18038_AquAir II_VIMS Installation Completion Report_20230427

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VIMS Installation Completion Report HD Charlotte Warehouse
13300 Sam Neely Road Charlotte, North Carolina Brownfields Project No. 18038-14-060 H&H Job No. TKC-008

Table of Contents

1.0 Introduction ................................................................................................................ 1
2.0 VIMS Installation and Influence Testing ................................................................ 4
2.1 VIMS Installation......................................................................................................4
2.2 VIMS Influence Testing ...........................................................................................6
3.0 Pre-Occupancy VIMS Effectiveness Sampling ....................................................... 8
3.1 Sub-Slab Soil Gas Sampling Methodology ..............................................................8
3.2 Sub-Slab Soil Gas Sampling Results ........................................................................9
3.3 Sub-Slab Soil Gas Vapor Intrusion Evaluation ......................................................11
3.4 Building Survey Activities ......................................................................................12
3.5 Indoor Air Sampling Methodology .........................................................................12
3.6 Indoor Air Sampling Results ..................................................................................14
3.7 Indoor Air Vapor Intrusion Evaluation ...................................................................15
4.0 Summary and Conclusions ...................................................................................... 17

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Tables
Table 1 Summary of Soil Gas Analytical Data
Table 2 Summary of Indoor Air Analytical Data
Figures
Figure 1 Site Location Map
Figure 2 Site Map

Appendices

Appendix A Redevelopment Plan
Appendix B Previous Assessment Summary Tables and Sample Location Map
Appendix C As-Built Drawings – VM-1, VM-2, VM-2A, VM-3, and VM-4
Appendix D Vapor Intrusion Mitigation System Product Specifications
Appendix E Installation Inspection Photographs and Inspection Logs
Appendix F Field Forms
Appendix G Laboratory Analytical Reports
Appendix H DEQ Risk Calculators
Appendix I Safety Data Sheets

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VIMS Installation Completion Report HD Charlotte Warehouse 13300 Sam Neely Road Charlotte, North Carolina
Brownfields Project No. 18038-14-060 H&H Job No. TKC-008
1.0 Introduction

On behalf of TKC Land Development II, Inc. (the Prospective Developer or PD), Hart & Hickman,
PC (H&H) has prepared this report to document vapor intrusion mitigation system (VIMS)
installation, influence testing, and post-construction sampling activities for the HD Charlotte
distribution warehouse and associated buildings on the west side of the AquAir II Brownfields
Property (Brownfields Project No. 18038-14-060) located at 13300 Sam Neely Road in Charlotte,
Mecklenburg County, North Carolina (Site). The Brownfields property consists of two contiguous
parcels, totaling approximately 154 acres, which are separated by the Southern Railway. The Site
consists of the portion of the Brownfields property to the west of the railway, which includes one
approximately 76-acre parcel located in a residential and commercial use area near the Interstate-
485 loop. A Site location map is provided as Figure 1, and the Site and surrounding area are shown
in Figure 2.

Redevelopment of the HD Charlotte warehouse is nearing completion and includes construction
of an industrial warehouse building with associated exterior material storage areas, trailer loading
and storage areas, guard house, fire pumphouse, and parking. In addition, stormwater management
ponds are under construction on the northern portion of the Site. The guardhouse is approximately
140 square feet (sq ft) and was constructed with slab on grade exterior foundation footings. The
industrial warehouse is approximately 403,200 sq ft and was constructed with concrete slab-on-
grade foundation and structural columns throughout the interior that includes an interior rail spur
in the northern portion of the building. In order to meet the load requirements for the forklifts and
storage on the warehouse slab, the building slab was constructed on compacted ABC-stone. The
fire pumphouse is approximately 495 sq ft and contains mechanical systems for the Site. The fire
pumphouse does not contain any office or long-term occupiable space, and will only be accessible
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to maintenance personnel to conduct maintenance or repairs on the systems. A copy of the
redevelopment plans for the HD Charlotte warehouse are included in Appendix A.

Former operations at the Site consisted of 1) vanadium catalyst manufacturing from 1965 to 1972,
2) solvent recovery, reclamation, and blending from 1974 to 1984, 3) bulk chemical repackaging
from 1974 to 1976, and 4) laboratory services and chromium compound manufacturing from 1977
to 1988, and was vacant thereafter. In the early 1990s, soil contamination was identified and the
Site was subsequently listed as a North Carolina Inactive Hazardous Site (AquAir Corporation
Site, NCD074511361). In 1999, stabilization measures were conducted at the Site including the
removal of vanadium pellets, debris, and a septic tank system. The on-Site buildings were
demolished in approximately 2000. Soil samples collected from 1990 through 2003 indicate
metals and chlorinated solvent compounds are the primary constituents of interest in soil. The
Brownfields agreement for the Site designates an “Area of Potential Soil Contamination” where
soil impacts may be present on the Site. Summary tables and a sample location map are included
in Appendix B.

Groundwater sampling was performed at the Site beginning in the early 1990s. Former
remediation efforts included the operation of a pump and treat groundwater recovery system and
a network of air sparge wells. On-Site groundwater is impacted by VOCs and metals at
concentrations exceeding the North Carolina Administrative Code (NCAC) 02L.0202
Groundwater Quality Standard (2L Standard) and/or the DEQ Non-Residential Groundwater
Screening Levels (GWSL). In October 2011, Hart & Hickman, PC performed a soil gas
investigation at the Site within the Limits of Groundwater Contamination, as depicted on the
Brownfields Plat, and supplemental soil gas sampling was conducted outside the Limits of
Groundwater Contamination on behalf of a potential purchaser of the Site in January 2016. The
results indicated that VOCs were detected at concentrations exceeding the DEQ Non-Residential
Soil Gas Screening Levels (SGSLs) in samples collected within the Limits of Groundwater
Contamination.

A Brownfields Agreement between DEQ and TKC Land Development II, LLC was recorded for
the Site on July 24, 2015. The recorded Brownfields Agreement includes a Land Use Restriction
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which generally states that no enclosed building may be constructed on the property until DEQ
determines in writing that the building would be protective of users from risks of potential vapor
intrusion. To address DEQ Brownfields requirements, H&H prepared a Vapor Intrusion
Mitigation Plan (VIMP) for the proposed warehouse and associated building. The VIMP revision
dated March 16, 2022 was approved by DEQ in a letter dated March 24, 2022. The DEQ-approved
VIMP includes installation of passive VIMS for the industrial warehouse building and guardhouse,
and installation of vapor barrier below the pumphouse slab.

This report documents installation and associated testing of the VIMS for the warehouse,
guardhouse, and fire pumphouse buildings at the Site. A discussion of VIMS installation and
influence testing activities is provided in Section 2.0; a summary of VIMS effectiveness sampling
activities is provided in Section 3.0; and summary and conclusions based on the results of the
VIMS installation and effectiveness sampling activities are provided in Section 4.0.

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2.0 VIMS Installation and Influence Testing

The Site redevelopment plan includes one industrial warehouse building, one guardhouse, and one
fire pumphouse. Vapor mitigation systems in the warehouse and guardhouse include a permeable
gravel layer, sub-slab vapor collection piping, vapor barrier, riser piping, and passive ventilators.
Due to the fire pumphouse being limited to minimal maintenance access only, as a conservative
approach, the VIMP includes installation of vapor barrier below the pumphouse slab. The as-built
system specifications and details (VM-1, VM-2, and VM-2A) and the drawings depicting the
layout of the VIMS (VM-3 and VM-4) are provided in Appendix C. Product specifications for the
VIMS components are included in Appendix D, and installation photographs and inspection logs
are included in Appendix E.

2.1 VIMS Installation

During installation of the VIMS, H&H conducted inspections during various phases of
construction to confirm the VIMS was installed in accordance with the DEQ-approved VIMP.
Inspections were completed during the following phases of installation:

(1) Inspection of the base course gravel layer, sub-slab piping layout, and monitoring points
prior to installation of the vapor barrier;
(2) Inspection of the vapor barrier prior to pouring concrete;
(3) Inspection of above-grade vertical riser piping; and
(4) Inspection of ventilators and riser pipe connections.

Based on observations made during the VIMS inspections and photographs of the installation
activities, the VIMS was installed in general accordance with the DEQ-approved VIMP. No
significant modifications were made during installation of the VIMS. A brief summary of the
main VIMS components is provided in the following paragraphs.

For the warehouse and guardhouse, passive sub-slab vapor extraction is achieved through an
interconnected system of 3-inch Schedule (SCH) 40 PVC vapor collection/conveyance piping
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installed in a 4-inch permeable gravel layer beneath the building slabs. The permeable gravel layer
(clean #57 stone) was installed beneath the entirety of each building slab to enhance sub-slab vapor
transmission and allow for air movement beneath the slabs. The sub-slab vapor collection piping
is connected to riser piping which extends vertically through the buildings and discharges vapors
through exhaust stacks installed above the building roofs. Aura PVC pipe cap ventilators were
installed on the discharge end of the exhaust stacks on the roofs.

Vaporblock® Plus™ 20 (VBP20), a vapor barrier manufactured by Raven Industries (Raven), was
installed above the gravel layer and beneath the concrete slab of each building, including the
pumphouse. In the warehouse building, a layer of ABC stone was installed above the permeable
gravel layer for structural purposes; therefore, the vapor barrier was installed above the ABC stone,
directly below the concrete. VBP20 is an ASTM-certified 20-mil, multi-layer, chemically resistant
vapor barrier, designed to prevent structural vapor intrusion of volatile organic compounds
(VOCs). The vapor barrier was installed by the construction contractor to cover the footprint of
enclosed spaces for each building. The exterior edges of the VBP20 were laid underneath the
footings. Seams within each building footprint have a minimum 12-inch overlap and are sealed
with VaporSeal™ tape. Utility banks in the warehouse building were installed along the interior
wall of the southwest end of the warehouse building, and because tape was deemed ineffective
around the banks, Pour-N-Seal™ was used to form an airtight seal around the penetrations. Pour-
N-Seal ™ is a two-part epoxy used to seal around penetrations in the VIMS. Locations where
Pour-N-Seal™ was used are noted on Sheet VM-3 in Appendix C.

Monitoring points were installed during construction to allow for influence testing and collection
of sub-slab vapor samples in the warehouse and guardhouse. The monitoring points in the
warehouse building (14 monitoring points) and the guardhouse (two monitoring points) are
constructed with 2-inch diameter SCH 40 PVC piping. The monitoring points in the warehouse
building include interior and exterior access points, and the monitoring points in the guardhouse
are finished at the building exterior. The monitoring point as-built details are included on Sheet
VM-2 and the locations of the monitoring points are shown on Sheets VM-2 and VM-4 (Appendix
C).

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2.2 VIMS Influence Testing
Influence testing was performed for the warehouse and the guardhouse to evaluate the vacuum
communication beneath the slabs and to document that sufficient sub-slab depressurization can be
obtained should electric fans be needed in the future. H&H completed influence testing for the
warehouse on February 6, 2023 and for the guardhouse on February 7, 2023. DEQ considers 4
Pascals (Pa) or 0.016 inches water column (in-WC) differential pressure to be the minimum
vacuum needed for an active depressurization system to effectively treat potential structural vapor
intrusion.

The influence testing was completed using Festa AMG Eagle Extreme (Eagle Extreme) and
RadonAway RP-145 (RP-145) fans to model an active depressurization system. Differential
pressure measurements were collected at each vacuum monitoring point using a Dwyer series 475
Mark III Digital manometer (capable of measuring 0.001 in-WC or 0.25 Pa), unless otherwise
noted on Appendix F-3, to establish baseline conditions prior to operation of the Eagle Extreme
and RP-145 electric fans. Following collection of baseline differential pressure measurements, the
electric fans were turned on and differential pressure measurements were collected at each
monitoring point.

Due to the number of risers in the warehouse building (30 within the warehouse slab on grade and
five {5} in the railspur) and the presence of the interior railspur, the influence test was conducted
in three parts. For the first test, electric fans were connected to the rooftop discharge of 15 of the
30 extraction points set under the slab-on-grade warehouse floor, indicated in the summary table
included as Appendix F-1, while the remaining risers remained open at the discharge. After the
fans were activated, the vacuum was recorded at each of the monitoring points using the
manometer. For the second test, the fans were moved to the other 15 risers, as indicated in the
summary tabled included as Appendix F-2, and the process was repeated.

As noted above, the warehouse building includes an interior railspur in the northern portion of the
building that is set lower than the warehouse slab-on-grade elevation to assist with loading
operations. The railspur is not connected by a gravel layer to the slab-on-grade warehouse area
and therefore communication between the sub-grade of the railspur and the sub-slab of the slab-
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on-grade warehouse was not anticipated. H&H completed an influence test of the railspur
separately from the slab-on-grade warehouse portion by connecting Eagle Extreme electric fans to
the five extraction points set in the railspur and collected vacuum readings from nearby monitoring
points (MP-2, MP-3, MP-4, and MP-6) set within the slab-on-grade portion of the building.
Influence was not measured, as anticipated, but readings collected at the extraction point discharge
indicated the discharge points were successfully pulling vacuum as shown in the summary table
included as Appendix F-3.

Similar to the slab-on-grade portions of the warehouse, the influence test in the guardhouse was
conducted by connecting an RP-145 electric fan to the rooftop discharge, and vacuum was
measured from both monitoring points in the guardhouse. The guardhouse influence test results
are included in the Appendix F-4 summary table.

Final results of the influence tests indicated sub-slab vacuum measured at the monitoring points
ranged from 0.074 in-WC to 0.356 in-WC (18.41 Pa to 88.59 Pa) for the warehouse and from
0.361 in-WC to 0.482 in-WC (89.83 Pa to 119.94 Pa) for the guardhouse, which demonstrates
vacuum above the DEQ minimum of 0.016 in-WC (4 Pa) can be achieved below the slabs of the
warehouse and the guardhouse. The locations of the monitoring points are shown in sheet VM-3
and VM-4 (Appendix C). The pilot test field data is included in summary tables Appendix F-1
through Appendix F-4.

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3.0 Pre-Occupancy VIMS Effectiveness Sampling
Following installation of the VIMS, completion of successful influence testing, and general
enclosure of the building envelope, H&H collected sub-slab soil vapor samples in accordance with
the DEQ-approved VIMP. Fourteen (14) sub-slab soil gas samples were collected from the
warehouse and one sub-slab soil gas sample was collected from the guardhouse. In addition, three
(3) indoor air samples were collected from the office area of the warehouse building concurrent
with the sub-slab soil gas samples.

The sub-slab soil gas and indoor air assessment activities were conducted in general accordance
with the DEQ-approved VIMP and the DEQ Department of Waste Management (DWM) Vapor
Intrusion Guidance (Guidance) dated March 2018. Details of the sub-slab soil vapor and indoor
air sampling activities and results are provided in the following sections.

3.1 Sub-Slab Soil Gas Sampling Methodology

On March 6 through 7, 2023, H&H collected sub-slab soil gas samples from permanent monitoring
points within the warehouse and guardhouse buildings. The sampling was performed following
VIMS installation activities and several weeks after installation of the ventilators. The sub-slab
soil vapor samples were collected from each permanent monitoring point in the warehouse (MP-1
through MP-14) and from one monitoring point in the guardhouse (MP-15) (see sample locations
on VM-3 and VM-4 in Appendix C).

For quality assurance/quality control (QA/QC) purposes, one duplicate sub-slab soil vapor sample
(MP-DUP) was collected from the MP-5 location. The duplicate sample was collected utilizing a
laboratory-supplied stainless-steel sampling “T” fitting which allows for the simultaneous
collection of two sub-slab soil vapor samples from a single air-intake.

To collect the sub-slab soil gas samples, Teflon sample tubing was secured to a 2-inch expandable
well cap with a sampling port that was secured onto the 2-inch diameter PVC monitoring point.
The tubing was connected to a laboratory-supplied airflow regulator and batch-certified 1-liter
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stainless steel Summa canister using a nut and ferrule assembly to create an airtight seal. The
airflow regulator was preset by the laboratory to collect a soil vapor sample over a 10-minute
period at a flow rate no greater than approximately 100 milliliters per minute.

Prior to sample collection, H&H conducted a leak test at each monitoring point by placing a shroud
around the monitoring point and sampling train including the Summa canister. The air within the
shroud was flooded with helium vapor and concentrations within the shroud were measured with
a calibrated helium detector. Helium concentrations within the shroud were maintained between
approximately 7% and 16%. A GilAir vacuum pump was connected to the sample tubing outside
of the shroud and used to purge a minimum of three volumes (monitoring point and sample train)
of soil vapor into a Tedlar® bag at each sampling point. The helium detector was used to measure
helium concentrations within the Tedlar bag sample to confirm helium concentrations in the
sample train were less than 10% of that measured within the shroud. Results of the helium leak
checks indicated that short-circuiting at the monitoring points or within the sampling train were
not present. Soil vapor sampling field forms completed by sampling personnel are included in
Appendix F.

Following successful leak checks, the airflow regulators were opened to allow collection of the
sub-slab soil gas samples. Vacuum in the Summa canisters was monitored during the sampling
event to confirm adequate sample volume was collected at each monitoring point location. Upon
completion of sample collection, the airflow regulator was closed to the Summa canister. The
canisters were labeled with the sample identification, beginning and ending times, pressure
measurements, and the requested analysis. The canisters were then placed in laboratory-supplied
shipping containers and delivered to SGS North America Inc. (SGS) under standard chain of
custody protocols for analysis of VOCs by EPA Method TO-15.

3.2 Sub-Slab Soil Gas Sampling Results
The sub-slab soil gas sample analytical results are summarized in Table 1. In Table 1, the soil gas
sample results are compared to the DEQ Non-Residential Vapor Intrusion Sub-Slab and Exterior
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Soil Gas Screening Levels (SGSLs) dated January 2023. The laboratory analytical report and the
chain of custody record are provided in Appendix G.

Warehouse
Laboratory analytical results for the warehouse building indicate that several compounds were
detected in the sub-slab samples at concentrations above the laboratory method detection limits
(MDLs). Benzene was detected in samples collected from MP-5 (up to 229 µg/m3) and MP-6 (171
µg/m3) at concentrations exceeding the Non-Residential SGSL of 160 µg/m3. Benzene was also
detected in MP-2, MP-3, MP-7, MP-12, and MP-13 at concentrations above the laboratory MDLs
but below the Non-Residential SGSLs. No other compounds were detected in the sub-slab soil
gas samples collected from the warehouse building at concentrations exceeding the Non-
Residential SGSLs.

The duplicate sub-slab soil gas sample (MP-DUP) was collected from monitoring point location
MP-5. Analytical results indicate an estimated benzene concentration in MP-DUP of 1.7 J µg/m3
compared to the detected benzene concentration in MP-5 of 229 µg/m3. Note that the J-Flag
designation indicates that the compound was detected at a concentration above the laboratory
method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated
concentration. A comparison of the parent and duplicate sample results for all other detected
compounds indicate relatively good correlation and therefore the discrepancy between the MP-5
and MP-DUP benzene concentrations is considered anomalous.

Guardhouse
Laboratory analytical results from MP-15 collected in the guardhouse building indicate that several
compounds were detected in the sub-slab soil gas sample at concentrations above the laboratory
MDLs; however, no compounds were detected at concentrations exceeding the Non-Residential
SGSLs.

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3.3 Sub-Slab Soil Gas Vapor Intrusion Evaluation
The DEQ Vapor Intrusion SGSLs are conservative and based on a lifetime incremental cancer risk
(LICR) of 1 x 10-6 and a hazard quotient (HQ) of 0.2 for potential non-carcinogenic risks. The
DEQ and EPA acceptable risk level for potential carcinogenic risks is a cumulative LICR of 1 x
10-4 or less, and the acceptable level for non-carcinogenic risks is a cumulative HI of 1.0 or less.
The HI is the sum of hazard quotients (HQs) for each target analyte detected in a sample.

To further evaluate sub-slab soil gas concentrations, H&H utilized the DEQ Risk Calculator
(January 2023) to calculate potential vapor intrusion risks for each building. H&H modeled a
worst-case scenario for the warehouse and the guardhouse by using the highest concentrations of
any compound detected in any sample below the slab of each building. Based on the planned uses
of the buildings, H&H calculated risks for both buildings assuming a non-residential use scenario.
The calculated cumulative LICR and HI values are provided in Table 1, and copies of the
completed DEQ Risk Calculators are provided in Appendix H. Results of risk calculations for
each Site building are discussed below.

Warehouse
As shown in Table 1, the non-residential worst-case risk calculation for the warehouse using the
sub-slab data indicates a calculated cumulative LICR of 1.5 x 10-6 and a HI value of 0.078. The
calculated cumulative LICR and HI values are within the acceptable levels established by the DEQ
and EPA. Thus, the sub-slab soil vapor analytical results and risk calculations indicate that the
VIMS is effectively minimizing the sub-slab accumulation of compounds at concentrations that
would pose potential vapor intrusion risks at unacceptable levels for the warehouse.

Guardhouse
As shown in Table 1, the non-residential worst-case risk calculation for the guardhouse indicates
a calculated cumulative LICR of 1.0 x 10-8 and a HI value of 0.0082. The calculated cumulative
LICR and HI values are within the acceptable levels established by the DEQ and EPA. Thus, the
sub-slab soil vapor analytical results and risk calculations indicate that the VIMS is effectively
minimizing the sub-slab accumulation of compounds at concentrations that would pose potential
vapor intrusion risks at unacceptable levels for the guardhouse.
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3.4 Building Survey Activities

Prior to collecting indoor air samples, H&H completed a survey within the office area of the
warehouse to identify potential above-slab sources of VOCs. At the time of sampling, some
interior finishing work had been completed and additional finishing work was ongoing, as
explained further below in Section 3.5. H&H observed use of heavy equipment inside and outside
of the warehouse for ongoing construction-related purposes on-Site. The heating, ventilation, and
air conditioning (HVAC) system for the office area of the warehouse was not yet installed at the
time of indoor air sampling.

H&H obtained available SDSs for building materials used around the time of the sampling event.
The SDSs provided by the general contractor are provided in Appendix I. The SDS for the
denatured alcohol observed in the warehouse indicates the denatured alcohol contains isopropanol
and methyl isobutyl ketone (4-methyl-2-pentanone). Note, neither benzene nor petroleum
products were identified in the SDSs provided by the general contractor. Copies of the indoor air
building survey form and the sampling forms completed by H&H sampling personnel during the
indoor air sampling event are included in Appendix F.

3.5 Indoor Air Sampling Methodology

On March 6, 2023, H&H collected three indoor air samples (IAS-1, IAS-2, and IAS-3) from within
the office area in the southwestern corner of the warehouse building. The indoor air samples were
collected prior to collection of sub-slab soil vapor samples with interior access points to avoid
potential cross-contamination associated with temporarily opening and purging the sub-slab
monitoring points.

The March 2023 indoor air sampling was performed following VIMS installation activities and
several weeks after installation of the ventilators. As noted above, the building envelope was
enclosed but construction and finishing work were ongoing and the HVAC systems were not
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operational. The drop ceiling in the office spaces and installation of doors was not completed at
the time of the indoor air sampling event and the office area was open to the warehouse space, in
which bay doors were open. Therefore, in order to isolate the sampled rooms from the warehouse
air, each room was sealed with plastic in place of the drop ceiling and doors. The locations of the
indoor air samples are shown on Sheet VM-3 of Appendix D. Note, the proposed sample location
for IAS-2 was in the break room area; however, in order to properly seal the space, the sample was
moved to the adjacent office as shown on VM-3. Each sample was located in an unfinished office
that included primed walls, installed windows, and an unfinished concrete floor.

In addition to the indoor air samples, an exterior background ambient air sample (BAS-1) was
collected at the time of the indoor air sampling event. The background sample was collected off
the western corner of the warehouse, upwind of the warehouse building as determined on the day
of the sampling event based on the prevailing wind direction.

The background and indoor air samples were collected using 6-liter stainless steel Summa sample
canisters connected to in-line flow controllers with a vacuum gauge. The indoor air samples were
collected using individually-certified Summa canisters, and the background air sample was
collected using a batch-certified Summa canister. The flow controllers were set by the laboratory
to allow collection of the samples over an 8-hour period. The sample intake point for each canister
was positioned approximately 5 ft above grade (typical breathing zone height). One duplicate
indoor air sample (IAS-DUP) was collected for quality assurance/quality control (QA/QC)
purposes from the IAS-1 parent location during the sampling event. The duplicate sample was
collected utilizing a laboratory-supplied stainless-steel sampling “T” fitting which allows for the
simultaneous collection of two indoor air samples from a single air intake.

During the sampling activities, indoor/outdoor air pressure differential was measured for the
building near the start, middle, and end of the 24-hour sampling period using a manometer
sensitive to 0.001 inches of water. In addition, Site-specific weather conditions including exterior
wind speed, exterior wind direction, indoor/outdoor temperature, barometric pressure, and
precipitation were recorded near the start, middle, and end of the sampling period. Indoor air
sampling field forms completed by sampling personnel are included in Appendix F.
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Prior to and after the indoor and background air samples were collected, vacuum in the canisters
was measured using a laboratory-supplied vacuum gauge and recorded by sampling personnel.
The starting vacuum was within 10% of the vacuum when the Summa canisters left the laboratory.
Vacuum within the sample canisters was not allowed to reach 0 inches of mercury; each sample
was collected when the canister reached 5 inches of mercury.

The starting and ending vacuums in each canister were recorded by sampling personnel on the
sample chain of custody. The sample canisters were then labeled, packaged in a laboratory
provided container, and shipped under standard chain of custody protocols to SGS for analysis of
a select list of VOCs by TO-15. The target analyte list was determined based on the VOCs detected
in the sub-slab soil vapor samples and any compounds detected at the Site during previous
evaluations. The select VOC list analyzed is included in Table 2.

3.6 Indoor Air Sampling Results
The analytical results for the indoor air samples are summarized in Table 2, and the laboratory
analytical report with chain of custody record is provided in Appendix G. In Table 2, the indoor
air laboratory analytical results are compared to the DEQ Non-Residential Vapor Intrusion Indoor
Air Screening Levels (IASLs) dated January 2023.

The indoor air sample analytical results indicate that several compounds were detected at
concentrations above laboratory MDLs in each sample. Benzene was detected at each indoor air
sample location (up to 2.7 µg/m3) at concentrations exceeding the Non-Residential IASL of 1.6
µg/m3. The analytical results for duplicate sample IAS-DUP-1, collected at the IAS-1 sample
location, indicate a benzene concentration of 2.1 µg/m3 which exceeds the Non-Residential IASL,
compared to the IAS-1 concentration of 1.5 µg/m3 which is below the Non-Residential IASL. No
other compounds were detected above the Non-Residential IASLs in the indoor air samples
collected from the warehouse building.

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The background ambient air sample IAS-BKG was collected upwind of the warehouse building to
evaluate ambient air conditions. Several compounds were detected in the background sample at
concentrations exceeding the laboratory MDLs, and chloroform was detected at a concentration of
0.73 J µg/m3 which exceeds the Non-Residential IASL of 0.53 µg/m3. In addition, benzene was
detected in the background sample at a concentration of 0.45 J µg/m3.

As noted during the building survey, heavy machinery was operating outside and inside the
warehouse as part of ongoing construction activities which could be a potential above grade source
of benzene in indoor air. Additionally, benzene was detected in the background air sample and
was not detected above the laboratory MDL in any sub-slab soil gas sample collected in the office
area (MP-9 through MP-11). Based on the ongoing construction activities, background air sample
detections, and the absence of benzene detections in the office area sub-slab, the benzene
concentrations detected in the indoor air samples are likely associated with above ground sources
and not sub-slab vapor intrusion.

The duplicate indoor air sample (IAS-DUP-1) indicates a trichloroethylene (TCE) concentration
of 1.5 µg/m3, but the parent sample (IAS-1) did not indicate TCE above the laboratory MDL of
0.10 µg/m3. The detected TCE concentration in the duplicate sample is below the Non-Residential
IASL of 1.8 µg/m3. TCE was not detected above the laboratory MDL in any sub-slab soil gas
sample collected from the warehouse and was not detected in any other indoor air sample.
Therefore, H&H considers the TCE detection in the duplicate indoor air sample to be an anomalous
detection and not representative of sub-slab vapor intrusion.

3.7 Indoor Air Vapor Intrusion Evaluation
The DEQ IASLs are conservative and based on a LICR for potential carcinogenic risks of
1 x 10-6 and a HQ of 0.2 for potential non-carcinogenic risks and only apply to indoor air
contaminants from structural vapor intrusion. As noted previously, The DEQ and EPA acceptable
risk level for potential carcinogenic risks is a cumulative LICR of 1 x 10-4 or less and the acceptable
level for non-carcinogenic risks is a HI of 1.0 or less.

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H&H utilized the DEQ Risk Calculator (January 2023) to evaluate risks associated with the
detected indoor air concentrations. Risk calculations were completed using a non-residential use
scenario for the industrial warehouse office space. A conservative, worst-case scenario was
evaluated using the highest concentration of any compound detected within any warehouse indoor
air sample. Note, although H&H considers the TCE detection in the duplicate indoor sample to
be an anomalous detection and the benzene concentrations to be attributed to above-slab sources,
both the TCE concentration and the highest benzene concentration were used in the worst-case
risk calculation as a conservative measure. The calculated cumulative LICR and HI values are
discussed below and are summarized in Table 2.

The calculated risks for a hypothetical worst-case non-residential scenario for the warehouse office
area indicate the cumulative LICR is 3.0 x 10-6 and the HI is 0.32. Risk calculator results indicate
that under a hypothetical worst-case scenario for non-residential use in the warehouse office area,
the cumulative LICR is less than 1 x 10-4 and the cumulative HI is less than 1.0. It is important to
note that the calculated cumulative LICR and HI values include compounds that are not considered
representative of Site conditions or attributable to outdoor, background air sources and/or above-
slab sources, as discussed above. If those compounds were removed from the risk calculations,
calculated risk levels would be lower. Copies of the completed risk calculators are provided in
Appendix H.

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4.0 Summary and Conclusions
Installation of the VIMS has been completed for the warehouse, guardhouse, and fire pumphouse
at the west side of the AquAir II Brownfields property (Brownfields Project No. 18038-14-060).
Results of installation inspections, influence testing, and effectiveness sampling activities indicate
that the VIMS has been successfully installed in accordance with the DEQ-approved VIMP.

During construction of the Site buildings, H&H conducted VIMS installation inspections to verify
that the systems were installed as designed and completed post-installation VIMS testing activities
to evaluate the effectiveness of the VIMS. A brief summary of the VIMS installation and post-
installation effectiveness assessment activities is provided below.

VIMS Installation and Influence Testing
VIMS installation has been completed for the warehouse, guardhouse, and the fire pumphouse.
The VIMS for the warehouse and the guardhouse include a gravel layer, vapor barrier, sub-slab
horizontal collection piping, and vertical extraction piping to the roof connected to pipe cap
ventilators. Because the fire pumphouse will not be occupied unless maintenance is being
conducted, the VIMS for the pumphouse includes a gravel layer and vapor barrier. During
installation of the VIMS, H&H personnel, under the direction of a NC licensed Professional
Engineer, conducted inspections during each stage of installation. As documented during the
inspections and in the Site photographs, the VIMS was installed in general accordance with the
DEQ-approved VIMP.

Following installation of the VIMS sub-slab piping network and riser piping, H&H completed
vacuum influence pilot testing to evaluate vacuum communication beneath the slab. Final vacuum
measurements collected during the pilot testing activities indicate that vacuum communication
beneath the slabs of the warehouse and guardhouse was achieved with acceptable differential
pressure levels.

VIMS Effectiveness Testing – Sub-Slab Soil Gas
Sub-slab soil gas analytical results for the warehouse indicate that with the exception of benzene,
no compounds were detected at concentrations above the DEQ Non-Residential Vapor Intrusion
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SGSLs. In addition, no compounds were detected above the Non-Residential SGSLs in the sub-
slab soil gas sample collected from the guardhouse. Results of the hypothetical worst-case risk
calculations for both the warehouse and the guardhouse indicate acceptable risk levels for a non-
residential exposure scenario. Based on the sub-slab soil vapor data and the DEQ Risk Calculator
results, the detected sub-slab vapor concentrations at the Site do not pose an unacceptable vapor
intrusion risk.

VIMS Effectiveness Testing – Warehouse Indoor Air
In accordance with the DEQ-approved VIMP, indoor air samples were collected from the office
area in the southwestern corner of the warehouse. The analytical results indicate that several VOCs
were detected in the samples at concentrations above the laboratory MDLs. Benzene was detected
above the DEQ Non-Residential Vapor Intrusion IASLs; however, no other compounds were
detected above the Non-Residential IASLs in indoor air. The background ambient air sample
results indicate that chloroform was detected at a concentration exceeding the Non-Residential
IASL. Benzene was detected in the ambient background sample above the laboratory MDL, was
not detected in the sub-slab vapor below the office, and H&H observed heavy machinery use inside
and outside the warehouse as part of ongoing construction activities during the indoor air sampling
event; therefore, the detected benzene concentrations in indoor air are likely attributable to above
grade sources. TCE was detected in the duplicate indoor air sample at a concentration above the
laboratory MDL but below the Non-Residential IASL and was not detected in the parent indoor
air sample, IAS-1. Because TCE was not detected in the sub-slab soil gas samples from the
warehouse nor was it detected in any other indoor air sample, including the parent sample, the
detected TCE concentration in the duplicate indoor air sample is considered anomalous.

The hypothetical worst-case risk calculations completed for the indoor air samples for a non-
residential use scenario indicate that the calculated risks associated with the detected indoor air
concentrations in the warehouse office area are within the acceptable risk levels established by
DEQ and EPA. Note, the worst-case scenario was calculated using compound concentrations
considered not representative of Site conditions or attributed to an above-grade source and
represents a conservative scenario.

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Summary
Based on the VIMS installation inspections, influence testing, post-installation sub-slab soil vapor
sampling results, and indoor air sampling results, the VIMS is effectively mitigating potential
vapor intrusion risks in the warehouse, guardhouse, and fire pumphouse. In accordance with the
DEQ-approved VIMP, post-occupancy sub-slab soil vapor sampling will be completed
approximately 6 months following the pre-occupancy event and on a semi-annual basis for future
events. In the office area of the warehouse, indoor air sampling will be completed concurrent with
the first post-occupancy sub-slab soil vapor sampling event. If semi-annual sampling results
indicate consistent or decreasing concentrations within acceptable risk levels, a request to modify
or terminate sampling will be submitted for DEQ approval. After each post-construction sampling
event, a brief report will be submitted to DEQ to document the sampling activities and results.

Engineer’s Certification
According to the DWM Vapor Intrusion Guidance: “Risk-based screening is used to identify sites
or buildings likely to pose a health concern, to identify buildings that may warrant immediate
action, to help focus site-specific investigation activities or to provide support for building
mitigation and other risk management options including remediation.” In addition, the DEQ-
approved VIMP was prepared to satisfy the standard vapor intrusion mitigation provisions
included in the Brownfields Agreement. Per the North Carolina Brownfields Property Reuse Act
130A-310.32, a prospective developer, with the assistance of H&H for this project, is to provide
DEQ with “information necessary to demonstrate that as a result of the implementation of the
brownfields agreement, the brownfields property will be suitable for the uses specified in the
agreement while fully protecting public health and the environment instead of being remediated to
unrestricted use standards.” It is in the context of these risk-based concepts that the H&H
professional engineer makes the following statement:

The Vapor Intrusion Mitigation System (VIMS) detailed herein is designed to mitigate intrusion
of subsurface vapors into the subject buildings from known Brownfields Property contaminants in
a manner that is in accordance with the most recent and applicable guidelines including, but not
limited to, DWM Vapor Intrusion Guidance, Interstate Technology & Regulatory Council (ITRC)
guidance, and American National Standards Institute (ANSI)/American Association of Radon
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Scientists and Technologists (AARST) standards. The sealing professional engineer below is
satisfied that the design and its installation are fully protective of public health from known
Brownfields Property contaminants.

Tables
Table 1Summary of Sub-Slab Soil Gas Analytical DataAquAir II Brownfields Site - West Side13300 Sam Neely RoadCharlotte, North CarolinaH&H Job No. TKC-008Sample LocationScreening CriteriaSample IDMP-1 MP-2 MP-3 MP-4 MP-6 MP-7 MP-8Sample Type Sub-Slab Sub-Slab Sub-Slab Sub-Slab Sub-Slab Sub-Slab Sub-SlabSample Date3/7/2023 3/6/2023 3/7/2023 3/6/2023 3/7/2023 3/7/2023 3/8/2023UnitsVOCs (TO-15)Acetone22 63.4 40.6 47.0 83.6 67.9 430 302 121 NEBenzene<0.8072.8 2.0 J<0.802291.7 J1712.8<0.801601,3-Butadiene<0.75 <0.75 <0.75 <0.75 <0.75 <0.75 <1.5 <0.75 <0.7541Carbon Disulfide<0.56 <0.562.1 J 1.5 J 1.3 J 1.3 J<1.11.3 J<0.5661,000Chloromethane1.1 J<0.740.93 J<0.741.9 2.0<1.51.2 J<0.747,900Cyclohexane<1.5 <1.5 <1.5 <1.5 <1.5 <1.5 <3.01.6 J<1.5530,000Dichlorodifluoromethane2.0 J 2.0 J 2.0 J 2.2 J 2.0 J 2.1 J<1.32.1 J 2.0 J 8,800Ethyl Acetate17 5.0 146 26 26 25 43.2 192<1.56,100Ethylbenzene<1.0 <1.01.9 J<1.0 <1.0 <1.0 <2.12.2 J<1.0490Heptane1.9 J<1.5 <1.51.6 J 2.8 J<1.5 <3.0 <1.5 <1.535,000n-Hexane<1.61.9 J<1.6 <1.61.9 J<1.6 <3.2 <1.6 <1.661,000Isopropyl Alchohol3.2 2.3 14 2.5 3.9 7.9 6.1 15<1.418,000Methyl Ethyl Ketone (MEK)4.7 34.8 24 28 44.5 25 366 273 43.4 440,000Methyl Tert Butyl Ether (MTBE)<1.2 <1.2 <1.2 <1.2 <1.2 <1.2 <2.3 <1.2 <1.24,700Methylene Chloride<0.764.5 3.8<0.76 <0.76 <0.765.2 J 2.9<0.7653,000Propene<0.982.7 J<0.98 <0.98 <0.98 <0.98 <1.9 <0.98 <0.98260,000Tetrachloroethene<0.38 <0.381.4<0.38 <0.38 <0.38 <0.75 <0.38 <0.383,500Tetrahydrofuran200 166 111 92.0 2,520 1,590 1,100 761 211 180,000Toluene2.6 J 3.0 11 1.9 J 15 5.3 11 12<0.87440,000o-Xylene<1.3 <1.31.7 J<1.3 <1.3 <1.3 <2.72.0 J<1.38,800m,p-Xylene<2.4 <2.45.6<2.43.4 J<2.4 <4.86.9<2.48,800DEQ Risk Calculator(2)Accetable Risk LevelsLICR (Non-Residential)<1.0 x 10-4Non-Carcinogenic HI (Non-Residential)<1.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated January 2023 and based upon TCR = 1 x 10-6 and THQ = 0.2.2) DEQ Cumulative Risk Calculator dated January 2023 and is based up on a TCR = 1 x 10-6 and THQ = 0.2.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses. Only compounds detected in at least one sample are shown in the above table.Bold values indicate an exceedance of DEQ Non-Residential SGSL . Cumulative LICR and HI values calculated using the highest concentration of any compound detected in any sample collected to evaluate each building. Results are compared to DEQ and EPA acceptable risk levels for carcinogenic and non carcinogenic risks.TCR = Target Cancer Risk; THQ = Non-Carcinogenic Target Hazard Quotient; LICR = Lifetime Incremental Cancer Risk; HI = Hazard IndexVOCs = volatile organic compounds; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.1.5x10-6µg/m3Warehouse BuildingMP-5 / MP-DUP3/7/2023Sub-SlabNon-Residential SGSLs (1)0.078https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Install Completion Report/TKC.008 Data Tables4/21/2023Table 1 (Page 1 of 2)Hart & Hickman, PC
Table 1Summary of Sub-Slab Soil Gas Analytical DataAquAir II Brownfields Site - West Side13300 Sam Neely RoadCharlotte, North CarolinaH&H Job No. TKC-008Sample LocationGuardhouse Screening CriteriaSample IDMP-9 MP-10 MP-11 MP-12 MP-13 MP-14 MP-15Sample Type Sub-Slab Sub-Slab Sub-Slab Sub-Slab Sub-Slab Sub-Slab Sub-SlabSample Date3/7/2023 3/7/2023 3/6/2023 3/7/2023 3/6/2023 3/6/2023 3/6/2023UnitsVOCs (TO-15)Acetone420 15,800 1,410 86.2 221 177 88.8 NEBenzene<0.80 <16 <3.23.5 2.2 J<0.801.6 J 1601,3-Butadiene<0.75 <0.75 <2.91.7 J<0.75 <0.75 <0.7541Carbon Disulfide<0.56 <11 <2.2 <0.56 <0.56 <0.56 <0.5661,000Chloromethane1.9<15 <2.9 <0.74 <0.74 <0.74 <0.747,900Cyclohexane<1.5 <30 <6.2 <1.52.1 J<1.53.3 530,000Dichlorodifluoromethane2.0 J<13 <2.52.2 J 2.1 J 2.1 J 2.2 J 8,800Ethyl Acetate30<3019 6.8 200 46.4 238 6,100Ethylbenzene<1.0 <21 <4.36.1 2.3 J<1.0 <1.0490Heptane<1.5 <30 <6.16.6<1.5 <1.52.6 J 35,000n-Hexane1.7 J<32 <6.32.4 J<1.6 <1.6 <1.661,000Isopropyl Alchohol5.7 44.0 18 2.5 16 11 4.7 18,000Methyl Ethyl Ketone (MEK)401 10,600 1,070 61.6 145 142 41.0 440,000Methyl Tert Butyl Ether (MTBE)<1.2130<4.7 <1.2 <1.2 <1.2 <1.24,700Methylene Chloride5.6<16 <3.1 <0.763.1 3.3 6.3 53,000Propene<0.98 <19 <4.0 <0.98 <0.98 <0.98 <0.98260,000Tetrachloroethene<0.38 <7.5 <1.5 <0.38 <0.38 <0.38 <0.383,500Tetrahydrofuran1,440 40,400 3,270 239 852 220 137 180,000Toluene2.1 J<179.0 J 19 12 2.3 J 7.9 440,000o-Xylene<1.3 <27 <5.26.1 2.0 J<1.3 <1.38,800m,p-Xylene2.6 J<48 <9.619 6.9<2.4 <2.48,800DEQ Risk Calculator(2)Accetable Risk LevelsLICR (Non-Residential)1.0 x 10-8<1.0 x 10-4Non-Carcinogenic HI (Non-Residential)0.0082 <1.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Vapor Intrusion Sub-Slab & Exterior Soil Gas Screening Levels (SGSLs) dated January 2023 and based upon TCR = 1 x 10-6 and THQ = 0.2.2) DEQ Cumulative Risk Calculator dated January 2023 and is based up on a TCR = 1 x 10-6 and THQ = 0.2.Concentrations are reported in micrograms per cubic meter (µg/m3).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical method is shown in parentheses. Only compounds detected in at least one sample are shown in the above table.Bold values indicate an exceedance of DEQ Non-Residential SGSL. Cumulative LICR and HI values calculated using the highest concentration of any compound detected in any January 2023 samples collected to evaluate each building. Results are compared to DEQ and EPA acceptable risk levels for carcinogenic and non carcinogenic risks.TCR = Target Cancer Risk; THQ = Non-Carcinogenic Target Hazard Quotient; LICR = Lifetime Incremental Cancer Risk; HI = Hazard IndexVOCs = volatile organic compounds; NE = not establishedJ = Compound was detected above the laboratory method detection limit, but below the laboratory reporting limit resulting in a laboratory estimated concentration.Warehouse Buildingµg/m31.5x10-60.078Non-Residential SGSLs (1)https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Install Completion Report/TKC.008 Data Tables4/21/2023Table 1 (Page 2 of 2)Hart & Hickman, PC
Table 2Summary of Indoor Air Analytical DataAquAir II Brownfields Site - West Side13300 Sam Neely RoadCharlotte, North CarolinaH&H Job No. TKC-008Sample LocationBackground Screening CriteriaSample IDIAS-2 IAS-3 IAS-BKGDate3/6/2023 3/6/2023 3/6/2023UnitsVOCs (TO-15)Acetone 73.2 90.5 64.9 167 7.1 NEBenzene 1.52.1 2.0 2.70.45 J 1.61,3-Butadiene<0.19 0.49 <0.19 <0.19 <0.190.412-Butanone (MEK) 13 19 27 156 1.6 4,400Carbon disulfide<0.14 <0.14 <0.141.2<0.14610Carbon tetrachloride<0.25 <0.25 <0.25 <0.25 <0.252.0Chlorobenzene<0.34 <0.34 <0.34 <0.34 <0.344.0Chloroform<0.18 <0.18 <0.18 <0.180.73 J0.53Chloromethane 1.2 1.3 1.1 1.3 1.2 79Cyclohexane 0.79 1.0 1.3 1.5<0.385,3001,2-Dichlorobenzene<0.90 <0.90 <0.90 <0.90 <0.90180Dichlorodifluoromethane 2.1 2.1 2.0 2.0 1.9 881,1-Dichloroethane<0.23 <0.23 <0.23 <0.23 <0.237.71,1-Dichloroethene<0.23 <0.23 <0.23 <0.23 <0.231801,2-Dichloroethane<0.28 <0.28 <0.28 <0.28 <0.280.47cis-1,2-Dichloroethene<0.31 <0.31 <0.31 <0.31 <0.3135trans-1,2-Dichloroethene<0.27 <0.27 <0.27 <0.27 <0.2735Ethyl Acetate 2.7 3.0 13 7.2 3.5 61Ethylbenzene 1.7 2.4 2.5 3.9<0.264.9Heptane 1.5 1.8 1.8 2.7<0.38350Hexachlorobutadiene<0.66 <0.66 <0.66 <2.1 <0.660.56Hexane 3.5 2.7 2.5<0.39 <0.39610Isopropanol 6.6 7.4 4.4 9.8 0.66 180Methyl tert-Butyl Ether<0.29 <0.29 <0.29 <0.29 <0.2947Methylene Chloride 4.9 0.69<0.190.73 0.73 5304-Methyl-2-pentanone (MIBK)<0.30 <0.300.45 J 0.70 J<0.302,600Propylene<0.24 <0.24 <0.247.2<0.242,6001,1,2,2-Tetrachloroethane<0.33 <0.33 <0.33 <0.33 <0.330.21Tetrachloroethene<0.095 <0.095 <0.095 <0.095 <0.09535Tetrahydrofuran 10 14 20 27<0.271,800Toluene 21 29 48.2 58.0 0.79 4,4001,2,4-Trichlorobenzene<0.89 <0.89 <0.89 <0.89 <0.891.81,1,1-Trichloroethane<0.20 <0.20 <0.20 <0.20 <0.204,4001,1,2-Trichloroethane<0.21 <0.21 <0.21 <0.21 <0.210.18Trichloroethene<0.101.5<0.10 <0.10 <0.101.8m&p-Xylene 6.1 7.8 6.5 11<0.6188o-Xylene 2.2 3.0 2.8 7.8<0.3388DEQ Risk Calculator2Acceptable Risk LevelsLICR (Non-Residential)--<1 x 10-4Non-Carcinogenic HI (Non-Residential)--<1.0Notes:1) NC Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Indoor Air Screening Levels (IASLs) (January 2023) based upon TCR = 1 x 10-6 and HQ = 0.2.2) DEQ Cumulative Risk Calculator dated January 2023 and is based up on a TCR = 1 x 10-6 and THQ = 0.2.Compound concentrations are reported in micrograms per cubic meter (μg/m3) and are reported to the laboratory method detection limits.Bold indicates concentration exceeds the Non-Residential IASL. Laboratory analytical methods are shown in parenthesesVOCs = volatile organic compounds; NE= Not Established; -- = Not CalculatedTCR = Target Cancer Risk; THQ = Non-Carcinogenic Target Hazard Quotient; LICR = Lifetime Incremental Cancer Risk; HI = Hazard IndexCumulative LICR and HI values calculated using the highest concentration of any compound detected in any indoor air sample. Results are compared to DEQ and EPA acceptable risk levels for carcinogenic and non carcinogenic risks.J = compound was detected above the laboratory method detection limit but below the laboratory reporting limit resulting in a laboratory estimated concentration.Non-Residential IASLs(1)3.0 x 10-60.32µg/m3Warehouse Office AreaIAS-1/IAS-DUP-13/6/2023https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Install Completion Report/TKC.008 Data TablesTable 2 (Page 1 of 1)Hart & Hickman, PC

Figures
BROWNFIELDS
PROPERTY
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE WEST, NORTH CAROLINA, 1996
TITLE
PROJECT
SITE LOCATION MAP
AQUAIR II BROWNFIELDS SITE - WEST SIDE 13300 SAM NEELY ROAD
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
10-28-21 0
1TKC-008
CR
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
FD
EF
L
CRCR
CR
REVISION NO. 0
JOB NO. TKC-008
DATE: 10-4-21
FIGURE NO. 3
AQUAIR II BROWNFIELDS SITE - WEST SIDE
13300 SAM NEELY ROAD
CHARLOTTE, NORTH CAROLINA
SITE MAP
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
LEGEND
BROWNFIELDS PROPERTY BOUNDARY
SITE BOUNDARY
LIMITS OF GROUNDWATER CONTAMINATION
RAILROAD TRACKS
SURFACE WATER FEATURE
FENCE LINE
PROPOSED BUILDING
FOOTPRINT
AREA OF POSSIBLE SOIL
CONTAMINATION
SAM NEELY ROAD
ALRO STEEL CORP.
(12933 SAM NEELY ROAD)
FORMER REMEDIATION
SYSTEM BUILDING
LAZY OAK LANE
RESIDENTIALRESIDENTIAL
TEXAS PIPE & SUPPLY CO.
(12910 SAM NEELY ROAD)
EXISTING STAPLES
WAREHOUSE BUILDING
STORMWATER MANAGEMENT
POND
SOURCES
1.SITE PLAN PROVIDED BY BURTON ENGINEERING.
2.BASE MAP OF THE HISTORICAL FEATURES FROM
S&ME, REMEDIAL INVESTIGATION REPORT,
OCTOBER 2011.
3.AERIAL PHOTOGRAPH FROM MECKLENBURG
COUNTY GIS.
FORMER
PRODUCTION
BUILDING
FORMER
LAB
BUILDING
FUTURE
CAROWINDS
BOULEVARD

Appendix A
Redevelopment Plan

HD CHARLOTTE BDC FDC403,200 SF195' - 0"420' - 0"280' - 0"195' - 0"960' - 0"445' - 3"SITE BOUNDARYSITE B O U N D AR YSITE BOUNDARYC A R O W I N D S B L V D44 TRAILER SPACES39 TRAILER SPACES5 FDC DOCK DOORS13 TRAILER SPACES2-BAY TARPING STRUCTURE5 BDC DOCK DOORS9 TRAILER SPACES 26 TRAILER SPACES23 TRAILER SPACES23 TRAILER SPACES26 TRAILER SPACES33 FUTURE TRAILER SPACES60' - 0"135' - 0"198 AUTO PARKING60' - 0"135' - 0"TRUCK SCALEA-1081A-10338' HIGH CHAIN-LINK FENCE WITH 3 STRANDS BARB WIRE -TYP. -SEE/6A-1028' HIGH CHAIN-LINK FENCE WITH 3 STRANDS BARB WIRE -TYP. -SEE/6A-1028' HIGH CHAIN-LINK FENCE WITH 3 STRANDS BARB WIRE -TYP. -SEE/6A-1028' HIGH CHAIN-LINK SWING GATE WITH 3 STRANDS BARB WIRE AT RAILROAD TRACK -SEE/1A-1038' HIGH CHAIN-LINK SWING GATE WITH 3 STRANDS BARB WIRE AT RAILROAD TRACK -SEE/1A-1036' HIGH BLACK VINYL COATED CHAIN-LINK FENCE AT ASSOCIATE PARKING -TYP. -SEE/7A-102DETENTIONDETENTION5 TRAILER SPACES4 TRAILER SPACES12 FDC DOCK DOORS1 TRAILER SPACES21 FUTURE TRAILER SPACESDETENTIONA-10210A-1029A-1028OUTDOOR STORAGE289,207 S.F.PROPANE PLATFORMHIGH SPEED AND DRIVE-IN DOORSFHRAIL STOP -BY OTHERSGENERATOR AND TRANSFORMER LOCATIONS -SEEFHFHFHFHFHFHFHFH/2A-105INBOUND OFFICE AREAMAIN OFFICE AREAFIRE PUMPHOUSECOMPACTOR LOCATIONRAIL STOP -BY OTHERS16 BAYS AT 60'-0"1 BAY AT 60' + 2 BAYS AT 50' + 1 BAY AT 100' + 2 BAYS AT 50'+ 1 BAY AT 60' 40' - 0"235' - 0"36' - 8"30' - 0"40' - 0"GUARD HOUSE8 IN-BOUND TRUCK QUEUINGLIGHTPOLE -TYP. ASSOCIATE ENTRYILLUMINATED SITE MONUMENT SIGNTRUCK ENTRY7' - 0"64' - 0"ILLUMINATED SITE MONUMENT SIGN32' - 0"2 7 ' - 0 "LIGHT DUTY CONCRETE PAVING AT AUTO PARKINGHEAVY DUTY CONCRETE PAVINGLIGHTPOLE W/ TYPICAL BOLLARD PROTECTIONA-1051A-1061A-10252 TRAILER SPACESPROPANE PLATFORM60' - 0"75' - 0"60' - 0"A-1091Macgregor Associates Architects, Inc. - 1987-2021CTHIS DRAWING, AS AN INSTRUMENT OF SERVICE, IS AND SHALL REMAIN THE PROPERTY OF THE DESIGN PROFESSIONAL AND SHALL NOT BE REPRODUCED, PUBLISHED OR USED IN ANY WAY WITHOUT THE PERMISSION OF THE DESIGN PROFESSIONAL.THE CONTRACTOR SHALL VERIFY ALL DIMENSIONS AND EXISTING CONDITIONS AT THE SITE BEFORE PROCEEDING WITH EACH PHASE OF HIS WORK.SEALCONSULTANTPRINT RECORDPROJECT INFORMATIONDATE PROJECT NOSHEET TITLESHEET NUMBERNUMBER DATE DESCRIPTION2727 Paces Ferry Road SEBuilding Two, Suite 1400Atlanta, Georgia 30339T 770.432.9400 F 770.432.9934PROJECT SKINNYBDC FDC10/14/21ISSUED FOR PERMIT10/14/2110/15/2021 7:29:33 AMOVERALL SITEPLANA-101FOR CONSTRUCTION2021-07810/14/2113005 SAM NEELY ROADCHARLOTTE, NCGRAPHIC SCALE040160801" = 70'-0"1OVERALL SITE PLANN

