MO-9324_40784_CA_MRP_20230207

100 East Ruffin Street, Mebane, North Carolina 27302
Telephone [phone] ·Facsimile [phone]
www.terraquestpc.com

GROUNDWATER MONITORING REPORT
(1/18/23 sampling event)

PERTH MINI MART
818 PERTH ROAD
TROUTMAN, IREDELL COUNTY, NORTH CAROLINA

Latitude: 35.684542° N Longitude: -80.895851° W

Release Information:
Date Release Discovered: November 30, 2017 (Lab Confirmed)
Estimated Release Quantity: Unknown
Release Cause/Source: Gasoline Underground Storage Tank System
Previous USTs (release source): 2, 6,000-gallon gas, 1, 4,000-gallon gas, 1, 2,000-gallon non-
ethanol gas (formerly held diesel)
Current (not leaking) USTs: 2, 12,000-gallon gas (compartmentalized)
Current (not leaking) AST: 1,2,000-gallon diesel
NCDEQ-DWM UST Release Incident Number: 40784
Risk Ranking Classification: High (active water supply wells)
Land-Use Classification: Residential

Facility ID: 00-0-0000024524

Property Owner & UST Owner/Operator:

Madhukunj, LLC
135 Corona Circle
Mooresville, NC 28117

Terraquest Project No. 08217

February 7, 2023

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 i Troutman, Iredell County, North Carolina
CERTIFICATION FOR THE SUBMITTAL
OF AN ENVIRONMENTAL/GEOLOGICAL ASSESSMENT

Attached is the Groundwater Monitoring Report for:

Release Address: Perth Mini Mart
Address: 818 Perth Road
City: Troutman State: NC Zip Code: 28166

Responsible Party: Madhukunj, LLC
Address: 135 Corona Circle
City: Mooresville State: NC Zip Code: 28117

I, Michael J. Brown, a Licensed Geologist in the State of North Carolina for TERRAQUEST
ENVIRONMENTAL CONSULTANTS, P.C. do hereby certify that I am familiar with and have
reviewed all material including figures within this report and that to the best of my knowledge
the data, site assessment, figures, and other associated materials are correct and accurate. All
work was performed under my direct supervision. My seal and signature are affixed below.

Terraquest Environmental Consultants, P.C. is licensed to practice geology and engineering in
North Carolina. The geology certification number of the corporation is C-291. The engineering
certification number of the corporation is C-4634. Engineering is practiced out of the Cary, NC
office.

TERRAQUEST ENVIRONMENTAL CONSULTANTS, P.C.

Ryan D. Kerins Michael J. Brown, P.G.
Project Manager President

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 ii Troutman, Iredell County, North Carolina
TABLE OF CONTENTS
EXECUTIVE SUMMARY .....................................................................................................................ii
1.0 INTRODUCTION ................................................................................................................... 1
2.0 UPDATE OF SITE HISTORY AND CHARACTERIZATION ......................................................... 1
2.1 UST Owner .............................................................................................................. 1
2.2 Tank and Release Information ................................................................................ 1
2.3 Receptor Information ............................................................................................. 4
2.4 Regional Geology and Hydrogeology ...................................................................... 5
2.5 Site Geology and Hydrogeology .............................................................................. 7
3.0 SOIL ASSESSMENT AND EXCAVATION............................................................................... 13
4.0 FREE PRODUCT ASSESSMENT AND RECOVERY ................................................................. 14
5.0 GROUNDWATER ASSESSMENT ......................................................................................... 21
6.0 CONCLUSIONS ................................................................................................................... 22
7.0 LIMITATIONS ..................................................................................................................... 23
REFERENCES .................................................................................................................................. 24

TABLES

1. Site History (UST/AST System Information)
2. Surrounding Property Owners
3. Water Supply Well Information
4. Monitoring Well Construction Information
5. Summary of Groundwater Sampling Results

FIGURES

1. Site Location Map
2. Site Vicinity Map
3. Site Layout Map
4. Potentiometric Surface Map (1/18/23)
5. Groundwater Analytical Results Map (1/18/23)

APPENDICES

A. Technical Methods/Standard Procedures
B. Chronological Site History
C. Historical Groundwater Data
D. Groundwater Analytical Report
ENVIRONMENTAL ACRONYMS

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 i Troutman, Iredell County, North Carolina
2L Standard Groundwater Standards Title 15A NCAC 2L
0.0202(g)
2B Standard Surface Water Standards Title 15A NCAC 2B
AFVR Aggressive Fluid-Vapor Recovery
AST Aboveground Storage Tank
BGL Below Ground Level
BTEX Benzene, toluene, ethylbenzene, xylenes
C&D Construction and Demolition
CAP Corrective Action Plan
CAPR Corrective Action Performance Report
CADR Corrective Action Design Report
CSA Comprehensive Site Assessment
DPE Dual-phase Extraction
EPA Environmental Protection Agency
ePATA Electronic Pre-Approval Task Authorization
EPH Extractable Petroleum Hydrocarbons
ESA Environmental Site Assessment
GCL Gross Contamination Level
LEL Lower Explosive Limit
LSA Limited Site Assessment
IPE di-Isopropyl Ether
ISCO In-situ Chemical Oxidation
MADEP Massachusetts Department of Environmental
Protection
MDL Method Detection Limit
MNA Monitored Natural Attenuation
MMPE Mobile Multi Phase Extraction
MSCC Maximum Soil Contaminant
Concentration
MSL Mean Sea Level
MSW Municipal Solid Waste
MTBE Methyl tertiary-Butyl Ether
NC North Carolina
NCAC NC Administrative Code
NCDENR NC Department of Environment and Natural
Resources
NCDEQ NC Department of Environmental
Quality
NCDOT NC Department of Transportation
NCDWM-SW NC Division of Waste Management’s Solid
Waste Section
NCDWM-UST NC Division of Waste Management’s UST
Section
NCDWQ NC Division of Water Quality
NFA No Further Action
NORR Notice of Regulatory Requirements
NORP Notice of Residual Petroleum
NOV Notice of Violation
NPDES National Pollutant Discharge
Elimination System
OVM Organic Vapor Meter
PID Photoionization Detector
PLC Programmable Logic Controller
POE Point of Entry (water treatment system)
POTW Publicly Owned Treatment Works
RBCA Risk Based Corrective Action
RDL Reporting Detection Limit
RP Responsible Party
SCFM Standard Cubic Feet per Minute
SVE Soil Vapor Extraction
STF Leaking UST State Trust Fund
STG Soil to Groundwater
TA Task Authorization
TCC Target Cleanup Concentrations
Terraquest Terraquest Environmental Consultants,
P.C.
TPH Total Petroleum Hydrocarbon
UST Underground Storage Tank
VOA Volatile Organic Analysis
VOC Volatile Organic Compound
VPH Volatile Petroleum Hydrocarbons
XP Explosion Proof

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 ii Troutman, Iredell County, North Carolina
EXECUTIVE SUMMARY

On behalf of Madhukunj, LLC, this Groundwater Monitoring Report has been prepared as
requested by the Mooresville Regional Office of the NCDWM-UST. A groundwater sampling
event conducted on January 18, 2023 for the Perth Mini Mart release incident reveals the
continued presence of over four feet of free-phase product, GCL violations, and 2L Standard
violations. The site is ranked a High Risk based on the presence of nineteen sole-source active
water supply wells located within 1,000 feet of the incident.

As the NCDWM-UST has previously approved a Corrective Action Plan Feasibility Study and
Corrective Action Design Report that details a sparge and vent treatment system, Terraquest
recommends the preparation of a Record of Decision to implement active remediation. Semi-
annual groundwater monitoring should continue until the treatment system is activated.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 1 Troutman, Iredell County, North Carolina
1.0 INTRODUCTION

On behalf of Madhukunj, LLC, Terraquest Environmental Consultants, P.C. (Terraquest) this
Groundwater Monitoring Report has been prepared as requested by the Mooresville Regional
Office of the NCDWM-UST for the Perth Mini Mart property located in Troutman, Iredell County,
North Carolina.. Pre-approval of costs was made by the NCDWM-UST on ePATA 40784-017.

The site location is depicted in Figure 1. The site vicinity is depicted in Figure 2. The site layout
and monitoring well network are depicted in Figure 3. Technical methods and standard
procedures generally utilized by Terraquest are detailed in Appendix A.

2.0 UPDATE OF SITE HISTORY AND CHARACTERIZATION

A detailed chronological site history is provided in Appendix B.

2.1 UST Owner:
The USTs are owned by Madhukunj, LLC.

2.2 Tank and Release Information:
According to the NC UST Database Records, two 6,000-gallon gasoline, one 4,000-gallon gasoline,
and one 2,000-gallon diesel USTs were installed at the site on March 4, 1980. Note that the
2,000-gallon diesel UST was converted to non-ethanol gasoline in 2018. A 2,000-gallon diesel
AST is also present onsite. The installation date of that tank is unknown. All USTs were closed
via excavation and removal in February 2019 as previously reported. Following closure, two new
12,000-gallon, gasoline, compartmentalized USTs were installed. A site history of the USTs and
AST on the property is included as Table 1. Previous tank locations are shown on Figure 3.

In 2017, the UST owner noted inventory record discrepancies based upon ATG reading for UST
T3, the 4,000-gallon gasoline tank. In response, the UST owner submitted an UST-17A UST

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 2 Troutman, Iredell County, North Carolina
Suspected Release 24-Hour Notice Form. The date and nature of the release is unknown but
inventory records show a shortage of approximately 300-400 gallons. Based on the lab results
of soil samples from beneath the other two gas USTs in the T3 basin, a release occurred from
those tanks also.

Terraquest is not aware of any AST release incidents.

The site and several properties in the area are commercial in nature with the remaining majority
used as residential as shown here:
SITE

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 3 Troutman, Iredell County, North Carolina
The closest residence is located approximately 330 feet north of the release area. There are no
places of public assembly within 1,500 feet. Land use in the vicinity of the site is highway business
and residential. The site and properties to the east are zoned Highway Business (HB). Most of
the remaining properties are zoned Residential (RS). Zoning classifications of the site and
surrounding properties are depicted on Figure 2 and below as taken from Iredell County’s GIS
online system at https://iredell.connectgis.com.

Initial abatement of the release included the removal of fuel from the T3 UST and placing it in
temporary closure. All tanks were subsequently closed via removal.

Environmental assessment activities were previously detailed in a Site Check Report, LSA Report,
CSA Report, and CAP Feasibility Study sent to the NCDWM-UST.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 4 Troutman, Iredell County, North Carolina
2.3 Receptor Information

As part of the LSA and to determine the risk classification of the site, Terraquest personnel
previously performed a reconnaissance of properties within a 1,500-foot radius of the source
area. The reconnaissance effort consisted of obtaining tax department and local zoning
information on properties and conducting door-to-door visits of certain properties within 1,500
feet of the source area, in addition to collecting other pertinent information from the appropriate
local and state officials.

Terraquest personnel inspected all properties within 1,500 feet of the site and attempted to
contact all the property owners within 1,000 feet in person. Property owners within a 500 -foot
radius were questioned, if available, as to the source of their water and if any water supply wells
were located on their property. If owners/occupants were not home, a survey form was left at
their residence or forwarded to the property owners through the mail. In all cases, Terraquest
also conducted a visual survey of the property. Table 2 lists the names and addresses of
surrounding property owners. Note that the PIN Numbers presented in Table 2 correspond with
those shown in Figure 2.

Terraquest has previously contacted the Town of Troutman’s Public Works Department to inquire
about the Town’s water supply system. Terraquest was put into contact with West Consultants,
PLLC, who maintains and operates the municipal supply system. Todd Poteet of West
Consultants, PLLC, verified water lines are available along Perth Rd. and Autumn Leaf Rd.;
however, not along Weddington Ln. Furthermore, since the subject area is not located within
the jurisdictional boundary of the Town of Troutman, property owners are not required to
connect to the municipal water supply system. Most are not interested in doing so as they would
be annexed into Troutman and its associated taxes.

Through the reconnaissance efforts, a total of thirty-three water supply wells were identified
within 1,500 feet or the source area. Of those identified wells, nineteen are sole source water

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 5 Troutman, Iredell County, North Carolina
supply wells located within 1,000 feet. One additional active water supply well is located on the
site within 250 feet of the source area. That well is used to fill minnow tanks at the store. Water
supply well information is listed in Table 3. Supply well locations are depicted on Figure 2.

As part of the reconnaissance effort, Terraquest also searched for any surface water bodies
within a 500-foot radius of the site. An unnamed tributary of Big Branch originates off the
western property boundary of the site and is located within 500 feet of the source area. The NC
Division of Water Quality (DWQ) classifies Big Branch as a Water Supply-IV “Waters used as
sources of water supply for drinking, culinary, or food processing purposes.” The unnamed
tributary of Big Branch is depicted on Figure 2.

2.4 Regional Geology and Hydrogeology

The site is in the Piedmont Physiographic Region of North Carolina. According to the Geologic
Map of North Carolina (Brown, et al, 1985), the site is in the Charlotte Belt and is underlain by
mafic metavolcanic bedrock lithologies. On a regional scale, the Piedmont is characterized by
land with moderate relief and some areas of low relief hills and valleys.

Groundwater in the region is part of the Catawba River Basin. Regionally, groundwater flows to
the southwest and feeds into Big Branch Creek and ultimately Lake Norman. Big Branch Creek is
listed as a Water Supply IV surface water body at https://deq.nc.gov/about/divisions/water-
resources/planning/classification-standards/classifications#DWRPrimaryClassification which
classifies surface water bodies with a WSIV classification as “sources of water supply for drinking,
culinary, or food processing.”

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 6 Troutman, Iredell County, North Carolina
The site’s location in reference to nearby water bodies as provided by the NCDEQ at
https://ncdenr.maps.arcgis.com/apps/webappviewer/index.html?id=6e125ad7628f494694e25
9c80dd64265 follows:

SITE
SITE

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 7 Troutman, Iredell County, North Carolina
2.5 Site Geology and Hydrogeology

ENCOUNTERED LITHOLOGY
The following lithologies were encountered at the site during the installation of soil borings and
the monitoring well network:

0 – 63’ BGL SILT (CL)
Mostly soft to medium-stiff (generally increasing consolidation with depth),
micaceous, red to brown to tan, with trace clay and characteristics of saprolite in
areas.

63-70’ BGL SAPROLITE
Mostly tan/brown heavily-weathered rock.

The drilling locations of the monitoring wells used to describe the lithology are depicted on Figure
3. Geologic cross sections of the site are based upon the soil boring logs are as follows:

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 8 Troutman, Iredell County, North Carolina

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 9 Troutman, Iredell County, North Carolina

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 10 Troutman, Iredell County, North Carolina
Depth-to-water measurements have been collected from the monitoring wells during various
stages of the assessment to estimate the direction of groundwater flow. Groundwater elevation
measurements were reduced to a common datum by surveying the relative elevation of the top
of the casing for each monitoring well. The water table elevation data as measured on January
18, 2023 was used to create a potentiometric surface map which illustrates the interpreted
direction and gradient of groundwater flow that is generally to the south, southwest. Recent
groundwater elevation data and monitoring well construction information is provided in Table 4.
Historical groundwater elevation data is provided in Appendix C.

The groundwater elevation measurements from April 30, 2019 reveal that the hydraulic head
within the shallow phreatic aquifer ranged from a relative value of 66.61 at monitoring well MW5
to 67.91 at MW4. In conjunction with other site measurements, the results indicate flow in the
phreatic aquifer in a south/southwest direction under an average hydraulic gradient of
approximately 0.02.

Water level data from the Type III monitoring well (MW11) and the interpreted groundwater
elevation in the phreatic aquifer in the vicinity of the Type III well (based on MW5) were used to
determine if a vertical head gradient existed in the phreatic aquifer. The vertical head gradient
was calculated using the following equation and groundwater elevation data collected on April
30, 2019: Vg =�ℎ𝑝𝑝ℎ𝑟𝑟𝑟𝑟𝑟𝑟𝑟𝑟𝑟𝑟𝑟𝑟−ℎ𝑀𝑀𝑀𝑀11�𝐷𝐷

where:

Vg = Vertical head gradient
Hphreatic = Water elevation in the shallow aquifer = 66.61’
HMW= Water elevation in deep well MW11 = 66.85’
D = The difference in elevation between the shallow water table and the
middle of the well screen in MW11 = (66.61 – 29.3) = 37.31’

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 11 Troutman, Iredell County, North Carolina
Vertical head gradient:
𝑉𝑉𝑔𝑔=66.61 −66.8537.31

= -0.0064

The head gradient suggests a value very near zero indicating that it is transition zone between a
recharge and discharge area. This seems reasonable as the site is located near Lake Norman
where local groundwater and surface water are discharging to.

To provide preliminary estimates of hydraulic conductivity (K) and groundwater flow velocity (v)
for the phreatic aquifer, Terraquest personnel performed slug tests on monitoring wells MW3,
MW5, and MW7 on December 3, 2018 as part of the CSA.

The preliminary hydraulic conductivity estimates range from 0.176 to 0.427 feet per day. Using
an average hydraulic conductivity value of 0.336 feet/day, an average groundwater seepage
velocity was determined to be 16.35 feet per year. An effective porosity of 15 percent was
chosen based on published values of effective porosity for silt with the value skewed toward silty
sands based on a silt range of 3-19 percent and a silty sand range of fine to silty sand of 10-28
percent (Sanders, 1998). An average hydraulic gradient as measured on December 3, 2018 across
the site was used.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 12 Troutman, Iredell County, North Carolina
2.6 Local Topography
The local topography is characterized by gently rolling, well rounded hills and long low ridges with
a few hundred feet of elevation difference between the hills and valleys. The majority of the
surrounding 1,000 feet of the site is mapped at approximately 800-900 feet above sea level. Local
topography is depicted in Figure 1.

2.7 Land Cover/Surface Drainage
The release area is currently overlain by asphalt as shown below. The property slopes to the
west, southwest behind the store where there are grass/gravel areas that precipitation can
infiltrate the ground.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 13 Troutman, Iredell County, North Carolina
3.0 SOIL ASSESSMENT AND EXCAVATION

Through the 2017 Site Check, 2018 LSA, the 2019 UST closure, the 2019 over-excavation, and the
CSA, a total of fifty-seven samples were collected to delineate the extent of soil contamination.

The area of STG MSCC violation is generally centered on the UST basin with a smaller area around
the northern dispenser island. The volume of contamination is a sum of these two areas. With
an average depth to water of 31 feet in monitoring wells near the UST basin in April 2019, the
calculated tonnage at the site includes 1,220 tons near the basin and 15 tons at the northern
dispenser area. The area is shown here:

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 14 Troutman, Iredell County, North Carolina
Note that Terraquest had discussions with the NCDWM-UST in 2019 prior to and during the UST
closure regarding further excavation of contaminated soil as it was exposed and readily available
to dig out. Ultimately, the Trust Fund did not authorize additional excavation. The RP chose to
dig out an additional 94.66 tons in the southwest direction from the UST basin as it extended
away in the direction where over six feet of product has been gauged. The limits of excavation
in the sloping direction of product flow were all still above the STG MSCCs including some
material that could have been excavated that was above the Residential MSCCs. Again,
Terraquest’s request to dig this material out was denied.

4.0 FREE PRODUCT ASSESSMENT AND RECOVERY

Discovery
Prior to developing monitoring wells MW2 – MW4 on June 19, 2018, monitoring wells were
visually checked for the presence of free product with a bailer prior to their development. At
that time, free product was observed in monitoring well MW2. Product was subsequently
discovered in monitoring well MW16 on September 23, 2020, monitoring well MW17 on March
22, 2021, and in soil vapor extraction (SVE) well SVE3 on November 22, 2021.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 15 Troutman, Iredell County, North Carolina
Free product pictures

Historic product presence
MW2 10/7/19: MW2 7/24/19: MW2 4/22/19:
MW16 9/23/20
DTW 29.15’
MW16 11/23/21
DTW 34.82’

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 16 Troutman, Iredell County, North Carolina

MW17
1/18/23

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 17 Troutman, Iredell County, North Carolina
SVE3 0.1-foot thickness prior to pilot test start
MW2 7.05 feet in October 2018 prior to MMPE
5.63 feet two months after MMPE in December 2018
4.11 feet in April 2019 before MMPE and following a one-foot water table increase
0.05-foot thickness following the April 2019 MMPE
0.18 feet four days after April 2019 MMPE and rising
4.12-foot product thickness on September 23, 2020
3.08-foot product thickness on March 22, 2021 prior to MMPE
No product on April 21, 2021, a month after MMPE
4.2-foot thickness prior to air sparge pilot test on November 23, 2021
3.69-foot thickness gauged prior to sampling May 9, 2022
4.43-foot thickness gauged prior to sampling January 18, 2023
MW3 0.28-foot thickness gauged prior to sampling May 9, 2022
0.3-foot thickness gauged prior to sampling January 18, 2023
MW15 3-foot thickness prior to air sparge pilot test on November 23, 2021
0.35-foot thickness gauged prior to sampling January 18, 2023
MW16 0.05-foot product thickness on September 23, 2020
2.85-foot product thickness on March 22, 2021 prior to MMPE
1.49-foot product thickness on April 21, 2021, a month after MMPE
4.78-foot thickness gauged prior to sampling January 18, 2023
MW17 0.12-foot product thickness on March 22, 2021
0.05-foot product thickness on April 21, 2021, a month after MMPE
Product detected in well, meter couldn’t collect accurate reading

Historical groundwater elevations and product thicknesses are detailed in Appendix C.

Recovery events
MMPE events have been conducted for this release incident as authorized on ePATAs 40784-002,
-007, and -013. All the events were five days in length. MMPE services were provided by Zava
Industrial, Inc. for the October 2018 event and by EarthX, Inc. for the April 2019 and March 2021
events. The October 2018 event was successful in removing 4,041 gallons of liquid, the April
2019 event recovered 3,461 gallons, and the March 2021 event recovered 4,679 gallons.
Emissions of 56.86 gallons, 64.23 gallons, and 20.72 gallons were reported for the three events,
respectively. Additional MMPE events were denied by the NCDWM-UST.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 18 Troutman, Iredell County, North Carolina
Free product delineation
Following a high-resolution study conducted in June 2020 by Dakota Technologies Company, LLC,
additional monitoring wells MW15, MW16, and MW17 were installed by an NC-licensed driller
on September 22-23, 2020 at previously selected locations validated by the high-res data. Their
locations around MW2 are shown on the enclosed Figure 3. Table 4 shows well construction
details. The screen intervals were extended above the water table on all three wells to capture
the product at shallower depths in accordance with typical well construction policy.

The high-resolution study identified higher concentrations within the analyzed area as follows:

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 19 Troutman, Iredell County, North Carolina
Product locations and water table fluctuations
As apparent from water table fluctuations and data from the high resolution study, several areas
of free product are present vertically at the site. Greater product thicknesses were noted when
the water table is lower. The majority of free-phase product is located 30 to 40 feet BGL.
Supporting information is as follows:

Date
MW2 Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
6/25/2018 6.25 61.95
10/22/2018 7.05 62.60
12/3/2018 5.63 63.68
4/22/2019 4.11 66.83
7/24/2019 2.85 67.06
9/23/2020 4.12 67.11
3/22/2021 3.08 69.56
9/23/2021 4.2 66.08
0
1
2
3
4
5
6
7
8
60.00 62.00 64.00 66.00 68.00 70.00
MW2 Free Product Thickness (feet)

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 20 Troutman, Iredell County, North Carolina
Free product evaluation
On September 23, 2020, Terraquest personnel used a disposable bailer to remove product from
monitoring well MW2 and subsequently record the rate of its return as requested by the
NCDWM-UST. Personnel bailed product from an initial thickness of 4.12 feet at static conditions
to a thickness of 0.25 feet that repeatedly showed up through several bails. As product was
bailed from the well, it was temporarily placed into a 5-gallon bucket at the well. When that
bucket filled, the contents were transferred to a transport can during which time the well would
fill back up with 6-8" of product. Complete removal of the product was not possible. In total,
over six gallons of product were removed through the efforts and later disposed of offsite in an
environmentally-sound manner. In summary, those efforts amount to a six-gallon recovery via
hand bailing in half an hour. Following the half-hour of bailing, the rate of return was recorded
for two hours following the bailing as detailed in tabular and graphical form:

Time
Top of
Casing
Elevation
(feet)
Depth to
Product from
Top of Casing
(feet)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation (feet)Comments
Type II Groundwater Monitoring Well
9:15:00 AM 97.83 28.58 32.70 4.12 68.14
9:45:00 AM 97.83 29.83 30.08 0.25 67.93
9:50:00 AM 97.83 29.69 30.00 0.31 68.06
9:55:00 AM 97.83 29.65 30.00 0.35 68.09
10:00:00 AM 97.83 29.66 30.05 0.39 68.06
10:05:00 AM 97.83 29.63 30.02 0.39 68.09
10:10:00 AM 97.83 29.60 29.97 0.37 68.13
10:15:00 AM 97.83 29.58 29.95 0.37 68.15
10:20:00 AM 97.83 29.55 29.94 0.39 68.17
10:25:00 AM 97.83 29.55 29.94 0.39 68.17
10:30:00 AM 97.83 29.55 29.95 0.40 68.17
10:35:00 AM 97.83 29.55 29.94 0.39 68.17
10:40:00 AM 97.83 29.55 29.95 0.40 68.17
10:45:00 AM 97.83 29.55 29.95 0.40 68.17
10:50:00 AM 97.83 29.55 29.94 0.39 68.17
10:55:00 AM 97.83 29.54 29.95 0.41 68.18
11:00:00 AM 97.83 29.54 29.95 0.41 68.18
11:05:00 AM 97.83 29.53 29.94 0.41 68.19
11:10:00 AM 97.83 29.52 29.94 0.42 68.20
11:15:00 AM 97.83 29.52 29.93 0.41 68.20
11:20:00 AM 97.83 29.51 29.93 0.42 68.21
11:25:00 AM 97.83 29.50 29.92 0.42 68.22
11:30:00 AM 97.83 29.50 29.92 0.42 68.22
11:35:00 AM 97.83 29.50 29.92 0.42 68.22
11:40:00 AM 97.83 29.49 29.92 0.43 68.22
11:45:00 AM 97.83 29.48 29.91 0.43 68.23
11:50:00 AM 97.83 29.48 29.90 0.42 68.24
11:55:00 AM 97.83 29.48 29.90 0.42 68.24
12:00:00 PM 97.83 29.48 29.90 0.42 68.24
Product removed from well with disposable bailer for half an hour. Could not remove product to a thickness less than 3". Removed product was placed into a 5-gallon bucket. When that
bucket was transferred to a transport can, the well would fill back up with 6-8" of product. Complete removal of the product was not possible.
0.23
0.28
0.33
0.38
0.43
0.48
9:45:00 AM9:50:00 AM9:55:00 AM10:00:00 AM10:05:00 AM10:10:00 AM10:15:00 AM10:20:00 AM10:25:00 AM10:30:00 AM10:35:00 AM10:40:00 AM10:45:00 AM10:50:00 AM10:55:00 AM11:00:00 AM11:05:00 AM11:10:00 AM11:15:00 AM11:20:00 AM11:25:00 AM11:30:00 AM11:35:00 AM11:40:00 AM11:45:00 AM11:50:00 AM11:55:00 AM12:00:00 PMFree Product Thickness (feet)
Free Product Thickness (feet)

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 21 Troutman, Iredell County, North Carolina
5.0 GROUNDWATER ASSESSMENT

Monitoring Well Network
Throughout various phases of assessment, a total of seventeen monitoring wells have been
installed to delineate groundwater quality. Those wells include sixteen Type II wells and one
Type III telescoping deep well. The well locations are shown on Figure 3, their construction is
detailed on Table 4.

Groundwater Sampling
The latest groundwater monitoring event was conducted on January 18, 2023 when Terraquest
personnel attempted to sample monitoring wells MW1-17 and water supply wells WSW1, WSW2,
and WSW4. Note that new gravel had been placed over monitoring well MW12, so field
personnel had to return with a metal detector and locate and sample the well on January 20,
2023. Monitoring wells MW2, 3, MW15, MW16, and MW17 contained free product and were
not sampled. Access agreements were sent to all water supply well owners prior to entry onto
their property. The owner at water supply well WSW3 did not allow sampling of that well.

