21015_five Points_Import-Export Rpt; 5.12.23 submittal

May 12, 2023

Ms. Carolyn Minnich
Brownfields Redevelopment Section
North Carolina Department of Environmental Quality
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115

Re: Borrow Source and Export Soil Sampling Report
Five Points Gateway
320 & 322 East Franklin Street
Monroe, North Carolina
Brownfields Project Number #21015-17-090

To Whom It May Concern:

On behalf of the City of Monroe, Resolve Environmental PLLC presents the attached Borrow Source and Export Soil
Sampling Report for the Five Points Gateway site located in Monroe, Union County, North Carolina for your review
and approval. Please do not hesitate to call with any further questions and/or comments during your review.

Sincerely,
Resolve Environmental Services, PLLC

Terry D. Kennedy, P.G.

Enclosure

cc: Chad Splawn/City of Monroe
Amanda Short/Parker Poe

May 12, 2023

Ms. Carolyn Minnich, Project Manager
Brownfields Section – Division of Waste Management
North Carolina Department of Environmental Quality
610 East Center Avenue, Suite 301
Mooresville, NC 28115

Re: Borrow Source and Export Soil Sampling Report
Five Points Gateway
320 & 322 East Franklin Street
Monroe, North Carolina
Brownfields Project Number #21015-17-090

Dear Ms. Minnich:

On behalf of the City of Monroe (COM), Resolve Environmental PLLC (Resolve) presents the results of the required
soil sampling at a potential borrow source (Martin Marietta-Bakers Quarry/Permit 90-02) located at 2111 N. Rocky
River Road in Monroe, Union County, North Carolina (Figure 1). In addition, Resolve concurrently conducted the
required pre-export soil sampling at the subject Brownfields site, “Five Points Gateway” located at 320-322 East
Franklin Street in Monroe Union County, North Carolina (Figure 2). The soil requiring export was deemed unsuitable
for building construction by the General Contractor (GC). The import and export sampling was conducted in
accordance with the approved Environmental Management Plan (EMP) dated June 17, 2021 and associated Import-
Export Soil Sampling Plan #1 – Revision #2 dated April 21, 2023 and subsequently approved by the North Carolina
Department of Environmental Quality’s (NCDEQ) Brownfields Program Manager on April 21, 2023 for the proposed
development of the Brownfields property.

BORROW SOURCE (IMPORT) SAMPLING
Resolve mobilized to the potential borrow source site on April 26, 2023. Per the approved Import-Export Soil
Sampling Plan #1 – Revision #2, a total of five (5) soil borings (SS-1-3’, SS-2-3’, SS-3-3’, SS-4-3’ and SS-5-3’) were
installed in the area of overburden located in the proposed borrow source, as specified by the quarry operator. The
borrow source was free of vegetation and consisted of brown silt. A soil sample was collected from 3 feet below

grade level in each of the five (5) soil borings. Each collected soil sample was screened with a photoionization
detector (PID) subsequent to collection. Field-screening results are provided in Table 1. Detectable concentrations
of volatile organic compounds (VOCs) ranging from 0.1 to 0.4 parts per million (PPM) were detected by the PID in
soil samples SS-2, SS-3 and SS-5. Soil sample (Sample ID: SS-5-3’) that exhibited the highest organic vapor reading
(0.4 ppm) was submitted to a North Carolina certified laboratory for analysis of volatile organic compounds using
SW-846 Method 8260D. In addition, the five (5) primary samples were composited (Sample ID: SS Comp) in the
field and submitted to the laboratory for analysis of semi-volatile organic compounds (SVOCs) using SW-846 Method
8270E and for RCRA metals by EPA Method 6020D/7471A. In addition, one aliquot from each collected soil sample
was submitted for laboratory hold and possible analyses of hexavalent chromium by EPA Method 7199 and/or TCLP
depending on results from the RCRA Metals analysis.

Soil samples were collected using a decontaminated hand auger. Each boring was backfilled with cuttings. Field
personnel collected each soil sample using a new pair of nitrile gloves. The samples were placed directly into
laboratory-supplied sample containers, immediately placed on ice in a sample cooler and transported to the
laboratory in the manner described above. Proper chain of custody procedures was maintained at all times. To
evaluate laboratory quality control and repeatability, one duplicate soil sample (Sample ID: SS Comp Dup) was
collected from the composite sample and analyzed for VOCs, SVOCs and RCRA metals. One (1) trip blank sample
accompanied the samples during the sampling event.

A concentration of arsenic in soil samples SS Comp exceeded the NCDEQ’s Residential and Industrial/Commercial
Preliminary Soil Remediation Goals (PSRG) but is considered to be a background level. Detectable and/or estimated
concentrations of barium, chromium, lead, selenium and silver were reported in soil sample SS Comp; however,
none of the concentrations exceeded the residential PSRGs (if established). Please note that an estimated
concentration of acetone was reported in the soil sample SS-5; however, the concentration did not exceed the
residential PSRG. No other detectable concentrations of Method 8260D compounds were reported in soil sample
SS-5. No detectable concentrations of SVOCs were reported in the soil samples. A Soil Sample Location Map
(Import) is provided as Figure 3. The soil sample analytical results have been summarized in Table 2 and Table 3.
Please note that estimated and/or detectable concentrations of VOCs reported in the trip blank are likely laboratory
contaminants, based on the case narrative within the laboratory report.

EXPORT SOIL SAMPLING

Resolve personnel mobilized to the site on April 26, 2023. Per the approved Import-Export Soil Sampling Plan #1 –
Revision #2 (dated and NCDEQ-approved on April 21, 2023), export soils were stockpiled on-site. Upon arrival at
the site, three (3) stockpiles were staged on the subject property. Five (5) primary samples were collected from

each of the stockpiles (SP-1-1 through SP-1-5 from Stockpile 1, SP-2-1 through SP-2-5 from Stockpile 2 and SP-3-1
through SP-3-5 from Stockpile 3). The samples were collected from depths ranging from 2 to 4 feet below grade
surface (BGS). The sampling areas were free of vegetation and generally consisted of brown silt with rock. Each
collected soil sample was screened with a PID subsequent to collection. Field-screening results are provided in
Table 4. The sample form each section with the highest PID result from each stockpile was submitted for laboratory
analyses for volatile organic compounds (VOCs). SP-1-3, SP-2-5 and SP-3-3, collected from soil stockpiles 1, 2 and
3, respectively, were submitted to a North Carolina certified laboratory for analysis by SW-846 Method 8260D. In
addition, the 5 primary samples from each Stockpile were composited (SP-1 Comp, SP-2 Comp and SP-3 Comp) in
the field and submitted to the laboratory for analysis of SVOCs using SW-846 Method 8270E and for RCRA metals
by EPA Method 6020D/7471A. In addition, separate aliquots from each collected soil sample were submitted for
laboratory hold and possible analyses of hexavalent chromium by EPA Method 7199 and/or TCLP depending on
results from the RCRA Metals analysis.

Soil samples were collected using a decontaminated hand auger. Each boring was backfilled with cuttings. Field
personnel collected each soil sample using a new pair of nitrile gloves. The samples were placed directly into
laboratory-supplied sample containers, immediately placed on ice in a sample cooler and transported to the
laboratory. Proper chain of custody procedures were maintained at all times. To evaluate laboratory quality control
and repeatability, one duplicate soil sample (SP-2 Comp Dup) was collected from SP-2 Comp and analyzed for VOCs,
SVOCs and RCRA metals. One (1) trip blank sample accompanied the samples during the sampling event.

Concentrations of arsenic in soil samples SP-1 Comp, SP-2 Comp and SP-3 Comp exceeded the NCDEQ’s Residential
and Commercial/Industrial Preliminary Soil Remediation Goals (PSRGs) but were considered to be background levels
which is consistent with historical soil sampling data. Detectable and/or estimated concentrations of barium,
cadmium, chromium, lead, selenium, silver and mercury were reported in each of the samples (SP-1 Comp, SP-2
Comp and SP-3 Comp); however, none of the concentrations exceeded the residential PSRGs (if established).
Detectable and/or estimated concentrations of acetone, benzene, toluene and n-Hexane were reported in the
samples SP-1-3’, SP-2-5’ and SP-3-3’. However, none of the reported concentrations exceeded the Residential
PSRGs. No detectable concentrations of SVOCs were reported in the soil samples. Please note that estimated
and/or detectable concentrations of VOCs reported in the trip blank are likely laboratory contaminants, based on
the case narrative within the laboratory report.

A Soil Sample Location Map (Export) is included as Figure 4. The soil sample analytical results have been
summarized in Tables 5 and 6. Subsurface boring logs are included as Appendix A. Copies of the laboratory
analytical reports have been attached as Appendix B.

Based on these data, it appears that the Martin Marietta-Bakers Quarry is a viable borrow source for the
development of the City of Monroe’s municipal project. In addition, the soil export options include transport of the
soils to (1) any Brownfields property, (2) a LCID/CD landfill, or (3) any available Subtitle D municipal waste
landfill/permitted landfarm, upon approval from the NCDEQ.

Please do not hesitate to call with any further questions and/or comments during your review.

Sincerely,
Resolve Environmental Services, PLLC

Terry D. Kennedy, P.G.

enclosures

cc: Chad Splawn, City of Monroe
Amanda Short, Parker Poe

FIGURES

Copyright:© 2013 National Geographic Society, i-cubed
FIGURE 1SITE LOCATION MAP320 E. FRANKLIN STREETMONROE, UNION COUNTY,NORTH CAROLINA
PREPARED BY:RESOLVE ENVIRONMETAL SERVICES, PPLC.OCTOBER 25, 2016
0 2,000 4,0001,000 Feet
SCALE: 1 INCH = 2,000 FEET
MAP CENTER LOCATIONLATITUDE: 34.982443° NLONGITUDE: 80.547068° W
`
SITE LOCATION
³
Five Points Gateway
21015-17-090
Soil Stockpile Location
100 ft
N➤➤N

TABLES

Date: 5/5/23
Sample ID
Primary Samples for
Composing Composite
Samples - 8270 & RCRA
Metals Analyses
Date Collected
(mm/dd/yy)
Sample Depth
(feet)
OVA Reading
(ppm)
SS-1-3'3 0.0
SS-2-3'3 0.1
SS-3-3'3 0.2
SS-4-3'3 0.0
SS-5-3'*3 0.4
Note:
• Results reported in ppm (parts per million).
• OVA-Photoionization detector. Calibrated to isobutlyene standard.
• * indicates sample submitted for 8260D analysis.
TABLE 1
SUMMARY OF OVA READINGS
MARTIN-MARIETTA BAKERS QUARRY
PROJECT ID: 21015-17-090
SS-Comp 04/26/23
FIVE POINTS GATEWAY
IMPORT SOIL
Date: 05/05/23
Sample ID Date Collected
(mm/dd/yy)
Sample Interval
(feet)
SS Comp 4/26/23 2.5-3 5.58 22.0 25.8 14.1 1.40 0.0081 J
SS Comp Dup 4/26/23 ---4.67 15.6 24.6 10.5 1.53 <0.0077
0.68 3,100 NE 400 78 78
3.0 47,000 NE 800 1,200 1,200
Notes:
• Results reported in mg/kg (milligrams per kilograms).
• PSRG: NCDEQ Preliminary Soil Remediation Goal (July 2022).
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type and italics exceed the Industrial/Commercial PSRG.
• NE: Not Established.
• J: Estimated concentration.
PROJECT ID: 21015-17-090
TABLE 2
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS - RCRA METALS
FIVE POINTS GATEWAY
MARTIN-MARIETTA BAKERS QUARRY
IMPORT SOIL
Residential PSRGs (mg/kg)
Industrial/Commercial PSRGs (mg/kg)
Analytical Method EPA Method
6020D/7471A
Contaminant of Concern ArsenicLeadSilverBariumSeleniumChromium
Date: 05/08/23
EPA Method
8260D
Sample ID Date Collected (mm/dd/yy)Sample Depth
(feet)
14,000
210,000
SS-5 4/26/23 2.5-3 0.005 J
SS-5 Duplicate 4/26/23 2.5-3 0.011 J
Trip Blank ------5.09
Notes:
• Results reported in mg/kg (milligrams per kilograms).
• PSRG: NCDEQ Preliminary Soil Remediation Goal.
• < : Less than the method detection limit specified in the laboratory report.
• NE: Not Established.
• J: Estimated value.
• Trip blank results reported in ug/L.
• Concentrations of MEK (1.27 J ug/L) and methylene chloride (0.520 J ug/L) were reported in the trip blank.
As noted in laboratory report, acetone, MEK and methylene chloride concentrations detected in trip blank
are likely due to laboratory contamination.
TABLE 3
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS - VOCs
MARTIN MARIETTA - BAKERS QUARRY
PROJECT ID: 21015-17-090
Analytical Method
Industrial/Commercial PSRGs (mg/kg)
IMPORT SOIL
FIVE POINTS GATEWAY
Contaminant of Concern AcetoneResidential PSRGs (mg/kg)
Date: 5/5/23
Sample ID
Primary Samples for
Composing Composite
Samples - 8270 & RCRA
Metals Analyses
Date Collected
(mm/dd/yy)
Sample Depth
(feet)
OVA Reading
(ppm)
SP-1-1 3 0.6
SP-1-2 4 0.5
SP-1-3 3 1.1*
SP-1-4 2 0.5
SP-1-5 4 0.3
SP-2-1 4 0.9
SP-2-2 3 1.3
SP-2-3 3 0.9
SP-2-4 4 0.9
SP-2-5 2 5.9*
SP-3-1 2 0.7
SP-3-2 3 0.7
SP-3-3 4 1.0*
SP-3-4 3 0.4
SP-3-5 4 0.3
Note:
• Results reported in ppm (parts per million).
• OVA-Photoionization detector. Calibrated to isobutlyene standard.
• * indicates sample submitted for 8260B analysis.
SP-3 04/26/23
SP-2 04/26/23
TABLE 4
SUMMARY OF OVA READINGS - EXPORT SOIL SAMPLES
FIVE POINTS GATEWAY
PROJECT ID: 21015-17-090
SP-1 04/26/23
Date: 05/05/23
Sample ID Date Collected
(mm/dd/yy)
Sample Interval
(feet)
SP-1 COMP 4/26/23 ---14.3 34.3 0.292 39.0 42.6 0.796 0.0311 J 0.0764 J
SP-2 COMP 4/26/23 ---10.6 31.9 0.0921 J 43.8 35.2 0.632 0.0331 J 0.0872 J
SP-2 COMP DUP 4/26/23 ---13.2 56.5 0.208 J 61.0 100 1.23 0.0756 J 0.102 J
SP-3 COMP 4/26/23 ---12.4 50.2 1.77 39.3 114 1.10 0.0812 J 0.118 J
0.68 3,100 NE NE NE 78 78 2.3
3.0 47,000 NE NE NE 1,200 1,200 9.7
Notes:
• Results reported in mg/kg (milligrams per kilograms).
• PSRG: NCDEQ Preliminary Soil Remediation Goal.
• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in bold face type exceed the Residential PSRG.
• Concentrations in bold face type and italics exceed the Industrial/Commercial PSRG.
• NE: Not Established.
• J: Estimated value.
Industrial/Commercial PSRGs (mg/kg)
Analytical Method EPA Method
6020D/7471A
Contaminant of Concern ArsenicChromiumMercuryBariumLeadResidential PSRGs (mg/kg)CadmiumSeleniumSilverPROJECT ID: 21015-17-090
TABLE 5
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS - RCRA METALS
FIVE POINTS GATEWAY
Date: 05/08/23
Sample ID Date Collected
(mm/dd/yy)
Sample Depth
(feet)
14,000 1.2 990 130
210,000 5.4 9,700 540
SP-1-3 (3')4/26/23 2.5-3 0.025 <0.0007 <0.0008 <0.0008
SP-2-5 (2')4/26/23 1.5-2 0.011 J 0.002 J 0.0009 J <0.0008
SP-2-5 DUP 4/26/23 1.5-2 0.017 J 0.001 J <0.0008 0.003 J
SP-3-3 (4')4/26/23 3.5-4 0.020 J <0.0007 <0.0008 <0.0008
Trip Blank ------5.00 <0.180 <0.220 <1.30
Notes:
• Results reported in mg/kg (milligrams per kilograms).
• PSRG: NCDEQ Preliminary Soil Remediation Goal.
• < : Less than the method detection limit specified in the laboratory report.
• NE: Not Established.
• J: Estimated value.
• Trip blank results reported in ug/L.
• Concentrations of MEK (1.96 J ug/L) and methylene chloride (0.562 J ug/L) were reported in the trip blank.
As noted in laboratory report, acetone, MEK and methylene chloride concentrations detected in trip blank
are likely due to laboratory contamination.
Residential PSRGs (mg/kg)
Industrial/Commercial PSRGs (mg/kg)
Analytical Method
Contaminant of Concern BenzeneTABLE 6
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS - VOCs
FIVE POINTS GATEWAY
PROJECT ID: 21015-17-090
n-HexaneTolueneEPA Method
8260D
Acetone

APPENDICES

APPENDIX A
Subsurface Boring Logs

Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Martin Marietta-Bakers Quarry
Address 2111 N. Rocky River Road, Monroe
Boring Number SS-1-3'Date Drilled
Sample Method Grab (SS-1-3')/Composite Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller Resolve Log By S. Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0 - 3.0' Brown SILT
2
TD 3 feet
4
6
8
10

12
14
16

18
20
22

24
26
28

30
04/26/23
1 of 5 0-3.0 0.0
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Martin Marietta-Bakers Quarry
Address 2111 N. Rocky River Road, Monroe
Boring Number SS-2-3'Date Drilled
Sample Method Grab (SS-2-3')/Composite Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller Resolve Log By S. Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0 - 3.0' Brown SILT
2
TD 3 feet
4
6
8
10

12
14
16

18
20
22

24
26
28

30
04/26/23
2 of 5 0-3.0 0.1
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Martin Marietta-Bakers Quarry
Address 2111 N. Rocky River Road, Monroe
Boring Number SS-3-3'Date Drilled
Sample Method Grab (SS-3-3')/Composite Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller Resolve Log By S. Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0 - 3.0' Brown SILT
2
TD 3 feet
4
6
8
10

12
14
16

18
20
22

24
26
28

30
04/26/23
3 of 5 0-3.0 0.2
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Martin Marietta-Bakers Quarry
Address 2111 N. Rocky River Road, Monroe
Boring Number SS-4-3'Date Drilled
Sample Method Grab (SS-4-3')/Composite Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller Resolve Log By S. Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0 - 3.0' Brown SILT
2
TD 3 feet
4
6
8
10

12
14
16

18
20
22

24
26
28

30
04/26/23
4 of 5 0-3.0 0.0
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Martin Marietta-Bakers Quarry
Address 2111 N. Rocky River Road, Monroe
Boring Number SS-5-3'Date Drilled
Sample Method Grab (SS-5-3')/Composite Drilling Method Hand Auger
Completion Details Abandoned by backfilling boring with soil cuttings
Driller Resolve Log By S. Ball
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0 - 3.0' Brown SILT
2
TD 3 feet
4
6
8
10

12
14
16

18
20
22

24
26
28

30
04/26/23
5 of 5 0-3.0 0.4

APPENDIX B
Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/5/2023
Resolve Environmental Laura Minor
500 Devonport Dr. Matthews, NC, 28104
Ref: Analytical Testing
Lab Report Number: 23-117-0010 Client Project Description: 5 Points Gateway
Dear Laura Minor:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/27/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Danyale Love Project Manager
Page 1 of 78
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-117-0010
Page 2 of 78
Report Number:
Sample Summary Table
Client Project Description:
23-117-0010
5 Points Gateway
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
04/26/2023 08:07Solids 94899 SP-1-3 (3')04/27/2023
04/26/2023 08:16Solids 94900 SP-1 Comp 04/27/2023
04/26/2023 08:16Solids 94900 SP-1 Comp 04/27/2023 7471A WP MTN -
04/26/2023 08:16Solids 94900 SP-1 Comp 04/27/2023 6020B WP MTN -
04/26/2023 08:44Solids 94902 SP-2-5 04/27/2023
04/26/2023 08:44Solids 94903 SP-2-5 Dup 04/27/2023
04/26/2023 09:00Solids 94904 SP-2 Comp 04/27/2023
04/26/2023 09:00Solids 94904 SP-2 Comp 04/27/2023 7471A WP MTN -
04/26/2023 09:00Solids 94904 SP-2 Comp 04/27/2023 6020B WP MTN -
04/26/2023 09:00Solids 94906 SP-2 Comp Dup 04/27/2023
04/26/2023 09:00Solids 94906 SP-2 Comp Dup 04/27/2023 7471A WP MTN -
04/26/2023 09:00Solids 94906 SP-2 Comp Dup 04/27/2023 6020B WP MTN -
04/26/2023 09:14Solids 94908 SP-3-3 04/27/2023
04/26/2023 09:40Solids 94909 SP-3 Comp 04/27/2023
04/26/2023 09:40Solids 94909 SP-3 Comp 04/27/2023 6020B WP MTN -
04/26/2023 09:40Solids 94909 SP-3 Comp 04/27/2023 7471A WP MTN -
04/26/2023Aqueous 94911 Trip Blank 04/27/2023
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 78
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-117-0010
Report Limit
Project:5 Points Gateway
V 94899SP-1-3 (3')
0.025 05/01/2023 12:398260DAcetonemg/Kg - dry 0.003
20.0 04/30/2023 12:45SW-DRYWT Moisture %
V 94900SP-1 Comp
14.3 05/03/2023 14:076020BArsenicmg/Kg - dry 0.0983
34.3 05/03/2023 14:076020BBariummg/Kg - dry 0.049
0.292 05/03/2023 14:076020BCadmiummg/Kg - dry 0.0298
39.0 05/03/2023 14:076020BChromiummg/Kg - dry 0.133
42.6 05/03/2023 14:076020BLeadmg/Kg - dry 0.0356
0.796 05/03/2023 14:076020BSeleniummg/Kg - dry 0.118
J0.0311 05/03/2023 14:076020BSilvermg/Kg - dry 0.0077
J0.0764 05/04/2023 12:537471AMercury (Total)mg/Kg - dry 0.0251
13.1 04/30/2023 12:45SW-DRYWT Moisture %
V 94902SP-2-5
J0.011 05/01/2023 13:078260DAcetonemg/Kg - dry 0.002
J0.002 05/01/2023 13:078260DBenzenemg/Kg - dry 0.0007
J0.0009 05/01/2023 13:078260DToluenemg/Kg - dry 0.0008
12.2 04/30/2023 12:45SW-DRYWT Moisture %
V 94903SP-2-5 Dup
J0.017 05/01/2023 13:348260DAcetonemg/Kg - dry 0.002
J0.001 05/01/2023 13:348260DBenzenemg/Kg - dry 0.0007
J0.003 05/01/2023 13:348260Dn-Hexane mg/Kg - dry 0.0008
14.4 04/30/2023 12:45SW-DRYWT Moisture %
V 94904SP-2 Comp
10.6 05/03/2023 14:526020BArsenicmg/Kg - dry 0.0962
31.9 05/03/2023 14:526020BBariummg/Kg - dry 0.048
J0.0921 05/03/2023 14:526020BCadmiummg/Kg - dry 0.0291
43.8 05/03/2023 14:526020BChromiummg/Kg - dry 0.130
35.2 05/03/2023 14:526020BLeadmg/Kg - dry 0.0349
0.632 05/03/2023 14:526020BSeleniummg/Kg - dry 0.115
J0.0331 05/03/2023 14:526020BSilvermg/Kg - dry 0.0075
J0.0872 05/04/2023 13:037471AMercury (Total)mg/Kg - dry 0.0238
11.2 04/30/2023 12:45SW-DRYWT Moisture %
V 94906SP-2 Comp Dup
13.2 05/03/2023 14:566020BArsenicmg/Kg - dry 0.0980
Page 4 of 78
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-117-0010
Report Limit
Project:5 Points Gateway
V 94906SP-2 Comp Dup
56.5 05/03/2023 14:566020BBariummg/Kg - dry 0.048
J0.208 05/03/2023 14:566020BCadmiummg/Kg - dry 0.0297
61.0 05/04/2023 17:466020BChromiummg/Kg - dry 0.266
100 05/03/2023 14:566020BLeadmg/Kg - dry 0.0355
1.23 05/03/2023 14:566020BSeleniummg/Kg - dry 0.118
J0.0756 05/03/2023 14:566020BSilvermg/Kg - dry 0.0077
J0.102 05/04/2023 13:057471AMercury (Total)mg/Kg - dry 0.0229
12.8 04/30/2023 12:45SW-DRYWT Moisture %
V 94908SP-3-3
J0.020 05/01/2023 14:018260DAcetonemg/Kg - dry 0.002
13.9 04/30/2023 12:45SW-DRYWT Moisture %
V 94909SP-3 Comp
12.4 05/03/2023 15:006020BArsenicmg/Kg - dry 0.0973
50.2 05/03/2023 15:006020BBariummg/Kg - dry 0.048
1.77 05/03/2023 15:006020BCadmiummg/Kg - dry 0.0294
39.3 05/03/2023 15:006020BChromiummg/Kg - dry 0.132
114 05/03/2023 15:006020BLeadmg/Kg - dry 0.0353
1.10 05/03/2023 15:006020BSeleniummg/Kg - dry 0.117
J0.0812 05/03/2023 15:006020BSilvermg/Kg - dry 0.0076
J0.118 05/04/2023 13:097471AMercury (Total)mg/Kg - dry 0.0227
12.2 04/30/2023 12:45SW-DRYWT Moisture %
V 94911Trip Blank
5.00 05/02/2023 15:448260DAcetoneµg/L 1.80
J1.96 05/02/2023 15:448260DMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.562 05/02/2023 15:448260DMethylene Chloride µg/L 0.330
Page 5 of 78

Client: Resolve Environmental CASE NARRATIVE Project: 5 Points Gateway
Lab Report Number: 23-117-0010 Date: 5/5/2023
Metals Analyses Method 6020B Sample 95000 (IDW-Soil)
Analyte: Arsenic QC Batch No: L679823/L679484
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil)
Analyte: Barium QC Batch No: L679823/L679484
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil)
Analyte: Cadmium QC Batch No: L679823/L679484
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 95000 (IDW-Soil) Analyte: Chromium QC Batch No: L679823/L679484 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil) Analyte: Lead
QC Batch No: L679823/L679484 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil) Analyte: Selenium
QC Batch No: L679823/L679484 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 84607 (SB-2) Analyte: Mercury QC Batch No: L680090/L679881 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 6 of 78

Volatile Organic Compounds - GC/MS Method 8260D
Sample 94911 (Trip Blank) Hits in this sample are likely due to lab contamination.
Analyte: 1,1,2,2-Tetrachloroethane
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: 1,2,3-Trichlorobenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: 1,2,3-Trichloropropane
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: 1,2,4-Trichlorobenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: 1,2-Dichlorobenzene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples Analyte: 1,3,5-Trimethylbenzene QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: 2-Chlorotoluene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: 4-Chlorotoluene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: Bromobenzene QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: Chloroethane QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Page 7 of 78

Analyte: Hexachlorobutadiene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: Isopropylbenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: Naphthalene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: n-Butylbenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: n-Propylbenzene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: tert-Butylbenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Semivolatile Organic Compounds - GC/MS Method 8270E Sample 94900 (SP-1 Comp) QC Batch No: V32788/V32670
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample was a thick dark liquid with bubbles. Running at a lower dilution could cause instrumentation issues.
Sample 94904 (SP-2 Comp) QC Batch No: V32788/V32670 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample was a thick dark liquid with bubbles. Running at a lower dilution could cause instrumentation issues.
Sample 94906 (SP-2 Comp Dup) QC Batch No: V32788/V32670 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample was a thick dark liquid with bubbles. Running at a lower dilution could cause instrumentation issues. Sample 94909 (SP-3 Comp) QC Batch No: V32788/V32670 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Sample was a thick dark liquid with bubbles. Running at a lower dilution could cause instrumentation issues.
Page 8 of 78

Analyte: Benzo(b)fluoranthene
QC Batch No: V32788/V32670 CCV saw high recoveries for this compound. All other QC was within method parameters. Results for this
compound are estimated high.
Analyte: Benzo(g,h,i)perylene QC Batch No: V32788/V32670
CCV saw high recoveries for this compound. All other QC was within method parameters. Results for this compound are estimated high.

