60-140
Carbon tetrachloride ug/L 19.020 95 60-140
Chlorobenzene ug/L 19.320 96 60-140
Chloroethane ug/L 19.920 99 60-140
Chloroform ug/L 18.920 94 60-140
Chloromethane ug/L 21.320 107 60-140
cis-1,2-Dichloroethene ug/L 18.820 94 60-140
cis-1,3-Dichloropropene ug/L 21.020 105 60-140
Dibromochloromethane ug/L 19.120 95 60-140
Dibromomethane ug/L 18.320 91 60-140
Dichlorodifluoromethane ug/L 21.220 106 60-140
Diisopropyl ether ug/L 18.520 93 60-140
Ethylbenzene ug/L 19.020 95 60-140
Hexachloro-1,3-butadiene ug/L 18.920 95 60-140
Isopropylbenzene (Cumene)ug/L 20.420 102 60-140
m&p-Xylene ug/L 37.740 94 60-140
Methyl-tert-butyl ether ug/L 18.320 92 60-140
Methylene Chloride ug/L 20.620 103 60-140
n-Butylbenzene ug/L 20.820 104 60-140
n-Propylbenzene ug/L 18.720 93 60-140
Naphthalene ug/L 19.420 97 60-140
o-Xylene ug/L 19.520 97 60-140
sec-Butylbenzene ug/L 19.920 99 60-140
Styrene ug/L 20.020 100 60-140
tert-Butylbenzene ug/L 16.220 81 60-140
Tetrachloroethene ug/L 20.020 100 60-140
Toluene ug/L 19.220 96 60-140
trans-1,2-Dichloroethene ug/L 19.920 99 60-140
trans-1,3-Dichloropropene ug/L 20.420 102 60-140
Trichloroethene ug/L 19.720 99 60-140
Trichlorofluoromethane ug/L 19.420 97 60-140
Vinyl chloride ug/L 17.620 88 60-140
1,2-Dichloroethane-d4 (S)%103 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%106 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3995247MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662169004
3995248
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 113 60-140109 3 3020ND22.5 21.8
1,1,1-Trichloroethane ug/L 20 119 60-140116 3 3020ND23.9 23.2
1,1,2,2-Tetrachloroethane ug/L 20 112 60-140112 0 3020ND22.4 22.3
1,1,2-Trichloroethane ug/L 20 111 60-140120 8 3020ND22.2 24.1
1,1-Dichloroethane ug/L 20 103 60-140120 15 3020ND20.7 23.9
1,1-Dichloroethene ug/L 20 125 60-140125 1 3020ND25.1 24.9
1,1-Dichloropropene ug/L 20 134 60-140134 0 3020ND26.7 26.8
1,2,3-Trichlorobenzene ug/L 20 120 60-140121 1 3020ND23.9 24.1
1,2,3-Trichloropropane ug/L 20 107 60-140106 1 3020ND21.4 21.2
1,2,4-Trichlorobenzene ug/L 20 122 60-140118 3 3020ND24.3 23.7
1,2,4-Trimethylbenzene ug/L 20 122 60-140118 3 3020ND24.3 23.7
1,2-Dibromo-3-
chloropropane ug/L 20 103 60-140102 1 3020ND20.7 20.4
1,2-Dibromoethane (EDB)ug/L 20 115 60-140122 6 3020ND23.0 24.5
1,2-Dichlorobenzene ug/L 20 112 60-140110 2 3020ND22.4 22.0
1,2-Dichloroethane ug/L 20 107 60-140109 2 3020ND21.5 21.8
1,2-Dichloropropane ug/L 20 116 60-140114 1 3020ND23.2 22.9
1,3,5-Trimethylbenzene ug/L 20 121 60-140117 3 3020ND24.2 23.4
1,3-Dichlorobenzene ug/L 20 113 60-140111 2 3020ND22.7 22.2
1,3-Dichloropropane ug/L 20 108 60-140117 8 3020ND21.6 23.4
1,4-Dichlorobenzene ug/L 20 111 60-140110 1 3020ND22.1 21.9
2,2-Dichloropropane ug/L 20 121 60-140119 2 3020ND24.2 23.7
2-Chlorotoluene ug/L 20 111 60-140108 3 3020ND22.3 21.7
4-Chlorotoluene ug/L 20 114 60-140113 1 3020ND22.8 22.5
Benzene ug/L M12014760-140122 3 3020132162157
Bromobenzene ug/L 20 108 60-140104 3 3020ND21.5 20.9
Bromochloromethane ug/L 20 110 60-140111 1 3020ND21.9 22.2
