WS-4540_14744_CA_ LSA_20150731_PhaseI

2725 East Millbrook Road
Suite 121
Raleigh, NC 27604
Tel: [phone]
Fax: [phone]
www.atcassociates.com
N.C. Engineering License No. C-1598

July 31, 2015

Mr. Linda Blalock
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Underground Storage Tank Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Re: Phase I Limited Site Assessment
Sheltontown Grocery
3170 Westfield Road
Mt. Airy, Surry County, North Carolina
NCDENR Incident No. 14744
ATC Project No. 45.18514.4027

Dear Ms. Blalock:

ATC Associates of North Carolina, P.C. (ATC) is submitting the enclosed Phase I Limited Site
Assessment for the Sheltontown Grocery site. The report presents investigative procedures, field
activities, and laboratory analytical results for assessment activities conducted in July 2014 and
August 2014. If you have any questions or require additional information, please contact our office
at [phone].

Sincerely,

ATC Associates of North Carolina, P.C.

Ashley M. Winkelman, P.G. Gabriel Araos, P.E.
Project Geologist Senior Project Manager

Jeffrey A. Corson
Program Manager

Phase I Limited Site Assessment

Sheltontown Grocery
Incident #14744
3170 Westfield Road
Mt. Airy, Surry County, North Carolina
ATC Project No. 45.18514.4027

July 31, 2015

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION .......................................................................................1
2.0 EXECUTIVE SUMMARY .....................................................................................2 
3.0 SITE DESCRIPTION .............................................................................................3 
3.1 Site Characterization ................................................................................3 
3.2 Site Background .......................................................................................3 
4.0 RISK CHARACTERIZATION .............................................................................4 
5.0 RECEPTOR INFORMATION..............................................................................4 
5.1 Water Supply Wells .................................................................................4 
5.2 Public Water Supplies ..............................................................................5 
5.3 Surface Water ...........................................................................................5 
5.4 Wellhead Protection Areas ......................................................................5 
5.5 Deep Aquifers in the Coastal Plain ..........................................................5 
5.6 Subsurface Structures...............................................................................6 
5.7 Land Use ..................................................................................................6 
5.8 Property Owners and Occupants ..............................................................6 
6.0 SITE CHARACTERISTICS...................................................................................6 
6.1 Regional Geology ....................................................................................6 
6.2  Site Geology.............................................................................................6 
6.3 Regional Hydrogeology ...........................................................................7 
6.4 Site Hydrogeology ...................................................................................7 
7.0 SOIL INVESTIGATION ........................................................................................8 
8.0 GROUNDWATER CHARACTERIZATION.......................................................9 
8.1 Groundwater Quality ...............................................................................9 
8.2 Water Supply Well Sampling ..................................................................10 
9.0 CONCLUSIONS AND RECOMMENDATIONS .................................................11 

TABLES
Table 1 UST Owner/Operator Information
Table 2 Water Supply Well Information
Table 3 Adjacent Property Owner Information
Table 4 Monitoring Well Construction Information
Table 5 Groundwater Elevation Data
Table 6 Soil Analytical Results
Table 7 Groundwater Analytical Results
Table 8 Water Supply Well Analytical Results

FIGURES
Figure 1 Site Topographic Map
Figure 2 Site Map
Figure 3 Potential Receptor Map
Figure 4 Soil Sampling Locations

APPENDICES
Appendix A Current Site Photographs
Appendix B Limited Site Assessment Risk Classification and Land Use Form
Appendix C Water Supply Well Information Forms
Appendix D Soil Boring Logs and Well Construction Record
Appendix E Field Notes and Access Agreements
Appendix F Laboratory Analytical Results

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Sheltontown Grocery (Incident #14744) ATC Project No. 45.18514.4027
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2.0 EXECUTIVE SUMMARY

ATC Associates of North Carolina, P.C. (ATC) has completed a Phase I Limited Site Assessment
(LSA) for the Sheltontown Grocery site. This report documents soil sampling, monitoring well
installation activities, groundwater sampling, and a receptor survey performed between July 2014
and August 2014. The LSA was performed based on a June 24, 2014 Task Authorization (TA-1) by
the Trust Fund Branch of the Underground Storage Tank (UST) Section, Division of Waste
Management, North Carolina Department of Environment and Natural Resources (NCDENR). The
work is being performed as part of the State Lead Contract #N14004i between NCDENR and ATC.

The former Sheltontown Grocery is located at 3170 Westfield Road in Mt. Airy, Surry County,
North Carolina. The site is developed with one single-story building that is currently used as a
convenience store and retail petroleum facility. Twenty-four water supply wells (SW-1 through
SW-24) are also located within 1,000 feet of the site. One potable water supply well is located on-
site. Municipal water is not available to the site and vicinity.

On July 10, 2014, ATC personnel mobilized to the site to collect soil samples from the source area
and to install monitoring well MW-1. On August 14, 2014, a groundwater sample was collected
from MW-1. Water supply well samples SW-1, SW-3, SW-16, SW-17, and SW-22 were also
collected.

Based on topography at the site, it appears groundwater flow is to the southwest toward the
nearest surface water body. Soil, groundwater, and water supply well analytical results do not
indicate petroleum concentrations above laboratory detection limits. Based on the results of this
LSA, the site is a candidate for site closure.
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3.0 SITE DESCRIPTION

3.1 Site Characterization

The site covers an approximate 0.851-acre parcel of land and is currently developed with Jacks
Grocery which is a convenience store and retail gasoline facility. It should be noted the property
address was 3120 Westfield Road at the time of the incident release; however, the site address is
currently 3170 Westfield Road. The former UST system associated with Incident #14744 consisted
of two 4,000-gallon gasoline USTs and one 2,000-gallon gasoline UST. The UST system was
installed in May 1976 and was removed from the site in June 1994. Currently, on-site is a
compartmentalized UST with a 4,000-gallon compartment and a 6,000-gallon compartment, both
for gasoline storage. Former and current UST system owner and operator information is included as
Table 1.

The site is bounded to the north, southeast, and west by residences and to the east and southwest by
undeveloped vacant lots. Twenty four water supply wells (SW-1 through SW-24) are located
within 1,000 feet of the site. Water supply well ownership information is included in Table 2. A
site topographic map is included as Figure 1 and a site map depicting pertinent site features is
included as Figure 2. A Potential Receptor Map showing water supply well locations is included
as Figure 3. Current site photographs are included in Appendix A.

3.2 Site Background

On June 24, 1994, the UST system associated with Incident # 14744 was removed from the site.
The system consisted of two 4,000-gallon gasoline USTs and one 2,000-gallon gasoline USTs.
Following system removal, soil samples were collected from beneath the tanks, product lines,
and dispensers. Laboratory results for the soil samples indicated total petroleum hydrocarbon
(TPH) concentrations ranging from 472 milligrams per kilogram (mg/kg) to 26,161 mg/kg
beneath the USTs and TPH concentrations ranging 15,900 mg/kg to 20,154 mg/kg beneath the
product lines and dispensers. A Site Investigation Report for Permanent Closure of UST & Site
Check Report documenting the UST closure was submitted to NCDENR in July 1994. It should
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be noted ATC did not have access to this report and acquired this information from the site
background section in the Receptor Survey and Water Supply Well Sampling Report submitted
on October 30, 2006.

Based on the October 2006 receptor survey, 24 water supply wells were identified within 1,000
feet of the site. Samples were collected from seven water supply wells (SW-1, SW-2, SW-3,
SW-4, SW-5, SW-16, and SW-19). Based on laboratory results, SW-3 indicated petroleum
compounds above laboratory detection limits but below 2L Standards. Water supply well SW-4
indicated benzene, methyl tert-butyl ether (MTBE) and naphthalene above 2L Standards. It
should be noted the sample was collected from the influent portion of the point-of-entry system
for SW-4. Water supply well SW-4 formerly supplied water to the residence at 3156 Westfield
Road; however, based on an interview with Ms. Sheila Cox, the property owner of 3156
Westfield Road, water supply well SW-1 became the source of water for the residence in August
2009.

4.0 RISK CHARACTERIZATION

In accordance with 15A NCAC 2L .0115, a completed Limited Site Assessment Risk
Classification and Land Use Form provided by the NCDENR is included in Appendix B.
Answers and explanations included on the form are based on information obtained by ATC
during the LSA activities. Based on information collected during this LSA, the site appears to
meet the criteria for “high” risk classification.

5.0 RECEPTOR INFORMATION

5.1 Water Supply Wells

ATC performed a survey to identify water supply wells within 1,000 feet of the site on July 10,
2014. The survey was performed by visually observing for the presence of water supply wells
and when possible, contacting area residents to confirm water usage. A water supply well
questionnaire form was distributed to properties within 500 feet of the site. Based on the
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returned water supply well information forms and the visual reconnaissance, there are twenty-
four water supply wells within 1,000 feet of the site, twenty-two which are used for drinking, one
which is inactive, and one with an unknown use. The nearest active water supply well is located
on-site approximately 35 feet southeast of the source area. Water supply well information is
included in Table 2. A Potential Receptor Map is included as Figure 3. The returned Water
Supply Well Information forms are included in Appendix C.

5.2 Public Water Supplies
ATC contacted the City of Mt. Airy Utility Department and spoke with property owners in the area
to identify public water sources in the area. Municipal water is not provided to the site or
surrounding properties.

5.3 Surface Water
ATC reviewed a USGS Quadrangle Topographic Map to identify surface water bodies in the site
vicinity. In addition, ATC conducted a visual reconnaissance for surface water bodies in the
area. Based on this evaluation, the nearest surface water body is an unnamed tributary of Seed
Cane Creek located approximately 330 feet southwest of the site. The surface water body is
shown on Figure 1. This unnamed tributary does not have a classification per the NCDENR
Division of Water Quality; however, Seed Cane Creek is classified as a Class C surface water body.
Therefore, ATC conservatively assumes the unnamed tributary would share the Class C
classification.

5.4 Wellhead Protection Areas
According the NCDENR Division of Water Resources Wellhead Protection Program, there are
no wellhead protection areas in Surry County.

5.5 Deep Aquifers in the Coastal Plain
The Sheltontown Grocery site is located in the Piedmont Physiographic Region; therefore this
section is not applicable.

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5.6 Subsurface Structures
Subsurface lines at the site include water (from on-site well) and lines related to a septic system.
Municipal water and sewer lines do not exist in the vicinity. There are also overhead power and
communication lines at the site. According to Surry County Geographical Information Systems
(GIS), structures at the site and on adjacent properties do not appear to extend beneath the
subsurface (i.e. basements).

5.7 Land Use
According to the Surry County Zoning Department, the site is zoned Rural Business and
surrounding properties are zoned Residential General. The nearest residence is located
approximately 165 feet west of the site.

5.8 Property Owners and Occupants
Residences are located to the north, southeast, and west of the site. Undeveloped and vacant lots are
located to the east and southwest of the site. Adjacent property ownership information is
summarized on Table 3. A map depicting adjacent property occupants is included as Figure 3.

6.0 SITE CHARACTERISTICS

6.1 Regional Geology
According to the Geologic Map of North Carolina (1985) produced by Philip Brown, et al, the
referenced site is located within the Piedmont Physiographic Region of North Carolina. More
specifically, the site is underlain by banded gneiss which is interlayered with calc-silicate rock,
metaconglomerate, amphibolite, sillimanite-mica schist, and granitic rock.

6.2 Site Geology
According to the Soil Survey of Surry County, North Carolina, prepared by the United States
Department of Agriculture Soil Conservation Service, the site lies within the Braddock fine
sandy loam complex and the Woolwine-Fairview-Westfield complex. The Braddox complex is
characterized by 8 to 15 percent slopes, is well drained, has a moderately high to high capacity to
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transmit water, and originates from old colluvium and/or old alluvium derived from igneous
rocks. The Woolwine-Fairview-Westfield complex is characterized by 15 to 25 percent slopes,
is also well drained, has a low to very low capacity to transmit water, and originates from
saprolite derived from schist and/or gneiss.

