WA-749_38592_CA_TCR_20171023

October 24, 2016

Mr. Scott Ryals
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, N.C. 27699-1646

Reference: Report of UST Closure Assessment
Former Bazemore Grocery
730/732 Mt. Olive Road
Republican, Bertie County, North Carolina
NCDEQ Incident No: 38592
NCDEQ Contract No: N17006
ECS Proposal No: 49:3455-A

Dear Mr. Ryals:

As authorized by your acceptance of ECS Proposal No. 49:5955 dated July 20, 2017, ECS
Southeast, LLP (ECS) has completed the Report of UST Closure Assessment for the above-
referenced site. Included in this report is a description of the field activities, the results obtained,
and our conclusions and recommendations.

We appreciate the opportunity to provide our services to you. If there are questions regarding
this report, or a need for further information, please contact us at [phone].

Respectfully submitted,

ECS SOUTHEAST, LLP

Kevin Ferguson Sarah Kordon
Environmental Technician Environmental Scientist
[e-mail] [e-mail]
919-861-9814 919-616-8145

John S. Lair, P.G.
Principal Geologist
[e-mail]
910-726-3035

Report of UST Closure Assessment
Former Bazemore Grocery
730/732 Mt. Olive Road
Republican, Bertie County, North Carolina
NCDEQ Incident No: 38592
NCDEQ Contract No: N17006
ECS Project No: 49:3455-A

SITE INFORMATION

Site Name and Location: Former Bazemore Grocery
730/732 Mt. Olive Road
Republican, Bertie County, North Carolina

Incident Number TF-38592

Parcel Number 5875342404

Latitude and Longitude: 36.082583° North, -77.060094° West

Date of Report: October 24, 2017

Land Use Category: Commercial
Contacts

Primary Contact: Mr. Scott Ryals
NCDEQ, Division of Waste Management, UST Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Soil Removal: Zebra Environmental and Industrial Services, LLC.
901 East Springfield Road
High Point, North Carolina 27263
[phone]

Primary Consultant: ECS Southeast, LLP
9001 Glenwood Avenue
Raleigh, North Carolina 27617
[phone]
Attn: Matthew Gillis

Laboratory: Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078
[phone]
Laboratory I.D. # 37706

Report of UST Closure Assessment and Initial Abatement Action Report
Former Bazemore Grocery
730/732 Mt. Olive Road
Republican, Bertie County, North Carolina
NCDEQ Incident No: 38592
NCDEQ Contract No: N17006
ECS Project No: 49:3455-A

1

TABLE OF CONTENTS

1. BACKGROUND INFORMATION ........................................................................................ 2
2. FIELD ACTIVITIES ............................................................................................................. 2
3. LABORATORY ANALYSIS ................................................................................................. 3
4. CONCLUSIONS AND RECOMMENDATIONS.................................................................... 3
5. QUALIFICATIONS OF REPORT ........................................................................................ 4

FIGURES Figure 1 - USGS Topographic Map
Figure 2 - Site Location Map
Figure 3 - Soil Sample Location Map

TABLES Table 1 - Summary of TPH-GRO Soil Sample Analytical Results

APPENDIX A - Site Photographs
B - Non-Hazardous Materials Manifest
C - Non Laboratory Analytical Results and Chain of Custody
Report of UST Removal and Soil Assessment
730/732 Mt. Olive Road
Republican, Bertie County, North Carolina
NCDEQ Incident No: 38592
NCDEQ Contract No: N17006
ECS Project No: 49:3455-A

2

1. BACKGROUND INFORMATION

The Former Bazemore Grocery site is approximately 1.1 acres in size and is located at 730/732
Mt. Olive Road, in Republican, Bertie County, North Carolina (Figure 1). According to the Bertie
County Online GIS Database, the Parcel Identification Number (PIN) is 5875342404 (Figure 2).
The property is currently developed with an abandoned residential building. The site previously
operated two 2,000-gallon USTs, one 1,500-gallon UST, and one septic tank.

2. FIELD ACTIVITIES

Prior to conducting field activities, ECS contacted the public utility locator service (North
Carolina One-Call Center) and contracted with a private utility locator to mark utilities and the
UST prior to performing excavation activities.