Monitoring and supply wells were sampled by Terraquest field personnel as detailed in Appendix
A. The retrieved samples were placed on ice pending transit to an NC-certified laboratory for
analysis. All wells were sampled for 6200B targeting VOCs found in the subject contaminant,
gasoline.

The analytical results of the sampling events reveal an oval-shaped plume that extends from
beyond monitoring well MW12 to the south, between monitoring wells MW4 and MW7 to the
north, to the west of monitoring well MW10, and to the east of monitoring well MW6 beneath
Perth Road. The 2L Standard violation plume, applicable to this High Risk site, measures 170 feet
long by 110 feet across at the widest point and covers an area of 13,700 square feet and is
approximately the same size and shape as when last sampled in May 2022. The GCL violation

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 22 Troutman, Iredell County, North Carolina
plume covers an area of 4,300 square feet and the extent of product is estimated at 1,000 square
feet. The analytical results are summarized on Table 5 and on Figure 5.

Further details of the results follow:

Free product: MW2 (4.43’), MW3 (0.3’), MW15 (0.35’), MW16 (4.78’), MW17
(MW17: meter had trouble reading thickness. Product presence was
confirmed with bailer.)
>GCL: MW5, MW6
> 2L Standards: MW1, MW4, MW8, MW10-13
<2L Standards: MW7, MW9, MW14

Historical groundwater analytical data is summarized in Appendix C. The full analytical report for
the recent event is provided in Appendix D.

The vertical extent of groundwater contamination was estimated based upon the concentrations
noted in the Type III (MW11) groundwater monitoring well. Petroleum-type compounds were
reported above the 2L Groundwater Standards in the deep well that is screened from 65-70 feet
BGL. The estimated vertical extent of 2L Standard violations in groundwater is approximately 80
feet BGL.

6.0 CONCLUSIONS

A groundwater sampling event conducted on January 18, 2023 for the Perth Mini Mart release
incident reveals the continued presence of over four feet of free-phase product, GCL violations,
and 2L Standard violations. The site is ranked a High Risk based on the presence of nineteen sole-
source active water supply wells located within 1,000 feet of the incident.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 23 Troutman, Iredell County, North Carolina
As the NCDWM-UST has previously approved a Corrective Action Plan Feasibility Study and
Corrective Action Design Report that details a sparge and vent treatment system, Terraquest
recommends the preparation of a Record of Decision to implement active remediation. Semi-
annual groundwater monitoring should continue until the treatment system is activated.

7.0 LIMITATIONS

This report is limited to the investigation of dissolved petroleum hydrocarbons, such as gasoline,
in groundwater and does not imply that other unforeseen adverse impacts to the environment
are not present at or around the Perth Mini Mart property located in Troutman, Iredell County,
North Carolina. In addition, subsurface heterogeneities not identified during this study may
influence the migration of groundwater or contaminants in unpredicted ways. The limited
amount of sampling and testing conducted during this study cannot practically reveal all
subsurface heterogeneities. Furthermore, the subsurface conditions, particularly groundwater
flow, elevations, and water quality may very through time. The opinions and conclusions arrived
at in this report are in accordance with North Carolina Department of Environmental Quality
regulations and guidelines and industry-accepted geologic and hydrogeologic practices at this
time and location. No warranty is implied or intended.

Groundwater Monitoring Report (1/18/23 event) Madhukunj, LLC
Terraquest Environmental Consultants, P.C. #40784 Perth Mini Mart
Prepared: 2/7/23 24 Troutman, Iredell County, North Carolina
REFERENCES

Brown, et al., 1985. Geologic Map of North Carolina, North Carolina. Department of Natural
Resources and Community Development, 1:500,000 scale.

Sanders, Laura L. 1998. A Manual of Field Hydrogeology. Upper Saddle River, New Jersey: Prentice
Hall Inc.: 196.

TABLES

Table 1
Date: 1/23/23 Facility ID No: 0-0024524
Capacity
UST Product (Gallons)Release Discovered
T1 Gasoline 6,000 3/4/80 2/25/19 Yes
T2 Gasoline 6,000 3/4/80 2/25/19 Yes
T3 Gasoline 4,000 3/4/80 2/25/19 Yes
T4 Non-ethanol gasoline*2,000 3/4/80 2/19/19 No
AST1 Diesel 2,000 unknown Active No
T5**Gasoline 12,000 2/27/19 Active No
T6**Gasoline 12,000 2/27/19 Active No
Notes:
1. Information obtained from the North Carolina UST Database Records and field observations.
2. * Tank T4 held diesel fuel until its conversion to non-ethanol gasoline in 2018.
3. ** Tanks are compartmentalized.
4. Tanks T1-T4 were of single-walled steel construction. T5 and T6 are double-walled fiberglass.
Active USTs/AST
SITE HISTORY (UST/AST SYSTEM INFORMATION)
Incident Name: Perth Mini Mart Incident No. 40784
Date Installed Date Closed
Closed USTs
Table 2
Date: 1/23/23 Facility ID: 0-0024524
Tax Parcel Number
(PIN Number)Property Owner Property Owner Address Property Address
Pennell, Gary & Sherry PO Box 712 131 Weddington LaneTroutman, NC 28166 Troutman, NC 28166
Tsitouris, Steve & Michael 569 Autumn Leaf Road 569 Autumn Leaf Road
Troutman, NC 28166 Troutman, NC 28166
Geiger, Lee and Katie 782 Perth Road 782 Perth Road
Troutman, NC 28166 Troutman, NC 28166
TCJ Development, LLC PO Box 3395 803 Perth Road
Mooresville, NC 28117 Troutman, NC 28166
Thompson, Wayne PO Box 886 858 Perth Road
Troutman, NC 28166 Troutman, NC 28166
Madhukunj, LLC 135 Corona Circle 818 Perth Road
Mooresville, NC 28115 Troutman, NC 28166
Notes:
1. Information gathered from field interviews and Iredell County Geographic Information System.
2. Last 4 digits of MAP ID numbers correspond with those displayed on Figure 2.
SURROUNDING PROPERTY OWNERS
Incident Name: Perth Mini Mart Incident No.: 40784
SITE
4730-63-9494
4730-69-9930
4730-79-2085
4730-79-2769
4730-79-4509
4731-50-7091
Table 3
Date: 1/23/23 Facility ID: 0-0024524
Well Depth Type Casing Depth Screen Interval Distance from SourceWell ID No. Well Owner/Address Well Address Well Use (feet BGS)of Well (feet BGS)(feet BGS)Area of Release (feet)Madhukunj, LLC
WSW1 135 Corona Circle 818 Perth Road Active 170 Drilled 95 95-170 107
Mooresville, NC 28115 Troutman, NC 28166 (minnow tank in store)
Tsitouris, Steve & Michael
WSW2 569 Autumn Leaf Road 569 Autumn Leaf Road Secondary Source uknown Drilled uknown uknown 447
Troutman, NC 28166 Troutman, NC 28166
TCJ Development
WSW3 PO Box 3395 562 Autumn Leaf Road Inactive uknown Drilled uknown uknown 464Mooresville, NC 28117 Troutman, NC 28166Pennell, Gary & Sherry
WSW4 PO Box 712 117 Weddington Lane Sole Source unknown Drilled uknown uknown 384
Troutman, NC 28166 Troutman, NC 28166
Upright, Renny & Debbie
WSW5 547 Autumn Leaf Road 547 Autumn Leaf Road Sole Source uknown Drilled uknown uknown 614
Troutman, NC 28166 Troutman, NC 28166
TCJ DevelopmentWSW6PO Box 3395 795 Perth Road Sole Source uknown Drilled uknown uknown 541Mooresville, NC 28117 Troutman, NC 28166
Grant, Nancy & Jeffrey
WSW7 782 Perth Road 782 Perth Road Sole Source uknown Drilled uknown uknown 582
Troutman, NC 28166 Troutman, NC 28166
Pennell, Gary & Sherry
WSW8 PO Box 712 131 Weddington Lane Sole Source 90 Drilled unknown unknown 534
Troutman, NC 28166 Troutman, NC 28166Thompson, K. WayneWSW9PO Box 886 858 Perth Road Sole Source 300 Drilled unknown unknown 679
Troutman, NC 28166 Troutman, NC 28166
Thompson, Tommy
WSW10 855 Perth Road 105 Spicewood Circle Sole Source unknown Drilled unknown unknown 595
Troutman, NC 28166 Troutman, NC 28166
Geiger, Lee
WSW11 533 Autumn Leaf Road 533 Autumn Leaf Road Sole Source unknown Drilled unknown unknown 923Troutman, NC 28166 Troutman, NC 28166TCJ DevelopmentWSW12PO Box 3395 532 Autumn Leaf Road Sole Source unknown Drilled unknown unknown 1000
Mooresville, NC 28117 Troutman, NC 28166
Brown, Gertrude P Heirs
WSW13 9117 J Ruth Street 785 Perth Road Sole Source unknown Drilled unknown unknown 1148
Mount Pleasant, NC 28124 Troutman, NC 28166
Weber, Glenn & Rozelle
WSW14 765 Perth Road 765 Perth Road Sole Source unknown Drilled unknown unknown 1267Troutman, NC 28166 Troutman, NC 28166Weber, Glenn & Rozelle
WSW15 765 Perth Road 765 Perth Road Inactive unknown Bored unknown unknown 1192
Troutman, NC 28166 Troutman, NC 28166
Cowan, Hugh
WSW16 755 Perth Road 755 Perth Road Sole Source unknown Drilled unknown unknown 1322
Troutman, NC 28166 Troutman, NC 28166 2-inch
Cowan, HughWSW17755 Perth Road 755 Perth Road Inactive unknown Bored unknown unknown 1313Troutman, NC 28166 Troutman, NC 28166
Weber, Glenn & Rozelle
WSW18 765 Perth Road 106 Weddington Lane Inactive unknown Drilled unknown unknown 1098
Troutman, NC 28166 Troutman, NC 28166 2-inch
Wagner, Betty etal
WSW19 2795 Westonridge Dr.129 Weddington Lane Sole Source unknown Drilled unknown unknown 659
Cincinnati, OH 45239 Troutman, NC 28166Wagner, Betty & MichaelWSW20PO Box 464 120 Weddington Lane Sole Source unknown Drilled unknown unknown 916Troutman, NC 28166 Troutman, NC 28166
Guentner, Gregory & Julie
WSW21 397 Isle of Pines Road 146 Weddington Lane Sole Source unknown Drilled unknown unknown 833
Mooresville, NC 28115 Troutman, NC 28166 2-inch
Coffey, Robert & Rebecca
WSW22 PO Box 1094 165 Weddington Lane Sole Source unknown Drilled unknown unknown 826
Troutman, NC 28166 Troutman, NC 28166American IRA, LLCWSW23242 Templeton Road 104 Spicewood Circle Sole Source unknown Drilled unknown unknown 814
Mooresville, NC 28117 Troutman, NC 28166
Haynes, Larry
WSW24 118 Spicewood Circle 118 Spicewood Circle Sole Source unknown Drilled unknown unknown 893
Troutman, NC 28166 Troutman, NC 28166
Neel, Henry
WSW25 PO Box 245 123 Spicewood Circle Sole Source unknown Drilled unknown unknown 731Troutman, NC 28166 Troutman, NC 28166Sherrill, Shirley
WSW26 PO Box 73 129 Spicewood Circle Sole Source unknown Drilled unknown unknown 780
Troutman, NC 28166 Troutman, NC 28166
Phelps, Gary
WSW27 147 Spicewood Circle 147 Spicewood Circle Sole Source unknown Drilled unknown unknown 830
Troutman, NC 28166 Troutman, NC 28166
Shoemaker, Nancy
WSW28 151 Spicewood Circle 151 Spicewood Circle Sole Source unknown Drilled unknown unknown 880Troutman, NC 28166 Troutman, NC 28166Davis, Shelly
WSW29 153 Spicewood Circle 153 Spicewood Circle Sole Source unknown Drilled unknown unknown 1,131
Troutman, NC 28166 Troutman, NC 28166
Gilleland, Marilyn
WSW30 294 Spicewood Circle 294 Spicewood Circle Sole Source unknown Drilled unknown unknown 1,019
Troutman, NC 28166 Troutman, NC 28166
Sparrow, WarnerWSW31104 Nutmeg Lane 104 Nutmeg Lane Sole Source unknown Drilled unknown unknown 1,088Troutman, NC 28166 Troutman, NC 28166
Wilcox, Robert
WSW32 138 Spicewood Circle 138 Spicewood Circle Sole Source unknown Drilled unknown unknown 1,050
Troutman, NC 28166 Troutman, NC 28166
Wittie, Richard
WSW33 171 Spicewood Circle 171 Spicewood Circle Sole Source unknown Drilled unknown unknown 1,475
Troutman, NC 28166 Troutman, NC 28166Notes:1. "BGS" = feet below ground surface, .
2. Information obtained from Terraquest field interviews & Iredell County GIS
3. Well ID numbers are displayed on Figure 2.
WATER SUPPLY WELL INFORMATION
Incident Name: Perth Mini Mart Incident No.: 40784
Table 4
Date: 1/23/23 Facility ID: 0-0024524
Well ID Date Installed
Date Water
Level
Measured
Screened Interval (x
to y feet BGS)
Bottom of Well
(feet BGS)
Top of
Casing
Elevation
(feet)
Depth to Water
from Top of
Casing (feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation (feet)CommentsMW11/16/18 1/18/23 30-50 50 98.78 32.76 0 66.02 Type II Groundwater Monitoring WellMW26/18/18 1/18/23 30-50 50 97.83 35.63 4.43 65.44 Type II Groundwater Monitoring Well
MW3 6/18/18 1/18/23 30-50 50 98.54 33.1 0.3 65.66 Type II Groundwater Monitoring Well
MW4 6/19/18 1/18/23 30-50 50 99.68 33.13 0 66.55 Type II Groundwater Monitoring WellMW511/26/18 1/18/23 30-50 50 96.31 31.25 0 65.06 Type II Groundwater Monitoring WellMW611/26/18 1/18/23 30-50 50 97.53 32.44 0 65.09 Type II Groundwater Monitoring Well
MW7 11/26/18 1/18/23 30-50 50 99.37 33.05 0 66.32 Type II Groundwater Monitoring Well
MW8 11/27/18 1/18/23 30-50 50 98.72 33.27 0 65.45 Type II Groundwater Monitoring WellMW911/27/18 1/18/23 30-40 40 89.72 23.96 0 65.76 Type II Groundwater Monitoring WellMW1011/28/18 1/18/23 30-40 40 90.75 25.30 0 65.45 Type II Groundwater Monitoring Well
MW11 11/28/18 1/18/23 OC: 55 IC: 65 65-70 70 96.80 31.96 0 64.84 Type III vertical delineation well
MW12 4/29/19 1/20/23 25-40 40 94.74 29.57 0 65.17 Type II Groundwater Monitoring WellMW134/29/19 1/18/23 25-40 40 94.30 29.34 0 64.96 Type II Groundwater Monitoring WellMW144/30/19 1/18/23 25-40 40 96.30 31.29 0 65.01 Type II Groundwater Monitoring Well
MW15 9/22/20 1/18/23 25-45 45 97.25 32.00 0.35 65.51 Type II Groundwater Monitoring Well
MW16 9/22/20 1/18/23 25-45 45 97.38 35.55 4.78 65.32 Type II Groundwater Monitoring WellMW179/22/20 1/18/23 20-45 45 98.41 32.67 yes*#VALUE!Type II Groundwater Monitoring WellAS111/16/21 -55-60 60 98.06 ---1"-diameter air sparge well
SVE1 11/16/21 -20-35 35 98.34 ---2"-diameter SVE well
SVE2 11/16/21 -20-35 35 97.96 ---2"-diameter SVE wellSVE311/16/21 -20-35 35 97.99 ---2"-diameter SVE wellNotes:
1. "BGS" = below ground surface
2. "-" information not available
3. The groundwater elevations for monitoring wells with free product was corrected as follows: [Top of Casing Elevation - Depth to Water] + [Free Product Thickness x 0.7305]4. Note that data from monitoring wells MW9 and MW10 was collected on June 1, 2022 as vehicles were parked over those wells on May 9, 2022. 5. Meter had trouble reading thickness of free product but its presence was confirmed with a bailer.
25205520
20
20
3030
25
252525
30
30
303030
30
MONITORING WELL CONSTRUCTION INFORMATIONIncident Name: Peth Mini Mart Incident No.: 40784
Well Casing Depth (feet
BGS)3030
Table 5Date: 2/7/23
6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200BWell ID
Date
CollectedMW11/18/23 728 1,170 71.6 1,040 < 2.20 7.22 112 < 1.90 32.1 < 26.0 < 5.00 < 1.50 < 10.0 < 2.40 < 240 37.4 < 30.0 < 7.60 < 6.90MW21/18/23MW31/18/23MW41/18/23 1,920 1,620 430 2,330 < 2.20 14.3 217 < 1.90 87.1 32.6 < 5.00 < 1.50 < 10.0 < 2.40 < 240 42.1 < 30.0 7.85 47.9
MW5 1/18/23 6,610 28,200 1,810 11,700 250 82.3 642 < 38.0 210 < 520 < 100 < 30.0 < 200 < 48.0 < 4800 < 106 < 600 < 152 < 138MW61/18/23 9,050 14,100 1,370 7,170 58.8 72.3 842 < 19.0 341 < 260 < 50.0 < 15.0 < 100 < 24.0 < 2400 < 53.0 < 300 < 76.0 106MW71/18/23 0.407 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 < 0.190 < 0.560 < 2.60 < 0.500 < 0.150 < 1.00 < 0.240 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690MW81/18/23 44.7 < 0.410 < 0.500 4.26 < 0.220 0.766 < 0.820 < 0.190 0.699 < 2.60 < 0.500 < 0.150 < 1.00 < 0.240 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690MW91/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 < 0.190 < 0.560 < 2.60 < 0.500 < 0.150 < 1.00 < 0.240 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690
MW10 1/18/23 1.34 < 0.410 < 0.500 1.7 < 0.220 < 0.200 < 0.820 < 0.190 < 0.560 < 2.60 < 0.500 < 0.150 < 1.00 < 0.240 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690MW111/18/23 251 < 0.820 < 1.00 19.4 0.818 2.39 5.34 < 0.380 < 1.12 < 5.20 < 1.00 0.402 < 2.00 < 0.480 < 48.0 10 < 6.00 < 1.52 < 1.38MW121/20/23 313 < 2.05 6.8 29.2 4.37 1.43 5.85 < 0.950 < 2.80 < 13.0 < 2.50 < 0.750 < 5.00 < 1.20 < 120 < 2.65 < 15.0 < 3.80 < 3.45MW131/18/23 504 5.29 5.17 151 9.01 5.94 18.8 < 0.950 11 < 13.0 < 2.50 < 0.750 < 5.00 < 1.20 < 120 22.8 < 15.0 < 3.80 < 3.45MW141/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 0.313 < 0.560 < 2.60 < 0.500 < 0.150 < 1.00 < 0.240 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690
MW15 1/18/23MW161/18/23MW171/18/23WSW11/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 < 0.190 < 0.560 < 2.60 3.47 < 0.150 14.4 0.438 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690WSW21/18/23 < 0.130 < 0.410 < 0.500 < 1.60 0.231 < 0.200 < 0.820 < 0.190 < 0.560 < 2.60 < 0.500 < 0.150 < 1.00 < 0.240 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690
WSW4 1/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 < 0.190 < 0.560 < 2.60 < 0.500 < 0.150 < 1.00 < 0.240 < 24.0 < 0.530 < 3.00 < 0.760 < 0.690160060050020704000.4 400 4,000 0.6 50 70 0.4 4,000 70 6 70 705,000 260,000 84,500 85,500 20,000 70,000 28,500 400 25,000 4,000,000 600 50,000 70,000 400 4,000,000 25,000 6,000 6,900 30,000Notes:1. All results in µg/L.
2. Bold denotes a compound detection 3. Shading denotes a 2L Standard violation of a petroleum-type compound. 4. < - denotes less than sample detection limit5. Italics indicates a GCL violation
0.35 feet of free product4.78 feet of free product
4.43 feet of free product0.3 feet of free product
2L StandardGCL
Free product gauged in well - meter would not produce accurate reading n-ButylbenzeneDibromochloromethaneChlorobenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneBromodichloromethane1,2-DichloroethaneIsopropylbenzeneNaphthalenen-Propylbenzene2-Butanone (MEK)ChloroformEthanolSUMMARY OF GROUNDWATER SAMPLING RESULTSIncident Name: Perth Mini Mart Incident No.: 40784 Facility ID: 0-0024524
Analytical MethodContaminant of Concern
BenzeneTolueneEthylbenzeneTotal XylenesMTBEIPE

FIGURES

ONSULTANTS, P.C.CENVIRONMENTAL
ENVIRONMENTAL CONSULTANTS, P.C.
ENVIRONMENTAL CONSULTANTS, P.C.
ENVIRONMENTAL CONSULTANTS, P.C.

APPENDIX A

Page 1 of 8 
 TECHNICAL METHODS/STANDARD PROCEDURES 

Equipment Decontamination 

All soil sampling equipment utilized during site assessment activities is decontaminated according 
to standard and accepted protocol.  Cleaning solutions range from clean potable water to acidic 
solutions or organic solvents depending on the contaminants present at the site.  Equipment 
utilized at sites, such as hand augers, contaminated with petroleum hydrocarbons, is generally 
decontaminated with a low‐sudsing detergent such as Luiquinox® and triple rinsed with distilled 
water.  Larger equipment, such as drill rigs and associated tools, is steam cleaned.  All 
decontamination procedures are completed within an established decontamination area which is 
located away from the active study area.  Frequency of equipment decontamination depends on 
the nature of work being performed, but in no case is decontamination performed less frequently 
than once per test (i.e., soil boring, well installation, sample collection, etc.).  Equipment blanks are 
collected as a quality control measure when required by job specifications. 

Soil Boring Installation 

Soil borings are completed using hand‐operated sampling tools, truck‐mounted drills, or 
Geoprobe® drilling rigs depending on the depth of sample collection and other site‐specific 
conditions.  Hand operated stainless‐steel bucket augers are utilized to collect soil samples at 
regular intervals to determine site stratigraphy and to test for the presence of volatile organic 
compounds.  Samples retrieved from the hand auger are necessarily disturbed during the augering 
process, but can provide accurate information on soil type and contaminant concentrations when 
properly interpreted.  Soil samples from hand augered borings are generally retrieved at one to 
two foot intervals. 

Truck‐mounted or Geoprobe® drilling equipment is often utilized when sample retrieval depths 
exceed twenty feet or subsurface conditions prevent utilization of hand augers (i.e., buried rocks, 
wood, bricks or other materials occur in the subsurface).  Truck‐mounted drilling rigs usually 
retrieve soil via a hollow‐stem auger/split spoon collection method.  Geoprobe® rigs usually employ 
a Macro‐Core® tube retrieval system.   

Hollow stem augers provide relatively undisturbed 2‐foot cores of soil samples.  Soil samples are 
generally collected at five foot intervals utilizing standard penetration test procedures as defined 
by the American Society for Testing and Materials (ASTM) or are pushed to the desired depth using 
the head of the drill rig.  The standard penetration test involves driving a 2" outside diameter by 1‐
3/8" inside diameter split‐spoon sampler a minimum distance of one foot with a 340‐lb. slide 
hammer falling a distance of 30 inches.   

A Geoprobe® rig is a hydraulically‐powered soil probing machine.  The probe utilizes static force 
and percussion to advance a small diameter sampling device into the subsurface.  The sampling 
apparatus provides relatively undisturbed 5‐foot cores of soil samples.  Soil samples are collected 
Page 2 of 8 
continuously.  The Macro‐Core® tube contains an inserted poly‐vinyl chloride (PVC) liner which 
retains the soil sample as the tube is driven into the ground.  The Macro‐Core® tube is 
decontaminated between each 5‐foot sample interval in a soil boring using a Liquinox and tap‐
water mixture.  A new PVC liner is used to collect soil from each sample interval in a soil boring.    

Soil samples retrieved from the hollow‐stem augers or Geoprobe are then carefully described 
according to the Unified Soil Classification System.  Soil descriptions are recorded on a soil 
boring log. 

Soil Sampling 

Soils to be analyzed by a North Carolina‐certified laboratory are prepared according to the specified 
analytical method.  Initially, soil samples are removed from the ground using either a hand auger, 
backhoe bucket, spilt spoon auger, or a Macro‐Core® sampling tube.  During the removal, care is 
taken to keep the disturbance of the soil structure to a minimum to reduce the loss of 
contaminants.  Once removed, the samples are placed in the proper sample container for the 
specified analytical method.  For samples collected for the MADEP VPH and EPA Method 8260, a 
TerraCore® sampler is used to collect one 5‐gram allotment of soil.  The allotment is placed in 
methanol‐preserved 40 mL vials.  Also, one 5‐gram allotment of soil is placed into sodium bisulfate‐
preserved 40 mL vials (one 5‐gram allotment per vial, 2 vials per sample) for the 8260 low 
concentration method.  A 250‐mL glass jar of the sampled soil is also collected to provide moisture 
content information.  Soils sampled for MADEP EPH, EPA Method 8270 and TPH 5030 and 3550 are 
placed in a 250‐mL glass jar (for MADEP EPH analysis an amber jar is required).  TPH 5030 samples 
are preserved in methanol similar to the 8260 analysis.  Field personnel wear new, disposable 
nitrile gloves during the collection of each sample.  

The soil samples are labeled with the sample location, sample identification, date and time of 
collection, and the analytical method.  The samples are placed on ice, sent to a laboratory, and 
analyzed before the expiration of an analytical method’s prescribed holding time.  Chain‐of‐custody 
documentation is maintained for each sample collected in the field. 

If the soil is being sampled for volatile or semi‐volatile compounds, a portion of the collected soil is 
placed in a sealable bag and screened for volatile organic vapors.  Head screening procedures are 
described in the following paragraph.  

Headspace Screening 

Collected soil samples are routinely tested for the presence of volatile organic compounds (VOCs).  
After retrieval from the ground, a portion of a soil sample is placed in a sealable plastic bag.  The 
soil samples are then set aside for approximately five minutes so that volatile constituents present 
in the sample can reach equilibrium concentrations with headspace gases in the bag.  Once a 
suitable time period has passed, the probe of the sampling instrument, typically an Organic Vapor 
Monitor (OVM) or a Photo Ionization Detector (PID), is inserted into the bag and the relative 
concentration of total VOCs is measured and permanently recorded in a field note book.  VOC 
Page 3 of 8 
concentrations are measured using either a Thermo Electron Corp. Innova Series catalytic OVM or 
an Ion Science PhoCheck PID.  Both the OVM and PID instrumentation are periodically calibrated 
according to the manufacturer’s recommended procedures. 

The OVM and PID are qualitative tools employed to detect and estimate the concentration of 
organic or hydrocarbon vapors.  A thin probe is inserted through a small break in the seal of a 
bagged soil sample.  For the OVM, an air sample from the headspace of the bag is drawn through 
the probe into an internal chamber where the vapors are catalyzed.  The concentration of the VOCs 
is registered on a digital scale in parts per million (ppm).  For the PID, an air sample from the 
headspace of the bag is drawn across the face of a lamp causing the sample to emit photons, the 
presence of which are converted into a VOC ppm reading that is displayed.  Oxygen levels are field 
calibrated prior to each use.  VOC calibration occurs periodically depending upon use by using a 
span gas of known concentration in a process recommended by the manufacturer.   

Well Installation/Construction 

Monitoring wells are installed using hand‐operated sampling tools, a truck‐mounted drill rig, or a 
Geoprobe drilling rig depending on the depth of well and other site‐specific conditions. All 
monitoring wells are installed according to the requirements of 15A NCAC 2C‐Well Construction 
Standards.  Specifically, individual monitoring wells are constructed of 2‐inch diameter, schedule 40 
PVC casing riser and screen.  The screen interval is generally 10 to 15 feet of machine slotted PVC 
with a slot size of 0.010".  Only flush threaded joints are used.  The annulus space around the 
screen is filled with washed filter pack No. 2 sand.  The filter pack extends one to two feet above 
the top of the screen.  A one to two foot‐thick bentonite pellet seal is then placed above the filter 
pack.  The remainder of the well annulus is completely filled with a Portland (Type I/II) cement 
grout mixture.  A protective outer steel manhole, locking cap, and concrete pad is installed for each 
well. 