As part of the Phase I LSA drilling activities, soils were continuously classified using hand auger
cuttings and drilling cuttings. The lithology of the soil samples was described in accordance
with the Unified Soil Classification System. Soils encountered during drilling activities
consisted primarily of brown, orange, and tan silty clay from the ground surface to bedrock, with
was encountered approximately 12 feet below ground surface (bgs). Boring logs are included as
Appendix D. Field notes collected during assessment activities, including drilling, are included
as Appendix E.

6.3 Regional Hydrogeology

The occurrence and movement of groundwater in the Piedmont is within two separate but
interconnected water-bearing zones. A shallow water-bearing zone occurs within the surficial
soils and a deeper zone occurs within the underlying bedrock. Groundwater in the shallow soil
zone occurs in the interstitial pore spaces between the grains comprising the surficial
soils. Groundwater in this zone is typically unconfined. Groundwater movement is generally
lateral from recharge areas to small streams that serve as localized discharge points. The
occurrence and movement of groundwater in the underlying water-bearing zone within the
crystalline bedrock is controlled by secondary joints, fractures and faults within the bedrock. On
a regional scale, the direction of groundwater flow is typically from uplands to major streams
and groundwater sinks.

6.4 Site Hydrogeology

As part of Phase I LSA activities, monitoring well MW-1 was installed on July 10, 2014, to a
depth of 40 feet bgs. Depth to groundwater in the monitoring well was measured at 8.23 feet bgs
on August 14, 2014. It should be noted what although depth to groundwater was measured at a
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depth shallower than bedrock, ATC assumes groundwater originated from the bedrock. Depth to
water was measured using an oil water interface probe. Based on topography, it appears
groundwater flow is to the southwest, towards the unnamed tributary of Sand Cane Creek. A
well construction record is included in Appendix D. Monitoring well construction information is
included as Table 4 and groundwater elevation data is included as Table 5.

7.0 SOIL INVESTIGATION

On July 10, 2014, ATC supervised the advancement of soil boring SS as part of LSA activities.
ATC based the location of the soil boring on an interview with the store personnel which
indicated the location of the former UST system. It should be noted that overhead power lines at
the site caused ATC to place the soil boring and monitoring well to the east of the former UST
system (potentially upgradient) as opposed to the west of the system (potentially downgradient).
Prior to drilling activities, ATC Program Manager Mr. Jeff Corson contacted Ms. Linda Blalock
to confirm she approved of the drilling location.

During drilling, groundwater appeared to be encountered at a depth of approximately 40 feet bgs
and bedrock was encountered at 12 feet bgs. Therefore, soil samples were collected in the
unsaturated zone at a depth of 0-5 feet bgs, 5-10 feet bgs, and 10-12 feet bgs. The samples were
placed in laboratory supplied sample containers and shipped in an ice filled cooler under chain of
custody to Contest Analytical Laboratory (Contest) in East Longmeadow, Massachusetts.
Samples from the 0-5 feet and 10-12 feet interval were analyzed for volatile organic compounds
(VOCs) by Environmental Protection Agency (EPA) Method 8260B and volatile petroleum
hydrocarbons (VPH) by the Massachusetts Department of Environmental Protection (MADEP)
method. The sample collected from the 5-10 feet interval was analyzed for MADEP VPH.

The results of the soil analyses indicated acetone and methylene chloride above laboratory
detection limit but below Soil-to-Groundwater Maximum Soil Contaminant Concentrations
(MSCCs). Acetone and methylene chloride are typically considered to be laboratory
contaminants and most likely did not originate from the site. Historically at the site, the
maximum detection of TPH-GRO was 26,161 mg/kg from a sample collected from the beneath
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the former USTs. Soil analytical results are summarized in Table 6. Laboratory analytical
reports are included in Appendix F. Historical soil sample locations are shown of Figure 4.

As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of
the laboratory report was conducted. During the review, it was concluded that samples were
received by the laboratory in acceptable condition and properly preserved. The samples were
analyzed within the correct holding times, and the chain of custody was properly completed by
all parties. The laboratory QC report shows an internal blank was analyzed for each method that
was used for the original samples. The laboratory fortified blank (LFB) and laboratory control
sample (LCS) data results were also provided for each analytical method. Refer to the laboratory
reports in Appendix F for details regarding QA results for the laboratory samples and any noted
exceptions. ATC concludes that the laboratory results are usable and any exceptions do not
significantly impact the conclusions presented in this report.

8.0 GROUNDWATER CHARACTERIZATION

8.1 Groundwater Quality

Initially, ATC intended to install MW-1 in the soil boring location SS; however, due to the close
proximity of the boring to on-site water supply well SW-1, ATC moved the location of MW-1 in
order to reduce the chance of damaging SW-1 with the force of the air drilling rig. The
monitoring well was installed by North Carolina certified well driller Carolina Soil
Investigations and is located northeast of the former UST pit.

On August 14, 2014, a groundwater sample was collected from monitoring well MW-1, packed in
ice and delivered under chain-of-custody protocol to Contest for analyses. The groundwater
sample was analyzed for VOCs by EPA Method 6200B, MADEP VPH, and lead by method
6020A.

The laboratory analytical results indicated the presence of lead above 2L Standards. No other
compounds were detected above laboratory detection limit. Because no other petroleum
compounds were detected in the groundwater sample, ATC believes the lead detected is naturally
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occurring. Groundwater analytical data is summarized in Table 7. The laboratory analytical
report and chain-of-custody forms are included in Appendix F. The QA/QC measures and
conditions applicable to the soil sampling also applies to the groundwater sampling.

8.2 Water Supply Well Sampling

Twenty-four water supply wells (SW-1 through SW-24) are located within 1,000 feet of the site,
twenty-two of which are used for drinking purposes (SW-1 through SW-3, SW-5 through SW-
10, and SW-12 through SW-24), one of which is inactive (SW-4), and one of which the use is
unknown (SW-11B). Historically at the site, the former water supply well influent sample SW-4
contained benzene at 177 micrograms/liter (µg/L), MTBE 527 µg/L, and naphthalene at 23.8
µg/L. It should be noted this well formerly supplied water to 3156 Westfield Road; however,
based on and interview with Ms. Sheila Cox, property owner of 3156 Westfield Road, SW-1 has
been supplying this property water since August 2009.

As part of receptor survey activities, ATC sent water supply well information forms to all
properties whose boundaries were located within 500 feet of the source area. In addition, ATC
sent water supply well access forms to these properties. A total of 17 access agreements were
sent to property owners. Of the 17 agreements, ATC received responses from three property
owners. Owners of water supply wells SW-1 and SW-3 (same property owner), SW-16, and
SW-17 granted access for well sampling. During sampling activities, ATC was able to acquire a
verbal agreement from the property owner of SW-22. Water supply well access agreements are
included in Appendix E.

ATC sampled water supply wells SW-1, SW-3, SW-16, SW-17, and SW-22 on August 14, 2014.
Samples were collected in laboratory-approved containers, packed in ice and delivered under
chain-of-custody protocol to Contest to analyze for VOCs by EPA Method 6200B. Laboratory
results for did not indicate any compound concentrations above laboratory detection limit. Water
supply well analytical results are included in Table 8. Laboratory results are included in
Appendix F. The QA/QC measures and conditions applicable to the soil sampling also applies
to the water supply well sampling.
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9.0 CONCLUSIONS AND RECOMMENDATIONS

On behalf of the Trust Fund Branch of the UST Section, ATC has completed a Phase I LSA
documenting assessment activities performed in July 2014 and August 2014 for the Sheltontown
Grocery site located at 3170 Westfield Road (formerly 3120 Westfield Road) in Mt. Airy, Surry
County, North Carolina. Results from LSA did not indicate VOC impact to soil, groundwater,
water supply well samples collected. In addition, ATC performed a receptor survey and
identified twenty-four water supply wells within 1,000 feet of the site, twenty-two of which are
used for drinking purposes, one which is inactive, and one of which the use is unknown. The site
meets the criteria for “high” risk classification.

Soil analytical results indicated acetone and methylene chloride at concentrations above
laboratory detection limits but below Soil-to-Groundwater MSCCs. Acetone and methylene
chloride are typically considered to be laboratory contaminants and most likely do not originate
from the site. Groundwater analytical results do not indicate concentrations exceeding
laboratory analytical results with the exception of lead, which was detected above 2L Standard.
Because no other compounds were detected in the groundwater sample, ATC assumes the lead is
naturally occurring. Finally, water supply well analytical results did not indicate compound
concentrations exceeding laboratory detection limits. Based on the results of this LSA, the site is
a candidate for site closure.