On August 14 and 15, 2017, ECS observed the removal of two 2,000-gallon USTs, one 1,500-
gallon UST, and one septic tank UST by Zebra. ECS observed rust and holes on the two 2,000-
gallon USTs, one 1,500-gallon UST and detected a petroleum odor from the surrounding soils.
The USTs was transported to an approved facility for disposal. The excavation extent measured
approximately thirty (30) feet in length, twenty (20) feet in width, and six (6) feet in depth.
Groundwater was encountered at approximately 6 ft bgs therefore base samples were not
collected. Zebra removed and disposed of approximately 1,937 gallons of contaminated fluid
from the USTs and approximately 98.88 tons of petroleum-impacted soil from the excavation.
Site photographs documenting field activities are included in Appendix A. A copy of Zebras
Certificate of Disposal, Tank Disposal Certificate, and Non-Hazardous Materials Manifest are
included in Appendix B.

ECS collected a total of sixteen (16) soil samples along the sidewalls of the septic tank
excavation (SW-1 through SW-4) and UST excavation (SW-5 through SW-16). The locations of
the soil samples are shown on Figure 3. The soil samples were collected at approximately 4 feet
below the ground surface (ft bgs). ECS screened the soil samples using a Photoionization
Detector (PID) to detect volatile organic vapors. VOCs were detected in soil samples SW-7
through SW-16 ranging from 1.2 (parts per million) ppm to 25.0 ppm. VOCs were not detected
near the eastern edge of excavation, closest to monitoring well MW-20, in soil samples SW-5
and SW-6; therefore, the excavation was not advanced to the east but rather the northwest of
the site.

The soil samples were appropriately packaged and submitted to Pace Analytical Laboratory to
be analyzed for TPH-GRO using EPA Method 5035/8015. ECS maintained proper Chain-of-
Custody (COC) procedures throughout sample collection and transportation process.

ECS was contracted to abandon, reinstall, and collect groundwater samples from monitoring
MW-20 and collect groundwater samples from monitoring wells MW-2 and MWD-7. ECS was
unable to locate monitoring wells MW-2 and MWD-7. Monitoring well MW-20 was located. On
August 15, 2017, ECS measured approximately two (2) feet of free-product in monitoring well
MW-20 and was unable to collect the groundwater sample. Additionally, a sorbent sock was
previously installed in monitoring well MW-20. ECS removed and disposed of the sorbent sock.
No monitoring wells were installed during field activities as no monitoring wells were presumably
destroyed during tank removal, soil exaction, and soil removal tasks.
Report of UST Removal and Soil Assessment
Former Bazemore Grocery
730/732 Mt. Olive Road
Republican, Bertie County, North Carolina
NCDEQ Incident No: 38592
NCDEQ Contract No: N17006
ECS Project No: 49:3455-A

3

3. LABORATORY ANALYSIS

Laboratory analysis detected TPH-GRO at a concentration above the North Carolina
Department of Environmental Quality (NCDEQ) UST Section’s Action Level of 50 mg/kg in soil
samples SW-14 and SW-16.

Laboratory analysis detected TPH-GRO at concentrations above the laboratory reporting limit
but below the NCDEQ UST Section’s Action Level of 50 mg/kg in oil samples SW-8, SW-9, SW-
11, and SW-13.

Laboratory analysis did not report TPH-GRO at concentrations above the laboratory reporting
limit in soil samples SW-1 through SW-7, SW-10, SW-12 or SW-15.

A summary of the laboratory analytical results is included in Table 1. The laboratory analytical
report and COC are included in Appendix C.

4. CONCLUSIONS AND RECOMMENDATIONS

Based on the field observation and laboratory analytical results of the soil samples collected
during this assessment, ECS concludes the following:

 On August 14 and 15, 2017, ECS observed the removal of two 2,000-gallon USTs, one
1,500-gallon UST, and one septic tank UST by Zebra. ECS observed rust and holes on
the two 2,000-gallon USTs, one 1,500-gallon UST and detected a petroleum odor from
the surrounding soils;

 On August 15, 2017, ECS measured approximately two feet of free-product in
monitoring well MW-20;

 Laboratory analysis reported TPH-GRO at concentrations above the NCDEQ UST
Section’s Action Level in the soil samples SW-14 and SW-16; therefore, laboratory
analysis of soil samples collected from the three USTs’ basin confirms a release most
likely occurred;

