WA-1095_13127_CA_MRP_20180510

Groundwater Monitoring Report

J.C. Penney Company, Inc.
607 North Berkeley Boulevard
Goldsboro, North Carolina 27534
UST Incident Number: 13127
Blue Ridge Project No. 18-6057.1

Prepared for:
Capitol Funds, Inc.
Mr. David W. Royster, III
720 South Lafeyette Street
Shelby, NC 28150

May 10, 2018

Prepared by:
Blue Ridge Environmental Services, Inc.
2315 Kings Rd. Extension
Shelby, North Carolina 28152
704-482-2111
Fax [phone]
Email: [e-mail]

2315 Kings Road Extension
Shelby, North Carolina 28152 
(O)  704.482.2111 
(F)  704.482.4335                     
Email: BRESI@BlueRidge‐ESI.com 
May 10, 2018

Ms. Carrie Stone
N.C. Department of Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

RE: Groundwater Monitoring Report
J.C. Penney Company, Inc.
607 North Berkeley Boulevard
Goldsboro, Wayne County, North Carolina 27534
Incident No. 13127
Blue Ridge Project No. 18-6057.1

Dear Ms. Stone:

Blue Ridge is pleased to submit the Groundwater Monitoring Report for the J.C. Penney
Company, Inc. Site. If you have any questions or concerns, please contact the
undersigned at 704-482-2111 or [e-mail].

Sincerely,
Blue Ridge Environmental Services, Inc.

Jeffrey R. White
Environmental Scientist/Project Manager

2315 Kings Road Extension
Shelby, North Carolina 28152 
(O)  704.482.2111 
(F)  704.482.4335 
Email: BRESI@BlueRidge‐ESI.com 

May 10, 2018

Ms. Carrie Stone
N.C. Department of Environmental Quality
Washington Regional Office
943 Washington Square Mall
Washington, North Carolina 27889

Subject: Groundwater Monitoring Report
J.C. Penney Company, Inc.
607 North Berkeley Boulevard
Goldsboro, Wayne County, North Carolina 27534
Incident No. 13127
Blue Ridge Project No. 18-6057.1

Dear Ms. Stone:

On behalf of Capital Funds, Inc., Blue Ridge Environmental Services, Inc. (Blue Ridge),
is submitting the results of groundwater sampling for the above referenced release
incident at the subject site (“Site”) location shown on Figure 1. The release incident (No.
13127) is the result of soil and groundwater contamination discovered as part of a 550-
gallon fuel oil UST Closure in 1994. Subsequent and most recent historical information
described groundwater sampling activities in August 1999.

In response to the Notice of Regulatory Requirements (NORR) letter dated March 12,
2018 from your office (copy included in Appendix A) and per our phone conversation on
March 28th, 2018, Blue Ridge sampled monitoring well MW-1 and deep monitoring well
DW-1, to determine if historical contaminant concentrations in groundwater have been
remediated to below the North Carolina 2L Groundwater Quality Standards (2L
Standards). A Phase II Limited Site Assessment report, dated August 1999, was the last
historical report submitted. A site map showing the location of the Site monitoring wells
is included as Figure 2.

Summary of Analytical Results

On April 5, 2018, groundwater in monitoring wells MW-1 and DW-1 was gauged, purged
and sampled. Water levels in the monitoring wells sampled were 6.23 feet below grade
level (bgl) at MW-1 and 5.87 feet bgl at DW-1. Current groundwater flow direction was
not calculated during this assessment because only 2 wells were gauged and sampled;
however, groundwater flow direction has historically been determined to the northeast.

Groundwater Monitoring Report May 10, 2018
J.C. Penney Company, Inc. Page 2
Goldsboro, North Carolina 27534
Blue Ridge Project No. 18-6057.1

Historic and recent groundwater data is displayed in Table 1- Relative Groundwater
Elevations.

Groundwater samples collected as part of this event were analyzed for typical petroleum
hydrocarbon constituents by EPA Method 602 with Xylenes, EPA Method 625, MADEP
VPH and MADEP EPH. The results of these analyses, along with the historical data are
presented in Table 2 - Summary of Groundwater Laboratory Analytical Results. A copy
of the Groundwater Laboratory Analytical Data and Chain of Custody has been included
in Appendix B.

