WS-96113_96490_CA_IAR_20210809

May 7, 2021
Mr. Scott Wellborn SEGRA
One Lumos Plaza Waynesboro, Virginia 22980 Reference: Initial Abatement Report Pole Storage Area Northstate Telephone Service Garage 1201 West Fairfield Road High Point, Guilford County, North Carolina ECS Project No. 49-12119A Dear Mr. Wellborn:
As authorized by your acceptance of ECS Proposal 49:21442-P dated November 18, 2020 and authorized on January 27, 2021, ECS Southeast, LLP (ECS) has completed the Initial Abatement
Report for the utility pole storage area at the above referenced site. Included in this report is a description of the field activities, the results obtained, and our conclusions and recommendations. ECS appreciates the opportunity to provide our services to you. If there are questions regarding
this report, or a need for further information, please contact us.
Respectfully submitted, ECS SOUTHEAST, LLP
Randy H. Cavallier Assistant Staff Project Manager [e-mail]
Roger A. Smith, P.G. Principal Geologist [e-mail] cc: Ashley Dinkins – Guilford County Department of Environmental Health

SOIL EXCAVATION REPORT
POLE STORAGE AREA NORTHSTATE TELEPHONE 1201 WEST FAIRFIELD ROAD HIGH POINT, GUILFORD COUNTY, NORTH CAROLINA ECS PROJECT NO. 49-12119a
PREPARED FOR
SEGRA WAYNESBORO, VIRGINIA
MAY 7, 2021
Soil Excavation Report Pole Storage Area
Northstate Telephone Service Garage 1201 West Fairfield Road High Point, Guilford County, North Carolina
ECS Project No. 49-12119A May 7, 2021
1
TABLE OF CONTENTS 1.0 PROJECT INFORMATION ............................................................................................... 1
2.0 SCOPE OF SERVICES .................................................................................................... 1
3.0 RESULTS ......................................................................................................................... 2
4.0 CONCLUSIONS ............................................................................................................... 2
5.0 RECOMMENDATIONS .................................................................................................... 3
6.0 QUALIFICATIONS OF REPORT ...................................................................................... 3
FIGURES Figure 1 Site Topographic Map Figure 2 Aerial Site Map Figure 3 Sample Location Map Figure 4 Sample Location Map TABLES Table 1 Summary of Soil Analytical Results Table 2 Summary of Confirmation Soil Analytical Results APPENDICES Appendix A Site Photograph Log Appendix B Non-Hazardous Manifest and Transportation Weight Tickets Appendix C Laboratory Data Sheets and Chain-of-Custody Records

Soil Excavation Report Pole Storage Area
Northstate Telephone Service Garage 1201 West Fairfield Road High Point, Guilford County, North Carolina
ECS Project No. 49-12119A May 7, 2021
1
1.0 PROJECT INFORMATION The site is the Northstate Telephone utility pole storage area located at 1201 West Fairfield Road in High Point, Guilford County, North Carolina (Figure 1 and Figure 2). In August 2020, ECS completed a soil and groundwater assessment at the site (ECS Project 49-12119) in order to assess the site for potential impacts related to the vehicle service and maintenance operations, as well as site operations. Laboratory analysis of soil sample HA-1 (Figure 3) collected in the vicinity of the utility pole storage area detected pentachlorophenol at a concentration (72.4 mg/kg) above its respective Soil-to-Groundwater, Residential and
Industrial/Commercial Maximum Soil Contaminant Concentrations (MSCCs) of5 milligrams per kilogram (mg/kg) and 48 mg/kg, respectively. Laboratory analysis of soil sample HA-2 collected in the vicinity of the utility pole storage area detected pentachlorophenol at a concentration (8.7
mg/kg) above its Residential MSCC (5 mg/kg). A groundwater sample collected in the vicinity of soil sample HA-1 did not detect pentachlorophenol above the laboratory reporting limit or its North Carolina 2L Groundwater Quality Standard (NC2LGWQS).
On December 15, 2020, based on the laboratory analytical results of soil samples HA-1 and HA-2, soil borings HA-3 through HA-10 (Figure 3) were drilled using a decontaminated hand auger in the utility pole storage area. Laboratory analysis of soil sample HA-3 detected benzo(a)pyrene at the concentration of 3.2 mg/kg which is above its Soil-to-Groundwater, Residential and Industrial/Commercial MSCC of 0.78 mg/kg (Table 1).
Mr. Scott Wellborn with SEGRA contracted ECS to perform soil removal/disposal in the vicinity of soil samples HA-1 and HA-3 in an effort to reduce the contaminant concentrations
below their respective Industrial/Commercial MSCCs.
2.0 SCOPE OF SERVICES The soil removal activities consisted of the excavation and off-disposal of approximately 152 tons of impacted soil and collection of confirmation soil samples from the sidewalls and base of the final excavation. The subcontractor used for this project was Contaminant Control, Inc. (CCI). Excavation and sampling activities were conducted on March 4, 2021 and April 15, 2021. A photographic log documenting the field sampling activities is provided in Appendix A. 2.1 Public Utility Locate
Prior to commencing with field activities, ECS contacted the North Carolina 811 service to locate/mark public utilities at the site. Required separation distances between subsurface activities and marked utilities (typically 30-inches) were maintained during the field activities.

Soil Excavation Report Pole Storage Area
Northstate Telephone Service Garage 1201 West Fairfield Road High Point, Guilford County, North Carolina
ECS Project No. 49-12119A May 7, 2021
2
2.2 Soil Remediation Activities On March 4, 2021, ECS observed and documented the removal of approximately 107 tons of impacted soil in the vicinity of previous hand auger soil samples HA-1 and HA-3. The soil was removed using a mini-excavator and loaded directly into dump trucks. The soil was transported to the Waste Management Great Oaks Landfill facility (Great Oaks) in Randleman, Randolph County, North Carolina for disposal. The Non-Hazardous manifest and transportation weight tickets are included in Appendix B. the final excavation measured 70 feet long, 15 feet wide, and 3 feet deep.
Following the soil excavation ECS collected soil samples SS-1 through SS-6 from the sidewalls and base of the excavation (Figure 4). The soil samples were placed into laboratory provided jars, labeled, and maintained on ice until delivered to Pace Analytical Services, LLC (Pace), a
North Carolina certified laboratory to be analyzed for semi-volatile organic compounds (SVOC) using EPA Method 8270. The samples were maintained under chain-of-custody until delivered to the Pace. Chain-of Custody Records are included in Appendix C.
Based on the laboratory analytical results from the March soil sampling, ECS and CCI returned to the site and removed and additional 45 tons of soil from the southern sidewall and base of the excavation, for disposal at the Great Oaks facility. Following the soil excavation, ECS collected soil samples SS-SW and SS-Base from the sidewalls and base of the excavation (Figure 4). 3.0 RESULTS 3.1 Soil Sample Analytical Results Laboratory analysis of soil samples SS-1 (collected from the southern sidewall of the March excavation) and SS-5 (collected from the base of the March excavation) detected
pentachlorophenol at concentrations of 6.4 mg/kg and 41.5 mg/kg, respectively, which are greater than the Residential MSCC but less than the Commercial/Industrial MSCC.
Laboratory analysis of soil samples SS-SW (collected of the southern sidewall of the April excavation) and SS-Base (collected from the base of the April excavation) did not detect pentachlorophenol above the laboratory reporting limit; however, the reporting limit of 0.38 mg/kg
is above its Soil-to-Groundwater MSCC of 0.0065 mg/kg, but below the Residential and Commercial/Industrial MSCCs. The laboratory results are summarized in Table 2. The laboratory data sheets are included in Appendix C. 4.0 CONCLUSIONS
Based on the laboratory analytical results; ECS concludes the following:
Soil Excavation Report Pole Storage Area
Northstate Telephone Service Garage 1201 West Fairfield Road High Point, Guilford County, North Carolina
ECS Project No. 49-12119A May 7, 2021
3
• Approximately 152 tons of impacted soils were excavated, loaded into trucks and removed
for off-site disposal at a permitted facility.
• Pentachlorophenol and benzo(a)pyrene, the contaminants whose concentrations were
above their Industrial/Commercial MSCCs have been remediated to below their respective Industrial/Commercial and Residential MSCCs.
• A regulatory (NCDEQ) reporting requirement may exist for the site. 5.0 RECOMMENDATIONS Based on the results of the environmental assessment, ECS recommends the following:
• ECS recommends seeking legal counsel concerning possible reporting requirements to the North Carolina Department of Environmental Quality (NCDEQ).
• It’s likely that if the NCDEQ assigns an incident to the site that closure may be obtained by completion of a Notice of Residual Petroleum and attaching to the deed, restricting
the use of the property to commercial use. 6.0 QUALIFICATIONS OF REPORT The activities and evaluative approaches used in this assessment are consistent with those normally employed in environmental assessment projects of this type. Our evaluation of site conditions has been based on our understanding of the site project information and the data obtained during our field activities. This report was prepared for the express use of SEGRA. Use of this report by other individuals or companies implies their acceptance of the General Conditions of Service of the original contract.
FIGURES
SOURCE:
USGS TOPOGRAPHIC MAP
7.5 –MINUTE SERIES
HIGH POINT WEST + HIGH POINT EAST, NC
DATED: 2019
SCALE: 1 : 24,000
CONTOUR INVERVAL = 10’
FIGURE 1
SITE TOPOGRAPHIC MAP
1201 WEST FAIRFIELD ROAD
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-12119A
APPROXIMATE SITE LOCATION
SOURCE:
GUILFORD COUNTY GIS
SCALE:
344 fEET
LEGEND
SAMPLE LOCATION
APPROXIMATE UST LOCATION
APPROXIMATE SITE BOUNDARY
FIGURE 2
AERIALSITE MAP
1201 WEST FAIRFIELD ROAD
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-12119A
P-2
T-1
SOURCE
GUILFORD COUNTY GIS
SCALE: NTS
LEGEND
SAMPLE LOCATION
APPROXIMATE UST LOCATION
APPROXIMATE SITE BOUNDARY
FIGURE 3
SAMPLE LOCATION MAP
1201 WEST FAIRFIELD ROAD
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-12119A
GP-1 GP-2
GP-3/GW-1
GP-4
GP-5/GW-2
GP-6
GP-7GP-8
Soil Sample Location
Area Impacted above Industrial/Commercial MSCCs
HA-2
HA-3 HA-1
HA-4
HA-5
HA-6
HA-7
HA-8
HA-9
HA-10
SOURCE
GUILFORD COUNTY GIS
SCALE: NTS
LEGEND
SAMPLE LOCATION
APPROXIMATE UST LOCATION
APPROXIMATE SITE BOUNDARY
FIGURE 4
SAMPLE LOCATION MAP
1201 WEST FAIRFIELD ROAD
HIGH POINT, GUILFORD COUNTY, NC
ECS PROJECT NO. 49-12119A
GP-1 GP-2
GP-3/GW-1
GP-4
GP-5/GW-2
GP-6
GP-7GP-8
SS-1
SS-2
SS-3
SS-4
SS-5/SS-Base
SS-6
SS-SW
Sidewall Soil Sample Location
Base Soil Sample Location
Extent of March Excavation
Extent of April Excavation

TABLE
Northstate Telephone
Pole Storage Area
1201 West Fairfield Road
High Point, Guilford County, North Carolina
ECS Project No. 49-12119A
Sample Identification HA-1 HA-2 HA-3 HA-4 HA-5 HA-6 HA-7 HA-8 HA-9 HA-10
Soil to
Groundwater
MSCC
(mg/kg)
Residential
MSCC
(mg/kg)
Indusrtial/
Commercial
MSCC
(mg/kg)
Sample Date
FID Readings 6.5 6.4 -- -- -- -- -- -- -- --
AllTarget Compounds ND ND NS NS NS NS NS NS NS NS -- -- --
Anthracene <0.38 <0.38 0.39 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 0.76 940 4,600 122,000
Acenaphthylene <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 0.51 11 469 12,264
Benzo(a)anthracene <0.38 <0.38 0.99 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 2.2 0.35 0.88 8
Benzo(a)pyrene <0.38 <0.38 3.2 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 1.7 0.096 0.088 0.78
Benzo(g,h,i)perylene <0.38 <0.38 0.59 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 1.3 6,400 469 12,264
Benzo(b)fluoranthene <0.38 <0.38 3.2 <0.38 0.80 <0.38 <0.38 <0.38 <0.38 5.6 1.2 0.88 8
Benzo(k)fluoranthene <0.38 <0.38 1.2 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 1.5 12 9 78
Chrysene <0.38 <0.38 2.2 <0.38 0.62 <0.38 <0.38 <0.38 <0.38 3.1 39 88 780
Fluoranthene <3.0 <3.0 3.0 <0.38 0.89 <0.38 <0.38 <0.38 <0.38 3.3 290 620 16,400
Indeno(1,2,3-cd)pyrene <0.38 <0.38 0.60 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 1.2 3.4 0.88 8
Pentachlorophenol 72.4 8.7 3.5 <0.75*1.8 1.5 <0.75*<0.75*<0.75*<0.75*0.0065 5 48
Phenanthrene <0.38 <0.38 0.45 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 <0.38 56 469 12,264
Pyrene <0.38 <0.38 2.6 <0.38 <0.80 <0.38 <0.38 <0.38 <0.38 5.1 270 469 12,264
NOTES:
VOCs = Volatile Organic Compounds mg/kg = milligrams per kilogram = ppm (parts per million)
SVOCs = Semi-volatile Organic Compounds BOLD = Concentration Exceeds Soil-to-Groundwater MSCC
MSCC = Maximum Soil Contaminant Concentration UNDERLINE = Concentration Exceeds Residential MSCC
ND = Not Detected Above Laboratory Reporting Limits
NS = Parameter Not Sampled For
SVOCs by EPA 8270
* = Reporting Limit Above Soil-to-Groundwater MSCC
3/4/2021
TABLE 1: SUMMARY OF SOIL ANALYTICAL RESULTS
ITALICS = Concentration Exceeds Industrial/Commercial MSCC
VOCs by EPA 8260
8/13/2020
Northstate Telephone
Pole Storage Area
1201 West Fairfield Road
High Point, Guilford County, North Carolina
ECS Project No. 49-12119A
Sample Identification SS-1 SS-2 SS-3 SS-4 SS-5 SS-6 SS-Base SS-SW
Soil to
Groundwater
MSCC
(mg/kg)
Residential
MSCC
(mg/kg)
Indusrtial/
Commercial
MSCC
(mg/kg)
Sample Date
Benzo(a)pyrene <0.37 0.41 <0.37 <0.37 <0.39 <0.38 <0.38 <0.36 0.096 0.088 0.78
Benzo(g,h,i)perylene <0.37 0.40 <0.37 <0.37 <0.39 <0.38 <0.38 <0.36 6,400 469 12,264
Benzo(b)fluoranthene <0.37 0.87 <0.37 <0.37 0.55 <0.38 <0.38 <0.36 1.2 0.88 8
Benzo(k)fluoranthene 0.42 <0.37 <0.37 <0.37 <0.39 <0.38 <0.38 <0.36 12 9 78
Chrysene <0.37 0.66 <0.37 <0.37 0.49 <0.38 <0.38 <0.36 39 88 780
Fluoranthene 0.64 1.4 <0.37 <0.37 0.97 <0.38 <0.38 <0.36 290 620 16,400
Pentachlorophenol 6.4 1.1 <0.37*2.0 41.5 <0.38*<0.38*<0.36*0.0065 5 48
Phenanthrene <0.37 0.54 <0.37 <0.37 <0.39 <0.38 <0.38 <0.36 56 469 12,264
Pyrene 0.55 1.1 <0.37 <0.37 0.73 <0.38 <0.38 <0.36 270 469 12,264
NOTES:
VOCs = Volatile Organic Compounds mg/kg = milligrams per kilogram = ppm (parts per million)
SVOCs = Semi-volatile Organic Compounds BOLD = Concentration Exceeds Soil-to-Groundwater MSCC
MSCC = Maximum Soil Contaminant Concentration UNDERLINE = Concentration Exceeds Residential MSCC
ND = Not Detected Above Laboratory Reporting Limits
NS = Parameter Not Sampled For
TABLE 2: SUMMARY OF CONFIRMATION SOIL ANALYTICAL RESULTS
ITALICS = Concentration Exceeds Industrial/Commercial MSCC
3/4/2021 4/15/2021
SVOCs by EPA 8270
* = Reporting Limit Above Soil-to-Groundwater MSCC

APPENDIX A

PHOTOGRAPH LOG
NORTHSTATE TELEPHONE POLE STORAGE AREA
1201 WEST FAIRFIELD ROAD
HIGH POINT, GUILFORD COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-12119A
Photograph 1: Excavation of Impacted Soil Using a Mini-Excavator on March 4, 2021
Photograph 2: Direct Loading of Soil Into Truck
Photograph 3: Approximate Area of Excavation
Photograph 4: Caution Tape Marking Depth of March 4, 2021 Excavation
PHOTOGRAPH LOG
NORTHSTATE TELEPHONE POLE STORAGE AREA
1201 WEST FAIRFIELD ROAD
HIGH POINT, GUILFORD COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-12119A
Photograph 5: Placing/Compacting Backfill with Excavator Bucket
Photograph 6: Excavation of Additional Soil on April 15, 2021
PHOTOGRAPH LOG
NORTHSTATE TELEPHONE POLE STORAGE AREA
1201 WEST FAIRFIELD ROAD
HIGH POINT, GUILFORD COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-12119A

APPENDIX B

APPENDIX C

#=CL#
March 12, 2021
LIMS USE: FR - RANDY CAVALLIER
LIMS OBJECT ID: 92525998
92525998
Project:
Pace Project No.:
RE:
Mr. Randy Cavallier
ECS Southeast, LLP
4811 Koger Blvd.
Greensboro, NC 27407
Northstate 12119-B
Dear Mr. Cavallier:
Enclosed are the analytical results for sample(s) received by the laboratory on March 05, 2021. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 36
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 36
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92525998
Northstate 12119-B
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92525998001 SS-1 EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92525998002 SS-2 EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92525998003 SS-3 EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92525998004 SS-4 EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92525998005 SS-5 EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92525998006 SS-6 EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-1 Lab ID:92525998001 Collected:03/04/21 12:50 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/10/21 16:32 83-32-903/10/21 10:020.37 1
Acenaphthylene ND mg/kg 03/10/21 16:32 208-96-803/10/21 10:020.37 1
Aniline ND mg/kg 03/10/21 16:32 62-53-303/10/21 10:020.37 1
Anthracene ND mg/kg 03/10/21 16:32 120-12-703/10/21 10:020.37 1
Benzo(a)anthracene ND mg/kg 03/10/21 16:32 56-55-303/10/21 10:020.37 1
Benzo(a)pyrene ND mg/kg 03/10/21 16:32 50-32-803/10/21 10:020.37 1
Benzo(b)fluoranthene 0.42 mg/kg 03/10/21 16:32 205-99-203/10/21 10:020.37 1
Benzo(g,h,i)perylene ND mg/kg 03/10/21 16:32 191-24-203/10/21 10:020.37 1
Benzo(k)fluoranthene ND mg/kg 03/10/21 16:32 207-08-903/10/21 10:020.37 1
Benzoic Acid ND mg/kg 03/10/21 16:32 65-85-003/10/21 10:021.9 1
Benzyl alcohol ND mg/kg 03/10/21 16:32 100-51-603/10/21 10:020.75 1
4-Bromophenylphenyl ether ND mg/kg 03/10/21 16:32 101-55-303/10/21 10:020.37 1
Butylbenzylphthalate ND mg/kg 03/10/21 16:32 85-68-7 v103/10/21 10:020.37 1
4-Chloro-3-methylphenol ND mg/kg 03/10/21 16:32 59-50-703/10/21 10:020.75 1
4-Chloroaniline ND mg/kg 03/10/21 16:32 106-47-803/10/21 10:020.75 1
bis(2-Chloroethoxy)methane ND mg/kg 03/10/21 16:32 111-91-103/10/21 10:020.37 1
bis(2-Chloroethyl) ether ND mg/kg 03/10/21 16:32 111-44-403/10/21 10:020.37 1
2-Chloronaphthalene ND mg/kg 03/10/21 16:32 91-58-703/10/21 10:020.37 1
2-Chlorophenol ND mg/kg 03/10/21 16:32 95-57-803/10/21 10:020.37 1
4-Chlorophenylphenyl ether ND mg/kg 03/10/21 16:32 7005-72-303/10/21 10:020.37 1
Chrysene ND mg/kg 03/10/21 16:32 218-01-903/10/21 10:020.37 1
Dibenz(a,h)anthracene ND mg/kg 03/10/21 16:32 53-70-303/10/21 10:020.37 1
Dibenzofuran ND mg/kg 03/10/21 16:32 132-64-903/10/21 10:020.37 1
1,2-Dichlorobenzene ND mg/kg 03/10/21 16:32 95-50-103/10/21 10:020.37 1
1,3-Dichlorobenzene ND mg/kg 03/10/21 16:32 541-73-103/10/21 10:020.37 1
1,4-Dichlorobenzene ND mg/kg 03/10/21 16:32 106-46-703/10/21 10:020.37 1
3,3'-Dichlorobenzidine ND mg/kg 03/10/21 16:32 91-94-103/10/21 10:020.75 1
2,4-Dichlorophenol ND mg/kg 03/10/21 16:32 120-83-203/10/21 10:020.37 1
Diethylphthalate ND mg/kg 03/10/21 16:32 84-66-203/10/21 10:020.37 1
2,4-Dimethylphenol ND mg/kg 03/10/21 16:32 105-67-903/10/21 10:020.37 1
Dimethylphthalate ND mg/kg 03/10/21 16:32 131-11-303/10/21 10:020.37 1
Di-n-butylphthalate ND mg/kg 03/10/21 16:32 84-74-203/10/21 10:020.37 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/10/21 16:32 534-52-103/10/21 10:020.75 1
2,4-Dinitrophenol ND mg/kg 03/10/21 16:32 51-28-503/10/21 10:021.9 1
2,4-Dinitrotoluene ND mg/kg 03/10/21 16:32 121-14-203/10/21 10:020.37 1
2,6-Dinitrotoluene ND mg/kg 03/10/21 16:32 606-20-203/10/21 10:020.37 1
Di-n-octylphthalate ND mg/kg 03/10/21 16:32 117-84-003/10/21 10:020.37 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/10/21 16:32 117-81-7 v103/10/21 10:020.37 1
Fluoranthene 0.64 mg/kg 03/10/21 16:32 206-44-003/10/21 10:020.37 1
Fluorene ND mg/kg 03/10/21 16:32 86-73-703/10/21 10:020.37 1
Hexachloro-1,3-butadiene ND mg/kg 03/10/21 16:32 87-68-3 v103/10/21 10:020.37 1
Hexachlorobenzene ND mg/kg 03/10/21 16:32 118-74-103/10/21 10:020.37 1
Hexachlorocyclopentadiene ND mg/kg 03/10/21 16:32 77-47-403/10/21 10:020.37 1
Hexachloroethane ND mg/kg 03/10/21 16:32 67-72-103/10/21 10:020.37 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/10/21 16:32 193-39-503/10/21 10:020.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-1 Lab ID:92525998001 Collected:03/04/21 12:50 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND mg/kg 03/10/21 16:32 78-59-103/10/21 10:020.37 1
1-Methylnaphthalene ND mg/kg 03/10/21 16:32 90-12-003/10/21 10:020.37 1
2-Methylnaphthalene ND mg/kg 03/10/21 16:32 91-57-603/10/21 10:020.37 1
2-Methylphenol(o-Cresol)ND mg/kg 03/10/21 16:32 95-48-703/10/21 10:020.37 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/10/21 16:32 15831-10-403/10/21 10:020.37 1
Naphthalene ND mg/kg 03/10/21 16:32 91-20-303/10/21 10:020.37 1
2-Nitroaniline ND mg/kg 03/10/21 16:32 88-74-403/10/21 10:021.9 1
3-Nitroaniline ND mg/kg 03/10/21 16:32 99-09-2 IL03/10/21 10:021.9 1
4-Nitroaniline ND mg/kg 03/10/21 16:32 100-01-603/10/21 10:020.75 1
Nitrobenzene ND mg/kg 03/10/21 16:32 98-95-303/10/21 10:020.37 1
2-Nitrophenol ND mg/kg 03/10/21 16:32 88-75-503/10/21 10:020.37 1
4-Nitrophenol ND mg/kg 03/10/21 16:32 100-02-703/10/21 10:021.9 1
N-Nitrosodimethylamine ND mg/kg 03/10/21 16:32 62-75-903/10/21 10:020.37 1
N-Nitroso-di-n-propylamine ND mg/kg 03/10/21 16:32 621-64-703/10/21 10:020.37 1
N-Nitrosodiphenylamine ND mg/kg 03/10/21 16:32 86-30-603/10/21 10:020.37 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/10/21 16:32 108-60-103/10/21 10:020.37 1
Pentachlorophenol 6.4 mg/kg 03/10/21 16:32 87-86-503/10/21 10:020.75 1
Phenanthrene ND mg/kg 03/10/21 16:32 85-01-803/10/21 10:020.37 1
Phenol ND mg/kg 03/10/21 16:32 108-95-203/10/21 10:020.37 1
Pyrene 0.55 mg/kg 03/10/21 16:32 129-00-003/10/21 10:020.37 1
Pyridine ND mg/kg 03/10/21 16:32 110-86-103/10/21 10:020.37 1
1,2,4-Trichlorobenzene ND mg/kg 03/10/21 16:32 120-82-103/10/21 10:020.37 1
2,4,5-Trichlorophenol ND mg/kg 03/10/21 16:32 95-95-403/10/21 10:020.37 1
2,4,6-Trichlorophenol ND mg/kg 03/10/21 16:32 88-06-203/10/21 10:020.37 1
Surrogates
Nitrobenzene-d5 (S)47 %03/10/21 16:32 4165-60-003/10/21 10:0221-130 1
2-Fluorobiphenyl (S)39 %03/10/21 16:32 321-60-803/10/21 10:0219-130 1
Terphenyl-d14 (S)54 %03/10/21 16:32 1718-51-003/10/21 10:0215-130 1
Phenol-d6 (S)38 %03/10/21 16:32 13127-88-303/10/21 10:0218-130 1
2-Fluorophenol (S)38 %03/10/21 16:32 367-12-403/10/21 10:0218-130 1
2,4,6-Tribromophenol (S)52 %03/10/21 16:32 118-79-603/10/21 10:0218-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.6 %03/08/21 12:11 N20.10 1
Sample:SS-2 Lab ID:92525998002 Collected:03/04/21 12:55 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/10/21 16:58 83-32-903/10/21 10:020.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-2 Lab ID:92525998002 Collected:03/04/21 12:55 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthylene ND mg/kg 03/10/21 16:58 208-96-803/10/21 10:020.37 1
Aniline ND mg/kg 03/10/21 16:58 62-53-303/10/21 10:020.37 1
Anthracene ND mg/kg 03/10/21 16:58 120-12-703/10/21 10:020.37 1
Benzo(a)anthracene ND mg/kg 03/10/21 16:58 56-55-303/10/21 10:020.37 1
Benzo(a)pyrene 0.41 mg/kg 03/10/21 16:58 50-32-803/10/21 10:020.37 1
Benzo(b)fluoranthene 0.87 mg/kg 03/10/21 16:58 205-99-203/10/21 10:020.37 1
Benzo(g,h,i)perylene 0.40 mg/kg 03/10/21 16:58 191-24-203/10/21 10:020.37 1
Benzo(k)fluoranthene ND mg/kg 03/10/21 16:58 207-08-903/10/21 10:020.37 1
Benzoic Acid ND mg/kg 03/10/21 16:58 65-85-003/10/21 10:021.9 1
Benzyl alcohol ND mg/kg 03/10/21 16:58 100-51-603/10/21 10:020.74 1
4-Bromophenylphenyl ether ND mg/kg 03/10/21 16:58 101-55-303/10/21 10:020.37 1
Butylbenzylphthalate ND mg/kg 03/10/21 16:58 85-68-7 v103/10/21 10:020.37 1
4-Chloro-3-methylphenol ND mg/kg 03/10/21 16:58 59-50-703/10/21 10:020.74 1
4-Chloroaniline ND mg/kg 03/10/21 16:58 106-47-803/10/21 10:020.74 1
bis(2-Chloroethoxy)methane ND mg/kg 03/10/21 16:58 111-91-103/10/21 10:020.37 1
bis(2-Chloroethyl) ether ND mg/kg 03/10/21 16:58 111-44-403/10/21 10:020.37 1
2-Chloronaphthalene ND mg/kg 03/10/21 16:58 91-58-703/10/21 10:020.37 1
2-Chlorophenol ND mg/kg 03/10/21 16:58 95-57-803/10/21 10:020.37 1
4-Chlorophenylphenyl ether ND mg/kg 03/10/21 16:58 7005-72-303/10/21 10:020.37 1
Chrysene 0.66 mg/kg 03/10/21 16:58 218-01-903/10/21 10:020.37 1
Dibenz(a,h)anthracene ND mg/kg 03/10/21 16:58 53-70-303/10/21 10:020.37 1
Dibenzofuran ND mg/kg 03/10/21 16:58 132-64-903/10/21 10:020.37 1
1,2-Dichlorobenzene ND mg/kg 03/10/21 16:58 95-50-103/10/21 10:020.37 1
1,3-Dichlorobenzene ND mg/kg 03/10/21 16:58 541-73-103/10/21 10:020.37 1
1,4-Dichlorobenzene ND mg/kg 03/10/21 16:58 106-46-703/10/21 10:020.37 1
3,3'-Dichlorobenzidine ND mg/kg 03/10/21 16:58 91-94-103/10/21 10:020.74 1
2,4-Dichlorophenol ND mg/kg 03/10/21 16:58 120-83-203/10/21 10:020.37 1
Diethylphthalate ND mg/kg 03/10/21 16:58 84-66-203/10/21 10:020.37 1
2,4-Dimethylphenol ND mg/kg 03/10/21 16:58 105-67-903/10/21 10:020.37 1
Dimethylphthalate ND mg/kg 03/10/21 16:58 131-11-303/10/21 10:020.37 1
Di-n-butylphthalate ND mg/kg 03/10/21 16:58 84-74-203/10/21 10:020.37 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/10/21 16:58 534-52-103/10/21 10:020.74 1
2,4-Dinitrophenol ND mg/kg 03/10/21 16:58 51-28-503/10/21 10:021.9 1
2,4-Dinitrotoluene ND mg/kg 03/10/21 16:58 121-14-203/10/21 10:020.37 1
2,6-Dinitrotoluene ND mg/kg 03/10/21 16:58 606-20-203/10/21 10:020.37 1
Di-n-octylphthalate ND mg/kg 03/10/21 16:58 117-84-003/10/21 10:020.37 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/10/21 16:58 117-81-7 v103/10/21 10:020.37 1
Fluoranthene 1.4 mg/kg 03/10/21 16:58 206-44-003/10/21 10:020.37 1
Fluorene ND mg/kg 03/10/21 16:58 86-73-703/10/21 10:020.37 1
Hexachloro-1,3-butadiene ND mg/kg 03/10/21 16:58 87-68-3 v103/10/21 10:020.37 1
Hexachlorobenzene ND mg/kg 03/10/21 16:58 118-74-103/10/21 10:020.37 1
Hexachlorocyclopentadiene ND mg/kg 03/10/21 16:58 77-47-403/10/21 10:020.37 1
Hexachloroethane ND mg/kg 03/10/21 16:58 67-72-103/10/21 10:020.37 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/10/21 16:58 193-39-503/10/21 10:020.37 1
Isophorone ND mg/kg 03/10/21 16:58 78-59-103/10/21 10:020.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-2 Lab ID:92525998002 Collected:03/04/21 12:55 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1-Methylnaphthalene ND mg/kg 03/10/21 16:58 90-12-003/10/21 10:020.37 1
2-Methylnaphthalene ND mg/kg 03/10/21 16:58 91-57-603/10/21 10:020.37 1
2-Methylphenol(o-Cresol)ND mg/kg 03/10/21 16:58 95-48-703/10/21 10:020.37 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/10/21 16:58 15831-10-403/10/21 10:020.37 1
Naphthalene ND mg/kg 03/10/21 16:58 91-20-303/10/21 10:020.37 1
2-Nitroaniline ND mg/kg 03/10/21 16:58 88-74-403/10/21 10:021.9 1
3-Nitroaniline ND mg/kg 03/10/21 16:58 99-09-2 IL03/10/21 10:021.9 1
4-Nitroaniline ND mg/kg 03/10/21 16:58 100-01-603/10/21 10:020.74 1
Nitrobenzene ND mg/kg 03/10/21 16:58 98-95-303/10/21 10:020.37 1
2-Nitrophenol ND mg/kg 03/10/21 16:58 88-75-503/10/21 10:020.37 1
4-Nitrophenol ND mg/kg 03/10/21 16:58 100-02-7 v103/10/21 10:021.9 1
N-Nitrosodimethylamine ND mg/kg 03/10/21 16:58 62-75-903/10/21 10:020.37 1
N-Nitroso-di-n-propylamine ND mg/kg 03/10/21 16:58 621-64-703/10/21 10:020.37 1
N-Nitrosodiphenylamine ND mg/kg 03/10/21 16:58 86-30-603/10/21 10:020.37 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/10/21 16:58 108-60-103/10/21 10:020.37 1
Pentachlorophenol 1.1 mg/kg 03/10/21 16:58 87-86-503/10/21 10:020.74 1
Phenanthrene 0.54 mg/kg 03/10/21 16:58 85-01-803/10/21 10:020.37 1
Phenol ND mg/kg 03/10/21 16:58 108-95-203/10/21 10:020.37 1
Pyrene 1.1 mg/kg 03/10/21 16:58 129-00-003/10/21 10:020.37 1
Pyridine ND mg/kg 03/10/21 16:58 110-86-103/10/21 10:020.37 1
1,2,4-Trichlorobenzene ND mg/kg 03/10/21 16:58 120-82-103/10/21 10:020.37 1
2,4,5-Trichlorophenol ND mg/kg 03/10/21 16:58 95-95-403/10/21 10:020.37 1
2,4,6-Trichlorophenol ND mg/kg 03/10/21 16:58 88-06-203/10/21 10:020.37 1
Surrogates
Nitrobenzene-d5 (S)68 %03/10/21 16:58 4165-60-003/10/21 10:0221-130 1
2-Fluorobiphenyl (S)58 %03/10/21 16:58 321-60-803/10/21 10:0219-130 1
Terphenyl-d14 (S)66 %03/10/21 16:58 1718-51-003/10/21 10:0215-130 1
Phenol-d6 (S)59 %03/10/21 16:58 13127-88-303/10/21 10:0218-130 1
2-Fluorophenol (S)58 %03/10/21 16:58 367-12-403/10/21 10:0218-130 1
