25073 Fulbright Laboratories ESA 20220524

Groundwater Assessment Report

Fulbright Laboratories Brownfields Property
1919, 1923, and 1933 South Boulevard
Charlotte, North Carolina

H&H Job No. SLC-001
May 24, 2021

#C-1269 Engineering
#C-245 Geology

i

https://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Southern Land Company (SLC)/SLC-001 South
Boulevard Assemblage/April 2022 Temp Well Installation/Final Report Docs/Groundwater Assessment Report - 1919-1933 South Boulevard
(5-24-22).doc
Groundwater Assessment Report
Fulbright Laboratories Brownfields Property
1919, 1923, and 1933 South Boulevard
Charlotte, North Carolina
H&H Job No. SLC-001

Table of Contents

1.0 Introduction and Background ....................................................................................................... 1 
2.0 Groundwater Assessment Activities ............................................................................................. 3 
2.1 Geophysical Survey/Utility Locating ..................................................................................... 3 
2.2 Groundwater Assessment Methodology ................................................................................ 4 
2.3 Temporary Well Abandonment and Investigation Derived Waste ...................................... 6 
3.0 Groundwater Analytical Results ................................................................................................... 7 
4.0 Conclusions and Recommendations ............................................................................................. 8 

List of Tables

Table 1 Summary of Temporary Well Construction and Water Level Data
Table 2 Summary of Groundwater Analytical Data

List of Figures

Figure 1 Site Location Map
Figure 2 Site and Temporary Well Location Map

List of Appendices

Appendix A Boring Logs & Well Abandonment Records
Appendix B Groundwater Sampling Forms
Appendix C Laboratory Analytical Reports

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1933 South Boulevard (5-24-22).doc
Groundwater Assessment Report
Fulbright Laboratories Brownfields Property
1919, 1923, and 1933 South Boulevard
Charlotte, North Carolina
H&H Job No. SLC-001

1.0 Introduction and Background

Hart & Hickman, PC (H&H) has prepared this Groundwater Assessment Report on behalf of
Southern Land Company, LLC to document assessment activities conducted at the commercial
properties located at 1919, 1923, and 1933 South Boulevard in Charlotte, Mecklenburg County,
North Carolina (Site or subject Site). A Site location map is included as Figure 1.

The Site consists of three contiguous parcels of land that total approximately 0.92 acre. The Site is
developed with one approximate 4,400-square foot (sq ft) restaurant (1933 South Boulevard), one
approximate 5,000-sq ft office building (1923 South Boulevard), and one approximate 4,500-sq ft
multi-tenant office building (1919 South Boulevard). Remaining portions of the Site consist of
asphalt-paved vehicle access and parking areas, concrete-paved sidewalks, and vegetated areas. A
Site map is included as Figure 2.

The Site consisted of three retail stores (including the current building at 1923 South Boulevard), a
residence, and two ancillary structures by at least the early 1900s. By the late 1920s, additional
retail buildings and a beverage bottling facility were developed on the Site. From the late 1930s
until the early 1970s, the Site buildings were occupied by various businesses including grocery
stores, various retailers, a construction company, a roofing supply company, and a chemical
laboratory/manufacturing company. Residential and commercial use continued on the Site until the
late 1980s, when the current restaurant and office building were developed in the northern and
western portions of the Site, respectively. Since the mid-1980s, the Site buildings have been
occupied by restaurants, various retailers, fitness companies, and various offices.

H&H performed initial groundwater sampling activities at the Site during a Phase II Environmental
Site Assessment (ESA) in August 2021. The Phase II ESA was conducted to evaluate potential
environmental impacts associated with a former on-Site chemical mixing facility (Fulbright

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1933 South Boulevard (5-24-22).doc
Laboratories), an on-Site gasoline underground storage tank (UST), an off-Site former
manufacturing facility (Parks Cramer) to the west of the Site, and an existing automotive service
garage (H&H Auto) to the northeast of the Site. Results of groundwater assessment activities
completed in areas downgradient of the Parks Cramer property and the H&H Auto facility did not
indicate the presence of volatile organic compounds (VOCs) or semi-VOCs (SVOCs) at
concentrations above the North Carolina 2L Groundwater Standards (2L Standards) or the Vapor
Intrusion Groundwater Screening Levels (GWSLs). Chromium was detected above the 2L
Standard in an unfiltered groundwater sample collected downgradient of the H&H Auto facility
(TMW-3). The analytical results of analysis of the filtered sample from TMW-3 did not indicate
the presence of chromium above the 2L Standard.

Results of groundwater assessment activities completed in the area of the former chemical mixing
building indicated the presence the chlorinated compounds cis-1,2-dichloroethene, trans-1,2-
dichloroethene, tetrachloroethene (PCE), trichloroethene (TCE), and vinyl chloride at
concentrations above the 2L Standards and/or the GWSLs. The petroleum-related compound
naphthalene was detected below the 2L Standard but above the Residential GWSL in the
groundwater sample collected near the former chemical mixing building.

H&H understands that Southern Land Company, LLC plans to redevelop the Site with a multi-
story retail and residential building with ground floor parking and leasing/amenities areas. To
address environmental concerns associated with the Site, Southern Land Company, LLC elected
to enter the Site into the North Carolina Department of Environmental Quality (DEQ)
Brownfields Program. A Letter of Eligibility to participate in the Brownfields Program was
received on November 19, 2021. The Brownfields project is referred to as Fulbright
Laboratories and is awaiting a Project Manager assignment.

In March and April 2022, H&H conducted additional groundwater assessment at the Site to
evaluate the potential for shallow groundwater infiltration into excavations associated with
proposed elevator pits and a subgrade generator room, and to evaluate groundwater quality in the
proposed excavation areas. Methods and results of the groundwater assessment activities are
detailed in the following sections.

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2.0 Groundwater Assessment Activities

In March and April 2022, H&H completed additional groundwater assessment activities at the
Site to evaluate the potential for de-watering during future building construction and to evaluate
groundwater quality in the areas of potential de-watering.

The assessment activities were conducted in general accordance with the DEQ Inactive Hazardous
Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated July 2021, the DEQ Division of
Waste Management (DWM) Vapor Intrusion Guidance (VI Guidance) dated March 2018, and the
most recent version of the U.S. Environmental Protection Agency (EPA) Region IV Laboratory
Services and Applied Science Division (LSASD) Field Branches Quality System and Technical
Procedures guidance.

In accordance with the Mecklenburg County requirements, H&H obtained a Subsurface
Investigation Permit (SIP No. 70002922) from the Mecklenburg County Land Use and
Environmental Services Agency (LUESA) prior to conducting groundwater assessment
activities. Per Mecklenburg County regulations, well abandonment records will be provided to
LUESA in order to close the SIP.

2.1 Geophysical Survey/Utility Locating

Prior to conducting the assessment activities, H&H contacted North Carolina 811, the public
utility locator, to mark subsurface utilities on the Site. H&H also contracted with Probe Utility
Locating, a private utility locator, to screen proposed sample locations for subgrade utilities and
to confirm public utility locator markings using electromagnetic and ground-penetrating radar
methods. Soil boring locations were hand cleared using a decontaminated stainless-steel hand
auger to approximately 5 ft below ground surface (bgs) prior to use of mechanical drilling
equipment to further screen the boring locations for the presence of subsurface utilities.

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1933 South Boulevard (5-24-22).doc
2.2 Groundwater Assessment Methodology

H&H contracted with Ameriprobe, Inc. (Ameriprobe), a North Carolina-licensed drilling
contractor, to advance five soil borings and convert each boring to temporary monitoring wells
(TMW-4 through TMW-8) using a track-mounted direct push technology (DPT) drill rig and a
hand auger. Temporary monitoring well locations are described below and are depicted on
Figure 2.

 Temporary monitoring wells TMW-4 and TMW-5 were installed in the location of the
proposed subgrade generator room in the southeastern portion of the Site.
 Temporary monitoring wells TMW-6, TMW-7, and TMW-8 were installed the proposed
locations for three elevator shaft pits in the central portion of the Site.

TMW-4 and TMW-5 were hand augered to a depth of 5 ft bgs, which is the approximate depth
below current grade of the proposed subgrade generator room. The proposed elevator pits are
estimated to be at least 15 ft below current grade. Therefore, TMW-6 was installed at
approximately 20 ft bgs, and TMW-7 and TMW-8 were installed to approximately 15 ft bgs
using DPT drilling methods.

During the well installation process, continuous soil samples were collected from the borings,
logged for lithologic description, and screened for the presence of staining, odors, and volatile
organic vapors using a calibrated photoionization detector (PID). No obvious evidence of soil
impacts was identified during field screening. Boring logs are provided in Appendix A.

The temporary monitoring wells were constructed of 1-inch diameter PVC with 5 to 15 ft of well
screen set to bracket the water table and/or capture potential perched water. In temporary wells
TMW-4 and TMW-5, filter sand was placed in the well annulus from the base of the borehole to
approximately 1.5 ft bgs. In TMW-6 and TMW-7, filter sand was placed from the bottom of the
borehole to approximately 1 ft above the well screen. A hydrated bentonite seal was placed from
the top the filter sand to the ground surface. Temporary monitoring well construction details are
provided in Table 1 and depicted on boring logs in Appendix A.

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Prior to purging and sampling, H&H measured the depth to water in the temporary wells using an
electronic water level indicator. Groundwater was measured at depths of approximately 2.13 ft bgs
in TMW-4, 3.36 ft bgs in TMW-6, 1.52 ft bgs in TMW-7, and 5.05 ft bgs in TMW-8. TMW- 5 was
dry approximately four days after installation. Depth to groundwater measurements are displayed in
Table 1. Based on the lithology observed in the borings, the primary water-bearing zone appears to
be located beyond 15 ft bgs. However, perched water was identified at depth intervals of
approximately 4 to 5 ft bgs in TMW-4, 2 to 7 ft bgs in TMW-7, and 4 to 6 ft in TMW-8. The
shallow water observed in the temporary wells is likely due to perched groundwater within shallow
fill material and pressurized conditions in the shallow aquifer. Based on Site topography,
groundwater at the Site is expected to flow to the south.

Following well installations, H&H developed the temporary monitoring wells by removing at least
three well volumes or until purged dry (due to poor recharge) using a peristaltic pump and dedicated
polyethylene tubing. Prior to sample collection, H&H attempted to use a peristaltic pump and low
flow techniques to purge the temporary wells until field parameters of temperature, pH, specific
conductivity, and oxidation reduction potential (ORP) stabilized and turbidity was less than 10
Nephelometric Turbidity Units (NTUs). Due to poor recharge, collection of field measurements
was limited, and turbidity of less than NTUs could not be achieved. Therefore, H&H used a 0.45-
micron filter to collect a filtered sample from each well for Resource Conservation and Recovery
Act (RCRA) metals analysis. Groundwater sampling field forms completed by H&H sampling
personnel are provided in Appendix B.

The groundwater samples were placed in dedicated laboratory-supplied sample containers and then
delivered to Waypoint Analytical under standard chain of custody protocols. Groundwater samples
were analyzed for VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and RCRA metals
by EPA Methods 6020/7470. As noted above, a turbidity reading of 10 NTUs or less could not be
reasonably achieved during groundwater sampling activities at temporary wells TMW-4, TMW-6,
TMW-7, and TMW-8; therefore, H&H collected filtered and unfiltered groundwater samples for
laboratory analysis of RCRA metals by EPA Methods 6020/7470.

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2.3 Temporary Well Abandonment and Investigation Derived Waste

Upon completion of the groundwater assessment activities, Ameriprobe abandoned the temporary
monitoring wells by removing the PVC riser pipe from the ground and filling the boreholes using
hydrated bentonite. The ground surface was then restored to approximate pre-drilling conditions.
Soil cuttings and well development water generated during drilling and groundwater sampling
activities were spread on-Site.

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3.0 Groundwater Analytical Results

Groundwater data were compared to the 2L Groundwater Standards dated April 2022, the North
Carolina 2B Surface Water Standards (2B Standards) dated July 2021, and the DEQ DWM
Residential and Non-Residential Vapor Intrusion GWSLs dated January 2022. The 2B Standards
are used to evaluate potential groundwater discharge to the storm sewer during construction-related
dewatering in accordance with 15A NCAC 2H .0106(f)(7). A tabular summary of groundwater
analytical results is presented in Table 2. The laboratory analytical reports and chain of custody
records are provided in Appendix C.

Laboratory analytical data indicate that one or more VOCs were detected in samples TMW-4 and
TMW-6 through TMW-8. PCE was detected in sample TMW-6 at a concentration of 4.95 µg/L,
which exceeds the 2L Standard of 0.7 µg/L and the 2B Standard of 3.3 µg/L. TCE was detected in
sample TMW-6 at a concentration of 2.51 µg/L, which is above the residential GWSL but below the
non-residential GWSL and the 2L and 2B Standards. No other VOCs were detected in the
groundwater samples at concentrations above 2L Standards, 2B Standards, or GWSLs.

No SVOCs were detected in TMW-4 or TMW-6 through TMW-8 at concentrations above the
laboratory method detection limits (MDLs).

The metals barium, chromium, lead, and/or silver were detected in all of the unfiltered
groundwater samples collected from TMW-4 and TMW-6 through TMW-8 at concentrations
above 2L and/or 2B Standards. The results of analysis of the filtered groundwater samples
collected from TMW-4 and TMW-8 did not indicate the presence of metals at concentrations
above the 2L or 2B Standards. Therefore, the metals detections in unfiltered samples TMW-4 and
TMW-8 are likely due to high turbidity in the samples and not dissolved phase groundwater
contamination. Chromium (22.5 µg/L) was detected in the filtered sample collected from TMW-6
at a concentration above the 2L Standard of 10 µg/L and the acute and chronic 2B Standards of
16 µg/L and 11 µg/L, respectively. Lead was detected in filtered samples collected from TMW-6
(6.7 µg/L) and TMW-7 (5.27 µg/L) at concentrations below the 2L Standard but above the chronic
2B Standard of 1.62 µg/L.

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4.0 Conclusions and Recommendations

H&H has completed groundwater assessment activities on the commercial properties located at
1919, 1923, and 1933 South Boulevard in Charlotte, Mecklenburg County, North Carolina. The
assessment activities were conducted to evaluate the potential for shallow groundwater
infiltration into excavations associated with proposed elevator pits and a subgrade generator
room, and to evaluate groundwater quality in the proposed excavation areas. A summary of the
assessment results is provided below.

 Two temporary wells (TMW-4 and TMW-5) were installed to approximately 5 ft bgs in the
location of a proposed subgrade generator room. Perched water that appears to have
collected in shallow fill material was identified in TMW-4 at a depth of approximately
2.13 ft bgs. No measurable groundwater was identified in TMW-5, which is further
evidence that the shallow groundwater identified in TMW-4 is perched water and is not
representative of the shallow aquifer.
 Three temporary wells (TMW-6 through TMW-8) were installed to approximately 15 to
20 ft bgs in locations of proposed elevator pits. Groundwater was measured in TMW-6
through TMW-8 at depths ranging from approximately 1.52 ft bgs and 5.05 ft bgs. The
primary water-bearing zone appears to be at depths greater than 15 ft bgs. However,
perched water was identified at depths ranging from approximately 2 to 7 ft bgs. The
shallow water observed in the temporary wells is likely due to perched groundwater within
shallow fill material and pressurized conditions in the shallow aquifer.
 Groundwater analytical data for sample TMW-4 (proposed generator room) indicate that the
metals lead and silver were detected in the unfiltered sample at concentrations above the
surface water standards. No metals were detected in the filtered TMW-4 sample above the
groundwater or surface water standards.
 Groundwater analytical data for samples TMW-5 and TMW-6 through TMW-8 (proposed
elevator pits) indicate that the metals lead and chromium were detected in the unfiltered
samples at concentrations above the surface water and/or groundwater standards. Lead was
also detected in filtered samples TMW-6 and TMW-7 above the surface water standard, and
chromium was also detected in filtered sample TMW-6 above the groundwater and surface
water standards.

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 No significant vapor intrusion concern was identified based on analytical data for samples
TMW-4 and TMW-6 through TMW-8, and based on the ground level parking garage and
overlying commercial space and parking levels in the proposed building.
 Based on field observations and water level measurements in the temporary wells,
dewatering will likely be necessary for excavations associated with the generator room and
elevator pits. Further, groundwater analytical data indicate that groundwater in potential
dewatering areas will not likely be suitable for discharge to the storm sewer due to the
detection of PCE and metals at concentrations above the North Carolina surface water
standards.

Recommendations
Based on the results of the March and April 2022 groundwater assessment activities, H&H
recommends that a National Pollutant Discharge Elimination System (NPDES) Permit be obtained
from the DEQ Division of Water Resources to allow for on-Site treatment of groundwater prior to
discharge to the municipal storm sewer during construction activities. Alternatively, groundwater
could be containerized on-Site for further testing to determine the appropriate disposal method.
Note that groundwater management procedures will also be outlined in a DEQ Brownfields
Program-approved Environmental Management Plan.

Table 1Summary of Temporary Well Construction and Water Level Data Fulbright Laboratories Brownfields Property1919, 1923, and 1933 South Boulevard Charlotte, North CarolinaH&H Job No. SLC-001Well IDTotal Depth (ft bgs)Screen Length (ft)Screen Interval (ft bgs)Depth to Groundwater (ft bgs)TMW-4 5 5 0-5 2.13TMW-5 5 5 0-5 DryTMW-6 20 15 5-20 3.16TMW-7 15 10 5-15 1.52TMW-8 15 10 5-15 5.05Notes:Depth to groundwater measurements collected by H&H on April 1, 2022. TMW = temporary monitoring well; ft bgs = feet below ground surface;Dry = no water in wellhttps://harthick.sharepoint.com/sites/MasterFiles-1/Shared Documents/AAA-Master Projects/Southern Land Company (SLC)/SLC-001 South Boulevard Assemblage/April 2022 Temp Well Installation/Tables/Data Tables - RJC.xlsx5/20/2022Table 1Hart & Hickman, PC
Table 2 Summary of Groundwater Analytical Data Fulbright Laboratories Brownfields Property 1919, 1923, and 1933 South Boulevard Charlotte, North CarolinaH&H Job No. SLC-001Evaluation AreaSample IDDateAcute ChronicUnitsVOCs (8260D)Acetone3.60 J--5.81--9.27--6.75--6,0002,000 (4)NENENEChloroform <0.220--0.248 J--<0.220--<0.220--702,000 (3)NE0.81 3.6cis-1,2-Dichloroethene<0.200--0.428 J--<0.200--0.207 J--7060 (4)NENENEMethyl Ethyl Ketone (MEK)<0.710--1.62 J--<0.710--<0.710--4,00026,000 (4)NE450,000 1,900,000Methyl tert-butyl ether (MTBE) <0.140--0.801--<0.140--<0.140--201,500 (4)NE450 2,000Tetrachloroethene <0.220--4.95--0.221 J--0.617--0.73.3 (3)NE1248Toluene <0.220--0.291 J--<0.220--<0.220--60011 (3)NE3,80016,000Trichloroethene<0.180--2.51--0.554--0.832--3 30 (3)NE1.04.4SVOCs (8270E)ALL BDL--ALLBDL--ALL BDL--ALL BDL--------Metals (6020B/7470A)UnfilteredFilteredUnfilteredFilteredUnfilteredFilteredUnfilteredFilteredArsenic1.490.711 J3.16 J<2.452.53 J<2.457.801.201010 (3)NE-- --Barium 155 95.9 220 128 417 181820140 70021,000 (4)NE-- --Cadmium<0.150 <0.150 <0.750 <0.750 <0.750 <0.750 <0.750 <0.15021.93 (5)0.31 (5)----Chromium (Total)3.37<1.0085.325.522.4<5.002351.25 J1016 (6)11 (6)----Lead4.190.663 J32.16.7024.95.271711.411541.65 (5)1.62 (5)----Mercury<0.00007<0.00007<0.00007<0.00007<0.00007<0.00007<0.00007<0.0000710.012 (t)NE0.18 0.75Selenium<2.30 <2.30 <11.5 <11.5 <11.5 <11.5 <11.5 <2.30205 (t)NE-- --Silver 0.439 J<0.130 <0.650 <0.650 <0.650 <0.650 <0.650 <0.650201.62 (5)0.06 (3)----Notes:1)North Carolina Department of Environmental Quality (DEQ) 15A NCAC 02L.0202 Groundwater Standards (2L Standards) dated April 2022.2)NC 15A North Carolina Administrative Code 02B.0202 Surface Water Quality Standards (2B Standards) for Class C Surface Waters dated July 2021.3)EPA National Recommended Water Quality Criteria for Aquatic Life & Human Health for Class C Waters (June 10, 2019).4)North Carolina In-Stream Target Values for Surface Waters for Class C Waters (June 10, 2019).5)Standard derived using the DEQ Hardness-Dependent Metal Calculator dated July 2021 using the EPA published median hardness concentration for Little Sugar Creek of 67 mg/L as CaCO3.6)2B Standards are not established for total chromium. Hexavalent chromium 2B Standards are conservatively used in the table above.7)DEQ Division of Waste Management (DWM) Vapor Intrusion Groundwater Screening Levels (GWSLs) dated January 2022.Concentrations are reported in micrograms per liter (µg/L).Compound concentrations are reported to the laboratory method detection limits.Laboratory analytical methods are shown in parentheses.With the exception of metals, only constituents detected in at least one sample are shown in the table above.Bold values exceed the 2L Standard.Shaded values exceed a North Carolina surface water standard.Underlined values exceed the DWM Residential GWSL.VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; NE = not established; -- = not applicable; BDL = below the laboratory method detection limitJ = Estimated concentration between the laboratory method detection limit and the laboratory reporting limit (t)= based upon measurement of total recoverable metal. See 15A NCAC 02B .0211 for more information.2B Standards (2)4/1/20224/1/2022Proposed Subgrade Generator Roomµg/L2L Standards (1) Residential GWSLs (3)Screening Criteria Non-Residential GWSLs (3)Proposed Elevator PitsTMW-4TMW-6TMW-7TMW-84/1/20223/31/2022https://harthick.sharepoint.com/sites/MasterFiles‐1/Shared Documents/AAA‐Master Projects/Southern Land Company (SLC)/SLC‐001 South Boulevard Assemblage/April 2022 Temp Well Installation/Tables/Data Tables ‐ RJC.xlsx5/20/2022Table 2 Hart & Hickman, PC
Copyright:© 2013 National Geographic Society, i-cubed
SITE LOCATION MAP
FULBRIGHT LABORATORIES BROWNFIELDS PROPERTY1919, 1923, AND 1933 SOUTH BOULEVARDCHARLOTTE, NORTH CAROLINA
DATE: 8-9-21
JOB NO: SLC-001
REVISION NO: 0
FIGURE NO: 1
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007 (p) 704-586-0373 (f)License # C-1269 / # C-245 Geology
TITLE
PROJECT
0 2,000 4,000
SCALE IN FEET
SITE
Path: S:\AAA-Master Projects\Southern Land Company\SLC-001 South Boulevard Assemblage\Phase I ESA\Figures\Figure-1.mxdN
U.S.G.S. QUADRANGLE MAP
CHARLOTTE WEST, NORTH CAROLINA 2013CHARLOTTE EAST, NORTH CAROLINA 2013
QUADRANGLE7.5 MINUTE SERIES (TOPOGRAPHIC)
REVISION NO. 0
JOB NO. SLC-001
DATE: 5-23-22
FIGURE NO. 2
FULBRIGHT LABORATORIES BROWNFIELDS PROPERTY
1919, 1923, AND 1933 SOUTH BOULEVARD
CHARLOTTE, NORTH CAROLINA
SITE AND TEMPORARY WELL LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
APPROXIMATE LOCATION OF
CHEMICAL MIXING BUILDING (1951
AND 1953 SANBORN MAPS)
APPROXIMATE LOCATION OF
GASOLINE UST (1929 SANBORN
MAP)
APPROXIMATE LOCATION OF
GREASE RECEPTACLE
DUMPSTER
POLE-MOUNTED TRANSFORMER
TEMPORARY MONITORING WELL
PROPOSED ELEVATOR PIT AND
GENERATOR ROOM LOCATION
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES:
1. AERIAL IMAGERY OBTAINED FROM MECKLENBURG
COUNTY GIS (2021).
2. UST = UNDERGROUND STORAGE TANK
VACANT COMMERCIAL
(1923 SOUTH BOULEVARD)
TYBER CREEK PUB
(1933 SOUTH BOULEVARD)
COVERED PATIO
MULTI-TENANT COMMERCIAL
(1923 SOUTH BOULEVARD)
SULLIVAN'S STEAKHOUSE
(1928 SOUTH BOULEVARD)
H&H AUTO
(1909 SOUTH BOULEVARD)
VACANT COMMERCIAL PROPERTY
(1912 CLEVELAND AVENUE)
MAKE-A-WISH FOUNDATION
(217 E. TREMONT AVENUE)
MULTI-TENANT COMMERCIAL
(2102 SOUTH BOULEVARD)
ATHERTON BUSINESS PARK
(200 E. TREMONT AVENUE)
E.

