WS-2480_3596_P_NPDES_20170518

WATERS EDGE ENVIRONMENTAL, LLC
1434 CHESTER ROAD  RALEIGH, NC 27608  PHONE [phone]

May 18, 2017

Mr. Michael Rogers
North Carolina Department of Environment Quality (NCDEQ)
Division of Water Quality
Groundwater Section
585 Waughtown Street
Winston-Salem, North Carolina 27106

Reference: May 2017 Quarterly Influent/Effluent Results
Highland Industries/Takata
(Former Burlington Industries Site)
Kernersville, North Carolina
Waters Edge Job No. R1-06

Dear Mr. Rogers:

Waters Edge Environmental, LLC (Waters Edge) is pleased to submit this report summarizing the
quarterly influent/effluent sampling event conducted on May 3, 2017 at the Highland/Takata
facility located in Kernersville, North Carolina. The influent and effluent were grab sampled as
specified in the NCDEQ; Division of Water Quality permit number WQ0006751. The influent
detected 58,500 ug/L total VOCs with the only constituents being toluene. The effluent detected
1,940 ug/L toluene and 1.8 ug/L benzene for a removal efficiency of 96.68% which is above the
95% removal rate specified in the permit but the effluent does exceed the North Carolina
Groundwater Standard (NCGS) for toluene at 600 ug/L and benzene at 1 ug/L. We have included
Form GW-59 in Appendix A and documentation in Appendix B. These forms have also been
submitted to the NCDEQ Central Files located in Raleigh, North Carolina. Based on the results
exceeding NCGS, we will mobilize an environmental technician to perform additional O&M to
increase the efficiency.

If you have any questions or comments regarding this report, please contact Phillip L. Rahn at
919.859.9987 or [e-mail].

Sincerely,
WATERS EDGE ENVIRONMENTAL, LLC.
Phillip L. Rahn, P.G.
President
17-033/PLR/aht

cc: Mr. Bryan Roan– Highland Industries/Takata
NCDEQ Central Files and Permits and Compliance Unit

