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HomeMy WebLinkAboutWS-4481_14498_CA_MRP_20150909August 2015 Groundwater Monitoring Report Former Bennett and Bailey Store 2872 South Stratford Road Winston-Salem, North Carolina 27103 Facility ID 0-001934 Incident # 14498 Latitude 35.9553° North Longitude 80.0061° West September 9, 2015 Prepared for Property Owner 2915 Camp Circle Winston-Salem, North Carolina 27106 (336) 768-8968 Prepared by Best Geological and Environmental Consulting, P.A. 1009 Hayfield Lane Greensboro, North Carolina 27410 (336) 834-8382 BEST GEOLOGICAL AND ENVIRONMENTAL CONSULTING, P.A. 1009 Hayfield Lane Greensboro, North Carolina 27410 (336) 834-8382 Phone jbest6778gmai1.com September 9, 2015 Ms. Carin Kromm North Carolina Department of Environment and Natural Resources Division of Waste Management UST Section 585 Waughtown Street Winston-Salem, North Carolina 27107-2241 Reference: August 2015 Groundwater Monitoring Report Former Bennett and Bailey Store 2872 South Stratford Road Winston-Salem, Forsyth County, North Carolina Incident #14498 Dear Ms. Kromm: Best Geological and Environmental Consulting, P.A. (BGEC) is pleased to provide the results of the groundwater sampling activities performed at the former Bennett and Bailey store located in Winston-Salem, North Carolina. The purpose of this report is to provide a summary of the field activities and the laboratory analytical results, and to provide our conclusions and recommendations regarding this site. Sincerely, Best Geological and Environmental Consulting. P.A. Joseph P. Best, P.G. President/Project Manager cc: Property Owner Mr. Stephen R. Berlin R03-39-Qsamp8115 August 2015 Groundwater Monitoring Report Former Bennett and Bailey Store 2872 South Stratford Road Winston-Salem, North Carolina 27103 Incident Number 14498 September 9, 2015 1 Introduction and Background Information Best Geological and Environmental Consulting, P.A. (BGEC) is pleased to present this Groundwater Monitoring Report for the former Bennett and Bailey store located at 2872 South Stratford Road in Winston-Salem, North Carolina (see Figure 1). This report was prepared for the property owner and documents the results of the August 2015 quarterly groundwater sampling event. The property was formerly used for retail gasoline, diesel, and kerosene sales. A release was confirmed at the site in December 1993 during the removal of underground storage tanks (USTs). The USTs included one 4,000-gallon gasoline UST, one 3,000-gallon gasoline UST, one 2,000-gallon gasoline UST, one 1,000-gallon kerosene UST, and one 550-gallon diesel fuel UST (see Figure 2). Environmental Aspects of North Carolina, Inc. (EAI) of Raleigh, North Carolina submitted a Comprehensive Site Assessment (CSA) in January 1997 and a CSA addendum for the site in March 1997. EAT submitted a Corrective Action Plan (CAP) in June of 1997. The North Carolina Department of Environment and Natural Resources, Division of Waste Management, UST Section (DENR) approved the CSA and the CAP in 1997. EAI installed a soil and groundwater remediation system at the site in the fall of 1999. The system was started on December 15, 1999. The system utilizes air sparging (AS), soil vapor extraction (SVE), and two combination groundwater recovery and SVE wells. Extracted groundwater is treated using an air stripping and carbon filtration system. Treated effluent is discharged into a nearby intermittent tributary of Muddy Creek. Quarterly influent and effluent samples are collected as required by the NPDES permit. Passive free product recovery has been accomplished using recovery bailers. Land use in the vicinity of the former Bennett and Bailey Store is primarily residential and commercial. Seventeen private water supply wells have been identified by EAI within 1,000 feet of the source area. EAI identified four water supply wells within 250 feet of the source area. Two of these wells are not in use. One water supply well is located on the down-gradient trailer park property. This well serves the six residences of the trailer park. Municipal water is not available to the trailer park, but has been extended to within several hundred feet of the site. One surface water body is situated within 500 feet of the source area. An intermittent tributary of Muddy Creek is located immediately south of the trailer park. On September 16, 2014, the DENR issued a letter requesting that a New Technology Cleanup Plan (NTCP) to enhance the performance of the existing remediation system be submitted. The Page 1 of August 2015 Groundwater Monitoring Report Former Bennett and Bailey Store September 9, 2015 NTPC was submitted to the DENR for approval on June 15, 2015. The DENR approved the NTCP on July 6, 2015 and the soil excavation phase of the NTCP was initiated on August 13, 2015. The installation of the recovery pump and associated lines for the NTCP is currently in progress. 2 Sampling 2.1 Groundwater Sampling On August 6, 2015, BGEC personnel sampled monitoring wells (MW-2, MW-5, MW-9, MW- 12, MW-13, MW-14, DCW-1 and the Muddy Creek tributary). The monitoring well locations are shown on Figure 2. Prior to sampling, the water levels of the wells to be sampled were measured using an electronic water level meter or interface probe and recorded. The wells were purged of three well volumes or bailed to dryness - whichever occurred first. During purging, the field parameters of pH, temperature, and specific conductivity were measured and recorded. The field parameters and well construction details are presented in Table 1. The field activities were performed in accordance with the Standard Procedures contained in Appendix A. The groundwater samples were submitted to Pace Analytical Services, Inc. (Pace) of Huntersville, North Carolina to be analyzed for halogenated and aromatic volatile organic compounds using EPA Method 6200B and lead using 3010 preparation. The samples collected from monitoring wells MW-9, MW-13, and MW-14 were also analyzed for semi-volatile organic compounds using EPA Method 8270. 2.2 Water Supply Well Sampling One water supply well (WW-1) was sampled as part of the sampling event. The well was purged prior to sampling. WW-1 was sampled from a spigot located within the well house. The groundwater sample was submitted to Pace for laboratory analyses. The sample was analyzed for halogenated and aromatic volatile organic compounds using EPA Method 6200B, semi- volatile organic compounds using EPA Method 8270, and lead using 3010 preparation. 3 Groundwater Flow and Hydraulic Gradient The source area is covered with grass, low vegetation and asphalt pavement. The site slopes moderately from northeast to southwest. Depth to groundwater in the five shallow monitoring wells that were sampled ranged from 9.49 feet (MW-9) to 18.73 feet (MW-2) during the August 2015 sampling event. Based on the limited groundwater elevation data, shallow groundwater at the site flows generally toward the west under an average horizontal hydraulic gradient of approximately 0.0 15 feet per foot. The groundwater elevation data is presented in Table 1. Page 2 of 5 August 2015 Groundwater Monitoring Report Former Bennett and Bailey Store September 9, 2015 4 Laboratory Analytical Results The laboratory analyses indicated the presence of benzene (1,030 j.tg/L), ethylbenzene (217 p.gIL), toluene (528 tgIL), xylenes (779 p.g/L), MTBE (19.4 [tg/L), IPE (100 j.tg/L), isopropylbenzene (13.2 p.gIL), n-propylbenzene (44.1 .tgIL), 1,2,4-trimethylbenzene (303 .tg/L), 1,2 dichloroethane (30.8 pg/L), lead (11 .tg/L) and naphthalene (52.2 p.g/L) in the groundwater sample collected from monitoring well MW-2. The laboratory analyses indicated the presence of benzene (10,800 tg/L), ethylbenzene (836 p.g/L), toluene (16,600 .tgIL), xylenes (24,590 j.tg/L), IPE (1,570 p.gIL), 1,2,4-trimethylbenzene (7,020 .tg/L), 1,3,5- trimethylbenzene (2,300 j.tg/L), 1,2-dichioroethane (621 ig/L), isopropylbenzene (81.1 .tg/L), lead (26.6 p.g/L) and naphthalene (886 tgfL) in the groundwater sample collected from monitoring well MW-5. The laboratory analyses indicated the presence of benzene (6,170 tg/L), ethylbenzene (772 p.g/L), toluene (5,710 tgIL), xylenes (2,677 tgIL), IPE (764 tg/L), 1,2,4-trimethylbenzene (454 p.g/L), 1,3,5-trimethylbenzene (126 j.tg/L), n-propylbenzene (54 [tg/L), lead (15.1 .i.g/L) and naphthalene (103 p.g/L) in the groundwater sample collected from monitoring well MW-9. The laboratory analyses indicated the presence of lead (21.4 4g/L) in the groundwater sample collected from monitoring well MW-12. The laboratory analyses indicated the presence of benzene (1.2 p.g/L), IPE (2.1 tg/L), MTBE (1.2 .tg/L) and 1,2 dichloroethane (0.93 .tg/L) in the groundwater sample collected from deep well DCW-1. The laboratory analyses indicated the presence of lead (16.7 jtg/L) and MTBE (2.0 ig/L) in the water sample collected from water supply well WW-1. The laboratory analyses indicated the presence of no target compounds in the water samples collected from monitoring wells MW-13, MW-14 and the Muddy Creek Tributary (CREEK). The laboratory analytical results are summarized in Table 2. The complete laboratory report is contained in Appendix B. The historical laboratory analytical results are summarized in Table 3. 5 Discussion of Sampling Results The sampling results indicate groundwater at the site contains benzene, ethyl benzene, toluene, xylenes, MTBE, 1,2-dichloroethane, IPE, lead, naphthalene, 1,2,4-trimethylbenzene and 1,3,5- trimethylbenzene in concentrations exceeding the NCAC Title 15, Subchapter 2L Groundwater Quality Standards (2L). Concentrations of benzene exceeded the Gross Contamination Level (GCL) in monitoring wells MW-5 and MW-9. Concentrations of 1,2 dichloroethane exceeded the GCL in monitoring well MW-S. Page 3 of 5 August 2015 Groundwater Monitoring Report Former Bennett and Bailey Store September 9, 2015 The sample collected from water supply well WW-1 contained lead above the 2L and MTBE below the 2L. Historically this well has intermittently contained lead which is not associated with the release. 6 Remediation System Operation The monthly O&M visits involve a check of the applied vacuum on the SVE wells and the components of the treatment system. Filters are checked and changed if needed. The pump and treat and SVE are operating normally. Bimonthly O&M visits have reduced the algae buildup in both recovery wells and increased the amount of water removed. The air sparging component is not in operation and will require blower replacement. BGEC has informed the DENR UST Section that the sparging system is not operating. We do not recommend that the sparging system be activated because in our opinion the operation of the air sparging system may enhance plume migration. The UST Section agrees with this opinion and recommendation. In addition to the remediation system, a PetrobailerTM (passive skimmer) is utilized in monitoring well MW-5 to recover free product. A trace amount of free product was present in the PetrobailerTm situated in monitoring well MW-5. Monitoring well MW-5 has contained free product intermittently since 1999. A mobile Multi-Phase Extraction (MMPE) event was performed on MW-5 in December 2008. 7 Influent and Effluent Sampling Influent and effluent samples were collected during the August 2015 sampling event. The effluent sample was submitted to Pace to be analyzed for halogenated and aromatic volatile organic compounds using EPA Method 601/602, semi-volatile organic compounds using EPA Method 8270, lead using 3010 preparation and total suspended solids using standard method SM 2540D. The influent sample was analyzed for volatile organic compounds using EPA Method 602 and lead using 3010 preparation. The laboratory results are presented in Table 4. 8 Conclusions and Recommendations The vertical and horizontal extent of impact to groundwater has been largely defined. The concentrations of petroleum related compounds in groundwater have exhibited seasonal fluctuations but have generally declined since 1996. The long axis of the groundwater contaminant plume appears to be oriented northeast to southwest while the direction of groundwater flow is generally to the west. Petroleum compounds exceeding the 2L standard have migrated onto the adjacent trailer park property to the southwest. The risk classification of the incident remains high risk due to the presence of water supply wells within 1,000 feet of the source area. Four water supply wells have been identified within 250 Page 4 of 5 August 2015 Groundwater Monitoring Report Former Bennett and Bailey Store September 9, 2015 feet of the source area. One private water supply well (WW-1) used to provide potable water to the adjacent trailer park is situated less than 250 feet down-gradient from the source area. This well has intermittently contained lead. The sample collected from this well on August 6, 2015 contained lead at a concentration exceeding the 2L. On August 20, 2015, Best received the laboratory report from Pace indicating that lead in excess of the 2L was present in the August 6, 2015 sample collected from water supply well WW-I. Best immediately forwarded the Pace laboratory report to Mr. Thomas Moore of the DENR. On August 24, 2015, the DENR issued a Health Risk evaluation (HRE) that recommended that the well water should not be used at this time for drinking or cooking and that that the property owner should provide bottled water to the 2880 South Stratford Road trailer park occupants. Mr. Alden Dull initiated bottled water to delivery to the trailer park owner, Mr. Dennis Wilkinson, at 2880 South Stratford Road on August 25, 2015. Bottled water for drinking and cooking is now being provided to the occupants of the 2880 South Stratford Road trailer park by a private supplier contacted by Mr. Dull. On August 24, 2015, the DENR issued a letter that requires that alternate water be provided to the trailer park residences until four consecutive quarters of sampling the water supply well indicate that lead is no longer in excess of the State's Maximum Contaminant Level (MCL). A copy of the HRE and the letter are included in Appendix C. Based on the results of the August 2015 sampling results BGEC recommends the following: To reduce the risk classification, all water supply wells within 250 feet of the source area should be approved by the DENR Leaking Petroleum Storage Tank Cleanup Fund for abandonment. Additionally, the DENR Leaking Petroleum Storage Tank Cleanup Fund should approve connection of the trailer park to the Winston-Salem/Forsyth municipal water system which has a water main within 300 feet. Continue to provide bottled water to the trailer park occupants until four consecutive quarters of sampling the water supply well indicate that lead is no longer in excess of the State's MCL. • Complete implementation of the NTCP. . Continue quarterly groundwater monitoring at the site. Page 5 of 5 FIGURES 1• - : L Aft - - - 5 - 1 I& SITE C I LOCATION Ek -- New Frtetnir ,, -' - 0 - Reference, USGS 7,5 Minute Series SM / - 6 Dated 1950 Revised 1994 i Best Geological and Scale: Date: Figure 1 Environmental Consulting, P.A. 1" = 2,000' 9/9/15 Site Location Map Greensboro, North Carolina Former Bennett and Bailey Store 2872 South Stratford Road Winston-Salem, North Carolina Monitoring Well Recovery Well A Deep Monitoring Well • Water Supply Well Best Geological and Scale: Date: Environmental Consulting, P.A. 1" = 50 9/9/15 Greensboro, North Carolina Figure 2 Site Map Bennett and Bailey 2872 South Stratford Road Winston-Salem, North Carolina TABLES — — Ir © • — — JD — • — E • — ai rl) 00 &r N N N N N N N N N N I I I I I I L( I I V) - I II If —• • 0c ©© : N N N N N N N N N N N m NNCC E O :E — LI ZZ-ZZZN00 00 r ZNC- N ZZZZ N N r N N - - 00 . fl N — Cl z N C C 00 00 - fl I-fl — N N N NNN N - fl N 1 00 00 N C N C N 00 N 00 — © C 00 0000NNN00NC00N -N00N N N N N N N N N N N I-fl I-fl — — — — — — — — — — — — — — — — — N N N N N N N N N N N N N N N N N -- - - - - - - - - 0000000000000000000000000000000000 -- -Nr N00 Z N i) os I- Ct C b ':4 0 z x '0 0 0 •0 V C.) C) C) •0 C) I-' C) •0 0 C. C C) I-C) + 0 0 r.4 C) C) •0 C) •0 C. o c6, 0 0 0'0 20 II I- C) I- 'd C. EE rA cQ 0 .- a) = . .- E oc =c ri Dual NN N 0 uqjqduK I' lual qqdu < 9 < 9 E < < 9 cqu- Z V 7 V V 7 Z V — UJUE < < 2 < 2 2 < < 2 9 7 V Z v v Z Z v N 2 UOI o < < 2 <29 < <2 7 7 V Z V V Z Z V 0 U r-2,6 — — - I1 — V V ,r V V — 8 0 Poll — N — — 8 0 tt 0 V V V 0 V 0 V N "C 3d! N N N 0 3LLVJ — V VVV V 8 Uo11c)( 0 — — — — 8 0 d'gw N tn 00 0 0 cq unto1 N N uf' 0 V 0 V I 0 V 0 V 0 V 0 V 0 C14 8 uozun N en N N N 00 N V V V V V V "C "0 00 0 0 0 N N UOZU8 ' V V V V V o auMITUL, < < 9 < 9 9 < < 9 (R) ozuas 7 7 V Z V V 7 7 V N I _ _ — — — — — — —tn fl — IlI — 1 E 0 00 00 00 00 00 00 00 00 N 0" en — p U I * ** - r3 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 Wet No. Date Benzene (ug19 Ethylbortzene (ug() Toluene (ugfl) Xylen.s (ugm MTBE (ugfl) 6138 (ligO) WE (ug/ 1,2 DCA (ug1) Lead (ag)1) Naphthalene 09,1) MC2L Standards 1 600 600 500 20 4410.4 70 0.38 15 6 - . 