T
R
EM
O
N
T

A
V
E
N
U
E
SOUT
H
B
O
ULEV
A
R
D
PAVED PARKING
SOUTH BOULEVARDPROPOSED ELEVATOR PIT
PROPOSED SUB-GRADE
GENERATOR ROOM
TMW-8
TMW-6
TMW-7
TMW-4
TMW-5
S:\AAA-Master Projects\Southern Land Company (SLC)\SLC-001 South Boulevard Assemblage\April 2022 Temp Well Installation\Figures\SLC.001_20220523.dwg, FIG 2 (2), 5/23/2022 10:01:23 AM, shaynesMULTI-TENANT
COMMERCIAL BUILDING(1910 SOUTH BOULEVARD)
ATHERTON MILL/PARKS CRAMER PROPERTY(2000-2140 SOUTH BOULEVARD)

Appendix A

Boring Logs & Well Abandonment Records
NOTES:
generated using GroundLogs.online
Client:
Project:
Address:
SLC (Southern Land Company)
SLC.001
1919, 1923, & 1933 S. Blvd.,Charlotte, NC
WELL LOG
Well No.
Page:
TMW-4
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/28/22
3/28/22
Ameriprobe
Other
Hand Auger
Jon Allen
Adam Michalak
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
5.0
3.25
2.13
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
5.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Asphalt
(0.3') Concrete
(1') SILT (ML); trace medium-coarse sand, few clay, medium stiff, moist, red brown
with medium brown
(2') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, red brown with
medium brown
(4') Lean CLAY (CL); trace medium-coarse sand, some silt, medium plasticity, soft,
wet, medium gray with medium brown
(5') Boring terminated
8.1
8.0
7.7
7.6
0
5
10
GR
NOTES: Elevated PID readings appear to be due to humidity.
generated using GroundLogs.online
Client:
Project:
Address:
SLC (Southern Land Company)
SLC.001
1919, 1923, & 1933 S. Blvd.,Charlotte, NC
WELL LOG
Well No.
Page:
TMW-5
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/28/22
3/28/22
Ameriprobe
Other
Hand Auger
Jon Allen
Adam Michalak
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
5.0
3.25
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
5.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
(0') Asphalt
(0.3') Concrete
(1') SILT (ML); trace medium-coarse sand, few clay, medium stiff, moist, red brown
with medium brown
(2') Lean CLAY (CL); some silt, medium plasticity, medium stiff, moist, red brown with
medium brown
(4') Lean CLAY (CL); trace medium-coarse sand, some silt, medium plasticity, soft,
moist, medium gray with medium brown
(5') Boring terminated
134.8
34.8
19.6
21.5
0
5
10
GR
NOTES: Hole precleared to 5.0' on 3/28/22 by Ameriprobe using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
SLC (Southern Land Company)
SLC.001
1919, 1923, & 1933 S. Blvd.,Charlotte, NC
WELL LOG
Well No.
Page:
TMW-6
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/28/22
3/28/22
Ameriprobe
Direct Push
Geoprobe 7720DT
Jon Allen
Adam Michalak
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
20.0
2.25
DP, GR
3.16
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
20.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
25
GR
DP
DP
DP
5.00
5.00
5.00
5.00
(0') Asphalt
(0.3') Well-graded GRAVEL (GW); very loose, dry, gray
(0.8') SILT (ML); trace medium-coarse sand, few clay, stiff, moist, reddish-dark brown
(2') Lean CLAY (CL); few silt, medium plasticity, stiff, moist, red brown with medium
gray
(3') some organics present
(4') Lean CLAY (CL); some silt, medium plasticity, very stiff, moist, green-gray with
green brown mottling
(5') Lean CLAY (CL); few silt, medium plasticity, very stiff, moist, green-gray with
green-brown and red mottling
(7') Lean CLAY with sand (CL); some fine sand, medium plasticity, very stiff, moist,
light gray with yellow-brown, dark brown, and red-brown mottling
(17') color change to light brown
(20') Boring terminated
9.0
11.8
10.2
10.6
10.2
9.0
8.6
9.1
9.4
0
5
10
15
20
25
(16') changed from moist to wet
NOTES: Hole precleared to 5.0' on 3/28/22 by Ameriprobe using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
SLC (Southern Land Company)
SLC.001
1919, 1923, & 1933 S. Blvd.,Charlotte, NC
WELL LOG
Well No.
Page:
TMW-7
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/28/22
3/28/22
Ameriprobe
Direct Push
Geoprobe 7720DT
Jon Allen
Adam Michalak
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
15.0
2.25
DP, GR
1.52
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
15.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR
DP
DP
5.00
5.00
5.00
(0') Asphalt
(0.3') Well-graded GRAVEL (GW); very loose, dry, gray
(0.8') Silty SAND (SM); mostly fine-coarse grained sand, some clay, loose, moist,
dark to medium brown
(1.5') becomes wet
(2') Lean CLAY (CL); trace coarse sand, some silt, medium plasticity, soft, wet,
red-brown with dark brown
(4') Lean CLAY (CL); some silt, medium plasticity, medium stiff, wet, gray
(5') color change to green-gray with green-brown mottling
(7') Sandy lean CLAY (CL); some fine sand, medium plasticity, very stiff, moist, light
gray with some green mottling
(13') color change to yellow-brown with light gray
(15') Boring terminated
6.3
5.6
5.6
6.4
5.4
6.7
7.2
7.4
8.0
0
5
10
15
20
NOTES: Hole precleared to 5.0' on 3/28/22 by Ameriprobe using hand auger.
generated using GroundLogs.online
Client:
Project:
Address:
SLC (Southern Land Company)
SLC.001
1919, 1923, & 1933 S. Blvd.,Charlotte, NC
WELL LOG
Well No.
Page:
TMW-8
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
3/28/22
3/28/22
Ameriprobe
Direct Push
Geoprobe 7720DT
Jon Allen
Adam Michalak
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Top of Casing Elev. (ft):
Location (X,Y):
15.0
2.25
DP, GR
5.05
Well Depth (ft):
Well Diameter (in):
Screen Slot (in):
Riser Material:
Screen Material:
Seal Material(s):
Filter Type:
15.0
1.0
0.010
Sch 40 PVC
Sch 40 PVC Slotted
Bent. Chips
Sand pack
DEPTH (ft)LITHOLOGYWATER LEVELWELLCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
5
10
15
20
GR
DP
DP
5.00
5.00
5.00
(0') Asphalt
(0.3') Well-graded GRAVEL (GW); very loose, dry, gray
(0.8') Silty SAND (SM); some clay, loose, moist, dark to medium brown
(1.5') Lean CLAY (CL); few medium-coarse sand, some silt, medium plasticity, soft,
wet, red brown with dark brown and slight gray
(3') color change to yellow-brown with medium brown and green-gray
(4') Lean CLAY (CL); some fine-medium sand, some silt, medium plasticity, medium
stiff, wet, dark brown with yellow and red-brown
(5') color change to green-gray
(6') Lean CLAY with sand (CL); some fine sand, medium plasticity, very stiff, moist,
medium gray with green mottling
(12') color change to green-gray with yellow-brown and green-brown mottling
(15') Boring terminated
7.5
6.7
6.6
6.6
6.2
6.7
7.1
7.6
7.7
0
5
10
15
20
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1.Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3.Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8.Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9.Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
John Allen
4196-B ~1.1
AmeriProbe
40 lbs of Neat Cement
4/4/2022
Pulled all pipe from the hole, then grouted up the
borehole to the surface.
Tyber Creek Pub
1933 South Blvd., Charlotte, NC, 28203 4/13/2022
Mecklenburg
35.2097671 80.8591359
TMW-6
20
2 1/4''
13
5'
15'
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1.Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3.Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8.Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9.Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
John Allen
4196-B ~0.3
AmeriProbe
40 lbs of Neat Cement
4/4/2022
Pulled all pipe from the hole, then grouted up the
borehole to the surface.
Tyber Creek Pub
1933 South Blvd., Charlotte, NC, 28203 4/13/2022
Mecklenburg
35.2097271 80.8591775
TMW-7
15
2 1/4''
13
5'
10'
WELL ABANDONMENT RECORD
Form GW-30 North Carolina Department of Environmental Quality - Division of Water Resources Revised 2-22-2016
1.Well Contractor Information:
Well Contractor Name (or well owner personally abandoning well on his/her property)
NC Well Contractor Certification Number
Company Name
2.Well Construction Permit #:
List all applicable well construction permits (i.e. UIC, County, State, Variance, etc.) if known
3.Well use (check well use):
Water Supply Well:
□Agricultural □Municipal/Public
□Geothermal (Heating/Cooling Supply)□Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared)
□Irrigation
Non-Water Supply Well:
□Monitoring □Recovery
Injection Well:
□Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier
□Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop)□Tracer
□Geothermal (Heating/Cooling Return) □Other (explain under 7g)
4. Date well(s) abandoned:
5a. Well location:
Facility/Owner Name Facility ID# (if applicable)
Physical Address, City, and Zip
County Parcel Identification No. (PIN)
5b. Latitude and longitude in degrees/minutes/seconds or decimal degrees:
(if well field, one lat/long is sufficient)
N W
CONSTRUCTION DETAILS OF WELL(S) BEING ABANDONED
Attach well construction record(s) if available. For multiple injection or non-water supply wells
ONLY with the same construction/abandonment, you can submit one form.
6a. Well ID#:
6b. Total well depth: (ft.)
6c. Borehole diameter: (in.)
6d. Water level below ground surface: (ft.)
6e. Outer casing length (if known): (ft.)
6f. Inner casing/tubing length (if known): (ft.)
6g. Screen length (if known): (ft.)
WELL ABANDONMENT DETAILS
7a. For Geoprobe/DPT or Closed-Loop Geothermal Wells having the same
well construction/depth, only 1 GW-30 is needed. Indicate TOTAL NUMBER of
wells abandoned:
7b. Approximate volume of water remaining in well(s): (gal.)
FOR WATER SUPPLY WELLS ONLY:
7c. Type of disinfectant used:
7d. Amount of disinfectant used:
7e. Sealing materials used (check all that apply):
□Neat Cement Grout □Bentonite Chips or Pellets
□Sand Cement Grout □Dry Clay
□Concrete Grout □Drill Cuttings
□Specialty Grout □Gravel
□Bentonite Slurry □Other (explain under 7g)
7f. For each material selected above, provide amount of materials used:
7g. Provide a brief description of the abandonment procedure:
8.Certification:
Signature of Certified Well Contractor or Well Owner Date
By signing this form, I hereby certify that the well(s) was (were) abandoned in
accordance with 15A NCAC 02C .0100 or 2C .0200 Well Construction Standards
and that a copy of this record has been provided to the well owner.
9.Site diagram or additional well details:
You may use the back of this page to provide additional well site details or well
abandonment details. You may also attach additional pages if necessary.
SUBMITTAL INSTRUCTIONS
10a. For All Wells: Submit this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Information Processing Unit,
1617 Mail Service Center, Raleigh, NC 27699-1617
10b. For Injection Wells: In addition to sending the form to the address in 10a
above, also submit one copy of this form within 30 days of completion of well
abandonment to the following:
Division of Water Resources, Underground Injection Control Program,
1636 Mail Service Center, Raleigh, NC 27699-1636
10c. For Water Supply & Injection Wells: In addition to sending the form to the
address(es) above, also submit one copy of this form within 30 days of completion
of well abandonment to the county health department of the county where
abandoned.
For Internal Use ONLY:
John Allen
4196-B ~0.3
AmeriProbe
40 lbs of Neat Cement
4/4/2022
Pulled all pipe from the hole, then grouted up the
borehole to the surface.
Tyber Creek Pub
1933 South Blvd., Charlotte, NC, 28203 4/13/2022
Mecklenburg
35.2098071 80.8592221
TMW-8
15
2 1/4''
13
5'
10'

Appendix B

Groundwater Sampling Forms

Appendix C

Laboratory Analytical Reports

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/15/2022
Hart & Hickman (Charlotte) Bo Cappleman
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-094-0013 Client Project Description: SLC.001
Dear Bo Cappleman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/20/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 45
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-094-0013
Page 2 of 45
Report Number:
Sample Summary Table
Client Project Description:
22-094-0013
SLC.001
Lab No Client Sample ID Matrix Date Collected Date Received
04/01/2022 10:55Aqueous 97580 TMW-7 04/20/2022 12:50
04/01/2022 10:10Aqueous 97581 TMW-8 04/20/2022 12:50
04/01/2022Aqueous 97582 Trip Blank 04/20/2022 12:50
Page 3 of 45
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-094-0013
Report Limit
Project:SLC.001
V 97580TMW-7
J2.53 04/07/2022 18:476020BArsenicµg/L 2.45
417 04/07/2022 18:476020BBariumµg/L 17.0
181 04/15/2022 08:216020BDissolved Barium µg/L 17.0
22.4 04/07/2022 18:476020BChromiumµg/L 5.00
24.9 04/07/2022 18:476020BLeadµg/L 2.50
5.27 04/15/2022 08:216020BDissolved Lead µg/L 2.50
9.27 04/08/2022 21:198260DAcetoneµg/L 1.80
J0.221 04/08/2022 21:198260DTetrachloroetheneµg/L 0.220
0.554 04/08/2022 21:198260DTrichloroetheneµg/L 0.180
V 97581TMW-8
7.80 04/07/2022 18:546020BArsenicµg/L 2.45
1.20 04/15/2022 08:086020BDissolved Arsenic µg/L 0.490
820 04/07/2022 18:546020BBariumµg/L 17.0
140 04/15/2022 08:086020BDissolved Barium µg/L 3.40
235 04/07/2022 18:546020BChromiumµg/L 5.00
J1.25 04/15/2022 08:086020BDissolved Chromium µg/L 1.00
171 04/07/2022 18:546020BLeadµg/L 2.50
1.41 04/15/2022 08:086020BDissolved Lead µg/L 0.500
6.75 04/08/2022 21:448260DAcetoneµg/L 1.80
J0.207 04/08/2022 21:448260Dcis-1,2-Dichloroethene µg/L 0.200
J0.449 04/08/2022 21:448260D2-Hexanone µg/L 0.380
0.617 04/08/2022 21:448260DTetrachloroetheneµg/L 0.220
0.832 04/08/2022 21:448260DTrichloroetheneµg/L 0.180
Page 4 of 45