2,4,6-Tribromophenol (S)65 %03/10/21 16:58 118-79-603/10/21 10:0218-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.2 %03/08/21 12:11 N20.10 1
Sample:SS-3 Lab ID:92525998003 Collected:03/04/21 12:57 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/11/21 09:51 83-32-903/10/21 10:020.37 1
Acenaphthylene ND mg/kg 03/11/21 09:51 208-96-803/10/21 10:020.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-3 Lab ID:92525998003 Collected:03/04/21 12:57 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Aniline ND mg/kg 03/11/21 09:51 62-53-303/10/21 10:020.37 1
Anthracene ND mg/kg 03/11/21 09:51 120-12-703/10/21 10:020.37 1
Benzo(a)anthracene ND mg/kg 03/11/21 09:51 56-55-303/10/21 10:020.37 1
Benzo(a)pyrene ND mg/kg 03/11/21 09:51 50-32-803/10/21 10:020.37 1
Benzo(b)fluoranthene ND mg/kg 03/11/21 09:51 205-99-203/10/21 10:020.37 1
Benzo(g,h,i)perylene ND mg/kg 03/11/21 09:51 191-24-203/10/21 10:020.37 1
Benzo(k)fluoranthene ND mg/kg 03/11/21 09:51 207-08-903/10/21 10:020.37 1
Benzoic Acid ND mg/kg 03/11/21 09:51 65-85-003/10/21 10:021.9 1
Benzyl alcohol ND mg/kg 03/11/21 09:51 100-51-603/10/21 10:020.74 1
4-Bromophenylphenyl ether ND mg/kg 03/11/21 09:51 101-55-303/10/21 10:020.37 1
Butylbenzylphthalate ND mg/kg 03/11/21 09:51 85-68-703/10/21 10:020.37 1
4-Chloro-3-methylphenol ND mg/kg 03/11/21 09:51 59-50-703/10/21 10:020.74 1
4-Chloroaniline ND mg/kg 03/11/21 09:51 106-47-803/10/21 10:020.74 1
bis(2-Chloroethoxy)methane ND mg/kg 03/11/21 09:51 111-91-103/10/21 10:020.37 1
bis(2-Chloroethyl) ether ND mg/kg 03/11/21 09:51 111-44-403/10/21 10:020.37 1
2-Chloronaphthalene ND mg/kg 03/11/21 09:51 91-58-703/10/21 10:020.37 1
2-Chlorophenol ND mg/kg 03/11/21 09:51 95-57-803/10/21 10:020.37 1
4-Chlorophenylphenyl ether ND mg/kg 03/11/21 09:51 7005-72-303/10/21 10:020.37 1
Chrysene ND mg/kg 03/11/21 09:51 218-01-903/10/21 10:020.37 1
Dibenz(a,h)anthracene ND mg/kg 03/11/21 09:51 53-70-303/10/21 10:020.37 1
Dibenzofuran ND mg/kg 03/11/21 09:51 132-64-903/10/21 10:020.37 1
1,2-Dichlorobenzene ND mg/kg 03/11/21 09:51 95-50-103/10/21 10:020.37 1
1,3-Dichlorobenzene ND mg/kg 03/11/21 09:51 541-73-103/10/21 10:020.37 1
1,4-Dichlorobenzene ND mg/kg 03/11/21 09:51 106-46-703/10/21 10:020.37 1
3,3'-Dichlorobenzidine ND mg/kg 03/11/21 09:51 91-94-103/10/21 10:020.74 1
2,4-Dichlorophenol ND mg/kg 03/11/21 09:51 120-83-203/10/21 10:020.37 1
Diethylphthalate ND mg/kg 03/11/21 09:51 84-66-203/10/21 10:020.37 1
2,4-Dimethylphenol ND mg/kg 03/11/21 09:51 105-67-903/10/21 10:020.37 1
Dimethylphthalate ND mg/kg 03/11/21 09:51 131-11-303/10/21 10:020.37 1
Di-n-butylphthalate ND mg/kg 03/11/21 09:51 84-74-203/10/21 10:020.37 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/11/21 09:51 534-52-103/10/21 10:020.74 1
2,4-Dinitrophenol ND mg/kg 03/11/21 09:51 51-28-503/10/21 10:021.9 1
2,4-Dinitrotoluene ND mg/kg 03/11/21 09:51 121-14-203/10/21 10:020.37 1
2,6-Dinitrotoluene ND mg/kg 03/11/21 09:51 606-20-203/10/21 10:020.37 1
Di-n-octylphthalate ND mg/kg 03/11/21 09:51 117-84-003/10/21 10:020.37 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/11/21 09:51 117-81-703/10/21 10:020.37 1
Fluoranthene ND mg/kg 03/11/21 09:51 206-44-003/10/21 10:020.37 1
Fluorene ND mg/kg 03/11/21 09:51 86-73-703/10/21 10:020.37 1
Hexachloro-1,3-butadiene ND mg/kg 03/11/21 09:51 87-68-3 v103/10/21 10:020.37 1
Hexachlorobenzene ND mg/kg 03/11/21 09:51 118-74-103/10/21 10:020.37 1
Hexachlorocyclopentadiene ND mg/kg 03/11/21 09:51 77-47-403/10/21 10:020.37 1
Hexachloroethane ND mg/kg 03/11/21 09:51 67-72-103/10/21 10:020.37 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/11/21 09:51 193-39-503/10/21 10:020.37 1
Isophorone ND mg/kg 03/11/21 09:51 78-59-103/10/21 10:020.37 1
1-Methylnaphthalene ND mg/kg 03/11/21 09:51 90-12-003/10/21 10:020.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-3 Lab ID:92525998003 Collected:03/04/21 12:57 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Methylnaphthalene ND mg/kg 03/11/21 09:51 91-57-603/10/21 10:020.37 1
2-Methylphenol(o-Cresol)ND mg/kg 03/11/21 09:51 95-48-703/10/21 10:020.37 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/11/21 09:51 15831-10-403/10/21 10:020.37 1
Naphthalene ND mg/kg 03/11/21 09:51 91-20-303/10/21 10:020.37 1
2-Nitroaniline ND mg/kg 03/11/21 09:51 88-74-403/10/21 10:021.9 1
3-Nitroaniline ND mg/kg 03/11/21 09:51 99-09-2 IL03/10/21 10:021.9 1
4-Nitroaniline ND mg/kg 03/11/21 09:51 100-01-603/10/21 10:020.74 1
Nitrobenzene ND mg/kg 03/11/21 09:51 98-95-3 v103/10/21 10:020.37 1
2-Nitrophenol ND mg/kg 03/11/21 09:51 88-75-503/10/21 10:020.37 1
4-Nitrophenol ND mg/kg 03/11/21 09:51 100-02-7 v103/10/21 10:021.9 1
N-Nitrosodimethylamine ND mg/kg 03/11/21 09:51 62-75-903/10/21 10:020.37 1
N-Nitroso-di-n-propylamine ND mg/kg 03/11/21 09:51 621-64-703/10/21 10:020.37 1
N-Nitrosodiphenylamine ND mg/kg 03/11/21 09:51 86-30-603/10/21 10:020.37 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/11/21 09:51 108-60-103/10/21 10:020.37 1
Pentachlorophenol ND mg/kg 03/11/21 09:51 87-86-503/10/21 10:020.74 1
Phenanthrene ND mg/kg 03/11/21 09:51 85-01-803/10/21 10:020.37 1
Phenol ND mg/kg 03/11/21 09:51 108-95-203/10/21 10:020.37 1
Pyrene ND mg/kg 03/11/21 09:51 129-00-003/10/21 10:020.37 1
Pyridine ND mg/kg 03/11/21 09:51 110-86-103/10/21 10:020.37 1
1,2,4-Trichlorobenzene ND mg/kg 03/11/21 09:51 120-82-103/10/21 10:020.37 1
2,4,5-Trichlorophenol ND mg/kg 03/11/21 09:51 95-95-403/10/21 10:020.37 1
2,4,6-Trichlorophenol ND mg/kg 03/11/21 09:51 88-06-203/10/21 10:020.37 1
Surrogates
Nitrobenzene-d5 (S)43 %03/11/21 09:51 4165-60-003/10/21 10:0221-130 1
2-Fluorobiphenyl (S)37 %03/11/21 09:51 321-60-803/10/21 10:0219-130 1
Terphenyl-d14 (S)52 %03/11/21 09:51 1718-51-003/10/21 10:0215-130 1
Phenol-d6 (S)37 %03/11/21 09:51 13127-88-303/10/21 10:0218-130 1
2-Fluorophenol (S)37 %03/11/21 09:51 367-12-403/10/21 10:0218-130 1
2,4,6-Tribromophenol (S)39 %03/11/21 09:51 118-79-603/10/21 10:0218-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.3 %03/08/21 12:11 N20.10 1
Sample:SS-4 Lab ID:92525998004 Collected:03/04/21 12:35 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/11/21 19:40 83-32-903/11/21 13:220.37 1
Acenaphthylene ND mg/kg 03/11/21 19:40 208-96-803/11/21 13:220.37 1
Aniline ND mg/kg 03/11/21 19:40 62-53-303/11/21 13:220.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-4 Lab ID:92525998004 Collected:03/04/21 12:35 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Anthracene ND mg/kg 03/11/21 19:40 120-12-703/11/21 13:220.37 1
Benzo(a)anthracene ND mg/kg 03/11/21 19:40 56-55-303/11/21 13:220.37 1
Benzo(a)pyrene ND mg/kg 03/11/21 19:40 50-32-803/11/21 13:220.37 1
Benzo(b)fluoranthene ND mg/kg 03/11/21 19:40 205-99-203/11/21 13:220.37 1
Benzo(g,h,i)perylene ND mg/kg 03/11/21 19:40 191-24-203/11/21 13:220.37 1
Benzo(k)fluoranthene ND mg/kg 03/11/21 19:40 207-08-903/11/21 13:220.37 1
Benzoic Acid ND mg/kg 03/11/21 19:40 65-85-003/11/21 13:221.8 1
Benzyl alcohol ND mg/kg 03/11/21 19:40 100-51-603/11/21 13:220.74 1
4-Bromophenylphenyl ether ND mg/kg 03/11/21 19:40 101-55-303/11/21 13:220.37 1
Butylbenzylphthalate ND mg/kg 03/11/21 19:40 85-68-703/11/21 13:220.37 1
4-Chloro-3-methylphenol ND mg/kg 03/11/21 19:40 59-50-703/11/21 13:220.74 1
4-Chloroaniline ND mg/kg 03/11/21 19:40 106-47-803/11/21 13:220.74 1
bis(2-Chloroethoxy)methane ND mg/kg 03/11/21 19:40 111-91-103/11/21 13:220.37 1
bis(2-Chloroethyl) ether ND mg/kg 03/11/21 19:40 111-44-403/11/21 13:220.37 1
2-Chloronaphthalene ND mg/kg 03/11/21 19:40 91-58-703/11/21 13:220.37 1
2-Chlorophenol ND mg/kg 03/11/21 19:40 95-57-803/11/21 13:220.37 1
4-Chlorophenylphenyl ether ND mg/kg 03/11/21 19:40 7005-72-303/11/21 13:220.37 1
Chrysene ND mg/kg 03/11/21 19:40 218-01-903/11/21 13:220.37 1
Dibenz(a,h)anthracene ND mg/kg 03/11/21 19:40 53-70-303/11/21 13:220.37 1
Dibenzofuran ND mg/kg 03/11/21 19:40 132-64-903/11/21 13:220.37 1
1,2-Dichlorobenzene ND mg/kg 03/11/21 19:40 95-50-103/11/21 13:220.37 1
1,3-Dichlorobenzene ND mg/kg 03/11/21 19:40 541-73-103/11/21 13:220.37 1
1,4-Dichlorobenzene ND mg/kg 03/11/21 19:40 106-46-703/11/21 13:220.37 1
3,3'-Dichlorobenzidine ND mg/kg 03/11/21 19:40 91-94-1 IL03/11/21 13:220.74 1
2,4-Dichlorophenol ND mg/kg 03/11/21 19:40 120-83-203/11/21 13:220.37 1
Diethylphthalate ND mg/kg 03/11/21 19:40 84-66-203/11/21 13:220.37 1
2,4-Dimethylphenol ND mg/kg 03/11/21 19:40 105-67-903/11/21 13:220.37 1
Dimethylphthalate ND mg/kg 03/11/21 19:40 131-11-303/11/21 13:220.37 1
Di-n-butylphthalate ND mg/kg 03/11/21 19:40 84-74-203/11/21 13:220.37 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/11/21 19:40 534-52-103/11/21 13:220.74 1
2,4-Dinitrophenol ND mg/kg 03/11/21 19:40 51-28-503/11/21 13:221.8 1
2,4-Dinitrotoluene ND mg/kg 03/11/21 19:40 121-14-203/11/21 13:220.37 1
2,6-Dinitrotoluene ND mg/kg 03/11/21 19:40 606-20-203/11/21 13:220.37 1
Di-n-octylphthalate ND mg/kg 03/11/21 19:40 117-84-003/11/21 13:220.37 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/11/21 19:40 117-81-703/11/21 13:220.37 1
Fluoranthene ND mg/kg 03/11/21 19:40 206-44-003/11/21 13:220.37 1
Fluorene ND mg/kg 03/11/21 19:40 86-73-703/11/21 13:220.37 1
Hexachloro-1,3-butadiene ND mg/kg 03/11/21 19:40 87-68-303/11/21 13:220.37 1
Hexachlorobenzene ND mg/kg 03/11/21 19:40 118-74-103/11/21 13:220.37 1
Hexachlorocyclopentadiene ND mg/kg 03/11/21 19:40 77-47-403/11/21 13:220.37 1
Hexachloroethane ND mg/kg 03/11/21 19:40 67-72-103/11/21 13:220.37 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/11/21 19:40 193-39-503/11/21 13:220.37 1
Isophorone ND mg/kg 03/11/21 19:40 78-59-103/11/21 13:220.37 1
1-Methylnaphthalene ND mg/kg 03/11/21 19:40 90-12-003/11/21 13:220.37 1
2-Methylnaphthalene ND mg/kg 03/11/21 19:40 91-57-603/11/21 13:220.37 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-4 Lab ID:92525998004 Collected:03/04/21 12:35 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
2-Methylphenol(o-Cresol)ND mg/kg 03/11/21 19:40 95-48-703/11/21 13:220.37 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/11/21 19:40 15831-10-403/11/21 13:220.37 1
Naphthalene ND mg/kg 03/11/21 19:40 91-20-303/11/21 13:220.37 1
2-Nitroaniline ND mg/kg 03/11/21 19:40 88-74-403/11/21 13:221.8 1
3-Nitroaniline ND mg/kg 03/11/21 19:40 99-09-203/11/21 13:221.8 1
4-Nitroaniline ND mg/kg 03/11/21 19:40 100-01-603/11/21 13:220.74 1
Nitrobenzene ND mg/kg 03/11/21 19:40 98-95-303/11/21 13:220.37 1
2-Nitrophenol ND mg/kg 03/11/21 19:40 88-75-503/11/21 13:220.37 1
4-Nitrophenol ND mg/kg 03/11/21 19:40 100-02-703/11/21 13:221.8 1
N-Nitrosodimethylamine ND mg/kg 03/11/21 19:40 62-75-9 v103/11/21 13:220.37 1
N-Nitroso-di-n-propylamine ND mg/kg 03/11/21 19:40 621-64-703/11/21 13:220.37 1
N-Nitrosodiphenylamine ND mg/kg 03/11/21 19:40 86-30-603/11/21 13:220.37 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/11/21 19:40 108-60-103/11/21 13:220.37 1
Pentachlorophenol 2.0 mg/kg 03/11/21 19:40 87-86-503/11/21 13:220.74 1
Phenanthrene ND mg/kg 03/11/21 19:40 85-01-803/11/21 13:220.37 1
Phenol ND mg/kg 03/11/21 19:40 108-95-2 v103/11/21 13:220.37 1
Pyrene ND mg/kg 03/11/21 19:40 129-00-003/11/21 13:220.37 1
Pyridine ND mg/kg 03/11/21 19:40 110-86-103/11/21 13:220.37 1
1,2,4-Trichlorobenzene ND mg/kg 03/11/21 19:40 120-82-103/11/21 13:220.37 1
2,4,5-Trichlorophenol ND mg/kg 03/11/21 19:40 95-95-403/11/21 13:220.37 1
2,4,6-Trichlorophenol ND mg/kg 03/11/21 19:40 88-06-203/11/21 13:220.37 1
Surrogates
Nitrobenzene-d5 (S)52 %03/11/21 19:40 4165-60-003/11/21 13:2221-130 1
2-Fluorobiphenyl (S)45 %03/11/21 19:40 321-60-803/11/21 13:2219-130 1
Terphenyl-d14 (S)63 %03/11/21 19:40 1718-51-003/11/21 13:2215-130 1
Phenol-d6 (S)54 %03/11/21 19:40 13127-88-303/11/21 13:2218-130 1
2-Fluorophenol (S)50 %03/11/21 19:40 367-12-403/11/21 13:2218-130 1
2,4,6-Tribromophenol (S)55 %03/11/21 19:40 118-79-603/11/21 13:2218-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 11.3 %03/08/21 12:11 N20.10 1
Sample:SS-5 Lab ID:92525998005 Collected:03/04/21 13:00 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/11/21 08:59 83-32-903/10/21 10:020.39 1
Acenaphthylene ND mg/kg 03/11/21 08:59 208-96-803/10/21 10:020.39 1
Aniline ND mg/kg 03/11/21 08:59 62-53-303/10/21 10:020.39 1
Anthracene ND mg/kg 03/11/21 08:59 120-12-703/10/21 10:020.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-5 Lab ID:92525998005 Collected:03/04/21 13:00 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Benzo(a)anthracene ND mg/kg 03/11/21 08:59 56-55-303/10/21 10:020.39 1