TABLES
TABLE 1
UST OWNER/OPERATOR INFORMATION
SHELTONTOWN GROCERY
3170 WESTFIELD ROAD
MT. AIRY, SURRY COUNTY, NORTH CAROLINA
INCIDENT #14744
ATC PROJECT No. 45.18514.4027
UST ID
Number Product Capacity
(gallons)
Date
Installed
Date taken out of
Use
Date
Permanently
Closed
Was Release
Associated With UST
System?
1 Gasoline 4,000 5/8/1976 Unknown 6/24/1994 Unknown
2 Gasoline 2,000 5/8/1976 Unknown 6/24/1994 Unknown
3 Gasoline 4,000 5/8/1976 Unknown 6/24/1994 Unknown
Facility ID No.Owner or Operator?
0-008824 Owner
UST ID
Number Product Capacity
(gallons)
Date
Installed
Date taken out of
Use
Date
Permanently
Closed
Was Release
Associated With UST
System?
Gasoline 4,000
Gasoline 6,000
Facility ID No.Owner or Operator?
0-034690 Owner
Facility ID No.Owner or Operator?
0-034690 Owner
Facility ID No.Owner or Operator?
0-034690 Owner
3170 Westifeld Road, Mt. Airy, NC 27030 336-786-6164
Former USTs
Current USTs
4
(Compartment)6/22/1995 Not Applicable/ In
Use
Not Applicable/
In Use Unknown
Name of Owner or Operator Dates of Ownership / Operation
Jack Jr. and Sheila Cox 2005 - Present
Address Telephone Number
Dates of Ownership / Operation
Unknown
Name of Owner or Operator
Mitch Kirkman
Unknown Unknown
Address Telephone Number
Name of Owner or Operator Dates of Ownership / Operation
Brian Willis Unknown
Unknown Unknown
Address Telephone Number
Unknown Unknown
Name of Owner or Operator Dates of Ownership / Operation
Mitch Kirkman 1995 to Unknown
Address Telephone Number
TABLE 2
WATER SUPPLY WELL INFORMATION
SHELTONTOWN GROCERY
3170 WESTFIELD ROAD
MT. AIRY, SURRY COUNTY, NORTH CAROLINA
INCIDENT #14744
ATC PROJECT No. 45.18514.4027
Well # Well Owner Property Address Well Use
Well Depth
(feet)
Distancefrom
Source Area
(feet)
Connected to
Municipal
Water
Upgradient or
Downgradient
3170 Westfield Road
3156 Westfield Road
140 Snowflake Way
135 Snowflake Way
3169 Westfield Road
109 Mythology Lane
SW-4
Jack Jr. and Sheila Cox
5536 Westfield Road
Westfield, NC 27053
336-786-6164
3156 Westfield Road Inactive Unknown 180 No Downgradient
SW-5
Virginia Hiatt c/o Donna Brinegar
296 Wendex Drive
Mt. Airy, NC 27030
Phone number not available
223 Wendex Drive Drinking
35
(per historical
reports)
525 No Downgradient
SW-6
R.J. and Betty Hiatt
117 Poteat Road
Mt. Airy, NC 27030
336-786-4666
117 Poteat Road Drinking Unknown 520 No Downgradient
SW-7
Steven and Michelle Kirkman
362 Poteat Road
Mt. Airy, NC 27030
336-789-5692
159 Poteat Road Drinking Unknown 905 No Downgradient
SW-8
Todd Jessup
138 Poteat Road
Mt. Airy, NC 27030
336-789-3742
138 Poteat Road Drinking Unknown 830 No Downgradient
SW-9
Wilbur and Freda Hawks Estate
143 Poteat Road
Mt. Airy, NC 27030
Phone number not available
143 Poteat Road Drinking Unknown 750 No Downgradient
SW-10
Ruth Taylor
124 Poteat Road
Mt. Airy, NC 27030
336-789-5953
124 Poteat Road Drinking
20-24
(per historical
reports)
760 No Downgradient
Unknown 1030
Unknown 980
SW-12
Claybern Jr. and Peggy Taylor
3096 Westfield Road
Mt. Airy, NC 27030
336-786-2831
3096 Westfield Road Drinking Unknown 760 No Downgradient
SW-13
Bryan Taylor
126 Kirkwood Trail
Mt. Airy, NC 27030
336-786-9299
3114 Westfield Road Drinking Unknown 675 No Downgradient
Downgradient
No
SW-11
(A and B)
Claybern Jr. and Peggy Taylor
3096 Westfield Road
Mt. Airy, NC 27030
336-786-2831
112 Fresno Way
Unknown
(assumed one used
for drinking and
one for irrigation
or inactive)
No
No Crossgradient
SW-1 Drinking
SW-3
Donald and Bonnie Shelton
3161 Westfield Road
Mt. Airy, NC 27030
336-489-4629
Drinking 100 170 Crossgradient
Jack Jr. and Sheila Cox
5536 Westfield Road
Westfield, NC 27053
336-786-6164
Unknown No35 Crossgradient
SW-2
Ronald and Kimberly Hudson
135 Snowflake Way
Mt. Airy, NC 27030
Phone number not available
Drinking Unknown 375
Page 1 of 2
TABLE 2
WATER SUPPLY WELL INFORMATION
SHELTONTOWN GROCERY
3170 WESTFIELD ROAD
MT. AIRY, SURRY COUNTY, NORTH CAROLINA
INCIDENT #14744
ATC PROJECT No. 45.18514.4027
Well # Well Owner Property Address Well Use
Well Depth
(feet)
Distancefrom
Source Area
(feet)
Connected to
Municipal
Water
Upgradient or
Downgradient
SW-14
Joe Haymore
3083 Westfield Road
Mt. Airy, NC 27030
336-786-8764
3083 Westfield Road Drinking Unknown 930 No Downgradient
SW-15
Bryan Taylor
3091 Westfield Road
Mt. Airy, NC 27030
Phone number not available
3091 Westfield Road Drinking Unknown 790 No Downgradient
SW-16
Donald Shelton
3161 Westfield Road
Mt. Airy, NC 27030
336-489-4629
3161 Westfield Road Drinking 40 490 No Crossgradient
SW-17
Clindon Cook
121 Mythology Lane
Mt. Airy, NC 27030
336-648-1788
121 Mythology Lane Drinking 38 380 No Upgradient
SW-18
Wesley Kirkman
3201 Westfield Road
Mt. Airy, NC 27030
Phone number not available
3201 Westfield Road Drinking Unknown 370 No Upgradient
SW-19
Ronnie and Sharon Chamblin
2274 Old Winston Road
Pinnacle, NC 27043
Phone number not available
3196 Westfield Road Drinking Unknown 370 No Upgradient
SW-20
Lily's Lands, LLC
1060 S. Main Street
Mt. Airy, NC 27030
Phone number not available
139 Blue Hollow Road Drinking Unknown 780 No Upgradient
SW-21
Jimmy Love Life Estate
3283 Westfield Road
Mt. Airy, NC 27030
Phone number not available
116 Elgin Lane Drinking Unknown 820 No Upgradient
SW-22
Cleon and Linda Gammons
315 Norman Road
Mt. Airy, NC 27030
336-786-1693 / 336-755-5364
3250 Westfield Road Drinking Unknown 715 No Upgradient
SW-23
Treva and Gretchen Kirkman
125 Blue Hollow Road
Mt. Airy, NC 27030
336-789-2214
107 Blue Hollow Road Drinking Unknown 560 No Upgradient
SW-24
Gary and Marian O'Neal
608 Braewyck Lane
Winston-Salem, NC 27104
336-760-6936
3129 Westfield Road Drinking Unknown 510 No Downgradient
Page 2 of 2
TABLE 3
ADJACENT PROPERTY OWNER INFORMATION
SHELTONTOWN GROCERY
3170 WESTFIELD ROAD
MT. AIRY, SURRY COUNTY, NORTH CAROLINA
INCIDENT #14744
ATC PROJECT No. 45.18514.4027
Property Address Property Owner
PIN Number
Parcel Use
Zoning
Site: Jack Jr. and Sheila Cox 504004628221
3170 Westfield Road 5536 Westfield Road Jack's Grocery - Convenience store and gas station
Mt. Airy, NC 27030 Westfield, NC 27053 Rural Business (RB)
North: Donald Shelton 504004627415
3169 Westfield Road 3161 Westfield Road Residence
Mt. Airy, NC 27030 Mt. Airy, NC 27030 Residential General (RG)
Northeast: Aliceia Fallin and Michael Hedrick 504000627424
109 Mythology Lane 674 Bryants Place Court Residence
Mt. Airy, NC 27030 Pinnacle, NC 27043 Residential General (RG)
East: Ronald Hudson and Kimerly Kirkman 504000627119
3270 Westfield Road 135 Snowflake Way Vacant Lot
Mt. Airy, NC 27030 Mt. Airy, NC 27030 Residential General (RG)
Southeast: Ronald Hudson and Kimerly Kirkman 504000628121
140 Snowflake Way 135 Snowflake Way Residence
Mt. Airy, NC 27030 Mt. Airy, NC 27030 Residential General (RG)
Southwest: Johnny and Franklie Cox 504000618661
Snowflake Way 291 Moss Hollow Lane Undeveloped Lot
Mt. Airy, NC 27030 Mt. Airy, NC 27030 Residential General (RG)
West: Jack Jr. and Sheila Cox 504000625069
3156 Westfield Road 5536 Westfield Road Residence
Mt. Airy, NC 27030 Westfield, NC 27053 Residential General (RG)
TABLE 4
MONITORING WELL CONSTRUCTION INFORMATION
SHELTONTOWN GROCERY
3170 WESTFIELD ROAD
MT. AIRY, SURRY COUNTY, NORTH CAROLINA
INCIDENT #14744
ATC PROJECT No. 45.18514.4027
Well ID Date Installed
Well
Diameter
(inches)
Screen Slot
Size (inches)
Screened
Interval
(feet)
Total
Depth
(feet)
Status
MW-1 7/10/2014 2 0.01 20-40 40 Active
TABLE 5
GROUNDWATER ELEVATION DATA
SHELTONTOWN GROCERY
3170 WESTFIELD ROAD
MT. AIRY, SURRY COUNTY, NORTH CAROLINA
INCIDENT #14744
ATC PROJECT No. 45.18514.4027
WELL I.D. Date
TOC Elevation
(ft)
Depth to
Product (ft)
Depth to
Groundwater (ft)
Product Thickness
(ft)
Groundwater
Elevations (ft)
MW-1 8/14/2014 NS -- 8.23 -- NM
Notes:
1. TOC = Top of well casing.
2. NS = Not Surveyed.
2. NM = Not Measured.
TABLE 6SOIL ANALYTICAL RESULTSSHELTONTOWN GROCERY3170 WESTFIELD ROADMT. AIRY, SURRY COUNTY, NORTH CAROLINAINCIDENT #14744ATC PROJECT No. 45.18514.40275030Boring I.D. Depth (feet) Sampling Date TPH-GROBenzeneTolueneEthylbenzeneTotal XylenesMTBEAcetoneMethylene ChlorideC5-C8 AliphaticsC9-C18 Aliphatics*C9-C22 Aromatics**Former USTs1Unknown 7/6/1994471 - 26,161NA NA NA NA NA NA NA NA NA NAFormer Product Lines and Pump Islands1Unknown 7/6/199415,900 - 20,154NA NA NA NA NA NA NA NA NA NASS-1 0-5 7/10/2014 NA <0.00085 <0.00097 <0.00097 <0.0021 <0.0011 0.034J 0.0097J <16 <16 <16SS-2 5-10 7/10/2014 NA NA NA NA NA NA NA NA <16 <16 <16SS-3 10-15 7/10/2014 NA <0.00082 <0.00093 <0.00093 <0.0023 <0.001 0.053J 0.0089J <14 <14 <1410 NE NE NE NE NE NE NE NE NE NENE 0.0056 4.3 4.9 4.6 0.091 24 0.02 68 540 31NE 18 1,200 1,560 3,129 350 14,000 85 939 1,500 469NE 164 32,000 40,000 81,760 3,100 360,000 763 24,528 40,000 12,264Notes:2. Concentrations reported in milligrams per kilogram (mg/kg).3. * Final C9-C18 aliphatics values are equal to C9-C12 aliphatics reported in the laboratory report4. ** Final C9-C22 Aromatics are equal to C9-C10 aromatics reported in the laboratory analytical report5. The MADEP VPH values were obtained from Table 10 in the "Guidelines for Assessment and corrective Action for UST Releases, dated July 15, 2008, updated April 2013.6. NA = Not Analyzed.7. MSCCs = Maximum Soil Contaminant Concentration8. Bold concentrations equal or exceed the lowest applicable MSCCs or Cleanup Levels.8. "<" = concentration less than laboratory detection limit (or reporting limit when detection limit is not reported)1. A range of concentrations detected for the specified portions of the UST system were reported in the Receptor Survey & Supply Well Sampling Report dated October 31, 2006, which referenced the 20-Day Report submitted in July 1994. However, ATC did not have access to the 20-Day Report and therefore could not discern specific concentrations for each location.MADEP VPHEPA Method:Soil-to-Groundwater MSCCsResidential Soil Cleanup LevelsIndustrial/Commercial Soil Cleanup LevelsNCDENR Action Level8260B
TABLE 7GROUNDWATER ANALYTICAL RESULTSSHELTONTOWN GROCERY3170 WESTFIELD ROADMT. AIRY, SURRY COUNTY, NORTH CAROLINAINCIDENT #14744ATC PROJECT No. 45.18514.40276020AMW-18/14/2014 <0.079 <0.09 <0.092 <0.18 <0.09 <0.18 <0.12110<100 <100 <1001 600 600 500 20 70 6 15 400 700 2005,000 260,000 84,500 85,500 20,000 70,000 6,000 15,000 NE NE NENotes:1. "<" or ND = None detected above method detection limit.2. 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard 3. GCL = Gross Contaminant Level established by NCDENR.4. NE = Not established.5. MTBE = Methyl tertiary butyl ether6. Values in BOLD indicate levels above 2L Groundwater Standards.7. All concentrations in micrograms per liter (ug/L).8. * Final C9-C18 aliphatics values are equal to C9-C12 aliphatics reported in the laboratory report9. ** Final C9-C22 Aromatics are equal to C9-C10 aromatics reported in the laboratory analytical report10. The MADEP VPH values were obtained from Table 10 in the "Guidelines for Assessment and corrective Action for UST Releases, dated July 15, 2008, updated April 2013.EPA METHOD 6200BAnalytical Methods:C9-C22 Aromatics**MTBEIsopropyl etherMADEP VPHWELL I.D.DATE SAMPLEDBenzeneC9-C18 Aliphatics*C5-C8 AliphaticsEthylbenzeneTolueneTotal Xylenes2L GW StandardGCLLeadNaphthalene
TABLE 8
WATER SUPPLY WELL ANALYTICAL RESULTS
SHELTONTOWN GROCERY
3170 WESTFIELD ROAD
MT. AIRY, SURRY COUNTY, NORTH CAROLINA
INCIDENT #14744
ATC PROJECT No. 45.18514.4027
9/20/2006 <0.5 <0.5 <0.5 <0.1 ND <0.5 <0.5 <0.5 <0.5
8/14/2014 <0.079 <0.09 <0.092 <0.18 ND <0.09 <0.18 <0.12 <0.18
SW-2 9/20/2006 <0.5 <0.5 <0.5 <1 ND <0.5 <0.5 <0.5 <0.5
9/20/2006 <0.5 <0.5 <0.5 <1 ND <0.5 <0.5 4.57 0.64
8/14/2014 <0.079 <0.09 <0.092 <0.18 ND <0.09 <0.18 <0.12 <0.18
SW-4 9/20/2006 177 <10 <10 <10 177 527 26.2 23.8 <10
SW-5 9/20/2006 <0.5 <0.5 <0.5 <1 ND <0.5 <0.5 <0.5 <0.5
9/20/2006 <0.5 <0.5 <0.5 <1 ND <0.5 <0.5 <0.5 <0.5
8/14/2014 <0.079 <0.09 <0.092 <0.18 ND <0.09 <0.18 <0.12 <0.18
SW-17 8/14/2014 <0.079 <0.09 <0.092 <0.18 ND <0.09 <0.18 <0.12 <0.18
SW-19 9/20/2006 <0.5 <0.5 <0.5 <1 ND <0.5 <0.5 <0.5 <0.5
SW-22 8/14/2014 <0.079 <0.09 <0.092 <0.18 ND <0.09 <0.18 <0.12 <0.18
1 600 600 500 NE 20 70 6 400
5,000 260,000 84,500 85,500 NE 20,000 70,000 6,000 28,500
Notes:
1. "<" or ND = None detected above method detection limit or reporting limit
2. NC 2L GW Standard = Title 15A NCAC 2L .0202 Groundwater Standard
3. GCL = Gross Contaminant Level established by NCDENR.
4. NE = Not established.
5. MTBE = Methyl tertiary butyl ether
6. All concentrations in micrograms per liter (ug/L).1,2,4-TrimethylbenzeneAnalytical Methods: EPA METHOD 6200B
WELL I.D.DATE
SAMPLED
BenzeneTolueneEthylbenzeneTotal XylenesTotal BTEX2L GW Standard
GCL MTBEIsopropyl etherNaphthaleneSW-1
SW-3
SW-16