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: SLC.001 Lab Report Number: 22-094-0013
Date: 4/13/2022
Metals Analyses Method 6020B Sample 97580 (TMW-7) QC Batch No: V17145/V17088
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 97581 (TMW-8) QC Batch No: V17145/V17088
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Semivolatile Organic Compounds - GC/MS Method 8270E Analyte: Benzoic Acid
QC Batch No: V17342/V17141 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
2.53 which calculates to a recovery of 5%. Benzoic Acid is a known poor performer.
Analyte: Benzoic Acid QC Batch No: V17342/V17141
Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 4.62 which calculates to a recovery of 9%. Benzoic Acid is a known poor performer.
Analyte: Pyridine QC Batch No: V17342/V17141 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 5 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
2.53 J µg/L 2.45 5.00Arsenic 5 04/07/22 18:47 6020BEDV
<2.45 µg/L 2.45 5.00Dissolved Arsenic 5 04/15/22 08:21 6020BEDV
417 µg/L 17.0 50.0Barium 5 04/07/22 18:47 6020BEDV
181 µg/L 17.0 50.0Dissolved Barium 5 04/15/22 08:21 6020BEDV
<0.750 µg/L 0.750 5.00Cadmium 5 04/07/22 18:47 6020BEDV
<0.750 µg/L 0.750 5.00
Dissolved Cadmium 5 04/15/22 08:21 6020BEDV
22.4 µg/L 5.00 10.0Chromium 5 04/07/22 18:47 6020BEDV
<5.00 µg/L 5.00 10.0Dissolved Chromium 5 04/15/22 08:21 6020BEDV
24.9 µg/L 2.50 5.00Lead 5 04/07/22 18:47 6020BEDV
5.27 µg/L 2.50 5.00Dissolved Lead 5 04/15/22 08:21 6020BEDV
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 04/06/22 16:15 7470AEDV
<0.00007 mg/L 0.00007 0.00020Dissolved Mercury 1 04/15/22 12:43 7470AEDV
<11.5 µg/L 11.5 25.0
Selenium 5 04/07/22 18:47 6020BEDV
<11.5 µg/L 11.5 25.0Dissolved Selenium 5 04/15/22 08:21 6020BEDV
<0.650 µg/L 0.650 5.00Silver 5 04/07/22 18:47 6020BEDV
<0.650 µg/L 0.650 5.00Dissolved Silver 5 04/15/22 08:21 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 6 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
9.27 µg/L 1.80 5.00Acetone 1 04/08/22 21:19 V17236JLB
<2.00 µg/L 2.00 5.00Acrolein 1 04/08/22 21:19 V17236JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 04/08/22 21:19 V17236JLB
<0.180 µg/L 0.180 0.500Benzene 1 04/08/22 21:19 V17236JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/08/22 21:19 V17236JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/08/22 21:19 V17236JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/08/22 21:19 V17236JLB
<1.50 µg/L 1.50 5.00Bromoform 1 04/08/22 21:19 V17236JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 04/08/22 21:19 V17236JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 04/08/22 21:19 V17236JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/08/22 21:19 V17236JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/08/22 21:19 V17236JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 04/08/22 21:19 V17236JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/08/22 21:19 V17236JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/08/22 21:19 V17236JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 04/08/22 21:19 V17236JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 04/08/22 21:19 V17236JLB
<0.220 µg/L 0.220 0.500Chloroform 1 04/08/22 21:19 V17236JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 04/08/22 21:19 V17236JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/08/22 21:19 V17236JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/08/22 21:19 V17236JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 04/08/22 21:19 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 7 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/08/22 21:19 V17236JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/08/22 21:19 V17236JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/08/22 21:19 V17236JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/08/22 21:19 V17236JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/08/22 21:19 V17236JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/08/22 21:19 V17236JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/08/22 21:19 V17236JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/08/22 21:19 V17236JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 04/08/22 21:19 V17236JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/08/22 21:19 V17236JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/08/22 21:19 V17236JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/08/22 21:19 V17236JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/08/22 21:19 V17236JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/08/22 21:19 V17236JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/08/22 21:19 V17236JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 04/08/22 21:19 V17236JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/08/22 21:19 V17236JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/08/22 21:19 V17236JLB
<42.0 µg/L 42.0 200Ethanol 1 04/08/22 21:19 V17236JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 04/08/22 21:19 V17236JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 04/08/22 21:19 V17236JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 04/08/22 21:19 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 8 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 04/08/22 21:19 V17236JLB
<0.380 µg/L 0.380 5.002-Hexanone 1 04/08/22 21:19 V17236JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 04/08/22 21:19 V17236JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/08/22 21:19 V17236JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/08/22 21:19 V17236JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 04/08/22 21:19 V17236JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 04/08/22 21:19 V17236JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 04/08/22 21:19 V17236JLB
<0.470 µg/L 0.470 1.00
Naphthalene 1 04/08/22 21:19 V17236JLB
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/08/22 21:19 V17236JLB
<0.220 µg/L 0.220 0.500Styrene 1 04/08/22 21:19 V17236JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/08/22 21:19 V17236JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/08/22 21:19 V17236JLB
0.221 J µg/L 0.220 0.500Tetrachloroethene 1 04/08/22 21:19 V17236JLB
<0.220 µg/L 0.220 0.500Toluene 1 04/08/22 21:19 V17236JLB
<0.380 µg/L 0.380 2.00
1,2,3-Trichlorobenzene 1 04/08/22 21:19 V17236JLB
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 04/08/22 21:19 V17236JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/08/22 21:19 V17236JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/08/22 21:19 V17236JLB
0.554 µg/L 0.180 0.500Trichloroethene 1 04/08/22 21:19 V17236JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/08/22 21:19 V17236JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 04/08/22 21:19 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 9 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/08/22 21:19 V17236JLB
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 04/08/22 21:19 V17236JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/08/22 21:19 V17236JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 04/08/22 21:19 V17236JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 04/08/22 21:19 V17236JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 04/08/22 21:19 V17236
Surrogate: 4-Bromofluorobenzene 103 Limits: 80-124%04/08/22 21:191 JLB V17236
Surrogate: Dibromofluoromethane 98.0 Limits: 75-129%04/08/22 21:191 JLB V17236
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 63-136%04/08/22 21:191 JLB V17236
Surrogate: Toluene-d8 97.4 Limits: 77-123%04/08/22 21:191 JLB V17236
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<8.08 µg/L 8.08 22.7Acenaphthene 1 04/11/22 18:23 V17342ANG
<7.88 µg/L 7.88 22.7Acenaphthylene 1 04/11/22 18:23 V17342ANG
<8.10 µg/L 8.10 56.8Aniline 1 04/11/22 18:23 V17342ANG
<7.49 µg/L 7.49 11.4Anthracene 1 04/11/22 18:23 V17342ANG
<6.44 µg/L 6.44 11.4Benzo(a)anthracene 1 04/11/22 18:23 V17342ANG
<5.32 µg/L 5.32 11.4Benzo(a)pyrene 1 04/11/22 18:23 V17342ANG
<5.15 µg/L 5.15 11.4
Benzo(b)fluoranthene 1 04/11/22 18:23 V17342ANG
<4.83 µg/L 4.83 11.4Benzo(g,h,i)perylene 1 04/11/22 18:23 V17342ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 10 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<5.34 µg/L 5.34 11.4Benzo(k)fluoranthene 1 04/11/22 18:23 V17342ANG
<13.1 µg/L 13.1 114Benzoic Acid 1 04/11/22 18:23 V17342ANG
<9.80 µg/L 9.80 11.4Benzyl alcohol 1 04/11/22 18:23 V17342ANG
<6.46 µg/L 6.46 11.4Bis(2-Chloroethoxy)methane 1 04/11/22 18:23 V17342ANG
<8.32 µg/L 8.32 11.4Bis(2-Chloroethyl)ether 1 04/11/22 18:23 V17342ANG
<7.51 µg/L 7.51 11.4Bis(2-Chloroisopropyl)ether 1 04/11/22 18:23 V17342ANG
<10.0 µg/L 10.0 11.4Bis(2-ethylhexyl)phthalate 1 04/11/22 18:23 V17342ANG
<7.11 µg/L 7.11 22.74-Bromophenyl phenyl ether 1 04/11/22 18:23 V17342ANG
<3.35 µg/L 3.35 11.4
Butyl benzyl phthalate 1 04/11/22 18:23 V17342ANG
<5.96 µg/L 5.96 11.44-Chloro-3-methylphenol 1 04/11/22 18:23 V17342ANG
<6.18 µg/L 6.18 11.44-Chloroaniline 1 04/11/22 18:23 V17342ANG
<8.38 µg/L 8.38 22.72-Chloronaphthalene 1 04/11/22 18:23 V17342ANG
<7.50 µg/L 7.50 11.42-Chlorophenol 1 04/11/22 18:23 V17342ANG
<7.93 µg/L 7.93 22.74-Chlorophenyl phenyl ether 1 04/11/22 18:23 V17342ANG
<6.13 µg/L 6.13 11.4Chrysene 1 04/11/22 18:23 V17342ANG
<6.82 µg/L 6.82 22.7
Dibenz(a,h)anthracene 1 04/11/22 18:23 V17342ANG
<5.77 µg/L 5.77 22.7Dibenzofuran 1 04/11/22 18:23 V17342ANG
<6.74 µg/L 6.74 11.41,2-Dichlorobenzene 1 04/11/22 18:23 V17342ANG
<6.65 µg/L 6.65 11.41,3-Dichlorobenzene 1 04/11/22 18:23 V17342ANG
<6.74 µg/L 6.74 11.41,4-Dichlorobenzene 1 04/11/22 18:23 V17342ANG
<7.52 µg/L 7.52 11.43,3'-Dichlorobenzidine 1 04/11/22 18:23 V17342ANG
<6.32 µg/L 6.32 11.42,4-Dichlorophenol 1 04/11/22 18:23 V17342ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 11 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<10.6 µg/L 10.6 22.7Diethyl phthalate 1 04/11/22 18:23 V17342ANG
<8.91 µg/L 8.91 11.4Dimethyl phthalate 1 04/11/22 18:23 V17342ANG
<12.4 µg/L 12.4 22.72,4-Dimethylphenol 1 04/11/22 18:23 V17342ANG
<8.38 µg/L 8.38 11.4Di-n-butyl phthalate 1 04/11/22 18:23 V17342ANG
<11.3 µg/L 11.3 34.14,6-Dinitro-2-methylphenol 1 04/11/22 18:23 V17342ANG
<12.0 µg/L 12.0 34.12,4-Dinitrophenol 1 04/11/22 18:23 V17342ANG
<5.93 µg/L 5.93 11.42,4-Dinitrotoluene 1 04/11/22 18:23 V17342ANG
<6.70 µg/L 6.70 22.72,6-Dinitrotoluene 1 04/11/22 18:23 V17342ANG
<5.71 µg/L 5.71 11.4
Di-n-Octyl Phthalate 1 04/11/22 18:23 V17342ANG
<6.87 µg/L 6.87 11.4Fluoranthene 1 04/11/22 18:23 V17342ANG
<8.29 µg/L 8.29 11.4Fluorene 1 04/11/22 18:23 V17342ANG
<6.53 µg/L 6.53 22.7Hexachlorobenzene 1 04/11/22 18:23 V17342ANG
<6.67 µg/L 6.67 22.7Hexachlorobutadiene 1 04/11/22 18:23 V17342ANG
<6.70 µg/L 6.70 22.7Hexachlorocyclopentadiene 1 04/11/22 18:23 V17342ANG
<5.95 µg/L 5.95 11.4Hexachloroethane 1 04/11/22 18:23 V17342ANG
<7.07 µg/L 7.07 11.4
Indeno(1,2,3-cd)pyrene 1 04/11/22 18:23 V17342ANG
<7.65 µg/L 7.65 11.4Isophorone 1 04/11/22 18:23 V17342ANG
<8.36 µg/L 8.36 11.41-Methylnaphthalene 1 04/11/22 18:23 V17342ANG
<7.89 µg/L 7.89 11.42-Methylnaphthalene 1 04/11/22 18:23 V17342ANG
<6.00 µg/L 6.00 11.42-Methylphenol 1 04/11/22 18:23 V17342ANG
<2.82 µg/L 2.82 11.43&4 Methylphenol 1 04/11/22 18:23 V17342ANG
<8.98 µg/L 8.98 11.4Naphthalene 1 04/11/22 18:23 V17342ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 12 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-7
97580 Matrix:
4/1/2022 10:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<5.61 µg/L 5.61 11.42-Nitroaniline 1 04/11/22 18:23 V17342ANG
<5.19 µg/L 5.19 11.43-Nitroaniline 1 04/11/22 18:23 V17342ANG
<5.81 µg/L 5.81 11.44-Nitroaniline 1 04/11/22 18:23 V17342ANG
<8.98 µg/L 8.98 11.4Nitrobenzene 1 04/11/22 18:23 V17342ANG
<6.26 µg/L 6.26 11.42-Nitrophenol 1 04/11/22 18:23 V17342ANG
<3.20 µg/L 3.20 11.44-Nitrophenol 1 04/11/22 18:23 V17342ANG
<7.40 µg/L 7.40 11.4N-Nitrosodimethylamine 1 04/11/22 18:23 V17342ANG
<12.4 µg/L 12.4 22.7N-Nitrosodiphenylamine 1 04/11/22 18:23 V17342ANG
<9.19 µg/L 9.19 22.7
N-Nitroso-di-n-propylamine 1 04/11/22 18:23 V17342ANG
<11.1 µg/L 11.1 56.8Pentachlorophenol 1 04/11/22 18:23 V17342ANG
<7.23 µg/L 7.23 11.4Phenanthrene 1 04/11/22 18:23 V17342ANG
<3.26 µg/L 3.26 11.4Phenol 1 04/11/22 18:23 V17342ANG
<6.18 µg/L 6.18 11.4Pyrene 1 04/11/22 18:23 V17342ANG
<6.06 µg/L 6.06 11.4Pyridine 1 04/11/22 18:23 V17342ANG
<7.13 µg/L 7.13 11.41,2,4-Trichlorobenzene 1 04/11/22 18:23 V17342ANG
<6.59 µg/L 6.59 22.7
2,4,5-Trichlorophenol 1 04/11/22 18:23 V17342ANG
<7.14 µg/L 7.14 22.72,4,6-Trichlorophenol 1 04/11/22 18:23 V17342ANG
8270ESurrogate: Phenol-d5 25.6 Limits: 11-100%04/11/22 18:231 ANG
Surrogate: 2-Fluorobiphenyl 53.9 Limits: 44-119%04/11/22 18:231 ANG V17342
Surrogate: 2-Fluorophenol 39.4 Limits: 19-119%04/11/22 18:231 ANG V17342
Surrogate: Nitrobenzene-d5 54.8 Limits: 44-120%04/11/22 18:231 ANG V17342
Surrogate: 4-Terphenyl-d14 69.2 Limits: 50-134%04/11/22 18:231 ANG V17342
Surrogate: 2,4,6-Tribromophenol 68.0 Limits: 43-140%04/11/22 18:231 ANG V17342
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 13 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
7.80 µg/L 2.45 5.00Arsenic 5 04/07/22 18:54 6020BEDV
1.20 µg/L 0.490 1.00Dissolved Arsenic 1 04/15/22 08:08 6020BEDV
820 µg/L 17.0 50.0Barium 5 04/07/22 18:54 6020BEDV
140 µg/L 3.40 10.0Dissolved Barium 1 04/15/22 08:08 6020BEDV
<0.750 µg/L 0.750 5.00Cadmium 5 04/07/22 18:54 6020BEDV
<0.150 µg/L 0.150 1.00
Dissolved Cadmium 1 04/15/22 08:08 6020BEDV
235 µg/L 5.00 10.0Chromium 5 04/07/22 18:54 6020BEDV
1.25 J µg/L 1.00 2.00Dissolved Chromium 1 04/15/22 08:08 6020BEDV
171 µg/L 2.50 5.00Lead 5 04/07/22 18:54 6020BEDV
1.41 µg/L 0.500 1.00Dissolved Lead 1 04/15/22 08:08 6020BEDV
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 04/06/22 16:17 7470AEDV
<0.00007 mg/L 0.00007 0.00020Dissolved Mercury 1 04/15/22 12:28 7470AEDV
<11.5 µg/L 11.5 25.0
Selenium 5 04/07/22 18:54 6020BEDV
<2.30 µg/L 2.30 5.00Dissolved Selenium 1 04/15/22 08:08 6020BEDV
<0.650 µg/L 0.650 5.00Silver 5 04/07/22 18:54 6020BEDV
<0.130 µg/L 0.130 1.00Dissolved Silver 1 04/15/22 08:08 6020BEDV
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 14 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
6.75 µg/L 1.80 5.00Acetone 1 04/08/22 21:44 V17236JLB
<2.00 µg/L 2.00 5.00Acrolein 1 04/08/22 21:44 V17236JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 04/08/22 21:44 V17236JLB
<0.180 µg/L 0.180 0.500Benzene 1 04/08/22 21:44 V17236JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/08/22 21:44 V17236JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/08/22 21:44 V17236JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/08/22 21:44 V17236JLB
<1.50 µg/L 1.50 5.00Bromoform 1 04/08/22 21:44 V17236JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 04/08/22 21:44 V17236JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 04/08/22 21:44 V17236JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/08/22 21:44 V17236JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/08/22 21:44 V17236JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 04/08/22 21:44 V17236JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/08/22 21:44 V17236JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/08/22 21:44 V17236JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 04/08/22 21:44 V17236JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 04/08/22 21:44 V17236JLB
<0.220 µg/L 0.220 0.500Chloroform 1 04/08/22 21:44 V17236JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 04/08/22 21:44 V17236JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/08/22 21:44 V17236JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/08/22 21:44 V17236JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 04/08/22 21:44 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 15 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/08/22 21:44 V17236JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/08/22 21:44 V17236JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/08/22 21:44 V17236JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/08/22 21:44 V17236JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/08/22 21:44 V17236JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/08/22 21:44 V17236JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/08/22 21:44 V17236JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/08/22 21:44 V17236JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 04/08/22 21:44 V17236JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/08/22 21:44 V17236JLB
0.207 J µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/08/22 21:44 V17236JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/08/22 21:44 V17236JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/08/22 21:44 V17236JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/08/22 21:44 V17236JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/08/22 21:44 V17236JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 04/08/22 21:44 V17236JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/08/22 21:44 V17236JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/08/22 21:44 V17236JLB
<42.0 µg/L 42.0 200Ethanol 1 04/08/22 21:44 V17236JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 04/08/22 21:44 V17236JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 04/08/22 21:44 V17236JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 04/08/22 21:44 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 16 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 04/08/22 21:44 V17236JLB
0.449 J µg/L 0.380 5.002-Hexanone 1 04/08/22 21:44 V17236JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 04/08/22 21:44 V17236JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/08/22 21:44 V17236JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/08/22 21:44 V17236JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 04/08/22 21:44 V17236JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 04/08/22 21:44 V17236JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 04/08/22 21:44 V17236JLB
<0.470 µg/L 0.470 1.00
Naphthalene 1 04/08/22 21:44 V17236JLB
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/08/22 21:44 V17236JLB
<0.220 µg/L 0.220 0.500Styrene 1 04/08/22 21:44 V17236JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/08/22 21:44 V17236JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/08/22 21:44 V17236JLB
0.617 µg/L 0.220 0.500Tetrachloroethene 1 04/08/22 21:44 V17236JLB
<0.220 µg/L 0.220 0.500Toluene 1 04/08/22 21:44 V17236JLB
<0.380 µg/L 0.380 2.00
1,2,3-Trichlorobenzene 1 04/08/22 21:44 V17236JLB
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 04/08/22 21:44 V17236JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/08/22 21:44 V17236JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/08/22 21:44 V17236JLB
0.832 µg/L 0.180 0.500Trichloroethene 1 04/08/22 21:44 V17236JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/08/22 21:44 V17236JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 04/08/22 21:44 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 17 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/08/22 21:44 V17236JLB
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 04/08/22 21:44 V17236JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/08/22 21:44 V17236JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 04/08/22 21:44 V17236JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 04/08/22 21:44 V17236JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 04/08/22 21:44 V17236
Surrogate: 4-Bromofluorobenzene 100 Limits: 80-124%04/08/22 21:441 JLB V17236
Surrogate: Dibromofluoromethane 102 Limits: 75-129%04/08/22 21:441 JLB V17236
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 63-136%04/08/22 21:441 JLB V17236
Surrogate: Toluene-d8 96.6 Limits: 77-123%04/08/22 21:441 JLB V17236
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<7.58 µg/L 7.58 21.3Acenaphthene 1 04/11/22 18:45 V17342ANG
<7.39 µg/L 7.39 21.3Acenaphthylene 1 04/11/22 18:45 V17342ANG
<7.59 µg/L 7.59 53.2Aniline 1 04/11/22 18:45 V17342ANG
<6.96 µg/L 6.96 10.6Anthracene 1 04/11/22 18:45 V17342ANG
<5.99 µg/L 5.99 10.6Benzo(a)anthracene 1 04/11/22 18:45 V17342ANG
<4.95 µg/L 4.95 10.6Benzo(a)pyrene 1 04/11/22 18:45 V17342ANG
<4.79 µg/L 4.79 10.6
Benzo(b)fluoranthene 1 04/11/22 18:45 V17342ANG
<4.49 µg/L 4.49 10.6Benzo(g,h,i)perylene 1 04/11/22 18:45 V17342ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 18 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<4.96 µg/L 4.96 10.6Benzo(k)fluoranthene 1 04/11/22 18:45 V17342ANG
<12.2 µg/L 12.2 106Benzoic Acid 1 04/11/22 18:45 V17342ANG
<9.12 µg/L 9.12 10.6Benzyl alcohol 1 04/11/22 18:45 V17342ANG
<6.01 µg/L 6.01 10.6Bis(2-Chloroethoxy)methane 1 04/11/22 18:45 V17342ANG
<7.74 µg/L 7.74 10.6Bis(2-Chloroethyl)ether 1 04/11/22 18:45 V17342ANG
<6.99 µg/L 6.99 10.6Bis(2-Chloroisopropyl)ether 1 04/11/22 18:45 V17342ANG
<9.33 µg/L 9.33 10.6Bis(2-ethylhexyl)phthalate 1 04/11/22 18:45 V17342ANG
<6.67 µg/L 6.67 21.34-Bromophenyl phenyl ether 1 04/11/22 18:45 V17342ANG
<3.12 µg/L 3.12 10.6
Butyl benzyl phthalate 1 04/11/22 18:45 V17342ANG
<5.54 µg/L 5.54 10.64-Chloro-3-methylphenol 1 04/11/22 18:45 V17342ANG
<5.75 µg/L 5.75 10.64-Chloroaniline 1 04/11/22 18:45 V17342ANG
<7.86 µg/L 7.86 21.32-Chloronaphthalene 1 04/11/22 18:45 V17342ANG
<6.97 µg/L 6.97 10.62-Chlorophenol 1 04/11/22 18:45 V17342ANG
<7.44 µg/L 7.44 21.34-Chlorophenyl phenyl ether 1 04/11/22 18:45 V17342ANG
<5.70 µg/L 5.70 10.6Chrysene 1 04/11/22 18:45 V17342ANG
<6.40 µg/L 6.40 21.3
Dibenz(a,h)anthracene 1 04/11/22 18:45 V17342ANG
<5.41 µg/L 5.41 21.3Dibenzofuran 1 04/11/22 18:45 V17342ANG
<6.26 µg/L 6.26 10.61,2-Dichlorobenzene 1 04/11/22 18:45 V17342ANG
<6.18 µg/L 6.18 10.61,3-Dichlorobenzene 1 04/11/22 18:45 V17342ANG
<6.26 µg/L 6.26 10.61,4-Dichlorobenzene 1 04/11/22 18:45 V17342ANG
<7.00 µg/L 7.00 10.63,3'-Dichlorobenzidine 1 04/11/22 18:45 V17342ANG
<5.87 µg/L 5.87 10.62,4-Dichlorophenol 1 04/11/22 18:45 V17342ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 19 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<9.96 µg/L 9.96 21.3Diethyl phthalate 1 04/11/22 18:45 V17342ANG
<8.29 µg/L 8.29 10.6Dimethyl phthalate 1 04/11/22 18:45 V17342ANG
<11.6 µg/L 11.6 21.32,4-Dimethylphenol 1 04/11/22 18:45 V17342ANG
<7.79 µg/L 7.79 10.6Di-n-butyl phthalate 1 04/11/22 18:45 V17342ANG
<10.5 µg/L 10.5 31.94,6-Dinitro-2-methylphenol 1 04/11/22 18:45 V17342ANG
<11.3 µg/L 11.3 31.92,4-Dinitrophenol 1 04/11/22 18:45 V17342ANG
<5.51 µg/L 5.51 10.62,4-Dinitrotoluene 1 04/11/22 18:45 V17342ANG
<6.28 µg/L 6.28 21.32,6-Dinitrotoluene 1 04/11/22 18:45 V17342ANG
<5.31 µg/L 5.31 10.6
Di-n-Octyl Phthalate 1 04/11/22 18:45 V17342ANG
<6.39 µg/L 6.39 10.6Fluoranthene 1 04/11/22 18:45 V17342ANG
<7.71 µg/L 7.71 10.6Fluorene 1 04/11/22 18:45 V17342ANG
<6.12 µg/L 6.12 21.3Hexachlorobenzene 1 04/11/22 18:45 V17342ANG
<6.26 µg/L 6.26 21.3Hexachlorobutadiene 1 04/11/22 18:45 V17342ANG
<6.28 µg/L 6.28 21.3Hexachlorocyclopentadiene 1 04/11/22 18:45 V17342ANG
<5.53 µg/L 5.53 10.6Hexachloroethane 1 04/11/22 18:45 V17342ANG
<6.57 µg/L 6.57 10.6
Indeno(1,2,3-cd)pyrene 1 04/11/22 18:45 V17342ANG
<7.11 µg/L 7.11 10.6Isophorone 1 04/11/22 18:45 V17342ANG
<7.77 µg/L 7.77 10.61-Methylnaphthalene 1 04/11/22 18:45 V17342ANG
<7.34 µg/L 7.34 10.62-Methylnaphthalene 1 04/11/22 18:45 V17342ANG
<5.58 µg/L 5.58 10.62-Methylphenol 1 04/11/22 18:45 V17342ANG
<2.62 µg/L 2.62 10.63&4 Methylphenol 1 04/11/22 18:45 V17342ANG
<8.35 µg/L 8.35 10.6Naphthalene 1 04/11/22 18:45 V17342ANG
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 20 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:TMW-8
97581 Matrix:
4/1/2022 10:10
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<5.22 µg/L 5.22 10.62-Nitroaniline 1 04/11/22 18:45 V17342ANG
<4.82 µg/L 4.82 10.63-Nitroaniline 1 04/11/22 18:45 V17342ANG
<5.41 µg/L 5.41 10.64-Nitroaniline 1 04/11/22 18:45 V17342ANG
<8.35 µg/L 8.35 10.6Nitrobenzene 1 04/11/22 18:45 V17342ANG
<5.82 µg/L 5.82 10.62-Nitrophenol 1 04/11/22 18:45 V17342ANG
<2.98 µg/L 2.98 10.64-Nitrophenol 1 04/11/22 18:45 V17342ANG
<6.88 µg/L 6.88 10.6N-Nitrosodimethylamine 1 04/11/22 18:45 V17342ANG
<11.6 µg/L 11.6 21.3N-Nitrosodiphenylamine 1 04/11/22 18:45 V17342ANG
<8.63 µg/L 8.63 21.3
N-Nitroso-di-n-propylamine 1 04/11/22 18:45 V17342ANG
<10.4 µg/L 10.4 53.2Pentachlorophenol 1 04/11/22 18:45 V17342ANG
<6.72 µg/L 6.72 10.6Phenanthrene 1 04/11/22 18:45 V17342ANG
<3.03 µg/L 3.03 10.6Phenol 1 04/11/22 18:45 V17342ANG
<5.75 µg/L 5.75 10.6Pyrene 1 04/11/22 18:45 V17342ANG
<5.64 µg/L 5.64 10.6Pyridine 1 04/11/22 18:45 V17342ANG
<6.63 µg/L 6.63 10.61,2,4-Trichlorobenzene 1 04/11/22 18:45 V17342ANG
<6.19 µg/L 6.19 21.3
2,4,5-Trichlorophenol 1 04/11/22 18:45 V17342ANG
<6.70 µg/L 6.70 21.32,4,6-Trichlorophenol 1 04/11/22 18:45 V17342ANG
8270ESurrogate: Phenol-d5 22.3 Limits: 11-100%04/11/22 18:451 ANG
Surrogate: 2-Fluorobiphenyl 47.9 Limits: 44-119%04/11/22 18:451 ANG V17342
Surrogate: 2-Fluorophenol 33.7 Limits: 19-119%04/11/22 18:451 ANG V17342
Surrogate: Nitrobenzene-d5 48.7 Limits: 44-120%04/11/22 18:451 ANG V17342
Surrogate: 4-Terphenyl-d14 65.0 Limits: 50-134%04/11/22 18:451 ANG V17342
Surrogate: 2,4,6-Tribromophenol 61.1 Limits: 43-140%04/11/22 18:451 ANG V17342
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 21 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:Trip Blank
97582 Matrix:
4/1/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<1.80 µg/L 1.80 5.00Acetone 1 04/08/22 17:37 V17236JLB
<2.00 µg/L 2.00 5.00Acrolein 1 04/08/22 17:37 V17236JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 04/08/22 17:37 V17236JLB
<0.180 µg/L 0.180 0.500Benzene 1 04/08/22 17:37 V17236JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/08/22 17:37 V17236JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/08/22 17:37 V17236JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/08/22 17:37 V17236JLB
<1.50 µg/L 1.50 5.00Bromoform 1 04/08/22 17:37 V17236JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 04/08/22 17:37 V17236JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 04/08/22 17:37 V17236JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/08/22 17:37 V17236JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/08/22 17:37 V17236JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 04/08/22 17:37 V17236JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/08/22 17:37 V17236JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/08/22 17:37 V17236JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 04/08/22 17:37 V17236JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 04/08/22 17:37 V17236JLB
<0.220 µg/L 0.220 0.500Chloroform 1 04/08/22 17:37 V17236JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 04/08/22 17:37 V17236JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/08/22 17:37 V17236JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/08/22 17:37 V17236JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 04/08/22 17:37 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 22 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:Trip Blank
97582 Matrix:
4/1/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/08/22 17:37 V17236JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/08/22 17:37 V17236JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/08/22 17:37 V17236JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/08/22 17:37 V17236JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/08/22 17:37 V17236JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/08/22 17:37 V17236JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/08/22 17:37 V17236JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/08/22 17:37 V17236JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 04/08/22 17:37 V17236JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/08/22 17:37 V17236JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/08/22 17:37 V17236JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/08/22 17:37 V17236JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/08/22 17:37 V17236JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/08/22 17:37 V17236JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/08/22 17:37 V17236JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 04/08/22 17:37 V17236JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/08/22 17:37 V17236JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/08/22 17:37 V17236JLB