3/13196 13,100 43 231 9,160 - 6,090 254 0200 '125 11940 1,130 NA NA 114 140 7117/96 10,500 1,220 5,820 0250 050 '250 1,000 126196 9,480 242 2,310 1,810 020 3.190 882 NA 100 12/3/96 8,490 '10 6,730 2,780 010 3.140 934 18 47.3 3/26/97 11,500 742 9.180 5,250 3,450 3 3,920 870 65 172 2/2199 10,800 1,200 9,000 3.100 4,500 NA 2.100 NA NA NA 10/27/99 9,560 610 3.390 2,581 3,130 '2.0 2.170 02 63 NA 1/5/00 14,900 336 1,650 1.421 1,618 '2 1,940 05 5 NA 512190 4,770 706 4,240 2,415 762 '1 '1 183 40 NA 7120)00 9,540 '1 1,680 1,520 1,630 .j 1,170 <2 38 NA 10/19/00 6,870 33 137 214 1,510 '2 1,610 '4 30.1 NA 1118191 8,750 38 141 115 1,210 '2 1,482 04 12 NA 4/18/01 11,580 347 82.8 234.3 2,388 < 2,680 04 12 NA 8/30101 4.680 42,8 590 187.7 1.630 02 1,330 380 99 81.5 11/27)01 5,820 35 111 48 1,690 '2 2,290 294 42 187 2(14/02 1 ,230 2,690 334 1.049 697 NA 413 NA 11 NA 4/15/02 1 470 , 522 3,060 2,846 848 NA 438 NA 7 NA 8)8)02 2,140,0 94.5 89.7 213 1,530 00.5 1,060 05 o5 44.5 11/13192 985 1,050 1.230 4,358 303 NA 231 1 NA 0 98 2/11103 2,320 146 715 1,402 1,350 NA 766 NA 11 NA 5/22103 3,000 2,070 1,110 4,384 3,360 NA 1,830 NA 12.1 83 8/26193 2,550 446 217 929 5,450 NA 1,400 NA 30.6 46 12/1103 2,800 250 '100 1,400 2,500 '100 1.000 0100 200 52 MW-2 3111 3M 67.500 3,600 33,400 21,700 040.000 <250 010.000 8.350 NA 452 7/17/96 FP FP PP PP PP FP FP PP PP FP 7126106 PP FP FP PP FP FP FP FP FP PP 12/3/96 PP Pp FP FP PP FP FP PP FP FP 3(28/97 10,400 10,800 30,300 69.000 1,490 <500 1 2,700 <500 40 349 20/99 PP FP FP FP PP FP FP PP FP FP throiaih 850101 PP FP FP FP FP PP PP PP PP FP 11/27101 51500 1,240 8,828 13,680 971 68 1.630 476 115 532 2/14102 NS NS NS NO NS NS NS NO NS NO 4115102 7,500 1,010 7,050 12,510 1,060 NA 1,610 NA 123 NA 8/8/02 4.790 1 443 3,230 5.180 05 36.8 720 690 39.9 NA 11113102 2,830 458 4,590 7.030 112 NA 597 NA 41.4 NA 2/11)03 1,570 357 3.510 3.770 1 71.7 NA 423 NA 182 NA 5/22)03 3,000 2,070 1,110 4,584 3,360 NA 1,530 NA 12.1 83 8/28/03 2,550 446 211 929 5,410 NA 1,400 NA 30.6 46 522M 3,000 2070, 1.110 4,884 3,360 NA 1,830 NA 12.1 83 8126103 2,550 446 217 929 5,410 NA 1400 NA 30.6 46 2/29104 1,200 410 1,900 2,300 69 "50 240 NA 30.6 46 5/2604 2,400 410 2,200 2,500 84 NA 550 '50 25.0 NA 8/26104 3,700 800 420 1,500 5,900 NA 1,900 '50 13.0 NA 2110195 770 220 780 '25 025 NA 11900 NA 25.0 NA 5/4106 1,400 1 130 1,300 1 960 120 1 NA 430 NA 17.0 NA 8(10195 1,400 320 1,700 1,500 120 NA 310 NA 15.0 NA 11127105 1,200 430 2,200 2,200 86 NA 430 NA 9.7 NA 2/26108 1,300 310 620 1,900 110 NA 330 NA 16.0 NA 5117106 3.700 370 2,300 2,500 100 NA 570 NA 72.0 NA 7120.186 1,400 380 1,100 1,000 "50 NA "50 NA 5.0 NA 11/29/06 770 280 930 910 050 NA 180 NA 15.0 NA 2/21/07 1,200 220 480 610 83 NA 200 NA 9.7 NA 5120/07 1,200 190 860 510 63 NA 240 NA 05 NA 8422107 1,600 324 910 1,270 77 NA 292 NA 12.5 NA 11/14197 1,030 206 303 781 050 NA 174 NA "5 NA 2/28198 216 26 99 114 9 NA 91 NA 8.5 NA 5/29198 184 19 16 85 9.8 1 NA 64 NA <5 31.6 8/25108 403 114 6 324 11.8 NA <5 NA "5 24.7 11,24/08 41.9 14.1 16.8 27.6 1.8 NA 14.5 NA "5 52.0 2/17109 56.2 8.0 1.9 24.5 1.7 NA 72 NA 05 13.5 5/21109 48.0 9.5 24.9 25.4 4.9 "0.5 28.4 14.4 10.9 32 8/24/09 496.0 136.0 35.6 302.0 23.7 '2.5 72.5 27.2 '5 23.1 11/21199 163 41.6 27.9 112.6 142 1,1 38.2 00.5 05 5.5 2/17/10 31 5.8 37.9 47.6 8.5 2.5 40.6 12 <5 02 5/12/10 316 67.8 180.0 330.0 30.7 3,5 121.0 44.1 "5 8.8 - 8124110 649 174.0 158.0 111 521.0 1 32.9 "2 93.9 333 5.1 44.5 Page 1 of 8 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 Well No. 04ee B.nzsn. (ugfll Ethylbenzene (u9) Toluen. (L91)1 Xylenss (18//l) I 8/796(1190) I 6DB (ugh) WE (ugfl) 1 1,2 DCA (ugh) I Lead (ugh) Phthal.ne NO '4C2L Stinditds 1 1 600 1 600 1 500 1 20 1 4x10-4 1 70 1 0.36 I 15 6 MW-2 I 1169110 696 1 394.0 1,360.0 1,839.0 346 1 "2.5 99.2 49.1 6.5 77.0 2/17/11 16.8 19.5 .0.5 8.5 25 "'015 10.9 6.7 .5 8.4 5/19111 169.0 35.6 77.6 93.5 7.2 1.9 45.5 21.9 22.5 62 8/25/11 874.0 241.0 607.0 1,022.0 30.4 0.92 122.0 40.7 5.3 54.8 11/10111 463.0 174.0 182.0 384.0 14.3 .2.5 49.5 14.4 52 45.4 2/9/12 312.0 105.0 5.1 122 5.0 .1.2 232 9.0 7.2 29.1 5/10/12 8780 269.0 1,390.0 1,113.0 20.3 "5 93.5 38.4 .5 83.5 8/17/12 639.0 199.0 736.0 603.0 16.5 .5 61.3 23.9 "5 64.0 11/9/12 1,060.0 263.0 1,830.0 1,103.0 25.9 .25 107.0 34.2 "5 74.8 2/27/13 400.0 164.0 127.0 410.0 6.0 "2 26.4 8.3 6.4 56.9 5/9/13 476.0 153.0 125.0 365.0 9.3 2.0 44.8 16.2 19.5 532 917113 582.0 204.0 699.0 695.0 135 "2.5 62.3 24.9 8.7 70.0 11/16113 1,360.0 371.0 2,420.0 1,660.0 33.1 .25 144.0 41.2 18.4 105.0 2/17114 988.0 227.0 795.0 810.0 18.5 .2.5 95.8 24.3 36.5 60.3 5/13/14 1,120.0 227.0 1,090.0 845.0 25.6 .5 122.0 42.6 60.3 62.5 8/13114 1,460.0 491.0 2,610.0 2,278.0 365 .5 183.0 28.6 33.7 125.0 1118114 1,510.0 555.0 3,310.0 2,680.0 33.6 "12.5 152.0 23.7 20.4 129.0 2/10/15 625.0 237.0 460.0 849.0 8.4 .2.5 40.9 12.6 19.7 70.9 5/21115 1,110.0 289.0 1,030.0 1,053.0 22.1 "2.5 106.0 49.4 92 74.9 8/8/15 1,030.0 217.0 528.0 7790 19.4 "5 100.0 30.6 11.0 52.2 MW-3 2/13186 .0.5 .1.0 .1.0 1.0 NS NS NS NS NS NS 7/17/96 "1.0 .1.0 "1.0 .1.0 1 .1.0 .1.0 1.0 "1.0 NA .5.0 7126/96 .1.0 1.0 .1.0 .1.0 12.8 "1.0 .1.0 .1.0 NA "5.0 12/3/96 4.31 1.0 3.19 .1.0 772 "1.0 "1.0 .1.0 65 u5.0 3/26/97 1.86 "1.0 2.1 3.3 222 .1.0 10.3 .1.0 41 .2.0 2/2/99 21 .5 .5 u15 57 NA 46 NA NA NA 10/37189 420 .5 "5 80 120 u2.0 472 .2.0 19 NA 115100 .1 .5 .5 <15 41.3 .2 .10 uS 10 NA 5/2/00 uI .1 1.96 3 5.9 1 "1 "2 .5 NA 7/20/00 1.17 .1 .1 3 13.6 .1 6.38 "2 "5 NA 10/19/00 ui 45 .15 "5 "2 10 .4 "5 NA 1/19101 1 45 15 .5 .2 10 4 .5 NA 4/18.01 1.69 .5 .15 6.54 .2 .10 .4 "5 NA 8/30/01 41 .5 15 .5 .2 "10 .4 .5 NA 11/27/01 .1 .5 '115 "5 .2 10 '14 .5 '20 2114102 NS HNS NS NS NS NS NS NS NS NS thro50h 11/27/02 NS NS NS NS NS NS NS NS NS 2/11903 1 5 .15 5 NA .5 NA .5 NA 5/22903 NS NS NS AS NE NS NS NS NS - 8/36/03 .1 .5 45 '(15 .5 NA .5 NA '5 "20 MW_ 7126186 '11.0 1.0 '11.0 .1.0 '1.0 .1.0 '11.0 .1.0 67 5.0 12131/96 '11.0 '11.0 .1.0 '11.0 .1.0 '11.0 '11.0 .1.0 26 .5.0 3126/97 .1.0 .1.0 "1.0 .1.0 '11.0 '11.0 .1.0 '11.0 40 .2.0 2/2/99 .1 uS .5 '115 .5 NA .10 NA NA NA 10/27/99 .1 .5 .5 .15 45 .2.0 .10 .2.0 74 NA 195100 NS NS NS NE NE NS NS NS NE NS through 4118101 NS NS NS NS NS NE NS NE NS NS 8(30191 <1 .5 56 .15 "5 .2 '10 "4 NA NA 11/27101 NS NS NS NS NS NS NE NS NS NS throi/0h 8/16/03 NS NS NE NE NS NE NS NS NS MW-S 7126996 2,150 2,860 2,50 9,560 .50 9,000 4,730 28.4 199 12/3/96 29,000 2,180 29,000 12,500 .100 I 10,800 545 196 166 3126/97 24.200 2.670 26.700 144.200 .200 11.400 3,940 166 145 2/2/99 FP FP PP FP FP PP PP PP FP llwo,u,h 4118901 FP PP FP PP PP FP PP FP FP 8/30101 lot91e-a99!ow for sampli,a 11/27901 13,600 1,730 18.500 6,570 782 1,600 8,230 2,970 94 2,518 2114/02 NS NS NE NE NS NS NS NE NS NS 4/15/02 6,540 262 7,960 14,630 474 NA 6,240 NA 269 NA 8002 4,360 641 6,940 17,820 uS 010 537 3,810 "5 503 11/13102 2,110 .5 2,310 13,380 254 NA 3,160 NA 193 NA 2/11/03 978 435 10,200 11,410 483 NA 6,700 NA 62 NA 5/22103 LPH LPH LPH LPH LPH LPH LPH LPH LPH LPH 8/26603 LPH LPH LPH LPH LPH LPN LPH LPN I.PH LPH 2/29604 LPH LPH LPH LPN LPH LPH LPH LPH LPH LPH 5/26604 LPH LPH LPH LPH LPH LPH LPN LPH l.PH LPH 8125104 10,000 1,700 21,000 18,000 .200 NA 4,100 NA <5 NA 2110/05 LPK LPH LPH LPH LPH LPH LPH LPH LPH l.PH 5/4/05 17,000 '11000 25,000 14,000 1000 NA 4,600 NA 22 NA 6/10105 LPH LPH LPH LPH LPH LPK LPH LPN LPH LPH 11/27105 11,000 1,200 22,000 17,000 1 .1,000 NA 3,700 NA 24 NA 2/26106 13,000 1,100 21.00 17,000 "50 NA 3,600 NA 30 NA 5(17/06 17,000 1,400 25,000 18.000 "50 NA 570 NA 110 NA 7120/06 LPH LPH LPH LPH LPH LPH LPH LPH LPH LPN 11/29106 16,000 1,500 24,000 11,000 "500 NA 3,200 NA 21 NA 2/21107 15.000 1,400 24,000 10,000 .500 NA 3,300 NA 18 NA - 5/30607 16.000 1 1,500 1 24.000 7.900 "500 NA1 3.400 NA 15 NA Page 2 of 8 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 Well No. I Date I Benzsn. (LOM 921yb.nan. Tokien. (ugh) Xyl.ut.s (ugh) I MIBE (ugM I EDO (ugh) I IPE (ugh) 1 1,2 DCA(ugh) Lead NO NaphthaIsuts (ugl IC2LS 6.n4ards 1 600 600 500 20 4x10-4 10 0.38 1 15 6 0-5 8122/07 14,800 1.410 24,400 13.300 <500 NA 2,640 NA 13 NA 11/14/07 LPH l.PH LPH LPN LPH LPN LPH LPH LPH LPH 2i28/88 12,600 1,100 20.800 8,610 <5630 NA 3,140 NA 26 NA Sf29108 14,900 748 22,400 16,700 .500 NA 3430 NA 11 .1000 8/25/08 LPH LPH LPN LPN LPH LPH LPH LPH LPH LPH 11)24/08 LPH LPH LPN LPH LPH LPN LPH LPH LPH LPH 2117/09 15,800 0 1,530 22,060 20,600 .500 NA 2.898 NA 50 1,810 5/21/09 14,000 859 22,860 10,200 .100 1,540 2,406 -908 26 636 8124109 14,100 1,790 24,000 16,000 .200 1,300 2.110 999 16 3,020 11/21/89 10.000 1,310 21,000 16,360 .100 1,390 1 1.700 $19 36 465 2/17/10 10,500 444 15,000 1 13,960 '50 1,340 1,900 597 601 404 - 5/12/10 13,100 620 15,300 13,420 .50 1,290 1,860 131 124.0 380 6/24/10 10,400 693 17,700 11,620 .100 919 1,520 642 1710 4400 1119110 15,200 966 24.600 15,390 .100 468 2,150 1,350 150.0 <400 2117/11 11,100 1,080 15,400 18,180 .50 687 1,710 645 90.3 787 5119111 13,000 2,450 28,600 24,800 <50 1,5,0 _ 1,780 779 17.8 1.450 8125111 FP PP FP PP FP PP FP FP FP PP 11/10/11 13,100 1,040 23,200 20,000 .100 938 1,480 443 46.6 1,140 2/9/12 9,530 855 - 18,400 ,g61O 69,600 79.900 15,550 22,980 28,120 16,480 14,650 14,52 13,820 .100 945 1,110 403 117.0 457 5/10112 13,900 3,73 -38,500 28,700 20,100 12,600 -- 19,600 17,800 19,700 10,900 15,400 18,400_ 22,800 - __15,000 17,760 <100 1,390 1,330 4100 76.0 3,400 8117/12 14, 3,970 .100 1,240 1,250 <100 1230 3,480 1119/12 2/27113 -- 10,400 8,540 -- 10,80_ 9,310 007 934 639 605 767 427 489 679 1,380 976 547 - .100 755 1,200 513 55.4 483 .100 756 1,160 398 45.4 834 5/9/13 8/7113 .50 1,030 1,330 498 80.6 986 .100 792 1,300 637 87.9 <400 11116/13 10,800 .100 470 1,260 715 46.4 <400 2117114 7,950 .50 819 1,110 390 140 434 5/13114 9,070 - .50 1_ 1,170 411 9.0 390 8/13/14 11,400 16,200 7,120 2,0 - 14.590 .50 289 2.330 1 1,110 45.5 443 1118/14 2110115 23.320 .82.5 343 2,870 1,170 16.3 573 20,460 .100 <100 1,206 433 592 1,210 5/21115 13,880 .62.5 721 1,310 516 115 410 - 8015 10.800 836 16.800 24,580 <62.5 415 1.570 621 26.6 886 MW-6 7126196 594 105 911 1.390 5,140 <20 7,780 .20 - 24.7 <5.0 1212/86 581 91 225 790 9,110 .10 3.380 <10 19 17,610.0 3(26/97 1,410 12.2 658 423 16,800 <1.0 5,930 5.23 43 <2.0 2)269 71 42 10 89 150 I NA 310 NA NA NA 10127199 73.8 85 <5 10 622 1 <2.0 245 .2.0 8 NA 1/5/00 890 138 1,170 403 464 1 "2 625 '5 14 NA 5/2/00 280 40.3 280 299 527 <1 .1 2.21 6 I NA 7/20/00 15.4 41 94.8 132.6 76.1 1.20 986 .2 20 NA 10119/90 .1 .5 <5 <15 6.58 <2 .10 <4 25.4 NA 1118101 <1 <5 <5 .15 .5 <2 .10 <4 8 NA 4/18/01 13.3 8.92 8.79 39.4 1,510 .2 1.850 -4 117 NA 8/30/01 <1 .5 .5 .15 149 <2 .10 <4 202 NA 11/27/01 1 .5 .5 .15 9.21 <2 .10 -'4 17 <20 2/14/02 .1 .5 .5 <15 30 NA 24.7 NA 8 NA 4/14102 .1 .5 .5 <15 42.3 NA .10 NA 12 NA 8/8/02 0.94 0.65 2.59 361 .0.5 <0.5 <10 <5 106 .0.5 11113/02 1.27 .5 .5 9 10 NA <10 NA .5 <20 2/11/83 <1 <5 .5 8.9 45.6 NA 35.8 NA <5 NA 5/32103 .1 .5 .5 .15 852 NA 38.3 NA 8.8 <20 8/16/03 <1 <5 <5 <15 61.8 NA 17.0 NA 29.4 <20 11/30/03 uI <1 <1 .1 <1 .1 6.0 NA 14.0 .0.50 - 2/29/04 <1 .1 .1 <1 46.0 <50 21 .1 7.2 NA MW-i 7/26/06 .1.0 <1.0 .1.0 <1.0 23.3 <1.0 .1.0 <1.0 31 <1.0 12113/06 <1.0 <1.0 <1.0 <10 236 .1.0 .1.0 .1.0 26 <5.0 3/26/07 .1.0 41.0 .1.0 <1.0 31.4 <1.0 <10 .1.0 22 .2.0 22199 <1 .5 .5 - .5 NO NO <5 NS <5 <15 - <15 MS NO <15 NO NO .15 .5 NA .10 NA NA NA 10127199 .1 .5 .5 <5.0 <2.0 .10 61 NA - 1/5/00 NS NO NS NS NO NS NO NO throenh NO .5 N NS _______ 8/8/02 NS NS NO NS NS NO NO 11113/82 <1 .5 NA <10 NA 32.7 NA 2/11/03 NS NO NO NO NO NO NO 5/22/03 NO NS NS NS NO NS NO - 8/26/03 <1 <5 1 .5 NA .10 NA 182 <20 MW-6 12/3/96 11,300 3,250 21,300 14,800 .10 10.8 1430 838 93 152 3126197 FP FP FP FP FP FP PP PP PP PP lhrouah 2114 NO NO NO NO NO NO NO NO NO NO 4/15/02 10,308 2,170 13,100 11,250 2,630 NA 1.840 NA 68 NA 8/8/02 9,350 <5 17,000 15,140 <5 45 929 232 37.1 322 11113/82 331 334 1.730 5,860 465 NA 637 NA 134 NA 2/11103 1,140 315 12.3 1,442 356 NA 425 NA 200 NA 5/22103 NO NO NS NO NO NO NO NO NO NO 8/26103 2,490 617 4,470 4,410 .5 NA 438 NA 111 30 2)29/04 3,880 700 11,80() 6,700 .500 NA <500 .500 140 170 MW.9 12/3/96 11,700 1,310 5,190 - 5,430 <10 <10 3,090 .10 49 125 3126/97 jO,4O0 7,200 5,110 .1.0 .10 2,800 155 61 170 - 212/99 7,600 850 1 3.200 1 2.900 1 .5 1 NA 1100 NA NA NA Page 3 of 8 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 Well No. Date I 1 .nz.u. (ugIl I EthyLeazan. (ug/ ToIu.ne (ugll) I Xyl.n.. (agO)' I MTBE (agO) EDB (<gil) IPE (agO) 1 1,2 WA (ag/I) Lead (ugO) NPhIhS,Ie (ugO) NC2LS0/-Iards I 1 600 1 600 I 500 1 20 1 4xl0-4 1 70 1 0.35 1 15 6 MW-9 10127199 NS NO NO NS NS NS NS NO MS 1/5100 770 1,420 2,M .5 <2 1,310 <5 21 NA 512100 524 1,730 1,017 .1 .1 .1 .2 15 NA 111111 7120/00 .1 1,460 1.814 933 .1 <1 2.59 10 NA 10/19/00 X3930 553 1,160 1,624 "5 <2 1.120 <4 13.6 NA 1/18/01 587 594 1,799 <5 <2 689 <4 12 NA 4/18/01 530 1,550 1,552 752 .2 1,310 <4 22 NA 8/30/01 278 1.240 902 50.7 <2 859 <4 39 <20 11127101 24.4 123 151.5 111 .2 693 7.03 33 <20 2/14/02 11.3 16.6 17.33 38.4 NA 182 NA 10 NA 4115)02 973 99.6 127 1352 154 NA 355 NA <5 NA 8/8102 273 30.5 19.3 55.1 .0.5 <0.5 - 130 <5 3 4.56 11113/02 6.53 .5 .5 .15 <5 NA "10 NA 5.1 .20 2111/03 76.5 5.49 .5 <15 5.44 NA 26.4 NA 6.8 <20 5/22/03 1,050 42.8 32.1 315 .5 NA 99.9 NA <5 .20 8/26/03 716 78.4 7.04 36.97 <5 NA 122 NA 16.7 <20 11/30/03 970 99 140 5,800 .50 .50 250 .1 8.5 3.4 229104 210 41 8.4 36 .5 NA 62 <1 11 NA 5/30/04 720 100 <50 <1 .50 NA 1190 NA 7.1 NA 825104 1,490 160 57 190 .50 NA 300 <1 14 NA 2110/05 620 88 30 160 .20 NA <20 NA 33 NA SM/OS 660 78 31 110 <20 NA 210 NA 8 4 8/10/05 920 100 27 180 .20 NA 200 NA 19 6 11/27/05 1,100 88 <20 180 <20 NA 330 NA 13 4 2/26/06 430 30 <20 51 <20 NA 120 NA 17 <0.52 5/17/06 1,700 210 120 120 <20 NA 440 NA 95 11.9 7/20/06 1,700 200 110 330 <50 NA .50 NA 5 14.4 11129106 900 61 .50 110 <50 1 NA 220 NA 16 1.5 2121/07 400 25 40 45 <10 NA 100 NA 7.9 6.4 5/30/07 1,600 180 300 490 <10 NA 340 NA 11.0 27.9 8/07 3,910 408 1,010 1 444 <10 NA 823 5.4 26.7 11/14107 2,120 175 436 241 .10 NA 605 .5 5.3 2/28/08 869 56 91 .100 .50 NA 173 19.0 .1.9 5/39/08 35.2 3 4 5 <1 NA 7.7 22.6 7.9 8125/08 1,7506 158 500 350 .1 NA 427.0 UNA <5 10.1 11/24/08 1,270.0 101 126 170 .1 NA 275.0 21.7 <10.5 2/17/09 390.0 <50 .50 <100 .50 NA <50 18.4 <1.5 339.0 41 114 49 .1 <1 63.4 173 7.9 2,670.0 273 977 711 .10 <10 351.0 22.5 54.6 11/21109 1,470.0 192.0 536.0 462.0 <10 <10 188.0 <10 18.5 .40 2/17/10 2,370.0 381.0 1,580.0 869.0 .10 <10 312.0 <10 26.6 21.1 5/12/10 3,740.0 587.0 2,490.0 2,109.0 .0.5 <0.5 484.0 .0.5 12.3 115.0 8/24110 4,390.0 472.0 2,360.0 1,821.0 <12.5 <12.5 602.0 <12.5 40.7 783 1119/10 4,520.0 487.0 1,800.0 1,631.0 <20 .20 506.0 .20 21.7 12.9 2117/11 3,750.0 375.0 2,060.0 1,294.0 <0.5 4.5 390.0 <0.5 28.7 60.5 5/19111 4,770.0 694.0 2,980.0 1,780.0 .12.5 412.5 695.0 412.5 28.1 127.0 8/35/11 3,410.0 3610 1,0506 1,4566 .20 0.9 439.0 40.7 29.7 394 11/10/11 4,090.0 411.0 1,770.0 1,402.0 <12.5 <12.5 533.0 <12.5 34.3 142.0 2/9/12 3,160.0 382.0 1,840.0 1,198.0 .10 .10 359.0 .10 17.2 80.7 5110112 5,100.0 605.0 3,4006 2,349.0 .20 <20 603.0 <20 142 86.9 8117/12 6,930.0 749.0 4,160.0 2,127.0 .25 .25 751.0 .25 15.4 123.0 1119/12 3,650.0 447.0 3,160.0 1,562.0 <25 .25 399.0 .25 12.1 66.3 227113 166.0 39.5 152.0 100.1 <0.5 .0.5 17.3 .0.5 17.1 6.9 5013 2,060.0 332.0 1,820.0 857.0 40.5 .0.5 192.0 .0.5 20,1 41.0 8/7/13 3,540.0 584.0 3,110.0 2,112.0 <10 .10 388.0 .10 174 33.1 11/16/13 4,190.0 662.0 3,230.0 2,273.0 4125 .125 394.0 .12.5 12.5 101.0 2117/14 913.0 132.0 901.0 469.0 <2.5 .2.5 82.9 .2.5 16.6 172 5113114 5,210.0 655.0 5,560.0 2,781.0 .5 .5 440.0 .5 18.8 124.0 8/13114 3.9706 509.0 4,300.0 2,235.0 .25 <25 466.0 <25 14.3 40.0 11/8/14 3,800.0 512.0 3,170.0 1,930.0 .12.5 <12.5 493.0 <12.5 16.0 82.1 2/10/15 1,960.0 260.0 1,570.0 841.0 .12.5 <12.5 217.0 .12.5 22.4 .10 5/21/15 3,920.0 686.0 5,500.0 2,762.0 .10 .10 401.0 .10 18.2 104.0 8/6/15 6,170.0 772.0 5,710.0 2,877.0 .25 .25 764.0 .25 15.1 103.0 MW-b 12/03/96 <1.0 <1.0 .1.0 .1.0 .1.0 <1.0 .1.0 .1.0 43 45.0 3/26/97 .1.0 .1.0 .1.0 <1.0 .1.0 .1.0 <1.0 NO 55 <2.0 2/2/99 1.8 <5 .5 .15 <5 NA .10 NA NA NA 10127109 NS NO NO NO NS NS NO NS NO NO through 4/18101 NO NO NO NO NO NO NS NS NO NO 8120101 '11$ (well was d-y) - NO NS NO NO NO NO NO NS through "IS (well was dry) NO NO NO NO NO NO NO NO 2115/02 '(S (well was /I -NO NO NS NS NO NS NO NO 4/15/02 <1 <5 .5 <15 <5 NA .10 NA <5 NA 8(8/02 NO NO NO NO NO NS NO NO NS NO lhrouh 5122103 NO NO NO NS NO I NO NO NO NS NS 8/26,2003 .1 .5 <5 <15 .5 NA .10 NA 39.7 .20 2/29/2004 I .1 .1 .1 .1 .1 NA <1 .1 24 NA _MWi1_ 12/3(86 .1.0 .1.0 <1.0 .1.0 .1.0 .1.0 .1.0 <1.0 15 <5.0 3/26/97 .1.0 .1 .0 <1.0 .1 .0 .1.0 .1.0 <1.0 <2.0 .5 <5 <15 .5 NA .10 NA NA NA Page 4 of 8 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 WeU No. Date Benzene (ug4) Ethylbenzene (ug/1) Toluene (ugfl) Xylenes (ugh) MTBE (ugh) EDB (ugh) IPE (ugil) 1 1.2 DCA (ugh' I Lead (ugh) NapMhakn. NO tIC2LStards 1 600 600 500 20 4x10-4 70 1 0.38 1 15 6 MW-1 1 10127199 ]ABANDONED MW-12 512100 2.31 .1 20 25.45 443 .1 .1 02 6 NA 7120100 l .1 .1 .3 - .1 .1 .1 .2 14 NA 10/19/00 .1 .5 .5 .15 .5 .2 .10 .4 212 NA 1/18101 el .5 .5 .15 .5 .2 .10 .4 10 NA 4/18/01 129 .5 .5 .15 .5 .2 .10 .4 30 NA 8120101 .1 .5 .5 .15 .5 .2 .10 04 5 .20 11/27101 .1 .5 .5 .15 .5 .2 .10 .4 42 .20 2114102 .1 .5 .5 .15 .5 NA .10 NA 13 NA 4/15102 .1 .5 .5 .15 .5 NA .10 NA 19 NA 8/8/02 1.71 123 524 7.63 .5 .0.5 .10 .5 13.6 3.5 11113/02 .1 .5 .5 .15 .5 NA .10 NA 9.5 .20 2111103 .1 .5 .5 .15 .5 NA .10 NA 5.9 .20 5003 .1 .5 .5 015 .5 NA 010 NA .5 .20 8/29103 .1 .5 .5 .15 .5 NA .10 NA 10.9 .20 12/1/03 .1 .1 .1 .1 .1 .1 .1 .1 5.5 020 5/9/13 .0.5 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 40.6 .2 811/13 .0.5 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 19.4 - .2 1111613 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 29 .2 2/17/14 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 16.3 .2 5/13114 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 92 .2 8/12/14 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 52.6 .2 11/8/14 .0.5 L<0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 40.5 .2 2/10/15 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 32.4 .2 5/21/15 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 .5 .2 819115 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 21.4 .2 MW-13 9118191 .1 .5 .5 .15 11.8 .2 .10 .4 25 NA 11/27/01 .1 .5 .5 .15 29.7 .2 1 .10 .4 6 .20 2/14/02 .1 .5 .5 .15 14 NA .10 NA uS NA 4/15/02 .1 .5 .5 .15 13.4 NA .10 NA 14 NA 8/8/02 .1 .5 <5 .15 28.8 .0.5 4.16 .5 14 .0.5 11/131V2 .1 3 .5 .15 11.4 NA .10 NA .5 .38 2/11103 .1 .5 e5 .15 .5 NA .10 NA 5.7 .20 5/22103 - - .1 uS .5 .15 12.7 NA .10 NA 16.2 .20 11130/03 .1 .1 .1 .1 2 NA .1 .1 13 .0.50 2/29/04 .1 0 uI .1 12 NA 2.8 .1 5.9 .0.51 5,26/04 uI 0 .1 - .1 4.4 NA .1 .1 11 .0.50 8f25104 .1 - .1 .1 .1 9.6 NA 1.4 .1 .5 .0.51 _2/10/05 .1 .1 .1 .1 8.0 NA 1.6 NA 72 .0.50 5/4/05 .1 - .1 .1 .1 82 NA 1.7 NA .5 .0.51 8110/05 - .1 - .1 .1 .1 .1 NA .1 NA 6.8 .0.51 11/27/05 .1 .1 .1 .1 .1 NA ui NA .5 .0.50 226/06 .i <1 uI 0 5.0 NA .1 NA 7.7 .0.51 9117106 .1 .1 .1 .1 uI NA ui NA 32 .0.50 7120106 uI .1 .1 .1 1.1 NA .1 NA .5 .0.51 11/29106 .1 .1 .1 .1 2.1 NA ui NA 6.9 .0.50 2421197 .1 uI uI .1 .1 NA 0 NA .5 .0.50 540197 .1 uI .1 .1 22 NA .1 NA .5 .0.50 8/22/07 .1 .1 .1 .1 1.4 NA .1 NA .5 34.9 11/14107 .1 .1 0 .1 8.9 NA .1 NA .5 .1.5 2128198 .1 .1 .1 .1 .1 NA .1 NA .5 .1.5 5/29/08 .1 .1 .1 0 .1 NA .1 NA .5 .1.5 825198 .1 .1 .1 0 4.9 NA .1 NA 8.3 01.5 11/24108 .1 'I .1 .3 22 NA .1 NA .5 .106 2/17109 .1 ui uI .2 .1 NA .1 NA 7.6 .1.5 5/21/09 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 96 .2 8124/09 .0.5 .0.5 .0.5 .1 0.54 .0.5 .0.5 .0.5 12 .2 110109 .0.5 .0.5 .0.5 .1.5 1.1 .0.5 .0.5 .0.5 62 .2 2/17110 .0.5 .0.5 .0.5 .2 .0.5 .0.5 1 .0.5 .0.5 12.3 .2 5/12/10 .0.5 .0.5 .0.5 .1.5 1.3 .0.5 .0.5 .0.5 12.4 .2 8(24/10 .0.5 .0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 223 .12.5 11/9/10 .0.5 .0.5 .0.5 .1.5 1.4 .0.5 .0.5 .0.5 12.9 .11.9 2117/11 .0.5 .0.5 .0.5 .1 4.5 .0.5 .0.5 .0.5 .5 .2 5/18111 .0.5 .0.5 .0.5 ui .0.5 .0.5 .0.5 .0.5 uS .2 8/25111 .0.5 .0.5 .0.5 .1 .05 .0.5 .0.5 .0.5 12.3 .2 11/10/11 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 18.9 .2 2/9/12 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 8.6 .2 5/10/12 .0.5 .0.5 .0.5 .1 .0.5 00.5 .0.5 .0.5 16.3 .2 8/17/12 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 16.4 .2 11/9/12 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 11.0 .2 2/27113 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 72 .2 5/9/13 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 9.0 .2 8/7113 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 .5 .2 11/16113 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 5.1 .2 2/17/14 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 11.8 '2 5/13/14 .0.5 .0.5 .6.5 .1 .0.5 .0.5 .0.5 .0.5 112 .2 8/13/14 .0.5 .0.5 4.5 .1 4.5 .0.5 .0.5 .0.5 12.6 .2 11/8/14 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 136 .2 2/10/15 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 13.3 .2 5/21115 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 .5 .2 - 818/15 .0.5 .0.5 .0.5 ui .0.5 .0.5 .0.5 .0.5 .5 .2 MW-14 2/14/02 .1 .5 .5 .15 .5 NA .10 NA 7 NA 4/15/02 .1 .5 .5 .15 .5 NA .10 NA uS NA 8/8/02 .1 .5 0.53 4.72 .5 .0.5 .10 uS 6.1 .0.5 11/13/02 .1 .5 .5 .15 uS NA .10 NA 56 .20 2/11/03 .1 uS .5 .15 .5 NA .10 NA 8 .20 8122/03 .1 .5 15 .15 .5 NA .10 NA 18.7 .20 8/28103 .1 .5 .5 .15 .5 NA .10 NA 22 020 - 11/30/03 .1 .1 .1 .1 .1 .1 - .1 .1 97 1 .0.50 Page 5 of 8 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 WoO No. Date I I B.nzaiie (ugl) Ethyt.nz.n. (ug,1) Toloen. (ugl) I Xylenss (ug/ I 167818 (ugO) 8DB (uglU IPE (ug/ 1,2 DCA (ugil) Lead (ug/ NaPMhsna (ug/ NC21 Sbndards 1 1 600 1 600 1 500 1 20 1 4x104 1 70 1 0.38 11 15 6 MW-14 2129104 .1 "1 .1 .1 .1 "1 .1 5.8 .0.51 5/26/04 .1 '1 '1 .1 "1 .1 .1 "1 14 .0.50 Sf25104 "1 .1 "1 "1 "1 1 .1 .1 5.3 '0.50 2/10105 "1 "1 '1 ol .1 .1 "1 '/1 .5 .0.50 514105 .1 .1 .1 '1 '1 ol .1 .1 .5 "0.50 8110195 "1 .1 .1 .1 .1 .1 "1 '/1 8.3 .0.50 11/27/05 1 "1 "1 01 1 NA .1 NA "5 '0.53 2126196 .1 .1 .1 .1 1.2 NA 1 NA 5 '0.50 5/17/06 "1 .1 .1 .1 "1 - NA .1 NA 49 '0.50 7120196 01 .1 "1 <1 .1 NA .1 NA "5 00.50 11126106 .1 .1 .1 .1 "1 NA <1 NA .5 '0.50 2121107 .1 .1 .1 .1 .1 NA <1 NA .5 '0.50 5/20107 .1 "1 .i <1 .1 NA .1 NA .5 '0.50 8/22107 '1 "1 "1 .1 "1 NA .1 NA .5 .0.50 11114107 "1 <1 "1 .1 .1 NA .1 NA o5 01.50 2/28108 .1 .1 .1 .1 .1 NA .1 NA o5 "1.50 5129108 .1 .1 .1 - .1 .1 NA I NA o5 01.5 8/25108 .1 .1 .1 .1 '2 NA .1 NA 6.3 01.5 11124108 "1 .1 .1 .3 .2 NA .1 NA 05 11.1 2/17109 .1 1 ol "3 '2 NA .1 NA .5 01.5 5121109 00.5 .0.5 "0.5 1 "0.5 00.5 00.5 00.5 .5 "2 8124109 00.5 "0.5 "0.5 .1 .0.5 .0.5 .0.5 4.5 .5 "2 11121109 "0.5 00.5 00.5 01.5 00.5 '0.5 00.5 "0.5 10.5 .2 2/17/10 "0.5 "0.5 "0.5 '2 "0.5 '05 '0.5 00.5 86 02 5/12/10 "0.5 .0.5 "0.5 0.5 "0.5 .0.5 .05 .0.5 10.8 '2 8/24110 00.5 "0.5 "0.5 "1.5 .0.5 4.5 00.5 "0.5 16.7 011.9 1119/10 .0.5 00.5 .0.5 01.5 00.5 00.5 00.5 .0.5 0.4 "106 2/17/11 .0.5 .0.5 "0.5 "1 00.5 00.5 00.5 00.5 .5 "2 5/19/11 .0 .5 00.5 00.5 .1 00.5 00.5 00.5 .0.5 .5 .2 8/25/11 .0. 5 00.5 00.5 "1 "0.5 00.5 00.5 00.5 8.9 11/10/11 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 .0.5 24 .2 219/12 .0.5 .0.5 .0.5 01.5 15 00.5 00.5 .0.5 .5 5110/12 "0.5 .0.5 .015 .1.5 .0.5 .0.5 .0.5 .0 .5 .5 .2 8/17112 "0.5 .0.5 12 .1.5 .0.5 .0.5 .0.5 .0.5 .5 .2 1119/12 .0 .5 .0 .5 .05 .1.5 .0.5 .0.5 .0.5 .0.5 10.4 .2 2127/13 .0.5 "0.5 .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 .5 .2 519/13 .0.5 .0.5 .0.5 -1.5 .0.5 .0.5 - .0.5 .0.5 8.6 8/7/13 .0.5 .0.5 .0.5 .1.5 00.5 "0.5 "0.5 00.5 "5 .2 11/18/13 .0.5 .0.5 .0.5 .1.5 00.5 00.5 00.5 .0.5 22.7 '2 2/17/14 00.5 .0.5 .0.5 .1.5 .0.5 "0.5 00.5 00.5 11.3 '2 5/13/14 .0.5 .0.5 00.5 01.5 00.5 .0.5 .0.5 .0.5 8.6 8/13/14 .0.5 .0.5 .0.5 .1.5 .05 .0.5 00.5 00.5 10.8 "2 1118114 .0.5 .01 00.5 .1.5 .0.5 .0.5 .0.5 .0.5 174 '2 2110/15 .0.5 "0.5 .0.5 .1.5 .015 .0.5 00.5 .0.5 18 .2 5121/15 .0.5 .0.5 00.5 .1.5 .0.5 .0.5 .0.5 .0.5 .5 - 8/5/15 4.5 .0.5 00.5 "1.5 .0.5 .0.5 .0.5 .0.5 .5 '2 MW-IS 11/03812 .1 .5 .5 .15 .5 NA "10 NA 42.4 NA 2/11103 .1 .5 .5 .15 "5 NA 010 NA 151 NA 5/22/03 "1 .5 .5 .15 05 NA "10 NA 23.4 .20 8126103 .1 .5 .5 .15 .5 NA 00 NA 23 .20 - 12/1/03 "1 .1 .1 .1 <1 ol .1 .1 13 "0.50 OCW-1 7/29186 23.4 01.0 01.0 I "1.0 .1.0 .1.0 .1.0 4.48 .10 05.0 12113/96 18.9 .1.0 01.0 01.0 .1.0 .1.0 .1.0 .1.0 .10 05.0 3126197 2.64 0.0 5.39 4.78 .1.0 01.0 .1.0 .1.0 .10 02.0 22190 21 uS .5 .15 NA .10 NA NA NA 10127109 ol .5 .5 015 "5 .2.0 10 02.0 05.0 NA 1/5)00 NS NS NS NS NS NS NS NS NA NO throuM 10/19100 NO NA NS NS NS NS NA NA NS 1/18101 1 o5 o5 .15 .5 "2 .4 .5 NA 4/18/01 NA NS NS NS NO NS NA NA NS 8/30101 .1 <5 .5 .15 058 .2 .4 7 '20 11127101 "1 .5 'uS .15 .5 "2 MN 11 43 2/14102 .1 <5 .5 .15 00 NA NA .5 NA 4/15/02 .1 .5 .5 .15 'uS NA NA .5 NA 818192 NS NS NA NA NS NA NO NS NS 11113102 22 .5 .5 015 .5 NA 010 NA 26.1 .20 2/11103 19.1 .5 .5 .15 .5 NA 11.1 NA .5 .20 5/2203 8.76 .5 .5 .15 '5 NA "10 NA 32.8 .20 8/26103 27.8 .5 .5 .15 10.3 NA 296 NA .5 .20 11/30103 <1 15 .1 .1 9.7 "1 25 15 '5 .0.50 2/29104 2600 720 2300 2400 4200 NA 1100 '1 23 NA 5126104 "1 "1 'ul .1 .1 NA .1 .1 "5 NA 8125104 11 .1 "1 "1 5 NA 4.3 .1 "5 NA 2/10195 .1 .1 .1 ol S NA 1.9 NA '5 NA 5/4/05 'ul "1 .1 1.4 NA 36 NA .5 NA 8/10/05 6.9 .1 '1 .1 7 NA 12 NA .5 NA 11/27195 11 ol .1 "l IS NA 35 NA 'us NA 2126106 'ul .1 '1 .1 'ul .1 'ul NA .5 NA .1 .1 .1 1 .1 NA 64 NA 720106 1 12 .1 .1 01 30 59 .1 I NA 'u5 NA 11/29/06 1 3.9 .1 .1 'ul 11 NA 23 1 NA 'u5 NA - 2/21107 I .1 I .1 I .1 o1 ui NA I .1 I NA .5 NA Page 6 of 8 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 Well No. 8/ I IBSflZOfle ('0/) Ethylbenzen. (.511) Toluene (ugil) I I Xylenes (ugh) I 8/TOE (UgID EDO (ugh) WE(Ugh) 1,2 DCA (.g1) Lead (ugh NulIIlIh.S (uglU liC2LStrlards 1 600 600 500 1 20 1 4x10.4 1 70 1 0.38 1 15 6 PCW-1 5/30/07 .1 82 - "1 "1 <1 "1 .1 .1 NA .1 NA '5 NA 8122107 .1 76.7 NA 139 NA "5 NA 11/14107 8.1 - 1 <1 1 779 NA 125 NA "5 NA 2/38108 '1 - 1 1 1 22.1 7.5 .1 NA .5 NA 5/28/08 .1 .1 .1 .1 <1 NA 1 NA .5 NA 8125/08 .1 .1 .1 .1 8.1 NA 10 NA '5 NA 11/24108 .1 .1 .1 .3 11.0 NA 11.7 NA '5 NA 2117/09 .1 <1 .1 .3 22.4 NA 18.1 NA '5 '1.5 5121109 '0.5 1 <0.5 "0.5 .1 1 51.7 '0.5 71.8 .05 4 .2 8124100 6.8 .0.5 "0.5 .1 98.7 '0.5 156 "0.5 .5 42 11121109 0.87 .0.5 1.5 0.85 '0.5 4.5 '0.5 "0.5 173 '2 2/17/10 '10.5 .0.5 '0.5 "1.5 '0.5 '0.5 4.5 .0.5 '5 '2 5/12/10 .0.5 .0.5 4.5 "15 '0.5 '0.5 '0.5 .0.5 8.0 .2 8124/10 .0.5 .0.5 '0.5 '1.5 '0.5 '0.5 '0.5 .0.5 8.4 "2 1119/10 0.5 .0.5 '0.5 '1.5 '0.5 .0.5 "0.5 '0.5 '5.0 '2 2/17/11 .0.5 .0.5 .0.5 <1 0.5 0.5 .0.5 '0.5 .5 .2 5119/11 4.1 "0.5 "0.5 .1 1.5 "0.5 1.9 .0.5 .5 .2 8125/11 1.2 "0.5 "0.5 .1 02 "0.5 1.0 .0.5 .5 .2 11/19/11 '0.5 .0.5 .0.5 .1 0.70 .0.5 0.77 .0.5 .5 .2 2/9/12 4.5 '0.5 .0.5 .1.5 120 .0.5 1.30 .0.5 .5 .2 5/10/12 11 0.5 "0.5 "1.5 0.84 .0.5 0.99 .0.5 5.4 '2 8/17/12 154 6.5 44.7 34.6 17.80 .0.5 1.40 .0.5 .5 9 1119112 2.6 .0.5 .0.5 .1.5 2.30 .0.5 2.40 0.80 .5 .2 2/27113 24.2 .0.5 .0.5 0.64 4.60 .0.5 5.70 2.3 .5 .2 5)9/13 114 .0.5 .0.5 .1.5 5.10 .0.5 6.10 2.5 .5 .2 8/7/13 4.8 .0.5 .0.5 .1.5 2.70 .0.5 2.90 1.7 .5 .2 11/16/13 8.6 .0.5 .0.5 .1.5 2.30 .0.5 1.80 0.86 .5 .2 2M7t14 .0.5 .0.5 .0.5 .1.5 .0.5 0.5 0.5 .0.5 5 '2 "0 .5 .0 .5 .0.5 .1.5 .0.5 0.5 .0.5 .0.5 .5 .2 4 .0.5 .0.5 .1.5 1.30 .0.5 1.00 .0.5 .5 .2 2.5 .0.5 .0.5 .1.5 1.60 .0.5 1.00 '0.5 .5 '2 Z 2MOM5 .0.5 .0.5 .0.5 1.5 0.5 .0.5 '0.5 "0.5 .5 .2 .0.5 0.5 0.5 .1.5 .0.5 .0.5 .0.5 .0.5 .5 .2 1.2 .0.5 .0.5 1.5 1.20 "0.5 2.10 0.93 .5 '2 OCW2 .1.0 1.0 1.0 "1.0 '1.0 .1.0 .1.0 .1.0 .10 5.0 3/26197 42.3 .1.0 .1.0 .1.0 172 .1.0 19.3 5.68 .10 2.53 2)2)99 NO NO NO NO NO NS NS NO NS NO 10127/99 NO NS NO NO NS NS NO NS NS NO 1/5/00 .1 '5 .5 .15 .5 .2 .10 .5 '5 NA 5/2/00 .1 "1 .1 .3 .1 .1 <1 '2 "5 NA 7120190 1.33 .1 .1 '2 <1 .1 .1 .2 35 NA 10119190 .1 .5 .5 .15 .5 .2 <10 '5 "5 NA 4/18191 .1 .5 .5 .15 .5 .2 <10 .4 .5 NA 8/30101 .1 .5 .5 .15 .5 .2 .10 4 NA .20 11/27102 .1 .5 .5 '15 .5 .2 .10 <4 5 .20 2/14/02 NS NO NS NO NO NO NO NO NO NO 4115/02 .1 .5 "5 .15 .5 NA .10 NA 5 NA 8/8/02 NO NO NO NO NS NO NO NO NO NO 11/13)02 <1 .5 .5 .15 .5 NA - .10 NA 12.1 NA 2/11/03 NO NO NO NO NO NO NO NO NS NS - 5/22103 NO NS NO NO NS NO NO NS NS NO - 8126103 .1 5 .5 .15 5 NA .10 NA .5 .20 lAW-I 1213196 .1.0 .1.0 .1.0 1.0 .1.0 .1.0 .1.0 .1.0 .10 .5.0 3/26197 .1.0 "1.0 .1.0 .1.0 '5.0 .1.0 .1.0 .1.0 26 .1.0 2)2)99 NO NO NO NS NO NO NS NS NO NO 10/27/89 .1 .5 .5 <15 "5 .5.0 .10 '2.0 .5.0 NA 119/00 <1 .5 '5 .15 .5 2 .10 .5 .5 NA 5/22100 .1 .1 1 .3 1 .1 .1 .2 5 NA 7120/00 1 .1 1 .3 .1 .1 .1 .2 5 NA 10/1030 .1 .5 .5 .15 .5 "2 .10 .4 5 NA 1/18/01 .1 .5 .5 .15 .5 '2 .10 .4 8 NA 4/18/01 1 .5 .5 .15 .5 2 .10 .4 .5 NA 8/20101 M .1 .5 .5 .15 .5 .2 10 .4 .5 .20 11121101 .1 5 .5 .15 .5 .2 10 .4 .5 '20 2/14102 .1 5 .5 15 .5 NA 10 NA .5 NA 4115102 .1 5 .5 .15 5 NA 10 NA .5 NA 8/8/02 1 '5 .5 .15 "5 .0.5 .10 '5 62 '0.5 - 11/13/02 "1 .5 .5 <15 .5 NA .10 NA 5 NA 2111103 .1 .5 .5 .15 .5 NA .10 NA .5 NA 502/03 .1 .5 .5 .15 .5 NA .10 NA .5 NA 8/26/03 .1 1 .5 "5 .15 "5 NA "10 NA .5 NA 11/30/03 <1 <1 .1 <1 <1 .1 .1 15 .0.50 2/29104 .1 <1 .1 .1 .1 .1 '1 5.8 '0.51 5/26/04 .1 .1 .1 .1 .1 '1 .1 '1 .5 "0.51 8/25/04 .1 <1 .1 <1 .1 - <1 .1 .5 .0.51 2I10105 <1 .1 .1 .1 "1 .1 "1 .1 <5 .0.55 5/4105 <1 .1 .1 .1 .1 .1 .1 .1 5 .0.50 8110105 .1 .1 "1 .1 .1 .1 .1 .1 .5 .0150 11/27105 .1 .1 "1 .1 "1 .1 "1 .1 4 .0.53 2I28/06 .1 .1 '1 .1 '1 .1 .1 .1 6.1 .0.50 - 5/17/06 <1 <1 .1 .1 .1 I <1 <1 86 0.51 Page 7 of 8 Table 3 Historical Groundwater Analytical Data Bennett and Bailey Store, Winston Salem, North Carolina Incident No 14498 Well No. I Daft I9<<S (ugh) (ugID I Toluen. (u1) XyI.n.s (UOM I UTBE (ugh) I EDB (ugh) I WE (ag/I) 1 1,2 DCA (ag/I) Load (ugh) INU (ughI) 1C2LS0 -1.rda I 1 1 600 1 600 1 600 1 20 1 4x10.4 1 70 1 0.38 15 6 WW-1 .1 .1 <1 .1 .1 .1 .1 .1 <5 .0.50 6 <1 <1 <1 .1 .1 <1 .1 <1 <1 - <1 s1 NA <1 .5 .0.50 .1 <1 .1 .1 .1 .1 .1 .5 .051 s1 <1 .1 .1 .1 .1 .1 9.3 "051 <I .1 .1 .1 .1 <1 .1 .1 15.6 .5 .0.50 NA N7lr2O= NA NA NA NA NA NA 7 <1 .1 <1 .1 <1 .1 .5 .1.5 .1 .1 .1 .1 .1 .1 .1 <1 .5 .1.5 NA NA NA NA NA NA NA NA .5 <1.5 <1 .1 .1 .1 .1 5L .1 .1 .1 - <1 <1 14.3 <1 .1 .1 0 .1.5 .1 <5 <1.5 11124108 <1 <1 .1 .3 <1 .1 - - <1 <1 .0 .5 - <0.5 <0.5 .05 -- <0.5 - ,.05 .05 <05 <05 - <0.5 - - .05 <0 5 - - .5 <1.5 2117/09 .1 .1 .1 <2 .2 NA .0 .5 .0.5 <0.5 - <05 .05 <05 <05 <05 <0 5 -<1 .0.5 .5 .1.5 5/21109 .0.5 .0.5 .0.5 .1 .0.5 .5 <2 8/24109 .0.5 .0.5 .0.5 .1 .0.5 .0.5 .0.5 - <5 .2 11)21109 .0.5 .0.5 .0.5 .1.5 .0.5 14.3 .5 <2 .10 2117110 .0.5 .0.5 .0.5 .2 .0.5 <0.5 .0,5 .0,5 <05 .0,5 .0.5 5112(10 .0.5 <0.5 <95 .15 .0.5 <5 <2 8/24110 .0.5 .05 .0.5 -- .1.5 .0.5 <5 .2 1119110 .0.5 -0.5 L .5 .0.5 <0.5 <0.5 .0,5 <0.5 .0.5 -- .1.5 - <1 <1 <1 <1 <1 <1 <1 s1 .0 .5 .0. 5 A <05 <5 5 .5 '2.0 <2 2111/11 '0.5 <0.5 5119/11 .0.5 <0.5 .0.5 .0.5 <2 8/25/11 .0.5 <0.5 11/10/11 .0.5 <0.5 <0.5 .05 .0.5 .0.5 <0.5 .0.5 <05 <0 5 4.5 .0.5 .5 .2 2/9112 .0.5 .5 <5 .2 .2 5110/12 <0.5 <0.5 .0.5 u0.5 <0.5 <0.5 .0.5 .0.5 s0.5 - -0.5 .0,5 <0.5 <05 -- - <05 <05 <05 -. <05 _<05 .......,sQ-5 .0.5 -0.5 8117/12 .0.5 1.4 .2 11012 .0.5 .0.5 <0,5 - <5 .5 - <2 .2 2027113 <03 .0.5 .0.5 .1 .0.5 <0.5 <0.5 .0.5 .0.5 .0.5 <0.5 519113 .03 <0.5 <0.5 .1 .0.5 u05 - .5 .2 817/13 .05 .0.5 .0.5 .1 .0.5 <05 - 28.6 .2 11/16/13 <05 .0.5 50.5 .1 .05 505 - .0.5 .2 2117114 .05 <0.5 .0.5 <1 0.7 <05 - 102 .2 5(13(14 .0.5 <0.5 .0.5 .1 0.86 <05 - 11 .2 8/13114 .0.5 .0.5 .0.5 .1 0.7 0.77 0.67 0.53 <05 <05 <0.5 <0.5 <0.5 .0.5 .5 .5 .2 <2 11/8/14 <0.5 .0.5 4.5 .1 2(10/15 .0.5 .0.5 .0.5 <1 .0.5 - - 7.2 .5 .2 .2 5(21/15 <0.5 <0.5 .0.5 .1 <0.5 - 8/8/15 .0.5 .0.5 .0.5 .1 2 .0.5 <0.5 .0.5 18.7 .2 WS(-. 10/19/90 .1 .5 .5 .15 .5 NA <10 NA <5 NA 1/18/01 .1 <5 .5 .15 .5 <2 .10 .4 24 NA 4/18/81 .1 .5 .5 .15 .5 .2 .10 <4 9 NA 8/20/01 <1 -- .5 .5 <15 .5 <2 .10 .4 .5 <20 11127/81 .1 .5 .5 <15 .5 <2 .10 <4 9 .20 2114/02 .1 .5 .5 .15 .5 NA .10 NA .5 NA 4/15/82 .1 .5 .5 .15 .5 NA .10 NA .5 NA 8/9102 NO NO NO NS NO NS NS NS NO NS 11/13/02 .1 .5 .5 <15 .5 NA .10 NA 5.5 NA 2/11/03 .1 <5 <5 .15 .5 NA .10 NA 5.5 NA 5(22/03 NO NO NS NS NO NS NO NS NS NS 8126/83 NS NS NS NS NO NS NS NO NS NO - 12/1/03 .1 <1 .1 .1 .1 <1 .1 .1 26 .0.5 W$W-3 11/13/02 s1 .5 .5 <15 .5 NA .10 NA 151 NA 2/11/83 .1 .5 .5 .15 .5 NA .10 NA 76 NA 5/22/03 NS NO NO NO NO NO NO NS NO I NO 5126104 .1 .1 .1 .1 .1 NA <1 <1 15 NA WSW-4 - 1112712005 .1 <1 .1 .1 .1 NA .1 .1 <5 .0.51 SiNS-11 1/5100 5.70 .5 .5 .15 .5 .2 .10 .5 .5 NA SiNS-A 5/2100 14.9 <1 .1 53 .1 <1 .1 .2 5 NA 7/20/80 <1 .1 1 .1 <3 .1 <1 .1 .2 <5 NA 10/19100 .1 .5 .5 .15 .5 <2 .10 <4 .5 NA 11"I8/81 .1 .5 <5 .15 .5 .2 .10 .4 82 NA 4118101 .1 .5 .5 .15 .5 <2 .10 <4 .5 NA 8/30/01 NO (stream wrs dr5 NO NO NS NO NO NO NO NS through 6(8/82 NO(s/reamw dry NO NO NS NS NS NS NS NO S 11/13/02 .1 .5 .5 .15 .5 NA .10 NA <5 NA SWS.A 2/11/83 .1 .5 .5 <15 .5 - NA - .10 NA .5 NA 5/22/03 .1 .5 .5 .15 .5 NA <10 NA 6.5 .20 8126/83 .1 <5 .5 .15 .5 NA <10 NA .5 .20 - 9126103 .1 .1 .1 .1 2.5 .1 72 NA .5 <0.50 Creek 5/9/13 .0.5 .0.5 .0.5 .1.0 .0.5 .0.5 13.9 .0.5 .5 <2 8/7113 0.7 .0.5 5.3 .1.5 <0.5 .0.5 1.8 .0.5 .5 <2 11/16113 .0.5 .0.5 <0.5 .1.0 <0.5 .0.5 <0.5 <0.5 .5 <2 2/17/14 .0.5 .0.5 .0.5 <1.0 <0.5 <0.5 <0.5 .0.5 .5 <2 5/13114 1.9 .0.5 1.1 .1.5 .0.5 .0.5 0.8 .0.5 <5 .2 8/12114 34.6 12 2.6 1.4 .0.5 .0.5 13.8 .0.5 .5 <2 11/8/14 NS (stream we his) NO NS NO NO NO NO NO NO 2/10(15 0.68 50.5 I .0.5 .1.5 .0.5 .0.5 .0.5 .0.5 .5 <2 .0.5 1 .0.5 .1.5 <0.5 1 .0.5 <0.5 <0.5 <5 <2 Notes: Flo = Free Product F,gure,bo(dexeauconce,,5a5cnsabove/0 tCAC-2LSten 514 = Not MaSsed NS = Not Sampled sf= lefluent Sample Dcw = Type S! <'.11 SINS • steam samr4e '/SW= water supply all WSW-1 WeterSu WeH sample obtained from adjacent trailer ------KSW2 • Water Supply Well sample- obtained from abandoned trailer ( Sluteyporuefy) ___________WSW3= Water Supply Well sample- obtained from unused sesde sell CREEKstroamsampl See table 4 for efl!sen/ uamote moats rdo 1.030 1 - Page 8 of 8 • — — — — •- • — 'l• = — — vv z — — V oc — — — C') cj — — — VV — — VV ) ) 3000 C" 00 a-) a) 0 a) o . cz •0 a) I) - 0 a)a) N 0 c I) _ C/D 0 APPENDIX A Decontamination Procedures Equipment decontamination is performed to prevent cross-contamination between sample points. Wherever possible, disposable or laboratory decontaminated equipment is used. Field decontamination is often necessary for equipment such as hand augers and water level probes. Downhole drilling equipment (augers, rods, and split-spoon samplers) is decontaminated between borings using high pressure steam and allowed to air dry. Hand augers and other sampling equipment are decontaminated using the following procedure: Scrub with Alconox/water solution Rinse with tap water Rinse with deionized water Rinse with pesticide grade isopropanol Air dry Groundwater Samnhin2 Prior to groundwater sample collection, the depth to water is measured with a decontaminated electric water level probe. The well volume is calculated. The well is purged by removing three to five well volumes or until dry using a new disposable bailer. During purging, temperature, pH, and specific conductivity are measured and recorded. Groundwater samples are collected into laboratory-prepared containers appropriate for the analytical method. New disposable bailers and new nylon cord are used to withdraw the samples. Each sample container is labeled with the following information: Project name, date, sample identification, sampler's name, and requested analysis. The samples are immediately placed in an insulated cooler with ice. The samples are handled, stored and transported to the laboratory under EPA chain-of-custody control. APPENDIX B Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 lace AnalyticaI /wwwpaceiabacom August 14, 2015 Mr. Joe Best Best Geological & Environmental Consulting 1009 Hayfield Lane Greensboro, NC 27410 RE: Project: BENNETTAND BAILEY Pace Project No.: 92262422 Dear Mr. Best: Enclosed are the analytical results for sample(s) received by the laboratory on August 07, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Un1cL -fl1 ,on Angela Baioni angela.baioni@pacelabs.com Project Manager Enclosures .