FIGURES
.

2725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
[phone]
FIGURE 1
SITE TOPOGRAPHIC MAP
PROJECT NO: 45.18514.4027
REVIEWED BY: JC SCALE: 1” = 785’DATE: 9/4/14
SHELTONTOWN GROCERY– INCIDENT #14744
3170 WESTFIELD ROAD
MT. AIRY, NORTH CAROLINA
N
Site
Source: My Topo Maps
2725 E. Millbrook Road, Suite 121
Raleigh, NC 27604
[phone]
FIGURE 3
POTENTIAL RECEPTOR MAP
PROJECT NO: 45.18514.4027
REVIEWED BY: JC SCALE: 1” = 265’DATE: 9/4/14
SHELTONTOWN GROCERY– INCIDENT #14744
3170 WESTFIELD ROAD
MT. AIRY, NORTH CAROLINA
1
Potable Water Supply Well
Inactive Water Supply Well
Water Supply Well IDSource: Surry County NC GIS
Site
1,000 Foot Radius
500 Foot Radius
N
1
3
2
24
5
6
7
8 9
10
11B*
11A*
12
14 15
16 17 18
19
20
21
22
23
* = Note that ATC assumes either SW-11A or SW-11B is used for drinking purposes
while the other is used for irrigation purposes or is inactive; however, to be conservative
ATC identified both as drinking water supply wells on this figure.
4
13

APPENDIX A

CURRENT SITE PHOTOGRAPHS

Photo 2: Eas

Phot
stern side of o
Current S
Shelto
3170 W
Mt. Airy
Inci
to 1: On-site
on-site buildin
Site Photog

ontown Grocer
Westfield Roa
y, North Caro
ident #14744
building (Jac
ng, former US
raphs
ry
ad
olina
ck’s Grocery)
ST location, a

)
and potable w

well SW-1

APPENDIX B

LIMITED SITE ASSESSMENT RISK CLASSIFICATIONAND LAND USE
FORM

APPENDIX C

WATER SUPPLY WELL INFORMATION FORMS

APPENDIX D

SOIL BORING LOGS AND WELL CONSTRUCTION RECORD

Client: NCDENR State Lead Program
ATC Project No. 045.18514.4027
Mt. Airy, North Carolina
3120 Westfield Road
Sheltontown Grocery - Incident #14744
Terminated boring at 40 feet below ground surface (bgs).
BORING LOG: MW-1
(Page 1 of 1)
Date(s) Drilled : 710/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : HSA and Air Rig
Boring Diameter : 6 Inches
Sampling Method : Soil Cuttings
Sampling Interval : 5 feet
Logged By : Garrett Stancil
Depth In Feet0
5
10
15
20
25
30
35
40 USCSCL
CL
ME GRAPHICDESCRIPTION
Brownish orange silty CLAY, traces of gravel
Brown, orange, and tan silty CLAY
Bedrock
End of boring
Elev.: Not Surveyed
Well: MW-1
Grout
Bentonite
Sand Pack
Cover
Casing
Screen
Client: NCDENR State Lead Program
ATC Project No. 045.18514.4027
Mt. Airy, North Carolina
3120 Westfield Road
Sheltontown Grocery - Incident #14744
Reached refusal at 12 feet below ground surface (bgs).
Soil samples collected from 0-5, 5-10 and 10-12 feet bgs.
BORING LOG: SS
(Page 1 of 1)
Date(s) Drilled : 7/10/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : HSA Rig
Boring Diameter : 6 Inches
Sampling Method : Soil Cuttings
Sampling Interval : 5 feet
Logged By : Garrett Stancil
Depth In Feet0
1
2
3
4
5
6
7
8
9
10
11
12 USCSCL
CL GRAPHICDESCRIPTION
Brownish orange silty CLAY, traces of gravel
Brown, orange, and tan silty CLAY
Boring terminated