<42.0 µg/L 42.0 200Ethanol 1 04/08/22 17:37 V17236JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 04/08/22 17:37 V17236JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 04/08/22 17:37 V17236JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 04/08/22 17:37 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 23 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:Trip Blank
97582 Matrix:
4/1/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<1.30 µg/L 1.30 10.0n-Hexane 1 04/08/22 17:37 V17236JLB
<0.380 µg/L 0.380 5.002-Hexanone 1 04/08/22 17:37 V17236JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 04/08/22 17:37 V17236JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/08/22 17:37 V17236JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/08/22 17:37 V17236JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 04/08/22 17:37 V17236JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 04/08/22 17:37 V17236JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 04/08/22 17:37 V17236JLB
<0.470 µg/L 0.470 1.00
Naphthalene 1 04/08/22 17:37 V17236JLB
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/08/22 17:37 V17236JLB
<0.220 µg/L 0.220 0.500Styrene 1 04/08/22 17:37 V17236JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/08/22 17:37 V17236JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/08/22 17:37 V17236JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/08/22 17:37 V17236JLB
<0.220 µg/L 0.220 0.500Toluene 1 04/08/22 17:37 V17236JLB
<0.380 µg/L 0.380 2.00
1,2,3-Trichlorobenzene 1 04/08/22 17:37 V17236JLB
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 04/08/22 17:37 V17236JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/08/22 17:37 V17236JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/08/22 17:37 V17236JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/08/22 17:37 V17236JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/08/22 17:37 V17236JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 04/08/22 17:37 V17236JLB
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 24 of 45
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-094-0013
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/20/2022
SLC.001
Report Date : 04/15/2022
Sample ID :
Lab No :
Sampled:Trip Blank
97582 Matrix:
4/1/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17235 04/08/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/08/22 17:37 V17236JLB
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 04/08/22 17:37 V17236JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/08/22 17:37 V17236JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 04/08/22 17:37 V17236JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 04/08/22 17:37 V17236JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 04/08/22 17:37 V17236
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 80-124%04/08/22 17:371 JLB V17236
Surrogate: Dibromofluoromethane 101 Limits: 75-129%04/08/22 17:371 JLB V17236
Surrogate: 1,2-Dichloroethane - d4 96.6 Limits: 63-136%04/08/22 17:371 JLB V17236
Surrogate: Toluene-d8 98.2 Limits: 77-123%04/08/22 17:371 JLB V17236
Qualifiers/
Definitions
Estimated valueJDilution FactorDF
Method Quantitation LimitMQL
Page 25 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17145QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17088
Associated Lab Samples: 97580, 97581
LRB-V17088 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/07/22 15:491.000.490<0.490µg/LArsenic
04/07/22 15:4910.03.40<3.40µg/LBarium
04/07/22 15:491.000.150<0.150µg/LCadmium
04/07/22 15:492.001.00<1.00µg/LChromium
04/07/22 15:491.000.500<0.500µg/LLead
04/07/22 15:495.002.30<2.30µg/LSelenium
04/07/22 15:491.000.130<0.130µg/LSilver
LCS-V17088Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.092.4100µg/LArsenic 80-120
95.095.3100µg/LBarium 80-120
92.092.4100µg/LCadmium 80-120
95.095.0100µg/LChromium 80-120
95.094.5100µg/LLead 80-120
97.097.2100µg/LSelenium 80-120
93.092.6100µg/LSilver 80-120
V 97514-MS-V17088 V 97514-MSD-V17088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
97.4 96.095.81001001.49µg/LArsenic 94.0 75-125 1.6 20.0
243 88.0244100100155µg/LBarium 89.0 75-125 0.4 20.0
96.9 97.096.9100100< 0.150µg/LCadmium 97.0 75-125 0.0 20.0
98.4 95.098.81001003.37µg/LChromium 95.0 75-125 0.4 20.0
Page 1 of 18Date:04/15/2022 02:05 PM
Page 26 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17145QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17088
V 97514-MS-V17088 V 97514-MSD-V17088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
101 97.01001001004.19µg/LLead 96.0 75-125 0.9 20.0
99.1 99.093.0100100< 2.30µg/LSelenium 93.0 75-125 6.3 20.0
97.6 97.096.41001000.439µg/LSilver 96.0 75-125 1.2 20.0
V 97514-PDS-V17088Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/07/22 16:2299.050.4µg/LArsenic
04/07/22 16:2299.0126µg/LBarium
04/07/22 16:2210150.3µg/LCadmium
04/07/22 16:2299.051.3µg/LChromium
04/07/22 16:2299.051.7µg/LLead
04/07/22 16:2298.048.8µg/LSelenium
04/07/22 16:2210050.4µg/LSilver
Page 2 of 18Date:04/15/2022 02:05 PM
Page 27 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17508QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17502
Associated Lab Samples: 97580, 97581
LRB-V17502 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/15/22 07:411.000.490<0.490µg/LDissolved Arsenic
04/15/22 07:4110.03.40<3.40µg/LDissolved Barium
04/15/22 07:411.000.150<0.150µg/LDissolved Cadmium
04/15/22 07:412.001.00<1.00µg/LDissolved Chromium
04/15/22 07:411.000.500<0.500µg/LDissolved Lead
04/15/22 07:415.002.30<2.30µg/LDissolved Selenium
04/15/22 07:411.000.130<0.130µg/LDissolved Silver
LCS-V17502Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.094.2100µg/LDissolved Arsenic 80-120
108108100µg/LDissolved Barium 80-120
93.093.4100µg/LDissolved Cadmium 80-120
93.092.8100µg/LDissolved Chromium 80-120
10099.5100µg/LDissolved Lead 80-120
100100100µg/LDissolved Selenium 80-120
98.097.9100µg/LDissolved Silver 80-120
V 97580-V17498-MS-V17502 V 97580-V17498-MSD-V17502Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
93.9 94.094.3100100< 2.45µg/LDissolved Arsenic 94.0 75-125 0.4 20.0
291 110262100100181µg/LDissolved Barium 81.0 75-125 10.4 20.0
93.0 93.094.2100100< 0.750µg/LDissolved Cadmium 94.0 75-125 1.2 20.0
87.6 88.093.6100100< 5.00µg/LDissolved Chromium 94.0 75-125 6.6 20.0
Page 3 of 18Date:04/15/2022 02:05 PM
Page 28 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17508QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17502
V 97580-V17498-MS-V17502 V 97580-V17498-MSD-V17502Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
101 96.099.21001005.27µg/LDissolved Lead 94.0 75-125 1.7 20.0
99.8 10093.4100100< 11.5µg/LDissolved Selenium 93.0 75-125 6.6 20.0
92.8 93.094.2100100< 0.650µg/LDissolved Silver 94.0 75-125 1.4 20.0
V 97580-V17498-PDS-V17502Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/15/22 08:40106266µg/LDissolved Arsenic
04/15/22 08:40105359µg/LDissolved Barium
04/15/22 08:40106264µg/LDissolved Cadmium
04/15/22 08:4099.0248µg/LDissolved Chromium
04/15/22 08:40102257µg/LDissolved Lead
04/15/22 08:40101253µg/LDissolved Selenium
04/15/22 08:40102256µg/LDissolved Silver
Page 4 of 18Date:04/15/2022 02:05 PM
Page 29 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V17054,V17084QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V17014
Associated Lab Samples: 97580, 97581
LRB-V17014 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/06/22 14:330.000200.00007<0.00007mg/LMercury (Total)
LCS-V17014Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1000.009370.00937mg/LMercury (Total)80-120
V 97187-MS-V17014 V 97187-MSD-V17014Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00902 96.00.008970.009370.00937< 0.00007mg/LMercury (Total)96.0 80-120 0.5 20.0
V 97187-PDS-V17014Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/06/22 17:0695.00.00443mg/LMercury (Total)
Page 5 of 18Date:04/15/2022 02:05 PM
Page 30 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V17547QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V17503
Associated Lab Samples: 97580, 97581
LRB-V17503 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/15/22 12:220.000200.0000.00004mg/LDissolved Mercury
LCS-V17503Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.009510.00937mg/LDissolved Mercury 80-120
V 97581-V17498-MS-V17503 V 97581-V17498-MSD-V17503Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00249 27.0*0.002550.009370.00937< 0.00007mg/LDissolved Mercury 27.0*80-120 2.3 20.0
V 97581-V17498-PDS-V17503Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/15/22 12:3646.0*0.00215mg/LDissolved Mercury
Page 6 of 18* QC Fail Date:04/15/2022 02:05 PM
Page 31 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17236QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17235
Associated Lab Samples: 97580, 97581, 97582
LRB-V17235 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/08/22 14:445.001.80<1.80µg/LAcetone
04/08/22 14:445.002.00<2.00µg/LAcrolein
04/08/22 14:445.000.230<0.230µg/LAcrylonitrile
04/08/22 14:440.5000.180<0.180µg/LBenzene
04/08/22 14:440.5000.210<0.210µg/LBromobenzene
04/08/22 14:441.000.420<0.420µg/LBromochloromethane
04/08/22 14:440.5000.160<0.160µg/LBromodichloromethane
04/08/22 14:445.001.50<1.50µg/LBromoform
04/08/22 14:441.000.280<0.280µg/LBromomethane
04/08/22 14:441.000.185<0.185µg/Ln-Butylbenzene
04/08/22 14:440.5000.200<0.200µg/Lsec-Butyl benzene
04/08/22 14:442.000.920<0.920µg/Ltert-Butyl benzene
04/08/22 14:445.000.150<0.150µg/LCarbon Disulfide
04/08/22 14:440.5000.180<0.180µg/LCarbon Tetrachloride
04/08/22 14:440.5000.190<0.190µg/LChlorobenzene
04/08/22 14:440.5000.190<0.190µg/LChlorodibromomethane
04/08/22 14:441.000.430<0.430µg/LChloroethane
04/08/22 14:440.5000.220<0.220µg/LChloroform
04/08/22 14:440.5000.220<0.220µg/LChloromethane
04/08/22 14:440.5000.200<0.200µg/L2-Chlorotoluene
04/08/22 14:440.5000.200<0.200µg/L4-Chlorotoluene
04/08/22 14:445.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
04/08/22 14:442.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
04/08/22 14:440.5000.200<0.200µg/L1,2-Dibromoethane
04/08/22 14:440.5000.230<0.230µg/LDibromomethane
04/08/22 14:440.5000.220<0.220µg/L1,2-Dichlorobenzene
04/08/22 14:440.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 7 of 18Date:04/15/2022 02:05 PM
Page 32 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17236QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17235
Associated Lab Samples: 97580, 97581, 97582
LRB-V17235 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/08/22 14:440.5000.210<0.210µg/L1,4-Dichlorobenzene
04/08/22 14:445.001.20<1.20µg/LDichlorodifluoromethane
04/08/22 14:440.5000.240<0.240µg/L1,1-Dichloroethane
04/08/22 14:440.5000.150<0.150µg/L1,2-Dichloroethane
04/08/22 14:440.5000.150<0.150µg/L1,1-Dichloroethene
04/08/22 14:440.5000.200<0.200µg/Lcis-1,2-Dichloroethene
04/08/22 14:440.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
04/08/22 14:440.5000.190<0.190µg/L1,2-Dichloropropane
04/08/22 14:440.5000.130<0.130µg/L1,3-Dichloropropane
04/08/22 14:442.000.210<0.210µg/L2,2-Dichloropropane
04/08/22 14:440.5000.200<0.200µg/L1,1-Dichloropropene
04/08/22 14:440.5000.210<0.210µg/Lcis-1,3-Dichloropropene
04/08/22 14:440.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
04/08/22 14:4420042.0<42.0µg/LEthanol
04/08/22 14:440.5000.170<0.170µg/LEthylbenzene
04/08/22 14:4410.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
04/08/22 14:442.000.350<0.350µg/LHexachlorobutadiene
04/08/22 14:4410.01.30<1.30µg/Ln-Hexane
04/08/22 14:445.000.380<0.380µg/L2-Hexanone
04/08/22 14:445.000.180<0.180µg/LIsopropylbenzene
04/08/22 14:440.5000.089<0.089µg/L4-Isopropyl toluene
04/08/22 14:445.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
04/08/22 14:440.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
04/08/22 14:445.001.00<1.00µg/L4-Methyl-2-Pentanone
04/08/22 14:441.000.330<0.330µg/LMethylene Chloride
04/08/22 14:441.000.470<0.470µg/LNaphthalene
04/08/22 14:440.5000.190<0.190µg/Ln-Propylbenzene
Page 8 of 18Date:04/15/2022 02:05 PM
Page 33 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17236QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17235
Associated Lab Samples: 97580, 97581, 97582
LRB-V17235 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/08/22 14:440.5000.220<0.220µg/LStyrene
04/08/22 14:440.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
04/08/22 14:440.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
04/08/22 14:440.5000.220<0.220µg/LTetrachloroethene
04/08/22 14:440.5000.220<0.220µg/LToluene
04/08/22 14:442.000.380<0.380µg/L1,2,3-Trichlorobenzene
04/08/22 14:441.000.310<0.310µg/L1,2,4-Trichlorobenzene
04/08/22 14:440.5000.160<0.160µg/L1,1,1-Trichloroethane
04/08/22 14:440.5000.096<0.096µg/L1,1,2-Trichloroethane
04/08/22 14:440.5000.180<0.180µg/LTrichloroethene
04/08/22 14:440.5000.180<0.180µg/LTrichlorofluoromethane
04/08/22 14:441.000.270<0.270µg/L1,2,3-Trichloropropane
04/08/22 14:440.5000.180<0.180µg/L1,3,5-Trimethylbenzene
04/08/22 14:442.001.00<1.00µg/LVinyl Acetate
04/08/22 14:440.5000.170<0.170µg/LVinyl Chloride
04/08/22 14:440.5000.210<0.210µg/Lo-Xylene
04/08/22 14:441.000.420<0.420µg/Lm,p-Xylene
04/08/22 14:444-Bromofluorobenzene (S)100 80-124
04/08/22 14:44Dibromofluoromethane (S)102 75-129
04/08/22 14:441,2-Dichloroethane - d4 (S)98.4 63-136
04/08/22 14:44Toluene-d8 (S)98.6 77-123
LCS-V17235 LCSD-V17235Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
40.6 10287.234.940.0µg/LAcetone 40-166 15.0 20
Page 9 of 18Date:04/15/2022 02:05 PM
Page 34 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17236QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17235
LCS-V17235 LCSD-V17235Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.5 93.798.039.240.0µg/LAcrolein 70-130 4.4 20
39.0 97.510140.340.0µg/LAcrylonitrile 81-127 3.2 20
19.8 99.010120.220.0µg/LBenzene 77-128 2.0 20
19.5 97.597.019.420.0µg/LBromobenzene 78-129 0.5 20
20.4 10210220.320.0µg/LBromochloromethane 78-135 0.4 20
21.4 10710621.120.0µg/LBromodichloromethane 76-138 1.4 20
20.0 10099.519.920.0µg/LBromoform 71-135 0.5 20
19.5 97.592.018.420.0µg/LBromomethane 41-168 5.8 20
20.2 10110220.320.0µg/Ln-Butylbenzene 68-134 0.4 20
19.6 98.098.019.620.0µg/Lsec-Butyl benzene 71-131 0.0 20
19.4 97.098.519.720.0µg/Ltert-Butyl benzene 70-132 1.5 20
18.7 93.595.519.120.0µg/LCarbon Disulfide 59-135 2.1 20
20.2 10110220.320.0µg/LCarbon Tetrachloride 72-142 0.4 20
20.0 10010220.320.0µg/LChlorobenzene 78-119 1.4 20
20.2 10110420.720.0µg/LChlorodibromomethane 75-134 2.4 20
20.3 10298.519.720.0µg/LChloroethane 57-142 3.0 20
20.1 10110420.820.0µg/LChloroform 77-130 3.4 20
17.1 85.591.518.320.0µg/LChloromethane 47-145 6.7 20
19.3 96.598.019.620.0µg/L2-Chlorotoluene 74-126 1.5 20
19.6 98.098.019.620.0µg/L4-Chlorotoluene 78-129 0.0 20
19.9 99.510320.620.0µg/LDi-Isopropyl Ether (DIPE)60-154 3.4 20
19.6 98.099.019.820.0µg/L1,2-Dibromo-3-Chloropropane 63-134 1.0 20
20.3 10210721.320.0µg/L1,2-Dibromoethane 77-135 4.8 20
20.8 10410420.720.0µg/LDibromomethane 76-138 0.4 20
20.2 10110120.220.0µg/L1,2-Dichlorobenzene 78-128 0.0 20
19.8 99.098.019.620.0µg/L1,3-Dichlorobenzene 77-125 1.0 20
Page 10 of 18Date:04/15/2022 02:05 PM
Page 35 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17236QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17235
LCS-V17235 LCSD-V17235Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.6 98.099.519.920.0µg/L1,4-Dichlorobenzene 75-126 1.5 20
20.6 10310320.620.0µg/LDichlorodifluoromethane 28-163 0.0 20
20.4 10299.019.820.0µg/L1,1-Dichloroethane 70-130 2.9 20
20.8 10410621.220.0µg/L1,2-Dichloroethane 68-131 1.9 20
19.1 95.598.519.720.0µg/L1,1-Dichloroethene 70-154 3.0 20
19.6 98.099.519.920.0µg/Lcis-1,2-Dichloroethene 76-141 1.5 20
19.9 99.510120.220.0µg/Ltrans-1,2-Dichloroethene 76-135 1.4 20
19.9 99.510020.020.0µg/L1,2-Dichloropropane 77-130 0.5 20
20.4 10210521.020.0µg/L1,3-Dichloropropane 76-132 2.8 20
21.0 10510721.320.0µg/L2,2-Dichloropropane 29-149 1.4 20
20.1 10199.019.820.0µg/L1,1-Dichloropropene 71-136 1.5 20
20.7 10410420.820.0µg/Lcis-1,3-Dichloropropene 65-140 0.4 20
21.1 10610721.320.0µg/Ltrans-1,3-Dichloropropene 67-140 0.9 20
429 85.895.8479500µg/LEthanol 70-130 11.0 20
19.5 97.510220.420.0µg/LEthylbenzene 80-127 4.5 20
43.6 10910542.140.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 3.5 20
20.3 10299.519.920.0µg/LHexachlorobutadiene 61-134 1.9 20
19.0 95.093.518.720.0µg/Ln-Hexane 70-130 1.5 20
19.1 95.596.519.320.0µg/L2-Hexanone 64-137 1.0 20
19.8 99.099.019.820.0µg/LIsopropylbenzene 70-130 0.0 20
19.6 98.010320.520.0µg/L4-Isopropyl toluene 69-132 4.4 20
18.2 91.082.516.520.0µg/LMethyl Ethyl Ketone (MEK)71-134 9.7 20
20.9 10510120.120.0µg/LMethyl tert-butyl ether (MTBE)68-135 3.9 20
20.6 10310120.220.0µg/L4-Methyl-2-Pentanone 69-134 1.9 20
18.8 94.095.019.020.0µg/LMethylene Chloride 73-131 1.0 20
20.6 10392.518.520.0µg/LNaphthalene 64-136 10.7 20
Page 11 of 18Date:04/15/2022 02:05 PM
Page 36 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17236QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17235
LCS-V17235 LCSD-V17235Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.0 10099.019.820.0µg/Ln-Propylbenzene 72-132 1.0 20
20.3 10210420.820.0µg/LStyrene 78-129 2.4 20
20.4 10210020.020.0µg/L1,1,1,2-Tetrachloroethane 79-134 1.9 20
19.2 96.099.019.820.0µg/L1,1,2,2-Tetrachloroethane 62-127 3.0 20
20.2 10110120.120.0µg/LTetrachloroethene 80-129 0.4 20
20.1 10110120.220.0µg/LToluene 76-131 0.4 20
21.4 10792.018.420.0µg/L1,2,3-Trichlorobenzene 58-144 15.0 20
22.4 11210621.120.0µg/L1,2,4-Trichlorobenzene 66-139 5.9 20
20.4 10210520.920.0µg/L1,1,1-Trichloroethane 75-135 2.4 20
20.5 10310320.520.0µg/L1,1,2-Trichloroethane 70-140 0.0 20
19.7 98.510621.120.0µg/LTrichloroethene 77-133 6.8 20
20.4 10210621.120.0µg/LTrichlorofluoromethane 62-148 3.3 20
18.9 94.510320.620.0µg/L1,2,3-Trichloropropane 71-127 8.6 20
20.0 10099.019.820.0µg/L1,3,5-Trimethylbenzene 75-131 1.0 20
21.1 10610921.720.0µg/LVinyl Acetate 34-167 2.8 20
19.2 96.099.519.920.0µg/LVinyl Chloride 57-141 3.5 20
19.9 99.510120.120.0µg/Lo-Xylene 78-128 1.0 20
41.4 10410542.140.0µg/Lm,p-Xylene 77-133 1.6 20
97.897.24-Bromofluorobenzene (S)80-124
101100Dibromofluoromethane (S)75-129
1031041,2-Dichloroethane - d4 (S)63-136
98.499.4Toluene-d8 (S)77-123
Page 12 of 18Date:04/15/2022 02:05 PM
Page 37 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
Associated Lab Samples: 97580, 97581
LRB-V17141 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/11/22 15:4720.07.12<7.12µg/LAcenaphthene
04/11/22 15:4720.06.94<6.94µg/LAcenaphthylene
04/11/22 15:4750.07.13<7.13µg/LAniline
04/11/22 15:4710.06.57<6.57µg/LAnthracene
04/11/22 15:4710.05.65<5.65µg/LBenzo(a)anthracene
04/11/22 15:4710.04.67<4.67µg/LBenzo(a)pyrene
04/11/22 15:4710.04.52<4.52µg/LBenzo(b)fluoranthene
04/11/22 15:4710.04.24<4.24µg/LBenzo(g,h,i)perylene
04/11/22 15:4710.04.68<4.68µg/LBenzo(k)fluoranthene
04/11/22 15:4710011.5<11.5µg/LBenzoic Acid
04/11/22 15:4710.08.60<8.60µg/LBenzyl alcohol
04/11/22 15:4710.05.67<5.67µg/LBis(2-Chloroethoxy)methane
04/11/22 15:4710.07.30<7.30µg/LBis(2-Chloroethyl)ether
04/11/22 15:4710.06.59<6.59µg/LBis(2-Chloroisopropyl)ether
04/11/22 15:4710.08.80<8.80µg/LBis(2-ethylhexyl)phthalate
04/11/22 15:4720.06.26<6.26µg/L4-Bromophenyl phenyl ether
04/11/22 15:4710.02.94<2.94µg/LButyl benzyl phthalate
04/11/22 15:4710.05.23<5.23µg/L4-Chloro-3-methylphenol
04/11/22 15:4710.05.42<5.42µg/L4-Chloroaniline
04/11/22 15:4720.07.38<7.38µg/L2-Chloronaphthalene
04/11/22 15:4710.06.58<6.58µg/L2-Chlorophenol
04/11/22 15:4720.06.99<6.99µg/L4-Chlorophenyl phenyl ether
04/11/22 15:4710.05.38<5.38µg/LChrysene
04/11/22 15:4720.06.01<6.01µg/LDibenz(a,h)anthracene
04/11/22 15:4720.05.08<5.08µg/LDibenzofuran
04/11/22 15:4710.05.91<5.91µg/L1,2-Dichlorobenzene
04/11/22 15:4710.05.83<5.83µg/L1,3-Dichlorobenzene
Page 13 of 18Date:04/15/2022 02:05 PM
Page 38 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
Associated Lab Samples: 97580, 97581
LRB-V17141 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/11/22 15:4710.05.91<5.91µg/L1,4-Dichlorobenzene
04/11/22 15:4710.06.60<6.60µg/L3,3'-Dichlorobenzidine
04/11/22 15:4710.05.54<5.54µg/L2,4-Dichlorophenol
04/11/22 15:4720.09.35<9.35µg/LDiethyl phthalate
04/11/22 15:4710.07.82<7.82µg/LDimethyl phthalate
04/11/22 15:4720.010.9<10.9µg/L2,4-Dimethylphenol
04/11/22 15:4710.07.35<7.35µg/LDi-n-butyl phthalate
04/11/22 15:4730.09.92<9.92µg/L4,6-Dinitro-2-methylphenol
04/11/22 15:4730.010.6<10.6µg/L2,4-Dinitrophenol
04/11/22 15:4710.05.20<5.20µg/L2,4-Dinitrotoluene
04/11/22 15:4720.05.90<5.90µg/L2,6-Dinitrotoluene
04/11/22 15:4710.05.01<5.01µg/LDi-n-Octyl Phthalate
04/11/22 15:4710.06.03<6.03µg/LFluoranthene
04/11/22 15:4710.07.27<7.27µg/LFluorene
04/11/22 15:4720.05.75<5.75µg/LHexachlorobenzene
04/11/22 15:4720.05.88<5.88µg/LHexachlorobutadiene
04/11/22 15:4720.05.90<5.90µg/LHexachlorocyclopentadiene
04/11/22 15:4710.05.22<5.22µg/LHexachloroethane
04/11/22 15:4710.06.20<6.20µg/LIndeno(1,2,3-cd)pyrene
04/11/22 15:4710.06.71<6.71µg/LIsophorone
04/11/22 15:4710.07.33<7.33µg/L1-Methylnaphthalene
04/11/22 15:4710.06.92<6.92µg/L2-Methylnaphthalene
04/11/22 15:4710.05.26<5.26µg/L2-Methylphenol
04/11/22 15:4710.02.47<2.47µg/L3&4 Methylphenol
04/11/22 15:4710.07.88<7.88µg/LNaphthalene
04/11/22 15:4710.04.92<4.92µg/L2-Nitroaniline
04/11/22 15:4710.04.55<4.55µg/L3-Nitroaniline
Page 14 of 18Date:04/15/2022 02:05 PM
Page 39 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
Associated Lab Samples: 97580, 97581
LRB-V17141 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/11/22 15:4710.05.10<5.10µg/L4-Nitroaniline
04/11/22 15:4710.07.88<7.88µg/LNitrobenzene
04/11/22 15:4710.05.49<5.49µg/L2-Nitrophenol
04/11/22 15:4710.02.81<2.81µg/L4-Nitrophenol
04/11/22 15:4710.06.49<6.49µg/LN-Nitrosodimethylamine
04/11/22 15:4720.010.9<10.9µg/LN-Nitrosodiphenylamine
04/11/22 15:4720.08.10<8.10µg/LN-Nitroso-di-n-propylamine
04/11/22 15:4750.09.73<9.73µg/LPentachlorophenol
04/11/22 15:4710.06.34<6.34µg/LPhenanthrene
04/11/22 15:4710.02.86<2.86µg/LPhenol
04/11/22 15:4710.05.42<5.42µg/LPyrene
04/11/22 15:4710.05.32<5.32µg/LPyridine
04/11/22 15:4710.06.25<6.25µg/L1,2,4-Trichlorobenzene
04/11/22 15:4720.05.81<5.81µg/L2,4,5-Trichlorophenol
04/11/22 15:4720.06.29<6.29µg/L2,4,6-Trichlorophenol
04/11/22 15:472-Fluorobiphenyl (S)52.6 44-119
04/11/22 15:472-Fluorophenol (S)37.8 19-119
04/11/22 15:47Nitrobenzene-d5 (S)54.0 44-120
04/11/22 15:474-Terphenyl-d14 (S)70.4 50-134
04/11/22 15:472,4,6-Tribromophenol (S)65.2 43-140
04/11/22 15:47Phenol-d5 (S)22.9 11-100
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.3 72.670.635.350.0µg/LAcenaphthene 38-117 2.7 20.0
Page 15 of 18Date:04/15/2022 02:05 PM
Page 40 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.1 78.277.238.650.0µg/LAcenaphthylene 41-130 1.2 20.0
26.6 53.264.432.250.0µg/LAniline 12-197 19.0 20.0
45.1 90.285.042.550.0µg/LAnthracene 57-123 5.9 20.0
44.6 89.280.640.350.0µg/LBenzo(a)anthracene 58-125 10.1 20.0
49.5 99.088.644.350.0µg/LBenzo(a)pyrene 54-128 11.0 20.0
42.1 84.275.637.850.0µg/LBenzo(b)fluoranthene 53-131 10.7 20.0
43.8 87.677.838.950.0µg/LBenzo(g,h,i)perylene 50-134 11.8 20.0
43.4 86.878.439.250.0µg/LBenzo(k)fluoranthene 53-131 10.1 20.0
<11.5 0.0*0.0*<11.550.0µg/LBenzoic Acid 10-125 0.0 20.0
30.8 61.664.832.450.0µg/LBenzyl alcohol 31-112 5.0 20.0
33.2 66.469.434.750.0µg/LBis(2-Chloroethoxy)methane 48-120 4.4 20.0
33.8 67.664.032.050.0µg/LBis(2-Chloroethyl)ether 43-118 5.4 20.0
31.7 63.463.631.850.0µg/LBis(2-Chloroisopropyl)ether 37-130 0.3 20.0
47.9 95.886.843.450.0µg/LBis(2-ethylhexyl)phthalate 55-135 9.8 20.0
40.2 80.476.238.150.0µg/L4-Bromophenyl phenyl ether 55-124 5.3 20.0
44.8 89.681.440.750.0µg/LButyl benzyl phthalate 53-134 9.5 20.0
35.0 70.068.434.250.0µg/L4-Chloro-3-methylphenol 52-119 2.3 20.0
33.6 67.263.831.950.0µg/L4-Chloroaniline 33-117 5.1 20.0
32.3 64.663.031.550.0µg/L2-Chloronaphthalene 40-116 2.5 20.0
30.0 60.061.230.650.0µg/L2-Chlorophenol 38-117 1.9 20.0
40.7 81.478.439.250.0µg/L4-Chlorophenyl phenyl ether 53-121 3.7 20.0
43.8 87.679.239.650.0µg/LChrysene 59-123 10.0 20.0
38.0 76.067.033.550.0µg/LDibenz(a,h)anthracene 51-134 12.5 20.0
38.7 77.475.637.850.0µg/LDibenzofuran 53-118 2.3 20.0
18.5 37.034.617.350.0µg/L1,2-Dichlorobenzene 32-111 6.7 20.0
16.8 33.630.815.450.0µg/L1,3-Dichlorobenzene 28-110 8.6 20.0
Page 16 of 18* QC Fail Date:04/15/2022 02:05 PM
Page 41 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.1 34.231.815.950.0µg/L1,4-Dichlorobenzene 29-112 7.2 20.0
35.2 70.465.832.950.0µg/L3,3'-Dichlorobenzidine 27-129 6.7 20.0
32.1 64.263.231.650.0µg/L2,4-Dichlorophenol 47-121 1.5 20.0
43.4 86.881.440.750.0µg/LDiethyl phthalate 56-125 6.4 20.0
41.8 83.679.039.550.0µg/LDimethyl phthalate 45-127 5.6 20.0
34.8 69.668.434.250.0µg/L2,4-Dimethylphenol 31-124 1.7 20.0
48.8 97.689.844.950.0µg/LDi-n-butyl phthalate 59-127 8.3 20.0
39.1 78.276.038.050.0µg/L4,6-Dinitro-2-methylphenol 44-137 2.8 20.0
30.7 61.455.627.850.0µg/L2,4-Dinitrophenol 23-143 9.9 20.0
45.6 91.285.242.650.0µg/L2,4-Dinitrotoluene 57-128 6.8 20.0
44.8 89.685.642.850.0µg/L2,6-Dinitrotoluene 57-124 4.5 20.0
43.6 87.278.639.350.0µg/LDi-n-Octyl Phthalate 51-140 10.3 20.0
45.2 90.484.242.150.0µg/LFluoranthene 57-128 7.1 20.0
42.4 84.881.040.550.0µg/LFluorene 52-124 4.5 20.0
42.5 85.078.439.250.0µg/LHexachlorobenzene 53-125 8.0 20.0
15.1 30.226.813.450.0µg/LHexachlorobutadiene 22-124 11.9 20.0
18.2 36.436.218.150.0µg/LHexachlorocyclopentadiene 32-117 0.5 20.0
14.3 28.626.213.150.0µg/LHexachloroethane 21-115 8.7 20.0
41.8 83.674.637.350.0µg/LIndeno(1,2,3-cd)pyrene 52-134 11.3 20.0
30.4 60.860.630.350.0µg/LIsophorone 42-124 0.3 20.0
25.7 51.451.625.850.0µg/L1-Methylnaphthalene 41-119 0.3 20.0
23.9 47.847.823.950.0µg/L2-Methylnaphthalene 40-121 0.0 20.0
30.5 61.063.031.550.0µg/L2-Methylphenol 30-117 3.2 20.0
25.3 50.652.626.350.0µg/L3&4 Methylphenol 29-110 3.8 20.0
24.1 48.247.023.550.0µg/LNaphthalene 40-121 2.5 20.0
41.0 82.078.439.250.0µg/L2-Nitroaniline 55-127 4.4 20.0
Page 17 of 18Date:04/15/2022 02:05 PM
Page 42 of 45
Quality Control Data
22-094-0013Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
46.3 92.683.441.750.0µg/L3-Nitroaniline 41-128 10.4 20.0
44.4 88.883.041.550.0µg/L4-Nitroaniline 45-135 6.7 20.0
30.1 60.259.229.650.0µg/LNitrobenzene 45-121 1.6 20.0
30.5 61.060.030.050.0µg/L2-Nitrophenol 47-123 1.6 20.0
18.4 36.834.017.050.0µg/L4-Nitrophenol 10-105 7.9 20.0
20.0 40.039.819.950.0µg/LN-Nitrosodimethylamine 10-119 0.5 20.0
50.1 10096.048.050.0µg/LN-Nitrosodiphenylamine 51-123 4.2 20.0
34.9 69.872.636.350.0µg/LN-Nitroso-di-n-propylamine 49-119 3.9 20.0
48.6 97.290.645.350.0µg/LPentachlorophenol 35-138 7.0 20.0
43.7 87.482.841.450.0µg/LPhenanthrene 59-120 5.4 20.0
13.8 27.628.414.250.0µg/LPhenol 12-58 2.8 20.0
43.6 87.280.440.250.0µg/LPyrene 57-126 8.1 20.0
5.91 11.825.412.750.0µg/LPyridine 10-80 72.9*20.0
18.1 36.235.017.550.0µg/L1,2,4-Trichlorobenzene 29-126 3.3 20.0
39.8 79.675.437.750.0µg/L2,4,5-Trichlorophenol 53-123 5.4 20.0
39.6 79.275.637.850.0µg/L2,4,6-Trichlorophenol 50-125 4.6 20.0
64.065.22-Fluorobiphenyl (S)44-119
41.641.62-Fluorophenol (S)19-119
57.456.6Nitrobenzene-d5 (S)44-120
88.679.44-Terphenyl-d14 (S)50-134
93.086.32,4,6-Tribromophenol (S)43-140
26.526.7Phenol-d5 (S)11-100
Page 18 of 18* QC Fail Date:04/15/2022 02:05 PM
Page 43 of 45
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-094-0013
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 1.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:04/04/2022 13:04:44
Special precautions or instructions included?
Comments:
Page 44 of 45
Page 45 of 45

