WS-9507_44719_CA_CSA_20230126

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]

February 8, 2023

Mr. Ryan Bond
NCDEQ-UST Section
Winston-Salem Regional Office
450 W. Hanes Mill Road
Suite 300
Winston-Salem, NC 27105

Re: Comprehensive Site Assessment Report
August 2021 – December 2022
Trindale Mini Mart
7619 NC Highway 62
Trinity, Randolph County
North Carolina
Facility ID Number: 00-0-0000018398
Incident Number: 44719
GRI Project Number: 4236

Dear Mr. Bond,

Please find enclosed the referenced report for the abovementioned site.
If you have any questions, please contact Joanna Alley at 704-845-4010.

Sincerely,
Geological Resources, Inc.

Leslie Maxtone-Graham
Administrative Assistant

Enclosure

Cc: Ms. Joan Angel; Angels, Inc., file

3502 Hayes Road • Monroe, North Carolina 28110
113 West Firetower Road, Suite G • Winterville, North Carolina 28590
Phone [phone] • [phone] • Fax [phone]
Engineering Certification: C-2727 • Geology Certification: C-127
Comprehensive Site Assessment Report
August 2021 – December 2022
Trindale Mini Mart
7619 NC Highway 62
Trinity, Randolph County
North Carolina
Facility ID Number: 0-00-0000018398
Incident Number: 44719
GRI Project Number: 4236

Prepared for:

Ms. Joan Angel
Angels, Inc.
Post Office Box 4395
Archdale, North Carolina 27263

January 26, 2023

Joanna Alley, P.E.
Project Manager
Eric M. Eubanks, P.G.
Report Writer

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
i
EXECUTIVE SUMMARY
The Trindale Mini Mart site is an active convenience store and gasoline retail facility located at 7619 NC
Highway 62 in Trinity, Randolph County, North Carolina. The site is covered by concrete and asphalt. The
surrounding area consists of a mixture of residential, institutional, and commercial properties. One 3,000-
gallon kerosene, one 3,000-gallon gasoline, and one 4,000-gallon gasoline USTs were closed on April 27,
1990. One 7,000-gallon fuel oil UST was closed on July 31, 1990. One 3,000-gallon kerosene UST was
closed on August 1, 2016. Three 8,000-gallon gasoline USTs and associated pumps and product piping are
active at the site.

On August 1, 2016, one 3,000-gallon kerosene UST, and its associated dispenser and product piping were
removed from the site. Soil samples collected during the UST closure activities contained contaminant
concentrations that exceeded the soil-to-water MCCs, confirming the presence of a release at the site and
a LSA was required.

A receptor survey was conducted on April 25, 2017, during which eleven water supply wells were
identified within a 1,500-foot radius of the site. All residences with identified water supply wells were
connected to municipal water. No water supply wells were identified within a 250-foot radius of the
source area. No surface water bodies were identified within 500 feet of the source area. Public water is
available to the site and the surrounding properties.

One Type II monitoring well (MW-1) was installed during the LSA conducted at the site in April 2017. A
free product thickness of 0.10 feet was measured in MW-1 subsequent to installation. Well MW-1 was
gauged again on September 5, 2020, and 5.91 feet of free product was measured. Two 8-hour AFVR
events have been conducted on MW-1 to recover free product. On April 22, 2020, four additional Type II
monitoring wells (MW-2 through MW-5) were installed around the UST basin to delineate the free product
plume. Based on the results of the LSA and additional assessment activities, a CSA was required.

Between August 17, 2021, and December 19, 2022, seven Type II monitoring wells (MW-6 through MW-
12) and one Type III telescoping well (TW-1) were installed as part of CSA activities. The concentrations
of benzene, MTBE, naphthalene, TAA, TAME, TBA, n-butylbenzene, sec-butylbenzene, 1,2-DCA, IPE, 1-
methylnaphthalene, 2-methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C10 aromatics, C9-C18
aliphatics, C19-C36 aliphatics, and/or C11-C22 aromatics reported in the ground water samples collected
from MW-2, MW-4, MW-5, MW-7 through MW-12, and TW-1 exceeded the MACs. The concentration of
MTBE reported in the ground water sample collected from MW-7 exceeded the GCL. Free product was
measured in MW-2, MW-3, and MW-6 with maximum thicknesses of 0.72, 0.03, and 0.23 feet,
respectively.

Based on observations made during assessment activities, surficial soils observed at the site consist of
clayey to sandy silt and silty clay to depths of approximately 65 feet BGS. There appears to be a ground
water trough oriented toward the northeast and centered around the UST basin. The horizontal hydraulic

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
ii
gradient was convergent from the southeast and northwest with gradients of approximately 0.03 and 0.04
feet per foot, respectively. The vertical hydraulic gradient calculated for paired wells MW-4 and TW-1 was
approximately 0.06 feet per foot in the upward direction.

Rising head slug tests were conducted on MW-8, MW-9, and TW-1. The average hydraulic conductivity
calculated for the Type II monitoring wells was 1.449 x 10-3 feet per minute (2.086 feet per day) and the
average seepage velocity was 4.17 x 10-1 feet per day (152 feet per year). The hydraulic conductivity
calculated for the Type III monitoring well was 1.015 x 10-2 feet per minute (14.62 feet per day). The
seepage velocity calculated for the Type III monitoring well was 2.34 feet per day (854 feet per year).

The site risk classification has been deemed as intermediate risk based on the presence of free product
and/or GCL exceedances. Therefore, free product must be removed from the site and the ground water
contamination must be remediated to concentrations less than the GCLs.

According to NCDEQ correspondence dated January 11, 2023, the contaminant plume is sufficiently
defined. Free product removal should continue at the site until free product is no longer present. A
MMPE event is recommended to determine the influence of a 96-hour event at the site. A ground water
sampling event should be conducted at the site in June 2023 to confirm the results of the CSA ground
water sampling events. Based on the results of the MMPE event and June 2023 sampling event, a decision
to pursue corrective action or allow for natural attenuation can be made.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
iv
ACRONYMS
ACM: Asbestos Containing Materials
AFVR: Aggressive Fluid-Vapor Recovery
ARR: Acknowledgement of Report Receipt
AS: Air Sparging
AST: Aboveground Storage Tank
ASTM: American Society for Testing and
Materials
BGS: Below Ground Surface
CAP: Corrective Action Plan
CFR: Code of Federal Regulations
CSA: Comprehensive Site Assessment
DPE: Dual Phase Extraction
DRO: Total Petroleum Hydrocarbons Diesel
Range Organics
DWM: Division of Waste Management
DWR: Department of Water Resources
EPA: Environmental Protection Agency
EPH: Extractible Petroleum Hydrocarbons
ESA: Environmental Site Assessment
GCL: Gross Contamination Level
GRI: Geological Resources, Inc.
GRO: Total Petroleum Hydrocarbons
Gasoline Range Organics
LSA: Limited Site Assessment
MAC: Maximum Allowable Concentration as
specified in T15A NCAC 2L.0202
MADEP: Massachusetts Department of
Environmental Protection
MCC: Maximum Contaminant Concentrations
MMPE: Mobile Multi-Phase Extraction
NAPL: Non-Aqueous Phase Liquid, “Free
Product”
NCDEQ: North Carolina Department of
Environmental Quality
NCDOT: North Carolina Department of
Transportation
NFA: Notice of No Further Action
NORR: Notice of Regulatory Requirements
NOV: Notice of Violation
NPDES: National Pollutant Discharge
Elimination System
NRP: Notice of Residual Petroleum
O&M: Operation and Maintenance
PAHs: Polynuclear Aromatic Hydrocarbons
PCA: Pre-Construction Assessment
RAL: Regulatory Action Level
SCLs: Soil Cleanup Level
SPCC: Spill Prevention Control and
Countermeasures
SVE: Soil Vapor Extraction
SVOCs: Semi-Volatile Organic Compounds
SWAP: Source Water Assessment and
Protection
SWPPP: Stormwater Pollution Prevention Plan
TCLP: Toxicity Characteristic Leaching
Procedure (EPA Method SW-846 1311)
TOC: Top of Casing
TPH: Total Petroleum Hydrocarbons
USGS: United States Geological Survey
UST: Underground Storage Tank
UVF: Ultraviolet Fluorescence
VOCs: Volatile Organic Compounds
VPH: Volatile Petroleum Hydrocarbons

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
TABLE OF CONTENTS
EXECUTIVE SUMMARY ....................................................................................................................... i
SITE INFORMATION ........................................................................................................................... iii
ACRONYMS ....................................................................................................................................... iv
1.0 SITE HISTORY AND CHARACTERIZATION ...................................................................................1
2.0 RECEPTOR INFORMATION ........................................................................................................3
3.0 LAND USE ................................................................................................................................3
4.0 SOIL ASSESSMENT ...................................................................................................................3
5.0 GROUND WATER ASSESSMENT ................................................................................................4
6.0 FREE PRODUCT INVESTIGATION AND RECOVERY ......................................................................6
7.0 HYDROGEOLOGIC INVESTIGATION ...........................................................................................6
8.0 REGIONAL GEOLOGY AND HYDROGEOLOGY .............................................................................7
9.0 SITE GEOLOGY AND HYDROGEOLOGY ......................................................................................7
10.0 DISCUSSION ............................................................................................................................7
11.0 CONCLUSIONS AND RECOMMENDATIONS ...............................................................................8
12.0 PUBLIC NOTICE ........................................................................................................................8
13.0 LIMITATIONS ...........................................................................................................................8
14.0 REFERENCES ............................................................................................................................8

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3A: Site Vicinity Map
Figure 3B: Zoning Map
Figure 4: Cross-Section A-A’
Figure 5: Cross-Section B-B’
Figure 6: Ground Water Quality Map
Figure 7: MTBE Isoconcentration Map
Figure 8: Water Table Surface Map
TABLES
Table 1: UST Owner and Operator Information
Table 2: UST System Information
Table 3: Water Supply Well Information
Table 4: Adjacent Property Owner Information
Table 5: Land Use Information
Table 6: Summary of Soil Sample Analytical Results
Table 7: Summary of Ground Water Sample Analytical Results
Table 8: Summary of Free Product Recovery Evaluation

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
Table 9: Free Product Recovery Results
Table 10: Free Product Recovery Event Information
Table 11: Free Product Recovery Cost Summary
Table 12: Well Construction and Gauging Information
Table 13: Summary of Slug Test Analyses
APPENDICES
Appendix A: State Correspondence
Appendix B: Site-Specific Health and Safety Plan
Appendix C: Well Photographs
Appendix D: Well Permit, Well Construction Records, and Subsurface Logs
Appendix E: Laboratory Analytical Reports
Appendix F: Free Product Recovery Graphs
Appendix G: Slug Test Data
Appendix H: Public Notification

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
1
1.0 SITE HISTORY AND CHARACTERIZATION
GRI presents the results of the August 2021 through December 2022 CSA activities at the Trindale Mini
Mart site, located at 7619 NC Highway 62 in Trinity, Randolph County, North Carolina (Figure 1). These
activities were conducted in accordance with GRI Proposal Nos. 20-459 and 22-020. Proposal No. 20-459
was submitted to NCDEQ on September 23, 2020, and was approved as Task Authorization No. 44719-9
on October 2, 2020. A change order was submitted for proposal to include a DEQ well permit. The change
order was submitted to the NCDEQ on July 20, 2021 and was approved as Task Authorization No. 44719-
09-1 on July 26, 2021. Proposal No. 22-020 was split into two Task Authorization Nos. (44719-10 and
44719-11), which were submitted to NCDEQ on January 6, 2022, and December 9, 2022, and were
approved on February 1, 2022 and December 12, 2022, respectively. State correspondence is included as
Appendix A.

The site is currently owned by Joan S. Angel and is operated by Angels, Inc. Trindale Mini Mart as a
petroleum retail facility. A release was discovered in August 2016 during the removal of a 3,000-gallon
kerosene UST at the site. One 3,000-gallon kerosene, one 3,000-gallon gasoline, and one 4,000-gallon
gasoline USTs were closed on April 27, 1990. One 7,000-gallon fuel oil UST was closed on July 31, 1990.
Three 8,000-gallon gasoline USTs and associated pumps and product piping are active at the site. UST
owner/operator information and UST system information are included as Tables 1 and 2, respectively.
The Registered Tank Report is shown below:

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Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
2
On August 1, 2016, one 3,000-gallon kerosene UST was removed from the site. Soil samples collected
during the UST closure activities contained contaminant concentrations that exceeded the soil-to-water
MCCs. The UST closure results confirmed a release at the site and a LSA was required by the NCDEQ.

On April 26, 2017, one monitoring well (MW-1) was installed in the area of the former 3,000-gallon
kerosene UST basin. Two soil samples were collected during the installation of monitoring well MW-1.
The reported contaminant concentrations of several analyzed contaminants exceeded the soil-to-water
MCCs and/or the residential SCLs for the submitted soil samples. Subsequent to installation, free product
was measured in MW-1 with a thickness of 0.10 feet; therefore, the well was not sampled. Two AFVR
events have been conducted on MW-1 to recover free product.

On April 22, 2020, four additional Type II monitoring wells (MW-2 through MW-5) were installed to
delineate the free product plume. All on-site monitoring wells were gauged, purged, and/or sampled.
Free product was observed in monitoring wells MW-1 and MW-3 with free product thicknesses of 0.64
feet and 0.03 feet, respectively. The concentrations of several contaminant exceeded the MACs in the
ground water samples collected from MW-2, MW-4, and MW-5. Based on the results of LSA activities,
the site was assigned an intermediate risk classification and a CSA was required by the NCDEQ.

In August 2021, a CSA was conducted to delineate the horizontal and vertical extent of petroleum
contamination. Between August 17 and August 24, 2021, five additional Type II monitoring wells (MW-6
through MW-10) and one Type III telescoping monitoring well (TW-1) were installed, gauged, and/or
sampled as part of CSA activities. The contaminant concentrations of benzene, MTBE, naphthalene, TAA,
TBA, 1,2-DCA, IPE, 1-methylnaphthalene, 2-methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-
C10 aromatics, C9-C18 aliphatics and/or C11-C22 aromatics reported in the ground water samples
collected from MW-7, MW-8, MW-9, and TW-1 exceeded the MACs. The concentration of MTBE reported
in the ground water sample collected from MW-7 exceeded the GCL. Free product was measured in MW-
1, MW-3, and MW-6 with thicknesses of 0.66, 0.03, and 0.01 feet, respectively. Slug tests were performed
on MW-8, MW-9, and TW-1 on August 24, 2021.

Based on the results of the August 2021 CSA activities, two additional Type II monitoring wells (MW-11
and MW-12) were installed at the site on December 19, 2022. Monitoring wells MW-1 through MW-12
and TW-1 were gauged, purged, and/or sampled on December 20, 2022. The concentrations of benzene,
MTBE, naphthalene, TAA, TAME, TBA, n-butylbenzene, sec-butylbenzene, 1,2-DCA, IPE, 1-
methylnaphthalene, 2-methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C10 aromatics, C9-C18
aliphatics, C19-C36 aliphatics, and/or C11-C22 aromatics reported in the ground water samples collected
from MW-2, MW-4, MW-5, MW-7, MW-9 through MW-12, TW-1 exceeded the MACs. The concentration
of MTBE reported in the ground water sample collected from MW-7 exceeded the GCL. Free product was
measured in MW-2, MW-3, and MW-6 with thicknesses of 0.72, 0.01, and 0.23 feet, respectively. A Site
Map showing the locations of the monitoring wells and the structures on-site is included as Figure 2. A
copy of the site-specific Health and Safety Plan is included as Appendix B.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
3
2.0 RECEPTOR INFORMATION
Water Supply Wells:
According to the information determined during receptor survey activities conducted on April 25, 2017,
eleven non-potable water supply wells were identified within 1,500 feet of the site. A table summarizing
the Water Supply Well owner information is included as Table 3. A Site Vicinity Map showing the locations
of the water supply wells has been included as Figure 3.

Public Water Supplies:
Public water is available to the site and all of the surrounding properties. Water lines run along the public
streets in the area. Public water is supplied by Davidson Water Incorporated and the Archdale Water
Department.

Surface Water:
No surface water bodies were identified within a 500-foot radius of the source area. One creek feature
named Muddy Creek is located approximately 1,300 feet northwest of the source area.

Wellhead Protection Areas:
On December 28, 2022, GRI personnel accessed the NCDEQ SWAP Program’s website to identify wellhead
protection areas in the vicinity of the subject site. The site is not located within a wellhead protection
area.

Deep Aquifers in the Coastal Plain Physiographic Region:
The site is not located in the Coastal Plain Physiographic Region.

Subsurface Structures:
No structures with basements were observed in the vicinity of the source area. Utilities in the source area
are located along Trindale Road and Sealy Drive, and do not appear to intersect the seasonal high water
table.

3.0 LAND USE
The site is currently occupied by Trindale Mini Mart, a petroleum retail facility and convenience store.
The closest primary residence is located approximately 200 feet northwest of the source area. The
Trindale Children Center, Inc. is located approximately 750 feet to the southeast of the source area. The
adjoining properties are commercial and residential. According to the Randolph County GIS, the
surrounding areas are zoned HC (Highway Commercial), R-40 (Residential), and MW-1 (Heavy
Manufacturing). Adjacent property owner information and land use information are summarized in Tables
4 and 5, respectively. Land use and zoning information are presented on Figure 3B.

4.0 SOIL ASSESSMENT
On August 1, 2016, one 3,000-gallon kerosene UST, associated dispenser and product piping were
removed from the site. During the UST removal activities, confirmation soil samples were collected from
the UST basin. Concentrations of 1-methylnaphthalene, C9-C10 aromatics, C9-C18 aliphatics and C11-C22

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
4
aromatics that exceeded the soil-to-water MCCs were reported in soil sample SW-E (11’). None of the
contaminant concentrations exceeded the residential SCLs.

On April 26, 2017, two soil samples were collected during the installation of Type II monitoring well MW-
1. Concentrations of xylenes, MTBE, naphthalene, isopropylbenzene, n-propylbenzene, methylene
chloride, 1,2,4-trimethylbenzene, 1-methylnaphthalene, 2-methylnaphthalene, C9-C10 aromatics, C9-C18
aliphatics, and/or C11-C22 aromatics that exceeded the soil-to-water MCCs were reported in the soil
samples MW-1 (18’) and MW-1 (28’) collected during LSA activities. Concentrations of 1-
methylnaphthalene, C9-C18 aliphatics, and/or C11-C22 aromatics that exceeded the Residential SCLs
were reported in soil samples MW-1 (18’) and MW-1 (28’). A summary of analytical results for soil samples
collected at the site has been included as Table 6.

5.0 GROUND WATER ASSESSMENT
On April 26, 2017, one Type II monitoring well (MW-1) was installed during LSA activities at the site. Free
product was measured in MW-1 with a thickness of 0.10 feet.

On April 22, 2020, four Type II monitoring wells (MW-2 through MW-5) were installed at the site to
delineate free product. All on-site monitoring wells were subsequently gauged, purged, and/or sampled.
Free product with thicknesses of 0.64 and 0.03 feet was observed in monitoring wells MW-1 and MW-3,
respectively. The concentrations of benzene, MTBE, naphthalene, TAA, p-isopropyltoluene, n-
propylbenzene, 1,2,4-trimethylbenzene, methyl chloride, 1,2-DCA, 1-methylnaphthalene, 2-
methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C10 aromatics, C9-C18 aliphatics, and/or C11-
C22 aromatics reported in the ground water samples collected from MW-2, MW-4, and MW-5 exceeded
the MACs. All contaminant concentrations were below the GCLs. Based on the results of the LSA activities,
a CSA was required by the NCDEQ.

Between August 17 and August 19, 2021, and December 19, 2022, five Type II monitoring wells (MW-6
through MW-10) and one telescoping monitoring well (TW-1) were installed at the site. Monitoring wells
MW-6 through MW-10 were drilled to total depths ranging from 30 to 35 feet BGS and completed with
20-foot screened intervals. Telescoping well TW-1 was completed to a total depth of 65 feet with a five-
foot screen interval. Photographs of monitoring wells installed as part of CSA activities are included in
Appendix C.

On August 24, 2021, monitoring wells MW-1 through MW-10 and TW-1 were gauged, purged, and/or
sampled. The concentrations of benzene, MTBE, naphthalene, TAA, TBA, 1,2-DCA, IPE, 1-
methylnaphthalene, 2-methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C10 aromatics, C9-C18
aliphatics, and/or C11-C22 aromatics reported in the ground water samples collected from MW-7, MW-
8, MW-9, and TW-1 exceeded the MACs. The concentration of MTBE reported in the ground water sample
collected from MW-7 exceeded the GCL. Free product with thicknesses of 0.66, 0.03, and 0.01 feet was
measured in MW-1, MW-3, and MW-6, respectively. Based on the results of the August 2021 ground
water sampling event, additional wells were required to define the horizontal extent of the contaminant
plume.

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
5

On December 19, 2022, two monitoring wells (MW-11 and MW-12) were installed at the site. Each well
was installed to a total depth of 35 feet BGS with a 15-foot screened interval. On December 20, 2022,
monitoring wells MW-1 through MW-12 and TW-1 were gauged, purged, and/or sampled. The
concentrations of benzene, MTBE, naphthalene, TAA, TAME, TBA, n-butylbenzene, sec-butylbenzene, 1,2-
DCA, IPE, 1-methylnaphthalene, 2-methylnaphthalene, C5-C8 aliphatics, C9-C12 aliphatics, C9-C10
aromatics, C9-C18 aliphatics, C19-C36 aliphatics, and/or C11-C22 aromatics reported in the ground water
samples collected from MW-2, MW-4, MW-5, MW-7, MW-9 through MW-12, TW-1 exceeded the MACs.
The concentration of MTBE reported in the ground water sample collected from MW-7 exceeded the GCL.
Free product was measured in MW-2, MW-3, and MW-6 with thicknesses of 0.72, 0.01, and 0.23 feet,
respectively. Based on the established site cleanup goals, it was determined that no additional delineation
is required at this time. A summary of the December 20, 2022 ground water analytical data is shown
below:
Contaminant
of Concern Benzene Toluene Ethylbenzene Xylenes MTBE Naphthalene Well
ID
MACs (μg/l) 1 600 600 500 20 6
GCL (μg/l) 5,000 260,000 80,000 50,000 20,000 6,000
MW-1 FP FP FP FP FP FP
MW-2 <0.180 <0.220 <0.170 <0.210 35.2 <0.470
MW-3 FP FP FP FP FP FP
MW-4 10.4 1.87 5.30 75.3 394 33.9
MW-5 2.46 <0.220 <0.170 32.7 77.8 36.2
MW-6 FP FP FP FP FP FP
MW-7 6.41 <2.20 <1.70 10.0 J 85,000 <4.70
MW-8 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470
MW-9 121 <0.220 2.63 <0.210 38.9 167
MW-10 <0.180 <0.220 <0.170 <0.210 <0.140 16.3
MW-11 35.1 <0.220 <0.170 7.59 3,930 12.2
MW-12 <1.80 <2.20 <1.70 <2.10 57.7 17.3
TW-1 11.0 0.508 <0.170 <0.210 370 2.58

All samples were collected in accordance with the NCDEQ guidelines. Clean, disposable bailers and nitrile
gloves were used for the collection of the ground water samples. The samples were collected in laboratory
supplied containers and shipped to the laboratory in a cooler following proper chain-of-custody
procedures. A laboratory supplied trip blank was included in the sample cooler. No detectable
concentrations of requested method constituents were reported in the trip blank.

The locations of the monitoring wells are shown on Figure 2. The well permit, well construction records,
and boring logs for the monitoring wells installed during CSA activities are included as Appendix D.

Cross sections A-A’ and B-B’ are included as Figures 4 and 5; the lines of cross section are included on
Figure 2. A Ground Water Quality Map for the December 2022 ground water sampling event has been
included as Figure 6. An isoconcentration map for MTBE is provided as Figure 7. A summary of laboratory
analyses for the ground water samples collected during CSA activities is included as Table 7. Complete

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
6
copies of the laboratory reports for the ground water samples collected during CSA activities are included
as Appendix E.

6.0 FREE PRODUCT INVESTIGATION AND RECOVERY
Free product has historically been present in MW-1, MW-3, and MW-6. On August 16, 2017, two free
product evaluations were conducted on monitoring well MW-1. A free product thickness of 5.91 feet was
measured in MW-1 prior to the tests. Approximately 2 gallons of free product was hand bailed from MW-
1 prior to the start of Test #1. Due to equipment error, Test #1 was stopped after one hour. Test #2 was
started approximately 2 hours following the conclusion of Test #1 and lasted approximately 1.5 hours.
Approximately 2 gallons of free product were bailed from MW-1 before Test #2. Prior to Test #2, free
product was first measured at a thickness of 1.85 feet at the start of the event and achieved a measurable
thickness of 2.12 feet by the end of the 90-minute evaluation. A summary of the free product evaluation
and test is provided in Table 8 with recovery graphs included as Appendix F.

Two 8-hour AFVR events were conducted on monitoring well MW-1 to recover free product in August
2017 and February 2019. A combined total of approximately 1,176 gallons of petroleum-impacted ground
water was removed during these events. At the conclusion of these events, no free product was measured
in MW-1 or in the tanker. Summaries of the free product removal results and costs have been included
as Tables 9 through 11. Based on the results of the AFVR event, AFVR appears to be a cost-effective
method of free product removal.

7.0 HYDROGEOLOGIC INVESTIGATION
The depths to ground water in the Type II monitoring wells (MW-1 through MW-12) measured on
December 20, 2022, ranged from 22.24 to 30.55 feet below the tops of well casings. Ground water
elevations at the site, based on an assumed datum of 100.00 feet assigned to MW-1, ranged from 70.79
to 73.10 feet. Based on this information, there appears to be a ground water trough oriented toward the
northeast and centered around the UST basin. The horizontal hydraulic gradient was convergent from
the southeast and northwest with gradients of approximately 0.03 and 0.04 feet per foot, respectively.
There is a general ground water flow trend toward the north. The vertical hydraulic gradient calculated
for paired wells MW-4 and TW-1 was approximately 0.06 feet per foot in the upward direction. A
summary of ground water elevation data obtained during assessment activities to date is presented in
Table 12. A Water Table Surface Map based on the December 20, 2022, gauging data is included as Figure
8.

Rising head slug tests were conducted in MW-8, MW-9, and TW-1 on August 24, 2021. Hydraulic
conductivities in the Type II monitoring wells calculated using the Bouwer and Rice method, ranged from
1.389 x 10-4 feet per minute (0.200 feet per day) to 2.759 x 10-3 feet per minute (3.973 feet per day). The
average hydraulic conductivity was 1.449 x 10-3 feet per minute (2.086 feet per day). Seepage velocities,
calculated using the equation V = K(dh/dl)/ne, ranged from 4.00 x 10-2 to 7.95 x 10-1 feet per day (14.6 to
290 feet per year). The average seepage velocity was 4.17 x 10-1 feet per day (152 feet per year). The
hydraulic conductivity in the Type III monitoring well calculated using the Bouwer and Rice method was
1.015 x 10-2 feet per minute (14.62 feet per day). The seepage velocity calculated for the Type III

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
7
monitoring well was 2.34 feet per day (854 feet per year). A summary of the results of slug test analyses
is presented in Table 13. Calculations and raw data from the slug tests are included as Appendix G.

8.0 REGIONAL GEOLOGY AND HYDROGEOLOGY
According to the 1985 Geologic Map of North Carolina, the site is in the Carolina Slate Belt within the
Piedmont Physiographic Provence of North Carolina. The rocks underlaying the site are primarily
metamorphosed foliated granitic rocks.
9.0 SITE GEOLOGY AND HYDROGEOLOGY
Based on observations made during assessment activities, surficial soils observed at the site consist of
clayey to sandy silt and silty clay to depths of approximately 65 feet BGS. A summary of the December
2022 ground water gauging data is shown below:
Well ID
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of Casing
(feet)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
MW-1 29 – 49 49 100.00 29.51 0.72 71.11
MW-2 15 – 35 35 100.48 29.69 --- 70.79
MW-3 15 – 35 35 99.75 28.71 0.01 71.05
MW-4 15 – 35 35 98.17 27.36 --- 70.81
MW-5 15 – 35 35 97.97 27.09 --- 70.88
MW-6 15 – 35 35 101.53 28.63 0.23 73.10
MW-7 15 – 35 35 102.55 29.98 --- 72.57
MW-8 15 – 35 35 102.18 29.15 --- 73.03
MW-9 15 – 35 35 100.70 27.72 --- 72.98
MW-10 10 – 30 30 94.97 22.24 --- 72.73
MW-11 20 – 35 35 103.07 30.55 --- 72.52
MW-12 20 – 35 35 99.96 27.34 --- 72.62
TW-1 60 – 65 65 100.35 27.53 --- 72.82

On December 20, 2022, monitoring wells MW-1 through MW-12 and TW-1 were gauged, purged and/or
sampled. Depths to ground water in the Type II monitoring wells ranged from 22.24 to 30.55 feet below
the tops of well casings. Ground water elevations at the site, based on an assumed datum of 100.00 feet
assigned to MW-1, ranged from 70.79 to 73.10 feet. Ground water flow at the site was converged towards
a ground water trough that is centered around the UST basin.
10.0 DISCUSSION
On August 1, 2016, one 3,000-gallon kerosene UST and its associated dispenser and product piping were
removed from the subject site. Confirmation soil samples collected as part of the UST closure activities
identified a release from the UST system.

To date, twelve Type II monitoring wells and one telescoping well have been installed at the site to
determine the horizontal and vertical extent of the release. Free product has been observed in the vicinity
of the UST basin in monitoring wells MW-1, MW-3, and MW-6. Monitoring well MW-7 contained the
highest ground water contamination levels during CSA activities, with the reported concentration of MTBE
exceeding the GCL. Please note that MW-7 is also in the vicinity of the UST basin. According to NCDEQ

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
8
correspondence dated January 11, 2023, the contaminant plume is sufficiently defined.

The risk ranking for the site has been established as intermediate due to the presence of free product and
GCL exceedances. In order to lower the risk ranking of the site, free product recovery should continue at
the site until free product is no longer present and ground water concentrations are below GCLs.
11.0 CONCLUSIONS AND RECOMMENDATIONS
· No further soil assessment should be required.
· Ground water flow at the site was converged towards a ground water trough that is centered
around the UST basin.
· The ground water contaminant plume remains undefined vertically, as well as horizontally to the
north, east and west at the site; however, the NCDEQ Incident Manager has determined it to be
sufficiently delineated for the site-specific cleanup goals.
· Based on this site assessment, the site risk classification should remain intermediate.
· Free product removal should continue until free product is no longer present and ground water
concentrations are below GCLs. A MMPE event is recommended to determine the influence of a
96-hour event at the site.
· GRI recommends conducting a comprehensive ground water sampling event in June 2023. Based
on the results of the MMPE event and June 2023 sampling event, further recommendations can
be made.
12.0 PUBLIC NOTICE
Copies of the applicable portions of this CSA report have been forwarded to the appropriate local officials
by certified mail. Copies of the cover letters are included in Appendix H.
13.0 LIMITATIONS
This report has been prepared for the exclusive use of Angels, Inc. for specific application to the referenced
site in Randolph County, North Carolina. The assessment was conducted based on the scope of work and
level of effort desired by the NCDEQ and with resources adequate only for that scope of work. Our findings
have been developed in accordance with generally accepted standards of environmental practices in the
State of North Carolina, available information, and our professional judgment. No other warranty is
expressed or implied.

The data that is presented in this report is indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would
be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from this data.
14.0 REFERENCES
Bouwer, H., 1989, The Bouwer and Rice slug test - an update, Ground Water, vol.27, no. 3, pp.304-309

___________________________________________________________________________________________
Prepared by: Geological Resources, Inc. Comprehensive Site Assessment Report
Prepared on: January 26, 2023 Trindale Mini Mart
Project Manager: Joanna Alley, P.E. GRI Project No. 4236
9
Bouwer, H. and R.C. Rice, 1976, A slug test method for determining hydraulic conductivity of unconfined
aquifers with completely or partially penetrating wells, Water Resources Research, vol. 12, no.3,
pp. 423-428
Department of Natural Resources and Community Development, 1985, Geologic Map of North Carolina,
1 sheet
Fetter, C. W., 1988, Applied Hydrogeology, Second Edition, Macmillan Publishing Company, 592 p.
North Carolina Department of Environmental Quality, Division of Waste Management – UST Section
Assessment Guidelines; Petroleum and Hazardous Substance UST Releases, January 19, 2021
Version
Phase I Limited Site Assessment Report, Trindale Mini Mart, Geological Resources, Inc., June 7, 2017
Free Product Recovery Report, Trindale Mini Mart, Geological Resources, Inc., March 18, 2019

FIGURES
Copyright:© 2013 National Geographic Society, i-cubed
FIGURE 1
SITE LOCATION MAP
TRINDALE MINI MART
7619 N.C. HIGHWAY 62
TRINITY, RANDOLPH COUNTY,
NORTH CAROLINA
INCIDENT NO. 44719
GRI PROJECT NO. 4236
PREPARED BY:
GEOLOGICAL RESOURCES, INC.
AUGUST 29, 2016
0 2,000 4,0001,000
Feet
SCALE: 1 INCH = 2,000 FEET
MAP CENTER LOCATION
LATITUDE: 35.903109° N
LONGITUDE: 79.986786° W
`SITE LOCATION
³
"J
"J"J
"J
"J
"J
"J
"J
"J "J
"J
DJ
DJ
DJ
SITE
S
E
A
L
Y D
R
TRINDALE RDNC HWY 62ROCKFORD DRT
RI
NI
T
Y RDOLD ENGLI
SH FARM RDOFFICE PKW YENGLISH FARM RD
ROCKFORD DR EXTUt Muddy Creek
WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-1
WSW-11
WSW-10
7708757085
7708858110
7708669429
7708849043
7708756568
7708755108
7708755062
7708758200
7708853562
7708752470770875506277087515197708751582
7 708753 3 4 3
7708752035
770875514977087524267708668002
7708750718
WSW-2
1,500-FOOT RADIUS
250-FOOT RADIUS
1,000-FOOT RADIUS
FIGURE 3A: SITE VICINITY MAP
TRINDALE MINI MART
7619 NC HIGHWAY 62
TRINITY, RANDOLPH COUNTY
NORTH CAROLINA
INCIDENT NO. 44719
GRI PROJECT NO. 4236
PREPARED BY:
GEOLOGICAL RESOURCES, INC.
SEPTEMBER 21, 2021
³
0 300150
Feet
1 inch = 300 feet
LEGEND
"J Water Supply Well
DJ Water Supply Well (Inactive)
roads
streams
Lakes
Subject Property
parcels
NOTE:
THIS MAP IS BASED ON DATA FROM THE
RANDOLPH COUNTY, NC GIS WEBSITE.
SITE
M-2
M-2
M-1
M1
R-40
R-40
RM-CZ
RM-CZ
RM-CZ
RM-CZ
RM-CZ
RM-CZ
RM-CZ
RM-CZ
HC
HC
HC
R-15
R-15
R-10
B-1
RA
B-2
OI
O&I
RM-CZ
RM-CZRM-CZ
S
E
A
L
Y D
R
TRINDALE RDNC HWY 62ROCKFORD DRT
RI
NI
T
Y RDOLD ENGLI
SH FARM RDOFFICE PKW YENGLISH FARM RD
ROCKFORD DR EXTUt Muddy Creek
WSW-9
WSW-8
WSW-7
WSW-6
WSW-5
WSW-4
WSW-3
WSW-1
WSW-11
WSW-10
7708757085
WSW-2
1,500-FOOT RADIUS
250-FOOT RADIUS
1,000-FOOT RADIUS
FIGURE 3B: ZONING MAP
TRINDALE MINI MART
7619 NC HIGHWAY 62
TRINITY, RANDOLPH COUNTY
NORTH CAROLINA
INCIDENT NO. 44719
GRI PROJECT NO. 4236
PREPARED BY:
GEOLOGICAL RESOURCES, INC.
SEPTEMBER 21, 2021
³
0 300150
Feet
1 inch = 300 feet
LEGEND
ZONING O&I
ZONING OI
ZONING B-2
ZONING RA
ZONING B-1
ZONING R-10
ZONING R-15
ZONING HC
ZONING RM-CZ
ZONING R-40
ZONING M-1
ZONING M-2
Subject Property
parcels
"J Water Supply Well
DJ Water Supply Well (Inactive)
roads
Lakes
NOTE:
THIS MAP IS BASED ON DATA FROM THE
RANDOLPH COUNTY, NC GIS WEBSITE.
HC-CZ