Appendix B Previous Assessment Summary Tables and Sample Location Map

Table 1 (Page 1 of 5)Summary of Soil and Sediment Analytical DataAquAir II Brownfields PropertyCharlotte, North CarolinaH&H Job No. TKC-004Sampled ByGreenhorne & O'MaraSample IDSS-03 BAC-1 BAC-2 S-1 S-2 S-3 S-4 S-6 SED-1 SED-2 SED-3 SED-4TypeSoil Soil Soil Soil Soil Soil Soil Soil Sediment Sediment Sediment SedimentDepth (ft bgs)NR 1.0 1.0 1.0 1.0 1.0 1.0 1.0 0.5 0.5 0.5 0.5Sample Date10/25/1990 9/10/1992 9/10/1992 9/10/1992 9/10/1992 9/10/1992 9/10/1992 9/10/1992 9/10/1992 9/10/1992 9/10/1992 9/10/1992Range Range Mean Unitsmg/LVOCs (8260)AcetoneNS NS NS NS NS NS NS NS NS NS NS NS140,000---- ----BenzeneNS NS NS NS NS NS NS NS NS NS NS NS5.4---- ----2-Butanone (MEK)NS NS NS NS NS NS NS NS NS NS NS NS40,000---- ----Carbon DisulfideNS NS NS NS NS NS NS NS NS NS NS NS740---- ----Carbon Tetrachloride29<0.0065 <0.0065 <0.0065 <0.0055 <0.0143.40.026<0.32 <0.34 <0.010 <0.0263.0 ---- ----Chlorobenzene10NS NS NS NS NS NS NS NS NS NS NS280 ---- ----ChloroformBQL <0.0065 <0.00650.067<0.0055 <0.014 <0.280.025<0.32 <0.34 <0.010 <0.0261.5 ---- ----2-ChlorotolueneNS NS NS NS NS NS NS NS NS NS NS NS4,700 ---- ----1,2-DichlorobenzeneNS NS NS NS NS NS NS NS NS NS NS NS2,000 ---- ----1,1-DichloroethaneNS NS NS NS NS NS NS NS NS NS NS NS17 ---- ----1,2-DichloroethaneNS NS NS NS NS NS NS NS NS NS NS NS2.2 ---- ----1,1-DichloroetheneNS NS NS NS NS NS NS NS NS NS NS NS210 ---- ----cis-1,2-DichloroetheneNS NS NS NS NS NS NS NS NS NS NS NS470 ---- ----trans-1,2-DichloroetheneNS NS NS NS NS NS NS NS NS NS NS NS64 ---- ----Diisopropyl EtherNS NS NS NS NS NS NS NS NS NS NS NS2,000 ---- ----EthylbenzeneNS NS NS NS NS NS NS NS NS NS NS NS27 ---- ----HexachlorobutadieneNS NS NS NS NS NS NS NS NS NS NS NS5.6 ---- ----4-Methyl-2-pentanoneNS NS NS NS NS NS NS NS NS NS NS NS30,000 ---- ----Methylene ChlorideNS0.029 B 0.021 B 0.022 B 0.022 B<0.014 <0.280.021 B<0.32 <0.34 <0.010 <0.026650 ---- ----Tetrachloroethene150<0.0065 <0.00650.019<0.0055 <0.0141.3 0.18<0.32 <0.34 <0.010 <0.02682 ---- ----1,1,1,2-TetrachloroethaneNS NS NS NS NS NS NS NS NS NS NS NS9.3 ---- ----1,1,2,2,-TetrachloroethaneNS <0.0065 <0.0065 <0.0065 <0.00550.26<0.28 <0.0065 <0.32 <0.34 <0.010 <0.0262.8 ---- ----TolueneNS NS NS NS NS NS NS NS NS NS NS NS9,700 ---- ----1,2,3-TrichlorobenzeneNS NS NS NS NS NS NS NS NS NS NS NS190 ---- ----1,2,4-TrichlorobenzeneNS NS NS NS NS NS NS NS NS NS NS NS55 ---- ----1,1,1-Trichloroethane36<0.0065 <0.0065 <0.0065 <0.0055 <0.014 <0.280.007<0.32 <0.34 <0.010 <0.0267,600 ---- ----1,1,2-TrichloroethaneNS NS NS NS NS NS NS NS NS NS NS NS1.3 ---- ----Trichloroethene9.5<0.0065 <0.0065 <0.0065 <0.0055 <0.0141.2<0.0065 <0.32 <0.34 <0.010 <0.0264.0 ---- ----XylenesNS NS NS NS NS NS NS NS NS NS NS NS530 ---- ----SVOCs (8270)Benzoic Acid0.36 J/UDNA NA NA NA NA NA NA NA NA NA NA660,000 ---- ----Bis(2-Ethylhexyl)phthalate4.5 / 2.3 JDNA NA NA NA NA NA NA NA NA NA NA160 ---- ----Butylbenzylphthalate0.3 J/UDNA NA NA NA NA NA NA NA NA NA NA1,200 ---- ----1,4-Dichlorobenzene1.1 UDNA NA NA NA NA NA NA NA NA NA NA12 ---- ----Di-n-butylphthalate0.29 J/UD NA NA NA NA NA NA NA NA NA NA NA16,000 ---- ----Hexachlorobutadiene0.25 J/UDNA NA NA NA NA NA NA NA NA NA NA5.6 ---- ----Hexachloroethane0.2 J/UDNA NA NA NA NA NA NA NA NA NA NA8.5 ---- ----Phenol2.3 / 1.4 JDNA NA NA NA NA NA NA NA NA NA NA49,000 ---- ----1,2,4-Trichlorobenzene46 / 59DNA NA NA NA NA NA NA NA NA NA NA55 ---- ----RCRA Metals (6010/7470)ArsenicNA1<1.01.9 1.7 1.4 1.6<1.01.4 1.4 1.9<1.03 <1.0 - 1.0 1.0 - 18 4.8--Barium72.4 84 31 54 60 49 190 50 95 91 55 63 47,000 31 - 86.5 50 - 1,000 356--Cadmium788<1.0 <1.0 <1.0 <1.01.3 1.8<1.038 22 5.8 4.8 200 <1 - 9 1.0 - 10 4.3--Chromium (total)18,50022 10 30 50 74 95 110810 1,500200 300 6.5 10 - 24.4 7.0 - 300 65--Copper116NA NA NA NA NA NA NA NA NA NA NA9,300 NE 3.0 - 100 34--Lead2,8205 4 14 4 42 42 7.9 66 79 61 59 800 4 - 20.5 BRL - 50 16--Mercury11.1NA NA <0.25 <0.25 <0.25 <0.25 <0.250.91 0.46<0.25 <0.2570 BRL - <0.25 0.03 - 0.52 0.121--NickelBQL NA NA NA NA NA NA NA NA NA NA NA4,700 NE BRL - 150 23--SeleniumNA <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.01,200 NE <0.1 - 0.8 0.42--SilverBQL <2.0 <2.0 <2.0 <2.0 <2.0 <2.0 <2.09.8 3.0<2.0 <2.01,200 NE BRL - 5.0 NE--Vanadium106 130 74 140 3602,200370 1,150 700 340 510 290 1,200 NE 15 - 300 107--Zinc109NA NA NA NA NA NA NA NA NA NA NA70,000 NE 25 - 124 56--TCLP Metals (6010) {mg/L}CadmiumNA NA NA NA NA NA NA NA NA NA NA NA-- -- -- -- 1.0ChromiumNA NA NA NA NA NA NA NA NA NA NA NA-- -- -- -- 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.3) EPA Toxic Characteristic Leaching Procedure (TCLP) hazardous waste threshold level, 2004Only compounds detected in at least one sample are shown.Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Laboratory analytical methods are shown in parentheses.Bold values indicate compounds detected above Industrial/Commercial use PSRGs (and above regional background concentrations for metals).Underlined values indicate total concentration exceeds 20 times the TCLP regulatory levelVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act .NA = Not Analyzed; NE = Not Established; ft bgs = feet below the ground surface; -- = Not Applicable; NR = Not ReportedBQL = Below Laboratory Quantitation Limits; BRL = Below Reporting Limit; mg/L = milligrams per literJ = Analyte detected at a level less than the RL and greater than or equal to the MDL; D = Constituent was analyzed using a second dilution.U = Constituent was not detected using a second dilution; B = Constituent was also detected in the control blank.mg/kgDelta Environmental ConsultantsScreening CriteriaRegional Background Metals In Soil2TCLP Regulatory Threshold3Industrial/ CommercialPSRGs1Site-Specific Background Metals in Soilhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP Tables10/4/2021Table 1 (Page 1 of 5)Hart & Hickman, PC
Table 1 (Page 2 of 5)Summary of Soil and Sediment Analytical DataAquAir II Brownfields PropertyCharlotte, North CarolinaH&H Job No. TKC-004Sampled BySample IDTypeDepth (ft bgs)Sample Date UnitsVOCs (8260)AcetoneBenzene2-Butanone (MEK)Carbon DisulfideCarbon TetrachlorideChlorobenzeneChloroform2-Chlorotoluene1,2-Dichlorobenzene1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-DichloroetheneDiisopropyl EtherEthylbenzeneHexachlorobutadiene4-Methyl-2-pentanoneMethylene ChlorideTetrachloroethene1,1,1,2-Tetrachloroethane1,1,2,2,-TetrachloroethaneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneXylenesSVOCs (8270)Benzoic AcidBis(2-Ethylhexyl)phthalateButylbenzylphthalate1,4-DichlorobenzeneDi-n-butylphthalateHexachlorobutadieneHexachloroethanePhenol1,2,4-TrichlorobenzeneRCRA Metals (6010/7470)ArsenicBariumCadmiumChromium (total)CopperLeadMercuryNickelSeleniumSilverVanadiumZincTCLP Metals (6010) {mg/L}CadmiumChromiumSS-4 SS-5 SS-6 SS-7 SS-8 SUMP-1 SUMP-2 SED-1 SED-2 SED-3 SED-5 SED-6 SED-7Soil Soil Soil Soil Soil Soil Soil Sediment Sediment Sediment Sediment Sediment Sediment1.0 1.0 1.0 1.0 3.5 1.0 1.0 0.5 0.5 0.5 0.5 0.5 0.57/11/1996 7/11/1996 7/11/1996 7/11/1996 7/29/1996 7/11/1996 7/12/1996 1997 1997 1997 1997 1997 1997Range Range Meanmg/L0.220 0.900 J<15530 0.130 J<0.0063 <0.062NANA NA NA NA NA NA NA140,000---- ----<0.030 <0.731 <5.5 <39.3750.071<0.0063 <0.0062NANA NA NA NA NA NA NA5.4---- ----<0.060 <1.462 <31 <78.7500.210<0.0126 <0.0124NANA NA NA NA NA NA NA40,000---- ----0.0077 J<0.731 <15.5 <39.3750.013<0.0063 <0.0062NANA NA NA NA NA NA NA740---- ----<0.030 <0.7313.2 J<39.3753.5 D<0.0063 <0.0063NANA NA NA NA NA NA NA3.0 ---- ----0.037 0.600 J 120 8.6 J 0.140<0.0063 <0.0064NANA NA NA NA NA NA NA280 ---- ----0.170 0.8003.7 J<39.3751.1 DJ<0.0063 <0.0065NANA NA NA NA NA NA NA1.5 ---- ----<0.030 <0.731 <15.5 <39.3750.0081 J<0.0063 <0.0066NANA NA NA NA NA NA NA4,700 ---- ----0.018 J 3.6<15.5 <39.3750.720 DJ<0.0063 <0.0067NANA NA NA NA NA NA NA2,000 ---- ----0.024 J<0.731 <15.5 <39.3750.150<0.0063 <0.0068NANA NA NA NA NA NA NA17 ---- ----<0.030 <0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA2.2 ---- ----0.056<0.731 <15.5 <39.3751.6 J<0.0063 <0.0069NANA NA NA NA NA NA NA210 ---- ----0.640<0.731 <15.5 <39.3751.2<0.0063 <0.0061NANA NA NA NA NA NA NA470 ---- ----<0.030 <0.731 <15.5 <39.3750.089<0.0063 <0.00611NANA NA NA NA NA NA NA64 ---- ----<0.030 <0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA2,000 ---- ----<0.030 <0.731 <15.5 <39.3750.0067 J<0.0063 <0.00612NANA NA NA NA NA NA NA27 ---- ----<0.030 <0.731 <15.5 <39.3750.079<0.0063 <0.00613NANA NA NA NA NA NA NA5.6 ---- ----0.074<0.731 <15.5 <39.3750.530<0.0063 <0.00614NANA NA NA NA NA NA NA30,000 ---- ----<0.030 <0.731 <15.5 <39.3751.1<0.0063 <0.00615NANA NA NA NA NA NA NA650 ---- ----2.3 D 1949074082 D<0.0063 <0.00618NANA NA NA NA NA NA NA82 ---- ----<0.030 <0.731 <15.5 <39.3750.016 J 0.029<0.00616NANA NA NA NA NA NA NA9.3 ---- ----<0.03011 120<39.3750.650 0.05<0.00617NANA NA NA NA NA NA NA2.8 ---- ----0.030<0.7316.1 J<39.3750.084<0.0063 <0.00619NANA NA NA NA NA NA NA9,700 ---- ----0.015 J<0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA190 ---- ----<0.030 <0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA55 ---- ----<0.030 <0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA7,600 ---- ----<0.030 <0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA1.3 ---- ----<0.030 <0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA4.0 ---- ----<0.030 <0.731 <15.5 <39.375 <0.034 <0.0063 <0.0062NANA NA NA NA NA NA NA530 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA660,000 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA160 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA1,200 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA12 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA16,000 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA5.6 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA8.5 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA49,000 ---- ----NA NA NA NA NA NA NA NANA NA NA NA NA NA NA55 ---- ----3.82 4.61 4.59 3.42NA2.14 2.67NA NA NA NA NA NA NA NA3 <1.0 - 1.0 1.0 - 18 4.8--66.1 72 78.1 60.0NA46.6 62.8 570 230 84 49 66 160 100 150 47,000 31 - 86.5 50 - 1,000 356--11.6 J<0.582.95 38.3NA <0.64 <0.592.1 5.4 1.2 8 11 170 2.4 1.6 200 <1 - 9 1.0 - 10 4.3--1,220 J87.1 65.21,310NA11.8 236 40 73 30 110 1601,40063 29 6.5 10 - 24.4 7.0 - 300 65--NA NA NA NA NA NA NANA NA NA NA NA NA NA NA9,300 NE 3.0 - 100 34--22.7 22.3 18.3 27.7NA6.56 14.9 25 30 24 97 110 440 40 31 800 4 - 20.5 BRL - 50 16--<0.12 <0.120.31 0.7NA <0.13 <0.12 NA NA NA NA NA NA NA NA70 BRL - <0.25 0.03 - 0.52 0.121--NA NA NA NA NA NA NANA NA NA NA NA NA NA NA4,700 NE BRL - 150 23--NA NA NA NA NA NA NANA NA NA NA NA NA NA NA1,200 NE <0.1 - 0.8 0.42--<1.21 <1.16 <1.27 <1.29 NA <1.28 <1.18 NA NA NA NA NA NA NA NA1,200 NE BRL - 5.0 NE--NA NA NA NA NA NA NA110 330 82 430 680 1,000 130 90 1,200 NE 15 - 300 107--NA NA NA NA NA NA NANA NA NA NA NA NA NA NA70,000 NE 25 - 124 56--NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA-- -- -- -- 1.0NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA-- -- -- -- 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.3) EPA Toxic Characteristic Leaching Procedure (TCLP) hazardous waste threshold level, 2004Only compounds detected in at least one sample are shown.Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Laboratory analytical methods are shown in parentheses.Bold values indicate compounds detected above Industrial/Commercial use PSRGs (and above regional background concentrations for metals).Underlined values indicate total concentration exceeds 20 times the TCLP regulatory levelVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act .NA = Not Analyzed; NE = Not Established; ft bgs = feet below the ground surface; -- = Not Applicable; NR = Not ReportedBQL = Below Laboratory Quantitation Limits; BRL = Below Reporting Limit; mg/L = milligrams per literJ = Analyte detected at a level less than the RL and greater than or equal to the MDL; D = Constituent was analyzed using a second dilution.U = Constituent was not detected using a second dilution; B = Constituent was also detected in the control blank.Screening CriteriaIndustrial/ CommercialPSRGs1Site-Specific Background Metals in SoilGeraghty & MillerRegional Background Metals In Soil2TCLP Regulatory Threshold319970.5SedimentSED-4/DUPS&MEmg/kghttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP Tables10/4/2021Table 1 (Page 2 of 5)Hart & Hickman, PC
Table 1 (Page 3 of 5)Summary of Soil and Sediment Analytical DataAquAir II Brownfields PropertyCharlotte, North CarolinaH&H Job No. TKC-004Sampled BySample IDTypeDepth (ft bgs)Sample Date UnitsVOCs (8260)AcetoneBenzene2-Butanone (MEK)Carbon DisulfideCarbon TetrachlorideChlorobenzeneChloroform2-Chlorotoluene1,2-Dichlorobenzene1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-DichloroetheneDiisopropyl EtherEthylbenzeneHexachlorobutadiene4-Methyl-2-pentanoneMethylene ChlorideTetrachloroethene1,1,1,2-Tetrachloroethane1,1,2,2,-TetrachloroethaneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneXylenesSVOCs (8270)Benzoic AcidBis(2-Ethylhexyl)phthalateButylbenzylphthalate1,4-DichlorobenzeneDi-n-butylphthalateHexachlorobutadieneHexachloroethanePhenol1,2,4-TrichlorobenzeneRCRA Metals (6010/7470)ArsenicBariumCadmiumChromium (total)CopperLeadMercuryNickelSeleniumSilverVanadiumZincTCLP Metals (6010) {mg/L}CadmiumChromiumAAH-1 AAH-9 AAH-14 AAH-17 AAH-25AAH-31 AAH-33 AAH-34 AAH-38 AAH-47 AAH-49 AAH-51 APH-20Soil Soil Soil Soil SoilSoil Soil Soil Soil Soil Soil Soil Soil0.0-0.5 0.0-0.5 0.0-0.5 0.0-0.5 0.0-0.50.0-0.5 0.0-00.5 0.0-0.5 0.0-0.5 0.0-0.5 0.0-0.5 0.0-0.5 2.0-2.57/1/2003 7/1/2003 7/1/2003 7/1/2003 7/2/20037/2/2003 7/1/2013 7/1/2003 7/2/2003 7/2/2003 7/1/2003 7/2/2003 7/31/2003Range Range Meanmg/LNA NA NA NA NA NA NA NA NA NA NA NA<0.0056140,000---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.00565.4---- -- --NA NA NA NA NA NA NA NA NA NA NA NA<0.005640,000---- -- --NA NA NA NA NA NA NA NA NA NA NA NA<0.0056740---- -- --NA NA NA NA NA1.4NA63NA NA NA NA0.943.0 ---- -- --NA NA NA NA NA0.043NA <0.0057 NA NA NA NA<0.0056280 ---- -- --NA NA NA NA NA0.51NA0.260NA NA NA NA0.251.5 ---- -- --NA NA NA NA NA0.0088NA <0.0057 NA NA NA NA<0.00564,700 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.00562,000 ---- -- --NA NA NA NA NA0.16NA <0.0057 NA NA NA NA<0.005617 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.00562.2 ---- -- --NA NA NA NA NA0.28NA0.017NA NA NA NA0.39210 ---- -- --NA NA NA NA NA0.82NA <0.0057 NA NA NA NA0.11470 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA0.02964 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.00562,000 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.005627 ---- -- --NA NA NA NA NANANANANA NA NA NA<0.00565.6 ---- -- --NA NA NA NA NANANANANA NA NA NA<0.005630,000 ---- -- --NA NA NA NA NA0.43NA0.015NA NA NA NA 0.0057650 ---- -- --NA NA NA NA NA9.9NA4.1NA NA NA NA<0.005682 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.00569.3 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA0.642.8 ---- -- --NA NA NA NA NA0.044NA <0.0057 NA NA NA NA<0.00569,700 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.0056190 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.005655 ---- -- --NA NA NA NA NA0.99NA0.086NA NA NA NA<0.00567,600 ---- -- --NA NA NA NA NA0.013NA <0.0057 NA NA NA NA0.0191.3 ---- -- --NA NA NA NA NA11NA0.080NA NA NA NA5.54.0 ---- -- --NA NA NA NA NA <0.0054 NA <0.0057 NA NA NA NA<0.0056530 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA660,000 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA160 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA1,200 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA12 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA16,000 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA5.6 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA8.5 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA49,000 ---- -- --NA NA NA NA NANA NA NA NA NA NA NA NA55 ---- -- --NA NA NA NA1.1NA NA NA NA NA NA NA NA3 <1.0 - 1.0 1.0 - 18 4.8 --NA NA NA NA NANA NA NA NA NA NA NA NA47,000 31 - 86.5 50 - 1,000 356 --NA NA0.59 0.49 0.66<0.110.22 0.46 0.75 0.58 0.75 34NA200 <1 - 9 1.0 - 10 4.3 --110 110 71 34044018822.13442,30056 73 190NA6.5 10 - 24.4 7.0 - 300 65 --NA NA NA NA NANA NA NA NA NA NA NA NA9,300 NE 3.0 - 100 34 --NA NA NA NA NANA NA NA NA NA NA50NA800 4 - 20.5 BRL - 50 16 --NA NA NA NA NANA NA NA NA NA NA NA NA70 BRL - <0.25 0.03 - 0.52 0.121 --NA NA NA NA NANA NA NA NA NA NA NA NA4,700 NE BRL - 150 23 --NA NA NA NA NANA NA NA NA NA NA NA NA1,200 NE <0.1 - 0.8 0.42 --NA NA NA NA NANA NA NA NA NA NA NA NA1,200 NE BRL - 5.0 NE --660 450 480 89 86150 91 100 1,000 830 470 570NA1,200 NE 15 - 300 107 --NA NA NA NA NANA NA NA NA NA NA NA NA70,000 NE 25 - 124 56 --NA NA NA0.78NA NA NA NA0.12NA NA0.19NA-- -- -- -- 1.0NA NA NA0.31NA NA2.3NA0.07NA NANANA-- -- -- -- 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.3) EPA Toxic Characteristic Leaching Procedure (TCLP) hazardous waste threshold level, 2004Only compounds detected in at least one sample are shown.Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Laboratory analytical methods are shown in parentheses.Bold values indicate compounds detected above Industrial/Commercial use PSRGs (and above regional background concentrations for metals).Underlined values indicate total concentration exceeds 20 times the TCLP regulatory levelVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act .NA = Not Analyzed; NE = Not Established; ft bgs = feet below the ground surface; -- = Not Applicable; NR = Not ReportedBQL = Below Laboratory Quantitation Limits; BRL = Below Reporting Limit; mg/L = milligrams per literJ = Analyte detected at a level less than the RL and greater than or equal to the MDL; D = Constituent was analyzed using a second dilution.U = Constituent was not detected using a second dilution; B = Constituent was also detected in the control blank.Regional Background Metals In Soil2TCLP Regulatory Threshold3Industrial/ CommercialPSRGs1Site-Specific Background Metals in SoilScreening CriteriaS&MEhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP Tables10/4/2021Table 1 (Page 3 of 5)Hart & Hickman, PC
Table 1 (Page 4 of 5)Summary of Soil and Sediment Analytical DataAquAir II Brownfields PropertyCharlotte, North CarolinaH&H Job No. TKC-004Sampled BySample IDTypeDepth (ft bgs)Sample Date UnitsVOCs (8260)AcetoneBenzene2-Butanone (MEK)Carbon DisulfideCarbon TetrachlorideChlorobenzeneChloroform2-Chlorotoluene1,2-Dichlorobenzene1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-DichloroetheneDiisopropyl EtherEthylbenzeneHexachlorobutadiene4-Methyl-2-pentanoneMethylene ChlorideTetrachloroethene1,1,1,2-Tetrachloroethane1,1,2,2,-TetrachloroethaneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneXylenesSVOCs (8270)Benzoic AcidBis(2-Ethylhexyl)phthalateButylbenzylphthalate1,4-DichlorobenzeneDi-n-butylphthalateHexachlorobutadieneHexachloroethanePhenol1,2,4-TrichlorobenzeneRCRA Metals (6010/7470)ArsenicBariumCadmiumChromium (total)CopperLeadMercuryNickelSeleniumSilverVanadiumZincTCLP Metals (6010) {mg/L}CadmiumChromiumAPH-38 APH-58 APH-59Soil Soil Soil Soil Soil Soil Soil Soil Soil6.0-6.5 11.5-12.0 6.0-6.5 11.5-12.0 6.0-6.5 6.0-6.5 11.5-12.0 11.5-12.0 6.0-6.57/31/2003 7/31/2003 7/31/2003 7/31/2003 7/2/2003 7/30/2003 7/30/2003 7/31/2003 7/31/2003Range Range Meanmg/LNA NA NA NA <0.27 NA NA NA NA140,000---- -- --<0.0054 <0.0047 <0.0048 <0.0044 <0.27 <12 <1.2 <0.0048 <4.85.4---- -- --NA NA NA NA <0.27 NA NA NA NA40,000---- -- --NA NA NA NA <0.27 NA NA NA NA740---- -- --0.51 0.95 6.3 0.8915610361.51203.0 ---- -- --0.013 0.04 0.18 0.0481.4<12 <1.20.82 88 280 ---- -- --0.96 0.94 4.9 0.941117 1.7 2.3<4.81.5 ---- -- --<0.0054 <0.00470.011<0.0044 <0.27 <12 <1.2 <0.0048 <4.84,700 ---- -- --0.081 0.48<0.0048 <0.00441.5<12 <1.2 <0.0048 <4.82,000 ---- -- --0.0065<0.00470.24 0.0720.96<12 <1.20.031<4.817 ---- -- --<0.0054 <0.00474.8 0.057<0.27 <12 <1.20.13<4.82.2 ---- -- --0.015 0.01 0.22 0.0370.36<12 <1.20.061 4.8 210 ---- -- --0.16 0.12 0.15 0.03<0.27 <12 <1.20.02<4.8470 ---- -- --<0.00540.0059<0.0048 <0.0044 <0.27 <12 <1.2 <0.0048 <4.864 ---- -- --<0.0054 <0.0047 <0.0048 <0.0044 <0.27 <12 <1.20.035<4.82,000 ---- -- --<0.0054 <0.0047 <0.0048 <0.0044 <0.27 <12 <1.2 <0.0048 <4.827 ---- -- --NA NA NA NA<0.27NA NA NA NA5.6 ---- -- --NA NA NA NA<0.27NA NA NA NA30,000 ---- -- --0.57 0.32 0.8 69<12 <1.23 8 650 ---- -- --0.74 4.3 0.82 0.32<0.275203 1.62,70082 ---- -- --<0.0054 <0.0047 <0.0048 <0.0044 <0.27 <12 <1.2 <0.0048 <4.89.3 ---- -- --0.016 0.017 0.087<0.00440.35<12 <1.20.19<4.82.8 ---- -- --0.011 0.0093 0.590.015 3.1<12 <1.20.079 8.5 9,700 ---- -- --<0.0054 <0.0047 <0.0048 <0.0044 <0.27 <12 <1.2 <0.0048 <4.8190 ---- -- --0.0054<0.0047 <0.0048 <0.0044 <0.27 <12 <1.2 <0.0048 <4.855 ---- -- --0.041 0.052 0.24 0.363.6160 1.8 0.17 240 7,600 ---- -- --0.017 0.017 0.049 0.016<0.27 <12 <1.20.019<4.81.3 ---- -- --0.21 0.45 2.8 0.185.31601.8 14804.0 ---- -- --<0.0054 <0.00470.0110.005 0.11<12 <1.2 <0.004810 530 ---- -- --NA NA NA NA NA NA NA NA NA660,000 ---- -- --NA NA NA NA NA NA NA NA NA160 ---- -- --NA NA NA NA NA NA NA NA NA1,200 ---- -- --NA NA NA NA NA NA NA NA NA12 ---- -- --NA NA NA NA NA NA NA NA NA16,000 ---- -- --NA NA NA NA NA NA NA NA NA5.6 ---- -- --NA NA NA NA NA NA NA NA NA8.5 ---- -- --NA NA NA NA NA NA NA NA NA49,000 ---- -- --NA NA NA NA NA NA NA NA NA55 ---- -- --<0.52 NA NA NA NA NA NA NA NA3 <1.0 - 1.0 1.0 - 18 4.8 --NA NA NA NA NA NA NA NA NA47,000 31 - 86.5 50 - 1,000 356 --1.2NA3.4NA NA1.6NA NA NA200 <1 - 9 1.0 - 10 4.3 --54NA5.1NA NA16NA NA NA6.5 10 - 24.4 7.0 - 300 65 --NA NA NA NA NA NA NA NA NA9,300 NE 3.0 - 100 34 --NA NA NA NA NA NA NA NA NA800 4 - 20.5 BRL - 50 16 --NA NA NA NA NA NA NA NA NA70 BRL - <0.25 0.03 - 0.52 0.121 --NA NA NA NA NA NA NA NA NA4,700 NE BRL - 150 23 --NA NA NA NA NA NA NA NA NA1,200 NE <0.1 - 0.8 0.42 --NA NA NA NA NA NA NA NA NA1,200 NE BRL - 5.0 NE --41NA160NA NA85NA NA NA1,200 NE 15 - 300 107 --NA NA NA NA NA NA NA NA NA70,000 NE 25 - 124 56 --NA NA NA NA NA NA NA NA NA-- -- -- -- 1.0NA NA NA NA NA NA NA NA NA-- -- -- -- 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.3) EPA Toxic Characteristic Leaching Procedure (TCLP) hazardous waste threshold level, 2004Only compounds detected in at least one sample are shown.Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Laboratory analytical methods are shown in parentheses.Bold values indicate compounds detected above Industrial/Commercial use PSRGs (and above regional background concentrations for metals).Underlined values indicate total concentration exceeds 20 times the TCLP regulatory levelVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act .NA = Not Analyzed; NE = Not Established; ft bgs = feet below the ground surface; -- = Not Applicable; NR = Not ReportedBQL = Below Laboratory Quantitation Limits; BRL = Below Reporting Limit; mg/L = milligrams per literJ = Analyte detected at a level less than the RL and greater than or equal to the MDL; D = Constituent was analyzed using a second dilution.U = Constituent was not detected using a second dilution; B = Constituent was also detected in the control blank.Regional Background Metals In Soil2mg/kgIndustrial/ CommercialPSRGs1Site-Specific Background Metals in SoilTCLP Regulatory Threshold3APH-24 APH-32S&MEScreening CriteriaAPH-42https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP Tables10/4/2021Table 1 (Page 4 of 5)Hart & Hickman, PC
Table 1 (Page 5 of 5)Summary of Soil and Sediment Analytical DataAquAir II Brownfields PropertyCharlotte, North CarolinaH&H Job No. TKC-004Sampled BySample IDTypeDepth (ft bgs)Sample Date UnitsVOCs (8260)AcetoneBenzene2-Butanone (MEK)Carbon DisulfideCarbon TetrachlorideChlorobenzeneChloroform2-Chlorotoluene1,2-Dichlorobenzene1,1-Dichloroethane1,2-Dichloroethane1,1-Dichloroethenecis-1,2-Dichloroethenetrans-1,2-DichloroetheneDiisopropyl EtherEthylbenzeneHexachlorobutadiene4-Methyl-2-pentanoneMethylene ChlorideTetrachloroethene1,1,1,2-Tetrachloroethane1,1,2,2,-TetrachloroethaneToluene1,2,3-Trichlorobenzene1,2,4-Trichlorobenzene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroetheneXylenesSVOCs (8270)Benzoic AcidBis(2-Ethylhexyl)phthalateButylbenzylphthalate1,4-DichlorobenzeneDi-n-butylphthalateHexachlorobutadieneHexachloroethanePhenol1,2,4-TrichlorobenzeneRCRA Metals (6010/7470)ArsenicBariumCadmiumChromium (total)CopperLeadMercuryNickelSeleniumSilverVanadiumZincTCLP Metals (6010) {mg/L}CadmiumChromiumSB-01 SB-02 SB-03 SB-04 SB-05 SB-06 SB-07 SB-08 SB-09 SB-10 SB-11 SB-12 SB-13 SB-14 SB-15 SB-16 SB-17Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.5 0-0.512/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015 12/8/2015Range Range Meanmg/L<0.0875 <0.0908 <0.0914 <0.0866<0.108 <0.109 <0.112 <0.0863 <0.109 <0.101 <0.173 <0.1900.205<0.116 <0.186 <0.183 <0.117140,000---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00595.4---- -- --<0.0875 <0.0908 <0.0914 <0.0866<0.108 <0.109 <0.112 <0.0863 <0.109 <0.101 <0.173 <0.190 <0.0157 <0.116 <0.186 <0.183 <0.11740,000---- -- --NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA740---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00593.0 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.0059280 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00591.5 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00594,700 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00592,000 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.005917 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00592.2 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.0059210 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.0059470 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00594,700 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00592,000 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.005927 ---- -- --NA NA NA NANA NA NA NA NA NA NA NA NA NA NA NA NA5.6 ---- -- --<0.0437 <0.0454 <0.0457 <0.0433<0.0539 <0.0547 <0.0056 <0.0432 <0.0543 <0.0503 <0.0866 <0.0951 <0.0785 <0.0582 <0.0930 <0.0916 <0.058630,000 ---- -- --<0.0175 <0.0182 <0.01830.101<0.0215 <0.0219 <0.0224 <0.0173 <0.0217 <0.0201 <0.0347 <0.03800.0344 0.0334 0.0403<0.0367 <0.0234650 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043 <0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.00870.0107<0.0079 <0.0058 <0.0093 <0.0092 <0.005982 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00599.3 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00592.8 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00599,700 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.0059190 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.005955 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00597,600 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00591.3 ---- -- --<0.0044 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.00594.0 ---- -- --<0.0087 <0.0045 <0.0046 <0.0043<0.0054 <0.0055 <0.0056 <0.0043 <0.0054 <0.005 <0.0087 <0.0095 <0.0079 <0.0058 <0.0093 <0.0092 <0.0059530 ---- -- --<2.020 <2.040 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.447660,000 ---- -- --<0.405 <0.408 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.447160 ---- -- --<0.405 <0.408 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.4471,200 ---- -- --<0.405 <0.408 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.44712 ---- -- --<0.405 <0.408 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.44716,000 ---- -- --NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA5.6 ---- -- --<0.405 <0.408 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.4478.5 ---- -- --<0.405 <0.408 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.44749,000 ---- -- --<0.405 <0.408 <0.421 <0.398 <0.462 <0.404 <0.455 <0.409 <0.445 <0.432 <0.397 <0.413 <0.413 <0.351 <0.455 <0.422 <0.447190 ---- -- --<1.11.3 1.1<0.960 <1.1 <1.0 <1.00.9<0.940 <3.71.1<0.89 <0.81 <3.0 <0.714.1<0.743.0 <1.0 - 1.0 1.0 - 18 4.8 --102 76.6 88 80.1 57.1 36.5 57.7 63.1 59.0 98.6 50.2 55.4 77.3 61.6 83.2 179 10347,000 31 - 86.5 50 - 1,000 356 --<0.110 <0.110 <0.100 <0.096 <0.110 <0.1005.9<0.090 <0.0941.9<0.0862.4<0.081 <0.30 <0.0071 <0.39 <0.074200 <1 - 9 1.0 - 10 4.3 --64.5 85.3 24.2 91.8 18.4 49.6 158 12.4 3.7 182 40.0 90.1 41.6<1.59.6 52.6 10.16.5 10 - 24.4 7.0 - 300 65 --14.6 10 8 13.3 8.5 7 34.7 9.3 11.6 26.9 6.8 15.6 10 9.7 9.5 36 99,300 NE 3.0 - 100 34 --19 25.3 19 20 8.5 16 38.7 11.9 3.1 26.1 22.7 25.4 25<1.56.9 5.8 3.6800 4 - 20.5 BRL - 50 16 --0.029 0.036 0.033 0.045 0.069 0.044 0.2 0.044 0.013 0.049 0.023 0.049 0.016<0.00390.083 0.0097 0.0669.7 BRL - <0.25 0.03 - 0.52 0.121 --11.5 4.8 6.5 4 4.1 1.7 10.7 3.2 1.3 11.4 2.8 5 4.5 2.7 2.9 30.9 4.14,700 NE BRL - 150 23 --2 2.6 1.7 2.1 3.0 1.9 2.3 1.3 1.4<3.71.3 1.3 1.2<3.02.5<3.92.01,200 NE <0.1 - 0.8 0.42 --0.73<0.550 <0.510 <0.480 <0.570 <0.5003.6 0.51 0.58<1.8 <0.430 <0.4500.53<1.50.38<1.90.711,200 NE BRL - 5.0 NE --183 256 124 359 128 194 169 105 76.2 322 127 215 189 35.2 148 77.3 87.41,200 NE 15 - 300 107 --30.7 30.4 36.5 19.5 23.4 13.5 44.4 27.1 53 64.1 15.4 83.3 23.8 23.4 18.3 22.3 28.170,000 NE 25 - 124 56 --NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA-- -- -- -- 1.0NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA-- -- -- -- 5.0Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) (June 2021).2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.3) EPA Toxic Characteristic Leaching Procedure (TCLP) hazardous waste threshold level, 2004Only compounds detected in at least one sample are shown.Soil concentrations are reported in milligrams per kilogram (mg/kg) unless otherwise noted.Laboratory analytical methods are shown in parentheses.Bold values indicate compounds detected above Industrial/Commercial use PSRGs (and above regional background concentrations for metals).Underlined values indicate total concentration exceeds 20 times the TCLP regulatory levelVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; RCRA = Resource Conservation and Recovery Act .NA = Not Analyzed; NE = Not Established; ft bgs = feet below the ground surface; -- = Not Applicable; NR = Not ReportedBQL = Below Laboratory Quantitation Limits; BRL = Below Reporting Limit; mg/L = milligrams per literJ = Analyte detected at a level less than the RL and greater than or equal to the MDL; D = Constituent was analyzed using a second dilution.U = Constituent was not detected using a second dilution; B = Constituent was also detected in the control blank.mg/kgTerraconScreening CriteriaRegional Background Metals In Soil2TCLP Regulatory Threshold3Industrial/ CommercialPSRGs1Site-Specific Background Metals in Soilhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP Tables10/4/2021Table 1 (Page 5 of 5)Hart & Hickman, PC
Table 2 (Page 1 of 2)Summary of Groundwater Analytical DataAquAir II Brownfields PropertyCharlotte, North CarolinaH&H Job No. TKC-004Sampled ByS&MESample ID AMW-101 AMW-106* AMW-403 AMW-405*AMW-410*AMW-411* AMW-503 AMW-612* DW-1* DW-2 DW-3* DW-4Most Recent Sample Date 7/27/2011 3/3/2005 9/21/2006 3/4/20053/4/2005 7/28/2011 9/21/2006 7/28/20117/28/2011 9/21/2006 6/4/2004 9/21/2006Well Depth (ft bgs) 36 28 73 67 68 90 150 154 40 27 34 51UnitsVOCs (8260)Benzene0.001BRL<0.0010BRL BRL BRL <0.0010 BRL BRL<0.010 BRL<0.00100.001 0.069Carbon Tetrachloride3.22BRL0.011BRL BRL BRL <0.0010 BRL BRL0.68BRL <0.00100.0003 0.018Chloroform2.96BRL0.095BRL BRL BRL0.0028BRL BRL0.4BRL <0.00100.07 0.0361,1-Dichloroethane0.0938BRL0.0013BRL BRL BRL <0.0010 BRL BRL <0.010 BRL <0.00100.006 0.331,2-Dichloroethane0.0628BRL0.0043BRL BRL BRL <0.0010 BRL BRL0.017BRL <0.00100.0004 0.0981,1-Dichloroethene0.366BRL0.011BRL BRL BRL <0.0010 BRL BRL0.11BRL <0.00100.35 0.16cis-1,2-Dichloroethene0.17BRL0.024BRL BRL BRL <0.0010 BRL BRL0.13BRL <0.00100.07 NEMethylene Chloride0.0324BRL0.023BRL BRL BRL <0.0020 BRL BRL <0.020 BRL <0.00200.005 4.01,1,1,2-Tetrahloroethane0.0012NA NA NA NA NA NA NA NA NA NA NA0.001 0.016Tetrachloroethene3.86BRL0.075BRL BRL BRL0.0034BRL BRL0.85BRL <0.00100.0007 0.0481,1,1-Trichloroethane0.216BRL0.0012BRL BRL BRL <0.0010 BRL BRL <0.010 BRL <0.00100.2 6.21,1,2-Trichloroethane0.0086BRL <0.0010 BRL BRL BRL <0.0010 BRL BRL <0.010 BRL <0.00100.006 0.0052Trichloroethene2.48BRL0.085BRL BRL BRL0.0031BRL BRL0.71BRL <0.00100.003 0.0044SVOCs (8270)BRLNANANANANANANANANANANA----RCRA Metals (3010/3030c/245.1)Arsenic<0.0050 BRL NA BRL0.0059NA NA BRL BRL NA0.011NA0.01--Chromium0.0475NA NA NA NA NA NA NA NA NA NA NA0.01--Chromium III 0.0475NA NA NA NA NA NA NA NA NA NA NANE--Chromium VI<0.000050 NA NA NA NA NA NA NA NA NA NA NANE--Manganese0.99NA NA NA NA NA NA NA NA NA NA NA0.05--Notes:1) North Carolina Department of Environmental Quality (DEQ) 15A North Carolina Administrative Code 02L.0202 Groundwater Quality Standard (April 2013).2) DEQ Division of Waste Management (DWM) Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) (June 2021)Only those compounds detected above the 2L Standard or Non-Residential GWSL in at least one sample shown above (Chromium VI is shown since it was speciated.)Bold indicates an exceedance in the NCAC 2L Groundwater StandardUnderlined indicates an exceedance in the DEQ DWM Non-Residential GWSLLaboratoy analytical method show in parentheses. mg/L = milligrams per liter; ft bgs = feet below ground surfaceVOCs = volatile organic compounds; SVOCs = Semi-VOCs; RCRA = Resource Conservation and Recovery Act; BRL = below laboratory reporting limitsNE = Not Established; NA= Not Analyzed, -- = not applicable* = Lab report not available to specify reporting limitmg/LShield Engineering, INC.NCAC 2L Groundwater Standard(1)DWM Vapor Intrusion Non-Residential GWSLs(2)https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP Tables9/30/2021Table 2 (Page 1 of 2)Hart & Hickman, PC
Table 2 (Page 2 of 2)Summary of Groundwater Analytical DataAquAir II Brownfields PropertyCharlotte, North CarolinaH&H Job No. TKC-004Sampled ByDelta Environmental ConsultantsSample ID MW-1 MW-2 MW-3 MW-4* MW-5* MW-6 MW-7* MW-8* MW-9 MW-10 RW-2 RW-3Most Recent Sample Date 7/28/2011 7/28/2011 7/28/2011 3/2/20053/2/2005 7/28/2011 3/3/1992 3/2/20057/28/2011 7/28/2011 9/22/2006 9/22/2006Well Depth (ft bgs) 27272522272215222022105150UnitsVOCs (8260)Benzene<0.0010 <0.0010 <0.0010 BRL BRL <0.0010 NA BRL <0.0010 <0.0010 <0.100 <0.0100.001 0.069Carbon Tetrachloride0.07250.0025<0.0010 BRL BRL <0.0010 <0.010 BRL <0.0010 <0.00108.82.00.0003 0.018Chloroform0.2460.0081 0.0036BRL BRL <0.0010 <0.005 BRL0.0018<0.00102.21.70.07 0.0361,1-Dichloroethane 0.0035<0.0010 <0.0010 BRL BRL <0.0010 <0.005 BRL <0.0010 <0.0010 <0.100 <0.0100.006 0.331,2-Dichloroethane0.0129<0.0010 <0.0010 BRL BRL <0.0010 NA BRL <0.0010 <0.0010 <0.100 <0.0100.0004 0.0981,1-Dichloroethene<0.00100.0128 0.001BRL BRL <0.0010 <0.005 BRL <0.0010 <0.0010 <0.1000.088 0.35 0.16cis-1,2-Dichloroethene 0.0045<0.0010 <0.0010 BRL BRL <0.0010 BRL BRL <0.0010 <0.0010 <0.1000.0760.07 NEMethylene Chloride<0.0020 <0.0020 <0.0020 BRL BRL <0.00200.008 BBRL <0.0020 <0.00200.25 0.3200.005 4.01,1,1,2-Tetrahloroethane<0.0010 <0.0010 <0.0010 NA NA <0.0010 NA NA <0.0010 <0.0010 NA NA0.001 0.016Tetrachloroethene0.06390.1640.0031BRL BRL <0.0010 <0.005 BRL0.0019<0.00101.11.00.0007 0.0481,1,1-Trichloroethane 0.002<0.0010 <0.0010 BRL BRL <0.0010 <0.005 BRL <0.0010 <0.0010 <0.1000.025 0.2 6.21,1,2-Trichloroethane 0.0037<0.0010 <0.001 BRL BRL <0.0010 <0.005 BRL <0.0010 <0.0010 <0.100 <0.0100.006 0.0052Trichloroethene0.02310.02480.0018BRL BRL <0.0010 <0.005 BRL0.0019<0.00100.530.5500.003 0.0044SVOCs (8270)NA BRL NA NA NA BRL NA NA NA BRL NA NA----RCRA Metals (3010/3030c/245.1)ArsenicNA0.0067NA BRL BRL0.0054NA BRL NA0.0052NA NA0.01--ChromiumNA0.0175NA NA NA <0.0050 NA NA NA <0.0050 NA NA0.01--Chromium IIINA0.0175NA NA NA <0.0050 NA NA NA <0.0050 NA NANE--Chromium VINA <0.000050 NA NA NA <0.00005 NA NA NA <0.000050 NA NANE--ManganeseNA0.785NA NA NA0.778NA NA NA0.0171NA NA0.05--Notes:1) North Carolina Department of Environmental Quality (DEQ) 15A North Carolina Administrative Code 02L.0202 Groundwater Quality Standard (April 2013).2) DEQ Division of Waste Management (DWM) Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) (June 2021)Only those compounds detected above the 2L Standard or Non-Residential GWSL in at least one sample shown above (Chromium VI is shown since it was speciated.)Bold indicates an exceedance in the NCAC 2L Groundwater StandardUnderlined indicates an exceedance in the DEQ DWM Non-Residential GWSLMethod number follows parameter in parenthesismg/L = milligrams per liter; ft bgs = feet below ground surfaceVOCs = volatile organic compounds; SVOCs = Semi-VOCs; RCRA = Resource Conservation and Recovery Act; BRL = below laboratory reporting limitsNE = Not Established; NA= Not Analyzed, -- = not applicable* = Lab report not available to specify reporting limitNCAC 2L Groundwater Standard(1)DWM Vapor Intrusion Non-Residential GWSLs(2)mg/LShield Engineering, INC.Shield Engineering, INC.https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP Tables9/30/2021Table 2 (Page 2 of 2)Hart & Hickman, PC
Table 3 (Page 1 of 1)Summary of Soil Gas Analytical Data AquAir II Brownfields Property Charlotte, North CarolinaHart & Hickman Project No. TKC-004Carbon TetrachlorideChlorobenzeneChloroform1,2-Dichloroethane1,1-DichloroethyleneEthylbenzeneHexachlorobutadiene1,1,2,2-TetrachloroethaneTetrachloroethyleneToluene1,1,1-Trichloroethane1,1,2-TrichloroethaneTrichloroethylenem,p-XyleneSSGS-1 10/28/11 TO-15H&H160 50 47<2.0 <2.07.8<5.3 <3.41,900 29 12<2.782 20SSGS-2 10/28/11 TO-15H&H300,0007311,000 1,200 27,00022<211,600 700,000150 8,900780 110,00061SSGS-3 10/28/11 TO-15H&H11<0.469.8<0.40 <0.407.4 0.30<0.6968 30 1.4<0.551.8 22SSGS-4 10/28/11 TO-15H&H13,000,000 100,000 700,000 67,000 120,000 42,000<43,00024,000 16,000,00068,0001,400,000<22,0002,000,000 34,000SSGS-5 10/28/11 TO-15H&H56,0007.58,1002.8 47<8.73,600<1416,0002.4 350<11570<17SSGS-6 10/28/11 TO-15H&H48 0.49 4.6 0.55 0.63 6.9 1.4<0.6963 26 4.8 0.25 8.6 18SSGS-7 10/28/11 TO-15H&H14<0.469.6 0.28<0.4014 0.79<0.6914 56 2.2<0.551.6 41SV-01 12/15/15 TO-15Terracon<30 <22 <23 <19 <18 <20 <200 <32 <3238<26 <26 <25 <20SV-02 12/15/15 TO-15Terracon<30 <22 <23 <19 <18 <20 <200 <21 <20270<16 <16 <16 <13SV-03 12/15/15 TO-15Terracon<30 <22 <23 <19 <18 <20 <200 <32 <32100<26 <26 <25 <20SV-04 12/15/15 TO-15Terracon<7.7 <5.6 <6.0 <5.0 <4.815<52 <8.4 <8.3130<6.7 <6.7 <6.667200 4,400 53 47 18,000 490 56 21 3,500 440,000 440,000 18 180 8,800Notes:1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management (DWM) Non-Residential Sub-slab and Exterior Soil Gas Screening Levels (SGSLs) (June 2021)2) Only those analytes detected in at least one sample are shown in this table3) Bold indicates compound exceeds Non-Residential SGSL NE = Not Established, µg/m3 = micrograms per cubic meter Only compounds detected above the Non-Residential SGSL in at least one sample shownTCR = target cancer riskTHQ = target hazard quotientSample IDSampling Date µg/m3Non-Residential SGSLs(1)(TCR = 1 x 10-6 and THQ = 0.2)Analytical MethodConsultanthttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/EMP/EMP TablesEMP Tables9/30/2021Table 3 (Page 1 of 1)Hart & Hickman, PC
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
CR
CR
REVISION NO. 0
JOB NO. TKC-004
DATE: 10-4-21
FIGURE NO. 5
AQUAIR II BROWNFIELD PROPERTY
13300 SAM NEELY ROAD
CHARLOTTE, NORTH CAROLINA
SITE PLAN WITH SOIL AND SEDIMENT
SAMPLE RESULTS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
LEGEND
LIMITS OF GROUNDWATER
CONTAMINATION
RAILROAD TRACKS
PROPOSED BUILDING
FOOTPRINT
AREA OF POSSIBLE SOIL
CONTAMINATION
SOIL/ SEDIMENT SAMPLE LOCATION
CO-LOCATED SOIL AND SOIL GAS SAMPLE
LOCATION
SOIL SAMPLE CONTAINS CONCENTRATIONS
OF VOLATILE ORGANIC COMPOUNDS OR
METALS ABOVE THE DEPARTMENT OF
ENVIRONMENTAL QUALITY (DEQ) INACTIVE
HAZARDOUS WASTE SITES BRANCH (IHSB)
JUNE 2021 INDUSTRIAL/COMMERCIAL
PRELIMINARY SOIL REMEDIATION GOALS
PSRGs (AND REGIONAL BACKGROUND FOR
METALS).
SOIL SAMPLE CONTAINS CONCENTRATIONS
OF TOTAL METALS AND/OR CHLORINATED
VOLATILE ORGANIC COMPOUNDS WHICH
EXCEED 20 TIMES THE TOXICITY
CHARACTERISTIC LEACHING PROCEDURE
REGULATORY LEVEL AND INDUSTRIAL /
COMMERCIAL PSRGs.
SOIL SAMPLE DID NOT CONTAIN
CONCENTRATIONS OF CONTAMINANTS OF
INTEREST ABOVE THE INDUSTRIAL /
COMMERCIAL PSRGs.
SOURCES
1.SITE PLAN PROVIDED BY BURTON ENGINEERING.
2.BASE MAP OF THE HISTORICAL FEATURES FROM
S&ME, REMEDIAL INVESTIGATION REPORT,
OCTOBER 2011.
3.AERIAL PHOTOGRAPH FROM MECKLENBURG
COUNTY GIS.
SB-17
SB-11
SB-13
SB-16
SB-15
SED-4
SS-5
SS-8
AAH-34
APH-42S-4
SS-7
SS-4
AAH-31
SS-6 APH-59
APH-58
SS-03
APH-24 S-6
SUMP-1
SUMP-2
APH-32
SED-3
SED-5
S-3S-2S-1
SB-07
SB-10
SB-08
SB-05
SB-03
SB-02
SB-01
SB-04
SB-06
SB-12
SB-09
SB-14 AAH-38
AAH-1
AAH-09
AAH-14
AAH-17 AAH-25
AAH-33
AAH-49
AAH-47
AAH-51
APH-20
SED-1
SED-2
SED-7
SED-6
SS-03
SS-4
FORMER
PRODUCTION
BUILDING
FORMER
LAB
BUILDING
SB-13
APH-38
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
CR
CR
REVISION NO. 0
JOB NO. TKC-004
DATE: 10-4-21
FIGURE NO. 6
AQUAIR II BROWNFIELD PROPERTY
13300 SAM NEELY ROAD
CHARLOTTE, NORTH CAROLINA
SITE PLAN WITH GROUNDWATER SAMPLE
RESULTS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
LEGEND
LIMITS OF GROUNDWATER CONTAMINATION
RAILROAD TRACKS
PROPOSED BUILDING
FOOTPRINT
AREA OF POSSIBLE SOIL
CONTAMINATION
SHALLOW GROUNDWATER MONITORING
WELL LOCATION
DEEP GROUNDWATER MONITORING WELL
LOCATION
GROUNDWATER RECOVERY WELL
LOCATION
GROUNDWATER SAMPLE CONTAINS
CONCENTRATIONS OF VOLATILE ORGANIC
COMPOUNDS (VOCs) AND/OR METALS THAT
EXCEED THE NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL
QUALITY (DEQ) 15A NORTH CAROLINA
ADMINSTRATIVE CODE (NCAC) 02L:0202
(2L STANDARDS) GROUNDWATER QUALITY
STANDARD (APRIL 2013).
GROUNDWATER SAMPLE CONTAINS
CONCENTRATIONS OF VOCs OR METALS
THAT EXCEED THE DEQ 2L STANDARDS
AND ARE ABOVE THE DEQ DIVISION OF
WASTE MANAGEMENT (DWM)
NON-RESIDENTIAL VAPOR INTRUSION
GROUNDWATER SCREENING LEVELS
(GWSL) (JUNE 2021).
GROUNDWATER SAMPLE DID NOT CONTAIN
CONCENTRATIONS OF CONTAMINANTS OF
INTEREST ABOVE 2L STANDARD OR
NON-RESIDENTIAL GWSLs.
SOURCES
1.SITE PLAN PROVIDED BY BURTON ENGINEERING.
2.BASE MAP OF THE HISTORICAL FEATURES FROM
S&ME, REMEDIAL INVESTIGATION REPORT,
OCTOBER 2011.
3.AERIAL PHOTOGRAPH FROM MECKLENBURG
COUNTY GIS.
AMW-612
AMW-405
AMW-410
MW-9
DW-2
AMW-503AMW-403
DW-3 MW-6
MW-7
MW-5
MW-10
DW-4
MW-4
AMW-411
RW-3
MW-3
MW-2
AMW-101
MW-1
RW-2
MW-8 DW-1
AMW-106
DW-3
MW-1
FORMER
PRODUCTION
BUILDING
FORMER
LAB
BUILDING
MW-9
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
L
CR
CR
SSGS-2
SSGS-5
SSGS-4
SSGS-1
SSGS-3
SV-03
SV-02
SV-01
SV-04
SSGS-6
SSGS-7
REVISION NO. 0
JOB NO. TKC-004
DATE: 10-4-21
FIGURE NO. 7
AQUAIR II BROWNFIELD PROPERTY
13300 SAM NEELY ROAD
CHARLOTTE, NORTH CAROLINA
SITE PLAN WITH SOIL GAS SAMPLE RESULTS
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
LEGEND
LIMITS OF GROUNDWATER CONTAMINATION
RAILROAD TRACKS
PROPOSED BUILDING
FOOTPRINT
AREA OF POSSIBLE SOIL
CONTAMINATION
SUB-SURFACE SOIL-GAS SAMPLE LOCATION
CO-LOCATED SOIL AND SOIL GAS SAMPLE
LOCATION
SOIL GAS SAMPLE CONTAINS
CONCENTRATIONS OF VOLATILE ORGANIC
COMPOUNDS (VOCs) ABOVE THE NORTH
CAROLINA DEPARTMENT OF
ENVIRONMENTAL QUALITY (DEQ) DIVISION
OF WASTE MANAGEMENT (DWM)
NON-RESIDENTIAL SUB-SLAB AND
EXTERIOR SOIL GAS SCREENING LEVELS
(SGSLs) (JUNE 2021)
SOIL GAS SAMPLE DID NOT CONTAIN
CONCENTRATIONS OF VOCs ABOVE
NON-RESIDENTIAL SGSLs.
SOURCES
1.SITE PLAN PROVIDE BY BURTON ENGINEERING.
2.BASE MAP OF THE HISTORICAL FEATURES FROM
S&ME, REMEDIAL INVESTIGATION REPORT,
OCTOBER 2011.
3.AERIAL PHOTOGRAPH FROM MECKLENBURG
COUNTY GIS.
SSGS-4
FORMER
PRODUCTION
BUILDING
FORMER
LAB
BUILDING
SSGS-7

Appendix C As-Built Drawings – VM-1, VM-2, VM-2A, VM-3, and VM-4

H&H NO. TKC-008
VAPOR MITIGATION PLAN
PREPARED BY:
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
VAPOR INTRUSION
MITIGATION
SPECIFICATIONSHD CHARLOTTE BCR FDC13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINADEVELOPER:
THE KEITH
CORPORATION
VM-1
PROFESSIONAL
APPROVAL
AS-BUILT
APRIL 27, 2023
VAPOR INTRUSION MITIGATION SYSTEM (VIMS) SPECIFICATIONS
1.THIS VAPOR INTRUSION MITIGATION PLAN WAS INTENDED TO BE USED FOR DIRECTION OF VIMS COMPONENT INSTALLATION ONLY AND WAS NOT INTENDED TO GUIDE CONSTRUCTION OF STRUCTURAL
COMPONENTS NOT RELATED TO THE VIMS. CONSTRUCTION CONTRACTOR VERIFIED CONSISTENCY OF VIMS DETAILS WITH APPLICABLE STRUCTURAL, ARCHITECTURAL, MECHANICAL, AND PLUMBING PLANS AND
RESOLVE INCONSISTENCIES WITH THE DESIGN ENGINEER PRIOR TO VIMS INSTALLATION. THE VIMS WAS INSTALLED IN ACCORDANCE WITH APPLICABLE BUILDING CODES.
2.CONSTRUCTION CONTRACTORS AND SUB-CONTRACTORS USED "LOW OR NO VOC" PRODUCTS AND MATERIALS, WHEN POSSIBLE. NO PRODUCTS CONTAINING TETRACHLOROETHENE OR TRICHLOROETHENE WERE
PERMITTED.
3.VIMS VAPOR LINER IS VAPORBLOCK PLUS 20 VAPOR BARRIER MANUFACTURED BY RAVEN INDUSTRIES, INC. THE VAPOR LINER WAS INSTALLED AS SPECIFIED HEREIN AND PER MANUFACTURER INSTALLATION
INSTRUCTIONS TO CREATE A CONTINUOUS LINER BELOW GROUND FLOOR SLABS. A BASE COURSE CONSISTING OF CLEAN #57 WAS INSTALLED BENEATH THE VIMS VAPOR LINER. IN AREAS AROUND THE SUB-SLAB
PIPING, THE BASE COURSE LAYER IS THICK ENOUGH TO COVER THE SUB-SLAB PIPING WITH A MINIMUM 1-INCH LAYER BELOW THE PIPING. IN AREAS WITHOUT PIPING, THE BASE COURSE IS A MINIMUM OF 4-INCHES
THICK.
4.ALL PENETRATIONS WERE SEALED ACCORDING TO VAPOR LINER MANUFACTURER INSTALLATION INSTRUCTIONS AS FOUND IN THE MANUFACTURER INSTALLATION GUIDELINES. SMALL PUNCTURE HOLES WERE
SEALED WITH THE VAPORSEAL™TAPE, BUTYL SEAL DOUBLE SIDED TAPE, POUR-N-SEAL™AND LARGER HOLES, TEARS, OR DAMAGE WERE REPAIRED USING A PATCH THAT OVERLAPPED THE DAMAGED AREA AND
THEN WAS TAPED ALONG THE SEAMS. IN AREAS WHERE UTILITY PENETRATIONS (I.E. PIPING, DUCTS, ETC) WERE PRESENT AND THE USE OF TAPING WAS NOT PRACTICAL OR DEEMED AS "INEFFECTIVE" BY THE
DESIGN ENGINEER, POUR-N-SEAL WAS POURED INTO FORM TO PATCH THE PENETRATION BANK WITH AN AIRTIGHT SEAL. LOCATIONS WHERE POUR-N-SEAL WAS USED IS SHOWN ON VM-3.
5.CONSTRUCTION CONTRACTORS AND SUB-CONTRACTORS AVOIDED THE USE OF TEMPORARY FORM BOARDS THAT PENETRATED THE VAPOR LINER WHERE POSSIBLE. IF TEMPORARY FORM BOARDS WERE USED,
THE SIZE AND NUMBER OF PENETRATIONS THROUGH THE VAPOR LINER WAS LIMITED AND SMALL DIAMETER STAKES WERE USED. IN ALL CASES, AS FORM BOARDS WERE REMOVED, THE CONTRACTOR OR
SUB-CONTRACTORS SEALED ALL PENETRATIONS IN ACCORDANCE WITH VAPOR LINER MANUFACTURER INSTALLATION INSTRUCTIONS.
6.VIMS BELOW AND ABOVE GRADE PIPING IS SLOPED A MINIMUM OF 18 UNIT VERTICAL IN 12 UNITS HORIZONTAL (1% SLOPE) TO GRAVITY DRAIN. SOLID SECTIONS OF HORIZONTAL COLLECTION PIPE WERE SUPPORTED
TO PREVENT PIPE SAG OR LOW POINT AND MAINTAIN 1% SLOPE TOWARD SLOTTED SECTIONS TO DRAIN CONDENSATION. SUB-SLAB COLLECTION PIPING INCLUDED THREADED FLUSH JOINT OR GLUE JOINT 3" SCH 40
PVC PIPE WITH 0.020" TO 0.060" SLOT WIDTH AND 1
8" SLOT SPACING.
7.3" SCH 40 PVC RISER DUCT PIPING IN THE GUARDHOUSE AND 6" SCH 40 PVC RISER DUCT PIPING IN THE WAREHOUSE WAS INSTALLED TO CONNECT EACH SLAB PENETRATION LOCATIONS TO A ROOFTOP EXHAUST
DISCHARGE POINT WITH A AURA PVC PIPE CAP VENTILATOR (SEE DETAIL #15 ON VM-2A). ABOVE-SLAB RISER DUCT PIPES BETWEEN THE SLAB PENETRATION AND THE ROOFTOP EXHAUST DISCHARGE WERE
INSTALLED PER APPLICABLE NORTH CAROLINA PLUMBING AND BUILDING CODES AND AS SPECIFIED IN THE CONSTRUCTION DOCUMENTS AND DRAWINGS.
8.RISER DUCT PIPING EXTENDS IN A VERTICAL ORIENTATION THROUGH THE BUILDING ROOF AND TERMINATES A MINIMUM OF 2 FT ABOVE THE BUILDING ROOF LINE. AN EMPIRE MODEL STAINLESS STEEL TURBINE
VENTILATOR WAS INSTALLED ON THE EXHAUST DISCHARGE END OF EACH RISER DUCT PIPE. AN ADAPTOR COUPLING WAS INSTALLED AT THE DISCHARGE END OF THE 6" RISER DUCT PIPE (3" IN THE GUARDHOUSE)
AND THE VENTILATOR WAS SECURED TO THE PVC RISER IN A VERTICAL ORIENTATION. EXHAUST DISCHARGE LOCATIONS ARE A MINIMUM OF 10 FT FROM ANY OPERABLE OPENING OR AIR INTAKE INTO THE
BUILDING. AN ELECTRICAL JUNCTION BOX (120V, 60Hz AC REQUIRED) WAS INSTALLED NEAR THE FAN LOCATION ON THE ROOFTOP FOR CONVERSION TO ELECTRIC FANS, IF REQUIRED. ALL WIRING AND ELECTRICAL
WAS INSTALLED PER APPLICABLE BUILDING AND ELECTRICAL CODES.
9.ABOVE-SLAB ACCESSIBLE RISER DUCT PIPING IS PERMANENTLY IDENTIFIED BY MEANS OF A TAG OR STENCIL AT A MINIMUM OF ONCE EVERY 10-LINEAR FT WITH "VAPOR MITIGATION - CONTACT MAINTENANCE". THE
TURBINE VENTILATOR IS LABELED WITH "VAPOR MITIGATION - CONTACT MAINTENANCE IF DAMAGED".
10.NO COMPONENT OF THE VIMS WAS COVERED WITHOUT BEING INSPECTED AND APPROVED BY THE ENGINEER OR ENGINEER'S DESIGNEE. INSPECTIONS OF EACH COMPONENT OF THE VIMS WAS CONDUCTED BY
THE ENGINEER, OR ENGINEER'S DESIGNEE, TO CONFIRM VIMS COMPONENTS WERE INSTALLED PER THE APPROVED DESIGN. THE REQUIRED INSPECTIONS INCLUDED: (1) INSPECTION OF SUB-SLAB PIPING LAYOUT
AND GRAVEL PLACEMENT PRIOR TO INSTALLING VAPOR LINER; (2) INSPECTION OF VAPOR LINER PRIOR TO POURING CONCRETE; (3) INSPECTION OF ABOVE-GRADE PIPING LAYOUT; AND (4) INSPECTION OF FAN AND
VENT PIPE CONNECTIONS.S:\AAA-Master Projects\The Keith Corporation (TKC)\2021 New Building\VIMP\VIMP Sheets-As-Built.dwg, VM-1, 4/27/2023 5:53:52 PM, amckenzie
VIMS VAPOR LINER AND BASE COURSE (TYP)
VAPOR LINER (SEE SPECIFICATION #3)
CONCRETE FLOOR SLAB
SUB-BASE
VM2
BASE COURSE - CLEAN #57 STONE (WASHED
WITH NO FINES), MIN 4" THICK BENEATH VIMS
VAPOR LINER IN AREAS WITHOUT PIPING
ABC STONE (ONLY PRESENT IN WAREHOUSE)
1
NTS
PROTECTIVE
GEOTEXTILE LAYER
COVER
VIMS SLOTTED COLLECTION PIPING (TYP)
3" SCH 40 THREADED FLUSH JOINT
SLOTTED PVC PIPE (0.020" SLOT WIDTH,
1/8" SLOT SPACING)
SET WITHIN MIN 5" BASE COURSE
(SEE SPECIFICATIONS #3 AND #6)
VAPOR LINER (SEE SPECIFICATION #3
SUB-BASE
NTS
CONCRETE FLOOR SLAB
ABC STONE
VM2
2
PROTECTIVE
GEOTEXTILE LAYER
COVER
SECTION THROUGH EXTERIOR WALL
NTSVM2
BRICK OR BUILDING SIDING
EXTERNAL WALL (NOT
PRESENT AT ALL LOCATIONS)
3
EXTERIOR GRADE
BASE COURSE
(SEE SPECIFICATION #3)
VAPOR BARRIER SEALED TO COLUMN AT
EXTERIOR WALLS
ABC STONE
PROTECTIVE COVER (PLASTIC
SHEETING, GEOTEXTILE LAYER,
OR SIMILAR)
4A
NTSVM2
2" SCH 40 PVC 90 DEGREE ELBOW
VAPOR LINER PENETRATION SEALED TO
PIPE PER MANUFACTURER INSTRUCTIONS2" VENT SCREEN AT
END OF PIPE
EXTERNAL/STUD WALL
(NOT PRESENT IN ALL
LOCATIONS)
2" SOLID SCH 40 PVC
VACUUM MEASURING POINT
MONITORING POINT
POSITIONED SO VENT
SCREEN AT LEAST 5 FT
FROM AN EXTERNAL
WALL
2' MIN
EXTERNAL/STUD WALL
(NOT PRESENT IN ALL
LOCATIONS)
FLUSH WITH
FINISHED FLOOR
4" DIA ZURN INDUSTRIES MODEL
#Z1400 FLOOR CLEANOUT
VIMS VACUUM MEASURING POINT - DETAIL VIEW
NTSVM2
4B
FINISHED FLOOR SLAB
2" DRAIN EXPANSION TEST PLUG
ABC STONE
4" DIA ZURN INDUSTRIES MODEL #Z1400
FLOOR CLEANOUT
4" x 2" FLUSH REDUCER
BUSHING
VAPOR BARRIER PENETRATION SEALED TO
PIPE PER MANUFACTURER INSTRUCTIONS
2" SOLID SCH 40 PVC
NEW FOOTING
VAPOR BARRIER (SEE
SPECIFICATION #3)
BASE COURSE (SEE
SPECIFICATION #3)
SUBBASE
MONITORING POINT AT STEEL COLUMN (TYPICAL)
NTS
2" SCH SOLID PVC PIPE SET
WITHIN 5" BASE COURSE
VAPOR BARRIER SEALED PER
MANUFACTURERS INSTRUCTIONS
STEEL I-BEAM COLUMN
2" SCH 40 PVC
90° ELBOW
VM2
5
2" DRAIN EXPANSION TEST PLUG
EXTERIOR PERMANENT VACUUM MEASURING POINT (TYP)6
NTSVM2
WALL (VARIES)
VAPOR LINER SEALED TO CONCRETE PER
MANUFACTURERS INSTRUCTIONS (TYP)
2" SCH 40 PVC 90
DEGREE ELBOW
2" SOLID SCH 40 PVC PIPE
EXTERIOR GRADE
(VARIES)
BASE COURSE
2" OPEN ENDED PIPE, PLACED AT A MINIMUM OF
5' FROM EXTERIOR TURN-DOWN SLABS
VAPOR LINER
VAPOR LINER SEALED TO PIPE PER
MANUFACTURERS INSTRUCTIONS (TYP)
ABC STONE
LOCKABLE WEATHERPROOF
ENCLOSURE ON OUTSIDE OF BUILDING
WALL WITH REMOVABLE PIPE PLUG AT
END OF 2" PIPE.
EXTERIOR PERMANENT VACUUM MEASURING POINT (TYP)6A
NTSVM2
WALL (VARIES)
VAPOR LINER SEALED TO CONCRETE PER
MANUFACTURERS INSTRUCTIONS (TYP)
2" SOLID SCH 40 PVC PIPE
EXTERIOR GRADE
(VARIES)BASE COURSE
2" OPEN ENDED PIPE, PLACED AT A MINIMUM OF
5' FROM EXTERIOR TURN-DOWN SLABS
VAPOR LINER
VAPOR LINER SEALED TO PIPE PER
MANUFACTURERS INSTRUCTIONS (TYP)
ABC STONE
4C
NTSVM2
OPEN-ENDED 2" SCH 40 PVC PIPE
VAPOR LINER PENETRATION SEALED TO
PIPE PER MANUFACTURER INSTRUCTIONS
EXTERNAL/STUD WALL
(NOT PRESENT IN ALL
LOCATIONS)
2" SOLID SCH 40 PVC
VACUUM MEASURING POINT
4" DIA ZURN INDUSTRIES MODEL
#Z1400 FLOOR CLEANOUT
FLUSH WITH
FINISHED FLOOR
VIMS MONITORING POINT AT WALL CONNECTION
NTS
5A
VM2
BASE COURSE
VAPOR BARRIER SEALED TO PIPE
PER MANUFACTURER
INSTRUCTIONS
WALL (VARIES)
2" SCH 40 PVC 90
DEGREE ELBOW
VAPOR
BARRIER
12" X 12" WALL
ACCESS PANEL
2" DRAIN EXPANSION TEST PLUG
OPEN-ENDED PIPE
POSITIONED AT CENTER OF WALL
2" SOLID SCH 40 PVC PIPE
H&H NO. TKC-008
VAPOR MITIGATION PLAN
PREPARED BY:
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
VAPOR INTRUSION
MITIGATION DETAILSHD CHARLOTTE BCR FDC13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINADEVELOPER:
THE KEITH
CORPORATION
VM-2
PROFESSIONAL
APPROVAL
AS-BUILT
APRIL 27, 2023
S:\AAA-Master Projects\The Keith Corporation (TKC)\2021 New Building\VIMP\VIMP Sheets-As-Built.dwg, VM-2, 4/27/2023 5:54:50 PM, amckenzie
10
NTSVM2A
SINGLE RISER EXTRACTION POINT IN GUARDHOUSE
EXTERIOR WALL
3" PVC RISER DUCT PIPE.
OPEN-ENDED 3" DIA PVC
90-DEGREE ELBOW PLACED
WITHIN BASE COURSE
EXTERIOR GRADE
SUB-BALLAST
RAIL BALLAST
TOP OF RAIL
ELEVATION
VAPOR BARRIER SET
BETWEEN SUBGRADE
AND SUB-BALLAST
EXTERIOR WALL
6" PVC RISER DUCT PIPE.
FINISHED WAREHOUSE
FLOOR ELEVATION
RETAINING WALL AT
RAIL LINE- SEE DETAIL
#13
RISER IN RAIL LINE
NTSVM2A
11
BASE COURSE
AROUND RISER
INLET
RAIL LINE AT EXTERIOR BUILDING WALL
NTSVM2A
12
SUB-BALLAST
RAIL BALLAST
TOP OF RAIL
ELEVATION
VAPOR BARRIER SET
BETWEEN SUBGRADE
AND SUB-BALLAST
EXTERIOR WALL
6" PVC RISER DUCT PIPE.
FINISHED WAREHOUSE
FLOOR ELEVATION
RETAINING WALL AT
RAIL LINE- SEE DETAIL
#11
VIMS PIPE CAP VENTILATOR FAN & EXHAUST (TYPICAL)
NTS
AURA PVC PIPE CAP VENTILATOR FAN
ELECTRICAL JUNCTION BOX FOR POTENTIAL FUTURE
VACUUM FAN (REFER TO SPECIFICATION #8)
RISER DUCT PIPE THROUGH ROOF
FLASHING
ROOFTOP
6" HEAVY DUTY NO HUB
COUPLING
VM2A
15
PLEASE NOTE: THE RISER IN THE
GUARDHOUSE IS A 3" SCH 40 PVC
CONNECTED TO A 3" AURA VENTILATOR
RETAINING WALL AT RAIL LINE
NTSVM2A
13
RAIL LINE
INTERIOR
WAREHOUSE
SPACE
HANDRAIL
VAPOR LINER
(SEE SPECIFICATION #3)
SUBBASE
CONCRETE FLOOR SLAB
SUB-BALLAST
RAIL BALLAST
TOP OF RAIL
ELEVATION
VAPOR BARRIER SET BETWEEN SUBGRADE AND
SUB-BALLAST
VIMS VAPOR LINER AT FLOOR DRAIN
NTS
CONCRETE FLOOR
SLAB SLOPED
TOWARD DRAIN
BASE COURSE
(SEE SPECIFICATION #3)
VAPOR LINER
(SEE SPECIFICATION #3)
SUB-BASE
VM2A
14
FLOOR DRAIN
ABC STONE
PROTECTIVE
GEOTEXTILE LAYER
COVER
VAPOR LINER SEALED TO COLUMN PER
MANUFACTURER INSTRUCTIONS
TYPICAL VIMS LINER ABOVE COLUMN FOOTING7
NTSVM2A
BASE COURSE
(SEE SPECIFICATION #3)
VAPOR BARRIER SEALED TO CONCRETE
PER MANUFACTURER INSTRUCTIONS
ABC STONE
SEE DETAIL 9/VM2A
BASE COURSE
(SEE SPECIFICATION #3)
VAPOR LINER SEALED TO COLUMN PER
MANUFACTURER INSTRUCTIONS
TYPICAL RISER AT COLUMN FOOTING8
NTSVM2A
ABC STONE
STEEL COLUMN
TO DISCHARGE
POINT ON ROOF
VAPOR BARRIER PENETRATION
SEALED TO PIPE PENETRATION PER
MANUFACTURER INSTRUCTIONS
FOOTING
6" SCH 40 SOLID PVC
RISER TO ROOF
3" SCH 40 SOLID PVC PIPE SET
WITHIN 5" BASE COURSE
(SEE SPECIFICATION #3)
6" TO 3" SCH 40 SOLID PVC PIPE 45
DEGREE REDUCER
SEE DETAIL 9/VM2A
CIP CONCRETE COLUMN
CONCRETE FLOOR SLAB
VAPOR LINER
STEEL PLATE
VIMS AT COLUMNS - SLEEVE PLATE
NTSVM2A
9
VAPOR LINER SEALED TO COLUMN
PLATE PER MANUFACTURERS
INSTRUCTIONS
H&H NO. TKC-008
VAPOR MITIGATION PLAN
PREPARED BY:
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
VAPOR INTRUSION
MITIGATION DETAILSHD CHARLOTTE BCR FDC13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINADEVELOPER:
THE KEITH
CORPORATION
VM-2A
PROFESSIONAL
APPROVAL
AS-BUILT
APRIL 27, 2023
S:\AAA-Master Projects\The Keith Corporation (TKC)\2021 New Building\VIMP\VIMP Sheets-As-Built.dwg, VM2a, 4/27/2023 5:55:33 PM, amckenzie
FDFDFDFDFDFDCR FDCRCR
TCTC
FD
FD
FD
CR
CRFD
FDEFLT/FTG. = -5'-0"T/FTG. = -2'-0"SPARTIAL PLANSEE SHEET S-103PARTIAL PLANSEE SHEET S-104MATCH
LINE T/FTG. = -5'-0"T/FTG. = -2'-0"SMP-12
MP-6
MP-4
MP-13
MP-1
MP-5
MP-3
MP-14
MP-7
INTERIOR RAIL LINE SPUR
MP-2
MP-11
E-27
E-23
E-16
E-2
E-9
E-5
E-11
E-18
E-29
E-7
E-19
E-25
E-3
E-14
E-30
E-26
E-21
E-22
E-1
E-10
E-17
E-28
E-6
E-12 E-13
E-4
E-8
E-15
E-24
E-20
E-31 E-32 E-33 E-34 E-35
MP-9
MP-10
MP-8
H&H NO. TKC-008
VAPOR MITIGATION PLAN
PREPARED BY:
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
VAPOR INTRUSION
MITIGATION SYSTEM
SUB-SLAB LAYOUT -
WAREHOUSEHD CHARLOTTE BCR FDC13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINADEVELOPER:
THE KEITH
CORPORATION
VM-3
PROFESSIONAL
APPROVAL
AS-BUILT
APRIL 27, 2023LEGEND
EXTENT OF VAPOR LINER
SOIL GAS COLLECTION SYSTEM (SEE SPECIFICATION #6 ON
VM-1)
6" DIA SCH 40 SOLID PVC VERTICAL RISER WITH
IDENTIFICATION NUMBER
2" DIA SOLID PVC MONITORING POINT AND SUB-SLAB SOIL GAS
SAMPLE LOCATION
INDOOR AIR SAMPLE LOCATION
APPROXIMATE LOCATION OF UTILITY BANKS SEALED WITH
POUR-N-SEAL (SEE SPECIFICATION #4 ON VM-1)
E-7
MP-4
3
VM2
1
VM2
2
VM2
8
VM2A
6
VM2
4C
VM2
7
VM2A
8
VM2A
12
VM2A
11
VM2A
14
VM2A
11
VM2A
13
VM2A
4A
VM2
6
VM2
5
VM2
8
VM2A
IAS-1
IAS-1
IAS-2
IAS-3
6A
VM2
6A
VM2
5A
VM26
VM2
4A
VM2
5
VM2
6
VM2
4A
VM2
4A
VM2
S:\AAA-Master Projects\The Keith Corporation (TKC)\2021 New Building\VIMP\VIMP Sheets-As-Built.dwg, VM-3, 4/27/2023 5:56:30 PM, amckenzie
FDEF
L
WATER TANK
FIRE PUMPHOUSE
MP-15
GUARD HOUSE
E-31
MP-16
H&H NO. TKC-008
VAPOR MITIGATION PLAN
PREPARED BY:
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
VAPOR INTRUSION
MITIGATION SYSTEM
SUB-SLAB LAYOUT -
GUARDHOUSE & FIRE
PUMPHOUSEHD CHARLOTTE BCR FDC13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINADEVELOPER:
THE KEITH
CORPORATION
VM-4
PROFESSIONAL
APPROVAL
AS-BUILT
APRIL 27, 2023LEGEND
EXTENT OF VAPOR LINER
3" DIA SCH 40 SOLID PVC VERTICAL RISER WITH
IDENTIFICATION NUMBER
2" DIA SOLID PVC PRESSURE MONITORING POINT
E-31
MP-11
6
VM2
1
VM2
10
VM2A
3
VM2
6
VM2
SUB-SLAB SAMPLE LOCATION
S:\AAA-Master Projects\The Keith Corporation (TKC)\2021 New Building\VIMP\VIMP Sheets-As-Built.dwg, VM-4, 4/27/2023 5:57:17 PM, amckenzie

