09005_Canac Kitchens_Soils Request Correspondence_2023May24

1
Peacock, David
From:Frazier, William O <[e-mail]>
Sent:Wednesday, May 24, 2023 1:24 PM
To:Peacock, David; Bill Wickesberg
Cc:Dave Wamre; Thompson, Jordan L; Eric Schwarzkopf; Brinke, Hayden; Miller, Connor;
McCall, Robert; Heher, Eliot; Kerkhoff, Andrew
Subject:RE: [External] RE: Ashley Furniture Plant/Statesville, NC; Canac Kitchens (09005-05-049) -
EMP Approval
Attachments:Canac_Tables 1 and 2_Soil Analytical Data.pdf; 92667899_frc.pdf; Canac_Risk
Calculator_Soil Exposure (Slab Modifications).pdf; Appendix D - DEQ Risk Calculator_Soil
Exposure (Ashley Furniture).pdf; Table 1_Analytical Data (Ashley Furniture).pdf; Figure 3 -
Proposed Soil Reuse Area.pdf
Follow Up Flag:Follow up
Flag Status:Flagged
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Afternoon David,

Last week, we completed the soil sampling of the stockpiled soils in accordance with the procedures in the EMP. Based
on our field screening, there were two stockpiles (or more accurately, two types of stockpiles as the excavation
contractor created multiple stockpiles for site logistics/convenience reasons) to characterize: soils originating from
excavations at slab cuts where we identified evidence of potential impact (“Potentially Impacted”) and soils originating
from excavations at slab cuts where such evidence was not observed (“Presumed Clean”). I have a attached the lab
report, the summary data table (includes the prior grab VOC results from slab cut #26), and a risk assessment using the
highest concentration of each compound detected (including concentrations from the initial grab VOC sample).

Concentrations of VOCs, SVOCs, RCRA metals, and hexavalent chromium were not detected above their PSRGs in the
sample (and the duplicate) associated with the “Presumed Clean” stockpiled soil (SS-1 and DUP-01). Methylene chloride
was detected slightly in excess of its Protection of Groundwater PSRG and arsenic was detected above its Residential
PSRG (but not its PoG or Non-Residential PSRG) in the sample associated with the “Potentially Impacted” stockpiled
soil. The concentration of arsenic within this sample is similar to the concentrations detected within the other sample
(only slightly lower and below the PoG PSRG) and appears consistent with naturally occurring background
concentrations we see in the Piedmont of North Carolina.

The risk calculator indicates a carcinogenic risk to non-residential workers and construction workers in the 10^-7 and
10^8 range. The hazard indices for both exposure scenarios are below 0.1. Based on the risk evaluation and the small
quantity of soils contained in the “Potentially Impacted” stockpile (1 to 2 cubic yards), we do not feel that the methylene
chloride PoG exceedance warrants disposal to a lined Subtitle D landfill. I would note that Terracon assisted the
previous owner of the site (Ashley Furniture) with characterization of some excavated soils in 2022, which were found to
contain concentrations of chloromethane in excess of its PoG PSRG and DEQ provided approval to spread those soils on
the site based on the risk levels (slightly higher than the apparent risk we’ve identified from the soils currently stockpiled
on site). I have attached the summary data table and risk assessment from that prior characterization event.

Based on the above, we request approval for Dura to spread all stockpiled soils generated from their slab modification
work on the site in the location included in Figure 3 of the EMP (also attached for reference). Please let us know if we
2
can proceed with soil disposal operations, or if that determination must wait on the formal report documenting the
excavation, excavation oversight, and sampling results.

On a related note, we are still awaiting more specific information from Spectrum regarding the proposed fiber line
installation project. Dura and the property owner are ready to move forward with the concrete apron installation work
in the northwestern portion of the property. As such, we will be preparing the requested EMP addendum for your
review and approval shortly, to cover solely the apron work. A separate addendum will be prepared once the final
details on the fiber line installation have been decided.

Thanks,
Will

Will Frazier, P.G.
Licensed in North Carolina
Project Geologist

2701 Westport Road I Charlotte, North Carolina 28208
P [phone] I F [phone] I M [phone]
[e-mail] I Terracon.com

From: Peacock, David <[e-mail]>
Sent: Wednesday, May 10, 2023 11:43 AM
To: Frazier, William O <[e-mail]>; Bill Wickesberg <[e-mail]>
Cc: Dave Wamre <[e-mail]>; Thompson, Jordan L <[e-mail]>; Eric
Schwarzkopf <[e-mail]>; Brinke, Hayden <[e-mail]>; Miller, Connor
<[e-mail]>
Subject: RE: [External] RE: Ashley Furniture Plant/Statesville, NC; Canac Kitchens (09005-05-049) - EMP Approval

Will:

After reviewing the supplied analytical data, I ran the results through the DEQ Risk Calculator for additional measure
showing the low exposure risks of the volatile impacts located at cut #26. I agree with your assertion that no other
mitigation measures are necessary given the very low sample results concentrations and the limited visible extent of the
impacted area. Please continue with the concrete repair as indicated. However, any suspect soils removed from the area
should continue to be segregated and stockpiled accordingly. The final composite sampling (including metals, etc..) will
help with determining final disposal options.

DP

3
David Peacock
Env. Program Consultant, Brownfields Property Management Branch
Brownfields Redevelopment Section
Division of Waste Management
North Carolina Department of Environmental Quality
910.796.7401 (Office) | 919.280.3408 (Mobile)
[e-mail]

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

Join our Land Use Restrictions Update (LURU) reminder list: http://eepurl.com/cvVzfr

One-Stop Project Data Gate (Map, Inventory, Documents): http://deq.nc.gov/brownfields-sites-and-boundaries

From: Frazier, William O <[e-mail]>
Sent: Wednesday, May 10, 2023 10:32 AM
To: Peacock, David <[e-mail]>; Bill Wickesberg <[e-mail]>
Cc: Dave Wamre <[e-mail]>; Thompson, Jordan L <[e-mail]>; Eric
Schwarzkopf <[e-mail]>; Brinke, Hayden <[e-mail]>; Miller, Connor
<[e-mail]>
Subject: RE: [External] RE: Ashley Furniture Plant/Statesville, NC; Canac Kitchens (09005-05-049) - EMP Approval

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Morning David,

I have attached the laboratory report and summary table of the VOC analytical results from our sampling of the hot spot
at slab cut #26. A handful of petroleum-related compounds were detected above laboratory method detection limits.
Of these, the methylene chloride and naphthalene concentrations exceed their protection of groundwater PSRG. Given
the 950 ppm field screening value, these relatively low concentrations appear to indicate whatever release that occurred
happened quite some time ago and that most of the compounds present in the material released have had time to
break down and naturally attenuate a good bit in the subsurface. Taken together with the apparently limited spatial
extent of the impacts, we do not see the need to pursue installation of a vapor barrier prior to re-pouring of the
concrete at slab cut #26.

Regarding slab cut #22: yesterday prior to removing the concrete, we completed additional field screening in the sawcut
crack. Elevated PID readings were not observed in the crack at the southern end of this cut as they had been
previously. Upon removing the concrete, a hot spot such as the one at slab cut #26 was not identified. As the slab cut is
narrow (15-feet long by 3-feet wide), rather than delineate in a radius, Terracon collected field screening of three soil
samples collected from the southernmost portion, the middle, and the northernmost portion of the exposed soil
area. The soil samples were collected from beneath where an expansion seam/gap in two portions of the existing slab
had been located, as we would expect that as the most likely route for surface spills to enter the sub-slab—see the
attached picture for reference (please disregard the spray painted 18 marked on the concrete; those numbers do not
correspond to the numbering system on the figure we provided). The highest PID reading observed during this field
screening was 5.4 ppm. Based on these observations, it appears that impacts at this location are minor and also do not
appear to pose a concern requiring additional actions.

We have not yet made observations at slab cut #30 as the concrete has not been removed.

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Please advise if DEQ feels that additional action is required at slab cut #26. We would like to proceed with re-pouring of
concrete as soon as possible, as Dura cannot move their machinery into the building until after the concrete has cured
for 30 days.

Thanks,
Will

Will Frazier, P.G.
Licensed in North Carolina
Project Geologist

2701 Westport Road I Charlotte, North Carolina 28208
P [phone] I F [phone] I M [phone]
[e-mail] I Terracon.com

From: Peacock, David <[e-mail]>
Sent: Monday, May 8, 2023 10:49 AM
To: Frazier, William O <[e-mail]>; Bill Wickesberg <[e-mail]>
Cc: Dave Wamre <[e-mail]>; Thompson, Jordan L <[e-mail]>; Eric
Schwarzkopf <[e-mail]>; Brinke, Hayden <[e-mail]>; Miller, Connor
<[e-mail]>
Subject: RE: [External] RE: Ashley Furniture Plant/Statesville, NC; Canac Kitchens (09005-05-049) - EMP Approval

Hi Will,

Going by the provided information and photos the suspected VOC impacted soils in cut #26 appear to have a very minor
extent relative to the exposed soils, which I concur with your thoughts on the source. Hopefully that remains evident as
soils are being removed from the cut area for the thicken slab upfit. The sampling results should help with next steps in
addressing soil disposal. Please continue to keep us updated on the progress and those sampling results.

Sincerely,
DP

David Peacock
Env. Program Consultant, Brownfields Property Management Branch
Brownfields Redevelopment Section
Division of Waste Management
North Carolina Department of Environmental Quality
910.796.7401 (Office) | 919.280.3408 (Mobile)
[e-mail]

Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.