APPENDIX E

FIELD NOTES AND ACCESS AGREEMENTS

APPENDIX F

LABORATORY ANALYTICAL RESULTS

Page 1 of 30 14G0626_1 Contest_Final 07 21 14 1811
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
14G0626-01 5
14G0626-02 9
14G0626-03 11
Sample Preparation Information 15
QC Data 16
Volatile Organic Compounds by GC/MS 16
B100440 16
Petroleum Hydrocarbons Analyses - VPH 21
B100436 21
Flag/Qualifier Summary 23
Certifications 24
Chain of Custody/Sample Receipt 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
August 21, 2014
Garrett Stancil
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: Mount Airy (Sheltontown)
Client Job Number:
Project Number: 45.18514.4027
Laboratory Work Order Number: 14H0700
Enclosed are results of analyses for samples received by the laboratory on August 14, 2014. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 34
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
14H0700-01 5
14H0700-02 9
14H0700-03 11
14H0700-04 13
14H0700-05 15
14H0700-06 17
Sample Preparation Information 19
QC Data 20
Volatile Organic Compounds by GC/MS 20
B102986 20
Petroleum Hydrocarbons Analyses - VPH 24
B102978 24
Metals Analyses (Total) 26
B102832 26
Flag/Qualifier Summary 27
Certifications 28
Chain of Custody/Sample Receipt 31
Page 2 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
8/21/2014
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Garrett Stancil
45.18514.4027
14H0700
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Mount Airy (Sheltontown)
MW-1 14H0700-01 Water MADEP-VPH-04-1.1
SM18-20 6200B
SW-846 6020A
SW-1 14H0700-02 Water SM18-20 6200B
SW-17 14H0700-03 Water SM18-20 6200B
SW-16 14H0700-04 Water SM18-20 6200B
SW-3 14H0700-05 Water SM18-20 6200B
SW-22 14H0700-06 Water SM18-20 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 34
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
MADEP-VPH-04-1.1
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
2,2,4-Trimethylpentane
B102978-BS1
SM18-20 6200B
Qualifications:
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Bromoform
B102986-BSD1
Ethanol
B102986-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
Bromomethane
14H0700-01[MW-1], 14H0700-02[SW-1], 14H0700-03[SW-17], 14H0700-04[SW-16], 14H0700-05[SW-3], 14H0700-06[SW-22], B102986-BLK1, B102986-BS1,
B102986-BSD1
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported
result.
Analyte & Samples(s) Qualified:
V-16
Ethanol
14H0700-01[MW-1], 14H0700-02[SW-1], 14H0700-03[SW-17], 14H0700-04[SW-16], 14H0700-05[SW-3], 14H0700-06[SW-22], B102986-BLK1, B102986-BS1,
B102986-BSD1
MADEP-VPH-04-1.1
No significant modifications were made to the method. All VPH samples were received preserved properly at pH <2 in the proper containers as specified on the chain-of-custody
form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Laboratory Manager
Page 4 of 34
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-01
Field Sample #: MW-1
Sample Matrix: Water
Sampled: 8/14/2014 12:30
[TOC_2]14H0700-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 8/20/14 11:55 EEHg/L4.7 8/19/14SM18-20 6200B1Acetone
ND 0.50 8/20/14 11:55 EEHg/L0.079 8/19/14SM18-20 6200B1Benzene
ND 0.50 8/20/14 11:55 EEHg/L0.044 8/19/14SM18-20 6200B1Bromobenzene
ND 0.50 8/20/14 11:55 EEHg/L0.22 8/19/14SM18-20 6200B1Bromochloromethane
ND 0.50 8/20/14 11:55 EEHg/L0.088 8/19/14SM18-20 6200B1Bromodichloromethane
ND 0.50 8/20/14 11:55 EEHg/L0.21 8/19/14SM18-20 6200B1Bromoform
ND 1.0 8/20/14 11:55 EEHg/L0.94 8/19/14SM18-20 6200B1R-05Bromomethane
ND 5.0 8/20/14 11:55 EEHg/L2.4 8/19/14SM18-20 6200B12-Butanone (MEK)
ND 0.50 8/20/14 11:55 EEHg/L0.054 8/19/14SM18-20 6200B1n-Butylbenzene
ND 0.50 8/20/14 11:55 EEHg/L0.084 8/19/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 8/20/14 11:55 EEHg/L0.096 8/19/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 8/20/14 11:55 EEHg/L0.10 8/19/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B1Chlorobenzene
ND 50 8/20/14 11:55 EEHg/L28 8/19/14SM18-20 6200B1V-16Ethanol
ND 0.50 8/20/14 11:55 EEHg/L0.054 8/19/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 8/20/14 11:55 EEHg/L0.16 8/19/14SM18-20 6200B1Chloroethane
ND 0.50 8/20/14 11:55 EEHg/L0.14 8/19/14SM18-20 6200B1Chloroform
ND 5.0 8/20/14 11:55 EEHg/L0.32 8/19/14SM18-20 6200B1Chloromethane
ND 0.50 8/20/14 11:55 EEHg/L0.070 8/19/14SM18-20 6200B12-Chlorotoluene
ND 0.50 8/20/14 11:55 EEHg/L0.074 8/19/14SM18-20 6200B14-Chlorotoluene
ND 0.50 8/20/14 11:55 EEHg/L0.089 8/19/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 8/20/14 11:55 EEHg/L0.076 8/19/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 8/20/14 11:55 EEHg/L0.079 8/19/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 8/20/14 11:55 EEHg/L0.046 8/19/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 8/20/14 11:55 EEHg/L0.16 8/19/14SM18-20 6200B11,1-Dichloroethane
ND 5.0 8/20/14 11:55 EEHg/L0.19 8/19/14SM18-20 6200B11,2-Dichloroethane
ND 0.50 8/20/14 11:55 EEHg/L0.21 8/19/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 8/20/14 11:55 EEHg/L0.15 8/19/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 8/20/14 11:55 EEHg/L0.15 8/19/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 8/20/14 11:55 EEHg/L0.11 8/19/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 8/20/14 11:55 EEHg/L0.099 8/19/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 8/20/14 11:55 EEHg/L0.072 8/19/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 8/20/14 11:55 EEHg/L0.13 8/19/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 8/20/14 11:55 EEHg/L0.062 8/19/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 8/20/14 11:55 EEHg/L0.056 8/19/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 8/20/14 11:55 EEHg/L0.18 8/19/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 8/20/14 11:55 EEHg/L0.092 8/19/14SM18-20 6200B1Ethylbenzene
ND 5.0 8/20/14 11:55 EEHg/L1.5 8/19/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 8/20/14 11:55 EEHg/L0.11 8/19/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 8/20/14 11:55 EEHg/L0.090 8/19/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 8/20/14 11:55 EEHg/L3.2 8/19/14SM18-20 6200B1Methylene Chloride
ND 5.0 8/20/14 11:55 EEHg/L1.5 8/19/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 5 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-01
Field Sample #: MW-1
Sample Matrix: Water
Sampled: 8/14/2014 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B1Naphthalene
ND 0.50 8/20/14 11:55 EEHg/L0.094 8/19/14SM18-20 6200B1n-Propylbenzene
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B1Styrene
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 0.50 8/20/14 11:55 EEHg/L0.080 8/19/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 8/20/14 11:55 EEHg/L0.090 8/19/14SM18-20 6200B1Toluene
ND 0.50 8/20/14 11:55 EEHg/L0.14 8/19/14SM18-20 6200B11,2,3-Trichlorobenzene
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B11,2,4-Trichlorobenzene
ND 0.50 8/20/14 11:55 EEHg/L0.094 8/19/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 8/20/14 11:55 EEHg/L0.077 8/19/14SM18-20 6200B1Trichloroethylene
ND 0.50 8/20/14 11:55 EEHg/L0.15 8/19/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 8/20/14 11:55 EEHg/L0.12 8/19/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 8/20/14 11:55 EEHg/L0.18 8/19/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 8/20/14 11:55 EEHg/L0.10 8/19/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 8/20/14 11:55 EEHg/L1.3 8/19/14SM18-20 6200B1Vinyl Acetate
ND 0.50 8/20/14 11:55 EEHg/L0.13 8/19/14SM18-20 6200B1Vinyl Chloride
ND 1.0 8/20/14 11:55 EEHg/L0.18 8/19/14SM18-20 6200B1m+p Xylene
ND 0.50 8/20/14 11:55 EEHg/L0.11 8/19/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 8/20/14 11:5570-130
Toluene-d8 96.4 8/20/14 11:5570-130
4-Bromofluorobenzene 89.9 8/20/14 11:5570-130
Page 6 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-01
Field Sample #: MW-1
Sample Matrix: Water
Sampled: 8/14/2014 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - VPH
ND 100 8/19/14 11:54 EEHg/L 8/19/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 100 8/19/14 11:54 EEHg/L 8/19/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 100 8/19/14 11:54 EEHg/L 8/19/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 100 8/19/14 11:54 EEHg/L 8/19/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 100 8/19/14 11:54 EEHg/L 8/19/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)91.5 8/19/14 11:5470-130
2,5-Dibromotoluene (PID)72.5 8/19/14 11:5470-130
Page 7 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-01
Field Sample #: MW-1
Sample Matrix: Water
Sampled: 8/14/2014 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
110 2.0 8/18/14 16:13 KSHg/L0.22 8/16/14SW-846 6020A2Lead
Page 8 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-02
Field Sample #: SW-1
Sample Matrix: Water
Sampled: 8/14/2014 13:00
[TOC_2]14H0700-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 8/20/14 9:42 EEHg/L4.7 8/19/14SM18-20 6200B1Acetone
ND 0.50 8/20/14 9:42 EEHg/L0.079 8/19/14SM18-20 6200B1Benzene
ND 0.50 8/20/14 9:42 EEHg/L0.044 8/19/14SM18-20 6200B1Bromobenzene
ND 0.50 8/20/14 9:42 EEHg/L0.22 8/19/14SM18-20 6200B1Bromochloromethane
ND 0.50 8/20/14 9:42 EEHg/L0.088 8/19/14SM18-20 6200B1Bromodichloromethane
ND 0.50 8/20/14 9:42 EEHg/L0.21 8/19/14SM18-20 6200B1Bromoform
ND 1.0 8/20/14 9:42 EEHg/L0.94 8/19/14SM18-20 6200B1R-05Bromomethane
ND 5.0 8/20/14 9:42 EEHg/L2.4 8/19/14SM18-20 6200B12-Butanone (MEK)
ND 0.50 8/20/14 9:42 EEHg/L0.054 8/19/14SM18-20 6200B1n-Butylbenzene
ND 0.50 8/20/14 9:42 EEHg/L0.084 8/19/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 8/20/14 9:42 EEHg/L0.096 8/19/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 8/20/14 9:42 EEHg/L0.10 8/19/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B1Chlorobenzene
ND 50 8/20/14 9:42 EEHg/L28 8/19/14SM18-20 6200B1V-16Ethanol
ND 0.50 8/20/14 9:42 EEHg/L0.054 8/19/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 8/20/14 9:42 EEHg/L0.16 8/19/14SM18-20 6200B1Chloroethane
ND 0.50 8/20/14 9:42 EEHg/L0.14 8/19/14SM18-20 6200B1Chloroform
ND 5.0 8/20/14 9:42 EEHg/L0.32 8/19/14SM18-20 6200B1Chloromethane
ND 0.50 8/20/14 9:42 EEHg/L0.070 8/19/14SM18-20 6200B12-Chlorotoluene
ND 0.50 8/20/14 9:42 EEHg/L0.074 8/19/14SM18-20 6200B14-Chlorotoluene
ND 0.50 8/20/14 9:42 EEHg/L0.089 8/19/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 8/20/14 9:42 EEHg/L0.076 8/19/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 8/20/14 9:42 EEHg/L0.079 8/19/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 8/20/14 9:42 EEHg/L0.046 8/19/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 8/20/14 9:42 EEHg/L0.16 8/19/14SM18-20 6200B11,1-Dichloroethane
ND 5.0 8/20/14 9:42 EEHg/L0.19 8/19/14SM18-20 6200B11,2-Dichloroethane
ND 0.50 8/20/14 9:42 EEHg/L0.21 8/19/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 8/20/14 9:42 EEHg/L0.15 8/19/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 8/20/14 9:42 EEHg/L0.15 8/19/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 8/20/14 9:42 EEHg/L0.11 8/19/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 8/20/14 9:42 EEHg/L0.099 8/19/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 8/20/14 9:42 EEHg/L0.072 8/19/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 8/20/14 9:42 EEHg/L0.13 8/19/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 8/20/14 9:42 EEHg/L0.062 8/19/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 8/20/14 9:42 EEHg/L0.056 8/19/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 8/20/14 9:42 EEHg/L0.18 8/19/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 8/20/14 9:42 EEHg/L0.092 8/19/14SM18-20 6200B1Ethylbenzene