Appendix D Vapor Intrusion Mitigation System Product Specifications

PRODUCT PART #
VaporBlock® Plus™ 20 ................................................................ VBP20
UNDER-SLAB VAPOR / GAS BARRIER
Under-Slab Vapor/Gas Retarder
© 2018 RAVEN INDUSTRIES INC. All rights reserved.
VAPORBLOCK® PLUS™VBP20
PRODUCT DESCRIPTION
VaporBlock® Plus™ is a seven-layer co-extruded barrier
made using high quality virgin-grade polyethylene and
EVOH resins to provide unmatched impact strength as well
as superior resistance to gas and moisture transmission.
VaporBlock® Plus™ 20 is more than 100 times less permeable
than typical high-performance polyethylene vapor retarders
against Methane, Radon, and other harmful VOCs. Tested and
verified for unsurpassed protection against BTEX, HS, TCE, PCE,
methane, radon, other toxic chemicals and odors.
VaporBlock® Plus™ 20 multi-layer gas barrier is manufactured
with the latest EVOH barrier technology to mitigate hazardous
vapor intrusion from damaging indoor air quality, and the safety
and health of building occupants. VBP20 is one of the most
effective underslab gas barriers in the building industry today
far exceeding ASTM E-1745 (Plastic Water Vapor Retarders
Used in Contact with Soil or Granular Fill Under Concrete Slabs)
Class A, B and C requirements. Available in a 20 (Class A) mil
thicknesses designed to meet the most stringent requirements.
VaporBlock® Plus™ 20 is produced within the strict guidelines
of our ISO 9001 Certified Management System.
PRODUCT USE
VaporBlock® Plus™ 20 resists gas and moisture migration
into the building envelop when properly installed to provide
protection from toxic/harmful chemicals. It can be installed as
part of a passive or active control system extending across the
entire building including floors, walls and crawl spaces. When
installed as a passive system it is recommended to also include
a ventilated system with sump(s) that could be converted to an
active control system with properly designed ventilation fans.
VaporBlock® Plus™ 20 works to protect your flooring and
other moisture-sensitive furnishings in the building’s interior
from moisture and water vapor migration, greatly reducing
condensation, mold and degradation.
SIZE & PACKAGING
VaporBlock® Plus™ 20 is available in 10’ x 150’ rolls to
maximize coverage. All rolls are folded on heavy-duty cores
for ease in handling and installation. Other custom sizes
with factory welded seams are available based on minimum
volume requirements. Installation instructions and ASTM E-1745
classifications accompany each roll.
APPLICATIONS
Radon Barrier
Methane Barrier
VOC Barrier
Brownfields Barrier
Vapor Intrusion Barrier
Under-Slab Vapor Retarder
Foundation Wall Vapor Retarder
VaporBlock® Plus™ is a seven-layer co-extruded barrier made using high quality virgin-grade polyethylene and EVOH resins to provide unmatched impact strength as well as superior resistance to gas and moisture transmission.
VaporBlock® Plus™ Placement
All instructions on architectural or structural drawings should be reviewed and followed.
Detailed installation instructions accompany each roll of VaporBlock® Plus™ and can also be located at www.ravenefd.com.
ASTM E-1643 also provides general installation information for vapor retarders.
VAPORBLOCK® PLUS™ 20
PROPERTIES TEST METHOD IMPERIAL METRIC
AppeArAnce White/Gold
Thickness, nominAl 20 mil 0.51 mm
WeighT 102 lbs/MSF 498 g/m²
clAssificATion ASTM E 1745 CLASS A, B & C
³ Tensile sTrengTh
ASTM E 154Section 9(D-882)58 lbf 102 N
impAcT resisTAnce ASTM D 1709 2600 g
permeAnce (neW mATeriAl)
ASTM E 154Section 7ASTM E 96Procedure B
0.0098 Perms
grains/(ft²·hr·in·Hg)
0.0064 Perms
g/(24hr·m²·mm Hg)
permeAnce (AfTer condiTioning)
(sAme meAsuremenT As Above permeAnce)
ASTM E 154Section 8, E96Section 11, E96Section 12, E96Section 13, E96
0.00790.00790.00970.0113
0.00520.00520.00640.0074
WvTr ASTM E 96Procedure B 0.0040 grains/hr-ft²0.0028 gm/hr-m²
benzene permeAnce See Note ⁶1.13 x 10-¹⁰ m²/sec or 3.62 x 10-¹³ m/s
Toluene permeAnce See Note ⁶1.57 x 10-¹⁰ m²/sec or 1.46 x 10-¹³ m/s
eThylbenzene permeAnce See Note ⁶1.23 x 10-¹⁰ m²/sec or 3.34 x 10-¹⁴ m/s
m & p-Xylenes permeAnce See Note ⁶1.17 x 10-¹⁰ m²/sec or 3.81 x 10-¹⁴ m/s
o-Xylene permeAnce See Note ⁶1.10 x 10-¹⁰ m²/sec or 3.43 x 10-¹⁴ m/s
hydrogen sulfide See Note 9 1.92E-⁰⁹ m/s
TrichloroeThylene (Tce) See Note ⁶7.66 x 10-¹¹ m²/sec or 1.05 x 10-¹⁴ m/s
perchloroeThylene (pce)See Note ⁶7.22 x 10-¹¹ m²/sec or 1.04 x 10-¹⁴ m/s
rAdon diffusion coeffiecienT K124/02/95 < 1.1 x 10-13 m2/s
meThAne permeAnce ASTM D 1434 3.68E-¹² m/sGas Transmission Rate (GTR):0.32 mL/m²•day•atm
mAXimum sTATic use TemperATure 180° F 82° C
minimum sTATic use TemperATure - 70° F - 57° C
UNDER-SLAB VAPOR / GAS BARRIER
VAPORBLOCK® PLUS™VBP20
© 2018 RAVEN INDUSTRIES INC. All rights reserved.
Scan QR Code to download
current technical data sheets
via the Raven website.
Note: To the best of our knowledge, unless otherwise stated, these are typical property values and are intended as guides only, not as specification limits. Chemical resistance, odor transmission, longevity as well as other performance criteria is not implied or given and actual testing must be performed for applicability in specific applications and/or conditions. RAVEN INDUSTRIES MAKES NO WARRANTIES AS TO THE FITNESS FOR A SPECIFIC USE OR MERCHANTABILITY OF PRODUCTS REFERRED TO, no guarantee of satisfactory results from reliance upon contained information or recommendations and disclaims all liability for resulting loss or damage. Limited Warranty available at www.RavenEFD.com
061318 EFD 1125
RAVEN ENGINEERED FILMSP.O. Box 5107 Sioux Falls, SD 57117-5107Ph: [phone] • TF: [phone] [e-mail]
³ Tests are an average of machine and transverse directions.5 Raven Industries performs seam testing at 20” per minute.6 Aqueous Phase Film Permeance. Permeation of Volatile Organic Compounds through EVOH Thin Film Membranes and Coextruded LLDPE/EVOH/
LLDPE Geomembranes, McWatters and Rowe, Journal of Geotechnical and Geoenvironmental Engineering© ASCE/
September 2015. (Permeation is the Permeation Coefficient adjusted to actual film thickness - calculated at 1 kg/m³.)
The study used to determine PCE and TCE is titled: Evaluation of diffusion of PCE & TCE through high performance geomembranes by Di
Battista and Rowe, Queens University 8 Feb 2018.9 The study used to determine diffusion coefficients is titled: Hydrogen Sulfide (H₂S) Transport through Simulated Interim Covers with Conventional and Co-Extruded Ethylene-Vinyl Alcohol (EVOH) Geomembranes.
INSTALLATION GUIDELINES - With VaporSeal™ Tape
VaporSeal™
4” Tape
VaporSeal™ 4” Tape Optional Butyl Seal
2-Sided Tape
Gas Barrier Applications
Elements of a moisture/gas-resistant floor system. General illustration only.(Note: This example shows multiple options for waterstop placement.
VaporSeal™
4” Tape
VaporSeal™ 4” Tape Optional Butyl Seal
2-Sided Tape
Gas Barrier Applications
Fig. 2: VaporBlock® Plus™ Overlap Joint Sealing Methods
Fig. 1: VaporBlock® Plus™ Overlapping Roll-out Method
Please Note: Read these instructions thoroughly before installation to ensure proper use of VaporBlock® Plus™. ASTM E 1465, ASTM E 2121 and, ASTM E 1643 also provide valuable information regarding the installation of vapor / gas barriers. When installing this product, contractors shall conform to all applicable local, state and federal regulations and laws pertaining to residential and commercial building construction.
• When VaporBlock® Plus™ gas barrier is used as part of an active control system for radon or other gas, a ventilation system will be required.
• If designed as a passive system, it is recommended to install a ventilation system that could be converted to an active system if needed.
Materials List:VaporBlock® Plus™ Vapor / Gas BarrierVaporSeal™* 4” Seaming TapeVaporSeal™* 12” Seaming/Repair TapeButyl Seal 2-Sided TapeVaporBoot Plus Pipe Boots 12/Box (recommended)VaporBoot Tape (optional)POUR-N-SEAL™ (optional)1” Foam Weather Stripping (optional)Mako® Screed Supports (optional)
VAPORBLOCK® PLUS™ PLACEMENT
1.1. Level and tamp or roll granular base as specified. A base for a gas-reduction system may require a 4” to 6” gas permeable layer of clean coarse aggregate as specified by your architectural or structural drawings after installation of the recommended gas collection system. In this situation, a cushion layer consisting of a non-woven geotextile fabric placed directly under VaporBlock® Plus™ will help protect the barrier from damage due to possible sharp coarse aggregate.
1.2. Unroll VaporBlock® Plus™ running the longest dimension parallel with the direction of the pour and pull open all folds to full width. (Fig. 1)
1.3. Lap VaporBlock® Plus™ over the footings and seal with Raven Butyl Seal tape at the footing-wall connection. Prime concrete surfaces, when necessary, and assure they are dry and clean prior to applying Raven Butyl Seal Tape. Apply even and firm pressure with a rubber roller. Overlap joints a minimum of 6” and seal overlap with 4” VaporSeal™ Tape. When used as a gas barrier, overlap joints a minimum of 12” and seal in-between overlap with an optional 2-sided Raven Butyl Seal Tape. Then seal with 4” VaporSeal™ Tape centered on the overlap seam. (Fig. 2)
Page 1 of 4 Top original diagram and figure #1 were reprinted with permission by the Portland Cement Association.Reference: Kanare, Howard M., Concrete Floors and Moisture, EB119, Portland Cement Association, Skokie, Illinois, and National Ready Mixed Concrete Association, Silver Spring, Maryland, USA, 2008, 176 pages.
1.4. Seal around all plumbing, conduit, support columns or other penetrations that come through the VaporBlock® Plus™ membrane.
1.4a. Method 1: Pipes four inches or smaller can be sealed with Raven VaporBoot Plus preformed pipe boots. VaporBoot Plus preformed pipe boots are formed in steps for 1”, 2”, 3” and 4” PVC pipe or IPS size and are sold in units of 12 per box (Fig. 3 & 5).
Pipe boots may also be fabricated from excess VaporBlock® Plus™ membrane (Fig. 4 & 6) and sealed with VaporBoot Tape or VaporSeal™ Tape (sold separately).
1.4b. Method 2: To fabricate pipe boots from VaporBlock® Plus™ excess material (see Fig. 4 & 6 for A-F):
A) Cut a square large enough to overlap 12” in all directions.
B) Mark where to cut opening on the center of the square and cut four to eight slices about 3/8” less than the diameter of the pipe.
C) Force the square over the pipe leaving the tightly stretched cut area around the bottom of the pipe with approximately a 1/2” of the boot material running vertically up the pipe. (no more than a 1/2” of stretched boot material is recommended)
D) Once boot is positioned, seal the perimeter to the membrane by applying 2-sided Raven Butyl Seal Tape in between the two layers. Secure boot down firmly over the membrane taking care not to have any large folds or creases.
E) Use VaporBoot Tape or VaporSeal™ Tape to secure the boot to the
pipe.
VaporBoot Tape (option) – fold tape in half lengthwise, remove half of the release liner and wrap around the pipe allowing 1” extra for overlap sealing. Peel off the second half of the release liner and work the tape outward gradually forming a complete seal.
VaporSeal™ Tape (option) - Tape completely around pipe overlapping the VaporBlock® Plus™ square to create a tight seal against the pipe.
F) Complete the process by taping over the boot perimeter edge with VaporSeal™ Tape to create a monolithic membrane between the surface of the slab and gas/moisture sources below and at the slab perimeter. (Fig. 4 & 6)
Preformed Pipe Boot Square Material Pipe Boot
Fig. 3
SINGLE PENETRATION PIPE BOOT INSTALLATION
Fig. 5 Fig. 6
1. Cut a square of VaporBlock® Plus™ barrier to extend at least 12” from the pipe in all directions.
2. Cut four to eight slices about 3/8” less than the diameter of the pipe.
5. Use Raven VaporBoot or VaporSeal™ Tape and overlap 1” at the seam.
4. Tape over the boot perimeter edge with VaporSeal™ Tape.
1. Cut out one of the preformed boot steps (1” to 4”).
2. Tape the underside boot perimeter with 2-sided Butyl Seal Tape.
3. Force the boot over pipe and press tape firmly in place.
4. Use VaporSeal™ Tape
to secure boot to the pipe.
5. Tape around entire boot edge with VaporSeal™ Tape.
VaporBoot Flexible Tapeor VaporSeal™ 4” TapeVaporSeal™ 4” Tape
VaporBlock® Plus™Material
VaporSeal™ 4” Tape
Raven Butyl Seal2-Sided Tape Raven Butyl Seal2-Sided Tape
VaporBoot PlusPreformed Boot 12”(minimum)
3. Force over pipe and tape the underside boot perimeter to existing barrier with 2-sided Butyl Seal Tape.
Fig. 4
Page 2 of 4 Original figure #4 diagram is reprinted with permission by the Portland Cement Association.Reference: Kanare, Howard M., Concrete Floors and Moisture, EB119, Portland Cement Association, Skokie, Illinois, and National Ready Mixed Concrete Association, Silver Spring, Maryland, USA, 2008, 176 pages.Method 1
Method 2
VaporSeal™4” Tape VaporBoot PlusPerformed Boot
Raven Butyl Seal 2-sided Tape Raven Butyl Seal 2-sided Tape
1.5. Sealing side-by-side multiple penetrations (option 1);
A) Cut a patch large enough to overlap 12” in all directions (Fig. 7)
of penetrations.
B) Mark where to cut openings and cut four to eight slices about
3/8” less than the diameter of the penetration for each.
C) Force patch material over penetration to achieve a tight fit and
form a lip.
D) Once patch is positioned, seal the perimeter to the membrane
by applying 2-sided Raven Butyl Seal Tape in-between the two
layers. (Fig. 8)
E) After applying Raven Butyl Seal Tape between the patch and
membrane, tape around each of the penetrations and the patch
with VaporSeal™ 4” tape. (Fig. 9) For additional protection apply
POUR-N-SEAL™ or an acceptable polyurethane elastomeric
sealant around the penetrations. (Fig. 10)
Fig. 7 Fig. 8
Fig. 9 Fig. 10
MULTIPLE PENETRATION PIPE BOOT INSTALLATION
Fig. 6
Cut a patch large enough to overlap 12” in all directions and slide over penetrations (Make openings as tight as possible.)
Once the overlay patch is positioned, seal the perimeter to the membrane by applying 2-sided Raven Butyl Seal Tape in-between the two layers.
After applying Raven Butyl Seal Tapebetween the patch and membrane, tape around the perimeter of the penetration and the patch with VaporSeal™ 4” Tape.
For additional protection apply POUR-N-SEAL™ or an acceptable polyurethane elastomeric sealant around the penetrations.
VaporSeal™ 4” Tape VaporSeal™ 4” Tape
Page 3 of 4
Option 1
Raven Butyl Seal 2-sided Tape
1.6. POUR-N-SEAL™ method of sealing side-by-side multiple penetrations (option 2);
A) Install the vapor barrier as closely as possible to pipe penetrations to minimize the amount of POUR-N-SEAL™ necessary to seal around all penetrations.
B) Once barrier is in place, remove soil or other particles with a dry cloth or a fine broom to allow for improved adhesion to the POUR-N-SEAL™ liquid.
C) Create a dam around the penetration area approximately 2” away from the pipe or other vertical penetrations by removing the release liner from the back of a 1” weather stripping foam and adhere to the vapor barrier. Form a complete circle to contain the POUR-N-SEAL™ materials (Fig. 11).
D) Once mixed, pour contents around the pipe penetrations. If needed, a brush or a flat wooden stick can be used to direct the sealant completely around penetrations creating a complete seal (Fig. 12-13).
E) DO NOT leave excess POUR-N-SEAL™ in plastic container for longer than the time it takes to pour sealant.
Fig. 12 Fig. 13
Fig. 11
Option 2
VAPORBLOCK® PLUS™ REPAIR INSTRUCTIONS
1.7. Proper installation requires all holes and openings are repaired prior
to placing concrete. When patching small holes, simply cut a 12” long
piece of 12” wide VaporSeal™ tape. Remove release liner and center
over the opening. Apply pressure to create a seal (Fig. 14-15).
1.8. When installing VaporBlock® Plus™ around pipe penetrations,
vertical columns, electrical ducts and other obstructions, you will
find it necessary to cut it to the nearest outside edge. This cut can
be easily sealed with 12” wide VaporSeal™ tape, by simply centering
it over the cut, 6” on either side. Once the tape is placed correctly,
apply pressure to assure a complete seal (Fig. 16).
Reminder Note: All holes or penetrations through the membrane will need
to be patched with 12” VaporSeal™ Tape.
Fig. 14
Page 4 of 5
Fig. 15
2.1. When installing reinforcing steel and utilities, in addition to the
placement of concrete, take precaution to protect VaporBlock®
Plus™. Carelessness during installation can damage the most
puncture–resistant membrane. Sheets of plywood cushioned with
geotextile fabric temporarily placed on VaporBlock® Plus™ provide
for additional protection in high traffic areas including concrete
buggies.
2.2. Use only brick-type or chair-type reinforcing bar supports to protect
VaporBlock® Plus™ from puncture.
2.3. Avoid driving stakes through VaporBlock® Plus™. If this cannot be
avoided, each individual hole must be repaired per section 1.7.
2.4. To avoid penetrating VaporBlock® Plus™ when installing screed
supports, utilize non-penetrating support, such as the Mako®
Screed Support System (Fig. 17). Avoid driving stakes through
VaporBlock® Plus™. If this cannot be avoided, each individual hole
must be repaired per figures 14-15.
2.5. If a cushion or blotter layer is required in the design between
VaporBlock® Plus™ and the slab, additional care should be given if
sharp crushed rock is used. Washed rock will provide less chance of
damage during placement. Care must be taken to protect blotter layer
from precipitation before concrete is placed.
VaporBlock® Plus™ Gas & Moisture Barrier can be identified on site
as gold/white in color printed in black ink with following logo and
classification listing (Fig. 18)
Page 5 of 5
VaporBlock® Plus™
Gas & Moisture Barrier
Note: To the best of our knowledge, unless otherwise stated, these are typical property values and are intended as guides only, not as specification limits. Chemical resistance, odor transmission, longevity as well as other performance criteria is not implied or given and actual testing must be performed for applicability in specific applications and/or conditions. RAVEN INDUSTRIES MAKES NO WARRANTIES AS TO THE FITNESS FOR A SPECIFIC USE OR MERCHANTABILITY OF PRODUCTS REFERRED TO, no guarantee of satisfactory results from reliance upon contained information or recommendations and disclaims all liability for resulting loss or damage. Limited Warranty available at wwww.RavenEFD.com
ENGINEERED FILMSP.O. Box 5107 Sioux Falls, SD 57117-5107Ph: [phone] • TF: [phone]
[e-mail]
020316 EFD 1127
VAPORBLOCK® PLUS™ PROTECTION
Fig. 16
Fig. 18
Fig. 17
* Patent Pending
© Raven 2016. All Rights Reserved.
ACCESSORIES
SEAMING TAPES & OTHER ACCESSORIES FOR PLASTIC SHEETING
ACCESSORY TAPES AND EPOXY
Butyl Seal Tape (TP2BR / TP6BR)
Butyl Seal is a double-sided reinforced aggressive black butyl rubber tape used to join panels of polyethylene and polypropylene together by overlapping the edges and applying Butyl Seal in between. It is also used to adhere to concrete walls and footings when properly prepared. Butyl Seal is non-hardening and flexible. Available in 2” x 50’ and 6” x 50’ rolls.
R25B Tape (R25B)
R25B Tape is a single-sided aggressive synthetic elastomeric adhesive that bonds instantly to properly prepared polyethylene and polypropylene. The black polymer backing and adhesive is specially formulated to provide years of performance even in direct sunlight. A poly release liner provides for ease of installation. Available in 4” x 100’ roll.
VaporBond™ Tape (TVB4)
VaporBond™ Tape is a white single-sided tape that combines a heavy-duty, weather-resistant polyethylene backing with an aggressive rubber adhesive. VaporBond™ Tape offers excellent seaming capabilities for our materials with an “Easy Tear” feature to reduce installation time. TVB4 has a WVTR of 0.18 perms per ASTM D3833. Typical applications include vapor retarders, covers and liners. Available in 4” x 210’ roll.
VaporSeal™ Tape (TVSP4/TVSP12)
VaporSeal™ Tape is a patent pending single-sided 7-layer gas barrier tape with a release liner for ease of installation. The backing contains a layer of highly impermeable EVOH designed to block migration of radon, methane, and VOC’s. An aggressive acrylic adhesive provides outstanding adhesion to polyethylene over a wide temperature range. Typical uses include joining, repairing and sealing gas/moisture barriers. Available in 4” x 160’ and 12” x 50’ rolls.
VaporBoot™ Tape (TBOOT)
VaporBoot™ Tape is a single-sided elastomeric butyl tape used to complete pipe boot installations (sealing the boot to the pipe). The 100% stretchable butyl adhesive features excellent adhesion values and 3-D stretching that can be easily molded to multiple surfaces without any creases and folds. Available in 2” x 16.4’ roll.
ADDITIONAL ACCESSORIES
VaporBoot™ System (VBOOT)
The VaporBoot™ System is designed to assist in securing pipe and other penetrations that run vertically through the vapor retarder material. The VaporBoot™ System offers a quick solution and is delivered to the jobsite in a complete package. VaporBoots are produced from high performance VaporBlock® material.
Package Contents: 25 - VaporBoots (18” x 18”, w/precut center marker)1 - roll of VaporBoot Tape
VaporBoot™ Plus Preformed Pipe Boots (VBPBT)
VaporBoot™ Plus Preformed Pipe Boots are produced from heavy 40 mil co-extruded polyethylene and barrier resins for excellent strength and durability. The preformed boots are stepped to fit 1” to 4” wide pipe penetrations. VaporBoot™ Plus Preformed Pipe Boots are available in quantities of 12 per box.
From tie-down fasteners to field seaming tape, Raven Industries has the accessories you need to maximize your film’s versatility and minimize installation time on the job.
© 2021 RAVEN INDUSTRIES INC. All rights reserved.
POUR-N-SEAL™ (PNS1G)
POUR-N-SEAL™ is a gray two part epoxy used to seal around multi-pipe penetrations in areas where pipe boots are not practical, when installing underslab barriers. The POUR-N-SEAL™ system installation guide references a 1” x 25 lineal feet adhesive-backed foam to form a dam around multi-pipe penetrations to contain POUR-N-SEAL™ during the setting process. The 1” x 25 ft. adhesive-backed foam is sold seperately as FOAM25.
ACCESSORIES
ADDITIONAL ACCESSORIES (CONTINUED)
Tie-Down Buttons (BUTI) & Tarp Grabbers (BUTEZ)
Tie-Down Buttons and Tarp Grabbers help keep plastic sheeting securely in place. Tie-Down Buttons are designed to eliminate traditional grommets in plastic sheeting up to 10 mil thick and are reusable plastic fittings that are easy to install in any position. Tarp Grabbers are up to 4 times stronger than a brass grommet and are typically used in heavier plastic sheeting from 10 mil to 30 mil thick. Great for equipment covers, large storage covers and truck tarps.
Dura♦Skrim® Reinforced Sandbags
Dura♦Skrim® reinforced sandbags are used to secure large covers and liners to prevent wind damage. Sandbags are produced with strong Dura♦Skrim® 8 & 12 mil reinforced polyethylene. These 15” wide x 24” long bags are designed to hold 35 lbs. Sandbags are also available in other Raven reinforced materials with minimum order requirements. 11.8” Cable Ties are also available.
Dura-Clip™ (CLIP11)
These full size clips are 11” long and fit most commercial scaffolding. Dura-Clip™ will securely fasten your poly sheeting to scaffolding, reducing wind whip and increasing the life of your enclosure. The Dura-Clip™ is normally placed about every 3’ onto the enclosure.
Raven Welding Rod
Raven Welding Rod is used for field seaming, repairs and detail work, such as installing pipe boots. Packaged in 25 lb spools, it is available in 4mm and 5mm sizes to fit most brands of extrusion guns. Raven Welding Rod is made from a thermally UV stabilized LLDPE resin and is available in both black and white to correspond with the color of geomembranes being utilized.
SEAMING TAPES & OTHER ACCESSORIES FOR PLASTIC SHEETING
TAPE ACCESSORY PROPERTIES
PROPERTIES VaporBond Tape(TVB4)VaporSeal Tape(TVSP4 / TVSP12)VaporBoot Tape(TBOOT)R25B Tape(R25B)Butyl Seal Tape(TP2BR / TP6BR)
Backing 6.7 mil Polyethylene 7 mil EVOH/LLDPE 30 mil EPDM 8 mil Multi-Polymer N/A
Adhesive 3.3 mil Rubber Based Pressure-Sensitive 2 mil Acrylic Adhesive Pressure-Sensitive 20 milButyl Rubber 17 milSynthetic Elastomeric 40 milButyl Rubber
Color White Silver Black Black Black
Type Single Sided Single Sided Single Sided Single Sided Double Sided
Size 4” x 210’4” x 160’ / 12” x 50’2” x 16.4’4” x 100’2” x 50’ / 6” x 50’
Rolls per Case 12 12 / 4 64 6 16 / 4
Weight per Case 45 lbs 50 lbs / 18 lbs 45 lbs 33 lbs 47 lbs / 20 lbs
Adhesion Values 35 oz. / in. (to steel)80 oz. / in. (to steel)145 oz. / in. (to steel)144 oz. / in. (to steel)88 oz. / in. (to steel)
Perms 0.081 g/(24h*100 in²)0.014 g/(24h*100 in²)N/A <0.005 g/(24h*100 in²)0.82 g/(24h*100 in²)
Service Temp.-40° F to +180° F -40° F to +190° F +14° F to +122° F +20° F to +180° F 0° F to +170° F
Min.Application Temp.50° F 50° F 14° F 35° F 35° F
Ideal StorageTemp. / Humidity 70° F w/ 40-50 %60°-80° F w/ 40-60 %70° F w/ 70 %70° F w/ 40-50 %70° F w/ 40-50 %
© 2021 RAVEN INDUSTRIES INC. All rights reserved.
Scan QR Code to download current technical data sheets via the Raven website.
Note: To the best of our knowledge, unless otherwise stated, these are typical property values and are intended as guides only, not as specification limits. Chemical resistance, odor transmission, longevity as well as other performance criteria is not implied or given and actual testing must be performed for applicability in specific applications and/or conditions. RAVEN INDUSTRIES MAKES NO WARRANTIES AS TO THE FITNESS FOR A SPECIFIC USE OR MERCHANTABILITY OF PRODUCTS REFERRED TO, no guarantee of satisfactory results from reliance upon contained information or recommendations and disclaims all liability for resulting loss or damage. Limited Warranty available at www.RavenEFD.com
012021 EFD 1103
RAVEN ENGINEERED FILMSP.O. Box 5107 Sioux Falls, SD 57117-5107Ph: [phone] • TF: [phone] [e-mail]
Dimensional Data (inches and [ mm ]) are Subject to Manufacturing Tolerances and Change Without Notice
SPECIFICATION SHEET
TAG _______
®
* Regularly furnished unless otherwise specified.
Zurn Industries, LLC |Specification Drainage Operation
1801 Pittsburgh Avenue, Erie, PA U.S.A. 16502 · Ph. 855-663-9876, Fax [phone]
In Canada |Zurn Industries Limited
3544 Nashua Drive, Mississauga, Ontario L4V 1L2 · Ph. 905-405-8272, Fax [phone]
www.zurn.com
Z1400
EXTRA-HEAVY-DUTY "LEVEL-TROL"
ADJUSTABLE FLOOR CLEANOUT
PIPE SIZE (Specify size/type) OUTLET 'E' BODY HT. DIM.
2,3,4,6 [51,76,102,152]_____ IC Inside Caulk See Chart
2,3,4,6,8 [51,76,102,152,203]_____ NH No-Hub See Chart
2,3,4,6,8 [51,76,102,152,203]_____ NL Neo-Loc See Chart
OPTIONS (Check/specify appropriate options)
PREFIXES
_____ Z Dura Coated Cast Iron*
_____ ZB D.C.C.I. w/ Polished Bronze Light-Duty Top
(Deduct 1/2 [13] from 'Y' Dim.)
_____ ZN D.C.C.I. w/ Polished Nickel Bronze Light-Duty Top
(Deduct 1/2 [13] from 'Y' Dim.)
_____ ZS D.C.C.I. w/ Polished Stainless Steel Extra Heavy-Duty Top
(Add 3/16 [5] to 'Y' Dim.)
SUFFIXES
_____ -AR Acid Resisting Epoxy Coated Finish
_____ -BP Bronze Plug
_____ -CF Carpet Flange Cover (ZB and ZN only)
_____ -CM Carpet Marker
_____ -DC Duresist Cover
_____ -DX Round ZB or ZN Top with Dex-o-tex Flange
(2, 3, 4 [51, 76, 102] Sizes only)
_____ -G Galvanized Cast Iron
_____ -HD Extra-Heavy-Duty Veneer Top (Add 1/8 [3] to 'Y' Dim.)
(ZB and ZN only)
_____ -K Anchor Flange
_____ -KC Anchor Flange w/ Clamping Collar
_____ -PC Protective Cover
_____ -SG Solid Gasketed Cover
_____ -SM Special Marking Stamped on Top
_____ -T Square Top
_____ -TC Neo-Loc Test Cap Gasket
(2, 3, 4 [51, 76, 102] NL Bottom Outlet Only)
_____ -TX Square Top Recessed for 1/8 [3] Tile
(ZB and ZN only)
_____ -VP Vandal-Proof Screws
_____ -X Round Top Recessed for 1/8 [3] Tile
(ZB or ZN only)
_____ -Z Round Top Recessed for 1-1/4 [32] Terrazzo
(ZB or ZN only)
ENGINEERING SPECIFICATION: ZURN Z1400
"Level-Trol" Adjustable floor cleanout, Dura-Coated cast iron body with gas and watertight ABS tapered thread plug and round
scoriated cast iron extra-heavy-duty secured top (Specify finish Z, ZB, ZN, ZS) adjustable to finished floor.
7 [3]
8 [203]
Neo-Loc
No-Hub
Inside Caulk
A-Pipe Size C E
Approx.
Wt. Lbs.
[kg.]
Dimension In Inches[mm]
6 [152]
4 [102]
3 [76]
2 [51]
8 [203]
6 [152]
4 [102]
3 [76]
2 [51]
6 [152]
4 [102]
3 [76]
2 [51]13.8 [6.3]
14 [6.4]
18.3 [8.3]
32.2 [14.6]
29.9 [13.6]
10.6 [4.8]
7.9 [3.6]
11.9 [5.4]
21.9 [9.9]
23.5 [10.7]
6-7/8 [175]
6-7/8 [175]
6-7/8 [175]
6-7/8 [175]
4-5/8 [117]
4-3/4 [121]
4-3/4 [121]
4-3/4 [121]
7-1/2 [191]
4-3/4 [121]
4-3/4 [121]
4-3/4 [121]
5-7/8 [149]
6-1/2 [165]
6-1/8 [156]
6-1/8 [156]
7-1/4 [184]
9-1/4 [235]
4-1/8 [105]
4-1/8 [105]
5-1/8 [130]
8-1/4 [210]
9-1/4 [235]
4-1/8 [105]
5-1/8 [130]
5-1/8 [130]
8-1/4 [210]
9-1/4 [235]
7.7 [3.5]
10.3 [4.7]
22.2 [10.1]
Rev. T
Date: 09/28/2017
C.N. No. 138018
Prod. | Dwg. No. Z1400

Appendix E Installation Inspection Photographs and Inspection Logs

Photograph 1: General view of gravel and sub-slab piping in Building 1.TKC-0082923 S. Tryon Street, Suite 100
Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)
AQUAIR II –WEST SIDE
13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINA
Photograph 2: Riser at interior column.
Photograph 3: Interior access monitoring point.
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)
Photograph 4: Exterior access monitoring point.TKC-008AQUAIR II –WEST SIDE
13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINA
Photographs 5: Extraction point in railspur.
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)
Photograph 6: Geotextile fabric layer between gravel and ABC stone layers.TKC-008AQUAIR II –WEST SIDE
13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINA
Photograph 7: General view of installed vapor barrier.
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)TKC-008AQUAIR II –WEST SIDE
13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINA
Photograph 8: Pour-N-Seal around utility bank in warehouse.
Photograph 10: Riser with guard along warehouse column.
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)TKC-008AQUAIR II –WEST SIDE
13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINA
Photograph 9: Vapor barrier sealed around extraction point and monitoring point in the guardhouse.
2923 S. Tryon Street, Suite 100
Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)TKC-008AQUAIR II –WEST SIDE
13300 SAM NEELY ROADCHARLOTTE, NORTH CAROLINA
Photograph 11: Monitoring point with guard along warehouse column.
Photograph 12: Turbine ventilator on rooftop extraction point discharge.
Category Example Criteria
Proper base layer (i.e., gravel, aerated flooring) and thickness
Proper placement, type, and pitch of VIMS vent piping
Proper placement, type, and pitch of monitoring points
Correct vapor barrier type
Proper vapor barrier overlap and seals around penetrations per
manufacturer instructions
Proper vapor barrier installation along vertical walls (e.g. retaining walls,
elevators, etc.)
Good condition of vapor barrier
Riser pipe material and fitting connections
Proper pitch towards sub-slab (gravity drain)
Appropriate VIMS labels
Correct fan/ventilator
Fan/ventilator operation
Proper fittings and protection (varmint screens, electrical covers, etc.)
Appropriate VIMS labels
Proper distance from roof intakes and parapets
Pilot test completed
Monitoring points finished and accessible MRV
Pilot Test / Checkout
AEM
AEM
AEM
AEM
AEM
AEM
AEM
Fan/Ventilator
AEM
AEM
AEM
MRV
Sub-Slab
Vapor Barrier
Vent Riser Piping
AEM
AEM
AEM
AEM
AEM
Vapor Intrusion Mitigation System - Inspection Checklist
Building/Area ID: Warehouse
Start Date and End Date: 5/16/2022 - 2/6/2023
H&H Construction Manager: Alexis McKenzie
Proper Installation
(Initial below)
Site Name and H&H Project #: AquAir II - West Side (TKC-008)
DEQ Brownfields ID: 18038-14-060
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Install
Completion Report/Appendices/VIMS Inspection Checklist\Warehouse
Category Example Criteria
Proper base layer (i.e., gravel, aerated flooring) and thickness
Proper placement, type, and pitch of VIMS vent piping
Proper placement, type, and pitch of monitoring points
Correct vapor barrier type
Proper vapor barrier overlap and seals around penetrations per
manufacturer instructions
Proper vapor barrier installation along vertical walls (e.g. retaining walls,
elevators, etc.)
Good condition of vapor barrier
Riser pipe material and fitting connections
Proper pitch towards sub-slab (gravity drain)
Appropriate VIMS labels
Correct fan/ventilator
Fan/ventilator operation
Proper fittings and protection (varmint screens, electrical covers, etc.)
Appropriate VIMS labels
Proper distance from roof intakes and parapets
Pilot test completed
Monitoring points finished and accessible
Pilot Test / Checkout
DAK
DAK
Vent Riser Piping
AEM
AEM
AEM
Fan/Ventilator
AEM
AEM
AEM
AEM
AEM
Proper Installation
(Initial below)
Sub-Slab
AEM
AEM
AEM
Vapor Barrier
AEM
AEM
AEM
AEM
Vapor Intrusion Mitigation System - Inspection Checklist
Site Name and H&H Project #: AquAir II - West Side (TKC-008)
DEQ Brownfields ID: 18038-14-060
Building/Area ID: Guardhouse
Start Date and End Date: 11/1/2022 - 2/6/2023
H&H Construction Manager: Alexis McKenzie
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Install
Completion Report/Appendices/VIMS Inspection Checklist\Guardhouse
Category Example Criteria
Proper base layer (i.e., gravel, aerated flooring) and thickness
Proper placement, type, and pitch of VIMS vent piping
Proper placement, type, and pitch of monitoring points
Correct vapor barrier type
Proper vapor barrier overlap and seals around penetrations per
manufacturer instructions
Proper vapor barrier installation along vertical walls (e.g. retaining walls,
elevators, etc.)
Good condition of vapor barrier
Riser pipe material and fitting connections
Proper pitch towards sub-slab (gravity drain)
Appropriate VIMS labels
Correct fan/ventilator
Fan/ventilator operation
Proper fittings and protection (varmint screens, electrical covers, etc.)
Appropriate VIMS labels
Proper distance from roof intakes and parapets
Pilot test completed
Monitoring points finished and accessible
N/A = Not Applicable
Pilot Test / Checkout
N/A
N/A
Vent Riser Piping
N/A
N/A
N/A
Fan/Ventilator
N/A
N/A
N/A
N/A
N/A
Proper Installation
(Initial below)
Sub-Slab
N/A
N/A
N/A
Vapor Barrier
AEM
AEM
N/A
AEM
Vapor Intrusion Mitigation System - Inspection Checklist
Site Name and H&H Project #: AquAir II - West Side (TKC-008)
DEQ Brownfields ID: 18038-14-060
Building/Area ID: Fire Pumphouse
Start Date and End Date: 11/18/2022
H&H Construction Manager: Alexis McKenzie
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Install
Completion Report/Appendices/VIMS Inspection Checklist\Pumphouse

Appendix F Field Forms

Appendix F-1
Summary of VIMS Influence Test - Test 1
AquAir II Brownfields Site - West Side
13300 Sam Neely Road
Charlotte, North Carolina
H&H Job No. TKC-008
Baseline 25 Minute Reading 55 minute reading
E-1 RP-145 0.000 -1.033 -1.058
E-5 Eagle Extreme 0.000 -2.136 -2.348
E-11 RP-145 0.000 -0.918 -0.983
E-12 RP-145 0.000 -1.123 -1.178
E-7 RP-145 0.000 -0.994 -1.074
E-3 RP-145 0.000 -0.773 -0.723
E-15 Eagle Extreme 0.000 -2.863 -2.954
E-22 Eagle Extreme 0.000 -2.196 -2.176
E-27 RP-145 0.000 -0.998 -1.045
E-23 RP-145 0.000 -1.218 -1.209
E-18 Eagle Extreme 0.000 -2.601 -2.590
E-24 RP-145 0.000 -1.059 -1.069
E-25 RP-145 0.000 -1.065 -1.114
E-30 Eagle Extreme 0.000 -2.506 -2.296
E-21 RP-145 0.000 -0.719 -0.696
MP-1 --0.000 -0.231 -0.241
MP-2 --0.000 -0.216 -0.230
MP-3 --0.000 -0.286 -0.281
MP-4 --0.000 -0.098 -0.112
MP-5 --0.000 -0.300 -0.298
MP-6 --0.000 -0.241 -0.240
MP-7 --0.000 -0.356 -0.351
MP-8 --0.000 -0.199 -0.238
MP-9 --0.000 -0.203 -0.206
MP-10 --0.000 -0.270 -0.273
MP-11 --0.000 -0.170 -0.175
MP-12 --0.000 -0.310 -0.307
MP-13 --0.000 -0.354 -0.345
MP-14 --0.000 -0.173 -0.174
Notes
in-WC = Inches of Water
February 6, 2023
Extraction Point
Monitoring Point
Fan Used
Test #1 (Warehouse Slab-On-Grade)
Vacuum Measurements
(in-WC)Point IDDate Point Type
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Field Docs/Pilot Testing_Feb. 6-7 2023/Pilot Test Data_02062023
4/21/2023
Appendix F-1 (Page 1 of 1)
Hart & Hickman, PC
Appendix F-2
Summary of VIMS Influence Test - Test 2
AquAir II Brownfields Site - West Side
13300 Sam Neely Road
Charlotte, North Carolina
H&H Job No. TKC-008
Baseline 15 Minute Reading 40 minute reading
E-9 Eagle Extreme 0.000 -2.121 -2.326
E-10 RP-145 0.000 -1.059 -1.076
E-2 Eagle Extreme 0.000 -2.303 -2.273
E-6 RP-145 0.000 -1.055 -0.985
E-13 RP-145 0.000 -1.035 -1.034
E-14 Eagle Extreme 0.000 -1.960 -2.111
E-4 RP-145 0.000 -1.180 -1.123
E-8 RP-145 0.000 -0.688 -0.769
E-16 RP-145 0.000 -1.506 -1.498
E-17 RP-145 0.000 -1.132 -1.117
E-28 RP-145 0.000 -1.093 -1.082
E-29 Eagle Extreme 0.000 -2.537 -2.586
E-19 RP-145 0.000 -0.964 -0.993
E-20 RP-145 0.000 -0.703 -0.718
E-26 Eagle Extreme 0.000 -3.701 -3.664
MP-1 --0.000 -0.230 -0.239
MP-2 --0.000 -0.280 -0.275
MP-3 --0.000 -0.268 -0.270
MP-4 --0.000 -0.120 -0.118
MP-5 --0.000 -0.290 -0.280
MP-6 --0.000 -0.296 -0.293
MP-7 --0.000 -0.262 -0.251
MP-8 --0.000 -0.100 -0.100
MP-9 --0.000 -0.074 -0.076
MP-10 --0.000 -0.107 -0.108
MP-11 --0.000 -0.065 -0.080
MP-12 --0.000 -0.255 -0.245
MP-13 --0.000 -0.180 -0.190
MP-14 --0.000 -0.050 -0.058
Notes
in-WC = Inches of Water
February 6, 2023
Extraction Point
Monitoring
Point
Test #2 (Warehouse Slab-On-Grade)
Date Point Type Point ID Fan Used
Vacuum Measurements
(in-WC)
https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Field Docs/Pilot Testing_Feb. 6-7 2023/Pilot Test Data_02062023
4/21/2023
Appendix F-2 (Page 1 of 1)
Hart & Hickman, PC
Appendix F-3Summary of VIMS Influence Test - Test 3 AquAir II Brownfields Site - West Side 13300 Sam Neely RoadCharlotte, North CarolinaH&H Job No. TKC-008Baseline 10 Minute Reading 25 minute readingE-31 Eagle Extreme 0.000-4.910>-4.00 *E-32 Eagle Extreme 0.000-4.878> -4.00 *E-33 Eagle Extreme 0.000-4.956>-4.00 *E-34 Eagle Extreme 0.000>-4.00 *>-4.00 *E-35 Eagle Extreme 0.000>-4.00 *>-4.00 *MP-2--0.0000.0000.000MP-3--0.0000.0000.000MP-6--0.0000.0000.000MP-4--0.0000.0000.000Notesin-WC = Inches of Water*Hi Pressure manometer battery died after measuring E-31 through E-33 on the first round. Low pressure manometer has a range of 0-4.000 in. wc.February 6, 2023Extraction PointMonitoring PointTest #3 (Warehouse Railspur)Date Point Type Point ID Fan UsedVacuum Measurements (in-WC)https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Field Docs/Pilot Testing_Feb. 6-7 2023/Pilot Test Data_020620234/21/2023Appendix F-3 (Page 1 of 1)Hart & Hickman, PC
Appendix F-4Summary of VIMS Influence Test - Test 4AquAir II Brownfields Site - West Side13300 Sam Neely RoadCharlotte, North CarolinaH&H Job No. TKC.008Baseline 5 Minute Reading 10 minute readingExtraction Point E-36 RP-145 0.000 -1.329 -1.366MP-15 -- 0.000 -0.369 -0.361MP-16 -- 0.000 -0.482 -0.480Notesin-WC - Inches of WaterFebruary 7, 2023Monitoring PointTest 4 (Guardhouse)Date Point Type Point ID Fan UsedVacuum Measurements (in-WC)https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/The Keith Corporation (TKC)/2021 New Building/VIMP/Field Docs/Pilot Testing_Feb. 6-7 2023/Pilot Test Data_020620234/21/2023Appendix F-4 (Page 1 of 1)Hart & Hickman, PC
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INDOOR AIR BUILDING SURVEY
and SAMPLING FORM
Site Name: ____________________________________ DSCAID#: ______________________
Preparer’s name: ________________________________ Date: __________________________
Preparer’s affiliation: ____________________________ Phone #: _______________________
Part I - Occupants
Building Address: ____________________________________________________________________
Property Contact: _______________________________ Owner / Renter / other: ______________
Contact’s Phone: home ( )__________ work ( )______________ cell ( )____________
# of Building occupants: Children under age 13 _____ Children age 13-18 ______ Adults _____
Part II – Building Characteristics
Building type:
Describe building: ________________________________________ Year constructed: _________
Sensitive population:2WKHU(specify): _______________
Number of floors below grade: ______
Number of floors at or above grade: ______
Depth of basement below grade surface: ______ ft. Basement size: _______ ft
2
Basement floor construction: 
Foundation walls:
Basement sump present?<HV1RSumppump?<HV1R
Rther (specify): ________________
other(specify)_______________B
Water in sump?<HV1R
Type of heating system (cKHFN all that apply):
hot air circulation hot air radiation wood steam radiation
heat pump hot water radiation kerosene heater electric baseboard
other (specify): ________________________
Type of ventilation system (cKHFN all that apply):
bathroom ventilation fans
outside air intake
central air conditioning mechanical fans
individual air conditioning units kitchen range hood fan
other (specify): _________________
Type of fuel utilized (cKHFN all that apply):
Natural gas electric  fuel oil  wood  coal  solar kerosene
Are the basement walls or floor sealed with waterproof paint or epoxy coatings? <HV1R
HD Charlotte BCR FDC NA
CMB 3/6/23
Hart & Hickman [phone]
13300 Sam Neely Road
704
0 0
Warehouse 2023
0
1
0 0
Commercial
None
Concrete
Poured Concrete
other (specify) _____________
Is there a whole house fan?<HV1R
Septic system? <HV<HV%XWQRWXVHG1R
Irrigation/private well? <HV<HV%XWQRWXVHG1R
Type of ground cover outside of building:BBBBBBBBBBBBBBBBBBBBB
Existing subsurface depressurization (radon) system in place?<HV1R 7\SHBBBBBBBBBBBB
Sub-slab vapor/moisture barrier in place? <HV1R
Type of barrier: ____________________________BBBBBBBBBBBBBBB
Part III - Outside Contaminant Sources
Other stationary sources nearby (gas stations, emission stacks, etc.): _____________________________
Heavy vehicular traffic nearby (or other mobile sources): ______________________________________
Part IV – Indoor Contaminant Sources
Identify all potential indoor sources found in the building (including attached garages), the location of
the source (floor and room), and whether the item was removed from the building 48 hours prior to
indoor air sampling event. Any ventilation implemented after removal of the items should be completed
at least 24 hours prior to the commencement of the indoor air sampling event.
Potential Sources Location(s)Removed
(Yes / No / NA)
Gasoline storage cans
Gas-powered equipment
Kerosene storage cans
Paints / thinners / strippers
Cleaning solvents
Oven cleaners
Carpet / upholstery cleaners
Other house cleaning products
Moth balls
Polishes / waxes
Insecticides
Furniture / floor polish
Nail polish / polish remover
Hairspray
Cologne / perfume
Air fresheners
Fuel tank (inside building)
Wood stove or fireplace
New furniture / upholstery
New carpeting / flooring
Hobbies - glues, paints, etc.
None
Construction equipment inside and out.
N/A
Outside office spaces in the warehouse area.No
N/A
Behr Marquee paints in office spaces and being painted.No
Denatured Alcohol in office spaces.No
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
New flooring being laid. Tile adhesive cans.
Drywall joint compound.No
N/A
N/A
No
Asphalt
Passive
Raven VaporBlock 20
Part V – Miscellaneous Items
Do any occupants of the building smoke?<HV1RHow often? ______________
Last time someone smoked in the building? ____________ hours days ago
Does the building have an attached garage directly connected to living space? <HV1R
If so, is a car usually parked in the garage? <HV1R
Are gas-powered equipment or cans of gasoline/fuels stored in the garage?<HV1R
Do the occupants of the building have their clothes dry cleaned? <HV1R
If yes, how often?:HHNO\0RQWKO\7LPHVSHU\HDU
Do any of the occupants use solvents in work?<HV1R
If yes, what types of solvents are used? _______________________________________
If yes, are their clothes washed at work?<HV1R
+DYHDQ\SHVWLFLGHVKHUELFLGHVEHHQDSSOLHGDURXQGWKHEXLOGLQJRULQWKH\DUG"<HV1R
If so, when and which chemicals? _________________________________________________
Has there ever been a fire in the building?<HV1R If yes, when? _____________
Has painting or staining been done in the building in the last 6 months?
Yes  No
If yes, when __________________ and where? ____________________________
Part VI – Sampling Information
Sample Technician: ____________________________ Phone number:) _______ - __________
Sample SourceFKHFNDOOWKDWDSSO\
,QGRRU$LU&UDZOVSDFH$LU6XE6ODE1HDU6ODE6RLO*DV([WHULRU6RLO*DV
Sampler TypeFKHFNDOOWKDWDSSO\
7HGODU%DJ6RUEHQW6WDLQOHVV6WHHO&DQLVWHUOther (specify): _________________
Analytical Method:BBBBBBBBBBBBBBBBB2ther: _____________ Cert. Laboratory:BBBBBBBBBBBBB
Sample locations (floor, room):BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
Field ID # _____ - ________________________Field ID # _ _B-__________________________
Were “Instructions for Occupants” followed?
,IQRWGHVFULEHPRGLILFDWLRQVBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB
Concurrent All throughout.
CMB 0007586704
1&6L
SGS
IAS-1 Room A127 - Galley
Building is under construction.
Office spaces on main floor.
Room A106 ___IAS-3
IASBBB-BKGField ID # IAS-2 Room A128BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB)LHOG,'BB WestBBBBBBBBBBBBBcorner outside buildingBBBBBBBBBBBBBBB
TO-15
N/A
Provide Drawing of Sample Location(s) in Building
Part VII - Meteorological Conditions
Was there significant precipitation within 12 hours prior to (or during) the sampling event?Yes No
Describe the general weather conditions: _________________________________________________
_____________________________________________________________________________________
Part VIII – General Observations
Provide any information that may be pertinent to the sampling event and may assist in the data
interpretation process (e.g., observed that drycleaner operated with door or windows propped open for
ventilation).
(Adapted from the NJDEP Vapor Intrusion Guidance, October 2005)
Low 45F, high 74F, sunny, moderate wind.
Building is under construction with gas generators and vehicles in the warehouse area. Office spaces were being
painted during sampling. Drop ceilings in the office space had not been installed yet so the rooms that contained IA
samples were sealed with plastic over the door and ceiling so air could not connect with the warehouse area.
&Žƌŵ/^Ͳϭ,QGRRU$LU6DPSOLQJ)LHOG)RUP3URMHFW1RBBBBBBBBBBBBBBBBBBB 6DPSOHUBBBBBBBBBBBBBBBBBBBBBB :HDWKHUBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB'DWH3URSRVHG6DPSOLQJ'XUDWLRQ7LPH&DQLVWHU3UHVVXUH'LIIHUHQWLDO3UHVVXUH2XWGRRU7HPSHUDWXUH2XWGRRU+XPLGLW\,QGRRU7HPSHUDWXUH,QGRRU+XPLGLW\PPGG\\ +RXUV KU +J+2R)R)^͗%HJLQQLQJ͗0LGGOHZ͗(QG^͗%HJLQQLQJ͗0LGGOHZ͗(QG^͗%HJLQQLQJ͗0LGGOHZ͗(QG^͗%HJLQQLQJ͗0LGGOHZ͗(QG^͗%HJLQQLQJ͗0LGGOHZ͗(QG^͗%HJLQQLQJ͗0LGGOHZ͗(QG6 VDPSOH,'& FDQLVWHU,'5 UHJXODWRU,' 1RWHQHJDWLYHGLIIHUHQWLDOSUHVVXUHLQGLFDWHVWKDWLQGRRUSUHVVXUHZDVORZHUWKDQSUHVVXUHRXWGRRUV/DVWXSGDWHG+J LQFKHVRIPHUFXU\+2 LQFKHVRIZDWHUFROXPQ7LPH(671RWHVBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB3UHFLSLWDWLRQLQFKHVBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB%DURPHWULF3UHVVXUH+JBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB:LQG'LUHFWLRQBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB:LQG6SHHGPSKBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗,QGRRU3DUDPHWHUV6DPSOLQJ3HULRG6DPSOLQJ,QIRUPDWLRQ 2XWGRRU3DUDPHWHUV6DPSOH,'^ŝnjĞ͗&ůŽǁZĂƚĞ͗^ŝnjĞ͗&ůŽǁZĂƚĞ͗^͗ͰDĂƐƚĞƌdĞŵƉůĂƚĞƐͰ&ŽƌŵƐͲϮϬϮϮ&ŽƌŵƐͰsĂƉŽƌ^ĂŵƉůŝŶŐ&ŽƌŵƐͺsϲ͘Ϯ͘ƉĚĨ/ŶĚŽŽƌŝƌ^ĂŵƉůŝŶŐ&ŝĞůĚ&Žƌŵ,ĂƌƚΘ,ŝĐŬŵĂŶ͕WTKC.008 CMB45F, high 74F, sunnyIAS-10745 -29 0.000 45 87 50 856 LA7373/6/2381200 -18 0.000 68 46 52 7410900.75 L/hr1545 -7 0.000 72 45 57 64IAS-20750 -32 0.000 45 87 50 856 LA18693/6/2381200 -18 0.000 68 46 52 7410180.75 L/hr1550 -5 0.000 72 45 57 64IAS-30755 -30 0.000 45 87 50 856 LA21553/6/2381205 -17 0.000 68 46 52 7413040.75 L/hr1555 -5 0.000 72 45 57 64IAS-BKG0805 -30 -- 45 87 NA NA6 LA20553/6/2381205 -18 -- 68 46 NA NA10830.75 L/hr1605 -6 -- 72 45 NA NAIAS-DUP0745 -30 0.000 45 87 50 856 LA8803/6/2381200 -18 0.000 68 46 52 740.75 L/hr12861545 -6 0.000 72 45 57 640800 1210 1600Duplicate is from IAS-1 location.0.00 0.00 0.00Duplicate has its own regulator going to30.0 30.0same T-bar as parent sample.30.0to E to NE to NE2710

Appendix G Laboratory Analytical Reports

03/24/23
Technical Report for
Hart & Hickman
TKC.008, 13300 Sam Neely Road, Charlotte, NC
TKC-008
SGS Job Number: JD61814
Sampling Dates: 03/06/23 - 03/07/23
Report to:
Hart & Hickman
2923 South Tyron Street Suite 101
Charlotte, NC 28203
[e-mail]; [e-mail]
ATTN: Caleb Brehm
Total number of pages in report:
Certifications: NJ(12129), NY(10983), CA, CT, FL, IL, IN, KS, KY, LA, MA, MD, ME, MN, NC,
OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA(68-00408), RI, SC, TX, UT, VA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 2235 Route 130 • Dayton, NJ 08810 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Kelly Ramos 732-329-0200
David Chastain
General Manager
Dayton, NJ 03/24/23
Reissue #1
e-Hardcopy 2.0
Automated Report
103
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 103
JD61814
-

March 24, 2023

Mr. Caleb Brehm
Hart & Hickman
2923 South Tyron Street Suite 101
Charlotte, NC 28203

RE: SGS – Dayton, Job # JD61814 – Reissues

Dear Mr. Brehm,

The final report for SGS job number JD61814 has been edited to reflect corrections to the results.
These edits have been incorporated into the revised report which is attached.

Specifically, the Methyl Ethyl Ketone has been added to JD61814-10 as client’s original requested.
The attached revised report incorporates these revisions.

SGS apologizes for this occurrence and for any inconvenience this situation may have caused. Please
contact me if I can be of further assistance in this matter.

Sincerely,
Report Department
SGS North America Inc.

