WS-6178_23033_CA_LAB_20150727_Analytical_Data

#=CL#
July 27, 2015
LIMS USE: FR - WAYNE WATTERSON
LIMS OBJECT ID: 92259363
92259363
Project:
Pace Project No.:
RE:
Mr. Wayne Watterson
S&ME, Inc.
8646 West Market Street
Greensboro, NC 27409
FORMER SCOTT PROPERTY
Dear Mr. Watterson:
Enclosed are the analytical results for sample(s) received by the laboratory on July 17, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 18
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 18
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92259363001 WSW-2 SM 6200B 63 PASI-CCAH
92259363002 WSW-12 SM 6200B 63 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 18
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Method:
Client:S&ME, Inc.
SM 6200B
Date:July 27, 2015
Description:6200B MSV
General Information:
2 samples were analyzed for SM 6200B. All samples were received in acceptable condition with any exceptions noted below or on the
chain-of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: MSV/32684
L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
• LCS (Lab ID: 1517799)
• Hexachloro-1,3-butadiene
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MSV/32684
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92259368007
M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
• MS (Lab ID: 1517800)
• Hexachloro-1,3-butadiene
• MSD (Lab ID: 1517801)
• Hexachloro-1,3-butadiene
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1517800)
• Bromomethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 18
#=NA#
PROJECT NARRATIVE
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Method:
Client:S&ME, Inc.
SM 6200B
Date:July 27, 2015
Description:6200B MSV
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Sample:WSW-2 Lab ID:92259363001 Collected:07/14/15 10:10 Received:07/17/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 07/24/15 14:22 71-43-20.50 1
Bromobenzene <0.50 ug/L 07/24/15 14:22 108-86-10.50 1
Bromochloromethane <0.50 ug/L 07/24/15 14:22 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 07/24/15 14:22 75-27-40.50 1
Bromoform <0.50 ug/L 07/24/15 14:22 75-25-20.50 1
Bromomethane <5.0 ug/L 07/24/15 14:22 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 07/24/15 14:22 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 07/24/15 14:22 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 07/24/15 14:22 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 07/24/15 14:22 56-23-50.50 1
Chlorobenzene <0.50 ug/L 07/24/15 14:22 108-90-70.50 1
Chloroethane <1.0 ug/L 07/24/15 14:22 75-00-31.0 1
Chloroform <0.50 ug/L 07/24/15 14:22 67-66-30.50 1
Chloromethane <1.0 ug/L 07/24/15 14:22 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 07/24/15 14:22 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 07/24/15 14:22 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 07/24/15 14:22 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 07/24/15 14:22 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 07/24/15 14:22 106-93-40.50 1