Table 1
Summary of Soil Analytical Results
Canac Kitchens Brownfields Site
607 Meacham Road
Statesville, Iredell County, North Carolina
Terracon Project No. 71217582
Sample ID:CS-01 DUP-01
Highest PID Reading (ppm):0.1 0.1
0.0329 0.007J 0.015 23 99
1,2,4-Trimethylbenzene <0.0018 0.0047J 12 63 370
Compounds Not Detected Above Laboratory MDLs.
RCRA Metals and Nickel by EPA Method 6010/7471 (Chromium VI by Method 7199)
Arsenic 1.4 J 1.7 J 5.8 0.68 3.0
Barium 83.6 77.9 580 3,100 47,000
Cadium 0.59 0.47 3 1.4 20
Chromium, Trivalent 46.2 37.4 360,000 23,000 350,000
Chromium , Hexavalent 0.686 J 0.864 J 3.8 0.31 6.5
Lead 12.7 14.8 270 400 800
Mercury 0.054 0.039 1 2.3 9.7
Nickel 24.4 21.3 130 310 4700
Selenium 0.85 1.1 2.1 78 1200
Notes:
Samples collected 3/21/22
Results are shown in milligrams per kilogram (mg/kg).
PID = Photo-ionization detector
ppm - parts per million
Only compounds detected within one or more sample are shown.
Detections are indicated in bold.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
PSRG - NCDEQ Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (January 2022)
Shaded cells indicate the detected concentrations exceed the regulatory threshold of the corresponding color.
Residential PSRGs Non-Residential
PSRGs
Volatile Organic Compounds by EPA Method 8260
Semi-Volatile Organic Compounds by EPA Method 8270
PoG PSRG
Chloromethane
Table 2
Summary of Soil Stockpile Analytical Results
Canac Kitchens
Brownfields ID. 09005-05-049
607 Meacham Road
Statesville, Iredell County, North Carolina
Terracon Project No. 71237109
Sample ID SS-1 DUP-01 SS-2
Highest PID Reading (ppm)4.6 4.6 0.9
Volatile Organic Compounds by EPA Method 8260
Acetone <0.0037 <0.0321 0.104 J 25 1,400 210,000
Ethylbenzene <0.0024 <0.0023 0.0161 6.1 27 13
Isopropylbenzene (Cumene)<0.0018 <0.0017 0.399 2.3 410 2,100
p-Isopropyltoluene <0.0026 <0.0025 0.712 NE NE NE
Methylene Chloride <0.0144 <0.0137 0.203 0.025 58 650
Naphthalene <0.0028 <0.0026 0.0116 J 0.39 2.1 8.8
n-Propylbenzene <0.0019 <0.0018 1.41 2.6 780 5,100
Toluene <0.0036 <0.0035 0.0309 8.3 990 9,700
1,2,4-Trimethylbenzene <0.0031 <0.0030 11.1 12 63 370
1,3,5-Trimethylbenzene <0.0018 <0.0017 3.65 11 56 320
m&p-Xylene <0.0036 <0.0034 0.0763 9.8 120 500
o-Xylene <0.0023 <0.0022 0.22 9.8 140 590
Total Xylene <0.0030 <0.0029 0.297 9.9 120 530
Semi-Volatile Organic Compounds by EPA Method 8270
RCRA Metals by EPA Method 6010/7471 (Chromium VI by Method 7199)
Arsenic 0.58 J 0.60 J 0.77 J 5.8 0.68 3
Barium 278 343 298 580 3,100 47,000
Cadmium 0.35 0.23 0.16 3 1.4 20
Chromium (III)94.1 61.8 66.5 360,000 23,000 350,000
Chromium (VI)<0.289 <0.286 <0.271 3.8 0.31 6.5
Lead 9.9 3.2 1.9 270 400 800
Selenium <0.58 <0.36 <0.48 2.1 78 1,200
Silver 0.045 J 0.11 J 0.16 J 3.4 78 1,200
Mercury 0.0044 J 0.0079 J 0.0090 NE 4.7 70
Notes:
All samples collected on May 17, 2023.
Results are shown in milligrams per kilogram (mg/kg).
PID = Photo-ionization detector
ppm - parts per million
Only compounds detected above the laboratory method detection limits are shown.
Detections are indicated in bold.
PSRG - NCDEQ Inactive Hazardous Sites Branch Preliminary Soil Remediation Goals (January 2023)
PoG - Protection of Groundwater
Shaded cells indicate the detected concentrations exceed the regulatory threshold of the corresponding color.
PoG PSRG Residential PSRGs Non-Residential
PSRGs
Compounds Not Detected above Laboratory MDLs
Version Date:
Basis:
Site Name:
Site Address:
DEQ Section:
Site ID:
Exposure Unit ID:
Submittal Date:
Reviewed By:
Soils from Slab Modification Excavations (Worst Case Exposure)
North Carolina Department of Environmental Quality
Risk Calculator
Canac Kitchens
607 Meacham Road, Statesville, Iredell County, North Carolina
Brownfields Redevelopment Section
09005-05-049
January 2023
November 2022 EPA RSL Table
Prepared By:Terracon Consultants, Inc.
North Carolina DEQ Risk Calculator
Complete Exposure Pathways
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 09005-05-049
Exposure Unit ID: Soils from Slab Modification Excavations (Worst Case Exposure)
Note: Risk output will only be calculated for complete exposure pathways.
Receptor Pathway
Check box if
pathway
complete
Soil
Groundwater Use
Soil
Groundwater Use
Construction Worker Soil
Soil
Surface Water
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Groundwater to Indoor Air
Soil Gas to Indoor Air
Indoor Air
Source Soil
Source Groundwater
Source Soil
Source Groundwater
Input Form 1A
VAPOR INTRUSION PATHWAYS
DIRECT CONTACT SOIL AND WATER PATHWAYS
Resident
Non-Residential Worker
Recreator/Trespasser
Resident
Non-Residential Worker
CONTAMINANT MIGRATION PATHWAYS
Groundwater
Surface Water
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 09005-05-049
Exposure Unit ID: Soils from Slab Modification Excavations (Worst Case Exposure)
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil 3.1E-07 1.6E-02 NO
Groundwater Use*NC NC NC
Construction Worker Soil 5.4E-08 6.9E-02 NO
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not modeled, user did not check this pathway as complete.
4. NC = Pathway not calculated, required contaminant migration parameters were not entered.
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
North Carolina DEQ Risk Calculator
Risk for Individual Pathways Output Form 1A
Version Date: January 2022
Basis: November 2021 EPA RSL Table
Site ID:
Exposure Unit ID: Soil Stockpiles
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil 7.6E-06 2.5E-02 NO
Groundwater Use*NC NC NC
Construction Worker Soil 1.3E-05 1.6E-01 NO
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway
Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not calculated
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1. If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator
Exposure Point Concentrations
Version Date: January 2023
Basis: November 2022 EPA RSL Table
Site ID: 09005-05-049
Exposure Unit ID: Soils from Slab Modification Excavations (Worst Case Exposure)
NOTE: If the chemical list is changed from a prior calculator run, remember to select "See All Chemicals" on the data output sheet or newly added chemicals will not be included in risk calculations
Exposure Point
Concentration
(mg/kg)
Notes:CAS Number
Chemical
For the chemicals highlighted in blue, data entry notes are provided in the
PSRG Table link on the Main Menu
Minimum
Concentration
(Qualifier)
Maximum
Concentration
(Qualifier)
Units
Location of
Maximum
Concentration
Detection
Frequency
0.104 67-64-1 Acetone mg/kg
0.77 7440-38-2 Arsenic, Inorganic mg/kg
343 7440-39-3 Barium mg/kg
0.35 7440-43-9 Cadmium (Diet)mg/kg
94.1 16065-83-1 Chromium(III), Insoluble Salts mg/kg
0.399 98-82-8 Cumene mg/kg
0.0161 100-41-4 Ethylbenzene mg/kg
9.9 7439-92-1 ~Lead and Compounds mg/kg
0.009 7487-94-7 ~Mercuric Chloride (and other Mercury salts)mg/kg
0.203 75-09-2 Methylene Chloride mg/kg
0.499 91-20-3 ~Naphthalene mg/kg
1.41 103-65-1 Propyl benzene mg/kg
0.16 7440-22-4 Silver mg/kg
0.0309 108-88-3 Toluene mg/kg
11.1 95-63-6 Trimethylbenzene, 1,2,4-mg/kg
3.65 108-67-8 Trimethylbenzene, 1,3,5-mg/kg
0.0888 108-38-3 Xylene, m-mg/kg
0.22 95-47-6 Xylene, o-mg/kg
0.0888 106-42-3 Xylene, p-mg/kg
0.297 1330-20-7 Xylenes mg/kg
Soil Exposure Point Concentration Table
Description of Exposure Point Concentration Selection:
North Carolina DEQ Risk Calculator
Range of
Detection Limits
Concentration
Used for
Screening
Background
Value
Screening
Toxicity Value
(Screening
Level) (n/c)
Potential
ARAR/TBC
Value
Potential
ARAR/TBC
Source
COPC
Flag
(Y/N)
Rationale for
Selection or
Deletion
Input Form 2A
North Carolina DEQ Risk Calculator
Map of Proposed Excavated Soil Re-Use Area FIGURENO.
@A @A
@A@A
Meacham RoadSpeedball Road
Proposed SoilRe-Use Area
Proposed ExcavationAreas (see Figure 2 forExact Locations)
MW-4 MW-6
MW-7MW-8
NC Center for Geographic Information & Analysis
Legend
@A Monitoring WellsSite BoundaryTax Parcels
Environmental Management PlanCanac Kitchens Brownfields SiteDura Supreme Slab ModificationsNCBP ID# 09005-05-049607 Meacham RoadStatesville, Iredell County, North Carolina2701 Westport Road Charlotte, North Carolina 28208Phone: [phone] Fax: [phone]
³
0 250 500125Feet
PM:
Drawn By:
Checked By:
Approved By:
WOF
WOF
RSB
RSB
Project No:
Scale:
Filename:
Date:March 2023
71227537_EMP_3
1 inch = 250 feet
71237109
3
#=CL#
May 22, 2023
LIMS USE: FR - WILL FRAZIER
LIMS OBJECT ID: 92667899
92667899
Project:
Pace Project No.:
RE:
Will Frazier
Terracon
2701 Westport Rd
Charlotte, NC 28208
71237109-CANAC KITCHENS BROWNF
Dear Will Frazier:
Enclosed are the analytical results for sample(s) received by the laboratory on May 17, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National - Mt. Juliet
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor M Cannon
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 49
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Lab ID Sample ID Matrix Date Collected Date Received
92667899001 SS-1 Solid 05/17/23 11:50 05/17/23 13:55
92667899002 DUP-1 Solid 05/17/23 11:55 05/17/23 13:55
92667899003 SS-2 Solid 05/17/23 12:30 05/17/23 13:55
92667899004 EQUIP BLANK Water 05/17/23 12:45 05/17/23 13:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 49
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92667899001 SS-1 EPA 6010D 7 PASI-ADBB1
EPA 7471B 1 PASI-ANMP
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667899002 DUP-1 EPA 6010D 7 PASI-ADBB1
EPA 7471B 1 PASI-ANMP
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667899003 SS-2 EPA 6010D 7 PASI-ADBB1
EPA 7471B 1 PASI-ANMP
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CLMB
SW-846 1 PASI-CKDF
SM 2540G 1 PANCMK
EPA 7199 1 PANVSS
92667899004 EQUIP BLANK EPA 8260D 71 PASI-CJJK
PAN = Pace National - Mt. Juliet
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-1 Lab ID:92667899001 Collected:05/17/23 11:50 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 0.59J mg/kg 05/19/23 11:05 7440-38-205/18/23 09:222.5 0.089 1
Barium 278 mg/kg 05/19/23 11:05 7440-39-305/18/23 09:221.0 0.095 1
Cadmium 0.35 mg/kg 05/19/23 11:05 7440-43-905/18/23 09:220.10 0.012 1
Chromium 94.1 mg/kg 05/19/23 11:05 7440-47-305/18/23 09:220.51 0.13 1
Lead 9.9 mg/kg 05/19/23 11:05 7439-92-105/18/23 09:221.0 0.24 1
Selenium ND mg/kg 05/19/23 11:05 7782-49-205/18/23 09:221.0 0.58 1
Silver 0.045J mg/kg 05/19/23 11:05 7440-22-405/18/23 09:220.51 0.037 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.0044J mg/kg 05/18/23 14:07 7439-97-605/18/23 10:280.0049 0.0030 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/18/23 11:47 83-32-905/17/23 16:273411201
Acenaphthylene ND ug/kg 05/18/23 11:47 208-96-805/17/23 16:273411201
Aniline ND ug/kg 05/18/23 11:47 62-53-305/17/23 16:273411331
Anthracene ND ug/kg 05/18/23 11:47 120-12-705/17/23 16:273411111
Benzo(a)anthracene ND ug/kg 05/18/23 11:47 56-55-305/17/23 16:273411141
Benzo(a)pyrene ND ug/kg 05/18/23 11:47 50-32-805/17/23 16:273411181
Benzo(b)fluoranthene ND ug/kg 05/18/23 11:47 205-99-205/17/23 16:273411141
Benzo(g,h,i)perylene ND ug/kg 05/18/23 11:47 191-24-205/17/23 16:273411321
Benzo(k)fluoranthene ND ug/kg 05/18/23 11:47 207-08-905/17/23 16:273411201
Benzoic Acid ND ug/kg 05/18/23 11:47 65-85-005/17/23 16:2717007321
Benzyl alcohol ND ug/kg 05/18/23 11:47 100-51-605/17/23 16:276812581
4-Bromophenylphenyl ether ND ug/kg 05/18/23 11:47 101-55-305/17/23 16:273411311
Butylbenzylphthalate ND ug/kg 05/18/23 11:47 85-68-705/17/23 16:273411431
4-Chloro-3-methylphenol ND ug/kg 05/18/23 11:47 59-50-705/17/23 16:276812391
4-Chloroaniline ND ug/kg 05/18/23 11:47 106-47-805/17/23 16:276812671
bis(2-Chloroethoxy)methane ND ug/kg 05/18/23 11:47 111-91-105/17/23 16:273411411
bis(2-Chloroethyl) ether ND ug/kg 05/18/23 11:47 111-44-405/17/23 16:273411281
2-Chloronaphthalene ND ug/kg 05/18/23 11:47 91-58-705/17/23 16:273411351
2-Chlorophenol ND ug/kg 05/18/23 11:47 95-57-805/17/23 16:273411281
4-Chlorophenylphenyl ether ND ug/kg 05/18/23 11:47 7005-72-305/17/23 16:273411271
Chrysene ND ug/kg 05/18/23 11:47 218-01-905/17/23 16:273411241
Dibenz(a,h)anthracene ND ug/kg 05/18/23 11:47 53-70-305/17/23 16:273411311
Dibenzofuran ND ug/kg 05/18/23 11:47 132-64-905/17/23 16:273411231
1,2-Dichlorobenzene ND ug/kg 05/18/23 11:47 95-50-105/17/23 16:273411231
1,3-Dichlorobenzene ND ug/kg 05/18/23 11:47 541-73-105/17/23 16:273411211
1,4-Dichlorobenzene ND ug/kg 05/18/23 11:47 106-46-705/17/23 16:273411301
3,3'-Dichlorobenzidine ND ug/kg 05/18/23 11:47 91-94-105/17/23 16:276812301
2,4-Dichlorophenol ND ug/kg 05/18/23 11:47 120-83-205/17/23 16:273411331
Diethylphthalate ND ug/kg 05/18/23 11:47 84-66-205/17/23 16:273411251
2,4-Dimethylphenol ND ug/kg 05/18/23 11:47 105-67-905/17/23 16:273411411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-1 Lab ID:92667899001 Collected:05/17/23 11:50 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 05/18/23 11:47 131-11-305/17/23 16:273411241
Di-n-butylphthalate ND ug/kg 05/18/23 11:47 84-74-205/17/23 16:273411151
4,6-Dinitro-2-methylphenol ND ug/kg 05/18/23 11:47 534-52-105/17/23 16:276813181
2,4-Dinitrophenol ND ug/kg 05/18/23 11:47 51-28-505/17/23 16:27170010501
2,4-Dinitrotoluene ND ug/kg 05/18/23 11:47 121-14-205/17/23 16:273411311
2,6-Dinitrotoluene ND ug/kg 05/18/23 11:47 606-20-205/17/23 16:273411251
Di-n-octylphthalate ND ug/kg 05/18/23 11:47 117-84-005/17/23 16:273411341
bis(2-Ethylhexyl)phthalate ND ug/kg 05/18/23 11:47 117-81-705/17/23 16:273411321
Fluoranthene ND ug/kg 05/18/23 11:47 206-44-005/17/23 16:273411171