ND 5.0 8/20/14 9:42 EEHg/L1.5 8/19/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 8/20/14 9:42 EEHg/L0.11 8/19/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 8/20/14 9:42 EEHg/L0.090 8/19/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 8/20/14 9:42 EEHg/L3.2 8/19/14SM18-20 6200B1Methylene Chloride
ND 5.0 8/20/14 9:42 EEHg/L1.5 8/19/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 9 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-02
Field Sample #: SW-1
Sample Matrix: Water
Sampled: 8/14/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B1Naphthalene
ND 0.50 8/20/14 9:42 EEHg/L0.094 8/19/14SM18-20 6200B1n-Propylbenzene
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B1Styrene
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 0.50 8/20/14 9:42 EEHg/L0.080 8/19/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 8/20/14 9:42 EEHg/L0.090 8/19/14SM18-20 6200B1Toluene
ND 0.50 8/20/14 9:42 EEHg/L0.14 8/19/14SM18-20 6200B11,2,3-Trichlorobenzene
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B11,2,4-Trichlorobenzene
ND 0.50 8/20/14 9:42 EEHg/L0.094 8/19/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 8/20/14 9:42 EEHg/L0.077 8/19/14SM18-20 6200B1Trichloroethylene
ND 0.50 8/20/14 9:42 EEHg/L0.15 8/19/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 8/20/14 9:42 EEHg/L0.12 8/19/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 8/20/14 9:42 EEHg/L0.18 8/19/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 8/20/14 9:42 EEHg/L0.10 8/19/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 8/20/14 9:42 EEHg/L1.3 8/19/14SM18-20 6200B1Vinyl Acetate
ND 0.50 8/20/14 9:42 EEHg/L0.13 8/19/14SM18-20 6200B1Vinyl Chloride
ND 1.0 8/20/14 9:42 EEHg/L0.18 8/19/14SM18-20 6200B1m+p Xylene
ND 0.50 8/20/14 9:42 EEHg/L0.11 8/19/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 8/20/14 9:4270-130
Toluene-d8 95.2 8/20/14 9:4270-130
4-Bromofluorobenzene 90.3 8/20/14 9:4270-130
Page 10 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-03
Field Sample #: SW-17
Sample Matrix: Water
Sampled: 8/14/2014 13:30
[TOC_2]14H0700-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 8/20/14 10:09 EEHg/L4.7 8/19/14SM18-20 6200B1Acetone
ND 0.50 8/20/14 10:09 EEHg/L0.079 8/19/14SM18-20 6200B1Benzene
ND 0.50 8/20/14 10:09 EEHg/L0.044 8/19/14SM18-20 6200B1Bromobenzene
ND 0.50 8/20/14 10:09 EEHg/L0.22 8/19/14SM18-20 6200B1Bromochloromethane
ND 0.50 8/20/14 10:09 EEHg/L0.088 8/19/14SM18-20 6200B1Bromodichloromethane
ND 0.50 8/20/14 10:09 EEHg/L0.21 8/19/14SM18-20 6200B1Bromoform
ND 1.0 8/20/14 10:09 EEHg/L0.94 8/19/14SM18-20 6200B1R-05Bromomethane
ND 5.0 8/20/14 10:09 EEHg/L2.4 8/19/14SM18-20 6200B12-Butanone (MEK)
ND 0.50 8/20/14 10:09 EEHg/L0.054 8/19/14SM18-20 6200B1n-Butylbenzene
ND 0.50 8/20/14 10:09 EEHg/L0.084 8/19/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 8/20/14 10:09 EEHg/L0.096 8/19/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 8/20/14 10:09 EEHg/L0.10 8/19/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B1Chlorobenzene
ND 50 8/20/14 10:09 EEHg/L28 8/19/14SM18-20 6200B1V-16Ethanol
ND 0.50 8/20/14 10:09 EEHg/L0.054 8/19/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 8/20/14 10:09 EEHg/L0.16 8/19/14SM18-20 6200B1Chloroethane
ND 0.50 8/20/14 10:09 EEHg/L0.14 8/19/14SM18-20 6200B1Chloroform
ND 5.0 8/20/14 10:09 EEHg/L0.32 8/19/14SM18-20 6200B1Chloromethane
ND 0.50 8/20/14 10:09 EEHg/L0.070 8/19/14SM18-20 6200B12-Chlorotoluene
ND 0.50 8/20/14 10:09 EEHg/L0.074 8/19/14SM18-20 6200B14-Chlorotoluene
ND 0.50 8/20/14 10:09 EEHg/L0.089 8/19/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 8/20/14 10:09 EEHg/L0.076 8/19/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 8/20/14 10:09 EEHg/L0.079 8/19/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 8/20/14 10:09 EEHg/L0.046 8/19/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 8/20/14 10:09 EEHg/L0.16 8/19/14SM18-20 6200B11,1-Dichloroethane
ND 5.0 8/20/14 10:09 EEHg/L0.19 8/19/14SM18-20 6200B11,2-Dichloroethane
ND 0.50 8/20/14 10:09 EEHg/L0.21 8/19/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 8/20/14 10:09 EEHg/L0.15 8/19/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 8/20/14 10:09 EEHg/L0.15 8/19/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 8/20/14 10:09 EEHg/L0.11 8/19/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 8/20/14 10:09 EEHg/L0.099 8/19/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 8/20/14 10:09 EEHg/L0.072 8/19/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 8/20/14 10:09 EEHg/L0.13 8/19/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 8/20/14 10:09 EEHg/L0.062 8/19/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 8/20/14 10:09 EEHg/L0.056 8/19/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 8/20/14 10:09 EEHg/L0.18 8/19/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 8/20/14 10:09 EEHg/L0.092 8/19/14SM18-20 6200B1Ethylbenzene
ND 5.0 8/20/14 10:09 EEHg/L1.5 8/19/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 8/20/14 10:09 EEHg/L0.11 8/19/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 8/20/14 10:09 EEHg/L0.090 8/19/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 8/20/14 10:09 EEHg/L3.2 8/19/14SM18-20 6200B1Methylene Chloride
ND 5.0 8/20/14 10:09 EEHg/L1.5 8/19/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 11 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-03
Field Sample #: SW-17
Sample Matrix: Water
Sampled: 8/14/2014 13:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B1Naphthalene
ND 0.50 8/20/14 10:09 EEHg/L0.094 8/19/14SM18-20 6200B1n-Propylbenzene
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B1Styrene
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 0.50 8/20/14 10:09 EEHg/L0.080 8/19/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 8/20/14 10:09 EEHg/L0.090 8/19/14SM18-20 6200B1Toluene
ND 0.50 8/20/14 10:09 EEHg/L0.14 8/19/14SM18-20 6200B11,2,3-Trichlorobenzene
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B11,2,4-Trichlorobenzene
ND 0.50 8/20/14 10:09 EEHg/L0.094 8/19/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 8/20/14 10:09 EEHg/L0.077 8/19/14SM18-20 6200B1Trichloroethylene
ND 0.50 8/20/14 10:09 EEHg/L0.15 8/19/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 8/20/14 10:09 EEHg/L0.12 8/19/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 8/20/14 10:09 EEHg/L0.18 8/19/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 8/20/14 10:09 EEHg/L0.10 8/19/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 8/20/14 10:09 EEHg/L1.3 8/19/14SM18-20 6200B1Vinyl Acetate
ND 0.50 8/20/14 10:09 EEHg/L0.13 8/19/14SM18-20 6200B1Vinyl Chloride
ND 1.0 8/20/14 10:09 EEHg/L0.18 8/19/14SM18-20 6200B1m+p Xylene
ND 0.50 8/20/14 10:09 EEHg/L0.11 8/19/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 105 8/20/14 10:0970-130
Toluene-d8 97.9 8/20/14 10:0970-130
4-Bromofluorobenzene 90.8 8/20/14 10:0970-130
Page 12 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-04
Field Sample #: SW-16
Sample Matrix: Water
Sampled: 8/14/2014 14:00
[TOC_2]14H0700-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 8/20/14 10:35 EEHg/L4.7 8/19/14SM18-20 6200B1Acetone
ND 0.50 8/20/14 10:35 EEHg/L0.079 8/19/14SM18-20 6200B1Benzene
ND 0.50 8/20/14 10:35 EEHg/L0.044 8/19/14SM18-20 6200B1Bromobenzene
ND 0.50 8/20/14 10:35 EEHg/L0.22 8/19/14SM18-20 6200B1Bromochloromethane
ND 0.50 8/20/14 10:35 EEHg/L0.088 8/19/14SM18-20 6200B1Bromodichloromethane
ND 0.50 8/20/14 10:35 EEHg/L0.21 8/19/14SM18-20 6200B1Bromoform
ND 1.0 8/20/14 10:35 EEHg/L0.94 8/19/14SM18-20 6200B1R-05Bromomethane
ND 5.0 8/20/14 10:35 EEHg/L2.4 8/19/14SM18-20 6200B12-Butanone (MEK)
ND 0.50 8/20/14 10:35 EEHg/L0.054 8/19/14SM18-20 6200B1n-Butylbenzene
ND 0.50 8/20/14 10:35 EEHg/L0.084 8/19/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 8/20/14 10:35 EEHg/L0.096 8/19/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 8/20/14 10:35 EEHg/L0.10 8/19/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B1Chlorobenzene
ND 50 8/20/14 10:35 EEHg/L28 8/19/14SM18-20 6200B1V-16Ethanol
ND 0.50 8/20/14 10:35 EEHg/L0.054 8/19/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 8/20/14 10:35 EEHg/L0.16 8/19/14SM18-20 6200B1Chloroethane
ND 0.50 8/20/14 10:35 EEHg/L0.14 8/19/14SM18-20 6200B1Chloroform
ND 5.0 8/20/14 10:35 EEHg/L0.32 8/19/14SM18-20 6200B1Chloromethane
ND 0.50 8/20/14 10:35 EEHg/L0.070 8/19/14SM18-20 6200B12-Chlorotoluene
ND 0.50 8/20/14 10:35 EEHg/L0.074 8/19/14SM18-20 6200B14-Chlorotoluene
ND 0.50 8/20/14 10:35 EEHg/L0.089 8/19/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 8/20/14 10:35 EEHg/L0.076 8/19/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 8/20/14 10:35 EEHg/L0.079 8/19/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 8/20/14 10:35 EEHg/L0.046 8/19/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 8/20/14 10:35 EEHg/L0.16 8/19/14SM18-20 6200B11,1-Dichloroethane
ND 5.0 8/20/14 10:35 EEHg/L0.19 8/19/14SM18-20 6200B11,2-Dichloroethane
ND 0.50 8/20/14 10:35 EEHg/L0.21 8/19/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 8/20/14 10:35 EEHg/L0.15 8/19/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 8/20/14 10:35 EEHg/L0.15 8/19/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 8/20/14 10:35 EEHg/L0.11 8/19/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 8/20/14 10:35 EEHg/L0.099 8/19/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 8/20/14 10:35 EEHg/L0.072 8/19/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 8/20/14 10:35 EEHg/L0.13 8/19/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 8/20/14 10:35 EEHg/L0.062 8/19/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 8/20/14 10:35 EEHg/L0.056 8/19/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 8/20/14 10:35 EEHg/L0.18 8/19/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 8/20/14 10:35 EEHg/L0.092 8/19/14SM18-20 6200B1Ethylbenzene
ND 5.0 8/20/14 10:35 EEHg/L1.5 8/19/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 8/20/14 10:35 EEHg/L0.11 8/19/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 8/20/14 10:35 EEHg/L0.090 8/19/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 8/20/14 10:35 EEHg/L3.2 8/19/14SM18-20 6200B1Methylene Chloride
ND 5.0 8/20/14 10:35 EEHg/L1.5 8/19/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 13 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-04
Field Sample #: SW-16
Sample Matrix: Water
Sampled: 8/14/2014 14:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B1Naphthalene
ND 0.50 8/20/14 10:35 EEHg/L0.094 8/19/14SM18-20 6200B1n-Propylbenzene
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B1Styrene
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 0.50 8/20/14 10:35 EEHg/L0.080 8/19/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 8/20/14 10:35 EEHg/L0.090 8/19/14SM18-20 6200B1Toluene
ND 0.50 8/20/14 10:35 EEHg/L0.14 8/19/14SM18-20 6200B11,2,3-Trichlorobenzene
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B11,2,4-Trichlorobenzene
ND 0.50 8/20/14 10:35 EEHg/L0.094 8/19/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 8/20/14 10:35 EEHg/L0.077 8/19/14SM18-20 6200B1Trichloroethylene
ND 0.50 8/20/14 10:35 EEHg/L0.15 8/19/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 8/20/14 10:35 EEHg/L0.12 8/19/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 8/20/14 10:35 EEHg/L0.18 8/19/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 8/20/14 10:35 EEHg/L0.10 8/19/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 8/20/14 10:35 EEHg/L1.3 8/19/14SM18-20 6200B1Vinyl Acetate
ND 0.50 8/20/14 10:35 EEHg/L0.13 8/19/14SM18-20 6200B1Vinyl Chloride
ND 1.0 8/20/14 10:35 EEHg/L0.18 8/19/14SM18-20 6200B1m+p Xylene
ND 0.50 8/20/14 10:35 EEHg/L0.11 8/19/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 105 8/20/14 10:3570-130