SGS North America Inc. Mid-Atlantic 2235 US Highway 130 Dayton, NJ 08810, USA t [phone] www.sgs.com
Member of the SGS Group (SGS SA)
2 of 103
JD61814
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................6
Section 3: Sample Results ........................................................................................................15
3.1: JD61814-1: MP-1 .........................................................................................................16
3.2: JD61814-2: MP-2 .........................................................................................................18
3.3: JD61814-3: MP-3 .........................................................................................................20
3.4: JD61814-4: MP-4 .........................................................................................................22
3.5: JD61814-5: MP-5 .........................................................................................................24
3.6: JD61814-6: MP-6 .........................................................................................................26
3.7: JD61814-7: MP-7 .........................................................................................................28
3.8: JD61814-8: MP-8 .........................................................................................................30
3.9: JD61814-9: MP-9 .........................................................................................................32
3.10: JD61814-10: MP-10 ...................................................................................................34
3.11: JD61814-11: MP-11 ....................................................................................................36
3.12: JD61814-12: MP-12 ...................................................................................................38
3.13: JD61814-13: MP-13 ...................................................................................................40
3.14: JD61814-14: MP-14 ...................................................................................................42
3.15: JD61814-15: MP-15 ...................................................................................................44
3.16: JD61814-16: MP-DUP ................................................................................................46
Section 4: Misc. Forms ............................................................................................................48
4.1: Chain of Custody ...........................................................................................................49
4.2: Summa Canister and Flow Controller Log ....................................................................53
Section 5: MS Volatiles - QC Data Summaries .....................................................................55
5.1: Method Blank Summary ................................................................................................56
5.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................68
5.3: Duplicate Summary .......................................................................................................79
5.4: Summa Cleaning Certification ......................................................................................84
5.5: Instrument Performance Checks (BFB) .........................................................................92
5.6: Surrogate Recovery Summaries .....................................................................................102 123453 of 103
JD61814
SGS North America Inc.
Sample Summary
Hart & Hickman
Job No:JD61814
TKC.008, 13300 Sam Neely Road, Charlotte, NC
Project No: TKC-008
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
JD61814-1 03/07/23 11:29 CB 03/09/23 AIR Soil Vapor Comp.MP-1
JD61814-2 03/06/23 11:38 CB 03/09/23 AIR Soil Vapor Comp.MP-2
JD61814-3 03/07/23 09:05 CB 03/09/23 AIR Soil Vapor Comp.MP-3
JD61814-4 03/06/23 10:55 CB 03/09/23 AIR Soil Vapor Comp.MP-4
JD61814-5 03/07/23 10:49 CB 03/09/23 AIR Soil Vapor Comp.MP-5
JD61814-6 03/07/23 08:30 CB 03/09/23 AIR Soil Vapor Comp.MP-6
JD61814-7 03/07/23 09:38 CB 03/09/23 AIR Soil Vapor Comp.MP-7
JD61814-8 03/06/23 13:18 CB 03/09/23 AIR Soil Vapor Comp.MP-8
JD61814-9 03/07/23 12:35 CB 03/09/23 AIR Soil Vapor Comp.MP-9
JD61814-10 03/07/23 12:07 CB 03/09/23 AIR Soil Vapor Comp.MP-10
JD61814-11 03/06/23 09:06 CB 03/09/23 AIR Soil Vapor Comp.MP-11
JD61814-12 03/07/23 10:14 CB 03/09/23 AIR Soil Vapor Comp.MP-12
4 of 103
JD618141
SGS North America Inc.
Sample Summary
(continued)
Hart & Hickman
Job No:JD61814
TKC.008, 13300 Sam Neely Road, Charlotte, NC
Project No: TKC-008
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
JD61814-13 03/06/23 09:44 CB 03/09/23 AIR Soil Vapor Comp.MP-13
JD61814-14 03/06/23 10:20 CB 03/09/23 AIR Soil Vapor Comp.MP-14
JD61814-15 03/06/23 13:57 CB 03/09/23 AIR Soil Vapor Comp.MP-15
JD61814-16 03/07/23 10:49 CB 03/09/23 AIR Soil Vapor Comp.MP-DUP
5 of 103
JD618141
Summary of Hits Page 1 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD61814-1 MP-1
Acetone (2-Propanone)9.4 0.80 0.58 ppbv TO-15
Chloromethane 0.53 J 0.80 0.36 ppbv TO-15
Dichlorodifluoromethane 0.41 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 4.7 0.80 0.42 ppbv TO-15
Heptane 0.46 J 0.80 0.37 ppbv TO-15
Isopropyl Alcohol 1.3 0.80 0.56 ppbv TO-15
Methyl ethyl ketone 1.6 0.80 0.44 ppbv TO-15
Tetrahydrofuran 67.7 0.80 0.36 ppbv TO-15
Toluene 0.70 J 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)22 1.9 1.4 ug/m3 TO-15
Chloromethane 1.1 J 1.7 0.74 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 17 2.9 1.5 ug/m3 TO-15
Heptane 1.9 J 3.3 1.5 ug/m3 TO-15
Isopropyl Alcohol 3.2 2.0 1.4 ug/m3 TO-15
Methyl ethyl ketone 4.7 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 200 2.4 1.1 ug/m3 TO-15
Toluene 2.6 J 3.0 0.87 ug/m3 TO-15
JD61814-2 MP-2
Acetone (2-Propanone)26.7 0.80 0.58 ppbv TO-15
Benzene 22.8 0.80 0.25 ppbv TO-15
Dichlorodifluoromethane 0.41 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 1.4 0.80 0.42 ppbv TO-15
Hexane 0.54 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 0.94 0.80 0.56 ppbv TO-15
Methylene chloride 1.3 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 11.8 0.80 0.44 ppbv TO-15
Propylene 1.6 J 2.0 0.57 ppbv TO-15
Tetrahydrofuran 56.4 0.80 0.36 ppbv TO-15
Toluene 0.80 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)63.4 1.9 1.4 ug/m3 TO-15
Benzene 72.8 2.6 0.80 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 5.0 2.9 1.5 ug/m3 TO-15
Hexane 1.9 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 2.3 2.0 1.4 ug/m3 TO-15
Methylene chloride 4.5 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 34.8 2.4 1.3 ug/m3 TO-15
Propylene 2.7 J 3.4 0.98 ug/m3 TO-15
Tetrahydrofuran 166 2.4 1.1 ug/m3 TO-15
Toluene 3.0 3.0 0.87 ug/m3 TO-15
6 of 103
JD618142
Summary of Hits Page 2 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD61814-3 MP-3
Acetone (2-Propanone)17.1 0.80 0.58 ppbv TO-15
Benzene 0.63 J 0.80 0.25 ppbv TO-15
Carbon disulfide 0.68 J 0.80 0.18 ppbv TO-15
Chloromethane 0.45 J 0.80 0.36 ppbv TO-15
Dichlorodifluoromethane 0.41 J 0.80 0.13 ppbv TO-15
Ethylbenzene 0.44 J 0.80 0.24 ppbv TO-15
Ethyl Acetate 40.7 0.80 0.42 ppbv TO-15
Isopropyl Alcohol 5.5 0.80 0.56 ppbv TO-15
Methylene chloride 1.1 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 8.1 0.80 0.44 ppbv TO-15
Tetrachloroethylene 0.21 0.16 0.056 ppbv TO-15
Tetrahydrofuran 37.7 0.80 0.36 ppbv TO-15
Toluene 2.8 0.80 0.23 ppbv TO-15
m,p-Xylene 1.3 0.80 0.56 ppbv TO-15
o-Xylene 0.40 J 0.80 0.31 ppbv TO-15
Xylenes (total)1.7 0.80 0.31 ppbv TO-15
Acetone (2-Propanone)40.6 1.9 1.4 ug/m3 TO-15
Benzene 2.0 J 2.6 0.80 ug/m3 TO-15
Carbon disulfide 2.1 J 2.5 0.56 ug/m3 TO-15
Chloromethane 0.93 J 1.7 0.74 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Ethylbenzene 1.9 J 3.5 1.0 ug/m3 TO-15
Ethyl Acetate 146 2.9 1.5 ug/m3 TO-15
Isopropyl Alcohol 14 2.0 1.4 ug/m3 TO-15
Methylene chloride 3.8 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 24 2.4 1.3 ug/m3 TO-15
Tetrachloroethylene 1.4 1.1 0.38 ug/m3 TO-15
Tetrahydrofuran 111 2.4 1.1 ug/m3 TO-15
Toluene 11 3.0 0.87 ug/m3 TO-15
m,p-Xylene 5.6 3.5 2.4 ug/m3 TO-15
o-Xylene 1.7 J 3.5 1.3 ug/m3 TO-15
Xylenes (total)7.4 3.5 1.3 ug/m3 TO-15
JD61814-4 MP-4
Acetone (2-Propanone)19.8 0.80 0.58 ppbv TO-15
Carbon disulfide 0.48 J 0.80 0.18 ppbv TO-15
Dichlorodifluoromethane 0.44 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 7.3 0.80 0.42 ppbv TO-15
Heptane 0.38 J 0.80 0.37 ppbv TO-15
Isopropyl Alcohol 1.0 0.80 0.56 ppbv TO-15
Methyl ethyl ketone 9.6 0.80 0.44 ppbv TO-15
7 of 103
JD618142
Summary of Hits Page 3 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Tetrahydrofuran 31.2 0.80 0.36 ppbv TO-15
Toluene 0.51 J 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)47.0 1.9 1.4 ug/m3 TO-15
Carbon disulfide 1.5 J 2.5 0.56 ug/m3 TO-15
Dichlorodifluoromethane 2.2 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 26 2.9 1.5 ug/m3 TO-15
Heptane 1.6 J 3.3 1.5 ug/m3 TO-15
Isopropyl Alcohol 2.5 2.0 1.4 ug/m3 TO-15
Methyl ethyl ketone 28 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 92.0 2.4 1.1 ug/m3 TO-15
Toluene 1.9 J 3.0 0.87 ug/m3 TO-15
JD61814-5 MP-5
Acetone (2-Propanone)35.2 0.80 0.58 ppbv TO-15
Benzene 71.7 0.80 0.25 ppbv TO-15
Carbon disulfide 0.41 J 0.80 0.18 ppbv TO-15
Chloromethane 0.91 0.80 0.36 ppbv TO-15
Dichlorodifluoromethane 0.40 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 7.3 0.80 0.42 ppbv TO-15
Heptane 0.69 J 0.80 0.37 ppbv TO-15
Hexane 0.53 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 1.6 0.80 0.56 ppbv TO-15
Methyl ethyl ketone 15.1 0.80 0.44 ppbv TO-15
Tetrahydrofuran 855 8.0 3.6 ppbv TO-15
Toluene 4.1 0.80 0.23 ppbv TO-15
m,p-Xylene 0.78 J 0.80 0.56 ppbv TO-15
Xylenes (total)0.78 J 0.80 0.31 ppbv TO-15
Acetone (2-Propanone)83.6 1.9 1.4 ug/m3 TO-15
Benzene 229 2.6 0.80 ug/m3 TO-15
Carbon disulfide 1.3 J 2.5 0.56 ug/m3 TO-15
Chloromethane 1.9 1.7 0.74 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 26 2.9 1.5 ug/m3 TO-15
Heptane 2.8 J 3.3 1.5 ug/m3 TO-15
Hexane 1.9 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 3.9 2.0 1.4 ug/m3 TO-15
Methyl ethyl ketone 44.5 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 2520 24 11 ug/m3 TO-15
Toluene 15 3.0 0.87 ug/m3 TO-15
m,p-Xylene 3.4 J 3.5 2.4 ug/m3 TO-15
Xylenes (total)3.4 J 3.5 1.3 ug/m3 TO-15
8 of 103
JD618142
Summary of Hits Page 4 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD61814-6 MP-6
Acetone (2-Propanone)181 1.6 1.2 ppbv TO-15
Benzene 53.6 1.6 0.50 ppbv TO-15
Ethyl Acetate 12.0 1.6 0.83 ppbv TO-15
Isopropyl Alcohol 2.5 1.6 1.1 ppbv TO-15
Methylene chloride 1.5 J 1.6 0.45 ppbv TO-15
Methyl ethyl ketone 124 1.6 0.88 ppbv TO-15
Tetrahydrofuran 374 1.6 0.72 ppbv TO-15
Toluene 3.0 1.6 0.46 ppbv TO-15
Acetone (2-Propanone)430 3.8 2.9 ug/m3 TO-15
Benzene 171 5.1 1.6 ug/m3 TO-15
Ethyl Acetate 43.2 5.8 3.0 ug/m3 TO-15
Isopropyl Alcohol 6.1 3.9 2.7 ug/m3 TO-15
Methylene chloride 5.2 J 5.6 1.6 ug/m3 TO-15
Methyl ethyl ketone 366 4.7 2.6 ug/m3 TO-15
Tetrahydrofuran 1100 4.7 2.1 ug/m3 TO-15
Toluene 11 6.0 1.7 ug/m3 TO-15
JD61814-7 MP-7
Acetone (2-Propanone)127 0.80 0.58 ppbv TO-15
Benzene 0.87 0.80 0.25 ppbv TO-15
Carbon disulfide 0.42 J 0.80 0.18 ppbv TO-15
Chloromethane 0.56 J 0.80 0.36 ppbv TO-15
Cyclohexane 0.47 J 0.80 0.44 ppbv TO-15
Dichlorodifluoromethane 0.42 J 0.80 0.13 ppbv TO-15
Ethylbenzene 0.51 J 0.80 0.24 ppbv TO-15
Ethyl Acetate 53.4 0.80 0.42 ppbv TO-15
Isopropyl Alcohol 5.9 0.80 0.56 ppbv TO-15
Methylene chloride 0.83 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 92.4 0.80 0.44 ppbv TO-15
Tetrahydrofuran 258 1.6 0.72 ppbv TO-15
Toluene 3.2 0.80 0.23 ppbv TO-15
m,p-Xylene 1.6 0.80 0.56 ppbv TO-15
o-Xylene 0.45 J 0.80 0.31 ppbv TO-15
Xylenes (total)2.0 0.80 0.31 ppbv TO-15
Acetone (2-Propanone)302 1.9 1.4 ug/m3 TO-15
Benzene 2.8 2.6 0.80 ug/m3 TO-15
Carbon disulfide 1.3 J 2.5 0.56 ug/m3 TO-15
Chloromethane 1.2 J 1.7 0.74 ug/m3 TO-15
Cyclohexane 1.6 J 2.8 1.5 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Ethylbenzene 2.2 J 3.5 1.0 ug/m3 TO-15
Ethyl Acetate 192 2.9 1.5 ug/m3 TO-15
9 of 103
JD618142
Summary of Hits Page 5 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Isopropyl Alcohol 15 2.0 1.4 ug/m3 TO-15
Methylene chloride 2.9 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 273 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 761 4.7 2.1 ug/m3 TO-15
Toluene 12 3.0 0.87 ug/m3 TO-15
m,p-Xylene 6.9 3.5 2.4 ug/m3 TO-15
o-Xylene 2.0 J 3.5 1.3 ug/m3 TO-15
Xylenes (total)8.7 3.5 1.3 ug/m3 TO-15
JD61814-8 MP-8
Acetone (2-Propanone)51.0 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.41 J 0.80 0.13 ppbv TO-15
Methyl ethyl ketone 14.7 0.80 0.44 ppbv TO-15
Tetrahydrofuran 71.6 0.80 0.36 ppbv TO-15
Acetone (2-Propanone)121 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Methyl ethyl ketone 43.4 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 211 2.4 1.1 ug/m3 TO-15
JD61814-9 MP-9
Acetone (2-Propanone)177 0.80 0.58 ppbv TO-15
Chloromethane 0.92 0.80 0.36 ppbv TO-15
Dichlorodifluoromethane 0.40 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 8.4 0.80 0.42 ppbv TO-15
Hexane 0.47 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 2.3 0.80 0.56 ppbv TO-15
Methylene chloride 1.6 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 136 8.0 4.4 ppbv TO-15
Tetrahydrofuran 488 8.0 3.6 ppbv TO-15
Toluene 0.55 J 0.80 0.23 ppbv TO-15
m,p-Xylene 0.61 J 0.80 0.56 ppbv TO-15
Xylenes (total)0.61 J 0.80 0.31 ppbv TO-15
Acetone (2-Propanone)420 1.9 1.4 ug/m3 TO-15
Chloromethane 1.9 1.7 0.74 ug/m3 TO-15
Dichlorodifluoromethane 2.0 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 30 2.9 1.5 ug/m3 TO-15
Hexane 1.7 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 5.7 2.0 1.4 ug/m3 TO-15
Methylene chloride 5.6 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 401 24 13 ug/m3 TO-15
Tetrahydrofuran 1440 24 11 ug/m3 TO-15
Toluene 2.1 J 3.0 0.87 ug/m3 TO-15
m,p-Xylene 2.6 J 3.5 2.4 ug/m3 TO-15
10 of 103
JD618142
Summary of Hits Page 6 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Xylenes (total)2.6 J 3.5 1.3 ug/m3 TO-15
JD61814-10 MP-10
Acetone (2-Propanone) a 6650 100 74 ppbv TO-15
Isopropyl Alcohol 17.9 16 11 ppbv TO-15
Methyl ethyl ketone a 3600 100 56 ppbv TO-15
Methyl Tert Butyl Ether 36.1 16 6.4 ppbv TO-15
Tetrahydrofuran a 13700 100 46 ppbv TO-15
Acetone (2-Propanone) a 15800 240 180 ug/m3 TO-15
Isopropyl Alcohol 44.0 39 27 ug/m3 TO-15
Methyl ethyl ketone a 10600 290 170 ug/m3 TO-15
Methyl Tert Butyl Ether 130 58 23 ug/m3 TO-15
Tetrahydrofuran a 40400 290 140 ug/m3 TO-15
JD61814-11 MP-11
Acetone (2-Propanone)592 3.2 2.3 ppbv TO-15
Ethyl Acetate 5.2 3.2 1.7 ppbv TO-15
Isopropyl Alcohol 7.4 3.2 2.3 ppbv TO-15
Methyl ethyl ketone 363 3.2 1.8 ppbv TO-15
Tetrahydrofuran 1110 8.0 3.6 ppbv TO-15
Toluene 2.4 J 3.2 0.91 ppbv TO-15
Acetone (2-Propanone)1410 7.6 5.5 ug/m3 TO-15
Ethyl Acetate 19 12 6.1 ug/m3 TO-15
Isopropyl Alcohol 18 7.9 5.7 ug/m3 TO-15
Methyl ethyl ketone 1070 9.4 5.3 ug/m3 TO-15
Tetrahydrofuran 3270 24 11 ug/m3 TO-15
Toluene 9.0 J 12 3.4 ug/m3 TO-15
JD61814-12 MP-12
Acetone (2-Propanone)36.3 0.80 0.58 ppbv TO-15
1,3-Butadiene 0.79 J 0.80 0.34 ppbv TO-15
Benzene 1.1 0.80 0.25 ppbv TO-15
Dichlorodifluoromethane 0.45 J 0.80 0.13 ppbv TO-15
Ethylbenzene 1.4 0.80 0.24 ppbv TO-15
Ethyl Acetate 1.9 0.80 0.42 ppbv TO-15
Heptane 1.6 0.80 0.37 ppbv TO-15
Hexane 0.69 J 0.80 0.45 ppbv TO-15
Isopropyl Alcohol 1.0 0.80 0.56 ppbv TO-15
Methyl ethyl ketone 20.9 0.80 0.44 ppbv TO-15
Tetrahydrofuran 80.9 0.80 0.36 ppbv TO-15
Toluene 5.0 0.80 0.23 ppbv TO-15
m,p-Xylene 4.4 0.80 0.56 ppbv TO-15
11 of 103
JD618142
Summary of Hits Page 7 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
o-Xylene 1.4 0.80 0.31 ppbv TO-15
Xylenes (total)5.8 0.80 0.31 ppbv TO-15
Acetone (2-Propanone)86.2 1.9 1.4 ug/m3 TO-15
1,3-Butadiene 1.7 J 1.8 0.75 ug/m3 TO-15
Benzene 3.5 2.6 0.80 ug/m3 TO-15
Dichlorodifluoromethane 2.2 J 4.0 0.64 ug/m3 TO-15
Ethylbenzene 6.1 3.5 1.0 ug/m3 TO-15
Ethyl Acetate 6.8 2.9 1.5 ug/m3 TO-15
Heptane 6.6 3.3 1.5 ug/m3 TO-15
Hexane 2.4 J 2.8 1.6 ug/m3 TO-15
Isopropyl Alcohol 2.5 2.0 1.4 ug/m3 TO-15
Methyl ethyl ketone 61.6 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 239 2.4 1.1 ug/m3 TO-15
Toluene 19 3.0 0.87 ug/m3 TO-15
m,p-Xylene 19 3.5 2.4 ug/m3 TO-15
o-Xylene 6.1 3.5 1.3 ug/m3 TO-15
Xylenes (total)25 3.5 1.3 ug/m3 TO-15
JD61814-13 MP-13
Acetone (2-Propanone)92.9 0.80 0.58 ppbv TO-15
Benzene 0.69 J 0.80 0.25 ppbv TO-15
Cyclohexane 0.60 J 0.80 0.44 ppbv TO-15
Dichlorodifluoromethane 0.43 J 0.80 0.13 ppbv TO-15
Ethylbenzene 0.53 J 0.80 0.24 ppbv TO-15
Ethyl Acetate 55.7 0.80 0.42 ppbv TO-15
Isopropyl Alcohol 6.6 0.80 0.56 ppbv TO-15
Methylene chloride 0.88 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 49.1 0.80 0.44 ppbv TO-15
Tetrahydrofuran 289 4.0 1.8 ppbv TO-15
Toluene 3.2 0.80 0.23 ppbv TO-15
m,p-Xylene 1.6 0.80 0.56 ppbv TO-15
o-Xylene 0.46 J 0.80 0.31 ppbv TO-15
Xylenes (total)2.1 0.80 0.31 ppbv TO-15
Acetone (2-Propanone)221 1.9 1.4 ug/m3 TO-15
Benzene 2.2 J 2.6 0.80 ug/m3 TO-15
Cyclohexane 2.1 J 2.8 1.5 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Ethylbenzene 2.3 J 3.5 1.0 ug/m3 TO-15
Ethyl Acetate 200 2.9 1.5 ug/m3 TO-15
Isopropyl Alcohol 16 2.0 1.4 ug/m3 TO-15
Methylene chloride 3.1 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 145 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 852 12 5.3 ug/m3 TO-15
Toluene 12 3.0 0.87 ug/m3 TO-15
12 of 103
JD618142
Summary of Hits Page 8 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
m,p-Xylene 6.9 3.5 2.4 ug/m3 TO-15
o-Xylene 2.0 J 3.5 1.3 ug/m3 TO-15
Xylenes (total)9.1 3.5 1.3 ug/m3 TO-15
JD61814-14 MP-14
Acetone (2-Propanone)74.5 0.80 0.58 ppbv TO-15
Dichlorodifluoromethane 0.43 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 12.9 0.80 0.42 ppbv TO-15
Isopropyl Alcohol 4.4 0.80 0.56 ppbv TO-15
Methylene chloride 0.94 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 48.0 0.80 0.44 ppbv TO-15
Tetrahydrofuran 74.7 1.6 0.72 ppbv TO-15
Toluene 0.61 J 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)177 1.9 1.4 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 46.4 2.9 1.5 ug/m3 TO-15
Isopropyl Alcohol 11 2.0 1.4 ug/m3 TO-15
Methylene chloride 3.3 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 142 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 220 4.7 2.1 ug/m3 TO-15
Toluene 2.3 J 3.0 0.87 ug/m3 TO-15
JD61814-15 MP-15
Acetone (2-Propanone)37.4 0.80 0.58 ppbv TO-15
Benzene 0.50 J 0.80 0.25 ppbv TO-15
Cyclohexane 0.97 0.80 0.44 ppbv TO-15
Dichlorodifluoromethane 0.44 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 66.2 0.80 0.42 ppbv TO-15
Heptane 0.64 J 0.80 0.37 ppbv TO-15
Isopropyl Alcohol 1.9 0.80 0.56 ppbv TO-15
Methylene chloride 1.8 0.80 0.22 ppbv TO-15
Methyl ethyl ketone 13.9 0.80 0.44 ppbv TO-15
Tetrahydrofuran 46.5 0.80 0.36 ppbv TO-15
Toluene 2.1 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)88.8 1.9 1.4 ug/m3 TO-15
Benzene 1.6 J 2.6 0.80 ug/m3 TO-15
Cyclohexane 3.3 2.8 1.5 ug/m3 TO-15
Dichlorodifluoromethane 2.2 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 238 2.9 1.5 ug/m3 TO-15
Heptane 2.6 J 3.3 1.5 ug/m3 TO-15
Isopropyl Alcohol 4.7 2.0 1.4 ug/m3 TO-15
Methylene chloride 6.3 2.8 0.76 ug/m3 TO-15
Methyl ethyl ketone 41.0 2.4 1.3 ug/m3 TO-15
13 of 103
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Summary of Hits Page 9 of 9
Job Number:JD61814
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23 thru 03/07/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Tetrahydrofuran 137 2.4 1.1 ug/m3 TO-15
Toluene 7.9 3.0 0.87 ug/m3 TO-15
JD61814-16 MP-DUP
Acetone (2-Propanone)28.6 0.80 0.58 ppbv TO-15
Benzene 0.52 J 0.80 0.25 ppbv TO-15
Carbon disulfide 0.43 J 0.80 0.18 ppbv TO-15
Chloromethane 0.98 0.80 0.36 ppbv TO-15
Dichlorodifluoromethane 0.43 J 0.80 0.13 ppbv TO-15
Ethyl Acetate 7.0 0.80 0.42 ppbv TO-15
Isopropyl Alcohol 3.2 0.80 0.56 ppbv TO-15
Methyl ethyl ketone 8.4 0.80 0.44 ppbv TO-15
Tetrahydrofuran 538 8.0 3.6 ppbv TO-15
Toluene 1.4 0.80 0.23 ppbv TO-15
Acetone (2-Propanone)67.9 1.9 1.4 ug/m3 TO-15
Benzene 1.7 J 2.6 0.80 ug/m3 TO-15
Carbon disulfide 1.3 J 2.5 0.56 ug/m3 TO-15
Chloromethane 2.0 1.7 0.74 ug/m3 TO-15
Dichlorodifluoromethane 2.1 J 4.0 0.64 ug/m3 TO-15
Ethyl Acetate 25 2.9 1.5 ug/m3 TO-15
Isopropyl Alcohol 7.9 2.0 1.4 ug/m3 TO-15
Methyl ethyl ketone 25 2.4 1.3 ug/m3 TO-15
Tetrahydrofuran 1590 24 11 ug/m3 TO-15
Toluene 5.3 3.0 0.87 ug/m3 TO-15
(a) Sample analyzed by modified Method TO-15 - Tedlar bag sample containers substituted for passivated stainless
steel canisters.
14 of 103
JD618142
SGS North America Inc.
Sample Results
Report of Analysis
Dayton, NJ
Section 3
15 of 103
JD618143
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-1
Lab Sample ID:JD61814-1 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A585 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63841.D 1 03/16/23 15:36 TCH n/a n/a V2W2841
Run #2
Initial Volume
Run #1 100 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)9.4 0.80 0.58 ppbv 22 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane 0.53 0.80 0.36 ppbv J 1.1 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.41 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 4.7 0.80 0.42 ppbv 17 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 103
JD6181433.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-1
Lab Sample ID:JD61814-1 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A585 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane 0.46 0.80 0.37 ppbv J 1.9 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 1.3 0.80 0.56 ppbv 3.2 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 1.6 0.80 0.44 ppbv 4.7 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 67.7 0.80 0.36 ppbv 200 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.70 0.80 0.23 ppbv J 2.6 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 83%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 103
JD6181433.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-2
Lab Sample ID:JD61814-2 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A791 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63880.D 1 03/17/23 22:33 TCH n/a n/a V2W2842
Run #2
Initial Volume
Run #1 100 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)26.7 0.80 0.58 ppbv 63.4 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 22.8 0.80 0.25 ppbv 72.8 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.41 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 1.4 0.80 0.42 ppbv 5.0 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 103
JD6181433.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-2
Lab Sample ID:JD61814-2 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A791 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.54 0.80 0.45 ppbv J 1.9 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 0.94 0.80 0.56 ppbv 2.3 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.3 0.80 0.22 ppbv 4.5 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 11.8 0.80 0.44 ppbv 34.8 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene 1.6 2.0 0.57 ppbv J 2.7 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 56.4 0.80 0.36 ppbv 166 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.80 0.80 0.23 ppbv 3.0 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 87%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 103
JD6181433.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-3
Lab Sample ID:JD61814-3 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A490 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63843.D 1 03/16/23 16:43 TCH n/a n/a V2W2841
Run #2
Initial Volume
Run #1 100 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)17.1 0.80 0.58 ppbv 40.6 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 0.63 0.80 0.25 ppbv J 2.0 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide 0.68 0.80 0.18 ppbv J 2.1 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane 0.45 0.80 0.36 ppbv J 0.93 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.41 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene 0.44 0.80 0.24 ppbv J 1.9 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 40.7 0.80 0.42 ppbv 146 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 103
JD6181433.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-3
Lab Sample ID:JD61814-3 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A490 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 5.5 0.80 0.56 ppbv 14 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.1 0.80 0.22 ppbv 3.8 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 8.1 0.80 0.44 ppbv 24 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene 0.21 0.16 0.056 ppbv 1.4 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 37.7 0.80 0.36 ppbv 111 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 2.8 0.80 0.23 ppbv 11 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene 1.3 0.80 0.56 ppbv 5.6 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene 0.40 0.80 0.31 ppbv J 1.7 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)1.7 0.80 0.31 ppbv 7.4 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 85%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 103
JD6181433.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-4
Lab Sample ID:JD61814-4 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A603 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63844.D 1 03/16/23 17:17 TCH n/a n/a V2W2841
Run #2
Initial Volume
Run #1 100 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)19.8 0.80 0.58 ppbv 47.0 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide 0.48 0.80 0.18 ppbv J 1.5 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.44 0.80 0.13 ppbv J 2.2 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 7.3 0.80 0.42 ppbv 26 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 103
JD6181433.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-4
Lab Sample ID:JD61814-4 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A603 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane 0.38 0.80 0.37 ppbv J 1.6 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 1.0 0.80 0.56 ppbv 2.5 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 9.6 0.80 0.44 ppbv 28 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 31.2 0.80 0.36 ppbv 92.0 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 0.51 0.80 0.23 ppbv J 1.9 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 86%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 103
JD6181433.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-5
Lab Sample ID:JD61814-5 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A439 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63845.D 1 03/16/23 17:50 TCH n/a n/a V2W2841
Run #2 2W63881.D 1 03/17/23 23:05 TCH n/a n/a V2W2842
Initial Volume
Run #1 100 ml
Run #2 10.0 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)35.2 0.80 0.58 ppbv 83.6 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 71.7 0.80 0.25 ppbv 229 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide 0.41 0.80 0.18 ppbv J 1.3 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane 0.91 0.80 0.36 ppbv 1.9 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.40 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 7.3 0.80 0.42 ppbv 26 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
24 of 103
JD6181433.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-5
Lab Sample ID:JD61814-5 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A439 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane 0.69 0.80 0.37 ppbv J 2.8 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.53 0.80 0.45 ppbv J 1.9 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 1.6 0.80 0.56 ppbv 3.9 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 15.1 0.80 0.44 ppbv 44.5 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 855 b 8.0 3.6 ppbv 2520 b 24 11 ug/m3
108-88-3 92.14 Toluene 4.1 0.80 0.23 ppbv 15 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene 0.78 0.80 0.56 ppbv J 3.4 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)0.78 0.80 0.31 ppbv J 3.4 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 85%83%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
25 of 103
JD6181433.5
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-6
Lab Sample ID:JD61814-6 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A680 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63854.D 1 03/16/23 22:49 TCH n/a n/a V2W2841
Run #2
Initial Volume
Run #1 50.0 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)181 1.6 1.2 ppbv 430 3.8 2.9 ug/m3
106-99-0 54.09 1,3-Butadiene ND 1.6 0.67 ppbv ND 3.5 1.5 ug/m3
71-43-2 78.11 Benzene 53.6 1.6 0.50 ppbv 171 5.1 1.6 ug/m3
75-27-4 163.8 Bromodichloromethane ND 1.6 0.24 ppbv ND 11 1.6 ug/m3
75-25-2 252.8 Bromoform ND 1.6 0.57 ppbv ND 17 5.9 ug/m3
74-83-9 94.94 Bromomethane ND 1.6 0.55 ppbv ND 6.2 2.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 1.6 1.0 ppbv ND 8.2 5.2 ug/m3
75-15-0 76.14 Carbon disulfide ND 1.6 0.36 ppbv ND 5.0 1.1 ug/m3
108-90-7 112.6 Chlorobenzene ND 1.6 0.59 ppbv ND 7.4 2.7 ug/m3
75-00-3 64.52 Chloroethane ND 1.6 0.54 ppbv ND 4.2 1.4 ug/m3
67-66-3 119.4 Chloroform ND 1.6 0.30 ppbv ND 7.8 1.5 ug/m3
74-87-3 50.49 Chloromethane ND 1.6 0.72 ppbv ND 3.3 1.5 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 1.6 0.32 ppbv ND 10 2.0 ug/m3
110-82-7 84.16 Cyclohexane ND 1.6 0.88 ppbv ND 5.5 3.0 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 1.6 0.46 ppbv ND 6.5 1.9 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 1.6 0.47 ppbv ND 6.3 1.9 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 1.6 0.78 ppbv ND 12 6.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 1.6 0.56 ppbv ND 6.5 2.3 ug/m3
78-87-5 113 1,2-Dichloropropane ND 1.6 0.50 ppbv ND 7.4 2.3 ug/m3
123-91-1 88.12 1,4-Dioxane ND 1.6 0.94 ppbv ND 5.8 3.4 ug/m3
75-71-8 120.9 Dichlorodifluoromethane ND 1.6 0.26 ppbv ND 7.9 1.3 ug/m3
124-48-1 208.3 Dibromochloromethane ND 1.6 0.42 ppbv ND 14 3.6 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 1.6 0.55 ppbv ND 6.3 2.2 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 1.6 0.62 ppbv ND 6.3 2.5 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 1.6 0.50 ppbv ND 7.3 2.3 ug/m3
541-73-1 147 m-Dichlorobenzene ND 1.6 0.32 ppbv ND 9.6 1.9 ug/m3
95-50-1 147 o-Dichlorobenzene ND 1.6 1.2 ppbv ND 9.6 7.2 ug/m3
106-46-7 147 p-Dichlorobenzene ND 1.6 1.5 ppbv ND 9.6 9.0 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 1.6 0.81 ppbv ND 7.3 3.7 ug/m3
100-41-4 106.2 Ethylbenzene ND 1.6 0.49 ppbv ND 6.9 2.1 ug/m3
141-78-6 88 Ethyl Acetate 12.0 1.6 0.83 ppbv 43.2 5.8 3.0 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 1.6 0.76 ppbv ND 7.9 3.7 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
26 of 103
JD6181433.6
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-6
Lab Sample ID:JD61814-6 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A680 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 1.6 0.25 ppbv ND 12 1.9 ug/m3
76-14-2 170.9 Freon 114 ND 1.6 0.40 ppbv ND 11 2.8 ug/m3
142-82-5 100.2 Heptane ND 1.6 0.74 ppbv ND 6.6 3.0 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 1.6 0.50 ppbv ND 17 5.3 ug/m3
110-54-3 86.18 Hexane ND 1.6 0.90 ppbv ND 5.6 3.2 ug/m3
591-78-6 100 2-Hexanone ND 1.6 1.2 ppbv ND 6.5 4.9 ug/m3
67-63-0 60.1 Isopropyl Alcohol 2.5 1.6 1.1 ppbv 6.1 3.9 2.7 ug/m3
75-09-2 84.94 Methylene chloride 1.5 1.6 0.45 ppbv J 5.2 5.6 1.6 ug/m3
78-93-3 72.11 Methyl ethyl ketone 124 1.6 0.88 ppbv 366 4.7 2.6 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 1.6 0.58 ppbv ND 6.6 2.4 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 1.6 0.64 ppbv ND 5.8 2.3 ug/m3
91-20-3 128.17 Naphthalene ND 1.6 1.0 ppbv ND 8.4 5.2 ug/m3
115-07-1 42 Propylene ND 4.0 1.1 ppbv ND 6.9 1.9 ug/m3
100-42-5 104.1 Styrene ND 1.6 0.94 ppbv ND 6.8 4.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 1.6 0.30 ppbv ND 8.7 1.6 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 1.6 0.38 ppbv ND 11 2.6 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 1.6 0.30 ppbv ND 8.7 1.6 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 1.6 0.97 ppbv ND 12 7.2 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 1.6 0.70 ppbv ND 7.9 3.4 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 1.6 0.64 ppbv ND 7.9 3.1 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.32 0.11 ppbv ND 2.2 0.75 ug/m3
109-99-9 72.11 Tetrahydrofuran 374 1.6 0.72 ppbv 1100 4.7 2.1 ug/m3
108-88-3 92.14 Toluene 3.0 1.6 0.46 ppbv 11 6.0 1.7 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.32 0.15 ppbv ND 1.7 0.81 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 1.6 0.29 ppbv ND 9.0 1.6 ug/m3
75-01-4 62.5 Vinyl chloride ND 1.6 0.55 ppbv ND 4.1 1.4 ug/m3
108-05-4 86 Vinyl Acetate ND 1.6 0.90 ppbv ND 5.6 3.2 ug/m3
106.2 m,p-Xylene ND 1.6 1.1 ppbv ND 6.9 4.8 ug/m3
95-47-6 106.2 o-Xylene ND 1.6 0.62 ppbv ND 6.9 2.7 ug/m3
1330-20-7 106.2 Xylenes (total)ND 1.6 0.62 ppbv ND 6.9 2.7 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 88%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
27 of 103
JD6181433.6
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-7
Lab Sample ID:JD61814-7 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A583 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63846.D 1 03/16/23 18:23 TCH n/a n/a V2W2841
Run #2 2W63912.D 1 03/20/23 20:56 TCH n/a n/a V2W2844
Initial Volume
Run #1 100 ml
Run #2 50.0 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)127 0.80 0.58 ppbv 302 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 0.87 0.80 0.25 ppbv 2.8 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide 0.42 0.80 0.18 ppbv J 1.3 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane 0.56 0.80 0.36 ppbv J 1.2 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane 0.47 0.80 0.44 ppbv J 1.6 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.42 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene 0.51 0.80 0.24 ppbv J 2.2 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 53.4 0.80 0.42 ppbv 192 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
28 of 103
JD6181433.7
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-7
Lab Sample ID:JD61814-7 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A583 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 5.9 0.80 0.56 ppbv 15 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 0.83 0.80 0.22 ppbv 2.9 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 92.4 0.80 0.44 ppbv 273 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 258 b 1.6 0.72 ppbv 761 b 4.7 2.1 ug/m3
108-88-3 92.14 Toluene 3.2 0.80 0.23 ppbv 12 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene 1.6 0.80 0.56 ppbv 6.9 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene 0.45 0.80 0.31 ppbv J 2.0 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)2.0 0.80 0.31 ppbv 8.7 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 87%90%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
29 of 103
JD6181433.7
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-8
Lab Sample ID:JD61814-8 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A676 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63847.D 1 03/16/23 18:57 TCH n/a n/a V2W2841
Run #2
Initial Volume
Run #1 100 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)51.0 0.80 0.58 ppbv 121 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.41 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
30 of 103
JD6181433.8
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-8
Lab Sample ID:JD61814-8 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A676 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol ND 0.80 0.56 ppbv ND 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 14.7 0.80 0.44 ppbv 43.4 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 71.6 0.80 0.36 ppbv 211 2.4 1.1 ug/m3
108-88-3 92.14 Toluene ND 0.80 0.23 ppbv ND 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 83%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
31 of 103
JD6181433.8
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-9
Lab Sample ID:JD61814-9 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A432 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63856.D 1 03/16/23 23:55 TCH n/a n/a V2W2841
Run #2 2W63918.D 1 03/21/23 00:12 TCH n/a n/a V2W2844
Initial Volume
Run #1 100 ml
Run #2 10.0 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)177 0.80 0.58 ppbv 420 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane 0.92 0.80 0.36 ppbv 1.9 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.40 0.80 0.13 ppbv J 2.0 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 8.4 0.80 0.42 ppbv 30 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
32 of 103
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SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-9
Lab Sample ID:JD61814-9 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A432 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.47 0.80 0.45 ppbv J 1.7 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 2.3 0.80 0.56 ppbv 5.7 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.6 0.80 0.22 ppbv 5.6 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 136 b 8.0 4.4 ppbv 401 b 24 13 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 488 b 8.0 3.6 ppbv 1440 b 24 11 ug/m3
108-88-3 92.14 Toluene 0.55 0.80 0.23 ppbv J 2.1 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene 0.61 0.80 0.56 ppbv J 2.6 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)0.61 0.80 0.31 ppbv J 2.6 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 90%84%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
33 of 103
JD6181433.9
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-10
Lab Sample ID:JD61814-10 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A679,TBAG Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63857.D 1 03/17/23 00:27 TCH n/a n/a V2W2841
Run #2 a 2W63917.D 128 03/20/23 23:39 TCH n/a n/a V2W2844
Initial Volume
Run #1 5.0 ml
Run #2 100 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)6650 b 100 74 ppbv 15800 b 240 180 ug/m3
106-99-0 54.09 1,3-Butadiene ND 16 6.7 ppbv ND 35 15 ug/m3
71-43-2 78.11 Benzene ND 16 5.0 ppbv ND 51 16 ug/m3
75-27-4 163.8 Bromodichloromethane ND 16 2.4 ppbv ND 110 16 ug/m3
75-25-2 252.8 Bromoform ND 16 5.7 ppbv ND 170 59 ug/m3
74-83-9 94.94 Bromomethane ND 16 5.5 ppbv ND 62 21 ug/m3
100-44-7 126 Benzyl Chloride c ND 16 10 ppbv ND 82 52 ug/m3
75-15-0 76.14 Carbon disulfide ND 16 3.6 ppbv ND 50 11 ug/m3
108-90-7 112.6 Chlorobenzene ND 16 5.9 ppbv ND 74 27 ug/m3
75-00-3 64.52 Chloroethane ND 16 5.4 ppbv ND 42 14 ug/m3
67-66-3 119.4 Chloroform ND 16 3.0 ppbv ND 78 15 ug/m3
74-87-3 50.49 Chloromethane ND 16 7.2 ppbv ND 33 15 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 16 3.2 ppbv ND 100 20 ug/m3
110-82-7 84.16 Cyclohexane ND 16 8.8 ppbv ND 55 30 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 16 4.6 ppbv ND 65 19 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 16 4.7 ppbv ND 63 19 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 16 7.8 ppbv ND 120 60 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 16 5.6 ppbv ND 65 23 ug/m3
78-87-5 113 1,2-Dichloropropane ND 16 5.0 ppbv ND 74 23 ug/m3
123-91-1 88.12 1,4-Dioxane ND 16 9.4 ppbv ND 58 34 ug/m3
75-71-8 120.9 Dichlorodifluoromethane ND 16 2.6 ppbv ND 79 13 ug/m3
124-48-1 208.3 Dibromochloromethane ND 16 4.2 ppbv ND 140 36 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 16 5.5 ppbv ND 63 22 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 16 6.2 ppbv ND 63 25 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 16 5.0 ppbv ND 73 23 ug/m3
541-73-1 147 m-Dichlorobenzene ND 16 3.2 ppbv ND 96 19 ug/m3
95-50-1 147 o-Dichlorobenzene ND 16 12 ppbv ND 96 72 ug/m3
106-46-7 147 p-Dichlorobenzene ND 16 15 ppbv ND 96 90 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 16 8.1 ppbv ND 73 37 ug/m3
100-41-4 106.2 Ethylbenzene ND 16 4.9 ppbv ND 69 21 ug/m3
141-78-6 88 Ethyl Acetate ND 16 8.3 ppbv ND 58 30 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 16 7.6 ppbv ND 79 37 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
34 of 103
JD6181433.10
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-10
Lab Sample ID:JD61814-10 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A679,TBAG Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 16 2.5 ppbv ND 120 19 ug/m3
76-14-2 170.9 Freon 114 ND 16 4.0 ppbv ND 110 28 ug/m3
142-82-5 100.2 Heptane ND 16 7.4 ppbv ND 66 30 ug/m3
87-68-3 260.8 Hexachlorobutadiene c ND 16 5.0 ppbv ND 170 53 ug/m3
110-54-3 86.18 Hexane ND 16 9.0 ppbv ND 56 32 ug/m3
591-78-6 100 2-Hexanone ND 16 12 ppbv ND 65 49 ug/m3
67-63-0 60.1 Isopropyl Alcohol 17.9 16 11 ppbv 44.0 39 27 ug/m3
75-09-2 84.94 Methylene chloride ND 16 4.5 ppbv ND 56 16 ug/m3
78-93-3 72.11 Methyl ethyl ketone 3600 b 100 56 ppbv 10600 b 290 170 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 16 5.8 ppbv ND 66 24 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether 36.1 16 6.4 ppbv 130 58 23 ug/m3
91-20-3 128.17 Naphthalene ND 16 10 ppbv ND 84 52 ug/m3
115-07-1 42 Propylene ND 40 11 ppbv ND 69 19 ug/m3
100-42-5 104.1 Styrene ND 16 9.4 ppbv ND 68 40 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 16 3.0 ppbv ND 87 16 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 16 3.8 ppbv ND 110 26 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 16 3.0 ppbv ND 87 16 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 16 9.7 ppbv ND 120 72 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 16 7.0 ppbv ND 79 34 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 16 6.4 ppbv ND 79 31 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 3.2 1.1 ppbv ND 22 7.5 ug/m3
109-99-9 72.11 Tetrahydrofuran 13700 b 100 46 ppbv 40400 b 290 140 ug/m3
108-88-3 92.14 Toluene ND 16 4.6 ppbv ND 60 17 ug/m3
79-01-6 131.4 Trichloroethylene ND 3.2 1.5 ppbv ND 17 8.1 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 16 2.9 ppbv ND 90 16 ug/m3
75-01-4 62.5 Vinyl chloride ND 16 5.5 ppbv ND 41 14 ug/m3
108-05-4 86 Vinyl Acetate ND 16 9.0 ppbv ND 56 32 ug/m3
106.2 m,p-Xylene ND 16 11 ppbv ND 69 48 ug/m3
95-47-6 106.2 o-Xylene ND 16 6.2 ppbv ND 69 27 ug/m3
1330-20-7 106.2 Xylenes (total)ND 16 6.2 ppbv ND 69 27 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 89%85%65-128%
(a) Sample analyzed by modified Method TO-15 - Tedlar bag sample containers substituted for passivated stainless
steel canisters.
(b) Result is from Run# 2
(c) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
35 of 103
JD6181433.10
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-11
Lab Sample ID:JD61814-11 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: M205 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63855.D 1 03/16/23 23:22 TCH n/a n/a V2W2841
Run #2 2W63916.D 1 03/20/23 23:06 TCH n/a n/a V2W2844
Initial Volume
Run #1 25.0 ml
Run #2 10.0 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)592 3.2 2.3 ppbv 1410 7.6 5.5 ug/m3
106-99-0 54.09 1,3-Butadiene ND 3.2 1.3 ppbv ND 7.1 2.9 ug/m3
71-43-2 78.11 Benzene ND 3.2 0.99 ppbv ND 10 3.2 ug/m3
75-27-4 163.8 Bromodichloromethane ND 3.2 0.48 ppbv ND 21 3.2 ug/m3
75-25-2 252.8 Bromoform ND 3.2 1.1 ppbv ND 33 11 ug/m3
74-83-9 94.94 Bromomethane ND 3.2 1.1 ppbv ND 12 4.3 ug/m3
100-44-7 126 Benzyl Chloride a ND 3.2 2.0 ppbv ND 16 10 ug/m3
75-15-0 76.14 Carbon disulfide ND 3.2 0.72 ppbv ND 10 2.2 ug/m3
108-90-7 112.6 Chlorobenzene ND 3.2 1.2 ppbv ND 15 5.5 ug/m3
75-00-3 64.52 Chloroethane ND 3.2 1.1 ppbv ND 8.4 2.9 ug/m3
67-66-3 119.4 Chloroform ND 3.2 0.59 ppbv ND 16 2.9 ug/m3
74-87-3 50.49 Chloromethane ND 3.2 1.4 ppbv ND 6.6 2.9 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 3.2 0.64 ppbv ND 20 4.0 ug/m3
110-82-7 84.16 Cyclohexane ND 3.2 1.8 ppbv ND 11 6.2 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 3.2 0.91 ppbv ND 13 3.7 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 3.2 0.94 ppbv ND 13 3.7 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 3.2 1.6 ppbv ND 25 12 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 3.2 1.1 ppbv ND 13 4.5 ug/m3
78-87-5 113 1,2-Dichloropropane ND 3.2 0.99 ppbv ND 15 4.6 ug/m3
123-91-1 88.12 1,4-Dioxane ND 3.2 1.9 ppbv ND 12 6.8 ug/m3
75-71-8 120.9 Dichlorodifluoromethane ND 3.2 0.51 ppbv ND 16 2.5 ug/m3
124-48-1 208.3 Dibromochloromethane ND 3.2 0.83 ppbv ND 27 7.1 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 3.2 1.1 ppbv ND 13 4.4 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 3.2 1.2 ppbv ND 13 4.8 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 3.2 0.99 ppbv ND 15 4.5 ug/m3
541-73-1 147 m-Dichlorobenzene ND 3.2 0.64 ppbv ND 19 3.8 ug/m3
95-50-1 147 o-Dichlorobenzene ND 3.2 2.5 ppbv ND 19 15 ug/m3
106-46-7 147 p-Dichlorobenzene ND 3.2 3.1 ppbv ND 19 19 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 3.2 1.6 ppbv ND 15 7.3 ug/m3
100-41-4 106.2 Ethylbenzene ND 3.2 0.98 ppbv ND 14 4.3 ug/m3
141-78-6 88 Ethyl Acetate 5.2 3.2 1.7 ppbv 19 12 6.1 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 3.2 1.5 ppbv ND 16 7.4 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
36 of 103
JD6181433.11
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-11
Lab Sample ID:JD61814-11 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: M205 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 3.2 0.50 ppbv ND 25 3.8 ug/m3
76-14-2 170.9 Freon 114 ND 3.2 0.80 ppbv ND 22 5.6 ug/m3
142-82-5 100.2 Heptane ND 3.2 1.5 ppbv ND 13 6.1 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 3.2 0.99 ppbv ND 34 11 ug/m3
110-54-3 86.18 Hexane ND 3.2 1.8 ppbv ND 11 6.3 ug/m3
591-78-6 100 2-Hexanone ND 3.2 2.3 ppbv ND 13 9.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 7.4 3.2 2.3 ppbv 18 7.9 5.7 ug/m3
75-09-2 84.94 Methylene chloride ND 3.2 0.90 ppbv ND 11 3.1 ug/m3
78-93-3 72.11 Methyl ethyl ketone 363 3.2 1.8 ppbv 1070 9.4 5.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 3.2 1.2 ppbv ND 13 4.9 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 3.2 1.3 ppbv ND 12 4.7 ug/m3
91-20-3 128.17 Naphthalene ND 3.2 2.0 ppbv ND 17 10 ug/m3
115-07-1 42 Propylene ND 8.0 2.3 ppbv ND 14 4.0 ug/m3
100-42-5 104.1 Styrene ND 3.2 1.9 ppbv ND 14 8.1 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 3.2 0.59 ppbv ND 17 3.2 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 3.2 0.77 ppbv ND 22 5.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 3.2 0.61 ppbv ND 17 3.3 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 3.2 1.9 ppbv ND 24 14 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 3.2 1.4 ppbv ND 16 6.9 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 3.2 1.3 ppbv ND 16 6.4 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.64 0.22 ppbv ND 4.3 1.5 ug/m3
109-99-9 72.11 Tetrahydrofuran 1110 b 8.0 3.6 ppbv 3270 b 24 11 ug/m3
108-88-3 92.14 Toluene 2.4 3.2 0.91 ppbv J 9.0 12 3.4 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.64 0.30 ppbv ND 3.4 1.6 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 3.2 0.58 ppbv ND 18 3.3 ug/m3
75-01-4 62.5 Vinyl chloride ND 3.2 1.1 ppbv ND 8.2 2.8 ug/m3
108-05-4 86 Vinyl Acetate ND 3.2 1.8 ppbv ND 11 6.3 ug/m3
106.2 m,p-Xylene ND 3.2 2.2 ppbv ND 14 9.6 ug/m3
95-47-6 106.2 o-Xylene ND 3.2 1.2 ppbv ND 14 5.2 ug/m3
1330-20-7 106.2 Xylenes (total)ND 3.2 1.2 ppbv ND 14 5.2 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 87%87%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
37 of 103
JD6181433.11
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-12
Lab Sample ID:JD61814-12 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A536 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63848.D 1 03/16/23 19:30 TCH n/a n/a V2W2841
Run #2
Initial Volume
Run #1 100 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)36.3 0.80 0.58 ppbv 86.2 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene 0.79 0.80 0.34 ppbv J 1.7 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 1.1 0.80 0.25 ppbv 3.5 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.45 0.80 0.13 ppbv J 2.2 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene 1.4 0.80 0.24 ppbv 6.1 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 1.9 0.80 0.42 ppbv 6.8 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
38 of 103
JD6181433.12
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-12
Lab Sample ID:JD61814-12 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A536 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane 1.6 0.80 0.37 ppbv 6.6 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane 0.69 0.80 0.45 ppbv J 2.4 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 1.0 0.80 0.56 ppbv 2.5 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 20.9 0.80 0.44 ppbv 61.6 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 80.9 0.80 0.36 ppbv 239 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 5.0 0.80 0.23 ppbv 19 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene 4.4 0.80 0.56 ppbv 19 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene 1.4 0.80 0.31 ppbv 6.1 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)5.8 0.80 0.31 ppbv 25 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 84%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
39 of 103
JD6181433.12
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-13
Lab Sample ID:JD61814-13 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A724 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63849.D 1 03/16/23 20:03 TCH n/a n/a V2W2841
Run #2 2W63913.D 1 03/20/23 21:29 TCH n/a n/a V2W2844
Initial Volume
Run #1 100 ml
Run #2 20.0 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)92.9 0.80 0.58 ppbv 221 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 0.69 0.80 0.25 ppbv J 2.2 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane 0.60 0.80 0.44 ppbv J 2.1 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.43 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene 0.53 0.80 0.24 ppbv J 2.3 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 55.7 0.80 0.42 ppbv 200 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
40 of 103
JD6181433.13
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-13
Lab Sample ID:JD61814-13 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A724 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 6.6 0.80 0.56 ppbv 16 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 0.88 0.80 0.22 ppbv 3.1 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 49.1 0.80 0.44 ppbv 145 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 289 b 4.0 1.8 ppbv 852 b 12 5.3 ug/m3
108-88-3 92.14 Toluene 3.2 0.80 0.23 ppbv 12 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene 1.6 0.80 0.56 ppbv 6.9 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene 0.46 0.80 0.31 ppbv J 2.0 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)2.1 0.80 0.31 ppbv 9.1 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 87%86%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
41 of 103
JD6181433.13
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-14
Lab Sample ID:JD61814-14 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A1251 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63850.D 1 03/16/23 20:37 TCH n/a n/a V2W2841
Run #2 2W63914.D 1 03/20/23 22:01 TCH n/a n/a V2W2844
Initial Volume
Run #1 100 ml
Run #2 50.0 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)74.5 0.80 0.58 ppbv 177 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene ND 0.80 0.25 ppbv ND 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.43 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 12.9 0.80 0.42 ppbv 46.4 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
42 of 103
JD6181433.14
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-14
Lab Sample ID:JD61814-14 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A1251 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.4 0.80 0.56 ppbv 11 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 0.94 0.80 0.22 ppbv 3.3 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 48.0 0.80 0.44 ppbv 142 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 74.7 b 1.6 0.72 ppbv 220 b 4.7 2.1 ug/m3
108-88-3 92.14 Toluene 0.61 0.80 0.23 ppbv J 2.3 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 84%81%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
43 of 103
JD6181433.14
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-15
Lab Sample ID:JD61814-15 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A497 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63851.D 1 03/16/23 21:10 TCH n/a n/a V2W2841
Run #2
Initial Volume
Run #1 100 ml
Run #2
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)37.4 0.80 0.58 ppbv 88.8 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 0.50 0.80 0.25 ppbv J 1.6 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane ND 0.80 0.36 ppbv ND 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane 0.97 0.80 0.44 ppbv 3.3 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.44 0.80 0.13 ppbv J 2.2 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 66.2 0.80 0.42 ppbv 238 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
44 of 103
JD6181433.15
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-15
Lab Sample ID:JD61814-15 Date Sampled:03/06/23
Matrix:AIR - Soil Vapor Comp. Summa ID: A497 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane 0.64 0.80 0.37 ppbv J 2.6 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 1.9 0.80 0.56 ppbv 4.7 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride 1.8 0.80 0.22 ppbv 6.3 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 13.9 0.80 0.44 ppbv 41.0 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 46.5 0.80 0.36 ppbv 137 2.4 1.1 ug/m3
108-88-3 92.14 Toluene 2.1 0.80 0.23 ppbv 7.9 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 83%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
45 of 103
JD6181433.15
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MP-DUP
Lab Sample ID:JD61814-16 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: M420 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 2W63852.D 1 03/16/23 21:44 TCH n/a n/a V2W2841
Run #2 2W63915.D 1 03/20/23 22:34 TCH n/a n/a V2W2844
Initial Volume
Run #1 100 ml
Run #2 10.0 ml
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)28.6 0.80 0.58 ppbv 67.9 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 0.75 ug/m3
71-43-2 78.11 Benzene 0.52 0.80 0.25 ppbv J 1.7 2.6 0.80 ug/m3
75-27-4 163.8 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 0.80 ug/m3
75-25-2 252.8 Bromoform ND 0.80 0.28 ppbv ND 8.3 2.9 ug/m3
74-83-9 94.94 Bromomethane ND 0.80 0.28 ppbv ND 3.1 1.1 ug/m3
100-44-7 126 Benzyl Chloride a ND 0.80 0.50 ppbv ND 4.1 2.6 ug/m3
75-15-0 76.14 Carbon disulfide 0.43 0.80 0.18 ppbv J 1.3 2.5 0.56 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 1.4 ug/m3
75-00-3 64.52 Chloroethane ND 0.80 0.27 ppbv ND 2.1 0.71 ug/m3
67-66-3 119.4 Chloroform ND 0.80 0.15 ppbv ND 3.9 0.73 ug/m3
74-87-3 50.49 Chloromethane 0.98 0.80 0.36 ppbv 2.0 1.7 0.74 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 1.0 ug/m3
110-82-7 84.16 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 1.5 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 0.93 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 0.95 ug/m3
106-93-4 187.9 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 3.0 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
78-87-5 113 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 1.2 ug/m3
123-91-1 88.12 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 1.7 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.43 0.80 0.13 ppbv J 2.1 4.0 0.64 ug/m3
124-48-1 208.3 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 1.8 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 1.1 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 1.2 ug/m3
10061-01-5 111 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 1.1 ug/m3
541-73-1 147 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 0.96 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 3.7 ug/m3
106-46-7 147 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 4.6 ug/m3
10061-02-6 111 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 1.8 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 1.0 ug/m3
141-78-6 88 Ethyl Acetate 7.0 0.80 0.42 ppbv 25 2.9 1.5 ug/m3
622-96-8 120.19 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 1.9 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
46 of 103
JD6181433.16
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MP-DUP
Lab Sample ID:JD61814-16 Date Sampled:03/07/23
Matrix:AIR - Soil Vapor Comp. Summa ID: M420 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
76-13-1 187.4 Freon 113 ND 0.80 0.12 ppbv ND 6.1 0.92 ug/m3
76-14-2 170.9 Freon 114 ND 0.80 0.20 ppbv ND 5.6 1.4 ug/m3
142-82-5 100.2 Heptane ND 0.80 0.37 ppbv ND 3.3 1.5 ug/m3
87-68-3 260.8 Hexachlorobutadiene a ND 0.80 0.25 ppbv ND 8.5 2.7 ug/m3
110-54-3 86.18 Hexane ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
591-78-6 100 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 2.4 ug/m3
67-63-0 60.1 Isopropyl Alcohol 3.2 0.80 0.56 ppbv 7.9 2.0 1.4 ug/m3
75-09-2 84.94 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 0.76 ug/m3
78-93-3 72.11 Methyl ethyl ketone 8.4 0.80 0.44 ppbv 25 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 1.2 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 1.2 ug/m3
91-20-3 128.17 Naphthalene ND 0.80 0.51 ppbv ND 4.2 2.7 ug/m3
115-07-1 42 Propylene ND 2.0 0.57 ppbv ND 3.4 0.98 ug/m3
100-42-5 104.1 Styrene ND 0.80 0.47 ppbv ND 3.4 2.0 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 1.3 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 0.82 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 3.6 ug/m3
95-63-6 120.19 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 1.7 ug/m3
108-67-8 120.19 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 1.6 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 0.38 ug/m3
109-99-9 72.11 Tetrahydrofuran 538 b 8.0 3.6 ppbv 1590 b 24 11 ug/m3
108-88-3 92.14 Toluene 1.4 0.80 0.23 ppbv 5.3 3.0 0.87 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 0.41 ug/m3
75-69-4 137.4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 0.79 ug/m3
75-01-4 62.5 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 0.72 ug/m3
108-05-4 86 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 1.6 ug/m3
106.2 m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 2.4 ug/m3
95-47-6 106.2 o-Xylene ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 1.3 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 85%81%65-128%
(a) Associated CCV outside of control limits low. This compound in blank spike is outside in house QC limits bias
low.
(b) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
47 of 103
JD6181433.16
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
• Summa Canister and Flow Controller Log
Dayton, NJ
Section 4
48 of 103
JD618144
GHAIN OF GUSTODY - AIR
i644 ttil ot 3oStqy B7o 76{L PAGE /OF ?
ftt0^SGS North America lnc, - Dayton
223s Roule 130, Day,lon, NJ 088'10
rEL. 732-329-0200 FAX [phone]
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JD61814: Chain of Custody
Page 1 of 4
49 of 103
JD6181444.1
CHAIN OF CUSTODY.AIR PAGE < OF ?
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JD61814: Chain of Custody
Page 2 of 4
50 of 103
JD6181444.1
CLIENTAIN SEUPLING EQUIPTUENT RETURN FONNArPRoJEcT:IJOB #ADDITIoNAL CONTROLLERSD6t8lCONTROL#ADDITIoNAL SUMMA CANISTERS11 A6zttfl5011rb06al/ nut\(x,Ito,(ALfct 01l{( rt0Lt{ LttolFrnqb(t tuq(c rtL3ft t:rt1-)JJ--ZEt,|DATE &W;RECETVEDBY:2DATE &TIME:RECETVEDElG4OATE &TIME:RELINOUISHED BY:3DATE &TIME:CugroDY SEA#'s:# OF BOXES OR PIECES IN DEUVERYNOTES:sM085-03Pub date: 3/12l18JD61814: Chain of Custody
Page 3 of 4
51 of 103
JD6181444.1
Job Number:JD61814 Client:HART & HICKMAN
Date / Time Received:3/9/2023 10:00:00 AM Delivery Method:FEDEX
Project:TKC.008, CHARLOTTE, NC
4. No. Coolers:N/A
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
N/A
N/A
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
SM089-03
Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:231619 pH 12+:203117A Other: (Specify)
JD61814: Chain of Custody
Page 4 of 4
52 of 103
JD6181444.1
Summa Canister and Flow Controller Log Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Received:03/09/23
SUMMA CANISTERS
Shipping Receiving
Summa Vac Date SCC SCC Sample Date Vac Pres Final Dil
ID L " Hg Out By Batch FileID Number In By " Hg psig psig Fact
A585 1 29.4 01/31/23 ML CP120632W63053.D JD61814-1 03/14/23 DG 6.5 1
A791 1 29.4 01/31/23 ML CP120593W79066.D JD61814-2 03/14/23 DG 5 1
A490 1 29.4 02/10/23 ML CP120888W00256.D JD61814-3 03/14/23 DG 6 1
A603 1 29.4 01/31/23 ML CP120593W79066.D JD61814-4 03/14/23 DG 5.5 1
A439 1 29.4 01/31/23 ML CP120593W79066.D JD61814-5 03/14/23 DG 4.5 1
A680 1 29.4 02/10/23 ML CP120888W00256.D JD61814-6 03/14/23 DG 4 1
A583 1 29.4 02/10/23 ML CP120888W00256.D JD61814-7 03/14/23 DG 5 1
A676 1 29.4 01/31/23 ML CP120632W63053.D JD61814-8 03/14/23 DG 6 1
A432 1 29.4 01/31/23 ML CP120632W63053.D JD61814-9 03/14/23 DG 4 1
A679 1 29.4 01/31/23 ML CP120593W79066.D JD61814-10 03/14/23 DG 4.5 1
M205 1 29.4 02/10/23 ML CP120888W00256.D JD61814-11 03/14/23 DG 5 1
A536 1 29.4 01/31/23 ML CP120632W63053.D JD61814-12 03/14/23 DG 5 1
A724 1 29.4 02/10/23 ML CP120888W00256.D JD61814-13 03/14/23 DG 4 1
A1251 1 29.4 01/31/23 ML CP120632W63053.D JD61814-14 03/14/23 DG 5 1
A497 1 29.4 01/31/23 ML CP120593W79066.D JD61814-15 03/14/23 DG 5.5 1
M420 1 29.4 01/31/23 ML CP120593W79066.D JD61814-16 03/14/23 DG 5.5 1
FLOW CONTROLLERS / OTHER
Shipping Receiving
Flow Date cc/Time Date cc/Flow
Crtl ID Out By min hrs.In By min RPD Equipment Type
FC379 02/10/23 ML 83 .1667 03/14/23 ML 88 5.8 Flow Controller
FC413 02/10/23 ML 83 .1667 03/14/23 ML 84 1.2 Flow Controller
FC732 01/31/23 ML 83 .1667 03/14/23 ML 87 4.7 Flow Controller
FC899 01/31/23 ML 83 .1667 03/14/23 ML 85 2.4 Flow Controller
FC919 02/10/23 ML 84 .1667 03/14/23 ML 87 3.5 Flow Controller
FC962 01/31/23 ML 83 .1667 03/14/23 ML 86 3.6 Flow Controller
FC967 01/31/23 ML 83 .1667 03/14/23 ML 86 3.6 Flow Controller
FC986 01/31/23 ML 83 .1667 03/14/23 ML 85 2.4 Flow Controller
FC995 01/31/23 ML 83 .1667 03/14/23 ML 86 3.6 Flow Controller
FC1071 02/10/23 ML 83 .1667 03/14/23 ML 86 3.6 Flow Controller
FC1161 02/10/23 ML 83 .1667 03/14/23 ML 85 2.4 Flow Controller
FC1206 01/31/23 ML 84 .1667 03/13/23 ML 87 3.5 Flow Controller
FC1209 01/31/23 ML 83 .1667 03/14/23 ML 85 2.4 Flow Controller
FC1213 01/31/23 ML 84 .1667 03/14/23 ML 85 1.2 Flow Controller
FC1214 01/31/23 ML 84 .1667 03/14/23 ML 86 2.4 Flow Controller
FC1242 01/31/23 ML 83 .1667 03/14/23 ML 87 4.7 Flow Controller
FC1243 01/31/23 ML 82 .1667 03/14/23 ML 86 4.8 Flow Controller
FC1244 01/31/23 ML 84 .1667 03/14/23 ML 85 1.2 Flow Controller
FC1263 01/31/23 ML 84 .1667 03/13/23 ML 85 1.2 Flow Controller
53 of 103
JD6181444.2
Summa Canister and Flow Controller Log Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Received:03/09/23
FLOW CONTROLLERS / OTHER
Shipping Receiving
Flow Date cc/Time Date cc/Flow
Crtl ID Out By min hrs.In By min RPD Equipment Type
FC1270 01/31/23 ML 84 .1667 03/14/23 ML 87 3.5 Flow Controller
FC1272 01/31/23 ML 82 .1667 03/13/23 ML 86 4.8 Flow Controller
FC1278 02/10/23 ML 84 .1667 03/14/23 ML 87 3.5 Flow Controller
SGS Bottle Order(s):
KR-012523-49
KR-02923-173
Prep Date Room Temp(F)Bar Pres "Hg
01/31/23 70 29.92
02/10/23 70 29.92
54 of 103
JD6181444.2
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
• Instrument Performance Checks (BFB)
• Surrogate Recovery Summaries
Dayton, NJ
Section 5
55 of 103
JD618145
Method Blank Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2841-MB 2W63836.D 1 03/16/23 TCH n/a n/a V2W2841
The QC reported here applies to the following samples:Method: TO-15
JD61814-1, JD61814-3, JD61814-4, JD61814-5, JD61814-6, JD61814-7, JD61814-8, JD61814-9, JD61814-10, JD61814-
11, JD61814-12, JD61814-13, JD61814-14, JD61814-15, JD61814-16
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-27-4 Bromodichloromethane ND 0.20 0.030 ppbv ND 1.3 ug/m3
75-25-2 Bromoform ND 0.20 0.071 ppbv ND 2.1 ug/m3
74-83-9 Bromomethane ND 0.20 0.069 ppbv ND 0.78 ug/m3
100-44-7 Benzyl Chloride ND 0.20 0.13 ppbv ND 1.0 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
75-00-3 Chloroethane ND 0.20 0.068 ppbv ND 0.53 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.20 0.097 ppbv ND 1.5 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
78-87-5 1,2-Dichloropropane ND 0.20 0.062 ppbv ND 0.92 ug/m3
123-91-1 1,4-Dioxane ND 0.20 0.12 ppbv ND 0.72 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
124-48-1 Dibromochloromethane ND 0.20 0.052 ppbv ND 1.7 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.20 0.062 ppbv ND 0.91 ug/m3
541-73-1 m-Dichlorobenzene ND 0.20 0.040 ppbv ND 1.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
106-46-7 p-Dichlorobenzene ND 0.20 0.19 ppbv ND 1.2 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.20 0.10 ppbv ND 0.91 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
622-96-8 4-Ethyltoluene ND 0.20 0.095 ppbv ND 0.98 ug/m3
76-13-1 Freon 113 ND 0.20 0.031 ppbv ND 1.5 ug/m3
76-14-2 Freon 114 ND 0.20 0.050 ppbv ND 1.4 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
56 of 103
JD6181455.1.1
Method Blank Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2841-MB 2W63836.D 1 03/16/23 TCH n/a n/a V2W2841
The QC reported here applies to the following samples:Method: TO-15
JD61814-1, JD61814-3, JD61814-4, JD61814-5, JD61814-6, JD61814-7, JD61814-8, JD61814-9, JD61814-10, JD61814-
11, JD61814-12, JD61814-13, JD61814-14, JD61814-15, JD61814-16
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
591-78-6 2-Hexanone ND 0.20 0.15 ppbv ND 0.82 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
91-20-3 Naphthalene ND 0.20 0.13 ppbv ND 1.0 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
100-42-5 Styrene ND 0.20 0.12 ppbv ND 0.85 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.20 0.087 ppbv ND 0.98 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.20 0.080 ppbv ND 0.98 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
75-69-4 Trichlorofluoromethane ND 0.20 0.036 ppbv ND 1.1 ug/m3
75-01-4 Vinyl chloride ND 0.20 0.069 ppbv ND 0.51 ug/m3
108-05-4 Vinyl Acetate ND 0.20 0.11 ppbv ND 0.70 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 82%65-128%
57 of 103
JD6181455.1.1
Method Blank Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2842-MB 2W63867.D 1 03/17/23 TCH n/a n/a V2W2842
The QC reported here applies to the following samples:Method: TO-15
JD61814-2, JD61814-5
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-27-4 Bromodichloromethane ND 0.20 0.030 ppbv ND 1.3 ug/m3
75-25-2 Bromoform ND 0.20 0.071 ppbv ND 2.1 ug/m3
74-83-9 Bromomethane ND 0.20 0.069 ppbv ND 0.78 ug/m3
100-44-7 Benzyl Chloride ND 0.20 0.13 ppbv ND 1.0 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
75-00-3 Chloroethane ND 0.20 0.068 ppbv ND 0.53 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.20 0.097 ppbv ND 1.5 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
78-87-5 1,2-Dichloropropane ND 0.20 0.062 ppbv ND 0.92 ug/m3
123-91-1 1,4-Dioxane ND 0.20 0.12 ppbv ND 0.72 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
124-48-1 Dibromochloromethane ND 0.20 0.052 ppbv ND 1.7 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.20 0.062 ppbv ND 0.91 ug/m3
541-73-1 m-Dichlorobenzene ND 0.20 0.040 ppbv ND 1.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
106-46-7 p-Dichlorobenzene ND 0.20 0.19 ppbv ND 1.2 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.20 0.10 ppbv ND 0.91 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
622-96-8 4-Ethyltoluene ND 0.20 0.095 ppbv ND 0.98 ug/m3