Page 9 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1-3 (3')
94899 Matrix:
4/26/2023 8:07
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
20.0 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1-3 (3')
94899 Matrix:
4/26/2023 8:07
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
0.025 mg/Kg - dry 0.003 0.025Acetone 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.025Acrolein 1 05/01/23 12:39 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.025Acrylonitrile 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.006Benzene 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.006Bromobenzene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Bromochloromethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Bromodichloromethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Bromoform 1 05/01/23 12:39 V32647TBL
<0.002 mg/Kg - dry 0.002 0.012Bromomethane 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.006n-Butylbenzene 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.006sec-Butyl benzene 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.006tert-Butyl benzene 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.006Carbon Disulfide 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Carbon Tetrachloride 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.006Chlorobenzene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Chlorodibromomethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.012Chloroethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Chloroform 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.012Chloromethane 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0062-Chlorotoluene 1 05/01/23 12:39 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0064-Chlorotoluene 1 05/01/23 12:39 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.006Di-Isopropyl Ether (DIPE)1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0121,2-Dibromo-3-Chloropropane 1 05/01/23 12:39 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1-3 (3')
94899 Matrix:
4/26/2023 8:07
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0061,2-Dibromoethane 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.006Dibromomethane 1 05/01/23 12:39 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,2-Dichlorobenzene 1 05/01/23 12:39 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0061,3-Dichlorobenzene 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0061,4-Dichlorobenzene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.012Dichlorodifluoromethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0061,1-Dichloroethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0061,2-Dichloroethane 1 05/01/23 12:39 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,1-Dichloroethene 1 05/01/23 12:39 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.006cis-1,2-Dichloroethene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,2-Dichloroethene 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2-Dichloropropane 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3-Dichloropropane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0062,2-Dichloropropane 1 05/01/23 12:39 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.0061,1-Dichloropropene 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.006cis-1,3-Dichloropropene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006trans-1,3-Dichloropropene 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.006Ethylbenzene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.062Ethyl Tertiary Butyl Ether (ETBE)1 05/01/23 12:39 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.012Hexachlorobutadiene 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.012n-Hexane 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0252-Hexanone 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.006Isopropylbenzene 1 05/01/23 12:39 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1-3 (3')
94899 Matrix:
4/26/2023 8:07
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0064-Isopropyl toluene 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.025Methyl Ethyl Ketone (MEK)1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.006Methyl tert-butyl ether (MTBE)1 05/01/23 12:39 V32647TBL
<0.018 mg/Kg - dry 0.018 0.0254-Methyl-2-Pentanone 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.012Methylene Chloride 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.012Naphthalene 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.006n-Propylbenzene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Styrene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1,2-Tetrachloroethane 1 05/01/23 12:39 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0061,1,2,2-Tetrachloroethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Tetrachloroethene 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.006Toluene 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0121,2,3-Trichlorobenzene 1 05/01/23 12:39 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0121,2,4-Trichlorobenzene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0061,1,1-Trichloroethane 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,1,2-Trichloroethane 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.006Trichloroethene 1 05/01/23 12:39 V32647TBL
<0.002 mg/Kg - dry 0.002 0.012Trichlorofluoromethane 1 05/01/23 12:39 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0061,2,3-Trichloropropane 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0061,2,4-Trimethylbenzene 1 05/01/23 12:39 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0061,3,5-Trimethylbenzene 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Acetate 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.012Vinyl Chloride 1 05/01/23 12:39 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1-3 (3')
94899 Matrix:
4/26/2023 8:07
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.006o-Xylene 1 05/01/23 12:39 V32647TBL
<0.001 mg/Kg - dry 0.001 0.012m,p-Xylene 1 05/01/23 12:39 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.006Xylene (Total)1 05/01/23 12:39 V32647
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%05/01/23 12:391 TBL V32647
Surrogate: Dibromofluoromethane 102 Limits: 84-123%05/01/23 12:391 TBL V32647
Surrogate: Toluene-d8 86.9 Limits: 76-129%05/01/23 12:391 TBL V32647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1 Comp
94900 Matrix:
4/26/2023 8:16
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.1 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
14.3 mg/Kg - dry 0.0983 0.288Arsenic 5 05/03/23 14:07 6020BCPW
34.3 mg/Kg - dry 0.049 0.287Barium 5 05/03/23 14:07 6020BCPW
0.292 mg/Kg - dry 0.0298 0.288Cadmium 5 05/03/23 14:07 6020BCPW
39.0 mg/Kg - dry 0.133 0.287Chromium 5 05/03/23 14:07 6020BCPW
42.6 mg/Kg - dry 0.0356 0.288Lead 5 05/03/23 14:07 6020BCPW
0.0764 J mg/Kg - dry 0.0251 0.208Mercury (Total)1 05/04/23 12:53 7471AFDS
0.796 mg/Kg - dry 0.118 0.287Selenium 5 05/03/23 14:07 6020BCPW
0.0311 J mg/Kg - dry 0.0077 0.288Silver 5 05/03/23 14:07 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1 Comp
94900 Matrix:
4/26/2023 8:16
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<16.0 mg/Kg - dry 16.0 91.1Acenaphthene 4 05/03/23 12:39 V32788ANG
<14.5 mg/Kg - dry 14.5 91.1Acenaphthylene 4 05/03/23 12:39 V32788ANG
<20.9 mg/Kg - dry 20.9 91.1Aniline 4 05/03/23 12:39 V32788ANG
<19.8 mg/Kg - dry 19.8 91.1Anthracene 4 05/03/23 12:39 V32788ANG
<19.2 mg/Kg - dry 19.2 91.1Benzo(a)anthracene 4 05/03/23 12:39 V32788ANG
<20.3 mg/Kg - dry 20.3 91.1Benzo(a)pyrene 4 05/03/23 12:39 V32788ANG
<20.1 mg/Kg - dry 20.1 91.1Benzo(b)fluoranthene 4 05/03/23 12:39 V32788ANG
<18.8 mg/Kg - dry 18.8 91.1Benzo(g,h,i)perylene 4 05/03/23 12:39 V32788ANG
<18.9 mg/Kg - dry 18.9 91.1Benzo(k)fluoranthene 4 05/03/23 12:39 V32788ANG
<80.1 mg/Kg - dry 80.1 276Benzoic Acid 4 05/03/23 12:39 V32788ANG
<14.5 mg/Kg - dry 14.5 91.1Benzyl alcohol 4 05/03/23 12:39 V32788ANG
<16.3 mg/Kg - dry 16.3 91.1Bis(2-Chloroethoxy)methane 4 05/03/23 12:39 V32788ANG
<14.7 mg/Kg - dry 14.7 91.1Bis(2-Chloroethyl)ether 4 05/03/23 12:39 V32788ANG
<18.8 mg/Kg - dry 18.8 45.6Bis(2-Chloroisopropyl)ether 4 05/03/23 12:39 V32788ANG
<16.6 mg/Kg - dry 16.6 91.1Bis(2-ethylhexyl)phthalate 4 05/03/23 12:39 V32788ANG
<15.1 mg/Kg - dry 15.1 91.14-Bromophenyl phenyl ether 4 05/03/23 12:39 V32788ANG
<15.7 mg/Kg - dry 15.7 45.6Butyl benzyl phthalate 4 05/03/23 12:39 V32788ANG
<12.8 mg/Kg - dry 12.8 91.14-Chloro-3-methylphenol 4 05/03/23 12:39 V32788ANG
<15.4 mg/Kg - dry 15.4 45.64-Chloroaniline 4 05/03/23 12:39 V32788ANG
<16.0 mg/Kg - dry 16.0 91.12-Chloronaphthalene 4 05/03/23 12:39 V32788ANG
<13.6 mg/Kg - dry 13.6 91.12-Chlorophenol 4 05/03/23 12:39 V32788ANG
<17.4 mg/Kg - dry 17.4 1384-Chlorophenyl phenyl ether 4 05/03/23 12:39 V32788ANG
<19.6 mg/Kg - dry 19.6 91.1Chrysene 4 05/03/23 12:39 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1 Comp
94900 Matrix:
4/26/2023 8:16
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<31.8 mg/Kg - dry 31.8 91.1Dibenz(a,h)anthracene 4 05/03/23 12:39 V32788ANG
<16.5 mg/Kg - dry 16.5 91.1Dibenzofuran 4 05/03/23 12:39 V32788ANG
<13.0 mg/Kg - dry 13.0 91.11,2-Dichlorobenzene 4 05/03/23 12:39 V32788ANG
<13.5 mg/Kg - dry 13.5 91.11,3-Dichlorobenzene 4 05/03/23 12:39 V32788ANG
<13.5 mg/Kg - dry 13.5 45.61,4-Dichlorobenzene 4 05/03/23 12:39 V32788ANG
<20.3 mg/Kg - dry 20.3 91.13,3'-Dichlorobenzidine 4 05/03/23 12:39 V32788ANG
<13.2 mg/Kg - dry 13.2 91.12,4-Dichlorophenol 4 05/03/23 12:39 V32788ANG
<24.9 mg/Kg - dry 24.9 91.1Diethyl phthalate 4 05/03/23 12:39 V32788ANG
<24.1 mg/Kg - dry 24.1 91.1Dimethyl phthalate 4 05/03/23 12:39 V32788ANG
<15.0 mg/Kg - dry 15.0 45.62,4-Dimethylphenol 4 05/03/23 12:39 V32788ANG
<14.7 mg/Kg - dry 14.7 91.1Di-n-butyl phthalate 4 05/03/23 12:39 V32788ANG
<33.1 mg/Kg - dry 33.1 2074,6-Dinitro-2-methylphenol 4 05/03/23 12:39 V32788ANG
<71.8 mg/Kg - dry 71.8 2072,4-Dinitrophenol 4 05/03/23 12:39 V32788ANG
<13.3 mg/Kg - dry 13.3 91.12,4-Dinitrotoluene 4 05/03/23 12:39 V32788ANG
<15.0 mg/Kg - dry 15.0 91.12,6-Dinitrotoluene 4 05/03/23 12:39 V32788ANG
<19.8 mg/Kg - dry 19.8 45.6Di-n-Octyl Phthalate 4 05/03/23 12:39 V32788ANG
<17.0 mg/Kg - dry 17.0 91.1Fluoranthene 4 05/03/23 12:39 V32788ANG
<17.7 mg/Kg - dry 17.7 91.1Fluorene 4 05/03/23 12:39 V32788ANG
<14.6 mg/Kg - dry 14.6 91.1Hexachlorobenzene 4 05/03/23 12:39 V32788ANG
<13.5 mg/Kg - dry 13.5 91.1Hexachlorobutadiene 4 05/03/23 12:39 V32788ANG
<21.6 mg/Kg - dry 21.6 91.1Hexachlorocyclopentadiene 4 05/03/23 12:39 V32788ANG
<10.9 mg/Kg - dry 10.9 91.1Hexachloroethane 4 05/03/23 12:39 V32788ANG
<24.7 mg/Kg - dry 24.7 91.1Indeno(1,2,3-cd)pyrene 4 05/03/23 12:39 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1 Comp
94900 Matrix:
4/26/2023 8:16
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<26.4 mg/Kg - dry 26.4 91.1Isophorone 4 05/03/23 12:39 V32788ANG
<14.6 mg/Kg - dry 14.6 91.11-Methylnaphthalene 4 05/03/23 12:39 V32788ANG
<13.8 mg/Kg - dry 13.8 91.12-Methylnaphthalene 4 05/03/23 12:39 V32788ANG
<13.3 mg/Kg - dry 13.3 91.12-Methylphenol 4 05/03/23 12:39 V32788ANG
<11.7 mg/Kg - dry 11.7 91.13&4 Methylphenol 4 05/03/23 12:39 V32788ANG
<19.9 mg/Kg - dry 19.9 91.1Naphthalene 4 05/03/23 12:39 V32788ANG
<13.3 mg/Kg - dry 13.3 91.12-Nitroaniline 4 05/03/23 12:39 V32788ANG
<16.6 mg/Kg - dry 16.6 91.13-Nitroaniline 4 05/03/23 12:39 V32788ANG
<12.9 mg/Kg - dry 12.9 45.64-Nitroaniline 4 05/03/23 12:39 V32788ANG
<16.0 mg/Kg - dry 16.0 45.6Nitrobenzene 4 05/03/23 12:39 V32788ANG
<12.3 mg/Kg - dry 12.3 91.12-Nitrophenol 4 05/03/23 12:39 V32788ANG
<16.1 mg/Kg - dry 16.1 91.14-Nitrophenol 4 05/03/23 12:39 V32788ANG
<36.4 mg/Kg - dry 36.4 91.1N-Nitrosodimethylamine 4 05/03/23 12:39 V32788ANG
<25.0 mg/Kg - dry 25.0 91.1N-Nitrosodiphenylamine 4 05/03/23 12:39 V32788ANG
<16.3 mg/Kg - dry 16.3 91.1N-Nitroso-di-n-propylamine 4 05/03/23 12:39 V32788ANG
<47.9 mg/Kg - dry 47.9 138Pentachlorophenol 4 05/03/23 12:39 V32788ANG
<28.8 mg/Kg - dry 28.8 91.1Phenanthrene 4 05/03/23 12:39 V32788ANG
<15.4 mg/Kg - dry 15.4 91.1Phenol 4 05/03/23 12:39 V32788ANG
<18.5 mg/Kg - dry 18.5 91.1Pyrene 4 05/03/23 12:39 V32788ANG
<10.9 mg/Kg - dry 10.9 45.6Pyridine 4 05/03/23 12:39 V32788ANG
<14.7 mg/Kg - dry 14.7 91.11,2,4-Trichlorobenzene 4 05/03/23 12:39 V32788ANG
<13.2 mg/Kg - dry 13.2 91.12,4,5-Trichlorophenol 4 05/03/23 12:39 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-1 Comp
94900 Matrix:
4/26/2023 8:16
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<13.3 mg/Kg - dry 13.3 91.12,4,6-Trichlorophenol 4 05/03/23 12:39 V32788ANG
8270ESurrogate: Phenol-d5 47.4 Limits: 34-121%05/03/23 12:394 ANG
Surrogate: 2-Fluorobiphenyl 58.4 Limits: 44-115%05/03/23 12:394 ANG V32788
Surrogate: 2-Fluorophenol 51.0 Limits: 35-115%05/03/23 12:394 ANG V32788
Surrogate: Nitrobenzene-d5 53.0 Limits: 37-122%05/03/23 12:394 ANG V32788
Surrogate: 4-Terphenyl-d14 61.6 Limits: 54-127%05/03/23 12:394 ANG V32788
Surrogate: 2,4,6-Tribromophenol 46.5 Limits: 39-132%05/03/23 12:394 ANG V32788
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5
94902 Matrix:
4/26/2023 8:44
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.2 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5
94902 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
0.011 J mg/Kg - dry 0.002 0.022Acetone 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.022Acrolein 1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.022Acrylonitrile 1 05/01/23 13:07 V32647TBL
0.002 J mg/Kg - dry 0.0007 0.005Benzene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/01/23 13:07 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005sec-Butyl benzene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/01/23 13:07 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/01/23 13:07 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0054-Chlorotoluene 1 05/01/23 13:07 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/01/23 13:07 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/01/23 13:07 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5
94902 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Dibromomethane 1 05/01/23 13:07 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/01/23 13:07 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/01/23 13:07 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/01/23 13:07 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.056Ethyl Tertiary Butyl Ether (ETBE)1 05/01/23 13:07 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/01/23 13:07 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0222-Hexanone 1 05/01/23 13:07 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/01/23 13:07 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5
94902 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.022Methyl Ethyl Ketone (MEK)1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/01/23 13:07 V32647TBL
<0.017 mg/Kg - dry 0.017 0.0224-Methyl-2-Pentanone 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/01/23 13:07 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/01/23 13:07 V32647TBL
0.0009 J mg/Kg - dry 0.0008 0.005Toluene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/01/23 13:07 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/01/23 13:07 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/01/23 13:07 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/01/23 13:07 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/01/23 13:07 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/01/23 13:07 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Chloride 1 05/01/23 13:07 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5
94902 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/01/23 13:07 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/01/23 13:07 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/01/23 13:07 V32647
Surrogate: 4-Bromofluorobenzene 97.9 Limits: 70-130%05/01/23 13:071 TBL V32647
Surrogate: Dibromofluoromethane 91.2 Limits: 84-123%05/01/23 13:071 TBL V32647
Surrogate: Toluene-d8 89.1 Limits: 76-129%05/01/23 13:071 TBL V32647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5 Dup
94903 Matrix:
4/26/2023 8:44
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.4 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5 Dup
94903 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
0.017 J mg/Kg - dry 0.002 0.023Acetone 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/01/23 13:34 V32647TBL
0.001 J mg/Kg - dry 0.0007 0.005Benzene 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/01/23 13:34 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/01/23 13:34 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/01/23 13:34 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 05/01/23 13:34 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/01/23 13:34 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5 Dup
94903 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 05/01/23 13:34 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/01/23 13:34 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/01/23 13:34 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/01/23 13:34 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/01/23 13:34 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/01/23 13:34 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/01/23 13:34 V32647TBL
0.003 J mg/Kg - dry 0.0008 0.011n-Hexane 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/01/23 13:34 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/01/23 13:34 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5 Dup
94903 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 05/01/23 13:34 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/01/23 13:34 V32647TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/01/23 13:34 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/01/23 13:34 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/01/23 13:34 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/01/23 13:34 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/01/23 13:34 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/01/23 13:34 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/01/23 13:34 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 05/01/23 13:34 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2-5 Dup
94903 Matrix:
4/26/2023 8:44
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/01/23 13:34 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/01/23 13:34 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/01/23 13:34 V32647
Surrogate: 4-Bromofluorobenzene 98.9 Limits: 70-130%05/01/23 13:341 TBL V32647
Surrogate: Dibromofluoromethane 97.6 Limits: 84-123%05/01/23 13:341 TBL V32647
Surrogate: Toluene-d8 89.3 Limits: 76-129%05/01/23 13:341 TBL V32647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp
94904 Matrix:
4/26/2023 9:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
11.2 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
10.6 mg/Kg - dry 0.0962 0.282Arsenic 5 05/03/23 14:52 6020BCPW
31.9 mg/Kg - dry 0.048 0.281Barium 5 05/03/23 14:52 6020BCPW
0.0921 J mg/Kg - dry 0.0291 0.282Cadmium 5 05/03/23 14:52 6020BCPW
43.8 mg/Kg - dry 0.130 0.281Chromium 5 05/03/23 14:52 6020BCPW
35.2 mg/Kg - dry 0.0349 0.282Lead 5 05/03/23 14:52 6020BCPW
0.0872 J mg/Kg - dry 0.0238 0.197Mercury (Total)1 05/04/23 13:03 7471AFDS
0.632 mg/Kg - dry 0.115 0.281Selenium 5 05/03/23 14:52 6020BCPW
0.0331 J mg/Kg - dry 0.0075 0.282Silver 5 05/03/23 14:52 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp
94904 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<15.7 mg/Kg - dry 15.7 89.2Acenaphthene 4 05/03/23 13:02 V32788ANG
<14.2 mg/Kg - dry 14.2 89.2Acenaphthylene 4 05/03/23 13:02 V32788ANG
<20.5 mg/Kg - dry 20.5 89.2Aniline 4 05/03/23 13:02 V32788ANG
<19.4 mg/Kg - dry 19.4 89.2Anthracene 4 05/03/23 13:02 V32788ANG
<18.8 mg/Kg - dry 18.8 89.2Benzo(a)anthracene 4 05/03/23 13:02 V32788ANG
<19.8 mg/Kg - dry 19.8 89.2Benzo(a)pyrene 4 05/03/23 13:02 V32788ANG
<19.7 mg/Kg - dry 19.7 89.2Benzo(b)fluoranthene 4 05/03/23 13:02 V32788ANG
<18.4 mg/Kg - dry 18.4 89.2Benzo(g,h,i)perylene 4 05/03/23 13:02 V32788ANG
<18.5 mg/Kg - dry 18.5 89.2Benzo(k)fluoranthene 4 05/03/23 13:02 V32788ANG
<78.4 mg/Kg - dry 78.4 270Benzoic Acid 4 05/03/23 13:02 V32788ANG
<14.2 mg/Kg - dry 14.2 89.2Benzyl alcohol 4 05/03/23 13:02 V32788ANG
<16.0 mg/Kg - dry 16.0 89.2Bis(2-Chloroethoxy)methane 4 05/03/23 13:02 V32788ANG
<14.4 mg/Kg - dry 14.4 89.2Bis(2-Chloroethyl)ether 4 05/03/23 13:02 V32788ANG
<18.4 mg/Kg - dry 18.4 44.6Bis(2-Chloroisopropyl)ether 4 05/03/23 13:02 V32788ANG
<16.2 mg/Kg - dry 16.2 89.2Bis(2-ethylhexyl)phthalate 4 05/03/23 13:02 V32788ANG
<14.8 mg/Kg - dry 14.8 89.24-Bromophenyl phenyl ether 4 05/03/23 13:02 V32788ANG
<15.3 mg/Kg - dry 15.3 44.6Butyl benzyl phthalate 4 05/03/23 13:02 V32788ANG
<12.5 mg/Kg - dry 12.5 89.24-Chloro-3-methylphenol 4 05/03/23 13:02 V32788ANG
<15.1 mg/Kg - dry 15.1 44.64-Chloroaniline 4 05/03/23 13:02 V32788ANG
<15.7 mg/Kg - dry 15.7 89.22-Chloronaphthalene 4 05/03/23 13:02 V32788ANG
<13.3 mg/Kg - dry 13.3 89.22-Chlorophenol 4 05/03/23 13:02 V32788ANG
<17.0 mg/Kg - dry 17.0 1354-Chlorophenyl phenyl ether 4 05/03/23 13:02 V32788ANG
<19.1 mg/Kg - dry 19.1 89.2Chrysene 4 05/03/23 13:02 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp
94904 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<31.1 mg/Kg - dry 31.1 89.2Dibenz(a,h)anthracene 4 05/03/23 13:02 V32788ANG
<16.1 mg/Kg - dry 16.1 89.2Dibenzofuran 4 05/03/23 13:02 V32788ANG
<12.7 mg/Kg - dry 12.7 89.21,2-Dichlorobenzene 4 05/03/23 13:02 V32788ANG
<13.2 mg/Kg - dry 13.2 89.21,3-Dichlorobenzene 4 05/03/23 13:02 V32788ANG
<13.2 mg/Kg - dry 13.2 44.61,4-Dichlorobenzene 4 05/03/23 13:02 V32788ANG
<19.8 mg/Kg - dry 19.8 89.23,3'-Dichlorobenzidine 4 05/03/23 13:02 V32788ANG
<13.0 mg/Kg - dry 13.0 89.22,4-Dichlorophenol 4 05/03/23 13:02 V32788ANG
<24.3 mg/Kg - dry 24.3 89.2Diethyl phthalate 4 05/03/23 13:02 V32788ANG
<23.5 mg/Kg - dry 23.5 89.2Dimethyl phthalate 4 05/03/23 13:02 V32788ANG
<14.6 mg/Kg - dry 14.6 44.62,4-Dimethylphenol 4 05/03/23 13:02 V32788ANG
<14.4 mg/Kg - dry 14.4 89.2Di-n-butyl phthalate 4 05/03/23 13:02 V32788ANG
<32.4 mg/Kg - dry 32.4 2034,6-Dinitro-2-methylphenol 4 05/03/23 13:02 V32788ANG
<70.3 mg/Kg - dry 70.3 2032,4-Dinitrophenol 4 05/03/23 13:02 V32788ANG
<13.1 mg/Kg - dry 13.1 89.22,4-Dinitrotoluene 4 05/03/23 13:02 V32788ANG
<14.6 mg/Kg - dry 14.6 89.22,6-Dinitrotoluene 4 05/03/23 13:02 V32788ANG
<19.4 mg/Kg - dry 19.4 44.6Di-n-Octyl Phthalate 4 05/03/23 13:02 V32788ANG
<16.7 mg/Kg - dry 16.7 89.2Fluoranthene 4 05/03/23 13:02 V32788ANG
<17.3 mg/Kg - dry 17.3 89.2Fluorene 4 05/03/23 13:02 V32788ANG
<14.3 mg/Kg - dry 14.3 89.2Hexachlorobenzene 4 05/03/23 13:02 V32788ANG
<13.2 mg/Kg - dry 13.2 89.2Hexachlorobutadiene 4 05/03/23 13:02 V32788ANG
<21.2 mg/Kg - dry 21.2 89.2Hexachlorocyclopentadiene 4 05/03/23 13:02 V32788ANG
<10.7 mg/Kg - dry 10.7 89.2Hexachloroethane 4 05/03/23 13:02 V32788ANG
<24.2 mg/Kg - dry 24.2 89.2Indeno(1,2,3-cd)pyrene 4 05/03/23 13:02 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 32 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp
94904 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<25.8 mg/Kg - dry 25.8 89.2Isophorone 4 05/03/23 13:02 V32788ANG
<14.3 mg/Kg - dry 14.3 89.21-Methylnaphthalene 4 05/03/23 13:02 V32788ANG
<13.5 mg/Kg - dry 13.5 89.22-Methylnaphthalene 4 05/03/23 13:02 V32788ANG
<13.1 mg/Kg - dry 13.1 89.22-Methylphenol 4 05/03/23 13:02 V32788ANG
<11.5 mg/Kg - dry 11.5 89.23&4 Methylphenol 4 05/03/23 13:02 V32788ANG
<19.5 mg/Kg - dry 19.5 89.2Naphthalene 4 05/03/23 13:02 V32788ANG
<13.1 mg/Kg - dry 13.1 89.22-Nitroaniline 4 05/03/23 13:02 V32788ANG
<16.2 mg/Kg - dry 16.2 89.23-Nitroaniline 4 05/03/23 13:02 V32788ANG
<12.6 mg/Kg - dry 12.6 44.64-Nitroaniline 4 05/03/23 13:02 V32788ANG
<15.7 mg/Kg - dry 15.7 44.6Nitrobenzene 4 05/03/23 13:02 V32788ANG
<12.0 mg/Kg - dry 12.0 89.22-Nitrophenol 4 05/03/23 13:02 V32788ANG
<15.8 mg/Kg - dry 15.8 89.24-Nitrophenol 4 05/03/23 13:02 V32788ANG
<35.6 mg/Kg - dry 35.6 89.2N-Nitrosodimethylamine 4 05/03/23 13:02 V32788ANG
<24.4 mg/Kg - dry 24.4 89.2N-Nitrosodiphenylamine 4 05/03/23 13:02 V32788ANG
<16.0 mg/Kg - dry 16.0 89.2N-Nitroso-di-n-propylamine 4 05/03/23 13:02 V32788ANG
<46.8 mg/Kg - dry 46.8 135Pentachlorophenol 4 05/03/23 13:02 V32788ANG
<28.2 mg/Kg - dry 28.2 89.2Phenanthrene 4 05/03/23 13:02 V32788ANG
<15.1 mg/Kg - dry 15.1 89.2Phenol 4 05/03/23 13:02 V32788ANG
<18.1 mg/Kg - dry 18.1 89.2Pyrene 4 05/03/23 13:02 V32788ANG
<10.7 mg/Kg - dry 10.7 44.6Pyridine 4 05/03/23 13:02 V32788ANG
<14.4 mg/Kg - dry 14.4 89.21,2,4-Trichlorobenzene 4 05/03/23 13:02 V32788ANG
<13.0 mg/Kg - dry 13.0 89.22,4,5-Trichlorophenol 4 05/03/23 13:02 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 33 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp
94904 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<13.1 mg/Kg - dry 13.1 89.22,4,6-Trichlorophenol 4 05/03/23 13:02 V32788ANG
8270ESurrogate: Phenol-d5 55.5 Limits: 34-121%05/03/23 13:024 ANG
Surrogate: 2-Fluorobiphenyl 67.8 Limits: 44-115%05/03/23 13:024 ANG V32788
Surrogate: 2-Fluorophenol 59.0 Limits: 35-115%05/03/23 13:024 ANG V32788
Surrogate: Nitrobenzene-d5 60.6 Limits: 37-122%05/03/23 13:024 ANG V32788
Surrogate: 4-Terphenyl-d14 72.6 Limits: 54-127%05/03/23 13:024 ANG V32788
Surrogate: 2,4,6-Tribromophenol 54.6 Limits: 39-132%05/03/23 13:024 ANG V32788
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 34 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp Dup
94906 Matrix:
4/26/2023 9:00
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.8 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
13.2 mg/Kg - dry 0.0980 0.287Arsenic 5 05/03/23 14:56 6020BCPW
56.5 mg/Kg - dry 0.048 0.286Barium 5 05/03/23 14:56 6020BCPW
0.208 J mg/Kg - dry 0.0297 0.287Cadmium 5 05/03/23 14:56 6020BCPW
61.0 mg/Kg - dry 0.266 0.573Chromium 10 05/04/23 17:46 6020BCPW
100 mg/Kg - dry 0.0355 0.287Lead 5 05/03/23 14:56 6020BCPW
0.102 J mg/Kg - dry 0.0229 0.190Mercury (Total)1 05/04/23 13:05 7471AFDS
1.23 mg/Kg - dry 0.118 0.286Selenium 5 05/03/23 14:56 6020BCPW
0.0756 J mg/Kg - dry 0.0077 0.287Silver 5 05/03/23 14:56 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 35 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp Dup
94906 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<15.9 mg/Kg - dry 15.9 90.8Acenaphthene 4 05/03/23 13:24 V32788ANG
<14.4 mg/Kg - dry 14.4 90.8Acenaphthylene 4 05/03/23 13:24 V32788ANG
<20.9 mg/Kg - dry 20.9 90.8Aniline 4 05/03/23 13:24 V32788ANG
<19.7 mg/Kg - dry 19.7 90.8Anthracene 4 05/03/23 13:24 V32788ANG
<19.2 mg/Kg - dry 19.2 90.8Benzo(a)anthracene 4 05/03/23 13:24 V32788ANG
<20.2 mg/Kg - dry 20.2 90.8Benzo(a)pyrene 4 05/03/23 13:24 V32788ANG
<20.1 mg/Kg - dry 20.1 90.8Benzo(b)fluoranthene 4 05/03/23 13:24 V32788ANG
<18.7 mg/Kg - dry 18.7 90.8Benzo(g,h,i)perylene 4 05/03/23 13:24 V32788ANG
<18.8 mg/Kg - dry 18.8 90.8Benzo(k)fluoranthene 4 05/03/23 13:24 V32788ANG
<79.8 mg/Kg - dry 79.8 275Benzoic Acid 4 05/03/23 13:24 V32788ANG