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

4/20/2022
Hart & Hickman (Charlotte) Bo Cappleman
2923 South Tryon St. Ste 100 Charlotte, NC, 28203
Ref: Analytical Testing
Lab Report Number: 22-091-0033 Client Project Description: SLC.001
Dear Bo Cappleman:
Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/1/2022 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as-received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely,
Angela D Overcash Senior Project Manager
Page 1 of 55
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202237735State ProgramNorth Carolina
12/31/2022402State ProgramNorth Carolina
07/31/202299012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-091-0033
Page 2 of 55
Report Number:
Sample Summary Table
Client Project Description:
22-091-0033
SLC.001
Lab No Client Sample ID Matrix Date Collected Date Received
04/01/2022 11:20Aqueous 97514 TMW-4 04/01/2022 17:12
03/31/2022 10:15Aqueous 97515 TMW-6 04/01/2022 17:12
03/31/2022Aqueous 97516 TB-1 04/01/2022 17:12
Page 3 of 55
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-091-0033
Report Limit
Project:SLC.001
V 97514TMW-4
1.49 04/07/2022 16:026020BArsenicµg/L 0.490
J0.711 04/20/2022 14:426020BDissolved Arsenic µg/L 0.490
155 04/07/2022 16:026020BBariumµg/L 3.40
95.9 04/20/2022 14:426020BDissolved Barium µg/L 3.40
3.37 04/07/2022 16:026020BChromiumµg/L 1.00
4.19 04/07/2022 16:026020BLeadµg/L 0.500
J0.663 04/20/2022 14:426020BDissolved Lead µg/L 0.500
J0.439 04/07/2022 16:026020BSilverµg/L 0.130
J3.60 04/08/2022 07:418260DAcetoneµg/L 1.80
V 97515TMW-6
J3.16 04/07/2022 18:416020BArsenicµg/L 2.45
220 04/07/2022 18:416020BBariumµg/L 17.0
128 04/15/2022 08:146020BDissolved Barium µg/L 17.0
85.3 04/07/2022 18:416020BChromiumµg/L 5.00
25.5 04/15/2022 08:146020BDissolved Chromium µg/L 5.00
32.1 04/07/2022 18:416020BLeadµg/L 2.50
6.70 04/15/2022 08:146020BDissolved Lead µg/L 2.50
5.81 04/08/2022 08:058260DAcetoneµg/L 1.80
J0.248 04/08/2022 08:058260DChloroformµg/L 0.220
J0.428 04/08/2022 08:058260Dcis-1,2-Dichloroethene µg/L 0.200
J1.62 04/08/2022 08:058260DMethyl Ethyl Ketone (MEK)µg/L 0.710
0.801 04/08/2022 08:058260DMethyl tert-butyl ether (MTBE)µg/L 0.140
4.95 04/08/2022 08:058260DTetrachloroetheneµg/L 0.220
J0.291 04/08/2022 08:058260DTolueneµg/L 0.220
2.51 04/08/2022 08:058260DTrichloroetheneµg/L 0.180
Page 4 of 55

Client: Hart & Hickman (Charlotte) CASE NARRATIVE
Project: SLC.001 Lab Report Number: 22-091-0033
Date: 4/13/2022
Metals Analyses Method 6020B Sample 97515 (TMW-6) QC Batch No: V17145/V17088
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Semivolatile Organic Compounds - GC/MS Method 8270E Sample 97515 (TMW-6)
Analyte: 2-Fluorobiphenyl QC Batch No: V17076/V16999
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory
Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix.
Sample 97515 (TMW-6)
Analyte: Nitrobenzene-d5 QC Batch No: V17076/V16999
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory
Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Analyte: 2,4-Dinitrophenol
QC Batch No: V17076/V17141 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
21.0 ug/L which calculates to a recovery of 42% which is within the acceptable recovery range.
Analyte: 2,4-Dinitrophenol QC Batch No: V17076/V17141 Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 20.8 ug/L which calculates to a recovery of 41.6% which is within the acceptable recovery range.
Analyte: Benzoic Acid
QC Batch No: V17076/V17141 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 0.981 ug/L which calculates to a recovery of 1.9% which is below the acceptable recovery range. Analyte: Benzoic Acid QC Batch No: V17076/V17141
Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 1.01 ug/L which calculates to a recovery of 2% which is below the acceptable recovery range. Analyte: Benzoic Acid QC Batch No: V17342/V17141
Page 5 of 55

Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was
4.62 which calculates to a recovery of 9%. Benzoic Acid is a known poor performer.
Analyte: Benzoic Acid QC Batch No: V17342/V17141
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 2.53 which calculates to a recovery of 5%. Benzoic Acid is a known poor performer.
Analyte: Hexachlorobutadiene
QC Batch No: V17076/V17141 Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was
17.1 ug/L which calculates to a recovery of 34% which is within the acceptable recovery range.
Analyte: Hexachlorobutadiene QC Batch No: V17076/V17141
Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was 19.4 ug/L which calculates to a recovery of 38.7% which is within the acceptable recovery range.
Analyte: Hexachlorocyclopentadiene
QC Batch No: V17076/V17141 Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was
19.2 ug/L which calculates to a recovery of 38.4% which is within the acceptable recovery range. Analyte: N-nitrosodimethylamine QC Batch No: V17076/V17141
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Analyte: Pentachlorophenol QC Batch No: V17076/V17141 Analyte was flagged for 0% recovery in the LCSD due to the result being below the MQL. The actual result was 39.3 ug/L which calculates to a recovery of 78.6% which is within the acceptable recovery range. Analyte: Pentachlorophenol
QC Batch No: V17076/V17141 Analyte was flagged for 0% recovery in the LCS due to the result being below the MQL. The actual result was
42.1 ug/L which calculates to a recovery of 84% which is within the acceptable recovery range. Analyte: Pyridine QC Batch No: V17342/V17141 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.