Dibromomethane <0.50 ug/L 07/24/15 14:22 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 07/24/15 14:22 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 07/24/15 14:22 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 07/24/15 14:22 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 07/24/15 14:22 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 07/24/15 14:22 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 07/24/15 14:22 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 07/24/15 14:22 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 07/24/15 14:22 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 07/24/15 14:22 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 07/24/15 14:22 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 07/24/15 14:22 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 07/24/15 14:22 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 07/24/15 14:22 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 07/24/15 14:22 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 07/24/15 14:22 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 07/24/15 14:22 108-20-30.50 1
Ethylbenzene <0.50 ug/L 07/24/15 14:22 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 07/24/15 14:22 87-68-3 L32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 07/24/15 14:22 98-82-80.50 1
Methylene Chloride <2.0 ug/L 07/24/15 14:22 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 07/24/15 14:22 1634-04-40.50 1
Naphthalene <2.0 ug/L 07/24/15 14:22 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 07/24/15 14:22 103-65-10.50 1
Styrene <0.50 ug/L 07/24/15 14:22 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 07/24/15 14:22 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 07/24/15 14:22 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 07/24/15 14:22 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Sample:WSW-2 Lab ID:92259363001 Collected:07/14/15 10:10 Received:07/17/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 07/24/15 14:22 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 07/24/15 14:22 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 07/24/15 14:22 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 07/24/15 14:22 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 07/24/15 14:22 79-00-50.50 1
Trichloroethene <0.50 ug/L 07/24/15 14:22 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 07/24/15 14:22 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 07/24/15 14:22 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 07/24/15 14:22 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 07/24/15 14:22 108-67-80.50 1
Vinyl chloride <1.0 ug/L 07/24/15 14:22 75-01-41.0 1
m&p-Xylene <1.0 ug/L 07/24/15 14:22 179601-23-11.0 1
o-Xylene <0.50 ug/L 07/24/15 14:22 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %07/24/15 14:22 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %07/24/15 14:22 460-00-470-130 1
Toluene-d8 (S)101 %07/24/15 14:22 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Sample:WSW-12 Lab ID:92259363002 Collected:07/14/15 09:40 Received:07/17/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene <0.50 ug/L 07/24/15 14:38 71-43-20.50 1
Bromobenzene <0.50 ug/L 07/24/15 14:38 108-86-10.50 1
Bromochloromethane <0.50 ug/L 07/24/15 14:38 74-97-50.50 1
Bromodichloromethane <0.50 ug/L 07/24/15 14:38 75-27-40.50 1
Bromoform <0.50 ug/L 07/24/15 14:38 75-25-20.50 1
Bromomethane <5.0 ug/L 07/24/15 14:38 74-83-95.0 1
n-Butylbenzene <0.50 ug/L 07/24/15 14:38 104-51-80.50 1
sec-Butylbenzene <0.50 ug/L 07/24/15 14:38 135-98-80.50 1
tert-Butylbenzene <0.50 ug/L 07/24/15 14:38 98-06-60.50 1
Carbon tetrachloride <0.50 ug/L 07/24/15 14:38 56-23-50.50 1
Chlorobenzene <0.50 ug/L 07/24/15 14:38 108-90-70.50 1
Chloroethane <1.0 ug/L 07/24/15 14:38 75-00-31.0 1