<14.4 mg/Kg - dry 14.4 90.8Benzyl alcohol 4 05/03/23 13:24 V32788ANG
<16.3 mg/Kg - dry 16.3 90.8Bis(2-Chloroethoxy)methane 4 05/03/23 13:24 V32788ANG
<14.7 mg/Kg - dry 14.7 90.8Bis(2-Chloroethyl)ether 4 05/03/23 13:24 V32788ANG
<18.7 mg/Kg - dry 18.7 45.4Bis(2-Chloroisopropyl)ether 4 05/03/23 13:24 V32788ANG
<16.5 mg/Kg - dry 16.5 90.8Bis(2-ethylhexyl)phthalate 4 05/03/23 13:24 V32788ANG
<15.0 mg/Kg - dry 15.0 90.84-Bromophenyl phenyl ether 4 05/03/23 13:24 V32788ANG
<15.6 mg/Kg - dry 15.6 45.4Butyl benzyl phthalate 4 05/03/23 13:24 V32788ANG
<12.7 mg/Kg - dry 12.7 90.84-Chloro-3-methylphenol 4 05/03/23 13:24 V32788ANG
<15.4 mg/Kg - dry 15.4 45.44-Chloroaniline 4 05/03/23 13:24 V32788ANG
<15.9 mg/Kg - dry 15.9 90.82-Chloronaphthalene 4 05/03/23 13:24 V32788ANG
<13.5 mg/Kg - dry 13.5 90.82-Chlorophenol 4 05/03/23 13:24 V32788ANG
<17.3 mg/Kg - dry 17.3 1384-Chlorophenyl phenyl ether 4 05/03/23 13:24 V32788ANG
<19.5 mg/Kg - dry 19.5 90.8Chrysene 4 05/03/23 13:24 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 36 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp Dup
94906 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<31.7 mg/Kg - dry 31.7 90.8Dibenz(a,h)anthracene 4 05/03/23 13:24 V32788ANG
<16.4 mg/Kg - dry 16.4 90.8Dibenzofuran 4 05/03/23 13:24 V32788ANG
<13.0 mg/Kg - dry 13.0 90.81,2-Dichlorobenzene 4 05/03/23 13:24 V32788ANG
<13.4 mg/Kg - dry 13.4 90.81,3-Dichlorobenzene 4 05/03/23 13:24 V32788ANG
<13.4 mg/Kg - dry 13.4 45.41,4-Dichlorobenzene 4 05/03/23 13:24 V32788ANG
<20.2 mg/Kg - dry 20.2 90.83,3'-Dichlorobenzidine 4 05/03/23 13:24 V32788ANG
<13.2 mg/Kg - dry 13.2 90.82,4-Dichlorophenol 4 05/03/23 13:24 V32788ANG
<24.8 mg/Kg - dry 24.8 90.8Diethyl phthalate 4 05/03/23 13:24 V32788ANG
<24.0 mg/Kg - dry 24.0 90.8Dimethyl phthalate 4 05/03/23 13:24 V32788ANG
<14.9 mg/Kg - dry 14.9 45.42,4-Dimethylphenol 4 05/03/23 13:24 V32788ANG
<14.7 mg/Kg - dry 14.7 90.8Di-n-butyl phthalate 4 05/03/23 13:24 V32788ANG
<33.0 mg/Kg - dry 33.0 2064,6-Dinitro-2-methylphenol 4 05/03/23 13:24 V32788ANG
<71.6 mg/Kg - dry 71.6 2062,4-Dinitrophenol 4 05/03/23 13:24 V32788ANG
<13.3 mg/Kg - dry 13.3 90.82,4-Dinitrotoluene 4 05/03/23 13:24 V32788ANG
<14.9 mg/Kg - dry 14.9 90.82,6-Dinitrotoluene 4 05/03/23 13:24 V32788ANG
<19.7 mg/Kg - dry 19.7 45.4Di-n-Octyl Phthalate 4 05/03/23 13:24 V32788ANG
<17.0 mg/Kg - dry 17.0 90.8Fluoranthene 4 05/03/23 13:24 V32788ANG
<17.7 mg/Kg - dry 17.7 90.8Fluorene 4 05/03/23 13:24 V32788ANG
<14.6 mg/Kg - dry 14.6 90.8Hexachlorobenzene 4 05/03/23 13:24 V32788ANG
<13.4 mg/Kg - dry 13.4 90.8Hexachlorobutadiene 4 05/03/23 13:24 V32788ANG
<21.6 mg/Kg - dry 21.6 90.8Hexachlorocyclopentadiene 4 05/03/23 13:24 V32788ANG
<10.9 mg/Kg - dry 10.9 90.8Hexachloroethane 4 05/03/23 13:24 V32788ANG
<24.7 mg/Kg - dry 24.7 90.8Indeno(1,2,3-cd)pyrene 4 05/03/23 13:24 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 37 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp Dup
94906 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<26.3 mg/Kg - dry 26.3 90.8Isophorone 4 05/03/23 13:24 V32788ANG
<14.6 mg/Kg - dry 14.6 90.81-Methylnaphthalene 4 05/03/23 13:24 V32788ANG
<13.8 mg/Kg - dry 13.8 90.82-Methylnaphthalene 4 05/03/23 13:24 V32788ANG
<13.3 mg/Kg - dry 13.3 90.82-Methylphenol 4 05/03/23 13:24 V32788ANG
<11.7 mg/Kg - dry 11.7 90.83&4 Methylphenol 4 05/03/23 13:24 V32788ANG
<19.8 mg/Kg - dry 19.8 90.8Naphthalene 4 05/03/23 13:24 V32788ANG
<13.3 mg/Kg - dry 13.3 90.82-Nitroaniline 4 05/03/23 13:24 V32788ANG
<16.5 mg/Kg - dry 16.5 90.83-Nitroaniline 4 05/03/23 13:24 V32788ANG
<12.8 mg/Kg - dry 12.8 45.44-Nitroaniline 4 05/03/23 13:24 V32788ANG
<15.9 mg/Kg - dry 15.9 45.4Nitrobenzene 4 05/03/23 13:24 V32788ANG
<12.3 mg/Kg - dry 12.3 90.82-Nitrophenol 4 05/03/23 13:24 V32788ANG
<16.1 mg/Kg - dry 16.1 90.84-Nitrophenol 4 05/03/23 13:24 V32788ANG
<36.2 mg/Kg - dry 36.2 90.8N-Nitrosodimethylamine 4 05/03/23 13:24 V32788ANG
<24.9 mg/Kg - dry 24.9 90.8N-Nitrosodiphenylamine 4 05/03/23 13:24 V32788ANG
<16.3 mg/Kg - dry 16.3 90.8N-Nitroso-di-n-propylamine 4 05/03/23 13:24 V32788ANG
<47.7 mg/Kg - dry 47.7 138Pentachlorophenol 4 05/03/23 13:24 V32788ANG
<28.7 mg/Kg - dry 28.7 90.8Phenanthrene 4 05/03/23 13:24 V32788ANG
<15.4 mg/Kg - dry 15.4 90.8Phenol 4 05/03/23 13:24 V32788ANG
<18.5 mg/Kg - dry 18.5 90.8Pyrene 4 05/03/23 13:24 V32788ANG
<10.9 mg/Kg - dry 10.9 45.4Pyridine 4 05/03/23 13:24 V32788ANG
<14.7 mg/Kg - dry 14.7 90.81,2,4-Trichlorobenzene 4 05/03/23 13:24 V32788ANG
<13.2 mg/Kg - dry 13.2 90.82,4,5-Trichlorophenol 4 05/03/23 13:24 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 38 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-2 Comp Dup
94906 Matrix:
4/26/2023 9:00
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<13.3 mg/Kg - dry 13.3 90.82,4,6-Trichlorophenol 4 05/03/23 13:24 V32788ANG
8270ESurrogate: Phenol-d5 51.9 Limits: 34-121%05/03/23 13:244 ANG
Surrogate: 2-Fluorobiphenyl 62.6 Limits: 44-115%05/03/23 13:244 ANG V32788
Surrogate: 2-Fluorophenol 54.3 Limits: 35-115%05/03/23 13:244 ANG V32788
Surrogate: Nitrobenzene-d5 55.6 Limits: 37-122%05/03/23 13:244 ANG V32788
Surrogate: 4-Terphenyl-d14 69.0 Limits: 54-127%05/03/23 13:244 ANG V32788
Surrogate: 2,4,6-Tribromophenol 52.9 Limits: 39-132%05/03/23 13:244 ANG V32788
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 39 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3-3
94908 Matrix:
4/26/2023 9:14
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.9 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 40 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3-3
94908 Matrix:
4/26/2023 9:14
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
0.020 J mg/Kg - dry 0.002 0.023Acetone 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/01/23 14:01 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/01/23 14:01 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/01/23 14:01 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Carbon Disulfide 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/01/23 14:01 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/01/23 14:01 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/01/23 14:01 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Di-Isopropyl Ether (DIPE)1 05/01/23 14:01 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/01/23 14:01 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 41 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3-3
94908 Matrix:
4/26/2023 9:14
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 05/01/23 14:01 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/01/23 14:01 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/01/23 14:01 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/01/23 14:01 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,1-Dichloroethene 1 05/01/23 14:01 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/01/23 14:01 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/01/23 14:01 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/01/23 14:01 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/01/23 14:01 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/01/23 14:01 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/01/23 14:01 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/01/23 14:01 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/01/23 14:01 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 42 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3-3
94908 Matrix:
4/26/2023 9:14
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 05/01/23 14:01 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/01/23 14:01 V32647TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/01/23 14:01 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/01/23 14:01 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/01/23 14:01 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0111,2,4-Trichlorobenzene 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/01/23 14:01 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,1,2-Trichloroethane 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/01/23 14:01 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/01/23 14:01 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/01/23 14:01 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 05/01/23 14:01 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 43 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3-3
94908 Matrix:
4/26/2023 9:14
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/01/23 14:01 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/01/23 14:01 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/01/23 14:01 V32647
Surrogate: 4-Bromofluorobenzene 97.7 Limits: 70-130%05/01/23 14:011 TBL V32647
Surrogate: Dibromofluoromethane 101 Limits: 84-123%05/01/23 14:011 TBL V32647
Surrogate: Toluene-d8 87.4 Limits: 76-129%05/01/23 14:011 TBL V32647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 44 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3 Comp
94909 Matrix:
4/26/2023 9:40
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
12.2 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
12.4 mg/Kg - dry 0.0973 0.285Arsenic 5 05/03/23 15:00 6020BCPW
50.2 mg/Kg - dry 0.048 0.284Barium 5 05/03/23 15:00 6020BCPW
1.77 mg/Kg - dry 0.0294 0.285Cadmium 5 05/03/23 15:00 6020BCPW
39.3 mg/Kg - dry 0.132 0.284Chromium 5 05/03/23 15:00 6020BCPW
114 mg/Kg - dry 0.0353 0.285Lead 5 05/03/23 15:00 6020BCPW
0.118 J mg/Kg - dry 0.0227 0.188Mercury (Total)1 05/04/23 13:09 7471AFDS
1.10 mg/Kg - dry 0.117 0.284Selenium 5 05/03/23 15:00 6020BCPW
0.0812 J mg/Kg - dry 0.0076 0.285Silver 5 05/03/23 15:00 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 45 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3 Comp
94909 Matrix:
4/26/2023 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<15.8 mg/Kg - dry 15.8 90.2Acenaphthene 4 05/03/23 13:47 V32788ANG
<14.4 mg/Kg - dry 14.4 90.2Acenaphthylene 4 05/03/23 13:47 V32788ANG
<20.7 mg/Kg - dry 20.7 90.2Aniline 4 05/03/23 13:47 V32788ANG
<19.6 mg/Kg - dry 19.6 90.2Anthracene 4 05/03/23 13:47 V32788ANG
<19.0 mg/Kg - dry 19.0 90.2Benzo(a)anthracene 4 05/03/23 13:47 V32788ANG
<20.0 mg/Kg - dry 20.0 90.2Benzo(a)pyrene 4 05/03/23 13:47 V32788ANG
<19.9 mg/Kg - dry 19.9 90.2Benzo(b)fluoranthene 4 05/03/23 13:47 V32788ANG
<18.6 mg/Kg - dry 18.6 90.2Benzo(g,h,i)perylene 4 05/03/23 13:47 V32788ANG
<18.7 mg/Kg - dry 18.7 90.2Benzo(k)fluoranthene 4 05/03/23 13:47 V32788ANG
<79.3 mg/Kg - dry 79.3 273Benzoic Acid 4 05/03/23 13:47 V32788ANG
<14.4 mg/Kg - dry 14.4 90.2Benzyl alcohol 4 05/03/23 13:47 V32788ANG
<16.2 mg/Kg - dry 16.2 90.2Bis(2-Chloroethoxy)methane 4 05/03/23 13:47 V32788ANG
<14.6 mg/Kg - dry 14.6 90.2Bis(2-Chloroethyl)ether 4 05/03/23 13:47 V32788ANG
<18.6 mg/Kg - dry 18.6 45.1Bis(2-Chloroisopropyl)ether 4 05/03/23 13:47 V32788ANG
<16.4 mg/Kg - dry 16.4 90.2Bis(2-ethylhexyl)phthalate 4 05/03/23 13:47 V32788ANG
<14.9 mg/Kg - dry 14.9 90.24-Bromophenyl phenyl ether 4 05/03/23 13:47 V32788ANG
<15.5 mg/Kg - dry 15.5 45.1Butyl benzyl phthalate 4 05/03/23 13:47 V32788ANG
<12.6 mg/Kg - dry 12.6 90.24-Chloro-3-methylphenol 4 05/03/23 13:47 V32788ANG
<15.3 mg/Kg - dry 15.3 45.14-Chloroaniline 4 05/03/23 13:47 V32788ANG
<15.8 mg/Kg - dry 15.8 90.22-Chloronaphthalene 4 05/03/23 13:47 V32788ANG
<13.4 mg/Kg - dry 13.4 90.22-Chlorophenol 4 05/03/23 13:47 V32788ANG
<17.2 mg/Kg - dry 17.2 1374-Chlorophenyl phenyl ether 4 05/03/23 13:47 V32788ANG
<19.4 mg/Kg - dry 19.4 90.2Chrysene 4 05/03/23 13:47 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 46 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3 Comp
94909 Matrix:
4/26/2023 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<31.4 mg/Kg - dry 31.4 90.2Dibenz(a,h)anthracene 4 05/03/23 13:47 V32788ANG
<16.3 mg/Kg - dry 16.3 90.2Dibenzofuran 4 05/03/23 13:47 V32788ANG
<12.9 mg/Kg - dry 12.9 90.21,2-Dichlorobenzene 4 05/03/23 13:47 V32788ANG
<13.3 mg/Kg - dry 13.3 90.21,3-Dichlorobenzene 4 05/03/23 13:47 V32788ANG
<13.3 mg/Kg - dry 13.3 45.11,4-Dichlorobenzene 4 05/03/23 13:47 V32788ANG
<20.0 mg/Kg - dry 20.0 90.23,3'-Dichlorobenzidine 4 05/03/23 13:47 V32788ANG
<13.1 mg/Kg - dry 13.1 90.22,4-Dichlorophenol 4 05/03/23 13:47 V32788ANG
<24.6 mg/Kg - dry 24.6 90.2Diethyl phthalate 4 05/03/23 13:47 V32788ANG
<23.8 mg/Kg - dry 23.8 90.2Dimethyl phthalate 4 05/03/23 13:47 V32788ANG
<14.8 mg/Kg - dry 14.8 45.12,4-Dimethylphenol 4 05/03/23 13:47 V32788ANG
<14.6 mg/Kg - dry 14.6 90.2Di-n-butyl phthalate 4 05/03/23 13:47 V32788ANG
<32.8 mg/Kg - dry 32.8 2054,6-Dinitro-2-methylphenol 4 05/03/23 13:47 V32788ANG
<71.1 mg/Kg - dry 71.1 2052,4-Dinitrophenol 4 05/03/23 13:47 V32788ANG
<13.2 mg/Kg - dry 13.2 90.22,4-Dinitrotoluene 4 05/03/23 13:47 V32788ANG
<14.8 mg/Kg - dry 14.8 90.22,6-Dinitrotoluene 4 05/03/23 13:47 V32788ANG
<19.6 mg/Kg - dry 19.6 45.1Di-n-Octyl Phthalate 4 05/03/23 13:47 V32788ANG
<16.9 mg/Kg - dry 16.9 90.2Fluoranthene 4 05/03/23 13:47 V32788ANG
<17.5 mg/Kg - dry 17.5 90.2Fluorene 4 05/03/23 13:47 V32788ANG
<14.5 mg/Kg - dry 14.5 90.2Hexachlorobenzene 4 05/03/23 13:47 V32788ANG
<13.3 mg/Kg - dry 13.3 90.2Hexachlorobutadiene 4 05/03/23 13:47 V32788ANG
<21.4 mg/Kg - dry 21.4 90.2Hexachlorocyclopentadiene 4 05/03/23 13:47 V32788ANG
<10.8 mg/Kg - dry 10.8 90.2Hexachloroethane 4 05/03/23 13:47 V32788ANG
<24.5 mg/Kg - dry 24.5 90.2Indeno(1,2,3-cd)pyrene 4 05/03/23 13:47 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 47 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3 Comp
94909 Matrix:
4/26/2023 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<26.1 mg/Kg - dry 26.1 90.2Isophorone 4 05/03/23 13:47 V32788ANG
<14.5 mg/Kg - dry 14.5 90.21-Methylnaphthalene 4 05/03/23 13:47 V32788ANG
<13.7 mg/Kg - dry 13.7 90.22-Methylnaphthalene 4 05/03/23 13:47 V32788ANG
<13.2 mg/Kg - dry 13.2 90.22-Methylphenol 4 05/03/23 13:47 V32788ANG
<11.6 mg/Kg - dry 11.6 90.23&4 Methylphenol 4 05/03/23 13:47 V32788ANG
<19.7 mg/Kg - dry 19.7 90.2Naphthalene 4 05/03/23 13:47 V32788ANG
<13.2 mg/Kg - dry 13.2 90.22-Nitroaniline 4 05/03/23 13:47 V32788ANG
<16.4 mg/Kg - dry 16.4 90.23-Nitroaniline 4 05/03/23 13:47 V32788ANG
<12.8 mg/Kg - dry 12.8 45.14-Nitroaniline 4 05/03/23 13:47 V32788ANG
<15.8 mg/Kg - dry 15.8 45.1Nitrobenzene 4 05/03/23 13:47 V32788ANG
<12.2 mg/Kg - dry 12.2 90.22-Nitrophenol 4 05/03/23 13:47 V32788ANG
<15.9 mg/Kg - dry 15.9 90.24-Nitrophenol 4 05/03/23 13:47 V32788ANG
<36.0 mg/Kg - dry 36.0 90.2N-Nitrosodimethylamine 4 05/03/23 13:47 V32788ANG
<24.7 mg/Kg - dry 24.7 90.2N-Nitrosodiphenylamine 4 05/03/23 13:47 V32788ANG
<16.2 mg/Kg - dry 16.2 90.2N-Nitroso-di-n-propylamine 4 05/03/23 13:47 V32788ANG
<47.4 mg/Kg - dry 47.4 137Pentachlorophenol 4 05/03/23 13:47 V32788ANG
<28.5 mg/Kg - dry 28.5 90.2Phenanthrene 4 05/03/23 13:47 V32788ANG
<15.3 mg/Kg - dry 15.3 90.2Phenol 4 05/03/23 13:47 V32788ANG
<18.3 mg/Kg - dry 18.3 90.2Pyrene 4 05/03/23 13:47 V32788ANG
<10.8 mg/Kg - dry 10.8 45.1Pyridine 4 05/03/23 13:47 V32788ANG
<14.6 mg/Kg - dry 14.6 90.21,2,4-Trichlorobenzene 4 05/03/23 13:47 V32788ANG
<13.1 mg/Kg - dry 13.1 90.22,4,5-Trichlorophenol 4 05/03/23 13:47 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 48 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SP-3 Comp
94909 Matrix:
4/26/2023 9:40
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<13.2 mg/Kg - dry 13.2 90.22,4,6-Trichlorophenol 4 05/03/23 13:47 V32788ANG
8270ESurrogate: Phenol-d5 56.1 Limits: 34-121%05/03/23 13:474 ANG
Surrogate: 2-Fluorobiphenyl 69.0 Limits: 44-115%05/03/23 13:474 ANG V32788
Surrogate: 2-Fluorophenol 60.4 Limits: 35-115%05/03/23 13:474 ANG V32788
Surrogate: Nitrobenzene-d5 62.6 Limits: 37-122%05/03/23 13:474 ANG V32788
Surrogate: 4-Terphenyl-d14 76.2 Limits: 54-127%05/03/23 13:474 ANG V32788
Surrogate: 2,4,6-Tribromophenol 60.9 Limits: 39-132%05/03/23 13:474 ANG V32788
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 49 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94911 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
5.00 µg/L 1.80 5.00Acetone 1 05/02/23 15:44 V32721MSA
<2.00 µg/L 2.00 5.00Acrolein 1 05/02/23 15:44 V32721MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 05/02/23 15:44 V32721MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/02/23 15:44 V32721MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/02/23 15:44 V32721MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/02/23 15:44 V32721MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/02/23 15:44 V32721MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/02/23 15:44 V32721MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/02/23 15:44 V32721MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 05/02/23 15:44 V32721MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/02/23 15:44 V32721MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/02/23 15:44 V32721MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 05/02/23 15:44 V32721MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/02/23 15:44 V32721MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/02/23 15:44 V32721MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/02/23 15:44 V32721MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/02/23 15:44 V32721MSA
<0.220 µg/L 0.220 0.500Chloroform 1 05/02/23 15:44 V32721MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/02/23 15:44 V32721MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/02/23 15:44 V32721MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/02/23 15:44 V32721MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 05/02/23 15:44 V32721MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/02/23 15:44 V32721MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 50 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94911 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/02/23 15:44 V32721MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/02/23 15:44 V32721MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/02/23 15:44 V32721MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/02/23 15:44 V32721MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/02/23 15:44 V32721MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/02/23 15:44 V32721MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/02/23 15:44 V32721MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/02/23 15:44 V32721MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/02/23 15:44 V32721MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/02/23 15:44 V32721MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/02/23 15:44 V32721MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/02/23 15:44 V32721MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/02/23 15:44 V32721MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/02/23 15:44 V32721MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/02/23 15:44 V32721MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/02/23 15:44 V32721MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/02/23 15:44 V32721MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/02/23 15:44 V32721MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 15:44 V32721MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 05/02/23 15:44 V32721MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 05/02/23 15:44 V32721MSA
<0.380 µg/L 0.380 5.002-Hexanone 1 05/02/23 15:44 V32721MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 05/02/23 15:44 V32721MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 51 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94911 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/02/23 15:44 V32721MSA
1.96 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/02/23 15:44 V32721MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 05/02/23 15:44 V32721MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 05/02/23 15:44 V32721MSA
0.562 J µg/L 0.330 1.00Methylene Chloride 1 05/02/23 15:44 V32721MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/02/23 15:44 V32721MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/02/23 15:44 V32721MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/02/23 15:44 V32721MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/02/23 15:44 V32721MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/02/23 15:44 V32721MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 05/02/23 15:44 V32721MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/02/23 15:44 V32721MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 05/02/23 15:44 V32721MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 05/02/23 15:44 V32721MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/02/23 15:44 V32721MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/02/23 15:44 V32721MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/02/23 15:44 V32721MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/02/23 15:44 V32721MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 05/02/23 15:44 V32721MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 05/02/23 15:44 V32721MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/02/23 15:44 V32721MSA
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 05/02/23 15:44 V32721MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/02/23 15:44 V32721MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 52 of 78
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0010
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Received : 04/27/2023
5 Points Gateway
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94911 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 05/02/23 15:44 V32721MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/02/23 15:44 V32721MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/02/23 15:44 V32721
Surrogate: 4-Bromofluorobenzene 102 Limits: 80-124%05/02/23 15:441 MSA V32721
Surrogate: Dibromofluoromethane 99.2 Limits: 75-129%05/02/23 15:441 MSA V32721
Surrogate: 1,2-Dichloroethane - d4 97.0 Limits: 63-136%05/02/23 15:441 MSA V32721
Surrogate: Toluene-d8 101 Limits: 77-123%05/02/23 15:441 MSA V32721
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 53 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Metals Analyses
6020B
L679823QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L679484
Associated Lab Samples: 94900, 94904, 94906, 94909
LRB-L679484 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/03/23 13:430.2500.0855<0.0855mg/KgArsenic
05/03/23 13:430.2500.042<0.042mg/KgBarium
05/03/23 13:430.2500.0259<0.0259mg/KgCadmium
05/03/23 13:430.2500.116<0.116mg/KgChromium
05/03/23 13:430.2500.0310<0.0310mg/KgLead
05/03/23 13:430.2500.103<0.103mg/KgSelenium
05/03/23 13:430.2500.0067<0.0067mg/KgSilver
LCS-L679484Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.02.362.50mg/KgArsenic 80-120
91.04.565.00mg/KgBarium 80-120
95.00.4770.500mg/KgCadmium 80-120
93.04.675.00mg/KgChromium 80-120
94.02.362.50mg/KgLead 80-120
93.04.645.00mg/KgSelenium 80-120
95.00.4730.500mg/KgSilver 80-120
V 95000-MS-L679484 V 95000-MSD-L679484Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
10.1 0.0*10.72.482.3810.1mg/KgArsenic 24.0*75-125 5.7 80
26.9 0.0*26.44.974.7633.0mg/KgBarium 0.0*75-125 1.8 80
0.520 71.0*0.6050.4970.4760.180mg/KgCadmium 86.0 75-125 15.1 80
30.1 0.0*31.64.974.7632.9mg/KgChromium 0.0*75-125 4.8 80
Page 1 of 23* QC Fail Date:05/05/2023 03:54 PM
Page 54 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Metals Analyses
6020B
L679823QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L679484
V 95000-MS-L679484 V 95000-MSD-L679484Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.5 0.0*14.02.482.3814.5mg/KgLead 0.0*75-125 11.3 80
4.54 65.0*4.924.974.761.43mg/KgSelenium 70.0*75-125 8.0 80
0.409 80.00.4730.4970.4760.0302mg/KgSilver 89.0 75-125 14.5 80
V 95000-PDS-L679484Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/03/23 15:2491.02.00mg/KgArsenic
05/03/23 15:2494.05.30mg/KgBarium
05/03/23 15:2493.00.237mg/KgCadmium
05/03/23 15:2490.05.08mg/KgChromium
05/03/23 15:2492.02.42mg/KgLead
05/03/23 15:2491.02.29mg/KgSelenium
05/03/23 15:2494.00.227mg/KgSilver
Page 2 of 23* QC Fail Date:05/05/2023 03:54 PM
Page 55 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471A
L680090QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471A
QC Prep:L679878
Associated Lab Samples: 94900
LRB-L679878 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/04/23 12:170.1920.0232<0.0232mg/KgMercury (Total)
LCS-L679878Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1120.4470.400mg/KgMercury (Total)80-120
V 94900-MS-L679878 V 94900-MSD-L679878Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.457 1000.4950.3950.3890.0664mg/KgMercury (Total)108 80-120 7.9 20
V 94900-PDS-L679878Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/04/23 12:5990.00.740mg/KgMercury (Total)
Page 3 of 23Date:05/05/2023 03:54 PM
Page 56 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471A
L680090QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471A
QC Prep:L679881
Associated Lab Samples: 94904, 94906, 94909
LRB-L679881 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/04/23 13:000.1920.0232<0.0232mg/KgMercury (Total)
LCS-L679881Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1110.4450.400mg/KgMercury (Total)80-120
L 84607-MS-L679881 L 84607-MSD-L679881Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.432 1100.5270.3990.391<0.0227mg/KgMercury (Total)132*80-120 19.8 20
L 84607-PDS-L679881Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/04/23 13:261090.804mg/KgMercury (Total)
Page 4 of 23* QC Fail Date:05/05/2023 03:54 PM
Page 57 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
Associated Lab Samples: 94899, 94902, 94903, 94908
LRB-V32646 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/01/23 10:510.0200.002<0.002mg/KgAcetone
05/01/23 10:510.0200.001<0.001mg/KgAcrolein
05/01/23 10:510.0200.0008<0.0008mg/KgAcrylonitrile
05/01/23 10:510.0050.0006<0.0006mg/KgBenzene
05/01/23 10:510.0050.0005<0.0005mg/KgBromobenzene
05/01/23 10:510.0050.0008<0.0008mg/KgBromochloromethane
05/01/23 10:510.0050.001<0.001mg/KgBromodichloromethane
05/01/23 10:510.0050.001<0.001mg/KgBromoform
05/01/23 10:510.0100.001<0.001mg/KgBromomethane
05/01/23 10:510.0050.0005<0.0005mg/Kgn-Butylbenzene
05/01/23 10:510.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/01/23 10:510.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/01/23 10:510.0050.0006<0.0006mg/KgCarbon Disulfide
05/01/23 10:510.0050.001<0.001mg/KgCarbon Tetrachloride
05/01/23 10:510.0050.0007<0.0007mg/KgChlorobenzene
05/01/23 10:510.0050.0009<0.0009mg/KgChlorodibromomethane
05/01/23 10:510.0100.0009<0.0009mg/KgChloroethane
05/01/23 10:510.0050.001<0.001mg/KgChloroform
05/01/23 10:510.0100.0006<0.0006mg/KgChloromethane
05/01/23 10:510.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/01/23 10:510.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/01/23 10:510.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/01/23 10:510.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/01/23 10:510.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/01/23 10:510.0050.0006<0.0006mg/KgDibromomethane