 Laboratory analysis reported TPH-GRO at concentrations above its laboratory reporting
limits but below the NCDEQ UST Section’s Action Level of 50 mg/kg in the soil samples
SW-8, SW-9, SW-11, and SW-13;

 Laboratory analysis did not report TPH-GRO at concentrations above the laboratory
reporting limit in soil samples SW-1 through SW-7, SW-10, SW-12 or SW-15; and

 ECS recommends conducting an Aggressive Fluid Vapor Recovery (AFVR) event on
monitoring well MW-20 to remove existing free-product. Upon completion of the AFVR
event, ECS recommends installing an O-SOX remedial device in monitoring well MW-20.

Report of UST Removal and Soil Assessment
Former Bazemore Grocery
730/732 Mt. Olive Road
Republican, Bertie County, North Carolina
NCDEQ Incident No: 38592
NCDEQ Contract No: N17006
ECS Project No: 49:3455-A

4

5. QUALIFICATIONS OF REPORT

The activities and evaluative approaches used in this assessment are consistent with those
normally employed in UST closure assessments of this type. Our evaluation of site conditions
has been based on our understanding of the site project information and the data obtained
during our field activities. Based on the field observation and laboratory analytical

5

FIGURES

SOURCE:

USGS TOPOGRAPHIC MAP
REPUBLICAN, NC
QUADRANGLE
DATED 2016
SCALE: 1 : 24,000
FIGURE 1
USGS TOPOGRAPHIC MAP

FORMER BAZEMORE GROCERY
730/732 MT OLIVE ROAD
REPUBLICAN, BERTIE COUNTY,
NORTH CAROLINA
ECS PROJECT: 49:3455-A
SITE
SOURCE:

BERTIE COUNTY GIS
DATED 2016

FIGURE 2
SITE LOCATION MAP

FORMER BAZEMORE GROCERY
730/732 MT OLIVE ROAD
REPUBLICAN, BERTIE COUNTY,
NORTH CAROLINA
ECS PROJECT: 49:3455-A
1 inch = 45 feet
SITE
LEGEND

Approximate Site Boundary

SOURCE:

GOOGLE EARTH
DATED 2017

FIGURE 3
SOIL SAMPLE LOCATION MAP

FORMER BAZEMORE GROCERY
730/732 MT OLIVE ROAD
REPUBLICAN, BERTIE COUNTY,
NORTH CAROLINA
ECS PROJECT: 49:3455-A
1 inch = 30 feet
LEGEND

Approximate Site Boundary

Approximate Soil Sample Location

Approximate UST Location

Approximate Septic Tank Location

Approximate Monitoring Well Location

SW-4
SW-9
SW-10
SW-11
SW-1
SW-2
SW-3
SW-12
SW-6
SW-5
MW-20
~ 2 Feet Free-
Product
SW-14
SW-4

TABLE

EPA Method 8015
Sample ID Sample Date Sample Depth
(ft. bgs)
SW-1 8/14/2017 4 BRL
SW-2 8/14/2017 4 BRL
SW-3 8/14/2017 4 BRL
SW-4 8/14/2017 4 BRL
SW-5 8/14/2017 4 BRL
SW-6 8/14/2017 4 BRL
SW-7 8/14/2017 4 BRL
SW-8 8/14/2017 4 12.1
SW-9 8/15/2017 4 17.6
SW-10 8/15/2017 4 BRL
SW-11 8/15/2017 4 17.9
SW-12 8/15/2017 4 BRL
SW-13 8/15/2017 4 6.7
SW-14 8/15/2017 4 182
SW-15 8/15/2017 4 BRL
SW-16 8/15/2017 4 148
50
UST = Underground Storage Tank
mg/kg = milligram per kilogram
BRL = Below Reporting Limit
TPH = Total Petroleum Hydrocarbons
GRO = Gasoline Range Organics
Table 1
Summary of TPH-GRO Soil Sample Analytical Results
Former Bazemore Grocery
Republican, Bertie County, North Carolina
NCDEQ Contract No: N17006
NCDEQ UST Section's Action Level (mg/kg)
NCDEQ = North Carolina Department of Environmental Quality
730/732 Mt. Olive Road
NCDEQ Incident No: TF-38592
Contaminant of Concern (mg/kg)
TPH-GRO
ECS Project: 49:3455-A
Analytical Method

APPENDIX A

SITE PHOTOGRAPHS

FORMER BAZEMORE GROCERY
730/732 MOUNT OLIVE ROAD
REPUBLICAN, BERTIE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-38592
ECS PROJECT NO: 49:3455-A

Photograph 1: View of the existing commercial building located on the subject site,
view is facing east.