Bromodichloromethane ug/L 20 106 60-140104 2 3020ND21.2 20.7
Bromoform ug/L 20 105 60-140106 1 3020ND21.0 21.1
Bromomethane ug/L 20 74 60-14077 4 3020ND14.9 15.5
Carbon tetrachloride ug/L 20 117 60-140113 4 3020ND23.5 22.5
Chlorobenzene ug/L 20 111 60-140110 1 3020ND22.2 22.0
Chloroethane ug/L 20 114 60-140113 1 3020ND22.8 22.7
Chloroform ug/L 20 113 60-140111 2 3020ND22.6 22.1
Chloromethane ug/L 20 111 60-140114 3 3020ND22.2 22.8
cis-1,2-Dichloroethene ug/L 20 112 60-140111 1 3020ND22.3 22.2
cis-1,3-Dichloropropene ug/L 20 114 60-140119 4 3020ND22.9 23.9
Dibromochloromethane ug/L 20 110 60-140118 7 3020ND22.1 23.5
Dibromomethane ug/L 20 108 60-140104 4 3020ND21.5 20.7
Dichlorodifluoromethane ug/L 20 106 60-140105 1 3020ND21.2 21.0
Diisopropyl ether ug/L 20 106 60-140114 7 30201.3 22.6 24.2
Ethylbenzene ug/L 20 113 60-140112 1 30200.55 23.2 23.0
Hexachloro-1,3-butadiene ug/L 20 125 60-140116 7 3020ND25.0 23.2
Isopropylbenzene(Cumene)ug/L 20 133 60-140130 2 30206.2 32.7 32.1
m&p-Xylene ug/L 40 111 60-140110 1 3040ND44.5 44.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3995247MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92662169004
3995248
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 107 60-140113 5 3020ND21.4 22.6
Methylene Chloride ug/L 20 118 60-140121 3 3020ND23.6 24.2
n-Butylbenzene ug/L M12014560-140142 2 3020ND29.1 28.4
n-Propylbenzene ug/L 20 122 60-140117 3 30201034.4 33.3
Naphthalene ug/L M12015560-140150 1 302035.4 66.3 65.3
o-Xylene ug/L 20 113 60-140112 1 3020ND22.7 22.3
sec-Butylbenzene ug/L 20 129 60-140124 3 30205.5 31.2 30.3
Styrene ug/L 20 115 60-140115 0 3020ND23.1 23.1
tert-Butylbenzene ug/L 20 97 60-14096 1 30200.45J 19.8 19.6
Tetrachloroethene ug/L 20 116 60-140128 10 3020ND23.2 25.6
Toluene ug/L 20 105 60-140109 4 3020ND21.1 21.8
trans-1,2-Dichloroethene ug/L 20 116 60-140124 7 3020ND23.1 24.9
trans-1,3-Dichloropropene ug/L 20 114 60-140115 1 3020ND22.9 23.1
Trichloroethene ug/L 20 121 60-140120 1 3020ND24.3 24.0
Trichlorofluoromethane ug/L 20 118 60-140116 2 3020ND23.6 23.1
Vinyl chloride ug/L 20 101 60-140103 2 3020ND20.2 20.5
1,2-Dichloroethane-d4 (S)%103 70-130105
4-Bromofluorobenzene (S)%102 70-130102
Toluene-d8 (S)%98 70-130102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
768304
EPA 625.1
EPA 625.1
625 MSS
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662340001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3989086
Associated Lab Samples:92662340001
Matrix:Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 5.0 04/18/23 13:451.7
2,2'-Oxybis(1-chloropropane)ug/L ND 5.0 04/18/23 13:451.2
2,4,6-Trichlorophenol ug/L ND 10.0 04/18/23 13:451.6
2,4-Dichlorophenol ug/L ND 5.0 04/18/23 13:451.4
2,4-Dimethylphenol ug/L ND 10.0 04/18/23 13:451.7
2,4-Dinitrophenol ug/L ND 50.0 04/18/23 13:4526.0
2,4-Dinitrotoluene ug/L ND 5.0 04/18/23 13:451.6
2,6-Dinitrotoluene ug/L ND 5.0 04/18/23 13:451.7
2-Chloronaphthalene ug/L ND 5.0 04/18/23 13:451.7
2-Chlorophenol ug/L ND 5.0 04/18/23 13:451.2
2-Nitrophenol ug/L ND 5.0 04/18/23 13:451.4
3,3'-Dichlorobenzidine ug/L ND 10.0 04/18/23 13:458.1
