WS-2480_3596_P_NPDES_20160525

WATERS EDGE ENVIRONMENTAL, LLC
4901 WATERS EDGE DRIVE, SUITE 201  RALEIGH, NC 27606  PHONE [phone]  FAX [phone]

May 25, 2016

Mr. Michael Rogers
North Carolina Department of Environment Quality (NCDEQ)
Division of Water Quality
Groundwater Section
585 Waughtown Street
Winston-Salem, North Carolina 27106

Reference: April 2016 Quarterly Influent/Effluent Results
Highland Industries/Takada
(Former Burlington Industries Site)
Kernersville, North Carolina
Waters Edge Job No. R1-06

Dear Mr. Rogers:

Waters Edge Environmental, LLC (Waters Edge) is pleased to submit this report
summarizing the quarterly influent/effluent sampling event conducted on April 29, 2016
at the Takada facility located in Kernersville, North Carolina. The influent and effluent
were grab sampled as specified in the NCDEQ; Division of Water Quality permit number
WQ0006751. The influent detected 47,010 ug/L total VOCs with the only constituents
being toluene (46,600 ug/L) and tetrachloroethene (PCE- 410 ug/L). The effluent .
detected 910 ug/L toluene for a removal efficiency of 99.98% and the effluent is above
the North Carolina Groundwater Standard at 2.7 ug/L (NCGS at 0.7 ug/L). We would
also comment that the PCE may be from an offsite source not related to this facilityWe
have included Form GW-59 in Appendix A and documentation in Appendix B. These
forms have also been submitted to the NCDEQ Central Files located in Raleigh, North
Carolina.

If you have any questions or comments regarding this report, please contact Phillip L.
Rahn at 919.859.9987 or [e-mail].

Sincerely,
WATERS EDGE ENVIRONMENTAL, LLC.
Phillip L. Rahn, P.G.
President
16-048/PLR/aht

cc: Mr. Brian Roan– Highland Industries/Takada
NCDENR Central Files and Permits and Compliance Unit