Chloroform <0.50 ug/L 07/24/15 14:38 67-66-30.50 1
Chloromethane <1.0 ug/L 07/24/15 14:38 74-87-31.0 1
2-Chlorotoluene <0.50 ug/L 07/24/15 14:38 95-49-80.50 1
4-Chlorotoluene <0.50 ug/L 07/24/15 14:38 106-43-40.50 1
1,2-Dibromo-3-chloropropane <1.0 ug/L 07/24/15 14:38 96-12-81.0 1
Dibromochloromethane <0.50 ug/L 07/24/15 14:38 124-48-10.50 1
1,2-Dibromoethane (EDB)<0.50 ug/L 07/24/15 14:38 106-93-40.50 1
Dibromomethane <0.50 ug/L 07/24/15 14:38 74-95-30.50 1
1,2-Dichlorobenzene <0.50 ug/L 07/24/15 14:38 95-50-10.50 1
1,3-Dichlorobenzene <0.50 ug/L 07/24/15 14:38 541-73-10.50 1
1,4-Dichlorobenzene <0.50 ug/L 07/24/15 14:38 106-46-70.50 1
Dichlorodifluoromethane <0.50 ug/L 07/24/15 14:38 75-71-80.50 1
1,1-Dichloroethane <0.50 ug/L 07/24/15 14:38 75-34-30.50 1
1,2-Dichloroethane <0.50 ug/L 07/24/15 14:38 107-06-20.50 1
1,1-Dichloroethene <0.50 ug/L 07/24/15 14:38 75-35-40.50 1
cis-1,2-Dichloroethene <0.50 ug/L 07/24/15 14:38 156-59-20.50 1
trans-1,2-Dichloroethene <0.50 ug/L 07/24/15 14:38 156-60-50.50 1
1,2-Dichloropropane <0.50 ug/L 07/24/15 14:38 78-87-50.50 1
1,3-Dichloropropane <0.50 ug/L 07/24/15 14:38 142-28-90.50 1
2,2-Dichloropropane <0.50 ug/L 07/24/15 14:38 594-20-70.50 1
1,1-Dichloropropene <0.50 ug/L 07/24/15 14:38 563-58-60.50 1
cis-1,3-Dichloropropene <0.50 ug/L 07/24/15 14:38 10061-01-50.50 1
trans-1,3-Dichloropropene <0.50 ug/L 07/24/15 14:38 10061-02-60.50 1
Diisopropyl ether <0.50 ug/L 07/24/15 14:38 108-20-30.50 1
Ethylbenzene <0.50 ug/L 07/24/15 14:38 100-41-40.50 1
Hexachloro-1,3-butadiene <2.0 ug/L 07/24/15 14:38 87-68-3 L32.0 1
Isopropylbenzene (Cumene)<0.50 ug/L 07/24/15 14:38 98-82-80.50 1
Methylene Chloride <2.0 ug/L 07/24/15 14:38 75-09-22.0 1
Methyl-tert-butyl ether <0.50 ug/L 07/24/15 14:38 1634-04-40.50 1
Naphthalene <2.0 ug/L 07/24/15 14:38 91-20-32.0 1
n-Propylbenzene <0.50 ug/L 07/24/15 14:38 103-65-10.50 1
Styrene <0.50 ug/L 07/24/15 14:38 100-42-50.50 1
1,1,1,2-Tetrachloroethane <0.50 ug/L 07/24/15 14:38 630-20-60.50 1
1,1,2,2-Tetrachloroethane <0.50 ug/L 07/24/15 14:38 79-34-50.50 1
Tetrachloroethene <0.50 ug/L 07/24/15 14:38 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Sample:WSW-12 Lab ID:92259363002 Collected:07/14/15 09:40 Received:07/17/15 15:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene <0.50 ug/L 07/24/15 14:38 108-88-30.50 1
1,2,3-Trichlorobenzene <2.0 ug/L 07/24/15 14:38 87-61-62.0 1
1,2,4-Trichlorobenzene <2.0 ug/L 07/24/15 14:38 120-82-12.0 1
1,1,1-Trichloroethane <0.50 ug/L 07/24/15 14:38 71-55-60.50 1
1,1,2-Trichloroethane <0.50 ug/L 07/24/15 14:38 79-00-50.50 1
Trichloroethene <0.50 ug/L 07/24/15 14:38 79-01-60.50 1
Trichlorofluoromethane <1.0 ug/L 07/24/15 14:38 75-69-41.0 1
1,2,3-Trichloropropane <0.50 ug/L 07/24/15 14:38 96-18-40.50 1
1,2,4-Trimethylbenzene <0.50 ug/L 07/24/15 14:38 95-63-60.50 1
1,3,5-Trimethylbenzene <0.50 ug/L 07/24/15 14:38 108-67-80.50 1
Vinyl chloride <1.0 ug/L 07/24/15 14:38 75-01-41.0 1
m&p-Xylene <1.0 ug/L 07/24/15 14:38 179601-23-11.0 1
o-Xylene <0.50 ug/L 07/24/15 14:38 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %07/24/15 14:38 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %07/24/15 14:38 460-00-470-130 1
Toluene-d8 (S)103 %07/24/15 14:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32684
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92259363001, 92259363002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1517798