4,6-Dinitro-2-methylphenol ug/L ND 10.0 04/18/23 13:457.8
4-Bromophenylphenyl ether ug/L ND 5.0 04/18/23 13:451.8
4-Chloro-3-methylphenol ug/L ND 5.0 04/18/23 13:453.3
4-Chlorophenylphenyl ether ug/L ND 5.0 04/18/23 13:452.0
4-Nitrophenol ug/L ND 10.0 04/18/23 13:456.6
Acenaphthene ug/L ND 5.0 04/18/23 13:452.0
Acenaphthylene ug/L ND 5.0 04/18/23 13:452.0
Anthracene ug/L ND 5.0 04/18/23 13:452.3
Benzo(a)anthracene ug/L ND 5.0 04/18/23 13:452.7
Benzo(a)pyrene ug/L ND 5.0 04/18/23 13:452.8
Benzo(b)fluoranthene ug/L ND 5.0 04/18/23 13:452.6
Benzo(g,h,i)perylene ug/L ND 5.0 04/18/23 13:452.8
Benzo(k)fluoranthene ug/L ND 5.0 04/18/23 13:452.7
bis(2-Chloroethoxy)methane ug/L ND 10.0 04/18/23 13:451.8
bis(2-Chloroethyl) ether ug/L ND 5.0 04/18/23 13:451.9
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 04/18/23 13:453.7
Butylbenzylphthalate ug/L ND 5.0 04/18/23 13:453.1
Chrysene ug/L ND 5.0 04/18/23 13:452.8
Di-n-butylphthalate ug/L ND 5.0 04/18/23 13:452.2
Di-n-octylphthalate ug/L ND 5.0 04/18/23 13:453.9
Dibenz(a,h)anthracene ug/L ND 5.0 04/18/23 13:453.0
Diethylphthalate ug/L ND 5.0 04/18/23 13:452.0
Dimethylphthalate ug/L ND 5.0 04/18/23 13:452.1
Fluoranthene ug/L ND 5.0 04/18/23 13:452.2
Fluorene ug/L ND 5.0 04/18/23 13:452.1
Hexachloro-1,3-butadiene ug/L ND 5.0 04/18/23 13:451.8
Hexachlorobenzene ug/L ND 5.0 04/18/23 13:452.2
Hexachlorocyclopentadiene ug/L ND 10.0 04/18/23 13:451.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3989086
Associated Lab Samples:92662340001
Matrix:Water
AnalyzedMDL
Hexachloroethane ug/L ND 5.0 04/18/23 13:451.4
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 04/18/23 13:452.9
Isophorone ug/L ND 10.0 04/18/23 13:451.7
N-Nitroso-di-n-propylamine ug/L ND 5.0 04/18/23 13:451.3
N-Nitrosodimethylamine ug/L ND 5.0 04/18/23 13:451.9
N-Nitrosodiphenylamine ug/L ND 10.0 04/18/23 13:453.0
Naphthalene ug/L ND 5.0 04/18/23 13:452.1
Nitrobenzene ug/L ND 5.0 04/18/23 13:451.9
Pentachlorophenol ug/L ND 10.0 04/18/23 13:453.8
Phenanthrene ug/L ND 5.0 04/18/23 13:452.0
Phenol ug/L ND 5.0 04/18/23 13:451.4
Pyrene ug/L ND 5.0 04/18/23 13:452.2
2,4,6-Tribromophenol (S)%117 10-137 04/18/23 13:45
2-Fluorobiphenyl (S)%90 15-120 04/18/23 13:45
2-Fluorophenol (S)%82 10-120 04/18/23 13:45
Nitrobenzene-d5 (S)%95 10-120 04/18/23 13:45
Phenol-d6 (S)%63 10-120 04/18/23 13:45
Terphenyl-d14 (S)%137 11-131 S304/18/23 13:45
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989087LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 32.150 64 44-142
2,2'-Oxybis(1-chloropropane)ug/L 45.850 92 36-166
2,4,6-Trichlorophenol ug/L 62.050 124 37-144
2,4-Dichlorophenol ug/L 59.150 118 1-191
2,4-Dimethylphenol ug/L 93.5 L15018732-119
2,4-Dinitrophenol ug/L 381250 152 1-181
2,4-Dinitrotoluene ug/L 62.950 126 39-139
2,6-Dinitrotoluene ug/L 60.350 121 50-158
2-Chloronaphthalene ug/L 45.050 90 60-118
2-Chlorophenol ug/L 56.050 112 23-134
2-Nitrophenol ug/L 60.350 121 29-182
3,3'-Dichlorobenzidine ug/L 133100 133 1-262
4,6-Dinitro-2-methylphenol ug/L 156100 156 1-181