TABLES
UST ID Number 1 - 3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 5 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner
UST ID Number A1 - A3 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number 4 Facility ID Number
Owner or Operator?
Owner/Operator
UST ID Number A1 - A3 Facility ID Number
Owner or Operator?
Owner/Operator
Address Telephone Number
Post Office Box 4395, Archdale, North Carolina 27263 [phone]
Post Office Box 4395, Archdale, North Carolina 27263 [phone]
0-0018398
Name of Owner or Operator Dates of Ownership / Operation
Stephen K. Angel and Joan S. Angel 09/20/05 - Current
Address Telephone Number
Spencer Oil Company, Inc. 04/27/90 - 09/20/05
Address Telephone Number
7613 Highway 62, Trinity NC 27370 [phone]
0-0018398
Name of Owner or Operator Dates of Ownership / Operation
Stephen K. Angel and Joan S. Angel 09/20/05 - 08/01/16
Name of Owner or Operator Dates of Ownership / Operation
7613 Highway 62, Trinity NC 27370 [phone]
0-0018398
Name of Owner or Operator Dates of Ownership / Operation
Spencer Oil Company, Inc. 05/03/83 - 09/20/05
Address Telephone Number
7613 Highway 62, Trinity NC 27370 [phone]
0-0018398
Address Telephone Number
Spencer Oil Company, Inc. 05/09/59 - 04/27/90
Address Telephone Number
7613 Highway 62, Trinity NC 27370 [phone]
0-0018398
Name of Owner or Operator Dates of Ownership / Operation
Spencer Oil Company, Inc. 09/27/66 - 07/31/90
Name of Owner or Operator Dates of Ownership / Operation
TABLE 1
UST OWNER/OPERATOR INFORMATION
TRINDALE MINI MART (INCIDENT NO. 44719)
00-0-0000018398
Page 1 of 1
Date: 05/08/2020
Was
Release
Associated
with UST
System?
(Yes / No)
1 Kerosene Kerosene 3,000 5/09/59
Steel 5' 3" x 18' Steel
Removed
(4/27/90)No
2 Gasoline Gasoline 4,000 5/09/59
Steel 5' 3" x 24' Steel
Removed
(4/27/90)No
3 Gasoline Gasoline 3,000 5/09/59
Steel 5' 3" x 18' Steel
Removed
(4/27/90)No
4 Kerosene Diesel 3,000 5/03/83
Steel 5' 3" x 18' Enviro-Flex
Removed
(8/01/16)Yes
5 Fuel Oil Fuel Oil 7,000 9/27/66
Steel 8' x 19' Steel
Removed
(7/31/90)No
A1 Gasoline Gasoline 8,000 4/27/90 Single Wall FRP 8' x 21' 3" Single Wall FRP Current No
A2 Gasoline Gasoline 8,000 4/27/90 Single Wall FRP 8' x 21' 3" Single Wall FRP Current No
A3 Diesel Gasoline 8,000 4/27/90 Single Wall FRP 8' x 21' 3" Single Wall FRP
Temporarily
Closed No
Notes:
• FRP: Fiberglass reinforced plastic.
Tank
Dimensions
Description of
Associated
Product Piping
and
Pumps
Status
of
UST
TABLE 2
UST SYSTEM INFORMATION
TRINDALE MINI MART (INCIDENT NO. 44719)
Facility ID #: 00-0-0000018398
UST
ID
No.
Current
or Most
Recent
Contents
Previous
Contents
Capacity
(gallons)
Date
Installed
Construction
Details
Page 1 of 1
Facility ID #: 00-0-0000018398
Well
No. PIN Well Owner Mailing Address Well Address
Well Use
(Potable/ Non-
Potable etc.)
Connected to
Municipal Water
Yes/No
Distance from
Source Area of
Release
(ft.)
WSW-1 7708753343 Thomas & Diane Harris Life Estate
Post Office Box 671
Trinity, NC 27370
107 Sealy Drive
Trinity, NC 27370
Inactive
Non-potable Yes 515' NW
WSW-2 7708752470 Stacey Stanley
109 Sealy Drive
Trinity, NC 27370
109 Sealy Drive
Trinity, NC 27370 Unknown Yes 600' NW
WSW-3 7708752426 Michael & Natasha Byrd
6370 Weant Road
High Point, NC 27263
111 Sealy Drive
Trinity, NC 27370 Unknown Yes 646' NW
WSW-4 7708751582 Steven Morris Reddeck
2414 Mt. Willing Road
Efland, NC 27243
113 Sealy Drive
Trinity, NC 27370 Unknown Yes 740' NW
WSW-5 7708751519 Langley Mitchel Ruth
Post Office Box 78
Trinity, NC 27370
115 Sealy Drive
Trinity, NC 27370 Unknown Yes 850' NW
WSW-6 7708750718 Michael & Natasha Byrd
6370 Weant Road
High Point, NC 27263
119 Sealy Drive
Trinity, NC 27370 Unknown Yes 1,130' NW
WSW-7 7708669429 J.L Darr, III & Henry H. Darr
Post Office Box 7163
High Point, NC 27264 No Physical Address Inactive
Non-potable Yes 1,060' NW
WSW-8 7708668002 Miguel Sanchez Teodoro
1312 Bencini Place
High Point, NC 27260
129 Sealy Drive
Trinity, NC 27370
Inactive
Non-potable Yes 1,385' NW
WSW-9 7708756568 Henry H. Darr
Post Office Box 7163
High Point, NC 27264 No Physical Address Active
Non-potable Yes 505' NE
WSW-10 7708853562 Johnny S. Jarrett
623 Trindale Road
Trinity, NC 27370
623 Trindale Road
Trinity, NC 27370 Unknown Yes 888' NE
WSW-11 7708849043 RUSTIXX, LLC
1704 Laughlin Road
Randleman, NC 27317
12990 Trinity Road
Trinity, NC 27370 Unknown Yes 1,485' SE
Notes:
• Water supply wells are shown on Figure 3A.
TABLE 3
WATER SUPPLY WELL INFORMATION
TRINDALE MINI MART (INCIDENT NO. 44719)
Date: 12/28/2022
Page 1 of 1
Date: 12/28/2022 Facility ID #: 00-0-0000018398
PIN Property Owner Name Mailing Address
7708757085 (site) Joan S. Angel
P.O. Box 4395
Archdale, NC 27263
7708755062 Kimberlie E. Spencer & Anita L.
Everhart
324 Kanoy Road
Thomasville, NC 27360
7708755108 Doug Woodgeard
7613 NC Highway 62
Trinity, NC 27370
7708758200 R. H. Richardson Family, LLC.
788 Lake Forest Drive
New London, NC 28127
7708858110 J.L. Darr & Sons, Inc.
P.O. Box 7163
High Point, NC 27264
Note:
• Properties are keyed to Figure 3A.
TABLE 4
ADJACENT PROPERTY OWNER INFORMATION
TRINDALE MINI MART (INCIDENT NO. 44719)
Page 1 of 1
Date: 09/08/21 Facility ID # : 00-0-0000018398
Map ID No. Land Use Feature Zoning Description Address
Distance from
Source Area
(feet)
1 Trin-Dale Children Center, Inc. B-2 School
13089 Trinity Road
Trinity, NC 27370
~750
Southeast
2 Carl and Linda Grubb Family
YMCA M-2 Youth Organization
609 Trindale Road
Archdale, NC 27263
~1,500
Northeast
n/a OI Office and Institutional n/a n/a
n/a B-2 Highway Business n/a n/a
n/a RA
Residential and
Agricultural n/a n/a
n/a B-1 Business n/a n/a
n/a R-10 Residential 10 n/a n/a
n/a R-15 Residential 15 n/a n/a
n/a HC Highway Commerical n/a n/a
n/a RM-CZ
Residential Medium -
Conditional Zoning n/a n/a
n/a R-40 Residential 40 n/a n/a
n/a M-1 Mixed Use 1 n/a n/a
n/a M-2 Mixed Use 2 n/a n/a
Note:
• Properties are keyed to Figure 3B.
TABLE 5
LAND USE INFORMATION
TRINDALE MINI MART MART (INCIDENT NO: 44719)
Page 1 of 1
Date: 05/10/17
→5030/
8015C
3546/
8015C
50 100 NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE NE
NE NE 0.0072 5.4 8 6 0.085 0.2 6.6 6.6 0.054 1.5 68 540 31 540 NE 31
NE NE 12 1,250 60.3 3,120 156 5.5 156 156 22.8 62.5 625 1,560 469 1,560 31,200 469
UST-1-1 (10')08/01/16 10 164 20,000 <0.11 <0.099 <0.096 <0.25 NR NR NR NR NR NR NR NR NR NR NR NR
UST-1-2 (10')08/01/16 10 <5.9 <6.2 <0.14 <0.12 <0.12 <0.31 NR NR NR NR NR NR NR NR NR NR NR NR
DI-1 (3')08/01/16 3 22.4 1,860 <0.084 <0.075 <0.072 <0.19 NR NR NR NR NR NR NR NR NR NR NR NR
SW-N (11')08/01/16 11 NR NR <0.0013 <0.0012 <0.0012 <0.0030 <0.0012 <0.0021 <0.0011 <0.0011 <0.030 <0.021 <2.3 <2.3 <2.3 <5.8 <5.8 <8.7
SW-E (11')08/01/16 11 NR NR 0.0040 J <0.0014 <0.0013 0.0083 J <0.0014 0.0361 0.0082 0.0207 0.242 0.214 J 5.44 J 95.5 64.3 574 79.3 170
SW-S (11')08/01/16 11 NR NR <0.0016 <0.0015 <0.0014 <0.0037 <0.0014 <0.0026 <0.0013 <0.0013 <0.041 <0.030 <3.8 <3.8 <3.8 <8.0 <8.0 <12
SW-W (11')08/01/16 11 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
Bottom (13')08/01/16 13 NR NR <0.0016 <0.0014 <0.0014 <0.0036 <0.0014 <0.0025 <0.0013 <0.0013 <0.036 <0.026 <3.1 <3.1 <3.1 <7.0 <7.0 <11
SP-1 (0-200)08/01/16 NA 73.2 954 <0.11 <0.097 <0.094 <0.24 NR NR NR NR NR NR NR NR NR NR NR NR
MW-1 (18')04/26/17 18 NR NR <0.095 0.236 J 1.05 6.38 <0.078 21.6 11.4 4.06 19.0 24.3 15.0 287 462 3,390 645 1,670
MW-1 (28')04/26/17 28 NR NR <0.14 0.261 J 1.16 7.21 0.348 J 28.5 14.6 4.85 23.0 30.4 20.4 300 426 3,580 675 J 1,540
Notes:
• Results reported in mg/kg.
• ft-BGS: feet below ground surface.
• RAL: Regulatory Action Level.
• MCCs: Maximum Contaminant Concentrations (soils).
• SCLs: Soil Cleanup Levels.
• Concentrations in bold face type exceed the RALs and/or the soil-to-water MCCs.
• Concentrations in bold and italic face type exceed the residential SCL.
• <: Less than the method detection limit specified in the laboratory report.
• J: Estimated value.
• NR: Not Requested.
• NA: Not Available
• NE: Not Established.
• Concentrations of isopropylbenzene, n-propylbenzene and methylene chloride in MW-1 (18') and MW-1 (28') exceeded the soil to water MCCs.
• For other detectable contaminant concentrations below the MCCs, please refer to the laboratory report.C9-C18 AliphaticsC19-C36 AliphaticsC11-C22 AromaticsRAL
Soil-to-Water MCCs C9-C12 AliphaticsC9-C10 AromaticsBenzeneResidential SCLs 1,3,5-Trimethylbenzene1-Methylnaphthalene2-MethylnaphthaleneC5-C8 AliphaticsTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl-ether (MTBE)Naphthalene1,2,4-TrimethylbenzeneSample IDDate Collected(mm/dd/yy)Sample Depth(ft-BGS)Gasoline-Range TPHDiesel-Range TPHTABLE 6
SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS
TRINDALE MINI MART MART (INCIDENT NO: 44719)
Facility ID #: 00-0-0000018398
Analytical Method EPA Method 8260B and 8270D MADEP VPH MADEP EPH
Page 1 of 1
Date: 01/11/23
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 40 128 10 70 70 3 0.4 70 25 70 400 400 1 30 400 700 200 700 10,000 200
5,000 260,000 80,000 50,000 20,000 6,000 40,000 12,800 10,000 6,900 8,500 3,000 400 70,000 11,700 26,100 28,500 24,100 1,000 12,000 NE NE NE NE NE NE
12/20/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/20/22 <0.180 <0.220 <0.170 <0.210 35.2 <0.470 2.72 J <0.280 6.49 J <0.180 <0.200 <0.220 <0.150 4.41 <0.089 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR
12/20/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/20/22 10.4 1.87 5.30 75.3 394 33.9 52.2 3.43 J <1.60 5.60 7.63 <0.220 <0.150 30.0 8.01 9.68 242 68.3 NR NR NR NR NR NR NR NR
12/20/22 2.46 <0.220 <0.170 32.7 77.8 36.2 282 0.534 J 90.5 <0.180 5.04 <0.220 <0.150 9.80 8.61 10.0 184 96.6 NR NR NR NR NR NR NR NR
12/20/22 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
12/20/22 6.41 <2.20 <1.70 10.0 J 85,000 <4.70 11,700 377 <16.0 <1.80 <2.00 <2.20 <1.50 520 <0.890 <1.90 <1.90 <1.80 NR NR NR NR NR NR NR NR
12/20/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 1.60 J 0.443 J 0.545 <0.220 <0.150 <0.500 0.226 J <0.190 2.44 <0.180 NR NR NR NR NR NR NR NR
12/20/22 121 <0.220 2.63 <0.210 38.9 167 92.7 1.42 J 24.4 11.8 13.5 <0.220 <0.150 3.48 19.6 52.0 1.29 0.345 J NR NR NR NR NR NR NR NR
12/20/22 <0.180 <0.220 <0.170 <0.210 <0.140 16.3 <1.90 <0.280 <1.60 <0.180 <0.200 <0.220 <0.150 <0.500 <0.089 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR
MW-11 12/20/22 35.1 <0.220 <0.170 7.59 3,930 12.2 1,070 23.5 <1.60 0.304 J 0.633 <0.220 <0.150 91.7 <0.089 <0.190 2.01 <0.180 3.66 3.16 1,210 63.9 J 13.9 J 208 JB <128 93.2 J
MW-12 12/20/22 <1.80 <2.20 <1.70 <2.10 57.7 17.3 85.9 J <2.80 56.3 J 110 134 <2.20 <1.50 <5.00 16.4 26.6 <1.90 <1.80 196 141 540 6,440 9,360 350,000 20,800 155,000 J
12/20/22 11.0 0.508 <0.170 <0.210 370 2.58 730 J 14.1 <1.60 0.326 J 1.07 <0.220 1.37 12.5 <0.089 0.301 J <0.190 <0.180 NR NR NR NR NR NR NR NR
12/20/22 <0.180 <0.220 <0.170 <0.210 <0.140 <0.470 <1.90 <0.280 <1.60 <0.180 <0.200 <0.220 <0.150 <0.500 <0.089 <0.190 <0.190 <0.180 NR NR NR NR NR NR NR NR
Notes:
• Concentrations in bold face type indicate the MACs were below the reported concentrations.
• For other compounds reported which did not exceed the MACs, refer to the laboratory report.
SM 6200B EPA 625.1
• NA: Analyses not performed by laboratory.
• J: Estimated concentration.
• B: Analyte found in assoicated method blank.
Contaminant of Concern
→BenzeneTolueneEthylbenzeneTotal XylenesMethyl-tert-butyl ether(MTBE)Naphthalenetert-Amyl alcohol(TAA)• NR: Not requested.
• FP: Free Product.
• Results reported in µg/l (micrograms per liter).
• MAC: Maximum Allowable Concenration as specified in T15A NCAC 2L.0202.
• GCL: Gross contamination level.
• NE: Standard not established.tert-Amyl methyl ether (TAME)tert-Butyl alcohol(TBA)TABLE 7
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TRINDALE MINI MART (INCIDENT NO. 44719)
Analytical Method → MADEP VPH
Facility ID #: 00-0-0000018398
MADEP EPH
n-Butylbenzenesec-ButylbenzeneMethyl chloride(Chloromethane)1,2-DichloroethaneDi-isopropyl etherp-Isopropyltoluene(4-Isopropyltoluene)n-Propylbenzene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene• J: Estimated value.
MAC (µg/l)
GCL (µg/l)C19-C36 AliphaticsC11-C22 AromaticsC9-C12 AliphaticsC9-C10 AromaticsC9-C18 AliphaticsC5-C8 Aliphatics• < : Less than the method detection limit specified in the laboratory report.
• Concentrations in italics indicate the GCLs were below the reported concentrations.1-Methylnaphthalene2-MethylnaphthaleneMW-10
TW-1
Trip Blank
MW-1
MW-2
MW-3
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9
Page 1 of 1
Well ID MW-1 (Test #1)Well ID MW-1 (Test #2)
Date:9/5/2017 Date:9/5/2017
Intial Depth to Product (feet)29.41 Intial Depth to Product (feet)29.93
Intial Depth to Water (feet)35.32 Intial Depth to Water (feet)32.82
Intial Product Thickness (feet)5.91 Intial Product Thickness (feet)2.89
Time
(seconds)
Depth to Free
Product
(feet)
Depth to
Water
(feet)
Product
Thickness
(feet)
Time
(seconds)
Depth to Free
Product
(feet)
Depth to Water
(feet)
Product
Thickness
(feet)
Product Water Product Water
0 31.87 0 30.91 32.76 1.85
15 15 30.79 32.74 1.95
30 31.64 30 30.74 32.62 1.88
45 31.54 45 30.71 32.62 1.91
60 31.46 60 30.72 32.58 1.86
75 31.41 75 30.74 32.52 1.78
90 31.36 90 30.63 32.44 1.81
105 31.31 105 30.61 32.41 1.80
120 31.24 120 30.60 32.41 1.81
135 31.24 135 30.56 32.40 1.84
150 31.16 150 30.53 32.39 1.86
165 31.11 165 30.51 32.36 1.85
180 31.08 180 30.51 32.33 1.82
195 31.03 195 30.49 32.34 1.85
210 31.02 210 30.47 32.31 1.84
225 30.96 225 30.43 32.28 1.85
240 30.91 240 30.42 32.27 1.85
255 30.89 255 30.42 32.26 1.84
270 30.84 270 30.41 32.25 1.84
285 30.81 285 30.41 32.22 1.81
315 30.79 32.89 2.10 315 30.41 32.22 1.81
345 30.73 32.94 2.21 345 30.38 32.24 1.86
375 30.68 32.91 2.23 375 30.36 32.23 1.87
405 30.63 32.86 2.23 405 30.24 32.21 1.97
435 30.60 32.84 2.24 435 30.22 32.21 1.99
465 30.56 32.81 2.25 465 30.21 32.18 1.97
495 30.53 32.79 2.26 495 30.20 32.18 1.98
525 30.51 32.77 2.26 525 30.20 32.18 1.98
555 30.46 32.74 2.28 555 30.18 32.16 1.98
585 30.46 32.71 2.25 585 30.16 32.15 1.99
645 30.41 32.61 2.20 645 30.28 32.13 1.85
705 30.37 32.66 2.29 705 30.23 32.13 1.90
765 30.34 32.63 2.29 765 30.22 32.12 1.90
825 30.32 32.61 2.29 825 30.18 32.10 1.92
885 30.26 32.51 2.25 885 30.18 32.09 1.91
1185 30.18 32.31 2.13 1185 30.13 32.06 1.93
1485 30.11 32.30 2.19 1485 30.10 32.05 1.95
1785 30.08 32.50 2.42 1785 30.08 32.05 1.97
2685 30.01 32.51 2.50 2685 30.05 32.09 2.04
3585 29.99 32.56 2.57 3585 30.04 32.13 2.09
4485 30.01 32.16 2.15
5385 30.00 32.12 2.12
TABLE 8
SUMMARY OF FREE PRODUCT RECOVERY EVALUATION DATA
TRINDALE MINI MART (INCIDENT NO. 44719)
Date: 02/04/19
Method of Measurement:
Well ID Product Type
(gas, diesel, etc.)
Date of
Recovery
(mm/dd/yy)
Free Product
Recovery
Method*
Casing
Diameter
(inches)
Product Thickness
before Recovery
(feet)
Product Thickness
after Recovery
(feet)
Amount of Liquid
Recovered
(gallons)
Amount of
Product
Recovered
(gallons)
MW-1 Kerosene 09/05/17 Hand Bailing 2 5.19 2.89 4.00 4.00
MW-1 Kerosene 11/22/17 AFVR 2 6.43 0.00 741.00 0.00
MW-1 Kerosene 02/14/19 AFVR 2 2.95 0.00 435.60 0.00
Notes :
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Liquid Recovered (gallons) includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered (in gallons) includes only the volume of free product in the tanker at the end of the event (based on Disposal Manifest
and/or Field Notes).
TABLE 9
FREE PRODUCT RECOVERY RESULTS
TRINDALE MINI MART (INCIDENT NO. 44719)
Interface probe at top-of-casing
Facility ID #: 00-0-0000018398
Parge 1 of 1
Date: 02/04/19
MW-1 09/05/17 Hand Bailing --- --- --- ---4.00 4.00 4.00
MW-1 11/22/17 AFVR 1,143.86 152.29 583.29 0.25 741.00 0.00 0.25
MW-1 02/14/19 AFVR 118.24 66.71 84.23 0.01 435.60 0.00 0.01
0.26 1,180.60 4.00 4.26
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Amount of Vaporized Product (in gallons) is based on Vapor Emissions Summary Sheet, = total emissions in pounds/6.25
• Amount of Liquid Recovered includes Total liquids (Water and Free Product) as indicated on Disposal Manifest.
• Amount of Product Recovered as Liquid includes only the volume of free product in the tanker at the end of the event (based on Disposal
Manifest and/or Field Notes).
• Total Amount of Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Total Fluids Removed = Amount of Vaporized Product + Amount of Liquid Recovered
• Information regarding historical free product recovery activities is not available.
Current Event 435.61 0.01
Total To Date 1,180.86 4.26
Totals
SUMMARY OF FLUID REMOVAL
Summary Total Fluids Removed (in gallons)Total Product Removed (in gallons)
Amount of
Liquid
Recovered
(gallons)
Amount of
Product
Recovered as
Liquid
(gallons)
Total Amount
of Product
Recovered
(gallons)
TABLE 10
FREE PRODUCT RECOVERY EVENT INFORMATION
TRINDALE MINI MART (INCIDENT NO. 44719)
Well ID Date
(mm/dd/yy)
Product
Recovery
Method*
Average
Effluent
Velocity
(ft/min)
Average
Effluent
Temperature
(°F)
Average
Effluent
Concentration
(ppm)
Amount of
Vaporized
Product
(gallons)
Facility ID #: 00-0-0000018398
Page 1 of 1
Date: 02/04/19
Wells
Included in
Event
Product
Recovery
Method*
Date of
Event
(mm/dd/yy)
Total Amount of Free
Product plus Ground
Water Recovered
(gallons)
Cost of Free
Product
Recovery Event
Cost Per Gallon
(total liquids)
MW-1 Hand Bailing 09/05/17 4.00 $725.00 $181.25
MW-1 AFVR 11/22/17 741.25 $2,573.35 $3.47
MW-1 AFVR 02/14/19 435.61 $2,466.25 $5.66
1,180.86 $5,764.60 $4.88
Notes:
• *: Bailing, Skimming, Aggressive Fluid Vapor Recovery (AFVR), Mobile Multiphase Extraction (MMPE)
• Total Amount of Free Product Recovered = Amount of Vaporized Product + Amount of Product Recovered as Liquid
• Cost of Free Product Recovery Event includes supervision, travel, mileage, per diem, subcontractor costs, report preparation and project management.
TOTAL (to date)
TABLE 11
FREE PRODUCT RECOVERY COST SUMMARY
TRINDALE MINI MART (INCIDENT NO. 44719)
Comments
Cost per gallon for the event is based on a total volume of
4.00 gallons of free product.
Facility ID #: 00-0-0000018398
Cost per gallon for the event is based on a total volume of
435.61 gallons water and free product.
Cost per gallon for the event is based on a total volume of
741.25 gallons water and free product.
Page 1 of 1
Date: 12/28/22
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of
Casing
(ft)
Free
Product
Thickness
(ft.)
Ground
Water
Elevation
(ft.)
Comments
04/26/17 31.11 0.10 Free Product
09/05/17 35.32 5.91 Free Product
11/22/17 37.43 6.43 Before AFVR
11/22/17 33.66 ---After AFVR
02/14/19 24.75 2.95 Before AFVR
02/14/19 25.18 ---After AFVR
04/22/20 23.53 0.64 77.02
08/24/21 25.08 0.66 75.49
12/20/22 29.51 0.72 71.11
04/22/20 23.99 ---76.49
08/24/21 25.08 ---75.40
12/20/22 29.69 ---70.79
04/22/20 23.49 0.03 76.29
08/24/21 24.32 0.03 75.46
12/20/22 28.71 0.01 71.05
04/22/20 22.42 ---75.75
08/24/21 23.44 ---74.73
12/20/22 27.36 ---70.81
04/22/20 22.04 ---75.93
08/24/21 23.16 ---74.81
12/20/22 27.09 ---70.88
08/24/21 24.44 0.01 77.10
12/20/22 28.63 0.23 73.10
08/24/21 25.43 ---77.12
12/20/22 29.98 ---72.57
08/24/21 24.75 ---77.43
12/20/22 29.15 --- 73.03
08/24/21 23.78 ---76.92
12/20/22 27.72 ---72.98
08/24/21 18.56 ---76.41
12/20/22 22.24 ---72.73
MW-11 12/19/22 12/20/22 20 20 - 35 35 103.07 30.55 ---72.52
MW-12 12/19/22 12/20/22 20 20 - 35 35 99.96 27.34 --- 72.62
08/24/21 23.63 ---76.72
12/20/22 27.53 --- 72.82
Notes:
• Elevations relative to a temporary benchmark with an assumed elevation 100.00 ft.
• ft BGS : feet below ground surface.
• NM: Not measured.
15 - 35
15 15 - 35
35 98.17
35 97.97
MW-4 04/22/20
MW-5 04/22/20
15
TABLE 12
WELL CONSTRUCTION & GAUGING INFORMATION
TRINDALE MINI MART (INCIDENT NO. 44719)
Facility ID #: 00-0-0000018398
NMNM
MW-1 04/26/17 29 29 - 49 49
100.00
MW-2 04/22/20
MW-3 04/22/20
15 15 - 35 35 100.48
15 15 - 35 35 99.75
MW-6 08/18/21
MW-7 08/18/21
MW-8 08/18/21
MW-9 08/18/21
MW-10 08/18/21
TW-1 08/19/21
15 15 - 35 35 101.53
15 15 - 35 35 102.55
15 15 - 35 35 102.18
15 15 - 35 35 100.70
10 10 - 30 30 94.97
60 60 - 65 65 100.35
Page 1 of 1
Facility ID#: 00-0-0000018398
ft/min ft/day ft/day ft/year
MW-8 1.389E-04 2.000E-01 4.00E-02 1.46E+01
MW-9 2.759E-03 3.973E+00 7.95E-01 2.90E+02
AVG (MWs) 1.449E-03 2.086E+00 4.17E-01 1.52E+02
TW-1 1.015E-02 1.462E+01 2.34E+00 8.54E+02
Note:
Seepage velocities calculated using the equation v = k(dh/dl)/ne , where:
k = hydraulic conductivity
ne = effective porosity: MW-8 & 9 = 0.20 (fine sandy silt)
TW-1 = 0.25 (fine-medium sand)
dh/dl = hydraulic gradient = 0.04
TABLE 13
SUMMARY OF SLUG TEST ANALYSES
TRINDALE MINI MART (INCIDENT NO. 44719)
Date : 09/03/2021
Well Hydraulic Conductivity (k)Seepage Velocity (v)
Page 1 of 1

APPENDICES

APPENDIX A
State Correspondence

August 18, 2020

Mr. Stephen Angel
Angel’s Inc.
P.O. Box 4395
Archdale, NC 27263-4395

Re: Notice of Regulatory Requirements 15A NCAC
2L .0407(c)
Risk-based Assessment and Corrective Action
for Petroleum Underground Storage Tanks

Trindale Mini Mart
7619 NC Highway 62
Trinity, Randolph County
Incident Number: 44719
Risk Classification: Intermediate
Ranking: I232D

Dear Mr. Angel:

The Limited Site Assessment Report received by the UST Section, Division of Waste Management,
Winston-Salem Regional Office on June 26, 2017 and a Groundwater Monitoring Report received on June
4, 2020 have been reviewed. The risk posed by the discharge or release at the subject site is classified by
the Department of Environmental Quality as intermediate, as stipulated under Title 15A NCAC 2L .0406.
The land use at the site is classified as industrial/commercial. Title 15A NCAC 2L .0407(a) requires you to
notify the Department of any changes that might affect the risk or land use classifications that have been
assigned.

Title 15A NCAC 2L .0407(c) requires you to comply with assessment and cleanup requirements of Title
15A NCAC 2N .0706 and Title15A NCAC 2L .0106(c) and 2L .0106(g). A Comprehensive Site
Assessment (CSA) Report prepared in accordance with these requirements and the most recent version of
the Guidelines for Assessment and Corrective Action for UST Releases must be received by this office
within 90 days of the date of this notice. In addition, you must submit a summary of the CSA Report to the
local Health Director and the local Chief Administrative Officer in accordance with 15A NCAC 2L .0114.
The summary should be submitted to these persons no later than five working days after submittal of the
CSA Report to this office. Failure to comply in the manner and time specified, may result in the assessment
of civil penalties and /or the use of other enforcement mechanisms.

Effective October 1, 2004, the Department requires that all work following the submittal of the Limited
Site Assessment Report (Title 15A NCAC 2L .0405) be preapproved if State Trust Fund reimbursement is
anticipated. To comply with this requirement, a completed Preapproval/Claim Authorization Form,

encompassing the required remedial activities, must be received in this office within 14 days of the date of
this letter. Upon completion of the preapproved activities, you should submit your claim promptly.
Reimbursement funds are budgeted based on completed preapprovals, but lengthy delays in reimbursement
can occur if claims are not submitted immediately following work completion.

Because a release or discharge has been confirmed, a Licensed Geologist or a Professional Engineer,
certified by the State of North Carolina, is required to prepare and certify all reports submitted to the
Department in accordance with Title 15A NCAC 2L .0103(e) and 2L .0111(b).

If you have any questions regarding trust fund eligibility or reimbursement from the Commercial or
Noncommercial Leaking Petroleum Underground Storage Tank Cleanup Funds, please contact the UST
Section Trust Fund Branch at [phone]. If you have any questions regarding the actions that must
be taken or the rules mentioned in this letter, please contact me at the address or telephone number listed
below.

Sincerely,

Doug Whitmire, PG
Hydrogeologist
Winston-Salem Regional Office
UST Section, Division of Waste Management, NCDEQ

cc: Randolph County Health Department

Site Name City / County /Randolph Incident #44719
Resp Pty Name / Contact Incident Mgr Region WS
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #8
Consultant / Project Mgr /Corey N. Buchanan
Telephone / Fax Number /Task Authorization Number:9 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I232D RRA Date:8/4/2017
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode RO AuthProposed
Rate/Price
(Consultant)CO AuthProposed Task
Subtotal
(Consultant)
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
1.050 1 /agreement y $300.00 y $300.00 $300.00 /
3.101 175 /feet y $12.50 y $2,187.50 $2,187.50 /
3.101 65 /feet y $18.00 y $1,170.00 $1,170.00 /
3.113 175 /feet y $50.00 y $8,750.00 $8,750.00 /
3.115 65 /feet y $75.00 y $4,875.00 $4,875.00 /
3.351 6 /wells y $80.00 y $480.00 $480.00 /
3.398 1 /event y $350.00 y $350.00 $350.00 /
4.031 6 /wells y $110.00 y $660.00 $660.00 /
2.087 2 /wells y $50.00 y $100.00 $100.00 /
4.090 #240 7 /samples y $88.00 y $616.00 $616.00 /
4.090 #301 6 /samples y $196.00 y $1,176.00 $1,176.00 /
4.090 #341 6 /samples y $52.00 y $312.00 $312.00 /
4.090 #342 6 /samples y $94.00 y $564.00 $564.00 /
4.090 #590 1 /sample y $35.00 y $35.00 $35.00 /
4.090 #640 2 /samples y $121.00 y $242.00 $242.00 /
4.091 1 /shipment y $80.00 y $80.00 $80.00 /
5.010 1 /event y $1,300.00 y $1,300.00 $1,300.00 /
6.050 1 /report y $4,400.00 y $4,400.00 $4,400.00 /
6.174 1 /property y $500.00 y $500.00 $500.00 /
12.050 3 /trips y $250.00 n $750.00 $500.00 /
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$28,847.50 $28,597.50 TOTAL:
Total Standard Costs (Not Third Party)$28,847.50 $28,597.50 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:9/23/20 by:(PM)(Reserved for RO)
RO Review:10/1/20 by:(IM)Joint UST Preapproval Confirmed By:Date1 10/2/2020
CO Review:10/2/20 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 8/1/2020
CNB
Proposed
Units / Type
(Consultant)
Doug Whitmire
ActiveTRUE
20-459 September 2020
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
Angel's Inc.Ms. Angel
Geological Resources, Inc.
DIRECTED COSTS
Trinity
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Trindale Mini Mart
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed,incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order"in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Pleaseattach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion date of the FIRST completed task to remain within the Statute of Limitations.All ePATAs submitted within a claim are closed with
that claim,and may not be re-used in a separate submittal,even forcosts or tasks that were not originally claimed.Finalreimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
DLW
SCR
(Initials)
Doug Whitmire
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
The slug test task includes travel so teh mobe request for this is not allowed.
Site Name City / County /Randolph Incident #44719
Resp Pty Name / Contact Incident Mgr Region WS
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #9
Consultant / Project Mgr /Henry Wells
Telephone / Fax Number /Task Authorization Number:9 ChangeOrd:1
Project Mgr Email Site Risk / Rank / Abatement:I232D RRA Date:8/4/2017
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode RO AuthProposed
Rate/Price
(Consultant)CO AuthProposed Task
Subtotal
(Consultant)
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
3.080 1 /permit y $250.00 y $250.00 $250.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$250.00 $250.00 TOTAL:
Total Standard Costs (Not Third Party)$250.00 $250.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:7/20/21 by:(PM)(Reserved for RO)
RO Review:7/21/21 by:(IM)Joint UST Preapproval Confirmed By:Date1 7/26/2021
CO Review:7/23/21 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee and returned to the Trust Fund within a week of approval. Signature
indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work proceeding. Scope/cost
negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the UST Section and RP
is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 8/1/2020
DIRECTED COSTS
Trinity
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Trindale Mini Mart
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed,incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order"in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Pleaseattach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion date of the FIRST completed task to remain within the Statute of Limitations.All ePATAs submitted within a claim are closed with
that claim,and may not be re-used in a separate submittal,even forcosts or tasks that were not originally claimed.Finalreimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
DLW
SCR
(Initials)
Doug Whitmire
HW
Proposed
Units / Type
(Consultant)
Doug Whitmire
ActiveTRUE
20-459 August 2021
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
Yes
[e-mail]
Angel's Inc.Ms. Angel
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
7/26/2021
Site Name City / County /Randolph Incident #44719
Resp Pty Name / Contact Incident Mgr Region WS
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #9
Consultant / Project Mgr /Joanna R Alley
Telephone / Fax Number /Task Authorization Number:10 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I232D RRA Date:8/4/2017
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode
RO IM AuthProposed
Rate/Price
(Consultant)RO Supv. AuthProposed Task
Subtotal
(Consultant)
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
1.050 1 /agreement y $300.00 y $300.00 $300.00 /
3.080 1 /permit y $250.00 y $250.00 $250.00 /
3.101 70 /feet y $12.50 y $875.00 $875.00 /
3.113 70 /feet y $50.00 y $3,500.00 $3,500.00 /
3.351 2 /wells y $80.00 y $160.00 $160.00 /
3.398 1 /event y $350.00 y $350.00 $350.00 /
4.031 13 /wells y $110.00 y $1,430.00 $1,430.00 /
4.090 #240 14 /samples y $88.00 y $1,232.00 $1,232.00 /
4.090 #301 13 /samples 2 $196.00 y $2,548.00 $392.00 /
4.090 #341 2 /samples y $52.00 y $104.00 $104.00 /
4.090 #342 2 /samples y $94.00 y $188.00 $188.00 /
4.091 1 /shipment y $80.00 y $80.00 $80.00 /
6.050 1 /report y $4,400.00 y $4,400.00 $4,400.00 /
6.082 1 /site y $500.00 y $500.00 $500.00 /
12.050 1 /trip y $250.00 y $250.00 $250.00 /
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$16,167.00 $14,011.00 TOTAL:
Total Standard Costs (Not Third Party)$16,167.00 $14,011.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:1/6/22 by:(PM)(Reserved for RO)
RO Review:1/27/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 2/1/2022
RO Supv. Review:1/31/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted
in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work
proceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the
UST Section and RP is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 8/1/2020
DIRECTED - CAB ONLY
Trinity
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Trindale Mini Mart
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborate on the costs for the tasks listed below that describes the scope of work and the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed,incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order"in the provided space above prior to conducting those tasks.Include a copy of the prior ePATA form for confirmation.Pleaseattach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion date of the FIRST completed task to remain within the Statute of Limitations.All ePATAs submitted within a claim are closed with
that claim,and may not be re-used in a separate submittal,even forcosts or tasks that were not originally claimed.Finalreimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
DLW
LE
(Initials)
Doug Whitmire
JRA
Proposed
Units / Type
(Consultant)
Doug Whitmire
ActiveTRUE
22-020 February 2022
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
Angels, Inc.Joan Angel
Geological Resources, Inc.
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
DLW-Proposed SOW will bring total CSA work to $45,014.50 pre-approved. SOW is to drill 2 shallow
wells to help delineate horizontal extent.
Note: well screens should not extend below the water table by more than 10 feet.LE
CSA costs are being moved from TA 44719-9 to this TA.
Task 4.090, code 301-Analyze only two new monitorng wells. (The constituent concentrations found under 625 thus far
indicate that they are not the leaders for this intermediate-risk site.) LE
Note: The above changes brings the total CSA pre-approved costs to $38,708.
2/11/22
4236 Received FEB 22 2022
Site Name City / County /Randolph Incident #44719
Resp Pty Name / Contact Incident Mgr Region WS
RP Type (Owner/Operator / Landowner / Attny-in-fact)Change Order?Prev. TA #10
Consultant / Project Mgr /Joanna Alley
Telephone / Fax Number /Task Authorization Number:11 ChangeOrd:
Project Mgr Email Site Risk / Rank / Abatement:I-232-D RRA Date:8/4/2017
Proposal# / Scope Dates /% Commercial (C=100%, NC=0%, Both=1%-99%)
Has STF Eligibility Been Determined? (Y/N)Site Status (Active or NFA Date)
With Claim: [ ] All Main Consultant/Contractor invoices attached?[ ] Proof of payment attached directly to the front of each invoice?
Important: The date of reimbursement is dependent on the Trust Fund balance. There may be a delay in the reimbursement of claims for work under this ePATA.3rd Pty Ded?Task #Lab /
SubCode
RO IM AuthProposed
Rate/Price
(Consultant)RO Supv. AuthProposed Task
Subtotal
(Consultant)
Final
Preapproved
Subtotal
(UST Section)
Claimed
Amount3
(Consultant)
3.118 70 /feet y $5.00 Y $350.00 $350.00 /
3.397 1 /Mobe y $100.00 Y $100.00 $100.00 /
4.090 #240 14 /samples y $6.00 Y $84.00 $84.00 /
4.090 #301 2 /samples y $12.00 Y $24.00 $24.00 /
4.090 #341 2 /samples y $4.00 Y $8.00 $8.00 /
4.090 #342 2 /samples y $6.00 Y $12.00 $12.00 /
12.055 1 /trip y $50.00 Y $50.00 $50.00 /
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
//
Requested Preapproved Claimed 3
TOTAL:$628.00 $628.00 TOTAL:
Total Standard Costs (Not Third Party)$628.00 $628.00 Total Standard Costs
Total applied as Third Party Deductible/Damage Costs $0.00 $0.00 Total Third Pty Costs
Process Tracking (Date)
TA Submittal:12/9/22 by:(PM)(Reserved for RO)
RO Review:12/9/22 by:(IM)Joint UST Preapproval Confirmed By:Date1 12/12/2022
RO Supv. Review:12/12/22 by:(STF)RP or Designee Receipt Confirmation By:Date 4
1 - This ePATA expires one year from the Joint UST Preapproval date. This does not extend, alter, or supersede any regulatory deadlines (e.g., NORR's, NOV's, Enforcements, etc.)
2 - THE ONE YEAR STATUTE OF LIMITATIONS APPLIES TO EACH INDIVIDUAL TASK. Costs must be claimed within one year of completion of that task to be reimbursable.
3 - Only Tasks included on this ePATA may be claimed. Do not include other Tasks or claimed costs (i.e., Claim preparation) that were not preapproved or the claim will be returned.
4 - Preapproval is not valid (i.e., claimable) until receipt is signed as 'Confirmed' by the RP or their designee within a week of approval. The signed pre-approval must be submitted
in the submitted claim. Signature indicates acknowledgement of the tasks and amounts approved. Any objections/appeals must be submitted via Change Order prior to work
proceeding. Scope/cost negotiations do not supersede other regulatory deadlines as described in #1 above. Also, any ePATA that has been signed as 'Confirmed' by both the
UST Section and RP is not to be modified without written consent by all signatories.
5 - Tasks approved on Directed - CAB Only ePATAs must be performed in accordance with all applicable rules, statutes, and RRD Task Scopes of Work to be reimbursed in full.
DWM/UST ePATA 4/1/2022
JA
Proposed
Units / Type
(Consultant)
Ryan Bond
ActiveYes
22-020 Jun-22
704-845-4012
Dates of Work
(Consultant)
Started1 / Completed2
FINAL REIMBURSEMENT
100.00%
[e-mail]
Angels, Inc
Geological Resources, Inc.
DIRECTED - CAB ONLY
Trinity
(Must Complete with Claim Submittal)(See Instructions / RRD for Tasks requiring Preapproval / Task Authorization)
Owner/Operator
704-845-4010
(Reserved for Incident Manager)
PREAPPROVAL / TASK AUTHORIZATION
Trindale Mini Mart
Note:This Electronic Preapproval Task Authorization (ePATA)shall be used to receive preapproval from the UST Section.A proposal,including maps and figures,must be
attached to elaborateon the costs for the tasks listed below that describes the scope of workand the rationale for the proposed activities.If,following completion of this ePATA,
you discover that unexpected tasks must be performed, incurring costs for tasks not originally included with this form,you must complete and submit a separate ePATA request
designated as a "Change Order" inthe provided space above prior to conducting those tasks.Include a copy of the prior ePATAform for confirmation.Please attach this form to
the cover of the corresponding claim when requesting reimbursement.IMPORTANT:Only one claim may be submitted per ePATA and all work on the ePATA must have been
completed within 12 months of the completion date of the FIRST completed task to remain withintheStatuteof Limitations.All ePATAs submittedwithinaclaim are closed with that
claim,and may not be re-used in a separate submittal,even for costs or tasks that were not originally claimed.Final reimbursement of costs associated with the Total Claimed
amount below may be affected by the eligibility status of the site (i.e.,deductibles,apportionment,etc.),and the documentary validation of incurred costs as reasonable and
necessary expenses per 15A NCAC 2P .0402 and .0404.
RAB
JWB
(Initials)
ELECTRONIC PREAPPROVAL TASK AUTHORIZATION FORM
Dept of Environmental Quality -Division of Waste Management
12/12/22
1
Joanna Alley
From:Bond, Ryan A <[e-mail]>
Sent:Wednesday, January 11, 2023 9:21 AM
To:Joanna Alley
Subject:RE: [External] Trindale Mini Mart
Hi Joanna,

If the GCLs are defined, I agree.