Benzo(a)pyrene ND mg/kg 03/11/21 08:59 50-32-803/10/21 10:020.39 1
Benzo(b)fluoranthene 0.55 mg/kg 03/11/21 08:59 205-99-203/10/21 10:020.39 1
Benzo(g,h,i)perylene ND mg/kg 03/11/21 08:59 191-24-203/10/21 10:020.39 1
Benzo(k)fluoranthene ND mg/kg 03/11/21 08:59 207-08-903/10/21 10:020.39 1
Benzoic Acid ND mg/kg 03/11/21 08:59 65-85-003/10/21 10:021.9 1
Benzyl alcohol ND mg/kg 03/11/21 08:59 100-51-603/10/21 10:020.77 1
4-Bromophenylphenyl ether ND mg/kg 03/11/21 08:59 101-55-303/10/21 10:020.39 1
Butylbenzylphthalate ND mg/kg 03/11/21 08:59 85-68-703/10/21 10:020.39 1
4-Chloro-3-methylphenol ND mg/kg 03/11/21 08:59 59-50-703/10/21 10:020.77 1
4-Chloroaniline ND mg/kg 03/11/21 08:59 106-47-803/10/21 10:020.77 1
bis(2-Chloroethoxy)methane ND mg/kg 03/11/21 08:59 111-91-103/10/21 10:020.39 1
bis(2-Chloroethyl) ether ND mg/kg 03/11/21 08:59 111-44-403/10/21 10:020.39 1
2-Chloronaphthalene ND mg/kg 03/11/21 08:59 91-58-703/10/21 10:020.39 1
2-Chlorophenol ND mg/kg 03/11/21 08:59 95-57-803/10/21 10:020.39 1
4-Chlorophenylphenyl ether ND mg/kg 03/11/21 08:59 7005-72-303/10/21 10:020.39 1
Chrysene 0.49 mg/kg 03/11/21 08:59 218-01-903/10/21 10:020.39 1
Dibenz(a,h)anthracene ND mg/kg 03/11/21 08:59 53-70-303/10/21 10:020.39 1
Dibenzofuran ND mg/kg 03/11/21 08:59 132-64-903/10/21 10:020.39 1
1,2-Dichlorobenzene ND mg/kg 03/11/21 08:59 95-50-103/10/21 10:020.39 1
1,3-Dichlorobenzene ND mg/kg 03/11/21 08:59 541-73-103/10/21 10:020.39 1
1,4-Dichlorobenzene ND mg/kg 03/11/21 08:59 106-46-703/10/21 10:020.39 1
3,3'-Dichlorobenzidine ND mg/kg 03/11/21 08:59 91-94-103/10/21 10:020.77 1
2,4-Dichlorophenol ND mg/kg 03/11/21 08:59 120-83-203/10/21 10:020.39 1
Diethylphthalate ND mg/kg 03/11/21 08:59 84-66-203/10/21 10:020.39 1
2,4-Dimethylphenol ND mg/kg 03/11/21 08:59 105-67-903/10/21 10:020.39 1
Dimethylphthalate ND mg/kg 03/11/21 08:59 131-11-303/10/21 10:020.39 1
Di-n-butylphthalate ND mg/kg 03/11/21 08:59 84-74-203/10/21 10:020.39 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/11/21 08:59 534-52-103/10/21 10:020.77 1
2,4-Dinitrophenol ND mg/kg 03/11/21 08:59 51-28-503/10/21 10:021.9 1
2,4-Dinitrotoluene ND mg/kg 03/11/21 08:59 121-14-203/10/21 10:020.39 1
2,6-Dinitrotoluene ND mg/kg 03/11/21 08:59 606-20-203/10/21 10:020.39 1
Di-n-octylphthalate ND mg/kg 03/11/21 08:59 117-84-003/10/21 10:020.39 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/11/21 08:59 117-81-703/10/21 10:020.39 1
Fluoranthene 0.97 mg/kg 03/11/21 08:59 206-44-003/10/21 10:020.39 1
Fluorene ND mg/kg 03/11/21 08:59 86-73-703/10/21 10:020.39 1
Hexachloro-1,3-butadiene ND mg/kg 03/11/21 08:59 87-68-3 v103/10/21 10:020.39 1
Hexachlorobenzene ND mg/kg 03/11/21 08:59 118-74-103/10/21 10:020.39 1
Hexachlorocyclopentadiene ND mg/kg 03/11/21 08:59 77-47-403/10/21 10:020.39 1
Hexachloroethane ND mg/kg 03/11/21 08:59 67-72-103/10/21 10:020.39 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/11/21 08:59 193-39-503/10/21 10:020.39 1
Isophorone ND mg/kg 03/11/21 08:59 78-59-103/10/21 10:020.39 1
1-Methylnaphthalene ND mg/kg 03/11/21 08:59 90-12-003/10/21 10:020.39 1
2-Methylnaphthalene ND mg/kg 03/11/21 08:59 91-57-603/10/21 10:020.39 1
2-Methylphenol(o-Cresol)ND mg/kg 03/11/21 08:59 95-48-703/10/21 10:020.39 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-5 Lab ID:92525998005 Collected:03/04/21 13:00 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/11/21 08:59 15831-10-403/10/21 10:020.39 1
Naphthalene ND mg/kg 03/11/21 08:59 91-20-303/10/21 10:020.39 1
2-Nitroaniline ND mg/kg 03/11/21 08:59 88-74-403/10/21 10:021.9 1
3-Nitroaniline ND mg/kg 03/11/21 08:59 99-09-2 IL03/10/21 10:021.9 1
4-Nitroaniline ND mg/kg 03/11/21 08:59 100-01-603/10/21 10:020.77 1
Nitrobenzene ND mg/kg 03/11/21 08:59 98-95-3 v103/10/21 10:020.39 1
2-Nitrophenol ND mg/kg 03/11/21 08:59 88-75-503/10/21 10:020.39 1
4-Nitrophenol ND mg/kg 03/11/21 08:59 100-02-7 v103/10/21 10:021.9 1
N-Nitrosodimethylamine ND mg/kg 03/11/21 08:59 62-75-903/10/21 10:020.39 1
N-Nitroso-di-n-propylamine ND mg/kg 03/11/21 08:59 621-64-703/10/21 10:020.39 1
N-Nitrosodiphenylamine ND mg/kg 03/11/21 08:59 86-30-603/10/21 10:020.39 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/11/21 08:59 108-60-103/10/21 10:020.39 1
Pentachlorophenol 41.5 mg/kg 03/11/21 10:16 87-86-503/10/21 10:027.7 10
Phenanthrene ND mg/kg 03/11/21 08:59 85-01-803/10/21 10:020.39 1
Phenol ND mg/kg 03/11/21 08:59 108-95-203/10/21 10:020.39 1
Pyrene 0.73 mg/kg 03/11/21 08:59 129-00-003/10/21 10:020.39 1
Pyridine ND mg/kg 03/11/21 08:59 110-86-103/10/21 10:020.39 1
1,2,4-Trichlorobenzene ND mg/kg 03/11/21 08:59 120-82-103/10/21 10:020.39 1
2,4,5-Trichlorophenol ND mg/kg 03/11/21 08:59 95-95-403/10/21 10:020.39 1
2,4,6-Trichlorophenol ND mg/kg 03/11/21 08:59 88-06-203/10/21 10:020.39 1
Surrogates
Nitrobenzene-d5 (S)46 %03/11/21 08:59 4165-60-003/10/21 10:0221-130 1
2-Fluorobiphenyl (S)41 %03/11/21 08:59 321-60-803/10/21 10:0219-130 1
Terphenyl-d14 (S)51 %03/11/21 08:59 1718-51-003/10/21 10:0215-130 1
Phenol-d6 (S)38 %03/11/21 08:59 13127-88-303/10/21 10:0218-130 1
2-Fluorophenol (S)37 %03/11/21 08:59 367-12-403/10/21 10:0218-130 1
2,4,6-Tribromophenol (S)50 %03/11/21 08:59 118-79-603/10/21 10:0218-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.6 %03/08/21 12:51 N20.10 1
Sample:SS-6 Lab ID:92525998006 Collected:03/04/21 13:37 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 03/11/21 09:25 83-32-903/10/21 10:020.38 1
Acenaphthylene ND mg/kg 03/11/21 09:25 208-96-803/10/21 10:020.38 1
Aniline ND mg/kg 03/11/21 09:25 62-53-303/10/21 10:020.38 1
Anthracene ND mg/kg 03/11/21 09:25 120-12-703/10/21 10:020.38 1
Benzo(a)anthracene ND mg/kg 03/11/21 09:25 56-55-303/10/21 10:020.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-6 Lab ID:92525998006 Collected:03/04/21 13:37 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Benzo(a)pyrene ND mg/kg 03/11/21 09:25 50-32-803/10/21 10:020.38 1
Benzo(b)fluoranthene ND mg/kg 03/11/21 09:25 205-99-203/10/21 10:020.38 1
Benzo(g,h,i)perylene ND mg/kg 03/11/21 09:25 191-24-203/10/21 10:020.38 1
Benzo(k)fluoranthene ND mg/kg 03/11/21 09:25 207-08-903/10/21 10:020.38 1
Benzoic Acid ND mg/kg 03/11/21 09:25 65-85-003/10/21 10:021.9 1
Benzyl alcohol ND mg/kg 03/11/21 09:25 100-51-603/10/21 10:020.77 1
4-Bromophenylphenyl ether ND mg/kg 03/11/21 09:25 101-55-303/10/21 10:020.38 1
Butylbenzylphthalate ND mg/kg 03/11/21 09:25 85-68-703/10/21 10:020.38 1
4-Chloro-3-methylphenol ND mg/kg 03/11/21 09:25 59-50-703/10/21 10:020.77 1
4-Chloroaniline ND mg/kg 03/11/21 09:25 106-47-803/10/21 10:020.77 1
bis(2-Chloroethoxy)methane ND mg/kg 03/11/21 09:25 111-91-103/10/21 10:020.38 1
bis(2-Chloroethyl) ether ND mg/kg 03/11/21 09:25 111-44-403/10/21 10:020.38 1
2-Chloronaphthalene ND mg/kg 03/11/21 09:25 91-58-703/10/21 10:020.38 1
2-Chlorophenol ND mg/kg 03/11/21 09:25 95-57-803/10/21 10:020.38 1
4-Chlorophenylphenyl ether ND mg/kg 03/11/21 09:25 7005-72-303/10/21 10:020.38 1
Chrysene ND mg/kg 03/11/21 09:25 218-01-903/10/21 10:020.38 1
Dibenz(a,h)anthracene ND mg/kg 03/11/21 09:25 53-70-303/10/21 10:020.38 1
Dibenzofuran ND mg/kg 03/11/21 09:25 132-64-903/10/21 10:020.38 1
1,2-Dichlorobenzene ND mg/kg 03/11/21 09:25 95-50-103/10/21 10:020.38 1
1,3-Dichlorobenzene ND mg/kg 03/11/21 09:25 541-73-103/10/21 10:020.38 1
1,4-Dichlorobenzene ND mg/kg 03/11/21 09:25 106-46-703/10/21 10:020.38 1
3,3'-Dichlorobenzidine ND mg/kg 03/11/21 09:25 91-94-103/10/21 10:020.77 1
2,4-Dichlorophenol ND mg/kg 03/11/21 09:25 120-83-203/10/21 10:020.38 1
Diethylphthalate ND mg/kg 03/11/21 09:25 84-66-203/10/21 10:020.38 1
2,4-Dimethylphenol ND mg/kg 03/11/21 09:25 105-67-903/10/21 10:020.38 1
Dimethylphthalate ND mg/kg 03/11/21 09:25 131-11-303/10/21 10:020.38 1
Di-n-butylphthalate ND mg/kg 03/11/21 09:25 84-74-203/10/21 10:020.38 1
4,6-Dinitro-2-methylphenol ND mg/kg 03/11/21 09:25 534-52-103/10/21 10:020.77 1
2,4-Dinitrophenol ND mg/kg 03/11/21 09:25 51-28-503/10/21 10:021.9 1
2,4-Dinitrotoluene ND mg/kg 03/11/21 09:25 121-14-203/10/21 10:020.38 1
2,6-Dinitrotoluene ND mg/kg 03/11/21 09:25 606-20-203/10/21 10:020.38 1
Di-n-octylphthalate ND mg/kg 03/11/21 09:25 117-84-003/10/21 10:020.38 1
bis(2-Ethylhexyl)phthalate ND mg/kg 03/11/21 09:25 117-81-703/10/21 10:020.38 1
Fluoranthene ND mg/kg 03/11/21 09:25 206-44-003/10/21 10:020.38 1
Fluorene ND mg/kg 03/11/21 09:25 86-73-703/10/21 10:020.38 1
Hexachloro-1,3-butadiene ND mg/kg 03/11/21 09:25 87-68-3 v103/10/21 10:020.38 1
Hexachlorobenzene ND mg/kg 03/11/21 09:25 118-74-103/10/21 10:020.38 1
Hexachlorocyclopentadiene ND mg/kg 03/11/21 09:25 77-47-403/10/21 10:020.38 1
Hexachloroethane ND mg/kg 03/11/21 09:25 67-72-103/10/21 10:020.38 1
Indeno(1,2,3-cd)pyrene ND mg/kg 03/11/21 09:25 193-39-503/10/21 10:020.38 1
Isophorone ND mg/kg 03/11/21 09:25 78-59-103/10/21 10:020.38 1
1-Methylnaphthalene ND mg/kg 03/11/21 09:25 90-12-003/10/21 10:020.38 1
2-Methylnaphthalene ND mg/kg 03/11/21 09:25 91-57-603/10/21 10:020.38 1
2-Methylphenol(o-Cresol)ND mg/kg 03/11/21 09:25 95-48-703/10/21 10:020.38 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 03/11/21 09:25 15831-10-403/10/21 10:020.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 14 of 36
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92525998
Northstate 12119-B
Sample:SS-6 Lab ID:92525998006 Collected:03/04/21 13:37 Received:03/05/21 10:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Naphthalene ND mg/kg 03/11/21 09:25 91-20-303/10/21 10:020.38 1
2-Nitroaniline ND mg/kg 03/11/21 09:25 88-74-403/10/21 10:021.9 1
3-Nitroaniline ND mg/kg 03/11/21 09:25 99-09-2 IL03/10/21 10:021.9 1
4-Nitroaniline ND mg/kg 03/11/21 09:25 100-01-603/10/21 10:020.77 1
Nitrobenzene ND mg/kg 03/11/21 09:25 98-95-3 v103/10/21 10:020.38 1
2-Nitrophenol ND mg/kg 03/11/21 09:25 88-75-503/10/21 10:020.38 1
4-Nitrophenol ND mg/kg 03/11/21 09:25 100-02-7 v103/10/21 10:021.9 1
N-Nitrosodimethylamine ND mg/kg 03/11/21 09:25 62-75-903/10/21 10:020.38 1
N-Nitroso-di-n-propylamine ND mg/kg 03/11/21 09:25 621-64-703/10/21 10:020.38 1
N-Nitrosodiphenylamine ND mg/kg 03/11/21 09:25 86-30-603/10/21 10:020.38 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 03/11/21 09:25 108-60-103/10/21 10:020.38 1
Pentachlorophenol ND mg/kg 03/11/21 09:25 87-86-503/10/21 10:020.77 1
Phenanthrene ND mg/kg 03/11/21 09:25 85-01-803/10/21 10:020.38 1
Phenol ND mg/kg 03/11/21 09:25 108-95-203/10/21 10:020.38 1
Pyrene ND mg/kg 03/11/21 09:25 129-00-003/10/21 10:020.38 1
Pyridine ND mg/kg 03/11/21 09:25 110-86-103/10/21 10:020.38 1
1,2,4-Trichlorobenzene ND mg/kg 03/11/21 09:25 120-82-103/10/21 10:020.38 1
2,4,5-Trichlorophenol ND mg/kg 03/11/21 09:25 95-95-403/10/21 10:020.38 1
2,4,6-Trichlorophenol ND mg/kg 03/11/21 09:25 88-06-203/10/21 10:020.38 1
Surrogates
Nitrobenzene-d5 (S)63 %03/11/21 09:25 4165-60-003/10/21 10:0221-130 1
2-Fluorobiphenyl (S)52 %03/11/21 09:25 321-60-803/10/21 10:0219-130 1
Terphenyl-d14 (S)64 %03/11/21 09:25 1718-51-003/10/21 10:0215-130 1
Phenol-d6 (S)53 %03/11/21 09:25 13127-88-303/10/21 10:0218-130 1
2-Fluorophenol (S)54 %03/11/21 09:25 367-12-403/10/21 10:0218-130 1
2,4,6-Tribromophenol (S)60 %03/11/21 09:25 118-79-603/10/21 10:0218-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 14.0 %03/08/21 12:51 N20.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
605438
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92525998001, 92525998002, 92525998003, 92525998005, 92525998006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3189610
Associated Lab Samples:92525998001, 92525998002, 92525998003, 92525998005, 92525998006
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 03/10/21 13:51
1,2-Dichlorobenzene mg/kg ND 0.33 03/10/21 13:51
1,3-Dichlorobenzene mg/kg ND 0.33 03/10/21 13:51
1,4-Dichlorobenzene mg/kg ND 0.33 03/10/21 13:51
1-Methylnaphthalene mg/kg ND 0.33 03/10/21 13:51
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 03/10/21 13:51
2,4,5-Trichlorophenol mg/kg ND 0.33 03/10/21 13:51
2,4,6-Trichlorophenol mg/kg ND 0.33 03/10/21 13:51
2,4-Dichlorophenol mg/kg ND 0.33 03/10/21 13:51
2,4-Dimethylphenol mg/kg ND 0.33 03/10/21 13:51
2,4-Dinitrophenol mg/kg ND 1.6 03/10/21 13:51
2,4-Dinitrotoluene mg/kg ND 0.33 03/10/21 13:51
2,6-Dinitrotoluene mg/kg ND 0.33 03/10/21 13:51
2-Chloronaphthalene mg/kg ND 0.33 03/10/21 13:51
2-Chlorophenol mg/kg ND 0.33 03/10/21 13:51
2-Methylnaphthalene mg/kg ND 0.33 03/10/21 13:51
2-Methylphenol(o-Cresol)mg/kg ND 0.33 03/10/21 13:51