76-13-1 Freon 113 ND 0.20 0.031 ppbv ND 1.5 ug/m3
76-14-2 Freon 114 ND 0.20 0.050 ppbv ND 1.4 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
58 of 103
JD6181455.1.2
Method Blank Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2842-MB 2W63867.D 1 03/17/23 TCH n/a n/a V2W2842
The QC reported here applies to the following samples:Method: TO-15
JD61814-2, JD61814-5
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
591-78-6 2-Hexanone ND 0.20 0.15 ppbv ND 0.82 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
91-20-3 Naphthalene ND 0.20 0.13 ppbv ND 1.0 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
100-42-5 Styrene ND 0.20 0.12 ppbv ND 0.85 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.20 0.087 ppbv ND 0.98 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.20 0.080 ppbv ND 0.98 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
75-69-4 Trichlorofluoromethane ND 0.20 0.036 ppbv ND 1.1 ug/m3
75-01-4 Vinyl chloride ND 0.20 0.069 ppbv ND 0.51 ug/m3
108-05-4 Vinyl Acetate ND 0.20 0.11 ppbv ND 0.70 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 82%65-128%
59 of 103
JD6181455.1.2
Method Blank Summary Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2844-MB 2W63897.D 1 03/20/23 TCH n/a n/a V2W2844
The QC reported here applies to the following samples:Method: TO-15
JD61814-7, JD61814-9, JD61814-10, JD61814-11, JD61814-13, JD61814-14, JD61814-16
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 81%65-128%
60 of 103
JD6181455.1.3
Method Blank Summary Page 1 of 3
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-MB 2W63049.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here applies to the following samples:Method: TO-15
V2W2805-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-27-4 Bromodichloromethane ND 0.20 0.030 ppbv ND 1.3 ug/m3
75-25-2 Bromoform ND 0.20 0.071 ppbv ND 2.1 ug/m3
74-83-9 Bromomethane ND 0.20 0.069 ppbv ND 0.78 ug/m3
100-44-7 Benzyl Chloride ND 0.20 0.13 ppbv ND 1.0 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
75-00-3 Chloroethane ND 0.20 0.068 ppbv ND 0.53 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.20 0.097 ppbv ND 1.5 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
78-87-5 1,2-Dichloropropane ND 0.20 0.062 ppbv ND 0.92 ug/m3
123-91-1 1,4-Dioxane ND 0.20 0.12 ppbv ND 0.72 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
124-48-1 Dibromochloromethane ND 0.20 0.052 ppbv ND 1.7 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.20 0.062 ppbv ND 0.91 ug/m3
541-73-1 m-Dichlorobenzene ND 0.20 0.040 ppbv ND 1.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
106-46-7 p-Dichlorobenzene ND 0.20 0.19 ppbv ND 1.2 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.20 0.10 ppbv ND 0.91 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
622-96-8 4-Ethyltoluene ND 0.20 0.095 ppbv ND 0.98 ug/m3
76-13-1 Freon 113 ND 0.20 0.031 ppbv ND 1.5 ug/m3
76-14-2 Freon 114 ND 0.20 0.050 ppbv ND 1.4 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
61 of 103
JD6181455.1.4
Method Blank Summary Page 2 of 3
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-MB 2W63049.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here applies to the following samples:Method: TO-15
V2W2805-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
591-78-6 2-Hexanone ND 0.20 0.15 ppbv ND 0.82 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
91-20-3 Naphthalene ND 0.20 0.13 ppbv ND 1.0 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
100-42-5 Styrene ND 0.20 0.12 ppbv ND 0.85 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.20 0.087 ppbv ND 0.98 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.20 0.080 ppbv ND 0.98 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
75-69-4 Trichlorofluoromethane ND 0.20 0.036 ppbv ND 1.1 ug/m3
75-01-4 Vinyl chloride ND 0.20 0.069 ppbv ND 0.51 ug/m3
108-05-4 Vinyl Acetate ND 0.20 0.11 ppbv ND 0.70 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 91%65-128%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
124-38-9 Carbon dioxide 1.70 7.8 ppbv JN
62 of 103
JD6181455.1.4
Method Blank Summary Page 3 of 3
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-MB 2W63049.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here applies to the following samples:Method:
V2W2805-SCC
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
Total TIC, Volatile 0 ppbv
63 of 103
JD6181455.1.4
Method Blank Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-MB 3W79064.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-27-4 Bromodichloromethane ND 0.20 0.030 ppbv ND 1.3 ug/m3
75-25-2 Bromoform ND 0.20 0.071 ppbv ND 2.1 ug/m3
74-83-9 Bromomethane ND 0.20 0.069 ppbv ND 0.78 ug/m3
100-44-7 Benzyl Chloride ND 0.20 0.13 ppbv ND 1.0 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
75-00-3 Chloroethane ND 0.20 0.068 ppbv ND 0.53 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.20 0.097 ppbv ND 1.5 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
78-87-5 1,2-Dichloropropane ND 0.20 0.062 ppbv ND 0.92 ug/m3
123-91-1 1,4-Dioxane ND 0.20 0.12 ppbv ND 0.72 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
124-48-1 Dibromochloromethane ND 0.20 0.052 ppbv ND 1.7 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.20 0.062 ppbv ND 0.91 ug/m3
541-73-1 m-Dichlorobenzene ND 0.20 0.040 ppbv ND 1.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
106-46-7 p-Dichlorobenzene ND 0.20 0.19 ppbv ND 1.2 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.20 0.10 ppbv ND 0.91 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
622-96-8 4-Ethyltoluene ND 0.20 0.095 ppbv ND 0.98 ug/m3
76-13-1 Freon 113 ND 0.20 0.031 ppbv ND 1.5 ug/m3
76-14-2 Freon 114 ND 0.20 0.050 ppbv ND 1.4 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
64 of 103
JD6181455.1.5
Method Blank Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-MB 3W79064.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
591-78-6 2-Hexanone ND 0.20 0.15 ppbv ND 0.82 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
91-20-3 Naphthalene ND 0.20 0.13 ppbv ND 1.0 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
100-42-5 Styrene ND 0.20 0.12 ppbv ND 0.85 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.20 0.087 ppbv ND 0.98 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.20 0.080 ppbv ND 0.98 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
75-69-4 Trichlorofluoromethane ND 0.20 0.036 ppbv ND 1.1 ug/m3
75-01-4 Vinyl chloride ND 0.20 0.069 ppbv ND 0.51 ug/m3
108-05-4 Vinyl Acetate ND 0.20 0.11 ppbv ND 0.70 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 96%65-128%
65 of 103
JD6181455.1.5
Method Blank Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V8W11-MB 8W00255.D 1 02/08/23 TCH n/a n/a V8W11
The QC reported here applies to the following samples:Method: TO-15
V8W11-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-27-4 Bromodichloromethane ND 0.20 0.030 ppbv ND 1.3 ug/m3
75-25-2 Bromoform ND 0.20 0.071 ppbv ND 2.1 ug/m3
74-83-9 Bromomethane ND 0.20 0.069 ppbv ND 0.78 ug/m3
100-44-7 Benzyl Chloride ND 0.20 0.13 ppbv ND 1.0 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
75-00-3 Chloroethane ND 0.20 0.068 ppbv ND 0.53 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.20 0.097 ppbv ND 1.5 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
78-87-5 1,2-Dichloropropane ND 0.20 0.062 ppbv ND 0.92 ug/m3
123-91-1 1,4-Dioxane ND 0.20 0.12 ppbv ND 0.72 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
124-48-1 Dibromochloromethane ND 0.20 0.052 ppbv ND 1.7 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.20 0.062 ppbv ND 0.91 ug/m3
541-73-1 m-Dichlorobenzene ND 0.20 0.040 ppbv ND 1.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
106-46-7 p-Dichlorobenzene ND 0.20 0.19 ppbv ND 1.2 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.20 0.10 ppbv ND 0.91 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
622-96-8 4-Ethyltoluene ND 0.20 0.095 ppbv ND 0.98 ug/m3
76-13-1 Freon 113 ND 0.20 0.031 ppbv ND 1.5 ug/m3
76-14-2 Freon 114 ND 0.20 0.050 ppbv ND 1.4 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
66 of 103
JD6181455.1.6
Method Blank Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V8W11-MB 8W00255.D 1 02/08/23 TCH n/a n/a V8W11
The QC reported here applies to the following samples:Method: TO-15
V8W11-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
591-78-6 2-Hexanone ND 0.20 0.15 ppbv ND 0.82 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
91-20-3 Naphthalene ND 0.20 0.13 ppbv ND 1.0 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
100-42-5 Styrene ND 0.20 0.12 ppbv ND 0.85 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.20 0.087 ppbv ND 0.98 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.20 0.080 ppbv ND 0.98 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
75-69-4 Trichlorofluoromethane ND 0.20 0.036 ppbv ND 1.1 ug/m3
75-01-4 Vinyl chloride ND 0.20 0.069 ppbv ND 0.51 ug/m3
108-05-4 Vinyl Acetate ND 0.20 0.11 ppbv ND 0.70 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 95%65-128%
67 of 103
JD6181455.1.6
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2841-BS 2W63833.D 1 03/16/23 TCH n/a n/a V2W2841
V2W2841-BSD 2W63834.D 1 03/16/23 TCH n/a n/a V2W2841
The QC reported here applies to the following samples:Method: TO-15
JD61814-1, JD61814-3, JD61814-4, JD61814-5, JD61814-6, JD61814-7, JD61814-8, JD61814-9, JD61814-10, JD61814-
11, JD61814-12, JD61814-13, JD61814-14, JD61814-15, JD61814-16
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 10.1 101 10.3 103 2 70-130/30
106-99-0 1,3-Butadiene 10 11.6 116 11.9 119 3 70-130/30
71-43-2 Benzene 10 8.0 80 8.3 83 4 70-130/30
75-27-4 Bromodichloromethane 10 8.7 87 8.8 88 1 70-130/30
75-25-2 Bromoform 10 9.7 97 9.8 98 1 70-130/30
74-83-9 Bromomethane 10 10.9 109 11.0 110 1 70-130/30
100-44-7 Benzyl Chloride 10 5.9 59* a 6.1 61* a 3 70-130/30
75-15-0 Carbon disulfide 10 11.7 117 12.0 120 3 70-130/30
108-90-7 Chlorobenzene 10 9.5 95 9.8 98 3 70-130/30
75-00-3 Chloroethane 10 11.2 112 11.6 116 4 70-130/30
67-66-3 Chloroform 10 8.4 84 8.6 86 2 70-130/30
74-87-3 Chloromethane 10 12.0 120 12.2 122 2 70-130/30
56-23-5 Carbon tetrachloride 10 9.0 90 9.3 93 3 70-130/30
110-82-7 Cyclohexane 10 8.6 86 8.8 88 2 70-130/30
75-34-3 1,1-Dichloroethane 10 8.6 86 8.9 89 3 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.6 106 10.9 109 3 70-130/30
106-93-4 1,2-Dibromoethane (EDB)10 9.0 90 9.2 92 2 70-130/30
107-06-2 1,2-Dichloroethane 10 7.4 74 7.7 77 4 70-130/30
78-87-5 1,2-Dichloropropane 10 9.0 90 9.2 92 2 70-130/30
123-91-1 1,4-Dioxane 10 8.4 84 8.6 86 2 70-130/30
75-71-8 Dichlorodifluoromethane 10 9.6 96 9.8 98 2 70-130/30
124-48-1 Dibromochloromethane 10 10.2 102 10.5 105 3 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 8.9 89 9.3 93 4 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 9.1 91 9.4 94 3 70-130/30
10061-01-5 cis-1,3-Dichloropropene 10 8.1 81 8.3 83 2 70-130/30
541-73-1 m-Dichlorobenzene 10 10 100 10.2 102 2 70-130/30
95-50-1 o-Dichlorobenzene 10 9.9 99 10.1 101 2 70-130/30
106-46-7 p-Dichlorobenzene 10 9.9 99 10.2 102 3 70-130/30
10061-02-6 trans-1,3-Dichloropropene 10 7.6 76 7.8 78 3 70-130/30
100-41-4 Ethylbenzene 10 8.0 80 8.1 81 1 70-130/30
141-78-6 Ethyl Acetate 10 8.8 88 9.4 94 7 70-130/30
622-96-8 4-Ethyltoluene 10 9.1 91 9.3 93 2 70-130/30
76-13-1 Freon 113 10 11.3 113 11.7 117 3 70-130/30
76-14-2 Freon 114 10 10.7 107 11.1 111 4 70-130/30
142-82-5 Heptane 10 8.5 85 8.7 87 2 70-130/30
87-68-3 Hexachlorobutadiene 10 6.5 65* a 6.6 66* a 2 70-130/30
* = Outside of Control Limits.
68 of 103
JD6181455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2841-BS 2W63833.D 1 03/16/23 TCH n/a n/a V2W2841
V2W2841-BSD 2W63834.D 1 03/16/23 TCH n/a n/a V2W2841
The QC reported here applies to the following samples:Method: TO-15
JD61814-1, JD61814-3, JD61814-4, JD61814-5, JD61814-6, JD61814-7, JD61814-8, JD61814-9, JD61814-10, JD61814-
11, JD61814-12, JD61814-13, JD61814-14, JD61814-15, JD61814-16
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
110-54-3 Hexane 10 8.6 86 8.9 89 3 70-130/30
591-78-6 2-Hexanone 10 9.2 92 9.5 95 3 70-130/30
67-63-0 Isopropyl Alcohol 10 10.6 106 10.8 108 2 70-130/30
75-09-2 Methylene chloride 10 9.4 94 9.5 95 1 70-130/30
78-93-3 Methyl ethyl ketone 10 8.7 87 9.1 91 4 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 8.7 87 8.9 89 2 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 7.3 73 7.6 76 4 70-130/30
91-20-3 Naphthalene 10 8.2 82 8.3 83 1 70-130/30
115-07-1 Propylene 10 8.9 89 9.1 91 2 70-130/30
100-42-5 Styrene 10 9.0 90 9.2 92 2 70-130/30
71-55-6 1,1,1-Trichloroethane 10 7.8 78 8.1 81 4 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 9.0 90 9.2 92 2 70-130/30
79-00-5 1,1,2-Trichloroethane 10 8.8 88 8.8 88 0 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 7.8 78 7.9 79 1 70-130/30
95-63-6 1,2,4-Trimethylbenzene 10 8.7 87 9.0 90 3 70-130/30
108-67-8 1,3,5-Trimethylbenzene 10 8.7 87 8.9 89 2 70-130/30
127-18-4 Tetrachloroethylene 10 9.7 97 9.9 99 2 70-130/30
109-99-9 Tetrahydrofuran 10 9.0 90 9.5 95 5 70-130/30
108-88-3 Toluene 10 8.4 84 8.6 86 2 70-130/30
79-01-6 Trichloroethylene 10 8.7 87 8.8 88 1 70-130/30
75-69-4 Trichlorofluoromethane 10 9.4 94 9.7 97 3 70-130/30
75-01-4 Vinyl chloride 10 11.5 115 11.8 118 3 70-130/30
108-05-4 Vinyl Acetate 10 9.8 98 10.2 102 4 70-130/30
m,p-Xylene 20 15.8 79 16.1 81 2 70-130/30
95-47-6 o-Xylene 10 7.8 78 7.9 79 1 70-130/30
1330-20-7 Xylenes (total)30 23.6 79 24.0 80 2 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 84%84%65-128%
(a) Outside in house control limits.
* = Outside of Control Limits.
69 of 103
JD6181455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2842-BS 2W63864.D 1 03/17/23 TCH n/a n/a V2W2842
V2W2842-BSD 2W63865.D 1 03/17/23 TCH n/a n/a V2W2842
The QC reported here applies to the following samples:Method: TO-15
JD61814-2, JD61814-5
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 9.8 98 9.9 99 1 70-130/30
106-99-0 1,3-Butadiene 10 11.2 112 11.3 113 1 70-130/30
71-43-2 Benzene 10 7.7 77 7.9 79 3 70-130/30
75-27-4 Bromodichloromethane 10 8.4 84 8.6 86 2 70-130/30
75-25-2 Bromoform 10 9.3 93 9.4 94 1 70-130/30
74-83-9 Bromomethane 10 10.5 105 10.5 105 0 70-130/30
100-44-7 Benzyl Chloride 10 5.8 58* a 5.9 59* a 2 70-130/30
75-15-0 Carbon disulfide 10 11.4 114 11.4 114 0 70-130/30
108-90-7 Chlorobenzene 10 9.4 94 9.5 95 1 70-130/30
75-00-3 Chloroethane 10 10.7 107 10.9 109 2 70-130/30
67-66-3 Chloroform 10 8.2 82 8.3 83 1 70-130/30
74-87-3 Chloromethane 10 11.5 115 11.7 117 2 70-130/30
56-23-5 Carbon tetrachloride 10 8.7 87 8.9 89 2 70-130/30
110-82-7 Cyclohexane 10 8.3 83 8.6 86 4 70-130/30
75-34-3 1,1-Dichloroethane 10 8.3 83 8.5 85 2 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.5 105 10.3 103 2 70-130/30
106-93-4 1,2-Dibromoethane (EDB)10 8.8 88 9.1 91 3 70-130/30
107-06-2 1,2-Dichloroethane 10 7.2 72 7.4 74 3 70-130/30
78-87-5 1,2-Dichloropropane 10 8.8 88 9.0 90 2 70-130/30
123-91-1 1,4-Dioxane 10 8.3 83 8.4 84 1 70-130/30
75-71-8 Dichlorodifluoromethane 10 9.3 93 9.4 94 1 70-130/30
124-48-1 Dibromochloromethane 10 9.9 99 10.1 101 2 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 8.6 86 8.8 88 2 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 8.8 88 9.0 90 2 70-130/30
10061-01-5 cis-1,3-Dichloropropene 10 8.0 80 8.1 81 1 70-130/30
541-73-1 m-Dichlorobenzene 10 9.8 98 9.9 99 1 70-130/30
95-50-1 o-Dichlorobenzene 10 9.8 98 9.9 99 1 70-130/30
106-46-7 p-Dichlorobenzene 10 9.7 97 9.8 98 1 70-130/30
10061-02-6 trans-1,3-Dichloropropene 10 7.4 74 7.6 76 3 70-130/30
100-41-4 Ethylbenzene 10 7.9 79 7.9 79 0 70-130/30
141-78-6 Ethyl Acetate 10 8.4 84 8.5 85 1 70-130/30
622-96-8 4-Ethyltoluene 10 9.0 90 9.1 91 1 70-130/30
76-13-1 Freon 113 10 11.1 111 11.2 112 1 70-130/30
76-14-2 Freon 114 10 10.6 106 10.6 106 0 70-130/30
142-82-5 Heptane 10 8.3 83 8.4 84 1 70-130/30
87-68-3 Hexachlorobutadiene 10 6.5 65* a 6.5 65* a 0 70-130/30
* = Outside of Control Limits.
70 of 103
JD6181455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2842-BS 2W63864.D 1 03/17/23 TCH n/a n/a V2W2842
V2W2842-BSD 2W63865.D 1 03/17/23 TCH n/a n/a V2W2842
The QC reported here applies to the following samples:Method: TO-15
JD61814-2, JD61814-5
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
110-54-3 Hexane 10 8.2 82 8.4 84 2 70-130/30
591-78-6 2-Hexanone 10 9.1 91 9.4 94 3 70-130/30
67-63-0 Isopropyl Alcohol 10 10.3 103 10.0 100 3 70-130/30
75-09-2 Methylene chloride 10 9.2 92 9.1 91 1 70-130/30
78-93-3 Methyl ethyl ketone 10 8.3 83 8.6 86 4 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 8.5 85 8.7 87 2 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 7.0 70 7.2 72 3 70-130/30
91-20-3 Naphthalene 10 8.1 81 8.1 81 0 70-130/30
115-07-1 Propylene 10 8.5 85 8.6 86 1 70-130/30
100-42-5 Styrene 10 8.9 89 9.0 90 1 70-130/30
71-55-6 1,1,1-Trichloroethane 10 7.6 76 7.7 77 1 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 8.8 88 8.9 89 1 70-130/30
79-00-5 1,1,2-Trichloroethane 10 8.3 83 8.6 86 4 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 7.8 78 7.8 78 0 70-130/30
95-63-6 1,2,4-Trimethylbenzene 10 8.6 86 8.7 87 1 70-130/30
108-67-8 1,3,5-Trimethylbenzene 10 8.6 86 8.7 87 1 70-130/30
127-18-4 Tetrachloroethylene 10 9.5 95 9.8 98 3 70-130/30
109-99-9 Tetrahydrofuran 10 8.7 87 8.8 88 1 70-130/30
108-88-3 Toluene 10 8.2 82 8.4 84 2 70-130/30
79-01-6 Trichloroethylene 10 8.3 83 8.7 87 5 70-130/30
75-69-4 Trichlorofluoromethane 10 9.2 92 9.2 92 0 70-130/30
75-01-4 Vinyl chloride 10 10.9 109 11.1 111 2 70-130/30
108-05-4 Vinyl Acetate 10 9.5 95 9.7 97 2 70-130/30
m,p-Xylene 20 15.4 77 15.6 78 1 70-130/30
95-47-6 o-Xylene 10 7.7 77 7.7 77 0 70-130/30
1330-20-7 Xylenes (total)30 23.1 77 23.4 78 1 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 84%83%65-128%
(a) Outside in house control limits.
* = Outside of Control Limits.
71 of 103
JD6181455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2844-BS 2W63894.D 1 03/20/23 TCH n/a n/a V2W2844
V2W2844-BSD 2W63895.D 1 03/20/23 TCH n/a n/a V2W2844
The QC reported here applies to the following samples:Method: TO-15
JD61814-7, JD61814-9, JD61814-10, JD61814-11, JD61814-13, JD61814-14, JD61814-16
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 9.3 93 9.4 94 1 70-130/30
78-93-3 Methyl ethyl ketone 10 8.4 84 8.5 85 1 70-130/30
109-99-9 Tetrahydrofuran 10 8.6 86 9.0 90 5 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 83%83%65-128%
* = Outside of Control Limits.
72 of 103
JD6181455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-BS 2W63044.D 1 01/26/23 TCH n/a n/a V2W2805
V2W2805-BSD 2W63045.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here applies to the following samples:Method: TO-15
V2W2805-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 9.6 96 9.4 94 2 70-130/30
106-99-0 1,3-Butadiene 10 10.8 108 10.7 107 1 70-130/30
71-43-2 Benzene 10 9.4 94 9.3 93 1 70-130/30
75-27-4 Bromodichloromethane 10 9.8 98 9.9 99 1 70-130/30
75-25-2 Bromoform 10 10.3 103 10.2 102 1 70-130/30
74-83-9 Bromomethane 10 9.1 91 9.0 90 1 70-130/30
100-44-7 Benzyl Chloride 10 7.5 75 7.6 76 1 70-130/30
75-15-0 Carbon disulfide 10 8.9 89 8.7 87 2 70-130/30
108-90-7 Chlorobenzene 10 10.4 104 10.3 103 1 70-130/30
75-00-3 Chloroethane 10 10.3 103 10.2 102 1 70-130/30
67-66-3 Chloroform 10 9.3 93 9.3 93 0 70-130/30
74-87-3 Chloromethane 10 10.7 107 10.5 105 2 70-130/30
56-23-5 Carbon tetrachloride 10 9.8 98 9.7 97 1 70-130/30
110-82-7 Cyclohexane 10 9.8 98 10 100 2 70-130/30
75-34-3 1,1-Dichloroethane 10 10.2 102 10.1 101 1 70-130/30
75-35-4 1,1-Dichloroethylene 10 8.3 83 8.2 82 1 70-130/30
106-93-4 1,2-Dibromoethane (EDB)10 9.8 98 9.9 99 1 70-130/30
107-06-2 1,2-Dichloroethane 10 8.6 86 8.5 85 1 70-130/30
78-87-5 1,2-Dichloropropane 10 10.8 108 10.8 108 0 70-130/30
123-91-1 1,4-Dioxane 10 9.6 96 10.1 101 5 70-130/30
75-71-8 Dichlorodifluoromethane 10 8.5 85 8.3 83 2 70-130/30
124-48-1 Dibromochloromethane 10 10.9 109 11.0 110 1 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 10.3 103 10.2 102 1 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 10.3 103 1 70-130/30
10061-01-5 cis-1,3-Dichloropropene 10 9.6 96 9.6 96 0 70-130/30
541-73-1 m-Dichlorobenzene 10 10.5 105 10.5 105 0 70-130/30
95-50-1 o-Dichlorobenzene 10 10.3 103 10.3 103 0 70-130/30
106-46-7 p-Dichlorobenzene 10 10.6 106 10.5 105 1 70-130/30
10061-02-6 trans-1,3-Dichloropropene 10 9.2 92 9.2 92 0 70-130/30
100-41-4 Ethylbenzene 10 9.4 94 9.3 93 1 70-130/30
141-78-6 Ethyl Acetate 10 10.6 106 10.5 105 1 70-130/30
622-96-8 4-Ethyltoluene 10 10.6 106 10.5 105 1 70-130/30
76-13-1 Freon 113 10 7.8 78 7.7 77 1 70-130/30
76-14-2 Freon 114 10 8.8 88 8.7 87 1 70-130/30
142-82-5 Heptane 10 10.5 105 10.6 106 1 70-130/30
87-68-3 Hexachlorobutadiene 10 7.7 77 7.7 77 0 70-130/30
* = Outside of Control Limits.
73 of 103
JD6181455.2.4
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-BS 2W63044.D 1 01/26/23 TCH n/a n/a V2W2805
V2W2805-BSD 2W63045.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here applies to the following samples:Method: TO-15
V2W2805-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
110-54-3 Hexane 10 10.5 105 10.5 105 0 70-130/30
591-78-6 2-Hexanone 10 11.0 110 11.1 111 1 70-130/30
67-63-0 Isopropyl Alcohol 10 9.5 95 9.4 94 1 70-130/30
75-09-2 Methylene chloride 10 7.4 74 7.3 73 1 70-130/30
78-93-3 Methyl ethyl ketone 10 10.2 102 10.2 102 0 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 10.9 109 10.9 109 0 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 8.7 87 8.8 88 1 70-130/30
91-20-3 Naphthalene 10 9.8 98 9.6 96 2 70-130/30
115-07-1 Propylene 10 11.8 118 11.8 118 0 70-130/30
100-42-5 Styrene 10 10.3 103 10.2 102 1 70-130/30
71-55-6 1,1,1-Trichloroethane 10 9.0 90 9.0 90 0 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 10.3 103 10.2 102 1 70-130/30
79-00-5 1,1,2-Trichloroethane 10 9.9 99 9.9 99 0 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 9.0 90 9.0 90 0 70-130/30
95-63-6 1,2,4-Trimethylbenzene 10 10 100 10.4 104 4 70-130/30
108-67-8 1,3,5-Trimethylbenzene 10 10.6 106 10.1 101 5 70-130/30
127-18-4 Tetrachloroethylene 10 10 100 10 100 0 70-130/30
109-99-9 Tetrahydrofuran 10 10.6 106 10.5 105 1 70-130/30
108-88-3 Toluene 10 9.7 97 9.7 97 0 70-130/30
79-01-6 Trichloroethylene 10 9.8 98 9.9 99 1 70-130/30
75-69-4 Trichlorofluoromethane 10 7.9 79 7.7 77 3 70-130/30
75-01-4 Vinyl chloride 10 10.4 104 10.1 101 3 70-130/30
108-05-4 Vinyl Acetate 10 10.4 104 10.1 101 3 70-130/30
m,p-Xylene 20 18.6 93 18.5 93 1 70-130/30
95-47-6 o-Xylene 10 9.1 91 9.1 91 0 70-130/30
1330-20-7 Xylenes (total)30 27.7 92 27.6 92 0 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 94%93%65-128%
* = Outside of Control Limits.
74 of 103
JD6181455.2.4
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-BS 3W79061.D 1 01/30/23 TCH n/a n/a V3W3115
V3W3115-BSD 3W79062.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 7.1 71 7.0 70 1 70-130/30
106-99-0 1,3-Butadiene 10 8.9 89 8.7 87 2 70-130/30
71-43-2 Benzene 10 10.2 102 10.1 101 1 70-130/30
75-27-4 Bromodichloromethane 10 10.7 107 10.8 108 1 70-130/30
75-25-2 Bromoform 10 12.0 120 11.7 117 3 70-130/30
74-83-9 Bromomethane 10 8.5 85 8.2 82 4 70-130/30
100-44-7 Benzyl Chloride 10 12.6 126 12.5 125 1 70-130/30
75-15-0 Carbon disulfide 10 11.0 110 10.9 109 1 70-130/30
108-90-7 Chlorobenzene 10 11.5 115 11.3 113 2 70-130/30
75-00-3 Chloroethane 10 8.5 85 8.4 84 1 70-130/30
67-66-3 Chloroform 10 11.1 111 11.1 111 0 70-130/30
74-87-3 Chloromethane 10 8.3 83 8.2 82 1 70-130/30
56-23-5 Carbon tetrachloride 10 11.0 110 11.1 111 1 70-130/30
110-82-7 Cyclohexane 10 10.8 108 10.9 109 1 70-130/30
75-34-3 1,1-Dichloroethane 10 10.3 103 10.2 102 1 70-130/30
75-35-4 1,1-Dichloroethylene 10 11.4 114 11.3 113 1 70-130/30
106-93-4 1,2-Dibromoethane (EDB)10 12.1 121 11.9 119 2 70-130/30
107-06-2 1,2-Dichloroethane 10 11.6 116 11.6 116 0 70-130/30
78-87-5 1,2-Dichloropropane 10 9.4 94 9.3 93 1 70-130/30
123-91-1 1,4-Dioxane 10 11.9 119 11.9 119 0 70-130/30
75-71-8 Dichlorodifluoromethane 10 11.9 119 11.8 118 1 70-130/30
124-48-1 Dibromochloromethane 10 10.6 106 10.3 103 3 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 11.2 112 11.1 111 1 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 11.8 118 11.8 118 0 70-130/30
10061-01-5 cis-1,3-Dichloropropene 10 10.7 107 10.7 107 0 70-130/30
541-73-1 m-Dichlorobenzene 10 11.9 119 11.6 116 3 70-130/30
95-50-1 o-Dichlorobenzene 10 11.5 115 11.3 113 2 70-130/30
106-46-7 p-Dichlorobenzene 10 12.6 126 12.4 124 2 70-130/30
10061-02-6 trans-1,3-Dichloropropene 10 10.8 108 10.8 108 0 70-130/30
100-41-4 Ethylbenzene 10 10.9 109 10.8 108 1 70-130/30
141-78-6 Ethyl Acetate 10 10.4 104 10.2 102 2 70-130/30
622-96-8 4-Ethyltoluene 10 12.0 120 11.7 117 3 70-130/30
76-13-1 Freon 113 10 11.8 118 11.5 115 3 70-130/30
76-14-2 Freon 114 10 10.5 105 10.5 105 0 70-130/30
142-82-5 Heptane 10 7.6 76 7.6 76 0 70-130/30
87-68-3 Hexachlorobutadiene 10 12.6 126 12.3 123 2 70-130/30
* = Outside of Control Limits.
75 of 103
JD6181455.2.5
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-BS 3W79061.D 1 01/30/23 TCH n/a n/a V3W3115
V3W3115-BSD 3W79062.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here applies to the following samples:Method: TO-15
V3W3115-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
110-54-3 Hexane 10 9.7 97 9.6 96 1 70-130/30
591-78-6 2-Hexanone 10 10.1 101 10.0 100 1 70-130/30
67-63-0 Isopropyl Alcohol 10 8.6 86 8.6 86 0 70-130/30
75-09-2 Methylene chloride 10 10.3 103 10.2 102 1 70-130/30
78-93-3 Methyl ethyl ketone 10 11.1 111 10.9 109 2 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 9.1 91 9.0 90 1 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 10.9 109 10.9 109 0 70-130/30
91-20-3 Naphthalene 10 13.3 133* a 12.9 129 3 70-130/30
115-07-1 Propylene 10 7.4 74 7.4 74 0 70-130/30
100-42-5 Styrene 10 11.9 119 11.7 117 2 70-130/30
71-55-6 1,1,1-Trichloroethane 10 10.6 106 10.6 106 0 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 11.7 117 11.5 115 2 70-130/30
79-00-5 1,1,2-Trichloroethane 10 10.6 106 10.6 106 0 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 14.4 144* a 13.9 139* a 4 70-130/30
95-63-6 1,2,4-Trimethylbenzene 10 11.6 116 11.4 114 2 70-130/30
108-67-8 1,3,5-Trimethylbenzene 10 11.9 119 11.6 116 3 70-130/30
127-18-4 Tetrachloroethylene 10 12.1 121 11.8 118 3 70-130/30
109-99-9 Tetrahydrofuran 10 11.0 110 11.1 111 1 70-130/30
108-88-3 Toluene 10 10.2 102 10.1 101 1 70-130/30
79-01-6 Trichloroethylene 10 10.6 106 10.6 106 0 70-130/30
75-69-4 Trichlorofluoromethane 10 12.3 123 12.1 121 2 70-130/30
75-01-4 Vinyl chloride 10 9.8 98 9.8 98 0 70-130/30
108-05-4 Vinyl Acetate 10 13.0 130 12.9 129 1 70-130/30
m,p-Xylene 20 22.3 112 22.0 110 1 70-130/30
95-47-6 o-Xylene 10 11.0 110 10.8 108 2 70-130/30
1330-20-7 Xylenes (total)30 33.3 111 32.9 110 1 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 101%101%65-128%
(a) High percent recovery and no associated positive reported in the QC batch.
* = Outside of Control Limits.
76 of 103
JD6181455.2.5
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V8W11-BS 8W00252.D 1 02/08/23 TCH n/a n/a V8W11
V8W11-BSD 8W00253.D 1 02/08/23 TCH n/a n/a V8W11
The QC reported here applies to the following samples:Method: TO-15
V8W11-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 9.5 95 9.9 99 4 70-130/30
106-99-0 1,3-Butadiene 10 11.0 110 11.4 114 4 70-130/30
71-43-2 Benzene 10 10.1 101 10.6 106 5 70-130/30
75-27-4 Bromodichloromethane 10 11.0 110 11.2 112 2 70-130/30
75-25-2 Bromoform 10 9.7 97 9.9 99 2 70-130/30
74-83-9 Bromomethane 10 10.2 102 10.7 107 5 70-130/30
100-44-7 Benzyl Chloride 10 7.7 77 8.0 80 4 70-130/30
75-15-0 Carbon disulfide 10 10.9 109 11.4 114 4 70-130/30
108-90-7 Chlorobenzene 10 10.5 105 10.7 107 2 70-130/30
75-00-3 Chloroethane 10 10.7 107 11.1 111 4 70-130/30
67-66-3 Chloroform 10 11.3 113 11.6 116 3 70-130/30
74-87-3 Chloromethane 10 9.6 96 10 100 4 70-130/30
56-23-5 Carbon tetrachloride 10 10.1 101 10.4 104 3 70-130/30
110-82-7 Cyclohexane 10 10.3 103 10.6 106 3 70-130/30
75-34-3 1,1-Dichloroethane 10 10.7 107 11.1 111 4 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.8 108 11.2 112 4 70-130/30
106-93-4 1,2-Dibromoethane (EDB)10 10.5 105 10.8 108 3 70-130/30
107-06-2 1,2-Dichloroethane 10 11.3 113 11.6 116 3 70-130/30
78-87-5 1,2-Dichloropropane 10 10.8 108 11.1 111 3 70-130/30
123-91-1 1,4-Dioxane 10 10.2 102 10.7 107 5 70-130/30
75-71-8 Dichlorodifluoromethane 10 11.5 115 12.3 123 7 70-130/30
124-48-1 Dibromochloromethane 10 10.1 101 10.4 104 3 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 10.2 102 10.6 106 4 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 10.2 102 10.7 107 5 70-130/30
10061-01-5 cis-1,3-Dichloropropene 10 9.3 93 9.7 97 4 70-130/30
541-73-1 m-Dichlorobenzene 10 11.2 112 11.4 114 2 70-130/30
95-50-1 o-Dichlorobenzene 10 11.6 116 11.8 118 2 70-130/30
106-46-7 p-Dichlorobenzene 10 11.2 112 11.4 114 2 70-130/30
10061-02-6 trans-1,3-Dichloropropene 10 9.0 90 9.3 93 3 70-130/30
100-41-4 Ethylbenzene 10 8.9 89 9.2 92 3 70-130/30
141-78-6 Ethyl Acetate 10 11.4 114 11.8 118 3 70-130/30
622-96-8 4-Ethyltoluene 10 11.3 113 11.7 117 3 70-130/30
76-13-1 Freon 113 10 10.5 105 11.0 110 5 70-130/30
76-14-2 Freon 114 10 11.5 115 11.9 119 3 70-130/30
142-82-5 Heptane 10 10.3 103 10.6 106 3 70-130/30
87-68-3 Hexachlorobutadiene 10 10.4 104 10.7 107 3 70-130/30
* = Outside of Control Limits.
77 of 103
JD6181455.2.6
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V8W11-BS 8W00252.D 1 02/08/23 TCH n/a n/a V8W11
V8W11-BSD 8W00253.D 1 02/08/23 TCH n/a n/a V8W11
The QC reported here applies to the following samples:Method: TO-15
V8W11-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
110-54-3 Hexane 10 11.2 112 11.6 116 4 70-130/30
591-78-6 2-Hexanone 10 10.8 108 11.2 112 4 70-130/30
67-63-0 Isopropyl Alcohol 10 9.8 98 10.1 101 3 70-130/30
75-09-2 Methylene chloride 10 10.7 107 11.1 111 4 70-130/30
78-93-3 Methyl ethyl ketone 10 10.4 104 10.9 109 5 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 10.6 106 10.9 109 3 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 9.1 91 9.6 96 5 70-130/30
91-20-3 Naphthalene 10 11.8 118 11.9 119 1 70-130/30
115-07-1 Propylene 10 10.0 100 10.4 104 4 70-130/30
100-42-5 Styrene 10 10.4 104 10.7 107 3 70-130/30
71-55-6 1,1,1-Trichloroethane 10 10.0 100 10.4 104 4 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 11.8 118 12.0 120 2 70-130/30
79-00-5 1,1,2-Trichloroethane 10 11.1 111 11.4 114 3 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 10.8 108 11.1 111 3 70-130/30
95-63-6 1,2,4-Trimethylbenzene 10 12.3 123 12.6 126 2 70-130/30
108-67-8 1,3,5-Trimethylbenzene 10 11.6 116 11.8 118 2 70-130/30
127-18-4 Tetrachloroethylene 10 10.5 105 10.8 108 3 70-130/30
109-99-9 Tetrahydrofuran 10 10.5 105 11.0 110 5 70-130/30
108-88-3 Toluene 10 9.2 92 9.5 95 3 70-130/30
79-01-6 Trichloroethylene 10 10.6 106 10.9 109 3 70-130/30
75-69-4 Trichlorofluoromethane 10 11.4 114 11.8 118 3 70-130/30
75-01-4 Vinyl chloride 10 11.0 110 11.4 114 4 70-130/30
108-05-4 Vinyl Acetate 10 9.3 93 9.8 98 5 70-130/30
m,p-Xylene 20 18.7 94 19.2 96 3 70-130/30
95-47-6 o-Xylene 10 9.5 95 9.7 97 2 70-130/30
1330-20-7 Xylenes (total)30 28.1 94 28.9 96 3 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 101%100%65-128%
* = Outside of Control Limits.
78 of 103
JD6181455.2.6
Duplicate Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD61814-1DUP 2W63842.D 1 03/16/23 TCH n/a n/a V2W2841
JD61814-1 2W63841.D 1 03/16/23 TCH n/a n/a V2W2841
The QC reported here applies to the following samples:Method: TO-15
JD61814-1, JD61814-3, JD61814-4, JD61814-5, JD61814-6, JD61814-7, JD61814-8, JD61814-9, JD61814-10, JD61814-
11, JD61814-12, JD61814-13, JD61814-14, JD61814-15, JD61814-16
JD61814-1 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
67-64-1 Acetone (2-Propanone)9.4 9.3 1 25
106-99-0 1,3-Butadiene ND ND nc 25
71-43-2 Benzene ND ND nc 25
75-27-4 Bromodichloromethane ND ND nc 25
75-25-2 Bromoform ND ND nc 25
74-83-9 Bromomethane ND ND nc 25
100-44-7 Benzyl Chloride ND ND nc 25
75-15-0 Carbon disulfide ND ND nc 25
108-90-7 Chlorobenzene ND ND nc 25
75-00-3 Chloroethane ND ND nc 25
67-66-3 Chloroform ND ND nc 25
74-87-3 Chloromethane 0.53 J 0.44 J 19 25
56-23-5 Carbon tetrachloride ND ND nc 25
110-82-7 Cyclohexane ND ND nc 25
75-34-3 1,1-Dichloroethane ND ND nc 25
75-35-4 1,1-Dichloroethylene ND ND nc 25
106-93-4 1,2-Dibromoethane (EDB)ND ND nc 25
107-06-2 1,2-Dichloroethane ND ND nc 25
78-87-5 1,2-Dichloropropane ND ND nc 25
123-91-1 1,4-Dioxane ND ND nc 25
75-71-8 Dichlorodifluoromethane 0.41 J 0.43 J 5 25
124-48-1 Dibromochloromethane ND ND nc 25
156-60-5 trans-1,2-Dichloroethylene ND ND nc 25
156-59-2 cis-1,2-Dichloroethylene ND ND nc 25
10061-01-5 cis-1,3-Dichloropropene ND ND nc 25
541-73-1 m-Dichlorobenzene ND ND nc 25
95-50-1 o-Dichlorobenzene ND ND nc 25
106-46-7 p-Dichlorobenzene ND ND nc 25
10061-02-6 trans-1,3-Dichloropropene ND ND nc 25
100-41-4 Ethylbenzene ND ND nc 25
141-78-6 Ethyl Acetate 4.7 4.6 2 25
622-96-8 4-Ethyltoluene ND ND nc 25
76-13-1 Freon 113 ND ND nc 25
76-14-2 Freon 114 ND ND nc 25
142-82-5 Heptane 0.46 J 0.43 J 7 25
87-68-3 Hexachlorobutadiene ND ND nc 25
* = Outside of Control Limits.
79 of 103
JD6181455.3.1
Duplicate Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD61814-1DUP 2W63842.D 1 03/16/23 TCH n/a n/a V2W2841
JD61814-1 2W63841.D 1 03/16/23 TCH n/a n/a V2W2841
The QC reported here applies to the following samples:Method: TO-15
JD61814-1, JD61814-3, JD61814-4, JD61814-5, JD61814-6, JD61814-7, JD61814-8, JD61814-9, JD61814-10, JD61814-
11, JD61814-12, JD61814-13, JD61814-14, JD61814-15, JD61814-16
JD61814-1 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
110-54-3 Hexane ND ND nc 25
591-78-6 2-Hexanone ND ND nc 25
67-63-0 Isopropyl Alcohol 1.3 1.2 8 25
75-09-2 Methylene chloride ND ND nc 25
78-93-3 Methyl ethyl ketone 1.6 1.5 6 25
108-10-1 Methyl Isobutyl Ketone ND ND nc 25
1634-04-4 Methyl Tert Butyl Ether ND ND nc 25
91-20-3 Naphthalene ND ND nc 25
115-07-1 Propylene ND ND nc 25
100-42-5 Styrene ND ND nc 25
71-55-6 1,1,1-Trichloroethane ND ND nc 25
79-34-5 1,1,2,2-Tetrachloroethane ND ND nc 25
79-00-5 1,1,2-Trichloroethane ND ND nc 25
120-82-1 1,2,4-Trichlorobenzene ND ND nc 25
95-63-6 1,2,4-Trimethylbenzene ND ND nc 25
108-67-8 1,3,5-Trimethylbenzene ND ND nc 25
127-18-4 Tetrachloroethylene ND ND nc 25
109-99-9 Tetrahydrofuran 67.7 65.2 4 25
108-88-3 Toluene 0.70 J 0.68 J 3 25
79-01-6 Trichloroethylene ND ND nc 25
75-69-4 Trichlorofluoromethane ND ND nc 25
75-01-4 Vinyl chloride ND ND nc 25
108-05-4 Vinyl Acetate ND ND nc 25
m,p-Xylene ND ND nc 25
95-47-6 o-Xylene ND ND nc 25
1330-20-7 Xylenes (total)ND ND nc 25
CAS No.Surrogate Recoveries DUP JD61814-1 Limits
460-00-4 4-Bromofluorobenzene 84%83%65-128%
* = Outside of Control Limits.
80 of 103
JD6181455.3.1
Duplicate Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD61810-1DUP 2W63869.D 1 03/17/23 TCH n/a n/a V2W2842
JD61810-1 2W63868.D 1 03/17/23 TCH n/a n/a V2W2842
The QC reported here applies to the following samples:Method: TO-15
JD61814-2, JD61814-5
JD61810-1 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
67-64-1 Acetone (2-Propanone)27.4 28.3 3 25
106-99-0 1,3-Butadiene ND ND nc 25
71-43-2 Benzene 0.18 J 0.20 11 25
75-27-4 Bromodichloromethane ND ND nc 25
75-25-2 Bromoform ND ND nc 25
74-83-9 Bromomethane ND ND nc 25
100-44-7 Benzyl Chloride ND ND nc 25
75-15-0 Carbon disulfide ND ND nc 25
108-90-7 Chlorobenzene ND ND nc 25
75-00-3 Chloroethane ND ND nc 25
67-66-3 Chloroform 0.10 J 0.10 J 0 25
74-87-3 Chloromethane 0.70 0.71 1 25
56-23-5 Carbon tetrachloride ND ND nc 25
110-82-7 Cyclohexane 2.4 2.5 4 25
75-34-3 1,1-Dichloroethane ND ND nc 25
75-35-4 1,1-Dichloroethylene ND ND nc 25
106-93-4 1,2-Dibromoethane (EDB)ND ND nc 25
107-06-2 1,2-Dichloroethane 0.11 J 0.12 J 9 25
78-87-5 1,2-Dichloropropane 0.20 0.22 10 25
123-91-1 1,4-Dioxane ND ND nc 25
75-71-8 Dichlorodifluoromethane 0.40 0.43 7 25
124-48-1 Dibromochloromethane ND ND nc 25
156-60-5 trans-1,2-Dichloroethylene ND ND nc 25
156-59-2 cis-1,2-Dichloroethylene ND ND nc 25
10061-01-5 cis-1,3-Dichloropropene ND ND nc 25
541-73-1 m-Dichlorobenzene ND ND nc 25
95-50-1 o-Dichlorobenzene ND ND nc 25
106-46-7 p-Dichlorobenzene ND ND nc 25
10061-02-6 trans-1,3-Dichloropropene ND ND nc 25
100-41-4 Ethylbenzene 0.81 0.82 1 25
141-78-6 Ethyl Acetate 40.1 41.5 3 25
622-96-8 4-Ethyltoluene ND ND nc 25
76-13-1 Freon 113 ND ND nc 25
76-14-2 Freon 114 ND ND nc 25
142-82-5 Heptane 0.22 0.25 13 25
87-68-3 Hexachlorobutadiene ND ND nc 25
* = Outside of Control Limits.
81 of 103
JD6181455.3.2
Duplicate Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD61810-1DUP 2W63869.D 1 03/17/23 TCH n/a n/a V2W2842
JD61810-1 2W63868.D 1 03/17/23 TCH n/a n/a V2W2842
The QC reported here applies to the following samples:Method: TO-15
JD61814-2, JD61814-5
JD61810-1 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
110-54-3 Hexane 0.12 J 0.13 J 8 25
591-78-6 2-Hexanone ND ND nc 25
67-63-0 Isopropyl Alcohol 28.8 29.5 2 25
75-09-2 Methylene chloride 0.34 0.33 3 25
78-93-3 Methyl ethyl ketone 0.51 0.55 8 25
108-10-1 Methyl Isobutyl Ketone ND ND nc 25
1634-04-4 Methyl Tert Butyl Ether ND ND nc 25
91-20-3 Naphthalene ND ND nc 25
115-07-1 Propylene ND ND nc 25
100-42-5 Styrene 0.38 0.38 0 25
71-55-6 1,1,1-Trichloroethane ND ND nc 25
79-34-5 1,1,2,2-Tetrachloroethane ND ND nc 25
79-00-5 1,1,2-Trichloroethane ND ND nc 25
120-82-1 1,2,4-Trichlorobenzene ND ND nc 25
95-63-6 1,2,4-Trimethylbenzene 0.12 J 0.12 J 0 25
108-67-8 1,3,5-Trimethylbenzene ND ND nc 25
127-18-4 Tetrachloroethylene 0.063 0.062 2 25
109-99-9 Tetrahydrofuran ND ND nc 25
108-88-3 Toluene 3.1 3.2 3 25
79-01-6 Trichloroethylene ND ND nc 25
75-69-4 Trichlorofluoromethane 0.22 0.23 4 25
75-01-4 Vinyl chloride ND ND nc 25
108-05-4 Vinyl Acetate ND ND nc 25
m,p-Xylene 3.0 3.0 0 25
95-47-6 o-Xylene 1.4 1.4 0 25
1330-20-7 Xylenes (total)4.3 4.4 2 25
CAS No.Surrogate Recoveries DUP JD61810-1 Limits
460-00-4 4-Bromofluorobenzene 86%86%65-128%
* = Outside of Control Limits.
82 of 103
JD6181455.3.2
Duplicate Summary Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD61903-5DUP 2W63899.D 1 03/20/23 TCH n/a n/a V2W2844
JD61903-5 2W63898.D 1 03/20/23 TCH n/a n/a V2W2844
The QC reported here applies to the following samples:Method: TO-15
JD61814-7, JD61814-9, JD61814-10, JD61814-11, JD61814-13, JD61814-14, JD61814-16
JD61903-5 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
67-64-1 Acetone (2-Propanone)3.7 3.7 0 25
78-93-3 Methyl ethyl ketone 0.57 0.56 2 25
109-99-9 Tetrahydrofuran ND ND nc 25
CAS No.Surrogate Recoveries DUP JD61903-5 Limits
460-00-4 4-Bromofluorobenzene 82%82%65-128%
* = Outside of Control Limits.
83 of 103
JD6181455.3.3
Summa Cleaning Certification Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-SCC 2W63050.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here (Summa A501) applies to the following samples:Method: TO-15
Batch CP12063 cleaned 01/19/23: JD61814-8(A676), JD61814-9(A432), JD61814-12(A536), JD61814-14(A1251)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.80 0.58 ppbv ND 1.9 ug/m3
106-99-0 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 ug/m3
71-43-2 Benzene ND 0.80 0.25 ppbv ND 2.6 ug/m3
75-27-4 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 ug/m3
75-25-2 Bromoform ND 0.80 0.28 ppbv ND 8.3 ug/m3
74-83-9 Bromomethane ND 0.80 0.28 ppbv ND 3.1 ug/m3
100-44-7 Benzyl Chloride ND 0.80 0.50 ppbv ND 4.1 ug/m3
75-15-0 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 ug/m3
108-90-7 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 ug/m3
75-00-3 Chloroethane ND 0.80 0.27 ppbv ND 2.1 ug/m3
67-66-3 Chloroform ND 0.80 0.15 ppbv ND 3.9 ug/m3
74-87-3 Chloromethane ND 0.80 0.36 ppbv ND 1.7 ug/m3
56-23-5 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 ug/m3
110-82-7 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 ug/m3
75-34-3 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 ug/m3
107-06-2 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 ug/m3
78-87-5 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 ug/m3
123-91-1 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.80 0.13 ppbv ND 4.0 ug/m3
124-48-1 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 ug/m3
541-73-1 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 ug/m3
95-50-1 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 ug/m3
106-46-7 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 ug/m3
100-41-4 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 ug/m3
141-78-6 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 ug/m3
622-96-8 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 ug/m3
76-13-1 Freon 113 ND 0.80 0.12 ppbv ND 6.1 ug/m3
76-14-2 Freon 114 ND 0.80 0.20 ppbv ND 5.6 ug/m3
142-82-5 Heptane ND 0.80 0.37 ppbv ND 3.3 ug/m3
87-68-3 Hexachlorobutadiene ND 0.80 0.25 ppbv ND 8.5 ug/m3
84 of 103
JD6181455.4.1
Summa Cleaning Certification Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-SCC 2W63050.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here (Summa A501) applies to the following samples:Method: TO-15
Batch CP12063 cleaned 01/19/23: JD61814-8(A676), JD61814-9(A432), JD61814-12(A536), JD61814-14(A1251)
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.80 0.45 ppbv ND 2.8 ug/m3
591-78-6 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 ug/m3
67-63-0 Isopropyl Alcohol ND 0.80 0.56 ppbv ND 2.0 ug/m3
75-09-2 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 ug/m3
78-93-3 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 ug/m3
91-20-3 Naphthalene ND 0.80 0.51 ppbv ND 4.2 ug/m3
115-07-1 Propylene ND 2.0 0.57 ppbv ND 3.4 ug/m3
100-42-5 Styrene ND 0.80 0.47 ppbv ND 3.4 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 ug/m3
127-18-4 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 ug/m3
109-99-9 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 ug/m3
108-88-3 Toluene ND 0.80 0.23 ppbv ND 3.0 ug/m3
79-01-6 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 ug/m3
75-69-4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 ug/m3
75-01-4 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 ug/m3
108-05-4 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 ug/m3
m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 ug/m3
95-47-6 o-Xylene ND 0.80 0.31 ppbv ND 3.5 ug/m3
1330-20-7 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 91%65-128%
85 of 103
JD6181455.4.1
Summa Cleaning Certification Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-SCC 2W63051.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here (Summa A585) applies to the following samples:Method: TO-15
Batch CP12063 cleaned 01/19/23: JD61814-1(A585)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.80 0.58 ppbv ND 1.9 ug/m3
106-99-0 1,3-Butadiene ND 0.80 0.34 ppbv ND 1.8 ug/m3
71-43-2 Benzene ND 0.80 0.25 ppbv ND 2.6 ug/m3
75-27-4 Bromodichloromethane ND 0.80 0.12 ppbv ND 5.4 ug/m3
75-25-2 Bromoform ND 0.80 0.28 ppbv ND 8.3 ug/m3
74-83-9 Bromomethane ND 0.80 0.28 ppbv ND 3.1 ug/m3
100-44-7 Benzyl Chloride ND 0.80 0.50 ppbv ND 4.1 ug/m3
75-15-0 Carbon disulfide ND 0.80 0.18 ppbv ND 2.5 ug/m3
108-90-7 Chlorobenzene ND 0.80 0.30 ppbv ND 3.7 ug/m3
75-00-3 Chloroethane ND 0.80 0.27 ppbv ND 2.1 ug/m3
67-66-3 Chloroform ND 0.80 0.15 ppbv ND 3.9 ug/m3
74-87-3 Chloromethane ND 0.80 0.36 ppbv ND 1.7 ug/m3
56-23-5 Carbon tetrachloride ND 0.80 0.16 ppbv ND 5.0 ug/m3
110-82-7 Cyclohexane ND 0.80 0.44 ppbv ND 2.8 ug/m3
75-34-3 1,1-Dichloroethane ND 0.80 0.23 ppbv ND 3.2 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.80 0.24 ppbv ND 3.2 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.80 0.39 ppbv ND 6.1 ug/m3
107-06-2 1,2-Dichloroethane ND 0.80 0.28 ppbv ND 3.2 ug/m3
78-87-5 1,2-Dichloropropane ND 0.80 0.25 ppbv ND 3.7 ug/m3
123-91-1 1,4-Dioxane ND 0.80 0.47 ppbv ND 2.9 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.80 0.13 ppbv ND 4.0 ug/m3
124-48-1 Dibromochloromethane ND 0.80 0.21 ppbv ND 6.8 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.80 0.28 ppbv ND 3.2 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.80 0.31 ppbv ND 3.2 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.80 0.25 ppbv ND 3.6 ug/m3
541-73-1 m-Dichlorobenzene ND 0.80 0.16 ppbv ND 4.8 ug/m3
95-50-1 o-Dichlorobenzene ND 0.80 0.62 ppbv ND 4.8 ug/m3
106-46-7 p-Dichlorobenzene ND 0.80 0.76 ppbv ND 4.8 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.80 0.40 ppbv ND 3.6 ug/m3
100-41-4 Ethylbenzene ND 0.80 0.24 ppbv ND 3.5 ug/m3
141-78-6 Ethyl Acetate ND 0.80 0.42 ppbv ND 2.9 ug/m3
622-96-8 4-Ethyltoluene ND 0.80 0.38 ppbv ND 3.9 ug/m3
76-13-1 Freon 113 ND 0.80 0.12 ppbv ND 6.1 ug/m3
76-14-2 Freon 114 ND 0.80 0.20 ppbv ND 5.6 ug/m3
142-82-5 Heptane ND 0.80 0.37 ppbv ND 3.3 ug/m3
87-68-3 Hexachlorobutadiene ND 0.80 0.25 ppbv ND 8.5 ug/m3
86 of 103
JD6181455.4.2
Summa Cleaning Certification Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2805-SCC 2W63051.D 1 01/26/23 TCH n/a n/a V2W2805
The QC reported here (Summa A585) applies to the following samples:Method: TO-15
Batch CP12063 cleaned 01/19/23: JD61814-1(A585)
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.80 0.45 ppbv ND 2.8 ug/m3
591-78-6 2-Hexanone ND 0.80 0.58 ppbv ND 3.3 ug/m3
67-63-0 Isopropyl Alcohol ND 0.80 0.56 ppbv ND 2.0 ug/m3
75-09-2 Methylene chloride ND 0.80 0.22 ppbv ND 2.8 ug/m3
78-93-3 Methyl ethyl ketone ND 0.80 0.44 ppbv ND 2.4 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.80 0.29 ppbv ND 3.3 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.80 0.32 ppbv ND 2.9 ug/m3
91-20-3 Naphthalene ND 0.80 0.51 ppbv ND 4.2 ug/m3
115-07-1 Propylene ND 2.0 0.57 ppbv ND 3.4 ug/m3
100-42-5 Styrene ND 0.80 0.47 ppbv ND 3.4 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.80 0.19 ppbv ND 5.5 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.80 0.15 ppbv ND 4.4 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.80 0.48 ppbv ND 5.9 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.80 0.35 ppbv ND 3.9 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.80 0.32 ppbv ND 3.9 ug/m3
127-18-4 Tetrachloroethylene ND 0.16 0.056 ppbv ND 1.1 ug/m3
109-99-9 Tetrahydrofuran ND 0.80 0.36 ppbv ND 2.4 ug/m3
108-88-3 Toluene ND 0.80 0.23 ppbv ND 3.0 ug/m3
79-01-6 Trichloroethylene ND 0.16 0.076 ppbv ND 0.86 ug/m3
75-69-4 Trichlorofluoromethane ND 0.80 0.14 ppbv ND 4.5 ug/m3
75-01-4 Vinyl chloride ND 0.80 0.28 ppbv ND 2.0 ug/m3
108-05-4 Vinyl Acetate ND 0.80 0.45 ppbv ND 2.8 ug/m3
m,p-Xylene ND 0.80 0.56 ppbv ND 3.5 ug/m3
95-47-6 o-Xylene ND 0.80 0.31 ppbv ND 3.5 ug/m3
1330-20-7 Xylenes (total)ND 0.80 0.31 ppbv ND 3.5 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 92%65-128%
87 of 103
JD6181455.4.2
Summa Cleaning Certification Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-SCC 3W79066.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here (Summa A679) applies to the following samples:Method: TO-15
Batch CP12059 cleaned 01/18/23: JD61814-2(A791), JD61814-4(A603), JD61814-5(A439), JD61814-10(A679),
JD61814-15(A497), JD61814-16(M420)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-27-4 Bromodichloromethane ND 0.20 0.030 ppbv ND 1.3 ug/m3
75-25-2 Bromoform ND 0.20 0.071 ppbv ND 2.1 ug/m3
74-83-9 Bromomethane ND 0.20 0.069 ppbv ND 0.78 ug/m3
100-44-7 Benzyl Chloride ND 0.20 0.13 ppbv ND 1.0 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
75-00-3 Chloroethane ND 0.20 0.068 ppbv ND 0.53 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.20 0.097 ppbv ND 1.5 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
78-87-5 1,2-Dichloropropane ND 0.20 0.062 ppbv ND 0.92 ug/m3
123-91-1 1,4-Dioxane ND 0.20 0.12 ppbv ND 0.72 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
124-48-1 Dibromochloromethane ND 0.20 0.052 ppbv ND 1.7 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.20 0.062 ppbv ND 0.91 ug/m3
541-73-1 m-Dichlorobenzene ND 0.20 0.040 ppbv ND 1.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
106-46-7 p-Dichlorobenzene ND 0.20 0.19 ppbv ND 1.2 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.20 0.10 ppbv ND 0.91 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
622-96-8 4-Ethyltoluene ND 0.20 0.095 ppbv ND 0.98 ug/m3
76-13-1 Freon 113 ND 0.20 0.031 ppbv ND 1.5 ug/m3
76-14-2 Freon 114 ND 0.20 0.050 ppbv ND 1.4 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
88 of 103
JD6181455.4.3
Summa Cleaning Certification Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3115-SCC 3W79066.D 1 01/30/23 TCH n/a n/a V3W3115
The QC reported here (Summa A679) applies to the following samples:Method: TO-15
Batch CP12059 cleaned 01/18/23: JD61814-2(A791), JD61814-4(A603), JD61814-5(A439), JD61814-10(A679),
JD61814-15(A497), JD61814-16(M420)
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
591-78-6 2-Hexanone ND 0.20 0.15 ppbv ND 0.82 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
91-20-3 Naphthalene ND 0.20 0.13 ppbv ND 1.0 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
100-42-5 Styrene ND 0.20 0.12 ppbv ND 0.85 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.20 0.087 ppbv ND 0.98 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.20 0.080 ppbv ND 0.98 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
75-69-4 Trichlorofluoromethane ND 0.20 0.036 ppbv ND 1.1 ug/m3
75-01-4 Vinyl chloride ND 0.20 0.069 ppbv ND 0.51 ug/m3
108-05-4 Vinyl Acetate ND 0.20 0.11 ppbv ND 0.70 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 97%65-128%
89 of 103
JD6181455.4.3
Summa Cleaning Certification Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V8W11-SCC 8W00256.D 1 02/08/23 TCH n/a n/a V8W11
The QC reported here (Summa A1232) applies to the following samples:Method: TO-15
Batch CP12088 cleaned 02/04/23: JD61814-3(A490), JD61814-6(A680), JD61814-7(A583), JD61814-11(M205),
JD61814-13(A724)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-27-4 Bromodichloromethane ND 0.20 0.030 ppbv ND 1.3 ug/m3
75-25-2 Bromoform ND 0.20 0.071 ppbv ND 2.1 ug/m3
74-83-9 Bromomethane ND 0.20 0.069 ppbv ND 0.78 ug/m3
100-44-7 Benzyl Chloride ND 0.20 0.13 ppbv ND 1.0 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
75-00-3 Chloroethane ND 0.20 0.068 ppbv ND 0.53 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
106-93-4 1,2-Dibromoethane (EDB)ND 0.20 0.097 ppbv ND 1.5 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
78-87-5 1,2-Dichloropropane ND 0.20 0.062 ppbv ND 0.92 ug/m3
123-91-1 1,4-Dioxane ND 0.20 0.12 ppbv ND 0.72 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
124-48-1 Dibromochloromethane ND 0.20 0.052 ppbv ND 1.7 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
10061-01-5 cis-1,3-Dichloropropene ND 0.20 0.062 ppbv ND 0.91 ug/m3
541-73-1 m-Dichlorobenzene ND 0.20 0.040 ppbv ND 1.2 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
106-46-7 p-Dichlorobenzene ND 0.20 0.19 ppbv ND 1.2 ug/m3
10061-02-6 trans-1,3-Dichloropropene ND 0.20 0.10 ppbv ND 0.91 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
622-96-8 4-Ethyltoluene ND 0.20 0.095 ppbv ND 0.98 ug/m3
76-13-1 Freon 113 ND 0.20 0.031 ppbv ND 1.5 ug/m3
76-14-2 Freon 114 ND 0.20 0.050 ppbv ND 1.4 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
90 of 103
JD6181455.4.4
Summa Cleaning Certification Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V8W11-SCC 8W00256.D 1 02/08/23 TCH n/a n/a V8W11
The QC reported here (Summa A1232) applies to the following samples:Method: TO-15
Batch CP12088 cleaned 02/04/23: JD61814-3(A490), JD61814-6(A680), JD61814-7(A583), JD61814-11(M205),
JD61814-13(A724)
CAS No.Compound Result RL MDL Units Q Result RL Units
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
591-78-6 2-Hexanone ND 0.20 0.15 ppbv ND 0.82 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
91-20-3 Naphthalene ND 0.20 0.13 ppbv ND 1.0 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
100-42-5 Styrene ND 0.20 0.12 ppbv ND 0.85 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
95-63-6 1,2,4-Trimethylbenzene ND 0.20 0.087 ppbv ND 0.98 ug/m3
108-67-8 1,3,5-Trimethylbenzene ND 0.20 0.080 ppbv ND 0.98 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
75-69-4 Trichlorofluoromethane ND 0.20 0.036 ppbv ND 1.1 ug/m3
75-01-4 Vinyl chloride ND 0.20 0.069 ppbv ND 0.51 ug/m3
108-05-4 Vinyl Acetate ND 0.20 0.11 ppbv ND 0.70 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 94%65-128%
91 of 103
JD6181455.4.4
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2776-BFB Injection Date:12/14/22
Lab File ID:2W62382.D Injection Time:17:23
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 13015 22.8 Pass
75 30.0 - 66.0% of mass 95 30880 54.0 Pass
95 Base peak, 100% relative abundance 57157 100.0 Pass
96 5.0 - 9.0% of mass 95 3907 6.84 Pass
173 Less than 2.0% of mass 174 242 0.42 (0.57) a Pass
174 50.0 - 120.0% of mass 95 42512 74.4 Pass
175 4.0 - 9.01% of mass 174 3043 5.32 (7.16) a Pass
176 93.0 - 101.0% of mass 174 40504 70.9 (95.3) a Pass
177 5.0 - 9.0% of mass 176 2767 4.84 (6.83) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2776-IC2776 2W62383.D 12/14/22 17:55 00:32 Initial cal 0.04
V2W2776-IC2776 2W62384.D 12/14/22 18:28 01:05 Initial cal 0.1
V2W2776-IC2776 2W62385.D 12/14/22 18:59 01:36 Initial cal 0.2
V2W2776-IC2776 2W62386.D 12/14/22 19:31 02:08 Initial cal 0.5
V2W2776-IC2776 2W62388.D 12/14/22 20:33 03:10 Initial cal 5
V2W2776-ICC2776 2W62389.D 12/14/22 21:05 03:42 Initial cal 10
V2W2776-IC2776 2W62390.D 12/14/22 21:37 04:14 Initial cal 20
V2W2776-IC2776 2W62391.D 12/14/22 22:12 04:49 Initial cal 40
V2W2776-IC2776 2W62392.D 12/14/22 22:47 05:24 Initial cal 50
V2W2776-ICV2776 2W62395.D 12/15/22 00:22 06:59 Initial cal verification 10
92 of 103
JD6181455.5.1
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2805-BFB Injection Date:01/26/23
Lab File ID:2W63042.D Injection Time:08:09
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 9402 19.9 Pass
75 30.0 - 66.0% of mass 95 22693 48.0 Pass
95 Base peak, 100% relative abundance 47237 100.0 Pass
96 5.0 - 9.0% of mass 95 3157 6.68 Pass
173 Less than 2.0% of mass 174 187 0.40 (0.53) a Pass
174 50.0 - 120.0% of mass 95 35592 75.3 Pass
175 4.0 - 9.01% of mass 174 2486 5.26 (6.98) a Pass
176 93.0 - 101.0% of mass 174 33747 71.4 (94.8) a Pass
177 5.0 - 9.0% of mass 176 2180 4.62 (6.46) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2805-CC2776 2W63043.D 01/26/23 08:43 00:34 Continuing cal 10
V2W2805-BS 2W63044.D 01/26/23 09:30 01:21 Blank Spike
V2W2805-BSD 2W63045.D 01/26/23 10:03 01:54 Blank Spike Duplicate
V2W2805-MB 2W63049.D 01/26/23 12:57 04:48 Method Blank
V2W2805-SCC 2W63050.D 01/26/23 14:11 06:02 Summa Cleaning Certification
V2W2805-SCC 2W63051.D 01/26/23 14:44 06:35 Summa Cleaning Certification
V2W2805-SCC 2W63052.D 01/26/23 15:18 07:09 Summa Cleaning Certification
V2W2805-SCC 2W63053.D 01/26/23 15:51 07:42 Summa Cleaning Certification
ZZZZZZ 2W63054.D 01/26/23 16:25 08:16 (unrelated sample)
JD59186-2 2W63055.D 01/26/23 16:59 08:50 (used for QC only; not part of job JD61814)
JD59186-2DUP 2W63056.D 01/26/23 17:33 09:24 Duplicate
ZZZZZZ 2W63057.D 01/26/23 18:07 09:58 (unrelated sample)
ZZZZZZ 2W63058.D 01/26/23 18:42 10:33 (unrelated sample)
ZZZZZZ 2W63059.D 01/26/23 19:16 11:07 (unrelated sample)
ZZZZZZ 2W63060.D 01/26/23 19:49 11:40 (unrelated sample)
ZZZZZZ 2W63061.D 01/26/23 20:23 12:14 (unrelated sample)
ZZZZZZ 2W63062.D 01/26/23 20:57 12:48 (unrelated sample)
ZZZZZZ 2W63063.D 01/26/23 21:32 13:23 (unrelated sample)
ZZZZZZ 2W63070.D 01/27/23 02:11 18:02 (unrelated sample)
ZZZZZZ 2W63071.D 01/27/23 02:51 18:42 (unrelated sample)
ZZZZZZ 2W63072.D 01/27/23 03:32 19:23 (unrelated sample)
ZZZZZZ 2W63073.D 01/27/23 04:12 20:03 (unrelated sample)
ZZZZZZ 2W63074.D 01/27/23 04:53 20:44 (unrelated sample)
V2W2805-SCC 2W63077.D 01/27/23 06:35 22:26 Summa Cleaning Certification
93 of 103
JD6181455.5.2
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2841-BFB Injection Date:03/16/23
Lab File ID:2W63831.D Injection Time:08:45
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 11735 22.3 Pass
75 30.0 - 66.0% of mass 95 26539 50.4 Pass
95 Base peak, 100% relative abundance 52651 100.0 Pass
96 5.0 - 9.0% of mass 95 3186 6.05 Pass
173 Less than 2.0% of mass 174 270 0.51 (0.66) a Pass
174 50.0 - 120.0% of mass 95 41019 77.9 Pass
175 4.0 - 9.01% of mass 174 2943 5.59 (7.17) a Pass
176 93.0 - 101.0% of mass 174 40291 76.5 (98.2) a Pass
177 5.0 - 9.0% of mass 176 2484 4.72 (6.17) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2841-CC2776 2W63832.D 03/16/23 09:18 00:33 Continuing cal 10
V2W2841-BS 2W63833.D 03/16/23 09:52 01:07 Blank Spike
V2W2841-BSD 2W63834.D 03/16/23 10:26 01:41 Blank Spike Duplicate
V2W2841-MB 2W63836.D 03/16/23 11:45 03:00 Method Blank
ZZZZZZ 2W63837.D 03/16/23 13:23 04:38 (unrelated sample)
ZZZZZZ 2W63838.D 03/16/23 13:56 05:11 (unrelated sample)
ZZZZZZ 2W63839.D 03/16/23 14:30 05:45 (unrelated sample)
ZZZZZZ 2W63840.D 03/16/23 15:02 06:17 (unrelated sample)
JD61814-1 2W63841.D 03/16/23 15:36 06:51 MP-1
JD61814-1DUP 2W63842.D 03/16/23 16:10 07:25 Duplicate
JD61814-3 2W63843.D 03/16/23 16:43 07:58 MP-3
JD61814-4 2W63844.D 03/16/23 17:17 08:32 MP-4
JD61814-5 2W63845.D 03/16/23 17:50 09:05 MP-5
JD61814-7 2W63846.D 03/16/23 18:23 09:38 MP-7
JD61814-8 2W63847.D 03/16/23 18:57 10:12 MP-8
JD61814-12 2W63848.D 03/16/23 19:30 10:45 MP-12
JD61814-13 2W63849.D 03/16/23 20:03 11:18 MP-13
JD61814-14 2W63850.D 03/16/23 20:37 11:52 MP-14
JD61814-15 2W63851.D 03/16/23 21:10 12:25 MP-15
JD61814-16 2W63852.D 03/16/23 21:44 12:59 MP-DUP
JD61814-6 2W63854.D 03/16/23 22:49 14:04 MP-6
JD61814-11 2W63855.D 03/16/23 23:22 14:37 MP-11
JD61814-9 2W63856.D 03/16/23 23:55 15:10 MP-9
JD61814-10 2W63857.D 03/17/23 00:27 15:42 MP-10
94 of 103
JD6181455.5.3
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2842-BFB Injection Date:03/17/23
Lab File ID:2W63861.D Injection Time:09:09
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 11978 21.3 Pass
75 30.0 - 66.0% of mass 95 28765 51.3 Pass
95 Base peak, 100% relative abundance 56104 100.0 Pass
96 5.0 - 9.0% of mass 95 3602 6.42 Pass
173 Less than 2.0% of mass 174 245 0.44 (0.56) a Pass
174 50.0 - 120.0% of mass 95 44075 78.6 Pass
175 4.0 - 9.0% of mass 174 3134 5.59 (7.11) a Pass
176 93.0 - 101.0% of mass 174 43072 76.8 (97.7) a Pass
177 5.0 - 9.0% of mass 176 2551 4.55 (5.92) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2842-CC2776 2W63863.D 03/17/23 10:23 01:14 Continuing cal 10
V2W2842-BS 2W63864.D 03/17/23 11:03 01:54 Blank Spike
V2W2842-BSD 2W63865.D 03/17/23 11:36 02:27 Blank Spike Duplicate
V2W2842-MB 2W63867.D 03/17/23 12:57 03:48 Method Blank
JD61810-1 2W63868.D 03/17/23 13:45 04:36 (used for QC only; not part of job JD61814)
JD61810-1DUP 2W63869.D 03/17/23 14:24 05:15 Duplicate
ZZZZZZ 2W63870.D 03/17/23 16:04 06:55 (unrelated sample)
ZZZZZZ 2W63871.D 03/17/23 16:44 07:35 (unrelated sample)
ZZZZZZ 2W63872.D 03/17/23 17:24 08:15 (unrelated sample)
ZZZZZZ 2W63873.D 03/17/23 18:03 08:54 (unrelated sample)
ZZZZZZ 2W63874.D 03/17/23 18:42 09:33 (unrelated sample)
ZZZZZZ 2W63875.D 03/17/23 19:22 10:13 (unrelated sample)
ZZZZZZ 2W63876.D 03/17/23 20:01 10:52 (unrelated sample)
ZZZZZZ 2W63877.D 03/17/23 20:40 11:31 (unrelated sample)
ZZZZZZ 2W63878.D 03/17/23 21:20 12:11 (unrelated sample)
ZZZZZZ 2W63879.D 03/17/23 22:00 12:51 (unrelated sample)
JD61814-2 2W63880.D 03/17/23 22:33 13:24 MP-2
JD61814-5 2W63881.D 03/17/23 23:05 13:56 MP-5
95 of 103
JD6181455.5.4
Instrument Performance Check (BFB)Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2844-BFB Injection Date:03/20/23
Lab File ID:2W63892.D Injection Time:07:09
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 10405 20.9 Pass
75 30.0 - 66.0% of mass 95 25384 51.1 Pass
95 Base peak, 100% relative abundance 49675 100.0 Pass
96 5.0 - 9.0% of mass 95 3441 6.93 Pass
173 Less than 2.0% of mass 174 232 0.47 (0.59) a Pass
174 50.0 - 120.0% of mass 95 39624 79.8 Pass
175 4.0 - 9.01% of mass 174 3015 6.07 (7.61) a Pass
176 93.0 - 101.0% of mass 174 39125 78.8 (98.7) a Pass
177 5.0 - 9.0% of mass 176 2626 5.29 (6.71) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2844-CC2776 2W63893.D 03/20/23 07:43 00:34 Continuing cal 10
V2W2844-BS 2W63894.D 03/20/23 08:28 01:19 Blank Spike
V2W2844-BSD 2W63895.D 03/20/23 09:03 01:54 Blank Spike Duplicate
V2W2844-MB 2W63897.D 03/20/23 10:42 03:33 Method Blank
JD61903-5 2W63898.D 03/20/23 11:32 04:23 (used for QC only; not part of job JD61814)
JD61903-5DUP 2W63899.D 03/20/23 12:11 05:02 Duplicate
ZZZZZZ 2W63900.D 03/20/23 12:53 05:44 (unrelated sample)
ZZZZZZ 2W63901.D 03/20/23 14:10 07:01 (unrelated sample)
ZZZZZZ 2W63902.D 03/20/23 14:43 07:34 (unrelated sample)
ZZZZZZ 2W63903.D 03/20/23 15:17 08:08 (unrelated sample)
ZZZZZZ 2W63904.D 03/20/23 15:56 08:47 (unrelated sample)
ZZZZZZ 2W63905.D 03/20/23 16:35 09:26 (unrelated sample)
ZZZZZZ 2W63906.D 03/20/23 17:14 10:05 (unrelated sample)
ZZZZZZ 2W63907.D 03/20/23 17:53 10:44 (unrelated sample)
ZZZZZZ 2W63908.D 03/20/23 18:32 11:23 (unrelated sample)
ZZZZZZ 2W63909.D 03/20/23 19:11 12:02 (unrelated sample)
ZZZZZZ 2W63910.D 03/20/23 19:50 12:41 (unrelated sample)
ZZZZZZ 2W63911.D 03/20/23 20:24 13:15 (unrelated sample)
JD61814-7 2W63912.D 03/20/23 20:56 13:47 MP-7
JD61814-13 2W63913.D 03/20/23 21:29 14:20 MP-13
JD61814-14 2W63914.D 03/20/23 22:01 14:52 MP-14
JD61814-16 2W63915.D 03/20/23 22:34 15:25 MP-DUP
JD61814-11 2W63916.D 03/20/23 23:06 15:57 MP-11
JD61814-10 2W63917.D 03/20/23 23:39 16:30 MP-10
96 of 103
JD6181455.5.5
Instrument Performance Check (BFB)Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2844-BFB Injection Date:03/20/23
Lab File ID:2W63892.D Injection Time:07:09
Instrument ID:GCMS2W
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
JD61814-9 2W63918.D 03/21/23 00:12 17:03 MP-9
97 of 103
JD6181455.5.5
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V3W3100-BFB Injection Date:01/06/23
Lab File ID:3W78713.D Injection Time:09:28
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 24491 19.7 Pass
75 30.0 - 66.0% of mass 95 60821 49.0 Pass
95 Base peak, 100% relative abundance 124220 100.0 Pass
96 5.0 - 9.0% of mass 95 8288 6.67 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 91648 73.8 Pass
175 4.0 - 9.01% of mass 174 6856 5.52 (7.48) a Pass
176 93.0 - 101.0% of mass 174 88963 71.6 (97.1) a Pass
177 5.0 - 9.0% of mass 176 5915 4.76 (6.65) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3100-IC3100 3W78714.D 01/06/23 10:20 00:52 Initial cal 0.04
V3W3100-IC3100 3W78715.D 01/06/23 11:00 01:32 Initial cal 0.1
V3W3100-IC3100 3W78716.D 01/06/23 11:40 02:12 Initial cal 0.2
V3W3100-IC3100 3W78717.D 01/06/23 12:21 02:53 Initial cal 0.5
V3W3100-IC3100 3W78719.D 01/06/23 13:39 04:11 Initial cal 5
V3W3100-ICC3100 3W78720.D 01/06/23 14:19 04:51 Initial cal 10
V3W3100-IC3100 3W78721.D 01/06/23 15:01 05:33 Initial cal 20
V3W3100-IC3100 3W78722.D 01/06/23 15:47 06:19 Initial cal 40
V3W3100-IC3100 3W78723.D 01/06/23 16:34 07:06 Initial cal 50
V3W3100-ICV3100 3W78726.D 01/06/23 18:34 09:06 Initial cal verification 10
98 of 103
JD6181455.5.6
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V3W3115-BFB Injection Date:01/30/23
Lab File ID:3W79058.D Injection Time:08:48
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 19875 17.5 Pass
75 30.0 - 66.0% of mass 95 55733 49.1 Pass
95 Base peak, 100% relative abundance 113485 100.0 Pass
96 5.0 - 9.0% of mass 95 8145 7.18 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 91237 80.4 Pass
175 4.0 - 9.01% of mass 174 6705 5.91 (7.35) a Pass
176 93.0 - 101.0% of mass 174 86045 75.8 (94.3) a Pass
177 5.0 - 9.0% of mass 176 5554 4.89 (6.45) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3115-CC3100 3W79060.D 01/30/23 10:14 01:26 Continuing cal 10
V3W3115-BS 3W79061.D 01/30/23 10:57 02:09 Blank Spike
V3W3115-BSD 3W79062.D 01/30/23 11:37 02:49 Blank Spike Duplicate
V3W3115-MB 3W79064.D 01/30/23 13:12 04:24 Method Blank
V3W3115-SCC 3W79066.D 01/30/23 14:38 05:50 Summa Cleaning Certification
JD58999-4 3W79068.D 01/30/23 16:05 07:17 (used for QC only; not part of job JD61814)
JD58999-4DUP 3W79069.D 01/30/23 16:51 08:03 Duplicate
ZZZZZZ 3W79070.D 01/30/23 17:36 08:48 (unrelated sample)
ZZZZZZ 3W79071.D 01/30/23 18:22 09:34 (unrelated sample)
ZZZZZZ 3W79073.D 01/30/23 19:44 10:56 (unrelated sample)
ZZZZZZ 3W79074.D 01/30/23 20:24 11:36 (unrelated sample)
ZZZZZZ 3W79075.D 01/30/23 21:03 12:15 (unrelated sample)
ZZZZZZ 3W79076.D 01/30/23 21:43 12:55 (unrelated sample)
ZZZZZZ 3W79077.D 01/30/23 22:23 13:35 (unrelated sample)
ZZZZZZ 3W79078.D 01/30/23 23:01 14:13 (unrelated sample)
ZZZZZZ 3W79079.D 01/30/23 23:41 14:53 (unrelated sample)
ZZZZZZ 3W79080.D 01/31/23 00:20 15:32 (unrelated sample)
ZZZZZZ 3W79081.D 01/31/23 00:58 16:10 (unrelated sample)
99 of 103
JD6181455.5.7
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V8W1-BFB Injection Date:12/16/22
Lab File ID:8W00006.D Injection Time:16:27
Instrument ID:GCMS8W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 15729 13.6 Pass
75 30.0 - 66.0% of mass 95 56885 49.3 Pass
95 Base peak, 100% relative abundance 115283 100.0 Pass
96 5.0 - 9.0% of mass 95 7956 6.90 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 94600 82.1 Pass
175 4.0 - 9.01% of mass 174 6689 5.80 (7.07) a Pass
176 93.0 - 101.0% of mass 174 91331 79.2 (96.5) a Pass
177 5.0 - 9.0% of mass 176 5825 5.05 (6.38) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V8W1-IC0001 8W00007.D 12/16/22 17:01 00:34 Initial cal 0.04
V8W1-IC0001 8W00008.D 12/16/22 17:35 01:08 Initial cal 0.1
V8W1-IC0001 8W00009.D 12/16/22 18:09 01:42 Initial cal 0.2
V8W1-IC0001 8W00010.D 12/16/22 18:46 02:19 Initial cal 0.5
V8W1-IC0001 8W00012.D 12/16/22 19:56 03:29 Initial cal 5
V8W1-ICC0001 8W00013.D 12/16/22 20:32 04:05 Initial cal 10
V8W1-IC0001 8W00014.D 12/16/22 21:10 04:43 Initial cal 20
V8W1-IC0001 8W00015.D 12/16/22 21:51 05:24 Initial cal 40
V8W1-IC0001 8W00016.D 12/16/22 22:34 06:07 Initial cal 50
V8W1-ICV0001 8W00019.D 12/17/22 00:17 07:50 Initial cal verification 10
100 of 103
JD6181455.5.8
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V8W11-BFB Injection Date:02/08/23
Lab File ID:8W00250.D Injection Time:09:30
Instrument ID:GCMS8W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 14599 14.7 Pass
75 30.0 - 66.0% of mass 95 51725 52.2 Pass
95 Base peak, 100% relative abundance 99021 100.0 Pass
96 5.0 - 9.0% of mass 95 6958 7.03 Pass
173 Less than 2.0% of mass 174 485 0.49 (0.65) a Pass
174 50.0 - 120.0% of mass 95 74747 75.5 Pass
175 4.0 - 9.01% of mass 174 5281 5.33 (7.07) a Pass
176 93.0 - 101.0% of mass 174 71899 72.6 (96.2) a Pass
177 5.0 - 9.0% of mass 176 4746 4.79 (6.60) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V8W11-CC0001 8W00251.D 02/08/23 10:06 00:36 Continuing cal 10
V8W11-BS 8W00252.D 02/08/23 10:47 01:17 Blank Spike
V8W11-BSD 8W00253.D 02/08/23 11:23 01:53 Blank Spike Duplicate
V8W11-MB 8W00255.D 02/08/23 12:46 03:16 Method Blank
V8W11-SCC 8W00256.D 02/08/23 14:15 04:45 Summa Cleaning Certification
V8W11-SCC 8W00257.D 02/08/23 14:56 05:26 Summa Cleaning Certification
V8W11-SCC 8W00258.D 02/08/23 15:37 06:07 Summa Cleaning Certification
101 of 103
JD6181455.5.9
Surrogate Recovery Summary Page 1 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Method:TO-15 Matrix:AIR
Samples and QC shown here apply to the above method
Lab Lab
Sample ID File ID S1
JD61814-1 2W63841.D 83
JD61814-2 2W63880.D 87
JD61814-3 2W63843.D 85
JD61814-4 2W63844.D 86
JD61814-5 2W63881.D 83
JD61814-5 2W63845.D 85
JD61814-6 2W63854.D 88
JD61814-7 2W63912.D 90
JD61814-7 2W63846.D 87
JD61814-8 2W63847.D 83
JD61814-9 2W63918.D 84
JD61814-9 2W63856.D 90
JD61814-10 2W63917.D 85
JD61814-10 2W63857.D 89
JD61814-11 2W63916.D 87
JD61814-11 2W63855.D 87
JD61814-12 2W63848.D 84
JD61814-13 2W63913.D 86
JD61814-13 2W63849.D 87
JD61814-14 2W63914.D 81
JD61814-14 2W63850.D 84
JD61814-15 2W63851.D 83
JD61814-16 2W63915.D 81
JD61814-16 2W63852.D 85
JD61810-1DUP 2W63869.D 86
JD61814-1DUP 2W63842.D 84
JD61903-5DUP 2W63899.D 82
V2W2805-SCC 2W63050.D 91
V2W2805-SCC 2W63051.D 92
V2W2841-BS 2W63833.D 84
V2W2841-BSD 2W63834.D 84
V2W2841-MB 2W63836.D 82
V2W2842-BS 2W63864.D 84