Appendix A
GW-59 Rev. 4/98 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail Original to:DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: [phone] FACILITY INFORMATION Please Print Clearly or Type Facility Name: Highland Industries/Takata Permit Name (if different): Facility Address: 215 Drummond Street (Street) Kernersville NC 27284 County Forsyth (City) (State) (Zip) Contact Person: Bryan Roan Telephone #: [phone] Well Location/Site Name: No. of Wells to be Sampled: 1 (from Permit) NOTE: Values should reflect dissolved and colloidal concentrations. Date sample collected: 5.3.17 Date sample analyzed: 5.16.17 Laboratory Name: Pace Analytical Certification No. NC # 37706 Well Identification Number (from Permit): Well Depth: N/A ft. Well Diameter: N/A in. Screened Interval: N/A ft. to N/A ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is N/A ft. above land surface.For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Gallons of water pumped/bailed before sampling: --- Field analysis: pH , Specific Conductance uMhos Temp. C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO) COD mg/l Nitrite (NO2) as N mg/l Ni – Nickel mg/l Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/l PB – Lead mg/l Coliform: MF Total /100ml Phosphorous: Total as P mg/l Zn – Zinc mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Ammonia Nitrogen mg/l Dissolved Solids: Total mg/l Al – Aluminum mg/l Other (Specify Compounds and Concentration Units) pH (when analyzed) units Ba – Barium mg/l Toluene 58,500 ug/L TOC mg/l Ca – Calcium mg/l Chloride mg/l Cd – Cadmium mg/l Arsenic mg/l Chromium: Total mg/l Grease and Oils mg/l Cu – Copper mg/l Phenol mg/l Fe – Iron mg/l ORGANICS: (GC, GC/MS, HPLC) Sulfate mg/l HG – Mercury mg/l (Specify test and method #. Attach lab report.) Specific Conductance uMhos K – Potassium mg/l Report Attached? Yes X (1) No (0) Total Ammonia mg/l Mg – Magnesium mg/l VOC : method # = 6200B TKN as N mg/l Mn – Manganese mg/l : method # = : method # = I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Phillip Rahn – President, Waters Edge Environmental, LLC Permittee (or Authorized Agent) Name and Title – Please print or type 5.18.17 Signature of Permittee (or Authorized Agent) (Date) PERMIT #: EXPIRATION DATE: Not Specified Non-Discharge WQ0006751 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon X Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge
GW-59 Rev. 4/98 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail Original to:DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: [phone] FACILITY INFORMATION Please Print Clearly or Type Facility Name: Highland Industries/Takata Permit Name (if different): Facility Address: 215 Drummond Street (Street) Kernersville NC 27284 County Forsyth (City) (State) (Zip) Contact Person: Bryan Roan Telephone #: [phone] Well Location/Site Name: No. of Wells to be Sampled: 1 (from Permit) NOTE: Values should reflect dissolved and colloidal concentrations. Date sample collected: 5.3.17 Date sample analyzed: 5.11.17 Laboratory Name: Pace Analytical Certification No. NC # 37706 Well Identification Number (from Permit): Well Depth: N/A ft. Well Diameter: N/A in. Screened Interval: N/A ft. to N/A ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is N/A ft. above land surface.For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Gallons of water pumped/bailed before sampling: --- Field analysis: pH , Specific Conductance uMhos Temp. C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO) COD mg/l Nitrite (NO2) as N mg/l Ni – Nickel mg/l Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/l PB – Lead mg/l Coliform: MF Total /100ml Phosphorous: Total as P mg/l Zn – Zinc mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Ammonia Nitrogen mg/l Dissolved Solids: Total mg/l Al – Aluminum mg/l Other (Specify Compounds and Concentration Units) pH (when analyzed) units Ba – Barium mg/l Toluene 1,940 ug/L TOC mg/l Ca – Calcium mg/l Benzene 1.8 ug/L Chloride mg/l Cd – Cadmium mg/l Arsenic mg/l Chromium: Total mg/l Grease and Oils mg/l Cu – Copper mg/l Phenol mg/l Fe – Iron mg/l ORGANICS: (GC, GC/MS, HPLC) Sulfate mg/l HG – Mercury mg/l (Specify test and method #. Attach lab report.) Specific Conductance uMhos K – Potassium mg/l Report Attached? Yes X (1) No (0) Total Ammonia mg/l Mg – Magnesium mg/l VOC : method # = 6200B TKN as N mg/l Mn – Manganese mg/l : method # = : method # = I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Phillip Rahn – President, Waters Edge Environmental, LLC Permittee (or Authorized Agent) Name and Title – Please print or type 5.18.17 Signature of Permittee (or Authorized Agent) (Date) PERMIT #: EXPIRATION DATE: Not Specified Non-Discharge WQ0006751 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon X Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge

Appendix B
#=CL#
May 17, 2017
LIMS USE: FR - PHIL RAHN
LIMS OBJECT ID: 92339197
92339197
Project:
Pace Project No.:
RE:
Mr. Phil Rahn
Waters Edge Environmental
1434 Chester Road
Raleigh, NC 27606
BI-KERNERSVILLE
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on May 03, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 13
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Lab ID Sample ID Matrix Date Collected Date Received
92339197001 INFLUENT Water 05/03/17 11:00 05/03/17 13:25
92339197002 EFFLUENT Water 05/03/17 12:00 05/03/17 13:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 13
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92339197001 INFLUENT SM 6200B 16 PASI-CZDO
92339197002 EFFLUENT SM 6200B 16 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Sample:INFLUENT Lab ID:92339197001 Collected:05/03/17 11:00 Received:05/03/17 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B602 Volatiles by Method 6200
Benzene ND ug/L 05/16/17 17:37 71-43-2400400400
Chlorobenzene ND ug/L 05/16/17 17:37 108-90-7400400400
1,2-Dichlorobenzene ND ug/L 05/16/17 17:37 95-50-1400400400
1,3-Dichlorobenzene ND ug/L 05/16/17 17:37 541-73-1400400400
1,4-Dichlorobenzene ND ug/L 05/16/17 17:37 106-46-7400400400
Diisopropyl ether ND ug/L 05/16/17 17:37 108-20-3400400400
Ethylbenzene ND ug/L 05/16/17 17:37 100-41-4400400400
Isopropylbenzene (Cumene)ND ug/L 05/16/17 17:37 98-82-8400400400
Methyl-tert-butyl ether ND ug/L 05/16/17 17:37 1634-04-4400400400
Naphthalene ND ug/L 05/16/17 17:37 91-20-3800800400
Toluene 58500 ug/L 05/16/17 17:37 108-88-3400400400
m&p-Xylene ND ug/L 05/16/17 17:37 179601-23-1800800400
o-Xylene ND ug/L 05/16/17 17:37 95-47-6400400400
Surrogates
4-Bromofluorobenzene (S)100 %05/16/17 17:37 460-00-470-130 400
1,2-Dichloroethane-d4 (S)107 %05/16/17 17:37 17060-07-070-130 400
Toluene-d8 (S)105 %05/16/17 17:37 2037-26-570-130 400
Sample:EFFLUENT Lab ID:92339197002 Collected:05/03/17 12:00 Received:05/03/17 13:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B602 Volatiles by Method 6200
Benzene 1.8 ug/L 05/11/17 19:07 71-43-21.0 1.0 1
Chlorobenzene ND ug/L 05/11/17 19:07 108-90-71.0 1.0 1
1,2-Dichlorobenzene ND ug/L 05/11/17 19:07 95-50-11.0 1.0 1
1,3-Dichlorobenzene ND ug/L 05/11/17 19:07 541-73-11.0 1.0 1
1,4-Dichlorobenzene ND ug/L 05/11/17 19:07 106-46-71.0 1.0 1
Diisopropyl ether ND ug/L 05/11/17 19:07 108-20-31.0 1.0 1
Ethylbenzene ND ug/L 05/11/17 19:07 100-41-41.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 05/11/17 19:07 98-82-81.0 1.0 1
Methyl-tert-butyl ether ND ug/L 05/11/17 19:07 1634-04-41.0 1.0 1
Naphthalene ND ug/L 05/11/17 19:07 91-20-32.0 2.0 1
Toluene 1940 ug/L 05/11/17 19:07 108-88-3 E,M11.0 1.0 1
m&p-Xylene ND ug/L 05/11/17 19:07 179601-23-12.0 2.0 1
o-Xylene ND ug/L 05/11/17 19:07 95-47-61.0 1.0 1
Surrogates
4-Bromofluorobenzene (S)98 %05/11/17 19:07 460-00-4 P270-130 1
1,2-Dichloroethane-d4 (S)106 %05/11/17 19:07 17060-07-070-130 1
Toluene-d8 (S)100 %05/11/17 19:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/17/2017 01:53 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
360199
SM 6200B
SM 6200B
602 by 6200B
Associated Lab Samples:92339197002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1997601
Associated Lab Samples:92339197002
Matrix:Water
AnalyzedMDL
1,2-Dichlorobenzene ug/L ND 1.0 05/11/17 15:401.0
1,3-Dichlorobenzene ug/L ND 1.0 05/11/17 15:401.0
1,4-Dichlorobenzene ug/L ND 1.0 05/11/17 15:401.0
Benzene ug/L ND 1.0 05/11/17 15:401.0
Chlorobenzene ug/L ND 1.0 05/11/17 15:401.0
Diisopropyl ether ug/L ND 1.0 05/11/17 15:401.0
Ethylbenzene ug/L ND 1.0 05/11/17 15:401.0
Isopropylbenzene (Cumene)ug/L ND 1.0 05/11/17 15:401.0
m&p-Xylene ug/L ND 2.0 05/11/17 15:402.0
Methyl-tert-butyl ether ug/L ND 1.0 05/11/17 15:401.0
Naphthalene ug/L ND 2.0 05/11/17 15:402.0
o-Xylene ug/L ND 1.0 05/11/17 15:401.0
Toluene ug/L ND 1.0 05/11/17 15:401.0
1,2-Dichloroethane-d4 (S)%103 70-130 05/11/17 15:40
4-Bromofluorobenzene (S)%100 70-130 05/11/17 15:40