05/01/23 10:510.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/01/23 10:510.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 5 of 23Date:05/05/2023 03:54 PM
Page 58 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
Associated Lab Samples: 94899, 94902, 94903, 94908
LRB-V32646 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/01/23 10:510.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/01/23 10:510.0100.001<0.001mg/KgDichlorodifluoromethane
05/01/23 10:510.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/01/23 10:510.0050.001<0.001mg/Kg1,2-Dichloroethane
05/01/23 10:510.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/01/23 10:510.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/01/23 10:510.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/01/23 10:510.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/01/23 10:510.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/01/23 10:510.0050.001<0.001mg/Kg2,2-Dichloropropane
05/01/23 10:510.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/01/23 10:510.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/01/23 10:510.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/01/23 10:510.0050.0006<0.0006mg/KgEthylbenzene
05/01/23 10:510.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/01/23 10:510.0100.0008<0.0008mg/KgHexachlorobutadiene
05/01/23 10:510.0100.0007<0.0007mg/Kgn-Hexane
05/01/23 10:510.0200.0006<0.0006mg/Kg2-Hexanone
05/01/23 10:510.0050.0005<0.0005mg/KgIsopropylbenzene
05/01/23 10:510.0050.001<0.001mg/Kg4-Isopropyl toluene
05/01/23 10:510.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/01/23 10:510.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/01/23 10:510.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/01/23 10:510.0100.001<0.001mg/KgMethylene Chloride
05/01/23 10:510.0100.0010<0.0010mg/KgNaphthalene
05/01/23 10:510.0050.0005<0.0005mg/Kgn-Propylbenzene
05/01/23 10:510.0050.001<0.001mg/KgStyrene
Page 6 of 23Date:05/05/2023 03:54 PM
Page 59 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
Associated Lab Samples: 94899, 94902, 94903, 94908
LRB-V32646 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/01/23 10:510.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/01/23 10:510.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/01/23 10:510.0050.0009<0.0009mg/KgTetrachloroethene
05/01/23 10:510.0050.0007<0.0007mg/KgToluene
05/01/23 10:510.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/01/23 10:510.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/01/23 10:510.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/01/23 10:510.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/01/23 10:510.0050.0009<0.0009mg/KgTrichloroethene
05/01/23 10:510.0100.002<0.002mg/KgTrichlorofluoromethane
05/01/23 10:510.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/01/23 10:510.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/01/23 10:510.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/01/23 10:510.0100.0005<0.0005mg/KgVinyl Acetate
05/01/23 10:510.0100.0005<0.0005mg/KgVinyl Chloride
05/01/23 10:510.0050.0005<0.0005mg/Kgo-Xylene
05/01/23 10:510.0100.001<0.001mg/Kgm,p-Xylene
05/01/23 10:514-Bromofluorobenzene (S)99.8 70-130
05/01/23 10:51Dibromofluoromethane (S)97.8 84-123
05/01/23 10:51Toluene-d8 (S)91.0 76-129
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.119 1191120.1120.100mg/KgAcetone 29-198 6.0 20
0.079 79.376.60.0760.100mg/KgAcrolein 70-130 3.4 20
Page 7 of 23Date:05/05/2023 03:54 PM
Page 60 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.895.00.0950.100mg/KgAcrylonitrile 65-134 2.9 20
0.049 98.01020.0510.050mg/KgBenzene 74-127 4.0 20
0.042 84.61140.0560.050mg/KgBromobenzene 73-125 29.2*20
0.055 1101110.0550.050mg/KgBromochloromethane 72-134 0.9 20
0.053 1061080.0540.050mg/KgBromodichloromethane 75-122 1.8 20
0.052 1051040.0520.050mg/KgBromoform 66-135 0.5 20
0.037 74.878.00.0390.050mg/KgBromomethane 20-180 4.1 20
0.043 86.21160.0580.050mg/Kgn-Butylbenzene 65-135 29.8*20
0.043 86.475.20.0370.050mg/Kgsec-Butyl benzene 66-131 13.8 20
0.042 85.61070.0530.050mg/Kgtert-Butyl benzene 67-132 22.0*20
0.045 90.497.80.0480.050mg/KgCarbon Disulfide 61-129 7.8 20
0.052 1041090.0540.050mg/KgCarbon Tetrachloride 64-143 4.3 20
0.048 97.899.60.0490.050mg/KgChlorobenzene 74-118 1.8 20
0.050 10199.40.0490.050mg/KgChlorodibromomethane 73-122 1.9 20
0.029 58.684.20.0420.050mg/KgChloroethane 33-149 35.8*20
0.050 1011060.0530.050mg/KgChloroform 73-127 4.8 20
0.045 90.294.80.0470.050mg/KgChloromethane 45-143 4.9 20
0.043 86.21170.0580.050mg/Kg2-Chlorotoluene 67-124 29.9*20
0.043 86.21170.0580.050mg/Kg4-Chlorotoluene 71-126 29.9*20
0.049 98.61010.0500.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.8 20
0.051 1031230.0610.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 17.8 20
0.052 1051010.0500.050mg/Kg1,2-Dibromoethane 70-132 3.4 20
0.052 1051040.0510.050mg/KgDibromomethane 74-133 1.5 20
0.045 91.61180.0590.050mg/Kg1,2-Dichlorobenzene 72-123 25.5*20
0.046 92.481.00.0400.050mg/Kg1,3-Dichlorobenzene 71-120 13.1 20
0.044 89.496.80.0480.050mg/Kg1,4-Dichlorobenzene 71-123 7.9 20
Page 8 of 23* QC Fail Date:05/05/2023 03:54 PM
Page 61 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.290.80.0450.050mg/KgDichlorodifluoromethane 26-146 7.5 20
0.049 99.81030.0510.050mg/Kg1,1-Dichloroethane 74-127 3.5 20
0.050 1011020.0510.050mg/Kg1,2-Dichloroethane 68-128 1.3 20
0.047 94.61000.0500.050mg/Kg1,1-Dichloroethene 67-149 5.7 20
0.050 1001020.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 1.1 20
0.048 96.21040.0520.050mg/Kgtrans-1,2-Dichloroethene 73-132 7.9 20
0.050 1001010.0500.050mg/Kg1,2-Dichloropropane 73-130 1.3 20
0.049 98.497.80.0480.050mg/Kg1,3-Dichloropropane 75-124 0.6 20
0.051 1021030.0510.050mg/Kg2,2-Dichloropropane 50-142 0.9 20
0.050 1011050.0520.050mg/Kg1,1-Dichloropropene 71-130 3.7 20
0.054 1081080.0530.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20
0.054 1091110.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.8 20
0.046 92.895.80.0470.050mg/KgEthylbenzene 74-128 3.1 20
0.099 99.598.80.0980.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.7 20
0.046 92.8131*0.0650.050mg/KgHexachlorobutadiene 64-125 33.9*20
0.049 98.81060.0530.050mg/Kgn-Hexane 70-130 7.4 20
0.049 98.693.40.0460.050mg/Kg2-Hexanone 61-157 5.4 20
0.043 87.21160.0580.050mg/KgIsopropylbenzene 68-126 28.6*20
0.044 88.075.20.0370.050mg/Kg4-Isopropyl toluene 68-129 15.6 20
0.039 79.671.60.0350.050mg/KgMethyl Ethyl Ketone (MEK)63-149 10.5 20
0.049 99.41010.0500.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.5 20
0.054 1101060.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 3.7 20
0.042 85.885.40.0420.050mg/KgMethylene Chloride 74-129 0.4 20
0.047 94.61170.0580.050mg/KgNaphthalene 57-157 21.1*20
0.041 83.41160.0580.050mg/Kgn-Propylbenzene 67-130 33.0*20
0.049 98.499.20.0490.050mg/KgStyrene 77-121 0.8 20
Page 9 of 23* QC Fail Date:05/05/2023 03:54 PM
Page 62 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1011010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.3 20
0.040 80.21120.0560.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 33.0*20
0.053 1061070.0530.050mg/KgTetrachloroethene 68-130 1.1 20
0.049 98.81040.0520.050mg/KgToluene 71-129 5.1 20
0.048 96.81230.0610.050mg/Kg1,2,3-Trichlorobenzene 68-130 24.1*20
0.048 97.8128*0.0630.050mg/Kg1,2,4-Trichlorobenzene 66-125 26.5*20
0.050 1011050.0520.050mg/Kg1,1,1-Trichloroethane 67-131 4.2 20
0.049 98.697.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 1.0 20
0.052 1051070.0530.050mg/KgTrichloroethene 75-133 1.6 20
0.030 61.472.00.0360.050mg/KgTrichlorofluoromethane 44-146 15.8 20
0.047 95.01180.0590.050mg/Kg1,2,3-Trichloropropane 60-137 21.5*20
0.044 88.273.40.0360.050mg/Kg1,2,4-Trimethylbenzene 69-129 18.3 20
0.043 86.41160.0580.050mg/Kg1,3,5-Trimethylbenzene 69-128 29.5*20
0.045 91.090.20.0450.050mg/KgVinyl Acetate 60-140 0.8 20
0.046 93.697.40.0480.050mg/KgVinyl Chloride 48-147 3.9 20
0.046 92.695.20.0470.050mg/Kgo-Xylene 74-126 2.7 20
0.096 96.099.30.0990.100mg/Kgm,p-Xylene 75-124 3.3 20
1011074-Bromofluorobenzene (S)70-130
96.495.6Dibromofluoromethane (S)84-123
91.891.0Toluene-d8 (S)76-129
Page 10 of 23* QC Fail Date:05/05/2023 03:54 PM
Page 63 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
Associated Lab Samples: 94911
LRB-V32720 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 14:225.001.80<1.80µg/LAcetone
05/02/23 14:225.002.00<2.00µg/LAcrolein
05/02/23 14:225.000.230<0.230µg/LAcrylonitrile
05/02/23 14:220.5000.180<0.180µg/LBenzene
05/02/23 14:220.5000.210<0.210µg/LBromobenzene
05/02/23 14:221.000.420<0.420µg/LBromochloromethane
05/02/23 14:220.5000.160<0.160µg/LBromodichloromethane
05/02/23 14:225.001.50<1.50µg/LBromoform
05/02/23 14:221.000.280<0.280µg/LBromomethane
05/02/23 14:221.000.185<0.185µg/Ln-Butylbenzene
05/02/23 14:220.5000.200<0.200µg/Lsec-Butyl benzene
05/02/23 14:222.000.920<0.920µg/Ltert-Butyl benzene
05/02/23 14:225.000.150<0.150µg/LCarbon Disulfide
05/02/23 14:220.5000.180<0.180µg/LCarbon Tetrachloride
05/02/23 14:220.5000.190<0.190µg/LChlorobenzene
05/02/23 14:220.5000.190<0.190µg/LChlorodibromomethane
05/02/23 14:221.000.430<0.430µg/LChloroethane
05/02/23 14:220.5000.220<0.220µg/LChloroform
05/02/23 14:220.5000.220<0.220µg/LChloromethane
05/02/23 14:220.5000.200<0.200µg/L2-Chlorotoluene
05/02/23 14:220.5000.200<0.200µg/L4-Chlorotoluene
05/02/23 14:225.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
05/02/23 14:222.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
05/02/23 14:220.5000.200<0.200µg/L1,2-Dibromoethane
05/02/23 14:220.5000.230<0.230µg/LDibromomethane
05/02/23 14:220.5000.220<0.220µg/L1,2-Dichlorobenzene
05/02/23 14:220.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 11 of 23Date:05/05/2023 03:54 PM
Page 64 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
Associated Lab Samples: 94911
LRB-V32720 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 14:220.5000.210<0.210µg/L1,4-Dichlorobenzene
05/02/23 14:225.001.20<1.20µg/LDichlorodifluoromethane
05/02/23 14:220.5000.240<0.240µg/L1,1-Dichloroethane
05/02/23 14:220.5000.150<0.150µg/L1,2-Dichloroethane
05/02/23 14:220.5000.150<0.150µg/L1,1-Dichloroethene
05/02/23 14:220.5000.200<0.200µg/Lcis-1,2-Dichloroethene
05/02/23 14:220.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
05/02/23 14:220.5000.190<0.190µg/L1,2-Dichloropropane
05/02/23 14:220.5000.130<0.130µg/L1,3-Dichloropropane
05/02/23 14:222.000.210<0.210µg/L2,2-Dichloropropane
05/02/23 14:220.5000.200<0.200µg/L1,1-Dichloropropene
05/02/23 14:220.5000.210<0.210µg/Lcis-1,3-Dichloropropene
05/02/23 14:220.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
05/02/23 14:220.5000.170<0.170µg/LEthylbenzene
05/02/23 14:2210.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
05/02/23 14:222.000.350<0.350µg/LHexachlorobutadiene
05/02/23 14:2210.01.30<1.30µg/Ln-Hexane
05/02/23 14:225.000.380<0.380µg/L2-Hexanone
05/02/23 14:225.000.180<0.180µg/LIsopropylbenzene
05/02/23 14:220.5000.089<0.089µg/L4-Isopropyl toluene
05/02/23 14:225.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
05/02/23 14:220.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
05/02/23 14:225.001.00<1.00µg/L4-Methyl-2-Pentanone
05/02/23 14:221.000.330<0.330µg/LMethylene Chloride
05/02/23 14:221.000.470<0.470µg/LNaphthalene
05/02/23 14:220.5000.190<0.190µg/Ln-Propylbenzene
05/02/23 14:220.5000.220<0.220µg/LStyrene
Page 12 of 23Date:05/05/2023 03:54 PM
Page 65 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
Associated Lab Samples: 94911
LRB-V32720 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 14:220.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
05/02/23 14:220.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
05/02/23 14:220.5000.220<0.220µg/LTetrachloroethene
05/02/23 14:220.5000.220<0.220µg/LToluene
05/02/23 14:222.000.380<0.380µg/L1,2,3-Trichlorobenzene
05/02/23 14:221.000.310<0.310µg/L1,2,4-Trichlorobenzene
05/02/23 14:220.5000.160<0.160µg/L1,1,1-Trichloroethane
05/02/23 14:220.5000.096<0.096µg/L1,1,2-Trichloroethane
05/02/23 14:220.5000.180<0.180µg/LTrichloroethene
05/02/23 14:220.5000.180<0.180µg/LTrichlorofluoromethane
05/02/23 14:221.000.270<0.270µg/L1,2,3-Trichloropropane
05/02/23 14:220.5000.190<0.190µg/L1,2,4-Trimethylbenzene
05/02/23 14:220.5000.180<0.180µg/L1,3,5-Trimethylbenzene
05/02/23 14:222.001.00<1.00µg/LVinyl Acetate
05/02/23 14:220.5000.170<0.170µg/LVinyl Chloride
05/02/23 14:220.5000.210<0.210µg/Lo-Xylene
05/02/23 14:221.000.420<0.420µg/Lm,p-Xylene
05/02/23 14:224-Bromofluorobenzene (S)102 80-124
05/02/23 14:22Dibromofluoromethane (S)100 75-129
05/02/23 14:221,2-Dichloroethane - d4 (S)99.6 63-136
05/02/23 14:22Toluene-d8 (S)99.8 77-123
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
35.3 88.289.735.940.0µg/LAcetone 40-166 1.6 20.0
Page 13 of 23Date:05/05/2023 03:54 PM
Page 66 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.1 92.796.038.440.0µg/LAcrolein 70-130 3.4 20.0
41.5 10410441.440.0µg/LAcrylonitrile 81-127 0.2 20.0
20.0 10010020.020.0µg/LBenzene 77-128 0.0 20.0
19.9 99.510320.520.0µg/LBromobenzene 78-129 2.9 20.0
19.5 97.510320.520.0µg/LBromochloromethane 78-135 5.0 20.0
19.6 98.010320.620.0µg/LBromodichloromethane 76-138 4.9 20.0
19.5 97.593.518.720.0µg/LBromoform 71-135 4.1 20.0
19.7 98.599.519.920.0µg/LBromomethane 41-168 1.0 20.0
19.0 95.099.019.820.0µg/Ln-Butylbenzene 68-134 4.1 20.0
19.4 97.010020.020.0µg/Lsec-Butyl benzene 71-131 3.0 20.0
19.4 97.099.019.820.0µg/Ltert-Butyl benzene 70-132 2.0 20.0
18.6 93.094.518.920.0µg/LCarbon Disulfide 59-135 1.6 20.0
19.5 97.510420.820.0µg/LCarbon Tetrachloride 72-142 6.4 20.0
19.4 97.098.519.720.0µg/LChlorobenzene 78-119 1.5 20.0
20.4 10210220.420.0µg/LChlorodibromomethane 75-134 0.0 20.0
21.8 10910621.220.0µg/LChloroethane 57-142 2.7 20.0
19.7 98.510120.220.0µg/LChloroform 77-130 2.5 20.0
19.8 99.099.019.820.0µg/LChloromethane 47-145 0.0 20.0
19.6 98.010220.420.0µg/L2-Chlorotoluene 74-126 4.0 20.0
19.8 99.010220.320.0µg/L4-Chlorotoluene 78-129 2.4 20.0
19.1 95.598.519.720.0µg/LDi-Isopropyl Ether (DIPE)60-154 3.0 20.0
20.9 10598.019.620.0µg/L1,2-Dibromo-3-Chloropropane 63-134 6.4 20.0
20.2 10110120.220.0µg/L1,2-Dibromoethane 77-135 0.0 20.0
20.5 10310320.520.0µg/LDibromomethane 76-138 0.0 20.0
18.8 94.096.019.220.0µg/L1,2-Dichlorobenzene 78-128 2.1 20.0
19.9 99.510120.120.0µg/L1,3-Dichlorobenzene 77-125 1.0 20.0
Page 14 of 23Date:05/05/2023 03:54 PM
Page 67 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.3 96.596.019.220.0µg/L1,4-Dichlorobenzene 75-126 0.5 20.0
19.0 95.098.019.620.0µg/LDichlorodifluoromethane 28-163 3.1 20.0
19.8 99.010320.520.0µg/L1,1-Dichloroethane 70-130 3.4 20.0
18.6 93.097.519.520.0µg/L1,2-Dichloroethane 68-131 4.7 20.0
21.0 10510621.120.0µg/L1,1-Dichloroethene 70-154 0.4 20.0
20.0 10010020.020.0µg/Lcis-1,2-Dichloroethene 76-141 0.0 20.0
20.8 10410420.820.0µg/Ltrans-1,2-Dichloroethene 76-135 0.0 20.0
19.4 97.099.019.820.0µg/L1,2-Dichloropropane 77-130 2.0 20.0
18.7 93.596.019.220.0µg/L1,3-Dichloropropane 76-132 2.6 20.0
20.4 10299.519.920.0µg/L2,2-Dichloropropane 29-149 2.4 20.0
21.6 10810721.420.0µg/L1,1-Dichloropropene 71-136 0.9 20.0
19.7 98.510220.420.0µg/Lcis-1,3-Dichloropropene 65-140 3.4 20.0
19.2 96.096.019.220.0µg/Ltrans-1,3-Dichloropropene 67-140 0.0 20.0
19.7 98.599.519.920.0µg/LEthylbenzene 80-127 1.0 20.0
39.7 99.210240.640.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 2.2 20.0
18.1 90.598.019.620.0µg/LHexachlorobutadiene 61-134 7.9 20.0
21.2 10610220.420.0µg/Ln-Hexane 70-130 3.8 20.0
18.4 92.090.018.020.0µg/L2-Hexanone 64-137 2.1 20.0
20.6 10310420.820.0µg/LIsopropylbenzene 70-130 0.9 20.0
20.2 10110320.620.0µg/L4-Isopropyl toluene 69-132 1.9 20.0
17.1 85.588.017.620.0µg/LMethyl Ethyl Ketone (MEK)71-134 2.8 20.0
19.8 99.099.019.820.0µg/LMethyl tert-butyl ether (MTBE)68-135 0.0 20.0
18.0 90.090.018.020.0µg/L4-Methyl-2-Pentanone 69-134 0.0 20.0
20.6 10310020.020.0µg/LMethylene Chloride 73-131 2.9 20.0
16.8 84.080.016.020.0µg/LNaphthalene 64-136 4.8 20.0
19.6 98.010020.020.0µg/Ln-Propylbenzene 72-132 2.0 20.0
Page 15 of 23Date:05/05/2023 03:54 PM
Page 68 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.9 99.510220.420.0µg/LStyrene 78-129 2.4 20.0
19.6 98.099.519.920.0µg/L1,1,1,2-Tetrachloroethane 79-134 1.5 20.0
20.7 10410120.220.0µg/L1,1,2,2-Tetrachloroethane 62-127 2.4 20.0
19.8 99.010320.620.0µg/LTetrachloroethene 80-129 3.9 20.0
19.8 99.010220.420.0µg/LToluene 76-131 2.9 20.0
21.2 10697.519.520.0µg/L1,2,3-Trichlorobenzene 58-144 8.3 20.0
18.7 93.596.019.220.0µg/L1,2,4-Trichlorobenzene 66-139 2.6 20.0
19.7 98.510020.020.0µg/L1,1,1-Trichloroethane 75-135 1.5 20.0
19.6 98.010120.220.0µg/L1,1,2-Trichloroethane 70-140 3.0 20.0
20.2 10110320.620.0µg/LTrichloroethene 77-133 1.9 20.0
19.2 96.098.519.720.0µg/LTrichlorofluoromethane 62-148 2.5 20.0
19.6 98.099.519.920.0µg/L1,2,3-Trichloropropane 71-127 1.5 20.0
19.6 98.010120.220.0µg/L1,2,4-Trimethylbenzene 75-133 3.0 20.0
19.7 98.510120.120.0µg/L1,3,5-Trimethylbenzene 75-131 2.0 20.0
20.5 10310521.020.0µg/LVinyl Acetate 34-167 2.4 20.0
20.2 10110721.320.0µg/LVinyl Chloride 57-141 5.3 20.0
18.9 94.597.519.520.0µg/Lo-Xylene 78-128 3.1 20.0
40.0 10010140.540.0µg/Lm,p-Xylene 77-133 1.2 20.0
1001024-Bromofluorobenzene (S)80-124
99.498.8Dibromofluoromethane (S)75-129
98.698.61,2-Dichloroethane - d4 (S)63-136
100101Toluene-d8 (S)77-123
Page 16 of 23Date:05/05/2023 03:54 PM
Page 69 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
Associated Lab Samples: 94900, 94904, 94906, 94909
LRB-V32670 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/23 10:2419.83.48<3.48mg/KgAcenaphthene
05/03/23 10:2419.83.15<3.15mg/KgAcenaphthylene
05/03/23 10:2419.84.56<4.56mg/KgAniline
05/03/23 10:2419.84.29<4.29mg/KgAnthracene
05/03/23 10:2419.84.17<4.17mg/KgBenzo(a)anthracene
05/03/23 10:2419.84.41<4.41mg/KgBenzo(a)pyrene
05/03/23 10:2419.84.38<4.38mg/KgBenzo(b)fluoranthene
05/03/23 10:2419.84.08<4.08mg/KgBenzo(g,h,i)perylene
05/03/23 10:2419.84.11<4.11mg/KgBenzo(k)fluoranthene
05/03/23 10:2460.017.4<17.4mg/KgBenzoic Acid
05/03/23 10:2419.83.15<3.15mg/KgBenzyl alcohol
05/03/23 10:2419.83.54<3.54mg/KgBis(2-Chloroethoxy)methane
05/03/23 10:2419.83.21<3.21mg/KgBis(2-Chloroethyl)ether
05/03/23 10:249.904.08<4.08mg/KgBis(2-Chloroisopropyl)ether
05/03/23 10:2419.83.60<3.60mg/KgBis(2-ethylhexyl)phthalate
05/03/23 10:2419.83.27<3.27mg/Kg4-Bromophenyl phenyl ether
05/03/23 10:249.903.39<3.39mg/KgButyl benzyl phthalate
05/03/23 10:2419.82.77<2.77mg/Kg4-Chloro-3-methylphenol
05/03/23 10:249.903.36<3.36mg/Kg4-Chloroaniline
05/03/23 10:2419.83.48<3.48mg/Kg2-Chloronaphthalene
05/03/23 10:2419.82.95<2.95mg/Kg2-Chlorophenol
05/03/23 10:2430.03.78<3.78mg/Kg4-Chlorophenyl phenyl ether
05/03/23 10:2419.84.26<4.26mg/KgChrysene
05/03/23 10:2419.86.90<6.90mg/KgDibenz(a,h)anthracene
05/03/23 10:2419.83.57<3.57mg/KgDibenzofuran
05/03/23 10:2419.82.83<2.83mg/Kg1,2-Dichlorobenzene
05/03/23 10:2419.82.92<2.92mg/Kg1,3-Dichlorobenzene
Page 17 of 23Date:05/05/2023 03:54 PM
Page 70 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
Associated Lab Samples: 94900, 94904, 94906, 94909
LRB-V32670 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/23 10:249.902.93<2.93mg/Kg1,4-Dichlorobenzene
05/03/23 10:2419.84.41<4.41mg/Kg3,3'-Dichlorobenzidine
05/03/23 10:2419.82.87<2.87mg/Kg2,4-Dichlorophenol
05/03/23 10:2419.85.40<5.40mg/KgDiethyl phthalate
05/03/23 10:2419.85.22<5.22mg/KgDimethyl phthalate
05/03/23 10:249.903.24<3.24mg/Kg2,4-Dimethylphenol
05/03/23 10:2419.83.21<3.21mg/KgDi-n-butyl phthalate
05/03/23 10:2445.07.20<7.20mg/Kg4,6-Dinitro-2-methylphenol
05/03/23 10:2445.015.6<15.6mg/Kg2,4-Dinitrophenol
05/03/23 10:2419.82.90<2.90mg/Kg2,4-Dinitrotoluene
05/03/23 10:2419.83.24<3.24mg/Kg2,6-Dinitrotoluene
05/03/23 10:249.904.29<4.29mg/KgDi-n-Octyl Phthalate
05/03/23 10:2419.83.69<3.69mg/KgFluoranthene
05/03/23 10:2419.83.84<3.84mg/KgFluorene
05/03/23 10:2419.83.18<3.18mg/KgHexachlorobenzene
05/03/23 10:2419.82.93<2.93mg/KgHexachlorobutadiene
05/03/23 10:2419.84.71<4.71mg/KgHexachlorocyclopentadiene
05/03/23 10:2419.82.38<2.38mg/KgHexachloroethane
05/03/23 10:2419.85.37<5.37mg/KgIndeno(1,2,3-cd)pyrene
05/03/23 10:2419.85.73<5.73mg/KgIsophorone
05/03/23 10:2419.83.18<3.18mg/Kg1-Methylnaphthalene
05/03/23 10:2419.83.00<3.00mg/Kg2-Methylnaphthalene
05/03/23 10:2419.82.91<2.91mg/Kg2-Methylphenol
05/03/23 10:2419.82.55<2.55mg/Kg3&4 Methylphenol
05/03/23 10:2419.84.32<4.32mg/KgNaphthalene
05/03/23 10:2419.82.90<2.90mg/Kg2-Nitroaniline
05/03/23 10:2419.83.60<3.60mg/Kg3-Nitroaniline
Page 18 of 23Date:05/05/2023 03:54 PM
Page 71 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
Associated Lab Samples: 94900, 94904, 94906, 94909
LRB-V32670 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/23 10:249.902.80<2.80mg/Kg4-Nitroaniline
05/03/23 10:249.903.48<3.48mg/KgNitrobenzene
05/03/23 10:2419.82.66<2.66mg/Kg2-Nitrophenol
05/03/23 10:2419.83.51<3.51mg/Kg4-Nitrophenol
05/03/23 10:2419.87.89<7.89mg/KgN-Nitrosodimethylamine
05/03/23 10:2419.85.43<5.43mg/KgN-Nitrosodiphenylamine
05/03/23 10:2419.83.54<3.54mg/KgN-Nitroso-di-n-propylamine
05/03/23 10:2430.010.4<10.4mg/KgPentachlorophenol
05/03/23 10:2419.86.24<6.24mg/KgPhenanthrene
05/03/23 10:2419.83.36<3.36mg/KgPhenol
05/03/23 10:2419.84.02<4.02mg/KgPyrene
05/03/23 10:249.902.38<2.38mg/KgPyridine
05/03/23 10:2419.83.21<3.21mg/Kg1,2,4-Trichlorobenzene
05/03/23 10:2419.82.89<2.89mg/Kg2,4,5-Trichlorophenol
05/03/23 10:2419.82.90<2.90mg/Kg2,4,6-Trichlorophenol
05/03/23 10:242-Fluorobiphenyl (S)73.4 44-115
05/03/23 10:242-Fluorophenol (S)64.4 35-115
05/03/23 10:24Nitrobenzene-d5 (S)69.8 37-122
05/03/23 10:244-Terphenyl-d14 (S)81.4 54-127
05/03/23 10:242,4,6-Tribromophenol (S)64.3 39-132
05/03/23 10:24Phenol-d5 (S)62.0 34-121
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.5 73.074.837.450.0mg/KgAcenaphthene 40-123 2.4 20
Page 19 of 23Date:05/05/2023 03:54 PM
Page 72 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.8 75.676.838.450.0mg/KgAcenaphthylene 32-132 1.5 20
55.4 11111456.850.0mg/KgAniline 12-197 2.4 20
39.3 78.682.841.450.0mg/KgAnthracene 47-123 5.2 20
41.4 82.883.441.750.0mg/KgBenzo(a)anthracene 49-126 0.7 20
44.5 89.091.445.750.0mg/KgBenzo(a)pyrene 45-129 2.6 20
52.0 10410552.750.0mg/KgBenzo(b)fluoranthene 45-132 1.3 20
57.1 11411557.350.0mg/KgBenzo(g,h,i)perylene 43-134 0.3 20
45.7 91.492.646.350.0mg/KgBenzo(k)fluoranthene 47-132 1.3 20
35.2 70.478.439.250.0mg/KgBenzoic Acid 10-83 10.7 20
39.9 79.884.642.350.0mg/KgBenzyl alcohol 29-122 5.8 20
37.5 75.079.639.850.0mg/KgBis(2-Chloroethoxy)methane 36-121 5.9 20
32.4 64.869.834.950.0mg/KgBis(2-Chloroethyl)ether 31-120 7.4 20
37.4 74.880.040.050.0mg/KgBis(2-Chloroisopropyl)ether 33-131 6.7 20
47.7 95.495.847.950.0mg/KgBis(2-ethylhexyl)phthalate 51-133 0.4 20
38.5 77.079.239.650.0mg/Kg4-Bromophenyl phenyl ether 46-124 2.8 20
46.7 93.494.047.050.0mg/KgButyl benzyl phthalate 48-132 0.6 20
39.7 79.480.440.250.0mg/Kg4-Chloro-3-methylphenol 45-122 1.2 20
36.4 72.869.634.850.0mg/Kg4-Chloroaniline 17-106 4.4 20
36.2 72.475.437.750.0mg/Kg2-Chloronaphthalene 41-114 4.0 20
36.2 72.477.838.950.0mg/Kg2-Chlorophenol 34-121 7.1 20
39.3 78.681.040.550.0mg/Kg4-Chlorophenyl phenyl ether 45-121 3.0 20
38.5 77.077.238.650.0mg/KgChrysene 50-124 0.2 20
55.9 11211054.850.0mg/KgDibenz(a,h)anthracene 45-134 1.9 20
36.8 73.675.237.650.0mg/KgDibenzofuran 44-120 2.1 20
31.4 62.869.034.550.0mg/Kg1,2-Dichlorobenzene 33-117 9.4 20
30.4 60.866.633.350.0mg/Kg1,3-Dichlorobenzene 30-115 9.1 20
Page 20 of 23Date:05/05/2023 03:54 PM
Page 73 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
30.0 60.066.633.350.0mg/Kg1,4-Dichlorobenzene 31-115 10.4 20
38.5 77.071.035.550.0mg/Kg3,3'-Dichlorobenzidine 22-121 8.1 20
38.8 77.679.239.650.0mg/Kg2,4-Dichlorophenol 40-122 2.0 20
40.9 81.883.041.550.0mg/KgDiethyl phthalate 50-124 1.4 20
40.1 80.280.440.250.0mg/KgDimethyl phthalate 48-124 0.2 20
49.2 98.410351.450.0mg/Kg2,4-Dimethylphenol 30-127 4.3 20
46.3 92.694.247.150.0mg/KgDi-n-butyl phthalate 51-128 1.7 20
39.0 78.079.039.550.0mg/Kg4,6-Dinitro-2-methylphenol 29-132 1.2 20
49.6 99.297.048.550.0mg/Kg2,4-Dinitrophenol 27-129 2.2 20
43.3 86.686.643.350.0mg/Kg2,4-Dinitrotoluene 48-126 0.0 20
42.1 84.283.841.950.0mg/Kg2,6-Dinitrotoluene 46-124 0.4 20
66.6 13313467.050.0mg/KgDi-n-Octyl Phthalate 45-140 0.5 20
38.9 77.878.239.150.0mg/KgFluoranthene 50-127 0.5 20
38.6 77.278.439.250.0mg/KgFluorene 43-125 1.5 20
36.8 73.674.437.250.0mg/KgHexachlorobenzene 45-122 1.0 20
32.9 65.870.635.350.0mg/KgHexachlorobutadiene 32-123 7.0 20
35.0 70.072.236.150.0mg/KgHexachlorocyclopentadiene 32-117 3.0 20
30.8 61.667.233.650.0mg/KgHexachloroethane 28-117 8.6 20
61.7 12311959.650.0mg/KgIndeno(1,2,3-cd)pyrene 45-133 3.4 20
33.8 67.669.634.850.0mg/KgIsophorone 30-122 2.9 20
33.7 67.470.835.450.0mg/Kg1-Methylnaphthalene 40-119 4.9 20
34.1 68.272.036.050.0mg/Kg2-Methylnaphthalene 38-122 5.4 20
37.8 75.680.440.250.0mg/Kg2-Methylphenol 32-122 6.1 20
35.4 70.872.236.150.0mg/Kg3&4 Methylphenol 34-119 1.9 20
32.7 65.470.235.150.0mg/KgNaphthalene 35-123 7.0 20
44.7 89.489.644.850.0mg/Kg2-Nitroaniline 44-127 0.2 20
Page 21 of 23Date:05/05/2023 03:54 PM
Page 74 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.6 79.271.835.950.0mg/Kg3-Nitroaniline 33-119 9.8 20
40.4 80.878.439.250.0mg/Kg4-Nitroaniline 63-147 3.0 20
32.3 64.669.834.950.0mg/KgNitrobenzene 34-122 7.7 20
37.1 74.279.439.750.0mg/Kg2-Nitrophenol 36-123 6.7 20
42.5 85.086.043.050.0mg/Kg4-Nitrophenol 30-132 1.1 20
28.9 57.862.031.050.0mg/KgN-Nitrosodimethylamine 10-146 7.0 20
46.4 92.894.047.050.0mg/KgN-Nitrosodiphenylamine 38-127 1.2 20
37.4 74.879.639.850.0mg/KgN-Nitroso-di-n-propylamine 36-120 6.2 20
42.9 85.885.242.650.0mg/KgPentachlorophenol 25-133 0.7 20
38.4 76.878.439.250.0mg/KgPhenanthrene 50-121 2.0 20
35.7 71.476.038.050.0mg/KgPhenol 34-121 6.2 20
39.0 78.077.238.650.0mg/KgPyrene 47-127 1.0 20
18.9 37.840.220.150.0mg/KgPyridine 10-80 6.1 20
32.3 64.668.434.250.0mg/Kg1,2,4-Trichlorobenzene 34-118 5.7 20
39.8 79.681.040.550.0mg/Kg2,4,5-Trichlorophenol 41-124 1.7 20
39.1 78.280.840.450.0mg/Kg2,4,6-Trichlorophenol 39-126 3.2 20
73.475.82-Fluorobiphenyl (S)44-115
66.770.72-Fluorophenol (S)35-115
67.673.2Nitrobenzene-d5 (S)37-122
82.081.84-Terphenyl-d14 (S)54-127
72.672.32,4,6-Tribromophenol (S)39-132
63.768.1Phenol-d5 (S)34-121
Page 22 of 23Date:05/05/2023 03:54 PM
Page 75 of 78
Quality Control Data
23-117-0010Report No:
Project Description:
Client ID:Resolve Environmental
5 Points Gateway
Dry Weight Determination
SW-DRYWT
V32569QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94908-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/30/23 12:451.413.713.9%Moisture
V 95015-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/30/23 12:4513.94.885.61%Moisture
Page 23 of 23Date:05/05/2023 03:54 PM
Page 76 of 78
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-117-0010
Resolve Environmental
00238
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 0.9C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Danyale Love Date & Time:04/27/2023 10:36:22
Special precautions or instructions included?
Comments:
Page 77 of 78
Page 78 of 78