Type II Monitoring Well Construction  

Single‐cased monitoring wells are generally used in delineation of groundwater quality within the 
surficial aquifer.  The wells are constructed of 2‐inch diameter, schedule 40 PVC casing and screen.  
The screen interval is generally 10 to 15 feet of machine slotted PVC with a slot size of 0.010".  Only 
flush threaded joints are used.  The annulus space around the screen is filled with washed filter 
pack No. 2 sand.  The filter pack extends one to two feet above the top of the screen.  A one to two 
foot‐thick bentonite pellet seal is then placed above the filter pack.  The remainder of the well 
annulus is completely filled with a Portland (Type I/II) cement grout mixture.  A protective outer 
steel manhole, locking cap, and concrete pad are installed for each well. 

Type III Monitoring Well Construction 

Double‐cased monitoring wells are used in the delineation of groundwater quality within a deeper 
portion of the surficial aquifer or an additional aquifer (e.g. aquitard, bedrock).  A four to six‐inch 
outer casing is installed through the surficial aquifer until a sufficient depth or until the deeper 
Page 4 of 8 
aquifer is encountered.  The casing is secured with a Portland‐grout collar that is tremmied into the 
annular spaced from the bottom of the bore hole to the surface.  Once the grout has sufficiently 
cured, the bore hole is continued through the bottom of the outer casing to a depth approximately 
15 ‐ 20 feet beneath the outer casing.  The inner casing is constructed of 2‐inch diameter, schedule 
40 PVC casing riser and screen.  The screen interval is generally 5 to 10 feet of machine slotted PVC 
with a slot size of 0.010".  Only flush threaded joints are used.  The annulus space around the 
screen is filled with washed filter pack No. 2 sand.  The filter pack extends one to two feet above 
the top of the screen.  A one to two foot‐thick bentonite pellet seal is then placed above the filter 
pack.  The remainder of the well annulus is completely filled with the same Portland grout mixture 
used in the outer casing.  A protective outer steel manhole, locking cap, and concrete pad are 
installed for each well. 

Well Development 

Following installation of each well, surging and pumping or bailing techniques will be used to 
remove fines from the screened interval.  Groundwater is removed from each well until clear water 
is retrieved or a noticeable reduction in the amount of silt is achieved.  Purged groundwater is 
disposed of in an environmentally safe manner. 

Groundwater Sampling 

Petroleum Sites 

Groundwater samples are collected from temporary or permanent monitoring wells according to 
established sampling protocol.  When multiple monitoring wells or sampling points are sampled, 
sampling is completed beginning with the least contaminated well to the most contaminated well, 
if it is known.  When permanent monitoring wells for petroleum sites are sampled, the well is 
purged of a minimum of three well‐bore volumes prior to sample collection in order to assure that 
sampled water is representative of aquifer conditions.  In temporary wells, the first water which 
migrates into the open borehole is sampled.  Samples from both temporary and permanent 
monitoring wells are collected using individually wrapped disposable polyethylene bailers by field 
personnel wearing disposable nitrile gloves.  Only one well is sampled with a given bailer in order to 
prevent sample cross‐contamination.  During both well purging and sampling, proper protective 
clothing and equipment is used and is dependent upon the type and level of contaminants present. 
Also, field personnel change gloves between different samples to reduce the chance of cross‐
contamination. Water samples are transferred from the bailer to laboratory‐prepared sampling 
containers using slow emptying devices to reduce the chance of contamination loss through 
volatilization.  Preservatives, such as acids, are provided by the laboratory in pre‐prepared 
containers in which collected samples are placed if in‐field preservation is necessary.  The samples 
are labeled with the project name, project number, sample identification, required analysis, and 
date and time of collection.  The samples are placed on ice, shipped to a certified laboratory, and 
analyzed before the expiration of an analytical method’s prescribed holding time.  Chain‐of‐custody 
documentation is maintained for each sample collected in the field.   

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Other Groundwater Sampling Protocols 

When required by state or federal regulations, low‐flow groundwater sampling procedures are 
instituted.  Groundwater samples collected in low‐flow situations are collected using a peristaltic 
pump. A peristaltic pump is a type of positive displacement pump. The fluid is contained within a 
flexible tube fitted inside a circular pump casing.  A rotor with a number of rollers attached to the 
external circumference compresses the flexible tube. As the rotor turns, the part of tube under 
compression closes thus forcing the fluid to be pumped to move through the tube.  Groundwater 
parameters such as water level drawdown, pH, conductivity, dissolved oxygen (DO) and turbidity. 
Pumping rate, drawdown, and the time or volume required to obtain stabilization of parameter 
readings can be used as a future guide to purge the well. Measurements are collected at a pre‐
pumping established interval (typically five to ten minutes). Once all or a majority of the 
parameters have stabilized for three successive readings, stabilization has been achieved. In lieu of 
measuring all five parameters, a minimum subset would include pH, conductivity, and turbidity or 
DO. Three successive readings should be within ± 0.1 for pH, ± 3% for conductivity, and ± 10% for 
turbidity and DO.  

Upon parameter stabilization, sampling is initiated. Sampling flow rate is maintained at the estab‐
lished purge rate or is adjusted slightly to minimize aeration, bubble formation, turbulent filling of 
sample bottles, or loss of volatiles due to extended residence time in tubing. The same device used 
for purging is used to collect the groundwater sample. Generally, volatile parameters are sampled 
first. The sequence in which samples for inorganic parameters are collected is not determined 
unless filtered (dissolved) samples are collected. Preservatives, such as acids, are provided by the 
laboratory in pre‐prepared containers in which collected samples are placed if in‐field preservation 
is necessary.  The samples are labeled with the project name, project number, sample 
identification, required analysis, and date and time of collection.  The samples are placed on ice, 
shipped to a certified laboratory, and analyzed before the expiration of an analytical method’s 
prescribed holding time.  Chain‐of‐custody documentation is maintained for each sample collected 
in the field.   

During both well purging and sampling, proper protective clothing and equipment is used and is 
dependent upon the type and level of contaminants present.   Also, field personnel change gloves 
between different monitoring wells or sampling points to reduce the chance of cross‐
contamination.  When multiple monitoring wells or sampling points are sampled, sampling is 
completed beginning with the least contaminated well to the most contaminated well, if it is 
known. 

Stockpile Sampling 

The number of composite samples collected from a stockpile or a total quantity of excavated soil is 
based upon the cubic yardage.  One composite sample is collected for every 100 cubic yards of 
contaminated soil excavated.  The volume of a stockpile or total quantity of excavated soil is 
calculated by approximating the general geometry of a stockpile or estimating the capacity of the 
Page 6 of 8 
dump trucks used for hauling.  If a stockpile is sampled, a grid pattern is laid out on the stockpile, 
dividing the stockpile into segments of approximately 200 cubic yards.  Two soil borings are 
advanced within a grid and three soil samples are collected from each soil boring at various depths. 
 The six soil samples are mixed into a composite sample by a trained TerraQuest technician.  If truck 
loads are sampled, an aliquot sample is collected from the hauling trucks at a frequency based 
upon the capacity of the hauling trucks.   

Aliquots are gently mixed into a composite sample by a trained TerraQuest technician. Every effort 
is made to minimize the loss of contaminants through volatilization.  The composited soil samples 
are jarred in the appropriate laboratory‐prepared containers, labeled with the sample location, 
sample identification, date of collection, time of collection, the analytical method, and the 
preservative.  The samples are placed on ice, shipped to a laboratory, and analyzed before the 
expiration of an analytical method’s prescribed holding time.  Chain‐of‐custody documentation is 
maintained for each sample collected in the field. 

Surface Water Sampling 

Surface water samples, specifically samples from creeks or streams, are collected from a 
moving/flowing portion of the creek or stream to ensure that stagnant water is not collected.  Field 
personnel are careful to collect samples from flowing areas that are not so turbulent as to cause a 
loss of volatile contaminants which might have been contained in the creek’s/stream’s water.  
Samples are collected by field personnel wearing disposable nitrile gloves.  Field personnel change 
gloves between different locations to reduce the chance of cross‐contamination.  Samples are 
collected directly from the appropriate creek or stream location and placed into the appropriate 
laboratory‐prepared containers.  Preservatives, such as acids, are provided by the laboratory in pre‐
prepared containers in which collected samples are placed if in‐field preservation is necessary. The 
samples are labeled with the project name, project number, sample identification, required 
analysis, and date and time of collection.  The samples are cooled on ice to approximately four 
degrees centigrade, shipped to a certified laboratory, and analyzed before the expiration of an 
analytical method’s prescribed holding time.  Chain‐of‐custody documentation is maintained for 
each sample collected in the field.    

Potable Well Sampling 

Groundwater samples from potable wells are collected from sampling points, typically spigots, 
located in the closest proximity to the potable well pump house as possible.  Prior to sample 
collection, the water is run for a sufficient amount of time to purge the bladder tank and assure 
that sampled water is representative of aquifer conditions.  Once purged, the flow rate is reduced 
and samples are placed in the appropriate laboratory prepared containers with the appropriate 
acid preservatives added if preservation of the sample is necessary.  The samples are labeled with 
the project name, project number, sample identification, required analysis, and date and time of 
collection.  The samples are placed on ice, shipped to a laboratory, and analyzed before the 
expiration of an analytical method’s prescribed holding time.  Chain‐of‐custody documentation is 
maintained for each sample collected in the field.  
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Public Water Supply Line Sampling 

Groundwater samples from public water supply lines are collected from sampling points, typically 
spigots.  To sample the spigot, the flow rate is reduced and samples are placed in the appropriate 
laboratory prepared containers.  The samples are labeled with the sample location, sample 
identification, date of collection, time of collection, and required analytical method.  The samples 
are placed on ice, shipped to a laboratory, and analyzed before the expiration of an analytical 
method’s prescribed holding time.  Chain‐of‐custody documentation is maintained for each sample 
collected in the field.  

Air Sampling 

Air samples are collected with the aide of a manually operated MityVac® pump manufactured by 
Pristech, Inc.  The air sampling process begins by connecting a length of rubber hose from the 
MityVac® pump to the port to be sampled, or by hanging the hose inside of an emissions stack in 
such a manner as to ensure no outside air causes dilution.  Another length of hose is fixed to the 
outlet port of the pump and is connected to a new Tedlar bag.  Once the pump is hooked up, a 
valve on the Tedlar collection bag is opened and air is manually forced into the bag by the pumping 
action of sampling personnel.   

Field Measurements 

Field measurements taken to determine the pH, conductivity, temperature, and dissolved oxygen 
concentration of a particular groundwater sample are taken directly after a particular monitoring 
well has been adequately purged.  This ensures that the groundwater parameter data collected is 
representative of the aquifer conditions at a given location.  Once purging of the monitoring well is 
complete, the decontaminated probe head and cord of the appropriate unit is lowered into the 
required monitoring well.  If the depth to water in a specific monitoring well is greater than the 
length of cord for a particular unit, a new, disposable bailer is slowly lowered into the appropriate 
monitoring well and a representative groundwater sample is retrieved.  A slow pouring device is 
fitted onto the end of the disposable bailer and the sample is slowly poured into a new, disposable 
plastic cup.  Groundwater parameter data are then collected from the groundwater in the cup 
using the required unit.   

For pH, conductivity, and temperature, a Hanna Instruments Model 991300 portable meter is 
utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s operations 
manual by field personnel.  Prior to data collection, the unit is properly decontaminated to prevent 
cross‐contamination.  The unit is decontaminated between each sample.  The procedure used for 
sample measurement involves lowering the meter’s probe into the new, disposable cup containing 
the groundwater sample to be measured and slowly stirring the probe to force groundwater across 
the probe’s membrane.  The measurements displayed by the meter are then recorded.   

For dissolved oxygen concentration measurements, a YSI® Model 55 Handheld Dissolved Oxygen 
System is utilized.  This unit is periodically calibrated and maintained in accordance with the unit’s 
Page 8 of 8 
operations manual by field personnel.  Prior to data collection, the unit is properly decontaminated 
to prevent cross‐contamination.  The unit is decontaminated between each sample.  The procedure 
used for sample measurement involves adjusting the unit for the correct altitude where the 
sampling will take place and adjusting the reported units desired.  Once this is done, the unit’s 
probe is inserted into the groundwater sample to be measured and the probe is slowly stirred to 
force the groundwater across the probe’s membrane.  The measurements displayed by the unit are 
then recorded.   

For turbidity measurements, a Hach 2100P Portable Turbidity meter or equal equivalent is utilized.  
The unit is calibrated prior to use in accordance with the unit’s operations manual by field 
personnel.  Groundwater samples are collected in glass containers for measurement by the 
instrument.  The glass containers are washed with bottled‐water between each measurement 
collection.  Once the sample is collected and inserted into the instrument, the measurements 
displayed by the instrument are then recorded.   

APPENDIX B

Perth Mini Mart (#40784)
Chronological Site History
Terraquest Environmental Consultants, P.C.
Page 1 of 4

CHRONOLOGICAL SITE HISTORY

Perth Mini Mart
818 Perth Road, Troutman, NC
Facility ID#: 00-0-0000024524
NCDWM UST Incident No.: 40784
Terraquest Project No.: 08217

March 4, 1980 According to the North Carolina UST Database Records, two 6,000-
gallon gasoline, one 4,000-gallon gasoline, and one 2,000-gallon diesel
USTs were installed at the site.

November 16, 2017 Terraquest personnel mobilized to the Perth Mini Mart facility to
conduct a limited scope site check. The UST owner had recently noted
inventory record discrepancies based upon ATG reading for UST T3. To
investigate these irregularities, the UST owner had a tank tightness test
completed on this UST which resulted in failure. In response, the UST
owner submitted an UST-17A UST Suspected Release 24-Hour Notice
Form. A site check was then required to investigate a potential release
of petroleum.

Soil quality was assessed through the advancement of four soil borings
(B1 – B4) around the suspect UST. Samples from the B1(18-20), B2(8-
10), B3(8-10), and B4(13-15) were submitted for laboratory analysis
per EPA Method 8015 utilizing the 5030-extraction method for
gasoline range organics (GRO). Analytical results of the collected soil
samples revealed detectable concentrations of TPH GRO in each
sample; however, only the B1(18-20) sample contained a TPH GRO
concentration (497 ug/kg) above the 100 mg/kg action limit.

December 8, 2017 Terraquest submitted a copy of the Site Check Report Letter and UST-
61 24 Hour Release Reporting Form were submitted to the NCDWM-
UST. Three soil samples were collected from the MW1 soil boring at
the 10-12 ft. BGL, 20-22 ft. BGL, and 30-32 ft. BGL intervals.

December 19, 2017 The NCDWM-UST issued an NORR that confirmed receipt of the Site
Check Report and requested the completion of an LSA.

January 16, 2018 Terraquest personnel supervised the installation of one Type II
groundwater monitoring well (MW1) as part of a Phase I LSA in the
vicinity of the previous B1 soil boring.

Perth Mini Mart (#40784)
Chronological Site History
Terraquest Environmental Consultants, P.C.
Page 2 of 4
January 22, 2018 Terraquest personnel collected a groundwater sample from
monitoring well MW1 after gauging the well for free product using an
oil/water interface probe that did not detect any measurable amount
of free product. Prior to groundwater sample collection, Terraquest
gauged 6.25 feet of free product in monitoring well MW2. No
additional wells contained free product on this date. Groundwater
samples were collected from monitoring wells MW3 and MW4.

March 19, 2018 The NCDWM-UST LUST Trust Fund issued a correspondence regarding
the Commercial State Trust Fund Eligibility Application. The release
incident was found conditionally eligible following a $20,000
deductible that was noted as having been met.

June 18-19, 2018 Terraquest personnel supervised the installation of three additional
monitoring wells (MW2 – MW4) as part of the Phase II LSA.

August 3, 2018 Terraquest submitted an LSA Report (Phase I & II) to the NCDWM-UST.

August 6, 2018 Terraquest requested pre-approval of costs necessary to complete a
CSA.

September 6, 2018 Terraquest requested pre-approval of costs necessary to conduct free
product recovery via MMPE.

September 11, 2018 The NCDWM-UST grants pre-approval of costs for free product
recovery via MMPE.

October 3, 2018 The NCWM-UST grants pre-approval of costs for CSA activities.

October 22-26, 2018 Terraquest supervised an MMPE event at the site. A total of 4, 041
gallons of a free product/contaminated groundwater mixture were
recovered. Emissions stack calculations indicate the exhaust of 56.86
gallons of petroleum.

November 26-28, 2018 Terraquest personnel supervised the installation of groundwater
monitoring wells MW5-MW11. These wells were installed as part of
the CSA. Monitoring wells MW5-MW10 are Type II wells installed for
horizontal assessment while monitoring well MW11 is a Type III well
installed for vertical delineation of contamination. Soil borings

December 3, 2018 As part of the CSA, Terraquest personnel sampled monitoring wells
MW1 – MW11 and surveyed the casing elevations of recently installed

Perth Mini Mart (#40784)
Chronological Site History
Terraquest Environmental Consultants, P.C.
Page 3 of 4
wells MW5-MW11. Slug tests were conducted on monitoring wells
MW3, MW5, and MW7.

April 22-26, 2019 Terraquest supervised an MMPE event at the site. Free product was
removed from monitoring well MW2. A total of 3,461 gallons of
contaminated groundwater was removed. Emissions stack
calculations indicate the exhaust of 64.23 gallons of petroleum.

October 7-11, 2019 Terraquest supervised an MMPE event at the site. Free product was
removed from monitoring well MW2. A total of 3,027 gallons of
contaminated groundwater was removed. Emissions stack
calculations indicate the exhaust of 20.57 gallons of petroleum.

June 1, 2, and 3, 2020 Terraquest supervised a high-resolution study conducted by Dakota
Technologies Company, LLC. The study was requested by the NCDWM-
UST to identify the location of free product and involved the advancement
of ten borings that were analyzed using an Ultra-Violet Optical Screening
Tool (UVOST).

September 22-23, 2020 Terraquest supervised the installation of three free product monitoring
wells, MW15, MW16, and MW17. A free product evaluation was
performed on monitoring well MW2. Groundwater monitoring wells
without free product were sampled and sent off for VOC analysis.
While there were no indications of a release from the diesel AST, STF
demanded that 625 analysis be performed on all wells at the site at a
cost exceeding $3,000 to rule out a release.

March 22-26, 2021 Terraquest supervised an MMPE event at the site. Free product was
removed from monitoring wells MW2, MW16, and MW17. A total of
4,679 gallons of contaminated groundwater was removed. Emissions
stack calculations indicate the exhaust of 20.72 gallons of petroleum.

April 21, 2021 Terraquest personnel gauged monitoring wells and found free product
in MW16 (1.49’) and MW17 (0.05’).

November 16-17, 2021 Terraquest supervised the installation of pilot test wells SVE1, SVE2,
SVE3, and AS1.

November 22-23, 2021 Terraquest conducted SVE and air sparge pilot tests.

January 17, 2022 Terraquest submitted a Corrective Action Plan Feasibility Study to the
NCDWM-UST.

Perth Mini Mart (#40784)
Chronological Site History
Terraquest Environmental Consultants, P.C.
Page 4 of 4
February 23, 2022 The NCDWM-UST approved the CAP Feasibility Study.

May 9 & June 1, 2022 Terraquest sampled groundwater monitoring wells associated with the
release incident to provide updated information for the CAP Design
Report.

August 23, 2022 Terraquest submitted a Corrective Action Design Report to the
NCDWM-UST.

November 1, 2022 The NCDWM-UST issued an NORR requesting the completion of a
groundwater sampling event.

December 5, 2022 Terraquest requested an extension of the December 31, 2022 deadline
for the submittal of a monitoring report.

December 7, 2022 The NCDWM-UST granted an extension to the submittal deadline for
the Monitoring Report. The new submittal deadline is February 23,
2023.

January 18, 2023 Terraquest sampled all of monitoring wells MW1-17 that did not
contain free product. Free product thickness was recorded where
encountered. Monitoring well MW12 was covered in new gravel and
could not be located. Water supply wells WSW1, WSW2, and WSW4
were also sampled. The property owner for water supply well WSW3
did not grant permission to sample their well.

January 20, 2023 Terraquest returned to site and located monitoring well MW12 using a
metal detector. The well was purged and sampled.