Appendix A
GW-59 Rev. 4/98 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail Original to:DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: [phone] FACILITY INFORMATION Please Print Clearly or Type Facility Name: Highland Industries/Takada Permit Name (if different): Facility Address: 215 Drummond Street (Street) Kernersville NC 27284 County Forsyth (City) (State) (Zip) Contact Person: Brian Roan Telephone #: [phone] Well Location/Site Name: No. of Wells to be Sampled: 1 (from Permit) NOTE: Values should reflect dissolved and colloidal concentrations. Date sample collected: 4.29.16 Date sample analyzed: 5.13.16 Laboratory Name: Pace Analytical Certification No. NC # 37706 Well Identification Number (from Permit): Well Depth: N/A ft. Well Diameter: N/A in. Screened Interval: N/A ft. to N/A ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is N/A ft. above land surface.For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Gallons of water pumped/bailed before sampling: --- Field analysis: pH , Specific Conductance uMhos Temp. C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO) COD mg/l Nitrite (NO2) as N mg/l Ni – Nickel mg/l Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/l PB – Lead mg/l Coliform: MF Total /100ml Phosphorous: Total as P mg/l Zn – Zinc mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Ammonia Nitrogen mg/l Dissolved Solids: Total mg/l Al – Aluminum mg/l Other (Specify Compounds and Concentration Units) pH (when analyzed) units Ba – Barium mg/l Toluene 46,600 ug/L TOC mg/l Ca – Calcium mg/l Tetrachloroethene 410 ug/L Chloride mg/l Cd – Cadmium mg/l Arsenic mg/l Chromium: Total mg/l Grease and Oils mg/l Cu – Copper mg/l Phenol mg/l Fe – Iron mg/l ORGANICS: (GC, GC/MS, HPLC) Sulfate mg/l HG – Mercury mg/l (Specify test and method #. Attach lab report.) Specific Conductance uMhos K – Potassium mg/l Report Attached? Yes (1) No X (0) Total Ammonia mg/l Mg – Magnesium mg/l VOC : method # = 6200B TKN as N mg/l Mn – Manganese mg/l : method # = : method # = I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Phillip Rahn – President, Waters Edge Environmental, LLC Permittee (or Authorized Agent) Name and Title – Please print or type 5.25.16 Signature of Permittee (or Authorized Agent) (Date) PERMIT #: EXPIRATION DATE: 01/31/2013 Non-Discharge WQ0006751 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon X Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other:
GW-59 Rev. 4/98 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Mail Original to:DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH, NC 27699-1636 Phone: [phone] FACILITY INFORMATION Please Print Clearly or Type Facility Name: Highland Industries/Takada Permit Name (if different): Facility Address: 215 Drummond Street (Street) Kernersville NC 27284 County Forsyth (City) (State) (Zip) Contact Person: Brian Roan Telephone #: [phone] Well Location/Site Name: No. of Wells to be Sampled: 1 (from Permit) NOTE: Values should reflect dissolved and colloidal concentrations. Date sample collected: 14.29.16 Date sample analyzed: 513.16 Laboratory Name: Pace Analytical Certification No. NC # 37706 Well Identification Number (from Permit): Well Depth: N/A ft. Well Diameter: N/A in. Screened Interval: N/A ft. to N/A ft. Depth to Water Level: N/A ft. below measuring point. Measuring Point is N/A ft. above land surface.For Groundwater Treatment Systems Check One: Influent (98) Effluent (99) Gallons of water pumped/bailed before sampling: --- Field analysis: pH , Specific Conductance uMhos Temp. C, Odor Appearance PARAMETERS (Samples for metals were collected unfiltered YES NO and field acidified YES NO) COD mg/l Nitrite (NO2) as N mg/l Ni – Nickel mg/l Coliform: MF Fecal /100ml Nitrate (NO3) as N mg/l PB – Lead mg/l Coliform: MF Total /100ml Phosphorous: Total as P mg/l Zn – Zinc mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Ammonia Nitrogen mg/l Dissolved Solids: Total mg/l Al – Aluminum mg/l Other (Specify Compounds and Concentration Units) pH (when analyzed) units Ba – Barium mg/l Toluene 910 ug/L TOC mg/l Ca – Calcium mg/l Chloride mg/l Cd – Cadmium mg/l Arsenic mg/l Chromium: Total mg/l Grease and Oils mg/l Cu – Copper mg/l Phenol mg/l Fe – Iron mg/l ORGANICS: (GC, GC/MS, HPLC) Sulfate mg/l HG – Mercury mg/l (Specify test and method #. Attach lab report.) Specific Conductance uMhos K – Potassium mg/l Report Attached? Yes (1) No X (0) Total Ammonia mg/l Mg – Magnesium mg/l VOC : method # = 6200B TKN as N mg/l Mn – Manganese mg/l : method # = : method # = I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a North Carolina DWQ (formerly DEM) certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Phillip Rahn – President, Waters Edge Environmental, LLC Permittee (or Authorized Agent) Name and Title – Please print or type 5.25.16 Signature of Permittee (or Authorized Agent) (Date) PERMIT #: EXPIRATION DATE: 1/31/2013 Non-Discharge WQ0006751 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon X Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other:

Appendix B
#=CL#
May 13, 2016
LIMS USE: FR - PHIL RAHN
LIMS OBJECT ID: 92296229
92296229
Project:
Pace Project No.:
RE:
Mr. Phil Rahn
Waters Edge Environmental
4901 Water's Edge Drive
Suite 201
Raleigh, NC 27606
RI-KERNERSVILLE R1-06
Dear Mr. Rahn:
Enclosed are the analytical results for sample(s) received by the laboratory on May 04, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brittany Gibson
[e-mail]
Project Coordinator
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 1 of 13
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 2 of 13
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Lab ID Sample ID Matrix Date Collected Date Received
92296229001 INFLUENT Water 04/29/16 11:15 05/04/16 12:55
92296229002 EFFLUENT Water 04/29/16 11:45 05/04/16 12:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 3 of 13
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92296229001 INFLUENT SM 6200B 34 PASI-CCAH
92296229002 EFFLUENT SM 6200B 34 PASI-CCAH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 4 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Sample:INFLUENT Lab ID:92296229001 Collected:04/29/16 11:15 Received:05/04/16 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
1,1-Dichloroethane ND mg/L 05/13/16 10:23 75-34-30.12 0.062 250
1,1-Dichloroethene ND mg/L 05/13/16 10:23 75-35-40.12 0.062 250
1,1,1-Trichloroethane ND mg/L 05/13/16 10:23 71-55-60.12 0.062 250
1,1,2-Trichloroethane ND mg/L 05/13/16 10:23 79-00-50.12 0.062 250
1,1,2,2-Tetrachloroethane ND mg/L 05/13/16 10:23 79-34-50.12 0.062 250
1,2-Dichlorobenzene ND mg/L 05/13/16 10:23 95-50-10.12 0.062 250
1,2-Dichloroethane ND mg/L 05/13/16 10:23 107-06-20.12 0.062 250
1,2-Dibromoethane (EDB)ND mg/L 05/13/16 10:23 106-93-40.12 0.062 250
1,2-Dichloropropane ND mg/L 05/13/16 10:23 78-87-50.12 0.062 250
1,3-Dichlorobenzene ND mg/L 05/13/16 10:23 541-73-10.12 0.062 250
1,4-Dichlorobenzene ND mg/L 05/13/16 10:23 106-46-70.12 0.062 250
Bromodichloromethane ND mg/L 05/13/16 10:23 75-27-40.12 0.062 250
Bromomethane ND mg/L 05/13/16 10:23 74-83-91.2 0.12 250
Bromoform ND mg/L 05/13/16 10:23 75-25-20.12 0.062 250
cis-1,2-Dichloroethene ND mg/L 05/13/16 10:23 156-59-20.12 0.062 250
cis-1,3-Dichloropropene ND mg/L 05/13/16 10:23 10061-01-50.12 0.062 250
Carbon tetrachloride ND mg/L 05/13/16 10:23 56-23-50.12 0.062 250
Chlorobenzene ND mg/L 05/13/16 10:23 108-90-70.12 0.062 250
Chloroethane ND mg/L 05/13/16 10:23 75-00-30.25 0.12 250
Chloroform ND mg/L 05/13/16 10:23 67-66-30.12 0.062 250
Chloromethane ND mg/L 05/13/16 10:23 74-87-30.25 0.12 250
Dibromochloromethane ND mg/L 05/13/16 10:23 124-48-10.12 0.062 250
Dichlorodifluoromethane ND mg/L 05/13/16 10:23 75-71-80.12 0.062 250
Methylene Chloride ND mg/L 05/13/16 10:23 75-09-20.50 0.25 250
trans-1,2-Dichloroethene ND mg/L 05/13/16 10:23 156-60-50.12 0.062 250
trans-1,3-Dichloropropene ND mg/L 05/13/16 10:23 10061-02-60.12 0.062 250
Tetrachloroethene 0.41 mg/L 05/13/16 10:23 127-18-40.12 0.062 250
Toluene 46.6 mg/L 05/13/16 10:23 108-88-30.12 0.062 250
Trichloroethene ND mg/L 05/13/16 10:23 79-01-60.12 0.062 250
Trichlorofluoromethane ND mg/L 05/13/16 10:23 75-69-40.25 0.12 250
Vinyl chloride ND mg/L 05/13/16 10:23 75-01-40.25 0.062 250
Surrogates
1,2-Dichloroethane-d4 (S)107 %05/13/16 10:23 17060-07-070-130 250
4-Bromofluorobenzene (S)96 %05/13/16 10:23 460-00-470-130 250
Toluene-d8 (S)101 %05/13/16 10:23 2037-26-570-130 250
Sample:EFFLUENT Lab ID:92296229002 Collected:04/29/16 11:45 Received:05/04/16 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