Page 6 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
1.49 µg/L 0.490 1.00Arsenic 1 04/07/22 16:02 6020BEDV
0.711 J µg/L 0.490 1.00Dissolved Arsenic 1 04/20/22 14:42 6020BEDV
155 µg/L 3.40 10.0Barium 1 04/07/22 16:02 6020BEDV
95.9 µg/L 3.40 10.0Dissolved Barium 1 04/20/22 14:42 6020BEDV
<0.150 µg/L 0.150 1.00Cadmium 1 04/07/22 16:02 6020BEDV
<0.150 µg/L 0.150 1.00
Dissolved Cadmium 1 04/20/22 14:42 6020BEDV
3.37 µg/L 1.00 2.00Chromium 1 04/07/22 16:02 6020BEDV
<1.00 µg/L 1.00 2.00Dissolved Chromium 1 04/20/22 14:42 6020BEDV
4.19 µg/L 0.500 1.00Lead 1 04/07/22 16:02 6020BEDV
0.663 J µg/L 0.500 1.00Dissolved Lead 1 04/20/22 14:42 6020BEDV
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 04/06/22 16:10 7470AEDV
<0.00007 mg/L 0.00007 0.00020Dissolved Mercury 1 04/19/22 20:24 7470AEDV
<2.30 µg/L 2.30 5.00
Selenium 1 04/07/22 16:02 6020BEDV
<2.30 µg/L 2.30 5.00Dissolved Selenium 1 04/20/22 14:42 6020BEDV
0.439 J µg/L 0.130 1.00Silver 1 04/07/22 16:02 6020BEDV
<0.130 µg/L 0.130 1.00Dissolved Silver 1 04/20/22 14:42 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 7 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
3.60 J µg/L 1.80 5.00Acetone 1 04/08/22 07:41 V17188JLB
<2.00 µg/L 2.00 5.00Acrolein 1 04/08/22 07:41 V17188JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 04/08/22 07:41 V17188JLB
<0.180 µg/L 0.180 0.500Benzene 1 04/08/22 07:41 V17188JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/08/22 07:41 V17188JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/08/22 07:41 V17188JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/08/22 07:41 V17188JLB
<1.50 µg/L 1.50 5.00Bromoform 1 04/08/22 07:41 V17188JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 04/08/22 07:41 V17188JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 04/08/22 07:41 V17188JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/08/22 07:41 V17188JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/08/22 07:41 V17188JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 04/08/22 07:41 V17188JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/08/22 07:41 V17188JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/08/22 07:41 V17188JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 04/08/22 07:41 V17188JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 04/08/22 07:41 V17188JLB
<0.220 µg/L 0.220 0.500Chloroform 1 04/08/22 07:41 V17188JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 04/08/22 07:41 V17188JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/08/22 07:41 V17188JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/08/22 07:41 V17188JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 04/08/22 07:41 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 8 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/08/22 07:41 V17188JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/08/22 07:41 V17188JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/08/22 07:41 V17188JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/08/22 07:41 V17188JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/08/22 07:41 V17188JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/08/22 07:41 V17188JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/08/22 07:41 V17188JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/08/22 07:41 V17188JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 04/08/22 07:41 V17188JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/08/22 07:41 V17188JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/08/22 07:41 V17188JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/08/22 07:41 V17188JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/08/22 07:41 V17188JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/08/22 07:41 V17188JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/08/22 07:41 V17188JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 04/08/22 07:41 V17188JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/08/22 07:41 V17188JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/08/22 07:41 V17188JLB
<42.0 µg/L 42.0 200Ethanol 1 04/08/22 07:41 V17188JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 04/08/22 07:41 V17188JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 04/08/22 07:41 V17188JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 04/08/22 07:41 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 9 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<1.30 µg/L 1.30 10.0n-Hexane 1 04/08/22 07:41 V17188JLB
<0.380 µg/L 0.380 5.002-Hexanone 1 04/08/22 07:41 V17188JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 04/08/22 07:41 V17188JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/08/22 07:41 V17188JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/08/22 07:41 V17188JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 04/08/22 07:41 V17188JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 04/08/22 07:41 V17188JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 04/08/22 07:41 V17188JLB
<0.470 µg/L 0.470 1.00
Naphthalene 1 04/08/22 07:41 V17188JLB
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/08/22 07:41 V17188JLB
<0.220 µg/L 0.220 0.500Styrene 1 04/08/22 07:41 V17188JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/08/22 07:41 V17188JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/08/22 07:41 V17188JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/08/22 07:41 V17188JLB
<0.220 µg/L 0.220 0.500Toluene 1 04/08/22 07:41 V17188JLB
<0.380 µg/L 0.380 2.00
1,2,3-Trichlorobenzene 1 04/08/22 07:41 V17188JLB
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 04/08/22 07:41 V17188JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/08/22 07:41 V17188JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/08/22 07:41 V17188JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/08/22 07:41 V17188JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/08/22 07:41 V17188JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 04/08/22 07:41 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 10 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/08/22 07:41 V17188JLB
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 04/08/22 07:41 V17188JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/08/22 07:41 V17188JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 04/08/22 07:41 V17188JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 04/08/22 07:41 V17188JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 04/08/22 07:41 V17188
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 80-124%04/08/22 07:411 JLB V17188
Surrogate: Dibromofluoromethane 98.0 Limits: 75-129%04/08/22 07:411 JLB V17188
Surrogate: 1,2-Dichloroethane - d4 98.2 Limits: 63-136%04/08/22 07:411 JLB V17188
Surrogate: Toluene-d8 98.2 Limits: 77-123%04/08/22 07:411 JLB V17188
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<7.12 µg/L 7.12 20.0Acenaphthene 1 04/11/22 19:07 V17342ANG
<6.94 µg/L 6.94 20.0Acenaphthylene 1 04/11/22 19:07 V17342ANG
<7.13 µg/L 7.13 50.0Aniline 1 04/11/22 19:07 V17342ANG
<6.57 µg/L 6.57 10.0Anthracene 1 04/11/22 19:07 V17342ANG
<5.65 µg/L 5.65 10.0Benzo(a)anthracene 1 04/11/22 19:07 V17342ANG
<4.67 µg/L 4.67 10.0Benzo(a)pyrene 1 04/11/22 19:07 V17342ANG
<4.52 µg/L 4.52 10.0
Benzo(b)fluoranthene 1 04/11/22 19:07 V17342ANG
<4.24 µg/L 4.24 10.0Benzo(g,h,i)perylene 1 04/11/22 19:07 V17342ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 11 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<4.68 µg/L 4.68 10.0Benzo(k)fluoranthene 1 04/11/22 19:07 V17342ANG
<11.5 µg/L 11.5 100Benzoic Acid 1 04/11/22 19:07 V17342ANG
<8.60 µg/L 8.60 10.0Benzyl alcohol 1 04/11/22 19:07 V17342ANG
<5.67 µg/L 5.67 10.0Bis(2-Chloroethoxy)methane 1 04/11/22 19:07 V17342ANG
<7.30 µg/L 7.30 10.0Bis(2-Chloroethyl)ether 1 04/11/22 19:07 V17342ANG
<6.59 µg/L 6.59 10.0Bis(2-Chloroisopropyl)ether 1 04/11/22 19:07 V17342ANG
<8.80 µg/L 8.80 10.0Bis(2-ethylhexyl)phthalate 1 04/11/22 19:07 V17342ANG
<6.26 µg/L 6.26 20.04-Bromophenyl phenyl ether 1 04/11/22 19:07 V17342ANG
<2.94 µg/L 2.94 10.0
Butyl benzyl phthalate 1 04/11/22 19:07 V17342ANG
<5.23 µg/L 5.23 10.04-Chloro-3-methylphenol 1 04/11/22 19:07 V17342ANG
<5.42 µg/L 5.42 10.04-Chloroaniline 1 04/11/22 19:07 V17342ANG
<7.38 µg/L 7.38 20.02-Chloronaphthalene 1 04/11/22 19:07 V17342ANG
<6.58 µg/L 6.58 10.02-Chlorophenol 1 04/11/22 19:07 V17342ANG
<6.99 µg/L 6.99 20.04-Chlorophenyl phenyl ether 1 04/11/22 19:07 V17342ANG
<5.38 µg/L 5.38 10.0Chrysene 1 04/11/22 19:07 V17342ANG
<6.01 µg/L 6.01 20.0
Dibenz(a,h)anthracene 1 04/11/22 19:07 V17342ANG
<5.08 µg/L 5.08 20.0Dibenzofuran 1 04/11/22 19:07 V17342ANG
<5.91 µg/L 5.91 10.01,2-Dichlorobenzene 1 04/11/22 19:07 V17342ANG
<5.83 µg/L 5.83 10.01,3-Dichlorobenzene 1 04/11/22 19:07 V17342ANG
<5.91 µg/L 5.91 10.01,4-Dichlorobenzene 1 04/11/22 19:07 V17342ANG
<6.60 µg/L 6.60 10.03,3'-Dichlorobenzidine 1 04/11/22 19:07 V17342ANG
<5.54 µg/L 5.54 10.02,4-Dichlorophenol 1 04/11/22 19:07 V17342ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 12 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<9.35 µg/L 9.35 20.0Diethyl phthalate 1 04/11/22 19:07 V17342ANG
<7.82 µg/L 7.82 10.0Dimethyl phthalate 1 04/11/22 19:07 V17342ANG
<10.9 µg/L 10.9 20.02,4-Dimethylphenol 1 04/11/22 19:07 V17342ANG
<7.35 µg/L 7.35 10.0Di-n-butyl phthalate 1 04/11/22 19:07 V17342ANG
<9.92 µg/L 9.92 30.04,6-Dinitro-2-methylphenol 1 04/11/22 19:07 V17342ANG
<10.6 µg/L 10.6 30.02,4-Dinitrophenol 1 04/11/22 19:07 V17342ANG
<5.20 µg/L 5.20 10.02,4-Dinitrotoluene 1 04/11/22 19:07 V17342ANG
<5.90 µg/L 5.90 20.02,6-Dinitrotoluene 1 04/11/22 19:07 V17342ANG
<5.01 µg/L 5.01 10.0
Di-n-Octyl Phthalate 1 04/11/22 19:07 V17342ANG
<6.03 µg/L 6.03 10.0Fluoranthene 1 04/11/22 19:07 V17342ANG
<7.27 µg/L 7.27 10.0Fluorene 1 04/11/22 19:07 V17342ANG
<5.75 µg/L 5.75 20.0Hexachlorobenzene 1 04/11/22 19:07 V17342ANG
<5.88 µg/L 5.88 20.0Hexachlorobutadiene 1 04/11/22 19:07 V17342ANG
<5.90 µg/L 5.90 20.0Hexachlorocyclopentadiene 1 04/11/22 19:07 V17342ANG
<5.22 µg/L 5.22 10.0Hexachloroethane 1 04/11/22 19:07 V17342ANG
<6.20 µg/L 6.20 10.0
Indeno(1,2,3-cd)pyrene 1 04/11/22 19:07 V17342ANG
<6.71 µg/L 6.71 10.0Isophorone 1 04/11/22 19:07 V17342ANG
<7.33 µg/L 7.33 10.01-Methylnaphthalene 1 04/11/22 19:07 V17342ANG
<6.92 µg/L 6.92 10.02-Methylnaphthalene 1 04/11/22 19:07 V17342ANG
<5.26 µg/L 5.26 10.02-Methylphenol 1 04/11/22 19:07 V17342ANG
<2.47 µg/L 2.47 10.03&4 Methylphenol 1 04/11/22 19:07 V17342ANG
<7.88 µg/L 7.88 10.0Naphthalene 1 04/11/22 19:07 V17342ANG
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 13 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-4
97514 Matrix:
4/1/2022 11:20
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V17141 04/08/22 10:00
<4.92 µg/L 4.92 10.02-Nitroaniline 1 04/11/22 19:07 V17342ANG
<4.55 µg/L 4.55 10.03-Nitroaniline 1 04/11/22 19:07 V17342ANG
<5.10 µg/L 5.10 10.04-Nitroaniline 1 04/11/22 19:07 V17342ANG
<7.88 µg/L 7.88 10.0Nitrobenzene 1 04/11/22 19:07 V17342ANG
<5.49 µg/L 5.49 10.02-Nitrophenol 1 04/11/22 19:07 V17342ANG
<2.81 µg/L 2.81 10.04-Nitrophenol 1 04/11/22 19:07 V17342ANG
<6.49 µg/L 6.49 10.0N-Nitrosodimethylamine 1 04/11/22 19:07 V17342ANG
<10.9 µg/L 10.9 20.0N-Nitrosodiphenylamine 1 04/11/22 19:07 V17342ANG
<8.10 µg/L 8.10 20.0
N-Nitroso-di-n-propylamine 1 04/11/22 19:07 V17342ANG
<9.73 µg/L 9.73 50.0Pentachlorophenol 1 04/11/22 19:07 V17342ANG
<6.34 µg/L 6.34 10.0Phenanthrene 1 04/11/22 19:07 V17342ANG
<2.86 µg/L 2.86 10.0Phenol 1 04/11/22 19:07 V17342ANG
<5.42 µg/L 5.42 10.0Pyrene 1 04/11/22 19:07 V17342ANG
<5.32 µg/L 5.32 10.0Pyridine 1 04/11/22 19:07 V17342ANG
<6.25 µg/L 6.25 10.01,2,4-Trichlorobenzene 1 04/11/22 19:07 V17342ANG
<5.81 µg/L 5.81 20.0
2,4,5-Trichlorophenol 1 04/11/22 19:07 V17342ANG
<6.29 µg/L 6.29 20.02,4,6-Trichlorophenol 1 04/11/22 19:07 V17342ANG
8270ESurrogate: Phenol-d5 22.1 Limits: 11-100%04/11/22 19:071 ANG
Surrogate: 2-Fluorobiphenyl 52.0 Limits: 44-119%04/11/22 19:071 ANG V17342
Surrogate: 2-Fluorophenol 36.1 Limits: 19-119%04/11/22 19:071 ANG V17342
Surrogate: Nitrobenzene-d5 54.4 Limits: 44-120%04/11/22 19:071 ANG V17342
Surrogate: 4-Terphenyl-d14 74.2 Limits: 50-134%04/11/22 19:071 ANG V17342
Surrogate: 2,4,6-Tribromophenol 68.8 Limits: 43-140%04/11/22 19:071 ANG V17342
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 14 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
3.16 J µg/L 2.45 5.00Arsenic 5 04/07/22 18:41 6020BEDV
<2.45 µg/L 2.45 5.00Dissolved Arsenic 5 04/15/22 08:14 6020BEDV
220 µg/L 17.0 50.0Barium 5 04/07/22 18:41 6020BEDV
128 µg/L 17.0 50.0Dissolved Barium 5 04/15/22 08:14 6020BEDV
<0.750 µg/L 0.750 5.00Cadmium 5 04/07/22 18:41 6020BEDV
<0.750 µg/L 0.750 5.00
Dissolved Cadmium 5 04/15/22 08:14 6020BEDV
85.3 µg/L 5.00 10.0Chromium 5 04/07/22 18:41 6020BEDV
25.5 µg/L 5.00 10.0Dissolved Chromium 5 04/15/22 08:14 6020BEDV
32.1 µg/L 2.50 5.00Lead 5 04/07/22 18:41 6020BEDV
6.70 µg/L 2.50 5.00Dissolved Lead 5 04/15/22 08:14 6020BEDV
<0.00007 mg/L 0.00007 0.00020Mercury (Total)1 04/06/22 16:12 7470AEDV
<0.00007 mg/L 0.00007 0.00020Dissolved Mercury 1 04/15/22 12:41 7470AEDV
<11.5 µg/L 11.5 25.0
Selenium 5 04/07/22 18:41 6020BEDV
<11.5 µg/L 11.5 25.0Dissolved Selenium 5 04/15/22 08:14 6020BEDV
<0.650 µg/L 0.650 5.00Silver 5 04/07/22 18:41 6020BEDV
<0.650 µg/L 0.650 5.00Dissolved Silver 5 04/15/22 08:14 6020BEDV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 15 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
5.81 µg/L 1.80 5.00Acetone 1 04/08/22 08:05 V17188JLB
<2.00 µg/L 2.00 5.00Acrolein 1 04/08/22 08:05 V17188JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 04/08/22 08:05 V17188JLB
<0.180 µg/L 0.180 0.500Benzene 1 04/08/22 08:05 V17188JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/08/22 08:05 V17188JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/08/22 08:05 V17188JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/08/22 08:05 V17188JLB
<1.50 µg/L 1.50 5.00Bromoform 1 04/08/22 08:05 V17188JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 04/08/22 08:05 V17188JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 04/08/22 08:05 V17188JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/08/22 08:05 V17188JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/08/22 08:05 V17188JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 04/08/22 08:05 V17188JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/08/22 08:05 V17188JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/08/22 08:05 V17188JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 04/08/22 08:05 V17188JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 04/08/22 08:05 V17188JLB
0.248 J µg/L 0.220 0.500Chloroform 1 04/08/22 08:05 V17188JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 04/08/22 08:05 V17188JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/08/22 08:05 V17188JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/08/22 08:05 V17188JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 04/08/22 08:05 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 16 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/08/22 08:05 V17188JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/08/22 08:05 V17188JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/08/22 08:05 V17188JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/08/22 08:05 V17188JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/08/22 08:05 V17188JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/08/22 08:05 V17188JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/08/22 08:05 V17188JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/08/22 08:05 V17188JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 04/08/22 08:05 V17188JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/08/22 08:05 V17188JLB
0.428 J µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/08/22 08:05 V17188JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/08/22 08:05 V17188JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/08/22 08:05 V17188JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/08/22 08:05 V17188JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/08/22 08:05 V17188JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 04/08/22 08:05 V17188JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/08/22 08:05 V17188JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/08/22 08:05 V17188JLB
<42.0 µg/L 42.0 200Ethanol 1 04/08/22 08:05 V17188JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 04/08/22 08:05 V17188JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 04/08/22 08:05 V17188JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 04/08/22 08:05 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 17 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<1.30 µg/L 1.30 10.0n-Hexane 1 04/08/22 08:05 V17188JLB
<0.380 µg/L 0.380 5.002-Hexanone 1 04/08/22 08:05 V17188JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 04/08/22 08:05 V17188JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/08/22 08:05 V17188JLB
1.62 J µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/08/22 08:05 V17188JLB
0.801 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 04/08/22 08:05 V17188JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 04/08/22 08:05 V17188JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 04/08/22 08:05 V17188JLB
<0.470 µg/L 0.470 1.00
Naphthalene 1 04/08/22 08:05 V17188JLB
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/08/22 08:05 V17188JLB
<0.220 µg/L 0.220 0.500Styrene 1 04/08/22 08:05 V17188JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/08/22 08:05 V17188JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/08/22 08:05 V17188JLB
4.95 µg/L 0.220 0.500Tetrachloroethene 1 04/08/22 08:05 V17188JLB
0.291 J µg/L 0.220 0.500Toluene 1 04/08/22 08:05 V17188JLB
<0.380 µg/L 0.380 2.00
1,2,3-Trichlorobenzene 1 04/08/22 08:05 V17188JLB
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 04/08/22 08:05 V17188JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/08/22 08:05 V17188JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/08/22 08:05 V17188JLB
2.51 µg/L 0.180 0.500Trichloroethene 1 04/08/22 08:05 V17188JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/08/22 08:05 V17188JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 04/08/22 08:05 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 18 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/08/22 08:05 V17188JLB
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 04/08/22 08:05 V17188JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/08/22 08:05 V17188JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 04/08/22 08:05 V17188JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 04/08/22 08:05 V17188JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 04/08/22 08:05 V17188
Surrogate: 4-Bromofluorobenzene 99.2 Limits: 80-124%04/08/22 08:051 JLB V17188
Surrogate: Dibromofluoromethane 99.6 Limits: 75-129%04/08/22 08:051 JLB V17188
Surrogate: 1,2-Dichloroethane - d4 100 Limits: 63-136%04/08/22 08:051 JLB V17188
Surrogate: Toluene-d8 99.2 Limits: 77-123%04/08/22 08:051 JLB V17188
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V16999 04/05/22 10:10
<8.01 µg/L 8.01 22.5Acenaphthene 1 04/06/22 18:51 V17076JMV
<7.81 µg/L 7.81 22.5Acenaphthylene 1 04/06/22 18:51 V17076JMV
<8.01 µg/L 8.01 56.2Aniline 1 04/06/22 18:51 V17076JMV
<7.36 µg/L 7.36 11.2Anthracene 1 04/06/22 18:51 V17076JMV
<6.33 µg/L 6.33 11.2Benzo(a)anthracene 1 04/06/22 18:51 V17076JMV
<5.23 µg/L 5.23 11.2Benzo(a)pyrene 1 04/06/22 18:51 V17076JMV
<5.06 µg/L 5.06 11.2
Benzo(b)fluoranthene 1 04/06/22 18:51 V17076JMV
<4.75 µg/L 4.75 11.2Benzo(g,h,i)perylene 1 04/06/22 18:51 V17076JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 19 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V16999 04/05/22 10:10
<5.24 µg/L 5.24 11.2Benzo(k)fluoranthene 1 04/06/22 18:51 V17076JMV
<12.9 µg/L 12.9 112Benzoic Acid 1 04/06/22 18:51 V17076JMV
<9.63 µg/L 9.63 11.2Benzyl alcohol 1 04/06/22 18:51 V17076JMV
<6.35 µg/L 6.35 11.2Bis(2-Chloroethoxy)methane 1 04/06/22 18:51 V17076JMV
<8.18 µg/L 8.18 11.2Bis(2-Chloroethyl)ether 1 04/06/22 18:51 V17076JMV
<7.38 µg/L 7.38 11.2Bis(2-Chloroisopropyl)ether 1 04/06/22 18:51 V17076JMV
<9.86 µg/L 9.86 11.2Bis(2-ethylhexyl)phthalate 1 04/06/22 18:51 V17076JMV
<7.04 µg/L 7.04 22.54-Bromophenyl phenyl ether 1 04/06/22 18:51 V17076JMV
<3.29 µg/L 3.29 11.2
Butyl benzyl phthalate 1 04/06/22 18:51 V17076JMV
<5.86 µg/L 5.86 11.24-Chloro-3-methylphenol 1 04/06/22 18:51 V17076JMV
<6.07 µg/L 6.07 11.24-Chloroaniline 1 04/06/22 18:51 V17076JMV
<8.30 µg/L 8.30 22.52-Chloronaphthalene 1 04/06/22 18:51 V17076JMV
<7.37 µg/L 7.37 11.22-Chlorophenol 1 04/06/22 18:51 V17076JMV
<7.86 µg/L 7.86 22.54-Chlorophenyl phenyl ether 1 04/06/22 18:51 V17076JMV
<6.03 µg/L 6.03 11.2Chrysene 1 04/06/22 18:51 V17076JMV
<6.76 µg/L 6.76 22.5
Dibenz(a,h)anthracene 1 04/06/22 18:51 V17076JMV
<5.72 µg/L 5.72 22.5Dibenzofuran 1 04/06/22 18:51 V17076JMV
<6.62 µg/L 6.62 11.21,2-Dichlorobenzene 1 04/06/22 18:51 V17076JMV
<6.53 µg/L 6.53 11.21,3-Dichlorobenzene 1 04/06/22 18:51 V17076JMV
<6.62 µg/L 6.62 11.21,4-Dichlorobenzene 1 04/06/22 18:51 V17076JMV
<7.39 µg/L 7.39 11.23,3'-Dichlorobenzidine 1 04/06/22 18:51 V17076JMV
<6.20 µg/L 6.20 11.22,4-Dichlorophenol 1 04/06/22 18:51 V17076JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 20 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V16999 04/05/22 10:10
<10.5 µg/L 10.5 22.5Diethyl phthalate 1 04/06/22 18:51 V17076JMV
<8.76 µg/L 8.76 11.2Dimethyl phthalate 1 04/06/22 18:51 V17076JMV
<12.3 µg/L 12.3 22.52,4-Dimethylphenol 1 04/06/22 18:51 V17076JMV
<8.23 µg/L 8.23 11.2Di-n-butyl phthalate 1 04/06/22 18:51 V17076JMV
<11.1 µg/L 11.1 33.74,6-Dinitro-2-methylphenol 1 04/06/22 18:51 V17076JMV
<11.9 µg/L 11.9 33.72,4-Dinitrophenol 1 04/06/22 18:51 V17076JMV
<5.82 µg/L 5.82 11.22,4-Dinitrotoluene 1 04/06/22 18:51 V17076JMV
<6.64 µg/L 6.64 22.52,6-Dinitrotoluene 1 04/06/22 18:51 V17076JMV
<5.61 µg/L 5.61 11.2
Di-n-Octyl Phthalate 1 04/06/22 18:51 V17076JMV
<6.75 µg/L 6.75 11.2Fluoranthene 1 04/06/22 18:51 V17076JMV
<8.14 µg/L 8.14 11.2Fluorene 1 04/06/22 18:51 V17076JMV
<6.47 µg/L 6.47 22.5Hexachlorobenzene 1 04/06/22 18:51 V17076JMV
<6.62 µg/L 6.62 22.5Hexachlorobutadiene 1 04/06/22 18:51 V17076JMV
<6.64 µg/L 6.64 22.5Hexachlorocyclopentadiene 1 04/06/22 18:51 V17076JMV
<5.85 µg/L 5.85 11.2Hexachloroethane 1 04/06/22 18:51 V17076JMV
<6.94 µg/L 6.94 11.2
Indeno(1,2,3-cd)pyrene 1 04/06/22 18:51 V17076JMV
<7.52 µg/L 7.52 11.2Isophorone 1 04/06/22 18:51 V17076JMV
<8.21 µg/L 8.21 11.21-Methylnaphthalene 1 04/06/22 18:51 V17076JMV
<7.75 µg/L 7.75 11.22-Methylnaphthalene 1 04/06/22 18:51 V17076JMV
<5.89 µg/L 5.89 11.22-Methylphenol 1 04/06/22 18:51 V17076JMV
<2.77 µg/L 2.77 11.23&4 Methylphenol 1 04/06/22 18:51 V17076JMV
<8.83 µg/L 8.83 11.2Naphthalene 1 04/06/22 18:51 V17076JMV