4-Bromophenylphenyl ether ug/L 59.950 120 53-127
4-Chloro-3-methylphenol ug/L 118100 118 22-147
4-Chlorophenylphenyl ether ug/L 52.650 105 25-158
4-Nitrophenol ug/L 225250 90 1-132
Acenaphthene ug/L 50.750 101 47-145
Acenaphthylene ug/L 51.450 103 33-145
Anthracene ug/L 56.950 114 1-166
Benzo(a)anthracene ug/L 65.350 131 33-143
Benzo(a)pyrene ug/L 67.450 135 17-163
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3989087LABORATORY CONTROL SAMPLE:
LCSSpike
Benzo(b)fluoranthene ug/L 68.350 137 24-159
Benzo(g,h,i)perylene ug/L 69.450 139 1-219
Benzo(k)fluoranthene ug/L 66.750 133 11-162
bis(2-Chloroethoxy)methane ug/L 55.250 110 33-184
bis(2-Chloroethyl) ether ug/L 52.750 105 12-158
bis(2-Ethylhexyl)phthalate ug/L 70.650 141 8-158
Butylbenzylphthalate ug/L 72.650 145 1-152
Chrysene ug/L 65.150 130 17-168
Di-n-butylphthalate ug/L 68.5 L1501371-118
Di-n-octylphthalate ug/L 72.650 145 4-146
Dibenz(a,h)anthracene ug/L 71.750 143 1-227
Diethylphthalate ug/L 59.9 L1501201-114
Dimethylphthalate ug/L 57.5 L1501151-112
Fluoranthene ug/L 65.750 131 26-137
Fluorene ug/L 54.750 109 59-121
Hexachloro-1,3-butadiene ug/L 28.350 57 24-116
Hexachlorobenzene ug/L 60.350 121 1-152
Hexachlorocyclopentadiene ug/L 34.950 70 25-150
Hexachloroethane ug/L 27.050 54 40-113
Indeno(1,2,3-cd)pyrene ug/L 71.050 142 1-171
Isophorone ug/L 58.150 116 21-196
N-Nitroso-di-n-propylamine ug/L 53.750 107 1-230
N-Nitrosodimethylamine ug/L 50.150 100 25-150
N-Nitrosodiphenylamine ug/L 60.050 120 25-150
Naphthalene ug/L 39.050 78 21-133
Nitrobenzene ug/L 53.950 108 35-180
Pentachlorophenol ug/L 150100 150 14-176
Phenanthrene ug/L 60.3 L15012154-120
Phenol ug/L 38.250 76 5-112
Pyrene ug/L 68.5 L15013752-115
2,4,6-Tribromophenol (S)%S015710-137
2-Fluorobiphenyl (S)%104 15-120
2-Fluorophenol (S)%91 10-120
Nitrobenzene-d5 (S)%112 10-120
Phenol-d6 (S)%73 10-120
Terphenyl-d14 (S)%S015811-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3989088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35791132003
3989089
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 50 75 44-14285 12 30501.7U 37.7 42.4
2,2'-Oxybis(1-
chloropropane)ug/L 50 98 36-166106 8 30501.2U 49.0 53.2
2,4,6-Trichlorophenol ug/L 50 122 37-144134 9 30501.6U 60.8 66.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3989088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35791132003
3989089
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2,4-Dichlorophenol ug/L 50 115 1-191133 14 30501.4U 57.7 66.4
2,4-Dimethylphenol ug/L M05018932-119210 11 30501.7U 94.3 105
2,4-Dinitrophenol ug/L 250 53 1-18149 7 3025026.0U 132 122
2,4-Dinitrotoluene ug/L M15013039-139142 9 30501.6U 65.1 71.2
2,6-Dinitrotoluene ug/L 50 123 50-158134 9 30501.7U 61.4 67.1
2-Chloronaphthalene ug/L 50 88 60-11896 9 30501.7U 43.8 48.1
2-Chlorophenol ug/L 50 101 23-134110 8 30504.5J 55.0 59.5
2-Nitrophenol ug/L 50 119 29-182131 10 30501.4U 59.3 65.5
3,3'-Dichlorobenzidine ug/L 100 115 1-262121 5 301008.1U 115 121
4,6-Dinitro-2-methylphenol ug/L 100 141 1-181150 6 301007.8U 141 150
4-Bromophenylphenyl ether ug/L M15011953-127128 7 30501.8U 59.3 63.8