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

5/5/2023
Resolve Environmental Laura Minor
500 Devonport Dr. Matthews, NC, 28104
Ref: Analytical Testing
Lab Report Number: 23-117-0011 Client Project Description: Bakers Quarry
Dear Laura Minor:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/27/2023 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Danyale Love Project Manager
Page 1 of 55
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State Program Lab ID Expiration Date
02/29/202440750State ProgramAlabama
02/07/202488-0650State ProgramArkansas
06/30/20232904State ProgramCalifornia
06/30/2023E871157State Program - NELAPFlorida
11/14/2025C044State ProgramGeorgia
06/30/202304015State ProgramGeorgia
10/10/2023200078State Program - NELAPIllinois
06/30/202380215State ProgramKentucky
12/31/2023KY90047State ProgramKentucky
12/31/2023LA037State Program - NELAPLouisiana
06/30/202304015State Program - NELAPLouisiana
11/14/2025MSState ProgramMississippi
07/31/202347701State ProgramNorth Carolina
12/31/2023415State ProgramNorth Carolina
05/31/202468-03195State Program - NELAPPennsylvania
06/30/202384002State ProgramSouth Carolina
11/14/202502027State ProgramTennessee
09/30/2023T104704180State Program - NELAPTexas
06/30/202300106State ProgramVirginia
09/14/2023460181State Program - NELAPVirginia
Page 1 of 1 00016/23-117-0011
Page 2 of 55
Report Number:
Sample Summary Table
Client Project Description:
23-117-0011
Bakers Quarry
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
04/26/2023 07:38Solids 94928 SS-5 04/27/2023
04/26/2023 07:38Solids 94929 SS-5 Duplicate 04/27/2023
04/26/2023 07:45Solids 94930 SS Comp 04/27/2023
04/26/2023 07:45Solids 94930 SS Comp 04/27/2023 7471A WP MTN -
04/26/2023 07:45Solids 94930 SS Comp 04/27/2023 6020B WP MTN -
04/26/2023 07:45Solids 94931 SS Comp Dup 04/27/2023
04/26/2023 07:45Solids 94931 SS Comp Dup 04/27/2023 6020B WP MTN -
04/26/2023 07:45Solids 94931 SS Comp Dup 04/27/2023 7471A WP MTN -
04/26/2023Aqueous 94933 Trip Blank 04/27/2023
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 55
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
23-117-0011
Report Limit
Project:Bakers Quarry
V 94928SS-5
J0.005 05/01/2023 14:288260DAcetonemg/Kg - dry 0.002
14.9 04/30/2023 12:45SW-DRYWT Moisture %
V 94929SS-5 Duplicate
J0.011 05/01/2023 14:558260DAcetonemg/Kg - dry 0.002
14.8 04/30/2023 12:45SW-DRYWT Moisture %
V 94930SS Comp
5.58 05/03/2023 15:046020BArsenicmg/Kg - dry 0.0943
22.0 05/03/2023 15:046020BBariummg/Kg - dry 0.047
25.8 05/03/2023 15:046020BChromiummg/Kg - dry 0.127
14.1 05/03/2023 15:046020BLeadmg/Kg - dry 0.0342
1.40 05/03/2023 15:046020BSeleniummg/Kg - dry 0.113
J0.0081 05/03/2023 15:046020BSilvermg/Kg - dry 0.0074
9.36 04/30/2023 12:45SW-DRYWT Moisture %
V 94931SS Comp Dup
4.67 05/03/2023 15:086020BArsenicmg/Kg - dry 0.0982
15.6 05/03/2023 15:086020BBariummg/Kg - dry 0.049
24.6 05/03/2023 15:086020BChromiummg/Kg - dry 0.133
10.5 05/03/2023 15:086020BLeadmg/Kg - dry 0.0356
1.53 05/03/2023 15:086020BSeleniummg/Kg - dry 0.118
13.0 04/30/2023 12:45SW-DRYWT Moisture %
V 94933Trip Blank
5.09 05/02/2023 16:118260DAcetoneµg/L 1.80
J1.27 05/02/2023 16:118260DMethyl Ethyl Ketone (MEK)µg/L 0.710
J0.520 05/02/2023 16:118260DMethylene Chloride µg/L 0.330
Page 4 of 55

Client: Resolve Environmental CASE NARRATIVE Project: Bakers Quarry
Lab Report Number: 23-117-0011 Date: 5/4/2023
Metals Analyses Method 6020B Sample 95000 (IDW-Soil)
Analyte: Arsenic QC Batch No: L679823/L679484
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil)
Analyte: Barium QC Batch No: L679823/L679484
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil)
Analyte: Cadmium QC Batch No: L679823/L679484
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 95000 (IDW-Soil) Analyte: Chromium QC Batch No: L679823/L679484 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil) Analyte: Lead
QC Batch No: L679823/L679484 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected.
Sample 95000 (IDW-Soil) Analyte: Selenium
QC Batch No: L679823/L679484 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 84607 (SB-2) Analyte: Mercury QC Batch No: L680090/L679881 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 55

Volatile Organic Compounds - GC/MS Method 8260D
Sample 94933 (Trip Blank) Hits in this sample are likely due to lab contamination.
Analyte: 1,1,2,2-Tetrachloroethane
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: 1,2,3-Trichlorobenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: 1,2,3-Trichloropropane
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: 1,2,4-Trichlorobenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: 1,2-Dichlorobenzene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples Analyte: 1,3,5-Trimethylbenzene QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: 2-Chlorotoluene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: 4-Chlorotoluene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: Bromobenzene QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Analyte: Chloroethane QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Page 6 of 55

Analyte: Hexachlorobutadiene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: Isopropylbenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: Naphthalene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
No hits in samples
Analyte: n-Butylbenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: n-Propylbenzene
QC Batch No: V32647/V32646 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples
Analyte: tert-Butylbenzene QC Batch No: V32647/V32646
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. No hits in samples Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Benzo(b)fluoranthene QC Batch No: V32788/V32670
CCV saw high recoveries for this compound. All other QC was within method parameters. Results for this compound are estimated high.
Analyte: Benzo(g,h,i)perylene QC Batch No: V32788/V32670 CCV saw high recoveries for this compound. All other QC was within method parameters. Results for this compound are estimated high.