2-Nitroaniline mg/kg ND 1.6 03/10/21 13:51
2-Nitrophenol mg/kg ND 0.33 03/10/21 13:51
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 03/10/21 13:51
3,3'-Dichlorobenzidine mg/kg ND 0.66 03/10/21 13:51
3-Nitroaniline mg/kg ND 1.6 IL03/10/21 13:51
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 03/10/21 13:51
4-Bromophenylphenyl ether mg/kg ND 0.33 03/10/21 13:51
4-Chloro-3-methylphenol mg/kg ND 0.66 03/10/21 13:51
4-Chloroaniline mg/kg ND 0.66 03/10/21 13:51
4-Chlorophenylphenyl ether mg/kg ND 0.33 03/10/21 13:51
4-Nitroaniline mg/kg ND 0.66 03/10/21 13:51
4-Nitrophenol mg/kg ND 1.6 03/10/21 13:51
Acenaphthene mg/kg ND 0.33 03/10/21 13:51
Acenaphthylene mg/kg ND 0.33 03/10/21 13:51
Aniline mg/kg ND 0.33 03/10/21 13:51
Anthracene mg/kg ND 0.33 03/10/21 13:51
Benzo(a)anthracene mg/kg ND 0.33 03/10/21 13:51
Benzo(a)pyrene mg/kg ND 0.33 03/10/21 13:51
Benzo(b)fluoranthene mg/kg ND 0.33 03/10/21 13:51
Benzo(g,h,i)perylene mg/kg ND 0.33 03/10/21 13:51
Benzo(k)fluoranthene mg/kg ND 0.33 03/10/21 13:51
Benzoic Acid mg/kg ND 1.6 03/10/21 13:51
Benzyl alcohol mg/kg ND 0.66 03/10/21 13:51
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3189610
Associated Lab Samples:92525998001, 92525998002, 92525998003, 92525998005, 92525998006
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 03/10/21 13:51
bis(2-Chloroethyl) ether mg/kg ND 0.33 03/10/21 13:51
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 v103/10/21 13:51
Butylbenzylphthalate mg/kg ND 0.33 v103/10/21 13:51
Chrysene mg/kg ND 0.33 03/10/21 13:51
Di-n-butylphthalate mg/kg ND 0.33 03/10/21 13:51
Di-n-octylphthalate mg/kg ND 0.33 03/10/21 13:51
Dibenz(a,h)anthracene mg/kg ND 0.33 03/10/21 13:51
Dibenzofuran mg/kg ND 0.33 03/10/21 13:51
Diethylphthalate mg/kg ND 0.33 03/10/21 13:51
Dimethylphthalate mg/kg ND 0.33 03/10/21 13:51
Fluoranthene mg/kg ND 0.33 03/10/21 13:51
Fluorene mg/kg ND 0.33 03/10/21 13:51
Hexachloro-1,3-butadiene mg/kg ND 0.33 v103/10/21 13:51
Hexachlorobenzene mg/kg ND 0.33 03/10/21 13:51
Hexachlorocyclopentadiene mg/kg ND 0.33 03/10/21 13:51
Hexachloroethane mg/kg ND 0.33 03/10/21 13:51
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 03/10/21 13:51
Isophorone mg/kg ND 0.33 03/10/21 13:51
N-Nitroso-di-n-propylamine mg/kg ND 0.33 03/10/21 13:51
N-Nitrosodimethylamine mg/kg ND 0.33 03/10/21 13:51
N-Nitrosodiphenylamine mg/kg ND 0.33 03/10/21 13:51
Naphthalene mg/kg ND 0.33 03/10/21 13:51
Nitrobenzene mg/kg ND 0.33 03/10/21 13:51
Pentachlorophenol mg/kg ND 0.66 03/10/21 13:51
Phenanthrene mg/kg ND 0.33 03/10/21 13:51
Phenol mg/kg ND 0.33 03/10/21 13:51
Pyrene mg/kg ND 0.33 03/10/21 13:51
Pyridine mg/kg ND 0.33 03/10/21 13:51
2,4,6-Tribromophenol (S)%86 18-130 03/10/21 13:51
2-Fluorobiphenyl (S)%81 19-130 03/10/21 13:51
2-Fluorophenol (S)%79 18-130 03/10/21 13:51
Nitrobenzene-d5 (S)%92 21-130 03/10/21 13:51
Phenol-d6 (S)%78 18-130 03/10/21 13:51
Terphenyl-d14 (S)%110 15-130 03/10/21 13:51
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3189611LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.51.7 92 47-130
1,2-Dichlorobenzene mg/kg 1.41.7 84 49-130
1,3-Dichlorobenzene mg/kg 1.41.7 84 48-130
1,4-Dichlorobenzene mg/kg 1.41.7 86 49-130
1-Methylnaphthalene mg/kg 1.41.7 85 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3189611LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.61.7 93 38-130
2,4,5-Trichlorophenol mg/kg 1.51.7 90 49-130
2,4,6-Trichlorophenol mg/kg 1.51.7 92 50-130
2,4-Dichlorophenol mg/kg 1.51.7 92 51-130
2,4-Dimethylphenol mg/kg 1.61.7 97 53-130
2,4-Dinitrophenol mg/kg 7.48.3 88 39-130
2,4-Dinitrotoluene mg/kg 1.51.7 90 53-130
2,6-Dinitrotoluene mg/kg 1.51.7 92 55-130
2-Chloronaphthalene mg/kg 1.41.7 85 48-130
2-Chlorophenol mg/kg 1.41.7 84 54-130
2-Methylnaphthalene mg/kg 1.51.7 88 57-130
2-Methylphenol(o-Cresol)mg/kg 1.31.7 79 50-130
2-Nitroaniline mg/kg 3.13.3 93 49-130
2-Nitrophenol mg/kg 1.51.7 91 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.41.7 84 50-130
3,3'-Dichlorobenzidine mg/kg 2.63.3 77 47-130
3-Nitroaniline mg/kg 2.2 IL3.3 67 45-130
4,6-Dinitro-2-methylphenol mg/kg 3.23.3 95 50-142
4-Bromophenylphenyl ether mg/kg 1.71.7 100 55-130
4-Chloro-3-methylphenol mg/kg 3.13.3 94 52-130
4-Chloroaniline mg/kg 2.63.3 79 49-130
4-Chlorophenylphenyl ether mg/kg 1.61.7 94 53-130
4-Nitroaniline mg/kg 2.53.3 76 51-130
4-Nitrophenol mg/kg 9.88.3 117 40-130
Acenaphthene mg/kg 1.41.7 87 56-130
Acenaphthylene mg/kg 1.41.7 87 58-130
Aniline mg/kg 1.31.7 76 44-130
Anthracene mg/kg 1.51.7 90 60-130
Benzo(a)anthracene mg/kg 1.61.7 96 59-130
Benzo(a)pyrene mg/kg 1.61.7 98 57-130
Benzo(b)fluoranthene mg/kg 1.71.7 100 54-130
Benzo(g,h,i)perylene mg/kg 1.51.7 92 59-130
Benzo(k)fluoranthene mg/kg 1.61.7 95 54-130
Benzoic Acid mg/kg 6.28.3 74 19-130
Benzyl alcohol mg/kg 2.83.3 84 50-130
bis(2-Chloroethoxy)methane mg/kg 1.41.7 83 55-130
bis(2-Chloroethyl) ether mg/kg 1.41.7 85 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.7 v11.7 99 58-130
Butylbenzylphthalate mg/kg 1.7 v11.7 102 46-138
Chrysene mg/kg 1.51.7 90 57-130
Di-n-butylphthalate mg/kg 1.61.7 93 57-130
Di-n-octylphthalate mg/kg 1.71.7 102 57-130
Dibenz(a,h)anthracene mg/kg 1.61.7 93 60-130
Dibenzofuran mg/kg 1.51.7 89 54-130
Diethylphthalate mg/kg 1.61.7 94 55-130
Dimethylphthalate mg/kg 1.51.7 91 57-130
Fluoranthene mg/kg 1.61.7 93 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3189611LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.51.7 92 56-130
Hexachloro-1,3-butadiene mg/kg 1.7 v11.7 103 41-130
Hexachlorobenzene mg/kg 1.61.7 97 53-130
Hexachlorocyclopentadiene mg/kg 1.31.7 79 23-130
Hexachloroethane mg/kg 1.51.7 91 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.61.7 97 61-130
Isophorone mg/kg 1.51.7 93 49-130
N-Nitroso-di-n-propylamine mg/kg 1.51.7 92 52-130
N-Nitrosodimethylamine mg/kg 1.41.7 82 45-130
N-Nitrosodiphenylamine mg/kg 1.51.7 92 56-130
Naphthalene mg/kg 1.41.7 87 56-130
Nitrobenzene mg/kg 1.61.7 98 50-130
Pentachlorophenol mg/kg 2.83.3 85 33-130
Phenanthrene mg/kg 1.51.7 90 60-130
Phenol mg/kg 1.51.7 88 54-130
Pyrene mg/kg 1.71.7 100 61-130
Pyridine mg/kg 1.11.7 64 35-130
2,4,6-Tribromophenol (S)%90 18-130
2-Fluorobiphenyl (S)%80 19-130
2-Fluorophenol (S)%79 18-130
Nitrobenzene-d5 (S)%89 21-130
Phenol-d6 (S)%76 18-130
Terphenyl-d14 (S)%108 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3189612MATRIX SPIKE SAMPLE:
MSSpike
Result
92525841001
1,2,4-Trichlorobenzene mg/kg 1.52.5 61 22-130ND
1,2-Dichlorobenzene mg/kg 1.52.5 62 23-130ND
1,3-Dichlorobenzene mg/kg 1.52.5 61 26-130ND
1,4-Dichlorobenzene mg/kg 1.52.5 63 27-130ND
1-Methylnaphthalene mg/kg 1.32.5 55 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.82.5 76 30-130ND
2,4,5-Trichlorophenol mg/kg 1.82.5 74 26-130ND
2,4,6-Trichlorophenol mg/kg 1.82.5 75 23-130ND
2,4-Dichlorophenol mg/kg 1.92.5 76 29-130ND
2,4-Dimethylphenol mg/kg 1.92.5 78 13-130ND
2,4-Dinitrophenol mg/kg 9.412.1 78 10-131ND
2,4-Dinitrotoluene mg/kg 1.82.5 75 28-130ND
2,6-Dinitrotoluene mg/kg 1.82.5 73 36-130ND
2-Chloronaphthalene mg/kg 1.32.5 55 27-130ND
2-Chlorophenol mg/kg 1.72.5 71 29-130ND
2-Methylnaphthalene mg/kg 1.32.5 55 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.62.5 66 20-130ND
2-Nitroaniline mg/kg 4.04.8 82 29-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
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[phone]
Page 19 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3189612MATRIX SPIKE SAMPLE:
MSSpike
Result
92525841001
2-Nitrophenol mg/kg 1.82.5 76 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.82.5 73 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.84.8 59 15-130ND
3-Nitroaniline mg/kg 3.2 IL4.8 65 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.94.8 81 15-132ND
4-Bromophenylphenyl ether mg/kg 1.52.5 61 35-130ND
4-Chloro-3-methylphenol mg/kg 3.94.8 80 30-130ND
4-Chloroaniline mg/kg 3.24.8 67 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.42.5 58 32-130ND
4-Nitroaniline mg/kg 3.34.8 68 30-130ND
4-Nitrophenol mg/kg 11.512.1 95 17-130ND
Acenaphthene mg/kg 1.32.5 54 29-130ND
Acenaphthylene mg/kg 1.42.5 56 31-130ND
Aniline mg/kg 1.52.5 62 10-130ND
Anthracene mg/kg 1.32.5 55 33-130ND
Benzo(a)anthracene mg/kg 1.42.5 59 32-130ND
Benzo(a)pyrene mg/kg 1.42.5 58 32-130ND
Benzo(b)fluoranthene mg/kg 1.42.5 59 33-130ND
Benzo(g,h,i)perylene mg/kg 1.32.5 54 28-130ND
Benzo(k)fluoranthene mg/kg 1.42.5 57 31-130ND
Benzoic Acid mg/kg 3.612.1 30 10-130ND
Benzyl alcohol mg/kg 3.44.8 70 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.72.5 71 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.82.5 73 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.6 v12.5 66 40-130ND
Butylbenzylphthalate mg/kg 1.5 v12.5 64 40-130ND
Chrysene mg/kg 1.32.5 55 30-130ND
Di-n-butylphthalate mg/kg 1.42.5 58 41-130ND
Di-n-octylphthalate mg/kg 1.62.5 66 42-130ND
Dibenz(a,h)anthracene mg/kg 1.42.5 60 27-130ND
Dibenzofuran mg/kg 1.32.5 56 32-130ND
Diethylphthalate mg/kg 1.62.5 67 40-130ND
Dimethylphthalate mg/kg 1.92.5 76 37-130ND
Fluoranthene mg/kg 1.42.5 56 26-130ND
Fluorene mg/kg 1.42.5 57 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.5 v12.5 61 20-130ND
Hexachlorobenzene mg/kg 1.52.5 60 29-130ND
Hexachlorocyclopentadiene mg/kg 1.12.5 44 10-130ND
Hexachloroethane mg/kg 1.42.5 58 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.42.5 57 28-130ND
Isophorone mg/kg 1.92.5 78 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.92.5 80 31-130ND
N-Nitrosodimethylamine mg/kg 1.62.5 66 20-130ND
N-Nitrosodiphenylamine mg/kg 1.52.5 62 32-130ND
Naphthalene mg/kg 1.52.5 60 30-130ND
Nitrobenzene mg/kg 2.02.5 83 25-130ND
Pentachlorophenol mg/kg 3.24.8 66 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3189612MATRIX SPIKE SAMPLE:
MSSpike
Result
92525841001
Phenanthrene mg/kg 1.32.5 55 34-130ND
Phenol mg/kg 1.82.5 74 14-130ND
Pyrene mg/kg 1.52.5 61 31-130ND
Pyridine mg/kg 1.22.5 51 10-130ND
2,4,6-Tribromophenol (S)%67 18-130
2-Fluorobiphenyl (S)%46 19-130
2-Fluorophenol (S)%67 18-130
Nitrobenzene-d5 (S)%78 21-130
Phenol-d6 (S)%66 18-130
Terphenyl-d14 (S)%70 15-130
Parameter Units
Dup
Result QualifiersRPDResult
92525841002
3189613SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg NDND
3-Nitroaniline mg/kg ND ILND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92525841002
3189613SAMPLE DUPLICATE:
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg ND v1ND
Butylbenzylphthalate mg/kg ND v1ND
Chrysene mg/kg NDND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg ND v1ND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg NDND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg NDND
Pyrene mg/kg NDND
Pyridine mg/kg NDND
2,4,6-Tribromophenol (S)%6263
2-Fluorobiphenyl (S)%4245
2-Fluorophenol (S)%6361
Nitrobenzene-d5 (S)%7471
Phenol-d6 (S)%6259
Terphenyl-d14 (S)%6770
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
605607
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92525998004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3190641
Associated Lab Samples:92525998004
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 03/11/21 12:02
1,2-Dichlorobenzene mg/kg ND 0.33 03/11/21 12:02
1,3-Dichlorobenzene mg/kg ND 0.33 03/11/21 12:02
1,4-Dichlorobenzene mg/kg ND 0.33 03/11/21 12:02
1-Methylnaphthalene mg/kg ND 0.33 03/11/21 12:02
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 03/11/21 12:02
2,4,5-Trichlorophenol mg/kg ND 0.33 03/11/21 12:02
2,4,6-Trichlorophenol mg/kg ND 0.33 03/11/21 12:02
2,4-Dichlorophenol mg/kg ND 0.33 03/11/21 12:02
2,4-Dimethylphenol mg/kg ND 0.33 03/11/21 12:02
2,4-Dinitrophenol mg/kg ND 1.7 03/11/21 12:02
2,4-Dinitrotoluene mg/kg ND 0.33 03/11/21 12:02
2,6-Dinitrotoluene mg/kg ND 0.33 03/11/21 12:02
2-Chloronaphthalene mg/kg ND 0.33 03/11/21 12:02
2-Chlorophenol mg/kg ND 0.33 03/11/21 12:02
2-Methylnaphthalene mg/kg ND 0.33 03/11/21 12:02
2-Methylphenol(o-Cresol)mg/kg ND 0.33 03/11/21 12:02
2-Nitroaniline mg/kg ND 1.7 03/11/21 12:02
2-Nitrophenol mg/kg ND 0.33 03/11/21 12:02
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 03/11/21 12:02
3,3'-Dichlorobenzidine mg/kg ND 0.66 IL03/11/21 12:02
3-Nitroaniline mg/kg ND 1.7 03/11/21 12:02
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 03/11/21 12:02
4-Bromophenylphenyl ether mg/kg ND 0.33 03/11/21 12:02
4-Chloro-3-methylphenol mg/kg ND 0.66 03/11/21 12:02
4-Chloroaniline mg/kg ND 0.66 03/11/21 12:02
4-Chlorophenylphenyl ether mg/kg ND 0.33 03/11/21 12:02