4-Chloro-3-methylphenol ug/L M110014522-147163 12 301003.3U 145 163
4-Chlorophenylphenyl ether ug/L 50 113 25-158121 8 30502.0U 56.3 60.7
4-Nitrophenol ug/L 250 87 1-13286 1 302506.6U 217 216
Acenaphthene ug/L 50 98 47-145108 10 30502.0U 48.8 53.9
Acenaphthylene ug/L 50 95 33-145107 11 30502.0U 47.6 53.4
Anthracene ug/L 50 118 1-166129 9 30502.3U 59.0 64.6
Benzo(a)anthracene ug/L M15013233-143144 9 30502.7U 66.2 72.2
Benzo(a)pyrene ug/L 50 128 17-163137 7 30502.8U 64.1 68.5
Benzo(b)fluoranthene ug/L 50 130 24-159137 5 30502.6U 65.1 68.7
Benzo(g,h,i)perylene ug/L 50 142 1-219162 13 30502.8U 71.1 80.9
Benzo(k)fluoranthene ug/L 50 129 11-162132 2 30502.7U 64.4 66.0
bis(2-
Chloroethoxy)methane ug/L 50 110 33-184124 13 30501.8U 54.8 62.2
bis(2-Chloroethyl) ether ug/L 50 114 12-158123 7 30501.9U 57.0 61.4
bis(2-Ethylhexyl)phthalate ug/L 50 127 8-158138 9 30503.7U 63.3 69.2
Butylbenzylphthalate ug/L 50 123 1-152133 8 30503.1U 61.6 66.5
Chrysene ug/L 50 132 17-168136 3 30502.8U 65.9 67.9
Di-n-butylphthalate ug/L M0501281-118136 6 30502.2U 63.9 67.8
Di-n-octylphthalate ug/L 50 130 4-146141 8 30503.9U 64.9 70.6
Dibenz(a,h)anthracene ug/L 50 141 1-227156 10 30503.0U 70.5 77.9
Diethylphthalate ug/L M0501311-114134 2 30502.0U 65.5 67.0
Dimethylphthalate ug/L M0501201-112132 10 30502.1U 60.0 66.0
Fluoranthene ug/L M15014026-137146 4 30502.2U 69.8 72.8
Fluorene ug/L 50 112 59-121121 8 30502.1U 55.9 60.6
Hexachloro-1,3-butadiene ug/L 50 75 24-11685 13 30501.8U 37.3 42.6
Hexachlorobenzene ug/L 50 117 1-152132 12 30502.2U 58.6 66.1
Hexachlorocyclopentadiene ug/L 50 71 25-15076 6 30501.6U 35.6 37.9
Hexachloroethane ug/L 50 58 40-11364 10 30501.4U 29.0 32.0
Indeno(1,2,3-cd)pyrene ug/L 50 143 1-171156 8 30502.9U 71.6 78.0
Isophorone ug/L 50 128 21-196141 10 30501.7U 63.8 70.5
N-Nitroso-di-n-propylamine ug/L 50 123 1-230136 10 30501.3U 61.4 67.9
N-Nitrosodimethylamine ug/L 50 143 25-150145 2 30501.9U 71.3 72.5
N-Nitrosodiphenylamine ug/L 50 116 25-150130 11 30503.0U 58.2 65.2
Naphthalene ug/L 50 72 21-13383 12 30502.4J 38.7 43.7
Nitrobenzene ug/L 50 120 35-180127 6 30501.9U 59.9 63.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
3989088MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
35791132003
3989089
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Pentachlorophenol ug/L 100 147 14-176157 7 301003.8U 147 157
Phenanthrene ug/L M05012454-120135 9 30502.0U 62.0 67.5
Phenol ug/L 50 94 5-112105 7 305034.9 81.8 87.5
Pyrene ug/L M05013252-115143 8 30502.2U 66.1 71.5
2,4,6-Tribromophenol (S)%S014210-137147
2-Fluorobiphenyl (S)%94 15-120103
2-Fluorophenol (S)%89 10-12090
Nitrobenzene-d5 (S)%S012210-120125
Phenol-d6 (S)%88 10-12090
Terphenyl-d14 (S)%S013011-131134
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 51
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92662340
ACF-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
769793
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92662340001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3996532
Associated Lab Samples:92662340001