APPENDIX C

Well ID
Top of
Casing
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)MW1 98.78 38.60 0 60.18 36.43 0 62.35 35.74 0 63.04 34.59 0 64.19 31.50 0 67.28 31.25 0 67.53MW297.83 ---40.45 6.25 61.95 40.38 7.05 62.60 38.26 5.63 63.68 34.00 4.11 66.83 30.90 0.18 67.06
MW3 98.54 ---36.28 0 62.26 35.59 0 62.95 34.62 0 63.92 31.47 0 67.07 31.30 0 67.24MW499.68 ---37.02 0 62.66 36.3 0 63.38 35.11 0 64.57 ---31.77 0 67.91MW596.31 ---------32.95 0 63.36 ---29.70 0 66.61MW697.53 ---------34.23 0 63.30 ---29.89 0 67.64MW799.37 ---------35.00 0 64.37 ---31.52 0 67.85
MW8 98.72 ---------35.19 0 63.53 ---31.79 0 66.93MW989.72 ---------25.64 0 64.08 ---22.42 0 67.30MW1090.75 ---------26.95 0 63.80 ---23.80 0 66.95MW1196.80 ---------33.22 0 63.58 ---29.95 0 66.85MW1294.74 ---------------25.37 0 69.37
MW13 94.30 ---------------22.95 0 71.35MW1496.30 ---------------29.89 0 66.41Average shallow DTW:38.60 36.58 35.88 32.70 31.49 28.47
Well ID
Top of Casing Elevation (feet)
Depth to Water from Top of Casing (feet)
Free Product Thickness (feet)
Groundwater Elevation (feet)
Depth to Water from Top of Casing (feet)
Free Product Thickness (feet)
Groundwater Elevation (feet)
Depth to Water from Top of Casing (feet)
Free Product Thickness (feet)
Groundwater Elevation (feet)
Depth to Water from Top of Casing (feet)
Free Product Thickness (feet)
Groundwater Elevation (feet)
Depth to Water from Top of Casing (feet)
Free Product Thickness (feet)
Groundwater Elevation (feet)
Depth to Water from Top of Casing (feet)
Free Product Thickness (feet)
Groundwater Elevation (feet)MW1 98.78 ---30.20 -68.58 ---------32.13 0 66.65MW297.83 32.8 2.85 67.11 32.70 4.12 68.14 30.12 3.08 69.96 28.80 0 69.03 27.45 0 70.38 34.82 4.2 66.08MW398.54 ---29.73 -68.81 ------------
MW4 99.68 ---30.50 -69.18 ------------MW5 96.31 ---28.08 -68.23 ------------MW6 97.53 ---29.05 -68.48 ------------MW7 99.37 ---29.93 -69.44 ------------MW8 98.72 ---29.82 -68.9 ------------
MW9 89.72 ---21.45 -68.27 ------------MW10 90.75 ---22.76 -67.99 ------------MW11 96.80 ---28.96 -67.84 ------------MW12 94.74 ---26.73 -68.01 ------------MW13 94.30 ---26.57 -67.73 ------------
MW14 96.30 ---27.84 -68.46 ------------MW15 97.25 ---29.07 -68.18 27.3 0 69.95 27.59 0 69.66 27.00 0 70.25 34.05 3 65.39MW1697.38 ---29.15 0.05 68.26 29.58 2.85 69.881925 27.74 0 69.64 28.22 1.49 70.248445 34.82 4.82 66.08MW1798.41 ---30.05 -68.36 29.25 0.12 69.24766 28.59 0.1 69.89305 27.92 0.05 70.526525 32.05 0.05 66.40AS198.06 ---------------31.72 0 66.34
Average shallow DTW:27.98 29.06 28.18 27.65 33.27
Well ID
Top of
Casing
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
Depth to
Water
from Top
of Casing
(feet)
Free
Product
Thickness
(feet)
Groundwater
Elevation
(feet)
MW1 98.78 32.35 0 66.43 32.76 0 66.02MW297.83 34.63 3.69 65.90 35.63 4.43 65.44MW398.54 32.45 0.28 66.29 33.10 0.3 65.66MW499.68 32.76 0 66.92 33.13 0 66.55MW596.31 30.55 0 65.76 31.25 0 65.06
MW6 97.53 31.64 0 65.89 32.44 0 65.09MW799.37 32.39 0 66.98 33.05 0 66.32MW898.72 32.44 0 66.28 33.27 0 65.45MW989.72 23.85 0 65.87 23.96 0 65.76MW1090.75 25.17 0 65.58 25.3 0 65.45
MW11 96.80 29.15 0 67.65 31.96 0 64.84MW1294.74 29.24 0 65.50 29.57 0 65.17MW1394.30 28.85 0 65.45 29.34 0 64.96MW1496.30 30.40 0 65.90 31.29 0 65.01MW1597.25 31.30 0 65.95 32 0.35 65.505675
MW16 97.38 31.14 0.8 66.82 35.55 4.78 65.32179MW1798.41 32.25 0 66.16 32.67 0 65.74SVE198.34 32.07 0.00 66.27 ---Average shallow DTW:30.79 31.52Notes:
1. "BGS" = below ground surface
9/23/2021
4/30/2019
HISTORICAL GROUNDWATER ELEVATION DATAIncident Name: Peth Mini Mart Incident No.: 407841/22/2018 6/25/2018 12/3/201810/22/2018 4/22/2019
7/24/2019 9/23/2020 3/22/2021 3/26/2021 4/21/2021
5/9/2022 1/18/2023
Page 1 of 2
6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B/6256200B6200BWell ID Date Collected
MW1 1/22/18 484 2,500 476 2,890 <4.22 17.5 222 <4.50 <82 <<<<<<<2.22 65.8 <<<<<<<<<75.0 62 <2.35 <32.8
12/3/18 2,400 11,700 1,280 8,550 53.7 31.2 624 < 0.180 <156 < 0.0670 < 56.0 2.47 61.6 2.64 49.2 1.86 < 70.4 10.9 < 0.124 << 0.160 < 0.180 << 0.0600 3.34 < 3.00 124 32.2 <94.4
9/23/20 1,900 7,610 978 5,090 76.8 70 649 <<110 << 25.8 << 54.3 < 8.73 < 55.3 < 8.39 886 <<<< 9.54 << 9.31 << 8.40 28,400 153 66/77.7 <88.8
5/9/22 380 309 78 273 < 0.220 2.68 37 < 0.230 <9.38 < 0.640 < 2.60 < 0.570 < 1.40 < 0.560 < 1.80 < 0.710 < 10.0 < 0.540 < 0.210 << 1.00 < 0.240 < 0.850 0.795 0.917 < 24.0 32.3 < 3.00 <8.23
1/18/23 728 1,170 71.6 1,040 < 2.20 7.22 112 << 1.90 32.1 << 26.0 <<<<<<<< 5.00 < 1.50 < 10.0 < 2.40 <<<< 240 37.4 < 30.0 < 7.60 < 6.90
MW2 6/25/18
10/22/18
vac on MW2 10/22-26/18
10/26/18
12/3/184/22/19vac on MW2 4/22-26/194/26/19
4/30/19
vac on MW2 10/7-11/19
9/23/20
vac on MW2 3/22-26/21
5/9/22
1/18/23
MW3 6/25/18 2,920 7,210 718 3,630 <33.8 <18.4 316 <36.0 <114 <<56.0 <<<<<17.8 258 <<<<<<<<<600 <19.6 <18.8 <<13.0
12/3/18 1,850 5,510 542 2,919 35.9 15.1 283 < 0.180 <92 < 0.0670 < 28.0 < 0.0880 46.8 1.94 42.1 1.87 44.9 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 2.51 < 3.00 29.5 16.3 <59.5
9/23/20 5,560 20,700 2060 11,060 78 64 1,220 <<338 <261 <194 < 17.5 < 111 < 16.8 1,460 <<<< 19.1 << 18.6 << 16.8 < 8,310 85 154/121 <180
5/9/22
1/18/23
MW4 6/25/18 2,510 8,180 1,460 7,550 <16.9 <9.2 667 <18.0 <222 <646 <<<<< 8.9 423 <<<<<<<<<300 71 <9.4 <12212/3/18 3,290 19,900 1,920 10,510 18.5 32.6 852 < 0.180 <260 1.67 < 56.0 < 0.0880 79.2 12.1 61.7 3.05 < 70.4 < 0.132 < 0.124 <8.06 < 0.180 << 0.0600 5.99 < 3.00 < 19.6 9.24 <162
9/23/20 1,190 3,880 552 3,139 < 3.95 8.6 407 <<132 <110 << 43.5 22.4 < 44.2 < 6.71 1,060 <<<16.4 << 7.45 << 6.72 < 3,320 51 11/6.32 <77.2
5/9/22 384 479 92.6 441 < 0.440 0.882 55.7 < 0.460 <22.1 < 1.28 29 < 1.14 < 2.80 < 1.12 < 3.60 < 1.42 85.8 < 1.08 < 1.00 <2.69 < 0.480 < 1.70 < 1.52 < 1.40 < 48.0 11 < 6.00 <15.2
1/18/23 1,920 1,620 430 2,330 < 2.20 14.3 217 << 1.90 87.1 <32.6 <<<<<<<< 5.00 < 1.50 < 10.0 < 2.40 <<<< 240 42.1 < 30.0 7.85 47.9MW512/3/18 1,920 403 93 1,170 171 3.42 170 < 0.180 <84.7 < 0.0670 < 0.280 < 0.0880 23.7 < 0.0900 25.3 2.05 72.6 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 3.15 < 3.00 30.8 18.1 <35.39/23/20 8,220 8,880 931 4,390 41.8 29.5 503 <<153 << 25.8 <135 < 8.73 119 < 8.39 944 <<<< 9.54 << 9.31 << 8.40 < 4.150 29.8 39.8/32.4 <76.85/9/22 5,290 20,800 1,700 10,500 199 39 935 < 23.0 <254 < 64.0 474 < 57.0 < 140 < 56.0 < 180 < 71.0 < 1,000 < 54.0 < 50.0 << 100 < 24.0 < 85.0 < 76.0 < 70.0 < 2,400 68.5 < 300 <1131/18/23 6,610 28,200 1,810 11,700 250 82.3 642 << 38.0 210 << 520 <<<<<<<< 100 < 30.0 < 200 < 48.0 <<<< 4800 < 106 < 600 < 152 < 138MW612/3/18 1,070 824 205 1,069 6.34 3.5 140 < 0.180 <27.6 < 0.0670 < 0.280 < 0.0880 10.2 < 0.0900 6.74 1.03 < 0.352 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 < 0.0920 < 3.00 9.02 52.8 <19.69/23/20 2,780 8,340 1,750 9,810 82.2 16.6 1,740 <<532 <178 <163 < 6.98 95 < 6.71 1,170 <<<< 7.63 << 7.45 <9 < 3,320 112 350/199 <2785/9/22 5,440 5,810 580 2,590 41.6 32.4 285 < 11.5 <121 < 32.0 < 130 < 28.5 < 70.0 < 28.0 < 90.0 < 35.5 < 500 < 27.0 < 25.0 << 50.0 < 12.0 < 42.5 < 38.0 < 35.0 < 1,200 < 26.5 < 150 <37.51/18/23 9,050 14,100 1,370 7,170 58.8 72.3 842 << 19.0 341 << 260 <<<<<<<< 50.0 < 15.0 < 100 < 24.0 <<<< 2400 < 53.0 < 300 < 76.0 106MW712/3/18 28.2 42.7 12.3 55.4 < 0.169 < 0.0920 3.35 < 0.180 <3.91 < 0.0670 14.2 < 0.0880 11.5 < 0.0900 11.5 < 0.0890 6.96 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 < 0.0920 < 3.00 0.93 < 0.0940 <1.099/23/20 297 156 61.2 542.1 < 0.198 0.93 43.2 <<22.1 <38.6 <16.1 < 0.349 56.4 0.37 < 4.53 <<<0.54 << 0.372 <0.83 < 166 11.7 < 0.256/< 0.542 <12.45/9/22 1.87 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 < 0.230 << 0.560 < 0.640 < 2.60 < 0.570 < 1.40 < 0.560 < 1.80 < 0.710 < 10.0 < 0.540 < 0.500 << 1.00 < 0.240 < 0.850 < 0.760 < 0.700 < 24.0 < 0.530 < 3.00 << 0.690
1/18/23 0.407 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 << 0.190 < 0.560 << 2.60 <<<<<<<< 0.500 < 0.150 < 1.00 < 0.240 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.690
MW8 12/3/18 202 88 45.8 206.3 < 0.169 0.97 24.2 < 0.180 <6.87 < 0.0670 < 0.280 < 0.0880 5.74 < 0.0900 3.79 < 0.0890 < 0.352 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 < 0.0920 < 3.00 1.74 < 0.0940 <4.73
9/23/20 407 61.6 73.8 423 5.04 11.2 123 <<61.2 <20.5 <31.3 < 0.698 19.5 < 0.671 90.1 <<<1.46 << 0.745 <0.8 < 332 6.4 418/2.39 <11.9
5/9/22 2 < 0.500 < 0.500 2.02 0.887 1.68 < 0.820 < 0.230 <3.09 < 0.640 < 2.60 < 0.570 < 1.40 < 0.560 < 1.80 < 0.710 < 10.0 < 0.540 < 0.500 << 1.00 < 0.240 < 0.850 < 0.760 < 0.700 < 24.0 < 0.530 < 3.00 << 0.690
1/18/23 44.7 < 0.410 < 0.500 4.26 < 0.220 0.766 < 0.820 << 0.190 0.699 << 2.60 <<<<<<<< 0.500 < 0.150 < 1.00 < 0.240 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.690
MW9 12/3/18 < 0.119 5.84 0.79 3.75 < 0.169 < 0.0920 < 0.103 < 0.180 << 0.0870 < 0.0670 < 0.280 < 0.0880 < 0.320 < 0.0900 < 0.253 < 0.0890 < 0.352 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 < 0.0920 < 3.00 < 0.0980 < 0.0940 << 0.0650
9/23/20 < 0.388 < 0.366 < 0.355 < 0.359 < 0.198 < 0.359 0.34 <<< 0.352 << 1.03 << 2.17 < 0.349 < 2.21 < 0.336 < 4.53 <<<< 0.382 <1.77 << 0.336 < 166 < 0.363 < 0.256/< 0.542 << 0.307
6/1/22 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 <<< 0.560 << 2.60 << 1.40 < 0.560 < 1.80 < 0.710 < 10.0 <<<< 1.00 <<<< 0.700 < 24.0 < 0.530 < 3.00 << 0.690
1/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 << 0.190 < 0.560 << 2.60 <<<<<<<< 0.500 < 0.150 < 1.00 < 0.240 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.690
MW10 12/3/18 < 0.119 2.46 0.75 3.51 < 0.169 < 0.0920 0.63 < 0.180 << 0.0870 < 0.0670 < 0.280 < 0.0880 < 0.320 < 0.0900 < 0.253 < 0.0890 < 0.352 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 < 0.0920 < 3.00 < 0.0980 < 0.0940 << 0.0650
9/23/20 35.4 0.38 9.65 69 < 0.198 < 0.359 8.76 <<2.52 << 1.03 << 2.17 < 0.349 9.92 < 0.336 < 4.53 <<<0.78 <0.86 << 0.336 < 166 3.96 < 0.256/< 0.542 <1.55
6/1/22 17.1 < 0.410 1.73 23.1 < 0.220 0.419 2.7 <<0.561 << 2.60 << 1.40 < 0.560 < 1.80 < 0.710 < 10.0 <<<< 1.00 <<<< 0.700 < 24.0 2.02 < 3.00 << 0.6901/18/23 1.34 < 0.410 < 0.500 1.7 < 0.220 < 0.200 < 0.820 << 0.190 < 0.560 << 2.60 <<<<<<<< 0.500 < 0.150 < 1.00 < 0.240 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.6901,2,4-Trimethylbenzene1,2-Dibromoethane (EDB)1,2-DichloroethaneIsopropylbenzeneFree Product (6.25')Free Product (7.05')MMPE EVENT
NO PRODUCT
Free Product (5.63')
Free Product (4.11')
MMPE EVENT
Free Product (0.05')
Free Product (0.18')
Free Product (4.12')
MMPE EVENT
Free Product (3.69')Free Product (4.43')
MMPE EVENT
Free Product (0.28')
Free Product (0.3')2-HexanoneNaphthalenen-Butylbenzenen-PropylbenzeneEthanol4-Chlorotoluene4-Methyl-2-pentanone (MIBK)4-IsopropyltolueneAcetoneBromobenzeneBromodichloromethaneDibromochloromethanen-ButylbenzeneSec-ButylbenzeneChlorobenzeneChloroformAnalytical Method
Incident Name: Perth Mini Mart Incident No.: 40784HISTORICAL SUMMARY OF GROUNDWATER SAMPLING RESULTS
Contaminant of Concern
DichlorofluoromethaneMTBEIPEBenzeneTolueneEthylbenzeneTotal Xylenes1,3,5-Trimethylbenzene1,4-Dichlorobenzene2-Butanone (MEK)2-Chlorotoluene
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6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B6200B/6256200B6200BWell ID Date Collected 1,2,4-Trimethylbenzene1,2-Dibromoethane (EDB)1,2-DichloroethaneIsopropylbenzene2-HexanoneNaphthalenen-Butylbenzenen-PropylbenzeneEthanol4-Chlorotoluene4-Methyl-2-pentanone (MIBK)4-IsopropyltolueneAcetoneBromobenzeneBromodichloromethaneDibromochloromethanen-ButylbenzeneSec-ButylbenzeneChlorobenzeneChloroformAnalytical Method
Incident Name: Perth Mini Mart Incident No.: 40784HISTORICAL SUMMARY OF GROUNDWATER SAMPLING RESULTS
Contaminant of Concern
DichlorofluoromethaneMTBEIPEBenzeneTolueneEthylbenzeneTotal Xylenes1,3,5-Trimethylbenzene1,4-Dichlorobenzene2-Butanone (MEK)2-ChlorotolueneMW11 12/3/18 1.73 3.22 0.61 3.19 < 0.169 < 0.0920 0.54 < 0.180 << 0.0870 < 0.0670 7.4 < 0.0880 < 0.320 < 0.0900 < 0.253 < 0.0890 27.8 < 0.132 3.02 <13.4 1.27 << 0.0600 < 0.0920 < 3.00 < 0.0980 < 0.0940 << 0.0650
9/23/20 10.9 < 0.366 < 0.355 28.89 < 0.198 < 0.359 3.88 <<< 0.352 << 1.03 << 2.17 < 0.349 < 2.21 < 0.336 < 4.53 <<<< 0.382 << 0.372 << 0.336 < 166 2.74 0.29/< 0.542 << 0.307
5/9/22 80.8 0.862 < 0.500 15.7 < 0.220 1.15 5.07 < 0.230 <1.01 < 0.640 < 2.60 < 0.570 < 1.40 < 0.560 < 1.80 < 0.710 < 10.0 < 0.540 < 0.500 << 1.00 < 0.240 < 0.850 < 0.760 < 0.700 < 24.0 4.51 < 3.00 << 0.690
1/18/23 251 < 0.820 < 1.00 19.4 0.818 2.39 5.34 << 0.380 < 1.12 << 5.20 <<<<<<<< 1.00 0.402 < 2.00 < 0.480 <<<< 48.0 10 < 6.00 < 1.52 < 1.38MW124/30/19 < 0.119 < 0.0570 < 0.0920 < 0.122 3.48 < 0.0920 < 0.103 < 0.180 << 0.0870 < 0.0670 < 0.280 < 0.0880 < 0.320 < 0.0900 < 0.253 < 0.0890 < 0.352 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 < 0.0920 < 3.00 < 0.0980 < 0.0940 << 0.06509/23/20 63.1 < 0.366 7.19 14.3 6.48 0.36 3.28 <<< 0.352 << 1.03 << 2.17 < 0.349 < 2.21 < 0.336 < 4.53 <<<< 0.382 << 0.372 << 0.336 < 166 0.37 0.27/ < 0.542 <0.61
5/9/22 369 1.54 < 0.500 71.9 6.03 1.1 12.7 < 0.230 << 0.560 < 0.640 < 2.60 < 0.570 < 1.40 < 0.560 < 1.80 < 0.710 < 10.0 < 0.540 < 0.500 << 1.00 < 0.240 < 0.850 < 0.760 < 0.700 < 24.0 1.52 < 3.00 <2.59
1/20/23 313 < 2.05 6.8 29.2 4.37 1.43 5.85 << 0.950 < 2.80 << 13.0 <<<<<<<< 2.50 < 0.750 < 5.00 < 1.20 <<<< 120 < 2.65 < 15.0 < 3.80 < 3.45
MW13 4/30/19 273 1.67 3.31 173.8 7.12 10.8 34.2 < 0.180 <2.42 < 0.0670 < 0.280 < 0.0880 < 0.320 < 0.0900 < 0.253 0.53 < 0.352 < 0.132 < 0.124 << 0.160 < 0.180 <1.9 0.65 < 3.00 11.3 6.57 <2.06
9/23/20 1.49 < 0.366 < 0.355 2.58 < 0.198 < 0.359 0.69 <<< 0.352 << 1.03 << 2.17 < 0.349 < 2.21 < 0.336 < 4.53 <<<< 0.382 << 0.372 << 0.336 < 166 < 0.363 < 0.256/< 0.542 << 0.307
5/9/22 427 8.67 11.3 247 9.72 4.28 31.9 < 0.460 <10.1 < 1.28 < 5.20 < 1.14 < 2.80 < 1.12 < 3.60 < 1.42 < 20.0 < 1.08 < 1.00 << 2.00 < 0.480 < 1.70 < 1.52 < 1.40 < 48.0 18 14.4 <61.1
1/18/23 504 5.29 5.17 151 9.01 5.94 18.8 << 0.950 11 << 13.0 <<<<<<<< 2.50 < 0.750 < 5.00 < 1.20 <<<< 120 22.8 < 15.0 < 3.80 < 3.45MW144/30/19 < 0.119 < 0.0570 < 0.0920 < 0.122 < 0.169 < 0.0920 < 0.103 < 0.180 << 0.0870 < 0.0670 < 0.280 < 0.0880 < 0.320 < 0.0900 < 0.253 < 0.0890 < 0.352 < 0.132 < 0.124 << 0.160 < 0.180 << 0.0600 < 0.0920 < 3.00 < 0.0980 < 0.0940 << 0.0650
9/23/20 < 0.388 < 0.366 < 0.355 < 0.359 < 0.198 < 0.359 < 0.335 <<< 0.352 << 1.03 << 2.17 < 0.349 < 2.21 < 0.336 < 4.53 <<<< 0.382 << 0.372 << 0.336 < 166 < 0.363 < 0.256/< 0.542 << 0.307
5/9/22 0.794 0.414 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 < 0.230 << 0.560 < 0.640 < 2.60 < 0.570 < 1.40 < 0.560 < 1.80 < 0.710 < 10.0 < 0.540 < 0.500 << 1.00 < 0.240 < 0.850 < 0.760 < 0.700 < 24.0 < 0.530 < 3.00 << 0.690
1/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 <0.313 < 0.560 << 2.60 <<<<<<<< 0.500 < 0.150 < 1.00 < 0.240 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.690MW159/23/20 5,870 51,300 5,850 33,400 106 120 3,980 <<872 << 206 << 435 < 76.3 < 442 < 6.71 2,390 <<<< 76.3 << 74.5 << 67.2 < 33,200 598 490/335 <5745/9/22 4,180 44,000 2,470 14,800 91.7 108 1,000 < 23.0 <227 < 64.0 288 < 57.0 < 140 < 56.0 < 180 < 71.0 < 1,000 < 54.0 < 50.0 << 100 < 24.0 < 85.0 < 76.0 < 70.0 23,200 145 < 300 <1191/18/23MW169/23/20
vac on MW16 3/22-26/21
5/9/22
1/18/23MW179/23/20 5,540 41,700 4,190 24,380 504 300 2,770 <597 <1,000 << 109 < 17.5 < 111 < 16.8 1,860 <<<< 19.1 << 18.6 << 16.8 34,200 469 357/246 377
vac on MW17 3/22-26/215/9/22 6,920 49,400 3,480 20,900 352 216 1,360 < 46.0 312 < 128 761 < 114 < 280 < 112 < 360 < 142 < 2,000 < 108 < 100 << 200 < 48.0 < 170 < 152 < 140 80,300 220 < 600 175
1/18/23
WSW1 1/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 << 0.190 < 0.560 << 2.60 <<<<<<<3.47 < 0.150 14.4 0.438 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.690
WSW2 1/18/23 < 0.130 < 0.410 < 0.500 < 1.60 0.231 < 0.200 < 0.820 << 0.190 < 0.560 << 2.60 <<<<<<<< 0.500 < 0.150 < 1.00 < 0.240 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.690
WSW4 1/18/23 < 0.130 < 0.410 < 0.500 < 1.60 < 0.220 < 0.200 < 0.820 << 0.190 < 0.560 << 2.60 <<<<<<<< 0.500 < 0.150 < 1.00 < 0.240 <<<< 24.0 < 0.530 < 3.00 < 0.760 < 0.690
1 600 600 500 20 70 400 0.02 0.4 400 6 4,000 100 40 24 100 25 6,000 NE 0.6 50 70 0.4 1,000 70 70 4,000 70 6 70 70
5,000 260,000 84,500 85,500 20,000 70,000 28,500 50 400 25,000 6,000 4,000,000 NE 40,000 7,500 100,000 11,700 6,000,000 NE NE 50,000 70,000 400 140,000 6,900 8,500 4,000,000 25,000 6,000 6,900 30,000
Notes:
1. All results in µg/L.
2. Bold denotes a compound detection
3. Shading denotes a 2L Standard violation4. < - denotes less than sample detection limit5. Italics indicates a GCL violation6. NE - Not Established7. "-" - indicates sample not tested per that method
2L Standard
Free Product (0.35')
Free product gauged in well - meter would not produce accurate reading
Free Product (0.05')
Free Product (0.08')
Free Product (4.78')
MMPE EVENT
MMPE EVENT
GCL
625BNA625BNA625BNA625BNA625BNAMADEPVPHMADEPVPHMADEPVPH504.16010BWell ID Date CollectedMW11/22/18 -----4,450 3,870 834 <0.0115 <3.309/23/20 9.01 < 0.252 < 1.59 6.5 11.2 -----MW2 6/25/18 Free Product (6.25')10/22/18 Free Product (7.05')vac on MW2 10/22-26/18 MMPE EVENT10/26/18 NO PRODUCT
12/3/18 Free Product (5.63')4/22/19 Free Product (4.11')
vac on MW2 4/22-26/19 MMPE EVENT4/26/19 Free Product (0.05')
4/30/19 Free Product (0.18')
vac on MW2 10/7-11/19 MMPE EVENT
9/23/20 Free Product (4.12')
vac on MW2 3/22-26/21 MMPE EVENT
5/9/22 Free Product (3.69')
1/18/23 Free Product (4.43')MW3 6/25/18 -----12,700 6,190 983 <0.0111 <3.30
9/23/20 < 0.781 < 0.504 < 3.18 12.7 23.3 -----5/9/22 Free Product (0.28')
1/18/23 Free Product (0.3')MW4 6/25/18 -----20,300 12,300 1,620 <0.0109 <3.30
9/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW5 12/3/18 -----15,300 3,520 1,320 < 0.0108 < 2.37
9/23/20 < 0.391 < 0.252 < 1.59 3.98 8.17 -----MW6 12/3/18 -----9,980 3,470 825 < 0.0113 < 2.37
9/23/20 < 1.95 < 1.26 < 7.95 29.4 57.4 -----MW7 12/3/18 -----621 < 200 70 < 0.0111 3.72
9/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW8 12/3/18 -----1,820 518 94.1 < 0.0109 < 2.37
9/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW9 12/3/18 -----< 150 < 200 < 25.0 < 0.0110 < 2.37
9/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW10 12/3/18 -----< 150 < 200 < 25.0 < 0.0111 < 2.37
9/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW11 12/3/18 -----< 150 < 200 < 25.0 < 0.0112 < 2.379/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW12 4/30/19 -----< 150 < 25.0 < 200 < 0.0111 <7.19/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW13 4/30/19 -----1,360 26.2 366 < 0.0111 <7.19/23/20 < 0.391 < 0.252 < 1.59 < 1.50 < 2.91 -----MW14 4/30/19 -----< 150 < 25.0 < 200 < 0.0115 <7.19/23/20 < 0.391 0.34 2.96 < 1.50 < 2.91 -----
MW15 9/23/20 < 1.95 < 1.26 < 7.95 45.9 84.2 -----1/18/23
MW16 9/23/20
vac on MW16 3/22-26/21 MMPE EVENT5/9/22 Free Product (0.08')
1/18/23 Free Product (4.78')MW17 9/23/20 < 1.95 < 1.26 < 7.98 30.8 52.7 -----
vac on MW17 3/22-26/21
1/18/23 Free product gauged in well - meter would not produce accurate reading7007006,000 1 30 400 700 200*0.02 15
700,000 NE NE 1,000 12,500 NE NE NE 50 15,000Notes:
1. All results in µg/L. 2. Bold denotes a compound detection
3. Shading denotes a 2L Standard violation4. < - denotes less than sample detection limit5. Italics indicates a GCL violation6. NE - Not Established7. "-" - indicates sample not tested per that method
Incident Name: Perth Mini Mart Incident No.: 40784
Analytical MethodContaminant of Concern
SUMMARY OF RESULTS BY METHODS OTHER THAN 6200B
2L Standard
GCL
Free Product (0.35')Free Product (0.05') C5-C8 AliphaticsC9-C12 AliphaticsC9-C10 AromaticsEDBLeadBenzyl Alcoholdi-n-Butyl PhthalateDiethyl Phthalate1-Methylnaphthalene2-Methylnaphthalene