The results are also depicted on Figure 3 - Contaminant Concentration Map. The
analytical results from monitoring well MW-1 revealed detectable contaminant
concentrations of 1-Methylnaphthalene (11 ug/L), C9-C10 Aromatics (210 ug/L), C9-C18
Aliphatics (4,100 ug/L) and C11-C22 Aromatics (2,900 ug/L) remaining above the 2L
Standards. Several other contaminants were detected above laboratory detection limits;
however, they were below the 2L Standards. The remaining target analytes were not
detected above laboratory detection limits. The analytical results from DW-1 revealed a
detectable contaminant concentration of bis(2-Ethylhexylphthalate) (1.0 ug/L) found to be
present but below the 2L Standards. The remaining target analytes were not detected
above laboratory detection limits.

The recent groundwater sampling results demonstrate overall reduced levels of
contaminant concentrations; however, concentrations remain above the 2L Standards in
MW-1 after almost 20 years of natural attenuation. Capitol Funds, Inc. has indicated a
Notice of Residual Petroleum (NORP) is not desirable and would like to pursue an
“unconditional” No Further Action status. Therefore, based on the contaminant levels
remaining, Blue Ridge recommends that active remediation of groundwater may be
beneficial to further enhance reduction of contaminant concentrations to below 2L
Standards. Dual-phase technology and/or in-situ bioremediation appear to be
appropriate groundwater remediation technology applicable to the J.C. Penney
Company, Inc. Site. Capitol Funds, Inc. is currently evaluating the remediation options
presented by Blue Ridge.

Groundwater Monitoring Report May 10, 2018
J.C. Penney Company, Inc. Page 3
Goldsboro, North Carolina 27534
Blue Ridge Project No. 18-6057.1

If you have any questions regarding this matter, please do not hesitate to contact us at
[phone].

Respectfully Submitted:
BLUE RIDGE ENVIRONMENTAL SERVICES, INC.

Jeffrey R. White Cliff R. Lundgren, P.G.
Environmental Scientist/Project Manager Senior Consultant/President
N.C. Registration No.1359

cc: Mr. David Royster, III

Groundwater Monitoring Report May 10, 2018
J.C. Penney Company, Inc. Page 4
Goldsboro, North Carolina 27534
Blue Ridge Project No. 18-6057.1

ENCLOSURES

TABLES

Table 1 - Relative Groundwater Elevations
Table 2 - Summary of Groundwater Laboratory Analytical Results

FIGURES

Figure 1 - Site Vicinity Map
Figure 2 - Site Map
Figure 3 - Contaminant Concentration Map

APPENDICES

Appendix A – NORR Letter (March 12, 2018)
Appendix B - Laboratory Analytical Data and Chain of Custody