4-Nitroaniline mg/kg ND 0.66 03/11/21 12:02
4-Nitrophenol mg/kg ND 1.7 03/11/21 12:02
Acenaphthene mg/kg ND 0.33 03/11/21 12:02
Acenaphthylene mg/kg ND 0.33 03/11/21 12:02
Aniline mg/kg ND 0.33 03/11/21 12:02
Anthracene mg/kg ND 0.33 03/11/21 12:02
Benzo(a)anthracene mg/kg ND 0.33 03/11/21 12:02
Benzo(a)pyrene mg/kg ND 0.33 03/11/21 12:02
Benzo(b)fluoranthene mg/kg ND 0.33 03/11/21 12:02
Benzo(g,h,i)perylene mg/kg ND 0.33 03/11/21 12:02
Benzo(k)fluoranthene mg/kg ND 0.33 03/11/21 12:02
Benzoic Acid mg/kg ND 1.7 03/11/21 12:02
Benzyl alcohol mg/kg ND 0.66 03/11/21 12:02
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3190641
Associated Lab Samples:92525998004
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 03/11/21 12:02
bis(2-Chloroethyl) ether mg/kg ND 0.33 03/11/21 12:02
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 03/11/21 12:02
Butylbenzylphthalate mg/kg ND 0.33 03/11/21 12:02
Chrysene mg/kg ND 0.33 03/11/21 12:02
Di-n-butylphthalate mg/kg ND 0.33 03/11/21 12:02
Di-n-octylphthalate mg/kg ND 0.33 03/11/21 12:02
Dibenz(a,h)anthracene mg/kg ND 0.33 03/11/21 12:02
Dibenzofuran mg/kg ND 0.33 03/11/21 12:02
Diethylphthalate mg/kg ND 0.33 03/11/21 12:02
Dimethylphthalate mg/kg ND 0.33 03/11/21 12:02
Fluoranthene mg/kg ND 0.33 03/11/21 12:02
Fluorene mg/kg ND 0.33 03/11/21 12:02
Hexachloro-1,3-butadiene mg/kg ND 0.33 03/11/21 12:02
Hexachlorobenzene mg/kg ND 0.33 03/11/21 12:02
Hexachlorocyclopentadiene mg/kg ND 0.33 03/11/21 12:02
Hexachloroethane mg/kg ND 0.33 03/11/21 12:02
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 03/11/21 12:02
Isophorone mg/kg ND 0.33 03/11/21 12:02
N-Nitroso-di-n-propylamine mg/kg ND 0.33 03/11/21 12:02
N-Nitrosodimethylamine mg/kg ND 0.33 v103/11/21 12:02
N-Nitrosodiphenylamine mg/kg ND 0.33 03/11/21 12:02
Naphthalene mg/kg ND 0.33 03/11/21 12:02
Nitrobenzene mg/kg ND 0.33 03/11/21 12:02
Pentachlorophenol mg/kg ND 0.66 03/11/21 12:02
Phenanthrene mg/kg ND 0.33 03/11/21 12:02
Phenol mg/kg ND 0.33 v103/11/21 12:02
Pyrene mg/kg ND 0.33 03/11/21 12:02
Pyridine mg/kg ND 0.33 03/11/21 12:02
2,4,6-Tribromophenol (S)%68 18-130 03/11/21 12:02
2-Fluorobiphenyl (S)%62 19-130 03/11/21 12:02
2-Fluorophenol (S)%64 18-130 03/11/21 12:02
Nitrobenzene-d5 (S)%63 21-130 03/11/21 12:02
Phenol-d6 (S)%67 18-130 03/11/21 12:02
Terphenyl-d14 (S)%94 15-130 03/11/21 12:02
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3190642LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.31.7 81 47-130
1,2-Dichlorobenzene mg/kg 1.41.7 84 49-130
1,3-Dichlorobenzene mg/kg 1.31.7 81 48-130
1,4-Dichlorobenzene mg/kg 1.31.7 81 49-130
1-Methylnaphthalene mg/kg 1.31.7 80 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3190642LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 1.31.7 81 38-130
2,4,5-Trichlorophenol mg/kg 1.41.7 82 49-130
2,4,6-Trichlorophenol mg/kg 1.31.7 80 50-130
2,4-Dichlorophenol mg/kg 1.41.7 83 51-130
2,4-Dimethylphenol mg/kg 1.51.7 88 53-130
2,4-Dinitrophenol mg/kg 6.08.3 73 39-130
2,4-Dinitrotoluene mg/kg 1.41.7 85 53-130
2,6-Dinitrotoluene mg/kg 1.31.7 80 55-130
2-Chloronaphthalene mg/kg 1.31.7 77 48-130
2-Chlorophenol mg/kg 1.41.7 83 54-130
2-Methylnaphthalene mg/kg 1.31.7 79 57-130
2-Methylphenol(o-Cresol)mg/kg 1.51.7 88 50-130
2-Nitroaniline mg/kg 2.83.3 84 49-130
2-Nitrophenol mg/kg 1.41.7 86 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.51.7 89 50-130
3,3'-Dichlorobenzidine mg/kg 2.4 IL3.3 74 47-130
3-Nitroaniline mg/kg 2.33.3 69 45-130
4,6-Dinitro-2-methylphenol mg/kg 2.53.3 75 50-142
4-Bromophenylphenyl ether mg/kg 1.31.7 80 55-130
4-Chloro-3-methylphenol mg/kg 2.93.3 88 52-130
4-Chloroaniline mg/kg 2.43.3 72 49-130
4-Chlorophenylphenyl ether mg/kg 1.41.7 84 53-130
4-Nitroaniline mg/kg 2.73.3 81 51-130
4-Nitrophenol mg/kg 7.08.3 85 40-130
Acenaphthene mg/kg 1.41.7 82 56-130
Acenaphthylene mg/kg 1.31.7 81 58-130
Aniline mg/kg 1.21.7 75 44-130
Anthracene mg/kg 1.41.7 83 60-130
Benzo(a)anthracene mg/kg 1.41.7 87 59-130
Benzo(a)pyrene mg/kg 1.41.7 87 57-130
Benzo(b)fluoranthene mg/kg 1.41.7 86 54-130
Benzo(g,h,i)perylene mg/kg 1.41.7 82 59-130
Benzo(k)fluoranthene mg/kg 1.51.7 90 54-130
Benzoic Acid mg/kg 5.58.3 66 19-130
Benzyl alcohol mg/kg 2.93.3 88 50-130
bis(2-Chloroethoxy)methane mg/kg 1.31.7 79 55-130
bis(2-Chloroethyl) ether mg/kg 1.41.7 87 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.41.7 83 58-130
Butylbenzylphthalate mg/kg 1.41.7 83 46-138
Chrysene mg/kg 1.41.7 86 57-130
Di-n-butylphthalate mg/kg 1.31.7 79 57-130
Di-n-octylphthalate mg/kg 1.41.7 83 57-130
Dibenz(a,h)anthracene mg/kg 1.31.7 81 60-130
Dibenzofuran mg/kg 1.41.7 84 54-130
Diethylphthalate mg/kg 1.31.7 79 55-130
Dimethylphthalate mg/kg 1.31.7 78 57-130
Fluoranthene mg/kg 1.41.7 87 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3190642LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.41.7 84 56-130
Hexachloro-1,3-butadiene mg/kg 1.31.7 81 41-130
Hexachlorobenzene mg/kg 1.41.7 82 53-130
Hexachlorocyclopentadiene mg/kg 0.971.7 58 23-130
Hexachloroethane mg/kg 1.41.7 82 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.41.7 83 61-130
Isophorone mg/kg 1.31.7 79 49-130
N-Nitroso-di-n-propylamine mg/kg 1.51.7 88 52-130
N-Nitrosodimethylamine mg/kg 1.4 v11.7 83 45-130
N-Nitrosodiphenylamine mg/kg 1.31.7 78 56-130
Naphthalene mg/kg 1.31.7 79 56-130
Nitrobenzene mg/kg 1.31.7 81 50-130
Pentachlorophenol mg/kg 2.73.3 83 33-130
Phenanthrene mg/kg 1.41.7 84 60-130
Phenol mg/kg 1.6 v11.7 94 54-130
Pyrene mg/kg 1.51.7 88 61-130
Pyridine mg/kg 1.01.7 61 35-130
2,4,6-Tribromophenol (S)%80 18-130
2-Fluorobiphenyl (S)%73 19-130
2-Fluorophenol (S)%82 18-130
Nitrobenzene-d5 (S)%78 21-130
Phenol-d6 (S)%83 18-130
Terphenyl-d14 (S)%97 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3190643MATRIX SPIKE SAMPLE:
MSSpike
Result
92526696001
1,2,4-Trichlorobenzene mg/kg 1.51.9 81 22-130ND
1,2-Dichlorobenzene mg/kg 1.41.9 76 23-130ND
1,3-Dichlorobenzene mg/kg 1.51.9 77 26-130ND
1,4-Dichlorobenzene mg/kg 1.51.9 77 27-130ND
1-Methylnaphthalene mg/kg 1.51.9 77 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.51.9 76 30-130ND
2,4,5-Trichlorophenol mg/kg 1.61.9 82 26-130ND
2,4,6-Trichlorophenol mg/kg 1.51.9 78 23-130ND
2,4-Dichlorophenol mg/kg 1.61.9 85 29-130ND
2,4-Dimethylphenol mg/kg 1.71.9 87 13-130ND
2,4-Dinitrophenol mg/kg 7.49.6 77 10-131ND
2,4-Dinitrotoluene mg/kg 1.61.9 85 28-130ND
2,6-Dinitrotoluene mg/kg 1.51.9 81 36-130ND
2-Chloronaphthalene mg/kg 1.51.9 76 27-130ND
2-Chlorophenol mg/kg 1.51.9 78 29-130ND
2-Methylnaphthalene mg/kg 1.51.9 81 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.61.9 81 20-130ND
2-Nitroaniline mg/kg 3.23.8 83 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3190643MATRIX SPIKE SAMPLE:
MSSpike
Result
92526696001
2-Nitrophenol mg/kg 1.61.9 82 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.51.9 81 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.9 IL3.8 76 15-130ND
3-Nitroaniline mg/kg 2.93.8 76 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.13.8 80 15-132ND
4-Bromophenylphenyl ether mg/kg 1.51.9 79 35-130ND
4-Chloro-3-methylphenol mg/kg 3.23.8 85 30-130ND
4-Chloroaniline mg/kg 2.83.8 74 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.61.9 83 32-130ND
4-Nitroaniline mg/kg 3.23.8 83 30-130ND
4-Nitrophenol mg/kg 8.39.6 87 17-130ND
Acenaphthene mg/kg 1.51.9 78 29-130ND
Acenaphthylene mg/kg 1.51.9 79 31-130ND
Aniline mg/kg 1.31.9 67 10-130ND
Anthracene mg/kg 1.61.9 83 33-130ND
Benzo(a)anthracene mg/kg 1.61.9 86 32-130ND
Benzo(a)pyrene mg/kg 1.61.9 85 32-130ND
Benzo(b)fluoranthene mg/kg 1.71.9 86 33-130ND
Benzo(g,h,i)perylene mg/kg 1.51.9 80 28-130ND
Benzo(k)fluoranthene mg/kg 1.71.9 87 31-130ND
Benzoic Acid mg/kg 7.49.6 78 10-130ND
Benzyl alcohol mg/kg 3.13.8 81 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.51.9 80 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.61.9 82 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.61.9 85 40-130ND
Butylbenzylphthalate mg/kg 1.61.9 83 40-130ND
Chrysene mg/kg 1.61.9 84 30-130ND
Di-n-butylphthalate mg/kg 1.51.9 80 41-130ND
Di-n-octylphthalate mg/kg 1.61.9 85 42-130ND
Dibenz(a,h)anthracene mg/kg 1.61.9 82 27-130ND
Dibenzofuran mg/kg 1.61.9 82 32-130ND
Diethylphthalate mg/kg 1.51.9 80 40-130ND
Dimethylphthalate mg/kg 1.51.9 79 37-130ND
Fluoranthene mg/kg 1.71.9 87 26-130ND
Fluorene mg/kg 1.61.9 83 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.51.9 77 20-130ND
Hexachlorobenzene mg/kg 1.51.9 80 29-130ND
Hexachlorocyclopentadiene mg/kg 1.11.9 59 10-130ND
Hexachloroethane mg/kg 1.51.9 77 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.51.9 80 28-130ND
Isophorone mg/kg 1.51.9 80 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.61.9 82 31-130ND
N-Nitrosodimethylamine mg/kg 1.5 v11.9 76 20-130ND
N-Nitrosodiphenylamine mg/kg 1.51.9 79 32-130ND
Naphthalene mg/kg 1.51.9 79 30-130ND
Nitrobenzene mg/kg 1.51.9 79 25-130ND
Pentachlorophenol mg/kg 3.13.8 82 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3190643MATRIX SPIKE SAMPLE:
MSSpike
Result
92526696001
Phenanthrene mg/kg 1.61.9 85 34-130ND
Phenol mg/kg 1.7 v11.9 87 14-130ND
Pyrene mg/kg 1.71.9 87 31-130ND
Pyridine mg/kg 1.11.9 56 10-130ND
2,4,6-Tribromophenol (S)%78 18-130
2-Fluorobiphenyl (S)%68 19-130
2-Fluorophenol (S)%73 18-130
Nitrobenzene-d5 (S)%75 21-130
Phenol-d6 (S)%74 18-130
Terphenyl-d14 (S)%87 15-130
Parameter Units
Dup
Result QualifiersRPDResult
92526696002
3190644SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg ND ILND
3-Nitroaniline mg/kg NDND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
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[phone]
Page 28 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92526696002
3190644SAMPLE DUPLICATE:
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg NDND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg NDND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg ND v1ND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg ND v1ND
Pyrene mg/kg NDND
Pyridine mg/kg NDND
2,4,6-Tribromophenol (S)%4850
2-Fluorobiphenyl (S)%5451
2-Fluorophenol (S)%5151
Nitrobenzene-d5 (S)%6761
Phenol-d6 (S)%5757
Terphenyl-d14 (S)%7971
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
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[phone]
Page 29 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
604923
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92525998001, 92525998002, 92525998003, 92525998004
Parameter Units
Dup
Result QualifiersRPDResult
92525424001
3187240SAMPLE DUPLICATE:
Percent Moisture %93.3 N2092.9
Parameter Units
Dup
Result QualifiersRPDResult
50281181001
3187241SAMPLE DUPLICATE:
Percent Moisture %12.0 N2311.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 36
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92525998
Northstate 12119-B
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
604938
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92525998005, 92525998006
Parameter Units
Dup
Result QualifiersRPDResult
92526045001
3187286SAMPLE DUPLICATE:
Percent Moisture %17.9 N21116.0
Parameter Units
Dup
Result QualifiersRPDResult
20192495002
3187287SAMPLE DUPLICATE:
Percent Moisture %95.9 N2095.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
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[phone]
Page 31 of 36
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92525998
Northstate 12119-B
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
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Page 32 of 36
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92525998
Northstate 12119-B
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92525998001 605438 605502SS-1 EPA 3546 EPA 8270E
92525998002 605438 605502SS-2 EPA 3546 EPA 8270E
92525998003 605438 605502SS-3 EPA 3546 EPA 8270E
92525998004 605607 605910SS-4 EPA 3546 EPA 8270E
92525998005 605438 605502SS-5 EPA 3546 EPA 8270E
92525998006 605438 605502SS-6 EPA 3546 EPA 8270E
92525998001 604923SS-1 SW-846
92525998002 604923SS-2 SW-846
92525998003 604923SS-3 SW-846
92525998004 604923SS-4 SW-846
92525998005 604938SS-5 SW-846
92525998006 604938SS-6 SW-846
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 03/12/2021 08:47 AM
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Page 33 of 36
Page 34 of 36
Page 35 of 36
Page 36 of 36
#=CL#
April 23, 2021
LIMS USE: FR - RANDY CAVALLIER
LIMS OBJECT ID: 92533750
92533750
Project:
Pace Project No.:
RE:
Mr. Randy Cavallier
ECS Southeast, LLP
4811 Koger Blvd.
Greensboro, NC 27407
Northstate
Dear Mr. Cavallier:
Enclosed are the analytical results for sample(s) received by the laboratory on April 16, 2021. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
[phone]
Enclosures
cc:ECS Southeast Reporting, ECS Southeast
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92533750
Northstate
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 2 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92533750
Northstate
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92533750001 SS-Base EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
92533750002 SS-SW EPA 8270E 75 PASI-CBPJ
SW-846 1 PASI-CKDF
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 3 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92533750
Northstate
Sample:SS-Base Lab ID:92533750001 Collected:04/15/21 10:00 Received:04/16/21 09:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 04/22/21 13:40 83-32-904/21/21 13:400.38 1
Acenaphthylene ND mg/kg 04/22/21 13:40 208-96-804/21/21 13:400.38 1
Aniline ND mg/kg 04/22/21 13:40 62-53-304/21/21 13:400.38 1
Anthracene ND mg/kg 04/22/21 13:40 120-12-704/21/21 13:400.38 1
Benzo(a)anthracene ND mg/kg 04/22/21 13:40 56-55-304/21/21 13:400.38 1
Benzo(a)pyrene ND mg/kg 04/22/21 13:40 50-32-804/21/21 13:400.38 1
Benzo(b)fluoranthene ND mg/kg 04/22/21 13:40 205-99-204/21/21 13:400.38 1
Benzo(g,h,i)perylene ND mg/kg 04/22/21 13:40 191-24-204/21/21 13:400.38 1
Benzo(k)fluoranthene ND mg/kg 04/22/21 13:40 207-08-904/21/21 13:400.38 1
Benzoic Acid ND mg/kg 04/22/21 13:40 65-85-004/21/21 13:401.9 1
Benzyl alcohol ND mg/kg 04/22/21 13:40 100-51-604/21/21 13:400.76 1
4-Bromophenylphenyl ether ND mg/kg 04/22/21 13:40 101-55-304/21/21 13:400.38 1
Butylbenzylphthalate ND mg/kg 04/22/21 13:40 85-68-704/21/21 13:400.38 1
4-Chloro-3-methylphenol ND mg/kg 04/22/21 13:40 59-50-704/21/21 13:400.76 1
4-Chloroaniline ND mg/kg 04/22/21 13:40 106-47-804/21/21 13:400.76 1
bis(2-Chloroethoxy)methane ND mg/kg 04/22/21 13:40 111-91-104/21/21 13:400.38 1
bis(2-Chloroethyl) ether ND mg/kg 04/22/21 13:40 111-44-404/21/21 13:400.38 1
2-Chloronaphthalene ND mg/kg 04/22/21 13:40 91-58-704/21/21 13:400.38 1
2-Chlorophenol ND mg/kg 04/22/21 13:40 95-57-804/21/21 13:400.38 1
4-Chlorophenylphenyl ether ND mg/kg 04/22/21 13:40 7005-72-304/21/21 13:400.38 1
Chrysene ND mg/kg 04/22/21 13:40 218-01-904/21/21 13:400.38 1
Dibenz(a,h)anthracene ND mg/kg 04/22/21 13:40 53-70-304/21/21 13:400.38 1
Dibenzofuran ND mg/kg 04/22/21 13:40 132-64-904/21/21 13:400.38 1
1,2-Dichlorobenzene ND mg/kg 04/22/21 13:40 95-50-104/21/21 13:400.38 1
1,3-Dichlorobenzene ND mg/kg 04/22/21 13:40 541-73-104/21/21 13:400.38 1
1,4-Dichlorobenzene ND mg/kg 04/22/21 13:40 106-46-704/21/21 13:400.38 1
3,3'-Dichlorobenzidine ND mg/kg 04/22/21 13:40 91-94-1 IL04/21/21 13:400.76 1
2,4-Dichlorophenol ND mg/kg 04/22/21 13:40 120-83-204/21/21 13:400.38 1
Diethylphthalate ND mg/kg 04/22/21 13:40 84-66-204/21/21 13:400.38 1
2,4-Dimethylphenol ND mg/kg 04/22/21 13:40 105-67-904/21/21 13:400.38 1
Dimethylphthalate ND mg/kg 04/22/21 13:40 131-11-304/21/21 13:400.38 1
Di-n-butylphthalate ND mg/kg 04/22/21 13:40 84-74-204/21/21 13:400.38 1
4,6-Dinitro-2-methylphenol ND mg/kg 04/22/21 13:40 534-52-104/21/21 13:400.76 1
2,4-Dinitrophenol ND mg/kg 04/22/21 13:40 51-28-504/21/21 13:401.9 1
2,4-Dinitrotoluene ND mg/kg 04/22/21 13:40 121-14-204/21/21 13:400.38 1
2,6-Dinitrotoluene ND mg/kg 04/22/21 13:40 606-20-204/21/21 13:400.38 1
Di-n-octylphthalate ND mg/kg 04/22/21 13:40 117-84-004/21/21 13:400.38 1
bis(2-Ethylhexyl)phthalate ND mg/kg 04/22/21 13:40 117-81-704/21/21 13:400.38 1
Fluoranthene ND mg/kg 04/22/21 13:40 206-44-004/21/21 13:400.38 1
Fluorene ND mg/kg 04/22/21 13:40 86-73-704/21/21 13:400.38 1
Hexachloro-1,3-butadiene ND mg/kg 04/22/21 13:40 87-68-304/21/21 13:400.38 1
Hexachlorobenzene ND mg/kg 04/22/21 13:40 118-74-104/21/21 13:400.38 1
Hexachlorocyclopentadiene ND mg/kg 04/22/21 13:40 77-47-404/21/21 13:400.38 1
Hexachloroethane ND mg/kg 04/22/21 13:40 67-72-104/21/21 13:400.38 1
Indeno(1,2,3-cd)pyrene ND mg/kg 04/22/21 13:40 193-39-504/21/21 13:400.38 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
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Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92533750
Northstate
Sample:SS-Base Lab ID:92533750001 Collected:04/15/21 10:00 Received:04/16/21 09:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Isophorone ND mg/kg 04/22/21 13:40 78-59-104/21/21 13:400.38 1
1-Methylnaphthalene ND mg/kg 04/22/21 13:40 90-12-004/21/21 13:400.38 1
2-Methylnaphthalene ND mg/kg 04/22/21 13:40 91-57-604/21/21 13:400.38 1
2-Methylphenol(o-Cresol)ND mg/kg 04/22/21 13:40 95-48-704/21/21 13:400.38 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 04/22/21 13:40 15831-10-404/21/21 13:400.38 1
Naphthalene ND mg/kg 04/22/21 13:40 91-20-304/21/21 13:400.38 1
2-Nitroaniline ND mg/kg 04/22/21 13:40 88-74-404/21/21 13:401.9 1
3-Nitroaniline ND mg/kg 04/22/21 13:40 99-09-204/21/21 13:401.9 1
4-Nitroaniline ND mg/kg 04/22/21 13:40 100-01-604/21/21 13:400.76 1
Nitrobenzene ND mg/kg 04/22/21 13:40 98-95-304/21/21 13:400.38 1
2-Nitrophenol ND mg/kg 04/22/21 13:40 88-75-504/21/21 13:400.38 1
4-Nitrophenol ND mg/kg 04/22/21 13:40 100-02-704/21/21 13:401.9 1
N-Nitrosodimethylamine ND mg/kg 04/22/21 13:40 62-75-904/21/21 13:400.38 1
N-Nitroso-di-n-propylamine ND mg/kg 04/22/21 13:40 621-64-704/21/21 13:400.38 1
N-Nitrosodiphenylamine ND mg/kg 04/22/21 13:40 86-30-604/21/21 13:400.38 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 04/22/21 13:40 108-60-104/21/21 13:400.38 1
Pentachlorophenol ND mg/kg 04/22/21 13:40 87-86-504/21/21 13:400.76 1
Phenanthrene ND mg/kg 04/22/21 13:40 85-01-804/21/21 13:400.38 1
Phenol ND mg/kg 04/22/21 13:40 108-95-204/21/21 13:400.38 1
Pyrene ND mg/kg 04/22/21 13:40 129-00-004/21/21 13:400.38 1
Pyridine ND mg/kg 04/22/21 13:40 110-86-104/21/21 13:400.38 1
1,2,4-Trichlorobenzene ND mg/kg 04/22/21 13:40 120-82-104/21/21 13:400.38 1
2,4,5-Trichlorophenol ND mg/kg 04/22/21 13:40 95-95-404/21/21 13:400.38 1
2,4,6-Trichlorophenol ND mg/kg 04/22/21 13:40 88-06-204/21/21 13:400.38 1
Surrogates
Nitrobenzene-d5 (S)72 %04/22/21 13:40 4165-60-004/21/21 13:4021-130 1
2-Fluorobiphenyl (S)68 %04/22/21 13:40 321-60-804/21/21 13:4019-130 1
Terphenyl-d14 (S)65 %04/22/21 13:40 1718-51-004/21/21 13:4015-130 1
Phenol-d6 (S)66 %04/22/21 13:40 13127-88-304/21/21 13:4018-130 1
2-Fluorophenol (S)63 %04/22/21 13:40 367-12-404/21/21 13:4018-130 1
2,4,6-Tribromophenol (S)73 %04/22/21 13:40 118-79-604/21/21 13:4018-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 13.8 %04/16/21 17:52 N20.10 1
Sample:SS-SW Lab ID:92533750002 Collected:04/15/21 11:00 Received:04/16/21 09:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthene ND mg/kg 04/22/21 14:41 83-32-904/21/21 13:400.36 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
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Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92533750
Northstate
Sample:SS-SW Lab ID:92533750002 Collected:04/15/21 11:00 Received:04/16/21 09:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
Acenaphthylene ND mg/kg 04/22/21 14:41 208-96-804/21/21 13:400.36 1
Aniline ND mg/kg 04/22/21 14:41 62-53-304/21/21 13:400.36 1
Anthracene ND mg/kg 04/22/21 14:41 120-12-704/21/21 13:400.36 1
Benzo(a)anthracene ND mg/kg 04/22/21 14:41 56-55-304/21/21 13:400.36 1
Benzo(a)pyrene ND mg/kg 04/22/21 14:41 50-32-804/21/21 13:400.36 1
Benzo(b)fluoranthene ND mg/kg 04/22/21 14:41 205-99-204/21/21 13:400.36 1
Benzo(g,h,i)perylene ND mg/kg 04/22/21 14:41 191-24-204/21/21 13:400.36 1
Benzo(k)fluoranthene ND mg/kg 04/22/21 14:41 207-08-904/21/21 13:400.36 1
Benzoic Acid ND mg/kg 04/22/21 14:41 65-85-004/21/21 13:401.8 1
Benzyl alcohol ND mg/kg 04/22/21 14:41 100-51-604/21/21 13:400.72 1
4-Bromophenylphenyl ether ND mg/kg 04/22/21 14:41 101-55-304/21/21 13:400.36 1
Butylbenzylphthalate ND mg/kg 04/22/21 14:41 85-68-704/21/21 13:400.36 1
4-Chloro-3-methylphenol ND mg/kg 04/22/21 14:41 59-50-704/21/21 13:400.72 1
4-Chloroaniline ND mg/kg 04/22/21 14:41 106-47-804/21/21 13:400.72 1
bis(2-Chloroethoxy)methane ND mg/kg 04/22/21 14:41 111-91-104/21/21 13:400.36 1
bis(2-Chloroethyl) ether ND mg/kg 04/22/21 14:41 111-44-404/21/21 13:400.36 1
2-Chloronaphthalene ND mg/kg 04/22/21 14:41 91-58-704/21/21 13:400.36 1
2-Chlorophenol ND mg/kg 04/22/21 14:41 95-57-804/21/21 13:400.36 1
4-Chlorophenylphenyl ether ND mg/kg 04/22/21 14:41 7005-72-304/21/21 13:400.36 1
Chrysene ND mg/kg 04/22/21 14:41 218-01-904/21/21 13:400.36 1
Dibenz(a,h)anthracene ND mg/kg 04/22/21 14:41 53-70-304/21/21 13:400.36 1
Dibenzofuran ND mg/kg 04/22/21 14:41 132-64-904/21/21 13:400.36 1
1,2-Dichlorobenzene ND mg/kg 04/22/21 14:41 95-50-104/21/21 13:400.36 1
1,3-Dichlorobenzene ND mg/kg 04/22/21 14:41 541-73-104/21/21 13:400.36 1
1,4-Dichlorobenzene ND mg/kg 04/22/21 14:41 106-46-704/21/21 13:400.36 1
3,3'-Dichlorobenzidine ND mg/kg 04/22/21 14:41 91-94-1 IL04/21/21 13:400.72 1
2,4-Dichlorophenol ND mg/kg 04/22/21 14:41 120-83-204/21/21 13:400.36 1
Diethylphthalate ND mg/kg 04/22/21 14:41 84-66-204/21/21 13:400.36 1
2,4-Dimethylphenol ND mg/kg 04/22/21 14:41 105-67-904/21/21 13:400.36 1
Dimethylphthalate ND mg/kg 04/22/21 14:41 131-11-304/21/21 13:400.36 1
Di-n-butylphthalate ND mg/kg 04/22/21 14:41 84-74-204/21/21 13:400.36 1
4,6-Dinitro-2-methylphenol ND mg/kg 04/22/21 14:41 534-52-104/21/21 13:400.72 1
2,4-Dinitrophenol ND mg/kg 04/22/21 14:41 51-28-504/21/21 13:401.8 1
2,4-Dinitrotoluene ND mg/kg 04/22/21 14:41 121-14-204/21/21 13:400.36 1
2,6-Dinitrotoluene ND mg/kg 04/22/21 14:41 606-20-204/21/21 13:400.36 1
Di-n-octylphthalate ND mg/kg 04/22/21 14:41 117-84-004/21/21 13:400.36 1
bis(2-Ethylhexyl)phthalate ND mg/kg 04/22/21 14:41 117-81-704/21/21 13:400.36 1
Fluoranthene 0.44 mg/kg 04/22/21 14:41 206-44-004/21/21 13:400.36 1
Fluorene ND mg/kg 04/22/21 14:41 86-73-704/21/21 13:400.36 1
Hexachloro-1,3-butadiene ND mg/kg 04/22/21 14:41 87-68-304/21/21 13:400.36 1
Hexachlorobenzene ND mg/kg 04/22/21 14:41 118-74-104/21/21 13:400.36 1
Hexachlorocyclopentadiene ND mg/kg 04/22/21 14:41 77-47-404/21/21 13:400.36 1
Hexachloroethane ND mg/kg 04/22/21 14:41 67-72-104/21/21 13:400.36 1
Indeno(1,2,3-cd)pyrene ND mg/kg 04/22/21 14:41 193-39-504/21/21 13:400.36 1
Isophorone ND mg/kg 04/22/21 14:41 78-59-104/21/21 13:400.36 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92533750
Northstate
Sample:SS-SW Lab ID:92533750002 Collected:04/15/21 11:00 Received:04/16/21 09:49 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Pace Analytical Services - Charlotte
8270E MSSV Microwave
1-Methylnaphthalene ND mg/kg 04/22/21 14:41 90-12-004/21/21 13:400.36 1
2-Methylnaphthalene ND mg/kg 04/22/21 14:41 91-57-604/21/21 13:400.36 1
2-Methylphenol(o-Cresol)ND mg/kg 04/22/21 14:41 95-48-704/21/21 13:400.36 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 04/22/21 14:41 15831-10-404/21/21 13:400.36 1
Naphthalene ND mg/kg 04/22/21 14:41 91-20-304/21/21 13:400.36 1
2-Nitroaniline ND mg/kg 04/22/21 14:41 88-74-404/21/21 13:401.8 1
3-Nitroaniline ND mg/kg 04/22/21 14:41 99-09-204/21/21 13:401.8 1
4-Nitroaniline ND mg/kg 04/22/21 14:41 100-01-604/21/21 13:400.72 1
Nitrobenzene ND mg/kg 04/22/21 14:41 98-95-304/21/21 13:400.36 1
2-Nitrophenol ND mg/kg 04/22/21 14:41 88-75-504/21/21 13:400.36 1
4-Nitrophenol ND mg/kg 04/22/21 14:41 100-02-704/21/21 13:401.8 1
N-Nitrosodimethylamine ND mg/kg 04/22/21 14:41 62-75-904/21/21 13:400.36 1
N-Nitroso-di-n-propylamine ND mg/kg 04/22/21 14:41 621-64-704/21/21 13:400.36 1
N-Nitrosodiphenylamine ND mg/kg 04/22/21 14:41 86-30-604/21/21 13:400.36 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 04/22/21 14:41 108-60-104/21/21 13:400.36 1
Pentachlorophenol ND mg/kg 04/22/21 14:41 87-86-504/21/21 13:400.72 1
Phenanthrene ND mg/kg 04/22/21 14:41 85-01-804/21/21 13:400.36 1
Phenol ND mg/kg 04/22/21 14:41 108-95-204/21/21 13:400.36 1
Pyrene ND mg/kg 04/22/21 14:41 129-00-004/21/21 13:400.36 1
Pyridine ND mg/kg 04/22/21 14:41 110-86-104/21/21 13:400.36 1
1,2,4-Trichlorobenzene ND mg/kg 04/22/21 14:41 120-82-104/21/21 13:400.36 1
2,4,5-Trichlorophenol ND mg/kg 04/22/21 14:41 95-95-404/21/21 13:400.36 1
2,4,6-Trichlorophenol ND mg/kg 04/22/21 14:41 88-06-204/21/21 13:400.36 1
Surrogates
Nitrobenzene-d5 (S)69 %04/22/21 14:41 4165-60-004/21/21 13:4021-130 1
2-Fluorobiphenyl (S)66 %04/22/21 14:41 321-60-804/21/21 13:4019-130 1
Terphenyl-d14 (S)65 %04/22/21 14:41 1718-51-004/21/21 13:4015-130 1
Phenol-d6 (S)61 %04/22/21 14:41 13127-88-304/21/21 13:4018-130 1
2-Fluorophenol (S)55 %04/22/21 14:41 367-12-404/21/21 13:4018-130 1
2,4,6-Tribromophenol (S)77 %04/22/21 14:41 118-79-604/21/21 13:4018-130 1