Toluene-d8 86.2 8/20/14 10:3570-130
4-Bromofluorobenzene 89.7 8/20/14 10:3570-130
Page 14 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-05
Field Sample #: SW-3
Sample Matrix: Water
Sampled: 8/14/2014 14:30
[TOC_2]14H0700-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 8/20/14 11:02 EEHg/L4.7 8/19/14SM18-20 6200B1Acetone
ND 0.50 8/20/14 11:02 EEHg/L0.079 8/19/14SM18-20 6200B1Benzene
ND 0.50 8/20/14 11:02 EEHg/L0.044 8/19/14SM18-20 6200B1Bromobenzene
ND 0.50 8/20/14 11:02 EEHg/L0.22 8/19/14SM18-20 6200B1Bromochloromethane
ND 0.50 8/20/14 11:02 EEHg/L0.088 8/19/14SM18-20 6200B1Bromodichloromethane
ND 0.50 8/20/14 11:02 EEHg/L0.21 8/19/14SM18-20 6200B1Bromoform
ND 1.0 8/20/14 11:02 EEHg/L0.94 8/19/14SM18-20 6200B1R-05Bromomethane
ND 5.0 8/20/14 11:02 EEHg/L2.4 8/19/14SM18-20 6200B12-Butanone (MEK)
ND 0.50 8/20/14 11:02 EEHg/L0.054 8/19/14SM18-20 6200B1n-Butylbenzene
ND 0.50 8/20/14 11:02 EEHg/L0.084 8/19/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 8/20/14 11:02 EEHg/L0.096 8/19/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 8/20/14 11:02 EEHg/L0.10 8/19/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B1Chlorobenzene
ND 50 8/20/14 11:02 EEHg/L28 8/19/14SM18-20 6200B1V-16Ethanol
ND 0.50 8/20/14 11:02 EEHg/L0.054 8/19/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 8/20/14 11:02 EEHg/L0.16 8/19/14SM18-20 6200B1Chloroethane
ND 0.50 8/20/14 11:02 EEHg/L0.14 8/19/14SM18-20 6200B1Chloroform
ND 5.0 8/20/14 11:02 EEHg/L0.32 8/19/14SM18-20 6200B1Chloromethane
ND 0.50 8/20/14 11:02 EEHg/L0.070 8/19/14SM18-20 6200B12-Chlorotoluene
ND 0.50 8/20/14 11:02 EEHg/L0.074 8/19/14SM18-20 6200B14-Chlorotoluene
ND 0.50 8/20/14 11:02 EEHg/L0.089 8/19/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 8/20/14 11:02 EEHg/L0.076 8/19/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 8/20/14 11:02 EEHg/L0.079 8/19/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 8/20/14 11:02 EEHg/L0.046 8/19/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 8/20/14 11:02 EEHg/L0.16 8/19/14SM18-20 6200B11,1-Dichloroethane
ND 5.0 8/20/14 11:02 EEHg/L0.19 8/19/14SM18-20 6200B11,2-Dichloroethane
ND 0.50 8/20/14 11:02 EEHg/L0.21 8/19/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 8/20/14 11:02 EEHg/L0.15 8/19/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 8/20/14 11:02 EEHg/L0.15 8/19/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 8/20/14 11:02 EEHg/L0.11 8/19/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 8/20/14 11:02 EEHg/L0.099 8/19/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 8/20/14 11:02 EEHg/L0.072 8/19/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 8/20/14 11:02 EEHg/L0.13 8/19/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 8/20/14 11:02 EEHg/L0.062 8/19/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 8/20/14 11:02 EEHg/L0.056 8/19/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 8/20/14 11:02 EEHg/L0.18 8/19/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 8/20/14 11:02 EEHg/L0.092 8/19/14SM18-20 6200B1Ethylbenzene
ND 5.0 8/20/14 11:02 EEHg/L1.5 8/19/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 8/20/14 11:02 EEHg/L0.11 8/19/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 8/20/14 11:02 EEHg/L0.090 8/19/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 8/20/14 11:02 EEHg/L3.2 8/19/14SM18-20 6200B1Methylene Chloride
ND 5.0 8/20/14 11:02 EEHg/L1.5 8/19/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 15 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-05
Field Sample #: SW-3
Sample Matrix: Water
Sampled: 8/14/2014 14:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B1Naphthalene
ND 0.50 8/20/14 11:02 EEHg/L0.094 8/19/14SM18-20 6200B1n-Propylbenzene
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B1Styrene
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 0.50 8/20/14 11:02 EEHg/L0.080 8/19/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 8/20/14 11:02 EEHg/L0.090 8/19/14SM18-20 6200B1Toluene
ND 0.50 8/20/14 11:02 EEHg/L0.14 8/19/14SM18-20 6200B11,2,3-Trichlorobenzene
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B11,2,4-Trichlorobenzene
ND 0.50 8/20/14 11:02 EEHg/L0.094 8/19/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 8/20/14 11:02 EEHg/L0.077 8/19/14SM18-20 6200B1Trichloroethylene
ND 0.50 8/20/14 11:02 EEHg/L0.15 8/19/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 8/20/14 11:02 EEHg/L0.12 8/19/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 8/20/14 11:02 EEHg/L0.18 8/19/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 8/20/14 11:02 EEHg/L0.10 8/19/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 8/20/14 11:02 EEHg/L1.3 8/19/14SM18-20 6200B1Vinyl Acetate
ND 0.50 8/20/14 11:02 EEHg/L0.13 8/19/14SM18-20 6200B1Vinyl Chloride
ND 1.0 8/20/14 11:02 EEHg/L0.18 8/19/14SM18-20 6200B1m+p Xylene
ND 0.50 8/20/14 11:02 EEHg/L0.11 8/19/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 8/20/14 11:0270-130
Toluene-d8 98.6 8/20/14 11:0270-130
4-Bromofluorobenzene 89.0 8/20/14 11:0270-130
Page 16 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-06
Field Sample #: SW-22
Sample Matrix: Water
Sampled: 8/14/2014 15:00
[TOC_2]14H0700-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 8/20/14 11:28 EEHg/L4.7 8/19/14SM18-20 6200B1Acetone
ND 0.50 8/20/14 11:28 EEHg/L0.079 8/19/14SM18-20 6200B1Benzene
ND 0.50 8/20/14 11:28 EEHg/L0.044 8/19/14SM18-20 6200B1Bromobenzene
ND 0.50 8/20/14 11:28 EEHg/L0.22 8/19/14SM18-20 6200B1Bromochloromethane
ND 0.50 8/20/14 11:28 EEHg/L0.088 8/19/14SM18-20 6200B1Bromodichloromethane
ND 0.50 8/20/14 11:28 EEHg/L0.21 8/19/14SM18-20 6200B1Bromoform
ND 1.0 8/20/14 11:28 EEHg/L0.94 8/19/14SM18-20 6200B1R-05Bromomethane
ND 5.0 8/20/14 11:28 EEHg/L2.4 8/19/14SM18-20 6200B12-Butanone (MEK)
ND 0.50 8/20/14 11:28 EEHg/L0.054 8/19/14SM18-20 6200B1n-Butylbenzene
ND 0.50 8/20/14 11:28 EEHg/L0.084 8/19/14SM18-20 6200B1sec-Butylbenzene
ND 0.50 8/20/14 11:28 EEHg/L0.096 8/19/14SM18-20 6200B1tert-Butylbenzene
ND 0.50 8/20/14 11:28 EEHg/L0.10 8/19/14SM18-20 6200B1Carbon Tetrachloride
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B1Chlorobenzene
ND 50 8/20/14 11:28 EEHg/L28 8/19/14SM18-20 6200B1V-16Ethanol
ND 0.50 8/20/14 11:28 EEHg/L0.054 8/19/14SM18-20 6200B1Chlorodibromomethane
ND 0.50 8/20/14 11:28 EEHg/L0.16 8/19/14SM18-20 6200B1Chloroethane
ND 0.50 8/20/14 11:28 EEHg/L0.14 8/19/14SM18-20 6200B1Chloroform
ND 5.0 8/20/14 11:28 EEHg/L0.32 8/19/14SM18-20 6200B1Chloromethane
ND 0.50 8/20/14 11:28 EEHg/L0.070 8/19/14SM18-20 6200B12-Chlorotoluene
ND 0.50 8/20/14 11:28 EEHg/L0.074 8/19/14SM18-20 6200B14-Chlorotoluene
ND 0.50 8/20/14 11:28 EEHg/L0.089 8/19/14SM18-20 6200B11,2-Dibromoethane (EDB)
ND 0.50 8/20/14 11:28 EEHg/L0.076 8/19/14SM18-20 6200B11,2-Dichlorobenzene
ND 0.50 8/20/14 11:28 EEHg/L0.079 8/19/14SM18-20 6200B11,3-Dichlorobenzene
ND 0.50 8/20/14 11:28 EEHg/L0.046 8/19/14SM18-20 6200B11,4-Dichlorobenzene
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 8/20/14 11:28 EEHg/L0.16 8/19/14SM18-20 6200B11,1-Dichloroethane
ND 5.0 8/20/14 11:28 EEHg/L0.19 8/19/14SM18-20 6200B11,2-Dichloroethane
ND 0.50 8/20/14 11:28 EEHg/L0.21 8/19/14SM18-20 6200B11,1-Dichloroethylene
ND 0.50 8/20/14 11:28 EEHg/L0.15 8/19/14SM18-20 6200B1cis-1,2-Dichloroethylene
ND 0.50 8/20/14 11:28 EEHg/L0.15 8/19/14SM18-20 6200B1trans-1,2-Dichloroethylene
ND 0.50 8/20/14 11:28 EEHg/L0.11 8/19/14SM18-20 6200B11,2-Dichloropropane
ND 0.50 8/20/14 11:28 EEHg/L0.099 8/19/14SM18-20 6200B11,3-Dichloropropane
ND 0.50 8/20/14 11:28 EEHg/L0.072 8/19/14SM18-20 6200B12,2-Dichloropropane
ND 0.50 8/20/14 11:28 EEHg/L0.13 8/19/14SM18-20 6200B11,1-Dichloropropene
ND 0.50 8/20/14 11:28 EEHg/L0.062 8/19/14SM18-20 6200B1cis-1,3-Dichloropropene
ND 0.50 8/20/14 11:28 EEHg/L0.056 8/19/14SM18-20 6200B1trans-1,3-Dichloropropene
ND 0.50 8/20/14 11:28 EEHg/L0.18 8/19/14SM18-20 6200B1Diisopropyl Ether (DIPE)
ND 0.50 8/20/14 11:28 EEHg/L0.092 8/19/14SM18-20 6200B1Ethylbenzene
ND 5.0 8/20/14 11:28 EEHg/L1.5 8/19/14SM18-20 6200B12-Hexanone (MBK)
ND 0.50 8/20/14 11:28 EEHg/L0.11 8/19/14SM18-20 6200B1Isopropylbenzene (Cumene)
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 8/20/14 11:28 EEHg/L0.090 8/19/14SM18-20 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 8/20/14 11:28 EEHg/L3.2 8/19/14SM18-20 6200B1Methylene Chloride
ND 5.0 8/20/14 11:28 EEHg/L1.5 8/19/14SM18-20 6200B14-Methyl-2-pentanone (MIBK)
Page 17 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 8/14/2014
Work Order: 14H0700Sample Description:Project Location: Mount Airy (Sheltontown)
Sample ID: 14H0700-06
Field Sample #: SW-22
Sample Matrix: Water
Sampled: 8/14/2014 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B1Naphthalene
ND 0.50 8/20/14 11:28 EEHg/L0.094 8/19/14SM18-20 6200B1n-Propylbenzene
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B1Styrene
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2,2-Tetrachloroethane
ND 0.50 8/20/14 11:28 EEHg/L0.080 8/19/14SM18-20 6200B1Tetrachloroethylene
ND 0.50 8/20/14 11:28 EEHg/L0.090 8/19/14SM18-20 6200B1Toluene
ND 0.50 8/20/14 11:28 EEHg/L0.14 8/19/14SM18-20 6200B11,2,3-Trichlorobenzene
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B11,2,4-Trichlorobenzene
ND 0.50 8/20/14 11:28 EEHg/L0.094 8/19/14SM18-20 6200B11,1,1-Trichloroethane
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B11,1,2-Trichloroethane
ND 0.50 8/20/14 11:28 EEHg/L0.077 8/19/14SM18-20 6200B1Trichloroethylene
ND 0.50 8/20/14 11:28 EEHg/L0.15 8/19/14SM18-20 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 8/20/14 11:28 EEHg/L0.12 8/19/14SM18-20 6200B11,2,3-Trichloropropane
ND 0.50 8/20/14 11:28 EEHg/L0.18 8/19/14SM18-20 6200B11,2,4-Trimethylbenzene
ND 0.50 8/20/14 11:28 EEHg/L0.10 8/19/14SM18-20 6200B11,3,5-Trimethylbenzene
ND 5.0 8/20/14 11:28 EEHg/L1.3 8/19/14SM18-20 6200B1Vinyl Acetate
ND 0.50 8/20/14 11:28 EEHg/L0.13 8/19/14SM18-20 6200B1Vinyl Chloride
ND 1.0 8/20/14 11:28 EEHg/L0.18 8/19/14SM18-20 6200B1m+p Xylene
ND 0.50 8/20/14 11:28 EEHg/L0.11 8/19/14SM18-20 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 8/20/14 11:2870-130
Toluene-d8 97.8 8/20/14 11:2870-130
4-Bromofluorobenzene 92.3 8/20/14 11:2870-130
Page 18 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: MA VPH-MADEP-VPH-04-1.1
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B102978 08/19/145 5.0014H0700-01 [MW-1]
Prep Method: SW-846 5030B-SM18-20 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B102986 08/19/145 5.0014H0700-01 [MW-1]
B102986 08/19/145 5.0014H0700-02 [SW-1]
B102986 08/19/145 5.0014H0700-03 [SW-17]
B102986 08/19/145 5.0014H0700-04 [SW-16]
B102986 08/19/145 5.0014H0700-05 [SW-3]
B102986 08/19/145 5.0014H0700-06 [SW-22]
Prep Method: SW-846 3005A-SW-846 6020A
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B102832 08/16/1450.0 50.014H0700-01 [MW-1]
[TOC_1]Sample Preparation Information[TOC]
Page 19 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B102986 - SW-846 5030B
[TOC_3]B102986[TOC]
Blank (B102986-BLK1) Prepared: 08/19/14 Analyzed: 08/20/14
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0 R-05ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50 V-16ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L5.0ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L5.0ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L0.50ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 20 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B102986 - SW-846 5030B
Blank (B102986-BLK1) Prepared: 08/19/14 Analyzed: 08/20/14
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L5.0ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10827.0