( .1 "V REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 1 of 41 PeAnaIyticaI Pace Analytical Services, Inc. 9800 Kincey Ave Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NCO30 North Carolina Drinking Water Certification #: 37712 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 West Virginia Certification #: 357 VirginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 41 /71aceAnalytical wwpac&abscom 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: CREEK Lab ID: 92262422009 Collected: 08/06/15 11:30 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. QuaI 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug/L 5.0 1 08/10/15 16:15 08/13/15 22:58 7439-92-1 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 08/10115 22:11 71-43-2 Bromobenzene ND ug/L 0.50 1 08/10/15 22:11 108-86-1 Bromochloromethane ND ug/L 0.50 1 08/10/15 22:11 74-97-5 Bromodichloromethane ND ug/L 0.50 1 08/10/15 22:11 75-27-4 Bromoform ND ug/L 0.50 1 08/10/15 22:11 75-25-2 Bromomethane ND ug/L 5.0 1 08/10/15 22:11 74-83-9 n-Butylbenzene ND ug/L 0.50 1 08/10/15 22:11 104-51-8 sec- Butylbenzene ND ug/L 0.50 1 08/10/15 22:11 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 08/10/15 22:11 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 08/10/15 22:11 56-23-5 Chlorobenzene ND ug/L 0.50 1 08/10/15 22:11 108-90-7 Chloroethane ND ug/L 1.0 1 08/10/15 22:11 75-00-3 Chloroform ND ug/L 0.50 1 08/10/15 22:11 67-66-3 Chloromethane ND ug/L 1.0 1 08/10/15 22:11 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 08/10/15 22:11 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 08/10/15 22:11 106-43-4 1,2-Dibromo-3-chloropropane ND ugiL 1.0 1 08/10/15 22:11 96-12-8 Dibromochloromethane ND ug/L 0.50 1 08/10/15 22:11 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 08/10/15 22:11 106-93-4 Dibromomethane ND ug/L 0.50 1 08/10/15 22:11 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 08/10/15 22:11 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 08/10/15 22:11 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 08/10/15 22:11 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 08/10/15 22:11 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 08/10/15 22:11 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 08/10/15 22:11 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 08/10/15 22:11 75-35-4 cis-i,2-Dichloroethene ND ug/L 0.50 1 08/10/15 22:11 156-59-2 trans-i ,2-Dichloroethene ND ug/L 0.50 1 08/10/15 22:11 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 08/10/15 22:11 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 08/10/15 22:11 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 08/10/15 22:11 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 08/10/15 22:11 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 22:11 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 22:11 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 08/10/15 22:11 108-20-3 Ethylbenzene ND ug/L 0.50 1 08/10/15 22:11 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 08/10/15 22:11 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 08/10/15 22:11 98-82-8 Methylene Chloride ND ug/L 2.0 1 08/10/15 22:11 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 08/10/15 22:11 1634-04-4 Naphthalene ND ug/L 2.0 1 08/10/15 22:11 91-20-3 n-Propylbenzene ND ug/L 0.50 1 08/10/15 22:11 103-65-1 Styrene ND ug/L 0.50 1 08/10/15 22:11 100-42-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services, Inc. Page 20 of 41 /hAnaIyticaI Pace Analytical Services, Inc. 9800 Kincey Ave Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: BENNETT AND BAILEY 92262422 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92262422001 MWI4 EPA 6010 JDA 1 PASI-A EPA 8270 RES 21 PASI-C SM 6200B CAl-I 63 PASI-C 92262422002 WWI EPA 6010 JDA 1 PASI-A EPA 8270 RES 21 PASI-C SM 6200B CAl-I 63 PASI-C 92262422003 MWI3 EPA 6010 JDA 1 PASI-A EPA 8270 RES 21 PASI-C SM 6200B CAH 63 PASI-C 92262422004 MW9 EPA 6010 JDA 1 PASI-A EPA 8270 RES 21 PASI-C SM 6200B CAH 63 PASI-C 92262422005 DCWI EPA 6010 JDA 1 PASI-A SM 6200B CAH 63 PASI-C 92262422006 MW2 EPA 6010 JDA 1 PASI-A SM 6200B CAl-I 63 PASI-C 92262422007 MW5 EPA 6010 JDA 1 PASI-A SM 6200B CAH 63 PASt-C 92262422008 MWI2 EPA 6010 JDA 1 PASI-A SM 6200B CAH 63 PASI-C 92262422009 CREEK EPA 6010 JDA 1 PASI-A SM 6200B CAH 63 PASI-C 92262422010 EFFLUENT EPA 6010 JDA 1 PASI-A EPA 8270 RES 21 PASt-C SM 6200B CAH 42 PASI-C SM2540D MJP 1 PASI-A 92262422011 INF EPA 6010 JDA 1 PASt-A SM 6200B CAH 16 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 3 of 41 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 /~aceAnalytkal " pacescom ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MWI4 Lab ID: 92262422001 Collected: 08/06/15 09:45 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug/L 5.0 1 08/10/15 16:15 08/13/15 22:18 7439-92-1 8270 MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 83-32-9 Acenaphthylene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 208-96-8 Anthracene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 120-12-7 Benzo(a)anthracene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 56-55-3 Benzo(a)pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11115 15:47 50-32-8 Benzo(b)fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 205-99-2 Benzo(g,h,i)perylene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 191-24-2 Benzo(k)fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 207-08-9 L3 Chrysene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 53-70-3 Fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 206-44-0 Fluorene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 86-73-7 lndeno(1,2,3-cd)pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 193-39-5 1 -Methyl naphtha lene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 90-12-0 2-Methyl naphtha lene ND ugIL 10.0 1 08/11/15 12:00 08/11/15 15:47 91-57-6 Naphthalene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 91-20-3 Phenanthrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 85-01-8 Pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 15:47 129-00-0 Surrogates Nitrobenzene-d5 (S) 71 % 21-110 1 08/11/15 12:00 08/11/15 15:47 4165-60-0 2-Fluorobiphenyl (S) 74 % 27-110 1 08/11/15 12:00 08/11/15 15:47 321-60-8 Terphenyl-d14 (S) 53 % 31-107 1 08/11/15 12:00 08/11/15 15:47 1718-51-0 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 08/10/15 20:48 71-43-2 Bromobenzene ND ug/L 0.50 1 08/10/15 20:48 108-86-1 Bromochloromethane ND ug/L 0.50 1 08/10/15 20:48 74-97-5 Bromodichloromethane ND ug/L 0.50 1 08/10/15 20:48 75-27-4 Bromoform ND ug/L 0.50 1 08/10/15 20:48 75-25-2 Bromomethane ND ug/L 5.0 1 08/10/15 20:48 74-83-9 n-Butylbenzene ND ug/L 0.50 1 08/10/15 20:48 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 08/10/15 20:48 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 08/10/15 20:48 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 08/10/15 20:48 56-23-5 Chlorobenzene ND ug/L 0.50 1 08/10115 20:48 108-90-7 Chloroethane ND ug/L 1.0 1 08/10/15 20:48 75-00-3 Chloroform ND ug/L 0.50 1 08/10/15 20:48 67-66-3 Chloromethane ND ug/L 1.0 1 08/10/15 20:48 74-87-3 2-Chiorotoluene ND ugIL 0.50 1 08/10/15 20:48 95-49-8 4-Chlorotoluene ND ugiL 0.50 1 08/10/15 20:48 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 08/10/15 20:48 96-12-8 Dibromochloromethane ND ug/L 0.50 1 08/10/15 20:48 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 08/10/15 20:48 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08114/2015 0325 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 41 ,11aceMaI4icaI pace!abs.com 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MWI4 Lab ID: 92262422001 Collected: 08/06/15 09:45 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Dibromomethane ND ug/L 0.50 1 08/10/15 20:48 74-95-3 1,2-Dichlorobenzene NO ug/L 0.50 1 08/10/15 20:48 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 08110/15 20:48 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 08/10/15 20:48 106-46-7 Oichlorodifluoromethane ND ug/L 0.50 1 08/10/15 20:48 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 08/10/15 20:48 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 08/10/15 20:48 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 08/10/15 20:48 75-35-4 cis- 1,2-Dichloroethene ND ug/L 0.50 1 08/10/15 20:48 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 08/10/15 20:48 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 08/10/15 20:48 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 08/10/15 20:48 142-28-9 2,2-Oichloropropane ND ug/L 0.50 1 08/10/15 20:48 594-20-7 1,1-Oichloropropene ND ug/L 0.50 1 08/10/15 20:48 563-58-6 cis- 1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 20:48 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 20:48 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 08/10/15 20:48 108-20-3 Ethylbenzene ND ug/L 0.50 1 08/10/15 20:48 100-41-4 Hexachloro-1 ,3-butadiene ND ug/L 2.0 1 08/10/15 20:48 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 08/10/15 20:48 98-82-8 Methylene Chloride ND ug/L 2.0 1 08/10/15 20:48 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 08/10/15 20:48 1634-04-4 Naphthalene ND ug/L 2.0 1 08/10/15 20:48 91-20-3 n-Propylbenzene ND ug/L 0.50 1 08/10/15 20:48 103-65-1 Styrene ND ug/L 0.50 1 08/10/15 20:48 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 08/10/15 20:48 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 08/10/15 20:48 79-34-5 Tetrachloroethene ND ug/L 0.50 1 08/10/15 20:48 127-18-4 Toluene ND ug/L 0.50 1 08/10/15 20:48 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 08/10/15 20:48 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 08/10/15 20:48 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 08/10/15 20:48 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 08/10/15 20:48 79-00-5 Trichloroethene ND ug/L 0.50 1 08/10/15 20:48 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 08/10/15 20:48 75-69-4 1,2,3-Trichioropropane ND ug/L 0.50 1 08/10/15 20:48 96-18-4 1 ,2,4-Trimethylbenzene ND ug/L 0.50 1 08/10/15 20:48 95-63-6 1,3,5-Trimethylbenzene NO ug/L 0.50 1 08/10/15 20:48 108-67-8 Vinyl chloride ND ug/L 1.0 1 08/10/15 20:48 75-01-4 m&p-Xylene ND ug/L 1.0 1 08/10/15 20:48 179601-23-1 o-Xylene ND ug/L 0.50 1 08/10/15 20:48 95-47-6 Surrogates 1,2-Dichloroethane-d4 (5) 96 % 70-130 1 08/10/15 20:48 17060-07-0 4-Bromofluorobenzene (5) 99 % 70-130 1 08/10/15 20:48 460-00-4 Toluene-d8 (S) 101 % 70-130 1 08/10/15 20:48 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Dote- 0811412015 03:2 PM without the written coneent of Pace Analytical 6ervice3, Inc.. Pages 0t41 rw.. nhIoIyLIbQI cel vibea, 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 /AceAnaIyticaI /wwpacelab&com ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample; WWI Parameters 6010 MET ICP Lead 8270 MSSV Semivol Organic HVI Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Chrysene Dibenz(a,h)anthracene Fluoranthene Fluorene Indeno(1 ,2,3-cd)pyrene 1 -Methylnaphthalene 2-Methylnaphthalene Naphthalene Phena nth rene Pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 6200B MSV Benzene Bromobenzene Bromochioromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1 ,2-Dibromo-3-chloropropane Dibromochloromethane 1 ,2-Dibromoethane (EDB) Lab ID; 92262422002 Collected: 08/06/15 10:15 Received: 08/07/15 14:55 Matrix: Water Results Units Report Limit DF Prepared Analyzed CAS No. Qual Analytical Method: EPA 6010 Preparation Method: EPA 3010 16.7 ug/L 5.0 1 08/10/15 16:15 08/13/15 22:27 7439-92-1 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 83-32-9 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 208-96-8 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 120-12-7 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 56-55-3 ND ug/L 10.0 1 08/11/15 12:00 08/11115 16:13 50-32-8 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 205-99-2 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 191-24-2 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 207-08-9 L3 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 218-01-9 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 53-70-3 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 206-44-0 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 86-73-7 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 193-39-5 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 90-12-0 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 91-57-6 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 91-20-3 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 85-01-8 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:13 129-00-0 75 % 21-110 1 08/11/15 12:00 08/11/15 16:13 4165-60-0 85 27-110 1 08/11/15 12:00 08/11/15 16:13 321-60-8 64 % 31-107 1 08/11/15 12:00 08/11/15 16:13 1718-51-0 Analytical Method: SM 6200B ND ug/L 0.50 1 08/10/15 21:04 71-43-2 ND ug/L 0.50 1 08/10/15 21:04 108-86-1 ND ug/L 0.50 1 08/10/15 21:04 74-97-5 ND ug/L 0.50 1 08/10/15 21:04 75-27-4 ND ug/L 0.50 1 08/10/15 21:04 75-25-2 ND ug/L 5.0 1 08/10/15 21:04 74-83-9 ND ug/L 0.50 1 08/10/15 21:04 104-51-8 ND ug/L 0.50 1 08/10/15 21:04 135-98-8 ND ug/L 0.50 1 08/10/15 21:04 98-06-6 ND ug/L 0.50 1 08/10/15 21:04 56-23-5 ND ug/L 0.50 1 08/10/15 21:04 108-90-7 ND ug/L 1.0 1 08/10/15 21:04 75-00-3 ND ug/L 0.50 1 08/10/15 21:04 67-66-3 ND ug/L 1.0 1 08/10/15 21:04 74-87-3 ND ug/L 0.50 1 08/10/15 21:04 95-49-8 ND ug/L 0.50 1 08/10/15 21:04 106-43-4 ND ug/L 1.0 1 08/10/15 21:04 96-12-8 ND ug/L 0.50 1 08/10/15 21:04 124-48-1 ND ug/L 0.50 1 08/10/15 21:04 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date 08/1412018 03:25 PM without the written consent of Pace Analytical Services, Inc. - Page 6 0f41 /AeAnalytical / vwpacecom 9800 Kincey Ave. Suite 100 Huntersvite, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: WWI Lab ID: 92262422002 Collected: 08/06/15 10:15 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Dibromomethane ND ug/L 0.50 1 08/10/15 21:04 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:04 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:04 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:04 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 08/10/15 21:04 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 08/10/15 21:04 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 08/10/15 21:04 107-06-2 1,1-Dichloroethene ND ugJL 0.50 1 08/10/15 21:04 75-35-4 cis- i,2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:04 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:04 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 08/10/15 21:04 78-87-5 1,3-Dichioropropane ND ug/L 0.50 1 08/10/15 21:04 142-28-9 2,2-Dichioropropane ND ug/L 0.50 1 08/10/15 21:04 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 08/10/15 21:04 563-58-6 cis- i,3-Dichloropropene ND ug/L 0.50 1 08/10/15 21:04 10061-01-5 trans-i ,3-Dichloropropene ND ug/L 0.50 1 08/10/15 21:04 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 08/10/15 21:04 108-20-3 Ethylbenzene ND ug/L 0.50 1 08/10/15 21:04 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 08/10/15 21:04 87-68-3 lsopropylbenzene (Cumene) ND ug/L 0.50 1 08/10/15 21:04 98-82-8 Methylene Chloride ND ug/L 2.0 1 08/10/15 21:04 75-09-2 Methyl-tert-butyl ether 2.0 ug/L 0.50 1 08/10/1521:04 1634-04-4 Naphthalene ND ug/L 2.0 1 08/10/15 21:04 91-20-3 n-Propylbenzene ND ug/L 0.50 1 08/10/15 21:04 103-65-1 Styrene ND ug/L 0.50 1 08/10/15 21:04 100-42-5 11,1,2-Tetrachloroethane ND ug/L 0.50 1 08110/15 21:04 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 08/10/15 21:04 79-34-5 Tetrachloroethene ND ug/L 0.50 1 08/10/15 21:04 127-18-4 Toluene ND ug/L 0.50 1 08/10/15 21:04 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 08/10/15 21:04 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 08/10/15 21:04 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 08/10/15 21:04 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 08/10/15 21:04 79-00-5 Trichioroethene ND ug/L 0.50 1 08/10/15 21:04 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 08/10/15 21:04 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 1 08/10/15 21:04 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 08/10/15 21:04 95-63-6 1 ,3,5-Trimethylbenzene ND ug/L 0.50 1 08/10/15 21:04 108-67-8 Vinyl chloride ND ug/L 1.0 1 08/10/15 21:04 75-01-4 m&p-Xylene ND ug/L 1.0 1 08/10/15 21:04 179601-23-1 o-Xylene ND ug/L 0.50 1 08/10/15 21:04 95-47-6 Surrogates 1,2-Dichloroethane-d4 (5) 97 % 70-130 1 08/10/15 21:04 17060-07-0 4-Bromofluorobenzene (5) 98 % 70-130 1 08/10/15 21:04 460-00-4 Toluene-d8 (S) ioi 70-130 1 08/10/15 21:04 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date- 08/14/2015 03:25 PM without the written consent of Pace Analyticai Services, inc.. Page 7 of 41 Analytical Method: EPA 6010 Preparation Method: EPA 3010 NO ug/L 5.0 1 08/10/15 16:15 08/13/15 22:30 7439-92-1 Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 83-32-9 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 208-96-8 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 120-12-7 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 56-55-3 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 50-32-8 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 205-99-2 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 191-24-2 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 207-08-9 L3 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 218-01-9 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 53-70-3 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 206-44-0 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 86-73-7 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 193-39-5 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 90-12-0 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 91-57-6 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 91-20-3 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 85-01-8 ND ug/L 10.0 1 08/11/15 12:00 08/11/15 16:38 129-00-0 69 % 21-110 1 08/11/15 12:00 08/11/15 16:38 4165-60-0 82 % 27-110 1 08/11/15 12:00 08/11/15 16:38 321-60-8 53 % 31-107 1 08/11/15 12:00 08/11/15 16:38 1718-51-0 Analytical Method: SM 6200B iAceAnaI4icaI w%wpac&ab&m 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MWI3 Lab ID: 92262422003 Collected: 08/06/1510:35 Received: 08/07/1509:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Lead 8270 MSSV Semivol Organic HVI Acenaphthene Acenaphthylene Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g, h, i)perylene Benzo(k)fluoranthene Chrysene Dibenz(a,h)anthracene Fluoranthene Fl uorene Indeno(1 ,2,3-cd)pyrene 1 -Methylnaphthalene 2-Methyl naphtha lene Naphthalene Phena nth rene Pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 6200B MSV Benzene Bromobenzene Bromochioromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chioromethane 2-Chlorotoluene 4-Chlorotoluene 1 ,2-Dibromo-3-chloropropane Dibromochloromethane 1 2-Dibromoethane (EDB) ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 0.50 1 08/10/15 21:21 71-43-2 0.50 1 08/10/1521:21 108-86-1 0.50 1 08/10/15 21:21 74-97-5 0.50 1 08/10/15 21:21 75-27-4 0.50 1 08/10/15 21:21 75-25-2 5.0 1 08/10/15 21:21 74-83-9 0.50 1 08/10/15 21:21 104-51-8 0.50 1 08/10/15 21:21 