Page 7 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5
94928 Matrix:
4/26/2023 7:38
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.9 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5
94928 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
0.005 J mg/Kg - dry 0.002 0.023Acetone 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/01/23 14:28 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/01/23 14:28 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/01/23 14:28 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/01/23 14:28 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 05/01/23 14:28 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/01/23 14:28 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5
94928 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 05/01/23 14:28 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/01/23 14:28 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/01/23 14:28 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/01/23 14:28 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/01/23 14:28 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/01/23 14:28 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/01/23 14:28 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/01/23 14:28 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/01/23 14:28 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5
94928 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 05/01/23 14:28 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/01/23 14:28 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/01/23 14:28 V32647TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/01/23 14:28 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/01/23 14:28 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/01/23 14:28 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/01/23 14:28 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/01/23 14:28 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/01/23 14:28 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 05/01/23 14:28 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5
94928 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/01/23 14:28 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/01/23 14:28 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/01/23 14:28 V32647
Surrogate: 4-Bromofluorobenzene 98.7 Limits: 70-130%05/01/23 14:281 TBL V32647
Surrogate: Dibromofluoromethane 99.1 Limits: 84-123%05/01/23 14:281 TBL V32647
Surrogate: Toluene-d8 87.2 Limits: 76-129%05/01/23 14:281 TBL V32647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5 Duplicate
94929 Matrix:
4/26/2023 7:38
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
14.8 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5 Duplicate
94929 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
0.011 J mg/Kg - dry 0.002 0.023Acetone 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.023Acrolein 1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.023Acrylonitrile 1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Benzene 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Bromobenzene 1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Bromochloromethane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromodichloromethane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Bromoform 1 05/01/23 14:55 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Bromomethane 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Butylbenzene 1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005sec-Butyl benzene 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005tert-Butyl benzene 1 05/01/23 14:55 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Carbon Disulfide 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Carbon Tetrachloride 1 05/01/23 14:55 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Chlorobenzene 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chlorodibromomethane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Chloroethane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Chloroform 1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.011Chloromethane 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0052-Chlorotoluene 1 05/01/23 14:55 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0054-Chlorotoluene 1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005Di-Isopropyl Ether (DIPE)1 05/01/23 14:55 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0111,2-Dibromo-3-Chloropropane 1 05/01/23 14:55 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5 Duplicate
94929 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0007 mg/Kg - dry 0.0007 0.0051,2-Dibromoethane 1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Dibromomethane 1 05/01/23 14:55 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,2-Dichlorobenzene 1 05/01/23 14:55 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,3-Dichlorobenzene 1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0051,4-Dichlorobenzene 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Dichlorodifluoromethane 1 05/01/23 14:55 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.0051,1-Dichloroethane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,2-Dichloroethane 1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloroethene 1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005cis-1,2-Dichloroethene 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005trans-1,2-Dichloroethene 1 05/01/23 14:55 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.0051,2-Dichloropropane 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3-Dichloropropane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0052,2-Dichloropropane 1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.0051,1-Dichloropropene 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005cis-1,3-Dichloropropene 1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.005trans-1,3-Dichloropropene 1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Ethylbenzene 1 05/01/23 14:55 V32647TBL
<0.0010 mg/Kg - dry 0.0010 0.058Ethyl Tertiary Butyl Ether (ETBE)1 05/01/23 14:55 V32647TBL
<0.0009 mg/Kg - dry 0.0009 0.011Hexachlorobutadiene 1 05/01/23 14:55 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.011n-Hexane 1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.0232-Hexanone 1 05/01/23 14:55 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.005Isopropylbenzene 1 05/01/23 14:55 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5 Duplicate
94929 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.001 mg/Kg - dry 0.001 0.0054-Isopropyl toluene 1 05/01/23 14:55 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.023Methyl Ethyl Ketone (MEK)1 05/01/23 14:55 V32647TBL
<0.0007 mg/Kg - dry 0.0007 0.005Methyl tert-butyl ether (MTBE)1 05/01/23 14:55 V32647TBL
<0.017 mg/Kg - dry 0.017 0.0234-Methyl-2-Pentanone 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Methylene Chloride 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011Naphthalene 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005n-Propylbenzene 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Styrene 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1,2-Tetrachloroethane 1 05/01/23 14:55 V32647TBL
<0.0004 mg/Kg - dry 0.0004 0.0051,1,2,2-Tetrachloroethane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Tetrachloroethene 1 05/01/23 14:55 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.005Toluene 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0111,2,3-Trichlorobenzene 1 05/01/23 14:55 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0111,2,4-Trichlorobenzene 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.0051,1,1-Trichloroethane 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,1,2-Trichloroethane 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.005Trichloroethene 1 05/01/23 14:55 V32647TBL
<0.002 mg/Kg - dry 0.002 0.011Trichlorofluoromethane 1 05/01/23 14:55 V32647TBL
<0.0008 mg/Kg - dry 0.0008 0.0051,2,3-Trichloropropane 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,2,4-Trimethylbenzene 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.0051,3,5-Trimethylbenzene 1 05/01/23 14:55 V32647TBL
<0.0005 mg/Kg - dry 0.0005 0.011Vinyl Acetate 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.011Vinyl Chloride 1 05/01/23 14:55 V32647TBL
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS-5 Duplicate
94929 Matrix:
4/26/2023 7:38
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5035
8260D Prep Batch(es):V32646 05/01/23 08:00
<0.0006 mg/Kg - dry 0.0006 0.005o-Xylene 1 05/01/23 14:55 V32647TBL
<0.001 mg/Kg - dry 0.001 0.011m,p-Xylene 1 05/01/23 14:55 V32647TBL
<0.0006 mg/Kg - dry 0.0006 0.005Xylene (Total)1 05/01/23 14:55 V32647
Surrogate: 4-Bromofluorobenzene 85.7 Limits: 70-130%05/01/23 14:551 TBL V32647
Surrogate: Dibromofluoromethane 99.6 Limits: 84-123%05/01/23 14:551 TBL V32647
Surrogate: Toluene-d8 88.4 Limits: 76-129%05/01/23 14:551 TBL V32647
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp
94930 Matrix:
4/26/2023 7:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
9.36 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
5.58 mg/Kg - dry 0.0943 0.276Arsenic 5 05/03/23 15:04 6020BCPW
22.0 mg/Kg - dry 0.047 0.275Barium 5 05/03/23 15:04 6020BCPW
<0.0285 mg/Kg - dry 0.0285 0.276Cadmium 5 05/03/23 15:04 6020BCPW
25.8 mg/Kg - dry 0.127 0.275Chromium 5 05/03/23 15:04 6020BCPW
14.1 mg/Kg - dry 0.0342 0.276Lead 5 05/03/23 15:04 6020BCPW
<0.0244 mg/Kg - dry 0.0244 0.202Mercury (Total)1 05/04/23 13:10 7471AFDS
1.40 mg/Kg - dry 0.113 0.275Selenium 5 05/03/23 15:04 6020BCPW
0.0081 J mg/Kg - dry 0.0074 0.276Silver 5 05/03/23 15:04 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp
94930 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<3.84 mg/Kg - dry 3.84 21.8Acenaphthene 1 05/03/23 11:32 V32788ANG
<3.48 mg/Kg - dry 3.48 21.8Acenaphthylene 1 05/03/23 11:32 V32788ANG
<5.03 mg/Kg - dry 5.03 21.8Aniline 1 05/03/23 11:32 V32788ANG
<4.73 mg/Kg - dry 4.73 21.8Anthracene 1 05/03/23 11:32 V32788ANG
<4.60 mg/Kg - dry 4.60 21.8Benzo(a)anthracene 1 05/03/23 11:32 V32788ANG
<4.87 mg/Kg - dry 4.87 21.8Benzo(a)pyrene 1 05/03/23 11:32 V32788ANG
<4.83 mg/Kg - dry 4.83 21.8Benzo(b)fluoranthene 1 05/03/23 11:32 V32788ANG
<4.50 mg/Kg - dry 4.50 21.8Benzo(g,h,i)perylene 1 05/03/23 11:32 V32788ANG
<4.53 mg/Kg - dry 4.53 21.8Benzo(k)fluoranthene 1 05/03/23 11:32 V32788ANG
<19.2 mg/Kg - dry 19.2 66.2Benzoic Acid 1 05/03/23 11:32 V32788ANG
<3.48 mg/Kg - dry 3.48 21.8Benzyl alcohol 1 05/03/23 11:32 V32788ANG
<3.91 mg/Kg - dry 3.91 21.8Bis(2-Chloroethoxy)methane 1 05/03/23 11:32 V32788ANG
<3.54 mg/Kg - dry 3.54 21.8Bis(2-Chloroethyl)ether 1 05/03/23 11:32 V32788ANG
<4.50 mg/Kg - dry 4.50 10.9Bis(2-Chloroisopropyl)ether 1 05/03/23 11:32 V32788ANG
<3.97 mg/Kg - dry 3.97 21.8Bis(2-ethylhexyl)phthalate 1 05/03/23 11:32 V32788ANG
<3.61 mg/Kg - dry 3.61 21.84-Bromophenyl phenyl ether 1 05/03/23 11:32 V32788ANG
<3.74 mg/Kg - dry 3.74 10.9Butyl benzyl phthalate 1 05/03/23 11:32 V32788ANG
<3.06 mg/Kg - dry 3.06 21.84-Chloro-3-methylphenol 1 05/03/23 11:32 V32788ANG
<3.71 mg/Kg - dry 3.71 10.94-Chloroaniline 1 05/03/23 11:32 V32788ANG
<3.84 mg/Kg - dry 3.84 21.82-Chloronaphthalene 1 05/03/23 11:32 V32788ANG
<3.25 mg/Kg - dry 3.25 21.82-Chlorophenol 1 05/03/23 11:32 V32788ANG
<4.17 mg/Kg - dry 4.17 33.14-Chlorophenyl phenyl ether 1 05/03/23 11:32 V32788ANG
<4.70 mg/Kg - dry 4.70 21.8Chrysene 1 05/03/23 11:32 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp
94930 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<7.61 mg/Kg - dry 7.61 21.8Dibenz(a,h)anthracene 1 05/03/23 11:32 V32788ANG
<3.94 mg/Kg - dry 3.94 21.8Dibenzofuran 1 05/03/23 11:32 V32788ANG
<3.12 mg/Kg - dry 3.12 21.81,2-Dichlorobenzene 1 05/03/23 11:32 V32788ANG
<3.22 mg/Kg - dry 3.22 21.81,3-Dichlorobenzene 1 05/03/23 11:32 V32788ANG
<3.23 mg/Kg - dry 3.23 10.91,4-Dichlorobenzene 1 05/03/23 11:32 V32788ANG
<4.87 mg/Kg - dry 4.87 21.83,3'-Dichlorobenzidine 1 05/03/23 11:32 V32788ANG
<3.17 mg/Kg - dry 3.17 21.82,4-Dichlorophenol 1 05/03/23 11:32 V32788ANG
<5.96 mg/Kg - dry 5.96 21.8Diethyl phthalate 1 05/03/23 11:32 V32788ANG
<5.76 mg/Kg - dry 5.76 21.8Dimethyl phthalate 1 05/03/23 11:32 V32788ANG
<3.57 mg/Kg - dry 3.57 10.92,4-Dimethylphenol 1 05/03/23 11:32 V32788ANG
<3.54 mg/Kg - dry 3.54 21.8Di-n-butyl phthalate 1 05/03/23 11:32 V32788ANG
<7.94 mg/Kg - dry 7.94 49.64,6-Dinitro-2-methylphenol 1 05/03/23 11:32 V32788ANG
<17.2 mg/Kg - dry 17.2 49.62,4-Dinitrophenol 1 05/03/23 11:32 V32788ANG
<3.20 mg/Kg - dry 3.20 21.82,4-Dinitrotoluene 1 05/03/23 11:32 V32788ANG
<3.57 mg/Kg - dry 3.57 21.82,6-Dinitrotoluene 1 05/03/23 11:32 V32788ANG
<4.73 mg/Kg - dry 4.73 10.9Di-n-Octyl Phthalate 1 05/03/23 11:32 V32788ANG
<4.07 mg/Kg - dry 4.07 21.8Fluoranthene 1 05/03/23 11:32 V32788ANG
<4.24 mg/Kg - dry 4.24 21.8Fluorene 1 05/03/23 11:32 V32788ANG
<3.51 mg/Kg - dry 3.51 21.8Hexachlorobenzene 1 05/03/23 11:32 V32788ANG
<3.23 mg/Kg - dry 3.23 21.8Hexachlorobutadiene 1 05/03/23 11:32 V32788ANG
<5.20 mg/Kg - dry 5.20 21.8Hexachlorocyclopentadiene 1 05/03/23 11:32 V32788ANG
<2.63 mg/Kg - dry 2.63 21.8Hexachloroethane 1 05/03/23 11:32 V32788ANG
<5.92 mg/Kg - dry 5.92 21.8Indeno(1,2,3-cd)pyrene 1 05/03/23 11:32 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp
94930 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<6.32 mg/Kg - dry 6.32 21.8Isophorone 1 05/03/23 11:32 V32788ANG
<3.51 mg/Kg - dry 3.51 21.81-Methylnaphthalene 1 05/03/23 11:32 V32788ANG
<3.31 mg/Kg - dry 3.31 21.82-Methylnaphthalene 1 05/03/23 11:32 V32788ANG
<3.21 mg/Kg - dry 3.21 21.82-Methylphenol 1 05/03/23 11:32 V32788ANG
<2.81 mg/Kg - dry 2.81 21.83&4 Methylphenol 1 05/03/23 11:32 V32788ANG
<4.77 mg/Kg - dry 4.77 21.8Naphthalene 1 05/03/23 11:32 V32788ANG
<3.20 mg/Kg - dry 3.20 21.82-Nitroaniline 1 05/03/23 11:32 V32788ANG
<3.97 mg/Kg - dry 3.97 21.83-Nitroaniline 1 05/03/23 11:32 V32788ANG
<3.09 mg/Kg - dry 3.09 10.94-Nitroaniline 1 05/03/23 11:32 V32788ANG
<3.84 mg/Kg - dry 3.84 10.9Nitrobenzene 1 05/03/23 11:32 V32788ANG
<2.93 mg/Kg - dry 2.93 21.82-Nitrophenol 1 05/03/23 11:32 V32788ANG
<3.87 mg/Kg - dry 3.87 21.84-Nitrophenol 1 05/03/23 11:32 V32788ANG
<8.70 mg/Kg - dry 8.70 21.8N-Nitrosodimethylamine 1 05/03/23 11:32 V32788ANG
<5.99 mg/Kg - dry 5.99 21.8N-Nitrosodiphenylamine 1 05/03/23 11:32 V32788ANG
<3.91 mg/Kg - dry 3.91 21.8N-Nitroso-di-n-propylamine 1 05/03/23 11:32 V32788ANG
<11.5 mg/Kg - dry 11.5 33.1Pentachlorophenol 1 05/03/23 11:32 V32788ANG
<6.88 mg/Kg - dry 6.88 21.8Phenanthrene 1 05/03/23 11:32 V32788ANG
<3.71 mg/Kg - dry 3.71 21.8Phenol 1 05/03/23 11:32 V32788ANG
<4.44 mg/Kg - dry 4.44 21.8Pyrene 1 05/03/23 11:32 V32788ANG
<2.63 mg/Kg - dry 2.63 10.9Pyridine 1 05/03/23 11:32 V32788ANG
<3.54 mg/Kg - dry 3.54 21.81,2,4-Trichlorobenzene 1 05/03/23 11:32 V32788ANG
<3.19 mg/Kg - dry 3.19 21.82,4,5-Trichlorophenol 1 05/03/23 11:32 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp
94930 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<3.20 mg/Kg - dry 3.20 21.82,4,6-Trichlorophenol 1 05/03/23 11:32 V32788ANG
8270ESurrogate: Phenol-d5 54.4 Limits: 34-121%05/03/23 11:321 ANG
Surrogate: 2-Fluorobiphenyl 61.2 Limits: 44-115%05/03/23 11:321 ANG V32788
Surrogate: 2-Fluorophenol 57.9 Limits: 35-115%05/03/23 11:321 ANG V32788
Surrogate: Nitrobenzene-d5 60.8 Limits: 37-122%05/03/23 11:321 ANG V32788
Surrogate: 4-Terphenyl-d14 68.8 Limits: 54-127%05/03/23 11:321 ANG V32788
Surrogate: 2,4,6-Tribromophenol 59.3 Limits: 39-132%05/03/23 11:321 ANG V32788
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp Dup
94931 Matrix:
4/26/2023 7:45
Solids
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
13.0 %Moisture 1 04/30/23 12:45 SW-DRYWTPEB
4.67 mg/Kg - dry 0.0982 0.287Arsenic 5 05/03/23 15:08 6020BCPW
15.6 mg/Kg - dry 0.049 0.287Barium 5 05/03/23 15:08 6020BCPW
<0.0297 mg/Kg - dry 0.0297 0.287Cadmium 5 05/03/23 15:08 6020BCPW
24.6 mg/Kg - dry 0.133 0.287Chromium 5 05/03/23 15:08 6020BCPW
10.5 mg/Kg - dry 0.0356 0.287Lead 5 05/03/23 15:08 6020BCPW
<0.0255 mg/Kg - dry 0.0255 0.211Mercury (Total)1 05/04/23 13:12 7471AFDS
1.53 mg/Kg - dry 0.118 0.287Selenium 5 05/03/23 15:08 6020BCPW
<0.0077 mg/Kg - dry 0.0077 0.287Silver 5 05/03/23 15:08 6020BCPW
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp Dup
94931 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<4.00 mg/Kg - dry 4.00 22.8Acenaphthene 1 05/03/23 11:54 V32788ANG
<3.62 mg/Kg - dry 3.62 22.8Acenaphthylene 1 05/03/23 11:54 V32788ANG
<5.24 mg/Kg - dry 5.24 22.8Aniline 1 05/03/23 11:54 V32788ANG
<4.93 mg/Kg - dry 4.93 22.8Anthracene 1 05/03/23 11:54 V32788ANG
<4.79 mg/Kg - dry 4.79 22.8Benzo(a)anthracene 1 05/03/23 11:54 V32788ANG
<5.07 mg/Kg - dry 5.07 22.8Benzo(a)pyrene 1 05/03/23 11:54 V32788ANG
<5.03 mg/Kg - dry 5.03 22.8Benzo(b)fluoranthene 1 05/03/23 11:54 V32788ANG
<4.69 mg/Kg - dry 4.69 22.8Benzo(g,h,i)perylene 1 05/03/23 11:54 V32788ANG
<4.72 mg/Kg - dry 4.72 22.8Benzo(k)fluoranthene 1 05/03/23 11:54 V32788ANG
<20.0 mg/Kg - dry 20.0 69.0Benzoic Acid 1 05/03/23 11:54 V32788ANG
<3.62 mg/Kg - dry 3.62 22.8Benzyl alcohol 1 05/03/23 11:54 V32788ANG
<4.07 mg/Kg - dry 4.07 22.8Bis(2-Chloroethoxy)methane 1 05/03/23 11:54 V32788ANG
<3.69 mg/Kg - dry 3.69 22.8Bis(2-Chloroethyl)ether 1 05/03/23 11:54 V32788ANG
<4.69 mg/Kg - dry 4.69 11.4Bis(2-Chloroisopropyl)ether 1 05/03/23 11:54 V32788ANG
<4.14 mg/Kg - dry 4.14 22.8Bis(2-ethylhexyl)phthalate 1 05/03/23 11:54 V32788ANG
<3.76 mg/Kg - dry 3.76 22.84-Bromophenyl phenyl ether 1 05/03/23 11:54 V32788ANG
<3.90 mg/Kg - dry 3.90 11.4Butyl benzyl phthalate 1 05/03/23 11:54 V32788ANG
<3.18 mg/Kg - dry 3.18 22.84-Chloro-3-methylphenol 1 05/03/23 11:54 V32788ANG
<3.86 mg/Kg - dry 3.86 11.44-Chloroaniline 1 05/03/23 11:54 V32788ANG
<4.00 mg/Kg - dry 4.00 22.82-Chloronaphthalene 1 05/03/23 11:54 V32788ANG
<3.39 mg/Kg - dry 3.39 22.82-Chlorophenol 1 05/03/23 11:54 V32788ANG
<4.34 mg/Kg - dry 4.34 34.54-Chlorophenyl phenyl ether 1 05/03/23 11:54 V32788ANG
<4.90 mg/Kg - dry 4.90 22.8Chrysene 1 05/03/23 11:54 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp Dup
94931 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<7.93 mg/Kg - dry 7.93 22.8Dibenz(a,h)anthracene 1 05/03/23 11:54 V32788ANG
<4.10 mg/Kg - dry 4.10 22.8Dibenzofuran 1 05/03/23 11:54 V32788ANG
<3.25 mg/Kg - dry 3.25 22.81,2-Dichlorobenzene 1 05/03/23 11:54 V32788ANG
<3.36 mg/Kg - dry 3.36 22.81,3-Dichlorobenzene 1 05/03/23 11:54 V32788ANG
<3.37 mg/Kg - dry 3.37 11.41,4-Dichlorobenzene 1 05/03/23 11:54 V32788ANG
<5.07 mg/Kg - dry 5.07 22.83,3'-Dichlorobenzidine 1 05/03/23 11:54 V32788ANG
<3.30 mg/Kg - dry 3.30 22.82,4-Dichlorophenol 1 05/03/23 11:54 V32788ANG
<6.21 mg/Kg - dry 6.21 22.8Diethyl phthalate 1 05/03/23 11:54 V32788ANG
<6.00 mg/Kg - dry 6.00 22.8Dimethyl phthalate 1 05/03/23 11:54 V32788ANG
<3.72 mg/Kg - dry 3.72 11.42,4-Dimethylphenol 1 05/03/23 11:54 V32788ANG
<3.69 mg/Kg - dry 3.69 22.8Di-n-butyl phthalate 1 05/03/23 11:54 V32788ANG
<8.28 mg/Kg - dry 8.28 51.74,6-Dinitro-2-methylphenol 1 05/03/23 11:54 V32788ANG
<17.9 mg/Kg - dry 17.9 51.72,4-Dinitrophenol 1 05/03/23 11:54 V32788ANG
<3.33 mg/Kg - dry 3.33 22.82,4-Dinitrotoluene 1 05/03/23 11:54 V32788ANG
<3.72 mg/Kg - dry 3.72 22.82,6-Dinitrotoluene 1 05/03/23 11:54 V32788ANG
<4.93 mg/Kg - dry 4.93 11.4Di-n-Octyl Phthalate 1 05/03/23 11:54 V32788ANG
<4.24 mg/Kg - dry 4.24 22.8Fluoranthene 1 05/03/23 11:54 V32788ANG
<4.41 mg/Kg - dry 4.41 22.8Fluorene 1 05/03/23 11:54 V32788ANG
<3.66 mg/Kg - dry 3.66 22.8Hexachlorobenzene 1 05/03/23 11:54 V32788ANG
<3.37 mg/Kg - dry 3.37 22.8Hexachlorobutadiene 1 05/03/23 11:54 V32788ANG
<5.41 mg/Kg - dry 5.41 22.8Hexachlorocyclopentadiene 1 05/03/23 11:54 V32788ANG
<2.74 mg/Kg - dry 2.74 22.8Hexachloroethane 1 05/03/23 11:54 V32788ANG
<6.17 mg/Kg - dry 6.17 22.8Indeno(1,2,3-cd)pyrene 1 05/03/23 11:54 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp Dup
94931 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<6.59 mg/Kg - dry 6.59 22.8Isophorone 1 05/03/23 11:54 V32788ANG
<3.66 mg/Kg - dry 3.66 22.81-Methylnaphthalene 1 05/03/23 11:54 V32788ANG