APPENDIX D

ANALYTICAL REPORT
PREPARED FOR
Attn: Ryan Kerins
Terraquest Environmental Consultants, PC
100 E. Ruffin Street
Mebane, North Carolina 27302
Generated 2/2/2023 5:26:39 PM
JOB DESCRIPTION
Perth Mini Mart
JOB NUMBER
400-232047-1
See page two for job notes and contact information.
Pensacola FL 32514
3355 McLemore Drive
Eurofins Pensacola
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Eurofins Pensacola
Eurofins Pensacola is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report meet all NELAP requirements for accredited parameters, unless otherwise noted, and relate
only to the referenced samples. Pursuant to NELAP, this report may not be reproduced, except in full, without written
approval from the laboratory. For questions please contact the Project Manager at the e-mail address listed on this page, or
the telephone number at the bottom of the page. Eurofins Environment Testing Southeast LLC, Pensacola Certifications and
Approvals: Alabama (40150), Arizona (AZ0710), Arkansas (88-0689), Florida (E81010), Illinois (200041), Iowa (367), Kansas
(E-10253), Kentucky UST (53), Louisiana (30748), Maryland (233), Massachusetts (M-FL094), Michigan (9912), New
Hampshire (250510), New Jersey (FL006), North Carolina (314), Oklahoma (9810), Pennsylvania (68-00467), Rhode Island
(LAO00307), South Carolina (96026), Tennessee (TN02907), Texas (T104704286-10-2), Virginia (00008), Washington
(C2043), West Virginia (136), USDA Foreign Soil Permit (P330-08-00006).
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project
Manager.
Authorization
Generated
2/2/2023 5:26:39 PM
Authorized for release by
Chad Bechtold, Project Manager
[e-mail]
[phone]
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Table of Contents
Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Laboratory Job ID: 400-232047-1
Page 3 of 60 Eurofins Pensacola2/2/2023
Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .3
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .39
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .40
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .41
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .50
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .54
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .55
Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .56
Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .59
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Case Narrative
Client: Terraquest Environmental Consultants, PC Job ID: 400-232047-1
Project/Site: Perth Mini Mart
Job ID: 400-232047-1
Laboratory: Eurofins Pensacola
Narrative
Job Narrative
400-232047-1
Receipt
The samples were received on 1/20/2023 9:04 AM and 1/21/2023 9:23 AM. Unless otherwise noted below, the samples arrived in good
condition, and, where required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 0.0°C and 0.7°C
GC/MS VOA
Method SM6200_B: The following sample was diluted to bring the concentration of target analytes within the calibration range: MW12
(400-232072-1). Elevated reporting limits (RLs) are provided.
Method SM6200_B: The laboratory control sample (LCS) for analytical batch 400-609802 recovered outside control limits for the following
analytes: Bromochloromethane, Bromomethane, Trichloroethene, Trichlorofluoromethane and Vinyl chloride. These analytes were
biased high in the LCS and were not detected or not reported in the associated samples; therefore, the data have been reported.
Method SM6200_B: The following samples were diluted to bring the concentration of target analytes within the calibration range: MW1
(400-232047-1), MW4 (400-232047-2), MW5 (400-232047-3), MW6 (400-232047-4), MW11 (400-232047-9) and MW13 (400-232047-10).
Elevated reporting limits (RLs) are provided.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
GC Semi VOA
Method 504.1: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with
preparation batch 400-610674.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page.
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Detection Summary
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Client Sample ID: MW1 Lab Sample ID: 400-232047-1
1,2,4-Trimethylbenzene
RL
10.0 ug/L
MDL
8.20
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10112SM6200-B
1,3,5-Trimethylbenzene 10.0 ug/L5.60 Total/NA1032.1 SM6200-B
Benzene 10.0 ug/L1.30 Total/NA10728SM6200-B
Diisopropyl ether 10.0 ug/L2.00 Total/NA107.22 J SM6200-B
Ethylbenzene 10.0 ug/L5.00 Total/NA1071.6 SM6200-B
Isopropylbenzene 10.0 ug/L5.30 Total/NA1037.4 SM6200-B
m-Xylene & p-Xylene 50.0 ug/L6.30 Total/NA10737SM6200-B
o-Xylene 50.0 ug/L6.00 Total/NA10308SM6200-B
Toluene 10.0 ug/L4.10 Total/NA101170SM6200-B
Xylenes, Total 100 ug/L16.0 Total/NA101040SM6200-B
Client Sample ID: MW4 Lab Sample ID: 400-232047-2
1,2,4-Trimethylbenzene
RL
10.0 ug/L
MDL
8.20
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA10217SM6200-B
1,3,5-Trimethylbenzene 10.0 ug/L5.60 Total/NA1087.1 SM6200-B
2-Butanone (MEK)250 ug/L26.0 Total/NA1032.6 J SM6200-B
Benzene 10.0 ug/L1.30 Total/NA101920SM6200-B
Diisopropyl ether 10.0 ug/L2.00 Total/NA1014.3 SM6200-B
Ethylbenzene 10.0 ug/L5.00 Total/NA10430SM6200-B
Isopropylbenzene 10.0 ug/L5.30 Total/NA1042.1 SM6200-B
m-Xylene & p-Xylene 50.0 ug/L6.30 Total/NA101830SM6200-B
n-Butylbenzene 10.0 ug/L7.60 Total/NA107.85 J SM6200-B
N-Propylbenzene 10.0 ug/L6.90 Total/NA1047.9 SM6200-B
o-Xylene 50.0 ug/L6.00 Total/NA10493SM6200-B
Toluene 10.0 ug/L4.10 Total/NA101620SM6200-B
Xylenes, Total 100 ug/L16.0 Total/NA102330SM6200-B
Client Sample ID: MW5 Lab Sample ID: 400-232047-3
1,2,4-Trimethylbenzene
RL
200 ug/L
MDL
164
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA200642SM6200-B
1,3,5-Trimethylbenzene 200 ug/L112 Total/NA200210SM6200-B
Benzene 200 ug/L26.0 Total/NA2006610SM6200-B
Diisopropyl ether 200 ug/L40.0 Total/NA20082.3 J SM6200-B
Ethylbenzene 200 ug/L100 Total/NA2001810SM6200-B
Methyl tert-butyl ether 200 ug/L44.0 Total/NA200250SM6200-B
m-Xylene & p-Xylene 1000 ug/L126 Total/NA2008620SM6200-B
o-Xylene 1000 ug/L120 Total/NA2003050SM6200-B
Toluene 200 ug/L82.0 Total/NA20028200SM6200-B
Xylenes, Total 2000 ug/L320 Total/NA20011700SM6200-B
Client Sample ID: MW6 Lab Sample ID: 400-232047-4
1,2,4-Trimethylbenzene
RL
100 ug/L
MDL
82.0
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100842SM6200-B
1,3,5-Trimethylbenzene 100 ug/L56.0 Total/NA100341SM6200-B
Benzene 100 ug/L13.0 Total/NA1009050SM6200-B
Diisopropyl ether 100 ug/L20.0 Total/NA10072.3 J SM6200-B
Ethylbenzene 100 ug/L50.0 Total/NA1001370SM6200-B
Methyl tert-butyl ether 100 ug/L22.0 Total/NA10058.8 J SM6200-B
m-Xylene & p-Xylene 500 ug/L63.0 Total/NA1004380SM6200-B
Eurofins Pensacola
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Client Sample ID: MW6 (Continued)Lab Sample ID: 400-232047-4
N-Propylbenzene
RL
100 ug/L
MDL
69.0
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA100106SM6200-B
o-Xylene 500 ug/L60.0 Total/NA1002800SM6200-B
Toluene 100 ug/L41.0 Total/NA10014100SM6200-B
Xylenes, Total 1000 ug/L160 Total/NA1007170SM6200-B
Client Sample ID: MW7 Lab Sample ID: 400-232047-5
Benzene
RL
1.00 ug/L
MDL
0.130
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.407 SM6200-B
Client Sample ID: MW8 Lab Sample ID: 400-232047-6
1,3,5-Trimethylbenzene
RL
1.00 ug/L
MDL
0.560
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.699 SM6200-B
Benzene 1.00 ug/L0.130 Total/NA144.7 SM6200-B
Diisopropyl ether 1.00 ug/L0.200 Total/NA10.766 J SM6200-B
m-Xylene & p-Xylene 5.00 ug/L0.630 Total/NA11.51 J SM6200-B
o-Xylene 5.00 ug/L0.600 Total/NA12.75 J SM6200-B
Xylenes, Total 10.0 ug/L1.60 Total/NA14.26 J SM6200-B
Client Sample ID: MW9 Lab Sample ID: 400-232047-7
No Detections.
Client Sample ID: MW10 Lab Sample ID: 400-232047-8
Benzene
RL
1.00 ug/L
MDL
0.130
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.34 SM6200-B
m-Xylene & p-Xylene 5.00 ug/L0.630 Total/NA11.10 J SM6200-B
Xylenes, Total 10.0 ug/L1.60 Total/NA11.70 J SM6200-B
Client Sample ID: MW11 Lab Sample ID: 400-232047-9
1,2,4-Trimethylbenzene
RL
2.00 ug/L
MDL
1.64
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA25.34 SM6200-B
Benzene 2.00 ug/L0.260 Total/NA2251SM6200-B
Chlorobenzene 2.00 ug/L0.300 Total/NA20.402 J SM6200-B
Diisopropyl ether 2.00 ug/L0.400 Total/NA22.39 SM6200-B
Isopropylbenzene 2.00 ug/L1.06 Total/NA210.0 SM6200-B
Methyl tert-butyl ether 2.00 ug/L0.440 Total/NA20.818 J SM6200-B
m-Xylene & p-Xylene 10.0 ug/L1.26 Total/NA26.06 J SM6200-B
o-Xylene 10.0 ug/L1.20 Total/NA213.3 SM6200-B
Xylenes, Total 20.0 ug/L3.20 Total/NA219.4 J SM6200-B
Client Sample ID: MW13 Lab Sample ID: 400-232047-10
1,2,4-Trimethylbenzene
RL
5.00 ug/L
MDL
4.10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA518.8 SM6200-B
1,3,5-Trimethylbenzene 5.00 ug/L2.80 Total/NA511.0 SM6200-B
Benzene 5.00 ug/L0.650 Total/NA5504SM6200-B
Diisopropyl ether 5.00 ug/L1.00 Total/NA55.94 SM6200-B
Ethylbenzene 5.00 ug/L2.50 Total/NA55.17 SM6200-B
Isopropylbenzene 5.00 ug/L2.65 Total/NA522.8 SM6200-B
Methyl tert-butyl ether 5.00 ug/L1.10 Total/NA59.01 SM6200-B
Eurofins Pensacola
This Detection Summary does not include radiochemical test results.
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Detection Summary
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Client Sample ID: MW13 (Continued)Lab Sample ID: 400-232047-10
m-Xylene & p-Xylene
RL
25.0 ug/L
MDL
3.15
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA595.8 SM6200-B
o-Xylene 25.0 ug/L3.00 Total/NA554.9 SM6200-B
Toluene 5.00 ug/L2.05 Total/NA55.29 SM6200-B
Xylenes, Total 50.0 ug/L8.00 Total/NA5151SM6200-B
Client Sample ID: MW14 Lab Sample ID: 400-232047-11
1,2-Dichloroethane
RL
1.00 ug/L
MDL
0.190
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.313 SM6200-B
Client Sample ID: WSW1 Lab Sample ID: 400-232047-12
Bromodichloromethane
RL
1.00 ug/L
MDL
0.500
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA13.47 SM6200-B
Chloroform 1.00 ug/L1.00 Total/NA114.4 SM6200-B
Dibromochloromethane 1.00 ug/L0.240 Total/NA10.438 J SM6200-B
Client Sample ID: WSW2 Lab Sample ID: 400-232047-13
Methyl tert-butyl ether
RL
1.00 ug/L
MDL
0.220
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.231 SM6200-B
Client Sample ID: WSW4 Lab Sample ID: 400-232047-14
No Detections.
Client Sample ID: MW12 Lab Sample ID: 400-232072-1
1,2,4-Trimethylbenzene
RL
5.00 ug/L
MDL
4.10
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA55.85 SM6200-B
Benzene 5.00 ug/L0.650 Total/NA5313SM6200-B
Diisopropyl ether 5.00 ug/L1.00 Total/NA51.43 J SM6200-B
Ethylbenzene 5.00 ug/L2.50 Total/NA56.80 SM6200-B
Methyl tert-butyl ether 5.00 ug/L1.10 Total/NA54.37 J SM6200-B
m-Xylene & p-Xylene 25.0 ug/L3.15 Total/NA518.0 J SM6200-B
o-Xylene 25.0 ug/L3.00 Total/NA511.2 J SM6200-B
Xylenes, Total 50.0 ug/L8.00 Total/NA529.2 J SM6200-B
Eurofins Pensacola
This Detection Summary does not include radiochemical test results.
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Sample Summary
Client: Terraquest Environmental Consultants, PC Job ID: 400-232047-1
Project/Site: Perth Mini Mart
Lab Sample ID Client Sample ID Matrix Collected Received
400-232047-1 MW1 Water 01/18/23 12:24 01/20/23 09:04
400-232047-2 MW4 Water 01/18/23 12:21 01/20/23 09:04
400-232047-3 MW5 Water 01/18/23 12:13 01/20/23 09:04
400-232047-4 MW6 Water 01/18/23 12:17 01/20/23 09:04
400-232047-5 MW7 Water 01/18/23 12:04 01/20/23 09:04
400-232047-6 MW8 Water 01/18/23 12:10 01/20/23 09:04
400-232047-7 MW9 Water 01/18/23 11:40 01/20/23 09:04
400-232047-8 MW10 Water 01/18/23 11:30 01/20/23 09:04
400-232047-9 MW11 Water 01/18/23 12:08 01/20/23 09:04
400-232047-10 MW13 Water 01/18/23 12:01 01/20/23 09:04
400-232047-11 MW14 Water 01/18/23 11:50 01/20/23 09:04
400-232047-12 WSW1 Water 01/18/23 12:30 01/20/23 09:04
400-232047-13 WSW2 Water 01/18/23 12:55 01/20/23 09:04
400-232047-14 WSW4 Water 01/18/23 13:16 01/20/23 09:04
400-232072-1 MW12 Water 01/20/23 12:00 01/21/23 09:23
Eurofins PensacolaPage 8 of 60 2/2/2023
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-1Client Sample ID: MW1
Matrix: WaterDate Collected: 01/18/23 12:24
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1.60 U 10.0 1.60 ug/L 01/25/23 13:58 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
10.0 1.80 ug/L 01/25/23 13:58 101.80 U1,1,1-Trichloroethane
10.0 5.00 ug/L 01/25/23 13:58 105.00 U1,1,2,2-Tetrachloroethane
50.0 2.10 ug/L 01/25/23 13:58 102.10 U1,1,2-Trichloroethane
10.0 5.00 ug/L 01/25/23 13:58 105.00 U1,1-Dichloroethane
10.0 5.00 ug/L 01/25/23 13:58 105.00 U1,1-Dichloroethene
10.0 5.00 ug/L 01/25/23 13:58 105.00 U1,1-Dichloropropene
10.0 9.00 ug/L 01/25/23 13:58 109.00 U1,2,3-Trichlorobenzene
50.0 8.40 ug/L 01/25/23 13:58 108.40 U1,2,3-Trichloropropane
10.0 8.20 ug/L 01/25/23 13:58 108.20 U1,2,4-Trichlorobenzene
10.0 8.20 ug/L 01/25/23 13:58 101121,2,4-Trimethylbenzene
10.0 2.30 ug/L 01/25/23 13:58 102.30 U1,2-Dibromoethane (EDB)
10.0 5.00 ug/L 01/25/23 13:58 105.00 U1,2-Dichlorobenzene
10.0 1.90 ug/L 01/25/23 13:58 101.90 U1,2-Dichloroethane
10.0 5.00 ug/L 01/25/23 13:58 105.00 U1,2-Dichloropropane
10.0 5.60 ug/L 01/25/23 13:58 1032.11,3,5-Trimethylbenzene
10.0 5.40 ug/L 01/25/23 13:58 105.40 U1,3-Dichlorobenzene
10.0 5.00 ug/L 01/25/23 13:58 105.00 U1,3-Dichloropropane
10.0 6.40 ug/L 01/25/23 13:58 106.40 U1,4-Dichlorobenzene
10.0 5.00 ug/L 01/25/23 13:58 105.00 U2,2-Dichloropropane
250 26.0 ug/L 01/25/23 13:58 1026.0 U2-Butanone (MEK)
10.0 5.70 ug/L 01/25/23 13:58 105.70 U2-Chlorotoluene
250 14.0 ug/L 01/25/23 13:58 1014.0 U2-Hexanone
10.0 5.60 ug/L 01/25/23 13:58 105.60 U4-Chlorotoluene
250 18.0 ug/L 01/25/23 13:58 1018.0 U4-Methyl-2-pentanone (MIBK)
250 100 ug/L 01/25/23 13:58 10100UAcetone
10.0 1.30 ug/L 01/25/23 13:58 10728Benzene
10.0 5.40 ug/L 01/25/23 13:58 105.40 UBromobenzene
10.0 2.10 ug/L 01/25/23 13:58 102.10 U *+Bromochloromethane
10.0 5.00 ug/L 01/25/23 13:58 105.00 UBromodichloromethane
50.0 2.50 ug/L 01/25/23 13:58 102.50 UBromoform
10.0 9.80 ug/L 01/26/23 21:57 109.80 UBromomethane
10.0 1.90 ug/L 01/25/23 13:58 101.90 UCarbon tetrachloride
10.0 1.50 ug/L 01/25/23 13:58 101.50 UChlorobenzene
10.0 7.60 ug/L 01/25/23 13:58 107.60 UChloroethane
10.0 10.0 ug/L 01/25/23 13:58 1010.0 UChloroform
10.0 3.20 ug/L 01/25/23 13:58 103.20 UChloromethane
10.0 2.00 ug/L 01/25/23 13:58 102.00 Ucis-1,2-Dichloroethene
50.0 5.00 ug/L 01/25/23 13:58 105.00 Ucis-1,3-Dichloropropene
10.0 2.40 ug/L 01/25/23 13:58 102.40 UDibromochloromethane
10.0 8.50 ug/L 01/25/23 13:58 108.50 UDichlorodifluoromethane
10.0 2.00 ug/L 01/25/23 13:58 107.22 JDiisopropyl ether
1000 240 ug/L 01/25/23 13:58 10240UEthanol
10.0 5.00 ug/L 01/25/23 13:58 1071.6Ethylbenzene
10.0 5.30 ug/L 01/25/23 13:58 1037.4Isopropylbenzene
10.0 2.20 ug/L 01/25/23 13:58 102.20 UMethyl tert-butyl ether
50.0 30.0 ug/L 01/25/23 13:58 1030.0 UMethylene Chloride
50.0 6.30 ug/L 01/25/23 13:58 10737m-Xylene & p-Xylene
50.0 30.0 ug/L 01/25/23 13:58 1030.0 UNaphthalene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-1Client Sample ID: MW1
Matrix: WaterDate Collected: 01/18/23 12:24
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
7.60 U 10.0 7.60 ug/L 01/25/23 13:58 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
10.0 6.90 ug/L 01/25/23 13:58 106.90 UN-Propylbenzene
50.0 6.00 ug/L 01/25/23 13:58 10308o-Xylene
10.0 7.10 ug/L 01/25/23 13:58 107.10 Up-Cymene (p-Isopropyltoluene)
10.0 7.00 ug/L 01/25/23 13:58 107.00 Usec-Butylbenzene
10.0 10.0 ug/L 01/25/23 13:58 1010.0 UStyrene
10.0 6.30 ug/L 01/25/23 13:58 106.30 Utert-Butylbenzene
10.0 9.00 ug/L 01/25/23 13:58 109.00 UTetrachloroethene
10.0 4.10 ug/L 01/25/23 13:58 101170Toluene
10.0 5.00 ug/L 01/25/23 13:58 105.00 Utrans-1,2-Dichloroethene
50.0 2.00 ug/L 01/25/23 13:58 102.00 Utrans-1,3-Dichloropropene
10.0 1.50 ug/L 01/25/23 13:58 101.50 U *+Trichloroethene
10.0 5.20 ug/L 01/25/23 13:58 105.20 U *+Trichlorofluoromethane
250 9.30 ug/L 01/25/23 13:58 109.30 UVinyl acetate
10.0 5.00 ug/L 01/25/23 13:58 105.00 U *+Vinyl chloride
100 16.0 ug/L 01/25/23 13:58 101040Xylenes, Total
4-Bromofluorobenzene 88 72-119 01/25/23 13:58 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene 100 01/26/23 21:57 1072-119
Dibromofluoromethane 109 01/25/23 13:58 1075-126
Dibromofluoromethane 102 01/26/23 21:57 1075-126
Toluene-d8 (Surr)96 01/25/23 13:58 1064-132
Toluene-d8 (Surr)95 01/26/23 21:57 1064-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-2Client Sample ID: MW4
Matrix: WaterDate Collected: 01/18/23 12:21
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
1.60 U 10.0 1.60 ug/L 01/25/23 14:19 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
10.0 1.80 ug/L 01/25/23 14:19 101.80 U1,1,1-Trichloroethane
10.0 5.00 ug/L 01/25/23 14:19 105.00 U1,1,2,2-Tetrachloroethane
50.0 2.10 ug/L 01/25/23 14:19 102.10 U1,1,2-Trichloroethane
10.0 5.00 ug/L 01/25/23 14:19 105.00 U1,1-Dichloroethane
10.0 5.00 ug/L 01/25/23 14:19 105.00 U1,1-Dichloroethene
10.0 5.00 ug/L 01/25/23 14:19 105.00 U1,1-Dichloropropene
10.0 9.00 ug/L 01/25/23 14:19 109.00 U1,2,3-Trichlorobenzene
50.0 8.40 ug/L 01/25/23 14:19 108.40 U1,2,3-Trichloropropane
10.0 8.20 ug/L 01/25/23 14:19 108.20 U1,2,4-Trichlorobenzene
10.0 8.20 ug/L 01/25/23 14:19 102171,2,4-Trimethylbenzene
10.0 2.30 ug/L 01/25/23 14:19 102.30 U1,2-Dibromoethane (EDB)
10.0 5.00 ug/L 01/25/23 14:19 105.00 U1,2-Dichlorobenzene
10.0 1.90 ug/L 01/25/23 14:19 101.90 U1,2-Dichloroethane
10.0 5.00 ug/L 01/25/23 14:19 105.00 U1,2-Dichloropropane
10.0 5.60 ug/L 01/25/23 14:19 1087.11,3,5-Trimethylbenzene
10.0 5.40 ug/L 01/25/23 14:19 105.40 U1,3-Dichlorobenzene
10.0 5.00 ug/L 01/25/23 14:19 105.00 U1,3-Dichloropropane
10.0 6.40 ug/L 01/25/23 14:19 106.40 U1,4-Dichlorobenzene
10.0 5.00 ug/L 01/25/23 14:19 105.00 U2,2-Dichloropropane
250 26.0 ug/L 01/25/23 14:19 1032.6 J2-Butanone (MEK)
10.0 5.70 ug/L 01/25/23 14:19 105.70 U2-Chlorotoluene
250 14.0 ug/L 01/25/23 14:19 1014.0 U2-Hexanone
10.0 5.60 ug/L 01/25/23 14:19 105.60 U4-Chlorotoluene
250 18.0 ug/L 01/25/23 14:19 1018.0 U4-Methyl-2-pentanone (MIBK)
250 100 ug/L 01/25/23 14:19 10100UAcetone
10.0 1.30 ug/L 01/25/23 14:19 101920Benzene
10.0 5.40 ug/L 01/25/23 14:19 105.40 UBromobenzene
10.0 2.10 ug/L 01/25/23 14:19 102.10 U *+Bromochloromethane
10.0 5.00 ug/L 01/25/23 14:19 105.00 UBromodichloromethane
50.0 2.50 ug/L 01/25/23 14:19 102.50 UBromoform
10.0 9.80 ug/L 01/26/23 22:21 109.80 UBromomethane
10.0 1.90 ug/L 01/25/23 14:19 101.90 UCarbon tetrachloride
10.0 1.50 ug/L 01/25/23 14:19 101.50 UChlorobenzene
10.0 7.60 ug/L 01/25/23 14:19 107.60 UChloroethane
10.0 10.0 ug/L 01/25/23 14:19 1010.0 UChloroform
10.0 3.20 ug/L 01/26/23 22:21 103.20 UChloromethane
10.0 2.00 ug/L 01/25/23 14:19 102.00 Ucis-1,2-Dichloroethene
50.0 5.00 ug/L 01/25/23 14:19 105.00 Ucis-1,3-Dichloropropene
10.0 2.40 ug/L 01/25/23 14:19 102.40 UDibromochloromethane
10.0 8.50 ug/L 01/25/23 14:19 108.50 UDichlorodifluoromethane
10.0 2.00 ug/L 01/25/23 14:19 1014.3Diisopropyl ether
1000 240 ug/L 01/25/23 14:19 10240UEthanol
10.0 5.00 ug/L 01/25/23 14:19 10430Ethylbenzene
10.0 5.30 ug/L 01/25/23 14:19 1042.1Isopropylbenzene
10.0 2.20 ug/L 01/25/23 14:19 102.20 UMethyl tert-butyl ether
50.0 30.0 ug/L 01/25/23 14:19 1030.0 UMethylene Chloride
50.0 6.30 ug/L 01/25/23 14:19 101830m-Xylene & p-Xylene
50.0 30.0 ug/L 01/25/23 14:19 1030.0 UNaphthalene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-2Client Sample ID: MW4
Matrix: WaterDate Collected: 01/18/23 12:21
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
7.85 J 10.0 7.60 ug/L 01/25/23 14:19 10
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
10.0 6.90 ug/L 01/25/23 14:19 1047.9N-Propylbenzene
50.0 6.00 ug/L 01/25/23 14:19 10493o-Xylene
10.0 7.10 ug/L 01/25/23 14:19 107.10 Up-Cymene (p-Isopropyltoluene)
10.0 7.00 ug/L 01/25/23 14:19 107.00 Usec-Butylbenzene
10.0 10.0 ug/L 01/25/23 14:19 1010.0 UStyrene
10.0 6.30 ug/L 01/25/23 14:19 106.30 Utert-Butylbenzene
10.0 9.00 ug/L 01/25/23 14:19 109.00 UTetrachloroethene
10.0 4.10 ug/L 01/25/23 14:19 101620Toluene
10.0 5.00 ug/L 01/25/23 14:19 105.00 Utrans-1,2-Dichloroethene
50.0 2.00 ug/L 01/25/23 14:19 102.00 Utrans-1,3-Dichloropropene
10.0 1.50 ug/L 01/25/23 14:19 101.50 U *+Trichloroethene
10.0 5.20 ug/L 01/25/23 14:19 105.20 U *+Trichlorofluoromethane
250 9.30 ug/L 01/25/23 14:19 109.30 UVinyl acetate
10.0 5.00 ug/L 01/25/23 14:19 105.00 U *+Vinyl chloride
100 16.0 ug/L 01/25/23 14:19 102330Xylenes, Total
4-Bromofluorobenzene 87 72-119 01/25/23 14:19 10
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene 97 01/26/23 22:21 1072-119
Dibromofluoromethane 109 01/25/23 14:19 1075-126
Dibromofluoromethane 98 01/26/23 22:21 1075-126
Toluene-d8 (Surr)95 01/25/23 14:19 1064-132
Toluene-d8 (Surr)95 01/26/23 22:21 1064-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-3Client Sample ID: MW5
Matrix: WaterDate Collected: 01/18/23 12:13
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
32.0 U 200 32.0 ug/L 01/25/23 15:21 200
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
200 36.0 ug/L 01/25/23 15:21 20036.0 U1,1,1-Trichloroethane
200 100 ug/L 01/25/23 15:21 200100U1,1,2,2-Tetrachloroethane
1000 42.0 ug/L 01/25/23 15:21 20042.0 U1,1,2-Trichloroethane
200 100 ug/L 01/25/23 15:21 200100U1,1-Dichloroethane
200 100 ug/L 01/25/23 15:21 200100U1,1-Dichloroethene
200 100 ug/L 01/25/23 15:21 200100U1,1-Dichloropropene
200 180 ug/L 01/25/23 15:21 200180U1,2,3-Trichlorobenzene
1000 168 ug/L 01/25/23 15:21 200168U1,2,3-Trichloropropane
200 164 ug/L 01/25/23 15:21 200164U1,2,4-Trichlorobenzene
200 164 ug/L 01/25/23 15:21 2006421,2,4-Trimethylbenzene
200 46.0 ug/L 01/25/23 15:21 20046.0 U1,2-Dibromoethane (EDB)
200 100 ug/L 01/25/23 15:21 200100U1,2-Dichlorobenzene
200 38.0 ug/L 01/25/23 15:21 20038.0 U1,2-Dichloroethane
200 100 ug/L 01/25/23 15:21 200100U1,2-Dichloropropane
200 112 ug/L 01/25/23 15:21 2002101,3,5-Trimethylbenzene
200 108 ug/L 01/25/23 15:21 200108U1,3-Dichlorobenzene
200 100 ug/L 01/25/23 15:21 200100U1,3-Dichloropropane
200 128 ug/L 01/25/23 15:21 200128U1,4-Dichlorobenzene
200 100 ug/L 01/25/23 15:21 200100U2,2-Dichloropropane
5000 520 ug/L 01/25/23 15:21 200520U2-Butanone (MEK)
200 114 ug/L 01/25/23 15:21 200114U2-Chlorotoluene
5000 280 ug/L 01/25/23 15:21 200280U2-Hexanone
200 112 ug/L 01/25/23 15:21 200112U4-Chlorotoluene
5000 360 ug/L 01/25/23 15:21 200360U4-Methyl-2-pentanone (MIBK)
5000 2000 ug/L 01/25/23 15:21 2002000UAcetone
200 26.0 ug/L 01/25/23 15:21 2006610Benzene
200 108 ug/L 01/25/23 15:21 200108UBromobenzene
200 42.0 ug/L 01/25/23 15:21 20042.0 U *+Bromochloromethane
200 100 ug/L 01/25/23 15:21 200100UBromodichloromethane
1000 50.0 ug/L 01/25/23 15:21 20050.0 UBromoform
200 196 ug/L 01/25/23 15:21 200196U *+Bromomethane
200 38.0 ug/L 01/25/23 15:21 20038.0 UCarbon tetrachloride
200 30.0 ug/L 01/25/23 15:21 20030.0 UChlorobenzene
200 152 ug/L 01/25/23 15:21 200152UChloroethane
200 200 ug/L 01/25/23 15:21 200200UChloroform
200 64.0 ug/L 01/25/23 15:21 20064.0 UChloromethane
200 40.0 ug/L 01/25/23 15:21 20040.0 Ucis-1,2-Dichloroethene
1000 100 ug/L 01/25/23 15:21 200100Ucis-1,3-Dichloropropene
200 48.0 ug/L 01/25/23 15:21 20048.0 UDibromochloromethane
200 170 ug/L 01/25/23 15:21 200170UDichlorodifluoromethane
200 40.0 ug/L 01/25/23 15:21 20082.3 JDiisopropyl ether
20000 4800 ug/L 01/25/23 15:21 2004800UEthanol
200 100 ug/L 01/25/23 15:21 2001810Ethylbenzene
200 106 ug/L 01/25/23 15:21 200106UIsopropylbenzene
200 44.0 ug/L 01/25/23 15:21 200250Methyl tert-butyl ether
1000 600 ug/L 01/25/23 15:21 200600UMethylene Chloride
1000 126 ug/L 01/25/23 15:21 2008620m-Xylene & p-Xylene
1000 600 ug/L 01/25/23 15:21 200600UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-3Client Sample ID: MW5
Matrix: WaterDate Collected: 01/18/23 12:13
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
152 U 200 152 ug/L 01/25/23 15:21 200
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
200 138 ug/L 01/25/23 15:21 200138UN-Propylbenzene
1000 120 ug/L 01/25/23 15:21 2003050o-Xylene
200 142 ug/L 01/25/23 15:21 200142Up-Cymene (p-Isopropyltoluene)
200 140 ug/L 01/25/23 15:21 200140Usec-Butylbenzene
200 200 ug/L 01/25/23 15:21 200200UStyrene
200 126 ug/L 01/25/23 15:21 200126Utert-Butylbenzene
200 180 ug/L 01/25/23 15:21 200180UTetrachloroethene
200 82.0 ug/L 01/25/23 15:21 20028200Toluene
200 100 ug/L 01/25/23 15:21 200100Utrans-1,2-Dichloroethene
1000 40.0 ug/L 01/25/23 15:21 20040.0 Utrans-1,3-Dichloropropene
200 30.0 ug/L 01/25/23 15:21 20030.0 U *+Trichloroethene
200 104 ug/L 01/25/23 15:21 200104U *+Trichlorofluoromethane
5000 186 ug/L 01/25/23 15:21 200186UVinyl acetate
200 100 ug/L 01/25/23 15:21 200100U *+Vinyl chloride
2000 320 ug/L 01/25/23 15:21 20011700Xylenes, Total
4-Bromofluorobenzene 89 72-119 01/25/23 15:21 200
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 112 01/25/23 15:21 20075-126
Toluene-d8 (Surr)93 01/25/23 15:21 20064-132
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-4Client Sample ID: MW6
Matrix: WaterDate Collected: 01/18/23 12:17
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
16.0 U 100 16.0 ug/L 01/25/23 14:40 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
100 18.0 ug/L 01/25/23 14:40 10018.0 U1,1,1-Trichloroethane
100 50.0 ug/L 01/25/23 14:40 10050.0 U1,1,2,2-Tetrachloroethane
500 21.0 ug/L 01/25/23 14:40 10021.0 U1,1,2-Trichloroethane
100 50.0 ug/L 01/25/23 14:40 10050.0 U1,1-Dichloroethane
100 50.0 ug/L 01/25/23 14:40 10050.0 U1,1-Dichloroethene
100 50.0 ug/L 01/25/23 14:40 10050.0 U1,1-Dichloropropene
100 90.0 ug/L 01/25/23 14:40 10090.0 U1,2,3-Trichlorobenzene
500 84.0 ug/L 01/25/23 14:40 10084.0 U1,2,3-Trichloropropane
100 82.0 ug/L 01/25/23 14:40 10082.0 U1,2,4-Trichlorobenzene
100 82.0 ug/L 01/25/23 14:40 1008421,2,4-Trimethylbenzene
100 23.0 ug/L 01/25/23 14:40 10023.0 U1,2-Dibromoethane (EDB)
100 50.0 ug/L 01/25/23 14:40 10050.0 U1,2-Dichlorobenzene
100 19.0 ug/L 01/25/23 14:40 10019.0 U1,2-Dichloroethane
100 50.0 ug/L 01/25/23 14:40 10050.0 U1,2-Dichloropropane
100 56.0 ug/L 01/25/23 14:40 1003411,3,5-Trimethylbenzene
100 54.0 ug/L 01/25/23 14:40 10054.0 U1,3-Dichlorobenzene
100 50.0 ug/L 01/25/23 14:40 10050.0 U1,3-Dichloropropane
100 64.0 ug/L 01/25/23 14:40 10064.0 U1,4-Dichlorobenzene
100 50.0 ug/L 01/25/23 14:40 10050.0 U2,2-Dichloropropane
2500 260 ug/L 01/25/23 14:40 100260U2-Butanone (MEK)
100 57.0 ug/L 01/25/23 14:40 10057.0 U2-Chlorotoluene
2500 140 ug/L 01/25/23 14:40 100140U2-Hexanone
100 56.0 ug/L 01/25/23 14:40 10056.0 U4-Chlorotoluene
2500 180 ug/L 01/25/23 14:40 100180U4-Methyl-2-pentanone (MIBK)
2500 1000 ug/L 01/25/23 14:40 1001000UAcetone
100 13.0 ug/L 01/25/23 14:40 1009050Benzene
100 54.0 ug/L 01/25/23 14:40 10054.0 UBromobenzene
100 21.0 ug/L 01/25/23 14:40 10021.0 U *+Bromochloromethane
100 50.0 ug/L 01/25/23 14:40 10050.0 UBromodichloromethane
500 25.0 ug/L 01/25/23 14:40 10025.0 UBromoform
100 98.0 ug/L 01/27/23 00:24 10098.0 UBromomethane
100 19.0 ug/L 01/25/23 14:40 10019.0 UCarbon tetrachloride
100 15.0 ug/L 01/25/23 14:40 10015.0 UChlorobenzene
100 76.0 ug/L 01/25/23 14:40 10076.0 UChloroethane
100 100 ug/L 01/25/23 14:40 100100UChloroform