Fluorene ND ug/kg 05/18/23 11:47 86-73-705/17/23 16:273411201
Hexachloro-1,3-butadiene ND ug/kg 05/18/23 11:47 87-68-305/17/23 16:273411481
Hexachlorobenzene ND ug/kg 05/18/23 11:47 118-74-105/17/23 16:273411331
Hexachlorocyclopentadiene ND ug/kg 05/18/23 11:47 77-47-405/17/23 16:273411951
Hexachloroethane ND ug/kg 05/18/23 11:47 67-72-105/17/23 16:273411301
Indeno(1,2,3-cd)pyrene ND ug/kg 05/18/23 11:47 193-39-505/17/23 16:273411341
Isophorone ND ug/kg 05/18/23 11:47 78-59-105/17/23 16:273411521
1-Methylnaphthalene ND ug/kg 05/18/23 11:47 90-12-005/17/23 16:273411201
2-Methylnaphthalene ND ug/kg 05/18/23 11:47 91-57-605/17/23 16:273411361
2-Methylphenol(o-Cresol)ND ug/kg 05/18/23 11:47 95-48-705/17/23 16:273411391
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/18/23 11:47 15831-10-405/17/23 16:273411371
Naphthalene ND ug/kg 05/18/23 11:47 91-20-305/17/23 16:273411161
2-Nitroaniline ND ug/kg 05/18/23 11:47 88-74-405/17/23 16:2717002791
3-Nitroaniline ND ug/kg 05/18/23 11:47 99-09-205/17/23 16:2717002671
4-Nitroaniline ND ug/kg 05/18/23 11:47 100-01-605/17/23 16:276812591
Nitrobenzene ND ug/kg 05/18/23 11:47 98-95-305/17/23 16:273411581
2-Nitrophenol ND ug/kg 05/18/23 11:47 88-75-505/17/23 16:273411481
4-Nitrophenol ND ug/kg 05/18/23 11:47 100-02-705/17/23 16:2717006581
N-Nitrosodimethylamine ND ug/kg 05/18/23 11:47 62-75-905/17/23 16:273411151
N-Nitroso-di-n-propylamine ND ug/kg 05/18/23 11:47 621-64-705/17/23 16:273411281
N-Nitrosodiphenylamine ND ug/kg 05/18/23 11:47 86-30-605/17/23 16:273411211
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/18/23 11:47 108-60-105/17/23 16:273411621
Pentachlorophenol ND ug/kg 05/18/23 11:47 87-86-505/17/23 16:276813331
Phenanthrene ND ug/kg 05/18/23 11:47 85-01-805/17/23 16:273411111
Phenol ND ug/kg 05/18/23 11:47 108-95-205/17/23 16:273411521
Pyrene ND ug/kg 05/18/23 11:47 129-00-005/17/23 16:273411381
Pyridine ND ug/kg 05/18/23 11:47 110-86-105/17/23 16:273411071
1,2,4-Trichlorobenzene ND ug/kg 05/18/23 11:47 120-82-105/17/23 16:273411341
2,4,5-Trichlorophenol ND ug/kg 05/18/23 11:47 95-95-405/17/23 16:273411561
2,4,6-Trichlorophenol ND ug/kg 05/18/23 11:47 88-06-205/17/23 16:273411401
Surrogates
Nitrobenzene-d5 (S)43 %05/18/23 11:47 4165-60-005/17/23 16:2710-130 1
2-Fluorobiphenyl (S)44 %05/18/23 11:47 321-60-805/17/23 16:2710-130 1
Terphenyl-d14 (S)48 %05/18/23 11:47 1718-51-005/17/23 16:2710-130 1
Phenol-d6 (S)39 %05/18/23 11:47 13127-88-305/17/23 16:2710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-1 Lab ID:92667899001 Collected:05/17/23 11:50 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)40 %05/18/23 11:47 367-12-405/17/23 16:2710-130 1
2,4,6-Tribromophenol (S)48 %05/18/23 11:47 118-79-605/17/23 16:2710-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/18/23 06:42 67-64-105/17/23 23:2010533.7 1
Benzene ND ug/kg 05/18/23 06:42 71-43-205/17/23 23:205.2 2.1 1
Bromobenzene ND ug/kg 05/18/23 06:42 108-86-105/17/23 23:205.2 1.7 1
Bromochloromethane ND ug/kg 05/18/23 06:42 74-97-505/17/23 23:205.2 1.6 1
Bromodichloromethane ND ug/kg 05/18/23 06:42 75-27-405/17/23 23:205.2 2.0 1
Bromoform ND ug/kg 05/18/23 06:42 75-25-205/17/23 23:205.2 1.8 1
Bromomethane ND ug/kg 05/18/23 06:42 74-83-9 v205/17/23 23:2021.0 16.3 1
2-Butanone (MEK)ND ug/kg 05/18/23 06:42 78-93-305/17/23 23:2010525.2 1
n-Butylbenzene ND ug/kg 05/18/23 06:42 104-51-805/17/23 23:205.2 3.3 1
sec-Butylbenzene ND ug/kg 05/18/23 06:42 135-98-805/17/23 23:205.2 2.3 1
tert-Butylbenzene ND ug/kg 05/18/23 06:42 98-06-605/17/23 23:205.2 1.9 1
Carbon tetrachloride ND ug/kg 05/18/23 06:42 56-23-505/17/23 23:205.2 2.0 1
Chlorobenzene ND ug/kg 05/18/23 06:42 108-90-705/17/23 23:205.2 3.0 1
Chloroethane ND ug/kg 05/18/23 06:42 75-00-305/17/23 23:2010.5 4.0 1
Chloroform ND ug/kg 05/18/23 06:42 67-66-305/17/23 23:205.2 4.4 1
Chloromethane ND ug/kg 05/18/23 06:42 74-87-305/17/23 23:2010.5 4.4 1
2-Chlorotoluene ND ug/kg 05/18/23 06:42 95-49-805/17/23 23:205.2 1.9 1
4-Chlorotoluene ND ug/kg 05/18/23 06:42 106-43-405/17/23 23:205.2 2.9 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/18/23 06:42 96-12-805/17/23 23:205.2 2.0 1
Dibromochloromethane ND ug/kg 05/18/23 06:42 124-48-105/17/23 23:205.2 2.9 1
1,2-Dibromoethane (EDB)ND ug/kg 05/18/23 06:42 106-93-405/17/23 23:205.2 2.3 1
Dibromomethane ND ug/kg 05/18/23 06:42 74-95-305/17/23 23:205.2 1.1 1
1,2-Dichlorobenzene ND ug/kg 05/18/23 06:42 95-50-105/17/23 23:205.2 1.9 1
1,3-Dichlorobenzene ND ug/kg 05/18/23 06:42 541-73-105/17/23 23:205.2 1.6 1
1,4-Dichlorobenzene ND ug/kg 05/18/23 06:42 106-46-705/17/23 23:205.2 1.4 1
Dichlorodifluoromethane ND ug/kg 05/18/23 06:42 75-71-8 IH05/17/23 23:2010.5 5.3 1
1,1-Dichloroethane ND ug/kg 05/18/23 06:42 75-34-305/17/23 23:205.2 2.2 1
1,2-Dichloroethane ND ug/kg 05/18/23 06:42 107-06-205/17/23 23:205.2 3.5 1
1,1-Dichloroethene ND ug/kg 05/18/23 06:42 75-35-405/17/23 23:205.2 2.2 1
cis-1,2-Dichloroethene ND ug/kg 05/18/23 06:42 156-59-205/17/23 23:205.2 1.8 1
trans-1,2-Dichloroethene ND ug/kg 05/18/23 06:42 156-60-505/17/23 23:205.2 4.5 1
1,2-Dichloropropane ND ug/kg 05/18/23 06:42 78-87-505/17/23 23:205.2 1.6 1
1,3-Dichloropropane ND ug/kg 05/18/23 06:42 142-28-905/17/23 23:205.2 1.6 1
2,2-Dichloropropane ND ug/kg 05/18/23 06:42 594-20-705/17/23 23:205.2 4.0 1
1,1-Dichloropropene ND ug/kg 05/18/23 06:42 563-58-605/17/23 23:205.2 2.5 1
cis-1,3-Dichloropropene ND ug/kg 05/18/23 06:42 10061-01-505/17/23 23:205.2 1.4 1
trans-1,3-Dichloropropene ND ug/kg 05/18/23 06:42 10061-02-605/17/23 23:205.2 1.8 1
Diisopropyl ether ND ug/kg 05/18/23 06:42 108-20-305/17/23 23:205.2 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-1 Lab ID:92667899001 Collected:05/17/23 11:50 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 05/18/23 06:42 100-41-405/17/23 23:205.2 2.4 1
Hexachloro-1,3-butadiene ND ug/kg 05/18/23 06:42 87-68-305/17/23 23:2010.5 8.6 1
2-Hexanone ND ug/kg 05/18/23 06:42 591-78-605/17/23 23:2052.5 5.1 1
Isopropylbenzene (Cumene)ND ug/kg 05/18/23 06:42 98-82-805/17/23 23:205.2 1.8 1
p-Isopropyltoluene ND ug/kg 05/18/23 06:42 99-87-605/17/23 23:205.2 2.6 1
Methylene Chloride ND ug/kg 05/18/23 06:42 75-09-205/17/23 23:2021.0 14.4 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/18/23 06:42 108-10-105/17/23 23:2052.5 5.1 1
Methyl-tert-butyl ether ND ug/kg 05/18/23 06:42 1634-04-405/17/23 23:205.2 2.0 1
Naphthalene ND ug/kg 05/18/23 06:42 91-20-305/17/23 23:205.2 2.8 1
n-Propylbenzene ND ug/kg 05/18/23 06:42 103-65-105/17/23 23:205.2 1.9 1
Styrene ND ug/kg 05/18/23 06:42 100-42-505/17/23 23:205.2 1.4 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/18/23 06:42 630-20-605/17/23 23:205.2 2.0 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/18/23 06:42 79-34-505/17/23 23:205.2 1.4 1
Tetrachloroethene ND ug/kg 05/18/23 06:42 127-18-405/17/23 23:205.2 1.7 1
Toluene ND ug/kg 05/18/23 06:42 108-88-305/17/23 23:205.2 3.6 1
1,2,3-Trichlorobenzene ND ug/kg 05/18/23 06:42 87-61-605/17/23 23:205.2 4.2 1
1,2,4-Trichlorobenzene ND ug/kg 05/18/23 06:42 120-82-105/17/23 23:205.2 4.4 1
1,1,1-Trichloroethane ND ug/kg 05/18/23 06:42 71-55-605/17/23 23:205.2 2.7 1
1,1,2-Trichloroethane ND ug/kg 05/18/23 06:42 79-00-505/17/23 23:205.2 1.7 1
Trichloroethene ND ug/kg 05/18/23 06:42 79-01-605/17/23 23:205.2 4.2 1
Trichlorofluoromethane ND ug/kg 05/18/23 06:42 75-69-405/17/23 23:205.2 2.9 1
1,2,3-Trichloropropane ND ug/kg 05/18/23 06:42 96-18-405/17/23 23:205.2 2.7 1
1,2,4-Trimethylbenzene ND ug/kg 05/18/23 06:42 95-63-605/17/23 23:205.2 3.1 1
1,3,5-Trimethylbenzene ND ug/kg 05/18/23 06:42 108-67-805/17/23 23:205.2 1.8 1
Vinyl acetate ND ug/kg 05/18/23 06:42 108-05-405/17/23 23:2052.5 10.8 1
Vinyl chloride ND ug/kg 05/18/23 06:42 75-01-405/17/23 23:2010.5 2.7 1
Xylene (Total)ND ug/kg 05/18/23 06:42 1330-20-705/17/23 23:2010.5 3.0 1
m&p-Xylene ND ug/kg 05/18/23 06:42 179601-23-105/17/23 23:2010.5 3.6 1
o-Xylene ND ug/kg 05/18/23 06:42 95-47-605/17/23 23:205.2 2.3 1
Surrogates
Toluene-d8 (S)102 %05/18/23 06:42 2037-26-505/17/23 23:2070-130 1
4-Bromofluorobenzene (S)105 %05/18/23 06:42 460-00-405/17/23 23:2070-130 1
1,2-Dichloroethane-d4 (S)103 %05/18/23 06:42 17060-07-005/17/23 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 3.7 %05/17/23 14:57 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 88.1 %05/19/23 10:4605/19/23 10:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-1 Lab ID:92667899001 Collected:05/17/23 11:50 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/22/23 01:55 18540-29-905/19/23 07:121.14 0.289 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:DUP-1 Lab ID:92667899002 Collected:05/17/23 11:55 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 0.60J mg/kg 05/19/23 11:08 7440-38-205/18/23 09:221.6 0.055 1
Barium 343 mg/kg 05/19/23 11:08 7440-39-305/18/23 09:220.63 0.059 1
Cadmium 0.23 mg/kg 05/19/23 11:08 7440-43-905/18/23 09:220.063 0.0076 1
Chromium 61.8 mg/kg 05/19/23 11:08 7440-47-305/18/23 09:220.32 0.082 1
Lead 3.2 mg/kg 05/19/23 11:08 7439-92-105/18/23 09:220.63 0.15 1
Selenium ND mg/kg 05/19/23 11:08 7782-49-205/18/23 09:220.63 0.36 1
Silver 0.11J mg/kg 05/19/23 11:08 7440-22-405/18/23 09:220.32 0.023 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.0079 mg/kg 05/18/23 14:09 7439-97-605/18/23 10:280.0053 0.0033 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/18/23 12:15 83-32-905/17/23 16:273431201
Acenaphthylene ND ug/kg 05/18/23 12:15 208-96-805/17/23 16:273431201
Aniline ND ug/kg 05/18/23 12:15 62-53-305/17/23 16:273431341
Anthracene ND ug/kg 05/18/23 12:15 120-12-705/17/23 16:273431121
Benzo(a)anthracene ND ug/kg 05/18/23 12:15 56-55-305/17/23 16:273431141
Benzo(a)pyrene ND ug/kg 05/18/23 12:15 50-32-805/17/23 16:273431181
Benzo(b)fluoranthene ND ug/kg 05/18/23 12:15 205-99-205/17/23 16:273431141
Benzo(g,h,i)perylene ND ug/kg 05/18/23 12:15 191-24-205/17/23 16:273431331
Benzo(k)fluoranthene ND ug/kg 05/18/23 12:15 207-08-905/17/23 16:273431201
Benzoic Acid ND ug/kg 05/18/23 12:15 65-85-005/17/23 16:2717107361
Benzyl alcohol ND ug/kg 05/18/23 12:15 100-51-605/17/23 16:276852601
4-Bromophenylphenyl ether ND ug/kg 05/18/23 12:15 101-55-305/17/23 16:273431321
Butylbenzylphthalate ND ug/kg 05/18/23 12:15 85-68-705/17/23 16:273431441
4-Chloro-3-methylphenol ND ug/kg 05/18/23 12:15 59-50-705/17/23 16:276852411
4-Chloroaniline ND ug/kg 05/18/23 12:15 106-47-805/17/23 16:276852691
bis(2-Chloroethoxy)methane ND ug/kg 05/18/23 12:15 111-91-105/17/23 16:273431421
bis(2-Chloroethyl) ether ND ug/kg 05/18/23 12:15 111-44-405/17/23 16:273431291
2-Chloronaphthalene ND ug/kg 05/18/23 12:15 91-58-705/17/23 16:273431361
2-Chlorophenol ND ug/kg 05/18/23 12:15 95-57-805/17/23 16:273431291
4-Chlorophenylphenyl ether ND ug/kg 05/18/23 12:15 7005-72-305/17/23 16:273431281
Chrysene ND ug/kg 05/18/23 12:15 218-01-905/17/23 16:273431251
Dibenz(a,h)anthracene ND ug/kg 05/18/23 12:15 53-70-305/17/23 16:273431321
Dibenzofuran ND ug/kg 05/18/23 12:15 132-64-905/17/23 16:273431241
1,2-Dichlorobenzene ND ug/kg 05/18/23 12:15 95-50-105/17/23 16:273431241
1,3-Dichlorobenzene ND ug/kg 05/18/23 12:15 541-73-105/17/23 16:273431211
1,4-Dichlorobenzene ND ug/kg 05/18/23 12:15 106-46-705/17/23 16:273431311
3,3'-Dichlorobenzidine ND ug/kg 05/18/23 12:15 91-94-105/17/23 16:276852321
2,4-Dichlorophenol ND ug/kg 05/18/23 12:15 120-83-205/17/23 16:273431341
Diethylphthalate ND ug/kg 05/18/23 12:15 84-66-205/17/23 16:273431261
2,4-Dimethylphenol ND ug/kg 05/18/23 12:15 105-67-905/17/23 16:273431421
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:DUP-1 Lab ID:92667899002 Collected:05/17/23 11:55 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 05/18/23 12:15 131-11-305/17/23 16:273431251
Di-n-butylphthalate ND ug/kg 05/18/23 12:15 84-74-205/17/23 16:273431151
4,6-Dinitro-2-methylphenol ND ug/kg 05/18/23 12:15 534-52-105/17/23 16:276853201
2,4-Dinitrophenol ND ug/kg 05/18/23 12:15 51-28-505/17/23 16:27171010601
2,4-Dinitrotoluene ND ug/kg 05/18/23 12:15 121-14-205/17/23 16:273431321
2,6-Dinitrotoluene ND ug/kg 05/18/23 12:15 606-20-205/17/23 16:273431261
Di-n-octylphthalate ND ug/kg 05/18/23 12:15 117-84-005/17/23 16:273431351
bis(2-Ethylhexyl)phthalate ND ug/kg 05/18/23 12:15 117-81-705/17/23 16:273431331
Fluoranthene ND ug/kg 05/18/23 12:15 206-44-005/17/23 16:273431171
Fluorene ND ug/kg 05/18/23 12:15 86-73-705/17/23 16:273431201
Hexachloro-1,3-butadiene ND ug/kg 05/18/23 12:15 87-68-305/17/23 16:273431481
Hexachlorobenzene ND ug/kg 05/18/23 12:15 118-74-105/17/23 16:273431341
Hexachlorocyclopentadiene ND ug/kg 05/18/23 12:15 77-47-405/17/23 16:273431961
Hexachloroethane ND ug/kg 05/18/23 12:15 67-72-105/17/23 16:273431311
Indeno(1,2,3-cd)pyrene ND ug/kg 05/18/23 12:15 193-39-505/17/23 16:273431351
Isophorone ND ug/kg 05/18/23 12:15 78-59-105/17/23 16:273431531
1-Methylnaphthalene ND ug/kg 05/18/23 12:15 90-12-005/17/23 16:273431201
2-Methylnaphthalene ND ug/kg 05/18/23 12:15 91-57-605/17/23 16:273431371
2-Methylphenol(o-Cresol)ND ug/kg 05/18/23 12:15 95-48-705/17/23 16:273431401
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/18/23 12:15 15831-10-405/17/23 16:273431381
Naphthalene ND ug/kg 05/18/23 12:15 91-20-305/17/23 16:273431161
2-Nitroaniline ND ug/kg 05/18/23 12:15 88-74-405/17/23 16:2717102801
3-Nitroaniline ND ug/kg 05/18/23 12:15 99-09-205/17/23 16:2717102691
4-Nitroaniline ND ug/kg 05/18/23 12:15 100-01-605/17/23 16:276852611
Nitrobenzene ND ug/kg 05/18/23 12:15 98-95-305/17/23 16:273431591
2-Nitrophenol ND ug/kg 05/18/23 12:15 88-75-505/17/23 16:273431481