Analytical Method: SW-846
Pace Analytical Services - Charlotte
Percent Moisture
Percent Moisture 7.9 %04/16/21 17:52 N20.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
615138
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92533750001, 92533750002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3237100
Associated Lab Samples:92533750001, 92533750002
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 04/22/21 10:08
1,2-Dichlorobenzene mg/kg ND 0.33 04/22/21 10:08
1,3-Dichlorobenzene mg/kg ND 0.33 04/22/21 10:08
1,4-Dichlorobenzene mg/kg ND 0.33 04/22/21 10:08
1-Methylnaphthalene mg/kg ND 0.33 04/22/21 10:08
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 04/22/21 10:08
2,4,5-Trichlorophenol mg/kg ND 0.33 04/22/21 10:08
2,4,6-Trichlorophenol mg/kg ND 0.33 04/22/21 10:08
2,4-Dichlorophenol mg/kg ND 0.33 04/22/21 10:08
2,4-Dimethylphenol mg/kg ND 0.33 04/22/21 10:08
2,4-Dinitrophenol mg/kg ND 1.6 04/22/21 10:08
2,4-Dinitrotoluene mg/kg ND 0.33 04/22/21 10:08
2,6-Dinitrotoluene mg/kg ND 0.33 04/22/21 10:08
2-Chloronaphthalene mg/kg ND 0.33 04/22/21 10:08
2-Chlorophenol mg/kg ND 0.33 04/22/21 10:08
2-Methylnaphthalene mg/kg ND 0.33 04/22/21 10:08
2-Methylphenol(o-Cresol)mg/kg ND 0.33 04/22/21 10:08
2-Nitroaniline mg/kg ND 1.6 04/22/21 10:08
2-Nitrophenol mg/kg ND 0.33 04/22/21 10:08
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 04/22/21 10:08
3,3'-Dichlorobenzidine mg/kg ND 0.66 IL04/22/21 10:08
3-Nitroaniline mg/kg ND 1.6 04/22/21 10:08
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 04/22/21 10:08
4-Bromophenylphenyl ether mg/kg ND 0.33 04/22/21 10:08
4-Chloro-3-methylphenol mg/kg ND 0.66 04/22/21 10:08
4-Chloroaniline mg/kg ND 0.66 04/22/21 10:08
4-Chlorophenylphenyl ether mg/kg ND 0.33 04/22/21 10:08
4-Nitroaniline mg/kg ND 0.66 04/22/21 10:08
4-Nitrophenol mg/kg ND 1.6 04/22/21 10:08
Acenaphthene mg/kg ND 0.33 04/22/21 10:08
Acenaphthylene mg/kg ND 0.33 04/22/21 10:08
Aniline mg/kg ND 0.33 04/22/21 10:08
Anthracene mg/kg ND 0.33 04/22/21 10:08
Benzo(a)anthracene mg/kg ND 0.33 04/22/21 10:08
Benzo(a)pyrene mg/kg ND 0.33 04/22/21 10:08
Benzo(b)fluoranthene mg/kg ND 0.33 04/22/21 10:08
Benzo(g,h,i)perylene mg/kg ND 0.33 04/22/21 10:08
Benzo(k)fluoranthene mg/kg ND 0.33 04/22/21 10:08
Benzoic Acid mg/kg ND 1.6 04/22/21 10:08
Benzyl alcohol mg/kg ND 0.66 04/22/21 10:08
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:3237100
Associated Lab Samples:92533750001, 92533750002
Matrix:Solid
Analyzed
bis(2-Chloroethoxy)methane mg/kg ND 0.33 04/22/21 10:08
bis(2-Chloroethyl) ether mg/kg ND 0.33 04/22/21 10:08
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 04/22/21 10:08
Butylbenzylphthalate mg/kg ND 0.33 04/22/21 10:08
Chrysene mg/kg ND 0.33 04/22/21 10:08
Di-n-butylphthalate mg/kg ND 0.33 04/22/21 10:08
Di-n-octylphthalate mg/kg ND 0.33 04/22/21 10:08
Dibenz(a,h)anthracene mg/kg ND 0.33 04/22/21 10:08
Dibenzofuran mg/kg ND 0.33 04/22/21 10:08
Diethylphthalate mg/kg ND 0.33 04/22/21 10:08
Dimethylphthalate mg/kg ND 0.33 04/22/21 10:08
Fluoranthene mg/kg ND 0.33 04/22/21 10:08
Fluorene mg/kg ND 0.33 04/22/21 10:08
Hexachloro-1,3-butadiene mg/kg ND 0.33 04/22/21 10:08
Hexachlorobenzene mg/kg ND 0.33 04/22/21 10:08
Hexachlorocyclopentadiene mg/kg ND 0.33 04/22/21 10:08
Hexachloroethane mg/kg ND 0.33 04/22/21 10:08
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 04/22/21 10:08
Isophorone mg/kg ND 0.33 04/22/21 10:08
N-Nitroso-di-n-propylamine mg/kg ND 0.33 04/22/21 10:08
N-Nitrosodimethylamine mg/kg ND 0.33 04/22/21 10:08
N-Nitrosodiphenylamine mg/kg ND 0.33 04/22/21 10:08
Naphthalene mg/kg ND 0.33 04/22/21 10:08
Nitrobenzene mg/kg ND 0.33 04/22/21 10:08
Pentachlorophenol mg/kg ND 0.66 04/22/21 10:08
Phenanthrene mg/kg ND 0.33 04/22/21 10:08
Phenol mg/kg ND 0.33 04/22/21 10:08
Pyrene mg/kg ND 0.33 04/22/21 10:08
Pyridine mg/kg ND 0.33 04/22/21 10:08
2,4,6-Tribromophenol (S)%88 18-130 04/22/21 10:08
2-Fluorobiphenyl (S)%79 19-130 04/22/21 10:08
2-Fluorophenol (S)%74 18-130 04/22/21 10:08
Nitrobenzene-d5 (S)%81 21-130 04/22/21 10:08
Phenol-d6 (S)%76 18-130 04/22/21 10:08
Terphenyl-d14 (S)%84 15-130 04/22/21 10:08
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3237101LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.11.7 66 47-130
1,2-Dichlorobenzene mg/kg 1.01.7 62 49-130
1,3-Dichlorobenzene mg/kg 0.961.7 58 48-130
1,4-Dichlorobenzene mg/kg 1.01.7 61 49-130
1-Methylnaphthalene mg/kg 1.21.7 75 54-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3237101LABORATORY CONTROL SAMPLE:
LCSSpike
2,2'-Oxybis(1-chloropropane)mg/kg 0.901.7 54 38-130
2,4,5-Trichlorophenol mg/kg 1.41.7 84 49-130
2,4,6-Trichlorophenol mg/kg 1.41.7 86 50-130
2,4-Dichlorophenol mg/kg 1.21.7 73 51-130
2,4-Dimethylphenol mg/kg 1.41.7 82 53-130
2,4-Dinitrophenol mg/kg 7.98.3 96 39-130
2,4-Dinitrotoluene mg/kg 1.51.7 91 53-130
2,6-Dinitrotoluene mg/kg 1.41.7 86 55-130
2-Chloronaphthalene mg/kg 1.31.7 77 48-130
2-Chlorophenol mg/kg 1.01.7 61 54-130
2-Methylnaphthalene mg/kg 1.21.7 74 57-130
2-Methylphenol(o-Cresol)mg/kg 1.11.7 66 50-130
2-Nitroaniline mg/kg 2.83.3 84 49-130
2-Nitrophenol mg/kg 1.21.7 70 50-130
3&4-Methylphenol(m&p Cresol)mg/kg 1.21.7 70 50-130
3,3'-Dichlorobenzidine mg/kg 2.5 IL3.3 75 47-130
3-Nitroaniline mg/kg 2.63.3 78 45-130
4,6-Dinitro-2-methylphenol mg/kg 3.23.3 96 50-142
4-Bromophenylphenyl ether mg/kg 1.51.7 89 55-130
4-Chloro-3-methylphenol mg/kg 2.93.3 86 52-130
4-Chloroaniline mg/kg 2.43.3 72 49-130
4-Chlorophenylphenyl ether mg/kg 1.51.7 93 53-130
4-Nitroaniline mg/kg 2.83.3 84 51-130
4-Nitrophenol mg/kg 7.88.3 94 40-130
Acenaphthene mg/kg 1.41.7 85 56-130
Acenaphthylene mg/kg 1.41.7 85 58-130
Aniline mg/kg 1.01.7 62 44-130
Anthracene mg/kg 1.51.7 88 60-130
Benzo(a)anthracene mg/kg 1.51.7 92 59-130
Benzo(a)pyrene mg/kg 1.61.7 95 57-130
Benzo(b)fluoranthene mg/kg 1.61.7 93 54-130
Benzo(g,h,i)perylene mg/kg 1.51.7 93 59-130
Benzo(k)fluoranthene mg/kg 1.61.7 98 54-130
Benzoic Acid mg/kg 5.08.3 60 19-130
Benzyl alcohol mg/kg 2.33.3 68 50-130
bis(2-Chloroethoxy)methane mg/kg 1.21.7 71 55-130
bis(2-Chloroethyl) ether mg/kg 1.11.7 67 53-130
bis(2-Ethylhexyl)phthalate mg/kg 1.51.7 89 58-130
Butylbenzylphthalate mg/kg 1.51.7 90 46-138
Chrysene mg/kg 1.51.7 92 57-130
Di-n-butylphthalate mg/kg 1.41.7 87 57-130
Di-n-octylphthalate mg/kg 1.51.7 90 57-130
Dibenz(a,h)anthracene mg/kg 1.51.7 92 60-130
Dibenzofuran mg/kg 1.41.7 87 54-130
Diethylphthalate mg/kg 1.51.7 92 55-130
Dimethylphthalate mg/kg 1.51.7 91 57-130
Fluoranthene mg/kg 1.51.7 92 57-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
3237101LABORATORY CONTROL SAMPLE:
LCSSpike
Fluorene mg/kg 1.51.7 88 56-130
Hexachloro-1,3-butadiene mg/kg 1.21.7 70 41-130
Hexachlorobenzene mg/kg 1.51.7 92 53-130
Hexachlorocyclopentadiene mg/kg 1.11.7 68 23-130
Hexachloroethane mg/kg 0.991.7 60 48-130
Indeno(1,2,3-cd)pyrene mg/kg 1.61.7 96 61-130
Isophorone mg/kg 1.31.7 78 49-130
N-Nitroso-di-n-propylamine mg/kg 1.21.7 73 52-130
N-Nitrosodimethylamine mg/kg 0.991.7 60 45-130
N-Nitrosodiphenylamine mg/kg 1.51.7 90 56-130
Naphthalene mg/kg 1.11.7 68 56-130
Nitrobenzene mg/kg 1.11.7 66 50-130
Pentachlorophenol mg/kg 2.93.3 86 33-130
Phenanthrene mg/kg 1.51.7 89 60-130
Phenol mg/kg 1.21.7 71 54-130
Pyrene mg/kg 1.61.7 94 61-130
Pyridine mg/kg 0.751.7 45 35-130
2,4,6-Tribromophenol (S)%97 18-130
2-Fluorobiphenyl (S)%79 19-130
2-Fluorophenol (S)%63 18-130
Nitrobenzene-d5 (S)%71 21-130
Phenol-d6 (S)%66 18-130
Terphenyl-d14 (S)%81 15-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3237102MATRIX SPIKE SAMPLE:
MSSpike
Result
92533750001
1,2,4-Trichlorobenzene mg/kg 1.42 72 22-130ND
1,2-Dichlorobenzene mg/kg 1.32 69 23-130ND
1,3-Dichlorobenzene mg/kg 1.32 67 26-130ND
1,4-Dichlorobenzene mg/kg 1.32 69 27-130ND
1-Methylnaphthalene mg/kg 1.42 74 30-130ND
2,2'-Oxybis(1-chloropropane)mg/kg 1.32 65 30-130ND
2,4,5-Trichlorophenol mg/kg 1.52 77 26-130ND
2,4,6-Trichlorophenol mg/kg 1.52 77 23-130ND
2,4-Dichlorophenol mg/kg 1.52 78 29-130ND
2,4-Dimethylphenol mg/kg 1.42 70 13-130ND
2,4-Dinitrophenol mg/kg 7.99.7 81 10-131ND
2,4-Dinitrotoluene mg/kg 1.62 82 28-130ND
2,6-Dinitrotoluene mg/kg 1.52 79 36-130ND
2-Chloronaphthalene mg/kg 1.42 73 27-130ND
2-Chlorophenol mg/kg 1.42 70 29-130ND
2-Methylnaphthalene mg/kg 1.42 74 29-130ND
2-Methylphenol(o-Cresol)mg/kg 1.32 68 20-130ND
2-Nitroaniline mg/kg 2.93.9 74 29-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3237102MATRIX SPIKE SAMPLE:
MSSpike
Result
92533750001
2-Nitrophenol mg/kg 1.52 77 26-130ND
3&4-Methylphenol(m&p Cresol)mg/kg 1.42 70 10-176ND
3,3'-Dichlorobenzidine mg/kg 2.8 IL3.9 72 15-130ND
3-Nitroaniline mg/kg 2.83.9 72 28-130ND
4,6-Dinitro-2-methylphenol mg/kg 3.43.9 87 15-132ND
4-Bromophenylphenyl ether mg/kg 1.52 76 35-130ND
4-Chloro-3-methylphenol mg/kg 3.03.9 78 30-130ND
4-Chloroaniline mg/kg 2.73.9 70 28-130ND
4-Chlorophenylphenyl ether mg/kg 1.62 82 32-130ND
4-Nitroaniline mg/kg 2.93.9 76 30-130ND
4-Nitrophenol mg/kg 8.19.7 84 17-130ND
Acenaphthene mg/kg 1.52 76 29-130ND
Acenaphthylene mg/kg 1.52 77 31-130ND
Aniline mg/kg 1.22 61 10-130ND
Anthracene mg/kg 1.42 74 33-130ND
Benzo(a)anthracene mg/kg 1.52 79 32-130ND
Benzo(a)pyrene mg/kg 1.52 77 32-130ND
Benzo(b)fluoranthene mg/kg 1.52 79 33-130ND
Benzo(g,h,i)perylene mg/kg 1.52 75 28-130ND
Benzo(k)fluoranthene mg/kg 1.62 82 31-130ND
Benzoic Acid mg/kg 3.09.7 31 10-130ND
Benzyl alcohol mg/kg 2.93.9 74 31-130ND
bis(2-Chloroethoxy)methane mg/kg 1.52 76 30-130ND
bis(2-Chloroethyl) ether mg/kg 1.52 75 68-130ND
bis(2-Ethylhexyl)phthalate mg/kg 1.52 76 40-130ND
Butylbenzylphthalate mg/kg 1.52 76 40-130ND
Chrysene mg/kg 1.52 77 30-130ND
Di-n-butylphthalate mg/kg 1.42 73 41-130ND
Di-n-octylphthalate mg/kg 1.52 75 42-130ND
Dibenz(a,h)anthracene mg/kg 1.52 77 27-130ND
Dibenzofuran mg/kg 1.52 79 32-130ND
Diethylphthalate mg/kg 1.72 86 40-130ND
Dimethylphthalate mg/kg 1.62 84 37-130ND
Fluoranthene mg/kg 1.52 77 26-130ND
Fluorene mg/kg 1.62 81 31-130ND
Hexachloro-1,3-butadiene mg/kg 1.52 75 20-130ND
Hexachlorobenzene mg/kg 1.52 77 29-130ND
Hexachlorocyclopentadiene mg/kg 1.32 66 10-130ND
Hexachloroethane mg/kg 1.42 70 21-130ND
Indeno(1,2,3-cd)pyrene mg/kg 1.52 77 28-130ND
Isophorone mg/kg 1.52 77 32-130ND
N-Nitroso-di-n-propylamine mg/kg 1.42 74 31-130ND
N-Nitrosodimethylamine mg/kg 1.32 66 20-130ND
N-Nitrosodiphenylamine mg/kg 1.52 77 32-130ND
Naphthalene mg/kg 1.42 73 30-130ND
Nitrobenzene mg/kg 1.42 70 25-130ND
Pentachlorophenol mg/kg 2.83.9 73 10-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
3237102MATRIX SPIKE SAMPLE:
MSSpike
Result
92533750001
Phenanthrene mg/kg 1.52 76 34-130ND
Phenol mg/kg 1.52 75 14-130ND
Pyrene mg/kg 1.52 79 31-130ND
Pyridine mg/kg 1.02 53 10-130ND
2,4,6-Tribromophenol (S)%86 18-130
2-Fluorobiphenyl (S)%74 19-130
2-Fluorophenol (S)%68 18-130
Nitrobenzene-d5 (S)%75 21-130
Phenol-d6 (S)%71 18-130
Terphenyl-d14 (S)%66 15-130
Parameter Units
Dup
Result QualifiersRPDResult
92533750002
3237103SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg ND ILND
3-Nitroaniline mg/kg NDND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92533750002
3237103SAMPLE DUPLICATE:
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg NDND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg NDND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg ND0.44
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg NDND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg NDND
Pyrene mg/kg NDND
Pyridine mg/kg NDND
2,4,6-Tribromophenol (S)%5377
2-Fluorobiphenyl (S)%5066
2-Fluorophenol (S)%4655
Nitrobenzene-d5 (S)%5569
Phenol-d6 (S)%4861
Terphenyl-d14 (S)%6165
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92533750
Northstate
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
614385
SW-846
SW-846
Dry Weight/Percent Moisture
Laboratory:Pace Analytical Services - Charlotte
Associated Lab Samples:92533750001, 92533750002
Parameter Units
Dup
Result QualifiersRPDResult
92533770002
3233691SAMPLE DUPLICATE:
Percent Moisture %7.3 N237.6
Parameter Units
Dup
Result QualifiersRPDResult
92533751013
3233692SAMPLE DUPLICATE:
Percent Moisture %7.4 N257.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92533750
Northstate
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be
considered an estimated value.IL
The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92533750
Northstate
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92533750001 615138 615751SS-Base EPA 3546 EPA 8270E
92533750002 615138 615751SS-SW EPA 3546 EPA 8270E
92533750001 614385SS-Base SW-846
92533750002 614385SS-SW SW-846
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 04/23/2021 10:06 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 19
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