100 32.0 ug/L 01/25/23 14:40 10032.0 UChloromethane
100 20.0 ug/L 01/25/23 14:40 10020.0 Ucis-1,2-Dichloroethene
500 50.0 ug/L 01/25/23 14:40 10050.0 Ucis-1,3-Dichloropropene
100 24.0 ug/L 01/25/23 14:40 10024.0 UDibromochloromethane
100 85.0 ug/L 01/25/23 14:40 10085.0 UDichlorodifluoromethane
100 20.0 ug/L 01/25/23 14:40 10072.3 JDiisopropyl ether
10000 2400 ug/L 01/25/23 14:40 1002400UEthanol
100 50.0 ug/L 01/25/23 14:40 1001370Ethylbenzene
100 53.0 ug/L 01/25/23 14:40 10053.0 UIsopropylbenzene
100 22.0 ug/L 01/25/23 14:40 10058.8 JMethyl tert-butyl ether
500 300 ug/L 01/25/23 14:40 100300UMethylene Chloride
500 63.0 ug/L 01/25/23 14:40 1004380m-Xylene & p-Xylene
500 300 ug/L 01/25/23 14:40 100300UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-4Client Sample ID: MW6
Matrix: WaterDate Collected: 01/18/23 12:17
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
76.0 U 100 76.0 ug/L 01/25/23 14:40 100
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
100 69.0 ug/L 01/25/23 14:40 100106N-Propylbenzene
500 60.0 ug/L 01/25/23 14:40 1002800o-Xylene
100 71.0 ug/L 01/25/23 14:40 10071.0 Up-Cymene (p-Isopropyltoluene)
100 70.0 ug/L 01/25/23 14:40 10070.0 Usec-Butylbenzene
100 100 ug/L 01/25/23 14:40 100100UStyrene
100 63.0 ug/L 01/25/23 14:40 10063.0 Utert-Butylbenzene
100 90.0 ug/L 01/25/23 14:40 10090.0 UTetrachloroethene
100 41.0 ug/L 01/25/23 14:40 10014100Toluene
100 50.0 ug/L 01/25/23 14:40 10050.0 Utrans-1,2-Dichloroethene
500 20.0 ug/L 01/25/23 14:40 10020.0 Utrans-1,3-Dichloropropene
100 15.0 ug/L 01/25/23 14:40 10015.0 U *+Trichloroethene
100 52.0 ug/L 01/25/23 14:40 10052.0 U *+Trichlorofluoromethane
2500 93.0 ug/L 01/25/23 14:40 10093.0 UVinyl acetate
100 50.0 ug/L 01/25/23 14:40 10050.0 U *+Vinyl chloride
1000 160 ug/L 01/25/23 14:40 1007170Xylenes, Total
4-Bromofluorobenzene 87 72-119 01/25/23 14:40 100
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene 99 01/27/23 00:24 10072-119
Dibromofluoromethane 113 01/25/23 14:40 10075-126
Dibromofluoromethane 99 01/27/23 00:24 10075-126
Toluene-d8 (Surr)95 01/25/23 14:40 10064-132
Toluene-d8 (Surr)96 01/27/23 00:24 10064-132
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-5Client Sample ID: MW7
Matrix: WaterDate Collected: 01/18/23 12:04
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 16:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 16:47 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 16:47 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 16:47 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 16:47 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 16:47 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 16:47 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 16:47 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 16:47 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 16:47 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 16:47 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 16:47 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 16:47 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 16:47 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 16:47 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 16:47 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 16:47 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 16:47 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 16:47 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 16:47 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 16:47 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 16:47 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 16:47 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 16:47 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 16:47 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 16:47 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 16:47 10.407 JBenzene
1.00 0.540 ug/L 01/25/23 16:47 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 16:47 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 16:47 10.500 UBromodichloromethane
5.00 0.250 ug/L 01/25/23 16:47 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 16:47 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 16:47 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 16:47 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 16:47 10.760 UChloroethane
1.00 1.00 ug/L 01/25/23 16:47 11.00 UChloroform
1.00 0.320 ug/L 01/25/23 16:47 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 16:47 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 16:47 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 16:47 10.240 UDibromochloromethane
1.00 0.850 ug/L 01/25/23 16:47 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 16:47 10.200 UDiisopropyl ether
100 24.0 ug/L 01/25/23 16:47 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 16:47 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 16:47 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 16:47 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 16:47 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 16:47 10.630 Um-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 16:47 13.00 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-5Client Sample ID: MW7
Matrix: WaterDate Collected: 01/18/23 12:04
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 16:47 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 16:47 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 16:47 10.600 Uo-Xylene
1.00 0.710 ug/L 01/25/23 16:47 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 16:47 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 16:47 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 16:47 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 16:47 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 16:47 10.410 UToluene
1.00 0.500 ug/L 01/25/23 16:47 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 16:47 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 16:47 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 16:47 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 16:47 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 16:47 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 16:47 11.60 UXylenes, Total
4-Bromofluorobenzene 86 72-119 01/25/23 16:47 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 111 01/25/23 16:47 175-126
Toluene-d8 (Surr)92 01/25/23 16:47 164-132
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-6Client Sample ID: MW8
Matrix: WaterDate Collected: 01/18/23 12:10
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 17:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 17:08 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 17:08 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 17:08 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 17:08 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 17:08 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 17:08 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 17:08 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 17:08 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 17:08 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 17:08 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 17:08 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 17:08 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 17:08 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 17:08 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 17:08 10.699 J1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 17:08 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 17:08 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 17:08 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 17:08 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 17:08 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 17:08 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 17:08 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 17:08 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 17:08 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 17:08 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 17:08 144.7Benzene
1.00 0.540 ug/L 01/25/23 17:08 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 17:08 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 17:08 10.500 UBromodichloromethane
5.00 0.250 ug/L 01/25/23 17:08 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 17:08 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 17:08 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 17:08 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 17:08 10.760 UChloroethane
1.00 1.00 ug/L 01/25/23 17:08 11.00 UChloroform
1.00 0.320 ug/L 01/25/23 17:08 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 17:08 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 17:08 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 17:08 10.240 UDibromochloromethane
1.00 0.850 ug/L 01/25/23 17:08 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 17:08 10.766 JDiisopropyl ether
100 24.0 ug/L 01/25/23 17:08 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 17:08 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 17:08 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 17:08 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 17:08 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 17:08 11.51 Jm-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 17:08 13.00 UNaphthalene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-6Client Sample ID: MW8
Matrix: WaterDate Collected: 01/18/23 12:10
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 17:08 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 17:08 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 17:08 12.75 Jo-Xylene
1.00 0.710 ug/L 01/25/23 17:08 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 17:08 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 17:08 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 17:08 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 17:08 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 17:08 10.410 UToluene
1.00 0.500 ug/L 01/25/23 17:08 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 17:08 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 17:08 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 17:08 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 17:08 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 17:08 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 17:08 14.26 JXylenes, Total
4-Bromofluorobenzene 89 72-119 01/25/23 17:08 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 110 01/25/23 17:08 175-126
Toluene-d8 (Surr)92 01/25/23 17:08 164-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-7Client Sample ID: MW9
Matrix: WaterDate Collected: 01/18/23 11:40
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 17:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 17:29 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 17:29 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 17:29 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 17:29 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 17:29 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 17:29 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 17:29 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 17:29 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 17:29 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 17:29 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 17:29 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 17:29 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 17:29 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 17:29 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 17:29 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 17:29 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 17:29 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 17:29 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 17:29 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 17:29 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 17:29 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 17:29 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 17:29 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 17:29 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 17:29 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 17:29 10.130 UBenzene
1.00 0.540 ug/L 01/25/23 17:29 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 17:29 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 17:29 10.500 UBromodichloromethane
5.00 0.250 ug/L 01/25/23 17:29 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 17:29 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 17:29 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 17:29 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 17:29 10.760 UChloroethane
1.00 1.00 ug/L 01/25/23 17:29 11.00 UChloroform
1.00 0.320 ug/L 01/25/23 17:29 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 17:29 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 17:29 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 17:29 10.240 UDibromochloromethane
1.00 0.850 ug/L 01/25/23 17:29 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 17:29 10.200 UDiisopropyl ether
100 24.0 ug/L 01/25/23 17:29 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 17:29 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 17:29 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 17:29 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 17:29 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 17:29 10.630 Um-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 17:29 13.00 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-7Client Sample ID: MW9
Matrix: WaterDate Collected: 01/18/23 11:40
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 17:29 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 17:29 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 17:29 10.600 Uo-Xylene
1.00 0.710 ug/L 01/25/23 17:29 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 17:29 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 17:29 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 17:29 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 17:29 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 17:29 10.410 UToluene
1.00 0.500 ug/L 01/25/23 17:29 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 17:29 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 17:29 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 17:29 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 17:29 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 17:29 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 17:29 11.60 UXylenes, Total
4-Bromofluorobenzene 87 72-119 01/25/23 17:29 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 114 01/25/23 17:29 175-126
Toluene-d8 (Surr)94 01/25/23 17:29 164-132
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-8Client Sample ID: MW10
Matrix: WaterDate Collected: 01/18/23 11:30
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 17:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 17:50 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 17:50 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 17:50 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 17:50 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 17:50 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 17:50 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 17:50 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 17:50 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 17:50 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 17:50 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 17:50 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 17:50 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 17:50 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 17:50 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 17:50 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 17:50 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 17:50 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 17:50 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 17:50 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 17:50 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 17:50 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 17:50 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 17:50 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 17:50 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 17:50 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 17:50 11.34Benzene
1.00 0.540 ug/L 01/25/23 17:50 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 17:50 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 17:50 10.500 UBromodichloromethane
5.00 0.250 ug/L 01/25/23 17:50 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 17:50 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 17:50 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 17:50 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 17:50 10.760 UChloroethane
1.00 1.00 ug/L 01/25/23 17:50 11.00 UChloroform
1.00 0.320 ug/L 01/25/23 17:50 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 17:50 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 17:50 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 17:50 10.240 UDibromochloromethane
1.00 0.850 ug/L 01/25/23 17:50 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 17:50 10.200 UDiisopropyl ether
100 24.0 ug/L 01/25/23 17:50 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 17:50 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 17:50 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 17:50 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 17:50 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 17:50 11.10 Jm-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 17:50 13.00 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-8Client Sample ID: MW10
Matrix: WaterDate Collected: 01/18/23 11:30
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 17:50 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 17:50 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 17:50 10.600 Uo-Xylene
1.00 0.710 ug/L 01/25/23 17:50 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 17:50 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 17:50 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 17:50 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 17:50 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 17:50 10.410 UToluene
1.00 0.500 ug/L 01/25/23 17:50 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 17:50 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 17:50 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 17:50 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 17:50 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 17:50 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 17:50 11.70 JXylenes, Total
4-Bromofluorobenzene 88 72-119 01/25/23 17:50 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 112 01/25/23 17:50 175-126
Toluene-d8 (Surr)89 01/25/23 17:50 164-132
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-9Client Sample ID: MW11
Matrix: WaterDate Collected: 01/18/23 12:08
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.320 U 2.00 0.320 ug/L 01/25/23 13:17 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
2.00 0.360 ug/L 01/25/23 13:17 20.360 U1,1,1-Trichloroethane
2.00 1.00 ug/L 01/25/23 13:17 21.00 U1,1,2,2-Tetrachloroethane
10.0 0.420 ug/L 01/25/23 13:17 20.420 U1,1,2-Trichloroethane
2.00 1.00 ug/L 01/25/23 13:17 21.00 U1,1-Dichloroethane
2.00 1.00 ug/L 01/25/23 13:17 21.00 U1,1-Dichloroethene
2.00 1.00 ug/L 01/25/23 13:17 21.00 U1,1-Dichloropropene
2.00 1.80 ug/L 01/25/23 13:17 21.80 U1,2,3-Trichlorobenzene
10.0 1.68 ug/L 01/25/23 13:17 21.68 U1,2,3-Trichloropropane
2.00 1.64 ug/L 01/25/23 13:17 21.64 U1,2,4-Trichlorobenzene
2.00 1.64 ug/L 01/25/23 13:17 25.341,2,4-Trimethylbenzene
2.00 0.460 ug/L 01/25/23 13:17 20.460 U1,2-Dibromoethane (EDB)
2.00 1.00 ug/L 01/25/23 13:17 21.00 U1,2-Dichlorobenzene
2.00 0.380 ug/L 01/25/23 13:17 20.380 U1,2-Dichloroethane
2.00 1.00 ug/L 01/25/23 13:17 21.00 U1,2-Dichloropropane
2.00 1.12 ug/L 01/25/23 13:17 21.12 U1,3,5-Trimethylbenzene
2.00 1.08 ug/L 01/25/23 13:17 21.08 U1,3-Dichlorobenzene
2.00 1.00 ug/L 01/25/23 13:17 21.00 U1,3-Dichloropropane
2.00 1.28 ug/L 01/25/23 13:17 21.28 U1,4-Dichlorobenzene
2.00 1.00 ug/L 01/25/23 13:17 21.00 U2,2-Dichloropropane
50.0 5.20 ug/L 01/25/23 13:17 25.20 U2-Butanone (MEK)
2.00 1.14 ug/L 01/25/23 13:17 21.14 U2-Chlorotoluene
50.0 2.80 ug/L 01/25/23 13:17 22.80 U2-Hexanone
2.00 1.12 ug/L 01/25/23 13:17 21.12 U4-Chlorotoluene
50.0 3.60 ug/L 01/25/23 13:17 23.60 U4-Methyl-2-pentanone (MIBK)
50.0 20.0 ug/L 01/25/23 13:17 220.0 UAcetone
2.00 0.260 ug/L 01/25/23 13:17 2251Benzene
2.00 1.08 ug/L 01/25/23 13:17 21.08 UBromobenzene
2.00 0.420 ug/L 01/25/23 13:17 20.420 U *+Bromochloromethane
2.00 1.00 ug/L 01/25/23 13:17 21.00 UBromodichloromethane
10.0 0.500 ug/L 01/25/23 13:17 20.500 UBromoform
2.00 1.96 ug/L 01/25/23 13:17 21.96 U *+Bromomethane
2.00 0.380 ug/L 01/25/23 13:17 20.380 UCarbon tetrachloride
2.00 0.300 ug/L 01/25/23 13:17 20.402 JChlorobenzene
2.00 1.52 ug/L 01/25/23 13:17 21.52 UChloroethane
2.00 2.00 ug/L 01/25/23 13:17 22.00 UChloroform
2.00 0.640 ug/L 01/25/23 13:17 20.640 UChloromethane
2.00 0.400 ug/L 01/25/23 13:17 20.400 Ucis-1,2-Dichloroethene
10.0 1.00 ug/L 01/25/23 13:17 21.00 Ucis-1,3-Dichloropropene
2.00 0.480 ug/L 01/25/23 13:17 20.480 UDibromochloromethane
2.00 1.70 ug/L 01/25/23 13:17 21.70 UDichlorodifluoromethane
2.00 0.400 ug/L 01/25/23 13:17 22.39Diisopropyl ether
200 48.0 ug/L 01/25/23 13:17 248.0 UEthanol
2.00 1.00 ug/L 01/25/23 13:17 21.00 UEthylbenzene
2.00 1.06 ug/L 01/25/23 13:17 210.0Isopropylbenzene
2.00 0.440 ug/L 01/25/23 13:17 20.818 JMethyl tert-butyl ether
10.0 6.00 ug/L 01/25/23 13:17 26.00 UMethylene Chloride
10.0 1.26 ug/L 01/25/23 13:17 26.06 Jm-Xylene & p-Xylene
10.0 6.00 ug/L 01/25/23 13:17 26.00 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-9Client Sample ID: MW11
Matrix: WaterDate Collected: 01/18/23 12:08
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
1.52 U 2.00 1.52 ug/L 01/25/23 13:17 2
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
2.00 1.38 ug/L 01/25/23 13:17 21.38 UN-Propylbenzene
10.0 1.20 ug/L 01/25/23 13:17 213.3o-Xylene
2.00 1.42 ug/L 01/25/23 13:17 21.42 Up-Cymene (p-Isopropyltoluene)
2.00 1.40 ug/L 01/25/23 13:17 21.40 Usec-Butylbenzene
2.00 2.00 ug/L 01/25/23 13:17 22.00 UStyrene
2.00 1.26 ug/L 01/25/23 13:17 21.26 Utert-Butylbenzene
2.00 1.80 ug/L 01/25/23 13:17 21.80 UTetrachloroethene
2.00 0.820 ug/L 01/25/23 13:17 20.820 UToluene
2.00 1.00 ug/L 01/25/23 13:17 21.00 Utrans-1,2-Dichloroethene
10.0 0.400 ug/L 01/25/23 13:17 20.400 Utrans-1,3-Dichloropropene
2.00 0.300 ug/L 01/25/23 13:17 20.300 U *+Trichloroethene
2.00 1.04 ug/L 01/25/23 13:17 21.04 U *+Trichlorofluoromethane
50.0 1.86 ug/L 01/25/23 13:17 21.86 UVinyl acetate
2.00 1.00 ug/L 01/25/23 13:17 21.00 U *+Vinyl chloride
20.0 3.20 ug/L 01/25/23 13:17 219.4 JXylenes, Total
4-Bromofluorobenzene 87 72-119 01/25/23 13:17 2
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 110 01/25/23 13:17 275-126
Toluene-d8 (Surr)93 01/25/23 13:17 264-132
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-10Client Sample ID: MW13
Matrix: WaterDate Collected: 01/18/23 12:01
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.800 U 5.00 0.800 ug/L 01/25/23 13:37 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
5.00 0.900 ug/L 01/25/23 13:37 50.900 U1,1,1-Trichloroethane
5.00 2.50 ug/L 01/25/23 13:37 52.50 U1,1,2,2-Tetrachloroethane
25.0 1.05 ug/L 01/25/23 13:37 51.05 U1,1,2-Trichloroethane
5.00 2.50 ug/L 01/25/23 13:37 52.50 U1,1-Dichloroethane
5.00 2.50 ug/L 01/25/23 13:37 52.50 U1,1-Dichloroethene
5.00 2.50 ug/L 01/25/23 13:37 52.50 U1,1-Dichloropropene
5.00 4.50 ug/L 01/25/23 13:37 54.50 U1,2,3-Trichlorobenzene
25.0 4.20 ug/L 01/25/23 13:37 54.20 U1,2,3-Trichloropropane
5.00 4.10 ug/L 01/25/23 13:37 54.10 U1,2,4-Trichlorobenzene
5.00 4.10 ug/L 01/25/23 13:37 518.81,2,4-Trimethylbenzene
5.00 1.15 ug/L 01/25/23 13:37 51.15 U1,2-Dibromoethane (EDB)
5.00 2.50 ug/L 01/25/23 13:37 52.50 U1,2-Dichlorobenzene
5.00 0.950 ug/L 01/25/23 13:37 50.950 U1,2-Dichloroethane
5.00 2.50 ug/L 01/25/23 13:37 52.50 U1,2-Dichloropropane
5.00 2.80 ug/L 01/25/23 13:37 511.01,3,5-Trimethylbenzene
5.00 2.70 ug/L 01/25/23 13:37 52.70 U1,3-Dichlorobenzene
5.00 2.50 ug/L 01/25/23 13:37 52.50 U1,3-Dichloropropane
5.00 3.20 ug/L 01/25/23 13:37 53.20 U1,4-Dichlorobenzene
5.00 2.50 ug/L 01/25/23 13:37 52.50 U2,2-Dichloropropane
125 13.0 ug/L 01/25/23 13:37 513.0 U2-Butanone (MEK)
5.00 2.85 ug/L 01/25/23 13:37 52.85 U2-Chlorotoluene
125 7.00 ug/L 01/25/23 13:37 57.00 U2-Hexanone
5.00 2.80 ug/L 01/25/23 13:37 52.80 U4-Chlorotoluene
125 9.00 ug/L 01/25/23 13:37 59.00 U4-Methyl-2-pentanone (MIBK)
125 50.0 ug/L 01/25/23 13:37 550.0 UAcetone
5.00 0.650 ug/L 01/25/23 13:37 5504Benzene
5.00 2.70 ug/L 01/25/23 13:37 52.70 UBromobenzene
5.00 1.05 ug/L 01/25/23 13:37 51.05 U *+Bromochloromethane
5.00 2.50 ug/L 01/25/23 13:37 52.50 UBromodichloromethane
25.0 1.25 ug/L 01/25/23 13:37 51.25 UBromoform
5.00 4.90 ug/L 01/25/23 13:37 54.90 U *+Bromomethane
5.00 0.950 ug/L 01/25/23 13:37 50.950 UCarbon tetrachloride
5.00 0.750 ug/L 01/25/23 13:37 50.750 UChlorobenzene
5.00 3.80 ug/L 01/25/23 13:37 53.80 UChloroethane
5.00 5.00 ug/L 01/25/23 13:37 55.00 UChloroform
5.00 1.60 ug/L 01/25/23 13:37 51.60 UChloromethane
5.00 1.00 ug/L 01/25/23 13:37 51.00 Ucis-1,2-Dichloroethene
25.0 2.50 ug/L 01/25/23 13:37 52.50 Ucis-1,3-Dichloropropene
5.00 1.20 ug/L 01/25/23 13:37 51.20 UDibromochloromethane
5.00 4.25 ug/L 01/25/23 13:37 54.25 UDichlorodifluoromethane
5.00 1.00 ug/L 01/25/23 13:37 55.94Diisopropyl ether
500 120 ug/L 01/25/23 13:37 5120UEthanol
5.00 2.50 ug/L 01/25/23 13:37 55.17Ethylbenzene
5.00 2.65 ug/L 01/25/23 13:37 522.8Isopropylbenzene
5.00 1.10 ug/L 01/25/23 13:37 59.01Methyl tert-butyl ether
25.0 15.0 ug/L 01/25/23 13:37 515.0 UMethylene Chloride
25.0 3.15 ug/L 01/25/23 13:37 595.8m-Xylene & p-Xylene
25.0 15.0 ug/L 01/25/23 13:37 515.0 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-10Client Sample ID: MW13
Matrix: WaterDate Collected: 01/18/23 12:01
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
3.80 U 5.00 3.80 ug/L 01/25/23 13:37 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
5.00 3.45 ug/L 01/25/23 13:37 53.45 UN-Propylbenzene
25.0 3.00 ug/L 01/25/23 13:37 554.9o-Xylene
5.00 3.55 ug/L 01/25/23 13:37 53.55 Up-Cymene (p-Isopropyltoluene)
5.00 3.50 ug/L 01/25/23 13:37 53.50 Usec-Butylbenzene
5.00 5.00 ug/L 01/25/23 13:37 55.00 UStyrene
5.00 3.15 ug/L 01/25/23 13:37 53.15 Utert-Butylbenzene