4-Nitrophenol ND ug/kg 05/18/23 12:15 100-02-705/17/23 16:2717106631
N-Nitrosodimethylamine ND ug/kg 05/18/23 12:15 62-75-905/17/23 16:273431151
N-Nitroso-di-n-propylamine ND ug/kg 05/18/23 12:15 621-64-705/17/23 16:273431291
N-Nitrosodiphenylamine ND ug/kg 05/18/23 12:15 86-30-605/17/23 16:273431211
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/18/23 12:15 108-60-105/17/23 16:273431631
Pentachlorophenol ND ug/kg 05/18/23 12:15 87-86-505/17/23 16:276853351
Phenanthrene ND ug/kg 05/18/23 12:15 85-01-805/17/23 16:273431121
Phenol ND ug/kg 05/18/23 12:15 108-95-205/17/23 16:273431531
Pyrene ND ug/kg 05/18/23 12:15 129-00-005/17/23 16:273431391
Pyridine ND ug/kg 05/18/23 12:15 110-86-105/17/23 16:273431081
1,2,4-Trichlorobenzene ND ug/kg 05/18/23 12:15 120-82-105/17/23 16:273431351
2,4,5-Trichlorophenol ND ug/kg 05/18/23 12:15 95-95-405/17/23 16:273431571
2,4,6-Trichlorophenol ND ug/kg 05/18/23 12:15 88-06-205/17/23 16:273431411
Surrogates
Nitrobenzene-d5 (S)45 %05/18/23 12:15 4165-60-005/17/23 16:2710-130 1
2-Fluorobiphenyl (S)49 %05/18/23 12:15 321-60-805/17/23 16:2710-130 1
Terphenyl-d14 (S)54 %05/18/23 12:15 1718-51-005/17/23 16:2710-130 1
Phenol-d6 (S)41 %05/18/23 12:15 13127-88-305/17/23 16:2710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:DUP-1 Lab ID:92667899002 Collected:05/17/23 11:55 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)42 %05/18/23 12:15 367-12-405/17/23 16:2710-130 1
2,4,6-Tribromophenol (S)50 %05/18/23 12:15 118-79-605/17/23 16:2710-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone ND ug/kg 05/18/23 07:01 67-64-105/17/23 23:2010032.1 1
Benzene ND ug/kg 05/18/23 07:01 71-43-205/17/23 23:205.0 2.0 1
Bromobenzene ND ug/kg 05/18/23 07:01 108-86-105/17/23 23:205.0 1.6 1
Bromochloromethane ND ug/kg 05/18/23 07:01 74-97-505/17/23 23:205.0 1.5 1
Bromodichloromethane ND ug/kg 05/18/23 07:01 75-27-405/17/23 23:205.0 1.9 1
Bromoform ND ug/kg 05/18/23 07:01 75-25-205/17/23 23:205.0 1.8 1
Bromomethane ND ug/kg 05/18/23 07:01 74-83-9 v205/17/23 23:2020.0 15.5 1
2-Butanone (MEK)ND ug/kg 05/18/23 07:01 78-93-305/17/23 23:2010024.0 1
n-Butylbenzene ND ug/kg 05/18/23 07:01 104-51-805/17/23 23:205.0 3.2 1
sec-Butylbenzene ND ug/kg 05/18/23 07:01 135-98-805/17/23 23:205.0 2.2 1
tert-Butylbenzene ND ug/kg 05/18/23 07:01 98-06-605/17/23 23:205.0 1.8 1
Carbon tetrachloride ND ug/kg 05/18/23 07:01 56-23-505/17/23 23:205.0 1.9 1
Chlorobenzene ND ug/kg 05/18/23 07:01 108-90-705/17/23 23:205.0 2.9 1
Chloroethane ND ug/kg 05/18/23 07:01 75-00-305/17/23 23:2010.0 3.9 1
Chloroform ND ug/kg 05/18/23 07:01 67-66-305/17/23 23:205.0 4.2 1
Chloromethane ND ug/kg 05/18/23 07:01 74-87-305/17/23 23:2010.0 4.2 1
2-Chlorotoluene ND ug/kg 05/18/23 07:01 95-49-805/17/23 23:205.0 1.8 1
4-Chlorotoluene ND ug/kg 05/18/23 07:01 106-43-405/17/23 23:205.0 2.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 05/18/23 07:01 96-12-805/17/23 23:205.0 1.9 1
Dibromochloromethane ND ug/kg 05/18/23 07:01 124-48-105/17/23 23:205.0 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 05/18/23 07:01 106-93-405/17/23 23:205.0 2.2 1
Dibromomethane ND ug/kg 05/18/23 07:01 74-95-305/17/23 23:205.0 1.1 1
1,2-Dichlorobenzene ND ug/kg 05/18/23 07:01 95-50-105/17/23 23:205.0 1.8 1
1,3-Dichlorobenzene ND ug/kg 05/18/23 07:01 541-73-105/17/23 23:205.0 1.6 1
1,4-Dichlorobenzene ND ug/kg 05/18/23 07:01 106-46-705/17/23 23:205.0 1.3 1
Dichlorodifluoromethane ND ug/kg 05/18/23 07:01 75-71-8 IH05/17/23 23:2010.0 5.1 1
1,1-Dichloroethane ND ug/kg 05/18/23 07:01 75-34-305/17/23 23:205.0 2.1 1
1,2-Dichloroethane ND ug/kg 05/18/23 07:01 107-06-205/17/23 23:205.0 3.3 1
1,1-Dichloroethene ND ug/kg 05/18/23 07:01 75-35-405/17/23 23:205.0 2.1 1
cis-1,2-Dichloroethene ND ug/kg 05/18/23 07:01 156-59-205/17/23 23:205.0 1.7 1
trans-1,2-Dichloroethene ND ug/kg 05/18/23 07:01 156-60-505/17/23 23:205.0 4.3 1
1,2-Dichloropropane ND ug/kg 05/18/23 07:01 78-87-505/17/23 23:205.0 1.5 1
1,3-Dichloropropane ND ug/kg 05/18/23 07:01 142-28-905/17/23 23:205.0 1.6 1
2,2-Dichloropropane ND ug/kg 05/18/23 07:01 594-20-705/17/23 23:205.0 3.8 1
1,1-Dichloropropene ND ug/kg 05/18/23 07:01 563-58-605/17/23 23:205.0 2.4 1
cis-1,3-Dichloropropene ND ug/kg 05/18/23 07:01 10061-01-505/17/23 23:205.0 1.4 1
trans-1,3-Dichloropropene ND ug/kg 05/18/23 07:01 10061-02-605/17/23 23:205.0 1.7 1
Diisopropyl ether ND ug/kg 05/18/23 07:01 108-20-305/17/23 23:205.0 1.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:DUP-1 Lab ID:92667899002 Collected:05/17/23 11:55 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene ND ug/kg 05/18/23 07:01 100-41-405/17/23 23:205.0 2.3 1
Hexachloro-1,3-butadiene ND ug/kg 05/18/23 07:01 87-68-305/17/23 23:2010.0 8.2 1
2-Hexanone ND ug/kg 05/18/23 07:01 591-78-605/17/23 23:2050.1 4.8 1
Isopropylbenzene (Cumene)ND ug/kg 05/18/23 07:01 98-82-805/17/23 23:205.0 1.7 1
p-Isopropyltoluene ND ug/kg 05/18/23 07:01 99-87-605/17/23 23:205.0 2.5 1
Methylene Chloride ND ug/kg 05/18/23 07:01 75-09-205/17/23 23:2020.0 13.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/18/23 07:01 108-10-105/17/23 23:2050.1 4.8 1
Methyl-tert-butyl ether ND ug/kg 05/18/23 07:01 1634-04-405/17/23 23:205.0 1.9 1
Naphthalene ND ug/kg 05/18/23 07:01 91-20-305/17/23 23:205.0 2.6 1
n-Propylbenzene ND ug/kg 05/18/23 07:01 103-65-105/17/23 23:205.0 1.8 1
Styrene ND ug/kg 05/18/23 07:01 100-42-505/17/23 23:205.0 1.3 1
1,1,1,2-Tetrachloroethane ND ug/kg 05/18/23 07:01 630-20-605/17/23 23:205.0 1.9 1
1,1,2,2-Tetrachloroethane ND ug/kg 05/18/23 07:01 79-34-505/17/23 23:205.0 1.3 1
Tetrachloroethene ND ug/kg 05/18/23 07:01 127-18-405/17/23 23:205.0 1.6 1
Toluene ND ug/kg 05/18/23 07:01 108-88-305/17/23 23:205.0 3.5 1
1,2,3-Trichlorobenzene ND ug/kg 05/18/23 07:01 87-61-605/17/23 23:205.0 4.0 1
1,2,4-Trichlorobenzene ND ug/kg 05/18/23 07:01 120-82-105/17/23 23:205.0 4.2 1
1,1,1-Trichloroethane ND ug/kg 05/18/23 07:01 71-55-605/17/23 23:205.0 2.6 1
1,1,2-Trichloroethane ND ug/kg 05/18/23 07:01 79-00-505/17/23 23:205.0 1.7 1
Trichloroethene ND ug/kg 05/18/23 07:01 79-01-605/17/23 23:205.0 4.0 1
Trichlorofluoromethane ND ug/kg 05/18/23 07:01 75-69-405/17/23 23:205.0 2.8 1
1,2,3-Trichloropropane ND ug/kg 05/18/23 07:01 96-18-405/17/23 23:205.0 2.5 1
1,2,4-Trimethylbenzene ND ug/kg 05/18/23 07:01 95-63-605/17/23 23:205.0 3.0 1
1,3,5-Trimethylbenzene ND ug/kg 05/18/23 07:01 108-67-805/17/23 23:205.0 1.7 1
Vinyl acetate ND ug/kg 05/18/23 07:01 108-05-405/17/23 23:2050.1 10.3 1
Vinyl chloride ND ug/kg 05/18/23 07:01 75-01-405/17/23 23:2010.0 2.5 1
Xylene (Total)ND ug/kg 05/18/23 07:01 1330-20-705/17/23 23:2010.0 2.9 1
m&p-Xylene ND ug/kg 05/18/23 07:01 179601-23-105/17/23 23:2010.0 3.4 1
o-Xylene ND ug/kg 05/18/23 07:01 95-47-605/17/23 23:205.0 2.2 1
Surrogates
Toluene-d8 (S)102 %05/18/23 07:01 2037-26-505/17/23 23:2070-130 1
4-Bromofluorobenzene (S)104 %05/18/23 07:01 460-00-405/17/23 23:2070-130 1
1,2-Dichloroethane-d4 (S)103 %05/18/23 07:01 17060-07-005/17/23 23:2070-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 3.4 %05/17/23 14:57 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 89.2 %05/19/23 10:4605/19/23 10:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:DUP-1 Lab ID:92667899002 Collected:05/17/23 11:55 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/22/23 02:06 18540-29-905/19/23 07:121.12 0.286 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-2 Lab ID:92667899003 Collected:05/17/23 12:30 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 6010D Preparation Method: EPA 3050B
Pace Analytical Services - Asheville
6010 MET ICP
Arsenic 0.77J mg/kg 05/19/23 11:10 7440-38-205/18/23 09:222.1 0.073 1
Barium 298 mg/kg 05/19/23 11:10 7440-39-3 M105/18/23 09:220.84 0.078 1
Cadmium 0.16 mg/kg 05/19/23 11:10 7440-43-9 B05/18/23 09:220.084 0.010 1
Chromium 66.5 mg/kg 05/19/23 11:10 7440-47-3 M1,R105/18/23 09:220.42 0.11 1
Lead 1.9 mg/kg 05/19/23 11:10 7439-92-105/18/23 09:220.84 0.20 1
Selenium ND mg/kg 05/19/23 11:10 7782-49-205/18/23 09:220.84 0.48 1
Silver 0.16J mg/kg 05/19/23 11:10 7440-22-405/18/23 09:220.42 0.030 1
Analytical Method: EPA 7471B Preparation Method: EPA 7471B
Pace Analytical Services - Asheville
7471 Mercury
Mercury 0.0090 mg/kg 05/18/23 14:11 7439-97-605/18/23 10:280.0055 0.0034 1
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND ug/kg 05/18/23 13:11 83-32-905/17/23 16:273401201
Acenaphthylene ND ug/kg 05/18/23 13:11 208-96-805/17/23 16:273401201
Aniline ND ug/kg 05/18/23 13:11 62-53-305/17/23 16:273401331
Anthracene ND ug/kg 05/18/23 13:11 120-12-705/17/23 16:273401111
Benzo(a)anthracene ND ug/kg 05/18/23 13:11 56-55-305/17/23 16:273401131
Benzo(a)pyrene ND ug/kg 05/18/23 13:11 50-32-805/17/23 16:273401181
Benzo(b)fluoranthene ND ug/kg 05/18/23 13:11 205-99-205/17/23 16:273401131
Benzo(g,h,i)perylene ND ug/kg 05/18/23 13:11 191-24-205/17/23 16:273401321
Benzo(k)fluoranthene ND ug/kg 05/18/23 13:11 207-08-905/17/23 16:273401201
Benzoic Acid ND ug/kg 05/18/23 13:11 65-85-005/17/23 16:2717007311
Benzyl alcohol ND ug/kg 05/18/23 13:11 100-51-605/17/23 16:276812581
4-Bromophenylphenyl ether ND ug/kg 05/18/23 13:11 101-55-305/17/23 16:273401311
Butylbenzylphthalate ND ug/kg 05/18/23 13:11 85-68-705/17/23 16:273401431
4-Chloro-3-methylphenol ND ug/kg 05/18/23 13:11 59-50-705/17/23 16:276812391
4-Chloroaniline ND ug/kg 05/18/23 13:11 106-47-805/17/23 16:276812671
bis(2-Chloroethoxy)methane ND ug/kg 05/18/23 13:11 111-91-105/17/23 16:273401411
bis(2-Chloroethyl) ether ND ug/kg 05/18/23 13:11 111-44-405/17/23 16:273401281
2-Chloronaphthalene ND ug/kg 05/18/23 13:11 91-58-705/17/23 16:273401351
2-Chlorophenol ND ug/kg 05/18/23 13:11 95-57-805/17/23 16:273401281
4-Chlorophenylphenyl ether ND ug/kg 05/18/23 13:11 7005-72-305/17/23 16:273401271
Chrysene ND ug/kg 05/18/23 13:11 218-01-905/17/23 16:273401241
Dibenz(a,h)anthracene ND ug/kg 05/18/23 13:11 53-70-305/17/23 16:273401311
Dibenzofuran ND ug/kg 05/18/23 13:11 132-64-905/17/23 16:273401231
1,2-Dichlorobenzene ND ug/kg 05/18/23 13:11 95-50-105/17/23 16:273401231
1,3-Dichlorobenzene ND ug/kg 05/18/23 13:11 541-73-105/17/23 16:273401211
1,4-Dichlorobenzene ND ug/kg 05/18/23 13:11 106-46-705/17/23 16:273401301
3,3'-Dichlorobenzidine ND ug/kg 05/18/23 13:11 91-94-105/17/23 16:276812301
2,4-Dichlorophenol ND ug/kg 05/18/23 13:11 120-83-205/17/23 16:273401331
Diethylphthalate ND ug/kg 05/18/23 13:11 84-66-205/17/23 16:273401251
2,4-Dimethylphenol ND ug/kg 05/18/23 13:11 105-67-905/17/23 16:273401411
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-2 Lab ID:92667899003 Collected:05/17/23 12:30 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Dimethylphthalate ND ug/kg 05/18/23 13:11 131-11-305/17/23 16:273401241
Di-n-butylphthalate ND ug/kg 05/18/23 13:11 84-74-205/17/23 16:273401141
4,6-Dinitro-2-methylphenol ND ug/kg 05/18/23 13:11 534-52-105/17/23 16:276813181
2,4-Dinitrophenol ND ug/kg 05/18/23 13:11 51-28-505/17/23 16:27170010501
2,4-Dinitrotoluene ND ug/kg 05/18/23 13:11 121-14-205/17/23 16:273401311
2,6-Dinitrotoluene ND ug/kg 05/18/23 13:11 606-20-205/17/23 16:273401251
Di-n-octylphthalate ND ug/kg 05/18/23 13:11 117-84-005/17/23 16:273401341
bis(2-Ethylhexyl)phthalate ND ug/kg 05/18/23 13:11 117-81-705/17/23 16:273401321
Fluoranthene ND ug/kg 05/18/23 13:11 206-44-005/17/23 16:273401171
Fluorene ND ug/kg 05/18/23 13:11 86-73-705/17/23 16:273401201
Hexachloro-1,3-butadiene ND ug/kg 05/18/23 13:11 87-68-305/17/23 16:273401471
Hexachlorobenzene ND ug/kg 05/18/23 13:11 118-74-105/17/23 16:273401331
Hexachlorocyclopentadiene ND ug/kg 05/18/23 13:11 77-47-405/17/23 16:273401951
Hexachloroethane ND ug/kg 05/18/23 13:11 67-72-105/17/23 16:273401301
Indeno(1,2,3-cd)pyrene ND ug/kg 05/18/23 13:11 193-39-505/17/23 16:273401341
Isophorone ND ug/kg 05/18/23 13:11 78-59-105/17/23 16:273401521
1-Methylnaphthalene ND ug/kg 05/18/23 13:11 90-12-005/17/23 16:273401201
2-Methylnaphthalene ND ug/kg 05/18/23 13:11 91-57-605/17/23 16:273401361
2-Methylphenol(o-Cresol)ND ug/kg 05/18/23 13:11 95-48-705/17/23 16:273401391
3&4-Methylphenol(m&p Cresol)ND ug/kg 05/18/23 13:11 15831-10-405/17/23 16:273401371
Naphthalene ND ug/kg 05/18/23 13:11 91-20-305/17/23 16:273401151
2-Nitroaniline ND ug/kg 05/18/23 13:11 88-74-405/17/23 16:2717002781
3-Nitroaniline ND ug/kg 05/18/23 13:11 99-09-205/17/23 16:2717002671
4-Nitroaniline ND ug/kg 05/18/23 13:11 100-01-605/17/23 16:276812591
Nitrobenzene ND ug/kg 05/18/23 13:11 98-95-305/17/23 16:273401581
2-Nitrophenol ND ug/kg 05/18/23 13:11 88-75-505/17/23 16:273401471
4-Nitrophenol ND ug/kg 05/18/23 13:11 100-02-705/17/23 16:2717006581
N-Nitrosodimethylamine ND ug/kg 05/18/23 13:11 62-75-905/17/23 16:273401141
N-Nitroso-di-n-propylamine ND ug/kg 05/18/23 13:11 621-64-705/17/23 16:273401281
N-Nitrosodiphenylamine ND ug/kg 05/18/23 13:11 86-30-605/17/23 16:273401211
2,2'-Oxybis(1-chloropropane)ND ug/kg 05/18/23 13:11 108-60-105/17/23 16:273401621
Pentachlorophenol ND ug/kg 05/18/23 13:11 87-86-505/17/23 16:276813331
Phenanthrene ND ug/kg 05/18/23 13:11 85-01-805/17/23 16:273401111
Phenol ND ug/kg 05/18/23 13:11 108-95-205/17/23 16:273401521
Pyrene ND ug/kg 05/18/23 13:11 129-00-005/17/23 16:273401381
Pyridine ND ug/kg 05/18/23 13:11 110-86-105/17/23 16:273401071
1,2,4-Trichlorobenzene ND ug/kg 05/18/23 13:11 120-82-105/17/23 16:273401341
2,4,5-Trichlorophenol ND ug/kg 05/18/23 13:11 95-95-405/17/23 16:273401561
2,4,6-Trichlorophenol ND ug/kg 05/18/23 13:11 88-06-205/17/23 16:273401401
Surrogates
Nitrobenzene-d5 (S)41 %05/18/23 13:11 4165-60-005/17/23 16:2710-130 1