<3.45 mg/Kg - dry 3.45 22.82-Methylnaphthalene 1 05/03/23 11:54 V32788ANG
<3.34 mg/Kg - dry 3.34 22.82-Methylphenol 1 05/03/23 11:54 V32788ANG
<2.93 mg/Kg - dry 2.93 22.83&4 Methylphenol 1 05/03/23 11:54 V32788ANG
<4.97 mg/Kg - dry 4.97 22.8Naphthalene 1 05/03/23 11:54 V32788ANG
<3.33 mg/Kg - dry 3.33 22.82-Nitroaniline 1 05/03/23 11:54 V32788ANG
<4.14 mg/Kg - dry 4.14 22.83-Nitroaniline 1 05/03/23 11:54 V32788ANG
<3.22 mg/Kg - dry 3.22 11.44-Nitroaniline 1 05/03/23 11:54 V32788ANG
<4.00 mg/Kg - dry 4.00 11.4Nitrobenzene 1 05/03/23 11:54 V32788ANG
<3.06 mg/Kg - dry 3.06 22.82-Nitrophenol 1 05/03/23 11:54 V32788ANG
<4.03 mg/Kg - dry 4.03 22.84-Nitrophenol 1 05/03/23 11:54 V32788ANG
<9.07 mg/Kg - dry 9.07 22.8N-Nitrosodimethylamine 1 05/03/23 11:54 V32788ANG
<6.24 mg/Kg - dry 6.24 22.8N-Nitrosodiphenylamine 1 05/03/23 11:54 V32788ANG
<4.07 mg/Kg - dry 4.07 22.8N-Nitroso-di-n-propylamine 1 05/03/23 11:54 V32788ANG
<12.0 mg/Kg - dry 12.0 34.5Pentachlorophenol 1 05/03/23 11:54 V32788ANG
<7.17 mg/Kg - dry 7.17 22.8Phenanthrene 1 05/03/23 11:54 V32788ANG
<3.86 mg/Kg - dry 3.86 22.8Phenol 1 05/03/23 11:54 V32788ANG
<4.62 mg/Kg - dry 4.62 22.8Pyrene 1 05/03/23 11:54 V32788ANG
<2.74 mg/Kg - dry 2.74 11.4Pyridine 1 05/03/23 11:54 V32788ANG
<3.69 mg/Kg - dry 3.69 22.81,2,4-Trichlorobenzene 1 05/03/23 11:54 V32788ANG
<3.32 mg/Kg - dry 3.32 22.82,4,5-Trichlorophenol 1 05/03/23 11:54 V32788ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 26 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:SS Comp Dup
94931 Matrix:
4/26/2023 7:45
Solids
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3546
8270E Prep Batch(es):V32670 05/02/23 09:40
<3.33 mg/Kg - dry 3.33 22.82,4,6-Trichlorophenol 1 05/03/23 11:54 V32788ANG
8270ESurrogate: Phenol-d5 48.4 Limits: 34-121%05/03/23 11:541 ANG
Surrogate: 2-Fluorobiphenyl 56.4 Limits: 44-115%05/03/23 11:541 ANG V32788
Surrogate: 2-Fluorophenol 51.6 Limits: 35-115%05/03/23 11:541 ANG V32788
Surrogate: Nitrobenzene-d5 53.8 Limits: 37-122%05/03/23 11:541 ANG V32788
Surrogate: 4-Terphenyl-d14 56.6 Limits: 54-127%05/03/23 11:541 ANG V32788
Surrogate: 2,4,6-Tribromophenol 50.9 Limits: 39-132%05/03/23 11:541 ANG V32788
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 27 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94933 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
5.09 µg/L 1.80 5.00Acetone 1 05/02/23 16:11 V32721MSA
<2.00 µg/L 2.00 5.00Acrolein 1 05/02/23 16:11 V32721MSA
<0.230 µg/L 0.230 5.00Acrylonitrile 1 05/02/23 16:11 V32721MSA
<0.180 µg/L 0.180 0.500Benzene 1 05/02/23 16:11 V32721MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 05/02/23 16:11 V32721MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 05/02/23 16:11 V32721MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 05/02/23 16:11 V32721MSA
<1.50 µg/L 1.50 5.00Bromoform 1 05/02/23 16:11 V32721MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 05/02/23 16:11 V32721MSA
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 05/02/23 16:11 V32721MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 05/02/23 16:11 V32721MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 05/02/23 16:11 V32721MSA
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 05/02/23 16:11 V32721MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 05/02/23 16:11 V32721MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 05/02/23 16:11 V32721MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 05/02/23 16:11 V32721MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 05/02/23 16:11 V32721MSA
<0.220 µg/L 0.220 0.500Chloroform 1 05/02/23 16:11 V32721MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 05/02/23 16:11 V32721MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 05/02/23 16:11 V32721MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 05/02/23 16:11 V32721MSA
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 05/02/23 16:11 V32721MSA
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 05/02/23 16:11 V32721MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 28 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94933 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 05/02/23 16:11 V32721MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 05/02/23 16:11 V32721MSA
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 05/02/23 16:11 V32721MSA
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 05/02/23 16:11 V32721MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 05/02/23 16:11 V32721MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 05/02/23 16:11 V32721MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 05/02/23 16:11 V32721MSA
<0.150 µg/L 0.150 0.5001,2-Dichloroethane 1 05/02/23 16:11 V32721MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 05/02/23 16:11 V32721MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 05/02/23 16:11 V32721MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 05/02/23 16:11 V32721MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 05/02/23 16:11 V32721MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 05/02/23 16:11 V32721MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 05/02/23 16:11 V32721MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 05/02/23 16:11 V32721MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 05/02/23 16:11 V32721MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 05/02/23 16:11 V32721MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 05/02/23 16:11 V32721MSA
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 05/02/23 16:11 V32721MSA
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 05/02/23 16:11 V32721MSA
<1.30 µg/L 1.30 10.0n-Hexane 1 05/02/23 16:11 V32721MSA
<0.380 µg/L 0.380 5.002-Hexanone 1 05/02/23 16:11 V32721MSA
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 05/02/23 16:11 V32721MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 29 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94933 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 05/02/23 16:11 V32721MSA
1.27 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 05/02/23 16:11 V32721MSA
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 05/02/23 16:11 V32721MSA
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 05/02/23 16:11 V32721MSA
0.520 J µg/L 0.330 1.00Methylene Chloride 1 05/02/23 16:11 V32721MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 05/02/23 16:11 V32721MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 05/02/23 16:11 V32721MSA
<0.220 µg/L 0.220 0.500Styrene 1 05/02/23 16:11 V32721MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 05/02/23 16:11 V32721MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 05/02/23 16:11 V32721MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 05/02/23 16:11 V32721MSA
<0.220 µg/L 0.220 0.500Toluene 1 05/02/23 16:11 V32721MSA
<0.380 µg/L 0.380 2.001,2,3-Trichlorobenzene 1 05/02/23 16:11 V32721MSA
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 05/02/23 16:11 V32721MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 05/02/23 16:11 V32721MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 05/02/23 16:11 V32721MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 05/02/23 16:11 V32721MSA
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 05/02/23 16:11 V32721MSA
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 05/02/23 16:11 V32721MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 05/02/23 16:11 V32721MSA
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 05/02/23 16:11 V32721MSA
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 05/02/23 16:11 V32721MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 05/02/23 16:11 V32721MSA
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 30 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28104
23-117-0011
00238
Resolve Environmental
500 Devonport Dr.
Laura Minor
Matthews
Danyale Love
Project Manager
Received : 04/27/2023
Bakers Quarry
Report Date : 05/05/2023
Sample ID :
Lab No :
Sampled:Trip Blank
94933 Matrix:
4/26/2023 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V32720 05/02/23 09:00
<0.210 µg/L 0.210 0.500o-Xylene 1 05/02/23 16:11 V32721MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 05/02/23 16:11 V32721MSA
<0.21 µg/L 0.210 0.500Xylene (Total)1 05/02/23 16:11 V32721
Surrogate: 4-Bromofluorobenzene 101 Limits: 80-124%05/02/23 16:111 MSA V32721
Surrogate: Dibromofluoromethane 99.8 Limits: 75-129%05/02/23 16:111 MSA V32721
Surrogate: 1,2-Dichloroethane - d4 99.4 Limits: 63-136%05/02/23 16:111 MSA V32721
Surrogate: Toluene-d8 99.2 Limits: 77-123%05/02/23 16:111 MSA V32721
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 31 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Metals Analyses
6020B
L679823QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L679484
Associated Lab Samples: 94930, 94931
LRB-L679484 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/03/23 13:430.2500.0855<0.0855mg/KgArsenic
05/03/23 13:430.2500.042<0.042mg/KgBarium
05/03/23 13:430.2500.0259<0.0259mg/KgCadmium
05/03/23 13:430.2500.116<0.116mg/KgChromium
05/03/23 13:430.2500.0310<0.0310mg/KgLead
05/03/23 13:430.2500.103<0.103mg/KgSelenium
05/03/23 13:430.2500.0067<0.0067mg/KgSilver
LCS-L679484Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.02.362.50mg/KgArsenic 80-120
91.04.565.00mg/KgBarium 80-120
95.00.4770.500mg/KgCadmium 80-120
93.04.675.00mg/KgChromium 80-120
94.02.362.50mg/KgLead 80-120
93.04.645.00mg/KgSelenium 80-120
95.00.4730.500mg/KgSilver 80-120
V 95000-MS-L679484 V 95000-MSD-L679484Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
10.1 0.0*10.72.482.3810.1mg/KgArsenic 24.0*75-125 5.7 80
26.9 0.0*26.44.974.7633.0mg/KgBarium 0.0*75-125 1.8 80
0.520 71.0*0.6050.4970.4760.180mg/KgCadmium 86.0 75-125 15.1 80
30.1 0.0*31.64.974.7632.9mg/KgChromium 0.0*75-125 4.8 80
Page 1 of 22* QC Fail Date:05/05/2023 10:26 AM
Page 32 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Metals Analyses
6020B
L679823QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3050B
QC Prep:L679484
V 95000-MS-L679484 V 95000-MSD-L679484Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
12.5 0.0*14.02.482.3814.5mg/KgLead 0.0*75-125 11.3 80
4.54 65.0*4.924.974.761.43mg/KgSelenium 70.0*75-125 8.0 80
0.409 80.00.4730.4970.4760.0302mg/KgSilver 89.0 75-125 14.5 80
V 95000-PDS-L679484Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/03/23 15:2491.02.00mg/KgArsenic
05/03/23 15:2494.05.30mg/KgBarium
05/03/23 15:2493.00.237mg/KgCadmium
05/03/23 15:2490.05.08mg/KgChromium
05/03/23 15:2492.02.42mg/KgLead
05/03/23 15:2491.02.29mg/KgSelenium
05/03/23 15:2494.00.227mg/KgSilver
Page 2 of 22* QC Fail Date:05/05/2023 10:26 AM
Page 33 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Solids Total Mercury Analysis - CVAA
7471A
L680090QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7471A
QC Prep:L679881
Associated Lab Samples: 94930, 94931
LRB-L679881 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
05/04/23 13:000.1920.0232<0.0232mg/KgMercury (Total)
LCS-L679881Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1110.4450.400mg/KgMercury (Total)80-120
L 84607-MS-L679881 L 84607-MSD-L679881Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.432 1100.5270.3990.391<0.0227mg/KgMercury (Total)132*80-120 19.8 20
L 84607-PDS-L679881Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
05/04/23 13:261090.804mg/KgMercury (Total)
Page 3 of 22* QC Fail Date:05/05/2023 10:26 AM
Page 34 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
Associated Lab Samples: 94928, 94929
LRB-V32646 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/01/23 10:510.0200.002<0.002mg/KgAcetone
05/01/23 10:510.0200.001<0.001mg/KgAcrolein
05/01/23 10:510.0200.0008<0.0008mg/KgAcrylonitrile
05/01/23 10:510.0050.0006<0.0006mg/KgBenzene
05/01/23 10:510.0050.0005<0.0005mg/KgBromobenzene
05/01/23 10:510.0050.0008<0.0008mg/KgBromochloromethane
05/01/23 10:510.0050.001<0.001mg/KgBromodichloromethane
05/01/23 10:510.0050.001<0.001mg/KgBromoform
05/01/23 10:510.0100.001<0.001mg/KgBromomethane
05/01/23 10:510.0050.0005<0.0005mg/Kgn-Butylbenzene
05/01/23 10:510.0050.0006<0.0006mg/Kgsec-Butyl benzene
05/01/23 10:510.0050.0005<0.0005mg/Kgtert-Butyl benzene
05/01/23 10:510.0050.0006<0.0006mg/KgCarbon Disulfide
05/01/23 10:510.0050.001<0.001mg/KgCarbon Tetrachloride
05/01/23 10:510.0050.0007<0.0007mg/KgChlorobenzene
05/01/23 10:510.0050.0009<0.0009mg/KgChlorodibromomethane
05/01/23 10:510.0100.0009<0.0009mg/KgChloroethane
05/01/23 10:510.0050.001<0.001mg/KgChloroform
05/01/23 10:510.0100.0006<0.0006mg/KgChloromethane
05/01/23 10:510.0050.0005<0.0005mg/Kg2-Chlorotoluene
05/01/23 10:510.0050.0004<0.0004mg/Kg4-Chlorotoluene
05/01/23 10:510.0050.0007<0.0007mg/KgDi-Isopropyl Ether (DIPE)
05/01/23 10:510.0100.0004<0.0004mg/Kg1,2-Dibromo-3-Chloropropane
05/01/23 10:510.0050.0006<0.0006mg/Kg1,2-Dibromoethane
05/01/23 10:510.0050.0006<0.0006mg/KgDibromomethane
05/01/23 10:510.0050.0003<0.0003mg/Kg1,2-Dichlorobenzene
05/01/23 10:510.0050.0004<0.0004mg/Kg1,3-Dichlorobenzene
Page 4 of 22Date:05/05/2023 10:26 AM
Page 35 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
Associated Lab Samples: 94928, 94929
LRB-V32646 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/01/23 10:510.0050.0006<0.0006mg/Kg1,4-Dichlorobenzene
05/01/23 10:510.0100.001<0.001mg/KgDichlorodifluoromethane
05/01/23 10:510.0050.0008<0.0008mg/Kg1,1-Dichloroethane
05/01/23 10:510.0050.001<0.001mg/Kg1,2-Dichloroethane
05/01/23 10:510.0050.0007<0.0007mg/Kg1,1-Dichloroethene
05/01/23 10:510.0050.0008<0.0008mg/Kgcis-1,2-Dichloroethene
05/01/23 10:510.0050.001<0.001mg/Kgtrans-1,2-Dichloroethene
05/01/23 10:510.0050.0004<0.0004mg/Kg1,2-Dichloropropane
05/01/23 10:510.0050.0006<0.0006mg/Kg1,3-Dichloropropane
05/01/23 10:510.0050.001<0.001mg/Kg2,2-Dichloropropane
05/01/23 10:510.0050.0008<0.0008mg/Kg1,1-Dichloropropene
05/01/23 10:510.0050.0005<0.0005mg/Kgcis-1,3-Dichloropropene
05/01/23 10:510.0050.0008<0.0008mg/Kgtrans-1,3-Dichloropropene
05/01/23 10:510.0050.0006<0.0006mg/KgEthylbenzene
05/01/23 10:510.0500.0008<0.0008mg/KgEthyl Tertiary Butyl Ether (ETBE)
05/01/23 10:510.0100.0008<0.0008mg/KgHexachlorobutadiene
05/01/23 10:510.0100.0007<0.0007mg/Kgn-Hexane
05/01/23 10:510.0200.0006<0.0006mg/Kg2-Hexanone
05/01/23 10:510.0050.0005<0.0005mg/KgIsopropylbenzene
05/01/23 10:510.0050.001<0.001mg/Kg4-Isopropyl toluene
05/01/23 10:510.0200.0007<0.0007mg/KgMethyl Ethyl Ketone (MEK)
05/01/23 10:510.0050.0006<0.0006mg/KgMethyl tert-butyl ether (MTBE)
05/01/23 10:510.0200.015<0.015mg/Kg4-Methyl-2-Pentanone
05/01/23 10:510.0100.001<0.001mg/KgMethylene Chloride
05/01/23 10:510.0100.0010<0.0010mg/KgNaphthalene
05/01/23 10:510.0050.0005<0.0005mg/Kgn-Propylbenzene
05/01/23 10:510.0050.001<0.001mg/KgStyrene
Page 5 of 22Date:05/05/2023 10:26 AM
Page 36 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
Associated Lab Samples: 94928, 94929
LRB-V32646 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/01/23 10:510.0050.001<0.001mg/Kg1,1,1,2-Tetrachloroethane
05/01/23 10:510.0050.0003<0.0003mg/Kg1,1,2,2-Tetrachloroethane
05/01/23 10:510.0050.0009<0.0009mg/KgTetrachloroethene
05/01/23 10:510.0050.0007<0.0007mg/KgToluene
05/01/23 10:510.0100.0005<0.0005mg/Kg1,2,3-Trichlorobenzene
05/01/23 10:510.0100.0006<0.0006mg/Kg1,2,4-Trichlorobenzene
05/01/23 10:510.0050.001<0.001mg/Kg1,1,1-Trichloroethane
05/01/23 10:510.0050.0005<0.0005mg/Kg1,1,2-Trichloroethane
05/01/23 10:510.0050.0009<0.0009mg/KgTrichloroethene
05/01/23 10:510.0100.002<0.002mg/KgTrichlorofluoromethane
05/01/23 10:510.0050.0007<0.0007mg/Kg1,2,3-Trichloropropane
05/01/23 10:510.0050.0005<0.0005mg/Kg1,2,4-Trimethylbenzene
05/01/23 10:510.0050.0005<0.0005mg/Kg1,3,5-Trimethylbenzene
05/01/23 10:510.0100.0005<0.0005mg/KgVinyl Acetate
05/01/23 10:510.0100.0005<0.0005mg/KgVinyl Chloride
05/01/23 10:510.0050.0005<0.0005mg/Kgo-Xylene
05/01/23 10:510.0100.001<0.001mg/Kgm,p-Xylene
05/01/23 10:514-Bromofluorobenzene (S)99.8 70-130
05/01/23 10:51Dibromofluoromethane (S)97.8 84-123
05/01/23 10:51Toluene-d8 (S)91.0 76-129
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.119 1191120.1120.100mg/KgAcetone 29-198 6.0 20
0.079 79.376.60.0760.100mg/KgAcrolein 70-130 3.4 20
Page 6 of 22Date:05/05/2023 10:26 AM
Page 37 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.097 97.895.00.0950.100mg/KgAcrylonitrile 65-134 2.9 20
0.049 98.01020.0510.050mg/KgBenzene 74-127 4.0 20
0.042 84.61140.0560.050mg/KgBromobenzene 73-125 29.2*20
0.055 1101110.0550.050mg/KgBromochloromethane 72-134 0.9 20
0.053 1061080.0540.050mg/KgBromodichloromethane 75-122 1.8 20
0.052 1051040.0520.050mg/KgBromoform 66-135 0.5 20
0.037 74.878.00.0390.050mg/KgBromomethane 20-180 4.1 20
0.043 86.21160.0580.050mg/Kgn-Butylbenzene 65-135 29.8*20
0.043 86.475.20.0370.050mg/Kgsec-Butyl benzene 66-131 13.8 20
0.042 85.61070.0530.050mg/Kgtert-Butyl benzene 67-132 22.0*20
0.045 90.497.80.0480.050mg/KgCarbon Disulfide 61-129 7.8 20
0.052 1041090.0540.050mg/KgCarbon Tetrachloride 64-143 4.3 20
0.048 97.899.60.0490.050mg/KgChlorobenzene 74-118 1.8 20
0.050 10199.40.0490.050mg/KgChlorodibromomethane 73-122 1.9 20
0.029 58.684.20.0420.050mg/KgChloroethane 33-149 35.8*20
0.050 1011060.0530.050mg/KgChloroform 73-127 4.8 20
0.045 90.294.80.0470.050mg/KgChloromethane 45-143 4.9 20
0.043 86.21170.0580.050mg/Kg2-Chlorotoluene 67-124 29.9*20
0.043 86.21170.0580.050mg/Kg4-Chlorotoluene 71-126 29.9*20
0.049 98.61010.0500.050mg/KgDi-Isopropyl Ether (DIPE)59-159 2.8 20
0.051 1031230.0610.050mg/Kg1,2-Dibromo-3-Chloropropane 55-157 17.8 20
0.052 1051010.0500.050mg/Kg1,2-Dibromoethane 70-132 3.4 20
0.052 1051040.0510.050mg/KgDibromomethane 74-133 1.5 20
0.045 91.61180.0590.050mg/Kg1,2-Dichlorobenzene 72-123 25.5*20
0.046 92.481.00.0400.050mg/Kg1,3-Dichlorobenzene 71-120 13.1 20
0.044 89.496.80.0480.050mg/Kg1,4-Dichlorobenzene 71-123 7.9 20
Page 7 of 22* QC Fail Date:05/05/2023 10:26 AM
Page 38 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.042 84.290.80.0450.050mg/KgDichlorodifluoromethane 26-146 7.5 20
0.049 99.81030.0510.050mg/Kg1,1-Dichloroethane 74-127 3.5 20
0.050 1011020.0510.050mg/Kg1,2-Dichloroethane 68-128 1.3 20
0.047 94.61000.0500.050mg/Kg1,1-Dichloroethene 67-149 5.7 20
0.050 1001020.0500.050mg/Kgcis-1,2-Dichloroethene 76-134 1.1 20
0.048 96.21040.0520.050mg/Kgtrans-1,2-Dichloroethene 73-132 7.9 20
0.050 1001010.0500.050mg/Kg1,2-Dichloropropane 73-130 1.3 20
0.049 98.497.80.0480.050mg/Kg1,3-Dichloropropane 75-124 0.6 20
0.051 1021030.0510.050mg/Kg2,2-Dichloropropane 50-142 0.9 20
0.050 1011050.0520.050mg/Kg1,1-Dichloropropene 71-130 3.7 20
0.054 1081080.0530.050mg/Kgcis-1,3-Dichloropropene 71-125 0.3 20
0.054 1091110.0550.050mg/Kgtrans-1,3-Dichloropropene 68-123 1.8 20
0.046 92.895.80.0470.050mg/KgEthylbenzene 74-128 3.1 20
0.099 99.598.80.0980.100mg/KgEthyl Tertiary Butyl Ether (ETBE)70-130 0.7 20
0.046 92.8131*0.0650.050mg/KgHexachlorobutadiene 64-125 33.9*20
0.049 98.81060.0530.050mg/Kgn-Hexane 70-130 7.4 20
0.049 98.693.40.0460.050mg/Kg2-Hexanone 61-157 5.4 20
0.043 87.21160.0580.050mg/KgIsopropylbenzene 68-126 28.6*20
0.044 88.075.20.0370.050mg/Kg4-Isopropyl toluene 68-129 15.6 20
0.039 79.671.60.0350.050mg/KgMethyl Ethyl Ketone (MEK)63-149 10.5 20
0.049 99.41010.0500.050mg/KgMethyl tert-butyl ether (MTBE)70-130 1.5 20
0.054 1101060.0520.050mg/Kg4-Methyl-2-Pentanone 57-162 3.7 20
0.042 85.885.40.0420.050mg/KgMethylene Chloride 74-129 0.4 20
0.047 94.61170.0580.050mg/KgNaphthalene 57-157 21.1*20
0.041 83.41160.0580.050mg/Kgn-Propylbenzene 67-130 33.0*20
0.049 98.499.20.0490.050mg/KgStyrene 77-121 0.8 20
Page 8 of 22* QC Fail Date:05/05/2023 10:26 AM
Page 39 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32647QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5035
QC Prep:V32646
LCS-V32646 LCSD-V32646Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
0.050 1011010.0500.050mg/Kg1,1,1,2-Tetrachloroethane 72-115 0.3 20
0.040 80.21120.0560.050mg/Kg1,1,2,2-Tetrachloroethane 56-126 33.0*20
0.053 1061070.0530.050mg/KgTetrachloroethene 68-130 1.1 20
0.049 98.81040.0520.050mg/KgToluene 71-129 5.1 20
0.048 96.81230.0610.050mg/Kg1,2,3-Trichlorobenzene 68-130 24.1*20
0.048 97.8128*0.0630.050mg/Kg1,2,4-Trichlorobenzene 66-125 26.5*20