1,1-Dichloroethane ND mg/L 05/13/16 10:06 75-34-30.0025 0.0012 5
1,1-Dichloroethene ND mg/L 05/13/16 10:06 75-35-40.0025 0.0012 5
1,1,1-Trichloroethane ND mg/L 05/13/16 10:06 71-55-60.0025 0.0012 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/13/2016 04:25 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 5 of 13
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Sample:EFFLUENT Lab ID:92296229002 Collected:04/29/16 11:45 Received:05/04/16 12:55 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
1,1,2-Trichloroethane ND mg/L 05/13/16 10:06 79-00-50.0025 0.0012 5
1,1,2,2-Tetrachloroethane ND mg/L 05/13/16 10:06 79-34-50.0025 0.0012 5
1,2-Dichlorobenzene ND mg/L 05/13/16 10:06 95-50-10.0025 0.0012 5
1,2-Dichloroethane ND mg/L 05/13/16 10:06 107-06-20.0025 0.0012 5
1,2-Dibromoethane (EDB)ND mg/L 05/13/16 10:06 106-93-40.0025 0.0012 5
1,2-Dichloropropane ND mg/L 05/13/16 10:06 78-87-50.0025 0.0012 5
1,3-Dichlorobenzene ND mg/L 05/13/16 10:06 541-73-10.0025 0.0012 5
1,4-Dichlorobenzene ND mg/L 05/13/16 10:06 106-46-70.0025 0.0012 5
Bromodichloromethane ND mg/L 05/13/16 10:06 75-27-40.0025 0.0012 5
Bromomethane ND mg/L 05/13/16 10:06 74-83-90.025 0.0025 5
Bromoform ND mg/L 05/13/16 10:06 75-25-20.0025 0.0012 5
cis-1,2-Dichloroethene ND mg/L 05/13/16 10:06 156-59-20.0025 0.0012 5
cis-1,3-Dichloropropene ND mg/L 05/13/16 10:06 10061-01-50.0025 0.0012 5
Carbon tetrachloride ND mg/L 05/13/16 10:06 56-23-50.0025 0.0012 5
Chlorobenzene ND mg/L 05/13/16 10:06 108-90-70.0025 0.0012 5
Chloroethane ND mg/L 05/13/16 10:06 75-00-30.0050 0.0025 5
Chloroform ND mg/L 05/13/16 10:06 67-66-30.0025 0.0012 5
Chloromethane ND mg/L 05/13/16 10:06 74-87-30.0050 0.0025 5
Dibromochloromethane ND mg/L 05/13/16 10:06 124-48-10.0025 0.0012 5
Dichlorodifluoromethane ND mg/L 05/13/16 10:06 75-71-80.0025 0.0012 5
Methylene Chloride ND mg/L 05/13/16 10:06 75-09-20.010 0.0050 5
trans-1,2-Dichloroethene ND mg/L 05/13/16 10:06 156-60-50.0025 0.0012 5
trans-1,3-Dichloropropene ND mg/L 05/13/16 10:06 10061-02-60.0025 0.0012 5
Tetrachloroethene 0.0027 mg/L 05/13/16 10:06 127-18-40.0025 0.0012 5
Toluene 0.60 mg/L 05/13/16 10:06 108-88-30.0025 0.0012 5
Trichloroethene ND mg/L 05/13/16 10:06 79-01-60.0025 0.0012 5
Trichlorofluoromethane ND mg/L 05/13/16 10:06 75-69-40.0050 0.0025 5
Vinyl chloride ND mg/L 05/13/16 10:06 75-01-40.0050 0.0012 5
Surrogates
1,2-Dichloroethane-d4 (S)108 %05/13/16 10:06 17060-07-070-130 5
4-Bromofluorobenzene (S)95 %05/13/16 10:06 460-00-470-130 5
Toluene-d8 (S)101 %05/13/16 10:06 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/13/2016 04:25 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 6 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/36802
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92296229001, 92296229002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1733147
Associated Lab Samples:92296229001, 92296229002
Matrix:Water
AnalyzedMDL
1,1,1-Trichloroethane ug/L ND 0.50 05/13/16 02:210.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/13/16 02:210.25
1,1,2-Trichloroethane ug/L ND 0.50 05/13/16 02:210.25
1,1-Dichloroethane ug/L ND 0.50 05/13/16 02:210.25
1,1-Dichloroethene ug/L ND 0.50 05/13/16 02:210.25
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/13/16 02:210.25
1,2-Dichlorobenzene ug/L ND 0.50 05/13/16 02:210.25
1,2-Dichloroethane ug/L ND 0.50 05/13/16 02:210.25
1,2-Dichloropropane ug/L ND 0.50 05/13/16 02:210.25