Thanks,

Ryan A. Bond, P.G.
Environmental Program Consultant, UST Section
Division of Waste Management, NCDEQ
Winston-Salem Regional Office
336-776-9679 (Office)
[e-mail]

Samples collected from active UST systems should be analyzed for oxygenates

All UST Section “deliverables/documents” (letters, reports, recorded NRPs etc.) must be submitted
electronically to the appropriate Incident Manager (See below for county assignments and contact
information). If a document is too large to send via email, please contact the appropriate Incident
Manager for instructions. Please provide a responsible party email address with each submittal,
if available.

COUNTY ASSIGNMENTS (Subject to Change. Check List Frequently):
Guilford County: Gene Mao (336-641-3589) Ashley Dinkins (336-641-5557) Jordan Lerew (336-641-3541)
Christina Schroeter: Ashe and Forsyth (336-776-9683)
Mindy Lepard: Alamance and Surry (336-776-9686)
Linda Estkowski: Caswell, Davie, Rockingham, Stokes, Watauga, Yadkin (336-776-9680)
Ryan Bond: Alleghany, Davidson, Randolph, Wilkes (336-776-9679)
Karen Hall: All counties and phases through the LSA, Complaints and Spills (336-776-9681)
Samantha Kofroth: Noncommercial/Nonregulated USTs and Non-UST releases (336-776-9687)
Doug Whitmire: Soil Permits (336-776-9685)
Shelia McIntosh: File Reviews (336-776-9630)

2
ALL UST ARCHIVED FILES CAN BE FOUND ON THE FOLLOWING LINK:
https://deq.nc.gov/about/divisions/waste-management/laserfiche
DWM LOCATOR TOOL: USE MAP FOR LOCATING UST SITES ACROSS THE STATE:
https://ncdenr.maps.arcgis.com/apps/webappviewer/index.html?id=7dd59be2750b40bebebfa49fc383f688
UST FACILITY DATABASE (Facility Permitting and Inspection Documents):
https://xapps.ncdenr.org/wm/docs/WMDocs_Search.jsp

From: Joanna Alley <[e-mail]>
Sent: Tuesday, January 10, 2023 12:31 PM
To: Bond, Ryan A <[e-mail]>
Subject: [External] Trindale Mini Mart

CAUTION: External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
Report Spam.

Good Afternoon Ryan,

We just received the analytical for Trindal Mini Mart and it looks like GCLs are defined with the installation of the new
wells. Based on the site being Intermediate Risk, would you agree that this site is sufficiently defined or would like
additional wells installed to define to MACs?

Best Regards,
Joanna Alley, P.E.
Project Manager
Geological Resources, Inc.
2021 Winner of the Union County Chamber Excellence In Business Award
3502 Hayes Road | Monroe, NC 28110 | website | facebook |
704-845-4010-office | 704-698-1244-direct | 704-845-4012-fax

APPENDIX B
Site-Specific Health and Safety Plan

APPENDIX C
Well Photographs
Trindale Mini Mart
Trinity, North Carolina

MW-6

MW-7
Trindale Mini Mart
Trinity, North Carolina

MW-8

MW-9

Trindale Mini Mart
Trinity, North Carolina

MW-10

MW-11 MW-12

APPENDIX D
Well Permit, Well Construction Records, and Subsurface Logs

North Carolina Department of Environmental Quality | Division of Water Resources
Winston-Salem Regional Office | 450 W. Hanes Mill Rd, Suite 300 | Winston-Salem, North Carolina 27105
336.776.9800

December 2, 2022

Ms. Joan Angel
Angels Inc. DBA Trindale Mini Mart
7619 NC Highway 62
Trinity, North Carolina 27370

SUBJECT: MONITORING WELL CONSTRUCTION
PERMIT NO. WM0401416
COUNTY: Randolph
FILE NAME: 7613 NC Highway 62

Dear Ms. Angel:

In accordance with your application received on November 30, 2022, we are forwarding herewith:

1. Monitoring Well Construction Permit No. WM0401416 for the construction of one (1)
monitoring well at 7613 NC Highway 62 in Trinity in Randolph County.

Henceforth, correspondence and data relating to these wells shall be designated as specified in the
subject heading above. This Permit will be effective from the date of issuance and shall be subject
to the conditions and limitations as specified therein. If you have any questions regarding this
permit, please contact me or Jim Gonsiewski at [phone].

Sincerely,

Lon T. Snider
Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ - WSRO

cc: Doug Woodgeard (Electronic Copy)
Joanna Alley – Geological Resources, Inc. (Electronic Copy)

North Carolina Department of Environmental Quality | Division of Water Resources
Winston-Salem Regional Office | 450 W. Hanes Mill Rd, Suite 300 | Raleigh, North Carolina 27105
336.776.9800

NORTH CAROLINA
DEPARTMENT OF ENVIRONMENTAL QUALITY
DIVISION OF WATER RESOURCES – WATER QUALITY REGIONAL OPERATIONS
SECTION

PERMIT FOR THE CONSTRUCTION OF A MONITORING WELL

In accordance with the provisions of Article 7, Chapter 87, North Carolina General Statutes, and
other applicable Laws, Rules and Regulations.

PERMISSION IS HEREBY GRANTED TO

Angels Inc. DBA Trindale Mini Mart

FOR THE CONSTRUCTION OF A MONITOR WELL SYSTEM consisting of one (1)
monitoring well owned by Angels Inc. DBA Trindale Mini Mart. The well will be located at 7613
NC Highway 62 in Trinity, North Carolina, in Randolph County. This Permit is issued in
accordance with the application received on November 30, 2022 in conformity with specifications
and supporting data, all of which are filed with the Department of Environmental Quality and are
considered integral parts of this Permit.

This Permit is for well construction only and does not waive any provision or requirement of any
other applicable law or regulation. Construction of any well under this Permit shall be in strict
compliance with the North Carolina Well Construction Regulations and Standards (15A NCAC
02C .0100), and other State and Local Laws and regulations pertaining to well construction.

If any requirements or limitations specified in this Permit are unacceptable, you have a right to an
adjudicatory hearing upon written request within 30 days of receipt of this Permit. The request
must be in the form of a written petition conforming to Chapter 150B of the North Carolina General
Statutes and filed with the Office of Administrative Hearings, 6714 Mail Service Center, Raleigh,
North Carolina 27699-6714. Unless such a demand is made, this Permit is final and binding.

This Permit will be effective for one year from the date of its issuance and shall be subject to other
specified conditions, limitations, or exceptions as follows:

North Carolina Department of Environmental Quality | Division of Water Resources
Winston-Salem Regional Office | 450 W. Hanes Mill Rd, Suite 300 | Raleigh, North Carolina 27105
336.776.9800

1. Issuance of this Permit does not obligate reimbursement from State trust funds, if these
wells are being installed as part of an investigation for contamination from an underground
storage tank or dry cleaner incident.
2. Issuance of this Permit does not supersede any other agreement, permit, or requirement
issued by another agency.
3. The well(s) shall be located and constructed as shown on the attachments submitted as part
of the Permit application.
4. Each well shall have a Well Contractor Identification Plate in accordance with 15A NCAC
02C .0108(o).
5. Well construction records (GW-1) for each well shall be submitted to the Division of Water
Resources’ Information Processing Unit within 30 days of the well completion.
6. When the well is discontinued or abandoned, it shall be abandoned in accordance with 15A
NCAC 02C .0113 and a well abandonment record (GW-30) shall be submitted to the
Division of Water Resources’ Information Processing Unit within 30 days of the well
abandonment.
7. The County Health Department may require a county monitoring well construction permit.
Please contact the health department for their requirements.

Permit issued the 2nd day of December, 2022

FOR THE NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION

_______________________________________________
Lon T. Snider, Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources, NCDEQ - WSRO

By Authority of the Environmental Management Commission

Permit No. WM0401416

Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-6
6"
35
Well installed at completion
0 0.5 Asphalt
0.5 14 Silty Clay Red-brown Dry None
14 35 Clayey Silt Orange-brown Moist Present

Photo 1: Preclearing Photo 2: Completion
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-6
6"
101.53
19
13 35
11 13
0 11
0 15 2
15 35 2
11
13
35
15
35

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Sam Bowers
3220-A
Geological Resources, Inc.
8/18/2021 MW-6
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, 27370
Randolph 7708757085
35.903109 79.986786
1
35
19
6"
Solid Stem Auger
19 35 Clayey Silt
0 15 2 Sch 40 PVC
15 35 2 0.010 Sch 40 PVC
0 11 grout pour
11 13 bentonite pour
13 35 #2 Sand Pour
0 0.5 Asphalt
0.5 14 Silty Clay
14 35 Clayey Silt
8/18/2021
_______________
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-7
6"
35
Well installed at completion
0 0.5 Asphalt
0.5 16 Silty Clay Red-brown Dry None
16 35 Clayey Silt Tan Moist Present

Photo 1: Preclearing Photo 2: Completion
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-7
6"
102.55
23
13 35
11 13
0 11
0 15 2
15 35 2
11
13
35
15
35

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Sam Bowers
3220-A
Geological Resources, Inc.
8/18/2021 MW-7
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, 27370
Randolph 7708757085
35.903109 79.986786
1
35
23
6"
Solid Stem Auger
23 35 Clayey Silt
0 15 2 Sch 40 PVC
15 35 2 0.010 Sch 40 PVC
0 11 grout pour
11 13 bentonite pour
13 35 #2 Sand Pour
0 0.5 Asphalt
0.5 16 Silty Clay
16 35 Clayey Silt
8/18/2021
_______________
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-8
6"
35
Well installed at completion
0 0.5 Concrete
0.5 30 Silty Clay Red-brown Dry None
30 35 Silty Clay Light bown Moist None

Photo 1: Preclearing Photo 2: Completion
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-8
6"
102.18
20
13 35
11 13
0 11
0 15 2
15 35 2
11
13
35
15
35

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Sam Bowers
3220-A
Geological Resources, Inc.
8/18/2021 MW-8
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, 27370
Randolph 7708757085
35.903109 79.986786
1
35
20
6"
Solid Stem Auger
20 35 Silty Clay
0 15 2 Sch 40 PVC
15 35 2 0.010 Sch 40 PVC
0 11 grout pour
11 13 bentonite pour
13 35 #2 Sand Pour
0 0.5 Concrete
0.5 30 Silty Clay
30 35 Silty Clay
8/18/2021
_______________
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-9
6"
35
Well installed at completion
0 0.5 Concrete
0.5 14 Silty clay Red-brown Dry None
14 35 Clayey silt Tan Moist Present

Photo 1: Preclearing Photo 2: Completion
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-9
6"
100.70
20
13 35
11 13
0 11
0 15 2
15 35 2
11
13
35
15
35

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Sam Bowers
3220-A
Geological Resources, Inc.
8/18/2021 MW-9
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, 27370
Randolph 7708757085
35.903109 79.986786
1
35
20
6"
Solid Stem Auger
20 35 Silty clay
0 15 2 Sch 40 PVC
15 35 2 0.010 Sch 40 PVC
0 11 grout pour
11 13 bentonite pour
13 35 #2 Sand Pour
0 0.5 Concrete
0.5 14 Silty clay
14 35 Clayey silt
8/18/2021
_______________
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-10
6"
30
Well installed at completion
0 10 Silty clay Dark red Dry None
10 11 Clayey silt White-tan Dry None
11 30 Silty clay Tan-brown Moist Present

Photo 1: Preclearing Photo 2: Completion
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Trindale Mini Mart
4236
8/18/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Solid Stem Auger
3220-A
MW-10
6"
94.97
18
8 30
6 8
0 6
0 10 2
10 30 2
6
8
30
10
30

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Sam Bowers
3220-A
Geological Resources, Inc.
8/18/2021 MW-10
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, 27370
Randolph 7708757085
35.903109 79.986786
1
30
18
6"
Solid Stem Auger
18 30 Silty clay
0 10 2 Sch 40 PVC
10 30 2 0.010 Sch 40 PVC
0 6 grout pour
6 8 bentonite pour
8 30 #2 Sand Pour
0 10 Silty clay
10 11 Clayey silt
11 30 Silty clay
8/18/2021
_______________
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236 Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-11
6"
35
Well installed at completion
0 0.5 Asphalt
0.5 17 Clayey Silt Red-brown Moist None
17 24 Silt Orange-brown Moist None
24 30 Silt Brown Moist None
30 35 Silt Brown Wet None

Photo 1: Preclearing Photo 2: Completion
12/19/2022
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Trindale Mini Mart
4236 Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-11
6"
103.47
30.55
18 35
16 18
0 16
0 20 2
20 35 2
16
18
35
20
35
12/19/2022

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Matt Steele
4548-A
Geological Resources, Inc.
WM0401416
MW-11
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, NC 27370
Randolph 7708757085
35.903109 79.986786
1
35
30.55
6"
Solid Stem Auger
19 35 Clayey silt
0 20 2 Sch 40 PVC
20 35 2 0.010 Sch 40 PVC
0 16 grout pour
16 18 bentonite pour
18 35 #2 Sand Pour
0 0.5 Asphalt
0.5 17 Clayey Silt
17 24 Silt
24 30 Silt
30 35 Silt
_______________
12/19/2022
12/19/2022
12/19/2022
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236
12/19/2022
Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-12
6"
35
Well installed at completion
0 0.5 Concrete
0.5 10 Silty clay Red-brown Moist None
10 27 Silt Orange-brown Moist None
27 31 Clay with trace silt Brown Wet None
31 35 Clay with trace silt Brown Moist None

Photo 1: Preclearing Photo 2: Completion
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
Sand
Bentonite
Grout
Screen
Casing
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
DIAGRAM - MONITORING WELL
Sand
Bentonite
Grout Screen
Inner Casing
Outer Casing
Trindale Mini Mart
4236
12/19/2022
Eric Eubanks
Geological Resources, Inc.
Matt Steele
Solid Stem Auger
4548-A
MW-12
6"
99.96
27.34
18 35
16 18
0 16
0 20 2
20 35 2
16
18
35
20
35

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Matt Steele
4548-A
Geological Resources, Inc.
N/A
12/19/2022 MW-12
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, NC 27370
Randolph 7708757085
35.903109 79.986786
1
35
27.34
6"
Solid Stem Auger
0 20 2 Sch 40 PVC
20 35 2 0.010 Sch 40 PVC
0 16 grout pour
16 18 bentonite pour
18 35 #2 Sand Pour
0 0.5 Concrete
0.5 10 Silty clay
10 27 Silt
27 31 Clay with trace silt
31 35 Clay with trace silt
12/19/2022
_______________
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Depth:
Diameter:Completion Details:
PID Lab
From To (ppm)Sample Description Color Moisture Odor
Depth (ft)Lithology
SITE INFORMATION
DRILLING INFORMATION
BORING INFORMATION
Trindale Mini Mart
4236
8/19/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Mud Rotary
3220-A
TW-1
4.5"
65
Well installed at completion
0 0.5 Concrete
0.5 14 Silty clay Red/brown Dry None
14 26 Clayey silt Tan/brown Moist None
26 47 Clayey silt Tan/grey Moist Present
47 50 Fine sandy silt Tan Moist Present
50 65 Weathered rock

Photo 1: Preclearing Photo 2: Completion
Site Name:Date:
Project Number:Log Completed By:
Company:Drill Type:
Driller:License Number:
Boring ID:Top of Casing:
Diameter:Depth to Water:
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
From (ft)To (ft)From (ft)To (ft)Diameter (in)
SITE INFORMATION
DRILLING INFORMATION
WELL CONSTRUCTION INFORMATION
Sand Outer Casing
Bentonite
Grout
Inner Casing
Screen
Screen
Bentonite
Sand
DIAGRAM - TELESCOPING WELL
Grout
Outer
Casing
Inner Casing
Trindale Mini Mart
4236
8/19/2021
Stephanie Gainey
Geological Resources, Inc.
Sam Bowers
Mud Rotary
3220-A
TW-1
4.5"
100.35
18
58 65
56 58
0 56
0 50 5
0 60 2
60 65 2
56
58
65
50
60
65

WELLCONSTRUCTIONRECORD
Thisformcanbeusedforsingleormultiplewells
FormGW-1 NorthCarolinaDepartmentofEnvironmentandNaturalResources–DivisionofWaterResources RevisedAugust2013
1.WellContractorInformation:

WellContractorName

NCWellContractorCertificationNumber

CompanyName

2.WellConstructionPermit#:
List all applicable well permits (i.e. County, State, Variance, Injection, etc.)

3.WellUse(checkwelluse):
WaterSupplyWell:
□Agricultural□Municipal/Public
□Geothermal(Heating/CoolingSupply)□ResidentialWaterSupply(single)
□Industrial/Commercial□ResidentialWaterSupply(shared)
□Irrigation
Non-WaterSupplyWell:
□Monitoring□Recovery
InjectionWell:
□AquiferRecharge□GroundwaterRemediation
□AquiferStorageandRecovery□SalinityBarrier
□AquiferTest□StormwaterDrainage
□ExperimentalTechnology□SubsidenceControl
□Geothermal(ClosedLoop)□Tracer
□Geothermal(Heating/CoolingReturn)□Other(explainunder#21Remarks)

4.DateWell(s)Completed:____________WellID#______________________

5a.WellLocation:

Facility/OwnerNameFacilityID#(ifapplicable)

PhysicalAddress,City,andZip

CountyParcelIdentificationNo.(PIN)

5b.LatitudeandLongitudeindegrees/minutes/secondsordecimaldegrees:
(ifwellfield,onelat/longissufficient)

N W

6.Is(are)thewell(s):□Permanentor□Temporary

7.Isthisarepairtoanexistingwell:□Yesor□No
If this is a repair, fill out known well construction information and explain the nature of the
repair under #21 remarks section or on the back of this form.
8.Numberofwellsconstructed:
For multiple injection or non-water supply wells ONLY with the same construction, you can
submit one form.

9.Totalwelldepthbelowlandsurface: (ft.)
For multiple wells list all depths if different (example- 3@200’ and 2@100′)

10.Staticwaterlevelbelowtopofcasing:(ft.)
If water level is above casing, use “+”

11.Boreholediameter:(in.)

12.Wellconstructionmethod:
(i.e.auger,rotary,cable,directpush,etc.)

FORWATERSUPPLYWELLSONLY:
13a.Yield(gpm) Methodoftest:

13b.Disinfectiontype:Amount:

14.WATERZONES
FROMTODESCRIPTION
ft.ft.
ft.ft.
15.OUTERCASING(formulti-casedwells)ORLINER(ifapplicable)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
16.INNERCASINGORTUBING(geothermalclosed-loop)
FROMTODIAMETERTHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
17.SCREEN
FROMTODIAMETERSLOTSIZETHICKNESSMATERIAL
ft.ft.in.
ft.ft.in.
18.GROUT
FROMTOMATERIALEMPLACEMENTMETHOD&AMOUNT
ft.ft.
ft.ft.
ft.ft.
19.SAND/GRAVELPACK(ifapplicable)
FROMTOMATERIALEMPLACEMENTMETHOD
ft.ft.
ft.ft.
20.DRILLINGLOG(attachadditionalsheetsifnecessary)
FROMTODESCRIPTION(color,hardness,soil/rocktype,grainsize,etc.)
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
ft.ft.
21.REMARKS

22.Certification:

SignatureofCertifiedWellContractorDateBy signing this form, I hereby certify that the well(s) was (were) constructed in accordance
with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23.Sitediagramoradditionalwelldetails:Youmayusethebackofthispagetoprovideadditionalwellsitedetailsorwell
constructiondetails.Youmayalsoattachadditionalpagesifnecessary.

SUBMITTALINSTUCTIONS

24a.ForAllWells:Submit this formwithin30daysof completionof well
constructiontothefollowing:
DivisionofWaterResources,InformationProcessingUnit,
1617MailServiceCenter,Raleigh,NC27699-1617
24b.ForInjectionWellsONLY:Inadditiontosendingtheformtotheaddressin
24aabove,alsosubmitacopyofthisformwithin30 daysofcompletionof well
constructiontothefollowing:

DivisionofWaterResources,UndergroundInjectionControlProgram,
1636MailServiceCenter,Raleigh,NC27699-1636
24c.ForWaterSupply&InjectionWells:
Also submitone copyof this form within30days ofcompletionof
wellconstructiontothecountyhealthdepartment ofthecountywhere
constructed.
ForInternalUseONLY:
Sam Bowers
3220-A
Geological Resources, Inc.
8/19/2021 TW-1
Trindale Mini Mart 00-0-0000018398
7619 NC Highway 62, Trinity, 27370
Randolph 7708757085
35.903109 79.986786
1
65
18
4.5"
Mud Rotary
18 50 Clayey silt
50 65 Weathered rock
0 50 5 Sch 40 PVC
0 60 2 Sch 40 PVC
60 65 2 0.010 Sch 40 PVC
0 56 grout pour
56 58 bentonite pour
58 65 #2 Sand Pour
0 0.5 Concrete
0.5 14 Silty clay
14 26 Clayey silt
26 47 Clayey silt
47 50 Fine sandy silt
50 65 Weathered rock
8/19/2021
_______________

APPENDIX E
Laboratory Analytical Reports
Orlando, FL 09/16/21
Reissue #1
e-Hardcopy 2.0
Automated Report
95
SGS is the sole authority for authorizing edits or modifications to this document.Unauthorized modification of this report is strictly prohibited.Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas abouthow we can serve you better at:[e-mail]
1 of 95
FA88410
Florida ♦ 4405 Vineland Road ♦ Suite C-15 ♦ Orlando, FL 32811 ♦ tel: [phone] ♦ fax: [phone]

September 16, 2021

Mr. Henry Wells
Geological Resources Inc.
3502 Hayes Road
Monroe, NC 28110

RE: SGS North America Inc. - Orlando job FA88410 Reissue

Dear Mr. Wells,

The final report for job number FA88410 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

Oxygenates have been reported on sample #4.

SGS North America Inc. - Orlando apologies for any inconvenience this may have caused.
Please feel free to contact us if we can be of further assistance.

Sincerely,

SGS North America, Inc. - Orlando

2 of 95
FA88410
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................10
3.1: FA88410-1: MW-7 ........................................................................................................11
3.2: FA88410-2: MW-8 ........................................................................................................18
3.3: FA88410-3: MW-9 ........................................................................................................25
3.4: FA88410-4: MW-10 ......................................................................................................32
3.5: FA88410-5: TW-1 .........................................................................................................35
3.6: FA88410-6: MW-9-30' ..................................................................................................42
3.7: FA88410-7: MW-9-35' ..................................................................................................43
3.8: FA88410-8: TW-1-64' ...................................................................................................44
3.9: FA88410-9: TRIP BLANK ...........................................................................................45
Section 4: Misc. Forms ............................................................................................................48
4.1: Chain of Custody ...........................................................................................................49
Section 5: MS Volatiles - QC Data Summaries .....................................................................51
5.1: Method Blank Summary ................................................................................................52
5.2: Blank Spike Summary ...................................................................................................58
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................64
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................70
6.1: Method Blank Summary ................................................................................................71
6.2: Blank Spike Summary ...................................................................................................73
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................75
Section 7: GC Volatiles - QC Data Summaries .....................................................................77
7.1: Method Blank Summary ................................................................................................78
7.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................80
7.3: Duplicate Summary .......................................................................................................82
Section 8: GC/LC Semi-volatiles - QC Data Summaries .....................................................84
8.1: Method Blank Summary ................................................................................................85
8.2: Blank Spike/Blank Spike Duplicate Summary ..............................................................86
Section 9: Misc. Forms (SGS Dayton, NJ) .............................................................................88
9.1: Chain of Custody ...........................................................................................................89
Section 10: General Chemistry - QC Data (SGS Dayton, NJ) .............................................91
10.1: Method Blank and Spike Results Summary ................................................................92
10.2: Duplicate Results Summary ........................................................................................93
10.3: Matrix Spike Results Summary ...................................................................................94
10.4: Matrix Spike Duplicate Results Summary ..................................................................95 123456789103 of 95
FA88410
Sample Summary
Job No:
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
4 of 95
FA884101
Summary of Hits
Job Number:
Account:
Project:
Collected:
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA88410-1 MW-7
FA88410-2 MW-8
5 of 95
FA884102
Summary of Hits
Job Number:
Account:
Project:
Collected:
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA88410-3 MW-9
6 of 95
FA884102
Summary of Hits
Job Number:
Account:
Project:
Collected:
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA88410-4 MW-10
FA88410-5 TW-1
7 of 95
FA884102
Summary of Hits
Job Number:
Account:
Project:
Collected:
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA88410-6 MW-9-30'
FA88410-7 MW-9-35'
FA88410-8 TW-1-64'
8 of 95
FA884102
Summary of Hits
Job Number:
Account:
Project:
Collected:
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA88410-9 TRIP BLANK
9 of 95
FA884102
Orlando, FL
Section 3
10 of 95
FA884103
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
11 of 95
FA8841033.1
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
12 of 95
FA8841033.1
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
13 of 95
FA8841033.1
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
ABN Special List
CAS No.Compound Result RL MDL Units Q
14 of 95
FA8841033.1
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
ABN Special List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
15 of 95
FA8841033.1
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
16 of 95
FA8841033.1
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
MAEPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
17 of 95
FA8841033.1
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
18 of 95
FA8841033.2
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
19 of 95
FA8841033.2
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
20 of 95
FA8841033.2
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
ABN Special List
CAS No.Compound Result RL MDL Units Q
21 of 95
FA8841033.2
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
ABN Special List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
22 of 95
FA8841033.2
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
23 of 95
FA8841033.2
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
MAEPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
24 of 95
FA8841033.2
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
25 of 95
FA8841033.3
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
26 of 95
FA8841033.3
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
27 of 95
FA8841033.3
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
ABN Special List
CAS No.Compound Result RL MDL Units Q
28 of 95
FA8841033.3
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
ABN Special List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
29 of 95
FA8841033.3
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
30 of 95
FA8841033.3
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
MAEPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
31 of 95
FA8841033.3
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
32 of 95
FA8841033.4
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
33 of 95
FA8841033.4
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
34 of 95
FA8841033.4
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
35 of 95
FA8841033.5
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
36 of 95
FA8841033.5
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
37 of 95
FA8841033.5
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
ABN Special List
CAS No.Compound Result RL MDL Units Q
38 of 95
FA8841033.5
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
ABN Special List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
39 of 95
FA8841033.5
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
MADEP VPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
40 of 95
FA8841033.5
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Initial Volume Final Volume
MAEPH List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
41 of 95
FA8841033.5
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Percent Solids:
Project:
General Chemistry
Analyte Result RL Units DF Analyzed By Method
42 of 95
FA8841033.6
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Percent Solids:
Project:
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Particle Size Analysis (Sieve and Hydrometer Testing)
43 of 95
FA8841033.7
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Percent Solids:
Project:
General Chemistry
Analyte Result RL Units DF Analyzed By Method
Particle Size Analysis (Sieve and Hydrometer Testing)
44 of 95
FA8841033.8
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Purge Volume
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
45 of 95
FA8841033.9
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
46 of 95
FA8841033.9
Report of Analysis
Client Sample ID:
Lab Sample ID:Date Sampled:
Matrix:Date Received:
Method:Percent Solids:
Project:
VOA 6200B List
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
47 of 95
FA8841033.9
Orlando, FL
Section 4
48 of 95
FA884104
FA88410: Chain of Custody
Page 1 of 2
49 of 95
FA8841044.1
Job Number:FA88410 Client:GRI
Date / Time Received:8/26/2021 9:30:00 AM Delivery Method:FEDEX
Project:TRINDALE MINI MART
Airbill #'s:100963790710
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments TRIP BLANKS RECEIVED WITH HEADSPACE.SAMPLE 2 RECEIVED WITH TIME 13:20 ON LABELS INSTEAD OF 13:30.
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (5.6);
Cooler 1: (5.8);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:0.2; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:BRYANG Date:Date:8/26/2021 9:30:00 AM
FA88410: Chain of Custody
Page 2 of 2
50 of 95
FA8841044.1
Orlando, FL
Section 5
51 of 95
FA884105
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
52 of 95
FA8841055.1.1
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
53 of 95
FA8841055.1.1
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Surrogate Recoveries Limits
54 of 95
FA8841055.1.1
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
55 of 95
FA8841055.1.2
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
56 of 95
FA8841055.1.2
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Surrogate Recoveries Limits
57 of 95
FA8841055.1.2
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
58 of 95
FA8841055.2.1
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
59 of 95
FA8841055.2.1
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Surrogate Recoveries BSP Limits
60 of 95
FA8841055.2.1
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
61 of 95
FA8841055.2.2
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
62 of 95
FA8841055.2.2
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Surrogate Recoveries BSP Limits
63 of 95
FA8841055.2.2
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88410-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
64 of 95
FA8841055.3.1
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88410-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
65 of 95
FA8841055.3.1
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Surrogate Recoveries MS MSD FA88410-1 Limits
66 of 95
FA8841055.3.1
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88445-16 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67 of 95
FA8841055.3.2
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88445-16 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
68 of 95
FA8841055.3.2
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Surrogate Recoveries MS MSD FA88445-16 Limits
69 of 95
FA8841055.3.2
Orlando, FL
Section 6
70 of 95
FA884106
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
71 of 95
FA8841066.1.1
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
72 of 95
FA8841066.1.1
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
73 of 95
FA8841066.2.1
Blank Spike Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
CAS No.Surrogate Recoveries BSP Limits
74 of 95
FA8841066.2.1
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88411-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
75 of 95
FA8841066.3.1
Matrix Spike/Matrix Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88411-3 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
CAS No.Surrogate Recoveries MS MSD FA88411-3 Limits
76 of 95
FA8841066.3.1
Orlando, FL
Section 7
77 of 95
FA884107
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
78 of 95
FA8841077.1.1
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
79 of 95
FA8841077.1.2
Blank Spike/Blank Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
CAS No.Surrogate Recoveries BSP BSD Limits
80 of 95
FA8841077.2.1
Blank Spike/Blank Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
CAS No.Surrogate Recoveries BSP BSD Limits
81 of 95
FA8841077.2.2
Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88331-1 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
CAS No.Surrogate Recoveries DUP FA88331-1 Limits
82 of 95
FA8841077.3.1
Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
FA88410-5 DUP
CAS No.Compound ug/l Q ug/l Q RPD Limits
CAS No.Surrogate Recoveries DUP FA88410-5 Limits
83 of 95
FA8841077.3.2
Orlando, FL
Section 8
84 of 95
FA884108
Method Blank Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
CAS No.Compound Result RL MDL Units Q
CAS No.Surrogate Recoveries Limits
85 of 95
FA8841088.1.1
Blank Spike/Blank Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
Spike BSP BSP BSD BSD Limits
CAS No.Compound ug/l ug/l %ug/l %RPD Rec/RPD
CAS No.Surrogate Recoveries BSP BSD Limits
Sample Compound Col #1 Col #2 Breakthrough Limit
86 of 95
FA8841088.2.1
Blank Spike/Blank Spike Duplicate Summary
Job Number:
Account:
Project:
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
The QC reported here applies to the following samples:Method:
87 of 95
FA8841088.2.1
Orlando, FL
Section 9
88 of 95
FA884109
FA88410: Chain of Custody
Page 1 of 2
SGS Dayton, NJ
89 of 95
FA8841099.1
Job Number:FA88410 Client:
Date / Time Received:8/28/2021 10:40:00 AM Delivery Method:Fed Ex
Project:
4. No. Coolers:1
Airbill #'s:
Cooler Security
1. Custody Seals Present:
Y or N
2. Custody Seals Intact:
3. COC Present:
4. Smpl Dates/Time OK
2. Cooler temp verification:
Cooler Temperature Y or N
1. Temp criteria achieved:
3. Cooler media:
IR Gun
Ice (Bag)
Quality Control Preservation Y or N N/A
1. Trip Blank present / cooler:
2. Trip Blank listed on COC:
3. Samples preserved properly:
4. VOCs headspace free:
Sample Integrity - Documentation Y or N
1. Sample labels present on bottles:
2. Container labeling complete:
3. Sample container label / COC agree:
Sample Integrity - Condition Y or N
1. Sample recvd within HT:
3. Condition of sample:
2. All containers accounted for:
Sample Integrity - Instructions
1. Analysis requested is clear:
2. Bottles received for unspecified tests
3. Sufficient volume recvd for analysis:
4. Compositing instructions clear:
5. Filtering instructions clear:
Intact
Y or N
Comments
Y or N N/A
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (3.6);
Cooler 1: (2.7);
SM089-03
Rev. Date 12/7/17
SGS Sample Receipt Summary
Test Strip Lot #s:pH 1-12:212820 pH 12+:203117A Other: (Specify)
FA88410: Chain of Custody
Page 2 of 2
90 of 95
FA8841099.1
Orlando, FL
Section 10
91 of 95
FA8841010
METHOD BLANK AND SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA88410
Account: ALSE - SGS Orlando, FL
Project: GRINCC: Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
MB Spike BSP BSP QC
Analyte Batch ID RL Result Units Amount Result %Recov Limits
Total Organic Carbon GP35609/GN21555 1000 0.0 mg/kg 20000 20200 101.0 80-120%
Associated Samples:
Batch GP35609: FA88410-6
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
92 of 95
FA884101010.1
DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA88410
Account: ALSE - SGS Orlando, FL
Project: GRINCC: Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
QC Original DUP QC
Analyte Batch ID Sample Units Result Result RPD Limits
% Gravel GP35549/GN21781 JD30575-11 % 35.6 32.4 9.4 0-41%
% Sand GP35549/GN21781 JD30575-11 % 50.3 54.1 7.3 0-16%
% Silt, Clay, Colloids GP35549/GN21781 JD30575-11 % 14.1 13.5 4.3 0-40%
0.0015 mm (Hydrometer) GP35549/GN21781 JD30575-11 % 0.0 0.0 0.0 0-45%
0.005 mm (Hydrometer) GP35549/GN21781 JD30575-11 % 4.0 4.0 0.0 0-48%
0.030 mm (Hydrometer) GP35549/GN21781 JD30575-11 % 8.0 7.0 13.3 0-36%
0.375 Inch Sieve GP35549/GN21781 JD30575-11 % 77.7 73.9 5.1 0-14%
0.75 Inch Sieve GP35549/GN21781 JD30575-11 % 96.2 93.1 3.7 0-9%
1.5 Inch Sieve GP35549/GN21781 JD30575-11 % 100 100 0.0 0-20%
3 Inch Sieve GP35549/GN21781 JD30575-11 % 100 100 0.0 0-20%
No.10 Sieve (2.00 mm) GP35549/GN21781 JD30575-11 % 53.7 55.0 2.5 0-14%
No.100 Sieve (0.15 mm) GP35549/GN21781 JD30575-11 % 17.6 16.4 7.5 0-31%
No.16 Sieve (1.18 mm) GP35549/GN21781 JD30575-11 % 48.5 50.1 3.1 0-17%
No.200 Sieve (0.075 mm) GP35549/GN21781 JD30575-11 % 14.1 13.5 4.3 0-40%
No.30 Sieve (0.60 mm) GP35549/GN21781 JD30575-11 % 41.6 41.8 0.4 0-21%
No.4 Sieve (4.75 mm) GP35549/GN21781 JD30575-11 % 64.4 67.0 4.8 0-13%
No.50 Sieve (0.30 mm) GP35549/GN21781 JD30575-11 % 29.9 28.5 4.6 0-30%
No.8 Sieve (2.36 mm) GP35549/GN21781 JD30575-11 % 55.2 57.1 3.4 0-14%
Associated Samples:
Batch GP35549: FA88410-7, FA88410-8
(*) Outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
93 of 95
FA884101010.2
MATRIX SPIKE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA88410
Account: ALSE - SGS Orlando, FL
Project: GRINCC: Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
QC Original Spike MS QC
Analyte Batch ID Sample Units Result Amount Result %Rec Limits
Total Organic Carbon GP35609/GN21555 FA88445-11 mg/kg 0.00 33700 50400 149.7N(a) 10-113%
Associated Samples:
Batch GP35609: FA88410-6
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(a) Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.
__________________________________________________________________________________________________________________________
Page 1
94 of 95
FA884101010.3
MATRIX SPIKE DUPLICATE RESULTS SUMMARY
GENERAL CHEMISTRY
Login Number: FA88410
Account: ALSE - SGS Orlando, FL
Project: GRINCC: Trindale Mini Mart; 7619 NC Hwy 62, Trinity, NC
QC Original Spike MSD QC
Analyte Batch ID Sample Units Result Amount Result RPD Limit
Total Organic Carbon GP35609/GN21555 FA88445-11 mg/kg 0.00 33700 46900 5.0 31%
Associated Samples:
Batch GP35609: FA88410-6
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
__________________________________________________________________________________________________________________________
Page 1
95 of 95
FA884101010.4

Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.