Toluene-d8 (S)%104 70-130 05/11/17 15:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1997602LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 48.150 96 60-140
1,3-Dichlorobenzene ug/L 48.750 97 60-140
1,4-Dichlorobenzene ug/L 49.750 99 60-140
Benzene ug/L 51.650 103 60-140
Chlorobenzene ug/L 48.150 96 60-140
Diisopropyl ether ug/L 49.450 99 60-140
Ethylbenzene ug/L 50.350 101 60-140
Isopropylbenzene (Cumene)ug/L 49.250 98 60-140
m&p-Xylene ug/L 98.9100 99 60-140
Methyl-tert-butyl ether ug/L 53.350 107 60-140
Naphthalene ug/L 50.050 100 60-140
o-Xylene ug/L 49.650 99 60-140
Toluene ug/L 49.450 99 60-140
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/17/2017 01:53 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1997604MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92339197002
1997605
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2-Dichlorobenzene ug/L 20 108 60-140113 4 3020ND21.7 22.6
1,3-Dichlorobenzene ug/L 20 113 60-140116 2 3020ND22.6 23.1
1,4-Dichlorobenzene ug/L 20 114 60-140120 5 3020ND22.8 23.9
Benzene ug/L 20 116 60-140118 2 30201.8 24.9 25.5
Chlorobenzene ug/L 20 110 60-140114 4 3020ND22.1 22.9
Diisopropyl ether ug/L 20 115 60-140118 2 3020ND23.0 23.5
Ethylbenzene ug/L 20 115 60-140120 4 3020ND23.5 24.5
Isopropylbenzene (Cumene)ug/L 20 110 60-140115 4 3020ND22.1 23.0
m&p-Xylene ug/L 40 111 60-140115 3 3040ND45.4 46.9
Methyl-tert-butyl ether ug/L 20 117 60-140123 5 3020ND23.5 24.6
Naphthalene ug/L 20 107 60-140111 4 3020ND21.4 22.2
o-Xylene ug/L 20 112 60-140116 4 3020ND22.3 23.3
Toluene ug/L E,M120-856 60-140-968 1 3020194017701750
1,2-Dichloroethane-d4 (S)%107 70-130107
4-Bromofluorobenzene (S)%97 70-13099
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/17/2017 01:53 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
360759
SM 6200B
SM 6200B
602 by 6200B
Associated Lab Samples:92339197001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2000884
Associated Lab Samples:92339197001
Matrix:Water
AnalyzedMDL
1,2-Dichlorobenzene ug/L ND 1.0 05/16/17 16:281.0
1,3-Dichlorobenzene ug/L ND 1.0 05/16/17 16:281.0
1,4-Dichlorobenzene ug/L ND 1.0 05/16/17 16:281.0
Benzene ug/L ND 1.0 05/16/17 16:281.0
Chlorobenzene ug/L ND 1.0 05/16/17 16:281.0
Diisopropyl ether ug/L ND 1.0 05/16/17 16:281.0
Ethylbenzene ug/L ND 1.0 05/16/17 16:281.0
Isopropylbenzene (Cumene)ug/L ND 1.0 05/16/17 16:281.0
m&p-Xylene ug/L ND 2.0 05/16/17 16:282.0
Methyl-tert-butyl ether ug/L ND 1.0 05/16/17 16:281.0
Naphthalene ug/L ND 2.0 05/16/17 16:282.0
o-Xylene ug/L ND 1.0 05/16/17 16:281.0
Toluene ug/L ND 1.0 05/16/17 16:281.0
1,2-Dichloroethane-d4 (S)%103 70-130 05/16/17 16:28
4-Bromofluorobenzene (S)%100 70-130 05/16/17 16:28
Toluene-d8 (S)%107 70-130 05/16/17 16:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2000885LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichlorobenzene ug/L 50.650 101 60-140
1,3-Dichlorobenzene ug/L 52.250 104 60-140
1,4-Dichlorobenzene ug/L 52.450 105 60-140
Benzene ug/L 55.150 110 60-140
Chlorobenzene ug/L 51.150 102 60-140
Diisopropyl ether ug/L 53.950 108 60-140
Ethylbenzene ug/L 53.250 106 60-140
Isopropylbenzene (Cumene)ug/L 51.950 104 60-140
m&p-Xylene ug/L 104100 104 60-140
Methyl-tert-butyl ether ug/L 57.050 114 60-140
Naphthalene ug/L 52.150 104 60-140
o-Xylene ug/L 52.950 106 60-140
Toluene ug/L 52.850 106 60-140
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/17/2017 01:53 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/17/2017 01:53 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 9 of 13
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92339197
BI-KERNERSVILLE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92339197001 360759INFLUENTSM 6200B
92339197002 360199EFFLUENTSM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 05/17/2017 01:53 PM
Pace Analytical Services, LLC
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 10 of 13
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