Photograph 2: View of the UST location during excavation, view is facing southeast.
SITE PHOTOGRAPHS

FORMER BAZEMORE GROCERY
730/732 MOUNT OLIVE ROAD
REPUBLICAN, BERTIE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-38592
ECS PROJECT NO: 49:3455-A

Photograph 3: View of UST excavation, view is facing south.

Photograph 4: View of UST upon removal, view is facing northeast.
SITE PHOTOGRAPHS

FORMER BAZEMORE GROCERY
730/732 MOUNT OLIVE ROAD
REPUBLICAN, BERTIE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-38592
ECS PROJECT NO: 49:3455-A

Photograph 5: View of the UST excavation prior to backfill, view is facing southeast.

Photograph 6: View of septic tank during fluid removal, view is facing southeast.
SITE PHOTOGRAPHS

FORMER BAZEMORE GROCERY
730/732 MOUNT OLIVE ROAD
REPUBLICAN, BERTIE COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-38592
ECS PROJECT NO: 49:3455-A

Photograph 7: View of the UST excavation during Soil backfill, facing northeast.

Photograph 8: View of free-product from monitoring well MW-20, view is facing southeast.

APPENDIX B

APPENDIX C

#=CL#
August 18, 2017
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92351706
92351706
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
Former Bazemore Grocery
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on August 16, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Sample SW-4 is reported on a wet weight basis. The container for moisture was received empty. All
other containers are preserved.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc: Sarah Kordon, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92351706001 SW-1 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CKDF
92351706002 SW-2 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CKDF
92351706003 SW-3 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CKDF
92351706004 SW-4 EPA 8015 Modified 2 PASI-CWDV
92351706005 SW-5 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CKDF
92351706006 SW-6 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CKDF
92351706007 SW-7 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CKDF
92351706008 SW-8 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92351706001 SW-1
Percent Moisture 21.1 %08/17/17 07:520.10ASTM D2974-87
92351706002 SW-2
Percent Moisture 20.2 %08/17/17 07:520.10ASTM D2974-87
92351706003 SW-3
Percent Moisture 20.0 %08/17/17 07:520.10ASTM D2974-87
92351706005 SW-5
Percent Moisture 12.3 %08/17/17 07:520.10ASTM D2974-87
92351706006 SW-6
Percent Moisture 20.1 %08/17/17 07:530.10ASTM D2974-87
92351706007 SW-7
Percent Moisture 17.3 %08/17/17 07:530.10ASTM D2974-87
92351706008 SW-8
Gas Range Organics (C6-C10)12.1 mg/kg 08/17/17 20:105.0EPA 8015 Modified
Percent Moisture 18.0 %08/17/17 07:530.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-1 Lab ID: 92351706001 Collected: 08/14/17 17:10 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/17/17 16:4508/17/17 09:397.1 1
Surrogates
4-Bromofluorobenzene (S)89 %08/17/17 16:45 460-00-408/17/17 09:3970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.1 %08/17/17 07:520.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-2 Lab ID: 92351706002 Collected: 08/14/17 17:20 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/17/17 17:1508/17/17 09:396.6 1
Surrogates
4-Bromofluorobenzene (S)94 %08/17/17 17:15 460-00-408/17/17 09:3970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.2 %08/17/17 07:520.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-3 Lab ID: 92351706003 Collected: 08/14/17 17:28 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/17/17 17:4408/17/17 09:395.4 1
Surrogates
4-Bromofluorobenzene (S)89 %08/17/17 17:44 460-00-408/17/17 09:3970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.0 %08/17/17 07:520.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-4 Lab ID: 92351706004 Collected: 08/14/17 17:55 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "wet-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/17/17 18:1308/17/17 09:394.8 1
Surrogates
4-Bromofluorobenzene (S)89 %08/17/17 18:13 460-00-408/17/17 09:3970-167 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-5 Lab ID: 92351706005 Collected: 08/14/17 17:40 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/17/17 18:4208/17/17 09:395.3 1
Surrogates
4-Bromofluorobenzene (S)84 %08/17/17 18:42 460-00-408/17/17 09:3970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.3 %08/17/17 07:520.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-6 Lab ID: 92351706006 Collected: 08/14/17 17:45 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/17/17 19:1208/17/17 09:395.3 1
Surrogates