TABLES
Well ID DateTOC ElevationScreened Interval (ft)Depth to Product (ft.)FPP 2 Thickness (ft.)Depth to water (ft)Water Table Elevation (ft)7/16/99N/A1N/A 6.40 94.004/5/18 N/A N/A 6.23 94.177/16/99 N/A N/A 5.89 93.834/5/187/16/99 N/A N/A 5.45 93.954/5/187/16/99 N/A N/A 5.84 94.164/5/187/16/99 N/A N/A 5.10 93.744/5/18 N/A N/A 5.87 92.971:N/A - Not Applicableft. = feetIncident No.13127 Table 1 Relative Groundwater ElevationsJ.C. Penney Company, Inc.607 North Berkeley Boulevard Goldsboro, North Carolina 27534Blue Ridge Project No. 18-6057.1MW-1 100.40 3.5-10.5MW-2 99.72 3.5-13.5Not GaugedNot GaugedNot GaugedDW-1 98.84 20.5-23.5MW-3 99.40 3.5-13.5MW-4 100.00 3.5-13.5Page 1 of 1
Well IDDate CollectedIncident Phase6/3/98Phase I LSA12.317.8 90.5 258 21.8<10.045<10.0 387 297<10.0 13.8 <10.0 270 323,650 4,2001,1201,6307/21/99Phase II LSA11.44.5 39.9 81.6 38.421.845<20.0 463 30648.8 39.8 <20.0 130 202,140 1,6408901,0204/5/18Sampling Event<2.0<2.0 3.5 <2.0 3.1 1.1 3.2116.0 4.3 4.7 <0.62 2.2 <15.0 460210 4,1001,1002,900MW-2 6/9/99Phase II LSA<0.20 <0.20 <0.20 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3.0 <3.0 <3.0 <73 <58 <49MW-3 6/9/99Phase II LSA<0.20 <0.20 <0.20 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3.0 <3.0 <3.0 <73 <58 <49MW-4 6/9/99Phase II LSA<0.20 <0.20 <0.20 <0.60 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3.0 <3.0 <3.0 <73 <58 <496/9/99Phase II LSA<1.0<1.0 <1.0 <3.0 <1.05.56<1.0<1.07.64 5.16 <1.0 6.96 <1.0 <3.0 <3.0 27 86 1402204/5/18Sampling Event<0.40 <0.40 <0.40 <0.40 <0.11 1.0J <0.060 <0.40 <0.40 <0.13 <0.12 <0.26 <0.060 <15 <15 <5.0 <100 <100 <1001 600 600 500 80 3 300 1 30 6 200 N/A 200 400 700 200 700 10,000 2005,000 260,000 84,500 85,500 2,120 170 N/A 1,000 12,500 6,000 410 N/A 200 N/A N/A N/A N/A N/A N/A1: Keyed to Figure 3Concentrations in bold exceed the current NC 15A NCAC 2L .0202 Groundwater Standard.Please note that only common and detectable constituents are noted.J: Estimated result < Limit of Quantitation > Detection LimitN/A: Not Applicable1-MethylnaphthaleneBis (2-ethylhexyl) PhthalateMADEP VPH2L Standard (ug/l)GCL (ug/l)Naphthalene (625)PhenanthreneContaminant of Concern (ug/l)EthylbenzeneXylenesAcenaphtheneDW-1MW-1Fluorene2-MethylnaphthaleneTable 21 Summary of Groundwater Analytical Laboratory Results Blue Ridge Project No. 18-6057.1Incident No.13127 Goldsboro, North Carolina 27534607 North Berkeley Boulevard J.C. Penney Company, Inc.Analytical Method EPA METHOD 602TolueneBenzeneC11 - C22 AromaticsDi-n-butylphthalatePyreneC19 - C36 AliphaticsC9 - C18 AliphaticsEPA METHOD 625C9 - C12 AliphaticsC5 - C8 AliphaticsMADEP EPHC9 - C10 Aromatics