Associated Lab Samples:92259363001, 92259363002
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L <0.50 0.50 07/24/15 12:09
1,1,1-Trichloroethane ug/L <0.50 0.50 07/24/15 12:09
1,1,2,2-Tetrachloroethane ug/L <0.50 0.50 07/24/15 12:09
1,1,2-Trichloroethane ug/L <0.50 0.50 07/24/15 12:09
1,1-Dichloroethane ug/L <0.50 0.50 07/24/15 12:09
1,1-Dichloroethene ug/L <0.50 0.50 07/24/15 12:09
1,1-Dichloropropene ug/L <0.50 0.50 07/24/15 12:09
1,2,3-Trichlorobenzene ug/L <2.0 2.0 07/24/15 12:09
1,2,3-Trichloropropane ug/L <0.50 0.50 07/24/15 12:09
1,2,4-Trichlorobenzene ug/L <2.0 2.0 07/24/15 12:09
1,2,4-Trimethylbenzene ug/L <0.50 0.50 07/24/15 12:09
1,2-Dibromo-3-chloropropane ug/L <1.0 1.0 07/24/15 12:09
1,2-Dibromoethane (EDB)ug/L <0.50 0.50 07/24/15 12:09
1,2-Dichlorobenzene ug/L <0.50 0.50 07/24/15 12:09
1,2-Dichloroethane ug/L <0.50 0.50 07/24/15 12:09
1,2-Dichloropropane ug/L <0.50 0.50 07/24/15 12:09
1,3,5-Trimethylbenzene ug/L <0.50 0.50 07/24/15 12:09
1,3-Dichlorobenzene ug/L <0.50 0.50 07/24/15 12:09
1,3-Dichloropropane ug/L <0.50 0.50 07/24/15 12:09
1,4-Dichlorobenzene ug/L <0.50 0.50 07/24/15 12:09
2,2-Dichloropropane ug/L <0.50 0.50 07/24/15 12:09
2-Chlorotoluene ug/L <0.50 0.50 07/24/15 12:09
4-Chlorotoluene ug/L <0.50 0.50 07/24/15 12:09
Benzene ug/L <0.50 0.50 07/24/15 12:09
Bromobenzene ug/L <0.50 0.50 07/24/15 12:09
Bromochloromethane ug/L <0.50 0.50 07/24/15 12:09
Bromodichloromethane ug/L <0.50 0.50 07/24/15 12:09
Bromoform ug/L <0.50 0.50 07/24/15 12:09
Bromomethane ug/L <5.0 5.0 07/24/15 12:09
Carbon tetrachloride ug/L <0.50 0.50 07/24/15 12:09
Chlorobenzene ug/L <0.50 0.50 07/24/15 12:09
Chloroethane ug/L <1.0 1.0 07/24/15 12:09
Chloroform ug/L <0.50 0.50 07/24/15 12:09
Chloromethane ug/L <1.0 1.0 07/24/15 12:09
cis-1,2-Dichloroethene ug/L <0.50 0.50 07/24/15 12:09
cis-1,3-Dichloropropene ug/L <0.50 0.50 07/24/15 12:09
Dibromochloromethane ug/L <0.50 0.50 07/24/15 12:09
Dibromomethane ug/L <0.50 0.50 07/24/15 12:09
Dichlorodifluoromethane ug/L <0.50 0.50 07/24/15 12:09
Diisopropyl ether ug/L <0.50 0.50 07/24/15 12:09
Ethylbenzene ug/L <0.50 0.50 07/24/15 12:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1517798
Associated Lab Samples:92259363001, 92259363002
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L <2.0 2.0 07/24/15 12:09
Isopropylbenzene (Cumene)ug/L <0.50 0.50 07/24/15 12:09
m&p-Xylene ug/L <1.0 1.0 07/24/15 12:09
Methyl-tert-butyl ether ug/L <0.50 0.50 07/24/15 12:09
Methylene Chloride ug/L <2.0 2.0 07/24/15 12:09
n-Butylbenzene ug/L <0.50 0.50 07/24/15 12:09
n-Propylbenzene ug/L <0.50 0.50 07/24/15 12:09
Naphthalene ug/L <2.0 2.0 07/24/15 12:09
o-Xylene ug/L <0.50 0.50 07/24/15 12:09
sec-Butylbenzene ug/L <0.50 0.50 07/24/15 12:09
Styrene ug/L <0.50 0.50 07/24/15 12:09
tert-Butylbenzene ug/L <0.50 0.50 07/24/15 12:09
Tetrachloroethene ug/L <0.50 0.50 07/24/15 12:09
Toluene ug/L <0.50 0.50 07/24/15 12:09
trans-1,2-Dichloroethene ug/L <0.50 0.50 07/24/15 12:09
trans-1,3-Dichloropropene ug/L <0.50 0.50 07/24/15 12:09
Trichloroethene ug/L <0.50 0.50 07/24/15 12:09
Trichlorofluoromethane ug/L <1.0 1.0 07/24/15 12:09
Vinyl chloride ug/L <1.0 1.0 07/24/15 12:09
1,2-Dichloroethane-d4 (S)%99 70-130 07/24/15 12:09
4-Bromofluorobenzene (S)%102 70-130 07/24/15 12:09
Toluene-d8 (S)%100 70-130 07/24/15 12:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1517799LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 60.350 121 60-140