135-98-8 0.50 1 08/10/15 21:21 98-06-6 0.50 1 08/10/15 21:21 56-23-5 0.50 1 08/10/15 21:21 108-90-7 1.0 1 08/10/15 21:21 75-00-3 0.50 1 08/10/15 21:21 67-66-3 1.0 1 08/10/15 21:21 74-87-3 0.50 1 08/10/15 21:21 95-49-8 0.50 1 08/10/15 21:21 106-43-4 1.0 1 08/10/1521:21 96-12-8 0.50 1 08/10/15 21:21 124-48-1 0.50 1 08/10/15 21:21 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date- 08/14/2015 0325 PM without the written conent of Poce Analytical 3eivioe, Inc.. Page 8 0f41 /P(ceAnalytical / 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MWI3 Lab ID: 92262422003 Collected: 08/06/1510:35 Received: 08/07/1509:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method: SM 6200B Dibromomethane ND ug/L 0.50 1 08/10/15 21:21 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:21 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:21 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:21 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 08/10/15 21:21 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 08/10/15 21:21 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 08/10/15 21:21 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 08/10/15 21:21 75-35-4 cis- 1,2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:21 156-59-2 trans-i ,2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:21 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 08/10/15 21:21 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 08/10/15 21:21 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 08/10/15 21:21 594-20-7 1,1-Dichioropropene ND ug/L 0.50 1 08/10/15 21:21 563-58-6 cis- 1,3-Dich!oropropene ND ug/L 0.50 1 08/10/15 21:21 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 21:21 10061-02-6 DUsopropyl ether ND ugJL 0.50 1 08/10/15 21:21 108-20-3 Ethylbenzene ND ug/L 0.50 1 08/10/15 21:21 100-41-4 Hexachloro-i ,3-butadiene ND ug/L 2.0 1 08/10/15 21:21 87-68-3 lsopropylbenzene (Cumene) ND ug/L 0.50 1 08/10/15 21:21 98-82-8 Methylene Chloride ND ug/L 2.0 1 08/10/15 21:21 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 08/10/15 21:21 1634-04-4 Naphthalene ND ug/L 2.0 1 08/10/15 21:21 91-20-3 n-Propylbenzene ND ug/L 0.50 1 08/10/15 21:21 103-65-1 Styrene ND ug/L 0.50 1 08/10/15 21:21 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 08/10/15 21:21 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 08/10/15 21:21 79-34-5 Tetrachloroethene ND ug/L 0.50 1 08/10/15 21:21 127-18-4 Toluene ND ug/L 0.50 1 08/10/15 21:21 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 08/10/15 21:21 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 08/10/15 21:21 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 08/10/15 21:21 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 08/10/15 21:21 79-00-5 Trichloroethene ND ug/L 0.50 1 08/10/15 21:21 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 08/10/15 21:21 75-69-4 1,2,3-Trichioropropane ND ug/L 0.50 1 08/10/15 21:21 96-18-4 1 ,2,4-Trimethylbenzene ND ug/L 0.50 1 08/10/15 21:21 95-63-6 1 ,3,5-Trimethylbenzene ND ug/L 0.50 1 08/10/15 21:21 108-67-8 Vinyl chloride ND ug/L 1.0 1 08/10/15 21:21 75-01-4 m&p-Xylene ND ug/L 1.0 1 08/10/15 21:21 179601-23-1 o-Xylene ND ug/L 0.50 1 08/10/15 21:21 95-47-6 Surrogates 1 ,2-Dichloroethane-d4 (5) 95 % 70-130 1 08/10/15 21:21 17060-07-0 4-Bromofluorobenzene (5) 98 % 70-130 1 08/10/15 21:21 460-00-4 Toluene-d8 (S) 104 70-130 1 08/10/15 21:21 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date 08/1412015 03:25 PM without the written consent of Pace Analytical Services, Inc.. Page 9 0f41 /71aceAnayical /wwpacelab&com 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MW9 Lab ID: 92262422004 Collected: 08/06/15 11:55 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead 15.1 ug/L 5.0 1 08/10/15 16:15 08/13/15 22:42 7439-92-1 8270 MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 83-32-9 Acenaphthylene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 208-96-8 Anthracene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 120-12-7 Benzo(a)anthracene ND ug/L 10.0 1 08/11/15 12:00 08111/15 17:03 56-55-3 Benzo(a)pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 50-32-8 Benzo(b)fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 205-99-2 Benzo(g,h,i)perylene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 191-24-2 Benzo(k)fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 207-08-9 L3 Chrysene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 218-01-9 Dibenz(a,h)a nth racene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 53-70-3 Fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 206-44-0 Fluorene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 86-73-7 lndeno(1,2,3-cd)pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 193-39-5 1-Methylnaphthalene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 90-12-0 2-Methylnaphthalene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 91-57-6 Naphthalene 37.4 ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 91-20-3 Phenanthrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 85-01-8 Pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:03 129-00-0 Surrogates Nitrobenzene-d5 (S) 77 % 21-110 1 08/11/15 12:00 08/11/15 17:03 4165-60-0 2-Fluorobiphenyl (S) 79 % 27-110 1 08/11/15 12:00 08/11/15 17:03 321-60-8 Terphenyl-d14 (S) 72 % 31-107 1 08111/15 12:00 08/11/15 17:03 1718-51-0 6200B MSV Analytical Method: SM 6200B Benzene 6170 ug/L 25.0 50 08/10/15 23:01 71-43-2 Bromobenzene ND ug/L 25.0 50 08/10/15 23:01 108-86-1 Bromochloromethane ND ug/L 25.0 50 08/10/15 23:01 74-97-5 Bromodichioromethane ND ug/L 25.0 50 08/10/15 23:01 75-27-4 Bromoform ND ug/L 25.0 50 08/10/15 23:01 75-25-2 Bromomethane ND ug/L 250 50 08/10/15 23:01 74-83-9 n-Butylbenzene ND ug/L 25.0 50 08/10/15 23:01 104-51-8 sec-Butylbenzene ND ug/L 25.0 50 08/10/15 23:01 135-98-8 tert-Butylbenzene ND ug/L 25.0 50 08/10/15 23:01 98-06-6 Carbon tetrachloride ND ug/L 25.0 50 08/10/15 23:01 56-23-5 Chlorobenzene ND ug/L 25.0 50 08/10/15 23:01 108-90-7 Chioroethane ND ug/L 50.0 50 08/10/15 23:01 75-00-3 Chloroform ND ug/L 25.0 50 08/10/15 23:01 67-66-3 Chloromethane ND ug/L 50.0 50 08/10/15 23:01 74-87-3 2-Chlorotoluene ND ug/L 25.0 50 08/10/15 23:01 95-49-8 4-Chiorotoluene ND ug/L 25.0 50 08/10/15 23:01 106-43-4 12-Dibromo-3-chloropropane ND ug/L 50.0 50 08/10/15 23:01 96-12-8 Dibromochloromethane ND ug/L 25.0 50 08/10/15 23:01 124-48-1 12-Dibromoethane (EDB) ND ug/L 25.0 50 08/10/15 23:01 106-93-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Poe Analytical Services, Inc.. Page 10 of 41 /,P(ceAnaI4icaI vwpaceah&m 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MW9 Lab ID: 92262422004 Collected: 08/06/15 11:55 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 620DB MSV Dibromomethane 1 ,2-Dichlorobenzene 1 ,3-Dichlorobenzene 1 ,4-Dichlorobenzene Dichlorodifluoromethane 1 ,i-Dichloroethane 1 2-Dichloroethane 1 ,i-Dichloroethene cis- i ,2-Dichloroethene trans-i ,2-Dichloroethene 1 ,2-Dichloropropane 1 3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis- i ,3-Dichloropropene trans-i ,3-Dichloropropene DUsopropyl ether Ethylbenzene Hexachloro-1 ,3-butadiene lsopropylbenzene (Cumene) Methylene Chloride Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1 ,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1 ,2,3-Trichlorobenzene 1 ,2,4-Trichlorobenzene 1,1 ,i-Trichloroethane 1,1 ,2-Trichloroethane Trichioroethene Trichlorofluoromethane 1 2,3-Trichloropropane 1 ,2,4-Trimethylbenzene 1 ,3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1 ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B ND ug/L 25.0 50 08/10/15 23:01 74-95-3 ND ug/L 25.0 50 08/10/15 23:01 95-50-1 ND ug/L 25.0 50 08/10/15 23:01 541-73-1 ND ug/L 25.0 50 08/10/15 23:01 106-46-7 ND ug/L 25.0 50 08/10/15 23:01 75-71-8 ND ug/L 25.0 50 08/10/15 23:01 75-34-3 ND ug/L 25.0 50 08/10/15 23:01 107-06-2 ND ug/L 25.0 50 08/10/15 23:01 75-35-4 ND ug/L 25.0 50 08/10/15 23:01 156-59-2 ND ug/L 25.0 50 08/10/15 23:01 156-60-5 ND ugIL 25.0 50 08/10/15 23:01 78-87-5 ND ug/L 25.0 50 08/10/15 23:01 142-28-9 ND ug/L 25.0 50 08/10/15 23:01 594-20-7 ND ug/L 25.0 50 08/10/15 23:01 563-58-6 ND ug/L 25.0 50 08/10/15 23:01 10061-01-5 ND ug/L 25.0 50 08/10/15 23:01 10061-02-6 764 ug/L 25.0 50 08/10/15 23:01 108-20-3 772 ug/L 25.0 50 08/10/15 23:01 100-41-4 ND ug/L 100 50 08/10/15 23:01 87-68-3 ND ug/L 25.0 50 08/10/15 23:01 98-82-8 ND ug/L 100 50 08/10/15 23:01 75-09-2 ND ug/L 25.0 50 08/10/15 23:01 1634-04-4 103 ug/L iOO 50 08/10/15 23:01 91-20-3 54.0 ug/L 25.0 50 08/10/15 23:01 103-65-1 ND ug/L 25.0 50 08/10/15 23:01 100-42-5 ND ug/L 25.0 50 08/10/15 23:01 630-20-6 ND ug/L 25.0 50 08/10/15 23:01 79-34-5 ND ug/L 25.0 50 08/10/15 23:01 127-18-4 5710 ug/L 25.0 50 08/10/15 23:01 108-88-3 ND ug/L 100 50 08/10/15 23:01 87-61-6 ND ug/L 100 50 08/10/15 23:01 120-82-1 ND ug/L 25.0 50 08/10/15 23:01 71-55-6 ND ug/L 25.0 50 08/10/15 23:01 79-00-5 ND ug/L 25.0 50 08/10/15 23:01 79-01-6 ND ug/L 50.0 50 08/10/15 23:01 75-69-4 ND ug/L 25.0 50 08/10/15 23:01 96-18-4 454 ug/L 25.0 50 08/10/15 23:01 95-63-6 126 ug/L 25.0 50 08/10/15 23:01 108-67-8 ND ug/L 50.0 50 08/10/15 23:01 75-01-4 2080 ug/L 50.0 50 08/10/15 23:01 179601-23-1 597 ug/L 25.0 50 08/10/15 23:01 95-47-6 95 % 70-130 50 08/10/15 23:01 17060-07-0 100 % 70-130 50 08/10/15 23:01 460-00-4 101 % 70-130 50 08/10/15 23:01 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the wriften consent of Pace Analytical Services, Inc. Page 11 0r41 /7~ceAnalytical / www.pacabbs.com 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: DCWI Lab ID: 92262422005 Collected: 08/06/15 12:45 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead ND ug/L 5.0 1 08/10/15 16:15 08/13/15 22:45 7439-92-1 6200B MSV Analytical Method: SM 6200B Benzene 1.2 ug/L 0.50 1 08/10/1521:38 71 -43-2 Bromobenzene ND ug/L 0.50 1 08/10/1521:38 108-86-1 Bromochloromethane ND ug/L 0.50 1 08/10/15 21:38 74-97-5 Bromodichloromethane ND ug/L 0.50 1 08/10/15 21:38 75-27-4 Bromoform ND ug/L 0.50 1 08/10/15 21:38 75-25-2 Bromomethane ND ug/L 5.0 1 08/10/15 21:38 74-83-9 n-Butylbenzene ND ug/L 0.50 1 08/10/1521:38 104-51 -8 sec-Butylbenzene ND ug/L 0.50 1 08/10/15 21:38 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 08/10/15 21:38 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 08/10/15 21:38 56-23-5 Chlorobenzene ND ug/L 0.50 1 08/10/1521:38 108-90-7 Chloroethane ND ug/L 1.0 1 08/10/15 21:38 75-00-3 Chloroform ND ug/L 0.50 1 08/10/15 21:38 67-66-3 Chloromethane ND ug/L 1.0 1 08/10/1521:38 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 08/10/15 21:38 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 08/10/15 21:38 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 08/10/15 21:38 96-12-8 Dibromochloromethane ND ug/L 0.50 1 08/10/15 21:38 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 0.50 1 08/10/15 21:38 106-93-4 Dibromomethane ND ug/L 0.50 1 08/10/1521:38 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:38 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:38 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:38 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 08/10/15 21:38 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 08/10/15 21:38 75-34-3 1,2-Dichloroethane 0.93 ug/L 0.50 1 08/10/15 21:38 107-06-2 1,1-Dichloroethene ND ug/L 0.50 1 08/10/15 21:38 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:38 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:38 156-60-5 1,2-Dichioropropane ND ug/L 0.50 1 08/10/15 21:38 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 08/10/15 21:38 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 08/10/15 21:38 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 08/10/15 21:38 563-58-6 cis- 1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 21:38 10061 -01 -5 trans- 1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 21:38 10061-02-6 Diisopropyl ether 2.1 ug/L 0.50 1 08/10/15 21:38 108-20-3 Ethylbenzene ND ug/L 0.50 1 08/10/15 21:38 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 08/10/15 21:38 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 08/10/15 21:38 98-82-8 Methylene Chloride ND ug/L 2.0 1 08/10/15 21:38 75-09-2 Methyl-tert-butyl ether 1.2 ug/L 0.50 1 08/10/15 21:38 1634-04-4 Naphthalene ND ug/L 2.0 1 08/10/15 21:38 91-20-3 n-Propylbenzene ND ug/L 0.50 1 08/10/15 21:38 103-65-1 Styrene ND ug/L 0.50 1 08/10/15 21:38 100-42-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services, Inc.. Page 12 of 41 1~7AceAnalytical e pac&ab& corn 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: DCWI Lab ID: 92262422005 Collected: 08/06/1512:45 Received: 08/07/1514:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 620DB MSV 1,1,1 ,2-Tetrachloroethane 1,1 2,2-Tetrachloroethane Tetrachloroethene Toluene 1 ,2,3-Trichlorobenzene 1 ,2,4-Trichlorobenzene 1,1 ,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1 ,2,3-Trichloropropane 1 ,2,4-Trimethylbenzene 1 ,3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1 ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 95 % 100 % 101 % 0.50 1 08/10/15 21:38 630-20-6 0.50 1 08/10/15 21:38 79-34-5 0.50 1 08/10/15 21:38 127-18-4 0.50 1 08/10/15 21:38 108-88-3 2.0 1 08/10/15 21:38 87-61-6 2.0 1 08/10/15 21:38 120-82-1 0.50 1 08/10/1521:38 71-55-6 0.50 1 08/10/15 21:38 79-00-5 0.50 1 08/10/15 21:38 79-01-6 1.0 1 08/10/1521:38 75-69-4 0.50 1 08/10/15 21:38 96-18-4 0.50 1 08/10/15 21:38 95-63-6 0.50 1 08/10/15 21:38 108-67-8 1.0 1 08/10/15 21:38 75-01-4 1.0 1 08/10/15 21:38 179601-23-1 0.50 1 08/10/15 21:38 95-47-6 70-130 1 08/10/15 21:38 17060-07-0 70-130 1 08/10/15 21:38 460-00-4 70-130 1 08/10/1521:38 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 41 /,P(ceAnalytical wwwPaC&IM&COM 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MW2 Lab ID: 92262422006 Collected: 08/06/15 13:10 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua! Analytical Method: EPA 6010 Preparation Method: EPA 3010 11.0 ug/L 5.0 1 08/10/15 16:15 08/13/15 22:48 7439-92-1 Analytical Method: SM 6200B 6010 MET ICP Lead 620DB MSV Benzene Bromobenzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane n-Butylbenzene sec-Butylbenzene tert-Butylbenzene Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 2-Chlorotoluene 4-Chlorotoluene 1 ,2-Dibromo-3-chloropropane Dibromochioromethane 1 ,2-Dibromoethane (EDB) Dibromomethane 1 ,2-Dichlorobenzene 1 ,3-Dichlorobenzene 1 ,4-Dichlorobenzene Dichlorodifluoromethane il-Dichloroethane 1 2-Dichloroethane 1,1-Dichloroethene cis-i ,2-Dichloroethene trans-i ,2-Dichloroethene 1 2-Dichloropropane 1 ,3-Dichloropropane 2,2-Dichloropropane 1,1-Dichloropropene cis- i ,3-Dichloropropene trans-1 3-Dichloropropene Diisopropyl ether Ethylbenzene F-Iexachloro-1,3-butadiene Isopropy!benzene (Cumene) Methylene Chloride Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1030 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 30.8 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 100 ug/L 217 ug/L ND ug/L 13.2 ug/L ND ug/L 19.4 ug/L 52.2 ug/L 44.1 ug/L ND ug/L 5.0 10 08/10/15 23:17 71-43-2 5.0 10 08/10/15 23:17 108-86-1 5.0 10 08/10/15 23:17 74-97-5 5.0 10 08/10/15 23:17 75-27-4 5.0 10 08/10/15 23:17 75-25-2 50.0 10 08/10/15 23:17 74-83-9 5.0 10 08/10/15 23:17 104-51-8 5.0 10 08/10/15 23:17 135-98-8 5.0 10 08/10/15 23:17 98-06-6 5.0 10 08/10/15 23:17 56-23-5 5.0 10 08/10/15 23:17 108-90-7 10.0 10 08/10/15 23:17 75-00-3 5.0 10 08/10/15 23:17 67-66-3 10.0 10 08/10/15 23:17 74-87-3 5.0 10 08/10/15 23:17 95-49-8 5.0 10 08/10/15 23:17 106-43-4 10.0 10 08/10/15 23:17 96-12-8 5.0 10 08/10/15 23:17 124-48-1 5.0 10 08/10/15 23:17 106-93-4 5.0 10 08/10/15 23:17 74-95-3 5.0 10 08/10/15 23:17 95-50-1 5.0 10 08/10/15 23:17 541-73-1 5.0 10 08/10/15 23:17 106-46-7 5.0 10 08/10/15 23:17 75-71-8 5.0 10 08/10/15 23:17 75-34-3 5.0 10 08/10/15 23:17 107-06-2 5.0 10 08/10/15 23:17 75-35-4 5.0 10 08/10/15 23:17 156-59-2 5.0 10 08/10/15 23:17 156-60-5 5.0 10 08/10/15 23:17 78-87-5 5.0 10 08/10/15 23:17 142-28-9 5.0 10 08/10/15 23:17 594-20-7 5.0 10 08/10/15 23:17 563-58-6 5.0 10 08/10/15 23:17 10061-01-5 5.0 10 08/10/15 23:17 10061-02-6 5.0 10 08/10/15 23:17 108-20-3 5.0 10 08/10/15 23:17 100-41-4 20.0 10 08/10/15 23:17 87-68-3 5.0 10 08/10/15 23:17 98-82-8 20.0 10 08/10/15 23:17 75-09-2 5.0 10 08/10/15 23:17 1634-04-4 20.0 10 08/10/15 23:17 91-20-3 5.0 10 08/10/15 23:17 103-65-1 5.0 10 08/10/15 23:17 100-42-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Srvicss, Inc., Page 14 of 41 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 /PceAnapical wpaceb&com ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MW2 Lab ID: 92262422006 Collected: 08/06/15 13:10 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV 1,1,1,2-Tetrachloroethane 1 ,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1 ,2,3-Trichlorobenzene 1 ,2,4-Trichlorobenzene 1,1 ,1-Trichloroethane 1,1 ,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1 ,2,3-Trichloropropane 1 ,2,4-Trimethylbenzene 1 ,3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates I ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B ND ug/L ND ug/L ND ug/L 528 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 303 ug/L ND ug/L ND ug/L 423 ug/L 356 ug/L 94 % 99 % 102 % 5.0 10 08/10/15 23:17 630-20-6 5.0 10 08/10/15 23:17 79-34-5 5.0 10 08/10/15 23:17 127-18-4 5.0 10 08/10/15 23:17 108-88-3 20.0 10 08/10/15 23:17 87-61-6 20.0 10 08/10/15 23:17 120-82-1 5.0 10 08/10/15 23:17 71-55-6 5.0 10 08/10/15 23:17 79-00-5 5.0 10 08/10/15 23:17 79-01-6 10.0 10 08/10/15 23:17 75-69-4 5.0 10 08/10/15 23:17 96-18-4 5.0 10 08/10/15 23:17 95-63-6 5.0 10 08/10/15 23:17 108-67-8 10.0 10 08/10/15 23:17 75-01-4 10.0 10 08/10/15 23:17 179601-23-1 5.0 10 08/10/15 23:17 95-47-6 70-130 10 08/10/15 23:17 17060-07-0 70-130 10 08/10/15 23:17 460-00-4 70-130 10 08/10/15 23:17 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Poe Analytical Ser,ice. Inc Date' 08/1412015 03:25 PM Page 15 of 41 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 /7~ceAnaVkal' wwwpacab&com ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MW5 Lab ID: 92262422007 Collected: 08/06/15 13:30 