Matrix:Water
AnalyzedMDL
Aliphatic (C09-C18)ug/L ND 100 N204/24/23 09:20100
Aliphatic (C19-C36)ug/L ND 100 N204/24/23 09:20100
Aromatic (C11-C22)ug/L ND 100 N204/24/23 09:20100
1-Chlorooctadecane (S)%96 40-140 04/24/23 09:20
2-Bromonaphthalene (S)%100 40-140 04/24/23 09:20
2-Fluorobiphenyl (S)%99 40-140 04/24/23 09:20
o-Terphenyl (S)%93 40-140 04/24/23 09:20
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3996533LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
3996534
Aliphatic (C09-C18)ug/L 198 N23006640-14081243 21 50
Aliphatic (C19-C36)ug/L 460 N240011540-140135541 16 50
Aromatic (C11-C22)ug/L 772 N28509140-140102866 12 50
1-Chlorooctadecane (S)%87 40-14098
2-Bromonaphthalene (S)%49 40-14050
2-Fluorobiphenyl (S)%52 40-14054
o-Terphenyl (S)%86 40-140102
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 51
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92662340
ACF-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 51
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92662340
ACF-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92662340001 769793 769834HH TMW-1 MADEP EPH MADEP EPH
92662340001 768326 768332HH TMW-1 EPA 3010A EPA 6020B
92662340001 768304 768722HH TMW-1 EPA 625.1 EPA 625.1
92662340001 769533HH TMW-1 SM 6200B
92662340002 768966TRIP BLANK SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/26/2023 09:45 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 51
Page 36 of 51
Page 37 of 51
Page 38 of 51
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
April 24, 2023
Taylor Cannon
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Project Location: ACF-001
Client Job Number:
Project Number: 92662340
Laboratory Work Order Number: 23D1964
Enclosed are results of analyses for samples as received by the laboratory on April 18, 2023. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Rebecca Faust
Project Manager
Page 1 of 13
Table of Contents
Page 39 of 51
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
23D1964-01 5
Sample Preparation Information 6
QC Data 7
Petroleum Hydrocarbons Analyses - VPH 7
B337464 7
Flag/Qualifier Summary 9
Certifications 10
Chain of Custody/Sample Receipt 11
Page 2 of 13
Table of Contents
Page 40 of 51
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
4/24/2023
Pace Analytical Services - NC
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
ATTN: Taylor Cannon
92662340
23D1964
The results of analyses performed on the following samples submitted to CON-TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
ACF-001
HH TMW-1 23D1964-01 Water MADEP-VPH-Feb
2018 Rev 2.1
[TOC_1]Sample Summary[TOC]
Page 3 of 13
Table of Contents
Page 41 of 51
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method MA VPH only hydrocarbon ranges were requested and reported.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-Feb 2018 Rev 2.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
Analytical column used for VPH analysis is Restek, Rtx-502.2, 105meter, 0.53mmID, 3um df. Trap used for VPH analysis is Carbopack B/CarboSieveS-III.