1,1,1-Trichloroethane ug/L 57.450 115 60-140
1,1,2,2-Tetrachloroethane ug/L 58.150 116 60-140
1,1,2-Trichloroethane ug/L 54.850 110 60-140
1,1-Dichloroethane ug/L 54.350 109 60-140
1,1-Dichloroethene ug/L 54.550 109 60-140
1,1-Dichloropropene ug/L 59.150 118 60-140
1,2,3-Trichlorobenzene ug/L 55.250 110 60-140
1,2,3-Trichloropropane ug/L 57.050 114 60-140
1,2,4-Trichlorobenzene ug/L 55.250 110 60-140
1,2,4-Trimethylbenzene ug/L 59.750 119 60-140
1,2-Dibromo-3-chloropropane ug/L 55.450 111 60-140
1,2-Dibromoethane (EDB)ug/L 58.450 117 60-140
1,2-Dichlorobenzene ug/L 58.550 117 60-140
1,2-Dichloroethane ug/L 46.550 93 60-140
1,2-Dichloropropane ug/L 56.750 113 60-140
1,3,5-Trimethylbenzene ug/L 61.250 122 60-140
1,3-Dichlorobenzene ug/L 59.750 119 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
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Huntersville, NC 28078
[phone]
Page 11 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1517799LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 55.550 111 60-140
1,4-Dichlorobenzene ug/L 55.950 112 60-140
2,2-Dichloropropane ug/L 59.450 119 60-140
2-Chlorotoluene ug/L 58.550 117 60-140
4-Chlorotoluene ug/L 58.150 116 60-140
Benzene ug/L 58.650 117 60-140
Bromobenzene ug/L 54.550 109 60-140
Bromochloromethane ug/L 55.450 111 60-140
Bromodichloromethane ug/L 56.450 113 60-140
Bromoform ug/L 57.450 115 60-140
Bromomethane ug/L 47.550 95 60-140
Carbon tetrachloride ug/L 59.450 119 60-140
Chlorobenzene ug/L 60.150 120 60-140
Chloroethane ug/L 47.750 95 60-140
Chloroform ug/L 55.250 110 60-140
Chloromethane ug/L 52.750 105 60-140
cis-1,2-Dichloroethene ug/L 53.950 108 60-140
cis-1,3-Dichloropropene ug/L 58.250 116 60-140
Dibromochloromethane ug/L 57.950 116 60-140
Dibromomethane ug/L 55.150 110 60-140
Dichlorodifluoromethane ug/L 58.050 116 60-140
Diisopropyl ether ug/L 51.950 104 60-140
Ethylbenzene ug/L 61.850 124 60-140
Hexachloro-1,3-butadiene ug/L 71.4 L05014360-140
Isopropylbenzene (Cumene)ug/L 63.850 128 60-140
m&p-Xylene ug/L 125100 125 60-140
Methyl-tert-butyl ether ug/L 54.950 110 60-140
Methylene Chloride ug/L 47.450 95 60-140
n-Butylbenzene ug/L 65.450 131 60-140
n-Propylbenzene ug/L 64.350 129 60-140
Naphthalene ug/L 55.950 112 60-140
o-Xylene ug/L 59.150 118 60-140
sec-Butylbenzene ug/L 66.550 133 60-140
Styrene ug/L 59.150 118 60-140
tert-Butylbenzene ug/L 53.050 106 60-140
Tetrachloroethene ug/L 60.950 122 60-140
Toluene ug/L 58.050 116 60-140
trans-1,2-Dichloroethene ug/L 53.350 107 60-140
trans-1,3-Dichloropropene ug/L 56.350 113 60-140
Trichloroethene ug/L 58.250 116 60-140
Trichlorofluoromethane ug/L 53.750 107 60-140
Vinyl chloride ug/L 55.050 110 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1517800MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92259368007
1517801
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 121 60-140121 120ND24.3 24.1
1,1,1-Trichloroethane ug/L 20 129 60-140127 220ND25.8 25.4
1,1,2,2-Tetrachloroethane ug/L 20 118 60-140118 020ND23.6 23.6
1,1,2-Trichloroethane ug/L 20 116 60-140112 320ND23.1 22.3
1,1-Dichloroethane ug/L 20 120 60-140116 420ND24.1 23.2
1,1-Dichloroethene ug/L 20 123 60-140123 020ND24.6 24.6
1,1-Dichloropropene ug/L 20 125 60-140129 320ND25.0 25.7
1,2,3-Trichlorobenzene ug/L 20 117 60-140114 220ND23.3 22.8
1,2,3-Trichloropropane ug/L 20 120 60-140120 120ND24.1 23.9
1,2,4-Trichlorobenzene ug/L 20 117 60-140114 220ND23.3 22.8