g/L 25.0 70-130Surrogate: Toluene-d8 98.424.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 90.022.5
LCS (B102986-BS1) Prepared: 08/19/14 Analyzed: 08/20/14
Acetone g/L50 100 70-13079.979.9
Benzene g/L0.50 10.0 70-13011711.7
Bromobenzene g/L0.50 10.0 70-13010010.0
Bromochloromethane g/L0.50 10.0 70-13012512.5
Bromodichloromethane g/L0.50 10.0 70-13011211.2
Bromoform g/L0.50 10.0 70-13012712.7
Bromomethane g/L1.0 10.0 R-0560-14012312.3
2-Butanone (MEK)g/L5.0 100 70-13097.197.1
n-Butylbenzene g/L0.50 10.0 70-13012112.1
sec-Butylbenzene g/L0.50 10.0 70-13010810.8
tert-Butylbenzene g/L0.50 10.0 70-13010710.7
Carbon Tetrachloride g/L0.50 10.0 70-13012212.2
Chlorobenzene g/L0.50 10.0 70-13098.99.89
Ethanol g/L50 100 V-1670-13079.179.1
Chlorodibromomethane g/L0.50 10.0 70-13010910.9
Chloroethane g/L0.50 10.0 60-14099.49.94
Chloroform g/L0.50 10.0 70-13011011.0
Chloromethane g/L5.0 10.0 60-14092.49.24
2-Chlorotoluene g/L0.50 10.0 70-13085.78.57
4-Chlorotoluene g/L0.50 10.0 70-13096.49.64
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010910.9
1,2-Dichlorobenzene g/L0.50 10.0 70-13099.59.95
1,3-Dichlorobenzene g/L0.50 10.0 70-13010110.1
1,4-Dichlorobenzene g/L0.50 10.0 70-13010410.4
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14012712.7
1,1-Dichloroethane g/L0.50 10.0 70-13011611.6
1,2-Dichloroethane g/L5.0 10.0 70-13011211.2
1,1-Dichloroethylene g/L0.50 10.0 70-13094.19.41
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010810.8
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13011211.2
1,2-Dichloropropane g/L0.50 10.0 70-13010610.6
1,3-Dichloropropane g/L0.50 10.0 70-13011111.1
2,2-Dichloropropane g/L0.50 10.0 70-13010410.4
1,1-Dichloropropene g/L0.50 10.0 70-13011511.5
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010210.2
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010410.4
Page 21 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B102986 - SW-846 5030B
LCS (B102986-BS1) Prepared: 08/19/14 Analyzed: 08/20/14
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010610.6
Ethylbenzene g/L0.50 10.0 70-13010410.4
2-Hexanone (MBK)g/L5.0 100 70-130102102
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13094.19.41
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011611.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13011411.4
Methylene Chloride g/L5.0 10.0 70-13095.99.59
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130101101
Naphthalene g/L0.50 10.0 70-13092.89.28
n-Propylbenzene g/L0.50 10.0 70-13095.69.56
Styrene g/L0.50 10.0 70-13010210.2
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010310.3
Tetrachloroethylene g/L0.50 10.0 70-13010310.3
Toluene g/L0.50 10.0 70-13010510.5
1,2,3-Trichlorobenzene g/L0.50 10.0 70-13095.19.51
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13010710.7
1,1,1-Trichloroethane g/L0.50 10.0 70-13011711.7
1,1,2-Trichloroethane g/L0.50 10.0 70-13010510.5
Trichloroethylene g/L0.50 10.0 70-13011111.1
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13094.39.43
1,2,3-Trichloropropane g/L0.50 10.0 70-13010410.4
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011611.6
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13099.69.96
Vinyl Acetate g/L5.0 100 70-13092.692.6
Vinyl Chloride g/L0.50 10.0 60-14087.28.72
m+p Xylene g/L1.0 20.0 70-13099.719.9
o-Xylene g/L0.50 10.0 70-13097.99.79
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11027.4
g/L 25.0 70-130Surrogate: Toluene-d8 96.624.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 92.523.1
LCS Dup (B102986-BSD1) Prepared: 08/19/14 Analyzed: 08/20/14
Acetone g/L50 100 2570-13095.2 17.595.2
Benzene g/L0.50 10.0 2570-130118 1.1911.8
Bromobenzene g/L0.50 10.0 2570-130101 1.0910.1
Bromochloromethane g/L0.50 10.0 2570-130120 4.1512.0
Bromodichloromethane g/L0.50 10.0 2570-130112 0.44711.2
Bromoform g/L0.50 10.0 25 L-0770-130135 6.04*13.5
Bromomethane g/L1.0 10.0 25 R-0560-14094.1 26.5 *9.41
2-Butanone (MEK)g/L5.0 100 2570-130108 10.3108
n-Butylbenzene g/L0.50 10.0 2570-130117 3.4511.7
sec-Butylbenzene g/L0.50 10.0 2570-130103 4.1710.3
tert-Butylbenzene g/L0.50 10.0 2570-130105 2.5510.5
Carbon Tetrachloride g/L0.50 10.0 2570-130123 1.0612.3
Chlorobenzene g/L0.50 10.0 2570-13097.6 1.329.76
Ethanol g/L50 100 25 L-07, V-1670-13063.8 21.4*63.8
Chlorodibromomethane g/L0.50 10.0 2570-130108 0.27610.8
Chloroethane g/L0.50 10.0 2560-14098.7 0.7079.87
Chloroform g/L0.50 10.0 2570-130109 1.1810.9
Chloromethane g/L5.0 10.0 2560-14094.4 2.149.44
2-Chlorotoluene g/L0.50 10.0 2570-13085.3 0.4688.53
4-Chlorotoluene g/L0.50 10.0 2570-13093.4 3.169.34
Page 22 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B102986 - SW-846 5030B
LCS Dup (B102986-BSD1) Prepared: 08/19/14 Analyzed: 08/20/14
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130110 1.1011.0
1,2-Dichlorobenzene g/L0.50 10.0 2570-13096.4 3.169.64
1,3-Dichlorobenzene g/L0.50 10.0 2570-13097.0 4.149.70
1,4-Dichlorobenzene g/L0.50 10.0 2570-130101 2.4410.1
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-140121 4.8512.1
1,1-Dichloroethane g/L0.50 10.0 2570-130114 1.5611.4
1,2-Dichloroethane g/L5.0 10.0 2570-130110 1.2611.0
1,1-Dichloroethylene g/L0.50 10.0 2570-13092.7 1.509.27
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130111 2.2811.1
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130114 1.5911.4
1,2-Dichloropropane g/L0.50 10.0 2570-130106 0.094710.6
1,3-Dichloropropane g/L0.50 10.0 2570-130112 0.89411.2
2,2-Dichloropropane g/L0.50 10.0 2570-130104 0.095910.4
1,1-Dichloropropene g/L0.50 10.0 2570-130115 0.26111.5
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130104 1.7510.4
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130107 2.0810.7
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130103 3.3410.3
Ethylbenzene g/L0.50 10.0 2570-130104 0.095710.4
2-Hexanone (MBK)g/L5.0 100 2570-130112 9.16112
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13093.9 0.2139.39
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130111 4.5011.1
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-130116 2.0911.6
Methylene Chloride g/L5.0 10.0 2570-13097.3 1.459.73
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130111 9.07111
Naphthalene g/L0.50 10.0 2570-130109 16.310.9
n-Propylbenzene g/L0.50 10.0 2570-13094.5 1.169.45
Styrene g/L0.50 10.0 2570-130102 0.29410.2
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130109 5.5710.9
Tetrachloroethylene g/L0.50 10.0 2570-13099.9 2.969.99
Toluene g/L0.50 10.0 2570-130105 0.19010.5
1,2,3-Trichlorobenzene g/L0.50 10.0 2570-130111 15.211.1
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130110 3.0311.0
1,1,1-Trichloroethane g/L0.50 10.0 2570-130119 1.0211.9
1,1,2-Trichloroethane g/L0.50 10.0 2570-130107 1.6910.7
Trichloroethylene g/L0.50 10.0 2570-130112 1.1711.2
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13096.1 1.899.61
1,2,3-Trichloropropane g/L0.50 10.0 2570-130109 5.0610.9
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130114 1.3911.4
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13098.4 1.219.84
Vinyl Acetate g/L5.0 100 2570-130101 8.36101
Vinyl Chloride g/L0.50 10.0 2560-14093.8 7.299.38
m+p Xylene g/L1.0 20.0 2570-13098.6 1.1119.7
o-Xylene g/L0.50 10.0 2570-13095.9 2.069.59
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11127.7
g/L 25.0 70-130Surrogate: Toluene-d8 97.124.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 91.122.8
Page 23 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B102978 - MA VPH
[TOC_3]B102978[TOC]
Blank (B102978-BLK1) Prepared & Analyzed: 08/19/14
Unadjusted C5-C8 Aliphatics g/L100ND
C5-C8 Aliphatics g/L100ND
Unadjusted C9-C12 Aliphatics g/L100ND
C9-C12 Aliphatics g/L100ND
C9-C10 Aromatics g/L100ND
Benzene g/L1.0ND
Butylcyclohexane g/L1.0ND
Decane g/L1.0ND
Ethylbenzene g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
2-Methylpentane g/L1.0ND
Naphthalene g/L5.0ND
Nonane g/L1.0ND
Pentane g/L1.0ND
Toluene g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
2,2,4-Trimethylpentane g/L1.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)95.738.3
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)70.928.4
LCS (B102978-BS1) Prepared & Analyzed: 08/19/14
Benzene g/L1.0 100 70-13081.381.3
Butylcyclohexane g/L1.0 100 70-130101101
Decane g/L1.0 100 70-130117117
Ethylbenzene g/L1.0 100 70-13082.782.7
Methyl tert-Butyl Ether (MTBE)g/L1.0 100 70-13084.884.8
2-Methylpentane g/L1.0 100 70-130120120
Naphthalene g/L5.0 100 70-130122122
Nonane g/L1.0 100 70-130107107
Pentane g/L1.0 100 70-130127127
Toluene g/L1.0 100 70-13081.881.8
1,2,4-Trimethylbenzene g/L1.0 100 70-13083.183.1
2,2,4-Trimethylpentane g/L1.0 100 L-0770-130140*140
m+p Xylene g/L2.0 200 70-13083.3167
o-Xylene g/L1.0 100 70-13081.281.2
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12248.7
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)89.635.8
LCS Dup (B102978-BSD1) Prepared & Analyzed: 08/19/14
Benzene g/L1.0 100 2570-13077.3 4.9977.3
Butylcyclohexane g/L1.0 100 2570-13095.0 6.0695.0
Decane g/L1.0 100 2570-130111 5.12111
Ethylbenzene g/L1.0 100 2570-13078.6 5.1078.6
Methyl tert-Butyl Ether (MTBE)g/L1.0 100 2570-13079.4 6.6279.4
2-Methylpentane g/L1.0 100 2570-130110 8.93110
Naphthalene g/L5.0 100 2570-130102 17.7102
Nonane g/L1.0 100 2570-130101 5.95101
Pentane g/L1.0 100 2570-130119 5.70119
Toluene g/L1.0 100 2570-13077.8 4.9677.8
1,2,4-Trimethylbenzene g/L1.0 100 2570-13077.6 6.8477.6
Page 24 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B102978 - MA VPH
LCS Dup (B102978-BSD1) Prepared & Analyzed: 08/19/14
2,2,4-Trimethylpentane g/L1.0 100 2570-130127 9.61127
m+p Xylene g/L2.0 200 2570-13079.2 4.96158
o-Xylene g/L1.0 100 2570-13077.5 4.5977.5
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (FID)12951.4
g/L 40.0 70-130Surrogate: 2,5-Dibromotoluene (PID)81.732.7
Page 25 of 34
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B102832 - SW-846 3005A
[TOC_3]B102832[TOC]
Blank (B102832-BLK1) Prepared: 08/16/14 Analyzed: 08/18/14
Lead g/L2.0ND
LCS (B102832-BS1) Prepared: 08/16/14 Analyzed: 08/18/14
Lead g/L5.0 250 80-120102256
LCS Dup (B102832-BSD1) Prepared: 08/16/14 Analyzed: 08/18/14
Lead g/L5.0 250 2080-120104 0.998259
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may
be associated with reported result.
V-16
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-VPH-04-1.1 in Water
CT,NC,WA,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,WA,ME,NH-PC5-C8 Aliphatics
CT,NC,WA,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,WA,ME,NH-PC9-C12 Aliphatics
CT,NC,WA,ME,NH-PC9-C10 Aromatics
CT,NC,WA,ME,NH-PBenzene
CT,NC,WA,ME,NH-PEthylbenzene
CT,NC,WA,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,WA,ME,NH-PNaphthalene
CT,NC,WA,ME,NH-PToluene
CT,NC,WA,ME,NH-Pm+p Xylene
CT,NC,WA,ME,NH-Po-Xylene
SM18-20 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM18-20 6200B in Water
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 6020A in Water
CT,NH,NY,NC,ME,VA,NJLead
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLCAIHA 02/1/2016
M-MA100Massachusetts DEPMA 06/30/2015
PH-0567Connecticut Department of Publilc HealthCT 09/30/2015
10899 NELAPNew York State Department of HealthNY 04/1/2015
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2015
LAO00112Rhode Island Department of HealthRI 12/30/2014
652North Carolina Div. of Water QualityNC 12/31/2014
MA007 NELAPNew Jersey DEPNJ 06/30/2015
E871027 NELAPFlorida Department of HealthFL 06/30/2015
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2015
C2065State of Washington Department of EcologyWA 02/23/2015
2011028State of MaineME 06/9/2015
460217Commonwealth of VirginiaVA 12/14/2014
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2014
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