V2W2842-BSD 2W63865.D 83
V2W2842-MB 2W63867.D 82
V2W2844-BS 2W63894.D 83
V2W2844-BSD 2W63895.D 83
V2W2844-MB 2W63897.D 81
V3W3115-SCC 3W79066.D 97
V8W11-SCC 8W00256.D 94
102 of 103
JD6181455.6.1
Surrogate Recovery Summary Page 2 of 2
Job Number:JD61814
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Method:TO-15 Matrix:AIR
Samples and QC shown here apply to the above method
Lab Lab
Sample ID File ID S1
V2W2805-BS 2W63044.D 94
V2W2805-BSD 2W63045.D 93
V2W2805-MB 2W63049.D 91
V3W3115-BS 3W79061.D 101
V3W3115-BSD 3W79062.D 101
V3W3115-MB 3W79064.D 96
V8W11-BS 8W00252.D 101
V8W11-BSD 8W00253.D 100
V8W11-MB 8W00255.D 95
Surrogate Recovery
Compounds Limits
S1 = 4-Bromofluorobenzene 65-128%
103 of 103
JD6181455.6.1
04/06/23
Technical Report for
Hart & Hickman
TKC.008, 13300 Sam Neely Road, Charlotte, NC
TKC-008
SGS Job Number: JD61804
Sampling Date: 03/06/23
Report to:
Hart & Hickman
2923 South Tyron Street Suite 101
Charlotte, NC 28203
[e-mail]; [e-mail]
ATTN: Caleb Brehm
Total number of pages in report:
Certifications: NJ(12129), NY(10983), CA, CT, FL, IL, IN, KS, KY, LA, MA, MD, ME, MN, NC,
OH VAP (CL0056), AK (UST-103), AZ (AZ0786), PA(68-00408), RI, SC, TX, UT, VA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 2235 Route 130 • Dayton, NJ 08810 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Kelly Ramos 732-329-0200
David Chastain
General Manager
Dayton, NJ 04/06/23
e-Hardcopy 2.0
Automated Report
63
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
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how we can serve you better at:
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1 of 63
JD61804
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................8
3.1: JD61804-1: IAS-1 .........................................................................................................9
3.2: JD61804-2: IAS-2 .........................................................................................................11
3.3: JD61804-3: IAS-3 .........................................................................................................13
3.4: JD61804-4: IAS-DUP ...................................................................................................15
3.5: JD61804-5: IAS-BKG ..................................................................................................17
Section 4: Misc. Forms ............................................................................................................19
4.1: Chain of Custody ...........................................................................................................20
4.2: Summa Canister and Flow Controller Log ....................................................................23
Section 5: MS Volatiles - QC Data Summaries .....................................................................24
5.1: Method Blank Summary ................................................................................................25
5.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................34
5.3: Duplicate Summary .......................................................................................................43
5.4: Summa Cleaning Certification ......................................................................................46
5.5: Instrument Performance Checks (BFB) .........................................................................54
5.6: Surrogate Recovery Summaries .....................................................................................63 123452 of 63
JD61804
SGS North America Inc.
Sample Summary
Hart & Hickman
Job No:JD61804
TKC.008, 13300 Sam Neely Road, Charlotte, NC
Project No: TKC-008
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
JD61804-1 03/06/23 15:45 CB 03/09/23 AIR Indoor Air Comp.IAS-1
JD61804-2 03/06/23 15:50 CB 03/09/23 AIR Indoor Air Comp.IAS-2
JD61804-3 03/06/23 15:55 CB 03/09/23 AIR Indoor Air Comp.IAS-3
JD61804-4 03/06/23 00:00 CB 03/09/23 AIR Indoor Air Comp.IAS-DUP
JD61804-5 03/06/23 16:05 CB 03/09/23 AIR Ambient Air Comp.IAS-BKG
3 of 63
JD618041
Summary of Hits Page 1 of 4
Job Number:JD61804
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
JD61804-1 IAS-1
Acetone (2-Propanone)30.8 0.20 0.15 ppbv TO-15
Benzene 0.47 0.20 0.062 ppbv TO-15
Chloromethane 0.60 0.20 0.090 ppbv TO-15
Cyclohexane 0.23 0.20 0.11 ppbv TO-15
Dichlorodifluoromethane 0.42 0.20 0.032 ppbv TO-15
Ethylbenzene 0.40 0.20 0.061 ppbv TO-15
Ethyl Acetate 0.74 0.20 0.10 ppbv TO-15
Heptane 0.37 0.20 0.092 ppbv TO-15
Hexane 0.99 0.20 0.11 ppbv TO-15
Isopropyl Alcohol 2.7 0.20 0.14 ppbv TO-15
Methylene chloride 1.4 0.20 0.056 ppbv TO-15
Methyl ethyl ketone 4.4 0.20 0.11 ppbv TO-15
Tetrahydrofuran 3.4 0.20 0.090 ppbv TO-15
Toluene 5.6 0.20 0.057 ppbv TO-15
m,p-Xylene 1.4 0.20 0.14 ppbv TO-15
o-Xylene 0.50 0.20 0.077 ppbv TO-15
Xylenes (total)1.9 0.20 0.077 ppbv TO-15
Acetone (2-Propanone)73.2 0.48 0.36 ug/m3 TO-15
Benzene 1.5 0.64 0.20 ug/m3 TO-15
Chloromethane 1.2 0.41 0.19 ug/m3 TO-15
Cyclohexane 0.79 0.69 0.38 ug/m3 TO-15
Dichlorodifluoromethane 2.1 0.99 0.16 ug/m3 TO-15
Ethylbenzene 1.7 0.87 0.26 ug/m3 TO-15
Ethyl Acetate 2.7 0.72 0.36 ug/m3 TO-15
Heptane 1.5 0.82 0.38 ug/m3 TO-15
Hexane 3.5 0.70 0.39 ug/m3 TO-15
Isopropyl Alcohol 6.6 0.49 0.34 ug/m3 TO-15
Methylene chloride 4.9 0.69 0.19 ug/m3 TO-15
Methyl ethyl ketone 13 0.59 0.32 ug/m3 TO-15
Tetrahydrofuran 10 0.59 0.27 ug/m3 TO-15
Toluene 21 0.75 0.21 ug/m3 TO-15
m,p-Xylene 6.1 0.87 0.61 ug/m3 TO-15
o-Xylene 2.2 0.87 0.33 ug/m3 TO-15
Xylenes (total)8.3 0.87 0.33 ug/m3 TO-15
JD61804-2 IAS-2
Acetone (2-Propanone)27.3 0.20 0.15 ppbv TO-15
Benzene 0.62 0.20 0.062 ppbv TO-15
Chloromethane 0.55 0.20 0.090 ppbv TO-15
Cyclohexane 0.39 0.20 0.11 ppbv TO-15
Dichlorodifluoromethane 0.40 0.20 0.032 ppbv TO-15
Ethylbenzene 0.58 0.20 0.061 ppbv TO-15
4 of 63
JD618042
Summary of Hits Page 2 of 4
Job Number:JD61804
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Ethyl Acetate 3.6 0.20 0.10 ppbv TO-15
Heptane 0.45 0.20 0.092 ppbv TO-15
Hexane 0.71 0.20 0.11 ppbv TO-15
Isopropyl Alcohol 1.8 0.20 0.14 ppbv TO-15
Methyl ethyl ketone 9.0 0.20 0.11 ppbv TO-15
Methyl Isobutyl Ketone 0.11 J 0.20 0.073 ppbv TO-15
Tetrahydrofuran 6.8 0.20 0.090 ppbv TO-15
Toluene 12.8 0.20 0.057 ppbv TO-15
m,p-Xylene 1.5 0.20 0.14 ppbv TO-15
o-Xylene 0.65 0.20 0.077 ppbv TO-15
Xylenes (total)2.2 0.20 0.077 ppbv TO-15
Acetone (2-Propanone)64.9 0.48 0.36 ug/m3 TO-15
Benzene 2.0 0.64 0.20 ug/m3 TO-15
Chloromethane 1.1 0.41 0.19 ug/m3 TO-15
Cyclohexane 1.3 0.69 0.38 ug/m3 TO-15
Dichlorodifluoromethane 2.0 0.99 0.16 ug/m3 TO-15
Ethylbenzene 2.5 0.87 0.26 ug/m3 TO-15
Ethyl Acetate 13 0.72 0.36 ug/m3 TO-15
Heptane 1.8 0.82 0.38 ug/m3 TO-15
Hexane 2.5 0.70 0.39 ug/m3 TO-15
Isopropyl Alcohol 4.4 0.49 0.34 ug/m3 TO-15
Methyl ethyl ketone 27 0.59 0.32 ug/m3 TO-15
Methyl Isobutyl Ketone 0.45 J 0.82 0.30 ug/m3 TO-15
Tetrahydrofuran 20 0.59 0.27 ug/m3 TO-15
Toluene 48.2 0.75 0.21 ug/m3 TO-15
m,p-Xylene 6.5 0.87 0.61 ug/m3 TO-15
o-Xylene 2.8 0.87 0.33 ug/m3 TO-15
Xylenes (total)9.6 0.87 0.33 ug/m3 TO-15
JD61804-3 IAS-3
Acetone (2-Propanone)70.4 0.80 0.58 ppbv TO-15
Benzene 0.84 0.20 0.062 ppbv TO-15
Carbon disulfide 0.40 0.20 0.045 ppbv TO-15
Chloromethane 0.65 0.20 0.090 ppbv TO-15
Cyclohexane 0.43 0.20 0.11 ppbv TO-15
Dichlorodifluoromethane 0.41 0.20 0.032 ppbv TO-15
Ethylbenzene 0.90 0.20 0.061 ppbv TO-15
Ethyl Acetate 2.0 0.20 0.10 ppbv TO-15
Heptane 0.67 0.20 0.092 ppbv TO-15
Isopropyl Alcohol 4.0 0.20 0.14 ppbv TO-15
Methylene chloride 0.21 0.20 0.056 ppbv TO-15
Methyl ethyl ketone 52.9 0.80 0.44 ppbv TO-15
Methyl Isobutyl Ketone 0.17 J 0.20 0.073 ppbv TO-15
Propylene 4.2 0.50 0.14 ppbv TO-15
5 of 63
JD618042
Summary of Hits Page 3 of 4
Job Number:JD61804
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Tetrahydrofuran 9.2 0.20 0.090 ppbv TO-15
Toluene 15.4 0.20 0.057 ppbv TO-15
m,p-Xylene 2.6 0.20 0.14 ppbv TO-15
o-Xylene 1.8 0.20 0.077 ppbv TO-15
Xylenes (total)4.5 0.20 0.077 ppbv TO-15
Acetone (2-Propanone)167 1.9 1.4 ug/m3 TO-15
Benzene 2.7 0.64 0.20 ug/m3 TO-15
Carbon disulfide 1.2 0.62 0.14 ug/m3 TO-15
Chloromethane 1.3 0.41 0.19 ug/m3 TO-15
Cyclohexane 1.5 0.69 0.38 ug/m3 TO-15
Dichlorodifluoromethane 2.0 0.99 0.16 ug/m3 TO-15
Ethylbenzene 3.9 0.87 0.26 ug/m3 TO-15
Ethyl Acetate 7.2 0.72 0.36 ug/m3 TO-15
Heptane 2.7 0.82 0.38 ug/m3 TO-15
Isopropyl Alcohol 9.8 0.49 0.34 ug/m3 TO-15
Methylene chloride 0.73 0.69 0.19 ug/m3 TO-15
Methyl ethyl ketone 156 2.4 1.3 ug/m3 TO-15
Methyl Isobutyl Ketone 0.70 J 0.82 0.30 ug/m3 TO-15
Propylene 7.2 0.86 0.24 ug/m3 TO-15
Tetrahydrofuran 27 0.59 0.27 ug/m3 TO-15
Toluene 58.0 0.75 0.21 ug/m3 TO-15
m,p-Xylene 11 0.87 0.61 ug/m3 TO-15
o-Xylene 7.8 0.87 0.33 ug/m3 TO-15
Xylenes (total)20 0.87 0.33 ug/m3 TO-15
JD61804-4 IAS-DUP
Acetone (2-Propanone)38.1 0.20 0.15 ppbv TO-15
1,3-Butadiene 0.22 0.20 0.084 ppbv TO-15
Benzene 0.65 0.20 0.062 ppbv TO-15
Chloromethane 0.61 0.20 0.090 ppbv TO-15
Cyclohexane 0.29 0.20 0.11 ppbv TO-15
Dichlorodifluoromethane 0.42 0.20 0.032 ppbv TO-15
Ethylbenzene 0.55 0.20 0.061 ppbv TO-15
Ethyl Acetate 0.83 0.20 0.10 ppbv TO-15
Heptane 0.45 0.20 0.092 ppbv TO-15
Hexane 0.78 0.20 0.11 ppbv TO-15
Isopropyl Alcohol 3.0 0.20 0.14 ppbv TO-15
Methylene chloride 0.20 0.20 0.056 ppbv TO-15
Methyl ethyl ketone 6.3 0.20 0.11 ppbv TO-15
Tetrahydrofuran 4.8 0.20 0.090 ppbv TO-15
Toluene 7.7 0.20 0.057 ppbv TO-15
Trichloroethylene 0.27 0.040 0.019 ppbv TO-15
m,p-Xylene 1.8 0.20 0.14 ppbv TO-15
o-Xylene 0.68 0.20 0.077 ppbv TO-15
6 of 63
JD618042
Summary of Hits Page 4 of 4
Job Number:JD61804
Account:Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Collected:03/06/23
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Xylenes (total)2.5 0.20 0.077 ppbv TO-15
Acetone (2-Propanone)90.5 0.48 0.36 ug/m3 TO-15
1,3-Butadiene 0.49 0.44 0.19 ug/m3 TO-15
Benzene 2.1 0.64 0.20 ug/m3 TO-15
Chloromethane 1.3 0.41 0.19 ug/m3 TO-15
Cyclohexane 1.0 0.69 0.38 ug/m3 TO-15
Dichlorodifluoromethane 2.1 0.99 0.16 ug/m3 TO-15
Ethylbenzene 2.4 0.87 0.26 ug/m3 TO-15
Ethyl Acetate 3.0 0.72 0.36 ug/m3 TO-15
Heptane 1.8 0.82 0.38 ug/m3 TO-15
Hexane 2.7 0.70 0.39 ug/m3 TO-15
Isopropyl Alcohol 7.4 0.49 0.34 ug/m3 TO-15
Methylene chloride 0.69 0.69 0.19 ug/m3 TO-15
Methyl ethyl ketone 19 0.59 0.32 ug/m3 TO-15
Tetrahydrofuran 14 0.59 0.27 ug/m3 TO-15
Toluene 29 0.75 0.21 ug/m3 TO-15
Trichloroethylene 1.5 0.21 0.10 ug/m3 TO-15
m,p-Xylene 7.8 0.87 0.61 ug/m3 TO-15
o-Xylene 3.0 0.87 0.33 ug/m3 TO-15
Xylenes (total)11 0.87 0.33 ug/m3 TO-15
JD61804-5 IAS-BKG
Acetone (2-Propanone)3.0 0.20 0.15 ppbv TO-15
Benzene 0.14 J 0.20 0.062 ppbv TO-15
Chloroform 0.15 J 0.20 0.037 ppbv TO-15
Chloromethane 0.58 0.20 0.090 ppbv TO-15
Dichlorodifluoromethane 0.39 0.20 0.032 ppbv TO-15
Ethyl Acetate 0.96 0.20 0.10 ppbv TO-15
Isopropyl Alcohol 0.27 0.20 0.14 ppbv TO-15
Methylene chloride 0.21 0.20 0.056 ppbv TO-15
Methyl ethyl ketone 0.54 0.20 0.11 ppbv TO-15
Toluene 0.21 0.20 0.057 ppbv TO-15
Acetone (2-Propanone)7.1 0.48 0.36 ug/m3 TO-15
Benzene 0.45 J 0.64 0.20 ug/m3 TO-15
Chloroform 0.73 J 0.98 0.18 ug/m3 TO-15
Chloromethane 1.2 0.41 0.19 ug/m3 TO-15
Dichlorodifluoromethane 1.9 0.99 0.16 ug/m3 TO-15
Ethyl Acetate 3.5 0.72 0.36 ug/m3 TO-15
Isopropyl Alcohol 0.66 0.49 0.34 ug/m3 TO-15
Methylene chloride 0.73 0.69 0.19 ug/m3 TO-15
Methyl ethyl ketone 1.6 0.59 0.32 ug/m3 TO-15
Toluene 0.79 0.75 0.21 ug/m3 TO-15
7 of 63
JD618042
SGS North America Inc.
Sample Results
Report of Analysis
Dayton, NJ
Section 3
8 of 63
JD618043
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:IAS-1
Lab Sample ID:JD61804-1 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A737 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3W79855.D 1 04/03/23 09:09 TCH n/a n/a V3W3149
Run #2
Initial Volume
Run #1 400 ml
Run #2
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)30.8 0.20 0.15 ppbv 73.2 0.48 0.36 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 0.19 ug/m3
71-43-2 78.11 Benzene 0.47 0.20 0.062 ppbv 1.5 0.64 0.20 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 0.14 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 0.34 ug/m3
67-66-3 119.4 Chloroform ND 0.20 0.037 ppbv ND 0.98 0.18 ug/m3
74-87-3 50.49 Chloromethane 0.60 0.20 0.090 ppbv 1.2 0.41 0.19 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 0.25 ug/m3
110-82-7 84.16 Cyclohexane 0.23 0.20 0.11 ppbv 0.79 0.69 0.38 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 0.23 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 0.23 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 0.28 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.42 0.20 0.032 ppbv 2.1 0.99 0.16 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 0.27 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 0.31 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 0.90 ug/m3
100-41-4 106.2 Ethylbenzene 0.40 0.20 0.061 ppbv 1.7 0.87 0.26 ug/m3
141-78-6 88 Ethyl Acetate 0.74 0.20 0.10 ppbv 2.7 0.72 0.36 ug/m3
142-82-5 100.2 Heptane 0.37 0.20 0.092 ppbv 1.5 0.82 0.38 ug/m3
87-68-3 260.8 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 0.66 ug/m3
110-54-3 86.18 Hexane 0.99 0.20 0.11 ppbv 3.5 0.70 0.39 ug/m3
67-63-0 60.1 Isopropyl Alcohol 2.7 0.20 0.14 ppbv 6.6 0.49 0.34 ug/m3
75-09-2 84.94 Methylene chloride 1.4 0.20 0.056 ppbv 4.9 0.69 0.19 ug/m3
78-93-3 72.11 Methyl ethyl ketone 4.4 0.20 0.11 ppbv 13 0.59 0.32 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 0.30 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 0.29 ug/m3
115-07-1 42 Propylene ND 0.50 0.14 ppbv ND 0.86 0.24 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 0.20 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 0.33 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 0.21 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 0.89 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 0.095 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 63
JD6180433.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:IAS-1
Lab Sample ID:JD61804-1 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A737 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran 3.4 0.20 0.090 ppbv 10 0.59 0.27 ug/m3
108-88-3 92.14 Toluene 5.6 0.20 0.057 ppbv 21 0.75 0.21 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 0.10 ug/m3
106.2 m,p-Xylene 1.4 0.20 0.14 ppbv 6.1 0.87 0.61 ug/m3
95-47-6 106.2 o-Xylene 0.50 0.20 0.077 ppbv 2.2 0.87 0.33 ug/m3
1330-20-7 106.2 Xylenes (total)1.9 0.20 0.077 ppbv 8.3 0.87 0.33 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 102%65-128%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 63
JD6180433.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:IAS-2
Lab Sample ID:JD61804-2 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A1869 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3W79860.D 1 04/03/23 14:48 TCH n/a n/a V3W3149
Run #2
Initial Volume
Run #1 400 ml
Run #2
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)27.3 0.20 0.15 ppbv 64.9 0.48 0.36 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 0.19 ug/m3
71-43-2 78.11 Benzene 0.62 0.20 0.062 ppbv 2.0 0.64 0.20 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 0.14 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 0.34 ug/m3
67-66-3 119.4 Chloroform ND 0.20 0.037 ppbv ND 0.98 0.18 ug/m3
74-87-3 50.49 Chloromethane 0.55 0.20 0.090 ppbv 1.1 0.41 0.19 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 0.25 ug/m3
110-82-7 84.16 Cyclohexane 0.39 0.20 0.11 ppbv 1.3 0.69 0.38 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 0.23 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 0.23 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 0.28 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.40 0.20 0.032 ppbv 2.0 0.99 0.16 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 0.27 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 0.31 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 0.90 ug/m3
100-41-4 106.2 Ethylbenzene 0.58 0.20 0.061 ppbv 2.5 0.87 0.26 ug/m3
141-78-6 88 Ethyl Acetate 3.6 0.20 0.10 ppbv 13 0.72 0.36 ug/m3
142-82-5 100.2 Heptane 0.45 0.20 0.092 ppbv 1.8 0.82 0.38 ug/m3
87-68-3 260.8 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 0.66 ug/m3
110-54-3 86.18 Hexane 0.71 0.20 0.11 ppbv 2.5 0.70 0.39 ug/m3
67-63-0 60.1 Isopropyl Alcohol 1.8 0.20 0.14 ppbv 4.4 0.49 0.34 ug/m3
75-09-2 84.94 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 0.19 ug/m3
78-93-3 72.11 Methyl ethyl ketone 9.0 0.20 0.11 ppbv 27 0.59 0.32 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone 0.11 0.20 0.073 ppbv J 0.45 0.82 0.30 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 0.29 ug/m3
115-07-1 42 Propylene ND 0.50 0.14 ppbv ND 0.86 0.24 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 0.20 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 0.33 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 0.21 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 0.89 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 0.095 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 63
JD6180433.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:IAS-2
Lab Sample ID:JD61804-2 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A1869 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran 6.8 0.20 0.090 ppbv 20 0.59 0.27 ug/m3
108-88-3 92.14 Toluene 12.8 0.20 0.057 ppbv 48.2 0.75 0.21 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 0.10 ug/m3
106.2 m,p-Xylene 1.5 0.20 0.14 ppbv 6.5 0.87 0.61 ug/m3
95-47-6 106.2 o-Xylene 0.65 0.20 0.077 ppbv 2.8 0.87 0.33 ug/m3
1330-20-7 106.2 Xylenes (total)2.2 0.20 0.077 ppbv 9.6 0.87 0.33 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 104%65-128%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 63
JD6180433.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:IAS-3
Lab Sample ID:JD61804-3 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A2155 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3W79857.D 1 04/03/23 12:31 TCH n/a n/a V3W3149
Run #2 3W79881.D 1 04/04/23 23:40 TCH n/a n/a V3W3150
Initial Volume
Run #1 400 ml
Run #2 100 ml
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)70.4 a 0.80 0.58 ppbv 167 a 1.9 1.4 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 0.19 ug/m3
71-43-2 78.11 Benzene 0.84 0.20 0.062 ppbv 2.7 0.64 0.20 ug/m3
75-15-0 76.14 Carbon disulfide 0.40 0.20 0.045 ppbv 1.2 0.62 0.14 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 0.34 ug/m3
67-66-3 119.4 Chloroform ND 0.20 0.037 ppbv ND 0.98 0.18 ug/m3
74-87-3 50.49 Chloromethane 0.65 0.20 0.090 ppbv 1.3 0.41 0.19 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 0.25 ug/m3
110-82-7 84.16 Cyclohexane 0.43 0.20 0.11 ppbv 1.5 0.69 0.38 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 0.23 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 0.23 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 0.28 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.41 0.20 0.032 ppbv 2.0 0.99 0.16 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 0.27 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 0.31 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 0.90 ug/m3
100-41-4 106.2 Ethylbenzene 0.90 0.20 0.061 ppbv 3.9 0.87 0.26 ug/m3
141-78-6 88 Ethyl Acetate 2.0 0.20 0.10 ppbv 7.2 0.72 0.36 ug/m3
142-82-5 100.2 Heptane 0.67 0.20 0.092 ppbv 2.7 0.82 0.38 ug/m3
87-68-3 260.8 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 0.66 ug/m3
110-54-3 86.18 Hexane ND 0.20 0.11 ppbv ND 0.70 0.39 ug/m3
67-63-0 60.1 Isopropyl Alcohol 4.0 0.20 0.14 ppbv 9.8 0.49 0.34 ug/m3
75-09-2 84.94 Methylene chloride 0.21 0.20 0.056 ppbv 0.73 0.69 0.19 ug/m3
78-93-3 72.11 Methyl ethyl ketone 52.9 a 0.80 0.44 ppbv 156 a 2.4 1.3 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone 0.17 0.20 0.073 ppbv J 0.70 0.82 0.30 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 0.29 ug/m3
115-07-1 42 Propylene 4.2 0.50 0.14 ppbv 7.2 0.86 0.24 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 0.20 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 0.33 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 0.21 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 0.89 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 0.095 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 63
JD6180433.3
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:IAS-3
Lab Sample ID:JD61804-3 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A2155 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran 9.2 0.20 0.090 ppbv 27 0.59 0.27 ug/m3
108-88-3 92.14 Toluene 15.4 0.20 0.057 ppbv 58.0 0.75 0.21 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 0.10 ug/m3
106.2 m,p-Xylene 2.6 0.20 0.14 ppbv 11 0.87 0.61 ug/m3
95-47-6 106.2 o-Xylene 1.8 0.20 0.077 ppbv 7.8 0.87 0.33 ug/m3
1330-20-7 106.2 Xylenes (total)4.5 0.20 0.077 ppbv 20 0.87 0.33 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 106%109%65-128%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 63
JD6180433.3
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:IAS-DUP
Lab Sample ID:JD61804-4 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A880 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3W79858.D 1 04/03/23 13:18 TCH n/a n/a V3W3149
Run #2
Initial Volume
Run #1 400 ml
Run #2
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)38.1 0.20 0.15 ppbv 90.5 0.48 0.36 ug/m3
106-99-0 54.09 1,3-Butadiene 0.22 0.20 0.084 ppbv 0.49 0.44 0.19 ug/m3
71-43-2 78.11 Benzene 0.65 0.20 0.062 ppbv 2.1 0.64 0.20 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 0.14 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 0.34 ug/m3
67-66-3 119.4 Chloroform ND 0.20 0.037 ppbv ND 0.98 0.18 ug/m3
74-87-3 50.49 Chloromethane 0.61 0.20 0.090 ppbv 1.3 0.41 0.19 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 0.25 ug/m3
110-82-7 84.16 Cyclohexane 0.29 0.20 0.11 ppbv 1.0 0.69 0.38 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 0.23 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 0.23 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 0.28 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.42 0.20 0.032 ppbv 2.1 0.99 0.16 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 0.27 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 0.31 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 0.90 ug/m3
100-41-4 106.2 Ethylbenzene 0.55 0.20 0.061 ppbv 2.4 0.87 0.26 ug/m3
141-78-6 88 Ethyl Acetate 0.83 0.20 0.10 ppbv 3.0 0.72 0.36 ug/m3
142-82-5 100.2 Heptane 0.45 0.20 0.092 ppbv 1.8 0.82 0.38 ug/m3
87-68-3 260.8 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 0.66 ug/m3
110-54-3 86.18 Hexane 0.78 0.20 0.11 ppbv 2.7 0.70 0.39 ug/m3
67-63-0 60.1 Isopropyl Alcohol 3.0 0.20 0.14 ppbv 7.4 0.49 0.34 ug/m3
75-09-2 84.94 Methylene chloride 0.20 0.20 0.056 ppbv 0.69 0.69 0.19 ug/m3
78-93-3 72.11 Methyl ethyl ketone 6.3 0.20 0.11 ppbv 19 0.59 0.32 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 0.30 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 0.29 ug/m3
115-07-1 42 Propylene ND 0.50 0.14 ppbv ND 0.86 0.24 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 0.20 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 0.33 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 0.21 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 0.89 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 0.095 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 63
JD6180433.4
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:IAS-DUP
Lab Sample ID:JD61804-4 Date Sampled:03/06/23
Matrix:AIR - Indoor Air Comp. Summa ID: A880 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran 4.8 0.20 0.090 ppbv 14 0.59 0.27 ug/m3
108-88-3 92.14 Toluene 7.7 0.20 0.057 ppbv 29 0.75 0.21 ug/m3
79-01-6 131.4 Trichloroethylene 0.27 0.040 0.019 ppbv 1.5 0.21 0.10 ug/m3
106.2 m,p-Xylene 1.8 0.20 0.14 ppbv 7.8 0.87 0.61 ug/m3
95-47-6 106.2 o-Xylene 0.68 0.20 0.077 ppbv 3.0 0.87 0.33 ug/m3
1330-20-7 106.2 Xylenes (total)2.5 0.20 0.077 ppbv 11 0.87 0.33 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 105%65-128%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 63
JD6180433.4
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:IAS-BKG
Lab Sample ID:JD61804-5 Date Sampled:03/06/23
Matrix:AIR - Ambient Air Comp. Summa ID: A2055 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 3W79859.D 1 04/03/23 14:04 TCH n/a n/a V3W3149
Run #2
Initial Volume
Run #1 400 ml
Run #2
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
67-64-1 58.08 Acetone (2-Propanone)3.0 0.20 0.15 ppbv 7.1 0.48 0.36 ug/m3
106-99-0 54.09 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 0.19 ug/m3
71-43-2 78.11 Benzene 0.14 0.20 0.062 ppbv J 0.45 0.64 0.20 ug/m3
75-15-0 76.14 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 0.14 ug/m3
108-90-7 112.6 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 0.34 ug/m3
67-66-3 119.4 Chloroform 0.15 0.20 0.037 ppbv J 0.73 0.98 0.18 ug/m3
74-87-3 50.49 Chloromethane 0.58 0.20 0.090 ppbv 1.2 0.41 0.19 ug/m3
56-23-5 153.8 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 0.25 ug/m3
110-82-7 84.16 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 0.38 ug/m3
75-34-3 98.96 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 0.23 ug/m3
75-35-4 96.94 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 0.23 ug/m3
107-06-2 98.96 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 0.28 ug/m3
75-71-8 120.9 Dichlorodifluoromethane 0.39 0.20 0.032 ppbv 1.9 0.99 0.16 ug/m3
156-60-5 96.94 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 0.27 ug/m3
156-59-2 96.94 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 0.31 ug/m3
95-50-1 147 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 0.90 ug/m3
100-41-4 106.2 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 0.26 ug/m3
141-78-6 88 Ethyl Acetate 0.96 0.20 0.10 ppbv 3.5 0.72 0.36 ug/m3
142-82-5 100.2 Heptane ND 0.20 0.092 ppbv ND 0.82 0.38 ug/m3
87-68-3 260.8 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 0.66 ug/m3
110-54-3 86.18 Hexane ND 0.20 0.11 ppbv ND 0.70 0.39 ug/m3
67-63-0 60.1 Isopropyl Alcohol 0.27 0.20 0.14 ppbv 0.66 0.49 0.34 ug/m3
75-09-2 84.94 Methylene chloride 0.21 0.20 0.056 ppbv 0.73 0.69 0.19 ug/m3
78-93-3 72.11 Methyl ethyl ketone 0.54 0.20 0.11 ppbv 1.6 0.59 0.32 ug/m3
108-10-1 100.2 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 0.30 ug/m3
1634-04-4 88.15 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 0.29 ug/m3
115-07-1 42 Propylene ND 0.50 0.14 ppbv ND 0.86 0.24 ug/m3
71-55-6 133.4 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 0.20 ug/m3
79-34-5 167.85 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 0.33 ug/m3
79-00-5 133.4 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 0.21 ug/m3
120-82-1 181.5 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 0.89 ug/m3
127-18-4 165.8 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 0.095 ug/m3
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 63
JD6180433.5
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:IAS-BKG
Lab Sample ID:JD61804-5 Date Sampled:03/06/23
Matrix:AIR - Ambient Air Comp. Summa ID: A2055 Date Received:03/09/23
Method:TO-15 Percent Solids:n/a
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
VTO15 Special list
CAS No.MW Compound Result RL MDL Units Q Result RL MDL Units
109-99-9 72.11 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 0.27 ug/m3
108-88-3 92.14 Toluene 0.21 0.20 0.057 ppbv 0.79 0.75 0.21 ug/m3
79-01-6 131.4 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 0.10 ug/m3
106.2 m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 0.61 ug/m3
95-47-6 106.2 o-Xylene ND 0.20 0.077 ppbv ND 0.87 0.33 ug/m3
1330-20-7 106.2 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 0.33 ug/m3
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
460-00-4 4-Bromofluorobenzene 103%65-128%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 63
JD6180433.5
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
• Summa Canister and Flow Controller Log
Dayton, NJ
Section 4
19 of 63
JD618044
JD61804: Chain of Custody
Page 1 of 3
20 of 63
JD6180444.1
Job Number:JD61804 Client:HART & HICKMAN
Date / Time Received:3/9/2023 10:15:00 AM Delivery Method:FEDEX
Project:TKC.008, CHARLOTTE, NC
4. No. Coolers:N/A
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
N/A
N/A
Quality Control Preservatio Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
SM089-03
Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:231619 pH 12+:203117A Other: (Specify)
JD61804: Chain of Custody
Page 2 of 3
21 of 63
JD6180444.1
TAT (Days):7Received Date:3/9/2023Due Date:3/27/2023Project Description:TKC.008, 13300 Sam Neely Road, Charlotte, NCAccount Name:Hart & HickmanDeliverable:COMMBRequested Date:3/27/2023Job Change Order:JD61804PM:KRC/O Initiated By:KELLY_RAMSample #:JD61804-ALLChange:Please remove from hold and run for VTO15SL1Dept:=========================================================================================================================Client ID:TAT:7Above Changes Per:To Client: This Change Order is confirmation of the revisions, previously discussed with the Client Service Representative.Date/Time:3/27/2023Page 1 of 1Alexis McKenzieJD61804: Chain of Custody
Page 3 of 3
22 of 63
JD6180444.1
Summa Canister and Flow Controller Log Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Received:03/09/23
SUMMA CANISTERS
Shipping Receiving
Summa Vac Date SCC SCC Sample Date Vac Pres Final Dil
ID L " Hg Out By Batch FileID Number In By " Hg psig psig Fact
A737 6 29.4 02/01/23 ML CP118596W26414.D JD61804-1 03/15/23 DG 7 1
A1869 6 29.4 02/01/23 ML CP120628W00106.D JD61804-2 03/15/23 DG 3 1
A2155 6 29.4 02/01/23 ML CP120672W63112.D JD61804-3 03/15/23 DG 5 1
A880 6 29.4 02/01/23 ML CP120618W00145.D JD61804-4 03/15/23 DG 4 1
A2055 6 29.4 01/31/23 ML CP120413W78738.D JD61804-5 03/15/23 DG 7.5 1
FLOW CONTROLLERS / OTHER
Shipping Receiving
Flow Date cc/Time Date cc/Flow
Crtl ID Out By min hrs.In By min RPD Equipment Type
FC1018 01/31/23 ML 10.5 8 03/14/23 ML 10.5 0 Flow Controller
FC1083 01/31/23 ML 10.3 8 03/14/23 ML 10.5 1.9 Flow Controller
FC1090 01/31/23 ML 10.4 8 03/14/23 ML 10.6 1.9 Flow Controller
FC1286 01/31/23 ML 10.3 8 03/13/23 ML 10.5 1.9 Flow Controller
FC1304 01/31/23 ML 10.3 8 03/14/23 ML 10.5 1.9 Flow Controller
SGS Bottle Order(s):
KR-012523-49
Prep Date Room Temp(F)Bar Pres "Hg
01/31/23 70 29.92
02/01/23 70 29.92
23 of 63
JD6180444.2
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
• Instrument Performance Checks (BFB)
• Surrogate Recovery Summaries
Dayton, NJ
Section 5
24 of 63
JD618045
Method Blank Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3149-MB 3W79838.D 1 04/02/23 TCH n/a n/a V3W3149
The QC reported here applies to the following samples:Method: TO-15
JD61804-1, JD61804-2, JD61804-3, JD61804-4, JD61804-5
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
25 of 63
JD6180455.1.1
Method Blank Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3149-MB 3W79838.D 1 04/02/23 TCH n/a n/a V3W3149
The QC reported here applies to the following samples:Method: TO-15
JD61804-1, JD61804-2, JD61804-3, JD61804-4, JD61804-5
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 96%65-128%
26 of 63
JD6180455.1.1
Method Blank Summary Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3150-MB 3W79866.D 1 04/04/23 TCH n/a n/a V3W3150
The QC reported here applies to the following samples:Method: TO-15
JD61804-3
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 93%65-128%
CAS No.Tentatively Identified Compounds R.T.Est. Conc.Units Q
124-38-9 Carbon dioxide 4.09 24 ppbv JN
Total TIC, Volatile 0 ppbv
27 of 63
JD6180455.1.2
Method Blank Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-MB 3W78735.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
28 of 63
JD6180455.1.3
Method Blank Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-MB 3W78735.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 99%65-128%
29 of 63
JD6180455.1.3
Method Blank Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-MB 2W62999.D 1 01/24/23 TCH n/a n/a V2W2802
The QC reported here applies to the following samples:Method: TO-15
V2W2802-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
30 of 63
JD6180455.1.4
Method Blank Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-MB 2W62999.D 1 01/24/23 TCH n/a n/a V2W2802
The QC reported here applies to the following samples:Method: TO-15
V2W2802-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 94%65-128%
31 of 63
JD6180455.1.4
Method Blank Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2806-MB 2W63086.D 1 01/27/23 TCH n/a n/a V2W2806
The QC reported here applies to the following samples:Method: TO-15
V2W2806-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
32 of 63
JD6180455.1.5
Method Blank Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2806-MB 2W63086.D 1 01/27/23 TCH n/a n/a V2W2806
The QC reported here applies to the following samples:Method: TO-15
V2W2806-SCC
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 93%65-128%
33 of 63
JD6180455.1.5
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3149-BS 3W79835.D 1 04/02/23 TCH n/a n/a V3W3149
V3W3149-BSD 3W79836.D 1 04/02/23 TCH n/a n/a V3W3149
The QC reported here applies to the following samples:Method: TO-15
JD61804-1, JD61804-2, JD61804-3, JD61804-4, JD61804-5
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 9.5 95 9.7 97 2 70-130/30
106-99-0 1,3-Butadiene 10 10.4 104 10.4 104 0 70-130/30
71-43-2 Benzene 10 9.6 96 9.8 98 2 70-130/30
75-15-0 Carbon disulfide 10 9.4 94 9.5 95 1 70-130/30
108-90-7 Chlorobenzene 10 10.0 100 10.5 105 5 70-130/30
67-66-3 Chloroform 10 9.2 92 9.4 94 2 70-130/30
74-87-3 Chloromethane 10 9.4 94 9.4 94 0 70-130/30
56-23-5 Carbon tetrachloride 10 10.0 100 10.1 101 1 70-130/30
110-82-7 Cyclohexane 10 9.3 93 9.6 96 3 70-130/30
75-34-3 1,1-Dichloroethane 10 9.0 90 9.1 91 1 70-130/30
75-35-4 1,1-Dichloroethylene 10 9.0 90 9.2 92 2 70-130/30
107-06-2 1,2-Dichloroethane 10 10.2 102 10.4 104 2 70-130/30
75-71-8 Dichlorodifluoromethane 10 9.6 96 9.8 98 2 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 9.4 94 9.5 95 1 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 9.3 93 9.5 95 2 70-130/30
95-50-1 o-Dichlorobenzene 10 11.6 116 12.2 122 5 70-130/30
100-41-4 Ethylbenzene 10 9.8 98 10.3 103 5 70-130/30
141-78-6 Ethyl Acetate 10 10.3 103 10.4 104 1 70-130/30
142-82-5 Heptane 10 10.0 100 10.2 102 2 70-130/30
87-68-3 Hexachlorobutadiene 10 10.9 109 11.4 114 4 70-130/30
110-54-3 Hexane 10 9.5 95 9.7 97 2 70-130/30
67-63-0 Isopropyl Alcohol 10 9.4 94 9.5 95 1 70-130/30
75-09-2 Methylene chloride 10 8.7 87 9.0 90 3 70-130/30
78-93-3 Methyl ethyl ketone 10 9.8 98 10.2 102 4 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 10.6 106 10.9 109 3 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 8.6 86 8.8 88 2 70-130/30
115-07-1 Propylene 10 8.8 88 9.0 90 2 70-130/30
71-55-6 1,1,1-Trichloroethane 10 9.4 94 9.6 96 2 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 10.3 103 10.8 108 5 70-130/30
79-00-5 1,1,2-Trichloroethane 10 9.8 98 10.0 100 2 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 9.9 99 10.4 104 5 70-130/30
127-18-4 Tetrachloroethylene 10 9.7 97 10.2 102 5 70-130/30
109-99-9 Tetrahydrofuran 10 9.6 96 9.8 98 2 70-130/30
108-88-3 Toluene 10 10.1 101 10.4 104 3 70-130/30
79-01-6 Trichloroethylene 10 10.2 102 10.4 104 2 70-130/30
m,p-Xylene 20 20.5 103 21.6 108 5 70-130/30
* = Outside of Control Limits.
34 of 63
JD6180455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3149-BS 3W79835.D 1 04/02/23 TCH n/a n/a V3W3149
V3W3149-BSD 3W79836.D 1 04/02/23 TCH n/a n/a V3W3149
The QC reported here applies to the following samples:Method: TO-15
JD61804-1, JD61804-2, JD61804-3, JD61804-4, JD61804-5
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
95-47-6 o-Xylene 10 10.4 104 11.0 110 6 70-130/30
1330-20-7 Xylenes (total)30 30.9 103 32.6 109 5 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 106%108%65-128%
* = Outside of Control Limits.
35 of 63
JD6180455.2.1
Blank Spike/Blank Spike Duplicate Summary Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3150-BS 3W79863.D 1 04/04/23 TCH n/a n/a V3W3150
V3W3150-BSD 3W79864.D 1 04/04/23 TCH n/a n/a V3W3150
The QC reported here applies to the following samples:Method: TO-15
JD61804-3
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 8.9 89 9.2 92 3 70-130/30
78-93-3 Methyl ethyl ketone 10 9.1 91 9.4 94 3 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 108%111%65-128%
* = Outside of Control Limits.
36 of 63
JD6180455.2.2
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-BS 3W78732.D 1 01/09/23 TCH n/a n/a V3W3101
V3W3101-BSD 3W78733.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 8.2 82 8.0 80 2 70-130/30
106-99-0 1,3-Butadiene 10 11.1 111 10.8 108 3 70-130/30
71-43-2 Benzene 10 10.1 101 10.1 101 0 70-130/30
75-15-0 Carbon disulfide 10 10.5 105 10.6 106 1 70-130/30
108-90-7 Chlorobenzene 10 11.0 110 11.2 112 2 70-130/30
67-66-3 Chloroform 10 9.9 99 10.0 100 1 70-130/30
74-87-3 Chloromethane 10 9.8 98 9.8 98 0 70-130/30
56-23-5 Carbon tetrachloride 10 10.6 106 10.7 107 1 70-130/30
110-82-7 Cyclohexane 10 10.6 106 10.5 105 1 70-130/30
75-34-3 1,1-Dichloroethane 10 10.4 104 10.4 104 0 70-130/30
75-35-4 1,1-Dichloroethylene 10 10.1 101 10.2 102 1 70-130/30
107-06-2 1,2-Dichloroethane 10 10.8 108 10.8 108 0 70-130/30
75-71-8 Dichlorodifluoromethane 10 10.3 103 10.4 104 1 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 9.9 99 9.9 99 0 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 10.4 104 10.5 105 1 70-130/30
95-50-1 o-Dichlorobenzene 10 12.3 123 12.3 123 0 70-130/30
100-41-4 Ethylbenzene 10 10.2 102 10.4 104 2 70-130/30
141-78-6 Ethyl Acetate 10 11.4 114 11.4 114 0 70-130/30
142-82-5 Heptane 10 10.1 101 10.2 102 1 70-130/30
87-68-3 Hexachlorobutadiene 10 12.2 122 12.3 123 1 70-130/30
110-54-3 Hexane 10 10.7 107 10.8 108 1 70-130/30
67-63-0 Isopropyl Alcohol 10 10.7 107 10.7 107 0 70-130/30
75-09-2 Methylene chloride 10 9.4 94 9.5 95 1 70-130/30
78-93-3 Methyl ethyl ketone 10 10.7 107 10.8 108 1 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 10.6 106 10.7 107 1 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 10.4 104 10.3 103 1 70-130/30
115-07-1 Propylene 10 10.1 101 10.2 102 1 70-130/30
71-55-6 1,1,1-Trichloroethane 10 9.7 97 9.7 97 0 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 11.3 113 11.4 114 1 70-130/30
79-00-5 1,1,2-Trichloroethane 10 10.2 102 10.3 103 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 14.6 146* a 14.9 149* a 2 70-130/30
127-18-4 Tetrachloroethylene 10 10.5 105 10.8 108 3 70-130/30
109-99-9 Tetrahydrofuran 10 10.7 107 10.8 108 1 70-130/30
108-88-3 Toluene 10 9.6 96 9.7 97 1 70-130/30
79-01-6 Trichloroethylene 10 10.0 100 10.1 101 1 70-130/30
m,p-Xylene 20 21.3 107 21.5 108 1 70-130/30
* = Outside of Control Limits.
37 of 63
JD6180455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-BS 3W78732.D 1 01/09/23 TCH n/a n/a V3W3101
V3W3101-BSD 3W78733.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here applies to the following samples:Method: TO-15
V3W3101-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
95-47-6 o-Xylene 10 10.7 107 10.7 107 0 70-130/30
1330-20-7 Xylenes (total)30 32.0 107 32.3 108 1 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 103%100%65-128%
(a) High percent recovery and no associated positive reported in the QC batch.
* = Outside of Control Limits.
38 of 63
JD6180455.2.3
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-BS 2W62993.D 1 01/24/23 TCH n/a n/a V2W2802
V2W2802-BSD 2W62994.D 1 01/24/23 TCH n/a n/a V2W2802
The QC reported here applies to the following samples:Method: TO-15
V2W2802-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 9.0 90 9.0 90 0 70-130/30
106-99-0 1,3-Butadiene 10 10.1 101 10.1 101 0 70-130/30
71-43-2 Benzene 10 9.2 92 9.1 91 1 70-130/30
75-15-0 Carbon disulfide 10 8.6 86 8.5 85 1 70-130/30
108-90-7 Chlorobenzene 10 9.3 93 9.5 95 2 70-130/30
67-66-3 Chloroform 10 9.1 91 9.1 91 0 70-130/30
74-87-3 Chloromethane 10 10.3 103 10.0 100 3 70-130/30
56-23-5 Carbon tetrachloride 10 9.6 96 9.4 94 2 70-130/30
110-82-7 Cyclohexane 10 9.5 95 9.5 95 0 70-130/30
75-34-3 1,1-Dichloroethane 10 9.9 99 9.9 99 0 70-130/30
75-35-4 1,1-Dichloroethylene 10 8.0 80 7.9 79 1 70-130/30
107-06-2 1,2-Dichloroethane 10 8.6 86 8.4 84 2 70-130/30
75-71-8 Dichlorodifluoromethane 10 8.2 82 8.2 82 0 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 10 100 9.9 99 1 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 10 100 9.9 99 1 70-130/30
95-50-1 o-Dichlorobenzene 10 9.4 94 9.5 95 1 70-130/30
100-41-4 Ethylbenzene 10 8.5 85 8.6 86 1 70-130/30
141-78-6 Ethyl Acetate 10 10.3 103 10.2 102 1 70-130/30
142-82-5 Heptane 10 10.1 101 10.2 102 1 70-130/30
87-68-3 Hexachlorobutadiene 10 7.0 70 7.2 72 3 70-130/30
110-54-3 Hexane 10 10.2 102 10.1 101 1 70-130/30
67-63-0 Isopropyl Alcohol 10 9.2 92 9.1 91 1 70-130/30
75-09-2 Methylene chloride 10 7.1 71 7.0 70 1 70-130/30
78-93-3 Methyl ethyl ketone 10 10 100 9.9 99 1 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 10.5 105 10.5 105 0 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 8.7 87 8.7 87 0 70-130/30
115-07-1 Propylene 10 11.5 115 11.5 115 0 70-130/30
71-55-6 1,1,1-Trichloroethane 10 8.9 89 8.9 89 0 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 9.2 92 9.4 94 2 70-130/30
79-00-5 1,1,2-Trichloroethane 10 9.5 95 9.6 96 1 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 8.1 81 8.4 84 4 70-130/30
127-18-4 Tetrachloroethylene 10 9.5 95 9.5 95 0 70-130/30
109-99-9 Tetrahydrofuran 10 10.2 102 10.4 104 2 70-130/30
108-88-3 Toluene 10 9.4 94 9.3 93 1 70-130/30
79-01-6 Trichloroethylene 10 9.5 95 9.5 95 0 70-130/30
m,p-Xylene 20 16.8 84 17.2 86 2 70-130/30
* = Outside of Control Limits.
39 of 63
JD6180455.2.4
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-BS 2W62993.D 1 01/24/23 TCH n/a n/a V2W2802
V2W2802-BSD 2W62994.D 1 01/24/23 TCH n/a n/a V2W2802
The QC reported here applies to the following samples:Method: TO-15
V2W2802-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
95-47-6 o-Xylene 10 8.4 84 8.5 85 1 70-130/30
1330-20-7 Xylenes (total)30 25.2 84 25.6 85 2 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 98%97%65-128%
* = Outside of Control Limits.
40 of 63
JD6180455.2.4
Blank Spike/Blank Spike Duplicate Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2806-BS 2W63081.D 1 01/27/23 TCH n/a n/a V2W2806
V2W2806-BSD 2W63082.D 1 01/27/23 TCH n/a n/a V2W2806
The QC reported here applies to the following samples:Method: TO-15
V2W2806-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
67-64-1 Acetone (2-Propanone)10 10.1 101 10.0 100 1 70-130/30
106-99-0 1,3-Butadiene 10 11.7 117 11.7 117 0 70-130/30
71-43-2 Benzene 10 9.8 98 9.8 98 0 70-130/30
75-15-0 Carbon disulfide 10 9.3 93 9.2 92 1 70-130/30
108-90-7 Chlorobenzene 10 10.5 105 10.7 107 2 70-130/30
67-66-3 Chloroform 10 9.8 98 9.9 99 1 70-130/30
74-87-3 Chloromethane 10 11.7 117 11.4 114 3 70-130/30
56-23-5 Carbon tetrachloride 10 10.1 101 10.2 102 1 70-130/30
110-82-7 Cyclohexane 10 10.3 103 10.2 102 1 70-130/30
75-34-3 1,1-Dichloroethane 10 10.7 107 10.9 109 2 70-130/30
75-35-4 1,1-Dichloroethylene 10 8.6 86 8.5 85 1 70-130/30
107-06-2 1,2-Dichloroethane 10 9.3 93 9.4 94 1 70-130/30
75-71-8 Dichlorodifluoromethane 10 8.7 87 8.7 87 0 70-130/30
156-60-5 trans-1,2-Dichloroethylene 10 10.6 106 10.7 107 1 70-130/30
156-59-2 cis-1,2-Dichloroethylene 10 10.6 106 10.7 107 1 70-130/30
95-50-1 o-Dichlorobenzene 10 10.4 104 10.6 106 2 70-130/30
100-41-4 Ethylbenzene 10 9.6 96 9.7 97 1 70-130/30
141-78-6 Ethyl Acetate 10 11.2 112 11.3 113 1 70-130/30
142-82-5 Heptane 10 11.9 119 11.9 119 0 70-130/30
87-68-3 Hexachlorobutadiene 10 7.9 79 8.1 81 2 70-130/30
110-54-3 Hexane 10 11.2 112 11.3 113 1 70-130/30
67-63-0 Isopropyl Alcohol 10 10.7 107 10.8 108 1 70-130/30
75-09-2 Methylene chloride 10 7.5 75 7.6 76 1 70-130/30
78-93-3 Methyl ethyl ketone 10 10.6 106 10.9 109 3 70-130/30
108-10-1 Methyl Isobutyl Ketone 10 11.7 117 11.8 118 1 70-130/30
1634-04-4 Methyl Tert Butyl Ether 10 9.4 94 9.5 95 1 70-130/30
115-07-1 Propylene 10 13.0 130 13.4 134* a 3 70-130/30
71-55-6 1,1,1-Trichloroethane 10 9.5 95 9.6 96 1 70-130/30
79-34-5 1,1,2,2-Tetrachloroethane 10 10.5 105 10.5 105 0 70-130/30
79-00-5 1,1,2-Trichloroethane 10 10.4 104 10.2 102 2 70-130/30
120-82-1 1,2,4-Trichlorobenzene 10 9.2 92 9.3 93 1 70-130/30
127-18-4 Tetrachloroethylene 10 10.2 102 10.3 103 1 70-130/30
109-99-9 Tetrahydrofuran 10 10.9 109 11.0 110 1 70-130/30
108-88-3 Toluene 10 10.0 100 10.1 101 1 70-130/30
79-01-6 Trichloroethylene 10 10.3 103 10.3 103 0 70-130/30
m,p-Xylene 20 19.5 98 19.4 97 1 70-130/30
* = Outside of Control Limits.
41 of 63
JD6180455.2.5
Blank Spike/Blank Spike Duplicate Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2806-BS 2W63081.D 1 01/27/23 TCH n/a n/a V2W2806
V2W2806-BSD 2W63082.D 1 01/27/23 TCH n/a n/a V2W2806
The QC reported here applies to the following samples:Method: TO-15
V2W2806-SCC
Spike BSP BSP BSD BSD Limits
CAS No.Compound ppbv ppbv %ppbv %RPD Rec/RPD
95-47-6 o-Xylene 10 9.5 95 9.5 95 0 70-130/30
1330-20-7 Xylenes (total)30 29.0 97 28.9 96 0 70-130/30
CAS No.Surrogate Recoveries BSP BSD Limits
460-00-4 4-Bromofluorobenzene 93%95%65-128%
(a) Outside in house control limits.
* = Outside of Control Limits.
42 of 63
JD6180455.2.5
Duplicate Summary Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD61958-5DUP 3W79840.D 1 04/02/23 TCH n/a n/a V3W3149
JD61958-5 3W79839.D 1 04/02/23 TCH n/a n/a V3W3149
The QC reported here applies to the following samples:Method: TO-15
JD61804-1, JD61804-2, JD61804-3, JD61804-4, JD61804-5
JD61958-5 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
67-64-1 Acetone (2-Propanone)1.5 1.5 0 25
106-99-0 1,3-Butadiene ND ND nc 25
71-43-2 Benzene 0.15 J 0.15 J 0 25
75-15-0 Carbon disulfide ND ND nc 25
108-90-7 Chlorobenzene ND ND nc 25
67-66-3 Chloroform ND ND nc 25
74-87-3 Chloromethane 0.53 0.56 6 25
56-23-5 Carbon tetrachloride ND ND nc 25
110-82-7 Cyclohexane ND ND nc 25
75-34-3 1,1-Dichloroethane ND ND nc 25
75-35-4 1,1-Dichloroethylene ND ND nc 25
107-06-2 1,2-Dichloroethane ND ND nc 25
75-71-8 Dichlorodifluoromethane 0.40 0.41 2 25
156-60-5 trans-1,2-Dichloroethylene ND ND nc 25
156-59-2 cis-1,2-Dichloroethylene ND ND nc 25
95-50-1 o-Dichlorobenzene ND ND nc 25
100-41-4 Ethylbenzene ND ND nc 25
141-78-6 Ethyl Acetate 0.37 0.37 0 25
142-82-5 Heptane ND ND nc 25
87-68-3 Hexachlorobutadiene ND ND nc 25
110-54-3 Hexane ND ND nc 25
67-63-0 Isopropyl Alcohol 0.77 0.76 1 25
75-09-2 Methylene chloride 0.19 J 0.20 5 25
78-93-3 Methyl ethyl ketone 0.12 J 0.13 J 8 25
108-10-1 Methyl Isobutyl Ketone ND ND nc 25
1634-04-4 Methyl Tert Butyl Ether ND ND nc 25
115-07-1 Propylene 0.38 J 0.38 J 0 25
71-55-6 1,1,1-Trichloroethane ND ND nc 25
79-34-5 1,1,2,2-Tetrachloroethane ND ND nc 25
79-00-5 1,1,2-Trichloroethane ND ND nc 25
120-82-1 1,2,4-Trichlorobenzene ND ND nc 25
127-18-4 Tetrachloroethylene ND ND nc 25
109-99-9 Tetrahydrofuran ND ND nc 25
108-88-3 Toluene 0.16 J 0.16 J 0 25
79-01-6 Trichloroethylene ND ND nc 25
m,p-Xylene ND ND nc 25
* = Outside of Control Limits.
43 of 63
JD6180455.3.1
Duplicate Summary Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD61958-5DUP 3W79840.D 1 04/02/23 TCH n/a n/a V3W3149
JD61958-5 3W79839.D 1 04/02/23 TCH n/a n/a V3W3149
The QC reported here applies to the following samples:Method: TO-15
JD61804-1, JD61804-2, JD61804-3, JD61804-4, JD61804-5
JD61958-5 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
95-47-6 o-Xylene ND ND nc 25
1330-20-7 Xylenes (total)ND ND nc 25
CAS No.Surrogate Recoveries DUP JD61958-5 Limits
460-00-4 4-Bromofluorobenzene 99%102%65-128%
* = Outside of Control Limits.
44 of 63
JD6180455.3.1
Duplicate Summary Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
JD62274-1DUP 3W79872.D 1 04/04/23 TCH n/a n/a V3W3150
JD62274-1 3W79871.D 1 04/04/23 TCH n/a n/a V3W3150
The QC reported here applies to the following samples:Method: TO-15
JD61804-3
JD62274-1 DUP
CAS No.Compound ppbv Q ppbv Q RPD Limits
67-64-1 Acetone (2-Propanone)15.8 16.8 6 25
78-93-3 Methyl ethyl ketone 0.72 0.75 4 25
CAS No.Surrogate Recoveries DUP JD62274-1 Limits
460-00-4 4-Bromofluorobenzene 107%106%65-128%
* = Outside of Control Limits.
45 of 63
JD6180455.3.2
Summa Cleaning Certification Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-SCC 3W78738.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here (Summa A1622) applies to the following samples:Method: TO-15
Batch CP12041 cleaned 01/06/23: JD61804-5(A2055)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
46 of 63
JD6180455.4.1
Summa Cleaning Certification Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3W3101-SCC 3W78738.D 1 01/09/23 TCH n/a n/a V3W3101
The QC reported here (Summa A1622) applies to the following samples:Method: TO-15
Batch CP12041 cleaned 01/06/23: JD61804-5(A2055)
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 97%65-128%
47 of 63
JD6180455.4.1
Summa Cleaning Certification Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-SCC 2W63016.D 1 01/25/23 TCH n/a n/a V2W2802
The QC reported here (Summa A1869) applies to the following samples:Method: TO-15
Batch CP12062 cleaned 01/19/23: JD61804-2(A1869)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
48 of 63
JD6180455.4.2
Summa Cleaning Certification Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-SCC 2W63016.D 1 01/25/23 TCH n/a n/a V2W2802
The QC reported here (Summa A1869) applies to the following samples:Method: TO-15
Batch CP12062 cleaned 01/19/23: JD61804-2(A1869)
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 92%65-128%
49 of 63
JD6180455.4.2
Summa Cleaning Certification Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-SCC 2W63017.D 1 01/25/23 TCH n/a n/a V2W2802
The QC reported here (Summa A880) applies to the following samples:Method: TO-15
Batch CP12061 cleaned 01/18/23: JD61804-4(A880)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
50 of 63
JD6180455.4.3
Summa Cleaning Certification Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2802-SCC 2W63017.D 1 01/25/23 TCH n/a n/a V2W2802
The QC reported here (Summa A880) applies to the following samples:Method: TO-15
Batch CP12061 cleaned 01/18/23: JD61804-4(A880)
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 92%65-128%
51 of 63
JD6180455.4.3
Summa Cleaning Certification Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2806-SCC 2W63110.D 1 01/28/23 TCH n/a n/a V2W2806
The QC reported here (Summa A2155) applies to the following samples:Method: TO-15
Batch CP12067 cleaned 01/19/23: JD61804-3(A2155)
CAS No.Compound Result RL MDL Units Q Result RL Units
67-64-1 Acetone (2-Propanone)ND 0.20 0.15 ppbv ND 0.48 ug/m3
106-99-0 1,3-Butadiene ND 0.20 0.084 ppbv ND 0.44 ug/m3
71-43-2 Benzene ND 0.20 0.062 ppbv ND 0.64 ug/m3
75-15-0 Carbon disulfide ND 0.20 0.045 ppbv ND 0.62 ug/m3
108-90-7 Chlorobenzene ND 0.20 0.074 ppbv ND 0.92 ug/m3
67-66-3 Chloroform ND 0.20 0.037 ppbv ND 0.98 ug/m3
74-87-3 Chloromethane ND 0.20 0.090 ppbv ND 0.41 ug/m3
56-23-5 Carbon tetrachloride ND 0.20 0.040 ppbv ND 1.3 ug/m3
110-82-7 Cyclohexane ND 0.20 0.11 ppbv ND 0.69 ug/m3
75-34-3 1,1-Dichloroethane ND 0.20 0.057 ppbv ND 0.81 ug/m3
75-35-4 1,1-Dichloroethylene ND 0.20 0.059 ppbv ND 0.79 ug/m3
107-06-2 1,2-Dichloroethane ND 0.20 0.070 ppbv ND 0.81 ug/m3
75-71-8 Dichlorodifluoromethane ND 0.20 0.032 ppbv ND 0.99 ug/m3
156-60-5 trans-1,2-Dichloroethylene ND 0.20 0.069 ppbv ND 0.79 ug/m3
156-59-2 cis-1,2-Dichloroethylene ND 0.20 0.077 ppbv ND 0.79 ug/m3
95-50-1 o-Dichlorobenzene ND 0.20 0.15 ppbv ND 1.2 ug/m3
100-41-4 Ethylbenzene ND 0.20 0.061 ppbv ND 0.87 ug/m3
141-78-6 Ethyl Acetate ND 0.20 0.10 ppbv ND 0.72 ug/m3
142-82-5 Heptane ND 0.20 0.092 ppbv ND 0.82 ug/m3
87-68-3 Hexachlorobutadiene ND 0.20 0.062 ppbv ND 2.1 ug/m3
110-54-3 Hexane ND 0.20 0.11 ppbv ND 0.70 ug/m3
67-63-0 Isopropyl Alcohol ND 0.20 0.14 ppbv ND 0.49 ug/m3
75-09-2 Methylene chloride ND 0.20 0.056 ppbv ND 0.69 ug/m3
78-93-3 Methyl ethyl ketone ND 0.20 0.11 ppbv ND 0.59 ug/m3
108-10-1 Methyl Isobutyl Ketone ND 0.20 0.073 ppbv ND 0.82 ug/m3
1634-04-4 Methyl Tert Butyl Ether ND 0.20 0.080 ppbv ND 0.72 ug/m3
115-07-1 Propylene ND 0.50 0.14 ppbv ND 0.86 ug/m3
71-55-6 1,1,1-Trichloroethane ND 0.20 0.037 ppbv ND 1.1 ug/m3
79-34-5 1,1,2,2-Tetrachloroethane ND 0.20 0.048 ppbv ND 1.4 ug/m3
79-00-5 1,1,2-Trichloroethane ND 0.20 0.038 ppbv ND 1.1 ug/m3
120-82-1 1,2,4-Trichlorobenzene ND 0.20 0.12 ppbv ND 1.5 ug/m3
127-18-4 Tetrachloroethylene ND 0.040 0.014 ppbv ND 0.27 ug/m3
109-99-9 Tetrahydrofuran ND 0.20 0.090 ppbv ND 0.59 ug/m3
108-88-3 Toluene ND 0.20 0.057 ppbv ND 0.75 ug/m3
79-01-6 Trichloroethylene ND 0.040 0.019 ppbv ND 0.21 ug/m3
m,p-Xylene ND 0.20 0.14 ppbv ND 0.87 ug/m3
52 of 63
JD6180455.4.4
Summa Cleaning Certification Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V2W2806-SCC 2W63110.D 1 01/28/23 TCH n/a n/a V2W2806
The QC reported here (Summa A2155) applies to the following samples:Method: TO-15
Batch CP12067 cleaned 01/19/23: JD61804-3(A2155)
CAS No.Compound Result RL MDL Units Q Result RL Units
95-47-6 o-Xylene ND 0.20 0.077 ppbv ND 0.87 ug/m3
1330-20-7 Xylenes (total)ND 0.20 0.077 ppbv ND 0.87 ug/m3
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 92%65-128%
53 of 63
JD6180455.4.4
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2776-BFB Injection Date:12/14/22
Lab File ID:2W62382.D Injection Time:17:23
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 13015 22.8 Pass
75 30.0 - 66.0% of mass 95 30880 54.0 Pass
95 Base peak, 100% relative abundance 57157 100.0 Pass
96 5.0 - 9.0% of mass 95 3907 6.84 Pass
173 Less than 2.0% of mass 174 242 0.42 (0.57) a Pass
174 50.0 - 120.0% of mass 95 42512 74.4 Pass
175 4.0 - 9.01% of mass 174 3043 5.32 (7.16) a Pass
176 93.0 - 101.0% of mass 174 40504 70.9 (95.3) a Pass
177 5.0 - 9.0% of mass 176 2767 4.84 (6.83) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2776-IC2776 2W62383.D 12/14/22 17:55 00:32 Initial cal 0.04
V2W2776-IC2776 2W62384.D 12/14/22 18:28 01:05 Initial cal 0.1
V2W2776-IC2776 2W62385.D 12/14/22 18:59 01:36 Initial cal 0.2
V2W2776-IC2776 2W62386.D 12/14/22 19:31 02:08 Initial cal 0.5
V2W2776-IC2776 2W62388.D 12/14/22 20:33 03:10 Initial cal 5
V2W2776-ICC2776 2W62389.D 12/14/22 21:05 03:42 Initial cal 10
V2W2776-IC2776 2W62390.D 12/14/22 21:37 04:14 Initial cal 20
V2W2776-IC2776 2W62391.D 12/14/22 22:12 04:49 Initial cal 40
V2W2776-IC2776 2W62392.D 12/14/22 22:47 05:24 Initial cal 50
V2W2776-ICV2776 2W62395.D 12/15/22 00:22 06:59 Initial cal verification 10
54 of 63
JD6180455.5.1
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2802-BFB Injection Date:01/24/23
Lab File ID:2W62990.D Injection Time:08:55
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 12231 20.9 Pass
75 30.0 - 66.0% of mass 95 28269 48.3 Pass
95 Base peak, 100% relative abundance 58568 100.0 Pass
96 5.0 - 9.0% of mass 95 3913 6.68 Pass
173 Less than 2.0% of mass 174 215 0.37 (0.50) a Pass
174 50.0 - 120.0% of mass 95 43131 73.6 Pass
175 4.0 - 9.01% of mass 174 3061 5.23 (7.10) a Pass
176 93.0 - 101.0% of mass 174 41920 71.6 (97.2) a Pass
177 5.0 - 9.0% of mass 176 2694 4.60 (6.43) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2802-CC2776 2W62992.D 01/24/23 10:36 01:41 Continuing cal 10
V2W2802-BS 2W62993.D 01/24/23 11:17 02:22 Blank Spike
V2W2802-BSD 2W62994.D 01/24/23 11:51 02:56 Blank Spike Duplicate
V2W2802-MB 2W62999.D 01/24/23 15:54 06:59 Method Blank
ZZZZZZ 2W63000.D 01/24/23 16:28 07:33 (unrelated sample)
ZZZZZZ 2W63001.D 01/24/23 17:09 08:14 (unrelated sample)
ZZZZZZ 2W63002.D 01/24/23 17:49 08:54 (unrelated sample)
ZZZZZZ 2W63003.D 01/24/23 18:28 09:33 (unrelated sample)
ZZZZZZ 2W63004.D 01/24/23 19:07 10:12 (unrelated sample)
ZZZZZZ 2W63005.D 01/24/23 19:46 10:51 (unrelated sample)
JD58948-1 2W63006.D 01/24/23 20:26 11:31 (used for QC only; not part of job JD61804)
JD58948-1DUP 2W63007.D 01/24/23 21:05 12:10 Duplicate
ZZZZZZ 2W63008.D 01/24/23 21:44 12:49 (unrelated sample)
ZZZZZZ 2W63009.D 01/24/23 22:24 13:29 (unrelated sample)
ZZZZZZ 2W63010.D 01/24/23 23:04 14:09 (unrelated sample)
ZZZZZZ 2W63011.D 01/24/23 23:44 14:49 (unrelated sample)
V2W2802-SCC 2W63014.D 01/25/23 01:30 16:35 Summa Cleaning Certification
V2W2802-SCC 2W63015.D 01/25/23 02:09 17:14 Summa Cleaning Certification
V2W2802-SCC 2W63016.D 01/25/23 02:49 17:54 Summa Cleaning Certification
V2W2802-SCC 2W63017.D 01/25/23 03:29 18:34 Summa Cleaning Certification
V2W2802-SCC 2W63018.D 01/25/23 04:08 19:13 Summa Cleaning Certification
V2W2802-SCC 2W63019.D 01/25/23 04:48 19:53 Summa Cleaning Certification
55 of 63
JD6180455.5.2
Instrument Performance Check (BFB)Page 1 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2806-BFB Injection Date:01/27/23
Lab File ID:2W63078.D Injection Time:09:37
Instrument ID:GCMS2W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 10918 21.2 Pass
75 30.0 - 66.0% of mass 95 24856 48.3 Pass
95 Base peak, 100% relative abundance 51475 100.0 Pass
96 5.0 - 9.0% of mass 95 3362 6.53 Pass
173 Less than 2.0% of mass 174 182 0.35 (0.49) a Pass
174 50.0 - 120.0% of mass 95 37427 72.7 Pass
175 4.0 - 9.01% of mass 174 2575 5.00 (6.88) a Pass
176 93.0 - 101.0% of mass 174 35661 69.3 (95.3) a Pass
177 5.0 - 9.0% of mass 176 2427 4.71 (6.81) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2806-CC2776 2W63080.D 01/27/23 11:06 01:29 Continuing cal 10
V2W2806-BS 2W63081.D 01/27/23 11:53 02:16 Blank Spike
V2W2806-BSD 2W63082.D 01/27/23 12:27 02:50 Blank Spike Duplicate
V2W2806-MB 2W63086.D 01/27/23 16:22 06:45 Method Blank
ZZZZZZ 2W63087.D 01/27/23 17:06 07:29 (unrelated sample)
ZZZZZZ 2W63089.D 01/27/23 19:01 09:24 (unrelated sample)
JD58656-9R 2W63090.D 01/27/23 19:41 10:04 (used for QC only; not part of job JD61804)
JD58656-9RDUP 2W63091.D 01/27/23 20:20 10:43 Duplicate
ZZZZZZ 2W63092.D 01/27/23 21:00 11:23 (unrelated sample)
ZZZZZZ 2W63093.D 01/27/23 21:39 12:02 (unrelated sample)
ZZZZZZ 2W63094.D 01/27/23 22:18 12:41 (unrelated sample)
ZZZZZZ 2W63095.D 01/27/23 22:57 13:20 (unrelated sample)
ZZZZZZ 2W63096.D 01/27/23 23:36 13:59 (unrelated sample)
ZZZZZZ 2W63097.D 01/28/23 00:16 14:39 (unrelated sample)
ZZZZZZ 2W63098.D 01/28/23 00:55 15:18 (unrelated sample)
ZZZZZZ 2W63099.D 01/28/23 01:28 15:51 (unrelated sample)
ZZZZZZ 2W63100.D 01/28/23 02:01 16:24 (unrelated sample)
ZZZZZZ 2W63101.D 01/28/23 02:35 16:58 (unrelated sample)
ZZZZZZ 2W63102.D 01/28/23 03:08 17:31 (unrelated sample)
ZZZZZZ 2W63103.D 01/28/23 03:47 18:10 (unrelated sample)
ZZZZZZ 2W63104.D 01/28/23 04:21 18:44 (unrelated sample)
ZZZZZZ 2W63108.D 01/28/23 06:36 20:59 (unrelated sample)
V2W2806-SCC 2W63110.D 01/28/23 07:53 22:16 Summa Cleaning Certification
V2W2806-SCC 2W63111.D 01/28/23 08:31 22:54 Summa Cleaning Certification
56 of 63
JD6180455.5.3
Instrument Performance Check (BFB)Page 2 of 2
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V2W2806-BFB Injection Date:01/27/23
Lab File ID:2W63078.D Injection Time:09:37
Instrument ID:GCMS2W
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V2W2806-SCC 2W63112.D 01/28/23 09:10 23:33 Summa Cleaning Certification
V2W2806-SCC 2W63114.D 01/28/23 10:27 24:50 Summa Cleaning Certification
57 of 63
JD6180455.5.3
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V3W3100-BFB Injection Date:01/06/23
Lab File ID:3W78713.D Injection Time:09:28
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 24491 19.7 Pass
75 30.0 - 66.0% of mass 95 60821 49.0 Pass
95 Base peak, 100% relative abundance 124220 100.0 Pass
96 5.0 - 9.0% of mass 95 8288 6.67 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 91648 73.8 Pass
175 4.0 - 9.01% of mass 174 6856 5.52 (7.48) a Pass
176 93.0 - 101.0% of mass 174 88963 71.6 (97.1) a Pass
177 5.0 - 9.0% of mass 176 5915 4.76 (6.65) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3100-IC3100 3W78714.D 01/06/23 10:20 00:52 Initial cal 0.04
V3W3100-IC3100 3W78715.D 01/06/23 11:00 01:32 Initial cal 0.1
V3W3100-IC3100 3W78716.D 01/06/23 11:40 02:12 Initial cal 0.2
V3W3100-IC3100 3W78717.D 01/06/23 12:21 02:53 Initial cal 0.5
V3W3100-IC3100 3W78719.D 01/06/23 13:39 04:11 Initial cal 5
V3W3100-ICC3100 3W78720.D 01/06/23 14:19 04:51 Initial cal 10
V3W3100-IC3100 3W78721.D 01/06/23 15:01 05:33 Initial cal 20
V3W3100-IC3100 3W78722.D 01/06/23 15:47 06:19 Initial cal 40
V3W3100-IC3100 3W78723.D 01/06/23 16:34 07:06 Initial cal 50
V3W3100-ICV3100 3W78726.D 01/06/23 18:34 09:06 Initial cal verification 10
58 of 63
JD6180455.5.4
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V3W3101-BFB Injection Date:01/09/23
Lab File ID:3W78730.D Injection Time:10:32
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 25421 20.3 Pass
75 30.0 - 66.0% of mass 95 61248 49.0 Pass
95 Base peak, 100% relative abundance 124923 100.0 Pass
96 5.0 - 9.0% of mass 95 8149 6.52 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 90531 72.5 Pass
175 4.0 - 9.01% of mass 174 6719 5.38 (7.42) a Pass
176 93.0 - 101.0% of mass 174 87760 70.3 (96.9) a Pass
177 5.0 - 9.0% of mass 176 5809 4.65 (6.62) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3101-CC3100 3W78731.D 01/09/23 11:11 00:39 Continuing cal 10
V3W3101-BS 3W78732.D 01/09/23 11:53 01:21 Blank Spike
V3W3101-BSD 3W78733.D 01/09/23 12:34 02:02 Blank Spike Duplicate
V3W3101-MB 3W78735.D 01/09/23 14:34 04:02 Method Blank
V3W3101-SCC 3W78738.D 01/09/23 16:57 06:25 Summa Cleaning Certification
V3W3101-SCC 3W78739.D 01/09/23 17:42 07:10 Summa Cleaning Certification
V3W3101-SCC 3W78740.D 01/09/23 18:27 07:55 Summa Cleaning Certification
V3W3101-SCC 3W78742.D 01/09/23 19:54 09:22 Summa Cleaning Certification
V3W3101-SCC 3W78743.D 01/09/23 20:34 10:02 Summa Cleaning Certification
V3W3101-SCC 3W78744.D 01/09/23 21:14 10:42 Summa Cleaning Certification
V3W3101-SCC 3W78745.D 01/09/23 21:54 11:22 Summa Cleaning Certification
V3W3101-SCC 3W78746.D 01/09/23 22:33 12:01 Summa Cleaning Certification
V3W3101-SCC 3W78747.D 01/09/23 23:13 12:41 Summa Cleaning Certification
59 of 63
JD6180455.5.5
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V3W3146-BFB Injection Date:03/30/23
Lab File ID:3W79755.D Injection Time:19:26
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 25131 21.4 Pass
75 30.0 - 66.0% of mass 95 55896 47.7 Pass
95 Base peak, 100% relative abundance 117229 100.0 Pass
96 5.0 - 9.0% of mass 95 7739 6.60 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 102621 87.5 Pass
175 4.0 - 9.01% of mass 174 7732 6.60 (7.53) a Pass
176 93.0 - 101.0% of mass 174 97333 83.0 (94.8) a Pass
177 5.0 - 9.0% of mass 176 6716 5.73 (6.90) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3146-IC3146 3W79756.D 03/30/23 20:04 00:38 Initial cal 0.04
V3W3146-IC3146 3W79757.D 03/30/23 20:41 01:15 Initial cal 0.1
V3W3146-IC3146 3W79758.D 03/30/23 21:20 01:54 Initial cal 0.2
V3W3146-IC3146 3W79759.D 03/30/23 22:00 02:34 Initial cal 0.5
V3W3146-IC3146 3W79761.D 03/30/23 23:16 03:50 Initial cal 5
V3W3146-ICC3146 3W79762.D 03/30/23 23:55 04:29 Initial cal 10
V3W3146-IC3146 3W79763.D 03/31/23 00:35 05:09 Initial cal 20
V3W3146-IC3146 3W79764.D 03/31/23 01:20 05:54 Initial cal 40
V3W3146-IC3146 3W79765.D 03/31/23 02:05 06:39 Initial cal 50
V3W3146-ICV3146 3W79768.D 03/31/23 04:02 08:36 Initial cal verification 10
60 of 63
JD6180455.5.6
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V3W3149-BFB Injection Date:04/02/23
Lab File ID:3W79833.D Injection Time:16:53
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 52589 22.5 Pass
75 30.0 - 66.0% of mass 95 114677 49.0 Pass
95 Base peak, 100% relative abundance 233899 100.0 Pass
96 5.0 - 9.0% of mass 95 15395 6.58 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 207637 88.8 Pass
175 4.0 - 9.01% of mass 174 15681 6.70 (7.55) a Pass
176 93.0 - 101.0% of mass 174 199915 85.5 (96.3) a Pass
177 5.0 - 9.0% of mass 176 13331 5.70 (6.67) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3149-CC3146 3W79834.D 04/02/23 17:32 00:39 Continuing cal 10
V3W3149-BS 3W79835.D 04/02/23 18:11 01:18 Blank Spike
V3W3149-BSD 3W79836.D 04/02/23 18:50 01:57 Blank Spike Duplicate
V3W3149-MB 3W79838.D 04/02/23 20:13 03:20 Method Blank
JD61958-5 3W79839.D 04/02/23 20:57 04:04 (used for QC only; not part of job JD61804)
JD61958-5DUP 3W79840.D 04/02/23 21:41 04:48 Duplicate
ZZZZZZ 3W79841.D 04/02/23 22:30 05:37 (unrelated sample)
ZZZZZZ 3W79842.D 04/02/23 23:19 06:26 (unrelated sample)
ZZZZZZ 3W79843.D 04/03/23 00:07 07:14 (unrelated sample)
ZZZZZZ 3W79844.D 04/03/23 00:56 08:03 (unrelated sample)
ZZZZZZ 3W79845.D 04/03/23 01:45 08:52 (unrelated sample)
ZZZZZZ 3W79846.D 04/03/23 02:33 09:40 (unrelated sample)
ZZZZZZ 3W79847.D 04/03/23 03:13 10:20 (unrelated sample)
ZZZZZZ 3W79848.D 04/03/23 03:52 10:59 (unrelated sample)
ZZZZZZ 3W79849.D 04/03/23 04:31 11:38 (unrelated sample)
ZZZZZZ 3W79850.D 04/03/23 05:09 12:16 (unrelated sample)
ZZZZZZ 3W79853.D 04/03/23 07:45 14:52 (unrelated sample)
JD61804-1 3W79855.D 04/03/23 09:09 16:16 IAS-1
JD61804-3 3W79857.D 04/03/23 12:31 19:38 IAS-3
JD61804-4 3W79858.D 04/03/23 13:18 20:25 IAS-DUP
JD61804-5 3W79859.D 04/03/23 14:04 21:11 IAS-BKG
JD61804-2 3W79860.D 04/03/23 14:48 21:55 IAS-2
61 of 63
JD6180455.5.7
Instrument Performance Check (BFB)Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Sample:V3W3150-BFB Injection Date:04/04/23
Lab File ID:3W79861.D Injection Time:08:39
Instrument ID:GCMS3W
Raw % Relative
m/e Ion Abundance Criteria Abundance Abundance Pass/Fail
50 8.0 - 40.0% of mass 95 33160 22.0 Pass
75 30.0 - 66.0% of mass 95 73339 48.6 Pass
95 Base peak, 100% relative abundance 150997 100.0 Pass
96 5.0 - 9.0% of mass 95 10011 6.63 Pass
173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass
174 50.0 - 120.0% of mass 95 142629 94.5 Pass
175 4.0 - 9.01% of mass 174 10889 7.21 (7.63) a Pass
176 93.0 - 101.0% of mass 174 136957 90.7 (96.0) a Pass
177 5.0 - 9.0% of mass 176 9228 6.11 (6.74) b Pass
(a) Value is % of mass 174
(b) Value is % of mass 176
This check applies to the following Samples, MS, MSD, Blanks, and Standards:
Lab Lab Date Time Hours Client
Sample ID File ID Analyzed Analyzed Lapsed Sample ID
V3W3150-CC3146 3W79862.D 04/04/23 09:18 00:39 Continuing cal 10
V3W3150-BS 3W79863.D 04/04/23 10:06 01:27 Blank Spike
V3W3150-BSD 3W79864.D 04/04/23 10:45 02:06 Blank Spike Duplicate
V3W3150-MB 3W79866.D 04/04/23 12:15 03:36 Method Blank
JD62274-1 3W79871.D 04/04/23 16:33 07:54 (used for QC only; not part of job JD61804)
JD62274-1DUP 3W79872.D 04/04/23 17:17 08:38 Duplicate
ZZZZZZ 3W79873.D 04/04/23 18:02 09:23 (unrelated sample)
ZZZZZZ 3W79874.D 04/04/23 18:46 10:07 (unrelated sample)
ZZZZZZ 3W79875.D 04/04/23 19:35 10:56 (unrelated sample)
ZZZZZZ 3W79876.D 04/04/23 20:19 11:40 (unrelated sample)
ZZZZZZ 3W79877.D 04/04/23 21:04 12:25 (unrelated sample)
ZZZZZZ 3W79878.D 04/04/23 21:43 13:04 (unrelated sample)
ZZZZZZ 3W79879.D 04/04/23 22:22 13:43 (unrelated sample)
JD61804-3 3W79881.D 04/04/23 23:40 15:01 IAS-3
ZZZZZZ 3W79882.D 04/05/23 00:19 15:40 (unrelated sample)
ZZZZZZ 3W79883.D 04/05/23 00:58 16:19 (unrelated sample)
ZZZZZZ 3W79884.D 04/05/23 01:42 17:03 (unrelated sample)
ZZZZZZ 3W79885.D 04/05/23 02:27 17:48 (unrelated sample)
62 of 63
JD6180455.5.8
Surrogate Recovery Summary Page 1 of 1
Job Number:JD61804
Account:HAHNCC Hart & Hickman
Project:TKC.008, 13300 Sam Neely Road, Charlotte, NC
Method:TO-15 Matrix:AIR
Samples and QC shown here apply to the above method
Lab Lab
Sample ID File ID S1
JD61804-1 3W79855.D 102
JD61804-2 3W79860.D 104
JD61804-3 3W79881.D 109
JD61804-3 3W79857.D 106
JD61804-4 3W79858.D 105
JD61804-5 3W79859.D 103
JD61958-5DUP 3W79840.D 99
JD62274-1DUP 3W79872.D 107
V2W2802-SCC 2W63017.D 92
V2W2802-SCC 2W63016.D 92
V2W2806-SCC 2W63110.D 92
V3W3101-SCC 3W78738.D 97
V3W3149-BS 3W79835.D 106
V3W3149-BSD 3W79836.D 108
V3W3149-MB 3W79838.D 96
V3W3150-BS 3W79863.D 108
V3W3150-BSD 3W79864.D 111
V3W3150-MB 3W79866.D 93
V2W2802-BS 2W62993.D 98
V2W2802-BSD 2W62994.D 97
V2W2802-MB 2W62999.D 94
V2W2806-BS 2W63081.D 93
V2W2806-BSD 2W63082.D 95
V2W2806-MB 2W63086.D 93
V3W3101-BS 3W78732.D 103
V3W3101-BSD 3W78733.D 100
V3W3101-MB 3W78735.D 99
Surrogate Recovery
Compounds Limits
S1 = 4-Bromofluorobenzene 65-128%
63 of 63
JD6180455.6.1