4-Bromofluorobenzene (S)85 %08/17/17 19:12 460-00-408/17/17 09:3970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.1 %08/17/17 07:530.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-7 Lab ID: 92351706007 Collected: 08/14/17 17:52 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/17/17 19:4108/17/17 09:396.3 1
Surrogates
4-Bromofluorobenzene (S)86 %08/17/17 19:41 460-00-408/17/17 09:3970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.3 %08/17/17 07:530.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Sample: SW-8 Lab ID: 92351706008 Collected: 08/14/17 18:00 Received: 08/16/17 07:47 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)12.1 mg/kg 08/17/17 20:1008/17/17 09:395.0 1
Surrogates
4-Bromofluorobenzene (S)106 %08/17/17 20:10 460-00-408/17/17 09:3970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.0 %08/17/17 07:530.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
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Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
373814
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples:92351706001, 92351706002, 92351706003, 92351706004, 92351706005, 92351706006, 92351706007,
92351706008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2071156
Associated Lab Samples: 92351706001, 92351706002, 92351706003, 92351706004, 92351706005, 92351706006, 92351706007,
92351706008
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/17/17 11:10
4-Bromofluorobenzene (S)%93 70-167 08/17/17 11:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2071157LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 44.750 89 70-165
4-Bromofluorobenzene (S)%89 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2071158MATRIX SPIKE SAMPLE:
MSSpike
Result
92351844001
Gas Range Organics (C6-C10)mg/kg 62.560.6 101 47-187ND
4-Bromofluorobenzene (S)%93 70-167
Parameter Units
Dup
Result QualifiersRPDResult
92351844002
2071159SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%86 187
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
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Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
373695
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92351706001, 92351706002, 92351706003, 92351706005, 92351706006, 92351706007, 92351706008
Parameter Units
Dup
Result QualifiersRPDResult
92351436003
2070688SAMPLE DUPLICATE:
Percent Moisture %12.9 1011.6
Parameter Units
Dup
Result QualifiersRPDResult
92351804006
2070689SAMPLE DUPLICATE:
Percent Moisture %13.2 812.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
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[phone]
Page 14 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
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Page 15 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92351706
Former Bazemore Grocery
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92351706001 373814 373883SW-1 EPA 5035A/5030B EPA 8015 Modified
92351706002 373814 373883SW-2 EPA 5035A/5030B EPA 8015 Modified
92351706003 373814 373883SW-3 EPA 5035A/5030B EPA 8015 Modified
92351706004 373814 373883SW-4 EPA 5035A/5030B EPA 8015 Modified
92351706005 373814 373883SW-5 EPA 5035A/5030B EPA 8015 Modified
92351706006 373814 373883SW-6 EPA 5035A/5030B EPA 8015 Modified
92351706007 373814 373883SW-7 EPA 5035A/5030B EPA 8015 Modified
92351706008 373814 373883SW-8 EPA 5035A/5030B EPA 8015 Modified
92351706001 373695SW-1 ASTM D2974-87
92351706002 373695SW-2 ASTM D2974-87
92351706003 373695SW-3 ASTM D2974-87
92351706005 373695SW-5 ASTM D2974-87
92351706006 373695SW-6 ASTM D2974-87
92351706007 373695SW-7 ASTM D2974-87
92351706008 373695SW-8 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/18/2017 04:03 PM
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Page 16 of 19
Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
August 23, 2017
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92351969
92351969
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
FORMER BAZEMORE GROOM 493455A
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on August 17, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc: Sarah Kordon, ECS Southeast
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 1 of 21
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 21
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92351969001 SW-9 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
92351969002 SW-10 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
92351969003 SW-11 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
92351969004 SW-12 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
92351969005 SW-13 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
92351969006 SW-14 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
92351969007 SW-15 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
92351969008 SW-16 EPA 8015 Modified 2 PASI-CWDV
ASTM D2974-87 1 PASI-CCLW