0.050 1011050.0520.050mg/Kg1,1,1-Trichloroethane 67-131 4.2 20
0.049 98.697.60.0480.050mg/Kg1,1,2-Trichloroethane 70-133 1.0 20
0.052 1051070.0530.050mg/KgTrichloroethene 75-133 1.6 20
0.030 61.472.00.0360.050mg/KgTrichlorofluoromethane 44-146 15.8 20
0.047 95.01180.0590.050mg/Kg1,2,3-Trichloropropane 60-137 21.5*20
0.044 88.273.40.0360.050mg/Kg1,2,4-Trimethylbenzene 69-129 18.3 20
0.043 86.41160.0580.050mg/Kg1,3,5-Trimethylbenzene 69-128 29.5*20
0.045 91.090.20.0450.050mg/KgVinyl Acetate 60-140 0.8 20
0.046 93.697.40.0480.050mg/KgVinyl Chloride 48-147 3.9 20
0.046 92.695.20.0470.050mg/Kgo-Xylene 74-126 2.7 20
0.096 96.099.30.0990.100mg/Kgm,p-Xylene 75-124 3.3 20
1011074-Bromofluorobenzene (S)70-130
96.495.6Dibromofluoromethane (S)84-123
91.891.0Toluene-d8 (S)76-129
Page 9 of 22* QC Fail Date:05/05/2023 10:26 AM
Page 40 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
Associated Lab Samples: 94933
LRB-V32720 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 14:225.001.80<1.80µg/LAcetone
05/02/23 14:225.002.00<2.00µg/LAcrolein
05/02/23 14:225.000.230<0.230µg/LAcrylonitrile
05/02/23 14:220.5000.180<0.180µg/LBenzene
05/02/23 14:220.5000.210<0.210µg/LBromobenzene
05/02/23 14:221.000.420<0.420µg/LBromochloromethane
05/02/23 14:220.5000.160<0.160µg/LBromodichloromethane
05/02/23 14:225.001.50<1.50µg/LBromoform
05/02/23 14:221.000.280<0.280µg/LBromomethane
05/02/23 14:221.000.185<0.185µg/Ln-Butylbenzene
05/02/23 14:220.5000.200<0.200µg/Lsec-Butyl benzene
05/02/23 14:222.000.920<0.920µg/Ltert-Butyl benzene
05/02/23 14:225.000.150<0.150µg/LCarbon Disulfide
05/02/23 14:220.5000.180<0.180µg/LCarbon Tetrachloride
05/02/23 14:220.5000.190<0.190µg/LChlorobenzene
05/02/23 14:220.5000.190<0.190µg/LChlorodibromomethane
05/02/23 14:221.000.430<0.430µg/LChloroethane
05/02/23 14:220.5000.220<0.220µg/LChloroform
05/02/23 14:220.5000.220<0.220µg/LChloromethane
05/02/23 14:220.5000.200<0.200µg/L2-Chlorotoluene
05/02/23 14:220.5000.200<0.200µg/L4-Chlorotoluene
05/02/23 14:225.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
05/02/23 14:222.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
05/02/23 14:220.5000.200<0.200µg/L1,2-Dibromoethane
05/02/23 14:220.5000.230<0.230µg/LDibromomethane
05/02/23 14:220.5000.220<0.220µg/L1,2-Dichlorobenzene
05/02/23 14:220.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 10 of 22Date:05/05/2023 10:26 AM
Page 41 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
Associated Lab Samples: 94933
LRB-V32720 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 14:220.5000.210<0.210µg/L1,4-Dichlorobenzene
05/02/23 14:225.001.20<1.20µg/LDichlorodifluoromethane
05/02/23 14:220.5000.240<0.240µg/L1,1-Dichloroethane
05/02/23 14:220.5000.150<0.150µg/L1,2-Dichloroethane
05/02/23 14:220.5000.150<0.150µg/L1,1-Dichloroethene
05/02/23 14:220.5000.200<0.200µg/Lcis-1,2-Dichloroethene
05/02/23 14:220.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
05/02/23 14:220.5000.190<0.190µg/L1,2-Dichloropropane
05/02/23 14:220.5000.130<0.130µg/L1,3-Dichloropropane
05/02/23 14:222.000.210<0.210µg/L2,2-Dichloropropane
05/02/23 14:220.5000.200<0.200µg/L1,1-Dichloropropene
05/02/23 14:220.5000.210<0.210µg/Lcis-1,3-Dichloropropene
05/02/23 14:220.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
05/02/23 14:220.5000.170<0.170µg/LEthylbenzene
05/02/23 14:2210.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
05/02/23 14:222.000.350<0.350µg/LHexachlorobutadiene
05/02/23 14:2210.01.30<1.30µg/Ln-Hexane
05/02/23 14:225.000.380<0.380µg/L2-Hexanone
05/02/23 14:225.000.180<0.180µg/LIsopropylbenzene
05/02/23 14:220.5000.089<0.089µg/L4-Isopropyl toluene
05/02/23 14:225.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
05/02/23 14:220.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
05/02/23 14:225.001.00<1.00µg/L4-Methyl-2-Pentanone
05/02/23 14:221.000.330<0.330µg/LMethylene Chloride
05/02/23 14:221.000.470<0.470µg/LNaphthalene
05/02/23 14:220.5000.190<0.190µg/Ln-Propylbenzene
05/02/23 14:220.5000.220<0.220µg/LStyrene
Page 11 of 22Date:05/05/2023 10:26 AM
Page 42 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
Associated Lab Samples: 94933
LRB-V32720 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/02/23 14:220.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
05/02/23 14:220.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
05/02/23 14:220.5000.220<0.220µg/LTetrachloroethene
05/02/23 14:220.5000.220<0.220µg/LToluene
05/02/23 14:222.000.380<0.380µg/L1,2,3-Trichlorobenzene
05/02/23 14:221.000.310<0.310µg/L1,2,4-Trichlorobenzene
05/02/23 14:220.5000.160<0.160µg/L1,1,1-Trichloroethane
05/02/23 14:220.5000.096<0.096µg/L1,1,2-Trichloroethane
05/02/23 14:220.5000.180<0.180µg/LTrichloroethene
05/02/23 14:220.5000.180<0.180µg/LTrichlorofluoromethane
05/02/23 14:221.000.270<0.270µg/L1,2,3-Trichloropropane
05/02/23 14:220.5000.190<0.190µg/L1,2,4-Trimethylbenzene
05/02/23 14:220.5000.180<0.180µg/L1,3,5-Trimethylbenzene
05/02/23 14:222.001.00<1.00µg/LVinyl Acetate
05/02/23 14:220.5000.170<0.170µg/LVinyl Chloride
05/02/23 14:220.5000.210<0.210µg/Lo-Xylene
05/02/23 14:221.000.420<0.420µg/Lm,p-Xylene
05/02/23 14:224-Bromofluorobenzene (S)102 80-124
05/02/23 14:22Dibromofluoromethane (S)100 75-129
05/02/23 14:221,2-Dichloroethane - d4 (S)99.6 63-136
05/02/23 14:22Toluene-d8 (S)99.8 77-123
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
35.3 88.289.735.940.0µg/LAcetone 40-166 1.6 20.0
Page 12 of 22Date:05/05/2023 10:26 AM
Page 43 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.1 92.796.038.440.0µg/LAcrolein 70-130 3.4 20.0
41.5 10410441.440.0µg/LAcrylonitrile 81-127 0.2 20.0
20.0 10010020.020.0µg/LBenzene 77-128 0.0 20.0
19.9 99.510320.520.0µg/LBromobenzene 78-129 2.9 20.0
19.5 97.510320.520.0µg/LBromochloromethane 78-135 5.0 20.0
19.6 98.010320.620.0µg/LBromodichloromethane 76-138 4.9 20.0
19.5 97.593.518.720.0µg/LBromoform 71-135 4.1 20.0
19.7 98.599.519.920.0µg/LBromomethane 41-168 1.0 20.0
19.0 95.099.019.820.0µg/Ln-Butylbenzene 68-134 4.1 20.0
19.4 97.010020.020.0µg/Lsec-Butyl benzene 71-131 3.0 20.0
19.4 97.099.019.820.0µg/Ltert-Butyl benzene 70-132 2.0 20.0
18.6 93.094.518.920.0µg/LCarbon Disulfide 59-135 1.6 20.0
19.5 97.510420.820.0µg/LCarbon Tetrachloride 72-142 6.4 20.0
19.4 97.098.519.720.0µg/LChlorobenzene 78-119 1.5 20.0
20.4 10210220.420.0µg/LChlorodibromomethane 75-134 0.0 20.0
21.8 10910621.220.0µg/LChloroethane 57-142 2.7 20.0
19.7 98.510120.220.0µg/LChloroform 77-130 2.5 20.0
19.8 99.099.019.820.0µg/LChloromethane 47-145 0.0 20.0
19.6 98.010220.420.0µg/L2-Chlorotoluene 74-126 4.0 20.0
19.8 99.010220.320.0µg/L4-Chlorotoluene 78-129 2.4 20.0
19.1 95.598.519.720.0µg/LDi-Isopropyl Ether (DIPE)60-154 3.0 20.0
20.9 10598.019.620.0µg/L1,2-Dibromo-3-Chloropropane 63-134 6.4 20.0
20.2 10110120.220.0µg/L1,2-Dibromoethane 77-135 0.0 20.0
20.5 10310320.520.0µg/LDibromomethane 76-138 0.0 20.0
18.8 94.096.019.220.0µg/L1,2-Dichlorobenzene 78-128 2.1 20.0
19.9 99.510120.120.0µg/L1,3-Dichlorobenzene 77-125 1.0 20.0
Page 13 of 22Date:05/05/2023 10:26 AM
Page 44 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.3 96.596.019.220.0µg/L1,4-Dichlorobenzene 75-126 0.5 20.0
19.0 95.098.019.620.0µg/LDichlorodifluoromethane 28-163 3.1 20.0
19.8 99.010320.520.0µg/L1,1-Dichloroethane 70-130 3.4 20.0
18.6 93.097.519.520.0µg/L1,2-Dichloroethane 68-131 4.7 20.0
21.0 10510621.120.0µg/L1,1-Dichloroethene 70-154 0.4 20.0
20.0 10010020.020.0µg/Lcis-1,2-Dichloroethene 76-141 0.0 20.0
20.8 10410420.820.0µg/Ltrans-1,2-Dichloroethene 76-135 0.0 20.0
19.4 97.099.019.820.0µg/L1,2-Dichloropropane 77-130 2.0 20.0
18.7 93.596.019.220.0µg/L1,3-Dichloropropane 76-132 2.6 20.0
20.4 10299.519.920.0µg/L2,2-Dichloropropane 29-149 2.4 20.0
21.6 10810721.420.0µg/L1,1-Dichloropropene 71-136 0.9 20.0
19.7 98.510220.420.0µg/Lcis-1,3-Dichloropropene 65-140 3.4 20.0
19.2 96.096.019.220.0µg/Ltrans-1,3-Dichloropropene 67-140 0.0 20.0
19.7 98.599.519.920.0µg/LEthylbenzene 80-127 1.0 20.0
39.7 99.210240.640.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 2.2 20.0
18.1 90.598.019.620.0µg/LHexachlorobutadiene 61-134 7.9 20.0
21.2 10610220.420.0µg/Ln-Hexane 70-130 3.8 20.0
18.4 92.090.018.020.0µg/L2-Hexanone 64-137 2.1 20.0
20.6 10310420.820.0µg/LIsopropylbenzene 70-130 0.9 20.0
20.2 10110320.620.0µg/L4-Isopropyl toluene 69-132 1.9 20.0
17.1 85.588.017.620.0µg/LMethyl Ethyl Ketone (MEK)71-134 2.8 20.0
19.8 99.099.019.820.0µg/LMethyl tert-butyl ether (MTBE)68-135 0.0 20.0
18.0 90.090.018.020.0µg/L4-Methyl-2-Pentanone 69-134 0.0 20.0
20.6 10310020.020.0µg/LMethylene Chloride 73-131 2.9 20.0
16.8 84.080.016.020.0µg/LNaphthalene 64-136 4.8 20.0
19.6 98.010020.020.0µg/Ln-Propylbenzene 72-132 2.0 20.0
Page 14 of 22Date:05/05/2023 10:26 AM
Page 45 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V32721QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V32720
LCS-V32720 LCSD-V32720Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.9 99.510220.420.0µg/LStyrene 78-129 2.4 20.0
19.6 98.099.519.920.0µg/L1,1,1,2-Tetrachloroethane 79-134 1.5 20.0
20.7 10410120.220.0µg/L1,1,2,2-Tetrachloroethane 62-127 2.4 20.0
19.8 99.010320.620.0µg/LTetrachloroethene 80-129 3.9 20.0
19.8 99.010220.420.0µg/LToluene 76-131 2.9 20.0
21.2 10697.519.520.0µg/L1,2,3-Trichlorobenzene 58-144 8.3 20.0
18.7 93.596.019.220.0µg/L1,2,4-Trichlorobenzene 66-139 2.6 20.0
19.7 98.510020.020.0µg/L1,1,1-Trichloroethane 75-135 1.5 20.0
19.6 98.010120.220.0µg/L1,1,2-Trichloroethane 70-140 3.0 20.0
20.2 10110320.620.0µg/LTrichloroethene 77-133 1.9 20.0
19.2 96.098.519.720.0µg/LTrichlorofluoromethane 62-148 2.5 20.0
19.6 98.099.519.920.0µg/L1,2,3-Trichloropropane 71-127 1.5 20.0
19.6 98.010120.220.0µg/L1,2,4-Trimethylbenzene 75-133 3.0 20.0
19.7 98.510120.120.0µg/L1,3,5-Trimethylbenzene 75-131 2.0 20.0
20.5 10310521.020.0µg/LVinyl Acetate 34-167 2.4 20.0
20.2 10110721.320.0µg/LVinyl Chloride 57-141 5.3 20.0
18.9 94.597.519.520.0µg/Lo-Xylene 78-128 3.1 20.0
40.0 10010140.540.0µg/Lm,p-Xylene 77-133 1.2 20.0
1001024-Bromofluorobenzene (S)80-124
99.498.8Dibromofluoromethane (S)75-129
98.698.61,2-Dichloroethane - d4 (S)63-136
100101Toluene-d8 (S)77-123
Page 15 of 22Date:05/05/2023 10:26 AM
Page 46 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
Associated Lab Samples: 94930, 94931
LRB-V32670 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/23 10:2419.83.48<3.48mg/KgAcenaphthene
05/03/23 10:2419.83.15<3.15mg/KgAcenaphthylene
05/03/23 10:2419.84.56<4.56mg/KgAniline
05/03/23 10:2419.84.29<4.29mg/KgAnthracene
05/03/23 10:2419.84.17<4.17mg/KgBenzo(a)anthracene
05/03/23 10:2419.84.41<4.41mg/KgBenzo(a)pyrene
05/03/23 10:2419.84.38<4.38mg/KgBenzo(b)fluoranthene
05/03/23 10:2419.84.08<4.08mg/KgBenzo(g,h,i)perylene
05/03/23 10:2419.84.11<4.11mg/KgBenzo(k)fluoranthene
05/03/23 10:2460.017.4<17.4mg/KgBenzoic Acid
05/03/23 10:2419.83.15<3.15mg/KgBenzyl alcohol
05/03/23 10:2419.83.54<3.54mg/KgBis(2-Chloroethoxy)methane
05/03/23 10:2419.83.21<3.21mg/KgBis(2-Chloroethyl)ether
05/03/23 10:249.904.08<4.08mg/KgBis(2-Chloroisopropyl)ether
05/03/23 10:2419.83.60<3.60mg/KgBis(2-ethylhexyl)phthalate
05/03/23 10:2419.83.27<3.27mg/Kg4-Bromophenyl phenyl ether
05/03/23 10:249.903.39<3.39mg/KgButyl benzyl phthalate
05/03/23 10:2419.82.77<2.77mg/Kg4-Chloro-3-methylphenol
05/03/23 10:249.903.36<3.36mg/Kg4-Chloroaniline
05/03/23 10:2419.83.48<3.48mg/Kg2-Chloronaphthalene
05/03/23 10:2419.82.95<2.95mg/Kg2-Chlorophenol
05/03/23 10:2430.03.78<3.78mg/Kg4-Chlorophenyl phenyl ether
05/03/23 10:2419.84.26<4.26mg/KgChrysene
05/03/23 10:2419.86.90<6.90mg/KgDibenz(a,h)anthracene
05/03/23 10:2419.83.57<3.57mg/KgDibenzofuran
05/03/23 10:2419.82.83<2.83mg/Kg1,2-Dichlorobenzene
05/03/23 10:2419.82.92<2.92mg/Kg1,3-Dichlorobenzene
Page 16 of 22Date:05/05/2023 10:26 AM
Page 47 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
Associated Lab Samples: 94930, 94931
LRB-V32670 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/23 10:249.902.93<2.93mg/Kg1,4-Dichlorobenzene
05/03/23 10:2419.84.41<4.41mg/Kg3,3'-Dichlorobenzidine
05/03/23 10:2419.82.87<2.87mg/Kg2,4-Dichlorophenol
05/03/23 10:2419.85.40<5.40mg/KgDiethyl phthalate
05/03/23 10:2419.85.22<5.22mg/KgDimethyl phthalate
05/03/23 10:249.903.24<3.24mg/Kg2,4-Dimethylphenol
05/03/23 10:2419.83.21<3.21mg/KgDi-n-butyl phthalate
05/03/23 10:2445.07.20<7.20mg/Kg4,6-Dinitro-2-methylphenol
05/03/23 10:2445.015.6<15.6mg/Kg2,4-Dinitrophenol
05/03/23 10:2419.82.90<2.90mg/Kg2,4-Dinitrotoluene
05/03/23 10:2419.83.24<3.24mg/Kg2,6-Dinitrotoluene
05/03/23 10:249.904.29<4.29mg/KgDi-n-Octyl Phthalate
05/03/23 10:2419.83.69<3.69mg/KgFluoranthene
05/03/23 10:2419.83.84<3.84mg/KgFluorene
05/03/23 10:2419.83.18<3.18mg/KgHexachlorobenzene
05/03/23 10:2419.82.93<2.93mg/KgHexachlorobutadiene
05/03/23 10:2419.84.71<4.71mg/KgHexachlorocyclopentadiene
05/03/23 10:2419.82.38<2.38mg/KgHexachloroethane
05/03/23 10:2419.85.37<5.37mg/KgIndeno(1,2,3-cd)pyrene
05/03/23 10:2419.85.73<5.73mg/KgIsophorone
05/03/23 10:2419.83.18<3.18mg/Kg1-Methylnaphthalene
05/03/23 10:2419.83.00<3.00mg/Kg2-Methylnaphthalene
05/03/23 10:2419.82.91<2.91mg/Kg2-Methylphenol
05/03/23 10:2419.82.55<2.55mg/Kg3&4 Methylphenol
05/03/23 10:2419.84.32<4.32mg/KgNaphthalene
05/03/23 10:2419.82.90<2.90mg/Kg2-Nitroaniline
05/03/23 10:2419.83.60<3.60mg/Kg3-Nitroaniline
Page 17 of 22Date:05/05/2023 10:26 AM
Page 48 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
Associated Lab Samples: 94930, 94931
LRB-V32670 Matrix: SOLLab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
05/03/23 10:249.902.80<2.80mg/Kg4-Nitroaniline
05/03/23 10:249.903.48<3.48mg/KgNitrobenzene
05/03/23 10:2419.82.66<2.66mg/Kg2-Nitrophenol
05/03/23 10:2419.83.51<3.51mg/Kg4-Nitrophenol
05/03/23 10:2419.87.89<7.89mg/KgN-Nitrosodimethylamine
05/03/23 10:2419.85.43<5.43mg/KgN-Nitrosodiphenylamine
05/03/23 10:2419.83.54<3.54mg/KgN-Nitroso-di-n-propylamine
05/03/23 10:2430.010.4<10.4mg/KgPentachlorophenol
05/03/23 10:2419.86.24<6.24mg/KgPhenanthrene
05/03/23 10:2419.83.36<3.36mg/KgPhenol
05/03/23 10:2419.84.02<4.02mg/KgPyrene
05/03/23 10:249.902.38<2.38mg/KgPyridine
05/03/23 10:2419.83.21<3.21mg/Kg1,2,4-Trichlorobenzene
05/03/23 10:2419.82.89<2.89mg/Kg2,4,5-Trichlorophenol
05/03/23 10:2419.82.90<2.90mg/Kg2,4,6-Trichlorophenol
05/03/23 10:242-Fluorobiphenyl (S)73.4 44-115
05/03/23 10:242-Fluorophenol (S)64.4 35-115
05/03/23 10:24Nitrobenzene-d5 (S)69.8 37-122
05/03/23 10:244-Terphenyl-d14 (S)81.4 54-127
05/03/23 10:242,4,6-Tribromophenol (S)64.3 39-132
05/03/23 10:24Phenol-d5 (S)62.0 34-121
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.5 73.074.837.450.0mg/KgAcenaphthene 40-123 2.4 20
Page 18 of 22Date:05/05/2023 10:26 AM
Page 49 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.8 75.676.838.450.0mg/KgAcenaphthylene 32-132 1.5 20
55.4 11111456.850.0mg/KgAniline 12-197 2.4 20
39.3 78.682.841.450.0mg/KgAnthracene 47-123 5.2 20
41.4 82.883.441.750.0mg/KgBenzo(a)anthracene 49-126 0.7 20
44.5 89.091.445.750.0mg/KgBenzo(a)pyrene 45-129 2.6 20
52.0 10410552.750.0mg/KgBenzo(b)fluoranthene 45-132 1.3 20
57.1 11411557.350.0mg/KgBenzo(g,h,i)perylene 43-134 0.3 20
45.7 91.492.646.350.0mg/KgBenzo(k)fluoranthene 47-132 1.3 20
35.2 70.478.439.250.0mg/KgBenzoic Acid 10-83 10.7 20
39.9 79.884.642.350.0mg/KgBenzyl alcohol 29-122 5.8 20
37.5 75.079.639.850.0mg/KgBis(2-Chloroethoxy)methane 36-121 5.9 20
32.4 64.869.834.950.0mg/KgBis(2-Chloroethyl)ether 31-120 7.4 20
37.4 74.880.040.050.0mg/KgBis(2-Chloroisopropyl)ether 33-131 6.7 20
47.7 95.495.847.950.0mg/KgBis(2-ethylhexyl)phthalate 51-133 0.4 20
38.5 77.079.239.650.0mg/Kg4-Bromophenyl phenyl ether 46-124 2.8 20
46.7 93.494.047.050.0mg/KgButyl benzyl phthalate 48-132 0.6 20
39.7 79.480.440.250.0mg/Kg4-Chloro-3-methylphenol 45-122 1.2 20
36.4 72.869.634.850.0mg/Kg4-Chloroaniline 17-106 4.4 20
36.2 72.475.437.750.0mg/Kg2-Chloronaphthalene 41-114 4.0 20
36.2 72.477.838.950.0mg/Kg2-Chlorophenol 34-121 7.1 20
39.3 78.681.040.550.0mg/Kg4-Chlorophenyl phenyl ether 45-121 3.0 20
38.5 77.077.238.650.0mg/KgChrysene 50-124 0.2 20
55.9 11211054.850.0mg/KgDibenz(a,h)anthracene 45-134 1.9 20
36.8 73.675.237.650.0mg/KgDibenzofuran 44-120 2.1 20
31.4 62.869.034.550.0mg/Kg1,2-Dichlorobenzene 33-117 9.4 20
30.4 60.866.633.350.0mg/Kg1,3-Dichlorobenzene 30-115 9.1 20
Page 19 of 22Date:05/05/2023 10:26 AM
Page 50 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
30.0 60.066.633.350.0mg/Kg1,4-Dichlorobenzene 31-115 10.4 20
38.5 77.071.035.550.0mg/Kg3,3'-Dichlorobenzidine 22-121 8.1 20
38.8 77.679.239.650.0mg/Kg2,4-Dichlorophenol 40-122 2.0 20
40.9 81.883.041.550.0mg/KgDiethyl phthalate 50-124 1.4 20
40.1 80.280.440.250.0mg/KgDimethyl phthalate 48-124 0.2 20
49.2 98.410351.450.0mg/Kg2,4-Dimethylphenol 30-127 4.3 20
46.3 92.694.247.150.0mg/KgDi-n-butyl phthalate 51-128 1.7 20
39.0 78.079.039.550.0mg/Kg4,6-Dinitro-2-methylphenol 29-132 1.2 20
49.6 99.297.048.550.0mg/Kg2,4-Dinitrophenol 27-129 2.2 20
43.3 86.686.643.350.0mg/Kg2,4-Dinitrotoluene 48-126 0.0 20
42.1 84.283.841.950.0mg/Kg2,6-Dinitrotoluene 46-124 0.4 20
66.6 13313467.050.0mg/KgDi-n-Octyl Phthalate 45-140 0.5 20
38.9 77.878.239.150.0mg/KgFluoranthene 50-127 0.5 20
38.6 77.278.439.250.0mg/KgFluorene 43-125 1.5 20
36.8 73.674.437.250.0mg/KgHexachlorobenzene 45-122 1.0 20
32.9 65.870.635.350.0mg/KgHexachlorobutadiene 32-123 7.0 20
35.0 70.072.236.150.0mg/KgHexachlorocyclopentadiene 32-117 3.0 20
30.8 61.667.233.650.0mg/KgHexachloroethane 28-117 8.6 20
61.7 12311959.650.0mg/KgIndeno(1,2,3-cd)pyrene 45-133 3.4 20
33.8 67.669.634.850.0mg/KgIsophorone 30-122 2.9 20
33.7 67.470.835.450.0mg/Kg1-Methylnaphthalene 40-119 4.9 20
34.1 68.272.036.050.0mg/Kg2-Methylnaphthalene 38-122 5.4 20
37.8 75.680.440.250.0mg/Kg2-Methylphenol 32-122 6.1 20
35.4 70.872.236.150.0mg/Kg3&4 Methylphenol 34-119 1.9 20
32.7 65.470.235.150.0mg/KgNaphthalene 35-123 7.0 20
44.7 89.489.644.850.0mg/Kg2-Nitroaniline 44-127 0.2 20
Page 20 of 22Date:05/05/2023 10:26 AM
Page 51 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V32788QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3546
QC Prep:V32670
LCS-V32670 LCSD-V32670Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.6 79.271.835.950.0mg/Kg3-Nitroaniline 33-119 9.8 20
40.4 80.878.439.250.0mg/Kg4-Nitroaniline 63-147 3.0 20
32.3 64.669.834.950.0mg/KgNitrobenzene 34-122 7.7 20
37.1 74.279.439.750.0mg/Kg2-Nitrophenol 36-123 6.7 20
42.5 85.086.043.050.0mg/Kg4-Nitrophenol 30-132 1.1 20
28.9 57.862.031.050.0mg/KgN-Nitrosodimethylamine 10-146 7.0 20
46.4 92.894.047.050.0mg/KgN-Nitrosodiphenylamine 38-127 1.2 20
37.4 74.879.639.850.0mg/KgN-Nitroso-di-n-propylamine 36-120 6.2 20
42.9 85.885.242.650.0mg/KgPentachlorophenol 25-133 0.7 20
38.4 76.878.439.250.0mg/KgPhenanthrene 50-121 2.0 20
35.7 71.476.038.050.0mg/KgPhenol 34-121 6.2 20
39.0 78.077.238.650.0mg/KgPyrene 47-127 1.0 20
18.9 37.840.220.150.0mg/KgPyridine 10-80 6.1 20
32.3 64.668.434.250.0mg/Kg1,2,4-Trichlorobenzene 34-118 5.7 20
39.8 79.681.040.550.0mg/Kg2,4,5-Trichlorophenol 41-124 1.7 20
39.1 78.280.840.450.0mg/Kg2,4,6-Trichlorophenol 39-126 3.2 20
73.475.82-Fluorobiphenyl (S)44-115
66.770.72-Fluorophenol (S)35-115
67.673.2Nitrobenzene-d5 (S)37-122
82.081.84-Terphenyl-d14 (S)54-127
72.672.32,4,6-Tribromophenol (S)39-132
63.768.1Phenol-d5 (S)34-121
Page 21 of 22Date:05/05/2023 10:26 AM
Page 52 of 55
Quality Control Data
23-117-0011Report No:
Project Description:
Client ID:Resolve Environmental
Bakers Quarry
Dry Weight Determination
SW-DRYWT
V32569QC Analytical Batch:
Analysis Method:
Analysis Description:
V 94908-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/30/23 12:451.413.713.9%Moisture
V 95015-DUPDuplicate
Max RPD
Parameter
AnalyzedRPDDUP
Result
Result
Units
20.0 04/30/23 12:4513.94.885.61%Moisture
Page 22 of 22Date:05/05/2023 10:26 AM
Page 53 of 55
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:23-117-0011
Resolve Environmental
00238
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 0.5C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
ü
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)ü
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Danyale Love Date & Time:04/27/2023 10:55:32
Special precautions or instructions included?
Comments:
Page 54 of 55
Page 55 of 55