Appendix H DEQ Risk Calculators

Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Worst-Case Warehouse Building
North Carolina Department of Environmental Quality
Risk Calculator
AquAir II Brownfields Site - West Side
13300 Sam Neely Road
Brownfields Redevelopment Section
18038-14-060
January 2023
November 2022 EPA RSL Table
4/11/2023
Prepared By:H&H
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Warehouse Building
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Warehouse Building
Description of Exposure Point Concentration Selection:
Exposure Point
Concentration
(ug/m3)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC Flag
(Y/N)
Rationale for
Selection or
Deletion
15800 67-64-1 Acetone ug/m3
229 71-43-2 Benzene ug/m3
1.7 106-99-0 Butadiene, 1,3-ug/m3
2.1 75-15-0 Carbon Disulfide ug/m3
2 74-87-3 Chloromethane ug/m3
2.1 110-82-7 Cyclohexane ug/m3
2.2 75-71-8 Dichlorodifluoromethane ug/m3
200 141-78-6 Ethyl Acetate ug/m3
6.1 100-41-4 Ethylbenzene ug/m3
40400 109-99-9 ~Tetrahydrofuran ug/m3
6.6 142-82-5 Heptane, N-ug/m3
2.4 110-54-3 Hexane, N-ug/m3
44 67-63-0 Isopropanol ug/m3
10600 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3
130 1634-04-4 Methyl tert-Butyl Ether (MTBE)ug/m3
5.6 75-09-2 Methylene Chloride ug/m3
2.7 115-07-1 Propylene ug/m3
1.4 127-18-4 Tetrachloroethylene ug/m3
19 108-88-3 Toluene ug/m3
19 108-38-3 Xylene, m-ug/m3
6.1 95-47-6 Xylene, o-ug/m3
Input Form 2D
Soil Gas Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Warehouse Building
Description of Exposure Point Concentration Selection:
Exposure Point
Concentration
(ug/m3)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC Flag
(Y/N)
Rationale for
Selection or
Deletion
167 67-64-1 Acetone ug/m3
2.7 71-43-2 Benzene ug/m3
1.2 75-15-0 Carbon Disulfide ug/m3
1.3 74-87-3 Chloromethane ug/m3
1.5 110-82-7 Cyclohexane ug/m3
2.1 75-71-8 Dichlorodifluoromethane ug/m3
13 141-78-6 Ethyl Acetate ug/m3
3.9 100-41-4 Ethylbenzene ug/m3
27 109-99-9 ~Tetrahydrofuran ug/m3
2.7 142-82-5 Heptane, N-ug/m3
3.5 110-54-3 Hexane, N-ug/m3
9.8 67-63-0 Isopropanol ug/m3
156 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3
0.7 108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)ug/m3
4.9 75-09-2 Methylene Chloride ug/m3
7.2 115-07-1 Propylene ug/m3
58 108-88-3 Toluene ug/m3
1.5 79-01-6 Trichloroethylene ug/m3
11 108-38-3 Xylene, m-ug/m3
7.8 95-47-6 Xylene, o-ug/m3
Input Form 2E
Indoor Air Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Risks are calculated for these chemicals if indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are likely not associated with vapor intrusion.
If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Warehouse Building
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.5E-06 7.8E-02 NO
Indoor Air 3.0E-06 3.2E-01 NO
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Warehouse Building
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 15800 158 --
71-43-2 Benzene 229 2.29 1.6E+00 2.6E+01 1.5E-06 1.7E-02
106-99-0 Butadiene, 1,3-1.7 0.017 4.1E-01 1.8E+00 4.2E-08 1.9E-03
75-15-0 Carbon Disulfide 2.1 0.021 -6.1E+02 6.8E-06
74-87-3 Chloromethane 2 0.02 -7.9E+01 5.1E-05
110-82-7 Cyclohexane 2.1 0.021 -5.3E+03 8.0E-07
75-71-8 Dichlorodifluoromethane 2.2 0.022 -8.8E+01 5.0E-05
141-78-6 Ethyl Acetate 200 2 -6.1E+01 6.5E-03
100-41-4 Ethylbenzene 6.1 0.061 4.9E+00 8.8E+02 1.2E-08 1.4E-05
109-99-9 ~Tetrahydrofuran 40400 404 -1.8E+03 4.6E-02
142-82-5 Heptane, N-6.6 0.066 -3.5E+02 3.8E-05
110-54-3 Hexane, N-2.4 0.024 -6.1E+02 7.8E-06
67-63-0 Isopropanol 44 0.44 -1.8E+02 5.0E-04
78-93-3 Methyl Ethyl Ketone (2-Butanone)10600 106 -4.4E+03 4.8E-03
1634-04-4 Methyl tert-Butyl Ether (MTBE)130 1.3 4.7E+01 2.6E+03 2.8E-08 9.9E-05
75-09-2 Methylene Chloride 5.6 0.056 1.2E+03 5.3E+02 4.6E-11 2.1E-05
115-07-1 Propylene 2.7 0.027 -2.6E+03 2.1E-06
127-18-4 Tetrachloroethylene 1.4 0.014 4.7E+01 3.5E+01 3.0E-10 8.0E-05
108-88-3 Toluene 19 0.19 -4.4E+03 8.7E-06
108-38-3 Xylene, m-19 0.19 -8.8E+01 4.3E-04
95-47-6 Xylene, o-6.1 0.061 -8.8E+01 1.4E-04
Cumulative:1.5E-06 7.8E-02
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Warehouse Building
CAS #Chemical Name:
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 167 --
71-43-2 Benzene 2.7 1.6E+00 2.6E+01 1.7E-06 2.1E-02
75-15-0 Carbon Disulfide 1.2 -6.1E+02 3.9E-04
74-87-3 Chloromethane 1.3 -7.9E+01 3.3E-03
110-82-7 Cyclohexane 1.5 -5.3E+03 5.7E-05
75-71-8 Dichlorodifluoromethane 2.1 -8.8E+01 4.8E-03
141-78-6 Ethyl Acetate 13 -6.1E+01 4.2E-02
100-41-4 Ethylbenzene 3.9 4.9E+00 8.8E+02 8.0E-07 8.9E-04
109-99-9 ~Tetrahydrofuran 27 -1.8E+03 3.1E-03
142-82-5 Heptane, N-2.7 -3.5E+02 1.5E-03
110-54-3 Hexane, N-3.5 -6.1E+02 1.1E-03
67-63-0 Isopropanol 9.8 -1.8E+02 1.1E-02
78-93-3 Methyl Ethyl Ketone (2-Butanone)156 -4.4E+03 7.1E-03
108-10-1 Methyl Isobutyl Ketone (4-methyl-2-pentanone)0.7 -2.6E+03 5.3E-05
75-09-2 Methylene Chloride 4.9 1.2E+03 5.3E+02 4.0E-09 1.9E-03
115-07-1 Propylene 7.2 -2.6E+03 5.5E-04
108-88-3 Toluene 58 -4.4E+03 2.6E-03
79-01-6 Trichloroethylene 1.5 3.0E+00 1.8E+00 5.0E-07 1.7E-01
108-38-3 Xylene, m-11 -8.8E+01 2.5E-02
95-47-6 Xylene, o-7.8 -8.8E+01 1.8E-02
Cumulative:3.0E-06 3.2E-01
All concentrations are in ug/m3
Output Form 3F
** - Note that the EPA has no consensus on reference dose or cancer slope factor values for lead, therefore it is not possible to calculate carcinogenic risk
or hazard quotient. Lead concentrations are compared to the National Ambient Air Quality Standard of 0.15 μg/m3.
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Risks are calculated for these values if
indoor air concentrations are entered and indoor air screening levels have been established, but it should be noted that detections of these chemicals are
likely not associated with vapor intrusion.
North Carolina DEQ Risk Calculator
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
4/11/2023
Prepared By:H&H
Worst-Case Guardhouse
North Carolina Department of Environmental Quality
Risk Calculator
AquAir II Brownfields Site - West Side
13300 Sam Neely Road
Brownfields Redevelopment Section
18038-14-060
January 2023
November 2022 EPA RSL Table
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Guardhouse
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Guardhouse
Description of Exposure Point Concentration Selection:
Exposure Point
Concentration
(ug/m3)
Notes:CAS Number Chemical
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
Range of
Detection
Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC Flag
(Y/N)
Rationale for
Selection or
Deletion
88.8 67-64-1 Acetone ug/m3
1.6 71-43-2 Benzene ug/m3
3.3 110-82-7 Cyclohexane ug/m3
2.2 75-71-8 Dichlorodifluoromethane ug/m3
238 141-78-6 Ethyl Acetate ug/m3
137 109-99-9 ~Tetrahydrofuran ug/m3
2.6 142-82-5 Heptane, N-ug/m3
4.7 67-63-0 Isopropanol ug/m3
41 78-93-3 Methyl Ethyl Ketone (2-Butanone)ug/m3
6.3 75-09-2 Methylene Chloride ug/m3
7.9 108-88-3 Toluene ug/m3
Input Form 2D
Soil Gas Exposure Point Concentration Table
Note: Chemicals highlighted in orange are non-volatile chemicals. Since these chemicals do not pose a vapor intrusion risk, no risk values are calculated for these chemicals.
If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Guardhouse
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air 1.0E-08 8.2E-03 NO
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
DEQ Risk Calculator - Vapor Intrusion - Non-Residential Worker Soil Gas to Indoor Air
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 18038-14-060
Exposure Unit ID: Worst-Case Guardhouse
CAS #Chemical Name:
Soil Gas
Concentration
(ug/m3)
Calculated
Indoor Air
Concentration
(ug/m3)
Target Indoor
Air Conc. for
Carcinogens @
TCR = 1E-06
Target Indoor Air
Conc. for Non-
Carcinogens @
THQ = 0.2
Calculated
Carcinogenic
Risk
Calculated
Non-
Carcinogenic
Hazard
Quotient
67-64-1 Acetone 88.8 0.888 --
71-43-2 Benzene 1.6 0.016 1.6E+00 2.6E+01 1.0E-08 1.2E-04
110-82-7 Cyclohexane 3.3 0.033 -5.3E+03 1.3E-06
75-71-8 Dichlorodifluoromethane 2.2 0.022 -8.8E+01 5.0E-05
141-78-6 Ethyl Acetate 238 2.38 -6.1E+01 7.8E-03
109-99-9 ~Tetrahydrofuran 137 1.37 -1.8E+03 1.6E-04
142-82-5 Heptane, N-2.6 0.026 -3.5E+02 1.5E-05
67-63-0 Isopropanol 4.7 0.047 -1.8E+02 5.4E-05
78-93-3 Methyl Ethyl Ketone (2-Butanone)41 0.41 -4.4E+03 1.9E-05
75-09-2 Methylene Chloride 6.3 0.063 1.2E+03 5.3E+02 5.1E-11 2.4E-05
108-88-3 Toluene 7.9 0.079 -4.4E+03 3.6E-06
Cumulative:1.0E-08 8.2E-03
All concentrations are in ug/m3
Output Form 3E
Carcinogenic risk and hazard quotient cells highlighted in orange are associated with non-volatile chemicals. Since these chemicals do not pose a vapor intrusion
risk, no risk values are calculated for these chemicals.
North Carolina DEQ Risk Calculator

Appendix I Safety Data Sheets
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 1 of 8
15-Nov-2021
SAFETY DATA SHEET

Product Identifier : ARDEX 8+9™ Gray (Part 9 Gray Powder)
Product ID No. : 70010651
Trade Name/Synonyms : 8+9 Gray, Part 9 Gray Powder
Material Use : Rapid Waterproofing and Crack Isolation Compound
Uses Advised Against : Use only as recommended in the product’s Technical Data Sheet.
Manufacturer’s name and address:
ARDEX L.P.
400 Ardex Park Dr.
Aliquippa, PA 15001 USA

Information Telephone No. : [phone] or [phone]
Website Address : http://www.ardexamericas.com
24 Hr Emergency Telephone # : CHEM-TEL: [phone] OR 1-813-248-0585 (call collect)

GHS Classification per 29 CFR 1910.1200 (OSHA HCS 2012) and HPR (WHMIS 2015)
Skin corrosion/irritation, Category 1
Serious eye damage/eye irritation, Category 1
Carcinogenicity, Category 1
Specific target organ toxicity, repeated exposure, Category 1.

GHS Pictograms

Signal Word
Danger

Hazard Statements
Causes severe skin burns and eye damage.
May cause cancer by inhalation.
Causes damage to lungs through prolonged or repeated inhalation.

Precautionary Statements
Obtain special instructions before use. (See Section 7.) Do not handle until all
safety precautions have been read and understood. Do not breathe dust. Use only
in a well-ventilated area. Wash hands and exposed skin thoroughly after handling.
Wear protective gloves/protective clothing/eye protection. Wash contaminated
clothing before reuse. Keep container tightly closed. Protect from sunlight. Store
locked up. Dispose of contents / container in accordance with federal, state, and
local laws. Do not allow product to enter drains.

Hazards Not Otherwise Classified
None

SECTION 1 – PRODUCT AND COMPANY IDENTIFICATION
SECTION 2 – HAZARDS IDENTIFICATION
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 2 of 8
15-Nov-2021
% With Unknown Acute Toxicity : Up to 80% by weight of this product consists of ingredients with unknown acute
toxicity.

Ingredients CAS # % (by weight)
Calcium aluminate cement 65997-16-2 30 – 60
Calcium sulfate 7778-18-9 10 – 30
Crystalline silica, quartz 14808-60-7 10 - 30
Portland cement 65997-15-1 5 – 10
Limestone 1317-65-3 1 – 5
The exact percentages of the ingredients have been withheld by the manufacturer as trade secrets.

General : Call a Poison Center or doctor if you feel unwell.
Inhalation : Remove person to fresh air and keep at rest in a position comfortable for
breathing. Get medical attention.
Skin contact : Remove contaminated clothing. Flush affected skin with water. If irritation or rash
occurs, seek medical attention/advice.
Eye contact : Rinse cautiously with water for several minutes. Remove contact lenses, if present
and easy to do. Continue rinsing. Get medical attention.
Ingestion : Rinse mouth. Do NOT induce vomiting. Call a POISON CENTER or
doctor/physician if you feel unwell.
Notes for Physician : Treat symptomatically.

Signs and symptoms of short-term (acute) exposure
Inhalation : Symptoms may include coughing and shortness of breath.
Skin : Symptoms may include redness and itching. Contact with wet material, or moist
areas of skin, causes skin burns. Skin thickening, cracking, or fissuring may occur.
Eyes : Direct contact may strongly irritate or burn the eyes. Could cause blindness.
Ingestion : Symptoms such as gastric pain, nausea, vomiting, and diarrhea may occur.
Effects of long-term (chronic) exposure
: Prolonged inhalation may cause adverse lung effects with symptoms including
coughing and shortness of breath. Repeated or prolonged inhalation of fine dusts
may cause severe scarring of the lungs, a disease called silicosis, and alveolar
proteinosis (lower lung disease). Silicosis has been linked to kidney damage and
autoimmune disorders.
Indication of need for immediate medical attention or special treatment
: Difficulty breathing persists after removing the person to fresh air.
Any burn to the skin.
Any exposure to the eye which causes irritation.
Ingestion.

Suitable extinguishing media : Carbon dioxide, dry chemical powder, foam.
Unsuitable extinguishing media : High pressure water jet. Contact with water may cause hydration and formation of
caustic alkaline material.
Hazardous combustion products : Calcium oxide, calcium oxalate, vinyl acetate, acetic acid, formic acid,
formaldehydes, carbon monoxide, and carbon dioxide.
Special fire-fighting procedures/equipment
SECTION 3 – COMPOSITION/INFORMATION ON INGREDIENTS
SECTION 4 – FIRST AID MEASURES
SECTION 5 – FIRE FIGHTING MEASURES
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 3 of 8
15-Nov-2021
: Firefighters should wear proper protective equipment and self-contained breathing
apparatus with full face piece operated in positive pressure mode. Move
containers from fire area if safe to do so. Water spray may be useful in cooling
equipment exposed to heat and flame. After fires have been extinguished,
carefully clean all equipment and surfaces exposed to fumes.
Environmental precautions : Do not allow material to enter drains or contaminate ground water system.
Fire hazards/conditions of flammability
: Not flammable under normal conditions of use.
Flammability classification (OSHA 29 CFR 1910.1200, WHMIS 2015)
: Not flammable

Personal precautions : Restrict access to area until completion of clean-up. All persons dealing with
clean-up should wear the appropriate chemically protective equipment.
Protective equipment : Refer to Section 8 for information on acceptable personal protective equipment.
Emergency Procedures : This product does not contain chemicals requiring EPA notification for spills. In
case of a chemical spill, call the emergency telephone number listed in Section 1.
US CERCLA Reportable quantity (RQ): None reported.
Methods and materials for containment and cleaning up
: Ventilate area of release. Stop spill or leak at source if safely possible. Contain
material, preventing it from entering sewer lines or waterways. Using HEPA
vacuum, or other dustless methods, gather up spilled material and place in
suitable container for later disposal (see Section 13). Notify the appropriate
authorities as required.
Prohibited materials : Avoid adding water. This product becomes alkaline when wet.
Environmental precautions : Do not allow product to enter drains or waterways. Do not allow material to
contaminate ground water system.
Reference to other sections : See Section 13 for disposal information.

Special instructions : Use ventilation to control levels of dust in the work area.
Safe handling procedures : Wear chemically resistant protective equipment during handling. Use in a
well-ventilated area. Training the workers on the potential health hazards
associated with product dust is important. Secondary inhalation exposures could
occur when cleaning equipment, or when removing or laundering the clothing. Do
not breathe dust. Avoid and control operations which create dust. Keep containers
tightly closed when not in use. Wash hands and exposed skin thoroughly after
handling.
Storage requirements : Store in a cool, dry place. Store away from heat and open flame. Avoid storing in
direct sunlight. Store in original container. Keep tightly closed when not in use.
Store locked up. Keep out of reach of children.
Incompatible materials : Keep away from strong acids and oxidizing agents. (See Section 10.)
Special packaging materials : Always keep in containers made of the same materials as the supply container.

Permissible Exposure Limits : No exposure limits have been established for the product itself. Below are
exposure limits for the components in the product.

Threshold Limit Values
for the Ingredients
CAS # ACGIH TLV
TWA STEL
OSHA PEL
PEL STEL
SECTION 6 – ACCIDENTAL RELEASE MEASURES
SECTION 7 – HANDLING AND STORAGE
SECTION 8 – EXPOSURE CONTROLS AND PERSONAL PROTECTION
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 4 of 8
15-Nov-2021
Limestone 1317-65-3 TLV
Withdrawn
In 2007
N/Av 15 mg/m3
(Total dust);
5 mg/m3
(respirable)
N/Av
Calcium aluminate cement 65997-16-2 1 mg/m3
(as
Aluminum
metal and
insoluble
compounds)
N/Av N/Av N/Av
Calcium sulfate 7778-18-9 10 mg/m3
(inhalable)
N/Av 15 mg/m3
(Total dust);
5 mg/m3
(respirable)
N/Av
Portland cement 65997-15-1 1 mg/m3
(respirable, no
asbestos and
< 1%
crystalline
silica)
N/Av 15 mg/m3
(Total dust);
5 mg/m3
(respirable)
N/Av
Crystalline silica, quartz 14808-60-7 0.025 mg/m3
(respirable
fraction)
N/Av 0.05 mg/m3
(respirable)
(final rule
limit)
N/Av

Engineering Controls : Use general ventilation in combination with local exhaust ventilation with HEPA
filtration to maintain air concentrations below recommended exposure limits.
Ventilation should effectively remove and prevent buildup of any dust generated
from the handling of this product.
Personal Protective Equipment
Eye / face protection : Safety glasses or chemical goggles must be worn when using this product.
Additionally, a face shield is recommended if splashing is possible.
Skin protection : Wear chemical resistant protective clothing and impervious gloves. Glove
materials such as nitrile rubber or Viton (fluorocarbon rubber) are recommended.
Body protection : Where extensive exposure to product is possible, use resistant coveralls, apron
and boots to prevent contact.
Respiratory protection : If work process generates excessive quantities of dust, or exposures in excess of
any PEL, wear an appropriate particulate respirator (dust mask). Mask should be
rated at N-95 or higher.
Site safety equipment : An eyewash station and safety shower should be made available in the immediate
working area.
General hygiene considerations : Avoid contact with eyes, skin and clothing. Do not breathe dust. Do not eat, drink
or smoke when using this product. Clean all equipment and clothing at end of
each work shift. This product contains crystalline silica. Comply with all
requirements within OSHA Standard 29 CFR § 1926.1153 - Respirable crystalline
silica for Construction.

Physical state : solid Appearance : gray powder
Odor : No odor Odor threshold : N/Av
pH : 10 – 12 Specific gravity : 2.7 – 3.1
Boiling point : N/Ap Coefficient of water/oil distribution : N/Av
Melting/Freezing point : N/Av Solubility in water : < 55 g/L
Vapor pressure (mm Hg @ 20°C / 68°F) : N/Av Evaporation rate (n-Butyl acetate = 1) : N/Ap
Vapor density (Air = 1) : N/Av Volatiles (% by weight) : N/Av
Volatile organic compounds (VOCs) : 0 g/L
Particle size : N/Av Flammability classification : Not flammable
Flash point : N/Av Lower flammable limit (% by vol) : Not available
Flash point method : N/Av Upper flammable limit (% by vol) : Not available
SECTION 9 – PHYSICAL AND CHEMICAL PROPERTIES
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 5 of 8
15-Nov-2021
Auto-ignition temperature : N/Av Decomposition temperature : Not available
Viscosity : Not available Oxidizing properties : Not available
Explosion data: Sensitivity to mechanical impact / static discharge
: Not expected to be sensitive to mechanical impact or static discharge.

Reactivity : Contact with water may cause hydration and formation of caustic calcium
hydroxide.
Stability : Stable under the recommended storage and handling conditions prescribed.
Hazardous reactions : Hazardous polymerization does not occur.
Conditions to avoid : High temperatures.
Materials to avoid and incompatibility
: Oxidizing agents. Strong acids.
Hazardous decomposition products
: None known, refer to hazardous combustion products in Section 5.

Routes of exposure : Inhalation: YES Skin Absorption: NO Skin and Eyes: YES Ingestion: YES
Symptoms of exposure : See Section 4.
Calculated Acute Toxicity Estimates for the Product
Inhalation : Not Available
Oral : Not Available
Dermal : Not Available
Toxicological data : There are insufficient data for estimating the product’s acute toxicity. See below
for individual ingredient acute toxicity data.
Acute Toxicity Parameters
for the Ingredients
CAS # LC50, Inhalation
mg/L, Rat, 4 hr
LD50, Oral
mg/kg, rat
LD50, Dermal
mg/kg, rabbit
Limestone 1317-65-3 N/Av 6,450 N/Av
Calcium aluminate cement 65997-16-2 N/Av N/Av N/Av
Calcium sulfate 7778-18-9 N/Av > 3,000 N/Av
Portland cement 65997-15-1 N/Av N/Av N/Av
Crystalline silica, quartz 14808-60-7 N/Av N/Av N/Av

Skin corrosion or irritation : Causes skin corrosion when wet.
Serious eye damage / eye irritation
: Causes eye burns. May cause blindness.
Respiratory or skin sensitization : Portland cement may cause an allergic skin reaction, in hypersensitive individuals
possibly due to trace amounts of chromium.
Germ cell mutagenicity : None known.
Carcinogenic status : This product contains Crystalline silica. Crystalline silica (respirable size) is
classified as carcinogenic by inhalation by IARC (Group 1), ACGIH (Group A2),
NTP (Group 1) and OSHA (OSHA Select carcinogen). No other components are
listed as carcinogens by ACGIH, IARC, OSHA or NTP.
Reproductive toxicity : None known.
Specific Target Organ Toxicity, Single Exposure
SECTION 10 – REACTIVITY AND STABILITY INFORMATION
SECTION 11 – TOXICOLOGICAL INFORMATION
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 6 of 8
15-Nov-2021
: May cause respiratory irritation.
Specific Target Organ Toxicity, Repeated Exposure
: May cause lung damage (silicosis) upon repeated or prolonged exposure. Silicosis
may be accompanied by complications such as kidney damage and autoimmune
disorders.
Aspiration hazard : None known.
Additional information : N/Av

Environmental effects : The product should not be allowed to enter drains or water courses or be
deposited where it can affect ground or surface waters.
Ecotoxicological : No data is available on the product itself.
Ecotoxicity : No data available.
Biodegradability : No data available.
Bioaccumulative potential : No data available.
Mobility in soil : No data available.
PBT and vPvB assessment
: No data available.
Other adverse effects : No data available.

Handling for disposal : Handle waste according to recommendations in Section 7.
Methods of disposal : Dispose in accordance with all applicable federal, state, provincial and local
regulations. Contact your local, state, provincial or federal environmental agency
for specific rules.
Packaging : Handle contaminated packaging in the same manner as the product.
RCRA : For disposal of unused or waste material, check with local, state and federal
environmental agencies.

Regulatory
Information
UN
Number Shipping Name Class
Packing
Group Label
TDG None This product is not regulated according to Canadian
TDG regulations.
None

None None
TDG
Additional
Information
None
49 CFR/DOT None This product is not regulated according to US DOT
regulations.
None

None None
49 CFR/DOT
Additional Information
None
Not regulated by IMDG.
Not regulated by IATA.
Not a Marine Pollutant.

Canadian Information:
This product has been classified according to the hazard criteria of the Hazardous Products Regulations (HPR). This
SDS contains all information required by the HPR.
SECTION 12 – ECOLOGICAL INFORMATION
SECTION 13 – DISPOSAL CONSIDERATION
SECTION 14 – TRANSPORTATION INFORMATION
SECTION 15 – REGULATORY INFORMATION
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 7 of 8
15-Nov-2021
Canadian Environmental Protection Act (CEPA) information: All ingredients listed appear on either the Domestic
Substances List (DSL) or the Non- Domestic Substances List (NDSL).

US Federal Information:
TSCA: All listed ingredients appear on the Toxic Substances Control Act (TSCA) inventory.

CERCLA Reportable Quantity (RQ) (40 CFR 117.302): None reported.

SARA TITLE III: Sec. 311 and 312, SDS Requirements, 40 CFR 370 Hazard Classes:
Skin corrosion/irritation, Category 1
Serious eye damage/eye irritation, Category 1
Carcinogenicity, Category 1
Specific target organ toxicity, repeated exposure, Category 1.
Under SARA Sections 311 and 312, the EPA has established threshold quantities for the reporting of hazardous
chemicals. The threshold for this product is 10,000 pounds.

SARA TITLE III: Sec. 313, Toxic Chemicals Notification, 40 CFR 372: This material is not subject to SARA notification
requirements, since it does not contain any Toxic Chemical constituents above de minimus concentrations.

U.S. State Right to Know Laws
California Proposition 65: See product label for information regarding Proposition 65.

Other State Right to Know Laws:
Ingredient on State RTK Law? CAS # CA MA MN NJ NY PA RI
Limestone 1317-65-3 No YES No YES No YES YES
Portland cement 65997-15-1 No YES No YES No YES YES
Calcium sulfate 7778-18-9 No YES No YES No YES No
Crystalline silica, quartz 14808-60-7 No YES YES YES No YES YES

HMIS Rating : * - Chronic Hazard 0 - Minimal 1 – Slight 2 – Moderate 3 – Serious 4 – Severe
Health: *3 Flammability 0 Physical Hazard 1 PPE:
Gloves, safety glasses

Legend : ACGIH: American Conference of Governmental Industrial Hygienists
CAS: Chemical Abstract Services
CERCLA: Comprehensive Environmental Response, Compensation, and Liability Act of
1980
CFR: Code of Federal Regulations
DOT: Department of Transportation
DSL: Domestic Substances List
EPA: Environmental Protection Agency
GHS: Globally Harmonized System
HEPA: High Efficiency Particulate Air [filter]
HMIS: Hazardous Materials Information System
HPR: Hazardous Products Regulations
IARC: International Agency for Research on Cancer
Inh: Inhalation
mg/L: milligrams per Liter (of air)
mg/kg: milligrams per Kilogram (of body mass)
N/Av: Not Available
N/Ap: Not Applicable
NFPA: National Fire Protection Association
NIOSH: National Institute of Occupational Safety and Health
SECTION 16 – OTHER INFORMATION
ARDEX 8+9™ GRAY (Part 9 GRAY Powder) Page 8 of 8
15-Nov-2021
NTP: National Toxicology Program
OSHA: Occupational Safety and Health Administration
PBT: Persistent, Bioaccumlative, and/or Toxic
PEL: Permissible exposure limit
PPE: Personal Protection Equipment
RCRA: Resource Conservation and Recovery Act
SARA: Superfund Amendments and Reauthorization Act
STEL: Short Term Exposure Limit
TDG: Canadian Transportation of Dangerous Goods Act & Regulations
TLV: Threshold Limit Values
TSCA: Toxic Substance Control Act
TWA: Time Weighted Average
vPvB: (very) Persistent, (very) Bioaccumulative and/or Toxic
WHMIS: Workplace Hazardous Materials Identification System

Disclaimer of Liability
The Information presented herein is supplied as a guide to those who handle or use this product and has been prepared in good faith
by technically knowledgeable personnel. It is not intended to be all-inclusive. The manner and conditions of use and handling may
involve other and additional considerations. Safe work practices must be employed when working with any materials. It is important
that the end user determines the adequacy of the safety procedures employed during the use of this product.
No warranty of any kind is given or implied. ARDEX L.P. will not be liable for any damages, losses, injuries or consequential damages
which may result from the use or reliance on any information contained herein.

Prepared By:
ARDEX L.P.
400 Ardex Park Drive
Aliquippa, PA, U.S.A.
15001

[phone]
Visit our Website: http://www.ardexamericas.com

Revision date: : 15-Nov-2021
End of Document
ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic) Page 1 of 7
06-Jan-2017
SAFETY DATA SHEET

Manufacturer’s name and address:
ARDEX Engineered Cements
400 Ardex Park Dr.
Aliquippa, PA 15001 USA
Supplier’s name and address:

Refer to Manufacturer

Information Telephone No. : [phone] or [phone]
Website Address : http://www.ardexamericas.com
24 Hr Emergency Telephone # : CHEM-TEL: [phone] OR 1-813-248-0585 (call collect)
Product Identifier : ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic)
Product ID No. : 70012321
Trade Name/Synonyms : ARDEX D 14
Material Use : Tile Adhesive used for setting quarry, ceramic, mosaic and moisture-
insensitive stone tile over interior surfaces. Can also be used to set porcelain
tile over absorbent interior surfaces.
Uses Advised Against : No information available

GHS Classification per 29 CFR 1910.1200 (OSHA HCS 2012) and HPR (WHMIS 2015)
Not classified as hazardous.
GHS Pictograms
None.
Signal Word
None.

Hazard Statements
None.

Safe Handling Instructions: Avoid eye and skin contact. It is recommended to use safety glasses and
gloves during handling. During installation process, adequate ventilation of the
work area should be maintained. Although the adhesive is low in VOC,
persons who are sensitive to odors or chemicals should avoid the work area
during installation. Keep container closed. Do not subject to grinding. Dispose
of contents / container in accordance with federal, state, and local laws. Do not
allow product to enter drains.

During normal usage of the product as recommended, airborne dusts and mists will
not be present. See Sections 7 and 11 for further details.
Hazards Not Otherwise Classified
None. % With Unknown Acute Toxicity : Less than 1% by weight of this product is comprised of ingredients with
unknown acute toxicity

Ingredients CAS # % (by weight)
Limestone 1317-65-3 60 – 100
Sepiolite clay 63800-37-3 0.1 – 1.0
Crystalline silica, quartz* 14808-60-7 0.1 – 1.0
*Crystalline silica is present as an impurity from the Limestone and clay. It is not intentionally added.
SECTION 1 – PRODUCT AND COMPANY IDENTIFICATION
SECTION 2 – HAZARDS IDENTIFICATION
SECTION 3 – COMPOSITION/INFORMATION ON INGREDIENTS
ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic) Page 2 of 7
06-Jan-2017
Exact composition of the ingredients is claimed as a trade secret by the manufacturer.

General : Call a doctor if you feel unwell.
Inhalation : If a worker develops breathing problems while working with this material, remove
the worker to fresh air and keep at rest in a position comfortable for breathing.
Skin contact : Wash with plenty of soap and water. If irritations or symptoms develop, seek
medical attention/advice.
Eye contact : Rinse cautiously with water for several minutes. Remove contact lenses, if present
and easy to do. Continue rinsing. Get medical advice/attention.
Ingestion : Rinse mouth. Do NOT induce vomiting. Call a doctor/physician if you feel unwell.
Notes for Physician : Treat symptomatically.

Signs and symptoms of short-term (acute) exposure
Inhalation : May cause mild irritation of the nose, throat, mucous membranes, and respiratory
tract.
Skin : Symptoms may include mild redness or itching.
Eyes : Symptoms may include mild redness, itching, or pain.
Ingestion : Ingestion of large amounts may cause stomach irritation. May cause nausea,
vomiting, and diarrhea.
Effects of long-term (chronic) exposure
: Prolonged skin contact may cause skin irritations.
Indication of need for immediate medical attention or special treatment
: Difficulty breathing persists after removing the person to fresh air.
Any exposure to the eye which causes irritation.

Suitable extinguishing media : Carbon dioxide, dry chemical powder, alcohol foam or water spray.
Unsuitable extinguishing media : Water jet may spread the burning material.
Hazardous combustion products : Carbon monoxide, carbon dioxide, as well as other toxic vapors and gases which
are common to thermal degradation of organic compounds.
Special fire-fighting procedures/equipment
: Firefighters should wear proper protective equipment and self-contained breathing
apparatus with full face piece operated in positive pressure mode. Move containers
from fire area if safe to do so. Water spray may be useful in cooling equipment
exposed to heat and flame. After fires have been extinguished, carefully clean all
equipment and surfaces exposed to fumes.
Environmental precautions : Do not allow material to enter drains or contaminate ground water system.
Fire hazards/conditions of flammability
: Not flammable under normal conditions of use. Closed containers may rupture if
exposed to excess heat or flame due to a build-up of internal pressure.
Flammability classification (OSHA 29 CFR 1910.1200, WHMIS 2015)
: Not flammable.
NFPA Rating : 0 - Minimal 1 – Slight 2 – Moderate 3 – Serious 4 – Severe
Health: 1 Flammability 1 Instability 0 Special Hazards: None

Personal precautions : Restrict access to area until completion of clean-up. All persons dealing with
clean-up should wear the appropriate chemically protective equipment.
SECTION 4 – FIRST AID MEASURES
SECTION 5 – FIRE FIGHTING MEASURES
SECTION 6 – ACCIDENTAL RELEASE MEASURES
ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic) Page 3 of 7
06-Jan-2017
Protective equipment : Refer to Section 8 on this Safety Data Sheet, EXPOSURE CONTROLS /
PERSONAL PROTECTION, for additional information on acceptable personal
protective equipment.
Emergency Procedures : If a spill/release in excess of the EPA reportable quantity is made into the
environment, immediately notify the national response center in the United States
(phone: [phone]). Outside of the U.S. call the emergency number listed in
Section 1.
US CERCLA Reportable quantity (RQ): None reported.
Methods and materials for containment and cleaning up
: Ventilate area of release. Stop spill or leak at source if safely possible. Contain
product with inert absorbent material, preventing it from entering sewer lines or
waterways. Gather up spilled material and place in suitable container for later
disposal (see Section 13). Residual of product, while still wet, can be cleaned up
with warm soapy water. Notify the appropriate authorities as required.
Prohibited materials : None known.
Environmental precautions : Do not allow product to enter drains or waterways. Do not allow material to
contaminate ground water system.
Reference to other sections : See Section 13 for disposal information.

Safe handling procedures : Wear suitable protective equipment during handling. (See Section 8.) Observe
good hygiene standards. Use only with adequate ventilation. Wash thoroughly after
handling. Avoid contact with eyes, skin, or clothing. Sanding and grinding dusts
may be harmful if inhaled. When removing this product from existing flooring (i.e.
during a renovation), wear safety goggles and respiratory protection from dust due
to blasting, chipping, or mechanically pulverizing. Keep container tightly closed.
Storage requirements : Store in a cool, dry, well-ventilated area. Store away from heat and open flame.
Avoid storing in direct sunlight. Store in original container. Keep tightly closed when
not in use. Do not reuse empty container without commercial cleaning or
reconditioning.
Incompatible materials : See Section 10.
Special packaging materials : Always keep in containers made of the same materials as the supply container.

Permissible Exposure Limits : No exposure limits have been established for the product itself. Below are exposure
limits for the components in the product. Since this product is a paste, airborne dust is
not likely when the product is used according to the directions.
Ingredients CAS # ACGIH TLV
TWA STEL
OSHA PEL
PEL STEL
Limestone 1317-65-3
TLV
Withdrawn In 2007
N/Av 15 mg/m3
(Total dust); 5 mg/m3
(respirable)
N/Av
Sepiolite clay 63800-37-3
10 mg/m3
(Total dust);
5 mg/m3
(respirable)
N/Av 5 mg/m3
(respirable) N/Av
Crystalline silica, quartz 14808-60-7
0.025 mg/m3
(respirable
fraction)
N/Av 0.05 mg/m3
(respirable)
(final rule limit)
N/Av

Engineering Controls : Use general or local exhaust ventilation to maintain air concentrations below
recommended exposure limits. Ventilation should effectively remove and prevent
buildup of any vapor generated from the handling of this product.
Personal Protection Equipment
Eye / face protection : Chemical goggles or safety glasses, as appropriate for the job.
SECTION 7 – HANDLING AND STORAGE
SECTION 8 – EXPOSURE CONTROLS AND PERSONAL PROTECTION
ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic) Page 4 of 7
06-Jan-2017
Skin protection : Wear gloves which are impervious to the material. Materials such as nitrile rubber
or Viton (fluorocarbon rubber) are recommended.
Body protection : Where extensive exposure to product is possible, use resistant coveralls, apron and
boots to prevent contact.
Respiratory protection : Under normal conditions of use with adequate ventilation, respiratory protection
should not be necessary. If work process generates excessive quantities of vapor
or dust, or exposures in excess of any PEL, wear an appropriate organic vapor
respirator.
Site safety equipment : An eyewash station and safety shower should be made available in the immediate
working area.
General hygiene considerations : Avoid contact with eyes, skin and clothing. Avoid breathing vapors/dust. Do not eat,
drink or smoke when using this product. Upon completion of work, wash hands
thoroughly. Remove soiled clothing and wash it thoroughly before reuse. Clean all
equipment and clothing at end of each work shift.

Physical state : Paste Appearance : Off-white paste
Odor : Mild Odor threshold : N/Av
pH : 8.4 – 9.0 Specific gravity : 1.65 – 1.8
Boiling point : N/Av Coefficient of water/oil distribution : N/Av
Melting/Freezing point : N/Av Solubility in water : Miscible
Vapor pressure (mm Hg @ 20°C / 68°F) : N/Av Evaporation rate (n-Butyl acetate = 1) : N/Av
Vapor density (Air = 1) : N/Av Volatiles (% by weight) : 24 – 27%
Volatile organic compounds (VOCs) : 7.5 g/L SCAQMD 1168
Particle size : N/Av Flammability classification : Not flammable
Flash point : >93.3°C (>200°F) Lower flammable limit (% by vol) : Not available
Flash point method : Setaflash closed Upper flammable limit (% by vol) : Not available
Auto-ignition temperature : N/Av Decomposition temperature : Not available
Viscosity : N/Av Oxidizing properties : Not available
Explosion data: Sensitivity to mechanical impact / static discharge
: Not expected to be sensitive to mechanical impact or static discharge.

Reactivity : Not reactive.
Stability : Stable under the recommended storage and handling conditions prescribed.
Hazardous reactions : Hazardous polymerization does not occur.
Conditions to avoid : Extreme heat.
Materials to avoid and incompatibility
: Strong oxidizing agents; acids.
Hazardous decomposition products
: None known, refer to hazardous combustion products in Section 5.

Routes of exposure : Inhalation: YES Skin Absorption: NO Skin and Eyes: Yes Ingestion: YES
Symptoms of exposure : See Section 4.
Calculated Acute Toxicity Estimates for the Product
Inhalation : > 80 mg/L
Oral : > 7,000 mg/kg
Dermal : > 10,000 mg/kg
Toxicological data : See below for individual ingredient acute toxicity data.
SECTION 9 – PHYSICAL AND CHEMICAL PROPERTIES
SECTION 10 – REACTIVITY AND STABILITY INFORMATION
SECTION 11 – TOXICOLOGICAL INFORMATION
ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic) Page 5 of 7
06-Jan-2017
LC50 (4 hr) LD50
Ingredients CAS No. Inhalation, rat, mg/L Oral, rat mg/kg Dermal, rabbit, mg/kg
Limestone 1317-65-3 N/Av 6,450 N/Av
Crystalline silica,
quartz
14808-60-7 N/Av N/Av N/Av
Sepiolite clay 63800-37-3 N/Av N/Av N/Av

Skin corrosion or irritation : May cause mild irritation to skin.
Serious eye damage / eye irritation : May cause mild, temporary irritation to eyes.
Respiratory or skin sensitization : None known.
Germ cell mutagenicity : None known.
Carcinogenic status : This product contains Crystalline silica. Crystalline silica (respirable size) is
classified as carcinogenic by inhalation by IARC (Group 1), ACGIH (Group A2),
NTP (Group 1) and OSHA (OSHA Select carcinogen). Crystalline silica is a natural
impurity in minerals such as limestone and clay. Because Crystalline silica is only
carcinogenic by inhalation, this product is not considered to be a hazard. During
normal usage of the product as recommended, airborne dusts will not be present.
Do not sand off excess material, following initial application. When removing
product from existing floors, etc. (ie. during a renovation), do not mechanically
remove under dry conditions (e.g. blasting, chipping, mechanically pulverizing).
Reproductive toxicity : None known.
Specific Target Organ Toxicity, Single Exposure
: None known.
Specific Target Organ Toxicity, Repeated Exposure
: None known.
Aspiration hazard : None known.
Additional information : N/Av

Environmental effects : The product should not be allowed to enter drains or water courses, or be
deposited where it can affect ground or surface waters.
Ecotoxicity : No data available.
Biodegradability : No data available.
Bioaccumulative potential : No data available.
Mobility in soil : No data available.
PBT and vPvB assessment : No data available.
Other adverse effects : No data available.

Handling for disposal : Handle waste according to recommendations in Section 7.
Methods of disposal : You must test your waste using methods described in 40 CFR Part 261 to
determine if it meets applicable definitions of hazardous wastes. Dispose in
accordance with all applicable federal, state, provincial and local regulations.
Contact your local, state, provincial or federal environmental agency for specific
rules.
Packaging : Handle contaminated packaging in the same manner as the product.
RCRA : If this product, as supplied, becomes a waste in the United States, it may meet the
criteria of a hazardous waste as defined under RCRA, Title 40 CFR 261. It is the
responsibility of the waste generator to determine the proper waste identification
and disposal method. For disposal of unused or waste material, check with local,
state and federal environmental agencies.

SECTION 12 – ECOLOGICAL INFORMATION
SECTION 13 – DISPOSAL CONSIDERATION
SECTION 14 – TRANSPORTATION INFORMATION
ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic) Page 6 of 7
06-Jan-2017
Regulatory
Information
UN
Number Shipping Name Class
Packing
Group Label
TDG None This product is not regulated according to Canadian
TDG regulations.
None

None None
TDG
Additional
Information
None
49 CFR/DOT None This product is not regulated according to US DOT
regulations.
None

None None
49 CFR/DOT Additional
Information
None

IATA : Not regulated for Air Transport

IMDG : Not regulated for Ocean Transport

Canadian Information:
This product has been classified according to the hazard criteria of the Hazardous Products Regulations (HPR). This SDS
contains all of the information required by the HPR.
Canadian Environmental Protection Act (CEPA) information: All ingredients listed appear on either the Domestic Substances
List (DSL) or the Non- Domestic Substances List (NDSL).

US Federal Information:
TSCA: All ingredients appear on the Toxic Substances Control Act (TSCA) inventory.

CERCLA Reportable Quantity (RQ) (40 CFR 117.302): None reported.
SARA TITLE III: Sec. 302, Extremely Hazardous Substances, 40 CFR 355: No Extremely Hazardous Substances are
present in this material.
SARA TITLE III: Sec. 311 and 312, SDS Requirements, 40 CFR 370 Hazard Classes: Not Hazardous.
SARA TITLE III: Sec. 313, Toxic Chemicals Notification, 40 CFR 372: This product is not subject to SARA notification
requirements, since it does not contain any Toxic Chemical constituents above de minimus concentrations.
U.S. State Right To Know Laws
California Proposition 65: Warning. This product contains chemicals known to the State of California to cause cancer
and/or reproductive harm.

Other State Right to Know Laws:
Present on the State RTK List? CAS No. CA MA MN NJ NY PA RI
Limestone 1317-65-3 No YES No YES No YES YES
Crystalline silica, quartz* 14808-60-7 No YES YES YES No YES YES

HMIS Rating : * - Chronic Hazard 0 - Minimal 1 – Slight 2 – Moderate 3 – Serious 4 – Severe
Health: 1 Flammability 1 Physical Hazard 0 PPE: Gloves, safety glasses

Legend : ACGIH: American Conference of Governmental Industrial Hygienists
CAS: Chemical Abstract Services
CERCLA: Comprehensive Environmental Response, Compensation, and Liability
Act of 1980
CFR: Code of Federal Regulations
DOT: Department of Transportation
DSL: Domestic Substances List
EPA: Environmental Protection Agency
SECTION 15 – REGULATORY INFORMATION
SECTION 16 – OTHER INFORMATION
ARDEX D 14™ Type 1 Premixed Tile Adhesive (Mastic) Page 7 of 7
06-Jan-2017
GHS: Globally Harmonized System
HPR: Hazardous Products Regulations
IARC: International Agency for Research on Cancer
Inh: Inhalation
N/Av: Not Available
N/Ap: Not Applicable
NIOSH: National Institute of Occupational Safety and Health
NTP: National Toxicology Program
OSHA: Occupational Safety and Health Administration
PEL: Permissible exposure limit
RCRA: Resource Conservation and Recovery Act
SARA: Superfund Amendments and Reauthorization Act
STEL: Short Term Exposure Limit
TDG: Canadian Transportation of Dangerous Goods Act & Regulations
TLV: Threshold Limit Values
TSCA: Toxic Substance Control Act
TWA: Time Weighted Average
WHMIS: Workplace Hazardous Materials Identification System

Disclaimer of Liability
The Information presented herein is supplied as a guide to those who handle or use this product and has been prepared in good
faith by technically knowledgeable personnel. It is not intended to be all-inclusive. The manner and conditions of use and handling
may involve other and additional considerations. Safe work practices must be employed when working with any materials. It is important that the end user makes a determination regarding the adequacy of the safety procedures employed during the use of
this product.
No warranty of any kind is given or implied. ARDEX Engineered Cements will not be liable for any damages, losses, injuries or consequential damages which may result from the use or reliance on any information contained herein.

Prepared By:
ARDEX Engineered Cements
400 Ardex Park Drive
Aliquippa, PA, U.S.A.
15001