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 3 of 21
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92351969001 SW-9
Gas Range Organics (C6-C10)17.6 mg/kg 08/19/17 01:276.9EPA 8015 Modified
Percent Moisture 13.7 %08/18/17 08:550.10ASTM D2974-87
92351969002 SW-10
Percent Moisture 17.8 %08/18/17 08:550.10ASTM D2974-87
92351969003 SW-11
Gas Range Organics (C6-C10)17.9 mg/kg 08/22/17 15:506.3EPA 8015 Modified
Percent Moisture 7.2 %08/18/17 08:560.10ASTM D2974-87
92351969004 SW-12
Percent Moisture 6.5 %08/18/17 08:560.10ASTM D2974-87
92351969005 SW-13
Gas Range Organics (C6-C10)6.7 mg/kg 08/22/17 17:466.0EPA 8015 Modified
Percent Moisture 13.2 %08/18/17 08:560.10ASTM D2974-87
92351969006 SW-14
Gas Range Organics (C6-C10)182 mg/kg 08/22/17 18:154.9EPA 8015 Modified
Percent Moisture 11.7 %08/18/17 08:560.10ASTM D2974-87
92351969007 SW-15
Percent Moisture 13.6 %08/18/17 08:560.10ASTM D2974-87
92351969008 SW-16
Gas Range Organics (C6-C10)148 mg/kg 08/22/17 21:596.7EPA 8015 Modified
Percent Moisture 15.3 %08/18/17 08:570.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 4 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-9 Lab ID: 92351969001 Collected: 08/15/17 10:25 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)17.6 mg/kg 08/19/17 01:2708/18/17 09:136.9 1
Surrogates
4-Bromofluorobenzene (S)85 %08/19/17 01:27 460-00-408/18/17 09:1370-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.7 %08/18/17 08:550.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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Page 5 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-10 Lab ID: 92351969002 Collected: 08/15/17 12:00 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/19/17 01:5608/18/17 09:135.9 1
Surrogates
4-Bromofluorobenzene (S)80 %08/19/17 01:56 460-00-408/18/17 09:1370-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.8 %08/18/17 08:550.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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Page 6 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-11 Lab ID: 92351969003 Collected: 08/15/17 12:55 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)17.9 mg/kg 08/22/17 15:5008/22/17 08:496.3 1
Surrogates
4-Bromofluorobenzene (S)92 %08/22/17 15:50 460-00-408/22/17 08:4970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 7.2 %08/18/17 08:560.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-12 Lab ID: 92351969004 Collected: 08/15/17 13:00 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/22/17 16:4808/22/17 08:495.0 1
Surrogates
4-Bromofluorobenzene (S)86 %08/22/17 16:48 460-00-408/22/17 08:4970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 6.5 %08/18/17 08:560.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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Huntersville, NC 28078
[phone]
Page 8 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-13 Lab ID: 92351969005 Collected: 08/15/17 13:10 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)6.7 mg/kg 08/22/17 17:4608/22/17 08:496.0 1
Surrogates
4-Bromofluorobenzene (S)87 %08/22/17 17:46 460-00-408/22/17 08:4970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.2 %08/18/17 08:560.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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9800 Kincey Ave. Suite 100
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Page 9 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-14 Lab ID: 92351969006 Collected: 08/15/17 13:25 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)182 mg/kg 08/22/17 18:1508/22/17 08:494.9 1
Surrogates
4-Bromofluorobenzene (S)171 %08/22/17 18:15 460-00-4 S508/22/17 08:4970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 11.7 %08/18/17 08:560.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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Page 10 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-15 Lab ID: 92351969007 Collected: 08/15/17 13:40 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)ND mg/kg 08/22/17 18:4408/22/17 08:494.8 1
Surrogates
4-Bromofluorobenzene (S)90 %08/22/17 18:44 460-00-408/22/17 08:4970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.6 %08/18/17 08:560.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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Page 11 of 21
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Sample: SW-16 Lab ID: 92351969008 Collected: 08/15/17 12:20 Received: 08/17/17 13:05 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: EPA 8015 Modified Preparation Method: EPA 5035A/5030BGasoline Range Organics
Gas Range Organics (C6-C10)148 mg/kg 08/22/17 21:5908/22/17 08:596.7 1
Surrogates