5.00 4.50 ug/L 01/25/23 13:37 54.50 UTetrachloroethene
5.00 2.05 ug/L 01/25/23 13:37 55.29Toluene
5.00 2.50 ug/L 01/25/23 13:37 52.50 Utrans-1,2-Dichloroethene
25.0 1.00 ug/L 01/25/23 13:37 51.00 Utrans-1,3-Dichloropropene
5.00 0.750 ug/L 01/25/23 13:37 50.750 U *+Trichloroethene
5.00 2.60 ug/L 01/25/23 13:37 52.60 U *+Trichlorofluoromethane
125 4.65 ug/L 01/25/23 13:37 54.65 UVinyl acetate
5.00 2.50 ug/L 01/25/23 13:37 52.50 U *+Vinyl chloride
50.0 8.00 ug/L 01/25/23 13:37 5151Xylenes, Total
4-Bromofluorobenzene 91 72-119 01/25/23 13:37 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 114 01/25/23 13:37 575-126
Toluene-d8 (Surr)91 01/25/23 13:37 564-132
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-11Client Sample ID: MW14
Matrix: WaterDate Collected: 01/18/23 11:50
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 18:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 18:10 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 18:10 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 18:10 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 18:10 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 18:10 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 18:10 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 18:10 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 18:10 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 18:10 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 18:10 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 18:10 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 18:10 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 18:10 10.313 J1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 18:10 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 18:10 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 18:10 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 18:10 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 18:10 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 18:10 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 18:10 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 18:10 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 18:10 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 18:10 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 18:10 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 18:10 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 18:10 10.130 UBenzene
1.00 0.540 ug/L 01/25/23 18:10 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 18:10 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 18:10 10.500 UBromodichloromethane
5.00 0.250 ug/L 01/25/23 18:10 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 18:10 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 18:10 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 18:10 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 18:10 10.760 UChloroethane
1.00 1.00 ug/L 01/25/23 18:10 11.00 UChloroform
1.00 0.320 ug/L 01/25/23 18:10 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 18:10 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 18:10 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 18:10 10.240 UDibromochloromethane
1.00 0.850 ug/L 01/25/23 18:10 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 18:10 10.200 UDiisopropyl ether
100 24.0 ug/L 01/25/23 18:10 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 18:10 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 18:10 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 18:10 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 18:10 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 18:10 10.630 Um-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 18:10 13.00 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-11Client Sample ID: MW14
Matrix: WaterDate Collected: 01/18/23 11:50
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 18:10 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 18:10 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 18:10 10.600 Uo-Xylene
1.00 0.710 ug/L 01/25/23 18:10 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 18:10 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 18:10 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 18:10 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 18:10 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 18:10 10.410 UToluene
1.00 0.500 ug/L 01/25/23 18:10 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 18:10 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 18:10 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 18:10 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 18:10 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 18:10 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 18:10 11.60 UXylenes, Total
4-Bromofluorobenzene 84 72-119 01/25/23 18:10 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 111 01/25/23 18:10 175-126
Toluene-d8 (Surr)94 01/25/23 18:10 164-132
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-12Client Sample ID: WSW1
Matrix: WaterDate Collected: 01/18/23 12:30
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 18:31 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 18:31 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 18:31 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 18:31 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 18:31 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 18:31 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 18:31 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 18:31 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 18:31 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 18:31 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 18:31 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 18:31 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 18:31 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 18:31 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 18:31 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 18:31 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 18:31 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 18:31 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 18:31 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 18:31 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 18:31 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 18:31 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 18:31 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 18:31 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 18:31 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 18:31 10.130 UBenzene
1.00 0.540 ug/L 01/25/23 18:31 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 18:31 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 18:31 13.47Bromodichloromethane
5.00 0.250 ug/L 01/25/23 18:31 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 18:31 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 18:31 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 18:31 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 18:31 10.760 UChloroethane
1.00 1.00 ug/L 01/26/23 15:48 114.4Chloroform
1.00 0.320 ug/L 01/25/23 18:31 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 18:31 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 18:31 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 18:31 10.438 JDibromochloromethane
1.00 0.850 ug/L 01/25/23 18:31 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 18:31 10.200 UDiisopropyl ether
100 24.0 ug/L 01/25/23 18:31 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 18:31 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 18:31 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 18:31 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 18:31 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 18:31 10.630 Um-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 18:31 13.00 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-12Client Sample ID: WSW1
Matrix: WaterDate Collected: 01/18/23 12:30
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 18:31 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 18:31 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 18:31 10.600 Uo-Xylene
1.00 0.710 ug/L 01/25/23 18:31 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 18:31 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 18:31 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 18:31 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 18:31 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 18:31 10.410 UToluene
1.00 0.500 ug/L 01/25/23 18:31 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 18:31 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 18:31 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 18:31 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 18:31 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 18:31 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 18:31 11.60 UXylenes, Total
4-Bromofluorobenzene 83 72-119 01/25/23 18:31 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
4-Bromofluorobenzene 99 01/26/23 15:48 172-119
Dibromofluoromethane 111 01/25/23 18:31 175-126
Dibromofluoromethane 101 01/26/23 15:48 175-126
Toluene-d8 (Surr)93 01/25/23 18:31 164-132
Toluene-d8 (Surr)94 01/26/23 15:48 164-132
Method: EPA-DW 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
0.0151 U 0.0201 0.0151 ug/L 02/01/23 09:49 02/01/23 19:21 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dibromoethane (EDB)
4-Bromofluorobenzene 102 56-150 02/01/23 09:49 02/01/23 19:21 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-13Client Sample ID: WSW2
Matrix: WaterDate Collected: 01/18/23 12:55
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 18:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 18:52 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 18:52 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 18:52 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 18:52 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 18:52 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 18:52 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 18:52 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 18:52 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 18:52 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 18:52 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 18:52 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 18:52 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 18:52 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 18:52 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 18:52 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 18:52 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 18:52 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 18:52 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 18:52 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 18:52 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 18:52 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 18:52 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 18:52 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 18:52 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 18:52 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 18:52 10.130 UBenzene
1.00 0.540 ug/L 01/25/23 18:52 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 18:52 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 18:52 10.500 UBromodichloromethane
5.00 0.250 ug/L 01/25/23 18:52 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 18:52 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 18:52 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 18:52 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 18:52 10.760 UChloroethane
1.00 1.00 ug/L 01/25/23 18:52 11.00 UChloroform
1.00 0.320 ug/L 01/25/23 18:52 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 18:52 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 18:52 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 18:52 10.240 UDibromochloromethane
1.00 0.850 ug/L 01/25/23 18:52 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 18:52 10.200 UDiisopropyl ether
100 24.0 ug/L 01/25/23 18:52 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 18:52 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 18:52 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 18:52 10.231 JMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 18:52 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 18:52 10.630 Um-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 18:52 13.00 UNaphthalene
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-13Client Sample ID: WSW2
Matrix: WaterDate Collected: 01/18/23 12:55
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 18:52 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 18:52 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 18:52 10.600 Uo-Xylene
1.00 0.710 ug/L 01/25/23 18:52 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 18:52 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 18:52 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 18:52 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 18:52 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 18:52 10.410 UToluene
1.00 0.500 ug/L 01/25/23 18:52 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 18:52 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 18:52 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 18:52 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 18:52 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 18:52 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 18:52 11.60 UXylenes, Total
4-Bromofluorobenzene 86 72-119 01/25/23 18:52 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 114 01/25/23 18:52 175-126
Toluene-d8 (Surr)95 01/25/23 18:52 164-132
Method: EPA-DW 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
0.0151 U 0.0202 0.0151 ug/L 02/01/23 09:49 02/01/23 19:42 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dibromoethane (EDB)
4-Bromofluorobenzene 109 56-150 02/01/23 09:49 02/01/23 19:42 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Eurofins Pensacola
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-14Client Sample ID: WSW4
Matrix: WaterDate Collected: 01/18/23 13:16
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.160 U 1.00 0.160 ug/L 01/25/23 19:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
1.00 0.180 ug/L 01/25/23 19:13 10.180 U1,1,1-Trichloroethane
1.00 0.500 ug/L 01/25/23 19:13 10.500 U1,1,2,2-Tetrachloroethane
5.00 0.210 ug/L 01/25/23 19:13 10.210 U1,1,2-Trichloroethane
1.00 0.500 ug/L 01/25/23 19:13 10.500 U1,1-Dichloroethane
1.00 0.500 ug/L 01/25/23 19:13 10.500 U1,1-Dichloroethene
1.00 0.500 ug/L 01/25/23 19:13 10.500 U1,1-Dichloropropene
1.00 0.900 ug/L 01/25/23 19:13 10.900 U1,2,3-Trichlorobenzene
5.00 0.840 ug/L 01/25/23 19:13 10.840 U1,2,3-Trichloropropane
1.00 0.820 ug/L 01/25/23 19:13 10.820 U1,2,4-Trichlorobenzene
1.00 0.820 ug/L 01/25/23 19:13 10.820 U1,2,4-Trimethylbenzene
1.00 0.230 ug/L 01/25/23 19:13 10.230 U1,2-Dibromoethane (EDB)
1.00 0.500 ug/L 01/25/23 19:13 10.500 U1,2-Dichlorobenzene
1.00 0.190 ug/L 01/25/23 19:13 10.190 U1,2-Dichloroethane
1.00 0.500 ug/L 01/25/23 19:13 10.500 U1,2-Dichloropropane
1.00 0.560 ug/L 01/25/23 19:13 10.560 U1,3,5-Trimethylbenzene
1.00 0.540 ug/L 01/25/23 19:13 10.540 U1,3-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 19:13 10.500 U1,3-Dichloropropane
1.00 0.640 ug/L 01/25/23 19:13 10.640 U1,4-Dichlorobenzene
1.00 0.500 ug/L 01/25/23 19:13 10.500 U2,2-Dichloropropane
25.0 2.60 ug/L 01/25/23 19:13 12.60 U2-Butanone (MEK)
1.00 0.570 ug/L 01/25/23 19:13 10.570 U2-Chlorotoluene
25.0 1.40 ug/L 01/25/23 19:13 11.40 U2-Hexanone
1.00 0.560 ug/L 01/25/23 19:13 10.560 U4-Chlorotoluene
25.0 1.80 ug/L 01/25/23 19:13 11.80 U4-Methyl-2-pentanone (MIBK)
25.0 10.0 ug/L 01/25/23 19:13 110.0 UAcetone
1.00 0.130 ug/L 01/25/23 19:13 10.130 UBenzene
1.00 0.540 ug/L 01/25/23 19:13 10.540 UBromobenzene
1.00 0.210 ug/L 01/25/23 19:13 10.210 U *+Bromochloromethane
1.00 0.500 ug/L 01/25/23 19:13 10.500 UBromodichloromethane
5.00 0.250 ug/L 01/25/23 19:13 10.250 UBromoform
1.00 0.980 ug/L 01/25/23 19:13 10.980 U *+Bromomethane
1.00 0.190 ug/L 01/25/23 19:13 10.190 UCarbon tetrachloride
1.00 0.150 ug/L 01/25/23 19:13 10.150 UChlorobenzene
1.00 0.760 ug/L 01/25/23 19:13 10.760 UChloroethane
1.00 1.00 ug/L 01/25/23 19:13 11.00 UChloroform
1.00 0.320 ug/L 01/25/23 19:13 10.320 UChloromethane
1.00 0.200 ug/L 01/25/23 19:13 10.200 Ucis-1,2-Dichloroethene
5.00 0.500 ug/L 01/25/23 19:13 10.500 Ucis-1,3-Dichloropropene
1.00 0.240 ug/L 01/25/23 19:13 10.240 UDibromochloromethane
1.00 0.850 ug/L 01/25/23 19:13 10.850 UDichlorodifluoromethane
1.00 0.200 ug/L 01/25/23 19:13 10.200 UDiisopropyl ether
100 24.0 ug/L 01/25/23 19:13 124.0 UEthanol
1.00 0.500 ug/L 01/25/23 19:13 10.500 UEthylbenzene
1.00 0.530 ug/L 01/25/23 19:13 10.530 UIsopropylbenzene
1.00 0.220 ug/L 01/25/23 19:13 10.220 UMethyl tert-butyl ether
5.00 3.00 ug/L 01/25/23 19:13 13.00 UMethylene Chloride
5.00 0.630 ug/L 01/25/23 19:13 10.630 Um-Xylene & p-Xylene
5.00 3.00 ug/L 01/25/23 19:13 13.00 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232047-14Client Sample ID: WSW4
Matrix: WaterDate Collected: 01/18/23 13:16
Date Received: 01/20/23 09:04
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
0.760 U 1.00 0.760 ug/L 01/25/23 19:13 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
1.00 0.690 ug/L 01/25/23 19:13 10.690 UN-Propylbenzene
5.00 0.600 ug/L 01/25/23 19:13 10.600 Uo-Xylene
1.00 0.710 ug/L 01/25/23 19:13 10.710 Up-Cymene (p-Isopropyltoluene)
1.00 0.700 ug/L 01/25/23 19:13 10.700 Usec-Butylbenzene
1.00 1.00 ug/L 01/25/23 19:13 11.00 UStyrene
1.00 0.630 ug/L 01/25/23 19:13 10.630 Utert-Butylbenzene
1.00 0.900 ug/L 01/25/23 19:13 10.900 UTetrachloroethene
1.00 0.410 ug/L 01/25/23 19:13 10.410 UToluene
1.00 0.500 ug/L 01/25/23 19:13 10.500 Utrans-1,2-Dichloroethene
5.00 0.200 ug/L 01/25/23 19:13 10.200 Utrans-1,3-Dichloropropene
1.00 0.150 ug/L 01/25/23 19:13 10.150 U *+Trichloroethene
1.00 0.520 ug/L 01/25/23 19:13 10.520 U *+Trichlorofluoromethane
25.0 0.930 ug/L 01/25/23 19:13 10.930 UVinyl acetate
1.00 0.500 ug/L 01/25/23 19:13 10.500 U *+Vinyl chloride
10.0 1.60 ug/L 01/25/23 19:13 11.60 UXylenes, Total
4-Bromofluorobenzene 85 72-119 01/25/23 19:13 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 115 01/25/23 19:13 175-126
Toluene-d8 (Surr)95 01/25/23 19:13 164-132
Method: EPA-DW 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
RL MDL
0.0152 U 0.0202 0.0152 ug/L 02/01/23 09:49 02/01/23 20:02 1
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,2-Dibromoethane (EDB)
4-Bromofluorobenzene 110 56-150 02/01/23 09:49 02/01/23 20:02 1
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232072-1Client Sample ID: MW12
Matrix: WaterDate Collected: 01/20/23 12:00
Date Received: 01/21/23 09:23
Method: SM6200-B - Volatile Organic Compounds
RL MDL
0.800 U 5.00 0.800 ug/L 01/25/23 16:26 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
1,1,1,2-Tetrachloroethane
5.00 0.900 ug/L 01/25/23 16:26 50.900 U1,1,1-Trichloroethane
5.00 2.50 ug/L 01/25/23 16:26 52.50 U1,1,2,2-Tetrachloroethane
25.0 1.05 ug/L 01/25/23 16:26 51.05 U1,1,2-Trichloroethane
5.00 2.50 ug/L 01/25/23 16:26 52.50 U1,1-Dichloroethane
5.00 2.50 ug/L 01/25/23 16:26 52.50 U1,1-Dichloroethene
5.00 2.50 ug/L 01/25/23 16:26 52.50 U1,1-Dichloropropene
5.00 4.50 ug/L 01/25/23 16:26 54.50 U1,2,3-Trichlorobenzene
25.0 4.20 ug/L 01/25/23 16:26 54.20 U1,2,3-Trichloropropane
5.00 4.10 ug/L 01/25/23 16:26 54.10 U1,2,4-Trichlorobenzene
5.00 4.10 ug/L 01/25/23 16:26 55.851,2,4-Trimethylbenzene
5.00 1.15 ug/L 01/25/23 16:26 51.15 U1,2-Dibromoethane (EDB)
5.00 2.50 ug/L 01/25/23 16:26 52.50 U1,2-Dichlorobenzene
5.00 0.950 ug/L 01/25/23 16:26 50.950 U1,2-Dichloroethane
5.00 2.50 ug/L 01/25/23 16:26 52.50 U1,2-Dichloropropane
5.00 2.80 ug/L 01/25/23 16:26 52.80 U1,3,5-Trimethylbenzene
5.00 2.70 ug/L 01/25/23 16:26 52.70 U1,3-Dichlorobenzene
5.00 2.50 ug/L 01/25/23 16:26 52.50 U1,3-Dichloropropane
5.00 3.20 ug/L 01/25/23 16:26 53.20 U1,4-Dichlorobenzene
5.00 2.50 ug/L 01/25/23 16:26 52.50 U2,2-Dichloropropane
125 13.0 ug/L 01/25/23 16:26 513.0 U2-Butanone (MEK)
5.00 2.85 ug/L 01/25/23 16:26 52.85 U2-Chlorotoluene
125 7.00 ug/L 01/25/23 16:26 57.00 U2-Hexanone
5.00 2.80 ug/L 01/25/23 16:26 52.80 U4-Chlorotoluene
125 9.00 ug/L 01/25/23 16:26 59.00 U4-Methyl-2-pentanone (MIBK)
125 50.0 ug/L 01/25/23 16:26 550.0 UAcetone
5.00 0.650 ug/L 01/25/23 16:26 5313Benzene
5.00 2.70 ug/L 01/25/23 16:26 52.70 UBromobenzene
5.00 1.05 ug/L 01/25/23 16:26 51.05 UBromochloromethane
5.00 2.50 ug/L 01/25/23 16:26 52.50 UBromodichloromethane
25.0 1.25 ug/L 01/25/23 16:26 51.25 UBromoform
5.00 4.90 ug/L 01/25/23 16:26 54.90 UBromomethane
5.00 0.950 ug/L 01/25/23 16:26 50.950 UCarbon tetrachloride
5.00 0.750 ug/L 01/25/23 16:26 50.750 UChlorobenzene
5.00 3.80 ug/L 01/25/23 16:26 53.80 UChloroethane
5.00 5.00 ug/L 01/25/23 16:26 55.00 UChloroform
5.00 1.60 ug/L 01/25/23 16:26 51.60 UChloromethane
5.00 1.00 ug/L 01/25/23 16:26 51.00 Ucis-1,2-Dichloroethene
25.0 2.50 ug/L 01/25/23 16:26 52.50 Ucis-1,3-Dichloropropene
5.00 1.20 ug/L 01/25/23 16:26 51.20 UDibromochloromethane
5.00 4.25 ug/L 01/25/23 16:26 54.25 UDichlorodifluoromethane
5.00 1.00 ug/L 01/25/23 16:26 51.43 JDiisopropyl ether
500 120 ug/L 01/25/23 16:26 5120UEthanol
5.00 2.50 ug/L 01/25/23 16:26 56.80Ethylbenzene
5.00 2.65 ug/L 01/25/23 16:26 52.65 UIsopropylbenzene
5.00 1.10 ug/L 01/25/23 16:26 54.37 JMethyl tert-butyl ether
25.0 15.0 ug/L 01/25/23 16:26 515.0 UMethylene Chloride
25.0 3.15 ug/L 01/25/23 16:26 518.0 Jm-Xylene & p-Xylene
25.0 15.0 ug/L 01/25/23 16:26 515.0 UNaphthalene
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Client Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Lab Sample ID: 400-232072-1Client Sample ID: MW12
Matrix: WaterDate Collected: 01/20/23 12:00
Date Received: 01/21/23 09:23
Method: SM6200-B - Volatile Organic Compounds (Continued)
RL MDL
3.80 U 5.00 3.80 ug/L 01/25/23 16:26 5
Analyte Dil FacAnalyzedPreparedUnitDResultQualifier
n-Butylbenzene
5.00 3.45 ug/L 01/25/23 16:26 53.45 UN-Propylbenzene
25.0 3.00 ug/L 01/25/23 16:26 511.2 Jo-Xylene
5.00 3.55 ug/L 01/25/23 16:26 53.55 Up-Cymene (p-Isopropyltoluene)
5.00 3.50 ug/L 01/25/23 16:26 53.50 Usec-Butylbenzene
5.00 5.00 ug/L 01/25/23 16:26 55.00 UStyrene
5.00 3.15 ug/L 01/25/23 16:26 53.15 Utert-Butylbenzene
5.00 4.50 ug/L 01/25/23 16:26 54.50 UTetrachloroethene
5.00 2.05 ug/L 01/25/23 16:26 52.05 UToluene
5.00 2.50 ug/L 01/25/23 16:26 52.50 Utrans-1,2-Dichloroethene
25.0 1.00 ug/L 01/25/23 16:26 51.00 Utrans-1,3-Dichloropropene
5.00 0.750 ug/L 01/25/23 16:26 50.750 UTrichloroethene
5.00 2.60 ug/L 01/25/23 16:26 52.60 UTrichlorofluoromethane
125 4.65 ug/L 01/25/23 16:26 54.65 UVinyl acetate
5.00 2.50 ug/L 01/25/23 16:26 52.50 UVinyl chloride
50.0 8.00 ug/L 01/25/23 16:26 529.2 JXylenes, Total
4-Bromofluorobenzene 101 72-119 01/25/23 16:26 5
Surrogate Dil FacAnalyzedPreparedQualifierLimits%Recovery
Dibromofluoromethane 100 01/25/23 16:26 575-126
Toluene-d8 (Surr)95 01/25/23 16:26 564-132
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Definitions/Glossary
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Qualifiers
GC/MS VOA
Qualifier Description
*+LCS and/or LCSD is outside acceptance limits, high biased.
Qualifier
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
U Indicates the analyte was analyzed for but not detected.
GC Semi VOA
Qualifier Description
U Indicates the analyte was analyzed for but not detected.
Qualifier
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
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Surrogate Summary
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (72-119)(75-126)(64-132)
BFB DBFM TOL
88 109 96400-232047-1
Percent Surrogate Recovery (Acceptance Limits)
MW1
100 102 95400-232047-1 MW1
87 109 95400-232047-2 MW4
97 98 95400-232047-2 MW4
89 112 93400-232047-3 MW5
87 113 95400-232047-4 MW6
99 99 96400-232047-4 MW6
86 111 92400-232047-5 MW7
89 110 92400-232047-6 MW8
87 114 94400-232047-7 MW9
88 112 89400-232047-8 MW10
87 110 93400-232047-9 MW11
91 114 91400-232047-10 MW13
84 111 94400-232047-11 MW14
83 111 93400-232047-12 WSW1
99 101 94400-232047-12 WSW1
86 114 95400-232047-13 WSW2
85 115 95400-232047-14 WSW4
101 100 95400-232072-1 MW12
97 99 96LCS 400-609770/1002 Lab Control Sample
83 109 87LCS 400-609802/1002 Lab Control Sample
97 98 96LCS 400-610024/1002 Lab Control Sample
100 98 94MB 400-609770/4 Method Blank
87 114 95MB 400-609802/4 Method Blank
101 101 94MB 400-610024/6 Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
DBFM = Dibromofluoromethane
TOL = Toluene-d8 (Surr)
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (56-150)
BFB1
102400-232047-12
Percent Surrogate Recovery (Acceptance Limits)
WSW1
109400-232047-13 WSW2
110400-232047-14 WSW4
122LCS 400-610674/2-A Lab Control Sample
122LCSD 400-610674/3-A Lab Control Sample Dup
112MB 400-610674/1-A Method Blank
Surrogate Legend
BFB = 4-Bromofluorobenzene
Eurofins Pensacola
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QC Association Summary
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
GC/MS VOA
Analysis Batch: 609770
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B400-232072-1 MW12 Total/NA
Water SM6200-BMB 400-609770/4 Method Blank Total/NA
Water SM6200-BLCS 400-609770/1002 Lab Control Sample Total/NA
Analysis Batch: 609802
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B400-232047-1 MW1 Total/NA
Water SM6200-B400-232047-2 MW4 Total/NA
Water SM6200-B400-232047-3 MW5 Total/NA
Water SM6200-B400-232047-4 MW6 Total/NA
Water SM6200-B400-232047-5 MW7 Total/NA
Water SM6200-B400-232047-6 MW8 Total/NA
Water SM6200-B400-232047-7 MW9 Total/NA
Water SM6200-B400-232047-8 MW10 Total/NA
Water SM6200-B400-232047-9 MW11 Total/NA
Water SM6200-B400-232047-10 MW13 Total/NA
Water SM6200-B400-232047-11 MW14 Total/NA
Water SM6200-B400-232047-12 WSW1 Total/NA
Water SM6200-B400-232047-13 WSW2 Total/NA
Water SM6200-B400-232047-14 WSW4 Total/NA
Water SM6200-BMB 400-609802/4 Method Blank Total/NA
Water SM6200-BLCS 400-609802/1002 Lab Control Sample Total/NA
Analysis Batch: 610024
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM6200-B400-232047-1 MW1 Total/NA
Water SM6200-B400-232047-2 MW4 Total/NA
Water SM6200-B400-232047-4 MW6 Total/NA
Water SM6200-B400-232047-12 WSW1 Total/NA
Water SM6200-BMB 400-610024/6 Method Blank Total/NA
Water SM6200-BLCS 400-610024/1002 Lab Control Sample Total/NA
GC Semi VOA
Prep Batch: 610674
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 504.1400-232047-12 WSW1 Total/NA
Water 504.1400-232047-13 WSW2 Total/NA
Water 504.1400-232047-14 WSW4 Total/NA
Water 504.1MB 400-610674/1-A Method Blank Total/NA
Water 504.1LCS 400-610674/2-A Lab Control Sample Total/NA
Water 504.1LCSD 400-610674/3-A Lab Control Sample Dup Total/NA