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead 26.6 ug/L 5.0 1 08/10/15 16:15 08/13/15 22:51 7439-92-1 6200B MSV Analytical Method: SM 6200B Benzene 10800 ug/L 62.5 125 08/10/15 23:34 71-43-2 Bromobenzene ND ug/L 62.5 125 08/10/15 23:34 108-86-1 Bromochloromethane ND ug/L 62.5 125 08/10/15 23:34 74-97-5 Bromodichloromethane ND ug/L 62.5 125 08/10/15 23:34 75-27-4 Bromoform ND ug/L 62.5 125 08/10/15 23:34 75-25-2 Bromomethane ND ug/L 625 125 08/10/15 23:34 74-83-9 n-Butylbenzene ND ug/L 62.5 125 08/10/15 23:34 104-51-8 sec-Butylbenzene ND ug/L 62.5 125 08/10/15 23:34 135-98-8 tert-Butylbenzene ND ug/L 62.5 125 08/10/15 23:34 98-06-6 Carbon tetrachloride ND ug/L 62.5 125 08/10/15 23:34 56-23-5 Chlorobenzene ND ug/L 62.5 125 08/10/15 23:34 108-90-7 Chloroethane ND ug/L 125 125 08/10/15 23:34 75-00-3 Chloroform ND ug/L 62.5 125 08/10/1523:34 67-66-3 Chloromethane ND ug/L 125 125 08/10/1523:34 74-87-3 2-Chlorotoluene ND ug/L 62.5 125 08/10/15 23:34 95-49-8 4-Chlorotoluene ND ug/L 62.5 125 08/10/15 23:34 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 125 125 08/10/15 23:34 96-12-8 Dibromochloromethane ND ug/L 62.5 125 08/10/15 23:34 124-48-1 12-Dibromoethane(EDB) ND ug/L 62.5 125 08/10/15 23:34 106-93-4 Dibromomethane ND ug/L 62.5 125 08/10/15 23:34 74-95-3 1,2-Dichlorobenzene ND ug/L 62.5 125 08/10/15 23:34 95-50-1 13-Dichlorobenzene ND ug/L 62.5 125 08/10/15 23:34 541-73-1 14-Dichlorobenzene ND ug/L 62.5 125 08/10/15 23:34 106-46-7 Dichlorodifluoromethane ND ug/L 62.5 125 08/10/15 23:34 75-71-8 1 ,1-Dichloroethane ND ug/L 62.5 125 08/10/15 23:34 75-34-3 1,2-Dichloroethane 621 ug/L 62.5 125 08/10/15 23:34 107-06-2 1,1-Dichloroethene ND ug/L 62.5 125 08/10/15 23:34 75-35-4 cis-i,2-Dichloroethene ND ug/L 62.5 125 08/10/15 23:34 156-59-2 trans-i ,2-Dichloroethene ND ug/L 62.5 125 08/10/15 23:34 156-60-5 1,2-Dichloropropane ND ug/L 62.5 125 08/10/15 23:34 78-87-5 1,3-Dichioropropane ND ug/L 62.5 125 08/10/15 23:34 142-28-9 2,2-Dichloropropane ND ug/L 62.5 125 08/10/15 23:34 594-20-7 1,1-Dichloropropene ND ug/L 62.5 125 08/10/15 23:34 563-58-6 cis- 1, 3-Dichloropropene ND ug/L 62.5 125 08/10/15 23:34 10061-01-5 trans- i ,3-Dichloropropene ND ug/L 62.5 125 08/10/15 23:34 10061-02-6 Diisopropyl ether 1570 ug/L 62.5 125 08/10/15 23:34 108-20-3 Ethylbenzene 836 ug/L 62.5 125 08/10/15 23:34 100-41-4 Hexachloro-1,3-butadiene ND ug/L 250 125 08/10/15 23:34 87-68-3 lsopropylbenzene (Cumene) 81.1 ug/L 62.5 125 08/10/15 23:34 98-82-8 Methylene Chloride ND ug/L 250 125 08/10/15 23:34 75-09-2 Methyl-tert-butyl ether ND ug/L 62.5 125 08/10/15 23:34 1634-04-4 Naphthalene 886 ug/L 250 125 08/10/15 23:34 91-20-3 n-Propylbenzene ND ug/L 62.5 125 08/10/15 23:34 103-65-1 Styrene ND ug/L 62.5 125 08/10/15 23:34 100-42-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services, Inc.. Page 16 of 41 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 /AceAnayical' w,wpaceb& corn ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MW5 Lab ID: 92262422007 Collected: 08/06/15 13:30 Received: 08/07115 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV 1,1,1 2-Tetrachloroethane 11 ,2,2-Tetrachloroethane Tetrachloroethene Toluene 1 ,2,3-Trichlorobenzene 1 ,2,4-Trichlorobenzene 1,1 ,1-Trichloroethane 11 2-Trichloroethane Trichloroethene Trichlorofluoromethane 1 23-Trichloropropane 1 ,2,4-Trimethylbenzene 1 ,3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1 ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B ND ug/L 62.5 125 08/10/15 23:34 630-20-6 ND ug/L 62.5 125 08/10/15 23:34 79-34-5 ND ug/L 62.5 125 08/10/15 23:34 127-18-4 16600 ug/L 62.5 125 08/10/15 23:34 108-88-3 ND ug/L 250 125 08/10/15 23:34 87-61-6 ND ug/L 250 125 08/10/15 23:34 120-82-1 ND ug/L 62.5 125 08/10/15 23:34 71-55-6 ND ug/L 62.5 125 08/10/1523:34 79-00-5 ND ug/L 62.5 125 08/10/15 23:34 79-01-6 ND ug/L 125 125 08/10/15 23:34 75-69-4 ND ug/L 62.5 125 08/10/15 23:34 96-18-4 7020 ug/L 62.5 125 08/10/15 23:34 95-63-6 2300 ug/L 62.5 125 08/10/15 23:34 108-67-8 ND ug/L 125 125 08/10/15 23:34 75-01-4 16800 ug/L 125 125 08/10/15 23:34 179601-23-1 7790 ug/L 62.5 125 08/10/15 23:34 95-47-6 94 % 70-130 125 08/10/15 23:34 17060-07-0 100 % 70-130 125 08/10/15 23:34 460-00-4 100 % 70-130 125 08/10/15 23:34 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services. Inc Page 17 of 41 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 /~aceAnayical wwpacalabscorn ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MWI2 Lab ID: 92262422008 Collected: 08/06/15 11:15 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead 21.4 ug/L 5.0 1 08/10/15 16:15 08/13/15 22:55 7439-92-1 6200B MSV Analytical Method: SM 6200B Benzene ND ug/L 0.50 1 08/10/1521:54 71 -43-2 Bromobenzene ND ug/L 0.50 1 08/10/15 21:54 108-86-1 Bromochloromethane ND ug/L 0.50 1 08/10/15 21:54 74-97-5 Bromodichloromethane ND ug/L 0.50 1 08/10/15 21:54 75-27-4 Bromoform ND ug/L 0.50 1 08/10/1521:54 75-25-2 Bromomethane ND ug/L 5.0 1 08/10/15 21:54 74-83-9 n-Butylbenzene ND ug/L 0.50 1 08/10/15 21:54 104-51 -8 sec-Butylbenzene ND ug/L 0.50 1 08/10/1521:54 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 08/10/15 21:54 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 08/10/15 21:54 56-23-5 Chlorobenzene ND ug/L 0.50 1 08/10/15 21:54 108-90-7 Chloroethane ND ug/L 1.0 1 08/10/15 21:54 75-00-3 Chloroform ND ug/L 0.50 1 08/10/15 21:54 67-66-3 Chloromethane ND ug/L 1.0 1 08/10/15 21:54 74-87-3 2-Chlorotoluene ND ug/L 0.50 1 08/10/15 21:54 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 08/10/1521:54 106-43-4 12-Dibromo-3-chloropropane ND ug/L 1.0 1 08/10/15 21:54 96-12-8 Dibromochloromethane ND ug/L 0.50 1 08/10/15 21:54 124-48-1 12-Dibromoethane (EDB) ND ug/L 0.50 1 08/10/1521:54 106-93-4 Dibromomethane ND ug/L 0.50 1 08/10/15 21:54 74-95-3 12-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:54 95-50-1 13-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:54 541-73-1 14-Dichlorobenzene ND ug/L 0.50 1 08/10/15 21:54 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 08/10/15 21:54 75-71-8 1 ,1-Dichloroethane ND ug/L 0.50 1 08/10/15 21:54 75-34-3 12-Dichloroethane ND ug/L 0.50 1 08/10/15 21:54 107-06-2 1 ,1-Dichioroethene ND ug/L 0.50 1 08/10/1521:54 75-35-4 cis-i2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:54 156-59-2 trans-1 2-Dichloroethene ND ug/L 0.50 1 08/10/15 21:54 156-60-5 12-Dichioropropane ND ug/L 0.50 1 08/10/1521:54 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 08/10/15 21:54 142-28-9 22-Dichloropropane ND ug/L 0.50 1 08/10/15 21:54 594-20-7 li-Dichloropropene ND ug/L 0.50 1 08/10/15 21:54 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 1 08/10/15 21:54 10061-01-5 trans-1 3-Dichloropropene ND ug/L 0.50 1 08/10/15 21:54 10061-02-6 Dilsopropyl ether ND ug/L 0.50 1 08/10/15 21:54 108-20-3 Ethylbenzene ND ug/L 0.50 1 08/10/15 21:54 100-41-4 Hexachloro-13-butadiene ND ug/L 2.0 1 08/10/15 21:54 87-68-3 Isopropylbenzene (Cumene) ND ug/L 0.50 1 08/10/15 21:54 98-82-8 Methylene Chloride ND ug/L 2.0 1 08/10/15 21:54 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 08/10/15 21:54 1634-04-4 Naphthalene ND ug/L 2.0 1 08/10/15 21:54 91-20-3 n-Propylbenzene ND ug/L 0.50 1 08/10/15 21:54 103-65-1 Styrene ND ug/L 0.50 1 08/10/1521:54 100-42-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced except in full Date: 08/14/2015 03:25 PM without the written conGnt of Pace Analyticaj orica. Inc Page 16 of 41 /74eAnalyfical wwpacecom 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: MWI2 Lab ID: 92262422008 Collected: 08/06/1511:15 Received: 08/07/1514:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV 1,1,1 2-Tetrachtoroethane 1, 1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1 ,2,3-Trichlorobenzene 1 ,2,4-Trichlorobenzene 1,1 1-Trichloroethane 1,1 ,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1 ,2,3-Trichloropropane 1 ,2,4-Trimethylbenzerte 1 3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1 ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 96 % 99 % 103 % 0.50 1 08/10/15 21:54 630-20-6 0.50 1 08/10/1521:54 79-34-5 0.50 1 08/10/1521:54 127-18-4 0.50 1 08/10/15 21:54 108-88-3 2.0 1 08/10/1521:54 87-61-6 2.0 1 08/10/15 21:54 120-82-1 0.50 1 08/10/15 21:54 71-55-6 0.50 1 08/10/15 21:54 79-00-5 0.50 1 08/10/15 21:54 79-01-6 1.0 1 08/10/1521:54 75-69-4 0.50 1 08/10/1521:54 96-18-4 0.50 1 08/10/1521:54 95-63-6 0.50 1 08/10/1521:54 108-67-8 1.0 1 08/10/15 21:54 75-01-4 1.0 1 08/10115 21:54 179601-23-1 0.50 1 08/10/15 21:54 95-47-6 70-130 1 08/10/15 21:54 17060-07-0 70-130 1 08/10/15 21:54 460-00-4 70-130 1 08/10/15 21:54 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services Inc Date: 08/14/2015 03:25 PM Page 19 of 41 /TJ(ceAr4icaI www pac&aba corn 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: CREEK Lab ID: 92262422009 Collected: 08/06/15 11:30 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV 1,1,1 ,2-Tetrach!oroethane 1,1 ,2,2-Tetrachloroethane Tetrachloroethene Toluene 1 ,2,3-Trichlorobenzene 1 ,2,4-Trichlorobenzene 1,1 ,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1 ,2,3-Trichloropropane 1 ,2,4-Trimethylbenzene 1 ,3,5-Trimethylbenzene Vinyl chloride m&p-Xylene o-Xylene Surrogates 1 ,2-Dichloroethane-d4 (S) 4-Bromofluorobenzene (S) Toluene-d8 (S) Analytical Method: SM 6200B ND ug/L 0.50 1 08/10/15 22:11 630-20-6 ND ug/L 0.50 1 08/10/15 22:11 79-34-5 ND ug/L 0.50 1 08/10/15 22:11 127-18-4 ND ug/L 0.50 1 08/10/15 22:11 108-88-3 ND ug/L 2.0 1 08/10/15 22:11 87-61-6 ND ug/L 2.0 1 08/10/15 22:11 120-82-1 ND ug/L 0.50 1 08/10/15 22:11 71-55-6 ND ug/L 0.50 1 08110/15 22:11 79-00-5 ND ug/L 0.50 1 08/10/15 22:11 79-01-6 ND ug/L 1.0 1 08/10/15 22:11 75-69-4 ND ug/L 0.50 1 08/10/15 22:11 96-18-4 ND ug/L 0.50 1 08/10/15 22:11 95-63-6 ND ug/L 0.50 1 08/10/15 22:11 108-67-8 ND ug/L 1.0 1 08/10/15 22:11 75-01-4 ND ug/L 1.0 1 08/10/15 22:11 179601-23-1 ND ug/L 0.50 1 08/10/15 22:11 95-47-6 94 % 70-130 1 08/10/15 22:11 17060-07-0 98 % 70-130 1 08/10/15 22:11 460-00-4 100 % 70-130 1 08/10/15 22:11 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Paco Analytical Services. Inc Page 21 of 41 ./TAceAnIyticaI 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: EFFLUENT Lab ID: 92262422010 Collected: 08/06/15 13:55 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Lead 7.0 ug/L 5.0 1 08/10/15 16:15 08/13/15 23:01 7439-92-1 8270 MSSV Semivol Organic HVI Analytical Method: EPA 8270 Preparation Method: EPA 3510 Acenaphthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 83-32-9 Acenaphthylene ND ugIL 10.0 1 08/11/15 12:00 08/11/15 17:28 208-96-8 Anthracene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 120-12-7 Benzo(a)anthracene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 56-55-3 Benzo(a)pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 50-32-8 Benzo(b)fiuoranthene ND ug/L 10.0 1 08111/15 12:00 08/11/15 17:28 205-99-2 Benzo(g,h,i)perylene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 191-24-2 Benzo(k)fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 207-08-9 L3 Chrysene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 53-70-3 Fluoranthene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 206-44-0 Fluorene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 86-73-7 lndeno(12,3-cd)pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 193-39-5 1-Methylnaphthalene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 90-12-0 2-Methylnaphthalene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 91-57-6 Naphthalene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 91-20-3 Phenanthrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 85-01-8 Pyrene ND ug/L 10.0 1 08/11/15 12:00 08/11/15 17:28 129-00-0 Surrogates Nitrobenzene-d5 (S) 75 % 21-110 1 08/11/15 12:00 08/11/15 17:28 4165-60-0 2-Fluorobiphenyl (S) 93 % 27-110 1 08/11/15 12:00 08/11/15 17:28 321-60-8 Terphenyl-d14 (5) 61 % 31-107 1 08/11/15 12:00 08/11/15 17:28 1718-51-0 601/602 Volatiles by SM 6200 Analytical Method: SM 6200B Benzene 4.7 ug/L 1.0 1 08/11/15 11:09 71-43-2 Bromodichloromethane ND ug/L 1.0 1 08/11/15 11:09 75-27-4 Bromoform ND ug/L 1.0 1 08/11/15 11:09 75-25-2 Bromomethane ND ug/L 5.0 1 08/11/15 11:09 74-83-9 Carbon tetrachloride ND ug/L 1.0 1 08/11/15 11:09 56-23-5 Chlorobenzene ND ug/L 1.0 1 08/11/15 11:09 108-90-7 Chloroethane ND ug/L 1.0 1 08/11/15 11:09 75-00-3 Chloroform ND ug/L 1.0 1 08/11/15 11:09 67-66-3 Chloromethane ND ug/L 1.0 1 08/11/15 11:09 74-87-3 Dibromochloromethane ND ug/L 1.0 1 08/11/15 11:09 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 1 08/11/15 11:09 106-93-4 1,2-Dichlorobenzene ND ug/L 1.0 1 08/11/15 11:09 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 08/11/15 11:09 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 08/11/15 11:09 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 08/11/15 11:09 75-71-8 1,1-Dichioroethane ND ug/L 1.0 1 08/11/15 11:09 75-34-3 1,2-Dichioroethane ND ug/L 1.0 1 08/11/15 11:09 107-06-2 1,1-Dichioroethene ND ug/L 1.0 1 08/11/15 11:09 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 08/11/15 11:09 156-59-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Inc Page zz 0141 1.0 1 08/11/15 11:09 156-60-5 1.0 1 08/11/15 11:09 78-87-5 1.0 1 08/11/15 11:09 10061-01-5 1.0 1 08/11/15 11:09 10061-02-6 1.0 1 08/11/15 11:09 108-20-3 1.0 1 08/11/15 11:09 100-41-4 2.0 1 08/11/15 11:09 75-09-2 1.0 1 08/11/15 11:09 1634-04-4 2.0 1 08/11/15 11:09 91-20-3 1.0 1 08/11/15 11:09 79-34-5 1.0 1 08/11/15 11:09 127-18-4 1.0 1 08/11/15 11:09 108-88-3 1.0 1 08/11/15 11:09 71-55-6 1.0 1 08/11/15 11:09 79-00-5 1.0 1 08/11/15 11:09 79-01-6 1.0 1 08/11/15 11:09 75-69-4 1.0 1 08/11/15 11:09 75-01-4 2.0 1 08/11/15 11:09 1330-20-7 2.0 1 08/11115 11:09 179601-23-1 1.0 1 08/11/15 11:09 95-47-6 70-130 1 08/11/15 11:09 460-00-4 70-130 1 08/11/15 11:09 17060-07-0 70-130 1 08/11/15 11:09 2037-26-5 /71aceAnalytical wwwPaCeASUCOM 9800 Kincey Ave. Suite 100 huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: EFFLUENT Lab ID: 92262422010 Collected: 08/06/15 13:55 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua] 601/602 Volatiles by SM 6200 Analytical Method: SM 6200B trans-i ,2-Dichloroethene 1 ,2-Dichloropropane cis- i ,3-Dichloropropene trans-1 3-Dichloropropene Diisopropyl ether Ethylbenzene Methylene Chloride Methyl-tert-butyl ether Naphthalene 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,1 ,i-Trichloroethane 1,1 ,2-Trichloroethane Trichloroethene Trichlorofluoromethane Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1 ,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2540D Total Suspended Solids Total Suspended Solids ND ug/L ND ug/L ND ug/L ND ug/L 26.8 ug/L ND ug/L ND ug/L 3.4 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 104 % 95 % 103 % Analytical Method: SM 2540D 12.8 mg/L MIIIIIIIIIE 08/11/15 12:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services. Inc Page 23 of 41 /TAceAnalytical wwwpaceilabs.com 9800 Kincey Ave. Suite 100 l-luntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: BENNETT AND BAILEY Pace Project No.: 92262422 Sample: INF Lab ID: 92262422011 Collected: 08/06/15 13:40 Received: 08/07/15 14:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Lead 602 Volatiles by Method 6200 Benzene Chlorobenzene 1 ,2-Dichlorobenzene 1 3-Dichlorobenzene 1 4-Dichlorobenzene Diisopropyl ether Ethylbenzene lsopropylbenzene (Cumene) Methyl-tert-butyl ether Naphthalene Toluene m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1 ,2-Dichloroethane-d4 (S) Toluene-d8 (5) Analytical Method: EPA 6010 Preparation Method: EPA 3010 ND ug/L 5.0 1 08/10/15 16:15 08/13115 23:04 7439-92-1 Analytical Method: SM 6200B 2.4 ug/L 1.0 1 08/11/15 16:25 71-43-2 ND ug/L 1.0 1 08/11/15 16:25 108-90-7 ND ug/L 1.0 1 08/11/15 16:25 95-50-1 ND ug/L 1.0 1 08/11/15 16:25 541-73-1 ND ug/L 1.0 1 08/11/15 16:25 106-46-7 158 ug/L 1.0 1 08/11/15 16:25 108-20-3 ND ug/L 1.0 1 08111/15 16:25 100-41-4 ND ug/L 1.0 1 08/11/15 16:25 98-82-8 44.9 ug/L 1.0 1 08/11/15 16:25 1634-04-4 ND ug/L 2.0 1 08/11/15 16:25 91-20-3 ND ug/L 1.0 1 08/11/15 16:25 108-88-3 5.9 ug/L 2.0 1 08/11/15 16:25 179601-23-1 8.0 ug/L 1.0 1 08/11115 16:25 95-47-6 107 70-130 1 08/11/15 16:25 460-00-4 96 % 70-130 1 08/11/15 16:25 17060-07-0 102 % 70-130 1 08/11/15 16:25 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/1412015 03:25 PM without the written consent of Pace Analytical Services. Inc Page 24 of 41 /TAceAnalyfical MWpaCeb&cOm 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETTAND BAILEY Pace Project No.: 92262422 QC Batch: MPRP/1 9220 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Associated Lab Samples: 92262422001, 92262422002, 92262422003, 92262422004, 92262422005, 92262422006, 92262422007, 92262422008, 92262422009, 92262422010, 92262422011 METHOD BLANK: 1529961 Matrix: Water Associated Lab Samples: 92262422001, 92262422002, 92262422003, 92262422004, 92262422005, 92262422006, 92262422007, 92262422008, 92262422009, 92262422010, 92262422011 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead ug/L ND 5.0 08/13/15 22:12 LABORATORY CONTROL SAMPLE: 1529962 Spike LIDS LIDS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Lead ug/L 500 491 98 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1529963 1529964 MS MSD 92262422001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Lead ug/L ND 500 500 440 434 87 86 75-125 Results presented on this page are in the units indicated by the "units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services. Inc Page 25 of 41 /~aceAnalytical www.paceAab&corn 9500 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)575-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 QC Batch: MSV/32927 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 601/602 Volatiles by SM 6200 Associated Lab Samples: 92262422010 METHOD BLANK: 1530578 Associated Lab Samples: 92262422010 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 1,1,1-Trichloroethane ug/L ND 1.0 08/11/15 10:52 1,1,2,2-Tetrachloroethane ug/L ND 1.0 08/11/15 10:52 1,1,2-Trichloroethane ug/L ND 1.0 08/11/15 10:52 1,1-Dichloroethane ug/L ND 1.0 08/11/15 10:52 1,1-Dichloroethene ug/L ND 1.0 08/11/15 10:52 