4-Bromofluorobenzene (S)107 %08/22/17 21:59 460-00-408/22/17 08:5970-167 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 15.3 %08/18/17 08:570.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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Page 12 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
374020
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92351969001, 92351969002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2072236
Associated Lab Samples:92351969001, 92351969002
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/18/17 16:44
4-Bromofluorobenzene (S)%83 70-167 08/18/17 16:44
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2072237LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 43.950 88 70-165
4-Bromofluorobenzene (S)%78 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2072238MATRIX SPIKE SAMPLE:
MSSpike
Result
92351857001
Gas Range Organics (C6-C10)mg/kg 54.352.4 101 47-187ND
4-Bromofluorobenzene (S)%93 70-167
Parameter Units
Dup
Result QualifiersRPDResult
92351857002
2072239SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%77 883
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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Page 13 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
374261
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92351969003, 92351969004, 92351969005, 92351969006, 92351969007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2073582
Associated Lab Samples:92351969003, 92351969004, 92351969005, 92351969006, 92351969007
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/22/17 15:21
4-Bromofluorobenzene (S)%87 70-167 08/22/17 15:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2073583LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 43.150 86 70-165
4-Bromofluorobenzene (S)%90 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2073584MATRIX SPIKE SAMPLE:
MSSpike
Result
92351969003
Gas Range Organics (C6-C10)mg/kg 70.952.7 100 47-18717.9
4-Bromofluorobenzene (S)%89 70-167
Parameter Units
Dup
Result QualifiersRPDResult
92351969004
2073585SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%87 286
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 14 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
374286
EPA 5035A/5030B
EPA 8015 Modified
Gasoline Range Organics
Associated Lab Samples: 92351969008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2073685
Associated Lab Samples:92351969008
Matrix: Solid
Analyzed
Gas Range Organics (C6-C10)mg/kg ND 6.0 08/22/17 15:14
4-Bromofluorobenzene (S)%96 70-167 08/22/17 15:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2073686LABORATORY CONTROL SAMPLE:
LCSSpike
Gas Range Organics (C6-C10)mg/kg 40.350 81 70-165
4-Bromofluorobenzene (S)%95 70-167
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2073687MATRIX SPIKE SAMPLE:
MSSpike
Result
92351741001
Gas Range Organics (C6-C10)mg/kg 44.550.2 85 47-187ND
4-Bromofluorobenzene (S)%99 70-167
Parameter Units
Dup
Result QualifiersRPDResult
92351741002
2073688SAMPLE DUPLICATE:
Gas Range Organics (C6-C10)mg/kg NDND
4-Bromofluorobenzene (S)%89 291
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 21
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
373915
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92351969001, 92351969002, 92351969003, 92351969004, 92351969005, 92351969006, 92351969007,
92351969008
Parameter Units
Dup
Result QualifiersRPDResult
92351974001
2071799SAMPLE DUPLICATE:
Percent Moisture %1.3 41.3
Parameter Units
Dup
Result QualifiersRPDResult
92351969008
2071800SAMPLE DUPLICATE:
Percent Moisture %15.0 215.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 21
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 21
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92351969
FORMER BAZEMORE GROOM 493455A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92351969001 374020 374257SW-9 EPA 5035A/5030B EPA 8015 Modified
92351969002 374020 374257SW-10 EPA 5035A/5030B EPA 8015 Modified
92351969003 374261 374694SW-11 EPA 5035A/5030B EPA 8015 Modified
92351969004 374261 374694SW-12 EPA 5035A/5030B EPA 8015 Modified
92351969005 374261 374694SW-13 EPA 5035A/5030B EPA 8015 Modified
92351969006 374261 374694SW-14 EPA 5035A/5030B EPA 8015 Modified
92351969007 374261 374694SW-15 EPA 5035A/5030B EPA 8015 Modified
92351969008 374286 374690SW-16 EPA 5035A/5030B EPA 8015 Modified
92351969001 373915SW-9 ASTM D2974-87
92351969002 373915SW-10 ASTM D2974-87
92351969003 373915SW-11 ASTM D2974-87
92351969004 373915SW-12 ASTM D2974-87
92351969005 373915SW-13 ASTM D2974-87
92351969006 373915SW-14 ASTM D2974-87
92351969007 373915SW-15 ASTM D2974-87
92351969008 373915SW-16 ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/23/2017 03:33 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
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