2-Fluorobiphenyl (S)44 %05/18/23 13:11 321-60-805/17/23 16:2710-130 1
Terphenyl-d14 (S)49 %05/18/23 13:11 1718-51-005/17/23 16:2710-130 1
Phenol-d6 (S)38 %05/18/23 13:11 13127-88-305/17/23 16:2710-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-2 Lab ID:92667899003 Collected:05/17/23 12:30 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Surrogates
2-Fluorophenol (S)39 %05/18/23 13:11 367-12-405/17/23 16:2710-130 1
2,4,6-Tribromophenol (S)45 %05/18/23 13:11 118-79-605/17/23 16:2710-131 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Acetone 104J ug/kg 05/19/23 18:49 67-64-105/17/23 23:2028491.2 2.5
Benzene ND ug/kg 05/19/23 18:49 71-43-205/17/23 23:2014.2 5.7 2.5
Bromobenzene ND ug/kg 05/19/23 18:49 108-86-105/17/23 23:2014.2 4.6 2.5
Bromochloromethane ND ug/kg 05/19/23 18:49 74-97-505/17/23 23:2014.2 4.2 2.5
Bromodichloromethane ND ug/kg 05/19/23 18:49 75-27-405/17/23 23:2014.2 5.5 2.5
Bromoform ND ug/kg 05/19/23 18:49 75-25-205/17/23 23:2014.2 5.0 2.5
Bromomethane ND ug/kg 05/19/23 18:49 74-83-905/17/23 23:2056.8 44.0 2.5
2-Butanone (MEK)ND ug/kg 05/19/23 18:49 78-93-305/17/23 23:2028468.2 2.5
n-Butylbenzene ND ug/kg 05/19/23 18:49 104-51-805/17/23 23:2014.2 9.0 2.5
sec-Butylbenzene ND ug/kg 05/19/23 18:49 135-98-805/17/23 23:2014.2 6.3 2.5
tert-Butylbenzene ND ug/kg 05/19/23 18:49 98-06-605/17/23 23:2014.2 5.1 2.5
Carbon tetrachloride ND ug/kg 05/19/23 18:49 56-23-505/17/23 23:2014.2 5.3 2.5
Chlorobenzene ND ug/kg 05/19/23 18:49 108-90-705/17/23 23:2014.2 8.2 2.5
Chloroethane ND ug/kg 05/19/23 18:49 75-00-305/17/23 23:2028.4 11.0 2.5
Chloroform ND ug/kg 05/19/23 18:49 67-66-305/17/23 23:2014.2 11.9 2.5
Chloromethane ND ug/kg 05/19/23 18:49 74-87-305/17/23 23:2028.4 11.9 2.5
2-Chlorotoluene ND ug/kg 05/19/23 18:49 95-49-805/17/23 23:2014.2 5.0 2.5
4-Chlorotoluene ND ug/kg 05/19/23 18:49 106-43-405/17/23 23:2014.2 7.9 2.5
1,2-Dibromo-3-chloropropane ND ug/kg 05/19/23 18:49 96-12-805/17/23 23:2014.2 5.5 2.5
Dibromochloromethane ND ug/kg 05/19/23 18:49 124-48-105/17/23 23:2014.2 8.0 2.5
1,2-Dibromoethane (EDB)ND ug/kg 05/19/23 18:49 106-93-405/17/23 23:2014.2 6.3 2.5
Dibromomethane ND ug/kg 05/19/23 18:49 74-95-305/17/23 23:2014.2 3.0 2.5
1,2-Dichlorobenzene ND ug/kg 05/19/23 18:49 95-50-105/17/23 23:2014.2 5.1 2.5
1,3-Dichlorobenzene ND ug/kg 05/19/23 18:49 541-73-105/17/23 23:2014.2 4.4 2.5
1,4-Dichlorobenzene ND ug/kg 05/19/23 18:49 106-46-705/17/23 23:2014.2 3.7 2.5
Dichlorodifluoromethane ND ug/kg 05/19/23 18:49 75-71-8 IH,v105/17/23 23:2028.4 14.5 2.5
1,1-Dichloroethane ND ug/kg 05/19/23 18:49 75-34-305/17/23 23:2014.2 5.9 2.5
1,2-Dichloroethane ND ug/kg 05/19/23 18:49 107-06-205/17/23 23:2014.2 9.4 2.5
1,1-Dichloroethene ND ug/kg 05/19/23 18:49 75-35-405/17/23 23:2014.2 5.9 2.5
cis-1,2-Dichloroethene ND ug/kg 05/19/23 18:49 156-59-205/17/23 23:2014.2 4.9 2.5
trans-1,2-Dichloroethene ND ug/kg 05/19/23 18:49 156-60-505/17/23 23:2014.2 12.1 2.5
1,2-Dichloropropane ND ug/kg 05/19/23 18:49 78-87-505/17/23 23:2014.2 4.3 2.5
1,3-Dichloropropane ND ug/kg 05/19/23 18:49 142-28-905/17/23 23:2014.2 4.4 2.5
2,2-Dichloropropane ND ug/kg 05/19/23 18:49 594-20-705/17/23 23:2014.2 10.8 2.5
1,1-Dichloropropene ND ug/kg 05/19/23 18:49 563-58-605/17/23 23:2014.2 6.8 2.5
cis-1,3-Dichloropropene ND ug/kg 05/19/23 18:49 10061-01-505/17/23 23:2014.2 3.9 2.5
trans-1,3-Dichloropropene ND ug/kg 05/19/23 18:49 10061-02-605/17/23 23:2014.2 4.9 2.5
Diisopropyl ether ND ug/kg 05/19/23 18:49 108-20-305/17/23 23:2014.2 3.8 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-2 Lab ID:92667899003 Collected:05/17/23 12:30 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A/5030B
Pace Analytical Services - Charlotte
8260D/5035A/5030B Volatiles
Ethylbenzene 16.1 ug/kg 05/19/23 18:49 100-41-405/17/23 23:2014.2 6.6 2.5
Hexachloro-1,3-butadiene ND ug/kg 05/19/23 18:49 87-68-305/17/23 23:2028.4 23.2 2.5
2-Hexanone ND ug/kg 05/19/23 18:49 591-78-605/17/23 23:2014213.7 2.5
Isopropylbenzene (Cumene)399 ug/kg 05/19/23 18:49 98-82-805/17/23 23:2014.2 4.8 2.5
p-Isopropyltoluene 712 ug/kg 05/19/23 18:49 99-87-605/17/23 23:2014.2 7.0 2.5
Methylene Chloride 203 ug/kg 05/19/23 18:49 75-09-2 C905/17/23 23:2056.8 38.9 2.5
4-Methyl-2-pentanone (MIBK)ND ug/kg 05/19/23 18:49 108-10-105/17/23 23:2014213.7 2.5
Methyl-tert-butyl ether ND ug/kg 05/19/23 18:49 1634-04-405/17/23 23:2014.2 5.3 2.5
Naphthalene 11.6J ug/kg 05/19/23 18:49 91-20-305/17/23 23:2014.2 7.5 2.5
n-Propylbenzene 1410 ug/kg 05/19/23 18:49 103-65-105/17/23 23:2014.2 5.1 2.5
Styrene ND ug/kg 05/19/23 18:49 100-42-505/17/23 23:2014.2 3.8 2.5
1,1,1,2-Tetrachloroethane ND ug/kg 05/19/23 18:49 630-20-605/17/23 23:2014.2 5.5 2.5
1,1,2,2-Tetrachloroethane ND ug/kg 05/19/23 18:49 79-34-505/17/23 23:2014.2 3.8 2.5
Tetrachloroethene ND ug/kg 05/19/23 18:49 127-18-405/17/23 23:2014.2 4.5 2.5
Toluene 30.9 ug/kg 05/19/23 18:49 108-88-305/17/23 23:2014.2 9.8 2.5
1,2,3-Trichlorobenzene ND ug/kg 05/19/23 18:49 87-61-605/17/23 23:2014.2 11.5 2.5
1,2,4-Trichlorobenzene ND ug/kg 05/19/23 18:49 120-82-105/17/23 23:2014.2 11.9 2.5
1,1,1-Trichloroethane ND ug/kg 05/19/23 18:49 71-55-605/17/23 23:2014.2 7.4 2.5
1,1,2-Trichloroethane ND ug/kg 05/19/23 18:49 79-00-505/17/23 23:2014.2 4.7 2.5
Trichloroethene ND ug/kg 05/19/23 18:49 79-01-605/17/23 23:2014.2 11.5 2.5
Trichlorofluoromethane ND ug/kg 05/19/23 18:49 75-69-405/17/23 23:2014.2 7.8 2.5
1,2,3-Trichloropropane ND ug/kg 05/19/23 18:49 96-18-405/17/23 23:2014.2 7.2 2.5
1,2,4-Trimethylbenzene 11100 ug/kg 05/19/23 18:49 95-63-6 M105/17/23 23:2014.2 8.4 2.5
1,3,5-Trimethylbenzene 3650 ug/kg 05/19/23 18:49 108-67-8 M105/17/23 23:2014.2 4.8 2.5
Vinyl acetate ND ug/kg 05/19/23 18:49 108-05-405/17/23 23:2014229.2 2.5
Vinyl chloride ND ug/kg 05/19/23 18:49 75-01-405/17/23 23:2028.4 7.2 2.5
Xylene (Total)297 ug/kg 05/19/23 18:49 1330-20-705/17/23 23:2028.4 8.1 2.5
m&p-Xylene 76.3 ug/kg 05/19/23 18:49 179601-23-105/17/23 23:2028.4 9.7 2.5
o-Xylene 220 ug/kg 05/19/23 18:49 95-47-605/17/23 23:2014.2 6.3 2.5
Surrogates
Toluene-d8 (S)102 %05/19/23 18:49 2037-26-505/17/23 23:2070-130 2.5
4-Bromofluorobenzene (S)104 %05/19/23 18:49 460-00-405/17/23 23:2070-130 2.5
1,2-Dichloroethane-d4 (S)110 %05/19/23 18:49 17060-07-005/17/23 23:2070-130 2.5
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 4.0 %05/17/23 14:57 N20.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 G
Pace National - Mt. Juliet
Total Solids 2540 G-2011
Total Solids 94.1 %05/19/23 10:4605/19/23 10:091
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:SS-2 Lab ID:92667899003 Collected:05/17/23 12:30 Received:05/17/23 13:55 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 7199 Preparation Method: 3060A
Pace National - Mt. Juliet
Wet Chemistry 7199
Chromium, Hexavalent ND mg/kg 05/22/23 02:11 18540-29-9 ML05/19/23 07:121.06 0.271 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:EQUIP BLANK Lab ID:92667899004 Collected:05/17/23 12:45 Received:05/17/23 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Acetone 8.4J ug/L 05/18/23 05:49 67-64-125.0 3.0 1
Benzene ND ug/L 05/18/23 05:49 71-43-25.0 1.7 1
Bromobenzene ND ug/L 05/18/23 05:49 108-86-15.0 1.9 1
Bromochloromethane ND ug/L 05/18/23 05:49 74-97-55.0 2.1 1
Bromodichloromethane ND ug/L 05/18/23 05:49 75-27-45.0 1.1 1
Bromoform ND ug/L 05/18/23 05:49 75-25-25.0 1.0 1
Bromomethane ND ug/L 05/18/23 05:49 74-83-910.0 6.0 1
2-Butanone (MEK)ND ug/L 05/18/23 05:49 78-93-310.0 2.6 1
tert-Butyl Alcohol ND ug/L 05/18/23 05:49 75-65-010011.6 1
n-Butylbenzene ND ug/L 05/18/23 05:49 104-51-85.0 2.3 1
sec-Butylbenzene ND ug/L 05/18/23 05:49 135-98-85.0 2.2 1
tert-Butylbenzene ND ug/L 05/18/23 05:49 98-06-65.0 0.98 1
Carbon tetrachloride ND ug/L 05/18/23 05:49 56-23-55.0 2.2 1
Chlorobenzene ND ug/L 05/18/23 05:49 108-90-75.0 1.8 1
Chloroethane ND ug/L 05/18/23 05:49 75-00-310.0 4.1 1
Chloroform ND ug/L 05/18/23 05:49 67-66-35.0 1.3 1
Chloromethane ND ug/L 05/18/23 05:49 74-87-35.0 2.8 1
2-Chlorotoluene ND ug/L 05/18/23 05:49 95-49-85.0 1.8 1
4-Chlorotoluene ND ug/L 05/18/23 05:49 106-43-45.0 2.0 1
1,2-Dibromo-3-chloropropane ND ug/L 05/18/23 05:49 96-12-85.0 1.0 1
Dibromochloromethane ND ug/L 05/18/23 05:49 124-48-15.0 2.3 1
1,2-Dibromoethane (EDB)ND ug/L 05/18/23 05:49 106-93-45.0 1.9 1
Dibromomethane ND ug/L 05/18/23 05:49 74-95-35.0 1.0 1
1,2-Dichlorobenzene ND ug/L 05/18/23 05:49 95-50-15.0 1.9 1
1,3-Dichlorobenzene ND ug/L 05/18/23 05:49 541-73-15.0 1.7 1
1,4-Dichlorobenzene ND ug/L 05/18/23 05:49 106-46-75.0 1.9 1
Dichlorodifluoromethane ND ug/L 05/18/23 05:49 75-71-85.0 1.8 1
1,1-Dichloroethane ND ug/L 05/18/23 05:49 75-34-35.0 2.3 1
1,2-Dichloroethane ND ug/L 05/18/23 05:49 107-06-25.0 2.1 1
1,2-Dichloroethene (Total)ND ug/L 05/18/23 05:49 540-59-05.0 5.0 1
1,1-Dichloroethene ND ug/L 05/18/23 05:49 75-35-45.0 2.2 1
cis-1,2-Dichloroethene ND ug/L 05/18/23 05:49 156-59-25.0 2.2 1
trans-1,2-Dichloroethene ND ug/L 05/18/23 05:49 156-60-55.0 2.2 1
1,2-Dichloropropane ND ug/L 05/18/23 05:49 78-87-55.0 2.1 1
1,3-Dichloropropane ND ug/L 05/18/23 05:49 142-28-95.0 1.9 1
2,2-Dichloropropane ND ug/L 05/18/23 05:49 594-20-75.0 2.4 1
1,1-Dichloropropene ND ug/L 05/18/23 05:49 563-58-65.0 2.8 1
cis-1,3-Dichloropropene ND ug/L 05/18/23 05:49 10061-01-55.0 2.0 1
trans-1,3-Dichloropropene ND ug/L 05/18/23 05:49 10061-02-65.0 2.2 1
Diisopropyl ether ND ug/L 05/18/23 05:49 108-20-35.0 1.4 1
Ethylbenzene ND ug/L 05/18/23 05:49 100-41-45.0 1.8 1
Hexachloro-1,3-butadiene ND ug/L 05/18/23 05:49 87-68-3 v25.0 4.8 1
2-Hexanone ND ug/L 05/18/23 05:49 591-78-610.0 4.2 1
Isopropylbenzene (Cumene)ND ug/L 05/18/23 05:49 98-82-85.0 2.1 1
p-Isopropyltoluene ND ug/L 05/18/23 05:49 99-87-65.0 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 49
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Sample:EQUIP BLANK Lab ID:92667899004 Collected:05/17/23 12:45 Received:05/17/23 13:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D
Pace Analytical Services - Charlotte
8260D MSV
Methylene Chloride ND ug/L 05/18/23 05:49 75-09-25.0 3.3 1
4-Methyl-2-pentanone (MIBK)ND ug/L 05/18/23 05:49 108-10-110.0 4.7 1
Methyl-tert-butyl ether ND ug/L 05/18/23 05:49 1634-04-45.0 3.1 1
Naphthalene ND ug/L 05/18/23 05:49 91-20-35.0 2.1 1
n-Propylbenzene ND ug/L 05/18/23 05:49 103-65-15.0 2.0 1
Styrene ND ug/L 05/18/23 05:49 100-42-55.0 1.9 1
1,1,1,2-Tetrachloroethane ND ug/L 05/18/23 05:49 630-20-65.0 1.1 1
1,1,2,2-Tetrachloroethane ND ug/L 05/18/23 05:49 79-34-55.0 2.0 1
Tetrachloroethene ND ug/L 05/18/23 05:49 127-18-45.0 1.8 1
Toluene ND ug/L 05/18/23 05:49 108-88-35.0 2.0 1
1,2,3-Trichlorobenzene ND ug/L 05/18/23 05:49 87-61-65.0 2.2 1
1,2,4-Trichlorobenzene ND ug/L 05/18/23 05:49 120-82-15.0 2.3 1
1,1,1-Trichloroethane ND ug/L 05/18/23 05:49 71-55-65.0 2.1 1
1,1,2-Trichloroethane ND ug/L 05/18/23 05:49 79-00-55.0 2.0 1
Trichloroethene ND ug/L 05/18/23 05:49 79-01-65.0 1.8 1
Trichlorofluoromethane ND ug/L 05/18/23 05:49 75-69-410.0 1.5 1
1,2,3-Trichloropropane ND ug/L 05/18/23 05:49 96-18-45.0 1.1 1
1,2,4-Trimethylbenzene ND ug/L 05/18/23 05:49 95-63-65.0 2.0 1
1,3,5-Trimethylbenzene ND ug/L 05/18/23 05:49 108-67-85.0 2.1 1
Vinyl acetate ND ug/L 05/18/23 05:49 108-05-410.0 5.6 1
Vinyl chloride ND ug/L 05/18/23 05:49 75-01-45.0 1.8 1
m&p-Xylene ND ug/L 05/18/23 05:49 179601-23-110.0 4.1 1
o-Xylene ND ug/L 05/18/23 05:49 95-47-65.0 2.0 1
Surrogates
4-Bromofluorobenzene (S)101 %05/18/23 05:49 460-00-470-130 1
1,2-Dichloroethane-d4 (S)119 %05/18/23 05:49 17060-07-070-130 1
Toluene-d8 (S)101 %05/18/23 05:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775291
EPA 7471B
EPA 7471B
7471 Mercury
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92667899001, 92667899002, 92667899003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4023113
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
Mercury mg/kg ND 0.0060 05/18/23 14:020.0037
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4023114LABORATORY CONTROL SAMPLE:
LCSSpike
Mercury mg/kg 0.0840.083 101 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4023115MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
4023116
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.077 97 75-12599 4 200.0790.0090 0.083 0.087
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775257
EPA 3050B
EPA 6010D
6010 MET
Laboratory:Pace Analytical Services - Asheville
Associated Lab Samples:92667899001, 92667899002, 92667899003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4022972
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
Arsenic mg/kg ND 2.5 05/19/23 10:590.087
Barium mg/kg ND 1.0 05/19/23 10:590.093
Cadmium mg/kg 0.016J 0.10 05/19/23 10:590.012
Chromium mg/kg 0.40J 0.50 05/19/23 10:590.13
Lead mg/kg ND 1.0 05/19/23 10:590.23
Selenium mg/kg ND 1.0 05/19/23 10:590.57
Silver mg/kg ND 0.50 05/19/23 10:590.036
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022973LABORATORY CONTROL SAMPLE:
LCSSpike
Arsenic mg/kg 52.250 104 80-120
Barium mg/kg 53.350 107 80-120
Cadmium mg/kg 52.150 104 80-120
Chromium mg/kg 54.050 108 80-120
Lead mg/kg 52.550 105 80-120
Selenium mg/kg 50.050 100 80-120
Silver mg/kg 26.225 105 80-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4022974MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
4022975
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 42 95 75-12587 10 2041.30.77J 40.8 36.8
Barium mg/kg M14221575-125333 11 2041.3298 388 436
Cadmium mg/kg 42 94 75-12587 10 2041.30.16 39.7 36.0
Chromium mg/kg M1,R1428875-12532 26 2041.366.5 103 79.9
Lead mg/kg 42 95 75-12586 11 2041.31.9 41.7 37.6