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 21 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TMW-6
97515 Matrix:
3/31/2022 10:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
3510C
8270E Prep Batch(es):V16999 04/05/22 10:10
<5.51 µg/L 5.51 11.22-Nitroaniline 1 04/06/22 18:51 V17076JMV
<5.10 µg/L 5.10 11.23-Nitroaniline 1 04/06/22 18:51 V17076JMV
<5.71 µg/L 5.71 11.24-Nitroaniline 1 04/06/22 18:51 V17076JMV
<8.83 µg/L 8.83 11.2Nitrobenzene 1 04/06/22 18:51 V17076JMV
<6.15 µg/L 6.15 11.22-Nitrophenol 1 04/06/22 18:51 V17076JMV
<3.15 µg/L 3.15 11.24-Nitrophenol 1 04/06/22 18:51 V17076JMV
<7.27 µg/L 7.27 11.2N-Nitrosodimethylamine 1 04/06/22 18:51 V17076JMV
<12.3 µg/L 12.3 22.5N-Nitrosodiphenylamine 1 04/06/22 18:51 V17076JMV
<9.11 µg/L 9.11 22.5
N-Nitroso-di-n-propylamine 1 04/06/22 18:51 V17076JMV
<10.9 µg/L 10.9 56.2Pentachlorophenol 1 04/06/22 18:51 V17076JMV
<7.10 µg/L 7.10 11.2Phenanthrene 1 04/06/22 18:51 V17076JMV
<3.20 µg/L 3.20 11.2Phenol 1 04/06/22 18:51 V17076JMV
<6.07 µg/L 6.07 11.2Pyrene 1 04/06/22 18:51 V17076JMV
<5.96 µg/L 5.96 11.2Pyridine 1 04/06/22 18:51 V17076JMV
<7.00 µg/L 7.00 11.21,2,4-Trichlorobenzene 1 04/06/22 18:51 V17076JMV
<6.54 µg/L 6.54 22.5
2,4,5-Trichlorophenol 1 04/06/22 18:51 V17076JMV
<7.08 µg/L 7.08 22.52,4,6-Trichlorophenol 1 04/06/22 18:51 V17076JMV
8270ESurrogate: Phenol-d5 28.4 Limits: 11-100%04/06/22 18:511 JMV
Surrogate: 2-Fluorobiphenyl 37.0 *Limits: 44-119%04/06/22 18:511 JMV V17076
Surrogate: 2-Fluorophenol 38.8 Limits: 19-119%04/06/22 18:511 JMV V17076
Surrogate: Nitrobenzene-d5 40.6 *Limits: 44-120%04/06/22 18:511 JMV V17076
Surrogate: 4-Terphenyl-d14 54.4 Limits: 50-134%04/06/22 18:511 JMV V17076
Surrogate: 2,4,6-Tribromophenol 54.6 Limits: 43-140%04/06/22 18:511 JMV V17076
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 22 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TB-1
97516 Matrix:
3/31/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<1.80 µg/L 1.80 5.00Acetone 1 04/08/22 02:20 V17188JLB
<2.00 µg/L 2.00 5.00Acrolein 1 04/08/22 02:20 V17188JLB
<0.230 µg/L 0.230 5.00Acrylonitrile 1 04/08/22 02:20 V17188JLB
<0.180 µg/L 0.180 0.500Benzene 1 04/08/22 02:20 V17188JLB
<0.210 µg/L 0.210 0.500Bromobenzene 1 04/08/22 02:20 V17188JLB
<0.420 µg/L 0.420 1.00Bromochloromethane 1 04/08/22 02:20 V17188JLB
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 04/08/22 02:20 V17188JLB
<1.50 µg/L 1.50 5.00Bromoform 1 04/08/22 02:20 V17188JLB
<0.280 µg/L 0.280 1.00
Bromomethane 1 04/08/22 02:20 V17188JLB
<0.185 µg/L 0.185 1.00n-Butylbenzene 1 04/08/22 02:20 V17188JLB
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 04/08/22 02:20 V17188JLB
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 04/08/22 02:20 V17188JLB
<0.150 µg/L 0.150 5.00Carbon Disulfide 1 04/08/22 02:20 V17188JLB
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 04/08/22 02:20 V17188JLB
<0.190 µg/L 0.190 0.500Chlorobenzene 1 04/08/22 02:20 V17188JLB
<0.190 µg/L 0.190 0.500
Chlorodibromomethane 1 04/08/22 02:20 V17188JLB
<0.430 µg/L 0.430 1.00Chloroethane 1 04/08/22 02:20 V17188JLB
<0.220 µg/L 0.220 0.500Chloroform 1 04/08/22 02:20 V17188JLB
<0.220 µg/L 0.220 0.500Chloromethane 1 04/08/22 02:20 V17188JLB
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 04/08/22 02:20 V17188JLB
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 04/08/22 02:20 V17188JLB
<0.960 µg/L 0.960 5.00Di-Isopropyl Ether (DIPE)1 04/08/22 02:20 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 23 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TB-1
97516 Matrix:
3/31/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<1.10 µg/L 1.10 2.001,2-Dibromo-3-Chloropropane 1 04/08/22 02:20 V17188JLB
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 04/08/22 02:20 V17188JLB
<0.230 µg/L 0.230 0.500Dibromomethane 1 04/08/22 02:20 V17188JLB
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 04/08/22 02:20 V17188JLB
<0.190 µg/L 0.190 0.5001,3-Dichlorobenzene 1 04/08/22 02:20 V17188JLB
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 04/08/22 02:20 V17188JLB
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 04/08/22 02:20 V17188JLB
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 04/08/22 02:20 V17188JLB
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 04/08/22 02:20 V17188JLB
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 04/08/22 02:20 V17188JLB
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 04/08/22 02:20 V17188JLB
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 04/08/22 02:20 V17188JLB
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 04/08/22 02:20 V17188JLB
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 04/08/22 02:20 V17188JLB
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 04/08/22 02:20 V17188JLB
<0.200 µg/L 0.200 0.500
1,1-Dichloropropene 1 04/08/22 02:20 V17188JLB
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 04/08/22 02:20 V17188JLB
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 04/08/22 02:20 V17188JLB
<42.0 µg/L 42.0 200Ethanol 1 04/08/22 02:20 V17188JLB
<0.170 µg/L 0.170 0.500Ethylbenzene 1 04/08/22 02:20 V17188JLB
<1.80 µg/L 1.80 10.0Ethyl Tertiary Butyl Ether (ETBE)1 04/08/22 02:20 V17188JLB
<0.350 µg/L 0.350 2.00Hexachlorobutadiene 1 04/08/22 02:20 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 24 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TB-1
97516 Matrix:
3/31/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<1.30 µg/L 1.30 10.0n-Hexane 1 04/08/22 02:20 V17188JLB
<0.380 µg/L 0.380 5.002-Hexanone 1 04/08/22 02:20 V17188JLB
<0.180 µg/L 0.180 5.00Isopropylbenzene 1 04/08/22 02:20 V17188JLB
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 04/08/22 02:20 V17188JLB
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 04/08/22 02:20 V17188JLB
<0.140 µg/L 0.140 0.500Methyl tert-butyl ether (MTBE)1 04/08/22 02:20 V17188JLB
<1.00 µg/L 1.00 5.004-Methyl-2-Pentanone 1 04/08/22 02:20 V17188JLB
<0.330 µg/L 0.330 1.00Methylene Chloride 1 04/08/22 02:20 V17188JLB
<0.470 µg/L 0.470 1.00
Naphthalene 1 04/08/22 02:20 V17188JLB
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 04/08/22 02:20 V17188JLB
<0.220 µg/L 0.220 0.500Styrene 1 04/08/22 02:20 V17188JLB
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 04/08/22 02:20 V17188JLB
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 04/08/22 02:20 V17188JLB
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 04/08/22 02:20 V17188JLB
<0.220 µg/L 0.220 0.500Toluene 1 04/08/22 02:20 V17188JLB
<0.380 µg/L 0.380 2.00
1,2,3-Trichlorobenzene 1 04/08/22 02:20 V17188JLB
<0.310 µg/L 0.310 1.001,2,4-Trichlorobenzene 1 04/08/22 02:20 V17188JLB
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 04/08/22 02:20 V17188JLB
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 04/08/22 02:20 V17188JLB
<0.180 µg/L 0.180 0.500Trichloroethene 1 04/08/22 02:20 V17188JLB
<0.180 µg/L 0.180 0.500Trichlorofluoromethane 1 04/08/22 02:20 V17188JLB
<0.270 µg/L 0.270 1.001,2,3-Trichloropropane 1 04/08/22 02:20 V17188JLB
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 25 of 55
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28203
22-091-0033
01102
Hart & Hickman (Charlotte)
2923 South Tryon St. Ste 100
Bo Cappleman
Charlotte
Received : 04/01/2022
SLC.001
Report Date : 04/20/2022
Sample ID :
Lab No :
Sampled:TB-1
97516 Matrix:
3/31/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
5030B
8260D Prep Batch(es):V17186 04/07/22 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 04/08/22 02:20 V17188JLB
<1.00 µg/L 1.00 2.00Vinyl Acetate 1 04/08/22 02:20 V17188JLB
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 04/08/22 02:20 V17188JLB
<0.210 µg/L 0.210 0.500o-Xylene 1 04/08/22 02:20 V17188JLB
<0.420 µg/L 0.420 1.00m,p-Xylene 1 04/08/22 02:20 V17188JLB
<0.21 µg/L 0.210 0.500Xylene (Total)1 04/08/22 02:20 V17188
Surrogate: 4-Bromofluorobenzene 98.2 Limits: 80-124%04/08/22 02:201 JLB V17188
Surrogate: Dibromofluoromethane 100 Limits: 75-129%04/08/22 02:201 JLB V17188
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 63-136%04/08/22 02:201 JLB V17188
Surrogate: Toluene-d8 101 Limits: 77-123%04/08/22 02:201 JLB V17188
Qualifiers/
Definitions
Dilution FactorDFOutside QC Limit*
Method Quantitation LimitMQLEstimated valueJ
Page 26 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17145QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17088
Associated Lab Samples: 97514, 97515
LRB-V17088 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/07/22 15:491.000.490<0.490µg/LArsenic
04/07/22 15:4910.03.40<3.40µg/LBarium
04/07/22 15:491.000.150<0.150µg/LCadmium
04/07/22 15:492.001.00<1.00µg/LChromium
04/07/22 15:491.000.500<0.500µg/LLead
04/07/22 15:495.002.30<2.30µg/LSelenium
04/07/22 15:491.000.130<0.130µg/LSilver
LCS-V17088Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.092.4100µg/LArsenic 80-120
95.095.3100µg/LBarium 80-120
92.092.4100µg/LCadmium 80-120
95.095.0100µg/LChromium 80-120
95.094.5100µg/LLead 80-120
97.097.2100µg/LSelenium 80-120
93.092.6100µg/LSilver 80-120
V 97514-MS-V17088 V 97514-MSD-V17088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
97.4 96.095.81001001.49µg/LArsenic 94.0 75-125 1.6 20.0
243 88.0244100100155µg/LBarium 89.0 75-125 0.4 20.0
96.9 97.096.9100100< 0.150µg/LCadmium 97.0 75-125 0.0 20.0
98.4 95.098.81001003.37µg/LChromium 95.0 75-125 0.4 20.0
Page 1 of 27Date:04/20/2022 04:28 PM
Page 27 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17145QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17088
V 97514-MS-V17088 V 97514-MSD-V17088Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
101 97.01001001004.19µg/LLead 96.0 75-125 0.9 20.0
99.1 99.093.0100100< 2.30µg/LSelenium 93.0 75-125 6.3 20.0
97.6 97.096.41001000.439µg/LSilver 96.0 75-125 1.2 20.0
V 97514-PDS-V17088Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/07/22 16:2299.050.4µg/LArsenic
04/07/22 16:2299.0126µg/LBarium
04/07/22 16:2210150.3µg/LCadmium
04/07/22 16:2299.051.3µg/LChromium
04/07/22 16:2299.051.7µg/LLead
04/07/22 16:2298.048.8µg/LSelenium
04/07/22 16:2210050.4µg/LSilver
Page 2 of 27Date:04/20/2022 04:28 PM
Page 28 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17508QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17502
Associated Lab Samples: 97515
LRB-V17502 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/15/22 07:411.000.490<0.490µg/LDissolved Arsenic
04/15/22 07:4110.03.40<3.40µg/LDissolved Barium
04/15/22 07:411.000.150<0.150µg/LDissolved Cadmium
04/15/22 07:412.001.00<1.00µg/LDissolved Chromium
04/15/22 07:411.000.500<0.500µg/LDissolved Lead
04/15/22 07:415.002.30<2.30µg/LDissolved Selenium
04/15/22 07:411.000.130<0.130µg/LDissolved Silver
LCS-V17502Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
94.094.2100µg/LDissolved Arsenic 80-120
108108100µg/LDissolved Barium 80-120
93.093.4100µg/LDissolved Cadmium 80-120
93.092.8100µg/LDissolved Chromium 80-120
10099.5100µg/LDissolved Lead 80-120
100100100µg/LDissolved Selenium 80-120
98.097.9100µg/LDissolved Silver 80-120
V 97580-V17498-MS-V17502 V 97580-V17498-MSD-V17502Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
93.9 94.094.3100100< 2.45µg/LDissolved Arsenic 94.0 75-125 0.4 20.0
291 110262100100181µg/LDissolved Barium 81.0 75-125 10.4 20.0
93.0 93.094.2100100< 0.750µg/LDissolved Cadmium 94.0 75-125 1.2 20.0
87.6 88.093.6100100< 5.00µg/LDissolved Chromium 94.0 75-125 6.6 20.0
Page 3 of 27Date:04/20/2022 04:28 PM
Page 29 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17508QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17502
V 97580-V17498-MS-V17502 V 97580-V17498-MSD-V17502Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
101 96.099.21001005.27µg/LDissolved Lead 94.0 75-125 1.7 20.0
99.8 10093.4100100< 11.5µg/LDissolved Selenium 93.0 75-125 6.6 20.0
92.8 93.094.2100100< 0.650µg/LDissolved Silver 94.0 75-125 1.4 20.0
V 97580-V17498-PDS-V17502Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/15/22 08:40106266µg/LDissolved Arsenic
04/15/22 08:40105359µg/LDissolved Barium
04/15/22 08:40106264µg/LDissolved Cadmium
04/15/22 08:4099.0248µg/LDissolved Chromium
04/15/22 08:40102257µg/LDissolved Lead
04/15/22 08:40101253µg/LDissolved Selenium
04/15/22 08:40102256µg/LDissolved Silver
Page 4 of 27Date:04/20/2022 04:28 PM
Page 30 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17767QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17708
Associated Lab Samples: 97514
LRB-V17708 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/20/22 14:291.000.490<0.490µg/LDissolved Arsenic
04/20/22 14:2910.03.40<3.40µg/LDissolved Barium
04/20/22 14:291.000.150<0.150µg/LDissolved Cadmium
04/20/22 14:292.001.00<1.00µg/LDissolved Chromium
04/20/22 14:291.000.500<0.500µg/LDissolved Lead
04/20/22 14:295.002.30<2.30µg/LDissolved Selenium
04/20/22 14:291.000.130<0.130µg/LDissolved Silver
LCS-V17708Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
92.091.9100µg/LDissolved Arsenic 80-120
99.098.6100µg/LDissolved Barium 80-120
97.097.0100µg/LDissolved Cadmium 80-120
91.091.3100µg/LDissolved Chromium 80-120
94.093.7100µg/LDissolved Lead 80-120
98.098.0100µg/LDissolved Selenium 80-120
95.094.6100µg/LDissolved Silver 80-120
V 97514-V17654-MS-V17708 V 97514-V17654-MSD-V17708Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
92.7 92.093.01001000.711µg/LDissolved Arsenic 92.0 75-125 0.3 20.0
191 95.018410010095.9µg/LDissolved Barium 88.0 75-125 3.7 20.0
99.0 99.098.7100100< 0.150µg/LDissolved Cadmium 99.0 75-125 0.3 20.0
92.2 92.085.3100100< 1.00µg/LDissolved Chromium 85.0 75-125 7.7 20.0
Page 5 of 27Date:04/20/2022 04:28 PM
Page 31 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Metals Analyses
6020B
V17767QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3005A
QC Prep:V17708
V 97514-V17654-MS-V17708 V 97514-V17654-MSD-V17708Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
92.9 92.091.31001000.663µg/LDissolved Lead 91.0 75-125 1.7 20.0
103 103105100100< 2.30µg/LDissolved Selenium 105 75-125 1.9 20.0
87.3 87.081.4100100< 0.130µg/LDissolved Silver 81.0 75-125 6.9 20.0
V 97514-V17654-PDS-V17708Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/20/22 15:0197.048.9µg/LDissolved Arsenic
04/20/22 15:0197.095.1µg/LDissolved Barium
04/20/22 15:0199.049.7µg/LDissolved Cadmium
04/20/22 15:0191.045.6µg/LDissolved Chromium
04/20/22 15:0195.048.0µg/LDissolved Lead
04/20/22 15:0110351.4µg/LDissolved Selenium
04/20/22 15:0197.048.6µg/LDissolved Silver
Page 6 of 27Date:04/20/2022 04:28 PM
Page 32 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V17054,V17084QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V17014
Associated Lab Samples: 97514, 97515
LRB-V17014 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/06/22 14:330.000200.00007<0.00007mg/LMercury (Total)
LCS-V17014Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1000.009370.00937mg/LMercury (Total)80-120
V 97187-MS-V17014 V 97187-MSD-V17014Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00902 96.00.008970.009370.00937< 0.00007mg/LMercury (Total)96.0 80-120 0.5 20.0
V 97187-PDS-V17014Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/06/22 17:0695.00.00443mg/LMercury (Total)
Page 7 of 27Date:04/20/2022 04:28 PM
Page 33 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V17547QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V17503
Associated Lab Samples: 97515
LRB-V17503 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/15/22 12:220.000200.0000.00004mg/LDissolved Mercury
LCS-V17503Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1010.009510.00937mg/LDissolved Mercury 80-120
V 97581-V17498-MS-V17503 V 97581-V17498-MSD-V17503Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00249 27.0*0.002550.009370.00937< 0.00007mg/LDissolved Mercury 27.0*80-120 2.3 20.0
V 97581-V17498-PDS-V17503Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/15/22 12:3646.0*0.00215mg/LDissolved Mercury
Page 8 of 27* QC Fail Date:04/20/2022 04:28 PM
Page 34 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Total Aqueous Mercury Analysis - CVAA
7470A
V17712QC Analytical Batch(es):
Analysis Method:
Analysis Description:
7470A
QC Prep:V17672
Associated Lab Samples: 97514
LRB-V17672 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
04/19/22 20:170.000200.0000.00003mg/LDissolved Mercury
LCS-V17672Laboratory Control Sample
Parameter
LCS %RecLCS
Result
Spike
Conc.Units
% Rec
Limits
1090.01020.00937mg/LDissolved Mercury 80-120
V 97514-V17654-MS-V17672 V 97514-V17654-MSD-V17672Matrix Spike & Matrix Spike Duplicate
MS Result
Parameter
Max
RPD
MS
%Rec
MSD
Result
MSD
Spike
Conc.
MS Spike
Conc.ResultUnits
%Rec
Limits
MSD
%Rec RPD
0.00913 97.00.008730.009370.00937< 0.00007mg/LDissolved Mercury 93.0 80-120 4.4 20.0
V 97514-V17654-PDS-V17672Post Digestion Spike
Parameter
Analyzed%
Recovery
PDS
ResultUnits
04/19/22 20:4293.00.00436mg/LDissolved Mercury
Page 9 of 27Date:04/20/2022 04:28 PM
Page 35 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17188QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17186
Associated Lab Samples: 97514, 97515, 97516
LRB-V17186 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/08/22 01:555.001.80<1.80µg/LAcetone
04/08/22 01:555.002.00<2.00µg/LAcrolein
04/08/22 01:555.000.230<0.230µg/LAcrylonitrile
04/08/22 01:550.5000.180<0.180µg/LBenzene
04/08/22 01:550.5000.210<0.210µg/LBromobenzene
04/08/22 01:551.000.420<0.420µg/LBromochloromethane
04/08/22 01:550.5000.160<0.160µg/LBromodichloromethane
04/08/22 01:555.001.50<1.50µg/LBromoform
04/08/22 01:551.000.280<0.280µg/LBromomethane
04/08/22 01:551.000.185<0.185µg/Ln-Butylbenzene
04/08/22 01:550.5000.200<0.200µg/Lsec-Butyl benzene
04/08/22 01:552.000.920<0.920µg/Ltert-Butyl benzene
04/08/22 01:555.000.150<0.150µg/LCarbon Disulfide
04/08/22 01:550.5000.180<0.180µg/LCarbon Tetrachloride
04/08/22 01:550.5000.190<0.190µg/LChlorobenzene
04/08/22 01:550.5000.190<0.190µg/LChlorodibromomethane
04/08/22 01:551.000.430<0.430µg/LChloroethane
04/08/22 01:550.5000.220<0.220µg/LChloroform
04/08/22 01:550.5000.220<0.220µg/LChloromethane
04/08/22 01:550.5000.200<0.200µg/L2-Chlorotoluene
04/08/22 01:550.5000.200<0.200µg/L4-Chlorotoluene
04/08/22 01:555.000.960<0.960µg/LDi-Isopropyl Ether (DIPE)
04/08/22 01:552.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
04/08/22 01:550.5000.200<0.200µg/L1,2-Dibromoethane
04/08/22 01:550.5000.230<0.230µg/LDibromomethane
04/08/22 01:550.5000.220<0.220µg/L1,2-Dichlorobenzene
04/08/22 01:550.5000.190<0.190µg/L1,3-Dichlorobenzene
Page 10 of 27Date:04/20/2022 04:28 PM
Page 36 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17188QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17186
Associated Lab Samples: 97514, 97515, 97516
LRB-V17186 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/08/22 01:550.5000.210<0.210µg/L1,4-Dichlorobenzene
04/08/22 01:555.001.20<1.20µg/LDichlorodifluoromethane
04/08/22 01:550.5000.240<0.240µg/L1,1-Dichloroethane
04/08/22 01:550.5000.150<0.150µg/L1,2-Dichloroethane
04/08/22 01:550.5000.150<0.150µg/L1,1-Dichloroethene
04/08/22 01:550.5000.200<0.200µg/Lcis-1,2-Dichloroethene
04/08/22 01:550.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
04/08/22 01:550.5000.190<0.190µg/L1,2-Dichloropropane
04/08/22 01:550.5000.130<0.130µg/L1,3-Dichloropropane
04/08/22 01:552.000.210<0.210µg/L2,2-Dichloropropane
04/08/22 01:550.5000.200<0.200µg/L1,1-Dichloropropene
04/08/22 01:550.5000.210<0.210µg/Lcis-1,3-Dichloropropene
04/08/22 01:550.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
04/08/22 01:5520042.0<42.0µg/LEthanol
04/08/22 01:550.5000.170<0.170µg/LEthylbenzene
04/08/22 01:5510.01.80<1.80µg/LEthyl Tertiary Butyl Ether (ETBE)
04/08/22 01:552.000.350<0.350µg/LHexachlorobutadiene
04/08/22 01:5510.01.30<1.30µg/Ln-Hexane
04/08/22 01:555.000.380<0.380µg/L2-Hexanone
04/08/22 01:555.000.180<0.180µg/LIsopropylbenzene
04/08/22 01:550.5000.089<0.089µg/L4-Isopropyl toluene
04/08/22 01:555.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
04/08/22 01:550.5000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
04/08/22 01:555.001.00<1.00µg/L4-Methyl-2-Pentanone
04/08/22 01:551.000.330<0.330µg/LMethylene Chloride
04/08/22 01:551.000.470<0.470µg/LNaphthalene
04/08/22 01:550.5000.190<0.190µg/Ln-Propylbenzene
Page 11 of 27Date:04/20/2022 04:28 PM
Page 37 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17188QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17186
Associated Lab Samples: 97514, 97515, 97516
LRB-V17186 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/08/22 01:550.5000.220<0.220µg/LStyrene
04/08/22 01:550.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
04/08/22 01:550.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
04/08/22 01:550.5000.220<0.220µg/LTetrachloroethene
04/08/22 01:550.5000.220<0.220µg/LToluene
04/08/22 01:552.000.380<0.380µg/L1,2,3-Trichlorobenzene
04/08/22 01:551.000.310<0.310µg/L1,2,4-Trichlorobenzene
04/08/22 01:550.5000.160<0.160µg/L1,1,1-Trichloroethane
04/08/22 01:550.5000.096<0.096µg/L1,1,2-Trichloroethane
04/08/22 01:550.5000.180<0.180µg/LTrichloroethene
04/08/22 01:550.5000.180<0.180µg/LTrichlorofluoromethane
04/08/22 01:551.000.270<0.270µg/L1,2,3-Trichloropropane
04/08/22 01:550.5000.180<0.180µg/L1,3,5-Trimethylbenzene
04/08/22 01:552.001.00<1.00µg/LVinyl Acetate
04/08/22 01:550.5000.170<0.170µg/LVinyl Chloride
04/08/22 01:550.5000.210<0.210µg/Lo-Xylene
04/08/22 01:551.000.420<0.420µg/Lm,p-Xylene
04/08/22 01:554-Bromofluorobenzene (S)102 80-124
04/08/22 01:55Dibromofluoromethane (S)98.0 75-129
04/08/22 01:551,2-Dichloroethane - d4 (S)101 63-136
04/08/22 01:55Toluene-d8 (S)97.8 77-123
LCS-V17186 LCSD-V17186Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.5 91.296.238.540.0µg/LAcetone 40-166 5.3 20
Page 12 of 27Date:04/20/2022 04:28 PM
Page 38 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17188QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17186
LCS-V17186 LCSD-V17186Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
42.7 10710240.940.0µg/LAcrolein 70-130 4.3 20
43.6 10910742.840.0µg/LAcrylonitrile 81-127 1.8 20
19.7 98.599.019.820.0µg/LBenzene 77-128 0.5 20
20.0 10010220.420.0µg/LBromobenzene 78-129 1.9 20
20.0 10010120.120.0µg/LBromochloromethane 78-135 0.4 20
20.9 10510821.520.0µg/LBromodichloromethane 76-138 2.8 20
21.2 10610420.820.0µg/LBromoform 71-135 1.9 20
19.4 97.096.519.320.0µg/LBromomethane 41-168 0.5 20
19.8 99.010420.720.0µg/Ln-Butylbenzene 68-134 4.4 20
20.4 10210621.120.0µg/Lsec-Butyl benzene 71-131 3.3 20
19.7 98.510320.620.0µg/Ltert-Butyl benzene 70-132 4.4 20
19.3 96.597.519.520.0µg/LCarbon Disulfide 59-135 1.0 20
19.5 97.510220.420.0µg/LCarbon Tetrachloride 72-142 4.5 20
20.8 10410520.920.0µg/LChlorobenzene 78-119 0.4 20
21.5 10810821.520.0µg/LChlorodibromomethane 75-134 0.0 20
20.3 10210120.220.0µg/LChloroethane 57-142 0.4 20
19.8 99.010320.520.0µg/LChloroform 77-130 3.4 20
19.7 98.598.519.720.0µg/LChloromethane 47-145 0.0 20