1/10/2023

GeologicalResources,Inc.
JoannaAlley
3502HayesRoad
Monroe,NC,28110

Ref: AnalyticalTesting
LabReportNumber:22-354-0019
ClientProjectDescription:TrindaleMiniMart
GRI#4236

DearJoannaAlley:

WaypointAnalytical,LLC(Charlotte)receivedsample(s)on12/20/2022fortheanalysespresentedinthe
followingreport.

Theabovereferencedprojecthasbeenanalyzedperyourinstructions.Theanalyseswereperformedin
accordancewiththeapplicableanalyticalmethod.

Theanalyticaldatahasbeenvalidatedusingstandardqualitycontrolmeasuresperformedasrequiredbythe
analyticalmethod.QualityAssurance,methodvalidations,instrumentationmaintenanceandcalibrationforall
parameterswereperformedinaccordancewithguidelinesestablishedbytheUSEPA(including40CFR136
MethodUpdateRuleMay2021)unlessotherwiseindicated.

Certainparameters(chlorine,pH,dissolvedoxygen,sulfite...)arerequiredtobeanalyzedwithin15minutesof
sampling.Usually,butnotalways,anyfieldparameteranalyzedatthelaboratoryisoutsideofthisholdingtime.
Refertosampleanalysistimeforconfirmationofholdingtimecompliance.

TheresultsareshownontheattachedReportofAnalysis(s).Resultsforsolidmatricesarereportedonanas-
receivedbasisunlessotherwiseindicated.Thisreportshallnotbereproducedexceptinfullandrelatesonlyto
thesamplesincludedinthisreport.

Pleasedonothesitatetocontactmeorclientservicesifyouhaveanyquestionsorneedadditionalinformation.

Sincerely,
DanyaleLove
ProjectManager
Page 1 of 100
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State Program Lab ID Expiration Date
07/31/202337735State ProgramNorth Carolina
12/31/2023402State ProgramNorth Carolina
07/31/202399012State ProgramSouth Carolina
12/31/202299012State ProgramSouth Carolina
Page 1 of 1 00016/22-354-0019
Page 2 of 100
Report Number:
Sample Summary Table
Client Project Description:
22-354-0019
Trindale Mini Mart
GRI #4236
Lab No Client Sample ID Matrix Date Collected Date Received
12/20/2022 12:00Aqueous 96163 MW-2 12/20/2022 15:50
12/20/2022 13:22Aqueous 96164 MW-4 12/20/2022 15:50
12/20/2022 13:34Aqueous 96165 MW-5 12/20/2022 15:50
12/20/2022 13:15Aqueous 96166 MW-7 12/20/2022 15:50
12/20/2022 12:45Aqueous 96167 MW-8 12/20/2022 15:50
12/20/2022 13:00Aqueous 96168 MW-9 12/20/2022 15:50
12/20/2022 11:38Aqueous 96169 MW-10 12/20/2022 15:50
12/20/2022 11:00Aqueous 96170 MW-11 12/20/2022 15:50
12/20/2022 11:35Aqueous 96171 MW-12 12/20/2022 15:50
12/20/2022 13:55Aqueous 96172 TW-1 12/20/2022 15:50
12/20/2022Aqueous 96173 Trip Blanks 12/20/2022 15:50
Page 3 of 100
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-354-0019
Report Limit
Project:Trindale Mini Mart
V 96163MW-2
4.41 12/21/2022 17:036200BDi-Isopropyl Ether (DIPE)µg/L 0.500
35.2 12/21/2022 17:036200BMethyl tert-butyl ether (MTBE)µg/L 0.140
J6.49 12/21/2022 17:036200Btert-Butyl Alcohol (TBA)µg/L 1.60
J2.72 12/21/2022 17:036200Btert-Amyl Alcohol (TAA)µg/L 1.90
V 96164MW-4
10.4 12/21/2022 18:146200BBenzeneµg/L 0.180
5.60 12/21/2022 18:146200Bn-Butylbenzene µg/L 0.180
7.63 12/21/2022 18:146200Bsec-Butyl benzene µg/L 0.200
J1.19 12/21/2022 18:146200Btert-Butyl benzene µg/L 0.920
1.36 12/21/2022 18:146200BChloroformµg/L 0.220
30.0 12/21/2022 18:146200BDi-Isopropyl Ether (DIPE)µg/L 0.500
5.30 12/21/2022 18:146200BEthylbenzeneµg/L 0.170
5.90 12/21/2022 18:146200BIsopropylbenzeneµg/L 0.180
8.01 12/21/2022 18:146200B4-Isopropyl toluene µg/L 0.089
394 12/22/2022 19:166200BMethyl tert-butyl ether (MTBE)µg/L 1.40
2.41 12/21/2022 18:146200B4-Methyl-2-Pentanone µg/L 0.078
33.9 12/21/2022 18:146200BNaphthaleneµg/L 0.470
9.68 12/21/2022 18:146200Bn-Propylbenzene µg/L 0.190
52.2 12/21/2022 18:146200Btert-Amyl Alcohol (TAA)µg/L 1.90
J3.43 12/21/2022 18:146200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
1.87 12/21/2022 18:146200BTolueneµg/L 0.220
242 12/22/2022 19:166200B1,2,4-Trimethylbenzene µg/L 1.90
68.3 12/21/2022 18:146200B1,3,5-Trimethylbenzene µg/L 0.180
45.4 12/21/2022 18:146200Bo-Xylene µg/L 0.210
29.9 12/21/2022 18:146200Bm,p-Xylene µg/L 0.420
75.3 12/21/2022 18:146200BXylene (Total)µg/L 0.210
V 96165MW-5
2.46 12/21/2022 17:506200BBenzeneµg/L 0.180
5.04 12/21/2022 17:506200Bsec-Butyl benzene µg/L 0.200
J0.984 12/21/2022 17:506200Btert-Butyl benzene µg/L 0.920
0.668 12/21/2022 17:506200BChloroformµg/L 0.220
9.80 12/21/2022 17:506200BDi-Isopropyl Ether (DIPE)µg/L 0.500
3.48 12/21/2022 17:506200BIsopropylbenzeneµg/L 0.180
8.61 12/21/2022 17:506200B4-Isopropyl toluene µg/L 0.089
77.8 12/21/2022 17:506200BMethyl tert-butyl ether (MTBE)µg/L 0.140
36.2 12/21/2022 17:506200BNaphthaleneµg/L 0.470
Page 4 of 100
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-354-0019
Report Limit
Project:Trindale Mini Mart
V 96165MW-5
10.0 12/21/2022 17:506200Bn-Propylbenzene µg/L 0.190
90.5 12/21/2022 17:506200Btert-Butyl Alcohol (TBA)µg/L 1.60
282 12/22/2022 18:526200Btert-Amyl Alcohol (TAA)µg/L 19.0
J0.534 12/21/2022 17:506200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
184 12/22/2022 18:526200B1,2,4-Trimethylbenzene µg/L 1.90
96.6 12/22/2022 18:526200B1,3,5-Trimethylbenzene µg/L 1.80
6.27 12/21/2022 17:506200Bo-Xylene µg/L 0.210
26.4 12/21/2022 17:506200Bm,p-Xylene µg/L 0.420
32.7 12/21/2022 17:506200BXylene (Total)µg/L 0.210
V 96166MW-7
6.41 12/21/2022 21:506200BBenzeneµg/L 1.80
520 12/21/2022 21:506200BDi-Isopropyl Ether (DIPE)µg/L 5.00
85000 12/22/2022 21:596200BMethyl tert-butyl ether (MTBE)µg/L 140
11700 12/22/2022 21:596200Btert-Amyl Alcohol (TAA)µg/L 1900
377 12/21/2022 21:506200Btert-Amyl Methyl Ether (TAME)µg/L 2.80
J4.75 12/21/2022 21:506200Bo-Xylene µg/L 2.10
J5.25 12/21/2022 21:506200Bm,p-Xylene µg/L 4.20
J10.0 12/21/2022 21:506200BXylene (Total)µg/L 2.10
V 96167MW-8
J0.443 12/21/2022 19:516200Bn-Butylbenzene µg/L 0.180
0.545 12/21/2022 19:516200Bsec-Butyl benzene µg/L 0.200
6.42 12/21/2022 19:516200BChloroformµg/L 0.220
J0.226 12/21/2022 19:516200B4-Isopropyl toluene µg/L 0.089
J1.60 12/21/2022 19:516200Btert-Butyl Alcohol (TBA)µg/L 1.60
0.550 12/21/2022 19:516200BTetrachloroetheneµg/L 0.220
2.44 12/21/2022 19:516200B1,2,4-Trimethylbenzene µg/L 0.190
V 96168MW-9
121 12/22/2022 19:396200BBenzeneµg/L 1.80
11.8 12/21/2022 20:156200Bn-Butylbenzene µg/L 0.180
13.5 12/21/2022 20:156200Bsec-Butyl benzene µg/L 0.200
J1.46 12/21/2022 20:156200Btert-Butyl benzene µg/L 0.920
3.48 12/21/2022 20:156200BDi-Isopropyl Ether (DIPE)µg/L 0.500
2.63 12/21/2022 20:156200BEthylbenzeneµg/L 0.170
29.1 12/21/2022 20:156200BIsopropylbenzeneµg/L 0.180
19.6 12/21/2022 20:156200B4-Isopropyl toluene µg/L 0.089
Page 5 of 100
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-354-0019
Report Limit
Project:Trindale Mini Mart
V 96168MW-9
38.9 12/21/2022 20:156200BMethyl tert-butyl ether (MTBE)µg/L 0.140
7.32 12/21/2022 20:156200B4-Methyl-2-Pentanone µg/L 0.078
J0.434 12/21/2022 20:156200BMethylene Chloride µg/L 0.330
167 12/22/2022 19:396200BNaphthaleneµg/L 4.70
52.0 12/21/2022 20:156200Bn-Propylbenzene µg/L 0.190
24.4 12/21/2022 20:156200Btert-Butyl Alcohol (TBA)µg/L 1.60
92.7 12/21/2022 20:156200Btert-Amyl Alcohol (TAA)µg/L 1.90
J1.42 12/21/2022 20:156200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
1.29 12/21/2022 20:156200B1,2,4-Trimethylbenzene µg/L 0.190
J0.345 12/21/2022 20:156200B1,3,5-Trimethylbenzene µg/L 0.180
V 96169MW-10
16.3 12/21/2022 20:386200BNaphthaleneµg/L 0.470
V 96170MW-11
35.1 12/21/2022 21:026200BBenzeneµg/L 0.180
J0.304 12/21/2022 21:026200Bn-Butylbenzene µg/L 0.180
0.633 12/21/2022 21:026200Bsec-Butyl benzene µg/L 0.200
J0.365 12/21/2022 21:026200BChloroformµg/L 0.220
91.7 12/21/2022 21:026200BDi-Isopropyl Ether (DIPE)µg/L 0.500
J0.265 12/21/2022 21:026200B1,4-Dichlorobenzene µg/L 0.210
3930 12/22/2022 20:496200BMethyl tert-butyl ether (MTBE)µg/L 14.0
12.2 12/21/2022 21:026200BNaphthaleneµg/L 0.470
1070 12/22/2022 20:496200Btert-Amyl Alcohol (TAA)µg/L 190
23.5 12/21/2022 21:026200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
2.01 12/21/2022 21:026200B1,2,4-Trimethylbenzene µg/L 0.190
5.87 12/21/2022 21:026200Bo-Xylene µg/L 0.210
1.72 12/21/2022 21:026200Bm,p-Xylene µg/L 0.420
7.59 12/21/2022 21:026200BXylene (Total)µg/L 0.210
3.66 12/23/2022 15:36625.1 1-Methylnaphthalene µg/L 1.19
3.16 12/23/2022 15:36625.1 2-Methylnaphthalene µg/L 0.695
4.58 12/23/2022 15:36625.1 Naphthalene µg/L 0.760
1210 12/21/2022 21:02CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 115
J63.9 12/21/2022 14:02CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 25.8
J13.9 12/21/2022 14:02CALCULATIONAromatic C9-C10 (Adjusted)µg/L 4.02
J93.2 12/23/2022 15:36CALCULATIONAromatic C11-C22 (Adjusted)µg/L 63.4
JB20801/07/2023 04:20MADEP-EPH Aliphatic C9-C18 µg/L 29.2
J97.8 01/07/2023 04:20MADEP-EPH Aromatic C11-C22 µg/L 63.4
Page 6 of 100
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-354-0019
Report Limit
Project:Trindale Mini Mart
V 96170MW-11
1250 12/22/2022 08:31MADEP-VPH Aliphatic C5-C8 µg/L 115
85.4 12/21/2022 14:02MADEP-VPH Aliphatic C9-C12 µg/L 25.8
J13.9 12/21/2022 14:02MADEP-VPH Aromatic C9-C10 µg/L 4.02
V 96171MW-12
110 12/21/2022 22:146200Bn-Butylbenzene µg/L 1.80
134 12/21/2022 22:146200Bsec-Butyl benzene µg/L 2.00
33.0 12/21/2022 22:146200BIsopropylbenzeneµg/L 1.80
16.4 12/21/2022 22:146200B4-Isopropyl toluene µg/L 0.890
57.7 12/21/2022 22:146200BMethyl tert-butyl ether (MTBE)µg/L 1.40
17.3 12/21/2022 22:146200BNaphthaleneµg/L 4.70
26.6 12/21/2022 22:146200Bn-Propylbenzene µg/L 1.90
J56.3 12/21/2022 22:146200Btert-Butyl Alcohol (TBA)µg/L 16.0
J85.9 12/21/2022 22:146200Btert-Amyl Alcohol (TAA)µg/L 19.0
J1.52 12/23/2022 15:59625.1 Chrysene µg/L 0.417
8.64 12/23/2022 15:59625.1 Fluoranthene µg/L 0.257
93.7 12/23/2022 15:59625.1 Fluorene µg/L 0.831
196 12/23/2022 15:59625.1 1-Methylnaphthalene µg/L 1.17
141 12/23/2022 15:59625.1 2-Methylnaphthalene µg/L 0.685
165 12/23/2022 15:59625.1 Phenanthrene µg/L 0.440
40.4 12/23/2022 15:59625.1 Pyrene µg/L 0.447
540 12/21/2022 14:50CALCULATIONAliphatic C5-C8 (Adjusted)µg/L 115
6440 12/21/2022 14:50CALCULATIONAliphatics C9-C12 (Adjusted)µg/L 258
9360 12/21/2022 14:50CALCULATIONAromatic C9-C10 (Adjusted)µg/L 40.2
J15500012/23/2022 15:59CALCULATIONAromatic C11-C22 (Adjusted)µg/L 2520
350000 01/09/2023 16:47MADEP-EPH Aliphatic C9-C18 µg/L 1160
20800 01/09/2023 16:47MADEP-EPH Aliphatic C19-C36 µg/L 5110
155000 01/09/2023 16:47MADEP-EPH Aromatic C11-C22 µg/L 2520
540 12/21/2022 14:50MADEP-VPH Aliphatic C5-C8 µg/L 115
15800 12/21/2022 14:50MADEP-VPH Aliphatic C9-C12 µg/L 258
9360 12/21/2022 14:50MADEP-VPH Aromatic C9-C10 µg/L 40.2
V 96172TW-1
11.0 12/21/2022 21:266200BBenzeneµg/L 0.180
J0.326 12/21/2022 21:266200Bn-Butylbenzene µg/L 0.180
1.07 12/21/2022 21:266200Bsec-Butyl benzene µg/L 0.200
0.919 12/21/2022 21:266200BChloroformµg/L 0.220
12.5 12/21/2022 21:266200BDi-Isopropyl Ether (DIPE)µg/L 0.500
Page 7 of 100
Summary of Detected Analytes
QualifiersAnalyzedUnitsResult
Report Number:
Client Sample ID
Method Parameters
Lab Sample ID
22-354-0019
Report Limit
Project:Trindale Mini Mart
V 96172TW-1
1.37 12/21/2022 21:266200B1,2-Dichloroethane µg/L 0.150
J0.321 12/21/2022 21:266200BIsopropylbenzeneµg/L 0.180
370 12/22/2022 21:136200BMethyl tert-butyl ether (MTBE)µg/L 14.0
2.58 12/21/2022 21:266200BNaphthaleneµg/L 0.470
J0.301 12/21/2022 21:266200Bn-Propylbenzene µg/L 0.190
J73012/22/2022 21:136200Btert-Amyl Alcohol (TAA)µg/L 190
14.1 12/21/2022 21:266200Btert-Amyl Methyl Ether (TAME)µg/L 0.280
0.508 12/21/2022 21:266200BTolueneµg/L 0.220
Page 8 of 100

Client:GeologicalResources,Inc. CASENARRATIVE
Project:TrindaleMiniMart
LabReportNumber:22-354-0019
Date:1/10/2023

625.1-Base/NeutralsandAcidsbyGC/MSMethod625.1
QCBatchNo:V28406/V28235
RelativePercentDifference(RPD)fortheduplicateanalysiswasoutsideoftheallowableQClimitsforseveral
analytes..

Analyte:1,2,4-Trichlorobenzene
QCBatchNo:V28406/V28235
ThistargetanalytewasflaggedforrecoveriesoutsideQClimitsintheassociatedLCS/LCSD.Dataforthis
analyteisflagged"M"toindicatethatresultsshouldbeconsideredminimumconcentrationduetothepotentialfor
alowbias.

Analyte:2-Chloronaphthalene
QCBatchNo:V28406/V28235
ThistargetanalytewasflaggedforrecoveriesoutsideQClimitsintheassociatedLCS/LCSD.Dataforthis
analyteisflagged"M"toindicatethatresultsshouldbeconsideredminimumconcentrationduetothepotentialfor
alowbias.

Analyte:Hexachlorocyclopentadiene
QCBatchNo:V28406/V28235
ThistargetanalytewasflaggedforrecoveriesoutsideQClimitsintheassociatedLCS/LCSD.Dataforthis
analyteisflagged"M"toindicatethatresultsshouldbeconsideredminimumconcentrationduetothepotentialfor
alowbias.

Analyte:Hexachloroethane
QCBatchNo:V28406/V28235
ThistargetanalytewasflaggedforrecoveriesoutsideQClimitsintheassociatedLCS/LCSD.Dataforthis
analyteisflagged"M"toindicatethatresultsshouldbeconsideredminimumconcentrationduetothepotentialfor
alowbias.

Analyte:Nitrobenzene-d5
QCBatchNo:V28406/V28235
Surrogaterecoveryisbelowrange.

Sample96171(MW-12)
Analyte:Nitrobenzene-d5
QCBatchNo:V28406/V28235
Surrogaterecoveryaboverangeduetosamplematrix.

MassachusettsEPHMethodMADEP-EPH
QCBatchNo:V28712
Fractionationsurrogaterecoveriesareaboverange.

Sample96171(MW-12)
QCBatchNo:V28712
Samplerequiresdilutionduetohighlevelsoftargetand/ornon-targetanalytes.
Page 9 of 100

Analyte:2-Bromonaphthalene
QCBatchNo:V28712/V28366
SurrogateOut

Sample96170(MW-11)
Analyte:2-Bromonaphthalene
QCBatchNo:V28712/V28366
Surrogate(s)exhibitedahighbiasinthisprojectsamplewherenotargetanalytesweredetected.Thehigh
recovery(s)hadnoimpactonthedata.BatchQCsamples(methodblankandlaboratorycontrolsamples)all
showedsurrogateswithinQClimits.

Sample96170(MW-11)
Analyte:2-Fluorobiphenyl
QCBatchNo:V28712/V28366
Surrogate(s)exhibitedahighbiasinthisprojectsamplewherenotargetanalytesweredetected.Thehigh
recovery(s)hadnoimpactonthedata.BatchQCsamples(methodblankandlaboratorycontrolsamples)all
showedsurrogateswithinQClimits.

Sample96171(MW-12)
Analyte:Chlorooctadecane
QCBatchNo:V28712/V28366
Surrogateisdilutedoutduetoahighdilution.

Sample96171(MW-12)
Analyte:o-Terphenyl
QCBatchNo:V28712/V28366
Surrogateisdilutedoutduetoahighdilution.

MassachusettsVPHMethodMADEP-VPH
Sample96171(MW-12)
QCBatchNo:V28153
Surrogate(s)wasflaggedforrecoveryoutsideQClimitsinthisprojectsample.Thissamplewasre-analyzedfor
verification,and/ordilutionoftargetanalytes.BatchQCsamples(methodblankandlaboratorycontrolsamples)
allshowedsurrogateswithinQClimits.

VolatileOrganicCompounds-GC/MSMethod6200B
Sample96171(MW-12)
QCBatchNo:V28165/V28164
Thesamplewasdilutedduetothenatureofthesamplematrix.Reportinglimitshavebeenadjustedaccordingly.

QCBatchNo:V28231/V28175
LCSDsawRPDfailuresoccur.BothLCSandLCSDcompoundparameterspass.Datawasnotaffected.No
furtheractiontaken.

Analyte:1,1-Dichloroethene
QCBatchNo:V28231/V28175
RecoveryfortheLCSexceededtheupperacceptancelimit.However,allsampleresultsassociatedwiththe
batcharebelowtheMQL,sothishighbiashadnoimpactupontheclientdata.Theresultsareconsideredtobe
acceptable.

Page 10 of 100

Analyte:1,2-Dibromoethane
QCBatchNo:V28165/V28175
RelativePercentDifference(RPD)fortheduplicateanalysiswasoutsideoftheallowableQClimits.

Analyte:1,3-Dichloropropane
QCBatchNo:V28165/V28175
RelativePercentDifference(RPD)fortheduplicateanalysiswasoutsideoftheallowableQClimits.

Analyte:2-Butanone
QCBatchNo:V28165/V28175
RelativePercentDifference(RPD)fortheduplicateanalysiswasoutsideoftheallowableQClimits.

Analyte:3,3-Dimethyl-1-butanol
QCBatchNo:V28231/V28175
RecoveryfortheLCSexceededtheupperacceptancelimit.However,allsampleresultsassociatedwiththe
batcharebelowtheMQL,sothishighbiashadnoimpactupontheclientdata.Theresultsareconsideredtobe
acceptable.

Analyte:Chlorodibromomethane
QCBatchNo:V28165/V28175
RelativePercentDifference(RPD)fortheduplicateanalysiswasoutsideoftheallowableQClimits.

Analyte:Tetrachloroethene
QCBatchNo:V28165/V28175
RelativePercentDifference(RPD)fortheduplicateanalysiswasoutsideoftheallowableQClimits.