1,2-Dibromoethane (EDB) ug/L ND 1.0 08/11/15 10:52 1,2-Dichlorobenzene ug/L ND 1.0 08/11/15 10:52 1,2-Dichloroethane ug/L ND 1.0 08/11/15 10:52 1,2-Dichioropropane ug/L ND 1.0 08/11/15 10:52 1,3-Dichlorobenzene ug/L ND 1.0 08/11/15 10:52 1,4-Dichlorobenzene ug/L ND 1.0 08/11/15 10:52 Benzene ug/L ND 1.0 08/11/15 10:52 Bromodichloromethane ug/L ND 1.0 08/11/15 10:52 Bromoform ug/L ND 1.0 08/11/15 10:52 Bromomethane ug/L ND 5.0 08/11/15 10:52 Carbon tetrachloride ug/L ND 1.0 08/11/15 10:52 Chlorobenzene ug/L ND 1.0 08/11/15 10:52 Chloroethane ug/L ND 1.0 08/11/15 10:52 Chloroform ug/L ND 1.0 08/11/15 10:52 Chloromethane ug/L ND 1.0 08/11/15 10:52 cis-1,2-Dichloroethene ug/L ND 1.0 08/11/15 10:52 cis- 1,3-Dichloropropene ug/L ND 1.0 08/11/15 10:52 Dibromochloromethane ug/L ND 1.0 08/11/15 10:52 Dichlorodifluoromethane ug/L ND 1.0 08/11/15 10:52 Diisopropyl ether ug/L ND 1.0 08/11/15 10:52 Ethylbenzene ug/L ND 1.0 08/11/15 10:52 m&p-Xylene ug/L ND 2.0 08111/15 10:52 Methyl-tert-butyl ether ug/L ND 1.0 08/11/15 10:52 Methylene Chloride ug/L ND 2.0 08/11/15 10:52 Naphthalene ug/L ND 2.0 08/11/15 10:52 o-Xylene ug/L ND 1.0 08/11/15 10:52 Tetrachloroethene ug/L ND 1.0 08/11/15 10:52 Toluene ug/L ND 1.0 08/11/15 10:52 trans-i ,2-Dichloroethene ug/L ND 1.0 08/11/15 10:52 trans-i ,3-Dichloropropene ug/L ND 1.0 08/11/15 10:52 Trichloroethene ug/L ND 1.0 08/11/15 10:52 Trichlorofluoromethane ug/L ND 1.0 08/11/15 10:52 Vinyl chloride ug/L ND 1.0 08/11/15 10:52 Xylene (Total) ug/L ND 2.0 08/11/15 10:52 1,2-Dichloroethane-d4 (S) % 95 70-130 08/11/15 10:52 4-Bromofluorobenzene (S) 98 70-130 08/11/15 10:52 Qualifiers Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Puce Analytical Secacea, Inc Page 26 of 41 /iA'ceAnIyticaI wwwPace4ab&OOM 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 METHOD BLANK: 1530578 Associated Lab Samples: 92262422010 Parameter Units Toluene-d8 (S) % Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers 100 70-130 08/11/15 10:52 LABORATORY CONTROL SAMPLE: 1530579 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1-Trichloroethane ug/L 50 49.4 99 60-140 1,1,2,2-Tetrachloroethane ug/L 50 48.4 97 60-140 1,1,2-Trichloroethane ug/L 50 49.8 100 60-140 1,1-Dichloroethane ug/L 50 50.0 100 60-140 1,1-Dichloroethene ug/L 50 53.9 108 60-140 1,2-Dibromoethane (EDB) ug/L 50 51.0 102 60-140 1,2-Dichlorobenzene ug/L 50 51.0 102 60-140 1,2-Dichloroethane ug/L 50 43.3 87 60-140 1,2-Dichloropropane ug/L 50 49.3 99 60-140 1,3-Dichlorobenzene ug/L 50 45.6 91 60-140 1,4-Dichlorobenzene ug/L 50 47.2 94 60-140 Benzene ug/L 50 52.3 105 60-140 Bromodichloromethane ug/L 50 50.0 100 60-140 Bromoform ug/L 50 47.6 95 60-140 Bromomethane ug/L 50 40.8 82 60-140 Carbon tetrachloride ug/L 50 52.1 104 60-140 Chlorobenzene ug/L 50 47.4 95 60-140 Chloroethane ug/L 50 51.6 103 60-140 Chloroform ug/L 50 51.7 103 60-140 Chloromethane ug/L 50 51.0 102 60-140 cis- 1,2-Dichloroethene ug/L 50 51.0 102 60-140 cis-1,3-Dichloropropene ug/L 50 52.1 104 60-140 Dibromochloromethane ug/L 50 49.4 99 60-140 Dichlorodifluoromethane ug/L 50 61.5 123 60-140 Diisopropyl ether ug/L 50 55.9 112 60-140 Ethylbenzene ug/L 50 46.7 93 60-140 m&p-Xylene ug/L 100 95.4 95 60-140 Methyl-tert-butyl ether ug/L 50 51.9 104 60-140 Methylene Chloride ug/L 50 55.0 110 60-140 Naphthalene ug/L 50 44.5 89 60-140 o-Xylene ug/L 50 48.4 97 60-140 Tetrachloroethene ug/L 50 47.7 95 60-140 Toluene ug/L 50 50.1 100 60-140 trans-1,2-Dichloroethene ug/L 50 52.4 105 60-140 trans-1,3-Dichloropropene ug/L 50 50.3 101 60-140 Trichloroethene ug/L 50 46.5 93 60-140 Trichlorofluoromethane ug/L 50 55.2 110 60-140 Vinyl chloride ug/L 50 55.5 111 60-140 Xylene (Total) ug/L 150 144 96 60-140 Results presented on this page are in the units indicated by the Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08114/2015 03:25 PM without the written consent of Pace Analytical Services, Inc Page 27 of 41 74eAnaI4icaI vwpacjm 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 LABORATORY CONTROL SAMPLE: 1530579 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits 1,2-Dichloroethane-d4 (S) 99 70-130 4-Bromofluorobenzene (5) 100 70-130 Toluene-d8 (S) % 102 70-130 Qualifiers Results presented on this page are in the units indicated by the Units' column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical SGMCeC. Inc Page 23 of 41 /AeAr,aIyticaI' wwwPacaM&GOM 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 QC Batch: MSV/32925 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 602 by 6200B Associated Lab Samples: 92262422011 METHOD BLANK: 1530471 Associated Lab Samples: 92262422011 Parameter Units Matrix: Blank Result Water Reporting Limit Analyzed 12-Dichlorobenzene ug/L ND 1.0 08/11/15 10:52 13-Dichlorobenzene ug/L ND 1.0 08/11/15 10:52 1,4-Dichlorobenzene ug/L ND 1.0 08/11/15 10:52 Benzene ug/L ND 1.0 08/11/15 10:52 Chlorobenzene ug/L ND 1.0 08/11/15 10:52 Diisopropyi ether ug/L ND 1.0 08/11/15 10:52 Ethylbenzene ug/L ND 1.0 08/11/15 10:52 lsopropylbenzene (Cumene) ug/L ND 1.0 08/11/15 10:52 m&p-Xylene ug/L ND 2.0 08/11/15 10:52 Methyl-tert-butyl ether ug/L ND 1.0 08/11/15 10:52 Naphthalene ug/L ND 2.0 08/11/15 10:52 o-Xylene ug/L ND 1.0 08/11/15 10:52 Toluene ug/L ND 1.0 08/11/15 10:52 1,2-Dichloroethane-d4 (5) % 95 70-130 08/11/15 10:52 4-Bromofluorobenzene (5) % 98 70-130 08111/15 10:52 Toluene-d8 (5) % 100 70-130 08/11/15 10:52 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 1530472 Units Spike Conc. LCS LCS Result % Rec 1 2-Dichlorobenzene ug/L 50 51.0 1 ,3-Dichlorobenzene ug/L 50 45.6 1 4-Dichlorobenzene ug/L 50 47.2 Benzene ug/L 50 52.3 Chlorobenzene ug/L 50 47.4 Diisopropyl ether ug/L 50 55.9 Ethylbenzerie ug/L 50 46.7 lsopropylbenzene (Cumene) ug/L 50 52.7 m&p-Xylene ug/L 100 95.4 Methyl-tert-butyl ether ug/L 50 51.9 Naphthalene ug/L 50 44.5 o-Xylene ug/L 50 48.4 Toluene ug/L 50 50.1 1 ,2-Dichloroethane-d4 (5) % 4-Bromofluorobenzene (S) % Toluene-d8 (5) % % Rec Limits 102 60-140 91 60-140 94 60-140 105 60-140 95 60-140 112 60-140 93 60-140 105 60-140 95 60-140 104 60-140 89 60-140 97 60-140 100 60-140 99 70-130 100 70-130 102 70-130 Qualifiers Results presented on this page are in the units indicated by the 'units column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Anslyticoi Sri—s. Inc Pe 25 of 41 TKceAnalXical' acab& corn 9800 Kincey Ave. Suite 100 Nuntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 QC Batch: MSV/32913 Analysis Method: SM 6200B QC Batch Method: SM 6200B Analysis Description: 6200B MSV Associated Lab Samples: 92262422001, 92262422002, 92262422003, 92262422004, 92262422005, 92262422006, 92262422007, 92262422008, 92262422009 METHOD BLANK: 1529807 Matrix: Water Associated Lab Samples: 92262422001, 92262422002, 92262422003, 92262422004, 92262422005, 92262422006, 92262422007, 92262422008, 92262422009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachioroethane ug/L ND 0.50 08/10/15 19:41 1,1,1-Trichloroethane ug/L ND 0.50 08/10/15 19:41 1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/10/15 19:41 1,1,2-Trichloroethane ug/L ND 0.50 08/10/15 19:41 1,1-Dichioroethane ug/L ND 0.50 08/10/15 19:41 1,1-Dichloroethene ug/L ND 0.50 08/10/15 19:41 1,1-Dichloropropene ug/L ND 0.50 08/10/15 19:41 1,2,3-Trichlorobenzene ug/L ND 2.0 08/10/15 19:41 1,2,3-Trichloropropane ug/L ND 0.50 08/10/15 19:41 1,2,4-Trichlorobenzene ug/L ND 2.0 08/10/15 19:41 1,2,4-Trimethylbenzene ug/L ND 0.50 08/10/15 19:41 1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/10/15 19:41 1,2-Dibromoethane (EDB) ug/L ND 0.50 08/10/15 19:41 1,2-Dichlorobenzene ug/L ND 0.50 08/10/15 19:41 1,2-Dichioroethane ug/L ND 0.50 08/10/15 19:41 1,2-Dichloropropane ug/L ND 0.50 08/10/15 19:41 1,3,5-Trimethylberizene ug/L ND 0.50 08/10/15 19:41 1,3-Dichlorobenzene ug/L ND 0.50 08/10/15 19:41 1,3-Dichloropropane ug/L ND 0.50 08/10/15 19:41 1 ,4-Dichlorobenzene ug/L ND 0.50 08/10/15 19:41 2,2-Dichloropropane ug/L ND 0.50 08/10/15 19:41 2-Chlorotoluene ug/L ND 0.50 08/10/15 19:41 4-Chlorotoluene ug/L ND 0.50 08/10/15 19:41 Benzene ug/L ND 0.50 08/10/15 19:41 Bromobenzene ug/L ND 0.50 08/10/15 19:41 Bromochloromethane ug/L ND 0.50 08/10/15 19:41 Bromodichloromethane ug/L ND 0.50 08/10/15 19:41 Bromoform ug/L ND 0.50 08/10/15 19:41 Bromomethane ug/L ND 5.0 08/10/15 19:41 Carbon tetrachloride ug/L ND 0.50 08/10/15 19:41 Chlorobenzene ugIL ND 0.50 08/10/15 19:41 Chloroethane ug/L ND 1.0 08/10/15 19:41 Chloroform ug/L ND 0.50 08/10/15 19:41 Chloromethane ug/L ND 1.0 08/10/15 19:41 cis-1,2-Dichloroethene ug/L ND 0.50 08/10/15 19:41 cis-1,3-Dichloropropene ug/L ND 0.50 08/10/15 19:41 Dibromochloromethane ug/L ND 0.50 08/10/15 19:41 Dibromomethane ug/L ND 0.50 08/10/15 19:41 Dichlorodifluoromethane ug/L ND 0.50 08/10/15 19:41 Diisopropyl ether ug/L ND 0.50 08/10/15 19:41 Results presented on this page are in the units indicated by the Units column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08114/2015 03:25 PM without the written consent of Pace Analytical Services. Inc Page 30 of 41 /'AceAn/yticaI' wpacelabacom 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 METHOD BLANK: 1529807 Matrix: Water Associated Lab Samples: 92262422001, 92262422002, 92262422003, 92262422004, 92262422005, 92262422006, 92262422007, 92262422008, 92262422009 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Ethylbenzene ug/L ND 0.50 08/10115 19:41 Hexachloro-1,3-butadiene ug/L ND 2.0 08/10/15 19:41 Isopropylbenzene (Cumene) ug/L ND 0.50 08/10/15 19:41 m&p-Xylene ug/L ND 1.0 08/10/15 19:41 Methyl-tert-butyl ether ug/L ND 0.50 08/10/15 19:41 Methylene Chloride ug/L 2.1 2.0 08/10/15 19:41 n-Butylbenzene ug/L ND 0.50 08/10/15 19:41 n-Propylbenzene ug/L ND 0.50 08/10/15 19:41 Naphthalene ug/L ND 2.0 08/10/15 19:41 o-Xylene ug/L ND 0.50 08/10/15 19:41 sec-Butylbenzene ug/L ND 0.50 08/10/15 19:41 Styrene ug/L ND 0.50 08/10/15 19:41 tert-Butylbenzene ug/L ND 0.50 08/10/15 19:41 Tetrachloroethene ug/L ND 0.50 08/10/15 19:41 Toluene ug/L ND 0.50 08/10115 19:41 trans-i ,2-Dichloroethene ug/L ND 0.50 08/10/15 19:41 trans-i ,3-Dichloropropene ug/L ND 0.50 08/10/15 19:41 Trichloroethene ug/L ND 0.50 08/10/15 19:41 Trichiorofluoromethane ug/L ND 1.0 08/10/15 19:41 Vinyl chloride ug/L ND 1.0 08/10/15 19:41 1 ,2-Dichloroethane-d4 (5) % 96 70-130 08/10/15 19:41 4-Bromofluorobenzene (5) % 98 70-130 08/10/15 19:41 Toluene-d8 (S) % 103 70-130 08/10/15 19:41 LABORATORY CONTROL SAMPLE: Parameter 1529808 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.1 102 60-140 1,1,1-Trichloroethane ug/L 50 52.1 104 60-140 1,1,2,2-Tetrachloroethane ug/L 50 52.1 104 60-140 1,1,2-Trichioroethane ug/L 50 50.3 101 60-140 1,1-Dichloroethane ug/L 50 52.6 105 60-140 1,1-Dichloroethene ug/L 50 55.6 111 60-140 1,1-Dichloropropene ug/L 50 56.2 112 60-140 1,2,3-Trichlorobenzene ug/L 50 51.1 102 60-140 1,2,3-Trichioroproparie ug/L 50 48.7 97 60-140 1,2,4-Trichlorobenzene ug/L 50 49.3 99 60-140 1,2,4-Trimethylbenzene ug/L 50 51.7 103 60-140 1 ,2-Dibromo-3-chloropropane ug/L 50 53.6 107 60-140 1,2-Dibromoethane (EDB) ug/L 50 54.3 109 60-140 1,2-Dichlorobenzene ug/L 50 51.1 102 60-140 1,2-Dichloroethane ug/L 50 45.8 92 60-140 1,2-Dichloropropane ug/L 50 50.8 102 60-140 Results presented on this page are in the units indicated by the Units column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services. Inc Page 31 of 41 /~KceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 LABORATORY CONTROL SAMPLE: Parameter 1529808 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 13,5-Trimethylbenzene ug/L 50 51.2 102 60-140 1,3-Dichlorobenzene ug/L 50 51.9 104 60-140 1,3-Dichloropropane ug/L 50 52.5 105 60-140 1,4-Dichlorobenzene ug/L 50 50.0 100 60-140 2,2-Dichloropropane ug/L 50 51.4 103 60-140 2-Chlorotoluene ug/L 50 50.8 102 60-140 4-Chlorotoluene ug/L 50 50.7 101 60-140 Benzene ug/L 50 54.7 109 60-140 Bromobenzene ug/L 50 52.9 106 60-140 Bromochloromethane ug/L 50 58.3 117 60-140 Bromodichloromethane ug/L 50 52.5 105 60-140 Bromoform ug/L 50 49.6 99 60-140 Bromomethane ug/L 50 43.4 87 60-140 Carbon tetrachloride ug/L 50 53.5 107 60-140 Chlorobenzene ug/L 50 50.7 101 60-140 Chloroethane ug/L 50 49.1 98 60-140 Chloroform ug/L 50 54.9 110 60-140 Chloromethane ug/L 50 46.5 93 60-140 cis-1,2-Dichloroethene ug/L 50 53.8 108 60-140 cis-1,3-Dichloropropene ug/L 50 52.7 105 60-140 Dibromochloromethane ug/L 50 52.7 105 60-140 Dibromomethane ug/L 50 53.5 107 60-140 Dichlorodifluoromethane ug/L 50 66.1 132 60-140 Diisopropyl ether ug/L 50 59.0 118 60-140 Ethylbenzene ug/L 50 49.6 99 60-140 Hexachloro-1,3-butadiene ug/L 50 58.3 117 60-140 lsopropylbenzene (Cumene) ug/L 50 55.8 112 60-140 m&p-Xylene ug/L 100 101 101 60-140 Methyl-tert-butyl ether ug/L 50 54.5 109 60-140 Methylene Chloride ug/L 50 59.2 118 60-140 n-Butylbenzene ug/L 50 51.1 102 60-140 n-Propylbenzene ug/L 50 50.0 100 60-140 Naphthalene ug/L 50 53.0 106 60-140 o-Xylene ug/L 50 51.8 104 60-140 sec-Butylbenzene ug/L 50 52.0 104 60-140 Styrene ug/L 50 53.2 106 60-140 tert-Butylbenzene ug/L 50 43.4 87 60-140 Tetrachloroethene ug/L 50 49.9 100 60-140 Toluene ug/L 50 51.7 103 60-140 trans-i ,2-Dichloroethene ug/L 50 54.2 108 60-140 trans-1,3-Dichloropropene ug/L 50 53.3 107 60-140 Trichioroethene ug/L 50 47.6 95 60-140 Trichiorofluoromethane ug/L 50 52.2 104 60-140 Vinyl chloride ug/L 50 56.6 113 60-140 1 ,2-Dichloroethane-d4 (S) 100 70-130 4-Bromofluorobenzene (S) % 103 70-130 Toluene-d8 (5) % 102 70-130 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical 5rvices Inc Page 32 of 41 [KceAnalytbl 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1529809 1529810 MS MSD 92262048001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual 1,11,2-Tetrachloroethane ug/L <0.50 20 20 19.1 18.9 95 95 60-140 1 1,1,1-Trichloroethane ug/L <0.50 20 20 20.8 21.3 104 106 60-140 2 1,1,2,2-Tetrachloroethane ug/L <0.50 20 20 21.0 21.3 105 107 60-140 1 1,1,2-Trichloroethane ug/L <0.50 20 20 19.9 19.5 100 98 60-140 2 1,1-Dichloroethane ug/L <0.50 20 20 21.5 21.4 107 107 60-140 0 1,1-Dichloroethene ug/L <0.50 20 20 24.0 28.3 120 142 60-140 17 Ml 1,1-Dichloropropene ug/L <0.50 20 20 24.0 23.2 120 116 60-140 3 1,2,3-Trichlorobenzene ug/L <2.0 20 20 17.9 18.1 89 90 60-140 1 1,2,3-Trichloropropane ug/L <0.50 20 20 20.0 19.9 100 100 60-140 0 1,2,4-Trichlorobenzene ug/L <2.0 20 20 17.3 17.8 87 89 60-140 3 1,2,4-Trimethylbenzene ug/L <0.50 20 20 20.9 21.3 105 106 60-140 2 1,2-Dibromo-3-chloropropane ug/L <1.0 20 20 18.4 19.0 92 95 60-140 4 1,2-Dibromoethane (EDB) ug/L <0.50 20 20 20.8 20.2 104 101 60-140 3 1,2-Dichlorobenzene ug/L <0.50 20 20 21.2 20.5 106 102 60-140 4 1,2-Dichloroethane ug/L <0.50 20 20 17.7 17.6 88 87 60-140 1 1,2-Dichloropropane ug/L <0.50 20 20 20.4 20.3 102 101 60-140 1 1,3,5-Trimethylbenzene ug/L <0.50 20 20 21.8 21.3 109 106 60-140 2 1,3-Dichlorobenzene ug/L <0.50 20 20 22.0 20.2 110 101 60-140 9 1,3-Dichloropropane ug/L <0.50 20 20 20.3 19.8 102 99 60-140 2 1,4-Dichlorobenzene ug/L <0.50 20 20 20.0 19.7 100 98 60-140 2 2,2-Dichloropropane ug/L <0.50 20 20 17.3 17.2 87 86 60-140 1 2-Chlorotoluene ug/L <0.50 20 20 23.0 21.7 115 109 60-140 5 4-Chlorotoluene ug/L <0.50 20 20 21.9 21.6 110 108 60-140 1 Benzene ug/L <0.50 20 20 22.4 22.3 112 112 60-140 0 Bromobenzene ug/L <0.50 20 20 23.2 21.0 116 105 60-140 10 Bromochloromethane ug/L <0.50 20 20 22.9 22.9 114 115 60-140 0 Bromodichloromethane ug/L <0.50 20 20 19.4 19.4 97 97 60-140 0 Bromoform ug/L <0.50 20 20 17.4 15.5 87 78 60-140 12 Bromomethane ug/L <5.0 20 20 15.3 14.9 77 74 60-140 3 Carbon tetrachloride ug/L <0.50 20 20 21.5 21.6 108 108 60-140 0 Chlorobenzene ug/L <0.50 20 20 20.4 19.8 102 99 60-140 3 Chloroethane ug/L <1.0 20 20 26.6 19.8 133 99 60-140 29 Chloroform ug/L <0.50 20 20 21.9 21.1 109 106 60-140 4 Chloromethane ug/L <1.0 20 20 20.4 21.2 102 106 60-140 4 cis- 1,2-Dichloroethene ug/L <0.50 20 20 21.8 21.6 109 108 60-140 1 cis-1,3-Dichloropropene ug/L <0.50 20 20 19.0 19.3 95 96 60-140 1 Dibromochloromethane ug/L <0.50 20 20 18.3 17.3 92 87 60-140 6 Dibromomethane ug/L <0.50 20 20 20.4 19.7 102 99 60-140 3 Dichlorodifluoromethane ug/L <0.50 20 20 28.8 28.1 144 141 60-140 2 Ml Diisopropyl ether ug/L <0.50 20 20 23.1 22.9 115 114 60-140 1 Ethylbenzene ug/L <0.50 20 20 20.4 19.4 102 97 60-140 5 Hexachloro-1,3-butadiene ug/L <2.0 20 20 22.0 21.9 110 109 60-140 1 lsopropylbenzene (Cumene) ug/L <0.50 20 20 25.5 21.5 128 107 60-140 17 m&p-Xylene ug/L <1.0 40 40 43.4 39.4 109 99 60-140 10 Methyl-tert-butyl ether ug/L 7.1 20 20 28.4 28.4 107 107 60-140 0 Methylene Chloride ug/L <2.0 20 20 22.7 22.4 113 112 60-140 1 Results presented on this page are in the units indicated by the "Units column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services, Inc Page 33 of 41 /'iJ5ceAnalylical rvwpac&b&m 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1529809 1529810 MS MSD 92262048001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual n-Butylbenzene ug/L <0.50 20 20 22.3 19.5 111 97 60-140 13 n-Propylbenzene ug/L <0.50 20 20 22.2 20.2 111 101 60-140 9 Naphthalene ug/L <2.0 20 20 18.7 19.5 93 97 60-140 4 o-Xylene ug/L <0.50 20 20 22.5 19.6 112 98 60-140 14 sec-Butylbenzene ug/L <0.50 20 20 21.2 21.7 106 109 60-140 2 Styrene ug/L <0.50 20 20 22.2 18.9 111 94 60-140 16 tert-Butylbenzene ug/L <0.50 20 20 18.1 18.4 91 92 60-140 1 Tetrachloroethene ug/L <0.50 20 20 21.2 21.0 106 105 60-140 1 Toluene ug/L <0.50 20 20 21.0 20.8 105 104 60-140 1 trans-1,2-Dichloroethene ug/L <0.50 20 20 22.3 22.1 111 111 60-140 1 trans-13-Dichloropropene ug/L <0.50 20 20 18.2 18.7 91 93 60-140 2 Trichioroethene ug/L <0.50 20 20 19.5 19.9 98 99 60-140 2 Trichlorofluoromethane ug/L <1.0 20 20 29.3 26.7 147 133 60-140 9 Ml Vinyl chloride ug/L <1.0 20 20 23.8 22.7 119 113 60-140 5 1 2-Dichloroethane-d4 (5) % 94 95 70-130 4-Bromofluorobenzene (5) % 110 103 70-130 Toluene-d8 (5) % 100 101 70-130 Results presented on this page are in the units indicated by the Units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services, Inc Page 34 of 41 /71aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 QC Batch: OEXT/36988 Analysis Method: EPA 8270 QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV Associated Lab Samples: 92262422001 