20.1 10110220.420.0µg/L2-Chlorotoluene 74-126 1.4 20
20.1 10110320.620.0µg/L4-Chlorotoluene 78-129 2.4 20
20.5 10310320.520.0µg/LDi-Isopropyl Ether (DIPE)60-154 0.0 20
21.4 10710420.820.0µg/L1,2-Dibromo-3-Chloropropane 63-134 2.8 20
21.4 10710821.620.0µg/L1,2-Dibromoethane 77-135 0.9 20
21.2 10610621.120.0µg/LDibromomethane 76-138 0.4 20
21.4 10710721.320.0µg/L1,2-Dichlorobenzene 78-128 0.4 20
20.2 10110320.520.0µg/L1,3-Dichlorobenzene 77-125 1.4 20
Page 13 of 27Date:04/20/2022 04:28 PM
Page 39 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17188QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17186
LCS-V17186 LCSD-V17186Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.4 10210320.520.0µg/L1,4-Dichlorobenzene 75-126 0.4 20
18.5 92.598.019.620.0µg/LDichlorodifluoromethane 28-163 5.7 20
20.0 10010320.520.0µg/L1,1-Dichloroethane 70-130 2.4 20
21.1 10610220.320.0µg/L1,2-Dichloroethane 68-131 3.8 20
19.5 97.510120.120.0µg/L1,1-Dichloroethene 70-154 3.0 20
19.1 95.510020.020.0µg/Lcis-1,2-Dichloroethene 76-141 4.6 20
20.0 10010320.620.0µg/Ltrans-1,2-Dichloroethene 76-135 2.9 20
19.5 97.599.519.920.0µg/L1,2-Dichloropropane 77-130 2.0 20
21.2 10610420.720.0µg/L1,3-Dichloropropane 76-132 2.3 20
19.0 95.094.518.920.0µg/L2,2-Dichloropropane 29-149 0.5 20
19.2 96.099.019.820.0µg/L1,1-Dichloropropene 71-136 3.0 20
20.3 10210320.520.0µg/Lcis-1,3-Dichloropropene 65-140 0.9 20
20.7 10410621.120.0µg/Ltrans-1,3-Dichloropropene 67-140 1.9 20
569 11499.6498500µg/LEthanol 70-130 13.3 20
19.9 99.510520.920.0µg/LEthylbenzene 80-127 4.9 20
42.0 10510742.740.0µg/LEthyl Tertiary Butyl Ether (ETBE)70-130 1.6 20
19.8 99.010120.220.0µg/LHexachlorobutadiene 61-134 2.0 20
20.4 10294.018.820.0µg/Ln-Hexane 70-130 8.1 20
20.7 10410721.320.0µg/L2-Hexanone 64-137 2.8 20
20.4 10210520.920.0µg/LIsopropylbenzene 70-130 2.4 20
20.3 10210621.120.0µg/L4-Isopropyl toluene 69-132 3.8 20
19.2 96.096.019.220.0µg/LMethyl Ethyl Ketone (MEK)71-134 0.0 20
20.6 10310220.420.0µg/LMethyl tert-butyl ether (MTBE)68-135 0.9 20
21.8 10910821.620.0µg/L4-Methyl-2-Pentanone 69-134 0.9 20
19.1 95.598.019.620.0µg/LMethylene Chloride 73-131 2.5 20
21.2 10610520.920.0µg/LNaphthalene 64-136 1.4 20
Page 14 of 27Date:04/20/2022 04:28 PM
Page 40 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
8260D
V17188QC Analytical Batch(es):
Analysis Method:
Analysis Description:
5030B
QC Prep:V17186
LCS-V17186 LCSD-V17186Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
20.4 10210520.920.0µg/Ln-Propylbenzene 72-132 2.4 20
20.7 10410520.920.0µg/LStyrene 78-129 0.9 20
20.7 10410520.920.0µg/L1,1,1,2-Tetrachloroethane 79-134 0.9 20
20.5 10310420.820.0µg/L1,1,2,2-Tetrachloroethane 62-127 1.4 20
19.8 99.010120.120.0µg/LTetrachloroethene 80-129 1.5 20
19.7 98.510220.320.0µg/LToluene 76-131 3.0 20
20.8 10410721.320.0µg/L1,2,3-Trichlorobenzene 58-144 2.3 20
21.7 10910921.820.0µg/L1,2,4-Trichlorobenzene 66-139 0.4 20
19.9 99.510320.620.0µg/L1,1,1-Trichloroethane 75-135 3.4 20
20.6 10310320.620.0µg/L1,1,2-Trichloroethane 70-140 0.0 20
20.0 10010520.920.0µg/LTrichloroethene 77-133 4.4 20
19.7 98.510420.820.0µg/LTrichlorofluoromethane 62-148 5.4 20
21.6 10810521.020.0µg/L1,2,3-Trichloropropane 71-127 2.8 20
20.0 10010420.820.0µg/L1,3,5-Trimethylbenzene 75-131 3.9 20
20.0 10099.019.820.0µg/LVinyl Acetate 34-167 1.0 20
19.1 95.597.519.520.0µg/LVinyl Chloride 57-141 2.0 20
20.3 10210420.820.0µg/Lo-Xylene 78-128 2.4 20
41.8 10510642.240.0µg/Lm,p-Xylene 77-133 0.9 20
99.698.04-Bromofluorobenzene (S)80-124
97.499.4Dibromofluoromethane (S)75-129
1011021,2-Dichloroethane - d4 (S)63-136
10199.8Toluene-d8 (S)77-123
Page 15 of 27Date:04/20/2022 04:28 PM
Page 41 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17076QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V16999
Associated Lab Samples: 97515
LRB-V16999 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/22 14:0020.07.12<7.12µg/LAcenaphthene
04/06/22 14:0020.06.94<6.94µg/LAcenaphthylene
04/06/22 14:0050.07.13<7.13µg/LAniline
04/06/22 14:0010.06.57<6.57µg/LAnthracene
04/06/22 14:0010.05.65<5.65µg/LBenzo(a)anthracene
04/06/22 14:0010.04.67<4.67µg/LBenzo(a)pyrene
04/06/22 14:0010.04.52<4.52µg/LBenzo(b)fluoranthene
04/06/22 14:0010.04.24<4.24µg/LBenzo(g,h,i)perylene
04/06/22 14:0010.04.68<4.68µg/LBenzo(k)fluoranthene
04/06/22 14:0010011.5<11.5µg/LBenzoic Acid
04/06/22 14:0010.08.60<8.60µg/LBenzyl alcohol
04/06/22 14:0010.05.67<5.67µg/LBis(2-Chloroethoxy)methane
04/06/22 14:0010.07.30<7.30µg/LBis(2-Chloroethyl)ether
04/06/22 14:0010.06.59<6.59µg/LBis(2-Chloroisopropyl)ether
04/06/22 14:0010.08.80<8.80µg/LBis(2-ethylhexyl)phthalate
04/06/22 14:0020.06.26<6.26µg/L4-Bromophenyl phenyl ether
04/06/22 14:0010.02.94<2.94µg/LButyl benzyl phthalate
04/06/22 14:0010.05.23<5.23µg/L4-Chloro-3-methylphenol
04/06/22 14:0010.05.42<5.42µg/L4-Chloroaniline
04/06/22 14:0020.07.38<7.38µg/L2-Chloronaphthalene
04/06/22 14:0010.06.58<6.58µg/L2-Chlorophenol
04/06/22 14:0020.06.99<6.99µg/L4-Chlorophenyl phenyl ether
04/06/22 14:0010.05.38<5.38µg/LChrysene
04/06/22 14:0020.06.01<6.01µg/LDibenz(a,h)anthracene
04/06/22 14:0020.05.08<5.08µg/LDibenzofuran
04/06/22 14:0010.05.91<5.91µg/L1,2-Dichlorobenzene
04/06/22 14:0010.05.83<5.83µg/L1,3-Dichlorobenzene
Page 16 of 27Date:04/20/2022 04:28 PM
Page 42 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17076QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V16999
Associated Lab Samples: 97515
LRB-V16999 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/22 14:0010.05.91<5.91µg/L1,4-Dichlorobenzene
04/06/22 14:0010.06.60<6.60µg/L3,3'-Dichlorobenzidine
04/06/22 14:0010.05.54<5.54µg/L2,4-Dichlorophenol
04/06/22 14:0020.09.35<9.35µg/LDiethyl phthalate
04/06/22 14:0010.07.82<7.82µg/LDimethyl phthalate
04/06/22 14:0020.010.9<10.9µg/L2,4-Dimethylphenol
04/06/22 14:0010.07.35<7.35µg/LDi-n-butyl phthalate
04/06/22 14:0030.09.92<9.92µg/L4,6-Dinitro-2-methylphenol
04/06/22 14:0030.010.6<10.6µg/L2,4-Dinitrophenol
04/06/22 14:0010.05.20<5.20µg/L2,4-Dinitrotoluene
04/06/22 14:0020.05.90<5.90µg/L2,6-Dinitrotoluene
04/06/22 14:0010.05.01<5.01µg/LDi-n-Octyl Phthalate
04/06/22 14:0010.06.03<6.03µg/LFluoranthene
04/06/22 14:0010.07.27<7.27µg/LFluorene
04/06/22 14:0020.05.75<5.75µg/LHexachlorobenzene
04/06/22 14:0020.05.88<5.88µg/LHexachlorobutadiene
04/06/22 14:0020.05.90<5.90µg/LHexachlorocyclopentadiene
04/06/22 14:0010.05.22<5.22µg/LHexachloroethane
04/06/22 14:0010.06.20<6.20µg/LIndeno(1,2,3-cd)pyrene
04/06/22 14:0010.06.71<6.71µg/LIsophorone
04/06/22 14:0010.07.33<7.33µg/L1-Methylnaphthalene
04/06/22 14:0010.06.92<6.92µg/L2-Methylnaphthalene
04/06/22 14:0010.05.26<5.26µg/L2-Methylphenol
04/06/22 14:0010.02.47<2.47µg/L3&4 Methylphenol
04/06/22 14:0010.07.88<7.88µg/LNaphthalene
04/06/22 14:0010.04.92<4.92µg/L2-Nitroaniline
04/06/22 14:0010.04.55<4.55µg/L3-Nitroaniline
Page 17 of 27Date:04/20/2022 04:28 PM
Page 43 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17076QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V16999
Associated Lab Samples: 97515
LRB-V16999 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/06/22 14:0010.05.10<5.10µg/L4-Nitroaniline
04/06/22 14:0010.07.88<7.88µg/LNitrobenzene
04/06/22 14:0010.05.49<5.49µg/L2-Nitrophenol
04/06/22 14:0010.02.81<2.81µg/L4-Nitrophenol
04/06/22 14:0010.06.49<6.49µg/LN-Nitrosodimethylamine
04/06/22 14:0020.010.9<10.9µg/LN-Nitrosodiphenylamine
04/06/22 14:0020.08.10<8.10µg/LN-Nitroso-di-n-propylamine
04/06/22 14:0050.09.73<9.73µg/LPentachlorophenol
04/06/22 14:0010.06.34<6.34µg/LPhenanthrene
04/06/22 14:0010.02.86<2.86µg/LPhenol
04/06/22 14:0010.05.42<5.42µg/LPyrene
04/06/22 14:0010.05.32<5.32µg/LPyridine
04/06/22 14:0010.06.25<6.25µg/L1,2,4-Trichlorobenzene
04/06/22 14:0020.05.81<5.81µg/L2,4,5-Trichlorophenol
04/06/22 14:0020.06.29<6.29µg/L2,4,6-Trichlorophenol
04/06/22 14:002-Fluorobiphenyl (S)68.6 44-119
04/06/22 14:002-Fluorophenol (S)47.2 19-119
04/06/22 14:00Nitrobenzene-d5 (S)74.0 44-120
04/06/22 14:004-Terphenyl-d14 (S)88.8 50-134
04/06/22 14:002,4,6-Tribromophenol (S)83.4 43-140
04/06/22 14:00Phenol-d5 (S)31.2 11-100
LCS-V16999 LCSD-V16999Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
37.3 74.675.637.850.0µg/LAcenaphthene 38-117 1.3 20.0
Page 18 of 27Date:04/20/2022 04:28 PM
Page 44 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17076QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V16999
LCS-V16999 LCSD-V16999Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.4 78.881.040.550.0µg/LAcenaphthylene 41-130 2.7 20.0
50.0 10010351.350.0µg/LAniline 12-197 2.5 20.0
42.9 85.885.642.850.0µg/LAnthracene 57-123 0.2 20.0
41.5 83.083.041.550.0µg/LBenzo(a)anthracene 58-125 0.0 20.0
57.3 11511858.850.0µg/LBenzo(a)pyrene 54-128 2.5 20.0
50.2 10010753.750.0µg/LBenzo(b)fluoranthene 53-131 6.7 20.0
49.2 98.499.649.850.0µg/LBenzo(g,h,i)perylene 50-134 1.2 20.0
49.5 99.098.249.150.0µg/LBenzo(k)fluoranthene 53-131 0.8 20.0
<11.5 0.0*0.0*<11.550.0µg/LBenzoic Acid 10-125 0.0 20.0
38.4 76.878.839.450.0µg/LBenzyl alcohol 31-112 2.5 20.0
41.6 83.281.840.950.0µg/LBis(2-Chloroethoxy)methane 48-120 1.6 20.0
35.1 70.269.234.650.0µg/LBis(2-Chloroethyl)ether 43-118 1.4 20.0
38.8 77.677.238.650.0µg/LBis(2-Chloroisopropyl)ether 37-130 0.5 20.0
51.0 10210351.550.0µg/LBis(2-ethylhexyl)phthalate 55-135 0.9 20.0
41.3 82.682.841.450.0µg/L4-Bromophenyl phenyl ether 55-124 0.2 20.0
49.4 98.810050.050.0µg/LButyl benzyl phthalate 53-134 1.2 20.0
37.4 74.877.838.950.0µg/L4-Chloro-3-methylphenol 52-119 3.9 20.0
38.0 76.078.239.150.0µg/L4-Chloroaniline 33-117 2.8 20.0
34.4 68.870.835.450.0µg/L2-Chloronaphthalene 40-116 2.8 20.0
36.6 73.273.836.950.0µg/L2-Chlorophenol 38-117 0.8 20.0
39.1 78.280.040.050.0µg/L4-Chlorophenyl phenyl ether 53-121 2.2 20.0
40.8 81.683.041.550.0µg/LChrysene 59-123 1.7 20.0
43.4 86.887.443.750.0µg/LDibenz(a,h)anthracene 51-134 0.6 20.0
38.5 77.078.239.150.0µg/LDibenzofuran 53-118 1.5 20.0
20.3 40.646.023.050.0µg/L1,2-Dichlorobenzene 32-111 12.4 20.0
18.5 37.042.021.050.0µg/L1,3-Dichlorobenzene 28-110 12.6 20.0
Page 19 of 27* QC Fail Date:04/20/2022 04:28 PM
Page 45 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17076QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V16999
LCS-V16999 LCSD-V16999Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
19.0 38.041.820.950.0µg/L1,4-Dichlorobenzene 29-112 9.5 20.0
36.2 72.474.637.350.0µg/L3,3'-Dichlorobenzidine 27-129 2.9 20.0
37.4 74.874.637.350.0µg/L2,4-Dichlorophenol 47-121 0.2 20.0
41.9 83.885.242.650.0µg/LDiethyl phthalate 56-125 1.6 20.0
40.5 81.081.040.550.0µg/LDimethyl phthalate 45-127 0.0 20.0
39.7 79.479.439.750.0µg/L2,4-Dimethylphenol 31-124 0.0 20.0
49.8 99.699.649.850.0µg/LDi-n-butyl phthalate 59-127 0.0 20.0
37.4 74.876.038.050.0µg/L4,6-Dinitro-2-methylphenol 44-137 1.5 20.0
20.8 0.0*0.0*21.050.0µg/L2,4-Dinitrophenol 23-143 0.0 20.0
42.0 84.084.642.350.0µg/L2,4-Dinitrotoluene 57-128 0.7 20.0
43.1 86.287.643.850.0µg/L2,6-Dinitrotoluene 57-124 1.6 20.0
58.8 11812261.250.0µg/LDi-n-Octyl Phthalate 51-140 4.0 20.0
43.1 86.286.043.050.0µg/LFluoranthene 57-128 0.2 20.0
40.0 80.082.041.050.0µg/LFluorene 52-124 2.4 20.0
42.5 85.085.242.650.0µg/LHexachlorobenzene 53-125 0.2 20.0
17.1 0.0*0.0*19.450.0µg/LHexachlorobutadiene 22-124 0.0 20.0
19.2 0.0*43.021.550.0µg/LHexachlorocyclopentadiene 32-117 7.2 20.0
16.5 33.038.019.050.0µg/LHexachloroethane 21-115 14.0 20.0
49.3 98.610150.350.0µg/LIndeno(1,2,3-cd)pyrene 52-134 2.0 20.0
35.9 71.871.235.650.0µg/LIsophorone 42-124 0.8 20.0
29.9 59.861.430.750.0µg/L1-Methylnaphthalene 41-119 2.6 20.0
29.2 58.460.630.350.0µg/L2-Methylnaphthalene 40-121 3.6 20.0
36.0 72.071.435.750.0µg/L2-Methylphenol 30-117 0.8 20.0
28.8 57.658.029.050.0µg/L3&4 Methylphenol 29-110 0.6 20.0
27.6 55.255.427.750.0µg/LNaphthalene 40-121 0.3 20.0
42.5 85.086.843.450.0µg/L2-Nitroaniline 55-127 2.0 20.0
Page 20 of 27* QC Fail Date:04/20/2022 04:28 PM
Page 46 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17076QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V16999
LCS-V16999 LCSD-V16999Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
43.9 87.888.444.250.0µg/L3-Nitroaniline 41-128 0.6 20.0
45.4 90.888.844.450.0µg/L4-Nitroaniline 45-135 2.2 20.0
34.9 69.867.433.750.0µg/LNitrobenzene 45-121 3.4 20.0
34.9 69.868.634.350.0µg/L2-Nitrophenol 47-123 1.7 20.0
19.3 38.639.019.550.0µg/L4-Nitrophenol 10-105 1.0 20.0
16.4 32.848.824.450.0µg/LN-Nitrosodimethylamine 10-119 39.2*20.0
47.8 95.698.449.250.0µg/LN-Nitrosodiphenylamine 51-123 2.8 20.0
41.9 83.885.842.950.0µg/LN-Nitroso-di-n-propylamine 49-119 2.3 20.0
39.3 0.0*0.0*42.150.0µg/LPentachlorophenol 35-138 0.0 20.0
42.1 84.285.242.650.0µg/LPhenanthrene 59-120 1.1 20.0
17.2 34.434.217.150.0µg/LPhenol 12-58 0.5 20.0
43.9 87.886.443.250.0µg/LPyrene 57-126 1.6 20.0
18.3 36.641.620.850.0µg/LPyridine 10-80 12.7 20.0
21.4 42.845.822.950.0µg/L1,2,4-Trichlorobenzene 29-126 6.7 20.0
39.6 79.279.239.650.0µg/L2,4,5-Trichlorophenol 53-123 0.0 20.0
41.1 82.283.641.850.0µg/L2,4,6-Trichlorophenol 50-125 1.6 20.0
69.669.02-Fluorobiphenyl (S)44-119
47.647.52-Fluorophenol (S)19-119
67.265.2Nitrobenzene-d5 (S)44-120
86.285.64-Terphenyl-d14 (S)50-134
86.587.62,4,6-Tribromophenol (S)43-140
31.531.6Phenol-d5 (S)11-100
Page 21 of 27* QC Fail Date:04/20/2022 04:28 PM
Page 47 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
Associated Lab Samples: 97514
LRB-V17141 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/11/22 15:4720.07.12<7.12µg/LAcenaphthene
04/11/22 15:4720.06.94<6.94µg/LAcenaphthylene
04/11/22 15:4750.07.13<7.13µg/LAniline
04/11/22 15:4710.06.57<6.57µg/LAnthracene
04/11/22 15:4710.05.65<5.65µg/LBenzo(a)anthracene
04/11/22 15:4710.04.67<4.67µg/LBenzo(a)pyrene
04/11/22 15:4710.04.52<4.52µg/LBenzo(b)fluoranthene
04/11/22 15:4710.04.24<4.24µg/LBenzo(g,h,i)perylene
04/11/22 15:4710.04.68<4.68µg/LBenzo(k)fluoranthene
04/11/22 15:4710011.5<11.5µg/LBenzoic Acid
04/11/22 15:4710.08.60<8.60µg/LBenzyl alcohol
04/11/22 15:4710.05.67<5.67µg/LBis(2-Chloroethoxy)methane
04/11/22 15:4710.07.30<7.30µg/LBis(2-Chloroethyl)ether
04/11/22 15:4710.06.59<6.59µg/LBis(2-Chloroisopropyl)ether
04/11/22 15:4710.08.80<8.80µg/LBis(2-ethylhexyl)phthalate
04/11/22 15:4720.06.26<6.26µg/L4-Bromophenyl phenyl ether
04/11/22 15:4710.02.94<2.94µg/LButyl benzyl phthalate
04/11/22 15:4710.05.23<5.23µg/L4-Chloro-3-methylphenol
04/11/22 15:4710.05.42<5.42µg/L4-Chloroaniline
04/11/22 15:4720.07.38<7.38µg/L2-Chloronaphthalene
04/11/22 15:4710.06.58<6.58µg/L2-Chlorophenol
04/11/22 15:4720.06.99<6.99µg/L4-Chlorophenyl phenyl ether
04/11/22 15:4710.05.38<5.38µg/LChrysene
04/11/22 15:4720.06.01<6.01µg/LDibenz(a,h)anthracene
04/11/22 15:4720.05.08<5.08µg/LDibenzofuran
04/11/22 15:4710.05.91<5.91µg/L1,2-Dichlorobenzene
04/11/22 15:4710.05.83<5.83µg/L1,3-Dichlorobenzene
Page 22 of 27Date:04/20/2022 04:28 PM
Page 48 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
Associated Lab Samples: 97514
LRB-V17141 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/11/22 15:4710.05.91<5.91µg/L1,4-Dichlorobenzene
04/11/22 15:4710.06.60<6.60µg/L3,3'-Dichlorobenzidine
04/11/22 15:4710.05.54<5.54µg/L2,4-Dichlorophenol
04/11/22 15:4720.09.35<9.35µg/LDiethyl phthalate
04/11/22 15:4710.07.82<7.82µg/LDimethyl phthalate
04/11/22 15:4720.010.9<10.9µg/L2,4-Dimethylphenol
04/11/22 15:4710.07.35<7.35µg/LDi-n-butyl phthalate
04/11/22 15:4730.09.92<9.92µg/L4,6-Dinitro-2-methylphenol
04/11/22 15:4730.010.6<10.6µg/L2,4-Dinitrophenol
04/11/22 15:4710.05.20<5.20µg/L2,4-Dinitrotoluene
04/11/22 15:4720.05.90<5.90µg/L2,6-Dinitrotoluene
04/11/22 15:4710.05.01<5.01µg/LDi-n-Octyl Phthalate
04/11/22 15:4710.06.03<6.03µg/LFluoranthene
04/11/22 15:4710.07.27<7.27µg/LFluorene
04/11/22 15:4720.05.75<5.75µg/LHexachlorobenzene
04/11/22 15:4720.05.88<5.88µg/LHexachlorobutadiene
04/11/22 15:4720.05.90<5.90µg/LHexachlorocyclopentadiene
04/11/22 15:4710.05.22<5.22µg/LHexachloroethane
04/11/22 15:4710.06.20<6.20µg/LIndeno(1,2,3-cd)pyrene
04/11/22 15:4710.06.71<6.71µg/LIsophorone
04/11/22 15:4710.07.33<7.33µg/L1-Methylnaphthalene
04/11/22 15:4710.06.92<6.92µg/L2-Methylnaphthalene
04/11/22 15:4710.05.26<5.26µg/L2-Methylphenol
04/11/22 15:4710.02.47<2.47µg/L3&4 Methylphenol
04/11/22 15:4710.07.88<7.88µg/LNaphthalene
04/11/22 15:4710.04.92<4.92µg/L2-Nitroaniline
04/11/22 15:4710.04.55<4.55µg/L3-Nitroaniline
Page 23 of 27Date:04/20/2022 04:28 PM
Page 49 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
Associated Lab Samples: 97514
LRB-V17141 Matrix: AQULab Reagent Blank
Parameter
AnalyzedMQLMDLBlank
ResultUnits
%
Recovery
% Rec
Limits
04/11/22 15:4710.05.10<5.10µg/L4-Nitroaniline
04/11/22 15:4710.07.88<7.88µg/LNitrobenzene
04/11/22 15:4710.05.49<5.49µg/L2-Nitrophenol
04/11/22 15:4710.02.81<2.81µg/L4-Nitrophenol
04/11/22 15:4710.06.49<6.49µg/LN-Nitrosodimethylamine
04/11/22 15:4720.010.9<10.9µg/LN-Nitrosodiphenylamine
04/11/22 15:4720.08.10<8.10µg/LN-Nitroso-di-n-propylamine
04/11/22 15:4750.09.73<9.73µg/LPentachlorophenol
04/11/22 15:4710.06.34<6.34µg/LPhenanthrene
04/11/22 15:4710.02.86<2.86µg/LPhenol
04/11/22 15:4710.05.42<5.42µg/LPyrene
04/11/22 15:4710.05.32<5.32µg/LPyridine
04/11/22 15:4710.06.25<6.25µg/L1,2,4-Trichlorobenzene
04/11/22 15:4720.05.81<5.81µg/L2,4,5-Trichlorophenol
04/11/22 15:4720.06.29<6.29µg/L2,4,6-Trichlorophenol
04/11/22 15:472-Fluorobiphenyl (S)52.6 44-119
04/11/22 15:472-Fluorophenol (S)37.8 19-119
04/11/22 15:47Nitrobenzene-d5 (S)54.0 44-120
04/11/22 15:474-Terphenyl-d14 (S)70.4 50-134
04/11/22 15:472,4,6-Tribromophenol (S)65.2 43-140
04/11/22 15:47Phenol-d5 (S)22.9 11-100
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
36.3 72.670.635.350.0µg/LAcenaphthene 38-117 2.7 20.0
Page 24 of 27Date:04/20/2022 04:28 PM
Page 50 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
39.1 78.277.238.650.0µg/LAcenaphthylene 41-130 1.2 20.0
26.6 53.264.432.250.0µg/LAniline 12-197 19.0 20.0
45.1 90.285.042.550.0µg/LAnthracene 57-123 5.9 20.0
44.6 89.280.640.350.0µg/LBenzo(a)anthracene 58-125 10.1 20.0
49.5 99.088.644.350.0µg/LBenzo(a)pyrene 54-128 11.0 20.0
42.1 84.275.637.850.0µg/LBenzo(b)fluoranthene 53-131 10.7 20.0
43.8 87.677.838.950.0µg/LBenzo(g,h,i)perylene 50-134 11.8 20.0
43.4 86.878.439.250.0µg/LBenzo(k)fluoranthene 53-131 10.1 20.0
<11.5 0.0*0.0*<11.550.0µg/LBenzoic Acid 10-125 0.0 20.0
30.8 61.664.832.450.0µg/LBenzyl alcohol 31-112 5.0 20.0
33.2 66.469.434.750.0µg/LBis(2-Chloroethoxy)methane 48-120 4.4 20.0
33.8 67.664.032.050.0µg/LBis(2-Chloroethyl)ether 43-118 5.4 20.0
31.7 63.463.631.850.0µg/LBis(2-Chloroisopropyl)ether 37-130 0.3 20.0
47.9 95.886.843.450.0µg/LBis(2-ethylhexyl)phthalate 55-135 9.8 20.0
40.2 80.476.238.150.0µg/L4-Bromophenyl phenyl ether 55-124 5.3 20.0
44.8 89.681.440.750.0µg/LButyl benzyl phthalate 53-134 9.5 20.0
35.0 70.068.434.250.0µg/L4-Chloro-3-methylphenol 52-119 2.3 20.0
33.6 67.263.831.950.0µg/L4-Chloroaniline 33-117 5.1 20.0
32.3 64.663.031.550.0µg/L2-Chloronaphthalene 40-116 2.5 20.0
30.0 60.061.230.650.0µg/L2-Chlorophenol 38-117 1.9 20.0
40.7 81.478.439.250.0µg/L4-Chlorophenyl phenyl ether 53-121 3.7 20.0
43.8 87.679.239.650.0µg/LChrysene 59-123 10.0 20.0
38.0 76.067.033.550.0µg/LDibenz(a,h)anthracene 51-134 12.5 20.0
38.7 77.475.637.850.0µg/LDibenzofuran 53-118 2.3 20.0
18.5 37.034.617.350.0µg/L1,2-Dichlorobenzene 32-111 6.7 20.0
16.8 33.630.815.450.0µg/L1,3-Dichlorobenzene 28-110 8.6 20.0
Page 25 of 27* QC Fail Date:04/20/2022 04:28 PM
Page 51 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
17.1 34.231.815.950.0µg/L1,4-Dichlorobenzene 29-112 7.2 20.0
35.2 70.465.832.950.0µg/L3,3'-Dichlorobenzidine 27-129 6.7 20.0
32.1 64.263.231.650.0µg/L2,4-Dichlorophenol 47-121 1.5 20.0
43.4 86.881.440.750.0µg/LDiethyl phthalate 56-125 6.4 20.0
41.8 83.679.039.550.0µg/LDimethyl phthalate 45-127 5.6 20.0
34.8 69.668.434.250.0µg/L2,4-Dimethylphenol 31-124 1.7 20.0
48.8 97.689.844.950.0µg/LDi-n-butyl phthalate 59-127 8.3 20.0
39.1 78.276.038.050.0µg/L4,6-Dinitro-2-methylphenol 44-137 2.8 20.0
30.7 61.455.627.850.0µg/L2,4-Dinitrophenol 23-143 9.9 20.0
45.6 91.285.242.650.0µg/L2,4-Dinitrotoluene 57-128 6.8 20.0
44.8 89.685.642.850.0µg/L2,6-Dinitrotoluene 57-124 4.5 20.0
43.6 87.278.639.350.0µg/LDi-n-Octyl Phthalate 51-140 10.3 20.0
45.2 90.484.242.150.0µg/LFluoranthene 57-128 7.1 20.0
42.4 84.881.040.550.0µg/LFluorene 52-124 4.5 20.0
42.5 85.078.439.250.0µg/LHexachlorobenzene 53-125 8.0 20.0
15.1 30.226.813.450.0µg/LHexachlorobutadiene 22-124 11.9 20.0
18.2 36.436.218.150.0µg/LHexachlorocyclopentadiene 32-117 0.5 20.0
14.3 28.626.213.150.0µg/LHexachloroethane 21-115 8.7 20.0
41.8 83.674.637.350.0µg/LIndeno(1,2,3-cd)pyrene 52-134 11.3 20.0
30.4 60.860.630.350.0µg/LIsophorone 42-124 0.3 20.0
25.7 51.451.625.850.0µg/L1-Methylnaphthalene 41-119 0.3 20.0
23.9 47.847.823.950.0µg/L2-Methylnaphthalene 40-121 0.0 20.0
30.5 61.063.031.550.0µg/L2-Methylphenol 30-117 3.2 20.0
25.3 50.652.626.350.0µg/L3&4 Methylphenol 29-110 3.8 20.0
24.1 48.247.023.550.0µg/LNaphthalene 40-121 2.5 20.0
41.0 82.078.439.250.0µg/L2-Nitroaniline 55-127 4.4 20.0
Page 26 of 27Date:04/20/2022 04:28 PM
Page 52 of 55
Quality Control Data
22-091-0033Report No:
Project Description:
Client ID:Hart & Hickman (Charlotte)
SLC.001
QC Prep Batch Method:
Semivolatile Organic Compounds - GC/MS
8270E
V17342QC Analytical Batch(es):
Analysis Method:
Analysis Description:
3510C
QC Prep:V17141
LCS-V17141 LCSD-V17141Laboratory Control Sample & LCSD
LCSD
ResultParameter Max
RPD
LCSD
% Rec
LCS
%Rec
LCS
Result
Spike
Conc.Units
% Rec
Limits RPD
46.3 92.683.441.750.0µg/L3-Nitroaniline 41-128 10.4 20.0
44.4 88.883.041.550.0µg/L4-Nitroaniline 45-135 6.7 20.0
30.1 60.259.229.650.0µg/LNitrobenzene 45-121 1.6 20.0
30.5 61.060.030.050.0µg/L2-Nitrophenol 47-123 1.6 20.0
18.4 36.834.017.050.0µg/L4-Nitrophenol 10-105 7.9 20.0
20.0 40.039.819.950.0µg/LN-Nitrosodimethylamine 10-119 0.5 20.0
50.1 10096.048.050.0µg/LN-Nitrosodiphenylamine 51-123 4.2 20.0
34.9 69.872.636.350.0µg/LN-Nitroso-di-n-propylamine 49-119 3.9 20.0
48.6 97.290.645.350.0µg/LPentachlorophenol 35-138 7.0 20.0
43.7 87.482.841.450.0µg/LPhenanthrene 59-120 5.4 20.0
13.8 27.628.414.250.0µg/LPhenol 12-58 2.8 20.0
43.6 87.280.440.250.0µg/LPyrene 57-126 8.1 20.0
5.91 11.825.412.750.0µg/LPyridine 10-80 72.9*20.0
18.1 36.235.017.550.0µg/L1,2,4-Trichlorobenzene 29-126 3.3 20.0
39.8 79.675.437.750.0µg/L2,4,5-Trichlorophenol 53-123 5.4 20.0
39.6 79.275.637.850.0µg/L2,4,6-Trichlorophenol 50-125 4.6 20.0
64.065.22-Fluorobiphenyl (S)44-119
41.641.62-Fluorophenol (S)19-119
57.456.6Nitrobenzene-d5 (S)44-120
88.679.44-Terphenyl-d14 (S)50-134
93.086.32,4,6-Tribromophenol (S)43-140
26.526.7Phenol-d5 (S)11-100
Page 27 of 27* QC Fail Date:04/20/2022 04:28 PM
Page 53 of 55
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-091-0033
Hart & Hickman (Charlotte)
01102
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 2.7C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Signature:Sarah J. Locklear Date & Time:04/01/2022 17:40:07
Special precautions or instructions included?
Comments:
Page 54 of 55
Page 55 of 55