Selenium mg/kg 42 92 75-12583 12 2041.3ND 38.7 34.4
Silver mg/kg 21 104 75-12595 10 2020.60.16J 22.0 19.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775213
EPA 5035A/5030B
EPA 8260D
8260D 5035A 5030B
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667899001, 92667899002, 92667899003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4022883
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 05/18/23 02:061.9
1,1,1-Trichloroethane ug/kg ND 5.0 05/18/23 02:062.6
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 05/18/23 02:061.3
1,1,2-Trichloroethane ug/kg ND 5.0 05/18/23 02:061.7
1,1-Dichloroethane ug/kg ND 5.0 05/18/23 02:062.1
1,1-Dichloroethene ug/kg ND 5.0 05/18/23 02:062.1
1,1-Dichloropropene ug/kg ND 5.0 05/18/23 02:062.4
1,2,3-Trichlorobenzene ug/kg ND 5.0 05/18/23 02:064.0
1,2,3-Trichloropropane ug/kg ND 5.0 05/18/23 02:062.5
1,2,4-Trichlorobenzene ug/kg ND 5.0 05/18/23 02:064.2
1,2,4-Trimethylbenzene ug/kg ND 5.0 05/18/23 02:063.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 05/18/23 02:061.9
1,2-Dibromoethane (EDB)ug/kg ND 5.0 05/18/23 02:062.2
1,2-Dichlorobenzene ug/kg ND 5.0 05/18/23 02:061.8
1,2-Dichloroethane ug/kg ND 5.0 05/18/23 02:063.3
1,2-Dichloropropane ug/kg ND 5.0 05/18/23 02:061.5
1,3,5-Trimethylbenzene ug/kg ND 5.0 05/18/23 02:061.7
1,3-Dichlorobenzene ug/kg ND 5.0 05/18/23 02:061.6
1,3-Dichloropropane ug/kg ND 5.0 05/18/23 02:061.6
1,4-Dichlorobenzene ug/kg ND 5.0 05/18/23 02:061.3
2,2-Dichloropropane ug/kg ND 5.0 05/18/23 02:063.8
2-Butanone (MEK)ug/kg ND 100 05/18/23 02:0624.0
2-Chlorotoluene ug/kg ND 5.0 05/18/23 02:061.8
2-Hexanone ug/kg ND 50.0 05/18/23 02:064.8
4-Chlorotoluene ug/kg ND 5.0 05/18/23 02:062.8
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 05/18/23 02:064.8
Acetone ug/kg ND 100 05/18/23 02:0632.1
Benzene ug/kg ND 5.0 05/18/23 02:062.0
Bromobenzene ug/kg ND 5.0 05/18/23 02:061.6
Bromochloromethane ug/kg ND 5.0 05/18/23 02:061.5
Bromodichloromethane ug/kg ND 5.0 05/18/23 02:061.9
Bromoform ug/kg ND 5.0 05/18/23 02:061.8
Bromomethane ug/kg ND 20.0 v205/18/23 02:0615.5
Carbon tetrachloride ug/kg ND 5.0 05/18/23 02:061.9
Chlorobenzene ug/kg ND 5.0 05/18/23 02:062.9
Chloroethane ug/kg ND 10.0 05/18/23 02:063.9
Chloroform ug/kg ND 5.0 05/18/23 02:064.2
Chloromethane ug/kg ND 10.0 05/18/23 02:064.2
cis-1,2-Dichloroethene ug/kg ND 5.0 05/18/23 02:061.7
cis-1,3-Dichloropropene ug/kg ND 5.0 05/18/23 02:061.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4022883
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
Dibromochloromethane ug/kg ND 5.0 05/18/23 02:062.8
Dibromomethane ug/kg ND 5.0 05/18/23 02:061.1
Dichlorodifluoromethane ug/kg ND 10.0 IH05/18/23 02:065.1
Diisopropyl ether ug/kg ND 5.0 05/18/23 02:061.4
Ethylbenzene ug/kg ND 5.0 05/18/23 02:062.3
Hexachloro-1,3-butadiene ug/kg ND 10.0 05/18/23 02:068.2
Isopropylbenzene (Cumene)ug/kg ND 5.0 05/18/23 02:061.7
m&p-Xylene ug/kg ND 10.0 05/18/23 02:063.4
Methyl-tert-butyl ether ug/kg ND 5.0 05/18/23 02:061.9
Methylene Chloride ug/kg ND 20.0 05/18/23 02:0613.7
n-Butylbenzene ug/kg ND 5.0 05/18/23 02:063.2
n-Propylbenzene ug/kg ND 5.0 05/18/23 02:061.8
Naphthalene ug/kg ND 5.0 05/18/23 02:062.6
o-Xylene ug/kg ND 5.0 05/18/23 02:062.2
p-Isopropyltoluene ug/kg ND 5.0 05/18/23 02:062.5
sec-Butylbenzene ug/kg ND 5.0 05/18/23 02:062.2
Styrene ug/kg ND 5.0 05/18/23 02:061.3
tert-Butylbenzene ug/kg ND 5.0 05/18/23 02:061.8
Tetrachloroethene ug/kg ND 5.0 05/18/23 02:061.6
Toluene ug/kg ND 5.0 05/18/23 02:063.4
trans-1,2-Dichloroethene ug/kg ND 5.0 05/18/23 02:064.2
trans-1,3-Dichloropropene ug/kg ND 5.0 05/18/23 02:061.7
Trichloroethene ug/kg ND 5.0 05/18/23 02:064.0
Trichlorofluoromethane ug/kg ND 5.0 05/18/23 02:062.8
Vinyl acetate ug/kg ND 50.0 05/18/23 02:0610.3
Vinyl chloride ug/kg ND 10.0 05/18/23 02:062.5
Xylene (Total)ug/kg ND 10.0 05/18/23 02:062.8
1,2-Dichloroethane-d4 (S)%105 70-130 05/18/23 02:06
4-Bromofluorobenzene (S)%103 70-130 05/18/23 02:06
Toluene-d8 (S)%102 70-130 05/18/23 02:06
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022884LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 463500 93 70-130
1,1,1-Trichloroethane ug/kg 479500 96 70-130
1,1,2,2-Tetrachloroethane ug/kg 476500 95 70-130
1,1,2-Trichloroethane ug/kg 466500 93 70-130
1,1-Dichloroethane ug/kg 492500 98 70-130
1,1-Dichloroethene ug/kg 524500 105 70-130
1,1-Dichloropropene ug/kg 502500 100 70-130
1,2,3-Trichlorobenzene ug/kg 487500 97 70-130
1,2,3-Trichloropropane ug/kg 467500 93 70-130
1,2,4-Trichlorobenzene ug/kg 478500 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022884LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trimethylbenzene ug/kg 489500 98 70-130
1,2-Dibromo-3-chloropropane ug/kg 461500 92 67-130
1,2-Dibromoethane (EDB)ug/kg 467500 93 70-130
1,2-Dichlorobenzene ug/kg 473500 95 70-130
1,2-Dichloroethane ug/kg 481500 96 70-130
1,2-Dichloropropane ug/kg 479500 96 70-130
1,3,5-Trimethylbenzene ug/kg 496500 99 70-130
1,3-Dichlorobenzene ug/kg 464500 93 70-130
1,3-Dichloropropane ug/kg 461500 92 70-130
1,4-Dichlorobenzene ug/kg 443500 89 70-130
2,2-Dichloropropane ug/kg 432500 86 67-130
2-Butanone (MEK)ug/kg 9991000 100 66-130
2-Chlorotoluene ug/kg 489500 98 70-130
2-Hexanone ug/kg 10001000 100 70-130
4-Chlorotoluene ug/kg 484500 97 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 10101000 101 70-130
Acetone ug/kg 9161000 92 67-130
Benzene ug/kg 459500 92 70-130
Bromobenzene ug/kg 476500 95 70-130
Bromochloromethane ug/kg 477500 95 70-130
Bromodichloromethane ug/kg 462500 92 70-130
Bromoform ug/kg 449500 90 70-130
Bromomethane ug/kg 357 v35007153-175
Carbon tetrachloride ug/kg 470500 94 70-130
Chlorobenzene ug/kg 469500 94 70-130
Chloroethane ug/kg 458500 92 70-135
Chloroform ug/kg 472500 94 70-130
Chloromethane ug/kg 539500 108 64-130
cis-1,2-Dichloroethene ug/kg 486500 97 70-130
cis-1,3-Dichloropropene ug/kg 426500 85 70-130
Dibromochloromethane ug/kg 459500 92 70-130
Dibromomethane ug/kg 467500 93 70-130
Dichlorodifluoromethane ug/kg 551 IH50011063-145
Diisopropyl ether ug/kg 488500 98 68-130
Ethylbenzene ug/kg 438500 88 70-130
Hexachloro-1,3-butadiene ug/kg 467500 93 70-130
Isopropylbenzene (Cumene)ug/kg 481500 96 70-130
m&p-Xylene ug/kg 9331000 93 70-130
Methyl-tert-butyl ether ug/kg 452500 90 70-130
Methylene Chloride ug/kg 508500 102 67-130
n-Butylbenzene ug/kg 482500 96 70-130
n-Propylbenzene ug/kg 481500 96 70-130
Naphthalene ug/kg 485500 97 70-130
o-Xylene ug/kg 469500 94 70-130
p-Isopropyltoluene ug/kg 500500 100 70-130
sec-Butylbenzene ug/kg 480500 96 70-130
Styrene ug/kg 478500 96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022884LABORATORY CONTROL SAMPLE:
LCSSpike
tert-Butylbenzene ug/kg 491500 98 64-130
Tetrachloroethene ug/kg 468500 94 70-130
Toluene ug/kg 452500 90 70-130
trans-1,2-Dichloroethene ug/kg 510500 102 70-130
trans-1,3-Dichloropropene ug/kg 463500 93 70-130
Trichloroethene ug/kg 468500 94 70-130
Trichlorofluoromethane ug/kg 426500 85 70-130
Vinyl acetate ug/kg 9951000 100 70-134
Vinyl chloride ug/kg 420500 84 68-130
Xylene (Total)ug/kg 14001500 93 70-130
1,2-Dichloroethane-d4 (S)%97 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4022885MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
4022886
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 1420 65 58-14076 15 301420ND9221070
1,1,1-Trichloroethane ug/kg 1420 71 58-14485 18 301420ND10101210
1,1,2,2-Tetrachloroethane ug/kg 1420 72 52-13984 15 301420ND10201190
1,1,2-Trichloroethane ug/kg 1420 70 56-14079 13 301420ND9881130
1,1-Dichloroethane ug/kg 1420 73 58-14586 17 301420ND10301220
1,1-Dichloroethene ug/kg 1420 79 57-15894 17 301420ND11201330
1,1-Dichloropropene ug/kg 1420 75 58-15188 16 301420ND10601250
1,2,3-Trichlorobenzene ug/kg 1420 67 48-14979 17 301420ND9541130
1,2,3-Trichloropropane ug/kg 1420 72 54-13286 18 301420ND10201230
1,2,4-Trichlorobenzene ug/kg 1420 66 51-15180 20 301420ND9331140
1,2,4-Trimethylbenzene ug/kg M11420138-170-33 4 301420111001120010700
1,2-Dibromo-3-
chloropropane ug/kg 1420 66 44-13477 14 301420ND9421090
1,2-Dibromoethane (EDB)ug/kg 1420 63 60-13873 16 301420ND8911040
1,2-Dichlorobenzene ug/kg 1420 62 59-14774 18 301420ND8851060
1,2-Dichloroethane ug/kg 1420 72 57-13985 17 301420ND10201210
1,2-Dichloropropane ug/kg 1420 67 62-14579 16 301420ND9541120
1,3,5-Trimethylbenzene ug/kg M114204647-15946 0 301420365043004300
1,3-Dichlorobenzene ug/kg 1420 62 58-14475 18 301420ND8841060
1,3-Dichloropropane ug/kg 1420 67 60-14279 16 301420ND9511120
1,4-Dichlorobenzene ug/kg 1420 63 57-14375 18 301420ND8941070
2,2-Dichloropropane ug/kg 1420 74 37-14488 18 301420ND10501250
2-Butanone (MEK)ug/kg 2840 71 28-14681 13 302840ND20202300
2-Chlorotoluene ug/kg 1420 94 55-158104 10 301420ND13401480
2-Hexanone ug/kg 2840 73 44-14183 13 302840ND20702370
4-Chlorotoluene ug/kg 1420 73 55-14687 17 301420ND10401230
4-Methyl-2-pentanone
(MIBK)ug/kg 2840 71 50-13881 13 302840ND20202310
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4022885MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
4022886
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Acetone ug/kg 2840 68 20-13680 15 302840104J20402380
Benzene ug/kg 1420 69 60-14582 17 301420ND9781160
Bromobenzene ug/kg 1420 62 59-14573 16 301420ND8841030
Bromochloromethane ug/kg 1420 69 57-14379 14 301420ND9761120
Bromodichloromethane ug/kg 1420 68 53-13380 17 301420ND9601130
Bromoform ug/kg 1420 61 48-13371 16 301420ND8671010
Bromomethane ug/kg 1420 40 10-16749 21 301420ND569702
Carbon tetrachloride ug/kg 1420 68 57-14783 20 301420ND9641180
Chlorobenzene ug/kg 1420 65 61-14479 19 301420ND9291120
Chloroethane ug/kg 1420 27 10-15335 26 301420ND381492
Chloroform ug/kg 1420 72 58-14184 17 301420ND10201200
Chloromethane ug/kg 1420 81 54-16596 16 301420ND11701370
cis-1,2-Dichloroethene ug/kg 1420 73 59-14486 16 301420ND10401220
cis-1,3-Dichloropropene ug/kg 1420 69 56-13782 17 301420ND9741160
Dibromochloromethane ug/kg 1420 64 53-13974 15 301420ND9041050
Dibromomethane ug/kg 1420 62 60-13672 15 301420ND8821030
Dichlorodifluoromethane ug/kg IH,v1142011249-177131 15 301420ND16001860
Diisopropyl ether ug/kg 1420 68 53-13681 17 301420ND9721160
Ethylbenzene ug/kg 1420 63 53-15074 16 30142016.1 909 1070
Hexachloro-1,3-butadiene ug/kg 1420 62 42-18675 18 301420ND8871060
Isopropylbenzene
(Cumene)ug/kg 1420 69 62-15481 11 30142039913801550
m&p-Xylene ug/kg 2840 69 49-15682 17 30284076.3 2040 2410
Methyl-tert-butyl ether ug/kg 1420 66 54-13378 16 301420ND9391100
Methylene Chloride ug/kg 1420 69 50-15385 17 30142020311901400
n-Butylbenzene ug/kg 1420 83 44-17497 15 301420ND11901380
n-Propylbenzene ug/kg 1420 58 52-15760 1 301420141022402260
Naphthalene ug/kg 1420 74 37-15085 14 30142011.6J 1060 1220
o-Xylene ug/kg 1420 66 54-15075 11 30142022011601290
p-Isopropyltoluene ug/kg 1420 68 50-16478 8 30142071216801820
sec-Butylbenzene ug/kg 1420 86 58-161101 16 301420ND12201430
Styrene ug/kg 1420 67 60-14879 17 301420ND9471120
tert-Butylbenzene ug/kg 1420 72 44-15183 14 301420ND10301180
Tetrachloroethene ug/kg 1420 63 53-15173 14 301420ND8971040
Toluene ug/kg 1420 69 52-14881 16 30142030.9 1010 1180
trans-1,2-Dichloroethene ug/kg 1420 75 60-14889 17 301420ND10701260
trans-1,3-Dichloropropene ug/kg 1420 70 55-13384 18 301420ND9941190
Trichloroethene ug/kg 1420 66 60-14877 16 301420ND9351100
Trichlorofluoromethane ug/kg 1420 60 10-15474 21 301420ND8471050
Vinyl acetate ug/kg 2840 68 50-14980 15 302840ND19402270
Vinyl chloride ug/kg 1420 77 57-15790 16 301420ND10901280
Xylene (Total)ug/kg 4260 68 52-15380 15 30426029732003700
1,2-Dichloroethane-d4 (S)%109 70-130108
4-Bromofluorobenzene (S)%103 70-130103
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775135
EPA 8260D
EPA 8260D
8260D MSV
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667899004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4022454
Associated Lab Samples:92667899004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 5.0 05/18/23 00:581.1
1,1,1-Trichloroethane ug/L ND 5.0 05/18/23 00:582.1
1,1,2,2-Tetrachloroethane ug/L ND 5.0 05/18/23 00:582.0
1,1,2-Trichloroethane ug/L ND 5.0 05/18/23 00:582.0
1,1-Dichloroethane ug/L ND 5.0 05/18/23 00:582.3
1,1-Dichloroethene ug/L ND 5.0 05/18/23 00:582.2
1,1-Dichloropropene ug/L ND 5.0 05/18/23 00:582.8
1,2,3-Trichlorobenzene ug/L ND 5.0 05/18/23 00:582.2
1,2,3-Trichloropropane ug/L ND 5.0 05/18/23 00:581.1
1,2,4-Trichlorobenzene ug/L ND 5.0 05/18/23 00:582.3
1,2,4-Trimethylbenzene ug/L ND 5.0 05/18/23 00:582.0
1,2-Dibromo-3-chloropropane ug/L ND 5.0 05/18/23 00:581.0
1,2-Dibromoethane (EDB)ug/L ND 5.0 05/18/23 00:581.9
1,2-Dichlorobenzene ug/L ND 5.0 05/18/23 00:581.9
1,2-Dichloroethane ug/L ND 5.0 05/18/23 00:582.1
1,2-Dichloroethene (Total)ug/L ND 5.0 05/18/23 00:585.0
1,2-Dichloropropane ug/L ND 5.0 05/18/23 00:582.1
1,3,5-Trimethylbenzene ug/L ND 5.0 05/18/23 00:582.1
1,3-Dichlorobenzene ug/L ND 5.0 05/18/23 00:581.7
1,3-Dichloropropane ug/L ND 5.0 05/18/23 00:581.9
1,4-Dichlorobenzene ug/L ND 5.0 05/18/23 00:581.9
2,2-Dichloropropane ug/L ND 5.0 05/18/23 00:582.4
2-Butanone (MEK)ug/L ND 10.0 05/18/23 00:582.6
2-Chlorotoluene ug/L ND 5.0 05/18/23 00:581.8
2-Hexanone ug/L ND 10.0 05/18/23 00:584.2
4-Chlorotoluene ug/L ND 5.0 05/18/23 00:582.0
4-Methyl-2-pentanone (MIBK)ug/L ND 10.0 05/18/23 00:584.7
Acetone ug/L ND 25.0 05/18/23 00:583.0
Benzene ug/L ND 5.0 05/18/23 00:581.7
Bromobenzene ug/L ND 5.0 05/18/23 00:581.9
Bromochloromethane ug/L ND 5.0 05/18/23 00:582.1
Bromodichloromethane ug/L ND 5.0 05/18/23 00:581.1