The results of analyses reported only relate to samples submitted to Con-Test, a Pace Analytical Laboratory, for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 4 of 13
Table of Contents
Page 42 of 51
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Date Received: 4/18/2023
Work Order: 23D1964Sample Description:Project Location: ACF-001
Sample ID: 23D1964-01
Field Sample #: HH TMW-1
Sample Matrix: Water
Sampled: 4/13/2023 13:00
[TOC_2]23D1964-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 4/19/23 16:14 EEHg/L 4/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C5-C8 Aliphatics
ND 100 4/19/23 16:14 EEHg/L 4/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C5-C8 Aliphatics
ND 100 4/19/23 16:14 EEHg/L 4/18/23MADEP-VPH-Feb 2018
Rev 2.1
1Unadjusted C9-C12 Aliphatics
ND 100 4/19/23 16:14 EEHg/L 4/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C12 Aliphatics
ND 100 4/19/23 16:14 EEHg/L 4/18/23MADEP-VPH-Feb 2018
Rev 2.1
1C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)80.2 4/19/23 16:1470-130
2,5-Dibromotoluene (PID)78.7 4/19/23 16:1470-130
[TOC_1]Sample Results[TOC]
Page 5 of 13
Table of Contents
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Sample Extraction Data
Prep Method: MA VPH Analytical Method: MADEP-VPH-Feb 2018 Rev 2.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B337464 04/18/235 5.0023D1964-01 [HH TMW-1]
[TOC_1]Sample Preparation Information[TOC]
Page 6 of 13
Table of Contents
Page 44 of 51
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B337464 - MA VPH
[TOC_3]B337464[TOC]
Blank (B337464-BLK1) Prepared: 04/18/23 Analyzed: 04/19/23
Unadjusted C5-C8 Aliphatics g/L100ND
C5-C8 Aliphatics g/L100ND
Unadjusted C9-C12 Aliphatics g/L100ND
C9-C12 Aliphatics g/L100ND
C9-C10 Aromatics g/L100ND
Benzene g/L1.0ND
Butylcyclohexane g/L1.0ND
Decane g/L1.0ND
Ethylbenzene g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
2-Methylpentane g/L1.0ND
Naphthalene g/L5.0ND
Nonane g/L1.0ND
Pentane g/L1.0ND
Toluene g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
2,2,4-Trimethylpentane g/L1.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)86.334.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)85.134.0
LCS (B337464-BS1) Prepared: 04/18/23 Analyzed: 04/19/23
Unadjusted C5-C8 Aliphatics g/L100 150 70-13095.2143
Unadjusted C9-C12 Aliphatics g/L100 150 70-13099.2149
C9-C10 Aromatics g/L100 50.0 70-13010452.2
Benzene g/L1.0 50.0 70-13010954.4
Butylcyclohexane g/L1.0 50.0 70-13010853.9
Decane g/L1.0 50.0 70-13080.440.2
Ethylbenzene g/L1.0 50.0 70-13010653.0
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 70-13010652.9
2-Methylpentane g/L1.0 50.0 70-13010150.3
Naphthalene g/L5.0 50.0 70-13078.039.0
Nonane g/L1.0 50.0 70-13010954.7
Pentane g/L1.0 50.0 70-13091.145.6
Toluene g/L1.0 50.0 70-13010753.4
1,2,4-Trimethylbenzene g/L1.0 50.0 70-13010452.2
2,2,4-Trimethylpentane g/L1.0 50.0 70-13093.946.9
m+p Xylene g/L2.0 100 70-130105105
o-Xylene g/L1.0 50.0 70-13010753.4
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10441.6
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)10843.0
[TOC_1]QC Data[TOC]
Page 7 of 13
Table of Contents
Page 45 of 51
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B337464 - MA VPH
LCS Dup (B337464-BSD1) Prepared: 04/18/23 Analyzed: 04/19/23
Unadjusted C5-C8 Aliphatics g/L100 150 2570-13094.5 0.806142
Unadjusted C9-C12 Aliphatics g/L100 150 2570-13097.0 2.24145
C9-C10 Aromatics g/L100 50.0 2570-130105 0.95052.7
Benzene g/L1.0 50.0 2570-130111 1.8455.4
Butylcyclohexane g/L1.0 50.0 2570-130105 2.2452.7
Decane g/L1.0 50.0 2570-13078.2 2.8339.1
Ethylbenzene g/L1.0 50.0 2570-130108 1.7153.9
Methyl tert-Butyl Ether (MTBE)g/L1.0 50.0 2570-130106 0.59753.2
2-Methylpentane g/L1.0 50.0 2570-130100 0.24350.2
Naphthalene g/L5.0 50.0 2570-13080.5 3.2040.2
Nonane g/L1.0 50.0 2570-130107 1.8153.7
Pentane g/L1.0 50.0 2570-13090.1 1.0845.1
Toluene g/L1.0 50.0 2570-130108 1.2354.1
1,2,4-Trimethylbenzene g/L1.0 50.0 2570-130105 0.95052.7
2,2,4-Trimethylpentane g/L1.0 50.0 2570-13092.8 1.1546.4
m+p Xylene g/L2.0 100 2570-130107 1.62107
o-Xylene g/L1.0 50.0 2570-130108 1.0654.0
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)10943.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)11144.6
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-Feb 2018 Rev 2.1 in Water
CT,NC,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,ME,NH-PC5-C8 Aliphatics
CT,NC,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,ME,NH-PC9-C12 Aliphatics
CT,NC,ME,NH-PC9-C10 Aromatics
[TOC_1]Certifications[TOC]
Con-Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code Description Number Expires
PH-0821Connecticut Department of Public HealthCT 12/31/2024
652North Carolina Div. of Water QualityNC 12/31/2023
MA00100State of MaineME 06/9/2023
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2023
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Appendix D

Prior Assessment Results
REFERENCE
DATE:DWG SCALE:
DRAWN BY:CHECKED BY:APPROVED BY:
PROJECT NO:
FIGURE NO.:
SAMPLE LOCATION MAP
322-6951"=20'JUL 2022
PAB AJK BDR 2
GALLIVAN, WHITE & BOYD, P.A.