Page 11 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-2
96163 Matrix:
12/20/2022 12:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 17:03 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/21/22 17:031 MSA V28176
Surrogate: Dibromofluoromethane 93.0 Limits: 70-130%12/21/22 17:031 MSA V28176
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%12/21/22 17:031 MSA V28176
Surrogate: Toluene-d8 99.8 Limits: 70-130%12/21/22 17:031 MSA V28176
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 12 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-2
96163 Matrix:
12/20/2022 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 17:03 V28176MSA
<0.180 µg/L 0.180 0.500
Benzene 1 12/21/22 17:03 V28176MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 17:03 V28176MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 17:03 V28176MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 17:03 V28176MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 17:03 V28176MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 17:03 V28176MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 17:03 V28176MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 17:03 V28176MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 17:03 V28176MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 17:03 V28176MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 17:03 V28176MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 17:03 V28176MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 17:03 V28176MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/21/22 17:03 V28176MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 17:03 V28176MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 17:03 V28176MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 17:03 V28176MSA
4.41 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 17:03 V28176MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 17:03 V28176MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 17:03 V28176MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 17:03 V28176MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 13 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-2
96163 Matrix:
12/20/2022 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 17:03 V28176MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 17:03 V28176MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 17:03 V28176MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 17:03 V28176MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 17:03 V28176MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 17:03 V28176MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 17:03 V28176MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 17:03 V28176MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 17:03 V28176MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 17:03 V28176MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 17:03 V28176MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 17:03 V28176MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 17:03 V28176MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 17:03 V28176MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 17:03 V28176MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 17:03 V28176MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 17:03 V28176MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 17:03 V28176MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 17:03 V28176MSA
<0.180 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 17:03 V28176MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 17:03 V28176MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 17:03 V28176MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 14 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-2
96163 Matrix:
12/20/2022 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00
35.2 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/21/22 17:03 V28176MSA
<0.078 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 17:03 V28176MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 17:03 V28176MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/21/22 17:03 V28176MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 17:03 V28176MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 17:03 V28176MSA
6.49 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 17:03 V28176MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 17:03 V28176MSA
2.72 J µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/21/22 17:03 V28176MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 17:03 V28176MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 17:03 V28176MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 17:03 V28176MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 17:03 V28176MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/21/22 17:03 V28176MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 17:03 V28176MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 17:03 V28176MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 17:03 V28176MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 17:03 V28176MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 17:03 V28176MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 17:03 V28176MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 17:03 V28176MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/21/22 17:03 V28176MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 15 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-2
96163 Matrix:
12/20/2022 12:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 17:03 V28176MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 17:03 V28176MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 17:03 V28176MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/21/22 17:03 V28176MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 17:03 V28176MSA
<0.21 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 17:03 V28176
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/21/22 17:031 MSA V28176
Surrogate: Dibromofluoromethane 93.0 Limits: 70-130%12/21/22 17:031 MSA V28176
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%12/21/22 17:031 MSA V28176
Surrogate: Toluene-d8 99.8 Limits: 70-130%12/21/22 17:031 MSA V28176
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 16 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-4
96164 Matrix:
12/20/2022 13:22
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 18:14 6200BMSA
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: Dibromofluoromethane 95.0 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: Toluene-d8 101 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%12/22/22 19:1610 MSA V28231
Surrogate: Dibromofluoromethane 94.2 Limits: 70-130%12/22/22 19:1610 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%12/22/22 19:1610 MSA V28231
Surrogate: Toluene-d8 100 Limits: 70-130%12/22/22 19:1610 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 17 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-4
96164 Matrix:
12/20/2022 13:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 18:14 V28176MSA
10.4 µg/L 0.180 0.500
Benzene 1 12/21/22 18:14 V28176MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 18:14 V28176MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 18:14 V28176MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 18:14 V28176MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 18:14 V28176MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 18:14 V28176MSA
5.60 µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 18:14 V28176MSA
7.63 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 18:14 V28176MSA
1.19 J µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 18:14 V28176MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 18:14 V28176MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 18:14 V28176MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 18:14 V28176MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 18:14 V28176MSA
1.36 µg/L 0.220 0.500Chloroform 1 12/21/22 18:14 V28176MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 18:14 V28176MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 18:14 V28176MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 18:14 V28176MSA
30.0 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 18:14 V28176MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 18:14 V28176MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 18:14 V28176MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 18:14 V28176MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 18 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-4
96164 Matrix:
12/20/2022 13:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 18:14 V28176MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 18:14 V28176MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 18:14 V28176MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 18:14 V28176MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 18:14 V28176MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 18:14 V28176MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 18:14 V28176MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 18:14 V28176MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 18:14 V28176MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 18:14 V28176MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 18:14 V28176MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 18:14 V28176MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 18:14 V28176MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 18:14 V28176MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 18:14 V28176MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 18:14 V28176MSA
5.30 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 18:14 V28176MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 18:14 V28176MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 18:14 V28176MSA
5.90 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 18:14 V28176MSA
8.01 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 18:14 V28176MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 18:14 V28176MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 19 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-4
96164 Matrix:
12/20/2022 13:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
394 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 12/22/22 19:16 V28231MSA
2.41 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 18:14 V28176MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 18:14 V28176MSA
33.9 µg/L 0.470 1.00Naphthalene 1 12/21/22 18:14 V28176MSA
9.68 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 18:14 V28176MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 18:14 V28176MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 18:14 V28176MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 18:14 V28176MSA
52.2 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/21/22 18:14 V28176MSA
3.43 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 18:14 V28176MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 18:14 V28176MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 18:14 V28176MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 18:14 V28176MSA
1.87 µg/L 0.220 0.500Toluene 1 12/21/22 18:14 V28176MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 18:14 V28176MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 18:14 V28176MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 18:14 V28176MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 18:14 V28176MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 18:14 V28176MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 18:14 V28176MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 18:14 V28176MSA
242 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/22/22 19:16 V28231MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 20 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-4
96164 Matrix:
12/20/2022 13:22
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
68.3 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 18:14 V28176MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 18:14 V28176MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 18:14 V28176MSA
45.4 µg/L 0.210 0.500o-Xylene 1 12/21/22 18:14 V28176MSA
29.9 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 18:14 V28176MSA
75.3 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 18:14 V28176
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: Dibromofluoromethane 95.0 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: Toluene-d8 101 Limits: 70-130%12/21/22 18:141 MSA V28176
Surrogate: 4-Bromofluorobenzene 99.8 Limits: 70-130%12/22/22 19:1610 MSA V28231
Surrogate: Dibromofluoromethane 94.2 Limits: 70-130%12/22/22 19:1610 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%12/22/22 19:1610 MSA V28231
Surrogate: Toluene-d8 100 Limits: 70-130%12/22/22 19:1610 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 21 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-5
96165 Matrix:
12/20/2022 13:34
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 17:50 6200BMSA
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: Dibromofluoromethane 91.8 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: Toluene-d8 102 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%12/22/22 18:5210 MSA V28231
Surrogate: Dibromofluoromethane 91.6 Limits: 70-130%12/22/22 18:5210 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%12/22/22 18:5210 MSA V28231
Surrogate: Toluene-d8 98.4 Limits: 70-130%12/22/22 18:5210 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 22 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-5
96165 Matrix:
12/20/2022 13:34
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 17:50 V28176MSA
2.46 µg/L 0.180 0.500
Benzene 1 12/21/22 17:50 V28176MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 17:50 V28176MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 17:50 V28176MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 17:50 V28176MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 17:50 V28176MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 17:50 V28176MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 17:50 V28176MSA
5.04 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 17:50 V28176MSA
0.984 J µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 17:50 V28176MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 17:50 V28176MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 17:50 V28176MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 17:50 V28176MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 17:50 V28176MSA
0.668 µg/L 0.220 0.500Chloroform 1 12/21/22 17:50 V28176MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 17:50 V28176MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 17:50 V28176MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 17:50 V28176MSA
9.80 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 17:50 V28176MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 17:50 V28176MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 17:50 V28176MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 17:50 V28176MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 23 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-5
96165 Matrix:
12/20/2022 13:34
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 17:50 V28176MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 17:50 V28176MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 17:50 V28176MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 17:50 V28176MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 17:50 V28176MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 17:50 V28176MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 17:50 V28176MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 17:50 V28176MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 17:50 V28176MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 17:50 V28176MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 17:50 V28176MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 17:50 V28176MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 17:50 V28176MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 17:50 V28176MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 17:50 V28176MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 17:50 V28176MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 17:50 V28176MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 17:50 V28176MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 17:50 V28176MSA
3.48 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 17:50 V28176MSA
8.61 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 17:50 V28176MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 17:50 V28176MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 24 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-5
96165 Matrix:
12/20/2022 13:34
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
77.8 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/21/22 17:50 V28176MSA
<0.078 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 17:50 V28176MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 17:50 V28176MSA
36.2 µg/L 0.470 1.00Naphthalene 1 12/21/22 17:50 V28176MSA
10.0 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 17:50 V28176MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 17:50 V28176MSA
90.5 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 17:50 V28176MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 17:50 V28176MSA
282 µg/L 19.0 100tert-Amyl Alcohol (TAA)10 12/22/22 18:52 V28231MSA
0.534 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 17:50 V28176MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 17:50 V28176MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 17:50 V28176MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 17:50 V28176MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/21/22 17:50 V28176MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 17:50 V28176MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 17:50 V28176MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 17:50 V28176MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 17:50 V28176MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 17:50 V28176MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 17:50 V28176MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 17:50 V28176MSA
184 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/22/22 18:52 V28231MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 25 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-5
96165 Matrix:
12/20/2022 13:34
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28175 12/21/22 09:00 V28230 12/22/22 09:00
96.6 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 12/22/22 18:52 V28231MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 17:50 V28176MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 17:50 V28176MSA
6.27 µg/L 0.210 0.500o-Xylene 1 12/21/22 17:50 V28176MSA
26.4 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 17:50 V28176MSA
32.7 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 17:50 V28176
Surrogate: 4-Bromofluorobenzene 102 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: Dibromofluoromethane 91.8 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: 1,2-Dichloroethane - d4 99.6 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: Toluene-d8 102 Limits: 70-130%12/21/22 17:501 MSA V28176
Surrogate: 4-Bromofluorobenzene 97.4 Limits: 70-130%12/22/22 18:5210 MSA V28231
Surrogate: Dibromofluoromethane 91.6 Limits: 70-130%12/22/22 18:5210 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 104 Limits: 70-130%12/22/22 18:5210 MSA V28231
Surrogate: Toluene-d8 98.4 Limits: 70-130%12/22/22 18:5210 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 26 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-7
96166 Matrix:
12/20/2022 13:15
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 12/21/22 21:50 6200BMSA
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: Dibromofluoromethane 91.6 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 79.4 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: Toluene-d8 83.4 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%12/22/22 21:591000 MSA V28231
Surrogate: Dibromofluoromethane 92.0 Limits: 70-130%12/22/22 21:591000 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%12/22/22 21:591000 MSA V28231
Surrogate: Toluene-d8 98.8 Limits: 70-130%12/22/22 21:591000 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 27 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-7
96166 Matrix:
12/20/2022 13:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<18.0 µg/L 18.0 100Acetone 10 12/21/22 21:50 V28165MSA
6.41 µg/L 1.80 5.00
Benzene 10 12/21/22 21:50 V28165MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 12/21/22 21:50 V28165MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 12/21/22 21:50 V28165MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 12/21/22 21:50 V28165MSA
<15.0 µg/L 15.0 50.0
Bromoform 10 12/21/22 21:50 V28165MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 12/21/22 21:50 V28165MSA
<1.80 µg/L 1.80 5.00n-Butylbenzene 10 12/21/22 21:50 V28165MSA
<2.00 µg/L 2.00 5.00sec-Butyl benzene 10 12/21/22 21:50 V28165MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 12/21/22 21:50 V28165MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 12/21/22 21:50 V28165MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 12/21/22 21:50 V28165MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 12/21/22 21:50 V28165MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 12/21/22 21:50 V28165MSA
<2.20 µg/L 2.20 5.00Chloroform 10 12/21/22 21:50 V28165MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 12/21/22 21:50 V28165MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 12/21/22 21:50 V28165MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 12/21/22 21:50 V28165MSA
520 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 12/21/22 21:50 V28165MSA
<11.0 µg/L 11.0 20.0
1,2-Dibromo-3-Chloropropane 10 12/21/22 21:50 V28165MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 12/21/22 21:50 V28165MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 12/21/22 21:50 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 28 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-7
96166 Matrix:
12/20/2022 13:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 12/21/22 21:50 V28165MSA
<1.90 µg/L 1.90 5.00
1,3-Dichlorobenzene 10 12/21/22 21:50 V28165MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 12/21/22 21:50 V28165MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 12/21/22 21:50 V28165MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 12/21/22 21:50 V28165MSA
<1.50 µg/L 1.50 5.00
1,2-Dichloroethane 10 12/21/22 21:50 V28165MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 12/21/22 21:50 V28165MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 12/21/22 21:50 V28165MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 12/21/22 21:50 V28165MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 12/21/22 21:50 V28165MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 12/21/22 21:50 V28165MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 12/21/22 21:50 V28165MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 12/21/22 21:50 V28165MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 12/21/22 21:50 V28165MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 12/21/22 21:50 V28165MSA
<420 µg/L 420 2000Ethanol 10 12/21/22 21:50 V28165MSA
<1.70 µg/L 1.70 5.00Ethylbenzene 10 12/21/22 21:50 V28165MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 12/21/22 21:50 V28165MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 12/21/22 21:50 V28165MSA
<1.80 µg/L 1.80 5.00
Isopropylbenzene 10 12/21/22 21:50 V28165MSA
<0.890 µg/L 0.890 5.004-Isopropyl toluene 10 12/21/22 21:50 V28165MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 12/21/22 21:50 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 29 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-7
96166 Matrix:
12/20/2022 13:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
85000 µg/L 140 1000Methyl tert-butyl ether (MTBE)1000 12/22/22 21:59 V28231MSA
<0.780 µg/L 0.780 10.0
4-Methyl-2-Pentanone 10 12/21/22 21:50 V28165MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 12/21/22 21:50 V28165MSA
<4.70 µg/L 4.70 10.0Naphthalene 10 12/21/22 21:50 V28165MSA
<1.90 µg/L 1.90 5.00n-Propylbenzene 10 12/21/22 21:50 V28165MSA
<2.20 µg/L 2.20 5.00
Styrene 10 12/21/22 21:50 V28165MSA
<16.0 µg/L 16.0 100tert-Butyl Alcohol (TBA)10 12/21/22 21:50 V28165MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 12/21/22 21:50 V28165MSA
11700 µg/L 1900 10000tert-Amyl Alcohol (TAA)1000 12/22/22 21:59 V28231MSA
377 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 12/21/22 21:50 V28165MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 12/21/22 21:50 V28165MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 12/21/22 21:50 V28165MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 12/21/22 21:50 V28165MSA
<2.20 µg/L 2.20 5.00Toluene 10 12/21/22 21:50 V28165MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 12/21/22 21:50 V28165MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 12/21/22 21:50 V28165MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 12/21/22 21:50 V28165MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 12/21/22 21:50 V28165MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 12/21/22 21:50 V28165MSA
<1.80 µg/L 1.80 5.00
Trichlorofluoromethane 10 12/21/22 21:50 V28165MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 12/21/22 21:50 V28165MSA
<1.90 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/21/22 21:50 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 30 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-7
96166 Matrix:
12/20/2022 13:15
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<1.80 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 12/21/22 21:50 V28165MSA
<10.0 µg/L 10.0 50.0
Vinyl Acetate 10 12/21/22 21:50 V28165MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 12/21/22 21:50 V28165MSA
4.75 J µg/L 2.10 5.00o-Xylene 10 12/21/22 21:50 V28165MSA
5.25 J µg/L 4.20 10.0m,p-Xylene 10 12/21/22 21:50 V28165MSA
10.0 J
µg/L 2.10 5.00
Xylene (Total)10 12/21/22 21:50 V28165
Surrogate: 4-Bromofluorobenzene 97.8 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: Dibromofluoromethane 91.6 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 79.4 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: Toluene-d8 83.4 Limits: 70-130%12/21/22 21:5010 MSA V28165
Surrogate: 4-Bromofluorobenzene 99.4 Limits: 70-130%12/22/22 21:591000 MSA V28231
Surrogate: Dibromofluoromethane 92.0 Limits: 70-130%12/22/22 21:591000 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 101 Limits: 70-130%12/22/22 21:591000 MSA V28231
Surrogate: Toluene-d8 98.8 Limits: 70-130%12/22/22 21:591000 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 31 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-8
96167 Matrix:
12/20/2022 12:45
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 19:51 6200BMSA
Surrogate: 4-Bromofluorobenzene 95.4 Limits: 70-130%12/21/22 19:511 MSA V28165
Surrogate: Dibromofluoromethane 92.6 Limits: 70-130%12/21/22 19:511 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 79.8 Limits: 70-130%12/21/22 19:511 MSA V28165
Surrogate: Toluene-d8 82.6 Limits: 70-130%12/21/22 19:511 MSA V28165
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 32 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-8
96167 Matrix:
12/20/2022 12:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 19:51 V28165MSA
<0.180 µg/L 0.180 0.500
Benzene 1 12/21/22 19:51 V28165MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 19:51 V28165MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 19:51 V28165MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 19:51 V28165MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 19:51 V28165MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 19:51 V28165MSA
0.443 J µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 19:51 V28165MSA
0.545 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 19:51 V28165MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 19:51 V28165MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 19:51 V28165MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 19:51 V28165MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 19:51 V28165MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 19:51 V28165MSA
6.42 µg/L 0.220 0.500Chloroform 1 12/21/22 19:51 V28165MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 19:51 V28165MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 19:51 V28165MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 19:51 V28165MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 19:51 V28165MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 19:51 V28165MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 19:51 V28165MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 19:51 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 33 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-8
96167 Matrix:
12/20/2022 12:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 19:51 V28165MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 19:51 V28165MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 19:51 V28165MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 19:51 V28165MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 19:51 V28165MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 19:51 V28165MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 19:51 V28165MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 19:51 V28165MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 19:51 V28165MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 19:51 V28165MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 19:51 V28165MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 19:51 V28165MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 19:51 V28165MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 19:51 V28165MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 19:51 V28165MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 19:51 V28165MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 19:51 V28165MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 19:51 V28165MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 19:51 V28165MSA
<0.180 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 19:51 V28165MSA
0.226 J µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 19:51 V28165MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 19:51 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 34 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-8
96167 Matrix:
12/20/2022 12:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/21/22 19:51 V28165MSA
<0.078 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 19:51 V28165MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 19:51 V28165MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/21/22 19:51 V28165MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 19:51 V28165MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 19:51 V28165MSA
1.60 J µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 19:51 V28165MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 19:51 V28165MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/21/22 19:51 V28165MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 19:51 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 19:51 V28165MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 19:51 V28165MSA
0.550 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 19:51 V28165MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/21/22 19:51 V28165MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 19:51 V28165MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 19:51 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 19:51 V28165MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 19:51 V28165MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 19:51 V28165MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 19:51 V28165MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 19:51 V28165MSA
2.44 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/21/22 19:51 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 35 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-8
96167 Matrix:
12/20/2022 12:45
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 19:51 V28165MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 19:51 V28165MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 19:51 V28165MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/21/22 19:51 V28165MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 19:51 V28165MSA
<0.21 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 19:51 V28165
Surrogate: 4-Bromofluorobenzene 95.4 Limits: 70-130%12/21/22 19:511 MSA V28165
Surrogate: Dibromofluoromethane 92.6 Limits: 70-130%12/21/22 19:511 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 79.8 Limits: 70-130%12/21/22 19:511 MSA V28165
Surrogate: Toluene-d8 82.6 Limits: 70-130%12/21/22 19:511 MSA V28165
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 36 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-9
96168 Matrix:
12/20/2022 13:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 20:15 6200BMSA
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: Dibromofluoromethane 88.6 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 80.6 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: Toluene-d8 83.4 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/22/22 19:3910 MSA V28231
Surrogate: Dibromofluoromethane 92.2 Limits: 70-130%12/22/22 19:3910 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%12/22/22 19:3910 MSA V28231
Surrogate: Toluene-d8 99.6 Limits: 70-130%12/22/22 19:3910 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 37 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-9
96168 Matrix:
12/20/2022 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 20:15 V28165MSA
121 µg/L 1.80 5.00
Benzene 10 12/22/22 19:39 V28231MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 20:15 V28165MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 20:15 V28165MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 20:15 V28165MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 20:15 V28165MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 20:15 V28165MSA
11.8 µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 20:15 V28165MSA
13.5 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 20:15 V28165MSA
1.46 J µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 20:15 V28165MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 20:15 V28165MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 20:15 V28165MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 20:15 V28165MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 20:15 V28165MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/21/22 20:15 V28165MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 20:15 V28165MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 20:15 V28165MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 20:15 V28165MSA
3.48 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 20:15 V28165MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 20:15 V28165MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 20:15 V28165MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 20:15 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 38 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-9
96168 Matrix:
12/20/2022 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 20:15 V28165MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 20:15 V28165MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 20:15 V28165MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 20:15 V28165MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 20:15 V28165MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 20:15 V28165MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 20:15 V28165MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 20:15 V28165MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 20:15 V28165MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 20:15 V28165MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 20:15 V28165MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 20:15 V28165MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 20:15 V28165MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 20:15 V28165MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 20:15 V28165MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 20:15 V28165MSA
2.63 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 20:15 V28165MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 20:15 V28165MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 20:15 V28165MSA
29.1 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 20:15 V28165MSA
19.6 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 20:15 V28165MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 20:15 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 39 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-9
96168 Matrix:
12/20/2022 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
38.9 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/21/22 20:15 V28165MSA
7.32 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 20:15 V28165MSA
0.434 J µg/L 0.330 2.00Methylene Chloride 1 12/21/22 20:15 V28165MSA
167 µg/L 4.70 10.0Naphthalene 10 12/22/22 19:39 V28231MSA
52.0 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 20:15 V28165MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 20:15 V28165MSA
24.4 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 20:15 V28165MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 20:15 V28165MSA
92.7 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/21/22 20:15 V28165MSA
1.42 J µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 20:15 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 20:15 V28165MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 20:15 V28165MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 20:15 V28165MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/21/22 20:15 V28165MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 20:15 V28165MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 20:15 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 20:15 V28165MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 20:15 V28165MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 20:15 V28165MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 20:15 V28165MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 20:15 V28165MSA
1.29 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/21/22 20:15 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 40 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-9
96168 Matrix:
12/20/2022 13:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
0.345 J µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 20:15 V28165MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 20:15 V28165MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 20:15 V28165MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/21/22 20:15 V28165MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 20:15 V28165MSA
<0.21 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 20:15 V28165
Surrogate: 4-Bromofluorobenzene 99.6 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: Dibromofluoromethane 88.6 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 80.6 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: Toluene-d8 83.4 Limits: 70-130%12/21/22 20:151 MSA V28165
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/22/22 19:3910 MSA V28231
Surrogate: Dibromofluoromethane 92.2 Limits: 70-130%12/22/22 19:3910 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%12/22/22 19:3910 MSA V28231
Surrogate: Toluene-d8 99.6 Limits: 70-130%12/22/22 19:3910 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 41 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-10
96169 Matrix:
12/20/2022 11:38
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 20:38 6200BMSA
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Surrogate: Dibromofluoromethane 84.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 77.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Surrogate: Toluene-d8 84.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 42 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-10
96169 Matrix:
12/20/2022 11:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 20:38 V28165MSA
<0.180 µg/L 0.180 0.500
Benzene 1 12/21/22 20:38 V28165MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 20:38 V28165MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 20:38 V28165MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 20:38 V28165MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 20:38 V28165MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 20:38 V28165MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 20:38 V28165MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 20:38 V28165MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 20:38 V28165MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 20:38 V28165MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 20:38 V28165MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 20:38 V28165MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 20:38 V28165MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/21/22 20:38 V28165MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 20:38 V28165MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 20:38 V28165MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 20:38 V28165MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 20:38 V28165MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 20:38 V28165MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 20:38 V28165MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 20:38 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 43 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-10
96169 Matrix:
12/20/2022 11:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 20:38 V28165MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 20:38 V28165MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 20:38 V28165MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 20:38 V28165MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 20:38 V28165MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 20:38 V28165MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 20:38 V28165MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 20:38 V28165MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 20:38 V28165MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 20:38 V28165MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 20:38 V28165MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 20:38 V28165MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 20:38 V28165MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 20:38 V28165MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 20:38 V28165MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 20:38 V28165MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 20:38 V28165MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 20:38 V28165MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 20:38 V28165MSA
<0.180 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 20:38 V28165MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 20:38 V28165MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 20:38 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 44 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-10
96169 Matrix:
12/20/2022 11:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/21/22 20:38 V28165MSA
<0.078 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 20:38 V28165MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 20:38 V28165MSA
16.3 µg/L 0.470 1.00Naphthalene 1 12/21/22 20:38 V28165MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 20:38 V28165MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 20:38 V28165MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 20:38 V28165MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 20:38 V28165MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/21/22 20:38 V28165MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 20:38 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 20:38 V28165MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 20:38 V28165MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 20:38 V28165MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/21/22 20:38 V28165MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 20:38 V28165MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 20:38 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 20:38 V28165MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 20:38 V28165MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 20:38 V28165MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 20:38 V28165MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 20:38 V28165MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/21/22 20:38 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 45 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-10
96169 Matrix:
12/20/2022 11:38
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 20:38 V28165MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 20:38 V28165MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 20:38 V28165MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/21/22 20:38 V28165MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 20:38 V28165MSA
<0.21 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 20:38 V28165
Surrogate: 4-Bromofluorobenzene 93.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Surrogate: Dibromofluoromethane 84.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 77.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Surrogate: Toluene-d8 84.0 Limits: 70-130%12/21/22 20:381 MSA V28165
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 46 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 21:02 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.2 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: Dibromofluoromethane 81.4 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 76.4 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: Toluene-d8 82.2 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/22/22 20:49100 MSA V28231
Surrogate: Dibromofluoromethane 92.6 Limits: 70-130%12/22/22 20:49100 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%12/22/22 20:49100 MSA V28231
Surrogate: Toluene-d8 98.6 Limits: 70-130%12/22/22 20:49100 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 47 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 21:02 V28165MSA
35.1 µg/L 0.180 0.500
Benzene 1 12/21/22 21:02 V28165MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 21:02 V28165MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 21:02 V28165MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 21:02 V28165MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 21:02 V28165MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 21:02 V28165MSA
0.304 J µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 21:02 V28165MSA
0.633 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 21:02 V28165MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 21:02 V28165MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 21:02 V28165MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 21:02 V28165MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 21:02 V28165MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 21:02 V28165MSA
0.365 J µg/L 0.220 0.500Chloroform 1 12/21/22 21:02 V28165MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 21:02 V28165MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 21:02 V28165MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 21:02 V28165MSA
91.7 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 21:02 V28165MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 21:02 V28165MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 21:02 V28165MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 21:02 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 48 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 21:02 V28165MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 21:02 V28165MSA
0.265 J µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 21:02 V28165MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 21:02 V28165MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 21:02 V28165MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 21:02 V28165MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 21:02 V28165MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 21:02 V28165MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 21:02 V28165MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 21:02 V28165MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 21:02 V28165MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 21:02 V28165MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 21:02 V28165MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 21:02 V28165MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 21:02 V28165MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 21:02 V28165MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 21:02 V28165MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 21:02 V28165MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 21:02 V28165MSA
<0.180 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 21:02 V28165MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 21:02 V28165MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 21:02 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 49 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
3930 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/22/22 20:49 V28231MSA
<0.078 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 21:02 V28165MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 21:02 V28165MSA
12.2 µg/L 0.470 1.00Naphthalene 1 12/21/22 21:02 V28165MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 21:02 V28165MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 21:02 V28165MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 21:02 V28165MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 21:02 V28165MSA
1070 µg/L 190 1000tert-Amyl Alcohol (TAA)100 12/22/22 20:49 V28231MSA
23.5 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 21:02 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 21:02 V28165MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 21:02 V28165MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 21:02 V28165MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/21/22 21:02 V28165MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 21:02 V28165MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 21:02 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 21:02 V28165MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 21:02 V28165MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 21:02 V28165MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 21:02 V28165MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 21:02 V28165MSA
2.01 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/21/22 21:02 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 50 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 21:02 V28165MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 21:02 V28165MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 21:02 V28165MSA
5.87 µg/L 0.210 0.500o-Xylene 1 12/21/22 21:02 V28165MSA
1.72 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 21:02 V28165MSA
7.59 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 21:02 V28165
Surrogate: 4-Bromofluorobenzene 96.2 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: Dibromofluoromethane 81.4 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 76.4 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: Toluene-d8 82.2 Limits: 70-130%12/21/22 21:021 MSA V28165
Surrogate: 4-Bromofluorobenzene 101 Limits: 70-130%12/22/22 20:49100 MSA V28231
Surrogate: Dibromofluoromethane 92.6 Limits: 70-130%12/22/22 20:49100 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 103 Limits: 70-130%12/22/22 20:49100 MSA V28231
Surrogate: Toluene-d8 98.6 Limits: 70-130%12/22/22 20:49100 MSA V28231
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
<0.315 µg/L 0.315 2.09Acenaphthene 1 12/23/22 15:36 V28406JMV
<0.310 µg/L 0.310 2.09Acenaphthylene 1 12/23/22 15:36 V28406JMV
<0.873 µg/L 0.873 2.09Anthracene 1 12/23/22 15:36 V28406JMV
<1.39 µg/L 1.39 10.5
Benzidine 1 12/23/22 15:36 V28406JMV
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 51 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
<0.665 µg/L 0.665 2.09Benzo(a)anthracene 1 12/23/22 15:36 V28406JMV
<1.07 µg/L 1.07 2.09
Benzo(a)pyrene 1 12/23/22 15:36 V28406JMV
<2.61 µg/L 2.61 5.24Benzo(b)fluoranthene 1 12/23/22 15:36 V28406JMV
<1.06 µg/L 1.06 5.24Benzo(g,h,i)perylene 1 12/23/22 15:36 V28406JMV
<2.09 µg/L 2.09 5.24Benzo(k)fluoranthene 1 12/23/22 15:36 V28406JMV
<1.16 µg/L 1.16 10.5
Benzoic Acid 1 12/23/22 15:36 V28406JMV
<0.716 µg/L 0.716 5.24Benzyl alcohol 1 12/23/22 15:36 V28406JMV
<0.490 µg/L 0.490 5.24Bis(2-Chloroethoxy)methane 1 12/23/22 15:36 V28406JMV
<1.09 µg/L 1.09 5.24Bis(2-Chloroethyl)ether 1 12/23/22 15:36 V28406JMV
<1.13 µg/L 1.13 5.24Bis(2-Chloroisopropyl)ether 1 12/23/22 15:36 V28406JMV
<25.2 µg/L 25.2 52.4Bis(2-ethylhexyl)phthalate 1 12/23/22 15:36 V28406JMV
<1.16 µg/L 1.16 5.244-Bromophenyl phenyl ether 1 12/23/22 15:36 V28406JMV
<1.92 µg/L 1.92 5.24Butyl benzyl phthalate 1 12/23/22 15:36 V28406JMV
<1.24 µg/L 1.24 5.244-Chloro-3-methylphenol 1 12/23/22 15:36 V28406JMV
<7.71 µg/L 7.71 20.92-Chloronaphthalene 1 12/23/22 15:36 V28406JMV
<0.984 µg/L 0.984 10.52-Chlorophenol 1 12/23/22 15:36 V28406JMV
<1.79 µg/L 1.79 5.244-Chlorophenyl phenyl ether 1 12/23/22 15:36 V28406JMV
<0.423 µg/L 0.423 2.09Chrysene 1 12/23/22 15:36 V28406JMV
<0.453 µg/L 0.453 2.09Dibenz(a,h)anthracene 1 12/23/22 15:36 V28406JMV
<0.897 µg/L 0.897 5.24
Dibenzofuran 1 12/23/22 15:36 V28406JMV
<2.10 µg/L 2.10 5.241,2-Dichlorobenzene 1 12/23/22 15:36 V28406JMV
<2.10 µg/L 2.10 5.241,3-Dichlorobenzene 1 12/23/22 15:36 V28406JMV
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 52 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
<2.15 µg/L 2.15 5.241,4-Dichlorobenzene 1 12/23/22 15:36 V28406JMV
<1.98 µg/L 1.98 5.24
3,3'-Dichlorobenzidine 1 12/23/22 15:36 V28406JMV
<1.53 µg/L 1.53 10.52,4-Dichlorophenol 1 12/23/22 15:36 V28406JMV
<0.780 µg/L 0.780 5.24Diethyl phthalate 1 12/23/22 15:36 V28406JMV
<0.984 µg/L 0.984 5.24Dimethyl phthalate 1 12/23/22 15:36 V28406JMV
<1.64 µg/L 1.64 20.9
2,4-Dimethylphenol 1 12/23/22 15:36 V28406JMV
<2.16 µg/L 2.16 5.24Di-n-butyl phthalate 1 12/23/22 15:36 V28406JMV
<2.17 µg/L 2.17 10.54,6-Dinitro-2-methylphenol 1 12/23/22 15:36 V28406JMV
<2.02 µg/L 2.02 10.52,4-Dinitrophenol 1 12/23/22 15:36 V28406JMV
<1.16 µg/L 1.16 5.242,4-Dinitrotoluene 1 12/23/22 15:36 V28406JMV
<0.847 µg/L 0.847 5.242,6-Dinitrotoluene 1 12/23/22 15:36 V28406JMV
<1.73 µg/L 1.73 5.24Di-n-Octyl Phthalate 1 12/23/22 15:36 V28406JMV
<0.261 µg/L 0.261 2.09Fluoranthene 1 12/23/22 15:36 V28406JMV
<0.843 µg/L 0.843 2.09Fluorene 1 12/23/22 15:36 V28406JMV
<1.03 µg/L 1.03 5.24Hexachlorobenzene 1 12/23/22 15:36 V28406JMV
<2.86 µg/L 2.86 5.24Hexachlorobutadiene 1 12/23/22 15:36 V28406JMV
<2.15 M µg/L 2.15 5.24Hexachlorocyclopentadiene 1 12/23/22 15:36 V28406JMV
<1.84 M µg/L 1.84 5.24Hexachloroethane 1 12/23/22 15:36 V28406JMV
<0.498 µg/L 0.498 2.09Indeno(1,2,3-cd)pyrene 1 12/23/22 15:36 V28406JMV
<0.465 µg/L 0.465 5.24
Isophorone 1 12/23/22 15:36 V28406JMV
3.66 µg/L 1.19 2.091-Methylnaphthalene 1 12/23/22 15:36 V28406JMV
3.16 µg/L 0.695 2.092-Methylnaphthalene 1 12/23/22 15:36 V28406JMV
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 53 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
4.58 µg/L 0.760 2.09Naphthalene 1 12/23/22 15:36 V28406JMV
<0.948 µg/L 0.948 5.24
Nitrobenzene 1 12/23/22 15:36 V28406JMV
<0.516 µg/L 0.516 5.242-Nitrophenol 1 12/23/22 15:36 V28406JMV
<1.29 µg/L 1.29 10.54-Nitrophenol 1 12/23/22 15:36 V28406JMV
<1.15 µg/L 1.15 5.24N-Nitrosodiphenylamine 1 12/23/22 15:36 V28406JMV
<0.671 µg/L 0.671 5.24
N-Nitroso-di-n-propylamine 1 12/23/22 15:36 V28406JMV
<1.50 µg/L 1.50 5.24Pentachlorophenol 1 12/23/22 15:36 V28406JMV
<0.447 µg/L 0.447 2.09Phenanthrene 1 12/23/22 15:36 V28406JMV
<0.682 µg/L 0.682 5.24Phenol 1 12/23/22 15:36 V28406JMV
<0.453 µg/L 0.453 2.09Pyrene 1 12/23/22 15:36 V28406JMV
<2.32 µg/L 2.32 5.241,2,4-Trichlorobenzene 1 12/23/22 15:36 V28406JMV
<1.38 µg/L 1.38 5.242,4,6-Trichlorophenol 1 12/23/22 15:36 V28406JMV
625.1Surrogate: Phenol-d5 24.3 Limits: 10-63%12/23/22 15:361 JMV
Surrogate: 2-Fluorobiphenyl 60.1 Limits: 49-118%12/23/22 15:361 JMV V28406
Surrogate: 2-Fluorophenol 31.6 Limits: 22-84%12/23/22 15:361 JMV V28406
Surrogate: Nitrobenzene-d5 47.7 Limits: 43-123%12/23/22 15:361 JMV V28406
Surrogate: 4-Terphenyl-d14 90.3 Limits: 49-151%12/23/22 15:361 JMV V28406
Surrogate: 2,4,6-Tribromophenol 66.0 Limits: 31-144%12/23/22 15:361 JMV V28406
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 54 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
1210 µg/L 115 500Aliphatic C5-C8 (Adjusted)1 12/21/22 21:02
63.9 J
µg/L 25.8 50.0
Aliphatics C9-C12 (Adjusted)1 12/21/22 14:02
13.9 J µg/L 4.02 50.0Aromatic C9-C10 (Adjusted)1 12/21/22 14:02
93.2 J µg/L 63.4 259Aromatic C11-C22 (Adjusted)1 12/23/22 15:36
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V28366 12/29/22 09:00
208 JB µg/L 29.2 363Aliphatic C9-C18 1 01/07/23 04:20 V28712JMV
<128 µg/L 128 518Aliphatic C19-C36 1 01/07/23 04:20 V28712JMV
97.8 J
µg/L 63.4 259
Aromatic C11-C22 1 01/07/23 04:20 V28712JMV
MADEP-EPHSurrogate: 2-Bromonaphthalene 141 *Limits: 40-140%01/07/23 04:201 JMV
MADEP-EPHSurrogate: Chlorooctadecane 97.6 Limits: 40-140%01/07/23 04:201 JMV
MADEP-EPHSurrogate: OTP Surrogate 94.2 Limits: 40-140%01/07/23 04:201 JMV
Surrogate: 2-Fluorobiphenyl 140 *Limits: 40-140%01/07/23 04:201 JMV V28712
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28152 12/21/22 08:00
1250 µg/L 115 500Aliphatic C5-C8 10 12/22/22 08:31 V28153TBL
85.4 µg/L 25.8 50.0Aliphatic C9-C12 1 12/21/22 14:02 V28153TBL
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 55 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-11
96170 Matrix:
12/20/2022 11:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28152 12/21/22 08:00
13.9 J µg/L 4.02 50.0Aromatic C9-C10 1 12/21/22 14:02 V28153TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)96.5 Limits: 70-130%12/21/22 14:021 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)90.8 Limits: 70-130%12/21/22 14:021 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)78.2 Limits: 70-130%12/22/22 08:3110 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)75.6 Limits: 70-130%12/22/22 08:3110 TBL
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 56 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<10.0 µg/L 10.0 1003,3-Dimethyl-1-butanol 10 12/21/22 22:14 6200BMSA
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%12/21/22 22:1410 MSA V28165
Surrogate: Dibromofluoromethane 89.8 Limits: 70-130%12/21/22 22:1410 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 82.6 Limits: 70-130%12/21/22 22:1410 MSA V28165