Analysis Batch: 610718
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 504.1 610674400-232047-12 WSW1 Total/NA
Water 504.1 610674400-232047-13 WSW2 Total/NA
Water 504.1 610674400-232047-14 WSW4 Total/NA
Water 504.1 610674MB 400-610674/1-A Method Blank Total/NA
Water 504.1 610674LCS 400-610674/2-A Lab Control Sample Total/NA
Water 504.1 610674LCSD 400-610674/3-A Lab Control Sample Dup Total/NA
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds
Client Sample ID: Method BlankLab Sample ID: MB 400-609770/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609770
RL MDL
1,1,1,2-Tetrachloroethane 0.160 U 1.00 0.160 ug/L 01/25/23 10:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.180 U 0.1801.00 ug/L 01/25/23 10:41 11,1,1-Trichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 10:41 11,1,2,2-Tetrachloroethane
0.210 U 0.2105.00 ug/L 01/25/23 10:41 11,1,2-Trichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 10:41 11,1-Dichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 10:41 11,1-Dichloroethene
0.500 U 0.5001.00 ug/L 01/25/23 10:41 11,1-Dichloropropene
0.900 U 0.9001.00 ug/L 01/25/23 10:41 11,2,3-Trichlorobenzene
0.840 U 0.8405.00 ug/L 01/25/23 10:41 11,2,3-Trichloropropane
0.820 U 0.8201.00 ug/L 01/25/23 10:41 11,2,4-Trichlorobenzene
0.820 U 0.8201.00 ug/L 01/25/23 10:41 11,2,4-Trimethylbenzene
0.230 U 0.2301.00 ug/L 01/25/23 10:41 11,2-Dibromoethane (EDB)
0.500 U 0.5001.00 ug/L 01/25/23 10:41 11,2-Dichlorobenzene
0.190 U 0.1901.00 ug/L 01/25/23 10:41 11,2-Dichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 10:41 11,2-Dichloropropane
0.560 U 0.5601.00 ug/L 01/25/23 10:41 11,3,5-Trimethylbenzene
0.540 U 0.5401.00 ug/L 01/25/23 10:41 11,3-Dichlorobenzene
0.500 U 0.5001.00 ug/L 01/25/23 10:41 11,3-Dichloropropane
0.640 U 0.6401.00 ug/L 01/25/23 10:41 11,4-Dichlorobenzene
0.500 U 0.5001.00 ug/L 01/25/23 10:41 12,2-Dichloropropane
2.60 U 2.6025.0 ug/L 01/25/23 10:41 12-Butanone (MEK)
0.570 U 0.5701.00 ug/L 01/25/23 10:41 12-Chlorotoluene
1.40 U 1.4025.0 ug/L 01/25/23 10:41 12-Hexanone
0.560 U 0.5601.00 ug/L 01/25/23 10:41 14-Chlorotoluene
1.80 U 1.8025.0 ug/L 01/25/23 10:41 14-Methyl-2-pentanone (MIBK)
10.0 U 10.025.0 ug/L 01/25/23 10:41 1Acetone
0.130 U 0.1301.00 ug/L 01/25/23 10:41 1Benzene
0.540 U 0.5401.00 ug/L 01/25/23 10:41 1Bromobenzene
0.210 U 0.2101.00 ug/L 01/25/23 10:41 1Bromochloromethane
0.500 U 0.5001.00 ug/L 01/25/23 10:41 1Bromodichloromethane
0.250 U 0.2505.00 ug/L 01/25/23 10:41 1Bromoform
0.980 U 0.9801.00 ug/L 01/25/23 10:41 1Bromomethane
0.190 U 0.1901.00 ug/L 01/25/23 10:41 1Carbon tetrachloride
0.150 U 0.1501.00 ug/L 01/25/23 10:41 1Chlorobenzene
0.760 U 0.7601.00 ug/L 01/25/23 10:41 1Chloroethane
1.00 U 1.001.00 ug/L 01/25/23 10:41 1Chloroform
0.320 U 0.3201.00 ug/L 01/25/23 10:41 1Chloromethane
0.200 U 0.2001.00 ug/L 01/25/23 10:41 1cis-1,2-Dichloroethene
0.500 U 0.5005.00 ug/L 01/25/23 10:41 1cis-1,3-Dichloropropene
0.240 U 0.2401.00 ug/L 01/25/23 10:41 1Dibromochloromethane
0.850 U 0.8501.00 ug/L 01/25/23 10:41 1Dichlorodifluoromethane
0.200 U 0.2001.00 ug/L 01/25/23 10:41 1Diisopropyl ether
24.0 U 24.0100 ug/L 01/25/23 10:41 1Ethanol
0.500 U 0.5001.00 ug/L 01/25/23 10:41 1Ethylbenzene
0.530 U 0.5301.00 ug/L 01/25/23 10:41 1Isopropylbenzene
0.220 U 0.2201.00 ug/L 01/25/23 10:41 1Methyl tert-butyl ether
3.00 U 3.005.00 ug/L 01/25/23 10:41 1Methylene Chloride
0.630 U 0.6305.00 ug/L 01/25/23 10:41 1m-Xylene & p-Xylene
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-609770/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609770
RL MDL
Naphthalene 3.00 U 5.00 3.00 ug/L 01/25/23 10:41 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.760 U 0.7601.00 ug/L 01/25/23 10:41 1n-Butylbenzene
0.690 U 0.6901.00 ug/L 01/25/23 10:41 1N-Propylbenzene
0.600 U 0.6005.00 ug/L 01/25/23 10:41 1o-Xylene
0.710 U 0.7101.00 ug/L 01/25/23 10:41 1p-Cymene (p-Isopropyltoluene)
0.700 U 0.7001.00 ug/L 01/25/23 10:41 1sec-Butylbenzene
1.00 U 1.001.00 ug/L 01/25/23 10:41 1Styrene
0.630 U 0.6301.00 ug/L 01/25/23 10:41 1tert-Butylbenzene
0.900 U 0.9001.00 ug/L 01/25/23 10:41 1Tetrachloroethene
0.410 U 0.4101.00 ug/L 01/25/23 10:41 1Toluene
0.500 U 0.5001.00 ug/L 01/25/23 10:41 1trans-1,2-Dichloroethene
0.200 U 0.2005.00 ug/L 01/25/23 10:41 1trans-1,3-Dichloropropene
0.150 U 0.1501.00 ug/L 01/25/23 10:41 1Trichloroethene
0.520 U 0.5201.00 ug/L 01/25/23 10:41 1Trichlorofluoromethane
0.930 U 0.93025.0 ug/L 01/25/23 10:41 1Vinyl acetate
0.500 U 0.5001.00 ug/L 01/25/23 10:41 1Vinyl chloride
1.60 U 1.6010.0 ug/L 01/25/23 10:41 1Xylenes, Total
4-Bromofluorobenzene 100 72-119 01/25/23 10:41 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
98 01/25/23 10:41 1Dibromofluoromethane75-126
94 01/25/23 10:41 1Toluene-d8 (Surr)64-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-609770/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609770
1,1,1,2-Tetrachloroethane 50.0 45.93 ug/L 92 67 -131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 42.84 ug/L 86 68 -130
1,1,2,2-Tetrachloroethane 50.0 46.06 ug/L 92 70 -131
1,1,2-Trichloroethane 50.0 46.52 ug/L 93 70 -130
1,1-Dichloroethane 50.0 45.52 ug/L 91 70 -130
1,1-Dichloroethene 50.0 42.10 ug/L 84 63 -134
1,1-Dichloropropene 50.0 45.54 ug/L 91 70 -130
1,2,3-Trichlorobenzene 50.0 60.19 ug/L 120 60 -138
1,2,3-Trichloropropane 50.0 45.84 ug/L 92 70 -130
1,2,4-Trichlorobenzene 50.0 57.08 ug/L 114 60 -140
1,2,4-Trimethylbenzene 50.0 46.14 ug/L 92 70 -130
1,2-Dibromoethane (EDB)50.0 47.66 ug/L 95 70 -130
1,2-Dichlorobenzene 50.0 49.38 ug/L 99 67 -130
1,2-Dichloroethane 50.0 43.90 ug/L 88 69 -130
1,2-Dichloropropane 50.0 46.77 ug/L 94 70 -130
1,3,5-Trimethylbenzene 50.0 44.48 ug/L 89 69 -130
1,3-Dichlorobenzene 50.0 48.18 ug/L 96 70 -130
1,3-Dichloropropane 50.0 47.88 ug/L 96 70 -130
1,4-Dichlorobenzene 50.0 47.59 ug/L 95 70 -130
2,2-Dichloropropane 50.0 46.18 ug/L 92 52 -135
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-609770/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609770
2-Butanone (MEK)200 183.4 ug/L 92 61 -145
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
2-Chlorotoluene 50.0 43.95 ug/L 88 70 -130
2-Hexanone 200 180.9 ug/L 90 65 -137
4-Chlorotoluene 50.0 44.03 ug/L 88 70 -130
4-Methyl-2-pentanone (MIBK)200 199.1 ug/L 100 69 -138
Acetone 200 186.5 ug/L 93 43 -160
Benzene 50.0 46.31 ug/L 93 70 -130
Bromobenzene 50.0 46.01 ug/L 92 70 -132
Bromochloromethane 50.0 49.79 ug/L 100 70 -130
Bromodichloromethane 50.0 46.64 ug/L 93 67 -133
Bromoform 50.0 46.96 ug/L 94 57 -140
Bromomethane 50.0 46.65 ug/L 93 10 -160
Carbon tetrachloride 50.0 42.24 ug/L 84 61 -137
Chlorobenzene 50.0 46.01 ug/L 92 70 -130
Chloroethane 50.0 41.21 ug/L 82 55 -141
Chloroform 50.0 44.50 ug/L 89 69 -130
Chloromethane 50.0 41.16 ug/L 82 58 -137
cis-1,2-Dichloroethene 50.0 44.31 ug/L 89 68 -130
cis-1,3-Dichloropropene 50.0 50.14 ug/L 100 69 -132
Dibromochloromethane 50.0 46.40 ug/L 93 67 -135
Dichlorodifluoromethane 50.0 42.97 ug/L 86 41 -146
Diisopropyl ether 50.0 47.80 ug/L 96 64 -132
Ethanol 2000 1418 ug/L 71 20 -160
Ethylbenzene 50.0 44.51 ug/L 89 70 -130
Isopropylbenzene 50.0 43.83 ug/L 88 70 -130
Methyl tert-butyl ether 50.0 49.39 ug/L 99 66 -130
Methylene Chloride 50.0 41.68 ug/L 83 66 -135
m-Xylene & p-Xylene 50.0 43.82 ug/L 88 70 -130
Naphthalene 50.0 60.97 ug/L 122 47 -149
n-Butylbenzene 50.0 46.85 ug/L 94 67 -130
N-Propylbenzene 50.0 44.78 ug/L 90 70 -130
o-Xylene 50.0 44.61 ug/L 89 70 -130
p-Cymene (p-Isopropyltoluene)50.0 44.89 ug/L 90 65 -130
sec-Butylbenzene 50.0 44.05 ug/L 88 66 -130
Styrene 50.0 44.81 ug/L 90 70 -130
tert-Butylbenzene 50.0 41.12 ug/L 82 64 -139
Tetrachloroethene 50.0 45.74 ug/L 91 65 -130
Toluene 50.0 43.56 ug/L 87 70 -130
trans-1,2-Dichloroethene 50.0 44.02 ug/L 88 70 -130
trans-1,3-Dichloropropene 50.0 46.63 ug/L 93 63 -130
Trichloroethene 50.0 47.27 ug/L 95 70 -130
Trichlorofluoromethane 50.0 46.07 ug/L 92 65 -138
Vinyl acetate 100 107.2 ug/L 107 26 -160
Vinyl chloride 50.0 47.72 ug/L 95 59 -136
Xylenes, Total 100 88.43 ug/L 88 70 -130
4-Bromofluorobenzene 72 -119
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-609770/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609770
Dibromofluoromethane 75 -126
Surrogate
99
LCS LCS
Qualifier Limits%Recovery
96Toluene-d8 (Surr)64 -132
Client Sample ID: Method BlankLab Sample ID: MB 400-609802/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609802
RL MDL
1,1,1,2-Tetrachloroethane 0.160 U 1.00 0.160 ug/L 01/25/23 12:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.180 U 0.1801.00 ug/L 01/25/23 12:14 11,1,1-Trichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 12:14 11,1,2,2-Tetrachloroethane
0.210 U 0.2105.00 ug/L 01/25/23 12:14 11,1,2-Trichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 12:14 11,1-Dichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 12:14 11,1-Dichloroethene
0.500 U 0.5001.00 ug/L 01/25/23 12:14 11,1-Dichloropropene
0.900 U 0.9001.00 ug/L 01/25/23 12:14 11,2,3-Trichlorobenzene
0.840 U 0.8405.00 ug/L 01/25/23 12:14 11,2,3-Trichloropropane
0.820 U 0.8201.00 ug/L 01/25/23 12:14 11,2,4-Trichlorobenzene
0.820 U 0.8201.00 ug/L 01/25/23 12:14 11,2,4-Trimethylbenzene
0.230 U 0.2301.00 ug/L 01/25/23 12:14 11,2-Dibromoethane (EDB)
0.500 U 0.5001.00 ug/L 01/25/23 12:14 11,2-Dichlorobenzene
0.190 U 0.1901.00 ug/L 01/25/23 12:14 11,2-Dichloroethane
0.500 U 0.5001.00 ug/L 01/25/23 12:14 11,2-Dichloropropane
0.560 U 0.5601.00 ug/L 01/25/23 12:14 11,3,5-Trimethylbenzene
0.540 U 0.5401.00 ug/L 01/25/23 12:14 11,3-Dichlorobenzene
0.500 U 0.5001.00 ug/L 01/25/23 12:14 11,3-Dichloropropane
0.640 U 0.6401.00 ug/L 01/25/23 12:14 11,4-Dichlorobenzene
0.500 U 0.5001.00 ug/L 01/25/23 12:14 12,2-Dichloropropane
2.60 U 2.6025.0 ug/L 01/25/23 12:14 12-Butanone (MEK)
0.570 U 0.5701.00 ug/L 01/25/23 12:14 12-Chlorotoluene
1.40 U 1.4025.0 ug/L 01/25/23 12:14 12-Hexanone
0.560 U 0.5601.00 ug/L 01/25/23 12:14 14-Chlorotoluene
1.80 U 1.8025.0 ug/L 01/25/23 12:14 14-Methyl-2-pentanone (MIBK)
10.0 U 10.025.0 ug/L 01/25/23 12:14 1Acetone
0.130 U 0.1301.00 ug/L 01/25/23 12:14 1Benzene
0.540 U 0.5401.00 ug/L 01/25/23 12:14 1Bromobenzene
0.210 U 0.2101.00 ug/L 01/25/23 12:14 1Bromochloromethane
0.500 U 0.5001.00 ug/L 01/25/23 12:14 1Bromodichloromethane
0.250 U 0.2505.00 ug/L 01/25/23 12:14 1Bromoform
0.980 U 0.9801.00 ug/L 01/25/23 12:14 1Bromomethane
0.190 U 0.1901.00 ug/L 01/25/23 12:14 1Carbon tetrachloride
0.150 U 0.1501.00 ug/L 01/25/23 12:14 1Chlorobenzene
0.760 U 0.7601.00 ug/L 01/25/23 12:14 1Chloroethane
1.00 U 1.001.00 ug/L 01/25/23 12:14 1Chloroform
0.320 U 0.3201.00 ug/L 01/25/23 12:14 1Chloromethane
0.200 U 0.2001.00 ug/L 01/25/23 12:14 1cis-1,2-Dichloroethene
0.500 U 0.5005.00 ug/L 01/25/23 12:14 1cis-1,3-Dichloropropene
0.240 U 0.2401.00 ug/L 01/25/23 12:14 1Dibromochloromethane
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-609802/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609802
RL MDL
Dichlorodifluoromethane 0.850 U 1.00 0.850 ug/L 01/25/23 12:14 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
0.200 U 0.2001.00 ug/L 01/25/23 12:14 1Diisopropyl ether
24.0 U 24.0100 ug/L 01/25/23 12:14 1Ethanol
0.500 U 0.5001.00 ug/L 01/25/23 12:14 1Ethylbenzene
0.530 U 0.5301.00 ug/L 01/25/23 12:14 1Isopropylbenzene
0.220 U 0.2201.00 ug/L 01/25/23 12:14 1Methyl tert-butyl ether
3.00 U 3.005.00 ug/L 01/25/23 12:14 1Methylene Chloride
0.630 U 0.6305.00 ug/L 01/25/23 12:14 1m-Xylene & p-Xylene
3.00 U 3.005.00 ug/L 01/25/23 12:14 1Naphthalene
0.760 U 0.7601.00 ug/L 01/25/23 12:14 1n-Butylbenzene
0.690 U 0.6901.00 ug/L 01/25/23 12:14 1N-Propylbenzene
0.600 U 0.6005.00 ug/L 01/25/23 12:14 1o-Xylene
0.710 U 0.7101.00 ug/L 01/25/23 12:14 1p-Cymene (p-Isopropyltoluene)
0.700 U 0.7001.00 ug/L 01/25/23 12:14 1sec-Butylbenzene
1.00 U 1.001.00 ug/L 01/25/23 12:14 1Styrene
0.630 U 0.6301.00 ug/L 01/25/23 12:14 1tert-Butylbenzene
0.900 U 0.9001.00 ug/L 01/25/23 12:14 1Tetrachloroethene
0.410 U 0.4101.00 ug/L 01/25/23 12:14 1Toluene
0.500 U 0.5001.00 ug/L 01/25/23 12:14 1trans-1,2-Dichloroethene
0.200 U 0.2005.00 ug/L 01/25/23 12:14 1trans-1,3-Dichloropropene
0.150 U 0.1501.00 ug/L 01/25/23 12:14 1Trichloroethene
0.520 U 0.5201.00 ug/L 01/25/23 12:14 1Trichlorofluoromethane
0.930 U 0.93025.0 ug/L 01/25/23 12:14 1Vinyl acetate
0.500 U 0.5001.00 ug/L 01/25/23 12:14 1Vinyl chloride
1.60 U 1.6010.0 ug/L 01/25/23 12:14 1Xylenes, Total
4-Bromofluorobenzene 87 72-119 01/25/23 12:14 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
114 01/25/23 12:14 1Dibromofluoromethane75-126
95 01/25/23 12:14 1Toluene-d8 (Surr)64-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-609802/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609802
1,1,1,2-Tetrachloroethane 50.0 57.56 ug/L 115 67 -131
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,1,1-Trichloroethane 50.0 61.48 ug/L 123 68 -130
1,1,2,2-Tetrachloroethane 50.0 51.03 ug/L 102 70 -131
1,1,2-Trichloroethane 50.0 52.88 ug/L 106 70 -130
1,1-Dichloroethane 50.0 60.96 ug/L 122 70 -130
1,1-Dichloroethene 50.0 60.77 ug/L 122 63 -134
1,1-Dichloropropene 50.0 59.53 ug/L 119 70 -130
1,2,3-Trichlorobenzene 50.0 54.43 ug/L 109 60 -138
1,2,3-Trichloropropane 50.0 51.64 ug/L 103 70 -130
1,2,4-Trichlorobenzene 50.0 53.24 ug/L 106 60 -140
1,2,4-Trimethylbenzene 50.0 54.43 ug/L 109 70 -130
1,2-Dibromoethane (EDB)50.0 53.39 ug/L 107 70 -130
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-609802/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609802
1,2-Dichlorobenzene 50.0 58.21 ug/L 116 67 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
1,2-Dichloroethane 50.0 60.20 ug/L 120 69 -130
1,2-Dichloropropane 50.0 59.52 ug/L 119 70 -130
1,3,5-Trimethylbenzene 50.0 53.87 ug/L 108 69 -130
1,3-Dichlorobenzene 50.0 58.50 ug/L 117 70 -130
1,3-Dichloropropane 50.0 52.29 ug/L 105 70 -130
1,4-Dichlorobenzene 50.0 58.19 ug/L 116 70 -130
2,2-Dichloropropane 50.0 56.68 ug/L 113 52 -135
2-Butanone (MEK)200 218.7 ug/L 109 61 -145
2-Chlorotoluene 50.0 49.51 ug/L 99 70 -130
2-Hexanone 200 179.7 ug/L 90 65 -137
4-Chlorotoluene 50.0 53.86 ug/L 108 70 -130
4-Methyl-2-pentanone (MIBK)200 213.8 ug/L 107 69 -138
Acetone 200 211.6 ug/L 106 43 -160
Benzene 50.0 60.60 ug/L 121 70 -130
Bromobenzene 50.0 54.52 ug/L 109 70 -132
Bromochloromethane 50.0 65.61 *+ug/L 131 70 -130
Bromodichloromethane 50.0 61.61 ug/L 123 67 -133
Bromoform 50.0 54.50 ug/L 109 57 -140
Bromomethane 25.0 83.09 *+ug/L 332 10 -160
Carbon tetrachloride 50.0 64.51 ug/L 129 61 -137
Chlorobenzene 50.0 56.97 ug/L 114 70 -130
Chloroethane 25.0 26.56 ug/L 106 55 -141
Chloroform 50.0 62.04 ug/L 124 69 -130
Chloromethane 25.0 25.62 ug/L 102 58 -137
cis-1,2-Dichloroethene 50.0 58.85 ug/L 118 68 -130
cis-1,3-Dichloropropene 50.0 54.86 ug/L 110 69 -132
Dibromochloromethane 50.0 54.52 ug/L 109 67 -135
Dichlorodifluoromethane 25.0 29.09 ug/L 116 41 -146
Diisopropyl ether 25.0 27.21 ug/L 109 64 -132
Ethanol 1000 1192 ug/L 119 20 -160
Ethylbenzene 50.0 53.93 ug/L 108 70 -130
Isopropylbenzene 50.0 53.76 ug/L 108 70 -130
Methyl tert-butyl ether 50.0 52.60 ug/L 105 66 -130
Methylene Chloride 50.0 65.37 ug/L 131 66 -135
m-Xylene & p-Xylene 50.0 53.16 ug/L 106 70 -130
Naphthalene 50.0 43.65 ug/L 87 47 -149
n-Butylbenzene 50.0 49.61 ug/L 99 67 -130
N-Propylbenzene 50.0 54.46 ug/L 109 70 -130
o-Xylene 50.0 51.66 ug/L 103 70 -130
p-Cymene (p-Isopropyltoluene)50.0 54.36 ug/L 109 65 -130
sec-Butylbenzene 50.0 53.70 ug/L 107 66 -130
Styrene 50.0 55.03 ug/L 110 70 -130
tert-Butylbenzene 50.0 51.01 ug/L 102 64 -139
Tetrachloroethene 50.0 60.19 ug/L 120 65 -130
Toluene 50.0 52.26 ug/L 105 70 -130
trans-1,2-Dichloroethene 50.0 62.12 ug/L 124 70 -130
trans-1,3-Dichloropropene 50.0 47.93 ug/L 96 63 -130
Trichloroethene 50.0 66.54 *+ug/L 133 70 -130
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: SM6200-B - Volatile Organic Compounds (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-609802/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 609802
Trichlorofluoromethane 25.0 36.38 *+ug/L 146 65 -138
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Vinyl acetate 50.0 49.09 ug/L 98 26 -160
Vinyl chloride 25.0 35.35 *+ug/L 141 59 -136
Xylenes, Total 100 104.8 ug/L 105 70 -130
4-Bromofluorobenzene 72 -119
Surrogate
83
LCS LCS
Qualifier Limits%Recovery
109Dibromofluoromethane 75 -126
87Toluene-d8 (Surr)64 -132
Client Sample ID: Method BlankLab Sample ID: MB 400-610024/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610024
RL MDL
Bromomethane 0.980 U 1.00 0.980 ug/L 01/26/23 15:23 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
1.00 U 1.001.00 ug/L 01/26/23 15:23 1Chloroform
0.320 U 0.3201.00 ug/L 01/26/23 15:23 1Chloromethane
4-Bromofluorobenzene 101 72-119 01/26/23 15:23 1
MB MB
Surrogate Dil FacPreparedAnalyzedQualifierLimits%Recovery
101 01/26/23 15:23 1Dibromofluoromethane75-126
94 01/26/23 15:23 1Toluene-d8 (Surr)64-132
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-610024/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610024
Bromomethane 50.0 52.22 ug/L 104 10 -160
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
Chloroform 50.0 41.89 ug/L 84 69 -130
Chloromethane 50.0 39.61 ug/L 79 58 -137
4-Bromofluorobenzene 72 -119
Surrogate
97
LCS LCS
Qualifier Limits%Recovery
98Dibromofluoromethane 75 -126
96Toluene-d8 (Surr)64 -132
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC)
Client Sample ID: Method BlankLab Sample ID: MB 400-610674/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610718 Prep Batch: 610674
RL MDL
1,2-Dibromoethane (EDB)0.0150 U 0.0200 0.0150 ug/L 02/01/23 09:49 02/01/23 18:20 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResultQualifier
Eurofins Pensacola
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QC Sample Results
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method: 504.1 - EDB, DBCP and 1,2,3-TCP (GC) (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 400-610674/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610718 Prep Batch: 610674
4-Bromofluorobenzene 112 56-150 02/01/23 18:20 1
MB MB
Surrogate
02/01/23 09:49
Dil FacPreparedAnalyzedQualifierLimits%Recovery
Client Sample ID: Lab Control SampleLab Sample ID: LCS 400-610674/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610718 Prep Batch: 610674
1,2-Dibromoethane (EDB)0.101 0.09910 ug/L 98 70 -130
Analyte
LCS LCS
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits
4-Bromofluorobenzene 56 -150
Surrogate
122
LCS LCS
Qualifier Limits%Recovery
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 400-610674/3-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 610718 Prep Batch: 610674
1,2-Dibromoethane (EDB)0.101 0.09558 ug/L 95 70 -130 4 10
Analyte
LCSD LCSD
DUnitResultQualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
4-Bromofluorobenzene 56 -150
Surrogate
122
LCSD LCSD
Qualifier Limits%Recovery
Eurofins Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-232047-1
Project/Site: Perth Mini Mart
Client Sample ID: MW1 Lab Sample ID: 400-232047-1
Matrix: WaterDate Collected: 01/18/23 12:24
Date Received: 01/20/23 09:04
Analysis SM6200-B BEP01/26/23 21:5710 EET PEN610024
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis SM6200-B 10 609802 01/25/23 13:58 BPO EET PENTotal/NA 5 mL 5 mL
Client Sample ID: MW4 Lab Sample ID: 400-232047-2
Matrix: WaterDate Collected: 01/18/23 12:21
Date Received: 01/20/23 09:04
Analysis SM6200-B BEP01/26/23 22:2110 EET PEN610024
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis SM6200-B 10 609802 01/25/23 14:19 BPO EET PENTotal/NA 5 mL 5 mL
Client Sample ID: MW5 Lab Sample ID: 400-232047-3
Matrix: WaterDate Collected: 01/18/23 12:13
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 15:21200 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW6 Lab Sample ID: 400-232047-4
Matrix: WaterDate Collected: 01/18/23 12:17
Date Received: 01/20/23 09:04
Analysis SM6200-B BEP01/27/23 00:24100 EET PEN610024
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis SM6200-B 100 609802 01/25/23 14:40 BPO EET PENTotal/NA 5 mL 5 mL
Client Sample ID: MW7 Lab Sample ID: 400-232047-5
Matrix: WaterDate Collected: 01/18/23 12:04
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 16:471 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW8 Lab Sample ID: 400-232047-6
Matrix: WaterDate Collected: 01/18/23 12:10
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 17:081 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW9 Lab Sample ID: 400-232047-7
Matrix: WaterDate Collected: 01/18/23 11:40
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 17:291 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-232047-1
Project/Site: Perth Mini Mart
Client Sample ID: MW10 Lab Sample ID: 400-232047-8
Matrix: WaterDate Collected: 01/18/23 11:30
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 17:501 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW11 Lab Sample ID: 400-232047-9
Matrix: WaterDate Collected: 01/18/23 12:08
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 13:172 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW13 Lab Sample ID: 400-232047-10
Matrix: WaterDate Collected: 01/18/23 12:01
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 13:375 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: MW14 Lab Sample ID: 400-232047-11
Matrix: WaterDate Collected: 01/18/23 11:50
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 18:101 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: WSW1 Lab Sample ID: 400-232047-12
Matrix: WaterDate Collected: 01/18/23 12:30
Date Received: 01/20/23 09:04
Analysis SM6200-B BEP01/26/23 15:481 EET PEN610024
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis SM6200-B 1 609802 01/25/23 18:31 BPO EET PENTotal/NA 5 mL 5 mL
Prep 504.1 610674 02/01/23 09:49 DS EET PENTotal/NA 34.8 mL 35 mL
Analysis 504.1 1 610718 02/01/23 19:21 DS EET PENTotal/NA
Client Sample ID: WSW2 Lab Sample ID: 400-232047-13
Matrix: WaterDate Collected: 01/18/23 12:55
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 18:521 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 504.1 610674 02/01/23 09:49 DS EET PENTotal/NA 34.7 mL 35 mL
Analysis 504.1 1 610718 02/01/23 19:42 DS EET PENTotal/NA
Eurofins Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-232047-1
Project/Site: Perth Mini Mart
Client Sample ID: WSW4 Lab Sample ID: 400-232047-14
Matrix: WaterDate Collected: 01/18/23 13:16
Date Received: 01/20/23 09:04
Analysis SM6200-B BPO01/25/23 19:131 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Prep 504.1 610674 02/01/23 09:49 DS EET PENTotal/NA 34.6 mL 35 mL
Analysis 504.1 1 610718 02/01/23 20:02 DS EET PENTotal/NA
Client Sample ID: MW12 Lab Sample ID: 400-232072-1
Matrix: WaterDate Collected: 01/20/23 12:00
Date Received: 01/21/23 09:23
Analysis SM6200-B BEP01/25/23 16:265 EET PEN609770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-609770/4
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BEP01/25/23 10:411 EET PEN609770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-609802/4
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BPO01/25/23 12:141 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-610024/6
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BEP01/26/23 15:231 EET PEN610024
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Method Blank Lab Sample ID: MB 400-610674/1-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 504.1 DS02/01/23 09:49 EET PEN610674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 35 mL 35 mL
Analysis 504.1 1 610718 02/01/23 18:20 DS EET PENTotal/NA
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-609770/1002
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BEP01/25/23 07:471 EET PEN609770
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Eurofins Pensacola
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Lab Chronicle
Client: Terraquest Environmental Consultants, PC Job ID: 400-232047-1
Project/Site: Perth Mini Mart
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-609802/1002
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BPO01/25/23 10:581 EET PEN609802
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-610024/1002
Matrix: WaterDate Collected: N/A
Date Received: N/A
Analysis SM6200-B BEP01/26/23 14:221 EET PEN610024
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Client Sample ID: Lab Control Sample Lab Sample ID: LCS 400-610674/2-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 504.1 DS02/01/23 09:49 EET PEN610674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 35 mL 35 mL
Analysis 504.1 1 610718 02/01/23 18:41 DS EET PENTotal/NA
Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 400-610674/3-A
Matrix: WaterDate Collected: N/A
Date Received: N/A
Prep 504.1 DS02/01/23 09:49 EET PEN610674
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 35 mL 35 mL
Analysis 504.1 1 610718 02/01/23 19:01 DS EET PENTotal/NA
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins Pensacola
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Method Summary
Job ID: 400-232047-1Client: Terraquest Environmental Consultants, PC
Project/Site: Perth Mini Mart
Method Method Description LaboratoryProtocol
SMSM6200-B Volatile Organic Compounds EET PEN
EPA-DW504.1 EDB, DBCP and 1,2,3-TCP (GC)EET PEN
SW8465030BPurge and Trap EET PEN
EPA-DW504.1 Microextraction EET PEN
Protocol References:
EPA-DW = "Methods For The Determination Of Organic Compounds In Drinking Water", EPA/600/4-88/039, December 1988 And Its Supplements.
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL [phone]
Eurofins Pensacola
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Accreditation/Certification Summary
Client: Terraquest Environmental Consultants, PC Job ID: 400-232047-1
Project/Site: Perth Mini Mart
Laboratory: Eurofins Pensacola
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
North Carolina (WW/SW)State 314 12-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
SM6200-B Water 2-Butanone (MEK)
SM6200-B Water 2-Hexanone
SM6200-B Water 4-Methyl-2-pentanone (MIBK)
SM6200-B Water Acetone
SM6200-B Water Vinyl acetate
Eurofins Pensacola
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Login Sample Receipt Checklist
Client: Terraquest Environmental Consultants, PC Job Number: 400-232047-1
Login Number: 232047
Question Answer Comment
Creator: Perez, Trina M
List Source: Eurofins Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.0.0°C IR-8
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pensacola
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Login Sample Receipt Checklist
Client: Terraquest Environmental Consultants, PC Job Number: 400-232047-1
Login Number: 232072
Question Answer Comment
Creator: Whitley, Adrian
List Source: Eurofins Pensacola
List Number: 1
N/ARadioactivity wasn't checked or is </= background as measured by a survey
meter.
N/AThe cooler's custody seal, if present, is intact.
N/ASample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.0.7°C IR9
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Pensacola
Page 60 of 60 2/2/2023
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