ATLANTIC COAST FIRE TRUCKS
4718 MOUNTAIN CREEK AVE, DENVER
CATAWBA COUNTY, NORTH CAROLINA
www.cecinc.com
3701 Arco Corporate Drive · Suite 400 · Charlotte, NC 28273
Ph: 980.237.0373 · Fax: [phone]
NORTH
Table 1
Summary of Laboratory Results
Atlantic Coast Fire Trucks
4718 Mountain Creek Ave., Denver, NC 28037
Soil-to-Water
MSCC
Residential
MSCC
Industrial/
Commercial
MSCC Action Level CEC-A1 CEC-A2 CEC-A3 CEC-B1 CEC-B2 CEC-B3 CEC-C1 CEC- C2 CEC-D1 CEC-E1 CEC-F1 CEC-G1
Sample Date 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022 6/29/2022
Sample Depth 0.5-1 1-2 0-0.5 0.5-1 1-2 0-0.5 1.5-2 1-2 1.5-2 1.5-2 1-1.5 1-1.5
Diesel Range Organics (C10-C28)------100 150 1,300 5.5J 7.5J 6.0J 3.2J 45 7.8J 8.9J 8.3J ND 3.7J
Gasoline Range Organics (C6-C10)-- -- --50 ND ND ND ND ND ND ND ND ND ND ND ND
Bis(2-ethylhexyl)phalate (DEPH)6.6 47 233 --NA 0.16J NA NA ND NA NA NA ND NA NA ND
--NA NA NA NA NA NA NA NA ND
--NA NA NA NA NA NA NA NA ND
Acetone 24 14000 210000 --NA 0.058 NA NA 0.047 NA NA NA 0.11 NA NA ND
--NA NA NA NA NA NA NA NA 3.4J
Notes:
1) MSCC = NCDEQ UST Section - Compreshensive Tables for Corrective Action Guidelines, March 7, 2022 Version- Table 1 Maximum Soil Contaminant Concentration Levels (MSCC)
2) Soil action level - Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement, May 17, 2021 Version
3) ND = Not Detected
4) NA = Not Analyzed
5) Bold and shaded = constituent concentration exceeds MSCC or action level
6) J = Estimated Concentration, concentration above method detecction limit but less than laboratory reporting limit
7) Sample depth in Ft. BGS or BTC
Parameter
Soil Sample - Concentration of Constituents
SemiVolatile Organic Compounds-PAHs (SVOC-PAHs 8270)
Volatile Organic Compounds (VOCs) 8260D/5035A (ug/kg)
8015 GCS THC-Diesel (mg/kg)
8015 Gasoline Range Organics (mg/kg)
NCDEQ Comparison Criteria (mg/kg)

Soil sample location

Drawing / Project Name
Client
Project # Date
N
Base diagram from Google Earth.
Soil Sample Location Diagram (9/29/2022)
Soil Assessment
4718 Mountain Creek Ave.; Denver, North Carolina
Arnold and Smith, LLC

DB Fig. Scale
611001
As Shown
October 2022
3
PM PG
JB
PE
JB JB
Approximate Scale
feet
0 50 25
Stained
Areas
Sampling
Area
(9/29/2022
Collection DateDepth of Collection (feet BGS)SL-1 9/29/2022 Surface 33.4299.7SL-1A 9/29/2022 0.5 2.1 11Plastic 9/29/2022 na 39.2482.450 100Notes:Bold denotes concentration equal to or greater than State Action Limits.NCDEQ State Action LimitTable 1Summary of Analytical DataRedLab UVF (mg/Kg)Gasoline Range Organics Diesel Range OrganicsHES Project #611001Site Assessment - Denver, North CarolinaArnold and Smith, LLPAnalytical Method (e.g., VOC by EPA 8260B)Constituent of ConcernSample ID Number