Surrogate: Toluene-d8 82.0 Limits: 70-130%12/21/22 22:1410 MSA V28165
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 57 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<18.0 µg/L 18.0 100Acetone 10 12/21/22 22:14 V28165MSA
<1.80 µg/L 1.80 5.00
Benzene 10 12/21/22 22:14 V28165MSA
<2.10 µg/L 2.10 5.00Bromobenzene 10 12/21/22 22:14 V28165MSA
<4.20 µg/L 4.20 10.0Bromochloromethane 10 12/21/22 22:14 V28165MSA
<1.60 µg/L 1.60 5.00Bromodichloromethane 10 12/21/22 22:14 V28165MSA
<15.0 µg/L 15.0 50.0
Bromoform 10 12/21/22 22:14 V28165MSA
<2.80 µg/L 2.80 10.0Bromomethane 10 12/21/22 22:14 V28165MSA
110 µg/L 1.80 5.00n-Butylbenzene 10 12/21/22 22:14 V28165MSA
134 µg/L 2.00 5.00sec-Butyl benzene 10 12/21/22 22:14 V28165MSA
<9.20 µg/L 9.20 20.0tert-Butyl benzene 10 12/21/22 22:14 V28165MSA
<1.80 µg/L 1.80 5.00Carbon Tetrachloride 10 12/21/22 22:14 V28165MSA
<1.90 µg/L 1.90 5.00Chlorobenzene 10 12/21/22 22:14 V28165MSA
<1.90 µg/L 1.90 5.00Chlorodibromomethane 10 12/21/22 22:14 V28165MSA
<4.30 µg/L 4.30 10.0Chloroethane 10 12/21/22 22:14 V28165MSA
<2.20 µg/L 2.20 5.00Chloroform 10 12/21/22 22:14 V28165MSA
<2.20 µg/L 2.20 5.00Chloromethane 10 12/21/22 22:14 V28165MSA
<2.00 µg/L 2.00 5.002-Chlorotoluene 10 12/21/22 22:14 V28165MSA
<2.00 µg/L 2.00 5.004-Chlorotoluene 10 12/21/22 22:14 V28165MSA
<5.00 µg/L 5.00 5.00Di-Isopropyl Ether (DIPE)10 12/21/22 22:14 V28165MSA
<11.0 µg/L 11.0 20.0
1,2-Dibromo-3-Chloropropane 10 12/21/22 22:14 V28165MSA
<2.00 µg/L 2.00 5.001,2-Dibromoethane 10 12/21/22 22:14 V28165MSA
<2.30 µg/L 2.30 5.00Dibromomethane 10 12/21/22 22:14 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 58 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<2.20 µg/L 2.20 5.001,2-Dichlorobenzene 10 12/21/22 22:14 V28165MSA
<1.90 µg/L 1.90 5.00
1,3-Dichlorobenzene 10 12/21/22 22:14 V28165MSA
<2.10 µg/L 2.10 5.001,4-Dichlorobenzene 10 12/21/22 22:14 V28165MSA
<12.0 µg/L 12.0 50.0Dichlorodifluoromethane 10 12/21/22 22:14 V28165MSA
<2.40 µg/L 2.40 5.001,1-Dichloroethane 10 12/21/22 22:14 V28165MSA
<1.50 µg/L 1.50 5.00
1,2-Dichloroethane 10 12/21/22 22:14 V28165MSA
<1.50 µg/L 1.50 5.001,1-Dichloroethene 10 12/21/22 22:14 V28165MSA
<2.00 µg/L 2.00 5.00cis-1,2-Dichloroethene 10 12/21/22 22:14 V28165MSA
<1.80 µg/L 1.80 5.00trans-1,2-Dichloroethene 10 12/21/22 22:14 V28165MSA
<1.90 µg/L 1.90 5.001,2-Dichloropropane 10 12/21/22 22:14 V28165MSA
<1.30 µg/L 1.30 5.001,3-Dichloropropane 10 12/21/22 22:14 V28165MSA
<2.10 µg/L 2.10 20.02,2-Dichloropropane 10 12/21/22 22:14 V28165MSA
<2.00 µg/L 2.00 5.001,1-Dichloropropene 10 12/21/22 22:14 V28165MSA
<2.10 µg/L 2.10 5.00cis-1,3-Dichloropropene 10 12/21/22 22:14 V28165MSA
<1.50 µg/L 1.50 5.00trans-1,3-Dichloropropene 10 12/21/22 22:14 V28165MSA
<420 µg/L 420 2000Ethanol 10 12/21/22 22:14 V28165MSA
<1.70 µg/L 1.70 5.00Ethylbenzene 10 12/21/22 22:14 V28165MSA
<3.50 µg/L 3.50 30.0Hexachlorobutadiene 10 12/21/22 22:14 V28165MSA
<3.80 µg/L 3.80 10.02-Hexanone 10 12/21/22 22:14 V28165MSA
33.0 µg/L 1.80 5.00
Isopropylbenzene 10 12/21/22 22:14 V28165MSA
16.4 µg/L 0.890 5.004-Isopropyl toluene 10 12/21/22 22:14 V28165MSA
<7.10 µg/L 7.10 50.0Methyl Ethyl Ketone (MEK)10 12/21/22 22:14 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 59 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
57.7 µg/L 1.40 10.0Methyl tert-butyl ether (MTBE)10 12/21/22 22:14 V28165MSA
<0.780 µg/L 0.780 10.0
4-Methyl-2-Pentanone 10 12/21/22 22:14 V28165MSA
<3.30 µg/L 3.30 20.0Methylene Chloride 10 12/21/22 22:14 V28165MSA
17.3 µg/L 4.70 10.0Naphthalene 10 12/21/22 22:14 V28165MSA
26.6 µg/L 1.90 5.00n-Propylbenzene 10 12/21/22 22:14 V28165MSA
<2.20 µg/L 2.20 5.00
Styrene 10 12/21/22 22:14 V28165MSA
56.3 J µg/L 16.0 100tert-Butyl Alcohol (TBA)10 12/21/22 22:14 V28165MSA
<3.50 µg/L 3.50 100tert-Butyl formate (TBF)10 12/21/22 22:14 V28165MSA
85.9 J µg/L 19.0 100tert-Amyl Alcohol (TAA)10 12/21/22 22:14 V28165MSA
<2.80 µg/L 2.80 100tert-Amyl Methyl Ether (TAME)10 12/21/22 22:14 V28165MSA
<1.60 µg/L 1.60 5.001,1,1,2-Tetrachloroethane 10 12/21/22 22:14 V28165MSA
<1.60 µg/L 1.60 5.001,1,2,2-Tetrachloroethane 10 12/21/22 22:14 V28165MSA
<2.20 µg/L 2.20 5.00Tetrachloroethene 10 12/21/22 22:14 V28165MSA
<2.20 µg/L 2.20 5.00Toluene 10 12/21/22 22:14 V28165MSA
<3.80 µg/L 3.80 5.001,2,3-Trichlorobenzene 10 12/21/22 22:14 V28165MSA
<3.10 µg/L 3.10 5.001,2,4-Trichlorobenzene 10 12/21/22 22:14 V28165MSA
<1.60 µg/L 1.60 5.001,1,1-Trichloroethane 10 12/21/22 22:14 V28165MSA
<0.960 µg/L 0.960 5.001,1,2-Trichloroethane 10 12/21/22 22:14 V28165MSA
<1.80 µg/L 1.80 5.00Trichloroethene 10 12/21/22 22:14 V28165MSA
<1.80 µg/L 1.80 5.00
Trichlorofluoromethane 10 12/21/22 22:14 V28165MSA
<2.70 µg/L 2.70 5.001,2,3-Trichloropropane 10 12/21/22 22:14 V28165MSA
<1.90 µg/L 1.90 5.001,2,4-Trimethylbenzene 10 12/21/22 22:14 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 60 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<1.80 µg/L 1.80 5.001,3,5-Trimethylbenzene 10 12/21/22 22:14 V28165MSA
<10.0 µg/L 10.0 50.0
Vinyl Acetate 10 12/21/22 22:14 V28165MSA
<1.70 µg/L 1.70 5.00Vinyl Chloride 10 12/21/22 22:14 V28165MSA
<2.10 µg/L 2.10 5.00o-Xylene 10 12/21/22 22:14 V28165MSA
<4.20 µg/L 4.20 10.0m,p-Xylene 10 12/21/22 22:14 V28165MSA
<2.1 µg/L 2.10 5.00
Xylene (Total)10 12/21/22 22:14 V28165
Surrogate: 4-Bromofluorobenzene 104 Limits: 70-130%12/21/22 22:1410 MSA V28165
Surrogate: Dibromofluoromethane 89.8 Limits: 70-130%12/21/22 22:1410 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 82.6 Limits: 70-130%12/21/22 22:1410 MSA V28165
Surrogate: Toluene-d8 82.0 Limits: 70-130%12/21/22 22:1410 MSA V28165
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
<0.311 µg/L 0.311 2.06Acenaphthene 1 12/23/22 15:59 V28406JMV
<0.305 µg/L 0.305 2.06Acenaphthylene 1 12/23/22 15:59 V28406JMV
<0.861 µg/L 0.861 2.06Anthracene 1 12/23/22 15:59 V28406JMV
<1.36 µg/L 1.36 10.3
Benzidine 1 12/23/22 15:59 V28406JMV
<0.656 µg/L 0.656 2.06Benzo(a)anthracene 1 12/23/22 15:59 V28406JMV
<1.05 µg/L 1.05 2.06Benzo(a)pyrene 1 12/23/22 15:59 V28406JMV
<2.56 µg/L 2.56 5.15Benzo(b)fluoranthene 1 12/23/22 15:59 V28406JMV
<1.04 µg/L 1.04 5.15Benzo(g,h,i)perylene 1 12/23/22 15:59 V28406JMV
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 61 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
<2.05 µg/L 2.05 5.15Benzo(k)fluoranthene 1 12/23/22 15:59 V28406JMV
<1.13 µg/L 1.13 10.3
Benzoic Acid 1 12/23/22 15:59 V28406JMV
<0.704 µg/L 0.704 5.15Benzyl alcohol 1 12/23/22 15:59 V28406JMV
<0.482 µg/L 0.482 5.15Bis(2-Chloroethoxy)methane 1 12/23/22 15:59 V28406JMV
<1.07 µg/L 1.07 5.15Bis(2-Chloroethyl)ether 1 12/23/22 15:59 V28406JMV
<1.11 µg/L 1.11 5.15
Bis(2-Chloroisopropyl)ether 1 12/23/22 15:59 V28406JMV
<24.8 µg/L 24.8 51.5Bis(2-ethylhexyl)phthalate 1 12/23/22 15:59 V28406JMV
<1.14 µg/L 1.14 5.154-Bromophenyl phenyl ether 1 12/23/22 15:59 V28406JMV
<1.88 µg/L 1.88 5.15Butyl benzyl phthalate 1 12/23/22 15:59 V28406JMV
<1.22 µg/L 1.22 5.154-Chloro-3-methylphenol 1 12/23/22 15:59 V28406JMV
<7.60 µg/L 7.60 20.62-Chloronaphthalene 1 12/23/22 15:59 V28406JMV
<0.966 µg/L 0.966 10.32-Chlorophenol 1 12/23/22 15:59 V28406JMV
<1.76 µg/L 1.76 5.154-Chlorophenyl phenyl ether 1 12/23/22 15:59 V28406JMV
1.52 J µg/L 0.417 2.06Chrysene 1 12/23/22 15:59 V28406JMV
<0.447 µg/L 0.447 2.06Dibenz(a,h)anthracene 1 12/23/22 15:59 V28406JMV
<0.881 µg/L 0.881 5.15Dibenzofuran 1 12/23/22 15:59 V28406JMV
<2.06 µg/L 2.06 5.151,2-Dichlorobenzene 1 12/23/22 15:59 V28406JMV
<2.06 µg/L 2.06 5.151,3-Dichlorobenzene 1 12/23/22 15:59 V28406JMV
<2.11 µg/L 2.11 5.151,4-Dichlorobenzene 1 12/23/22 15:59 V28406JMV
<1.95 µg/L 1.95 5.15
3,3'-Dichlorobenzidine 1 12/23/22 15:59 V28406JMV
<1.50 µg/L 1.50 10.32,4-Dichlorophenol 1 12/23/22 15:59 V28406JMV
<0.767 µg/L 0.767 5.15Diethyl phthalate 1 12/23/22 15:59 V28406JMV
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 62 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
<0.967 µg/L 0.967 5.15Dimethyl phthalate 1 12/23/22 15:59 V28406JMV
<1.62 µg/L 1.62 20.6
2,4-Dimethylphenol 1 12/23/22 15:59 V28406JMV
<2.12 µg/L 2.12 5.15Di-n-butyl phthalate 1 12/23/22 15:59 V28406JMV
<2.13 µg/L 2.13 10.34,6-Dinitro-2-methylphenol 1 12/23/22 15:59 V28406JMV
<1.98 µg/L 1.98 10.32,4-Dinitrophenol 1 12/23/22 15:59 V28406JMV
<1.14 µg/L 1.14 5.15
2,4-Dinitrotoluene 1 12/23/22 15:59 V28406JMV
<0.833 µg/L 0.833 5.152,6-Dinitrotoluene 1 12/23/22 15:59 V28406JMV
<1.70 µg/L 1.70 5.15Di-n-Octyl Phthalate 1 12/23/22 15:59 V28406JMV
8.64 µg/L 0.257 2.06Fluoranthene 1 12/23/22 15:59 V28406JMV
93.7 µg/L 0.831 2.06Fluorene 1 12/23/22 15:59 V28406JMV
<1.01 µg/L 1.01 5.15Hexachlorobenzene 1 12/23/22 15:59 V28406JMV
<2.81 µg/L 2.81 5.15Hexachlorobutadiene 1 12/23/22 15:59 V28406JMV
<2.11 M µg/L 2.11 5.15Hexachlorocyclopentadiene 1 12/23/22 15:59 V28406JMV
<1.81 M µg/L 1.81 5.15Hexachloroethane 1 12/23/22 15:59 V28406JMV
<0.491 µg/L 0.491 2.06Indeno(1,2,3-cd)pyrene 1 12/23/22 15:59 V28406JMV
<0.457 µg/L 0.457 5.15Isophorone 1 12/23/22 15:59 V28406JMV
196 µg/L 1.17 2.061-Methylnaphthalene 1 12/23/22 15:59 V28406JMV
141 µg/L 0.685 2.062-Methylnaphthalene 1 12/23/22 15:59 V28406JMV
<0.749 µg/L 0.749 2.06Naphthalene 1 12/23/22 15:59 V28406JMV
<0.932 µg/L 0.932 5.15
Nitrobenzene 1 12/23/22 15:59 V28406JMV
<0.507 µg/L 0.507 5.152-Nitrophenol 1 12/23/22 15:59 V28406JMV
<1.27 µg/L 1.27 10.34-Nitrophenol 1 12/23/22 15:59 V28406JMV
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 63 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
625.1 (Prep)
625.1 Prep Batch(es):V28235 12/23/22 08:52
<1.13 µg/L 1.13 5.15N-Nitrosodiphenylamine 1 12/23/22 15:59 V28406JMV
<0.660 µg/L 0.660 5.15
N-Nitroso-di-n-propylamine 1 12/23/22 15:59 V28406JMV
<1.47 µg/L 1.47 5.15Pentachlorophenol 1 12/23/22 15:59 V28406JMV
165 µg/L 0.440 2.06Phenanthrene 1 12/23/22 15:59 V28406JMV
<0.670 µg/L 0.670 5.15Phenol 1 12/23/22 15:59 V28406JMV
40.4 µg/L 0.447 2.06
Pyrene 1 12/23/22 15:59 V28406JMV
<2.28 µg/L 2.28 5.151,2,4-Trichlorobenzene 1 12/23/22 15:59 V28406JMV
<1.36 µg/L 1.36 5.152,4,6-Trichlorophenol 1 12/23/22 15:59 V28406JMV
625.1Surrogate: Phenol-d5 14.4 Limits: 10-63%12/23/22 15:591 JMV
Surrogate: 2-Fluorobiphenyl 87.8 Limits: 49-118%12/23/22 15:591 JMV V28406
Surrogate: 2-Fluorophenol 22.3 Limits: 22-84%12/23/22 15:591 JMV V28406
Surrogate: Nitrobenzene-d5 I *Limits: 43-123%12/23/22 15:591 JMV V28406
Surrogate: 4-Terphenyl-d14 94.6 Limits: 49-151%12/23/22 15:591 JMV V28406
Surrogate: 2,4,6-Tribromophenol 93.1 Limits: 31-144%12/23/22 15:591 JMV V28406
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 64 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
CALCULATION
540 µg/L 115 500Aliphatic C5-C8 (Adjusted)10 12/21/22 14:50
6440 µg/L 258 500
Aliphatics C9-C12 (Adjusted)10 12/21/22 14:50
9360 µg/L 40.2 500Aromatic C9-C10 (Adjusted)10 12/21/22 14:50
155000 J µg/L 2520 10300Aromatic C11-C22 (Adjusted)1 12/23/22 15:59
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAEPH (Prep)
MADEP-EPH Prep Batch(es):V28366 12/29/22 09:00
350000 µg/L 1160 14400Aliphatic C9-C18 40 01/09/23 16:47 V28712JMV
20800 µg/L 5110 20600Aliphatic C19-C36 40 01/09/23 16:47 V28712JMV
155000 µg/L 2520 10300
Aromatic C11-C22 40 01/09/23 16:47 V28712JMV
MADEP-EPHSurrogate: 2-Bromonaphthalene 109 Limits: 40-140%01/09/23 16:4740 JMV
MADEP-EPHSurrogate: Chlorooctadecane 0 *Limits: 40-140%01/09/23 16:4740 JMV
MADEP-EPHSurrogate: OTP Surrogate 0 *Limits: 40-140%01/09/23 16:4740 JMV
Surrogate: 2-Fluorobiphenyl 133 Limits: 40-140%01/09/23 16:4740 JMV V28712
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28152 12/21/22 08:00
540 µg/L 115 500Aliphatic C5-C8 10 12/21/22 14:50 V28153TBL
15800 µg/L 258 500Aliphatic C9-C12 10 12/21/22 14:50 V28153TBL
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 65 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:MW-12
96171 Matrix:
12/20/2022 11:35
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
MAVPH (Prep)
MADEP-VPH Prep Batch(es):V28152 12/21/22 08:00
9360 µg/L 40.2 500Aromatic C9-C10 10 12/21/22 14:50 V28153TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (FID)21.1 *Limits: 70-130%12/21/22 14:5010 TBL
MADEP-VPHSurrogate: 2,5-Dibromotoluene (PID)21.2 *Limits: 70-130%12/21/22 14:5010 TBL
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 66 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:TW-1
96172 Matrix:
12/20/2022 13:55
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 21:26 6200BMSA
Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: Dibromofluoromethane 89.2 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 77.6 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: Toluene-d8 83.4 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/22/22 21:13100 MSA V28231
Surrogate: Dibromofluoromethane 92.6 Limits: 70-130%12/22/22 21:13100 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%12/22/22 21:13100 MSA V28231
Surrogate: Toluene-d8 98.0 Limits: 70-130%12/22/22 21:13100 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 67 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:TW-1
96172 Matrix:
12/20/2022 13:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 21:26 V28165MSA
11.0 µg/L 0.180 0.500
Benzene 1 12/21/22 21:26 V28165MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 21:26 V28165MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 21:26 V28165MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 21:26 V28165MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 21:26 V28165MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 21:26 V28165MSA
0.326 J µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 21:26 V28165MSA
1.07 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 21:26 V28165MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 21:26 V28165MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 21:26 V28165MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 21:26 V28165MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 21:26 V28165MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 21:26 V28165MSA
0.919 µg/L 0.220 0.500Chloroform 1 12/21/22 21:26 V28165MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 21:26 V28165MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 21:26 V28165MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 21:26 V28165MSA
12.5 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 21:26 V28165MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 21:26 V28165MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 21:26 V28165MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 21:26 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 68 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:TW-1
96172 Matrix:
12/20/2022 13:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 21:26 V28165MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 21:26 V28165MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 21:26 V28165MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 21:26 V28165MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 21:26 V28165MSA
1.37 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 21:26 V28165MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 21:26 V28165MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 21:26 V28165MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 21:26 V28165MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 21:26 V28165MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 21:26 V28165MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 21:26 V28165MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 21:26 V28165MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 21:26 V28165MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 21:26 V28165MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 21:26 V28165MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 21:26 V28165MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 21:26 V28165MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 21:26 V28165MSA
0.321 J
µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 21:26 V28165MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 21:26 V28165MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 21:26 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 69 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:TW-1
96172 Matrix:
12/20/2022 13:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
370 µg/L 14.0 100Methyl tert-butyl ether (MTBE)100 12/22/22 21:13 V28231MSA
<0.078 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 21:26 V28165MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 21:26 V28165MSA
2.58 µg/L 0.470 1.00Naphthalene 1 12/21/22 21:26 V28165MSA
0.301 J µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 21:26 V28165MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 21:26 V28165MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 21:26 V28165MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 21:26 V28165MSA
730 J µg/L 190 1000tert-Amyl Alcohol (TAA)100 12/22/22 21:13 V28231MSA
14.1 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 21:26 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 21:26 V28165MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 21:26 V28165MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 21:26 V28165MSA
0.508 µg/L 0.220 0.500Toluene 1 12/21/22 21:26 V28165MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 21:26 V28165MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 21:26 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 21:26 V28165MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 21:26 V28165MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 21:26 V28165MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 21:26 V28165MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 21:26 V28165MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/21/22 21:26 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 70 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:TW-1
96172 Matrix:
12/20/2022 13:55
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00 V28230 12/22/22 09:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 21:26 V28165MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 21:26 V28165MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 21:26 V28165MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/21/22 21:26 V28165MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 21:26 V28165MSA
<0.21 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 21:26 V28165
Surrogate: 4-Bromofluorobenzene 96.6 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: Dibromofluoromethane 89.2 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 77.6 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: Toluene-d8 83.4 Limits: 70-130%12/21/22 21:261 MSA V28165
Surrogate: 4-Bromofluorobenzene 100 Limits: 70-130%12/22/22 21:13100 MSA V28231
Surrogate: Dibromofluoromethane 92.6 Limits: 70-130%12/22/22 21:13100 MSA V28231
Surrogate: 1,2-Dichloroethane - d4 102 Limits: 70-130%12/22/22 21:13100 MSA V28231
Surrogate: Toluene-d8 98.0 Limits: 70-130%12/22/22 21:13100 MSA V28231
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 71 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
96173 Matrix:
12/20/2022 0:00
Aqueous
Test Results Units MDL MQL By Analytical
Method
Date / Time
Analyzed
DF
<1.00 µg/L 1.00 10.03,3-Dimethyl-1-butanol 1 12/21/22 19:03 6200BMSA
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%12/21/22 19:031 MSA V28165
Surrogate: Dibromofluoromethane 89.6 Limits: 70-130%12/21/22 19:031 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 78.8 Limits: 70-130%12/21/22 19:031 MSA V28165
Surrogate: Toluene-d8 97.0 Limits: 70-130%12/21/22 19:031 MSA V28165
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 72 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
96173 Matrix:
12/20/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<1.80 µg/L 1.80 10.0Acetone 1 12/21/22 19:03 V28165MSA
<0.180 µg/L 0.180 0.500
Benzene 1 12/21/22 19:03 V28165MSA
<0.210 µg/L 0.210 0.500Bromobenzene 1 12/21/22 19:03 V28165MSA
<0.420 µg/L 0.420 1.00Bromochloromethane 1 12/21/22 19:03 V28165MSA
<0.160 µg/L 0.160 0.500Bromodichloromethane 1 12/21/22 19:03 V28165MSA
<1.50 µg/L 1.50 5.00
Bromoform 1 12/21/22 19:03 V28165MSA
<0.280 µg/L 0.280 1.00Bromomethane 1 12/21/22 19:03 V28165MSA
<0.180 µg/L 0.180 0.500n-Butylbenzene 1 12/21/22 19:03 V28165MSA
<0.200 µg/L 0.200 0.500sec-Butyl benzene 1 12/21/22 19:03 V28165MSA
<0.920 µg/L 0.920 2.00tert-Butyl benzene 1 12/21/22 19:03 V28165MSA
<0.180 µg/L 0.180 0.500Carbon Tetrachloride 1 12/21/22 19:03 V28165MSA
<0.190 µg/L 0.190 0.500Chlorobenzene 1 12/21/22 19:03 V28165MSA
<0.190 µg/L 0.190 0.500Chlorodibromomethane 1 12/21/22 19:03 V28165MSA
<0.430 µg/L 0.430 1.00Chloroethane 1 12/21/22 19:03 V28165MSA
<0.220 µg/L 0.220 0.500Chloroform 1 12/21/22 19:03 V28165MSA
<0.220 µg/L 0.220 0.500Chloromethane 1 12/21/22 19:03 V28165MSA
<0.200 µg/L 0.200 0.5002-Chlorotoluene 1 12/21/22 19:03 V28165MSA
<0.200 µg/L 0.200 0.5004-Chlorotoluene 1 12/21/22 19:03 V28165MSA
<0.500 µg/L 0.500 0.500Di-Isopropyl Ether (DIPE)1 12/21/22 19:03 V28165MSA
<1.10 µg/L 1.10 2.00
1,2-Dibromo-3-Chloropropane 1 12/21/22 19:03 V28165MSA
<0.200 µg/L 0.200 0.5001,2-Dibromoethane 1 12/21/22 19:03 V28165MSA
<0.230 µg/L 0.230 0.500Dibromomethane 1 12/21/22 19:03 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 73 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
96173 Matrix:
12/20/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.220 µg/L 0.220 0.5001,2-Dichlorobenzene 1 12/21/22 19:03 V28165MSA
<0.190 µg/L 0.190 0.500
1,3-Dichlorobenzene 1 12/21/22 19:03 V28165MSA
<0.210 µg/L 0.210 0.5001,4-Dichlorobenzene 1 12/21/22 19:03 V28165MSA
<1.20 µg/L 1.20 5.00Dichlorodifluoromethane 1 12/21/22 19:03 V28165MSA
<0.240 µg/L 0.240 0.5001,1-Dichloroethane 1 12/21/22 19:03 V28165MSA
<0.150 µg/L 0.150 0.500
1,2-Dichloroethane 1 12/21/22 19:03 V28165MSA
<0.150 µg/L 0.150 0.5001,1-Dichloroethene 1 12/21/22 19:03 V28165MSA
<0.200 µg/L 0.200 0.500cis-1,2-Dichloroethene 1 12/21/22 19:03 V28165MSA
<0.180 µg/L 0.180 0.500trans-1,2-Dichloroethene 1 12/21/22 19:03 V28165MSA
<0.190 µg/L 0.190 0.5001,2-Dichloropropane 1 12/21/22 19:03 V28165MSA
<0.130 µg/L 0.130 0.5001,3-Dichloropropane 1 12/21/22 19:03 V28165MSA
<0.210 µg/L 0.210 2.002,2-Dichloropropane 1 12/21/22 19:03 V28165MSA
<0.200 µg/L 0.200 0.5001,1-Dichloropropene 1 12/21/22 19:03 V28165MSA
<0.210 µg/L 0.210 0.500cis-1,3-Dichloropropene 1 12/21/22 19:03 V28165MSA
<0.150 µg/L 0.150 0.500trans-1,3-Dichloropropene 1 12/21/22 19:03 V28165MSA
<42.0 µg/L 42.0 200Ethanol 1 12/21/22 19:03 V28165MSA
<0.170 µg/L 0.170 0.500Ethylbenzene 1 12/21/22 19:03 V28165MSA
<0.350 µg/L 0.350 3.00Hexachlorobutadiene 1 12/21/22 19:03 V28165MSA
<0.380 µg/L 0.380 1.002-Hexanone 1 12/21/22 19:03 V28165MSA
<0.180 µg/L 0.180 0.500
Isopropylbenzene 1 12/21/22 19:03 V28165MSA
<0.089 µg/L 0.089 0.5004-Isopropyl toluene 1 12/21/22 19:03 V28165MSA
<0.710 µg/L 0.710 5.00Methyl Ethyl Ketone (MEK)1 12/21/22 19:03 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 74 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
96173 Matrix:
12/20/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.140 µg/L 0.140 1.00Methyl tert-butyl ether (MTBE)1 12/21/22 19:03 V28165MSA
<0.078 µg/L 0.078 1.00
4-Methyl-2-Pentanone 1 12/21/22 19:03 V28165MSA
<0.330 µg/L 0.330 2.00Methylene Chloride 1 12/21/22 19:03 V28165MSA
<0.470 µg/L 0.470 1.00Naphthalene 1 12/21/22 19:03 V28165MSA
<0.190 µg/L 0.190 0.500n-Propylbenzene 1 12/21/22 19:03 V28165MSA
<0.220 µg/L 0.220 0.500
Styrene 1 12/21/22 19:03 V28165MSA
<1.60 µg/L 1.60 10.0tert-Butyl Alcohol (TBA)1 12/21/22 19:03 V28165MSA
<0.350 µg/L 0.350 10.0tert-Butyl formate (TBF)1 12/21/22 19:03 V28165MSA
<1.90 µg/L 1.90 10.0tert-Amyl Alcohol (TAA)1 12/21/22 19:03 V28165MSA
<0.280 µg/L 0.280 10.0tert-Amyl Methyl Ether (TAME)1 12/21/22 19:03 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1,2-Tetrachloroethane 1 12/21/22 19:03 V28165MSA
<0.160 µg/L 0.160 0.5001,1,2,2-Tetrachloroethane 1 12/21/22 19:03 V28165MSA
<0.220 µg/L 0.220 0.500Tetrachloroethene 1 12/21/22 19:03 V28165MSA
<0.220 µg/L 0.220 0.500Toluene 1 12/21/22 19:03 V28165MSA
<0.380 µg/L 0.380 0.5001,2,3-Trichlorobenzene 1 12/21/22 19:03 V28165MSA
<0.310 µg/L 0.310 0.5001,2,4-Trichlorobenzene 1 12/21/22 19:03 V28165MSA
<0.160 µg/L 0.160 0.5001,1,1-Trichloroethane 1 12/21/22 19:03 V28165MSA
<0.096 µg/L 0.096 0.5001,1,2-Trichloroethane 1 12/21/22 19:03 V28165MSA
<0.180 µg/L 0.180 0.500Trichloroethene 1 12/21/22 19:03 V28165MSA
<0.180 µg/L 0.180 0.500
Trichlorofluoromethane 1 12/21/22 19:03 V28165MSA
<0.270 µg/L 0.270 0.5001,2,3-Trichloropropane 1 12/21/22 19:03 V28165MSA
<0.190 µg/L 0.190 0.5001,2,4-Trimethylbenzene 1 12/21/22 19:03 V28165MSA
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 75 of 100
,
REPORT OF ANALYSISReport Number :
Project
Information :
NC 28110
22-354-0019
00087
Geological Resources, Inc.
3502 Hayes Road
Joanna Alley
Monroe
Danyale Love
Project Manager
GRI #4236 Received : 12/20/2022
Trindale Mini Mart
Report Date : 01/10/2023
Sample ID :
Lab No :
Sampled:Trip Blanks
96173 Matrix:
12/20/2022 0:00
Aqueous
Analytical Method:
Prep Method:
Test Results Units MDL MQL By Analytical
Batch
Date / Time
Analyzed
DF
6200 PT
6200B Prep Batch(es):V28164 12/21/22 14:00
<0.180 µg/L 0.180 0.5001,3,5-Trimethylbenzene 1 12/21/22 19:03 V28165MSA
<1.00 µg/L 1.00 5.00
Vinyl Acetate 1 12/21/22 19:03 V28165MSA
<0.170 µg/L 0.170 0.500Vinyl Chloride 1 12/21/22 19:03 V28165MSA
<0.210 µg/L 0.210 0.500o-Xylene 1 12/21/22 19:03 V28165MSA
<0.420 µg/L 0.420 1.00m,p-Xylene 1 12/21/22 19:03 V28165MSA
<0.21 µg/L 0.210 0.500
Xylene (Total)1 12/21/22 19:03 V28165
Surrogate: 4-Bromofluorobenzene 98.0 Limits: 70-130%12/21/22 19:031 MSA V28165
Surrogate: Dibromofluoromethane 89.6 Limits: 70-130%12/21/22 19:031 MSA V28165
Surrogate: 1,2-Dichloroethane - d4 78.8 Limits: 70-130%12/21/22 19:031 MSA V28165
Surrogate: Toluene-d8 97.0 Limits: 70-130%12/21/22 19:031 MSA V28165
Qualifiers/Definitions Analyte detected in blankBOutside QC Limit*
Recovery out of rangeIDilution FactorDF
Minimum valueMEstimated valueJ
Method Quantitation LimitMQL
Page 76 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28165QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28164
Associated Lab Samples: 96166, 96167, 96168, 96169, 96170, 96171, 96172, 96173
LRB-V28164 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/21/22 18:4010.01.80<1.80µg/LAcetone
12/21/22 18:400.5000.180<0.180µg/LBenzene
12/21/22 18:400.5000.210<0.210µg/LBromobenzene
12/21/22 18:401.000.420<0.420µg/LBromochloromethane
12/21/22 18:400.5000.160<0.160µg/LBromodichloromethane
12/21/22 18:405.001.50<1.50µg/LBromoform
12/21/22 18:401.000.280<0.280µg/LBromomethane
12/21/22 18:400.5000.180<0.180µg/Ln-Butylbenzene
12/21/22 18:400.5000.200<0.200µg/Lsec-Butyl benzene
12/21/22 18:402.000.920<0.920µg/Ltert-Butyl benzene
12/21/22 18:400.5000.180<0.180µg/LCarbon Tetrachloride
12/21/22 18:400.5000.190<0.190µg/LChlorobenzene
12/21/22 18:400.5000.190<0.190µg/LChlorodibromomethane
12/21/22 18:401.000.430<0.430µg/LChloroethane
12/21/22 18:400.5000.220<0.220µg/LChloroform
12/21/22 18:400.5000.220<0.220µg/LChloromethane
12/21/22 18:400.5000.200<0.200µg/L2-Chlorotoluene
12/21/22 18:400.5000.200<0.200µg/L4-Chlorotoluene
12/21/22 18:400.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/21/22 18:402.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/21/22 18:400.5000.200<0.200µg/L1,2-Dibromoethane
12/21/22 18:400.5000.230<0.230µg/LDibromomethane
12/21/22 18:400.5000.220<0.220µg/L1,2-Dichlorobenzene
12/21/22 18:400.5000.190<0.190µg/L1,3-Dichlorobenzene
12/21/22 18:400.5000.210<0.210µg/L1,4-Dichlorobenzene
12/21/22 18:405.001.20<1.20µg/LDichlorodifluoromethane
12/21/22 18:400.5000.240<0.240µg/L1,1-Dichloroethane
Page 1 of 21Date:01/10/2023 12:16 PM
Page 77 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28165QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28164
Associated Lab Samples: 96166, 96167, 96168, 96169, 96170, 96171, 96172, 96173
LRB-V28164 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/21/22 18:400.5000.150<0.150µg/L1,2-Dichloroethane
12/21/22 18:400.5000.150<0.150µg/L1,1-Dichloroethene
12/21/22 18:400.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/21/22 18:400.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/21/22 18:400.5000.190<0.190µg/L1,2-Dichloropropane
12/21/22 18:400.5000.130<0.130µg/L1,3-Dichloropropane
12/21/22 18:402.000.210<0.210µg/L2,2-Dichloropropane
12/21/22 18:400.5000.200<0.200µg/L1,1-Dichloropropene
12/21/22 18:400.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/21/22 18:400.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/21/22 18:4020042.0<42.0µg/LEthanol
12/21/22 18:400.5000.170<0.170µg/LEthylbenzene
12/21/22 18:403.000.350<0.350µg/LHexachlorobutadiene
12/21/22 18:401.000.380<0.380µg/L2-Hexanone
12/21/22 18:400.5000.180<0.180µg/LIsopropylbenzene
12/21/22 18:400.5000.089<0.089µg/L4-Isopropyl toluene
12/21/22 18:405.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/21/22 18:401.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/21/22 18:401.000.078<0.078µg/L4-Methyl-2-Pentanone
12/21/22 18:402.000.330<0.330µg/LMethylene Chloride
12/21/22 18:401.000.470<0.470µg/LNaphthalene
12/21/22 18:400.5000.190<0.190µg/Ln-Propylbenzene
12/21/22 18:400.5000.220<0.220µg/LStyrene
12/21/22 18:4010.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
12/21/22 18:4010.00.350<0.350µg/Ltert-Butyl formate (TBF)
12/21/22 18:4010.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
12/21/22 18:4010.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 2 of 21Date:01/10/2023 12:16 PM
Page 78 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28165QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28164
Associated Lab Samples: 96166, 96167, 96168, 96169, 96170, 96171, 96172, 96173
LRB-V28164 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/21/22 18:400.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/21/22 18:400.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/21/22 18:400.5000.220<0.220µg/LTetrachloroethene
12/21/22 18:400.5000.220<0.220µg/LToluene
12/21/22 18:400.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/21/22 18:400.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/21/22 18:400.5000.160<0.160µg/L1,1,1-Trichloroethane
12/21/22 18:400.5000.096<0.096µg/L1,1,2-Trichloroethane
12/21/22 18:400.5000.180<0.180µg/LTrichloroethene
12/21/22 18:400.5000.180<0.180µg/LTrichlorofluoromethane
12/21/22 18:400.5000.270<0.270µg/L1,2,3-Trichloropropane
12/21/22 18:400.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/21/22 18:400.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/21/22 18:405.001.00<1.00µg/LVinyl Acetate
12/21/22 18:400.5000.170<0.170µg/LVinyl Chloride
12/21/22 18:400.5000.210<0.210µg/Lo-Xylene
12/21/22 18:401.000.420<0.420µg/Lm,p-Xylene
12/21/22 18:4010.01.00<1.00µg/L3,3-Dimethyl-1-butanol
12/21/22 18:404-Bromofluorobenzene (S)95.6 70-130
12/21/22 18:40Dibromofluoromethane (S)100 70-130
12/21/22 18:401,2-Dichloroethane - d4 (S)83.8 70-130
12/21/22 18:40Toluene-d8 (S)89.8 70-130
Page 3 of 21Date:01/10/2023 12:16 PM
Page 79 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28165QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28164
LCS-V28164 LCSD-V28164Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
35.5 88.798.039.240.0µg/LAcetone 40-160 9.9 20.0
22.4 11211322.520.0µg/LBenzene 70-130 0.4 20.0
16.8 84.086.517.320.0µg/LBromobenzene 70-130 2.9 20.0
22.0 11011122.120.0µg/LBromochloromethane 70-130 0.4 20.0
20.0 10010220.420.0µg/LBromodichloromethane 70-130 1.9 20.0
17.5 87.589.017.820.0µg/LBromoform 70-130 1.6 20.0
15.6 78.074.514.920.0µg/LBromomethane 60-140 4.5 20.0
17.8 89.091.018.220.0µg/Ln-Butylbenzene 70-130 2.2 20.0
17.9 89.588.517.720.0µg/Lsec-Butyl benzene 70-130 1.1 20.0
17.8 89.087.017.420.0µg/Ltert-Butyl benzene 70-130 2.2 20.0
21.2 10610420.720.0µg/LCarbon Tetrachloride 70-130 2.3 20.0
17.8 89.090.018.020.0µg/LChlorobenzene 70-130 1.1 20.0
20.8 10476.515.320.0µg/LChlorodibromomethane 70-130 30.4*20.0
18.2 91.090.518.120.0µg/LChloroethane 60-140 0.5 20.0
21.0 10510821.520.0µg/LChloroform 70-130 2.3 20.0
18.6 93.094.518.920.0µg/LChloromethane 60-140 1.6 20.0
17.6 88.087.017.420.0µg/L2-Chlorotoluene 70-130 1.1 20.0
17.8 89.087.017.420.0µg/L4-Chlorotoluene 70-130 2.2 20.0
22.8 11411523.020.0µg/LDi-Isopropyl Ether (DIPE)70-130 0.8 20.0
19.2 96.094.518.920.0µg/L1,2-Dibromo-3-Chloropropane 70-130 1.5 20.0
20.9 10579.015.820.0µg/L1,2-Dibromoethane 70-130 27.7*20.0
20.6 10310120.220.0µg/LDibromomethane 70-130 1.9 20.0
18.0 90.089.517.920.0µg/L1,2-Dichlorobenzene 70-130 0.5 20.0
18.3 91.588.517.720.0µg/L1,3-Dichlorobenzene 70-130 3.3 20.0
18.0 90.088.017.620.0µg/L1,4-Dichlorobenzene 70-130 2.2 20.0
17.3 86.583.516.720.0µg/LDichlorodifluoromethane 60-140 3.5 20.0
Page 4 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 80 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28165QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28164
LCS-V28164 LCSD-V28164Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
22.4 11211523.020.0µg/L1,1-Dichloroethane 70-130 2.6 20.0
19.5 97.598.019.620.0µg/L1,2-Dichloroethane 70-130 0.5 20.0
20.5 10311422.720.0µg/L1,1-Dichloroethene 70-130 10.1 20.0
22.2 11111021.920.0µg/Lcis-1,2-Dichloroethene 70-130 1.3 20.0
20.9 10511322.620.0µg/Ltrans-1,2-Dichloroethene 70-130 7.8 20.0
22.4 11211222.420.0µg/L1,2-Dichloropropane 70-130 0.0 20.0
20.2 10174.514.920.0µg/L1,3-Dichloropropane 70-130 30.1*20.0
23.8 11911422.820.0µg/L2,2-Dichloropropane 70-130 4.2 20.0
22.6 11311222.320.0µg/L1,1-Dichloropropene 70-130 1.3 20.0
21.2 10696.519.320.0µg/Lcis-1,3-Dichloropropene 70-130 9.3 20.0
20.8 10491.018.220.0µg/Ltrans-1,3-Dichloropropene 70-130 13.3 20.0
484 96.8111554500µg/LEthanol 60-140 13.4 20.0
17.9 89.590.518.120.0µg/LEthylbenzene 70-130 1.1 20.0
21.2 10610420.820.0µg/LHexachlorobutadiene 70-130 1.9 20.0
18.8 94.080.016.020.0µg/L2-Hexanone 60-140 16.0 20.0
18.6 93.010020.020.0µg/LIsopropylbenzene 70-130 7.2 20.0
18.8 94.092.018.420.0µg/L4-Isopropyl toluene 70-130 2.1 20.0
23.5 11893.518.720.0µg/LMethyl Ethyl Ketone (MEK)60-140 22.7*20.0
20.1 10110621.120.0µg/LMethyl tert-butyl ether (MTBE)70-130 4.8 20.0
20.0 10083.516.720.0µg/L4-Methyl-2-Pentanone 60-140 17.9 20.0
21.7 10912024.020.0µg/LMethylene Chloride 70-130 10.0 20.0
19.4 97.082.016.420.0µg/LNaphthalene 70-130 16.7 20.0
17.8 89.088.517.720.0µg/Ln-Propylbenzene 70-130 0.5 20.0
17.7 88.590.518.120.0µg/LStyrene 70-130 2.2 20.0
26.2 65.564.525.840.0µg/Ltert-Butyl Alcohol (TBA)40-140 1.5 20.0
50.0 12512851.340.0µg/Ltert-Butyl formate (TBF)40-140 2.5 20.0
Page 5 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 81 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28165QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28164
LCS-V28164 LCSD-V28164Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
18.6 93.094.018.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 1.0 20.0
42.4 10610742.740.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 0.7 20.0
18.1 90.590.518.120.0µg/L1,1,1,2-Tetrachloroethane 70-130 0.0 20.0
16.1 80.583.016.620.0µg/L1,1,2,2-Tetrachloroethane 70-130 3.0 20.0
22.5 11381.516.320.0µg/LTetrachloroethene 70-130 31.9*20.0
21.6 10895.019.020.0µg/LToluene 70-130 12.8 20.0
23.1 11699.019.820.0µg/L1,2,3-Trichlorobenzene 70-130 15.3 20.0
21.9 11010821.620.0µg/L1,2,4-Trichlorobenzene 70-130 1.3 20.0
20.7 10410721.320.0µg/L1,1,1-Trichloroethane 70-130 2.8 20.0
20.5 10393.518.720.0µg/L1,1,2-Trichloroethane 70-130 9.1 20.0
21.7 10911122.220.0µg/LTrichloroethene 70-130 2.2 20.0
18.5 92.598.019.620.0µg/LTrichlorofluoromethane 60-140 5.7 20.0
16.0 80.080.016.020.0µg/L1,2,3-Trichloropropane 70-130 0.0 20.0
18.1 90.589.517.920.0µg/L1,2,4-Trimethylbenzene 70-130 1.1 20.0
18.2 91.090.018.020.0µg/L1,3,5-Trimethylbenzene 70-130 1.1 20.0
23.1 11612424.720.0µg/LVinyl Acetate 60-140 6.6 20.0
19.9 99.597.019.420.0µg/LVinyl Chloride 60-140 2.5 20.0
17.3 86.589.517.920.0µg/Lo-Xylene 70-130 3.4 20.0
38.1 95.295.238.140.0µg/Lm,p-Xylene 70-130 0.0 20.0
18.2 91.077.515.520.0µg/L3,3-Dimethyl-1-butanol 70-130 16.0 20.0
95.096.44-Bromofluorobenzene (S)70-130
88.889.8Dibromofluoromethane (S)70-130
78.078.41,2-Dichloroethane - d4 (S)70-130
10174.8Toluene-d8 (S)70-130
Page 6 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 82 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28175
Associated Lab Samples: 96163, 96164, 96165
LRB-V28175 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/21/22 13:3310.01.80<1.80µg/LAcetone
12/21/22 13:330.5000.180<0.180µg/LBenzene
12/21/22 13:330.5000.210<0.210µg/LBromobenzene
12/21/22 13:331.000.420<0.420µg/LBromochloromethane
12/21/22 13:330.5000.160<0.160µg/LBromodichloromethane
12/21/22 13:335.001.50<1.50µg/LBromoform
12/21/22 13:331.000.280<0.280µg/LBromomethane
12/21/22 13:330.5000.180<0.180µg/Ln-Butylbenzene
12/21/22 13:330.5000.200<0.200µg/Lsec-Butyl benzene
12/21/22 13:332.000.920<0.920µg/Ltert-Butyl benzene
12/21/22 13:330.5000.180<0.180µg/LCarbon Tetrachloride
12/21/22 13:330.5000.190<0.190µg/LChlorobenzene
12/21/22 13:330.5000.190<0.190µg/LChlorodibromomethane
12/21/22 13:331.000.430<0.430µg/LChloroethane
12/21/22 13:330.5000.220<0.220µg/LChloroform
12/21/22 13:330.5000.220<0.220µg/LChloromethane
12/21/22 13:330.5000.200<0.200µg/L2-Chlorotoluene
12/21/22 13:330.5000.200<0.200µg/L4-Chlorotoluene
12/21/22 13:330.5000.500<0.500µg/LDi-Isopropyl Ether (DIPE)
12/21/22 13:332.001.10<1.10µg/L1,2-Dibromo-3-Chloropropane
12/21/22 13:330.5000.200<0.200µg/L1,2-Dibromoethane
12/21/22 13:330.5000.230<0.230µg/LDibromomethane
12/21/22 13:330.5000.220<0.220µg/L1,2-Dichlorobenzene
12/21/22 13:330.5000.190<0.190µg/L1,3-Dichlorobenzene
12/21/22 13:330.5000.210<0.210µg/L1,4-Dichlorobenzene
12/21/22 13:335.001.20<1.20µg/LDichlorodifluoromethane
12/21/22 13:330.5000.240<0.240µg/L1,1-Dichloroethane
Page 7 of 21Date:01/10/2023 12:16 PM
Page 83 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28175
Associated Lab Samples: 96163, 96164, 96165
LRB-V28175 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/21/22 13:330.5000.150<0.150µg/L1,2-Dichloroethane
12/21/22 13:330.5000.150<0.150µg/L1,1-Dichloroethene
12/21/22 13:330.5000.200<0.200µg/Lcis-1,2-Dichloroethene
12/21/22 13:330.5000.180<0.180µg/Ltrans-1,2-Dichloroethene
12/21/22 13:330.5000.190<0.190µg/L1,2-Dichloropropane
12/21/22 13:330.5000.130<0.130µg/L1,3-Dichloropropane
12/21/22 13:332.000.210<0.210µg/L2,2-Dichloropropane
12/21/22 13:330.5000.200<0.200µg/L1,1-Dichloropropene
12/21/22 13:330.5000.210<0.210µg/Lcis-1,3-Dichloropropene
12/21/22 13:330.5000.150<0.150µg/Ltrans-1,3-Dichloropropene
12/21/22 13:3320042.0<42.0µg/LEthanol
12/21/22 13:330.5000.170<0.170µg/LEthylbenzene
12/21/22 13:333.000.350<0.350µg/LHexachlorobutadiene
12/21/22 13:331.000.380<0.380µg/L2-Hexanone
12/21/22 13:330.5000.180<0.180µg/LIsopropylbenzene
12/21/22 13:330.5000.089<0.089µg/L4-Isopropyl toluene
12/21/22 13:335.000.710<0.710µg/LMethyl Ethyl Ketone (MEK)
12/21/22 13:331.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/21/22 13:331.000.078<0.078µg/L4-Methyl-2-Pentanone
12/21/22 13:332.000.330<0.330µg/LMethylene Chloride
12/21/22 13:331.000.470<0.470µg/LNaphthalene
12/21/22 13:330.5000.190<0.190µg/Ln-Propylbenzene
12/21/22 13:330.5000.220<0.220µg/LStyrene
12/21/22 13:3310.01.60<1.60µg/Ltert-Butyl Alcohol (TBA)
12/21/22 13:3310.00.350<0.350µg/Ltert-Butyl formate (TBF)
12/21/22 13:3310.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
12/21/22 13:3310.00.280<0.280µg/Ltert-Amyl Methyl Ether (TAME)
Page 8 of 21Date:01/10/2023 12:16 PM
Page 84 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28175
Associated Lab Samples: 96163, 96164, 96165
LRB-V28175 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/21/22 13:330.5000.160<0.160µg/L1,1,1,2-Tetrachloroethane
12/21/22 13:330.5000.160<0.160µg/L1,1,2,2-Tetrachloroethane
12/21/22 13:330.5000.220<0.220µg/LTetrachloroethene
12/21/22 13:330.5000.220<0.220µg/LToluene
12/21/22 13:330.5000.380<0.380µg/L1,2,3-Trichlorobenzene
12/21/22 13:330.5000.310<0.310µg/L1,2,4-Trichlorobenzene
12/21/22 13:330.5000.160<0.160µg/L1,1,1-Trichloroethane
12/21/22 13:330.5000.096<0.096µg/L1,1,2-Trichloroethane
12/21/22 13:330.5000.180<0.180µg/LTrichloroethene
12/21/22 13:330.5000.180<0.180µg/LTrichlorofluoromethane
12/21/22 13:330.5000.270<0.270µg/L1,2,3-Trichloropropane
12/21/22 13:330.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/21/22 13:330.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/21/22 13:335.001.00<1.00µg/LVinyl Acetate
12/21/22 13:330.5000.170<0.170µg/LVinyl Chloride
12/21/22 13:330.5000.210<0.210µg/Lo-Xylene
12/21/22 13:331.000.420<0.420µg/Lm,p-Xylene
12/21/22 13:3310.01.00<1.00µg/L3,3-Dimethyl-1-butanol
12/21/22 13:334-Bromofluorobenzene (S)102 70-130
12/21/22 13:33Dibromofluoromethane (S)94.0 70-130
12/21/22 13:331,2-Dichloroethane - d4 (S)101 70-130
12/21/22 13:33Toluene-d8 (S)98.6 70-130
Page 9 of 21Date:01/10/2023 12:16 PM
Page 85 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28175
LCS-V28175 LCSD-V28175Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
49.3 12311545.840.0µg/LAcetone 40-160 7.3 20.0
19.7 98.598.519.720.0µg/LBenzene 70-130 0.0 20.0
19.0 95.010120.120.0µg/LBromobenzene 70-130 5.6 20.0
18.8 94.093.518.720.0µg/LBromochloromethane 70-130 0.5 20.0
18.6 93.092.018.420.0µg/LBromodichloromethane 70-130 1.0 20.0
19.7 98.597.019.420.0µg/LBromoform 70-130 1.5 20.0
19.0 95.090.518.120.0µg/LBromomethane 60-140 4.8 20.0
18.7 93.598.019.620.0µg/Ln-Butylbenzene 70-130 4.6 20.0
18.7 93.598.019.620.0µg/Lsec-Butyl benzene 70-130 4.6 20.0
18.9 94.598.519.720.0µg/Ltert-Butyl benzene 70-130 4.1 20.0
20.5 10399.019.820.0µg/LCarbon Tetrachloride 70-130 3.4 20.0
19.5 97.599.019.820.0µg/LChlorobenzene 70-130 1.5 20.0
17.3 86.585.517.120.0µg/LChlorodibromomethane 70-130 1.1 20.0
19.5 97.510521.020.0µg/LChloroethane 60-140 7.4 20.0
19.5 97.598.019.620.0µg/LChloroform 70-130 0.5 20.0
20.2 10110420.820.0µg/LChloromethane 60-140 2.9 20.0
19.2 96.098.519.720.0µg/L2-Chlorotoluene 70-130 2.5 20.0
19.0 95.096.519.320.0µg/L4-Chlorotoluene 70-130 1.5 20.0
22.5 11311122.220.0µg/LDi-Isopropyl Ether (DIPE)70-130 1.3 20.0
18.2 91.085.017.020.0µg/L1,2-Dibromo-3-Chloropropane 70-130 6.8 20.0
19.1 95.594.018.820.0µg/L1,2-Dibromoethane 70-130 1.5 20.0
18.9 94.591.518.320.0µg/LDibromomethane 70-130 3.2 20.0
19.0 95.095.519.120.0µg/L1,2-Dichlorobenzene 70-130 0.5 20.0
18.8 94.094.518.920.0µg/L1,3-Dichlorobenzene 70-130 0.5 20.0
19.0 95.095.019.020.0µg/L1,4-Dichlorobenzene 70-130 0.0 20.0
19.8 99.010320.620.0µg/LDichlorodifluoromethane 60-140 3.9 20.0
Page 10 of 21Date:01/10/2023 12:16 PM
Page 86 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28175
LCS-V28175 LCSD-V28175Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
20.4 10210521.020.0µg/L1,1-Dichloroethane 70-130 2.8 20.0
19.6 98.098.519.720.0µg/L1,2-Dichloroethane 70-130 0.5 20.0
21.0 10510721.420.0µg/L1,1-Dichloroethene 70-130 1.8 20.0
19.8 99.010020.020.0µg/Lcis-1,2-Dichloroethene 70-130 1.0 20.0
20.1 10110320.620.0µg/Ltrans-1,2-Dichloroethene 70-130 2.4 20.0
19.9 99.510120.220.0µg/L1,2-Dichloropropane 70-130 1.4 20.0
19.1 95.594.018.820.0µg/L1,3-Dichloropropane 70-130 1.5 20.0
18.7 93.510220.320.0µg/L2,2-Dichloropropane 70-130 8.2 20.0
20.6 10310721.420.0µg/L1,1-Dichloropropene 70-130 3.8 20.0
19.8 99.099.019.820.0µg/Lcis-1,3-Dichloropropene 70-130 0.0 20.0
19.4 97.097.019.420.0µg/Ltrans-1,3-Dichloropropene 70-130 0.0 20.0
488 97.6108539500µg/LEthanol 60-140 9.9 20.0
19.1 95.599.519.920.0µg/LEthylbenzene 70-130 4.1 20.0
18.4 92.094.518.920.0µg/LHexachlorobutadiene 70-130 2.6 20.0
20.9 10599.019.820.0µg/L2-Hexanone 60-140 5.4 20.0
19.4 97.010120.220.0µg/LIsopropylbenzene 70-130 4.0 20.0
19.0 95.099.519.920.0µg/L4-Isopropyl toluene 70-130 4.6 20.0
18.2 91.076.515.320.0µg/LMethyl Ethyl Ketone (MEK)60-140 17.3 20.0
21.2 10696.519.320.0µg/LMethyl tert-butyl ether (MTBE)70-130 9.3 20.0
21.2 10699.019.820.0µg/L4-Methyl-2-Pentanone 60-140 6.8 20.0
19.4 97.097.519.520.0µg/LMethylene Chloride 70-130 0.5 20.0
20.0 10094.518.920.0µg/LNaphthalene 70-130 5.6 20.0
19.0 95.099.019.820.0µg/Ln-Propylbenzene 70-130 4.1 20.0
18.6 93.098.019.620.0µg/LStyrene 70-130 5.2 20.0
41.3 10394.037.640.0µg/Ltert-Butyl Alcohol (TBA)40-140 9.3 20.0
40.6 10210040.040.0µg/Ltert-Butyl formate (TBF)40-140 1.4 20.0
Page 11 of 21Date:01/10/2023 12:16 PM
Page 87 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28176QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28175
LCS-V28175 LCSD-V28175Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
20.7 10410921.820.0µg/Ltert-Amyl Alcohol (TAA)40-140 5.1 20.0
41.9 10510240.740.0µg/Ltert-Amyl Methyl Ether (TAME)40-140 2.9 20.0
18.4 92.094.518.920.0µg/L1,1,1,2-Tetrachloroethane 70-130 2.6 20.0
18.4 92.092.518.520.0µg/L1,1,2,2-Tetrachloroethane 70-130 0.5 20.0
18.9 94.597.519.520.0µg/LTetrachloroethene 70-130 3.1 20.0
19.7 98.598.019.620.0µg/LToluene 70-130 0.5 20.0
20.6 10399.019.820.0µg/L1,2,3-Trichlorobenzene 70-130 3.9 20.0
19.1 95.598.519.720.0µg/L1,2,4-Trichlorobenzene 70-130 3.0 20.0
19.8 99.099.519.920.0µg/L1,1,1-Trichloroethane 70-130 0.5 20.0
19.4 97.098.019.620.0µg/L1,1,2-Trichloroethane 70-130 1.0 20.0
19.3 96.596.519.320.0µg/LTrichloroethene 70-130 0.0 20.0
19.6 98.099.019.820.0µg/LTrichlorofluoromethane 60-140 1.0 20.0
19.4 97.093.518.720.0µg/L1,2,3-Trichloropropane 70-130 3.6 20.0
18.9 94.597.519.520.0µg/L1,2,4-Trimethylbenzene 70-130 3.1 20.0
19.4 97.010120.220.0µg/L1,3,5-Trimethylbenzene 70-130 4.0 20.0
19.8 99.010120.220.0µg/LVinyl Acetate 60-140 2.0 20.0
20.3 10210420.820.0µg/LVinyl Chloride 60-140 2.4 20.0
19.0 95.096.519.320.0µg/Lo-Xylene 70-130 1.5 20.0
40.2 10110341.340.0µg/Lm,p-Xylene 70-130 2.6 20.0
19.8 99.011021.920.0µg/L3,3-Dimethyl-1-butanol 70-130 10.0 20.0
98.81024-Bromofluorobenzene (S)70-130
98.897.4Dibromofluoromethane (S)70-130
1051001,2-Dichloroethane - d4 (S)70-130
99.2101Toluene-d8 (S)70-130
Page 12 of 21Date:01/10/2023 12:16 PM
Page 88 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Volatile Organic Compounds - GC/MS
6200B
V28231QC Analytical Batch(es):
Analysis Method:
Analysis Description:
6200 PT
QC Prep:V28230
Associated Lab Samples: 96164, 96165, 96166, 96168, 96170, 96172
LRB-V28230 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/22/22 15:210.5000.180<0.180µg/LBenzene
12/22/22 15:211.000.140<0.140µg/LMethyl tert-butyl ether (MTBE)
12/22/22 15:211.000.470<0.470µg/LNaphthalene
12/22/22 15:2110.01.90<1.90µg/Ltert-Amyl Alcohol (TAA)
12/22/22 15:210.5000.190<0.190µg/L1,2,4-Trimethylbenzene
12/22/22 15:210.5000.180<0.180µg/L1,3,5-Trimethylbenzene
12/22/22 15:214-Bromofluorobenzene (S)100 70-130
12/22/22 15:21Dibromofluoromethane (S)93.6 70-130
12/22/22 15:211,2-Dichloroethane - d4 (S)98.2 70-130
12/22/22 15:21Toluene-d8 (S)99.2 70-130
LCS-V28230 LCSD-V28230Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
19.1 95.512124.120.0µg/LBenzene 70-130 23.1*20.0
19.5 97.512825.620.0µg/LMethyl tert-butyl ether (MTBE)70-130 27.0*20.0
20.8 10412825.620.0µg/LNaphthalene 70-130 20.6*20.0
24.2 12114028.020.0µg/Ltert-Amyl Alcohol (TAA)40-140 14.5 20.0
18.8 94.011623.220.0µg/L1,2,4-Trimethylbenzene 70-130 20.9*20.0
19.5 97.511923.820.0µg/L1,3,5-Trimethylbenzene 70-130 19.8 20.0
1011014-Bromofluorobenzene (S)70-130
96.2101Dibromofluoromethane (S)70-130
1021061,2-Dichloroethane - d4 (S)70-130
98.499.8Toluene-d8 (S)70-130
Page 13 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 89 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V28406QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V28235
Associated Lab Samples: 96170, 96171
LRB-V28235 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/23/22 14:292.000.302<0.302µg/LAcenaphthene
12/23/22 14:292.000.297<0.297µg/LAcenaphthylene
12/23/22 14:292.000.836<0.836µg/LAnthracene
12/23/22 14:2910.01.32<1.32µg/LBenzidine
12/23/22 14:292.000.637<0.637µg/LBenzo(a)anthracene
12/23/22 14:292.001.02<1.02µg/LBenzo(a)pyrene
12/23/22 14:295.002.49<2.49µg/LBenzo(b)fluoranthene
12/23/22 14:295.001.01<1.01µg/LBenzo(g,h,i)perylene
12/23/22 14:295.001.99<1.99µg/LBenzo(k)fluoranthene
12/23/22 14:2910.01.10<1.10µg/LBenzoic Acid
12/23/22 14:295.000.684<0.684µg/LBenzyl alcohol
12/23/22 14:295.000.468<0.468µg/LBis(2-Chloroethoxy)methane
12/23/22 14:295.001.04<1.04µg/LBis(2-Chloroethyl)ether
12/23/22 14:295.001.08<1.08µg/LBis(2-Chloroisopropyl)ether
12/23/22 14:2950.024.0<24.0µg/LBis(2-ethylhexyl)phthalate
12/23/22 14:295.001.11<1.11µg/L4-Bromophenyl phenyl ether
12/23/22 14:295.001.83<1.83µg/LButyl benzyl phthalate
12/23/22 14:295.001.18<1.18µg/L4-Chloro-3-methylphenol
12/23/22 14:2920.07.38<7.38µg/L2-Chloronaphthalene
12/23/22 14:2910.00.938<0.938µg/L2-Chlorophenol
12/23/22 14:295.001.71<1.71µg/L4-Chlorophenyl phenyl ether
12/23/22 14:292.000.405<0.405µg/LChrysene
12/23/22 14:292.000.434<0.434µg/LDibenz(a,h)anthracene
12/23/22 14:295.000.856<0.856µg/LDibenzofuran
12/23/22 14:295.002.00<2.00µg/L1,2-Dichlorobenzene
12/23/22 14:295.002.00<2.00µg/L1,3-Dichlorobenzene
12/23/22 14:295.002.05<2.05µg/L1,4-Dichlorobenzene
Page 14 of 21Date:01/10/2023 12:16 PM
Page 90 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V28406QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V28235
Associated Lab Samples: 96170, 96171
LRB-V28235 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/23/22 14:295.001.89<1.89µg/L3,3'-Dichlorobenzidine
12/23/22 14:2910.01.46<1.46µg/L2,4-Dichlorophenol
12/23/22 14:295.000.745<0.745µg/LDiethyl phthalate
12/23/22 14:295.000.939<0.939µg/LDimethyl phthalate
12/23/22 14:2920.01.57<1.57µg/L2,4-Dimethylphenol
12/23/22 14:295.002.06<2.06µg/LDi-n-butyl phthalate
12/23/22 14:2910.02.07<2.07µg/L4,6-Dinitro-2-methylphenol
12/23/22 14:2910.01.92<1.92µg/L2,4-Dinitrophenol
12/23/22 14:295.001.11<1.11µg/L2,4-Dinitrotoluene
12/23/22 14:295.000.809<0.809µg/L2,6-Dinitrotoluene
12/23/22 14:295.001.65<1.65µg/LDi-n-Octyl Phthalate
12/23/22 14:292.000.250<0.250µg/LFluoranthene
12/23/22 14:292.000.807<0.807µg/LFluorene
12/23/22 14:295.000.979<0.979µg/LHexachlorobenzene
12/23/22 14:295.002.73<2.73µg/LHexachlorobutadiene
12/23/22 14:295.002.05<2.05µg/LHexachlorocyclopentadiene
12/23/22 14:295.001.76<1.76µg/LHexachloroethane
12/23/22 14:292.000.477<0.477µg/LIndeno(1,2,3-cd)pyrene
12/23/22 14:295.000.444<0.444µg/LIsophorone
12/23/22 14:292.001.14<1.14µg/L1-Methylnaphthalene
12/23/22 14:292.000.666<0.666µg/L2-Methylnaphthalene
12/23/22 14:292.000.728<0.728µg/LNaphthalene
12/23/22 14:295.000.905<0.905µg/LNitrobenzene
12/23/22 14:295.000.493<0.493µg/L2-Nitrophenol
12/23/22 14:2910.01.23<1.23µg/L4-Nitrophenol
12/23/22 14:295.001.10<1.10µg/LN-Nitrosodiphenylamine
12/23/22 14:295.000.641<0.641µg/LN-Nitroso-di-n-propylamine
Page 15 of 21Date:01/10/2023 12:16 PM
Page 91 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V28406QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V28235
Associated Lab Samples: 96170, 96171
LRB-V28235 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/23/22 14:295.001.43<1.43µg/LPentachlorophenol
12/23/22 14:292.000.428<0.428µg/LPhenanthrene
12/23/22 14:295.000.651<0.651µg/LPhenol
12/23/22 14:292.000.434<0.434µg/LPyrene
12/23/22 14:295.002.21<2.21µg/L1,2,4-Trichlorobenzene
12/23/22 14:295.001.32<1.32µg/L2,4,6-Trichlorophenol
12/23/22 14:292-Fluorobiphenyl (S)72.0 49-118
12/23/22 14:292-Fluorophenol (S)43.4 22-84
12/23/22 14:29Nitrobenzene-d5 (S)65.0 43-123
12/23/22 14:294-Terphenyl-d14 (S)101 49-151
12/23/22 14:292,4,6-Tribromophenol (S)71.5 31-144
12/23/22 14:29Phenol-d5 (S)30.5 10-63
LCS-V28235 LCSD-V28235Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
28.2 56.468.634.350.0µg/LAcenaphthene 47-145 19.5 20.0
28.3 56.668.634.350.0µg/LAcenaphthylene 33-145 19.1 20.0
34.8 69.676.038.050.0µg/LAnthracene 27-133 8.7 20.0
23.2 46.448.424.250.0µg/LBenzidine 15-150 4.2 20.0
36.5 73.077.438.750.0µg/LBenzo(a)anthracene 33-143 5.8 20.0
35.7 71.477.038.550.0µg/LBenzo(a)pyrene 17-163 7.5 20.0
32.9 65.868.634.350.0µg/LBenzo(b)fluoranthene 24-159 4.1 20.0
30.9 61.864.832.450.0µg/LBenzo(g,h,i)perylene 10-219 4.7 20.0
30.6 61.266.433.250.0µg/LBenzo(k)fluoranthene 11-162 8.1 20.0
9.97 19.923.411.750.0µg/LBenzoic Acid 10-125 15.9 20.0
Page 16 of 21Date:01/10/2023 12:16 PM
Page 92 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V28406QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V28235
LCS-V28235 LCSD-V28235Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
24.6 49.260.230.150.0µg/LBenzyl alcohol 16-107 20.1*20.0
22.9 45.858.629.350.0µg/LBis(2-Chloroethoxy)methane 33-184 24.5*20.0
13.7 27.435.817.950.0µg/LBis(2-Chloroethyl)ether 12-158 26.5*20.0
22.0 44.055.427.750.0µg/LBis(2-Chloroisopropyl)ether 36-166 22.9*20.0
40.0 80.086.243.150.0µg/LBis(2-ethylhexyl)phthalate 10-158 7.4 20.0
32.7 65.474.237.150.0µg/L4-Bromophenyl phenyl ether 53-127 12.6 20.0
40.6 81.283.841.950.0µg/LButyl benzyl phthalate 10-152 3.1 20.0
27.6 55.264.432.250.0µg/L4-Chloro-3-methylphenol 22-147 15.3 20.0
25.3 50.6*65.832.950.0µg/L2-Chloronaphthalene 60-118 26.1*20.0
21.5 43.055.027.550.0µg/L2-Chlorophenol 23-134 24.4*20.0
31.6 63.272.036.050.0µg/L4-Chlorophenyl phenyl ether 25-158 13.0 20.0
38.0 76.081.440.750.0µg/LChrysene 17-168 6.8 20.0
31.3 62.664.832.450.0µg/LDibenz(a,h)anthracene 10-227 3.4 20.0
29.0 58.068.634.350.0µg/LDibenzofuran 39-114 16.7 20.0
18.6 37.246.823.450.0µg/L1,2-Dichlorobenzene 32-129 22.8*20.0
17.9 35.847.023.550.0µg/L1,3-Dichlorobenzene 20-124 27.0*20.0
17.8 35.646.423.250.0µg/L1,4-Dichlorobenzene 20-124 26.3*20.0
30.3 60.664.632.350.0µg/L3,3'-Dichlorobenzidine 10-262 6.3 20.0
23.2 46.458.429.250.0µg/L2,4-Dichlorophenol 39-135 22.9*20.0
35.1 70.278.639.350.0µg/LDiethyl phthalate 10-114 11.2 20.0
33.7 67.477.638.850.0µg/LDimethyl phthalate 10-112 14.0 20.0
25.9 51.862.831.450.0µg/L2,4-Dimethylphenol 32-119 19.1 20.0
39.8 79.685.442.750.0µg/LDi-n-butyl phthalate 10-118 7.0 20.0
29.6 59.263.431.750.0µg/L4,6-Dinitro-2-methylphenol 10-181 6.8 20.0
22.2 44.452.426.250.0µg/L2,4-Dinitrophenol 10-191 16.5 20.0
36.4 72.879.839.950.0µg/L2,4-Dinitrotoluene 39-139 9.1 20.0
Page 17 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 93 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V28406QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V28235
LCS-V28235 LCSD-V28235Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
35.2 70.478.239.150.0µg/L2,6-Dinitrotoluene 50-158 10.4 20.0
34.9 69.876.038.050.0µg/LDi-n-Octyl Phthalate 10-146 8.5 20.0
35.6 71.277.838.950.0µg/LFluoranthene 26-137 8.8 20.0
31.7 63.474.237.150.0µg/LFluorene 59-121 15.6 20.0
31.5 63.069.634.850.0µg/LHexachlorobenzene 10-152 9.9 20.0
18.0 36.048.424.250.0µg/LHexachlorobutadiene 24-116 29.3*20.0
6.87 13.7*19.7*9.8750.0µg/LHexachlorocyclopentadiene 32-117 35.8*20.0
15.8 31.6*41.620.850.0µg/LHexachloroethane 40-113 27.3*20.0
30.5 61.064.632.350.0µg/LIndeno(1,2,3-cd)pyrene 10-171 5.7 20.0
16.5 33.041.820.950.0µg/LIsophorone 21-196 23.5*20.0
21.4 42.854.827.450.0µg/L1-Methylnaphthalene 40-135 24.5*20.0
19.9 39.852.826.450.0µg/L2-Methylnaphthalene 18-121 28.0*20.0
19.6 39.250.425.250.0µg/LNaphthalene 21-133 25.0*20.0
21.0 42.051.225.650.0µg/LNitrobenzene 35-180 19.7 20.0
21.4 42.855.827.950.0µg/L2-Nitrophenol 29-182 26.3*20.0
19.5 39.028.014.050.0µg/L4-Nitrophenol 10-132 32.8*20.0
41.7 83.492.446.250.0µg/LN-Nitrosodiphenylamine 69-152 10.2 20.0
22.8 45.658.829.450.0µg/LN-Nitroso-di-n-propylamine 10-230 25.2*20.0
32.9 65.872.436.250.0µg/LPentachlorophenol 14-176 9.5 20.0
35.2 70.476.638.350.0µg/LPhenanthrene 54-120 8.4 20.0
11.4 22.829.214.650.0µg/LPhenol 10-112 24.6*20.0
38.5 77.083.841.950.0µg/LPyrene 52-115 8.4 20.0
18.7 37.4*49.824.950.0µg/L1,2,4-Trichlorobenzene 44-142 28.4*20.0
28.8 57.671.035.550.0µg/L2,4,6-Trichlorophenol 37-144 20.8*20.0
51.266.22-Fluorobiphenyl (S)49-118
26.834.22-Fluorophenol (S)22-84
Page 18 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 94 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
625.1 - Base/Neutrals and Acids by GC/MS
625.1
V28406QC Analytical Batch(es):
Analysis Method:
Analysis Description:
625.1 (Prep)
QC Prep:V28235
LCS-V28235 LCSD-V28235Laboratory Control Sample & LCSD
LCSDResultParameter LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
39.6*50.0Nitrobenzene-d5 (S)43-123
86.894.24-Terphenyl-d14 (S)49-151
60.969.82,4,6-Tribromophenol (S)31-144
19.023.8Phenol-d5 (S)10-63
Page 19 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 95 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Massachusetts EPH
MADEP-EPH
V28712QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAEPH (Prep)
QC Prep:V28366
Associated Lab Samples: 96170, 96171
LRB-V28366 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
01/07/23 02:3135028.2108µg/LAliphatic C9-C18
01/07/23 02:31500124<124µg/LAliphatic C19-C36
01/07/23 02:3125061.2<61.2µg/LAromatic C11-C22
01/07/23 02:312-Fluorobiphenyl (S)136 40-140
01/07/23 02:312-Bromonaphthalene (S)138 40-140
01/07/23 02:31Chlorooctadecane (S)88.5 40-140
01/07/23 02:31OTP Surrogate (S)98.0 40-140
LCS-V28366 LCSD-V28366Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
667 111108648600µg/LAliphatic C9-C18 40-140 2.8 50.0
871 109104835800µg/LAliphatic C19-C36 40-140 4.2 50.0
1980 11613122201700µg/LAromatic C11-C22 40-140 11.4 50.0
148*163*2-Fluorobiphenyl (S)40-140
147*166*2-Bromonaphthalene (S)40-140
94.097.5Chlorooctadecane (S)40-140
109117OTP Surrogate (S)40-140
Page 20 of 21* QC Fail Date:01/10/2023 12:16 PM
Page 96 of 100
Quality Control Data
22-354-0019Report No:
Project Description:
Client ID:Geological Resources, Inc.
Trindale Mini Mart
QC Prep Batch Method:
Massachusetts VPH
MADEP-VPH
V28153QC Analytical Batch(es):
Analysis Method:
Analysis Description:
MAVPH (Prep)
QC Prep:V28152
Associated Lab Samples: 96170, 96171
LRB-V28152 Matrix: AQULab Reagent Blank
Parameter AnalyzedMQLMDLBlankResultUnits %Recovery % Rec Limits
12/21/22 13:3850.011.5<11.5µg/LAliphatic C5-C8
12/21/22 13:3850.025.8<25.8µg/LAliphatic C9-C12
12/21/22 13:3850.04.02<4.02µg/LAromatic C9-C10
12/21/22 13:382,5-Dibromotoluene (FID) (S)90.0 70-130
12/21/22 13:382,5-Dibromotoluene (PID) (S)89.6 70-130
LCS-V28152 LCSD-V28152Laboratory Control Sample & LCSD
LCSDResultParameter Max
RPD
LCSD% RecLCS%RecLCSResultSpikeConc.Units % RecLimits RPD
275 91.688.3265300µg/LAliphatic C5-C8 70-130 3.7 50.0
357 119114343300µg/LAliphatic C9-C12 70-130 4.0 50.0
110 110108108100µg/LAromatic C9-C10 70-130 1.8 50.0
93.988.02,5-Dibromotoluene (FID) (S)70-130
92.087.62,5-Dibromotoluene (PID) (S)70-130
Page 21 of 21Date:01/10/2023 12:16 PM
Page 97 of 100
Fed Ex
UPS
US Postal
Client
Lab
Courier
Other :
Shipment Receipt Form
Customer Number:
Customer Name:
Report Number:22-354-0019
Geological Resources, Inc.
00087
Shipping Method
Shipping container/cooler uncompromised?
Thermometer ID:IRT-15 0.6C
Chain of Custody (COC) present?Yes No
Yes No Not Present
Yes No Not Present
Yes No
COC agrees with sample label(s)? Yes No
COC properly completed
Samples in proper containers?
Sample containers intact?
Sufficient sample volume for indicated test(s)?
All samples received within holding time?
Cooler temperature in compliance?
Yes No
Yes No
Yes No
Yes No
Yes No
Yes NoCooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes No
Yes No N/A
Yes No N/A
Yes No N/ASoil VOA method 5035 – compliance criteria met
Water - Sample containers properly preserved
Water - VOA vials free of headspace Yes No N/A
Trip Blanks received with VOAs
Low concentration EnCore samplers (48 hr)
High concentration pre-weighed (methanol -14 d) Low conc pre-weighed vials (Sod Bis -14 d)
High concentration container (48 hr)
Custody seals intact on shipping container/cooler?
Custody seals intact on sample bottles?
Number of coolers/boxes received
Yes No
1
Sample dates and times were obtained from the sample labels. Samples MW-1,
MW-3 & MW-6 were not received.
Signature:Angelo Norvell Date & Time:12/20/2022 17:33:37
Special precautions or instructions included?
Comments:
Page 98 of 100
Page 99 of 100
Page 100 of 100