Bromoform ug/L ND 5.0 05/18/23 00:581.0
Bromomethane ug/L ND 10.0 05/18/23 00:586.0
Carbon tetrachloride ug/L ND 5.0 05/18/23 00:582.2
Chlorobenzene ug/L ND 5.0 05/18/23 00:581.8
Chloroethane ug/L ND 10.0 05/18/23 00:584.1
Chloroform ug/L ND 5.0 05/18/23 00:581.3
Chloromethane ug/L ND 5.0 05/18/23 00:582.8
cis-1,2-Dichloroethene ug/L ND 5.0 05/18/23 00:582.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4022454
Associated Lab Samples:92667899004
Matrix:Water
AnalyzedMDL
cis-1,3-Dichloropropene ug/L ND 5.0 05/18/23 00:582.0
Dibromochloromethane ug/L ND 5.0 05/18/23 00:582.3
Dibromomethane ug/L ND 5.0 05/18/23 00:581.0
Dichlorodifluoromethane ug/L ND 5.0 05/18/23 00:581.8
Diisopropyl ether ug/L ND 5.0 05/18/23 00:581.4
Ethylbenzene ug/L ND 5.0 05/18/23 00:581.8
Hexachloro-1,3-butadiene ug/L ND 5.0 v205/18/23 00:584.8
Isopropylbenzene (Cumene)ug/L ND 5.0 05/18/23 00:582.1
m&p-Xylene ug/L ND 10.0 05/18/23 00:584.1
Methyl-tert-butyl ether ug/L ND 5.0 05/18/23 00:583.1
Methylene Chloride ug/L ND 5.0 05/18/23 00:583.3
n-Butylbenzene ug/L ND 5.0 05/18/23 00:582.3
n-Propylbenzene ug/L ND 5.0 05/18/23 00:582.0
Naphthalene ug/L ND 5.0 05/18/23 00:582.1
o-Xylene ug/L ND 5.0 05/18/23 00:582.0
p-Isopropyltoluene ug/L ND 5.0 05/18/23 00:581.0
sec-Butylbenzene ug/L ND 5.0 05/18/23 00:582.2
Styrene ug/L ND 5.0 05/18/23 00:581.9
tert-Butyl Alcohol ug/L ND 100 05/18/23 00:5811.6
tert-Butylbenzene ug/L ND 5.0 05/18/23 00:580.98
Tetrachloroethene ug/L ND 5.0 05/18/23 00:581.8
Toluene ug/L ND 5.0 05/18/23 00:582.0
trans-1,2-Dichloroethene ug/L ND 5.0 05/18/23 00:582.2
trans-1,3-Dichloropropene ug/L ND 5.0 05/18/23 00:582.2
Trichloroethene ug/L ND 5.0 05/18/23 00:581.8
Trichlorofluoromethane ug/L ND 10.0 05/18/23 00:581.5
Vinyl acetate ug/L ND 10.0 05/18/23 00:585.6
Vinyl chloride ug/L ND 5.0 05/18/23 00:581.8
1,2-Dichloroethane-d4 (S)%119 70-130 05/18/23 00:58
4-Bromofluorobenzene (S)%99 70-130 05/18/23 00:58
Toluene-d8 (S)%101 70-130 05/18/23 00:58
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022455LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 21.520 107 70-130
1,1,1-Trichloroethane ug/L 22.820 114 70-130
1,1,2,2-Tetrachloroethane ug/L 23.120 116 70-130
1,1,2-Trichloroethane ug/L 21.520 108 70-130
1,1-Dichloroethane ug/L 23.420 117 70-130
1,1-Dichloroethene ug/L 24.720 124 70-130
1,1-Dichloropropene ug/L 23.820 119 70-130
1,2,3-Trichlorobenzene ug/L 21.120 106 70-130
1,2,3-Trichloropropane ug/L 22.420 112 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022455LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 20.720 103 70-130
1,2,4-Trimethylbenzene ug/L 22.720 114 70-130
1,2-Dibromo-3-chloropropane ug/L 20.720 103 70-131
1,2-Dibromoethane (EDB)ug/L 22.020 110 70-130
1,2-Dichlorobenzene ug/L 21.620 108 70-130
1,2-Dichloroethane ug/L 24.420 122 70-130
1,2-Dichloroethene (Total)ug/L 47.0
1,2-Dichloropropane ug/L 22.320 111 70-130
1,3,5-Trimethylbenzene ug/L 22.820 114 70-130
1,3-Dichlorobenzene ug/L 21.520 107 70-130
1,3-Dichloropropane ug/L 21.520 108 70-130
1,4-Dichlorobenzene ug/L 21.620 108 70-130
2,2-Dichloropropane ug/L 23.020 115 68-135
2-Butanone (MEK)ug/L 46.740 117 70-134
2-Chlorotoluene ug/L 23.320 117 70-130
2-Hexanone ug/L 48.240 121 70-131
4-Chlorotoluene ug/L 23.320 116 70-130
4-Methyl-2-pentanone (MIBK)ug/L 45.840 114 70-130
Acetone ug/L 47.140 118 70-133
Benzene ug/L 21.620 108 70-130
Bromobenzene ug/L 20.620 103 70-130
Bromochloromethane ug/L 22.120 110 70-130
Bromodichloromethane ug/L 21.720 108 70-130
Bromoform ug/L 20.220 101 70-130
Bromomethane ug/L 19.020 95 45-151
Carbon tetrachloride ug/L 21.520 108 70-130
Chlorobenzene ug/L 21.520 108 70-130
Chloroethane ug/L 24.820 124 39-152
Chloroform ug/L 23.720 119 70-130
Chloromethane ug/L 24.220 121 58-130
cis-1,2-Dichloroethene ug/L 23.620 118 70-130
cis-1,3-Dichloropropene ug/L 21.120 106 70-130
Dibromochloromethane ug/L 21.220 106 70-130
Dibromomethane ug/L 19.320 97 70-130
Dichlorodifluoromethane ug/L 22.220 111 54-133
Diisopropyl ether ug/L 23.020 115 70-130
Ethylbenzene ug/L 22.020 110 70-130
Hexachloro-1,3-butadiene ug/L 19.4 v3209770-135
Isopropylbenzene (Cumene)ug/L 21.420 107 70-130
m&p-Xylene ug/L 43.640 109 70-130
Methyl-tert-butyl ether ug/L 22.020 110 70-130
Methylene Chloride ug/L 23.520 117 66-130
n-Butylbenzene ug/L 22.920 115 70-130
n-Propylbenzene ug/L 23.020 115 70-130
Naphthalene ug/L 22.720 114 70-130
o-Xylene ug/L 20.620 103 70-130
p-Isopropyltoluene ug/L 22.120 110 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022455LABORATORY CONTROL SAMPLE:
LCSSpike
sec-Butylbenzene ug/L 21.920 110 70-130
Styrene ug/L 21.720 108 70-130
tert-Butyl Alcohol ug/L 230200 115 68-134
tert-Butylbenzene ug/L 18.320 91 63-130
Tetrachloroethene ug/L 18.920 94 70-130
Toluene ug/L 21.020 105 70-130
trans-1,2-Dichloroethene ug/L 23.420 117 70-130
trans-1,3-Dichloropropene ug/L 21.720 109 70-130
Trichloroethene ug/L 20.220 101 70-130
Trichlorofluoromethane ug/L 20.720 103 62-130
Vinyl acetate ug/L 49.740 124 70-144
Vinyl chloride ug/L 19.520 97 62-130
1,2-Dichloroethane-d4 (S)%118 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4022457MATRIX SPIKE SAMPLE:
MSSpike
Result
92667224015
1,1,1,2-Tetrachloroethane ug/L 26.520 132 70-141<1.1
1,1,1-Trichloroethane ug/L 26.820 134 70-150<2.1
1,1,2,2-Tetrachloroethane ug/L 25.220 126 69-142<2.0
1,1,2-Trichloroethane ug/L 24.820 124 70-138<2.0
1,1-Dichloroethane ug/L 25.320 127 70-150<2.3
1,1-Dichloroethene ug/L 29.220 144 70-156<2.2
1,1-Dichloropropene ug/L 29.520 148 70-150<2.8
1,2,3-Trichlorobenzene ug/L 25.620 128 70-148<2.2
1,2,3-Trichloropropane ug/L 24.220 121 70-140<1.1
1,2,4-Trichlorobenzene ug/L 24.320 122 70-146<2.3
1,2,4-Trimethylbenzene ug/L 26.020 130 70-149<2.0
1,2-Dibromo-3-chloropropane ug/L 24.520 122 68-146<1.0
1,2-Dibromoethane (EDB)ug/L 24.820 124 70-138<1.9
1,2-Dichlorobenzene ug/L 25.120 126 70-141<1.9
1,2-Dichloroethane ug/L 24.820 124 69-143<2.1
1,2-Dichloroethene (Total)ug/L 67.715.8
1,2-Dichloropropane ug/L 25.520 128 68-156<2.1
1,3,5-Trimethylbenzene ug/L 26.320 132 70-153<2.1
1,3-Dichlorobenzene ug/L 25.820 129 70-143<1.7
1,3-Dichloropropane ug/L 23.820 119 70-138<1.9
1,4-Dichlorobenzene ug/L 25.220 126 70-142<1.9
2,2-Dichloropropane ug/L 28.820 144 52-170<2.4
2-Butanone (MEK)ug/L 51.340 128 60-157<2.6
2-Chlorotoluene ug/L 25.620 128 70-147<1.8
2-Hexanone ug/L 50.740 127 68-146<4.2
4-Chlorotoluene ug/L 26.220 131 70-142<2.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
4022457MATRIX SPIKE SAMPLE:
MSSpike
Result
92667224015
4-Methyl-2-pentanone (MIBK)ug/L 49.140 123 70-141<4.7
Acetone ug/L 46.440 113 58-157<3.0
Benzene ug/L 25.820 129 70-142<1.7
Bromobenzene ug/L 25.120 126 70-143<1.9
Bromochloromethane ug/L 25.220 126 70-146<2.1
Bromodichloromethane ug/L 24.620 123 70-139<1.1
Bromoform ug/L 24.020 120 64-140<1.0
Bromomethane ug/L 18.820 94 28-192<6.0
Carbon tetrachloride ug/L 27.020 135 70-148<2.2
Chlorobenzene ug/L 25.720 128 70-141<1.8
Chloroethane ug/L 23.420 117 58-191<4.1
Chloroform ug/L 25.720 127 70-148<1.3
Chloromethane ug/L 24.320 121 43-162<2.8
cis-1,2-Dichloroethene ug/L 40.320 123 68-15115.8
cis-1,3-Dichloropropene ug/L 24.520 123 70-139<2.0
Dibromochloromethane ug/L 24.620 123 70-144<2.3
Dibromomethane ug/L 24.420 122 70-139<1.0
Dichlorodifluoromethane ug/L 22.720 114 39-171<1.8
Diisopropyl ether ug/L 24.220 121 67-142<1.4
Ethylbenzene ug/L 25.120 126 70-143<1.8
Hexachloro-1,3-butadiene ug/L 27.620 138 64-163<4.8
Isopropylbenzene (Cumene)ug/L 26.420 132 70-145<2.1
m&p-Xylene ug/L 50.840 127 70-144<4.1
Methyl-tert-butyl ether ug/L 23.320 116 65-143<3.1
Methylene Chloride ug/L 25.520 126 62-149<3.3
n-Butylbenzene ug/L 27.620 138 65-163<2.3
n-Propylbenzene ug/L 25.920 130 70-152<2.0
Naphthalene ug/L 24.520 122 67-147<2.1
o-Xylene ug/L 25.220 126 70-145<2.0
p-Isopropyltoluene ug/L 27.220 136 70-147<1.0
sec-Butylbenzene ug/L 26.820 134 70-144<2.2
Styrene ug/L 25.020 125 70-143<1.9
tert-Butyl Alcohol ug/L 342200 171 35-200<11.6
tert-Butylbenzene ug/L 21.620 108 62-133<0.98
Tetrachloroethene ug/L 25.920 129 70-145<1.8
Toluene ug/L 24.920 124 70-142<2.0
trans-1,2-Dichloroethene ug/L 27.420 137 70-151<2.2
trans-1,3-Dichloropropene ug/L 25.120 126 70-139<2.2
Trichloroethene ug/L 13820 143 62-146110
Trichlorofluoromethane ug/L 25.620 128 63-153<1.5
Vinyl acetate ug/L 49.040 123 61-162<5.6
Vinyl chloride ug/L 20.520 102 61-163<1.8
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667224013
4022456SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30<1.1
1,1,1-Trichloroethane ug/L ND 30<2.1
1,1,2,2-Tetrachloroethane ug/L ND 30<2.0
1,1,2-Trichloroethane ug/L ND 30<2.0
1,1-Dichloroethane ug/L ND 30<2.3
1,1-Dichloroethene ug/L 5.1 6 305.4
1,1-Dichloropropene ug/L ND 30<2.8
1,2,3-Trichlorobenzene ug/L ND 30<2.2
1,2,3-Trichloropropane ug/L ND 30<1.1
1,2,4-Trichlorobenzene ug/L ND 30<2.3
1,2,4-Trimethylbenzene ug/L ND 30<2.0
1,2-Dibromo-3-chloropropane ug/L ND 30<1.0
1,2-Dibromoethane (EDB)ug/L ND 30<1.9
1,2-Dichlorobenzene ug/L ND 30<1.9
1,2-Dichloroethane ug/L ND 30<2.1
1,2-Dichloroethene (Total)ug/L ND 30<5.0
1,2-Dichloropropane ug/L ND 30<2.1
1,3,5-Trimethylbenzene ug/L ND 30<2.1
1,3-Dichlorobenzene ug/L ND 30<1.7
1,3-Dichloropropane ug/L ND 30<1.9
1,4-Dichlorobenzene ug/L ND 30<1.9
2,2-Dichloropropane ug/L ND 30<2.4
2-Butanone (MEK)ug/L ND 30<2.6
2-Chlorotoluene ug/L ND 30<1.8
2-Hexanone ug/L ND 30<4.2
4-Chlorotoluene ug/L ND 30<2.0
4-Methyl-2-pentanone (MIBK)ug/L ND 30<4.7
Acetone ug/L ND 30<3.0
Benzene ug/L ND 30<1.7
Bromobenzene ug/L ND 30<1.9
Bromochloromethane ug/L ND 30<2.1
Bromodichloromethane ug/L ND 30<1.1
Bromoform ug/L ND 30<1.0
Bromomethane ug/L ND 30<6.0
Carbon tetrachloride ug/L ND 30<2.2
Chlorobenzene ug/L ND 30<1.8
Chloroethane ug/L ND 30<4.1
Chloroform ug/L ND 301.3J
Chloromethane ug/L ND 30<2.8
cis-1,2-Dichloroethene ug/L ND 30<2.2
cis-1,3-Dichloropropene ug/L ND 30<2.0
Dibromochloromethane ug/L ND 30<2.3
Dibromomethane ug/L ND 30<1.0
Dichlorodifluoromethane ug/L 3.4J 304.0J
Diisopropyl ether ug/L ND 30<1.4
Ethylbenzene ug/L ND 30<1.8
Hexachloro-1,3-butadiene ug/L ND 30<4.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667224013
4022456SAMPLE DUPLICATE:
Isopropylbenzene (Cumene)ug/L ND 30<2.1
m&p-Xylene ug/L ND 30<4.1
Methyl-tert-butyl ether ug/L ND 30<3.1
Methylene Chloride ug/L ND 30<3.3
n-Butylbenzene ug/L ND 30<2.3
n-Propylbenzene ug/L ND 30<2.0
Naphthalene ug/L ND 30<2.1
o-Xylene ug/L ND 30<2.0
p-Isopropyltoluene ug/L ND 30<1.0
sec-Butylbenzene ug/L ND 30<2.2
Styrene ug/L ND 30<1.9
tert-Butyl Alcohol ug/L ND 30<11.6
tert-Butylbenzene ug/L ND 30<0.98
Tetrachloroethene ug/L ND 30<1.8
Toluene ug/L ND 30<2.0
trans-1,2-Dichloroethene ug/L ND 30<2.2
trans-1,3-Dichloropropene ug/L ND 30<2.2
Trichloroethene ug/L ND 30<1.8
Trichlorofluoromethane ug/L 136 14 30155
Vinyl acetate ug/L ND 30<5.6
Vinyl chloride ug/L ND 30<1.8
1,2-Dichloroethane-d4 (S)%101120
4-Bromofluorobenzene (S)%9799
Toluene-d8 (S)%98101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775148
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667899001, 92667899002, 92667899003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4022606
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 325 05/18/23 10:51128
1,2-Dichlorobenzene ug/kg ND 325 05/18/23 10:51117
1,3-Dichlorobenzene ug/kg ND 325 05/18/23 10:51115
1,4-Dichlorobenzene ug/kg ND 325 05/18/23 10:51124
1-Methylnaphthalene ug/kg ND 325 05/18/23 10:51114
2,2'-Oxybis(1-chloropropane)ug/kg ND 325 05/18/23 10:51154
2,4,5-Trichlorophenol ug/kg ND 325 05/18/23 10:51149
2,4,6-Trichlorophenol ug/kg ND 325 05/18/23 10:51134
2,4-Dichlorophenol ug/kg ND 325 05/18/23 10:51127
2,4-Dimethylphenol ug/kg ND 325 05/18/23 10:51135
2,4-Dinitrophenol ug/kg ND 1620 05/18/23 10:511000
2,4-Dinitrotoluene ug/kg ND 325 05/18/23 10:51125
2,6-Dinitrotoluene ug/kg ND 325 05/18/23 10:51119
2-Chloronaphthalene ug/kg ND 325 05/18/23 10:51129
2-Chlorophenol ug/kg ND 325 05/18/23 10:51122
2-Methylnaphthalene ug/kg ND 325 05/18/23 10:51130
2-Methylphenol(o-Cresol)ug/kg ND 325 05/18/23 10:51133
2-Nitroaniline ug/kg ND 1620 05/18/23 10:51266
2-Nitrophenol ug/kg ND 325 05/18/23 10:51141
3&4-Methylphenol(m&p Cresol)ug/kg ND 325 05/18/23 10:51131
3,3'-Dichlorobenzidine ug/kg ND 649 05/18/23 10:51219
3-Nitroaniline ug/kg ND 1620 05/18/23 10:51255
4,6-Dinitro-2-methylphenol ug/kg ND 649 05/18/23 10:51303
4-Bromophenylphenyl ether ug/kg ND 325 05/18/23 10:51125
4-Chloro-3-methylphenol ug/kg ND 649 05/18/23 10:51228
4-Chloroaniline ug/kg ND 649 05/18/23 10:51255
4-Chlorophenylphenyl ether ug/kg ND 325 05/18/23 10:51121
4-Nitroaniline ug/kg ND 649 05/18/23 10:51247
4-Nitrophenol ug/kg ND 1620 05/18/23 10:51628
Acenaphthene ug/kg ND 325 05/18/23 10:51114
Acenaphthylene ug/kg ND 325 05/18/23 10:51114
Aniline ug/kg ND 325 05/18/23 10:51127
Anthracene ug/kg ND 325 05/18/23 10:51106
Benzo(a)anthracene ug/kg ND 325 05/18/23 10:51108
Benzo(a)pyrene ug/kg ND 325 05/18/23 10:51112
Benzo(b)fluoranthene ug/kg ND 325 05/18/23 10:51108
Benzo(g,h,i)perylene ug/kg ND 325 05/18/23 10:51126
Benzo(k)fluoranthene ug/kg ND 325 05/18/23 10:51114
Benzoic Acid ug/kg ND 1620 05/18/23 10:51697
Benzyl alcohol ug/kg ND 649 05/18/23 10:51246
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:4022606
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethoxy)methane ug/kg ND 325 05/18/23 10:51135
bis(2-Chloroethyl) ether ug/kg ND 325 05/18/23 10:51122
bis(2-Ethylhexyl)phthalate ug/kg ND 325 05/18/23 10:51126
Butylbenzylphthalate ug/kg ND 325 05/18/23 10:51137