[phone]
Visit our Website: http://www.ardexamericas.com

Revision date: : 06-Jan-2017
End of Document
SAFETY DATA SHEET
1. Identification
BEHR® Drywall Plus Interior Primer & SealerProduct identifier
Other means of identification
073Product number
Architectural CoatingRecommended use
None known.Recommended restrictions
Manufacturer/Importer/Supplier/Distributor information
Behr Process Corp.Supplier
1801 E. St. Andrew Place
Santa Ana, CA 92705
714-545-7101Telephone
[phone]Emergency telephone
[phone]
335213Access code
2. Hazard(s) identification
Not classified.Physical hazards
Not classified.Health hazards
Not classified.OSHA defined hazards
Label elements
None.Hazard symbol
Signal word None.
Hazard statement The mixture does not meet the criteria for classification.
Precautionary statement
Prevention Observe good industrial hygiene practices.
Response Wash hands after handling.
Storage Store away from incompatible materials.
Disposal Dispose of waste and residues in accordance with local authority requirements.
Hazard(s) not otherwise
classified (HNOC)
None known.
Supplemental information None.
3. Composition/information on ingredients
Mixtures
1317-65-3 7 - 13Limestone
CAS number %Chemical name
13463-67-7 7 - 13Titanium dioxide
14808-60-7 0.1 - 1Quartz (SiO2)
All concentrations are in percent by weight unless ingredient is a gas. Gas concentrations are in
percent by volume.
The manufacturer has claimed the exact percentage as trade secret under the OSHA Hazard
Communication Standard.
Composition comments
4. First-aid measures
Move to fresh air. Call a physician if symptoms develop or persist.Inhalation
Wash off with soap and water. Get medical attention if irritation develops and persists.Skin contact
BEHR® Drywall Plus Interior Primer & Sealer SDS US
953273 Version #: 02 Revision date: 16-June-2020 Issue date: 18-March-2020 1 / 7
Rinse with water. Get medical attention if irritation develops and persists.Eye contact
Rinse mouth. Get medical attention if symptoms occur.Ingestion
Direct contact with eyes may cause temporary irritation.Most important
symptoms/effects, acute and
delayed
Treat symptomatically.Indication of immediate
medical attention and special
treatment needed
Ensure that medical personnel are aware of the material(s) involved, and take precautions to
protect themselves.
General information
5. Fire-fighting measures
Water fog. Foam. Dry chemical powder. Carbon dioxide (CO2).Suitable extinguishing media
Do not use water jet as an extinguisher, as this will spread the fire.Unsuitable extinguishing
media
During fire, gases hazardous to health may be formed.Specific hazards arising from
the chemical
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.Special protective equipment
and precautions for firefighters
Move containers from fire area if you can do so without risk.Fire fighting
equipment/instructions
Use standard firefighting procedures and consider the hazards of other involved materials.Specific methods
No unusual fire or explosion hazards noted.General fire hazards
6. Accidental release measures
Keep unnecessary personnel away. For personal protection, see section 8 of the SDS.Personal precautions,
protective equipment and
emergency procedures
This product is miscible in water.
Large Spills: Stop the flow of material, if this is without risk. Dike the spilled material, where this is
possible. Absorb in vermiculite, dry sand or earth and place into containers. Following product
recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re-use. For waste disposal, see section 13 of the SDS.
Methods and materials for
containment and cleaning up
Avoid discharge into drains, water courses or onto the ground.Environmental precautions
7. Handling and storage
Observe good industrial hygiene practices.Precautions for safe handling
Store in tightly closed container. Store away from incompatible materials (see Section 10 of the
SDS).
Conditions for safe storage,
including any incompatibilities
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
ValueComponents Type
TWA 0.05 mg/m3Quartz (SiO2) (CAS
14808-60-7)
US. OSHA Table Z-1 Limits for Air Contaminants (29 CFR 1910.1000)
FormValueComponents Type
PEL 5 mg/m3 Respirable fraction.Limestone (CAS 1317-65-3)
15 mg/m3 Total dust.
PEL 15 mg/m3 Total dust.Titanium dioxide (CAS
13463-67-7)
BEHR® Drywall Plus Interior Primer & Sealer SDS US
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US. OSHA Table Z-3 (29 CFR 1910.1000)
FormValueComponents Type
TWA 0.1 mg/m3 Respirable.Quartz (SiO2) (CAS
14808-60-7)
2.4 mppcf Respirable.
TWA 5 mg/m3 Respirable fraction.Titanium dioxide (CAS
13463-67-7)
15 mg/m3 Total dust.
50 mppcf Total dust.
15 mppcf Respirable fraction.
US. ACGIH Threshold Limit Values
FormValueComponents Type
TWA 0.025 mg/m3 Respirable fraction.Quartz (SiO2) (CAS
14808-60-7)
TWA 10 mg/m3Titanium dioxide (CAS
13463-67-7)
US. NIOSH: Pocket Guide to Chemical Hazards
FormValueComponents Type
TWA 5 mg/m3 Respirable.Limestone (CAS 1317-65-3)
10 mg/m3 Total
TWA 0.05 mg/m3 Respirable dust.Quartz (SiO2) (CAS
14808-60-7)
No biological exposure limits noted for the ingredient(s).Biological limit values
Good general ventilation should be used. Ventilation rates should be matched to conditions. If
applicable, use process enclosures, local exhaust ventilation, or other engineering controls to
maintain airborne levels below recommended exposure limits. If exposure limits have not been
established, maintain airborne levels to an acceptable level.
Appropriate engineering
controls
Individual protection measures, such as personal protective equipment
Wear safety glasses with side shields (or goggles).Eye/face protection
Skin protection
Wear appropriate chemical resistant gloves.Hand protection
Skin protection
Wear appropriate chemical resistant clothing.Other
If airborne concentrations are above the applicable exposure limits, use NIOSH approved
respiratory protection. Use a positive-pressure air-supplied respirator if there is any potential for an
uncontrolled release, exposure levels are not known, or any other circumstances where
air-purifying respirators may not provide adequate protection.
Respiratory protection
Wear appropriate thermal protective clothing, when necessary.Thermal hazards
Always observe good personal hygiene measures, such as washing after handling the material
and before eating, drinking, and/or smoking. Routinely wash work clothing and protective
equipment to remove contaminants.
General hygiene
considerations
9. Physical and chemical properties
Appearance
Liquid.Physical state
Liquid.Form
White.Color
Slight.Odor
Odor threshold Not available.
pH 7 - 10
Melting point/freezing point Not available.
BEHR® Drywall Plus Interior Primer & Sealer SDS US
953273 Version #: 02 Revision date: 16-June-2020 Issue date: 18-March-2020 3 / 7
Initial boiling point and boiling
range
> 99 °F (> 37.2 °C)
Flash point Not applicable
Evaporation rate Not available.
Not applicable.Flammability (solid, gas)
Upper/lower flammability or explosive limits
Flammability limit - lower
(%)
Not available.
Flammability limit - upper
(%)
Not available.
Vapor pressure Not available.
Vapor density Not available.
Relative density 1.21
Solubility(ies)
Solubility (water)Soluble.
Partition coefficient
(n-octanol/water)
Not available.
Auto-ignition temperature Not available.
Decomposition temperature Not available.
Viscosity 50 - 140 KU at 25°C
Other information
Density 10.08 lbs/gal
Not explosive.Explosive properties
Not oxidizing.Oxidizing properties
VOC 10 g/l (including water) (Material)
42 g/l (excluding water) (Coating)
10. Stability and reactivity
The product is stable and non-reactive under normal conditions of use, storage and transport.Reactivity
Material is stable under normal conditions.Chemical stability
No dangerous reaction known under conditions of normal use.Possibility of hazardous
reactions
Contact with incompatible materials.Conditions to avoid
Fluorine.Incompatible materials
No hazardous decomposition products are known.Hazardous decomposition
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Prolonged inhalation may be harmful.
Skin contact Prolonged skin contact may cause temporary irritation.
Eye contact Direct contact with eyes may cause temporary irritation.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the
physical, chemical and
toxicological characteristics
Direct contact with eyes may cause temporary irritation.
Information on toxicological effects
Acute toxicity
Test ResultsComponents Species
Quartz (SiO2) (CAS 14808-60-7)
Inhalation
Chronic
LOEC Human 0.0563 mg/m3
BEHR® Drywall Plus Interior Primer & Sealer SDS US
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Test ResultsComponents Species
Titanium dioxide (CAS 13463-67-7)
Inhalation
Acute
LC50 Rat 3.43 mg/l, 4 Hours
Oral
LD50 Rat > 5000 mg/kg
Prolonged skin contact may cause temporary irritation.Skin corrosion/irritation
Direct contact with eyes may cause temporary irritation.Serious eye damage/eye
irritation
Respiratory or skin sensitization
Respiratory sensitization Not a respiratory sensitizer.
This product is not expected to cause skin sensitization.Skin sensitization
No data available to indicate product or any components present at greater than 0.1% are
mutagenic or genotoxic.
Germ cell mutagenicity
Carcinogenicity Due to the form of the product, exposure to the potentially carcinogenic components is not
expected.
IARC Monographs. Overall Evaluation of Carcinogenicity
Quartz (SiO2) (CAS 14808-60-7) 1 Carcinogenic to humans.
Titanium dioxide (CAS 13463-67-7) 2B Possibly carcinogenic to humans.
NTP Report on Carcinogens
Quartz (SiO2) (CAS 14808-60-7) Known To Be Human Carcinogen.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Quartz (SiO2) (CAS 14808-60-7) Cancer
This product is not expected to cause reproductive or developmental effects.Reproductive toxicity
Specific target organ toxicity -
single exposure
Not classified.
Specific target organ toxicity -
repeated exposure
Not classified.
Aspiration hazard Not an aspiration hazard.
Chronic effects Prolonged inhalation may be harmful.
12. Ecological information
The product is not classified as environmentally hazardous.Ecotoxicity
No data is available on the degradability of any ingredients in the mixture. Persistence and degradability
No data available.Bioaccumulative potential
No data available.Mobility in soil
Other adverse effects The product contains volatile organic compounds which have a photochemical ozone creation
potential.
13. Disposal considerations
Collect and reclaim or dispose in sealed containers at licensed waste disposal site.Disposal instructions
Dispose in accordance with all applicable regulations.Local disposal regulations
The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
Hazardous waste code
Dispose of in accordance with local regulations. Empty containers or liners may retain some
product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Waste from residues / unused
products
Since emptied containers may retain product residue, follow label warnings even after container is
emptied. Empty containers should be taken to an approved waste handling site for recycling or
disposal.
Contaminated packaging
14. Transport information
DOT
Not regulated as dangerous goods.
BEHR® Drywall Plus Interior Primer & Sealer SDS US
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IATA
Not regulated as dangerous goods.
IMDG
Not regulated as dangerous goods.
Not applicable.Transport in bulk according to
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
This product is not known to be a "Hazardous Chemical" as defined by the OSHA Hazard
Communication Standard, 29 CFR 1910.1200.
All components are listed on or exempt from the U.S. EPA TSCA Inventory List.
US federal regulations
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Not regulated.
CERCLA Hazardous Substance List (40 CFR 302.4)
Not listed.
SARA 304 Emergency release notification
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Quartz (SiO2) (CAS 14808-60-7) Cancer
lung effects
immune system effects
kidney effects
Toxic Substances Control Act (TSCA)
SARA 302 Extremely hazardous substance
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Not listed.
NoSARA 311/312 Hazardous
chemical
SARA 313 (TRI reporting)
Not regulated.
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Contains component(s) regulated under the Safe Drinking Water Act.Safe Drinking Water Act
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Limestone (CAS 1317-65-3)
Quartz (SiO2) (CAS 14808-60-7)
Titanium dioxide (CAS 13463-67-7)
US. New Jersey Worker and Community Right-to-Know Act
Limestone (CAS 1317-65-3)
Quartz (SiO2) (CAS 14808-60-7)
Titanium dioxide (CAS 13463-67-7)
US. Pennsylvania Worker and Community Right-to-Know Law
Limestone (CAS 1317-65-3)
Quartz (SiO2) (CAS 14808-60-7)
Titanium dioxide (CAS 13463-67-7)
US. Rhode Island RTK
Limestone (CAS 1317-65-3)
Quartz (SiO2) (CAS 14808-60-7)
Titanium dioxide (CAS 13463-67-7)
BEHR® Drywall Plus Interior Primer & Sealer SDS US
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16. Other information, including date of preparation or last revision
18-March-2020Issue date
16-June-2020Revision date
Version #02
HMIS® is a registered trade and service mark of the ACA.
B - Safety Glasses, Gloves
Further information
Health: 0
Flammability: 0
Physical hazard: 0
Personal protection: B
HMIS® ratings
List of abbreviations DOT: Department of Transportation (49 CFR 172.101).
IATA: International Air Transport Association.
IBC Code: International Code for the Construction and Equipment of Ships Carrying Dangerous
Chemicals in Bulk.
IMDG Code: International Maritime Dangerous Goods Code.
LC50: Lethal Concentration, 50%.
LD50: Lethal Dose, 50%.
LOEC: Lowest observable effect concentration.
MARPOL: International Convention for the Prevention of Pollution from Ships.
PEL: Permissible Exposure Limit.
TWA: Time Weighted Average Value.
HSDB® - Hazardous Substances Data Bank
IARC Monographs. Overall Evaluation of Carcinogenicity
References
Behr Process Corp cannot anticipate all conditions under which this information and its product, or
the products of other manufacturers in combination with its product, may be used. It is the user’s
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
Disclaimer
BEHR® Drywall Plus Interior Primer & Sealer SDS US
953273 Version #: 02 Revision date: 16-June-2020 Issue date: 18-March-2020 7 / 7
SAFETY DATA SHEET
1. Identification
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure WhiteProduct identifier
Other means of identification
4450Product number
Architectural CoatingRecommended use
None known.Recommended restrictions
Manufacturer/Importer/Supplier/Distributor information
Behr Process Corp.Supplier
1801 E. St. Andrew Place
Santa Ana, CA 92705
714-545-7101Telephone
[phone]Emergency telephone
[phone]
335213Access code
2. Hazard(s) identification
Not classified.Physical hazards
Category 1Sensitization, skinHealth hazards
Category 2Carcinogenicity
Not classified.OSHA defined hazards
Label elements
Signal word Warning
Hazard statement May cause an allergic skin reaction. Suspected of causing cancer.
Precautionary statement
Prevention Obtain special instructions before use. Do not handle until all safety precautions have been read
and understood. Avoid breathing mist/vapors. Contaminated work clothing must not be allowed
out of the workplace. Wear protective gloves/protective clothing/eye protection/face protection.
Response If on skin: Wash with plenty of water. If exposed or concerned: Get medical advice/attention. If
skin irritation or rash occurs: Get medical advice/attention. Take off contaminated clothing and
wash it before reuse.
Storage Store locked up.
Disposal Dispose of contents/container in accordance with local/regional/national/international regulations.
Hazard(s) not otherwise
classified (HNOC)
None known.
Supplemental information None.
3. Composition/information on ingredients
Mixtures
13463-67-7 10 - 30Titanium dioxide
CAS number %Chemical name
14464-46-1 1 - 5Cristobalite
330-54-1 0.1 - 1Diuron
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 1 / 8
68855-54-9 0.1 - 1Flux Calcined Diatomaceous
Earth (DE)
41556-26-7 0.1 - 1Hindered amine light stabilizer
All concentrations are in percent by weight unless ingredient is a gas. Gas concentrations are in
percent by volume.
The manufacturer has claimed the exact percentage as trade secret under the OSHA Hazard
Communication Standard.
Composition comments
4. First-aid measures
Move to fresh air. Call a physician if symptoms develop or persist.Inhalation
Remove contaminated clothing immediately and wash skin with soap and water. In case of
eczema or other skin disorders: Seek medical attention and take along these instructions.Skin contact
Rinse with water. Get medical attention if irritation develops and persists.Eye contact
Rinse mouth. Get medical attention if symptoms occur.Ingestion
May cause an allergic skin reaction. Dermatitis. Rash.Most important
symptoms/effects, acute and
delayed
Provide general supportive measures and treat symptomatically. Keep victim under observation.
Symptoms may be delayed.Indication of immediate
medical attention and special
treatment needed
IF exposed or concerned: Get medical advice/attention. Ensure that medical personnel are aware
of the material(s) involved, and take precautions to protect themselves. Wash contaminated
clothing before reuse.
General information
5. Fire-fighting measures
Water fog. Foam. Dry chemical powder. Carbon dioxide (CO2).Suitable extinguishing media
Do not use water jet as an extinguisher, as this will spread the fire.Unsuitable extinguishing
media
During fire, gases hazardous to health may be formed.Specific hazards arising from
the chemical
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.Special protective equipment
and precautions for firefighters
Move containers from fire area if you can do so without risk.Fire fighting
equipment/instructions
Use standard firefighting procedures and consider the hazards of other involved materials.Specific methods
No unusual fire or explosion hazards noted.General fire hazards
6. Accidental release measures
Keep unnecessary personnel away. Keep people away from and upwind of spill/leak. Wear
appropriate protective equipment and clothing during clean-up. Avoid breathing mist/vapors. Do
not touch damaged containers or spilled material unless wearing appropriate protective clothing.
Ensure adequate ventilation. Local authorities should be advised if significant spillages cannot be
contained. For personal protection, see section 8 of the SDS.
Personal precautions,
protective equipment and
emergency procedures
This product is miscible in water.
Large Spills: Stop the flow of material, if this is without risk. Dike the spilled material, where this is
possible. Absorb in vermiculite, dry sand or earth and place into containers. Following product
recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re-use. Put material in suitable, covered, labeled
containers. For waste disposal, see section 13 of the SDS.
Methods and materials for
containment and cleaning up
Avoid discharge into drains, water courses or onto the ground.Environmental precautions
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 2 / 8
7. Handling and storage
Obtain special instructions before use. Do not handle until all safety precautions have been read
and understood. Avoid breathing mist/vapors. Avoid contact with eyes, skin, and clothing. Avoid
prolonged exposure. Provide adequate ventilation. Wear appropriate personal protective
equipment. Observe good industrial hygiene practices.
Precautions for safe handling
Store locked up. Store in tightly closed container. Store away from incompatible materials (see
Section 10 of the SDS).
Conditions for safe storage,
including any incompatibilities
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
ValueComponents Type
TWA 0.05 mg/m3Flux Calcined
Diatomaceous Earth (DE)
(CAS 68855-54-9)
US. OSHA Table Z-1 Limits for Air Contaminants (29 CFR 1910.1000)
FormValueComponents Type
PEL 0.05 mg/m3 Respirable dust.Cristobalite (CAS
14464-46-1)
PEL 15 mg/m3 Total dust.Titanium dioxide (CAS
13463-67-7)
US. OSHA Table Z-3 (29 CFR 1910.1000)
FormValueComponents Type
TWA 0.05 mg/m3 Respirable.Cristobalite (CAS
14464-46-1)
1.2 mppcf Respirable.
TWA 5 mg/m3 Respirable fraction.Titanium dioxide (CAS
13463-67-7)
15 mg/m3 Total dust.
50 mppcf Total dust.
15 mppcf Respirable fraction.
US. ACGIH Threshold Limit Values
FormValueComponents Type
TWA 0.025 mg/m3 Respirable fraction.Cristobalite (CAS
14464-46-1)
TWA 10 mg/m3Diuron (CAS 330-54-1)
TWA 10 mg/m3Titanium dioxide (CAS
13463-67-7)
US. NIOSH: Pocket Guide to Chemical Hazards
FormValueComponents Type
TWA 0.05 mg/m3 Respirable dust.Cristobalite (CAS
14464-46-1)
TWA 10 mg/m3Diuron (CAS 330-54-1)
No biological exposure limits noted for the ingredient(s).Biological limit values
Good general ventilation should be used. Ventilation rates should be matched to conditions. If
applicable, use process enclosures, local exhaust ventilation, or other engineering controls to
maintain airborne levels below recommended exposure limits. If exposure limits have not been
established, maintain airborne levels to an acceptable level.
Appropriate engineering
controls
Individual protection measures, such as personal protective equipment
Wear safety glasses with side shields (or goggles).Eye/face protection
Skin protection
Wear appropriate chemical resistant gloves.Hand protection
Skin protection
Wear appropriate chemical resistant clothing. Use of an impervious apron is recommended.Other
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 3 / 8
If airborne concentrations are above the applicable exposure limits, use NIOSH approved
respiratory protection. Use a positive-pressure air-supplied respirator if there is any potential for an
uncontrolled release, exposure levels are not known, or any other circumstances where
air-purifying respirators may not provide adequate protection.
Respiratory protection
Wear appropriate thermal protective clothing, when necessary.Thermal hazards
Observe any medical surveillance requirements. Always observe good personal hygiene
measures, such as washing after handling the material and before eating, drinking, and/or
smoking. Routinely wash work clothing and protective equipment to remove contaminants.
Contaminated work clothing should not be allowed out of the workplace.
General hygiene
considerations
9. Physical and chemical properties
Appearance
Liquid.Physical state
Liquid.Form
White.Color
Slight.Odor
Odor threshold Not available.
pH 7 - 10
Melting point/freezing point Not available.
Initial boiling point and boiling
range
> 99 °F (> 37.2 °C)
Flash point Not available.
Evaporation rate Not available.
Not applicable.Flammability (solid, gas)
Upper/lower flammability or explosive limits
Flammability limit - lower
(%)
Not available.
Flammability limit - upper
(%)
Not available.
Vapor pressure Not available.
Vapor density Not available.
Relative density 1.37
Solubility(ies)
Solubility (water)Soluble.
Partition coefficient
(n-octanol/water)
Not available.
Auto-ignition temperature Not available.
Decomposition temperature Not available.
Viscosity 50 - 140 KU at 25°C
Other information
Density 11.39 lbs/gal
Not explosive.Explosive properties
Not oxidizing.Oxidizing properties
VOC 12 g/l (including water) (Material)
25 g/l (excluding water) (Coating)
10. Stability and reactivity
The product is stable and non-reactive under normal conditions of use, storage and transport.Reactivity
Material is stable under normal conditions.Chemical stability
No dangerous reaction known under conditions of normal use.Possibility of hazardous
reactions
Contact with incompatible materials.Conditions to avoid
Strong oxidizing agents.Incompatible materials
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 4 / 8
No hazardous decomposition products are known.Hazardous decomposition
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Prolonged inhalation may be harmful.
Skin contact May cause an allergic skin reaction.
Eye contact Direct contact with eyes may cause temporary irritation.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the
physical, chemical and
toxicological characteristics
May cause an allergic skin reaction. Dermatitis. Rash.
Information on toxicological effects
Acute toxicity
Test ResultsComponents Species
Titanium dioxide (CAS 13463-67-7)
Oral
Acute
LD50 Rat > 5000 mg/kg
Prolonged skin contact may cause temporary irritation.Skin corrosion/irritation
Direct contact with eyes may cause temporary irritation.Serious eye damage/eye
irritation
Respiratory or skin sensitization
Respiratory sensitization Not a respiratory sensitizer.
May cause an allergic skin reaction.Skin sensitization
No data available to indicate product or any components present at greater than 0.1% are
mutagenic or genotoxic.Germ cell mutagenicity
Carcinogenicity Suspected of causing cancer.
IARC Monographs. Overall Evaluation of Carcinogenicity
Cristobalite (CAS 14464-46-1) 1 Carcinogenic to humans.
Titanium dioxide (CAS 13463-67-7) 2B Possibly carcinogenic to humans.
NTP Report on Carcinogens
Cristobalite (CAS 14464-46-1) Known To Be Human Carcinogen.
Reasonably Anticipated to be a Human Carcinogen.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Cristobalite (CAS 14464-46-1) Cancer
Flux Calcined Diatomaceous Earth (DE)
(CAS 68855-54-9)
Cancer
This product is not expected to cause reproductive or developmental effects.Reproductive toxicity
Specific target organ toxicity -
single exposure
Not classified.
Specific target organ toxicity -
repeated exposure
Not classified.
Aspiration hazard Not an aspiration hazard.
Chronic effects Prolonged inhalation may be harmful.
12. Ecological information
Toxic to aquatic life with long lasting effects.Ecotoxicity
No data is available on the degradability of any ingredients in the mixture. Persistence and degradability
No data available.Bioaccumulative potential
No data available.Mobility in soil
Other adverse effects The product contains volatile organic compounds which have a photochemical ozone creation
potential.
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 5 / 8
13. Disposal considerations
Collect and reclaim or dispose in sealed containers at licensed waste disposal site. Incinerate the
material under controlled conditions in an approved incinerator. Dispose of contents/container in
accordance with local/regional/national/international regulations.
Disposal instructions
Dispose in accordance with all applicable regulations.Local disposal regulations
The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.Hazardous waste code
Dispose of in accordance with local regulations. Empty containers or liners may retain some
product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Waste from residues / unused
products
Since emptied containers may retain product residue, follow label warnings even after container is
emptied. Empty containers should be taken to an approved waste handling site for recycling or
disposal.
Contaminated packaging
14. Transport information
DOT
Not regulated as dangerous goods.
IATA
UN3082UN number
Environmentally hazardous substance, liquid, n.o.s. (Diuron, Bis
(1,2,2,6,6-pentamethyl-4-piperidinyl) sebacate)
UN proper shipping name
9Class
Transport hazard class(es)
-Subsidiary risk
IIIPacking group
YesEnvironmental hazards
9LERG Code
Read safety instructions, SDS and emergency procedures before handling.Special precautions for user
IMDG
UN3082UN number
ENVIRONMENTALLY HAZARDOUS SUBSTANCE, LIQUID, N.O.S. (Diuron, Bis
(1,2,2,6,6-pentamethyl-4-piperidinyl) sebacate)
UN proper shipping name
9Class
Transport hazard class(es)
-Subsidiary risk
IIIPacking group
YesMarine pollutant
Environmental hazards
F-A, S-FEmS
Read safety instructions, SDS and emergency procedures before handling.Special precautions for user
Not applicable.Transport in bulk according to
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
This product is a "Hazardous Chemical" as defined by the OSHA Hazard Communication
Standard, 29 CFR 1910.1200.
US federal regulations
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Not regulated.
CERCLA Hazardous Substance List (40 CFR 302.4)
2-Benzimidazole carbamic acid, methyl ester
(CAS 10605-21-7)
Listed.
Ammonium hydroxide (CAS 1336-21-6) Listed.
Diuron (CAS 330-54-1) Listed.
SARA 304 Emergency release notification
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Cristobalite (CAS 14464-46-1) Cancer
Flux Calcined Diatomaceous Earth (DE)
(CAS 68855-54-9)
Cancer
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 6 / 8
Cristobalite (CAS 14464-46-1) lung effects
Flux Calcined Diatomaceous Earth (DE)
(CAS 68855-54-9)
lung effects
Cristobalite (CAS 14464-46-1) immune system effects
Flux Calcined Diatomaceous Earth (DE)
(CAS 68855-54-9)
immune system effects
Cristobalite (CAS 14464-46-1) kidney effects
Flux Calcined Diatomaceous Earth (DE)
(CAS 68855-54-9)
kidney effects
Toxic Substances Control Act (TSCA)All components are listed on or exempt from the U.S. EPA TSCA Inventory
List.
SARA 302 Extremely hazardous substance
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Not listed.
YesSARA 311/312 Hazardous
chemical
Respiratory or skin sensitization
Carcinogenicity
Classified hazard
categories
SARA 313 (TRI reporting)
Not regulated.
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Contains component(s) regulated under the Safe Drinking Water Act.Safe Drinking Water Act
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Ammonium hydroxide (CAS 1336-21-6)
Cristobalite (CAS 14464-46-1)
Diuron (CAS 330-54-1)
Titanium dioxide (CAS 13463-67-7)
US. New Jersey Worker and Community Right-to-Know Act
2-Benzimidazole carbamic acid, methyl ester (CAS 10605-21-7)
Ammonium hydroxide (CAS 1336-21-6)
Cristobalite (CAS 14464-46-1)
Diuron (CAS 330-54-1)
Mildewcide (CAS 55406-53-6)
Titanium dioxide (CAS 13463-67-7)
US. Pennsylvania Worker and Community Right-to-Know Law
Ammonium hydroxide (CAS 1336-21-6)
Cristobalite (CAS 14464-46-1)
Diuron (CAS 330-54-1)
Flux Calcined Diatomaceous Earth (DE) (CAS 68855-54-9)
Titanium dioxide (CAS 13463-67-7)
US. Rhode Island RTK
Cristobalite (CAS 14464-46-1)
Diuron (CAS 330-54-1)
Titanium dioxide (CAS 13463-67-7)
16. Other information, including date of preparation or last revision
04-December-2019Issue date
13-August-2020Revision date
Version #02
Health: 2*
Flammability: 0
Physical hazard: 0
HMIS® ratings
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 7 / 8
List of abbreviations DOT: Department of Transportation (49 CFR 172.101).
IATA: International Air Transport Association.
IBC Code: International Code for the Construction and Equipment of Ships Carrying Dangerous
Chemicals in Bulk.
IMDG Code: International Maritime Dangerous Goods Code.
LC50: Lethal Concentration, 50%.
LD50: Lethal Dose, 50%.
MARPOL: International Convention for the Prevention of Pollution from Ships.
PEL: Permissible Exposure Limit.
TWA: Time Weighted Average Value.
HSDB® - Hazardous Substances Data Bank
IARC Monographs. Overall Evaluation of Carcinogenicity
References
Behr Process Corp cannot anticipate all conditions under which this information and its product, or
the products of other manufacturers in combination with its product, may be used. It is the user’s
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
Disclaimer
BEHR® MARQUEE Exterior Flat Paint & Primer - Ultra Pure White SDS US
952079 Version #: 02 Revision date: 13-August-2020 Issue date: 04-December-2019 8 / 8
SAFETY DATA SHEET
1. Identification
BEHR ULTRA™ Scuff Defense™ Interior Eggshell - Ultra Pure WhiteProduct identifier
Other means of identification
2750Product number
Architectural CoatingRecommended use
None known.Recommended restrictions
Manufacturer/Importer/Supplier/Distributor information
Behr Process Corp.Supplier
1801 E. St. Andrew Place
Santa Ana, CA 92705
714-545-7101Telephone
[phone]Emergency telephone
[phone]
335213Access code
2. Hazard(s) identification
Not classified.Physical hazards
Not classified.Health hazards
Not classified.OSHA defined hazards
Label elements
None.Hazard symbol
Signal word None.
Hazard statement The mixture does not meet the criteria for classification.
Precautionary statement
Prevention Observe good industrial hygiene practices.
Response Wash hands after handling.
Storage Store away from incompatible materials.
Disposal Dispose of waste and residues in accordance with local authority requirements.
Hazard(s) not otherwise
classified (HNOC)
None known.
Supplemental information None.
3. Composition/information on ingredients
Mixtures
13463-67-7 10 - 30Titanium dioxide
CAS number %Chemical name
All concentrations are in percent by weight unless ingredient is a gas. Gas concentrations are in
percent by volume.
The manufacturer has claimed the exact percentage as trade secret under the OSHA Hazard
Communication Standard.
Composition comments
4. First-aid measures
Move to fresh air. Call a physician if symptoms develop or persist.Inhalation
Wash off with soap and water. Get medical attention if irritation develops and persists.Skin contact
Rinse with water. Get medical attention if irritation develops and persists.Eye contact
Rinse mouth. Get medical attention if symptoms occur.Ingestion
BEHR ULTRA™ Scuff Defense™ Interior Eggshell - Ultra Pure White SDS US
951816 Version #: 01 Revision date: - Issue date: 15-July-2020 1 / 6
Direct contact with eyes may cause temporary irritation.Most important
symptoms/effects, acute and
delayed
Treat symptomatically.Indication of immediate
medical attention and special
treatment needed
Ensure that medical personnel are aware of the material(s) involved, and take precautions to
protect themselves.
General information
5. Fire-fighting measures
Water fog. Foam. Dry chemical powder. Carbon dioxide (CO2).Suitable extinguishing media
Do not use water jet as an extinguisher, as this will spread the fire.Unsuitable extinguishing
media
During fire, gases hazardous to health may be formed.Specific hazards arising from
the chemical
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.Special protective equipment
and precautions for firefighters
Move containers from fire area if you can do so without risk.Fire fighting
equipment/instructions
Use standard firefighting procedures and consider the hazards of other involved materials.Specific methods
No unusual fire or explosion hazards noted.General fire hazards
6. Accidental release measures
Keep unnecessary personnel away. For personal protection, see section 8 of the SDS.Personal precautions,
protective equipment and
emergency procedures
This product is miscible in water.
Large Spills: Stop the flow of material, if this is without risk. Dike the spilled material, where this is
possible. Absorb in vermiculite, dry sand or earth and place into containers. Following product
recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re-use. For waste disposal, see section 13 of the SDS.
Methods and materials for
containment and cleaning up
Avoid discharge into drains, water courses or onto the ground.Environmental precautions
7. Handling and storage
Observe good industrial hygiene practices.Precautions for safe handling
Store in tightly closed container. Store away from incompatible materials (see Section 10 of the
SDS).
Conditions for safe storage,
including any incompatibilities
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Table Z-1 Limits for Air Contaminants (29 CFR 1910.1000)
FormValueComponents Type
PEL 15 mg/m3 Total dust.Titanium dioxide (CAS
13463-67-7)
US. OSHA Table Z-3 (29 CFR 1910.1000)
FormValueComponents Type
TWA 5 mg/m3 Respirable fraction.Titanium dioxide (CAS
13463-67-7)
15 mg/m3 Total dust.
50 mppcf Total dust.
15 mppcf Respirable fraction.
BEHR ULTRA™ Scuff Defense™ Interior Eggshell - Ultra Pure White SDS US
951816 Version #: 01 Revision date: - Issue date: 15-July-2020 2 / 6
US. ACGIH Threshold Limit Values
ValueComponents Type
TWA 10 mg/m3Titanium dioxide (CAS
13463-67-7)
No biological exposure limits noted for the ingredient(s).Biological limit values
Good general ventilation should be used. Ventilation rates should be matched to conditions. If
applicable, use process enclosures, local exhaust ventilation, or other engineering controls to
maintain airborne levels below recommended exposure limits. If exposure limits have not been
established, maintain airborne levels to an acceptable level.
Appropriate engineering
controls
Individual protection measures, such as personal protective equipment
Wear safety glasses with side shields (or goggles).Eye/face protection
Skin protection
Wear appropriate chemical resistant gloves.Hand protection
Skin protection
Wear suitable protective clothing.Other
If airborne concentrations are above the applicable exposure limits, use NIOSH approved
respiratory protection. Use a positive-pressure air-supplied respirator if there is any potential for an
uncontrolled release, exposure levels are not known, or any other circumstances where
air-purifying respirators may not provide adequate protection.
Respiratory protection
Wear appropriate thermal protective clothing, when necessary.Thermal hazards
Always observe good personal hygiene measures, such as washing after handling the material
and before eating, drinking, and/or smoking. Routinely wash work clothing and protective
equipment to remove contaminants.
General hygiene
considerations
9. Physical and chemical properties
Appearance
Liquid.Physical state
Liquid.Form
White.Color
Slight.Odor
Odor threshold Not available.
pH 7 - 10
Melting point/freezing point Not available.
Initial boiling point and boiling
range
> 99 °F (> 37.2 °C)
Flash point Not applicable
Evaporation rate Not available.
Not applicable.Flammability (solid, gas)
Upper/lower flammability or explosive limits
Flammability limit - lower
(%)
Not available.
Flammability limit - upper
(%)
Not available.
Vapor pressure Not available.
Vapor density Not available.
Relative density 1.33
Solubility(ies)
Solubility (water)Soluble.
Partition coefficient
(n-octanol/water)
Not available.
Auto-ignition temperature Not available.
Decomposition temperature Not available.
Viscosity 50 - 140 KU at 25°C
BEHR ULTRA™ Scuff Defense™ Interior Eggshell - Ultra Pure White SDS US
951816 Version #: 01 Revision date: - Issue date: 15-July-2020 3 / 6
Other information
Density 11.05 lbs/gal
Not explosive.Explosive properties
Not oxidizing.Oxidizing properties
VOC 20 g/l (including water) (Material)
47 g/l (excluding water) (Coating)
10. Stability and reactivity
The product is stable and non-reactive under normal conditions of use, storage and transport.Reactivity
Material is stable under normal conditions.Chemical stability
No dangerous reaction known under conditions of normal use.Possibility of hazardous
reactions
Contact with incompatible materials.Conditions to avoid
Strong oxidizing agents.Incompatible materials
No hazardous decomposition products are known.Hazardous decomposition
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Prolonged inhalation may be harmful.
Skin contact Prolonged skin contact may cause temporary irritation.
Eye contact Direct contact with eyes may cause temporary irritation.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the
physical, chemical and
toxicological characteristics
Direct contact with eyes may cause temporary irritation.
Information on toxicological effects
Acute toxicity
Test ResultsComponents Species
Titanium dioxide (CAS 13463-67-7)
Oral
Acute
LD50 Rat > 5000 mg/kg
Prolonged skin contact may cause temporary irritation.Skin corrosion/irritation
Direct contact with eyes may cause temporary irritation.Serious eye damage/eye
irritation
Respiratory or skin sensitization
Respiratory sensitization Not a respiratory sensitizer.
This product is not expected to cause skin sensitization.Skin sensitization
No data available to indicate product or any components present at greater than 0.1% are
mutagenic or genotoxic.
Germ cell mutagenicity
Carcinogenicity Inhalation of titanium dioxide dust may cause cancer, however due to the physical form of the
product, inhalation of dust is not likely.
IARC Monographs. Overall Evaluation of Carcinogenicity
Titanium dioxide (CAS 13463-67-7) 2B Possibly carcinogenic to humans.
NTP Report on Carcinogens
Not listed.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Not listed.
This product is not expected to cause reproductive or developmental effects.Reproductive toxicity
Specific target organ toxicity -
single exposure
Not classified.
Specific target organ toxicity -
repeated exposure
Not classified.
BEHR ULTRA™ Scuff Defense™ Interior Eggshell - Ultra Pure White SDS US
951816 Version #: 01 Revision date: - Issue date: 15-July-2020 4 / 6
Aspiration hazard Not an aspiration hazard.
Chronic effects Prolonged inhalation may be harmful.
12. Ecological information
Harmful to aquatic life.Ecotoxicity
No data is available on the degradability of any ingredients in the mixture. Persistence and degradability
No data available.Bioaccumulative potential
No data available.Mobility in soil
Other adverse effects The product contains volatile organic compounds which have a photochemical ozone creation
potential.
13. Disposal considerations
Collect and reclaim or dispose in sealed containers at licensed waste disposal site. Incinerate the
material under controlled conditions in an approved incinerator.
Disposal instructions
Dispose in accordance with all applicable regulations.Local disposal regulations
The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.
Hazardous waste code
Dispose of in accordance with local regulations. Empty containers or liners may retain some
product residues. This material and its container must be disposed of in a safe manner (see:
Disposal instructions).
Waste from residues / unused
products
Since emptied containers may retain product residue, follow label warnings even after container is
emptied. Empty containers should be taken to an approved waste handling site for recycling or
disposal.
Contaminated packaging
14. Transport information
DOT
Not regulated as dangerous goods.
IATA
Not regulated as dangerous goods.
IMDG
Not regulated as dangerous goods.
Not applicable.Transport in bulk according to
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
This product is not known to be a "Hazardous Chemical" as defined by the OSHA Hazard
Communication Standard, 29 CFR 1910.1200.
All components are listed on or exempt from the U.S. EPA TSCA Inventory List.
US federal regulations
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Not regulated.
CERCLA Hazardous Substance List (40 CFR 302.4)
Ammonium hydroxide (CAS 1336-21-6) Listed.
SARA 304 Emergency release notification
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Not listed.
Toxic Substances Control Act (TSCA)
SARA 302 Extremely hazardous substance
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Not listed.
NoSARA 311/312 Hazardous
chemical
SARA 313 (TRI reporting)
Not regulated.
BEHR ULTRA™ Scuff Defense™ Interior Eggshell - Ultra Pure White SDS US
951816 Version #: 01 Revision date: - Issue date: 15-July-2020 5 / 6
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Contains component(s) regulated under the Safe Drinking Water Act.Safe Drinking Water Act
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Ammonium hydroxide (CAS 1336-21-6)
Titanium dioxide (CAS 13463-67-7)
US. New Jersey Worker and Community Right-to-Know Act
Ammonium hydroxide (CAS 1336-21-6)
Titanium dioxide (CAS 13463-67-7)
US. Pennsylvania Worker and Community Right-to-Know Law
Ammonium hydroxide (CAS 1336-21-6)
Titanium dioxide (CAS 13463-67-7)
US. Rhode Island RTK
Titanium dioxide (CAS 13463-67-7)
16. Other information, including date of preparation or last revision
15-July-2020Issue date
-Revision date
Version #01
Health: 0
Flammability: 0
Physical hazard: 0
Personal protection: B
HMIS® ratings
List of abbreviations DOT: Department of Transportation (49 CFR 172.101).
IATA: International Air Transport Association.
IBC Code: International Code for the Construction and Equipment of Ships Carrying Dangerous
Chemicals in Bulk.
IMDG Code: International Maritime Dangerous Goods Code.
LC50: Lethal Concentration, 50%.
LD50: Lethal Dose, 50%.
MARPOL: International Convention for the Prevention of Pollution from Ships.
PEL: Permissible Exposure Limit.
TWA: Time Weighted Average Value.
HSDB® - Hazardous Substances Data Bank
IARC Monographs. Overall Evaluation of Carcinogenicity
References
Behr Process Corp cannot anticipate all conditions under which this information and its product, or
the products of other manufacturers in combination with its product, may be used. It is the user’s
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
Disclaimer
BEHR ULTRA™ Scuff Defense™ Interior Eggshell - Ultra Pure White SDS US
951816 Version #: 01 Revision date: - Issue date: 15-July-2020 6 / 6
SAFETY DATA SHEET
1. Identification
BEHR® PREMIUM Interior/Exterior Direct-to-Metal Semi-Gloss Paint - Deep BaseProduct identifier
Other means of identification
3230Product number
Architectural CoatingRecommended use
None known.Recommended restrictions
Manufacturer/Importer/Supplier/Distributor information
Behr Process Corp.Supplier
1801 E. St. Andrew Place
Santa Ana, CA 92705
714-545-7101Telephone
[phone]Emergency telephone
[phone]
335213Access code
2. Hazard(s) identification
Not classified.Physical hazards
Category 2CarcinogenicityHealth hazards
Not classified.OSHA defined hazards
Label elements
Signal word Warning
Hazard statement Suspected of causing cancer.
Precautionary statement
Prevention Obtain special instructions before use. Do not handle until all safety precautions have been read
and understood. Wear protective gloves/protective clothing/eye protection/face protection.
Response If exposed or concerned: Get medical advice/attention.
Storage Store locked up.
Disposal Dispose of contents/container in accordance with local/regional/national/international regulations.
Hazard(s) not otherwise
classified (HNOC)
None known.
Supplemental information None.
3. Composition/information on ingredients
Mixtures
1332-58-7 5 - 10Kaolin
CAS number %Chemical name
119-61-9 0.1 - 1Diphenyl ketone
All concentrations are in percent by weight unless ingredient is a gas. Gas concentrations are in
percent by volume.
The manufacturer has claimed the exact percentage as trade secret under the OSHA Hazard
Communication Standard.
Composition comments
BEHR® PREMIUM Interior/Exterior Direct-to-Metal Semi-Gloss Paint - Deep Base SDS US
952106 Version #: 02 Revision date: 14-August-2020 Issue date: 05-December-2019 1 / 6
4. First-aid measures
Move to fresh air. Call a physician if symptoms develop or persist.Inhalation
Wash off with soap and water. Get medical attention if irritation develops and persists.Skin contact
Rinse with water. Get medical attention if irritation develops and persists.Eye contact
Rinse mouth. Get medical attention if symptoms occur.Ingestion
Direct contact with eyes may cause temporary irritation.Most important
symptoms/effects, acute and
delayed
Provide general supportive measures and treat symptomatically. Keep victim under observation.
Symptoms may be delayed.
Indication of immediate
medical attention and special
treatment needed
IF exposed or concerned: Get medical advice/attention. Ensure that medical personnel are aware
of the material(s) involved, and take precautions to protect themselves.
General information
5. Fire-fighting measures
Water fog. Foam. Dry chemical powder. Carbon dioxide (CO2).Suitable extinguishing media
Do not use water jet as an extinguisher, as this will spread the fire.Unsuitable extinguishing
media
During fire, gases hazardous to health may be formed.Specific hazards arising from
the chemical
Self-contained breathing apparatus and full protective clothing must be worn in case of fire.Special protective equipment
and precautions for firefighters
Move containers from fire area if you can do so without risk.Fire fighting
equipment/instructions
Use standard firefighting procedures and consider the hazards of other involved materials.Specific methods
No unusual fire or explosion hazards noted.General fire hazards
6. Accidental release measures
Keep unnecessary personnel away. Keep people away from and upwind of spill/leak. Wear
appropriate protective equipment and clothing during clean-up. Ensure adequate ventilation. Local
authorities should be advised if significant spillages cannot be contained. For personal protection,
see section 8 of the SDS.
Personal precautions,
protective equipment and
emergency procedures
This product is miscible in water.
Large Spills: Stop the flow of material, if this is without risk. Dike the spilled material, where this is
possible. Absorb in vermiculite, dry sand or earth and place into containers. Following product
recovery, flush area with water.
Small Spills: Wipe up with absorbent material (e.g. cloth, fleece). Clean surface thoroughly to
remove residual contamination.
Never return spills to original containers for re-use. Put material in suitable, covered, labeled
containers. For waste disposal, see section 13 of the SDS.
Methods and materials for
containment and cleaning up
Avoid discharge into drains, water courses or onto the ground.Environmental precautions
7. Handling and storage
Obtain special instructions before use. Do not handle until all safety precautions have been read
and understood. Avoid prolonged exposure. Should be handled in closed systems, if possible.
Provide adequate ventilation. Wear appropriate personal protective equipment. Observe good
industrial hygiene practices.
Precautions for safe handling
Store locked up. Store in tightly closed container. Store away from incompatible materials (see
Section 10 of the SDS).
Conditions for safe storage,
including any incompatibilities
8. Exposure controls/personal protection
Occupational exposure limits
US. OSHA Table Z-1 Limits for Air Contaminants (29 CFR 1910.1000)
FormValueComponents Type
PEL 5 mg/m3 Respirable fraction.Kaolin (CAS 1332-58-7)
15 mg/m3 Total dust.
BEHR® PREMIUM Interior/Exterior Direct-to-Metal Semi-Gloss Paint - Deep Base SDS US
952106 Version #: 02 Revision date: 14-August-2020 Issue date: 05-December-2019 2 / 6
US. OSHA Table Z-3 (29 CFR 1910.1000)
FormValueComponents Type
TWA 5 mg/m3 Respirable fraction.Kaolin (CAS 1332-58-7)
15 mg/m3 Total dust.
50 mppcf Total dust.
15 mppcf Respirable fraction.
US. ACGIH Threshold Limit Values
FormValueComponents Type
TWA 2 mg/m3 Respirable fraction.Kaolin (CAS 1332-58-7)
US. NIOSH: Pocket Guide to Chemical Hazards
FormValueComponents Type
TWA 5 mg/m3 Respirable.Kaolin (CAS 1332-58-7)
10 mg/m3 Total
US. Workplace Environmental Exposure Level (WEEL) Guides
ValueComponents Type
TWA 0.5 mg/m3Diphenyl ketone (CAS
119-61-9)
No biological exposure limits noted for the ingredient(s).Biological limit values
Good general ventilation should be used. Ventilation rates should be matched to conditions. If
applicable, use process enclosures, local exhaust ventilation, or other engineering controls to
maintain airborne levels below recommended exposure limits. If exposure limits have not been
established, maintain airborne levels to an acceptable level.
Appropriate engineering
controls
Individual protection measures, such as personal protective equipment
Wear safety glasses with side shields (or goggles).Eye/face protection
Skin protection
Wear appropriate chemical resistant gloves.Hand protection
Skin protection
Use of an impervious apron is recommended.Other
If airborne concentrations are above the applicable exposure limits, use NIOSH approved
respiratory protection. Use a positive-pressure air-supplied respirator if there is any potential for an
uncontrolled release, exposure levels are not known, or any other circumstances where
air-purifying respirators may not provide adequate protection.
Respiratory protection
Wear appropriate thermal protective clothing, when necessary.Thermal hazards
Observe any medical surveillance requirements. Always observe good personal hygiene
measures, such as washing after handling the material and before eating, drinking, and/or
smoking. Routinely wash work clothing and protective equipment to remove contaminants.
General hygiene
considerations
9. Physical and chemical properties
Appearance
Liquid.Physical state
Liquid.Form
Opaque.Color
Slight.Odor
Odor threshold Not available.
pH 7 - 10
Melting point/freezing point Not available.
Initial boiling point and boiling
range
> 99 °F (> 37.2 °C)
Flash point Not applicable.
BEHR® PREMIUM Interior/Exterior Direct-to-Metal Semi-Gloss Paint - Deep Base SDS US
952106 Version #: 02 Revision date: 14-August-2020 Issue date: 05-December-2019 3 / 6
Evaporation rate Not available.
Not applicable.Flammability (solid, gas)
Upper/lower flammability or explosive limits
Flammability limit - lower
(%)
Not available.
Flammability limit - upper
(%)
Not available.
Vapor pressure Not available.
Vapor density Not available.
Relative density 1.11
Solubility(ies)
Solubility (water)Soluble.
Partition coefficient
(n-octanol/water)
Not available.
Auto-ignition temperature Not available.
Decomposition temperature Not available.
Viscosity 50 - 140 KU at 25°C
Other information
Density 9.25 lbs/gal
Not explosive.Explosive properties
Not oxidizing.Oxidizing properties
VOC 14 g/l (including water) (Material)
42 g/l (excluding water) (Coating)
10. Stability and reactivity
The product is stable and non-reactive under normal conditions of use, storage and transport.Reactivity
Material is stable under normal conditions.Chemical stability
No dangerous reaction known under conditions of normal use.Possibility of hazardous
reactions
Contact with incompatible materials.Conditions to avoid
Strong oxidizing agents.Incompatible materials
No hazardous decomposition products are known.Hazardous decomposition
products
11. Toxicological information
Information on likely routes of exposure
Inhalation Prolonged inhalation may be harmful.
Skin contact Prolonged skin contact may cause temporary irritation.
Eye contact Direct contact with eyes may cause temporary irritation.
Ingestion Expected to be a low ingestion hazard.
Symptoms related to the
physical, chemical and
toxicological characteristics
Direct contact with eyes may cause temporary irritation.
Information on toxicological effects
Acute toxicity
Test ResultsComponents Species
Diphenyl ketone (CAS 119-61-9)
Dermal
Acute
LD50 Rabbit 3535 mg/kg
Prolonged skin contact may cause temporary irritation.Skin corrosion/irritation
Direct contact with eyes may cause temporary irritation.Serious eye damage/eye
irritation
BEHR® PREMIUM Interior/Exterior Direct-to-Metal Semi-Gloss Paint - Deep Base SDS US
952106 Version #: 02 Revision date: 14-August-2020 Issue date: 05-December-2019 4 / 6
Respiratory or skin sensitization
Respiratory sensitization Not a respiratory sensitizer.
This product is not expected to cause skin sensitization.Skin sensitization
No data available to indicate product or any components present at greater than 0.1% are
mutagenic or genotoxic.
Germ cell mutagenicity
Carcinogenicity Suspected of causing cancer.
IARC Monographs. Overall Evaluation of Carcinogenicity
Diphenyl ketone (CAS 119-61-9) 2B Possibly carcinogenic to humans.
NTP Report on Carcinogens
Not listed.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Not listed.
This product is not expected to cause reproductive or developmental effects.Reproductive toxicity
Specific target organ toxicity -
single exposure
Not classified.
Specific target organ toxicity -
repeated exposure
Not classified.
Aspiration hazard Not an aspiration hazard.
Chronic effects Prolonged inhalation may be harmful. Prolonged exposure may cause chronic effects.
12. Ecological information
Harmful to aquatic life with long lasting effects.Ecotoxicity
No data is available on the degradability of any ingredients in the mixture. Persistence and degradability
No data available.Bioaccumulative potential
No data available.Mobility in soil
Other adverse effects The product contains volatile organic compounds which have a photochemical ozone creation
potential.
13. Disposal considerations
Collect and reclaim or dispose in sealed containers at licensed waste disposal site. Incinerate the
material under controlled conditions in an approved incinerator. Dispose of contents/container in
accordance with local/regional/national/international regulations.
Disposal instructions
Dispose in accordance with all applicable regulations.Local disposal regulations
The waste code should be assigned in discussion between the user, the producer and the waste
disposal company.Hazardous waste code
Dispose of in accordance with local regulations. Empty containers or liners may retain some
product residues. This material and its container must be disposed of in a safe manner.
Waste from residues / unused
products
Since emptied containers may retain product residue, follow label warnings even after container is
emptied. Empty containers should be taken to an approved waste handling site for recycling or
disposal.
Contaminated packaging
14. Transport information
DOT
Not regulated as dangerous goods.
IATA
Not regulated as dangerous goods.
IMDG
Not regulated as dangerous goods.
Not applicable.Transport in bulk according to
Annex II of MARPOL 73/78 and
the IBC Code
15. Regulatory information
This product is a "Hazardous Chemical" as defined by the OSHA Hazard Communication
Standard, 29 CFR 1910.1200.US federal regulations
TSCA Section 12(b) Export Notification (40 CFR 707, Subpt. D)
Diphenyl ketone (CAS 119-61-9) 0.1 % One-Time Export Notification only.
BEHR® PREMIUM Interior/Exterior Direct-to-Metal Semi-Gloss Paint - Deep Base SDS US
952106 Version #: 02 Revision date: 14-August-2020 Issue date: 05-December-2019 5 / 6
CERCLA Hazardous Substance List (40 CFR 302.4)
Not listed.
SARA 304 Emergency release notification
Not regulated.
OSHA Specifically Regulated Substances (29 CFR 1910.1001-1053)
Not listed.
Toxic Substances Control Act (TSCA)All components are listed on or exempt from the U.S. EPA TSCA Inventory
List.
SARA 302 Extremely hazardous substance
Superfund Amendments and Reauthorization Act of 1986 (SARA)
Not listed.
YesSARA 311/312 Hazardous
chemical
CarcinogenicityClassified hazard
categories
SARA 313 (TRI reporting)
Not regulated.
Other federal regulations
Clean Air Act (CAA) Section 112 Hazardous Air Pollutants (HAPs) List
Not regulated.
Clean Air Act (CAA) Section 112(r) Accidental Release Prevention (40 CFR 68.130)
Not regulated.
Contains component(s) regulated under the Safe Drinking Water Act.Safe Drinking Water Act
(SDWA)
US state regulations
US. Massachusetts RTK - Substance List
Kaolin (CAS 1332-58-7)
US. New Jersey Worker and Community Right-to-Know Act
Kaolin (CAS 1332-58-7)
US. Pennsylvania Worker and Community Right-to-Know Law
Kaolin (CAS 1332-58-7)
US. Rhode Island RTK
Kaolin (CAS 1332-58-7)
16. Other information, including date of preparation or last revision
05-December-2019Issue date
14-August-2020Revision date
Version #02
Health: 0*
Flammability: 0
Physical hazard: 0
HMIS® ratings
List of abbreviations DOT: Department of Transportation (49 CFR 172.101).
IATA: International Air Transport Association.
IBC Code: International Code for the Construction and Equipment of Ships Carrying Dangerous
Chemicals in Bulk.
IMDG Code: International Maritime Dangerous Goods Code.
LD50: Lethal Dose 50%.
MARPOL: International Convention for the Prevention of Pollution from Ships.
PEL: Permissible Exposure Limit.
TWA: Time Weighted Average Value.
HSDB® - Hazardous Substances Data Bank
IARC Monographs. Overall Evaluation of Carcinogenicity
National Toxicology Program (NTP) Report on Carcinogens
References
Behr Process Corp cannot anticipate all conditions under which this information and its product, or
the products of other manufacturers in combination with its product, may be used. It is the user’s
responsibility to ensure safe conditions for handling, storage and disposal of the product, and to
assume liability for loss, injury, damage or expense due to improper use. The information in the
sheet was written based on the best knowledge and experience currently available.
Disclaimer
BEHR® PREMIUM Interior/Exterior Direct-to-Metal Semi-Gloss Paint - Deep Base SDS US
952106 Version #: 02 Revision date: 14-August-2020 Issue date: 05-December-2019 6 / 6
Page 1 of 10
COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SAFETY DATA SHEET This Safety Data Sheet conforms to ANSI Z400.5, and to the format requirements of the Global Harmonizing System. THIS SDS COMPLIES WITH 29 CFR 1910.1200 (HAZARD COMMUNICATION STANDARD) IMPORTANT: Read this SDS before handling & disposing of this product. Pass this information on to employees, customers, & users of this product. SECTION 1. IDENTIFICATION OF THE SUBSTANCE OR MIXTURE AND OF THE SUPPLIER PRODUCT IDENTITY: CROWN DENATURED ALCOHOL PRODUCT SYNONYMS: None PRODUCT USES: Alcohol Solvent COMPANY IDENTITY: Packaging Service Co., Inc. COMPANY ADDRESS: 1904 Mykawa Road COMPANY CITY: Pearland, TX 77581-3210 COMPANY PHONE: [phone] EMERGENCY PHONES: CHEMTREC: 1-800-424-9300 (USA) CANUTEC: 1-613-996-6666 (CANADA) SECTION 2. HAZARDS IDENTIFICATION DANGER!! 2.1 HAZARD STATEMENTS: (CAT = Hazard Category) (H200s) PHYSICAL: Flammable Liquids (CAT:2) H225 HIGHLY FLAMMABLE LIQUID AND VAPOR. (H300s) HEALTH: Acute Toxicity, Oral (CAT:3) H301 TOXIC IF SWALLOWED. (H300s) HEALTH: Acute Toxicity, Dermal (CAT:3) H311 TOXIC IN CONTACT WITH SKIN. (H300s) HEALTH: Skin Corrosion/Irritation (CAT:2) H315 CAUSES SKIN IRRITATION. (H300s) HEALTH: Serious Eye Damage/Eye Irritation (CAT:1) H318 CAUSES SERIOUS EYE DAMAGE. (H300s) HEALTH: Acute Toxicity, Inhalation (CAT:3) H331 TOXIC IF INHALED. (H300s) HEALTH: Target Organ Toxicity, Single Exposure; Respiratory Tract Effects (CAT:3) H335 MAY CAUSE RESPIRATORY IRRITATION. (H300s) HEALTH: Target Organ Toxicity, Single Exposure; Narcotic Effects (CAT:3) H336 MAY CAUSE DROWSINESS OR DIZZINESS. (H300s) HEALTH: Target Organ Toxicity, Single Exposure (CAT:1) H370 CAUSES DAMAGE TO ORGANS. (See Section 11 for Target Organ Information) 2.2 PRECAUTIONARY STATEMENTS: EXPOSURE PREVENTION: PREVENT DISPERSION OF MISTS OR DUST! AVOID EXPOSURE OF ADOLESCENTS, CHILDREN! P100s = General, P200s = Prevention, P300s = Response, P400s = Storage, P500s = Disposal P201 Obtain special instructions before use. P202 Do not handle until all safety precautions have been read and understood. P210 Keep away from heat, hot surfaces, sparks, open flames, and other ignition sources. No smoking. P233 Keep container tightly closed. P240 Ground/bond container and receiving equipment. P241 Use explosion-proof electrical/ventilating/lighting equipment. P242 Use only non-sparking tools. P243 Take precautionary measures against static discharge. P264 Wash with soap & water thoroughly after handling. P270 Do not eat, drink or smoke when using this product. P271 Use only outdoors or in a well-ventilated area. P280 Wear protective gloves/protective clothing/eye protection/face protection. P301+310 IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician. P302+350 IF ON SKIN: Gently wash with soap & water. P304+340 IF INHALED: Remove victim to fresh air & keep at rest in a position comfortable for breathing. P305+351+338 IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses if present & easy to do - Continue rinsing. P307+311 If exposed: Call a POISON CENTER or doctor/physician. P330 Rinse mouth. P332+313 If skin irritation occurs: Get medical advice/attention. P361 Remove/Take off immediately all contaminated clothing. P363 Wash contaminated clothing before reuse. P370+378 In case of fire: Use appropriate method to extinguish. P403+233 Store in a well-ventilated place. Keep container tightly closed. P405 Store locked up. P501 Dispose of contents/container according to: local/regional/national/international regulations. SEE SECTIONS 8, 11 & 12 FOR TOXICOLOGICAL INFORMATION.
Page 2 of 10
COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 3. COMPOSITION/INFORMATION ON INGREDIENTS MATERIAL CAS# EINECS# WT % Methanol 67-56-1 200-659-6 65-75 Ethanol 64-17-5 200-578-6 20-30 Isopropanol 67-63-0 200-661-7 0- 5 Methyl Isobutyl Ketone 108-10-1 203-550-1 0- 1 The specific chemical component identities and/or the exact component percentages of this material may be withheld as trade secrets. This information is made available to health professionals, employees, and designated representatives in accordance with the applicable provisions of 29 CFR 1910.1200 (I)(1). TRACE COMPONENTS: Trace ingredients (if any) are present in < 1% concentration, (< 0.1% for potential carcinogens, reproductive toxins, respiratory tract mutagens, and sensitizers). None of the trace ingredients contribute significant additional hazards at the concentrations that may be present in this product. All pertinent hazard information has been provided in this document, per the requirements of the Federal Occupational Safety and Health Administration Standard (29 CFR 1910.1200), U.S. State equivalents, and Canadian Hazardous Materials Identification System Standard (CPR 4). SECTION 4. FIRST AID MEASURES 4.1 MOST IMPORTANT SYMPTOMS/EFFECTS, ACUTE & CHRONIC: See Section 11 for symptoms/effects, acute & chronic. 4.2 GENERAL ADVICE: First Aid responders should pay attention to self-protection and use the recommended protective clothing (chemical resistant gloves, splash protection). If potential for exposure exists, refer to Section 8 for specific personal protective equipment. 4.3 EYE CONTACT: If this product enters the eyes, check for and remove any contact lenses. Open eyes while under gently running water. Use sufficient force to open eyelids. "Roll" eyes to expose more surface. Minimum flushing is for 15 minutes. Seek immediate medical attention. 4.4 SKIN CONTACT: If the product contaminates the skin, immediately begin decontamination with running water. Minimum flushing is for 15 minutes. Remove contaminated clothing, taking care not to contaminate eyes. If skin becomes irritated and irritation persists, medical attention may be necessary. Wash contaminated clothing before reuse, discard contaminated shoes. 4.5 INHALATION: After high vapor exposure, remove to fresh air. If breathing is difficult, give oxygen. If breathing has stopped, trained personnel should immediately begin artificial respiration. If the heart has stopped, trained personnel should immediately begin cardiopulmonary resuscitation (CPR). Seek immediate medical attention. 4.6 SWALLOWING: Do not induce vomiting. GET MEDICAL ATTENTION IMMEDIATELY. If person is fully conscious give 1 cup or 8 ounces of water. If medical advice is delayed and if an adult has swallowed several ounces of chemical, then give 3-4 ounces (1/3-1/2 cup) (90-120 ml) of hard liquor such as 80 proof whiskey. For children, give proportionally less liquor at a dose of 0.3 ounce (1 1/2 tsp) (8 ml) liquor for each 10 pounds of body weight, or 2 ml per kg body weight (for example: 1.2 ounce (2 1/3 tablespoon) for a 40 pound child or 36 ml for an 18 kg child). 4.7 RESCUERS: Victims of chemical exposure must be taken for medical attention. Rescuers should be taken for medical attention, if necessary. Take a copy of label and SDS to physician or health professional with victim. 4.8 INDICATION OF ANY IMMEDIATE MEDICAL ATTENTION AND SPECIAL TREATMENT NEEDED: NOTES TO PHYSICIAN: In cases where several ounces (60 - 100 ml) have been ingested, consider the use of ethanol and hemodialysis in the treatment. Consult standard literature for details of treatment. If ethanol is used, a therapeutically effective blood concentration in the range of 100 - 150 mg/dl may be achieved by a rapid loading dose followed by a continuous intravenous infusion. Consult standard literature for details of treatment.
Page 3 of 10
COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 4. FIRST AID MEASURES (CONTINUED) 4-Methyl pyrazole (Antizol TM) is an effective blocker of alcohol dehydrogenase and should be used in the treatment of ethylene glycol, di- or triethylene glycol, ethylene glycol butyl ether, or methanol intoxication if available. Fomepizol protocol (Brent, J. et al, New England Journal of Medicine, Feb 8, 2001, 344:6, p. 424-9): loading dose 15 mg/kg intravenously, follow by bolus dose of 10 mg/kg every 12 hours; after 48 hours, increase bolus dose to 15 mg/kg every 12 hours. Continue fomepizol until serum methanol, EG, DEG, or TEG are undetectable. The signs and symptoms of poisoning include anion gap metabolic acidosis, CNS depression, renal tubular injury, and possible late stage cranial nerve involvement. Respiratory symptoms, including pulmonary edema, may be delayed. Persons receiving significant exposure should be observed 24-48 hours for signs of respiratory distress. Maintain adequate ventilation and oxygenation of the patient. In severe poisoning, respiratory support with mechanical ventilation and positive end expiratory pressure may be required. Chemical eye burns may require extended irrigation. Obtain prompt consultation, preferably from an ophthalmologist. If lavage is performed, suggest endotracheal and/or esophageal control. Danger from lung aspiration must be weighted against toxicity when considering emptying the stomach. Treatment of exposure should be directed at the control of symptoms and the clinical condition of the patient. SECTION 5. FIRE FIGHTING MEASURES 5.1 FIRE & EXPLOSION PREVENTIVE MEASURES: NO open flames, NO sparks, & NO smoking. NO contact with oxidants. Above flash point, use a closed system, ventilation, explosion-proof electrical equipment, lighting. Do NOT use compressed air for filling, discharging, or handling. 5.2 SUITABLE (& UNSUITABLE) EXTINGUISHING MEDIA: Use dry powder, AFFF, alcohol-resistant foam, water in large amounts, carbon dioxide. 5.3 SPECIAL PROTECTIVE EQUIPMENT & PRECAUTIONS FOR FIRE FIGHTERS: Water spray may be ineffective on fire but can protect fire-fighters & cool closed containers. Use fog nozzles if water is used. Do not enter confined fire-space without full bunker gear. (Helmet with face shield, bunker coats, gloves & rubber boots). 5.4 SPECIFIC HAZARDS OF CHEMICAL & HAZARDOUS COMBUSTION PRODUCTS: FLAMMABLE!! VAPORS CAN CAUSE FLASH FIRE Isolate from oxidizers, heat, sparks, electric equipment & open flame. Closed containers may explode if exposed to extreme heat. Applying to hot surfaces requires special precautions. Empty container very hazardous! Continue all label precautions! SECTION 6. ACCIDENTAL RELEASE MEASURES 6.1 SPILL AND LEAK RESPONSE AND ENVIRONMENTAL PRECAUTIONS: Uncontrolled releases should be responded to by trained personnel using pre-planned procedures. No action shall be taken involving personal risk without suitable training. Keep unnecessary and unprotected personnel from entering spill area. Do not touch or walk through material. Avoid breathing vapor or mist. Provide adequate ventilation. Proper protective equipment should be used. In case of a spill, clear the affected area, protect people, and respond with trained personnel. ELIMINATE all ignition sources (no smoking, flares, sparks, or flames in immediate area). 6.2 PERSONAL PRECAUTIONS, PROTECTIVE EQUIPMENT, EMERGENCY PROCEDURES: The proper personal protective equipment for incidental releases (such as: 1 Liter of the product released in a well-ventilated area), use impermeable gloves, they should be Level B: triple-gloves (rubber gloves and nitrile gloves over latex gloves), chemical resistant suit and boots, hard-hat, and Self-Contained Breathing Apparatus specific for the material handled, goggles, face shield, and appropriate body protection. In the event of a large release, use impermeable gloves, specific for the material handled, chemically resistant suit and boots, and hard hat, and Self-Contained Breathing Apparatus or respirator. Personal protective equipment are required wherever engineering controls are not adequate or conditions for potential exposure exist. Select NIOSH/MSHA approved based on actual or potential airborne concentrations in accordance with latest OSHA and/or ANSI recommendations.
Page 4 of 10
COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 6. ACCIDENTAL RELEASE MEASURES (CONTINUED) 6.3 ENVIRONMENTAL PRECAUTIONS: Stop spill at source. Construct temporary dikes of dirt, sand, or any appropriate readily available material to prevent spreading of the material. Close or cap valves and/or block or plug hole in leaking container and transfer to another container. Keep from entering storm sewers and ditches which lead to waterways, and if necessary, call the local fire or police department for immediate emergency assistance. 6.4 METHODS AND MATERIAL FOR CONTAINMENT & CLEAN-UP: Absorb spilled liquid with poly pads or other suitable absorbent materials. If necessary, neutralize using suitable buffering material, (acid with soda ash or base with phosphoric acid), and test area with litmus paper to confirm neutralization. Clean up with non-combustible absorbent (such as: sand, soil, and so on). Shovel up and place all spill residue in suitable containers. Dispose of at an appropriate waste disposal facility according to current applicable laws and regulations and product characteristics at time of disposal (see Section 13 - Disposal Considerations). 6.5 NOTIFICATION PROCEDURES: In the event of a spill or accidental release, notify relevant authorities in accordance with all applicable regulations. US regulations require reporting release of this material to the environment which exceed the applicable reportable quantity or oil spills which could reach any waterway including intermittent dry creeks. The National Response Center can be reached at [phone]. SECTION 7. HANDLING AND STORAGE 7.1 PRECAUTIONS FOR SAFE HANDLING: Electrostatic charge may accumulate and create a hazardous condition when pumping and handling this material. Review all operations which have the potential of generating and accumulating an electrostatic charge and/or a flammable atmosphere (including tank and container filling, splash filling, tank cleaning, sampling, gauging, switch loading, filtering, mixing, agitation, and vacuum truck operations) and use appropriate mitigating procedures. For more information, refer to OSHA Standard 29 CR 1910.106, "Flammable and Combustible Liquids", National Fire Protection Association (NFPA 77, "Recommended Practice on Static Electricity", and/or the American Petroleum Institute (API) Recommended Practice 2003, "Protection Against Ignitions Arising Out of Static, Lightning, and Stray Currents". Ensure electrical continuity by bonding and grounding (earthing) all equipment. Restrict line velocity during pumping in order to avoid generation of electrostatic discharge (<= 1 m/sec until fill pipe submerged to twice its diameter. then <= 7 m/sec). Avoid splash filling. Do NOT use compressed air for filling, discharging or handling operations. Avoid free fall of liquid. Ground containers when transferring. Empty container very hazardous! Do not flame cut, saw, drill, braze, or weld. Continue all label precautions! 7.2 CONDITIONS FOR SAFE STORAGE, INCLUDING ANY INCOMPATIBILITIES: Keep in fireproof surroundings. Keep separated from strong oxidants, food & feedstuffs. Keep cool. Do not store above 49 C/120 F. Keep container tightly closed & upright when not in use to prevent leakage. 7.3 NONBULK: CONTAINERS: Store containers in a cool, dry location, away from direct sunlight, sources of intense heat, or where freezing is possible. Material should be stored in secondary containers or in a diked area, as appropriate. Store containers away from incompatible chemicals (see Section 10, Stability and Reactivity). Post warning and "NO SMOKING" signs in storage and use areas, as appropriate. Empty containers should be handled with care. Never store food, feed, or drinking water in containers which held this product. 7.4 BULK CONTAINERS: All tanks and pipelines which contain this material must be labeled. Perform routine maintenance on tanks or pipelines which contain this product. Report all leaks immediately to the proper personnel. 7.5 TANK CAR SHIPMENTS: Tank cars carrying this product should be loaded and unloaded in strict accordance with tank-car manufacturer's recommendation and all established on-site safety procedures. Appropriate personal protective equipment must be used (see Section 8, Engineering Controls and Personal Protective Equipment.). All loading and unloading equipment must be inspected, prior to each use. Loading and unloading operations must be attended, at all times. Tank cars must be level, brakes must be set or wheels must be locked or blocked prior to loading or unloading. Tank car (for loading) or storage tanks (for unloading) must be verified to be correct for receiving this product and be properly prepared, prior to starting the transfer operations. Hoses must be verified to be in the correct positions, before starting transfer operations. A sample (if required) must be taken and verified (if required) prior to starting transfer operations. All lines must be blown-down and purged before disconnecting them from the tank car or vessel.
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COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 7. HANDLING AND STORAGE (CONTINUED) 7.6 PROTECTIVE PRACTICES DURING MAINTENANCE OF CONTAMINATED EQUIPMENT: Follow practices indicated in Section 6 (Accidental Release Measures). Make certain application equipment is locked and tagged-out safely. Always use this product in areas where adequate ventilation is provided. Collect all rinsates and dispose of according to applicable Federal, State, Provincial, or local procedures. 7.7 EMPTY CONTAINER WARNING: Empty containers may contain residue and can be dangerous. Do not attempt to refill or clean containers without proper instructions. Empty drums should be completely drained and safely stored until appropriately reconditioned or disposed. Empty containers should be taken for recycling, recovery, or disposal through suitably qualified or licensed contractor and in accordance with governmental regulations. DO NOT PRESSURIZE, CUT, WELD, BRAZE, SOLDER, DRILL, GRIND, OR EXPOSE SUCH CONTAINERS TO HEAT, FLAME, SPARKS, STATIC ELECTRICITY, OR OTHER SOURCES OF IGNITION. THEY MAY BURST AND CAUSE INJURY OR DEATH. SECTION 8. EXPOSURE CONTROLS/PERSONAL PROTECTION 8.1 EXPOSURE LIMITS: MATERIAL CAS# EINECS# TWA (OSHA) TLV (ACGIH) Methanol 67-56-1 200-659-6 200 ppm S 200 ppm S Ethanol 64-17-5 200-578-6 1000 ppm 1000 ppm A4 Isopropanol 67-63-0 200-661-7 400 ppm 200 ppm A4 Methyl Isobutyl Ketone 108-10-1 203-550-1 100 ppm 20 ppm A3 MATERIAL CAS# EINECS# CEILING STEL(OSHA/ACGIH) HAP Methanol 67-56-1 200-659-6 None Known 250 ppm Yes Isopropanol 67-63-0 200-661-7 None Known 400 ppm No Methyl Isobutyl Ketone 108-10-1 203-550-1 None Known 75 ppm Yes Each component showing `Yes' under "HAP" is an EPA Hazardous Air Pollutant. 8.2 APPROPRIATE ENGINEERING CONTROLS: RESPIRATORY EXPOSURE CONTROLS Airborne concentrations should be kept to lowest levels possible. If vapor, dust or mist is generated and the occupational exposure limit of the product, or any component of the product, is exceeded, use appropriate NIOSH or MSHA approved air purifying or air-supplied respirator authorized in 29 CFR 1910.134, European Standard EN 149, or applicable State regulations, after determining the airborne concentration of the contaminant. Air supplied respirators should always be worn when airborne concentration of the contaminant or oxygen content is unknown. Maintain airborne contaminant concentrations below exposure limits. If adequate ventilation is not available or there is potential for airborne exposure above the exposure limits, a respirator may be worn up to the respirator exposure limitations, check with respirator equipment manufacturer's recommendations/limitations. For particulates, a particulate respirator (NIOSH Type N95 or better filters) may be worn. If oil particles (such as: lubricants, cutting fluids, glycerine, and so on) are present, use a NIOSH Type R or P filter. For a higher level of protection, use positive pressure supplied air respiration protection or Self-Contained Breathing Apparatus or if oxygen levels are below 19.5% or are unknown. EMERGENCY OR PLANNED ENTRY INTO UNKNOWN CONCENTRATIONS OR IDLH CONDITIONS Positive pressure, full-face piece Self-Contained Breathing Apparatus; or positive pressure, full-face piece Self-Contained Breathing Apparatus with an auxiliary positive pressure Self-Contained Breathing Apparatus. VENTILATION LOCAL EXHAUST: Necessary MECHANICAL (GENERAL): Necessary SPECIAL: None OTHER: None Please refer to ACGIH document, "Industrial Ventilation, A Manual of Recommended Practices", most recent edition, for details. 8.3 INDIVIDUAL PROTECTION MEASURES, SUCH AS PERSONAL PROTECTIVE EQUIPMENT: EYE PROTECTION: Safety eyewear complying with an approved standard should be used when a risk assessment indicates this is necessary to avoid exposure to liquid splashes, mists or dusts. If contact is possible, chemical splash goggles should be worn, when a higher degree of protection is necessary, use splash goggles or safety glasses. Face-shields are recommended when the operation can generate splashes, sprays or mists.
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COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 8. EXPOSURE CONTROLS/PERSONAL PROTECTION (CONTINUED) HAND PROTECTION: Use gloves chemically resistant to this material. Glove must be inspected prior to use. Preferred examples: Butyl rubber, Chlorinated Polyethylene, Polyethylene, Ethyl vinyl alcohol laminate ("EVAL"), Polyvinyl alcohol ("PVA"). Examples of acceptable glove barrier materials include: Natural rubber ("latex"), Neoprene, Nitrile/butadiene rubber ("nitrile") or ("NBR"), Polyvinyl chloride ("PVC") or "vinyl"), Viton. Chemical-resistant, impervious gloves complying with an approved standard should be worn at all times when handling chemical products if a risk assessment indicates this is necessary. Considering the parameters specified by the glove manufacturer, check during use that the gloves are still retaining their protective properties. It should be noted that the time to breakthrough for any glove material may be different for different glove manufacturers. In the case of mixtures, consisting of several substances, the protection time of the gloves cannot be accurately estimated. Use proper glove removal technique (without touching glove's outer surface) to avoid skin contact with this product. Dispose of contaminated gloves after use in accordance with applicable laws and good practices. Wash and dry hands. BODY PROTECTION: Use body protection appropriate for task. Cover-all, rubber aprons, or chemical protective clothing made from impervious materials are generally acceptable, depending on the task. WORK & HYGIENIC PRACTICES: Wash hands, forearms and face thoroughly after handling chemical products, before eating, smoking and using toilet facilities and at the end of the working period. Provide readily accessible eye wash stations & safety showers. Remove clothing that becomes contaminated. Destroy contaminated leather articles. Launder or discard contaminated clothing. SECTION 9. PHYSICAL & CHEMICAL PROPERTIES APPEARANCE: Liquid, Water-White ODOR: Ketone ODOR THRESHOLD: Not Available pH (Neutrality): Not Available MELTING POINT/FREEZING POINT: Not Available BOILING RANGE (IBP,50%,Dry Point): 63 66 83 C / 147 152 182 F FLASH POINT (TEST METHOD): 8 C / 48 F (TCC) EVAPORATION RATE (n-Butyl Acetate=1): 1.7 FLAMMABILITY CLASSIFICATION: Class I B LOWER FLAMMABLE LIMIT IN AIR (% by vol): 6.4 UPPER FLAMMABLE LIMIT IN AIR (% by vol): Not Available VAPOR PRESSURE (mm of Hg)@20 C 86.1 VAPOR DENSITY (air=1): 1.2 GRAVITY @ 68/68 F / 20/20 C: DENSITY: 0.791 SPECIFIC GRAVITY (Water=1): 0.792 POUNDS/GALLON: 6.597 WATER SOLUBILITY: Complete PARTITION COEFFICIENT (n-Octane/Water): Not Available AUTO IGNITION TEMPERATURE: 398 C / 750 F DECOMPOSITION TEMPERATURE: Not Available TOTAL VOC'S (TVOC)*: 100.0 Vol% / 792.0 g/L / 6.5 Lbs/Gal NONEXEMPT VOC'S (CVOC)*: 100.0 Vol% / 792.0 g/L / 6.5 Lbs/Gal HAZARDOUS AIR POLLUTANTS (HAPS): 73.0 Wt% / 578.2 g/L / 4.8 Lbs/Gal NONEXEMPT VOC PARTIAL PRESSURE (mm of Hg @ 20 C) 0.0 VISCOSITY @ 20 C (ASTM D445): Not Available * Using CARB (California Air Resources Board Rules).
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COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 10. STABILITY & REACTIVITY 10.1 REACTIVITY & CHEMICAL STABILITY: Stable under normal conditions, no hazardous reactions when kept from incompatibles. 10.2 POSSIBILITY OF HAZARDOUS REACTIONS & CONDITIONS TO AVOID: Isolate from oxidizers, heat, sparks, electric equipment & open flame. 10.3 INCOMPATIBLE MATERIALS: The substance can presumably form explosive peroxides, under the influence of light and air. Check for peroxide prior to distillation, eliminate if found. Reacts violently with strong oxidants, strong reducing agents, causing fire & explosion hazard. 10.4 HAZARDOUS DECOMPOSITION PRODUCTS: Carbon Monoxide, Carbon Dioxide from burning. 10.5 HAZARDOUS POLYMERIZATION: Will not occur. SECTION 11. TOXICOLOGICAL INFORMATION 11.1 ACUTE HAZARDS 11.1.1 SKIN CONTACT: Primary irritation to skin, defatting, dermatitis. 11.1.2 EYE CONTACT: Primary irritation to eyes, redness, tearing, blurred vision. Liquid can cause eye irritation. 11.1.3 INHALATION: Anesthetic. Irritates respiratory tract. Acute overexposure can cause serious nervous system depression. Vapor harmful. Breathing vapor can cause irritation. Acute overexposure can cause harm to affected organs by routes of entry. Repeated exposure over TLV can cause blindness. 11.1.4 SWALLOWING: Can be fatal or cause blindness if swallowed. Cannot be made non-poisonous. POISON ! Can cause irreversible nervous system damage & death. Harmful or fatal if swallowed. Swallowing can cause abdominal irritation, nausea, vomiting & diarrhea. 11.2 SUBCHRONIC HAZARDS/CONDITIONS AGGRAVATED MEDICAL CONDITIONS AGGRAVATED BY EXPOSURE: Pre-existing disorders of any target organs mentioned in this Document can be aggravated by over-exposure by routes of entry to components of this product. Persons with these disorders should avoid use of this product. 11.3 CHRONIC HAZARDS 11.3.1 CANCER, REPRODUCTIVE & OTHER CHRONIC HAZARDS: Potential Cancer Hazard based on tests with laboratory animals using Methyl Isobutyl Ketone. Overexposure may create cancer risk. Absorption thru skin may be harmful. Studies with laboratory animals indicate this product can cause damage to fetus. Depending on degree of exposure, periodic medical examination is indicated. 11.3.2 TARGET ORGANS: May cause damage to target organs, based on animal data. 11.3.3 IRRITANCY: Irritating to contaminated tissue. 11.3.4 SENSITIZATION: No component is known as a sensitizer. 11.3.5 MUTAGENICITY: No known reports of mutagenic effects in humans. 11.3.6 EMBRYOTOXICITY: No known reports of embryotoxic effects in humans. 11.3.7 TERATOGENICITY: No known reports of teratogenic effects in humans. 11.3.8 REPRODUCTIVE TOXICITY: No known reports of reproductive effects in humans.
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COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 11. TOXICOLOGICAL INFORMATION (CONTINUED) A MUTAGEN is a chemical which causes permanent changes to genetic material (DNA) such that the changes will propagate across generational lines. An EMBRYOTOXIN is a chemical which causes damage to a developing embryo (such as: within the first 8 weeks of pregnancy in humans), but the damage does not propagate across generational lines. A TERATOGEN is a chemical which causes damage to a developing fetus, but the damage does not propagate across generational lines. A REPRODUCTIVE TOXIN is any substance which interferes in any way with the reproductive process. 11.4 MAMMALIAN TOXICITY INFORMATION MATERIAL CAS# EINECS# LOWEST KNOWN LETHAL DOSE DATA LOWEST KNOWN LD50 (ORAL) Methanol 67-56-1 200-659-6 1000.0 mg/kg(Man) LOWEST KNOWN LC50 (VAPORS) Isopropanol 67-63-0 200-661-7 1600 ppm (Rats) LOWEST KNOWN LD50 (SKIN) Isopropanol 67-63-0 200-661-7 16400.0 mg/kg (Rabbits) SECTION 12. ECOLOGICAL INFORMATION 12.1 ALL WORK PRACTICES MUST BE AIMED AT ELIMINATING ENVIRONMENTAL CONTAMINATION. 12.2 EFFECT OF MATERIAL ON PLANTS AND ANIMALS: This product may be harmful or fatal to plant and animal life if released into the environment. Refer to Section 11 (Toxicological Information) for further data on the effects of this product's components on test animals. 12.3 EFFECT OF MATERIAL ON AQUATIC LIFE: The most sensitive known aquatic group to any component of this product is: Chub 250 ppm or mg/L (24 hour exposure). Keep out of sewers and natural water supplies. 12.4 MOBILITY IN SOIL This material is a mobile liquid. 12.5 DEGRADABILITY This product is completely biodegradable. 12.6 ACCUMULATION This product does not accumulate or biomagnify in the environment. SECTION 13. DISPOSAL CONSIDERATIONS THE GENERATION OF WASTE SHOULD BE AVOIDED OR MINIMIZED WHEREVER POSSIBLE. Dispose of surplus and non-recyclable products via a licensed waste disposal contractor. Waste should not be disposed of untreated to the sewer unless fully compliant with the requirements of all authorities with jurisdiction. Waste packaging should be recycled. Incineration or landfill should only be considered when recycling is not feasible. This material and its container must be disposed of in a safe way. Care should be taken when handling emptied containers that have not been cleaned or rinsed out. Empty containers and liners may retain some product residues. Vapor from some product residues may create a highly flammable or explosive atmosphere inside the container. DO NOT PRESSURIZE, CUT, WELD, BRAZE, SOLDER, DRILL, GRIND, OR EXPOSE USED CONTAINERS TO HEAT, FLAME, SPARKS, STATIC ELECTRICITY, OR OTHER SOURCES OF IGNITION. THEY MAY BURST AND CAUSE INJURY OR DEATH. Avoid dispersal of spilled material and runoff and contact with soil, waterways, drains and sewers. Processing, use or contamination may change the waste disposal requirements. Do not dispose of on land, in surface waters, or in storm drains. Waste should be recycled or disposed of in accordance with regulations. Large amounts should be collected for reuse or consigned to licensed hazardous waste haulers for disposal. ALL DISPOSAL MUST BE IN ACCORDANCE WITH ALL FEDERAL, STATE, PROVINCIAL, AND LOCAL REGULATIONS. IF IN DOUBT, CONTACT PROPER AGENCIES. EPA CHARACTERISTIC: D001
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COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 14. TRANSPORT INFORMATION IF > 6868 LB / 3121 KG OF THIS PRODUCT IS IN 1 CONTAINER, IT EXCEEDS THE RQ OF METHANOL. "RQ" MUST BE PUT BEFORE THE DOT SHIPPING NAME. DOT/TDG SHIP NAME: NA1987, Alcohols, n.o.s., (Contains: Ethanol, Methanol, Methyl Isobutyl Ketone), 3, PG-II DRUM LABEL: (FLAMMABLE LIQUID) IATA / ICAO: Alcohols, Toxic, n.o.s. (Contains: Ethanol, Methanol, Methyl Isobutyl Ketone), 3, (6.1), PG-II IMO / IMDG: UN1986, Alcohols, Toxic, n.o.s. (Contains: Ethanol, Methanol, Methyl Isobutyl Ketone), 3, (6.1), PG-II EMERGENCY RESPONSE GUIDEBOOK NUMBER: 131 SECTION 15. REGULATORY INFORMATION 15.1 EPA REGULATION: SARA SECTION 311/312 HAZARDS: Acute Health, Chronic Health, Fire All components of this product are on the TSCA list. SARA Title III Section 313 Supplier Notification This product contains the indicated <*> toxic chemicals subject to the reporting requirements of Section 313 of the Emergency Planning & Community Right-To-Know Act of 1986 & of 40 CFR 372. This information must be included in all MSDSs that are copied and distributed for this material. SARA TITLE III INGREDIENTS CAS# EINECS# WT% (REG.SECTION) RQ(LBS) *Methanol 67-56-1 200-659-6 65-75 (311,312,313,RCRA) 5000 *Methyl Isobutyl Ketone 108-10-1 203-550-1 0- 1 (311,312,313,RCRA) 5000 Any release equal to or exceeding the RQ must be reported to the National Response Center (800-424-8802) and appropriate state and local regulatory agencies as described in 40 CFR 302.6 and 40 CFR 355.40 respectively. Failure to report may result in substantial civil and criminal penalties. State & local regulations may be more restrictive than federal regulations. 15.2 STATE REGULATIONS: THIS PRODUCT MEETS REQUIREMENTS OF SOUTHERN CALIFORNIA AQMD RULE 443.1 & SIMILAR REGULATIONS CALIFORNIA SAFE DRINKING WATER & TOXIC ENFORCEMENT ACT (PROPOSITION 65): This product contains the following chemical known to the State of California to cause cancer: Methyl Isobutyl Ketone This product contains the following chemical known to the State of California to cause reproductive toxicity: Methanol 15.3 INTERNATIONAL REGULATIONS The identified components of this product are listed on the chemical inventories of the following countries: Australia (AICS), Canada (DSL or NDSL), China (IECSC), Europe (EINECS, ELINCS), Japan (METI/CSCL, MHLW/ISHL), South Korea (KECI), New Zealand (NZIoC), Philippines (PICCS), Switzerland (SWISS), Taiwan (NECSI), USA (TSCA). 15.4 CANADA: WORKPLACE HAZARDOUS MATERIALS INFORMATION SYSTEM (WHMIS) B2: Flammable Liquid. D2B: Irritating to skin / eyes. This product was classified using the hazard criteria of the Controlled Products Regulations (CPR). This Document contains all information required by the CPR.
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COMPANY IDENTITY: Packaging Service Co., Inc. SDS DATE: 03/25/2016 PRODUCT IDENTITY: CROWN DENATURED ALCOHOL REPLACES: 02/14/2013 SDS NUMBER: CR.DA SECTION 16. OTHER INFORMATION 16.1 HAZARD RATINGS: HEALTH (NFPA): 1, HEALTH (HMIS): 2, FLAMMABILITY: 3, PHYSICAL HAZARD: 0 (Personal Protection Rating to be supplied by user based on use conditions.) This information is intended solely for the use of individuals trained in the NFPA & HMIS hazard rating systems. 16.2 EMPLOYEE TRAINING See Section 2 (Hazards Identification). Employees should be made aware of all hazards of this material (as stated in this SDS) before handling it. 16.3 SDS DATE: 03/25/2016 NOTICE The supplier disclaims all expressed or implied warranties of merchantability or fitness for a specific use, with respect to the product or the information provided herein, except for conformation to contracted specifications. All information appearing herein is based upon data obtained from manufacturers and/or recognized technical sources. While the information is believed to be accurate, we make no representations as to its accuracy or sufficiency. Conditions of use are beyond our control, and therefore users are responsible for verifying the data under their own operating conditions to determine whether the product is suitable for their particular purposes and they assume all risks of their handling, and disposal of the product. Users also assume all risks in regards to the publication or use of, or reliance upon information contained herein. This information relates only to the product designated herein, and does not relate to its use in combination with any other material or process. Unless updated, the Safety Data Sheet is valid until 03/25/2019.