APPENDIX F
Free Product Recovery Graphs
29.00
30.00
31.00
32.00
33.00
0 500 1,000 1,500 2,000 2,500 3,000 3,500 4,000Recovery(feet)Time(seconds)
Product Water
APPENDIXF
FreeProductRecoveryEvaluationWellMW-1(Test1)
TrindaleMiniMart(IncidentNo.44719)
29.0
30.0
31.0
32.0
33.0
0 1,000 2,000 3,000 4,000 5,000Recovery(feet)Time(seconds)
Product Water
APPENDIXF
FreeProductRecoveryEvaluationWellMW-1(Test2)
TrindaleMiniMart(IncidentNo.44719)

APPENDIX G
Slug Test Data
0. 6. 12. 18. 24. 30.
0.1
1.
10.
Time (min)Displacement (ft)WELL TEST ANALYSIS
Data Set: F:\...\Revised_MW-8.aqt
Date: 09/17/21 Time: 07:47:11
PROJECT INFORMATION
Company: Geological Resources, Inc.
Client: Trindale Mini Mart
Project: 4236
Location: Trinity, NC
Test Well: MW-8
Test Date: 8/24/21
AQUIFER DATA
Saturated Thickness: 2.7 ft Anisotropy Ratio (Kz/Kr): 1.
WELL DATA (MW-8)
Initial Displacement: 1.75 ft Static Water Column Height: 10.26 ft
Total Well Penetration Depth: 10.26 ft Screen Length: 10.26 ft
Casing Radius: 0.085 ft Well Radius: 0.25 ft
Gravel Pack Porosity: 0.
SOLUTION
Aquifer Model: Unconfined Solution Method: Bouwer-Rice
K = 0.0001389 ft/min y0 = 0.4533 ft
Trindale Mini Mart
Well MW-8
Test Date 08/24/24
Initial DTW (ft) 24.82
Time Displacement
(min) (ft)
0.000 0.0000
0.017 4.5400
0.033 1.4750
0.050 1.1650
0.067 0.9790
0.083 0.8480
0.100 0.6970
0.117 0.6690
0.133 0.6210
0.150 0.5930
0.167 0.5730
0.183 0.5590
0.200 0.5450
0.217 0.5380
0.233 0.5240
0.250 0.5240
0.267 0.5170
0.283 0.5110
0.300 0.5040
0.317 0.5040
0.333 0.4970
0.350 0.4970
0.367 0.4900
0.383 0.4900
0.400 0.4900
0.417 0.4830
0.433 0.4830
0.450 0.4830
0.467 0.4760
0.483 0.4760
0.500 0.4830
0.517 0.4830
0.533 0.4690
0.550 0.4680
0.567 0.4680
0.583 0.4680
0.600 0.4680
0.617 0.4610
0.633 0.4610
0.650 0.4610
0.667 0.4610
0.683 0.4610
0.700 0.4540
0.717 0.4540
0.733 0.4540
0.750 0.4540
0.767 0.4540
0.783 0.4540
0.800 0.4480
0.817 0.4480
0.833 0.4480
0.850 0.4480
0.867 0.4480
0.883 0.4480
0.900 0.4480
0.917 0.4480
0.933 0.4490
0.950 0.4490
0.967 0.4420
0.983 0.4420
1.000 0.4420
1.017 0.4420
1.033 0.4420
1.050 0.4420
1.067 0.4420
1.083 0.4420
1.100 0.4350
1.117 0.4420
1.133 0.4350
1.150 0.4350
1.167 0.4350
1.183 0.4350
1.200 0.4350
1.217 0.4350
1.233 0.4350
1.250 0.4350
1.267 0.4350
1.283 0.4280
1.300 0.4280
1.317 0.4280
1.333 0.4280
1.350 0.4280
1.367 0.4280
1.383 0.4280
1.400 0.4280
1.417 0.4280
1.433 0.4280
1.450 0.4280
1.467 0.4280
1.483 0.4210
1.500 0.4210
1.517 0.4210
1.533 0.4210
1.550 0.4190
1.567 0.4190
1.583 0.4190
1.600 0.4190
1.617 0.4190
1.633 0.4190
1.650 0.4190
1.667 0.4190
1.683 0.4190
1.700 0.4190
1.717 0.4190
1.733 0.4190
1.750 0.4120
1.767 0.4120
1.783 0.4120
1.800 0.4120
1.817 0.4120
1.833 0.4120
1.850 0.4120
1.867 0.4120
1.883 0.4120
1.900 0.4120
1.917 0.4120
1.933 0.4120
1.950 0.4120
1.967 0.4050
1.983 0.4050
2.000 0.4120
2.017 0.4050
2.033 0.4050
2.050 0.4050
2.067 0.4050
2.083 0.4050
2.100 0.4050
2.117 0.4050
2.133 0.4050
2.150 0.4050
2.167 0.4050
2.183 0.4050
2.200 0.4050
2.217 0.4050
2.233 0.3980
2.250 0.3980
2.267 0.4050
2.283 0.4050
2.300 0.3980
2.317 0.3980
2.333 0.3980
2.350 0.3980
2.367 0.3980
2.383 0.3980
2.400 0.3980
2.417 0.3980
2.433 0.3980
2.450 0.3980
2.467 0.3980
2.483 0.3980
2.500 0.3980
2.517 0.3980
2.533 0.3990
2.550 0.3980
2.567 0.3910
2.583 0.3980
2.600 0.3980
2.617 0.3910
2.633 0.3910
2.650 0.3910
2.667 0.3910
2.683 0.3910
2.700 0.3910
2.717 0.3910
2.733 0.3910
2.750 0.3910
2.767 0.3910
2.783 0.3910
2.800 0.3850
2.817 0.3910
2.833 0.3910
2.850 0.3910
2.867 0.3850
2.883 0.3910
2.900 0.3910
2.917 0.3850
2.933 0.3850
2.950 0.3850
2.967 0.3910
2.983 0.3850
3.000 0.3850
3.017 0.3850
3.033 0.3850
3.050 0.3850
3.067 0.3850
3.083 0.3850
3.100 0.3850
3.117 0.3850
3.133 0.3850
3.150 0.3850
3.167 0.3850
3.183 0.3850
3.200 0.3780
3.217 0.3850
3.233 0.3850
3.250 0.3780
3.267 0.3780
3.283 0.3850
3.300 0.3850
3.317 0.3780
3.333 0.3780
3.350 0.3780
3.367 0.3780
3.383 0.3780
3.400 0.3780
3.417 0.3780
3.433 0.3780
3.450 0.3780
3.467 0.3780
3.483 0.3780
3.500 0.3780
3.517 0.3780
3.533 0.3710
3.550 0.3780
3.567 0.3780
3.583 0.3780
3.600 0.3780
3.617 0.3780
3.633 0.3780
3.650 0.3710
3.667 0.3710
3.683 0.3710
3.700 0.3710
3.717 0.3710
3.733 0.3710
3.750 0.3710
3.767 0.3710
3.783 0.3710
3.800 0.3710
3.817 0.3710
3.833 0.3720
3.850 0.3720
3.867 0.3720
3.883 0.3720
3.900 0.3720
3.917 0.3720
3.933 0.3720
3.950 0.3720
3.967 0.3720
3.983 0.3720
4.000 0.3720
4.017 0.3720
4.033 0.3720
4.050 0.3650
4.067 0.3720
4.083 0.3650
4.100 0.3650
4.117 0.3650
4.133 0.3650
4.150 0.3650
4.167 0.3650
4.183 0.3650
4.200 0.3650
4.217 0.3650
4.233 0.3650
4.250 0.3650
4.267 0.3650
4.283 0.3650
4.300 0.3650
4.317 0.3650
4.333 0.3650
4.350 0.3650
4.367 0.3650
4.383 0.3580
4.400 0.3650
4.417 0.3650
4.433 0.3580
4.450 0.3580
4.467 0.3660
4.483 0.3590
4.500 0.3590
4.517 0.3590
4.533 0.3590
4.550 0.3550
4.567 0.3550
4.583 0.3550
4.600 0.3550
4.617 0.3550
4.633 0.3550
4.650 0.3550
4.667 0.3550
4.683 0.3550
4.700 0.3550
4.717 0.3550
4.733 0.3550
4.750 0.3550
4.767 0.3550
4.783 0.3550
4.800 0.3550
4.817 0.3550
4.833 0.3550
4.850 0.3550
4.867 0.3550
4.883 0.3550
4.900 0.3480
4.917 0.3550
4.933 0.3550
4.950 0.3480
4.967 0.3480
4.983 0.3480
5.000 0.3480
5.017 0.3480
5.033 0.3480
5.050 0.3480
5.067 0.3480
5.083 0.3480
5.100 0.3480
5.117 0.3480
5.133 0.3480
5.150 0.3480
5.167 0.3480
5.183 0.3480
5.200 0.3480
5.217 0.3480
5.233 0.3480
5.250 0.3480
5.267 0.3480
5.283 0.3480
5.300 0.3480
5.317 0.3480
5.333 0.3410
5.350 0.3480
5.367 0.3410
5.383 0.3410
5.400 0.3410
5.417 0.3410
5.433 0.3410
5.450 0.3410
5.467 0.3410
5.483 0.3410
5.500 0.3410
5.517 0.3410
5.533 0.3410
5.550 0.3410
5.567 0.3410
5.583 0.3410
5.600 0.3410
5.617 0.3410
5.633 0.3410
5.650 0.3410
5.667 0.3410
5.683 0.3410
5.700 0.3410
5.717 0.3410
5.733 0.3410
5.750 0.3410
5.767 0.3410
5.783 0.3410
5.800 0.3410
5.817 0.3410
5.833 0.3410
5.850 0.3340
5.867 0.3340
5.883 0.3340
5.900 0.3340
5.917 0.3340
5.933 0.3340
5.950 0.3340
5.967 0.3340
5.983 0.3340
6.000 0.3340
6.017 0.3340
6.033 0.3340
6.050 0.3340
6.067 0.3340
6.083 0.3340
6.100 0.3340
6.117 0.3340
6.133 0.3340
6.150 0.3340
6.167 0.3340
6.183 0.3340
6.200 0.3270
6.217 0.3340
6.233 0.3340
6.250 0.3270
6.267 0.3270
6.283 0.3340
6.300 0.3340
6.317 0.3270
6.333 0.3270
6.350 0.3340
6.367 0.3260
6.383 0.3260
6.400 0.3260
6.417 0.3260
6.433 0.3260
6.450 0.3260
6.467 0.3260
6.483 0.3330
6.500 0.3260
6.517 0.3260
6.533 0.3260
6.550 0.3290
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6.683 0.3290
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6.783 0.3290
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6.833 0.3290
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6.900 0.3230
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6.967 0.3230
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7.000 0.3230
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7.283 0.3230
7.300 0.3230
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7.333 0.3230
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7.650 0.3150
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7.717 0.3150
7.733 0.3150
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7.867 0.3150
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7.900 0.3150
7.917 0.3150
7.933 0.3150
7.950 0.3150
7.967 0.3080
7.983 0.3160
8.000 0.3160
8.017 0.3090
8.033 0.3160
8.050 0.3160
8.067 0.3090
8.083 0.3160
8.100 0.3160
8.117 0.3160
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8.167 0.3160
8.183 0.3090
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8.250 0.3090
8.267 0.3090
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8.317 0.3090
8.333 0.3090
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8.483 0.3090
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8.533 0.3090
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8.567 0.3070
8.583 0.3070
8.600 0.3070
8.617 0.3070
8.633 0.3070
8.650 0.3070
8.667 0.3070
8.683 0.3000
8.700 0.3070
8.717 0.3070
8.733 0.3070
8.750 0.3070
8.767 0.3000
8.783 0.3000
8.800 0.3000
8.817 0.3000
8.833 0.3000
8.850 0.3000
8.867 0.3000
8.883 0.3000
8.900 0.3000
8.917 0.3000
8.933 0.3000
8.950 0.3000
8.967 0.3000
8.983 0.3000
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9.017 0.3000
9.033 0.3000
9.050 0.3000
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9.083 0.3000
9.100 0.3000
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9.133 0.3000
9.150 0.3000
9.167 0.3000
9.183 0.3000
9.200 0.3000
9.217 0.3000
9.233 0.3000
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9.267 0.3000
9.283 0.3000
9.300 0.3000
9.317 0.3000
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9.350 0.3000
9.367 0.3000
9.383 0.3000
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9.417 0.3000
9.433 0.3000
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9.467 0.2930
9.483 0.3000
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9.517 0.2930
9.533 0.2930
9.550 0.2920
9.567 0.2920
9.583 0.2920
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9.733 0.2920
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9.883 0.2920
9.900 0.2920
9.917 0.2920
9.933 0.2920
9.950 0.2850
9.967 0.2920
9.983 0.2920
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10.017 0.2920
10.033 0.2850
10.050 0.2920
10.067 0.2920
10.083 0.2850
10.100 0.2850
10.117 0.2850
10.133 0.2850
10.150 0.2850
10.167 0.2850
10.183 0.2850
10.200 0.2850
10.217 0.2850
10.233 0.2850
10.250 0.2850
10.267 0.2850
10.283 0.2850
10.300 0.2850
10.317 0.2850
10.333 0.2850
10.350 0.2850
10.367 0.2850
10.383 0.2850
10.400 0.2850
10.417 0.2850
10.433 0.2850
10.450 0.2850
10.467 0.2850
10.483 0.2850
10.500 0.2850
10.517 0.2850
10.533 0.2850
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10.567 0.2860
10.583 0.2860
10.600 0.2860
10.617 0.2860
10.633 0.2860
10.650 0.2860
10.667 0.2790
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10.700 0.2860
10.717 0.2860
10.733 0.2860
10.750 0.2790
10.767 0.2790
10.783 0.2860
10.800 0.2860
10.817 0.2790
10.833 0.2860
10.850 0.2790
10.867 0.2790
10.883 0.2790
10.900 0.2790
10.917 0.2790
10.933 0.2790
10.950 0.2790
10.967 0.2790
10.983 0.2790
11.000 0.2790
11.017 0.2790
11.033 0.2790
11.050 0.2790
11.067 0.2790
11.083 0.2790
11.100 0.2790
11.117 0.2790
11.133 0.2790
11.150 0.2790
11.167 0.2800
11.183 0.2800
11.200 0.2800
11.217 0.2800
11.233 0.2800
11.250 0.2800
11.267 0.2730
11.283 0.2800
11.300 0.2800
11.317 0.2800
11.333 0.2800
11.350 0.2800
11.367 0.2800
11.383 0.2800
11.400 0.2800
11.417 0.2800
11.433 0.2730
11.450 0.2730
11.467 0.2730
11.483 0.2730
11.500 0.2730
11.517 0.2800
11.533 0.2730
11.550 0.2700
11.567 0.2700
11.583 0.2700
11.600 0.2700
11.617 0.2700
11.633 0.2700
11.650 0.2700
11.667 0.2700
11.683 0.2700
11.700 0.2700
11.717 0.2700
11.733 0.2700
11.750 0.2700
11.767 0.2700
11.783 0.2700
11.800 0.2700
11.817 0.2700
11.833 0.2700
11.850 0.2700
11.867 0.2700
11.883 0.2700
11.900 0.2700
11.917 0.2700
11.933 0.2700
11.950 0.2700
11.967 0.2700
11.983 0.2700
12.000 0.2700
12.017 0.2700
12.033 0.2700
12.050 0.2700
12.067 0.2700
12.083 0.2700
12.100 0.2700
12.117 0.2700
12.133 0.2620
12.150 0.2690
12.167 0.2620
12.183 0.2620
12.200 0.2620
12.217 0.2620
12.233 0.2620
12.250 0.2620
12.267 0.2620
12.283 0.2620
12.300 0.2620
12.317 0.2620
12.333 0.2620
12.350 0.2620
12.367 0.2620
12.383 0.2620
12.400 0.2620
12.417 0.2620
12.433 0.2620
12.450 0.2620
12.467 0.2620
12.483 0.2620
12.500 0.2620
12.517 0.2620
12.533 0.2620
12.550 0.2640
12.567 0.2640
12.583 0.2640
12.600 0.2640
12.617 0.2630
12.633 0.2630
12.650 0.2630
12.667 0.2570
12.683 0.2570
12.700 0.2630
12.717 0.2630
12.733 0.2630
12.750 0.2630
12.767 0.2630
12.783 0.2570
12.800 0.2570
12.817 0.2570
12.833 0.2570
12.850 0.2570
12.867 0.2570
12.883 0.2570
12.900 0.2570
12.917 0.2570
12.933 0.2570
12.950 0.2570
12.967 0.2630
12.983 0.2570
13.000 0.2570
13.017 0.2570
13.033 0.2570
13.050 0.2570
13.067 0.2570
13.083 0.2570
13.100 0.2570
13.117 0.2570
13.133 0.2570
13.150 0.2560
13.167 0.2560
13.183 0.2560
13.200 0.2560
13.217 0.2560
13.233 0.2560
13.250 0.2560
13.267 0.2560
13.283 0.2560
13.300 0.2560
13.317 0.2560
13.333 0.2560
13.350 0.2560
13.367 0.2560
13.383 0.2490
13.400 0.2560
13.417 0.2560
13.433 0.2560
13.450 0.2560
13.467 0.2560
13.483 0.2490
13.500 0.2560
13.517 0.2560
13.533 0.2560
13.550 0.2520
13.567 0.2590
13.583 0.2520
13.600 0.2520
13.617 0.2530
13.633 0.2530
13.650 0.2530
13.667 0.2530
13.683 0.2530
13.700 0.2530
13.717 0.2530
13.733 0.2530
13.750 0.2530
13.767 0.2530
13.783 0.2530
13.800 0.2530
13.817 0.2530
13.833 0.2530
13.850 0.2530
13.867 0.2530
13.883 0.2530
13.900 0.2530
13.917 0.2530
13.933 0.2530
13.950 0.2530
13.967 0.2530
13.983 0.2530
14.000 0.2530
14.017 0.2530
14.033 0.2530
14.050 0.2530
14.067 0.2530
14.083 0.2530
14.100 0.2530
14.117 0.2530
14.133 0.2530
14.150 0.2530
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14.183 0.2530
14.200 0.2460
14.217 0.2530
14.233 0.2460
14.250 0.2530
14.267 0.2530
14.283 0.2530
14.300 0.2460
14.317 0.2460
14.333 0.2460
14.350 0.2460
14.367 0.2460
14.383 0.2460
14.400 0.2460
14.417 0.2460
14.433 0.2460
14.450 0.2460
14.467 0.2460
14.483 0.2460
14.500 0.2460
14.517 0.2460
14.533 0.2460
14.550 0.2450
14.567 0.2450
14.583 0.2450
14.600 0.2450
14.617 0.2450
14.633 0.2450
14.650 0.2450
14.667 0.2450
14.683 0.2450
14.700 0.2450
14.717 0.2450
14.733 0.2450
14.750 0.2450
14.767 0.2450
14.783 0.2450
14.800 0.2450
14.817 0.2450
14.833 0.2450
14.850 0.2450
14.867 0.2450
14.883 0.2450
14.900 0.2450
14.917 0.2450
14.933 0.2380
14.950 0.2450
14.967 0.2450
14.983 0.2380
15.000 0.2450
15.017 0.2450
15.033 0.2450
15.050 0.2380
15.067 0.2380
15.083 0.2380
15.100 0.2380
15.117 0.2450
15.133 0.2450
15.150 0.2380
15.167 0.2380
15.183 0.2380
15.200 0.2380
15.217 0.2380
15.233 0.2380
15.250 0.2380
15.267 0.2380
15.283 0.2380
15.300 0.2380
15.317 0.2380
15.333 0.2380
15.350 0.2380
15.367 0.2380
15.383 0.2380
15.400 0.2380
15.417 0.2380
15.433 0.2380
15.450 0.2380
15.467 0.2380
15.483 0.2380
15.500 0.2380
15.517 0.2380
15.533 0.2380
15.550 0.2370
15.567 0.2370
15.583 0.2370
15.600 0.2370
15.617 0.2370
15.633 0.2370
15.650 0.2370
15.667 0.2370
15.683 0.2380
15.700 0.2380
15.717 0.2380
15.733 0.2380
15.750 0.2380
15.767 0.2380
15.783 0.2380
15.800 0.2380
15.817 0.2310
15.833 0.2380
15.850 0.2380
15.867 0.2310
15.883 0.2310
15.900 0.2310
15.917 0.2310
15.933 0.2310
15.950 0.2380
15.967 0.2380
15.983 0.2380
16.000 0.2310
16.017 0.2310
16.033 0.2310
16.050 0.2310
16.067 0.2310
16.083 0.2310
16.100 0.2310
16.117 0.2310
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16.150 0.2310
16.167 0.2310
16.183 0.2310
16.200 0.2310
16.217 0.2310
16.233 0.2310
16.250 0.2310
16.267 0.2310
16.283 0.2310
16.300 0.2320
16.317 0.2320
16.333 0.2320
16.350 0.2320
16.367 0.2320
16.383 0.2320
16.400 0.2320
16.417 0.2320
16.433 0.2320
16.450 0.2320
16.467 0.2320
16.483 0.2320
16.500 0.2320
16.517 0.2320
16.533 0.2320
16.550 0.2290
16.567 0.2290
16.583 0.2290
16.600 0.2290
16.617 0.2290
16.633 0.2290
16.650 0.2290
16.667 0.2290
16.683 0.2220
16.700 0.2290
16.717 0.2290
16.733 0.2220
16.750 0.2220
16.767 0.2290
16.783 0.2220
16.800 0.2210
16.817 0.2280
16.833 0.2210
16.850 0.2210
16.867 0.2210
16.883 0.2210
16.900 0.2210
16.917 0.2210
16.933 0.2210
16.950 0.2210
16.967 0.2210
16.983 0.2210
17.000 0.2210
17.017 0.2210
17.033 0.2210
17.050 0.2210
17.067 0.2210
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17.100 0.2210
17.117 0.2210
17.133 0.2210
17.150 0.2210
17.167 0.2210
17.183 0.2210
17.200 0.2210
17.217 0.2210
17.233 0.2210
17.250 0.2210
17.267 0.2210
17.283 0.2210
17.300 0.2210
17.317 0.2210
17.333 0.2210
17.350 0.2210
17.367 0.2210
17.383 0.2210
17.400 0.2210
17.417 0.2210
17.433 0.2210
17.450 0.2210
17.467 0.2210
17.483 0.2210
17.500 0.2210
17.517 0.2210
17.533 0.2140
17.550 0.2220
17.567 0.2150
17.583 0.2220
17.600 0.2150
17.617 0.2220
17.633 0.2150
17.650 0.2220
17.667 0.2150
17.683 0.2150
17.700 0.2150
17.717 0.2150
17.733 0.2150
17.750 0.2150
17.767 0.2150
17.783 0.2150
17.800 0.2150
17.817 0.2150
17.833 0.2220
17.850 0.2150
17.867 0.2150
17.883 0.2150
17.900 0.2150
17.917 0.2150
17.933 0.2150
17.950 0.2150
17.967 0.2150
17.983 0.2150
18.000 0.2150
18.017 0.2150
18.033 0.2150
18.050 0.2150
18.067 0.2150
18.083 0.2150
18.100 0.2150
18.117 0.2150
18.133 0.2150
18.150 0.2150
18.167 0.2150
18.183 0.2150
18.200 0.2150
18.217 0.2150
18.233 0.2150
18.250 0.2150
18.267 0.2150
18.283 0.2150
18.300 0.2150
18.317 0.2150
18.333 0.2150
18.350 0.2150
18.367 0.2150
18.383 0.2150
18.400 0.2150
18.417 0.2080
18.433 0.2150
18.450 0.2080
18.467 0.2150
18.483 0.2080
18.500 0.2080
18.517 0.2080
18.533 0.2150
18.550 0.2090
18.567 0.2090
18.583 0.2160
18.600 0.2090
18.617 0.2160
18.633 0.2160
18.650 0.2090
18.667 0.2090
18.683 0.2090
18.700 0.2090
18.717 0.2090
18.733 0.2090
18.750 0.2090
18.767 0.2090
18.783 0.2090
18.800 0.2090
18.817 0.2090
18.833 0.2090
18.850 0.2090
18.867 0.2090
18.883 0.2090
18.900 0.2090
18.917 0.2090
18.933 0.2090
18.950 0.2090
18.967 0.2090
18.983 0.2090
19.000 0.2090
19.017 0.2090
19.033 0.2090
19.050 0.2090
19.067 0.2090
19.083 0.2090
19.100 0.2090
19.117 0.2090
19.133 0.2090
19.150 0.2090
19.167 0.2090
19.183 0.2090
19.200 0.2090
19.217 0.2090
19.233 0.2090
19.250 0.2090
19.267 0.2090
19.283 0.2100
19.300 0.2100
19.317 0.2100
19.333 0.2100
19.350 0.2100
19.367 0.2100
19.383 0.2100
19.400 0.2100
19.417 0.2100
19.433 0.2100
19.450 0.2100
19.467 0.2100
19.483 0.2100
19.500 0.2030
19.517 0.2100
19.533 0.2100
19.550 0.2080
19.567 0.2080
19.583 0.2080
19.600 0.2080
19.617 0.2080
19.633 0.2010
19.650 0.2010
19.667 0.2010
19.683 0.2010
19.700 0.2080
19.717 0.2080
19.733 0.2010
19.750 0.2010
19.767 0.2010
19.783 0.2010
19.800 0.2010
19.817 0.2080
19.833 0.2010
19.850 0.2010
19.867 0.2010
19.883 0.2010
19.900 0.2010
19.917 0.2010
19.933 0.2010
19.950 0.2010
19.967 0.2010
19.983 0.2010
20.000 0.2010
20.017 0.2010
20.033 0.2010
20.050 0.2010
20.067 0.2010
20.083 0.2010
20.100 0.2010
20.117 0.2010
20.133 0.2010
20.150 0.2010
20.167 0.2010
20.183 0.2010
20.200 0.2010
20.217 0.2010
20.233 0.2010
20.250 0.2010
20.267 0.2010
20.283 0.2010
20.300 0.2010
20.317 0.2010
20.333 0.2010
20.350 0.2010
20.367 0.2010
20.383 0.2010
20.400 0.2010
20.417 0.2010
20.433 0.2010
20.450 0.2010
20.467 0.2010
20.483 0.2010
20.500 0.2010
20.517 0.1940
20.533 0.2010
20.550 0.2010
20.567 0.2010
20.583 0.2010
20.600 0.2010
20.617 0.2010
20.633 0.2010
20.650 0.1940
20.667 0.2010
20.683 0.2010
20.700 0.2010
20.717 0.2010
20.733 0.1940
20.750 0.1940
20.767 0.2010
20.783 0.1940
20.800 0.1940
20.817 0.2010
20.833 0.2010
20.850 0.1940
20.867 0.2010
20.883 0.1940
20.900 0.1940
20.917 0.2010
20.933 0.1940
20.950 0.2010
20.967 0.1940
20.983 0.1940
21.000 0.1940
21.017 0.1940
21.033 0.1940
21.050 0.1940
21.067 0.1940
21.083 0.1940
21.100 0.1940
21.117 0.1940
21.133 0.1940
21.150 0.1940
21.167 0.1940
21.183 0.1940
21.200 0.1940
21.217 0.1940
21.233 0.1940
21.250 0.1940
21.267 0.1940
21.283 0.1940
21.300 0.1880
21.317 0.1940
21.333 0.1940
21.350 0.1880
21.367 0.1940
21.383 0.1940
0. 0.8 1.6 2.4 3.2 4.
0.01
0.1
1.
10.
Time (min)Displacement (ft)WELL TEST ANALYSIS
Data Set: F:\...\Revised_MW-9.aqt
Date: 09/17/21 Time: 07:50:58
PROJECT INFORMATION
Company: Geological Resources, Inc.
Client: Trindale Mini Mart
Project: 4236
Location: Trinity, NC
Test Well: MW-9
Test Date: 8/24/21
AQUIFER DATA
Saturated Thickness: 2.7 ft Anisotropy Ratio (Kz/Kr): 1.
WELL DATA (MW-9)
Initial Displacement: 1.75 ft Static Water Column Height: 8.84 ft
Total Well Penetration Depth: 8.84 ft Screen Length: 8.84 ft
Casing Radius: 0.085 ft Well Radius: 0.25 ft
Gravel Pack Porosity: 0.
SOLUTION
Aquifer Model: Unconfined Solution Method: Bouwer-Rice
K = 0.002759 ft/min y0 = 0.2624 ft
Trindale Mini Mart
Well MW-9
Test Date 08/24/21
Initial DTW (ft) 23.78
Time Displacement
(min) (ft)
0.000 0.000
0.017 1.336
0.033 1.419
0.050 1.095
0.067 0.868
0.083 0.696
0.100 0.572
0.117 0.482
0.133 0.420
0.150 0.386
0.167 0.358
0.183 0.331
0.200 0.310
0.217 0.296
0.233 0.282
0.250 0.275
0.267 0.262
0.283 0.255
0.300 0.248
0.317 0.241
0.333 0.234
0.350 0.227
0.367 0.220
0.383 0.213
0.400 0.207
0.417 0.207
0.433 0.200
0.450 0.193
0.467 0.193
0.483 0.186
0.500 0.179
0.517 0.172
0.533 0.172
0.550 0.172
0.567 0.165
0.583 0.158
0.600 0.158
0.617 0.158
0.633 0.158
0.650 0.145
0.667 0.145
0.683 0.138
0.700 0.138
0.717 0.138
0.733 0.138
0.750 0.145
0.767 0.138
0.783 0.131
0.800 0.124
0.817 0.124
0.833 0.124
0.850 0.117
0.867 0.117
0.883 0.117
0.900 0.117
0.917 0.109
0.933 0.110
0.950 0.110
0.967 0.103
0.983 0.103
1.000 0.103
1.017 0.103
1.033 0.096
1.050 0.096
1.067 0.096
1.083 0.096
1.100 0.096
1.117 0.089
1.133 0.089
1.150 0.089
1.167 0.089
1.183 0.089
1.200 0.083
1.217 0.083
1.233 0.083
1.250 0.083
1.267 0.083
1.283 0.076
1.300 0.076
1.317 0.076
1.333 0.076
1.350 0.076
1.367 0.076
1.383 0.076
1.400 0.076
1.417 0.070
1.433 0.070
1.450 0.070
1.467 0.070
1.483 0.070
1.500 0.070
1.517 0.070
1.533 0.070
1.550 0.063
1.567 0.063
1.583 0.063
1.600 0.063
1.617 0.063
1.633 0.063
1.650 0.063
1.667 0.063
1.683 0.056
1.700 0.056
1.717 0.056
1.733 0.056
1.750 0.056
1.767 0.056
1.783 0.056
1.800 0.056
1.817 0.056
1.833 0.049
1.850 0.056
1.867 0.049
1.883 0.049
1.900 0.050
1.917 0.045
1.933 0.045
1.950 0.045
1.967 0.045
1.983 0.045
2.000 0.045
2.017 0.045
2.033 0.045
2.050 0.045
2.067 0.045
2.083 0.045
2.100 0.045
2.117 0.038
2.133 0.038
2.150 0.038
2.167 0.038
2.183 0.038
2.200 0.038
2.217 0.038
2.233 0.038
2.250 0.038
2.267 0.038
2.283 0.038
2.300 0.038
2.317 0.031
2.333 0.031
2.350 0.031
2.367 0.031
2.383 0.031
2.400 0.031
2.417 0.031
2.433 0.031
2.450 0.031
2.467 0.031
2.483 0.031
2.500 0.031
2.517 0.031
2.533 0.031
2.550 0.031
2.567 0.031
2.583 0.031
2.600 0.031
2.617 0.031
2.633 0.031
2.650 0.031
2.667 0.031
2.683 0.024
2.700 0.031
2.717 0.031
2.733 0.024
2.750 0.031
2.767 0.024
2.783 0.024
2.800 0.031
2.817 0.024
2.833 0.024
2.850 0.024
2.867 0.024
2.883 0.024
2.900 0.024
2.917 0.025
2.933 0.025
2.950 0.025
2.967 0.025
2.983 0.025
3.000 0.025
3.017 0.025
3.033 0.025
3.050 0.025
3.067 0.025
3.083 0.025
3.100 0.025
3.117 0.025
3.133 0.025
3.150 0.025
3.167 0.025
3.183 0.025
3.200 0.019
3.217 0.025
3.233 0.025
3.250 0.019
3.267 0.025
3.283 0.019
3.300 0.019
3.317 0.019
3.333 0.019
3.350 0.019
3.367 0.019
3.383 0.019
3.400 0.019
3.417 0.019
3.433 0.019
3.450 0.019
3.467 0.019
3.483 0.019
3.500 0.019
3.517 0.019
3.533 0.019
3.550 0.019
3.567 0.019
3.583 0.018
3.600 0.018
3.617 0.018
3.633 0.018
3.650 0.018
3.667 0.018
3.683 0.018
3.700 0.018
3.717 0.018
3.733 0.018
3.750 0.018
3.767 0.018
3.783 0.018
3.800 0.018
3.817 0.018
3.833 0.018
3.850 0.018
3.867 0.018
3.883 0.018
3.900 0.018
3.917 0.019
3.933 0.019
3.950 0.019
3.967 0.019
3.983 0.019
4.000 0.019
4.017 0.019
4.033 0.019
4.050 0.019
4.067 0.012
4.083 0.012
4.100 0.012
4.117 0.019
4.133 0.019
4.150 0.012
4.167 0.012
4.183 0.012
4.200 0.012
4.217 0.019
4.233 0.012
4.250 0.012
4.267 0.012
4.283 0.012
4.300 0.012
4.317 0.012
4.333 0.019
4.350 0.012
4.367 0.012
4.383 0.012
4.400 0.012
4.417 0.012
4.433 0.012
4.450 0.012
4.467 0.012
4.483 0.012
4.500 0.012
4.517 0.012
4.533 0.012
4.550 0.012
4.567 0.012
4.583 0.012
4.600 0.012
4.617 0.012
4.633 0.012
4.650 0.012
4.667 0.012
4.683 0.012
4.700 0.012
4.717 0.012
4.733 0.012
4.750 0.012
4.767 0.012
4.783 0.012
4.800 0.012
4.817 0.012
4.833 0.012
4.850 0.012
4.867 0.012
4.883 0.012
4.900 0.012
4.917 0.012
4.933 0.012
4.950 0.012
4.967 0.012
4.983 0.012
5.000 0.012
5.017 0.012
5.033 0.012
5.050 0.012
5.067 0.012
5.083 0.012
5.100 0.012
5.117 0.012
5.133 0.012
5.150 0.012
5.167 0.012
5.183 0.012
5.200 0.012
5.217 0.012
5.233 0.012
5.250 0.012
5.267 0.012
5.283 0.012
5.300 0.012
5.317 0.012
5.333 0.012
5.350 0.012
5.367 0.012
5.383 0.012
5.400 0.012
5.417 0.012
5.433 0.005
5.450 0.012
5.467 0.012
5.483 0.005
5.500 0.012
5.517 0.012
5.533 0.012
5.550 0.012
5.567 0.012
5.583 0.005
5.600 0.012
5.617 0.012
5.633 0.012
5.650 0.012
5.667 0.005
5.683 0.005
5.700 0.012
5.717 0.012
5.733 0.012
5.750 0.005
5.767 0.005
5.783 0.012
5.800 0.012
5.817 0.012
5.833 0.005
5.850 0.006
5.867 0.006
5.883 0.006
5.900 0.013
5.917 0.004
5.933 0.004
5.950 0.004
5.967 0.004
5.983 0.004
6.000 0.004
6.017 0.004
6.033 0.004
6.050 0.004
6.067 0.004
6.083 0.004
6.100 0.004
6.117 0.004
6.133 0.004
6.150 0.004
6.167 0.004
6.183 0.004
6.200 0.004
6.217 0.004
6.233 0.004
6.250 0.004
6.267 0.004
6.283 0.004
6.300 0.004
6.317 0.004
6.333 0.004
6.350 0.004
6.367 0.004
6.383 0.004
6.400 0.004
6.417 0.004
6.433 0.004
6.450 0.004
6.467 0.004
6.483 0.004
6.500 0.004
6.517 0.004
6.533 0.004
6.550 0.004
6.567 0.004
6.583 0.004
6.600 0.004
6.617 0.004
6.633 0.004
6.650 0.004
6.667 0.004
6.683 0.004
6.700 0.004
6.717 0.004
6.733 0.004
6.750 0.004
6.767 0.004
6.783 0.004
6.800 0.004
6.817 0.004
6.833 0.004
6.850 0.004
6.867 0.004
6.883 0.004
6.900 0.004
6.917 0.004
6.933 0.004
6.950 0.004
6.967 0.004
6.983 0.004
7.000 0.004
7.017 0.004
7.033 0.004
7.050 0.004
7.067 0.004
7.083 0.004
7.100 0.004
7.117 0.004
7.133 0.004
7.150 0.004
7.167 0.004
7.183 0.004
7.200 0.004
7.217 0.004
7.233 0.004
7.250 0.004
7.267 0.004
7.283 0.004
7.300 0.004
7.317 0.004
7.333 0.004
7.350 0.004
7.367 0.004
7.383 0.004
7.400 0.004
7.417 0.004
7.433 0.004
7.450 0.004
7.467 0.004
7.483 0.004
7.500 0.004
7.517 0.004
7.533 0.004
7.550 0.004
7.567 0.004
7.583 0.004
7.600 0.004
7.617 0.004
7.633 0.004
7.650 0.004
7.667 0.004
7.683 0.004
7.700 0.004
7.717 0.004
7.733 0.004
7.750 0.004
7.767 0.004
7.783 0.004
7.800 0.004
7.817 0.004
7.833 0.004
7.850 0.004
7.867 0.004
7.883 0.004
7.900 0.004
7.917 0.004
7.933 0.004
7.950 0.004
7.967 0.004
7.983 0.004
8.000 0.004
8.017 0.004
8.033 0.004
8.050 0.004
8.067 0.004
8.083 0.004
8.100 0.004
8.117 0.004
8.133 0.004
8.150 0.004
8.167 0.004
8.183 0.004
8.200 0.004
8.217 0.004
8.233 -0.003
8.250 0.004
8.267 0.004
8.283 0.004
8.300 0.004
8.317 0.004
8.333 0.004
8.350 0.004
8.367 0.004
8.383 0.004
8.400 0.004
8.417 0.004
8.433 0.004
8.450 0.004
8.467 0.004
8.483 0.004
8.500 0.004
8.517 0.004
8.533 0.004
8.550 0.004
8.567 0.004
8.583 0.004
8.600 0.004
8.617 0.004
8.633 0.004
8.650 0.004
8.667 0.004
8.683 0.004
8.700 0.004
8.717 0.004
8.733 0.004
8.750 0.005
8.767 0.005
8.783 0.005
8.800 0.005
8.817 0.005
8.833 0.005
8.850 0.005
8.867 0.005
8.883 0.005
8.900 0.005
8.917 0.003
8.933 0.003
8.950 0.003
8.967 0.003
8.983 0.003
9.000 0.003
9.017 0.003
9.033 0.003
9.050 0.003
9.067 0.003
9.083 0.003
9.100 0.003
9.117 0.003
9.133 0.003
9.150 0.003
9.167 0.003
9.183 0.003
9.200 0.003
9.217 0.003
9.233 0.003
9.250 0.003
9.267 0.003
9.283 0.003
9.300 0.003
9.317 0.003
9.333 0.003
9.350 0.003
9.367 0.003
9.383 0.003
9.400 0.003
9.417 0.003
9.433 0.003
9.450 0.003
9.467 0.003
9.483 0.003
9.500 0.003
9.517 0.003
9.533 0.003
9.550 0.003
9.567 0.003
9.583 0.003
9.600 0.003
9.617 0.003
9.633 0.003
9.650 0.003
9.667 0.003
9.683 0.003
9.700 0.003
9.717 0.003
9.733 0.003
9.750 0.003
9.767 0.003
9.783 0.003
9.800 0.003
9.817 0.003
9.833 0.003
9.850 0.003
9.867 0.003
9.883 0.003
9.900 0.003
9.917 0.003
9.933 0.003
9.950 0.003
9.967 0.003
9.983 0.003
10.000 0.003
10.017 0.003
10.033 0.003
10.050 0.003
10.067 0.003
10.083 0.003
10.100 0.003
10.117 0.003
10.133 0.003
10.150 0.003
10.167 0.003
10.183 0.003
10.200 0.003
10.217 0.003
10.233 0.003
10.250 0.003
10.267 0.003
10.283 0.003
10.300 0.003
10.317 0.003
10.333 0.003
10.350 0.003
10.367 0.003
10.383 0.003
10.400 0.003
10.417 0.003
10.433 0.003
10.450 0.003
10.467 0.003
10.483 0.003
10.500 0.003
10.517 0.003
10.533 0.003
10.550 0.003
10.567 0.003
10.583 0.003
10.600 0.003
10.617 0.003
10.633 0.003
10.650 0.003
10.667 0.003
10.683 0.003
10.700 0.003
10.717 0.003
10.733 0.003
10.750 0.003
10.767 0.003
10.783 0.003
10.800 0.003
10.817 0.003
10.833 0.003
10.850 0.003
10.867 0.003
10.883 0.003
10.900 0.003
10.917 0.002
10.933 0.002
10.950 0.002
10.967 0.002
10.983 0.002
11.000 0.002
11.017 0.002
11.033 0.002
11.050 0.002
11.067 0.002
11.083 0.002
11.100 0.002
11.117 0.002
11.133 0.002
11.150 0.002
11.167 0.002
11.183 0.002
11.200 0.002
11.217 0.002
11.233 0.002
11.250 0.002
11.267 0.002
11.283 0.002
11.300 0.002
11.317 0.002
11.333 0.002
11.350 0.002
11.367 0.002
11.383 0.002
11.400 0.002
11.417 0.002
11.433 0.002
11.450 0.002
11.467 0.002
11.483 0.002
11.500 0.002
11.517 0.002
11.533 0.002
11.550 0.002
11.567 0.002
11.583 0.002
11.600 0.002
11.617 0.002
11.633 0.002
11.650 0.002
11.667 0.002
11.683 0.002
11.700 0.002
11.717 0.002
11.733 0.002
11.750 0.002
11.767 0.003
11.783 0.003
11.800 0.003
11.817 0.003
11.833 0.003
11.850 0.003
11.867 0.003
11.883 0.003
11.900 0.003
11.917 0.002
11.933 0.002
11.950 0.002
11.967 0.002
11.983 0.002
12.000 0.002
12.017 0.002
12.033 0.002
12.050 0.002
12.067 0.002
12.083 0.002
12.100 0.002
12.117 0.002
12.133 0.002
12.150 0.002
12.167 0.002
12.183 0.002
12.200 0.002
12.217 0.002
12.233 0.002
12.250 0.002
12.267 0.002
12.283 0.002
12.300 0.002
12.317 0.002
12.333 0.002
12.350 0.002
12.367 0.002
12.383 0.002
12.400 0.002
12.417 0.002
12.433 0.002
12.450 0.002
12.467 0.002
12.483 0.002
12.500 0.002
12.517 0.002
12.533 0.002
12.550 0.002
12.567 0.002
12.583 0.002
12.600 0.002
12.617 0.002
12.633 0.002
12.650 0.002
12.667 0.002
12.683 0.002
12.700 0.002
12.717 0.002
12.733 0.002
12.750 0.002
12.767 0.002
12.783 0.002
12.800 0.002
12.817 0.002
12.833 0.002
12.850 0.002
12.867 0.002
12.883 0.002
12.900 0.002
12.917 0.001
12.933 0.001
12.950 0.001
12.967 0.001
12.983 0.001
13.000 0.001
13.017 0.001
13.033 0.001
13.050 0.001
13.067 0.001
13.083 0.001
13.100 0.001
13.117 0.001
13.133 0.001
13.150 0.001
13.167 0.001
13.183 0.001
13.200 0.001
13.217 0.001
13.233 0.001
13.250 0.001
13.267 0.002
13.283 0.002
13.300 0.002
13.317 0.002
13.333 0.002
13.350 0.002
13.367 0.002
13.383 0.002
13.400 0.002
13.417 0.002
13.433 0.002
13.450 0.002
13.467 0.002
13.483 0.002
13.500 0.002
13.517 0.002
13.533 0.002
13.550 0.002
13.567 0.002
13.583 0.002
13.600 0.002
13.617 0.002
13.633 0.002
13.650 0.002
13.667 0.002
13.683 0.002
13.700 0.002
13.717 0.002
13.733 0.002
13.750 0.002
13.767 0.002
13.783 0.002
13.800 0.002
13.817 0.002
13.833 0.002
13.850 0.002
13.867 0.002
13.883 0.003
13.900 0.003