FIGURES
Approximate Scale: As Shown Figure 1
SITE VICINITY MAP North
Client:
Project:
Location:
Source:
Date: 4/27/18
Capitol Funds, Inc.
J.C. Penney Company, Inc.
607 North Berkeley Boulevard
Goldsboro, North Carolina 27534
MyTopo.com
FORMER CITGO VIEWMONT2200 NORTH CENTER STREETHICKORY, NORTH CAROLINAINCIDENT No. 22165 GROUNDWATER ANALYTICAL RESULTS LIMITED SITE ASSESSMENT - OCTOBER 2000Scale:Date:AS SHOWNJANUARY 2014EA Project No.:FIGURE13-9678.12Site MapJ. C. Penney Company, Inc.607 North Berkeley Blvd.Goldsboro, North Carolina 27534Wayne CountyApril 30, 201813127UST Incident No.:Figure 2N2315 Kings Road ExtensionShelby, North Carolina 28152(O) 704.482.2111(F) 704.482.4335Email: [e-mail] MONITORING WELLBlue Ridge Project No.:18-6057.10804016080 FeetJ. C. PenneyMW-2Berkeley MallLongHorn SteakhouseStarbucksNorth Berkeley Blvd.MONITORING WELLDUMPSTERMW-1MW-4MW-3DW-1Legend & Notes
FORMER CITGO VIEWMONT2200 NORTH CENTER STREETHICKORY, NORTH CAROLINAINCIDENT No. 22165 GROUNDWATER ANALYTICAL RESULTS LIMITED SITE ASSESSMENT - OCTOBER 2000Scale:Date:AS SHOWNJANUARY 2014EA Project No.:FIGURE13-9678.12Contaminant ConcentrationMapJ. C. Penney Company, Inc.607 North Berkeley Blvd.Goldsboro, North Carolina 27534Wayne CountyApril 30, 201813127UST Incident No.:Figure 3N2315 Kings Road ExtensionShelby, North Carolina 28152(O) 704.482.2111(F) 704.482.4335Email: [e-mail] MONITORING WELLBlue Ridge Project No.:18-6057.10804016080 FeetJ. C. PenneyMW-2Berkeley MallLongHorn SteakhouseStarbucksNorth Berkeley Blvd.MONITORING WELLDUMPSTERMW-1MW-4MW-3DW-1Legend & NotesMW‐1B: <2.0T: <2.0E: 3.5X: <2.0Ace: 3.1Bis: 1.1F: 3.21MNP: 112MNP: 6.0N: 4.3P: 4.7DNBP: <0.62Pyr: 2.2C5‐C8: <15.0C9‐C12: 460C9‐C10: 210C9‐C18: 4,100C19‐C36: 1,100C11‐C22: 2,900DW‐1B: <0.40T: <0.40E: <0.40X: <0.40Ace: <0.11Bis: 1.0 JF: <0.0601MNP: <0.402MNP: <0.40N: <0.13P: <0.12DNBP: <0.26Pyr: 0.060C5‐C8: <15C9‐C12: <15C9‐C10: <5.0C9‐C18: <100C19‐C36: <100C11‐C22: <100Concentrations in RED exceed the NCGWQSug/L = micrograms per literJ: Estimated Result < Limit of Quantitation (LOQ) and > Detection Limit (DL)B:  Benzene (ug/L)T:  Toluene (ug/L)E: Ethylbenzene (ug/L)X: Xylenes (ug/L)Ace: Acenaphthene (ug/L)Bis: Bis(2‐ethylhexyl) (ug/L)F: Fluorene (ug/L)1MNP: 1‐Methylnaphthalene (ug/L)2MNP: 2‐Methylnaphthalene (ug/L)N: Naphthalene (ug/L)P: Phenanthrene (ug/L)DNBP: Di‐n‐butylphthalate (ug/L)Pyr: Pyrene (ug/L)C5‐C8: Aliphatics (ug/L)C9‐C12: Aliphatics (ug/L)C9‐C10: Aromatics (ug/L)C9‐C18: Aliphatics (ug/L)C19‐C36: Aliphatics (ug/L)C11‐C22: Aromatics (ug/L)Groundwater Samples collected April 5, 2018

APPENDICES

APPENDIX A

APPENDIX B
SHEALY ENVIRONMENTAL SERVICES,INC.
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc.
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Report of Analysis
Blue Ridge Environmental Services
2315 Kings Road Ext.
Shelby,NC 28152
Attention:Cliff Lundgren
Project Name:J.C.Penny Company,Inc.
Project Number:13127
Lot Number:TD09051
Date Completed:04/24/2018
04/24/2018 1:32 PM
Approved and released by:
Project Manager:Kelly M.Nance
Page 1 of 48
SHEALY ENVIRONMENTAL SERVICES,INC.
SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639
Shealy Environmental Services,Inc.
106 Vantage Point Drive West Columbia,SC 29172 [phone] Fax [phone] www.shealylab.com
Case Narrative
Blue Ridge Environmental Services
Lot Number:TD09051
This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary
following this Case Narrative.The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt,sample analysis,and data review have been performed in accordance with the most
current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality
Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any
exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or
discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Volatiles
Sample -001 was diluted due to the sample matrix.The reporting limits have been raised accordingly.
MADEP EPH
Sample -001 had the surrogates recovered outside of the acceptance limits due to confirmed matrix
interference.
MADEP VPH
Sample -001 had the surrogate recovered outside of the acceptance limits due to objective evidence of
matrix interference.
Sample -002 had the surrogate recovered above the acceptance limits.This reflects a high bias for
compounds associated with this surrogate.There were no detections for these compounds in the sample;
therefore,there is no impact on data quality and no corrective action is required.
Page 2 of 48
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Blue Ridge Environmental Services
Lot Number: TD09051