Chrysene ug/kg ND 325 05/18/23 10:51118
Di-n-butylphthalate ug/kg ND 325 05/18/23 10:51109
Di-n-octylphthalate ug/kg ND 325 05/18/23 10:51128
Dibenz(a,h)anthracene ug/kg ND 325 05/18/23 10:51125
Dibenzofuran ug/kg ND 325 05/18/23 10:51117
Diethylphthalate ug/kg ND 325 05/18/23 10:51119
Dimethylphthalate ug/kg ND 325 05/18/23 10:51118
Fluoranthene ug/kg ND 325 05/18/23 10:51111
Fluorene ug/kg ND 325 05/18/23 10:51114
Hexachloro-1,3-butadiene ug/kg ND 325 05/18/23 10:51141
Hexachlorobenzene ug/kg ND 325 05/18/23 10:51127
Hexachlorocyclopentadiene ug/kg ND 325 05/18/23 10:51186
Hexachloroethane ug/kg ND 325 05/18/23 10:51124
Indeno(1,2,3-cd)pyrene ug/kg ND 325 05/18/23 10:51128
Isophorone ug/kg ND 325 05/18/23 10:51145
N-Nitroso-di-n-propylamine ug/kg ND 325 05/18/23 10:51122
N-Nitrosodimethylamine ug/kg ND 325 05/18/23 10:51109
N-Nitrosodiphenylamine ug/kg ND 325 05/18/23 10:51115
Naphthalene ug/kg ND 325 05/18/23 10:51110
Nitrobenzene ug/kg ND 325 05/18/23 10:51150
Pentachlorophenol ug/kg ND 649 05/18/23 10:51318
Phenanthrene ug/kg ND 325 05/18/23 10:51106
Phenol ug/kg ND 325 05/18/23 10:51145
Pyrene ug/kg ND 325 05/18/23 10:51132
Pyridine ug/kg ND 325 05/18/23 10:51102
2,4,6-Tribromophenol (S)%72 10-131 05/18/23 10:51
2-Fluorobiphenyl (S)%71 10-130 05/18/23 10:51
2-Fluorophenol (S)%64 10-130 05/18/23 10:51
Nitrobenzene-d5 (S)%68 10-130 05/18/23 10:51
Phenol-d6 (S)%62 10-130 05/18/23 10:51
Terphenyl-d14 (S)%71 10-130 05/18/23 10:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022607LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 10801690 64 43-130
1,2-Dichlorobenzene ug/kg 11301690 66 43-130
1,3-Dichlorobenzene ug/kg 10701690 63 43-130
1,4-Dichlorobenzene ug/kg 10801690 64 44-130
1-Methylnaphthalene ug/kg 12401690 73 47-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022607LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)ug/kg 11601690 69 29-130
2,4,5-Trichlorophenol ug/kg 11501690 68 47-130
2,4,6-Trichlorophenol ug/kg 11001690 65 47-130
2,4-Dichlorophenol ug/kg 11901690 70 45-130
2,4-Dimethylphenol ug/kg 17301690 102 45-130
2,4-Dinitrophenol ug/kg 55508470 65 27-140
2,4-Dinitrotoluene ug/kg 11201690 66 46-130
2,6-Dinitrotoluene ug/kg 11601690 68 48-130
2-Chloronaphthalene ug/kg 10701690 63 46-130
2-Chlorophenol ug/kg 11301690 67 43-130
2-Methylnaphthalene ug/kg 11501690 68 47-130
2-Methylphenol(o-Cresol)ug/kg 11701690 69 42-130
2-Nitroaniline ug/kg 21103390 62 41-130
2-Nitrophenol ug/kg 11901690 70 48-130
3&4-Methylphenol(m&p Cresol)ug/kg 13101690 77 39-130
3,3'-Dichlorobenzidine ug/kg 20603390 61 41-130
3-Nitroaniline ug/kg 19103390 56 37-130
4,6-Dinitro-2-methylphenol ug/kg 25103390 74 38-141
4-Bromophenylphenyl ether ug/kg 10701690 63 47-130
4-Chloro-3-methylphenol ug/kg 24203390 71 44-130
4-Chloroaniline ug/kg 20603390 61 41-130
4-Chlorophenylphenyl ether ug/kg 10601690 63 45-130
4-Nitroaniline ug/kg 18503390 54 42-130
4-Nitrophenol ug/kg 51108470 60 39-131
Acenaphthene ug/kg 11301690 67 49-130
Acenaphthylene ug/kg 11301690 66 50-130
Aniline ug/kg 8901690 53 38-130
Anthracene ug/kg 10801690 64 49-130
Benzo(a)anthracene ug/kg 10801690 63 51-130
Benzo(a)pyrene ug/kg 12001690 71 51-130
Benzo(b)fluoranthene ug/kg 1100 v316906549-130
Benzo(g,h,i)perylene ug/kg 1070 v316906348-140
Benzo(k)fluoranthene ug/kg 13001690 77 51-130
Benzoic Acid ug/kg 29608470 35 22-130
Benzyl alcohol ug/kg 21603390 64 43-130
bis(2-Chloroethoxy)methane ug/kg 11001690 65 43-130
bis(2-Chloroethyl) ether ug/kg 10601690 63 42-130
bis(2-Ethylhexyl)phthalate ug/kg 12501690 74 43-130
Butylbenzylphthalate ug/kg 12501690 74 44-131
Chrysene ug/kg 12801690 75 51-130
Di-n-butylphthalate ug/kg 11401690 67 46-130
Di-n-octylphthalate ug/kg 12401690 73 45-130
Dibenz(a,h)anthracene ug/kg 9951690 59 48-130
Dibenzofuran ug/kg 10801690 63 10-130
Diethylphthalate ug/kg 11401690 68 48-130
Dimethylphthalate ug/kg 11201690 66 48-130
Fluoranthene ug/kg 11201690 66 48-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
4022607LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene ug/kg 11201690 66 48-130
Hexachloro-1,3-butadiene ug/kg 11201690 66 39-130
Hexachlorobenzene ug/kg 10701690 63 47-130
Hexachlorocyclopentadiene ug/kg 10501690 62 17-130
Hexachloroethane ug/kg 11901690 70 40-130
Indeno(1,2,3-cd)pyrene ug/kg 11201690 66 50-130
Isophorone ug/kg 12101690 72 41-130
N-Nitroso-di-n-propylamine ug/kg 12501690 73 36-130
N-Nitrosodimethylamine ug/kg 9871690 58 34-130
N-Nitrosodiphenylamine ug/kg 11001690 65 48-130
Naphthalene ug/kg 11201690 66 46-130
Nitrobenzene ug/kg 11501690 68 39-130
Pentachlorophenol ug/kg 21703390 64 42-130
Phenanthrene ug/kg 11401690 68 50-130
Phenol ug/kg 11701690 69 42-130
Pyrene ug/kg 12501690 74 50-130
Pyridine ug/kg 9051690 53 26-130
2,4,6-Tribromophenol (S)%69 10-131
2-Fluorobiphenyl (S)%63 10-130
2-Fluorophenol (S)%59 10-130
Nitrobenzene-d5 (S)%66 10-130
Phenol-d6 (S)%64 10-130
Terphenyl-d14 (S)%69 10-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4022608MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
4022609
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1720 48 16-13045 5 301740ND819778
1,2-Dichlorobenzene ug/kg 1720 47 19-13044 6 301740ND803760
1,3-Dichlorobenzene ug/kg 1720 46 19-13043 5 301740ND784749
1,4-Dichlorobenzene ug/kg 1720 46 20-13042 6 301740ND788740
1-Methylnaphthalene ug/kg 1720 46 19-13042 6 301740ND785739
2,2'-Oxybis(1-
chloropropane)ug/kg 1720 37 10-13035 5 301740ND642612
2,4,5-Trichlorophenol ug/kg 1720 49 19-13044 8 301740ND837774
2,4,6-Trichlorophenol ug/kg 1720 49 18-13043 10 301740ND834754
2,4-Dichlorophenol ug/kg 1720 48 16-13045 6 301740ND833785
2,4-Dimethylphenol ug/kg 1720 66 10-13061 6 301740ND11301070
2,4-Dinitrophenol ug/kg 8590 29 10-14325 14 308710ND25202200
2,4-Dinitrotoluene ug/kg 1720 46 19-13041 11 301740ND799717
2,6-Dinitrotoluene ug/kg 1720 47 22-13042 10 301740ND803730
2-Chloronaphthalene ug/kg 1720 46 18-13043 5 301740ND787752
2-Chlorophenol ug/kg 1720 47 20-13043 7 301740ND799747
2-Methylnaphthalene ug/kg 1720 44 18-13041 6 301740ND759714
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4022608MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
4022609
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Methylphenol(o-Cresol)ug/kg 1720 45 13-13042 5 301740ND772736
2-Nitroaniline ug/kg 3440 42 18-13038 303480ND1430J1320J
2-Nitrophenol ug/kg 1720 47 19-13042 9 301740ND813740
3&4-Methylphenol(m&p
Cresol)ug/kg 1720 43 13-13042 3 301740ND745723
3,3'-Dichlorobenzidine ug/kg 3440 42 10-13039 6 303480ND14401360
3-Nitroaniline ug/kg 3440 41 22-13036 303480ND1410J1270J
4,6-Dinitro-2-methylphenol ug/kg 3440 44 10-14437 16 303480ND15001270
4-Bromophenylphenyl ether ug/kg 1720 47 18-13042 11 301740ND810726
4-Chloro-3-methylphenol ug/kg 3440 43 16-13041 5 303480ND14901420
4-Chloroaniline ug/kg 3440 40 17-13038 4 303480ND13701320
4-Chlorophenylphenyl ether ug/kg 1720 46 17-13042 10 301740ND798725
4-Nitroaniline ug/kg 3440 43 21-13036 16 303480ND14701260
4-Nitrophenol ug/kg 8590 42 13-13136 14 308710ND36103140
Acenaphthene ug/kg 1720 47 20-13042 8 301740ND804739
Acenaphthylene ug/kg 1720 47 21-13044 6 301740ND804758
Aniline ug/kg 1720 35 10-13034 0 301740ND594592
Anthracene ug/kg 1720 45 19-13041 10 301740ND780709
Benzo(a)anthracene ug/kg 1720 46 17-13042 8 301740ND798740
Benzo(a)pyrene ug/kg 1720 46 14-13042 9 301740ND796729
Benzo(b)fluoranthene ug/kg 1720 45 11-13441 7 301740ND768716
Benzo(g,h,i)perylene ug/kg 1720 55 12-13050 8 301740ND945870
Benzo(k)fluoranthene ug/kg 1720 48 15-13044 9 301740ND833760
Benzoic Acid ug/kg 8590 12 10-13011 308710ND1070J982J
Benzyl alcohol ug/kg 3440 40 20-13038 5 303480ND13801320
bis(2-
Chloroethoxy)methane ug/kg 1720 41 16-13038 7 301740ND703657
bis(2-Chloroethyl) ether ug/kg 1720 40 18-13038 6 301740ND693656
bis(2-Ethylhexyl)phthalate ug/kg 1720 45 11-13041 10 301740ND781708
Butylbenzylphthalate ug/kg 1720 45 10-13040 11 301740ND776695
Chrysene ug/kg 1720 48 17-13043 8 301740ND820756
Di-n-butylphthalate ug/kg 1720 46 16-13040 12 301740ND788700
Di-n-octylphthalate ug/kg 1720 43 16-13038 9 301740ND736670
Dibenz(a,h)anthracene ug/kg 1720 53 13-13048 10 301740ND919830
Dibenzofuran ug/kg 1720 46 19-13043 6 301740ND795745
Diethylphthalate ug/kg 1720 46 22-13040 12 301740ND783696
Dimethylphthalate ug/kg 1720 46 23-13041 10 301740ND782707
Fluoranthene ug/kg 1720 47 14-13043 8 301740ND803742
Fluorene ug/kg 1720 47 19-13043 9 301740ND811743
Hexachloro-1,3-butadiene ug/kg 1720 49 12-13044 9 301740ND847773
Hexachlorobenzene ug/kg 1720 48 17-13044 9 301740ND831763
Hexachlorocyclopentadiene ug/kg 1720 40 10-13037 6 301740ND685648
Hexachloroethane ug/kg 1720 45 14-13043 4 301740ND777745
Indeno(1,2,3-cd)pyrene ug/kg 1720 55 13-13050 8 301740ND945868
Isophorone ug/kg 1720 41 17-13039 5 301740ND709671
N-Nitroso-di-n-propylamine ug/kg 1720 40 10-13037 5 301740ND687653
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
4022608MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
4022609
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodimethylamine ug/kg 1720 41 16-13037 9 301740ND709649
N-Nitrosodiphenylamine ug/kg 1720 47 19-13043 7 301740ND810753
Naphthalene ug/kg 1720 46 18-13043 6 301740ND794751
Nitrobenzene ug/kg 1720 44 15-13041 6 301740ND755709
Pentachlorophenol ug/kg 3440 37 10-13030 18 303480ND12601050
Phenanthrene ug/kg 1720 48 17-13044 7 301740ND827768
Phenol ug/kg 1720 47 15-13044 5 301740ND804764
Pyrene ug/kg 1720 49 31-13044 9 301740ND846771
Pyridine ug/kg 1720 39 10-13038 2 301740ND672659
2,4,6-Tribromophenol (S)%49 10-13145
2-Fluorobiphenyl (S)%44 10-13043
2-Fluorophenol (S)%42 10-13041
Nitrobenzene-d5 (S)%42 10-13042
Phenol-d6 (S)%40 10-13039
Terphenyl-d14 (S)%47 10-13044
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
775097
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92667899001, 92667899002, 92667899003
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667448001
4022253SAMPLE DUPLICATE:
Percent Moisture %2.9 N25252.7
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667899003
4022418SAMPLE DUPLICATE:
Percent Moisture %3.9 N23254.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2062864
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92667899001, 92667899002, 92667899003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3927220-1
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
Total Solids %0.00200 05/19/23 10:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3927220-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667899003
R3927220-3SAMPLE DUPLICATE:
Total Solids %94.3 0.147 1094.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 49
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
2062698
3060A
EPA 7199
Wet Chemistry 7199
Laboratory:Pace National - Mt. Juliet
Associated Lab Samples:92667899001, 92667899002, 92667899003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3927517-1
Associated Lab Samples:92667899001, 92667899002, 92667899003
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 05/22/23 00:400.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3927517-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 8.7910.0 87.9 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3927517-6MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92667899003
R3927517-7
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg ML21.2 80.1 75.0-12570.1 13.3 2021.2ND 17.0 14.9
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3927517-8MATRIX SPIKE SAMPLE:
MSSpike
Result
92667899003
Chromium, Hexavalent mg/kg 731697 105 75.0-125ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1617398-04
R3927517-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92667899001
R3927517-4SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 49
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Common Laboratory Contaminant.C9
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Matrix spike recovery and/or matrix spike duplicate recovery was below laboratory control limits. Result may be biased
low.ML
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
RPD value was outside control limits.R1
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 49
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92667899
71237109-CANAC KITCHENS BROWNF
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92667899001 775257 775273SS-1 EPA 3050B EPA 6010D
92667899002 775257 775273DUP-1 EPA 3050B EPA 6010D
92667899003 775257 775273SS-2 EPA 3050B EPA 6010D
92667899001 775291 775313SS-1 EPA 7471B EPA 7471B
92667899002 775291 775313DUP-1 EPA 7471B EPA 7471B
92667899003 775291 775313SS-2 EPA 7471B EPA 7471B
92667899001 775148 775249SS-1 EPA 3546 EPA 8270E
92667899002 775148 775249DUP-1 EPA 3546 EPA 8270E
92667899003 775148 775249SS-2 EPA 3546 EPA 8270E
92667899001 775213 775240SS-1 EPA 5035A/5030B EPA 8260D
92667899002 775213 775240DUP-1 EPA 5035A/5030B EPA 8260D
92667899003 775213 775240SS-2 EPA 5035A/5030B EPA 8260D
92667899004 775135EQUIP BLANK EPA 8260D
92667899001 775097SS-1 SW-846
92667899002 775097DUP-1 SW-846
92667899003 775097SS-2 SW-846
92667899001 2062864 2062864SS-1 SM 2540 G SM 2540G
92667899002 2062864 2062864DUP-1 SM 2540 G SM 2540G
92667899003 2062864 2062864SS-2 SM 2540 G SM 2540G
92667899001 2062698 2062698SS-1 3060A EPA 7199
92667899002 2062698 2062698DUP-1 3060A EPA 7199
92667899003 2062698 2062698SS-2 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/22/2023 03:03 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 49
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