1,2,4-Trimethylbenzene ug/L 20 124 60-140123 120ND24.8 24.6
1,2-Dibromo-3-chloropropane ug/L 20 111 60-140111 020ND22.2 22.1
1,2-Dibromoethane (EDB)ug/L 20 119 60-140120 120ND23.7 24.0
1,2-Dichlorobenzene ug/L 20 122 60-140121 120ND24.4 24.2
1,2-Dichloroethane ug/L 20 101 60-140103 220ND20.2 20.6
1,2-Dichloropropane ug/L 20 123 60-140121 220ND24.6 24.2
1,3,5-Trimethylbenzene ug/L 20 128 60-140127 020ND25.5 25.5
1,3-Dichlorobenzene ug/L 20 122 60-140123 020ND24.5 24.6
1,3-Dichloropropane ug/L 20 117 60-140117 020ND23.4 23.4
1,4-Dichlorobenzene ug/L 20 119 60-140117 220ND23.8 23.4
2,2-Dichloropropane ug/L 20 133 60-140131 120ND26.7 26.3
2-Chlorotoluene ug/L 20 118 60-140121 320ND23.6 24.2
4-Chlorotoluene ug/L 20 123 60-140122 120ND24.7 24.5
Benzene ug/L 20 123 60-140121 220ND24.6 24.1
Bromobenzene ug/L 20 113 60-140111 220ND22.7 22.3
Bromochloromethane ug/L 20 123 60-140120 320ND24.7 24.0
Bromodichloromethane ug/L 20 114 60-140115 120ND22.7 23.0
Bromoform ug/L 20 100 60-14098 120ND19.9 19.6
Bromomethane ug/L M1205660-14060 720ND11.3 12.1
Carbon tetrachloride ug/L 20 129 60-140128 120ND25.8 25.6
Chlorobenzene ug/L 20 126 60-140125 120ND25.3 25.0
Chloroethane ug/L 20 108 60-14097 1020ND21.6 19.5
Chloroform ug/L 20 113 60-140121 720ND22.5 24.1
Chloromethane ug/L 20 97 60-14094 320ND20.0 19.4
cis-1,2-Dichloroethene ug/L 20 121 60-140119 220ND24.2 23.7
cis-1,3-Dichloropropene ug/L 20 119 60-140116 220ND23.8 23.3
Dibromochloromethane ug/L 20 109 60-140108 120ND21.9 21.6
Dibromomethane ug/L 20 115 60-140118 220ND23.0 23.5
Dichlorodifluoromethane ug/L 20 127 60-140128 120ND25.5 25.6
Diisopropyl ether ug/L 20 112 60-140112 020ND22.4 22.3
Ethylbenzene ug/L 20 129 60-140128 120ND25.8 25.6
Hexachloro-1,3-butadiene ug/L M02015460-140161 520ND30.7 32.2
Isopropylbenzene (Cumene)ug/L 20 133 60-140132 020ND26.5 26.5
m&p-Xylene ug/L 40 132 60-140131 140ND52.6 52.2
Methyl-tert-butyl ether ug/L 20 108 60-140108 020ND21.5 21.6
Methylene Chloride ug/L 20 106 60-140108 220ND21.2 21.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1517800MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92259368007
1517801
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 134 60-140132 120ND26.8 26.4
n-Propylbenzene ug/L 20 135 60-140135 020ND27.1 27.1
Naphthalene ug/L 20 116 60-140116 020ND23.1 23.2
o-Xylene ug/L 20 123 60-140122 120ND24.7 24.3
sec-Butylbenzene ug/L 20 139 60-140138 120ND27.8 27.7
Styrene ug/L 20 123 60-140123 020ND24.6 24.5
tert-Butylbenzene ug/L 20 111 60-140111 020ND22.2 22.3
Tetrachloroethene ug/L 20 132 60-140134 120ND26.5 26.8
Toluene ug/L 20 125 60-140122 220ND24.9 24.5
trans-1,2-Dichloroethene ug/L 20 120 60-140118 220ND23.9 23.5
trans-1,3-Dichloropropene ug/L 20 115 60-140114 120ND23.1 22.8
Trichloroethene ug/L 20 129 60-140128 120ND25.9 25.6
Trichlorofluoromethane ug/L 20 122 60-140120 220ND24.4 24.0
Vinyl chloride ug/L 20 118 60-140118 020ND23.6 23.7
1,2-Dichloroethane-d4 (S)%100 70-13095
4-Bromofluorobenzene (S)%100 70-130101
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 18
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 18
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92259363
FORMER SCOTT PROPERTY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92259363001 MSV/32684WSW-2 SM 6200B
92259363002 MSV/32684WSW-12 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/27/2015 02:03 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 18
Page 17 of 18
Page 18 of 18