Sample Number Sample ID Matrix Date Sampled Date Received
001 04/05/2018 1422MW-1 Aqueous 04/09/2018
002 04/05/2018 1444DW-1 Aqueous 04/09/2018
(2 samples)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 3 of 48
SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Blue Ridge Environmental Services
Lot Number: TD09051

Sample Sample ID Matrix Parameter Method Result Q Units Page
001 MW-1 Aqueous Ethylbenzene 8260B 3.5 J ug/L 6
001 MW-1 Aqueous Unknown 625.1 32 ug/L 7
001 MW-1 Aqueous Naphthalene, 2,7-dimethyl-625.1 42 ug/L 7
001 MW-1 Aqueous Hexadecane, 2,6,10,14-625.1 32 ug/L 7
001 MW-1 Aqueous Unknown 625.1 37 ug/L 7
001 MW-1 Aqueous Hexadecane 625.1 58 ug/L 7
001 MW-1 Aqueous Naphthalene, 2,3,6-625.1 58 ug/L 7
001 MW-1 Aqueous Unknown 625.1 41 ug/L 7
001 MW-1 Aqueous 1,4,5,8-625.1 28 ug/L 7
001 MW-1 Aqueous Azulene, 7-ethyl-1,4-625.1 44 ug/L 7
001 MW-1 Aqueous 4,4'-Dimethylbiphenyl 625.1 22 ug/L 7
001 MW-1 Aqueous Unknown 625.1 21 ug/L 7
001 MW-1 Aqueous Eicosane 625.1 31 ug/L 7
001 MW-1 Aqueous Hexadecane, 2,6,10,14-625.1 34 ug/L 7
001 MW-1 Aqueous Unknown 625.1 31 ug/L 7
001 MW-1 Aqueous Unknown 625.1 26 ug/L 7
001 MW-1 Aqueous Nonadecane 625.1 23 ug/L 7
001 MW-1 Aqueous Unknown 625.1 24 ug/L 7
001 MW-1 Aqueous Heneicosane 625.1 23 ug/L 7
001 MW-1 Aqueous Metolachlor 625.1 30 ug/L 7
001 MW-1 Aqueous Octadec-9-enoic acid 625.1 20 ug/L 7
001 MW-1 Aqueous Acenaphthene 625.1 3.1 ug/L 8
001 MW-1 Aqueous bis(2-Ethylhexyl)phthalate 625.1 1.1 J ug/L 8
001 MW-1 Aqueous Fluorene 625.1 3.2 ug/L 8
001 MW-1 Aqueous 1-Methylnaphthalene 625.1 11 ug/L 8
001 MW-1 Aqueous 2-Methylnaphthalene 625.1 6.0 ug/L 9
001 MW-1 Aqueous Naphthalene 625.1 4.3 ug/L 9
001 MW-1 Aqueous Phenanthrene 625.1 4.7 ug/L 9
001 MW-1 Aqueous Pyrene 625.1 2.2 ug/L 9
001 MW-1 Aqueous C9 - C18 Aliphatics MADEP-EPH-4100 ug/L 10
001 MW-1 Aqueous C19 - C36 Aliphatics MADEP-EPH-1100 ug/L 10
001 MW-1 Aqueous C11 - C22 Aromatics MADEP-EPH-2900 ug/L 11
001 MW-1 Aqueous C9 - C12 Aliphatics MADEP-VPH-460 ug/L 12
001 MW-1 Aqueous C9 - C10 Aromatics MADEP-VPH-210 ug/L 13
002 DW-1 Aqueous Ethanol, 2-butoxy-625.1 20 ug/L 15
002 DW-1 Aqueous Cyclopentasiloxane, 625.1 5.3 ug/L 15
002 DW-1 Aqueous Butanoic acid, butyl ester 625.1 3.5 ug/L 15
002 DW-1 Aqueous 9-Octadecenoic acid, (E)-625.1 16 ug/L 15
002 DW-1 Aqueous bis(2-Ethylhexyl)phthalate 625.1 1.0 J ug/L 16
(39 detections)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 4 of 48
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 5 04/16/2018 0618 JJG 69560
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzene 71-43-2 8260B ND 1ug/L2.05.0
Chlorobenzene 108-90-7 8260B ND 1ug/L2.05.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L2.05.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L2.05.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L2.05.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L2.05.0
Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L2.05.0
Ethylbenzene 100-41-4 8260B 3.5 J 1ug/L2.05.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L2.05.0
Toluene 108-88-3 8260B ND 1ug/L2.05.0
Xylenes (total)1330-20-7 8260B ND 1ug/L2.05.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 105 70-130
Bromofluorobenzene 108 70-130