1,3-Dichlorobenzene ug/L ND 0.50 05/13/16 02:210.25
1,4-Dichlorobenzene ug/L ND 0.50 05/13/16 02:210.25
Bromodichloromethane ug/L ND 0.50 05/13/16 02:210.25
Bromoform ug/L ND 0.50 05/13/16 02:210.25
Bromomethane ug/L ND 5.0 05/13/16 02:210.50
Carbon tetrachloride ug/L ND 0.50 05/13/16 02:210.25
Chlorobenzene ug/L ND 0.50 05/13/16 02:210.25
Chloroethane ug/L ND 1.0 05/13/16 02:210.50
Chloroform ug/L ND 0.50 05/13/16 02:210.25
Chloromethane ug/L ND 1.0 05/13/16 02:210.50
cis-1,2-Dichloroethene ug/L ND 0.50 05/13/16 02:210.25
cis-1,3-Dichloropropene ug/L ND 0.50 05/13/16 02:210.25
Dibromochloromethane ug/L ND 0.50 05/13/16 02:210.25
Dichlorodifluoromethane ug/L ND 0.50 05/13/16 02:210.25
Methylene Chloride ug/L ND 2.0 05/13/16 02:211.0
Tetrachloroethene ug/L ND 0.50 05/13/16 02:210.25
Toluene ug/L ND 0.50 05/13/16 02:210.25
trans-1,2-Dichloroethene ug/L ND 0.50 05/13/16 02:210.25
trans-1,3-Dichloropropene ug/L ND 0.50 05/13/16 02:210.25
Trichloroethene ug/L ND 0.50 05/13/16 02:210.25
Trichlorofluoromethane ug/L ND 1.0 05/13/16 02:210.50
Vinyl chloride ug/L ND 1.0 05/13/16 02:210.25
1,2-Dichloroethane-d4 (S)%105 70-130 05/13/16 02:21
4-Bromofluorobenzene (S)%95 70-130 05/13/16 02:21
Toluene-d8 (S)%99 70-130 05/13/16 02:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733148LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1-Trichloroethane ug/L 48.750 97 60-140
1,1,2,2-Tetrachloroethane ug/L 49.250 98 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/13/2016 04:25 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 7 of 13
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1733148LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,2-Trichloroethane ug/L 48.850 98 60-140
1,1-Dichloroethane ug/L 49.450 99 60-140
1,1-Dichloroethene ug/L 48.250 96 60-140
1,2-Dibromoethane (EDB)ug/L 51.650 103 60-140
1,2-Dichlorobenzene ug/L 45.650 91 60-140
1,2-Dichloroethane ug/L 46.150 92 60-140
1,2-Dichloropropane ug/L 50.150 100 60-140
1,3-Dichlorobenzene ug/L 46.650 93 60-140
1,4-Dichlorobenzene ug/L 45.450 91 60-140
Bromodichloromethane ug/L 49.150 98 60-140
Bromoform ug/L 51.150 102 60-140
Bromomethane ug/L 35.550 71 60-140
Carbon tetrachloride ug/L 47.050 94 60-140
Chlorobenzene ug/L 47.950 96 60-140
Chloroethane ug/L 45.450 91 60-140
Chloroform ug/L 48.250 96 60-140
Chloromethane ug/L 34.750 69 60-140
cis-1,2-Dichloroethene ug/L 49.450 99 60-140
cis-1,3-Dichloropropene ug/L 47.850 96 60-140
Dibromochloromethane ug/L 51.650 103 60-140
Dichlorodifluoromethane ug/L 37.050 74 60-140
Methylene Chloride ug/L 52.350 105 60-140
Tetrachloroethene ug/L 44.550 89 60-140
Toluene ug/L 46.450 93 60-140
trans-1,2-Dichloroethene ug/L 48.050 96 60-140
trans-1,3-Dichloropropene ug/L 47.450 95 60-140
Trichloroethene ug/L 44.950 90 60-140
Trichlorofluoromethane ug/L 44.950 90 60-140
Vinyl chloride ug/L 44.050 88 60-140
1,2-Dichloroethane-d4 (S)%108 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/13/2016 04:25 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Page 8 of 13
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/13/2016 04:25 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92296229
RI-KERNERSVILLE R1-06
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92296229001 MSV/36802INFLUENTSM 6200B
92296229002 MSV/36802EFFLUENTSM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 05/13/2016 04:25 PM
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
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