92262422002, 92262422003, 92262422004, 92262422010 METHOD BLANK: 1530415 Matrix: Water Associated Lab Samples: 92262422001 92262422002, 92262422003, 92262422004, 92262422010 Blank Reporting Parameter Units Result Limit Analyzed 1-Methylnaphthalene ug/L ND 10.0 08/11/15 13:42 2-Methyl naphtha lene ug/L ND 10.0 08/11/15 13:42 Acenaphthene ug/L ND 10.0 08/11/15 13:42 Acenaphthylene ug/L ND 10.0 08/11/15 13:42 Anthracene ug/L ND 10.0 08/11/15 13:42 Benzo(a)anthracene ug/L ND 10.0 08/11/15 13:42 Benzo(a)pyrene ug/L ND 10.0 08/11/15 13:42 Benzo(b)fluoranthene ug/L ND 10.0 08/11/15 13:42 Benzo(g,h,i)perylene ug/L ND 10.0 08/11/15 13:42 Benzo(k)fluoranthene ug/L ND 10.0 08/11/15 13:42 Chrysene ug/L ND 10.0 08/11/15 13:42 Dibenz(a,h)anthracene ug/L ND 10.0 08/11/15 13:42 Fluoranthene ug/L ND 10.0 08/11/15 13:42 Fluorene ug/L ND 10.0 08/11/15 13:42 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 08/11/15 13:42 Naphthalene ug/L ND 10.0 08/11/15 13:42 Phenanthrene ug/L ND 10.0 08/11/15 13:42 Pyrene ug/L ND 10.0 08/11/15 13:42 2-Fluorobiphenyl (S) 94 27-110 08/11/15 13:42 Nitrobenzene-d5 (5) % 76 21-110 08/11/15 13:42 Terphenyl-d14 (S) % 97 31-107 08/11/15 13:42 Qualifiers LABORATORY CONTROL SAMPLE & LCSD: 1530416 1530417 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 1-Methylnaphthalene ug/L 50 36.0 32.6 72 65 34-113 10 30 2-Methylnaphthalene ug/L 50 35.8 31.7 72 63 33-120 12 30 Acenaphthene ug/L 50 45.4 40.1 91 80 48-114 12 30 Acenaphthylene ug/L 50 45.7 40.6 91 81 48-112 12 30 Anthracene ug/L 50 49.4 46.9 99 94 57-118 5 30 Benzo(a)a nth race ne ug/L 50 46.5 44.5 93 89 56-121 4 30 Benzo(a)pyrene ug/L 50 62.8 62.1 126 124 55-127 1 30 Benzo(b)fluoranthene ug/L 50 58.2 57.3 116 115 53-128 1 30 Benzo(g,h,i)perylene ug/L 50 59.1 57.2 118 114 54-125 3 30 Benzo(k)fluoranthene ug/L 50 62.1 63.3 124 127 51-123 2 30 LO Chrysene ug/L 50 47.6 45.7 95 91 58-127 4 30 Dibenz(a,h)anthracene ug/L 50 59.9 57.7 120 115 53-129 4 30 Fluoranthene ug/L 50 51.2 47.9 102 96 57-125 7 30 Fluorene ug/L 50 43.8 39.2 88 78 53-118 11 30 Indeno(1,2,3-cd)pyrene ug/L 50 58.8 57.3 118 115 55-128 2 30 Results presented on this page are in the units indicated by the units' column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services. Inc PO9C 35 of 41 77,laceAnaykal pac&ab& corn 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 LABORATORY CONTROL SAMPLE & LCSD: 1530416 1530417 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Naphthalene ug/L 50 41.1 36.2 82 72 32-120 13 30 Phenanthrene ug/L 50 47.0 44.6 94 89 57-117 5 30 Pyrene ug/L 50 44.7 46.2 89 92 55-122 3 30 2-Fluorobiphenyl (S) % 93 78 27-110 Nitrobenzene-d5 (S) % 83 74 21-110 Terphenyl-d14 (S) % 94 92 31-107 Results presented on this page are in the units indicated by the Units column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 08/14/2015 03:25 PM without the written consent of PcaAnalyhcsl Services, I- Page 36 of 41 fAaceAnalytkal pacebs corn 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: BENNETT AND BAILEY Pace Project No.: 92262422 QC Batch: WET/39404 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92262422010 METHOD BLANK: 1530510 Matrix: Water Associated Lab Samples: 92262422010 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 08/11/15 12:17 LABORATORY CONTROL SAMPLE: 1530511 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 250 100 90-110 SAMPLE DUPLICATE: 1530512 92262559001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 176 466 90 D6 SAMPLE DUPLICATE: 1530513 92262280001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 13.0 15.8 19 D6 Results presented on this page are in the units indicated by the 'Units" column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical Services, Inc. Page 37 of 41 Kincey Ave. Suite 100 ,/"iteAnaIyticaI 9800 Huntersville, NC 28078 wswpacbarm (704)875-9092 QUALIFIERS Project: BENNETT AND BAILEY Pace Project No.: 92262422 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1 ,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. LO Analyte recovery in the laboratory control sample (LCS) was outside QC limits. L3 Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias. Ml Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace Analytical services, Inc. Page 38 of 41 7JAceAnalytica( cww.paceab& corn 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: BENNETT AND BAILEY Pace Project No. 92262422 Lab ID Sample ID QC Batch Method QC Batch Analytical Method 92262422001 MW14 EPA 3010 MPRP/19220 EPA 6010 92262422002 WWI EPA 3010 MPRP/19220 EPA 6010 92262422003 MW13 EPA 3010 MPRP119220 EPA 6010 92262422004 MW9 EPA 3010 MPRP/19220 EPA 6010 92262422005 DCWI EPA 3010 MPRPI19220 EPA 6010 92262422006 MW2 EPA 3010 MPRP/19220 EPA 6010 92262422007 MW5 EPA 3010 MPRP/19220 EPA 6010 92262422008 MW12 EPA 3010 MPRP/19220 EPA 6010 92262422009 CREEK EPA 3010 MPRP/19220 EPA 6010 92262422010 EFFLUENT EPA 3010 MPRP/19220 EPA 6010 92262422011 INF EPA 3010 MPRPI19220 EPA 6010 92262422001 MW14 EPA 3510 0EXTI36988 EPA 8270 92262422002 WWI EPA 3510 OEXT/36988 EPA8270 92262422003 MW13 EPA 3510 OEXT/36988 EPA 8270 92262422004 MW9 EPA 3510 OEXT/36988 EPA 8270 92262422010 EFFLUENT EPA 3510 OEXT/36988 EPA 8270 92262422010 EFFLUENT SM 6200B MSV/32927 92262422011 INF SM 6200B MSV/32925 92262422001 MW14 SM 6200B MSV/32913 92262422002 WWI SM 6200B MSV/32913 92262422003 MW13 SM 6200B MSV/32913 92262422004 MW9 SM 6200B MSV/32913 92262422005 DCWI SM 6200B MSV/32913 92262422006 MW2 SM 6200B MSV/32913 92262422007 MW5 SM 6200B MSV132913 92262422008 MWI2 SM 6200B MSV132913 92262422009 CREEK SM 6200B MSVI32913 92262422010 EFFLUENT SM 2540D WET/39404 Analytical Batch CPu 7283 IC P/17283 IC P/17283 IC P/17283 IC P/172 83 IC P/17283 lOP/i 7283 lop/i 7283 IC P/17283 lop/i 7283 lOP/i 7283 MSSV/1 1072 MSSV/1 1072 MSSV/1 1072 MSSV/1 1072 MSSV/1 1072 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 08/14/2015 03:25 PM without the written consent of Pace An2IyticI Serinec. Inc Page 39 of 41 Document Number: Issuing Authority: F-CHR-CS-003-rev.1 6 Pace Huntersvil!e QuaUtv Office Client Name: * Page 2 of 2 is for Internal Use Only Courier: fl Fed Ex LI UPSLI USPIJ ClientLili ComrnercialL]ther - Custody Seal on Cooler/Box Present LII yes ~~no Seals intact LI yI__ 1RrOJ ate Packing Material: Bubble \ifljp LI Bubble Bagsone Other_________ Thermometer Used:Siiii 404 ' Type o et Blue None ,'Samples on ice, cooling process has begun Temp Correction Factor T1401 No Correction _/____ Corrected Cooler Temp:. 1 c Biological Tissue is Frozen: Yes No [!cLontents: Temp should be above freezing to 6*C Comments: Chain of_ Custody Present: /t 'Y9 ONo ON/A 1. Chainof CustodyFilledOut: /Yes ONo ON/A 2. Chainof CustodyRelinquished: __ ONo ON/A 3. SamplerName&Signature onCOC: ONo ON/A 4. Samples Arrived within Hold Time: /3'Yes DNo/DN/A 5, ShortHoldTimeAnalysis(<72hr): DYes ___ ON/A 6. Rush Turn Around Time Requested: DYps_ o ON/A 7. SufficientVolume: _ DN0 ON/A 8. Correct Containers Used: 4No ON/A 9. -Pace Containers Used: __l'e, ONo ON/A Containers Intact: 1s ONo ON/A 10, FilteredvolumereceivedforDissolvedtests OYe - ENo 11. Sample Labels match CCC: es ONo ON/A 12. -Includes date/time/ID/Analysis Matrix: Z All containers needing preservation have been checked. / I1_JYes EINo 11 N/A 13. All containers needing preservation are found to be in ONo ON/A compliance with EPA recommendation. ;~/Yy~ exceptions: VOA, coirorra,TOO,O&G,Wt.DRO(water) )e{s ONo Samples checked for dechlorination: AYes ON7 ON/A 14, HeadspaceinVOA Vials (>6mm): OYes/No DN/ ¶5. Trip Blank Present: OYes ONe &A J6. Trip Blank Custody Seals Present OVes ON0 Pace Trip Blank Lot # (if purchased): Client Notification! Resolution: Field Data Required? Y / N Person Contacted: Date/Time: Comments! Resolution: SCURF Review:LI-1/1/5 Date: SRF Review: [Y\'(Y1) Date: ?Ho-iS Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e out of hold, incorrect preservative, out of temp, incorrect containers) WO#: 92262422 111111 1111111111111111 92262422 Page 40 of 41 LJO ft 968d E C) 0 U rn V o Ow 4a E 0 U)0 0w GJE w V —9 Ui >. 0 O -J (n-i 9 IL- - Z —c <rn Io I- r — — 4 MA N (*lQç( ('8 N/A A NIA N/A Ja 4) a3l IL NIA 4N!AN/A :p - ---- --- .- tial I W I OSei HORN L. ONH 'OS-'H III p.usidu i -i II V'i I >c.. LL 1VdI1dIWS o — ui zc 2 a w ) w w In In C > 0 U 0 -____ --------.----. --------------- 1B=o i 3QO3Xt8i I E IIEEE h Lw o Co CL S E - .--.. - -- '0 o w .0 = S----. ' u --- CL z --- ,_ .--- -;J - --' -- I.1 . - - - IL IL w ' w 0 ---' --- - --- - - -- E ro 2 g #W311 APPENDIX C NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory, Governor Division of Waste Management Donald R van der Vaal UST Section Secretary August 24 2015 CFElIfIED -MAIL 7011 1570 OOj 8546 100 Mr, Richard Morgan 912 Long Ridge WinstonSalem, NC 27106 Re Trailer Park Well Sample Results Bennett & Bailey Jncideit 2827 South Stratford Road, WinstonSa1em Forsyth County Incident Number: 14498 Risk Classification: High Ranking: H290D Dear Mr. Morgan: This letter is to notify you in writing the sample results for the water supply well located at 2827 South Stratford Road. The results indicate that the water is contaminated. The results were sent to David Lilley, State Toxicologist, for a health risk evaluation. Based on his evaluation, the water is not potable and should not be used for drinking or cooking. Please notify the residences at the trailer park concerning these results and provide potable water to them immediately. Attached to this letter is David Lilley's evaluation. If you have any questions, please contact Dave Lilley at (919) 707-8241 or me at the address or telephone number listed below for the Winston-Salem Regional Office. Sincerely, 4 Tirornas Moore Hydrogeologist Winston-Salem Regional Office cc: Forsyth County Health Department Wiriton-Salem (WS) - 585 Waughtown Street, Winston-Salem, NC 27107 (336) 771-5000 An Equal Opprtinity Atf;mat'ie Action Empoyer - EQ % Recycled iit) % Post Consr.r ape' NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory Donald R. van der \Iaart Governor Secretary August 24. 2015 TO: Thomas Moore Winston-Salem Regional Office NC UST Section RE: Health Risk Evaluation Incident Number 14498 Bennett & Bailey Trailer Park Well Sampling Results 2827 South Stratford Road Winston-Salem, NC During this sampling event, two contaminants were detected in the well water. One of the contaminants, lead, was detected at a concentration that exceedec the applicable standard. The standards used to determine if the water is suitable for drinking and cooking are the United States Environmental Protection Agency's Maximum Contaminant Levels (MCLs) or, if no MCLs exist, North Carolina Groundwater Standards (2L). If contaminant concentrations exceed the applicable standards for using the water for drinking and cooking, the contaminant concentrations are further analyzed to determine if the water is suitable for other non- ingestive uses, such as showering, bathing, washing dishes, flushing toilets, and hand washing. The chart below compares the detected contaminant concentrations with the applicable standards: Pull 15M Wkflt:alijj. Lead 92262422002 2.0 T Methyl-tert-butyl ether 20 Shaded boxes indicate a standard has been exceeded. * The abbreviation j.ig/l stands for micrograms of contaminant per liter of water and is roughly equivalent to parts per billion. RECOMMENDATION: The lead concentration in this well exceeds the MCL. Therefore, this water is not recommended for drinking or cooking at this time. No restrictions are recommended for using the water for other non-ingestive uses, such as showering, bathing, washing dishes, flushing toilets, and hand washing. 42j David Lilley, Environmental Toxicologist Division of Waste Management, NCDEYR 1601 Mail Service Center, Raleigh, Nonh Carona 27699-1601 P.one: 919-707-8600 n:ernet: w'w.nccenr.gov Aniva C;i iy Ar : kec.e:J /'A 'ceAnaJy1ica/ r4%vnhIQl7ub.1 ,lvrw.i 9630 lOncay Ave. S.he 130 HrersvUe, NC 2078 (7C4)87-9092 ANALYTICAL RESULTS Project BEN NETTAND BAILEY Pace Prcect No.: 92262422 Sample: W11 Lab ID: 92262422002 Collected: 06/C6115 10.15 Received. 08107/15 14:55 Matrix Water Parameters Results Unhls Report Limit OF Prepared Analyzed GAS No. Qai 6010 MET lOP Analytical Method: EPA 6010 Preparation Method: EPA3010 I /-~Lead~. C::l :67:) ugh. 5.0 1 08/10116 16:15 08/13/1522:27 743942-1 82 0 MSSVSemivol Organic HVI ArialytiI Method: EPA 8270 Preparaton Method: EPA 3513 Acer.aphthene Acenaphthylene Ant hracene 8enzca)antr2cerie Eenzc'(a)pyrene Benzc(b)fluo(ar.thene Benzo(g,t I)perylano Benzo)6uoranLhere Chrysene Dibenzah)anthracene FIor1here Fkiorene Indenoll 2,3-cd)pyrane I -Methylnaphthalere 2-Methylnaphthalena Naphthalene Phenantl'rer.e Pyrene Surrogates NItobenzene-5 (8) 2-FluocobipPonyl (S) Terpl'.enyl-d14 (8) NO tjg/L 10.0 1 08/11/15 12:00 08111/15 16:13 8342-9 ND ugh. 10.0 1 05/11115 12:00 08/11/15 16:13 208-96-8 NO ugP_ 10.0 1 08/11/15 12:00 08111/15 16:13 120.12-7 ND ug!L. 10.0 1 08/11/15 12:00 08111/15 16:13 58-564 NO ug/L 10.0 1 08/11/15 12:00 08/11/1516:13 50-32-8 ND ug/L 10.0 1 68/11/1512:00 08111115 16:13 205-99-2 NO 4/L 10.0 1 08111/16 12:00 08/11115 1813 191-24-2 NO ugIL 10.0 1 08111/1512:00 08/11115 16:13 207-08•9 L3 ND ugIL 10.0 1 08111/15 12:00 08/11/16 16:13 218-01-9 NO ug/L 10.0 1 08111/1512:00 08/11115 15:13 53-70-3 NO ug/L 10.0 1 08/11/IS 12:00 06/11/15 16:13 20644.0 NO ug!L 10.0 1 06/11115 12:00 08/11/15 16:13 86-73-7 NO u9/L 10.0 1 08111115 12:00 08/11115 16:13 193-39-5 ND ug/L 10.0 1 08/11,15 12:00 08/11115 18:13 90-12-0 ND ug/L 10,0 1 08/11115 12:00 08111/16 18:13 91-57-6 NO ugf_ 100 1 08/11/15 12:00 08111/1516:13 91-20-3 NO ug/L 10.0 1 08/11/15 12:00 08111/1516:13 55-01-B ND ugIL 10.0 1 08/11115 12:00 08/11115 16:13 129.03-0 75 21-110 1 08111/1512:00 08/11115 16:13 4165-80-0 85 27-110 1 08/11/15 12:00 08/11/15 16:13 321-60-8 64 31-107 1 08111116 12:00 08/11/1516:13 1718-01-0 62008 MSV Analytical Method: Slvl 62008 Benzene ND ug/L 0.50 1 08110/15 21.C4 7143-2 Bromooenzene ND u/L 3.50 1 08/10/1521:34 10846-1 BromoctilQromthane NO ugiL 0.50 1 08/10/16 21:04 7447.5 Bromodichloomethane NO ugtL 0.50 1 08/10116 21:04 75-27-4 Bromoforin NO Ugh. 0.50 1 08/10/1521:04 75-26-2 9romornethane NO ugh. 5.0 1 08/10/1521:04 74-83-9 nOUtylb$flZfl ND Lj9IL 0.50 1 08/10/1521:04 134.51-5 58c-ByIbei7ene NO ug/L 0.50 1 05110115 21:04 135-98-8 tet.BUt/lbflR4fle ND ug/L 0.50 1 06/10/1621:04 98-06-5 Carbor. tetrachiocide ND ugIL 0.50 1 08110115 21:04 58-23-6 Chloroberszene ND ug/L 3.50 I 08/I0/I5 21:04 138-93--7 Chlooethane ND ugiL 1.0 1 08110/15 21:04 75-00-3 Chlofrrn ND UqrL 0.50 1 08/10/iS 21:04 67-654 CNocmethane ND Ugh 1.0 1 08110115 2104 74-87-3 2-Chlorotoluerte ND ug/L 0.50 1 08110115 21:04 96-49-8 4-ChiOrotOlUene ND ugJL 0.50 1 08/10/15 21:04 106-43-4 12-Dtbromc-?-chioropropens ND LgJL 1.3 1 08/1Q115 21:04 98-12-5 Dibrchlerethane NO ug/L 3.50 1 08/1C/l6 2104 124-45-1 I 2-0i:orneethane (EDO) ND ugh 0.60 1 08/10/15 21:04 10693-4 REPORT OF LABORATORY ANALYSIS Tile gp' ehaU rot be reprediscd, exepl in WI, Date: 08/14/2015 03:25 PM withQul the wrilIeconeit ol PceAnat4ioeI 8Cri, Inc.. Page 6 of 41 , 600 Kincey Ave. Suite 100 Nj-Iersv6e, NC 28078 (704875-9G92 f/eAna1yticaf / ANALYTiCAL. RESULTS Project BENNETTAND BAILEY Pace Pojec No.: 92262422 Sample: WW1 Lab 10: 92262422002 CoLlected: 08/06115 10:15 Receved: 06/07115 14:55 MaIrix: tter Parameters Results Units Report Limit OF Fre,ared A.'aLyzed GAS No. Qual 6200 MSV Ana'ytical Method: SM 62039 Dtbrornomethie NO ugh. 0.50 1 08110/1521:04 74-95.3 1,2-Diccbe-izene NO ug/L 0.50 1 08110/1521:04 95-50-1 1,3-oroberizene ND ug/L 0.50 1 06/10/15 2104 541-73-1 1,4-Cictrloroberizene NO ug/L 0.50 1 08/10/1521:04 106-46-7 DichIoro.iiuorometha -e NO ugfi_ 0.50 1 08110115 21:04 75-71-6 11-01chioroethana NO ugh. 0.50 1 08/10/15 21:04 75-34-3 1.2-Dichloroethane ND ug/t. 0.50 1 0811011521:04 107-06-2 1.1-Dichlcroethene ND ug/_ 0.50 1 08110115 2104 75-354 c4s-1,2-D1rcetheoe NO ugi. 0.50 1 08/10/1521:04 156-59-2 trans-1.2-Dicelherre NO ug/L 0.50 1 08/1011521:04 156-80-5 1.2-Cicloropropane ND u/L 0,50 1 08/1011521:04 78-87-5 13-Cic)loroçrcpane NO ug/L 0150 1 06/10/1521:04 142-28-9 2,2-0ichloropropane NO ug/L 0.50 1 08/10115 2104 594-20-7 1,1-Dichioropropene NO ug/L 0.50 1 08/10115 21:04 583-58-8 cis-1,3-Jchoropropere NO ugIL 0.50 08/10115 21:04 10061-01-5 trans-1,3-Did'rloropropene NO ug)L 0.50 08/10115 21:04 10061-02-6 Diis.o7ropi ether NO ug/L 0.50 i 08110/1521:04 108-20-3 Ethyloizene NO ,ug/L 0.50 1 8/10/15 2104 100-414 HexactLoro-1.3-butiene NO ug/L 2.0 1 08/10/1521:04 87-68-3 !spr3pythanzer1e (Curnere) ND ugP. 0.53 It 08/10115 21:04 9842-8 Methylene C-rlcride ND ugl.. 2.0 1 08/10(152t04 75-09-2 Methyl-Iert-butyl ether 2.0 ug/L 0.50 1 08/10115 21:04 1834-04-4 Nap1h9Iene NO ug/L 2.0 1 08I10/152t04 91-20-3 rr-Prosylbenzec NO ug/L 0.50 1 08110/15 21:04 103-65-1 Styrene ND ug/L 0.50 1 08/10115 21:04 100-42-8 1.1,12-Tetchlorce1iane ND ugh.. 0.50 1 08/10/1521:04 830-206 1,122-Tetra;L1oroe 1.bane NO ug/L 0.50 08110/1521:04 79-34-5 Teitac-roroethene NO trg/L 0.50 1 0811011521:04 127-184 Totuure ND ug/L 0.50 1 08/101i52104 108-88-3 12,3-7rtchio:obenzene NO ug/L 2.0 1 08/.1011521:04 87-81-6 124-Trchlc'obenze1e ND ug/L 2.0 1 08/10/1521:04 120-82-1 1,11-7richlcroethane ND ug/L 0.50 1 08/10/1521:04 71-55-6 1,12-Trlchloroethar.e NO ug/L 0.50 1 08110/152t04 79-00-5 Tnchloroethene NO ug/L 0.50 1 08110/1521:04 79-01-8 Trtchlorolturrnetlrane NO ug/L 1.0 1 08/10/1521:04 75-88-4 123-Tñchtcropropne . NO ugP_ 0.50 1 08/10/152t04 98-184 12,4-Tr1meThyenzene NO ugf.. 0.50 1 0811011521:04 95-834 13,6-Tri,iiethybenzene NJ - ug/L 0.50 1 08/10/1521:04 108-67-8 Vinyl c-.lorlde NO ug/L 1.0 1 08/10/1521:04 75-01-4 rn&p-Xylena ND ugJL 10 1 08110/15 2104 1796C1-23-1 o-Xylerte ND ug/L 0.50 1 06/10115 21:04 95-47-6 Surrogate4 I ,2-Dlthtoroethape-d4 (6) 97 70-130 1 08/10/1521:04 17080-07-3 4-Brorioflucwobenzene (5) 95 11 70-130 1 08110115 21:04 450-00-4 Toluerre-d8 S) 131 70-130 1 08110/15 21:04 2337-28-S REPORT OF LABORATORY ANALYSIS This re:o-t shJ 'cl be reproduced, except in tu. Date. 08/14/2015 0325 PM Serces. Inc.. Page 7of41