0. 0.4 0.8 1.2 1.6 2.
1.0E-4
0.001
0.01
0.1
1.
10.
Time (min)Displacement (ft)WELL TEST ANALYSIS
Data Set: F:\...\Revised_TW-1.aqt
Date: 09/17/21 Time: 08:03:19
PROJECT INFORMATION
Company: Geological Resources, Inc.
Client: Trindale Mini Mart
Project: 4236
Location: Trinity, NC
Test Well: TW-1
Test Date: 8/24/21
AQUIFER DATA
Saturated Thickness: 2.7 ft Anisotropy Ratio (Kz/Kr): 1.
WELL DATA (TW-1)
Initial Displacement: 1.75 ft Static Water Column Height: 41.45 ft
Total Well Penetration Depth: 41.45 ft Screen Length: 5. ft
Casing Radius: 0.085 ft Well Radius: 0.1875 ft
SOLUTION
Aquifer Model: Unconfined Solution Method: Bouwer-Rice
K = 0.01015 ft/min y0 = 1.653 ft
Trindale Mini Mart
Well TW-1
Test Date 08/24/21
Initial DTW (ft) 23.63
Time Displacement
(min) (ft)
0 0
0.017 1.2494
0.033 1.5577
0.050 1.4776
0.067 1.4085
0.083 1.3476
0.100 1.2933
0.117 1.2405
0.133 1.1937
0.150 1.1455
0.167 1.1015
0.183 1.0617
0.200 1.0209
0.217 0.9843
0.233 0.9465
0.250 0.9126
0.267 0.8796
0.283 0.8474
0.300 0.8169
0.317 0.7864
0.333 0.7576
0.350 0.7307
0.367 0.7022
0.383 0.6758
0.400 0.6524
0.417 0.6278
0.433 0.6042
0.450 0.5821
0.467 0.5584
0.483 0.5382
0.500 0.5176
0.517 0.499
0.533 0.478
0.550 0.4599
0.567 0.4391
0.583 0.4246
0.600 0.4074
0.617 0.3913
0.633 0.3751
0.650 0.3566
0.667 0.3419
0.683 0.3285
0.700 0.315
0.717 0.3025
0.733 0.2895
0.750 0.2754
0.767 0.2646
0.783 0.2531
0.800 0.2431
0.817 0.2296
0.833 0.2133
0.850 0.2067
0.867 0.1986
0.883 0.192
0.900 0.1828
0.917 0.1767
0.933 0.1688
0.950 0.1597
0.967 0.1531
0.983 0.1447
1.000 0.1377
1.017 0.1303
1.033 0.1224
1.050 0.1162
1.067 0.1097
1.083 0.1015
1.100 0.0975
1.117 0.0905
1.133 0.0844
1.150 0.0803
1.167 0.0738
1.183 0.0691
1.200 0.0626
1.217 0.0587
1.233 0.0546
1.250 0.0501
1.267 0.045
1.283 0.0404
1.300 0.0364
1.317 0.0332
1.333 0.0296
1.350 0.0246
1.367 0.0213
1.383 0.0178
1.400 0.0131
1.417 0.0114
1.433 0.0081
1.450 0.0038
1.467 0.0007

GRAIN SIZE ANALYSIS ASTM D 422
Project:Trindale Mini Mart Fine sandy silt
Sample Location:MW-9
Sample Depth:35'
Size Total %
Particle Size % Finer % Retained Description
3"100.0 0.0
1 1/2"100.0 0.0
1"100.0 0.0
3/4"100.0 0.0 Gravel 1.60 GRAVEL 1.60
3/8"98.9 1.1
#4 98.4 0.5
#10 98.0 0.4 Coarse Sand Coarse Sand 0.40
#20 97.1 0.9
#40 94.2 2.9 Medium Sand 3.80
#60 89.7 4.5
#100 77.2 12.5 Fine Sand 22.20 SAND 26.40
#200 72.0 5.2
Particle Size % Finer % Retained Description
0.035 46.0 26.0
0.025 46.0 0.0
0.018 46.0 0.0
0.013 46.0 0.0 Silt 58.00 SILT 58.00
0.009 46.0 0.0
0.007 46.0 0.0
0.005 14.0 32.0
0.003 6.0 8.0
0.002 6.0 0.0 Clay 14.00 CLAY 14.00
Total %100.00 Total %100.00
Clay
Sieve Data
Gravel
Medium Sand
Fine Sand
Hydrometer Data
Silt
GRAIN SIZE ANALYSIS ASTM D 422
Project:Trindale Mini Mart Fine-medium sand
Sample Location:TW-1
Sample Depth:64'
Size Total %
Particle Size % Finer % Retained Description
3"100.0 0.0
1 1/2"100.0 0.0
1"100.0 0.0
3/4"100.0 0.0 Gravel 0.00 GRAVEL 0.00
3/8"100.0 0.0
#4 100.0 0.0
#10 96.6 3.4 Coarse Sand Coarse Sand 3.40
#20 82.6 14.0
#40 58.6 24.0 Medium Sand 38.00
#60 35.2 23.4
#100 12.8 22.4 Fine Sand 50.70 SAND 92.10
#200 7.9 4.9
Particle Size % Finer % Retained Description
0.035 0.9 7.0
0.025 0.9 0.0
0.018 0.9 0.0
0.013 0.9 0.0 Silt 6.96 SILT 6.96
0.009 0.9 0.0
0.007 0.9 0.0
0.005 0.9 0.0
0.003 0.9 0.0
0.002 0.9 0.0 Clay 0.94 CLAY 0.94
Total %100.00 Total %100.00
Clay
Sieve Data
Gravel
Medium Sand
Fine Sand
Hydrometer Data
Silt

APPENDIX H
Public Notification

•
•
••
January 26, 2023

CERTIFIED MAIL

Mayor Richard McNabb
Mayor of Trinity
6923 Stone Gables Drive
Thomasville, NC 27360

RE: Comprehensive Site Assessment – Public Notice
Trindale Mini Mart
7619 NC Highway 62
Trinity, North Carolina
Randolph County
Incident Number: 44719
GRI Project Number: 4236

Dear Mayor McNabb:

In August 2016, a petroleum release was reported at the above referenced property. In conjunction with
the North Carolina Department of Environmental Quality (NCDEQ), soil and ground water assessment
activities, including Phase I Limited Site Assessment (LSA) and Comprehensive Site Assessment (CSA), were
conducted at the site.

Please find enclosed a copy of the executive summary and pertinent figures and tables associated with
the CSA Report for the above referenced site in accordance with the public notice requirements listed 15A
NCAC 2L .0114 of the Guidelines for Assessment and Corrective Action published by the UST Section of
NCDEQ.

Please do not hesitate to contact the undersigned at [phone] if you have any questions or
comments.

Sincerely,

Joanna Alley, P.E.
Project Manager

enclosure

•
•
••
January 26, 2023

CERTIFIED MAIL

Tara Aker
Randolph County Health Director
2222 B South Fayetteville Street
Asheboro, NC 27205

RE: Comprehensive Site Assessment – Public Notice
Trindale Mini Mart
7619 NC Highway 62
Trinity, North Carolina
Randolph County
Incident Number: 44719
GRI Project Number: 4236

Dear Ms. Aker:

In August 2016, a petroleum release was reported at the above referenced property. In conjunction
with the North Carolina Department of Environmental Quality (NCDEQ), soil and ground water
assessment activities, including Phase I Limited Site Assessment (LSA) and Comprehensive Site
Assessment (CSA), were conducted at the site.

Please find enclosed a copy of the executive summary and pertinent figures and tables associated with
the CSA Report for the above referenced site in accordance with the public notice requirements listed
15A NCAC 2L .0114 of the Guidelines for Assessment and Corrective Action published by the UST Section
of NCDEQ.

Please do not hesitate to contact the undersigned at [phone] if you have any questions or
comments.

Sincerely,

Joanna Alley, P.E.
Project Manager

enclosure