Toluene-d8 102 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 5 of 48
Library Search
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 04/16/2018 1957 CMP2 69652
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Unknown 625.1 32 1ug/L
Naphthalene, 2,7-dimethyl-625.1 42 1ug/L
Hexadecane, 2,6,10,14-tetramethyl-625.1 32 1ug/L
Unknown 625.1 37 1ug/L
Hexadecane 625.1 58 1ug/L
Naphthalene, 2,3,6-trimethyl-625.1 58 1ug/L
Unknown 625.1 41 1ug/L
1,4,5,8-Tetramethylnaphthalene 625.1 28 1ug/L
Azulene, 7-ethyl-1,4-dimethyl-625.1 44 1ug/L
4,4'-Dimethylbiphenyl 625.1 22 1ug/L
Unknown 625.1 21 1ug/L
Eicosane 625.1 31 1ug/L
Hexadecane, 2,6,10,14-tetramethyl-625.1 34 1ug/L
Unknown 625.1 31 1ug/L
Unknown 625.1 26 1ug/L
Nonadecane 625.1 23 1ug/L
Unknown 625.1 24 1ug/L
Heneicosane 625.1 23 1ug/L
Metolachlor 625.1 30 1ug/L
Octadec-9-enoic acid 625.1 20 1ug/L
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 6 of 48
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 04/16/2018 1957 CMP2 04/11/2018 1012 69222
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 625.1 3.1 1ug/L0.111.6
Acenaphthylene 208-96-8 625.1 ND 1ug/L0.0601.6
Anthracene 120-12-7 625.1 ND 1ug/L0.0601.6
Benzo(a)anthracene 56-55-3 625.1 ND 1ug/L0.0701.6
Benzo(a)pyrene 50-32-8 625.1 ND 1ug/L0.0401.6
Benzo(b)fluoranthene 205-99-2 625.1 ND 1ug/L0.0501.6
Benzo(g,h,i)perylene 191-24-2 625.1 ND 1ug/L0.121.6
Benzo(k)fluoranthene 207-08-9 625.1 ND 1ug/L0.0701.6
Benzyl alcohol 100-51-6 625.1 ND 1ug/L2.03.2
4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1ug/L0.161.6
Butyl benzyl phthalate 85-68-7 625.1 ND 1ug/L0.151.6
bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1ug/L0.491.6
4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1ug/L0.401.6
bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1ug/L0.481.6
bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1ug/L0.501.6
2-Chloronaphthalene 91-58-7 625.1 ND 1ug/L0.401.6
2-Chlorophenol 95-57-8 625.1 ND 1ug/L0.341.6
4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1ug/L0.211.6
Chrysene 218-01-9 625.1 ND 1ug/L0.0501.6
Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1ug/L0.111.6
Dibenzofuran 132-64-9 625.1 ND 1ug/L1.01.6
1,2-Dichlorobenzene 95-50-1 625.1 ND 1ug/L0.461.6
1,3-Dichlorobenzene 541-73-1 625.1 ND 1ug/L0.401.6
1,4-Dichlorobenzene 106-46-7 625.1 ND 1ug/L0.411.6
3,3'-Dichlorobenzidine 91-94-1 625.1 ND 1ug/L1.68.0
2,4-Dichlorophenol 120-83-2 625.1 ND 1ug/L0.701.6
Diethylphthalate 84-66-2 625.1 ND 1ug/L0.191.6
Dimethyl phthalate 131-11-3 625.1 ND 1ug/L0.211.6
2,4-Dimethylphenol 105-67-9 625.1 ND 1ug/L0.621.6
Di-n-butyl phthalate 84-74-2 625.1 ND 1ug/L0.261.6
4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 1ug/L0.698.0
2,4-Dinitrophenol 51-28-5 625.1 ND 1ug/L0.658.0
Di-n-octylphthalate 117-84-0 625.1 ND 1ug/L0.0701.6
1,2-Diphenylhydrazine(as azobenzene)103-33-3 625.1 ND 1ug/L0.121.6
bis(2-Ethylhexyl)phthalate 117-81-7 625.1 1.1 J 1ug/L0.191.6
Fluoranthene 206-44-0 625.1 ND 1ug/L0.0501.6
Fluorene 86-73-7 625.1 3.2 1ug/L0.0601.6
Hexachlorobenzene 118-74-1 625.1 ND 1ug/L0.391.6
Hexachlorobutadiene 87-68-3 625.1 ND 1ug/L0.471.6
Hexachlorocyclopentadiene 77-47-4 625.1 ND 1ug/L0.148.0
Hexachloroethane 67-72-1 625.1 ND 1ug/L0.531.6
Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1ug/L0.111.6
Isophorone 78-59-1 625.1 ND 1ug/L0.441.6
1-Methylnaphthalene 90-12-0 625.1 11 1ug/L0.401.6
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 7 of 48
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 04/16/2018 1957 CMP2 04/11/2018 1012 69222
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Methylnaphthalene 91-57-6 625.1 6.0 1ug/L0.401.6
2-Methylphenol 95-48-7 625.1 ND 1ug/L0.671.6
3+4-Methylphenol 106-44-5 625.1 ND 1ug/L1.51.6
Naphthalene 91-20-3 625.1 4.3 1ug/L0.131.6
Nitrobenzene 98-95-3 625.1 ND 1ug/L1.11.6
2-Nitrophenol 88-75-5 625.1 ND 1ug/L0.883.2
4-Nitrophenol 100-02-7 625.1 ND 1ug/L1.28.0
N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1ug/L0.151.6
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 625.1 ND 1ug/L0.251.6
Pentachlorophenol 87-86-5 625.1 ND 1ug/L1.48.0
Phenanthrene 85-01-8 625.1 4.7 1ug/L0.121.6
Phenol 108-95-2 625.1 ND 1ug/L0.221.6
Pyrene 129-00-0 625.1 2.2 1ug/L0.0601.6
1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1ug/L0.571.6
2,4,6-Trichlorophenol 88-06-2 625.1 ND 1ug/L0.441.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 66 37-129
2-Fluorophenol 39 24-127
Nitrobenzene-d5 65 38-127
Phenol-d5 53 28-128
Terphenyl-d14 51 10-148
2,4,6-Tribromophenol 100 41-144
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 8 of 48
MADEP EPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH-MADEP-EPH-04 1 04/20/2018 2130 PMS 04/12/2018 1619 69614
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C18 Aliphatics MADEP-EPH-4100 2ug/L100100
C19 - C36 Aliphatics MADEP-EPH-1100 2ug/L100100
AcceptanceRun 2
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)N 7.4 40-140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 9 of 48
MADEP EPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH-MADEP-EPH-04 1 04/20/2018 2329 PMS 04/12/2018 1619 69616
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C11 - C22 Aromatics MADEP-EPH-2900 2ug/L100100
AcceptanceRun 2
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic)N 22 40-140
2-Fluorobiphenyl (fractionation 1)88 40-140
2-Bromonaphthalene (fractionation 2)83 40-140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 10 of 48
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 04/13/2018 1954 JJG 69590
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C5 - C8 Aliphatics MADEP-VPH-ND 1ug/L1575
C9 - C12 Aliphatics MADEP-VPH-460 1ug/L1575
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)118 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 11 of 48
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
MW-1
TD09051-001
04/05/2018 1422
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 VPH MADEP-VPH-04-1.1 1 04/18/2018 1621 JJG 69831
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C10 Aromatics MADEP-VPH-210 2ug/L5.025
AcceptanceRun 2
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)N 61 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 12 of 48
Volatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 04/16/2018 0533 JJG 69560
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Benzene 71-43-2 8260B ND 1ug/L0.401.0
Chlorobenzene 108-90-7 8260B ND 1ug/L0.401.0
1,2-Dibromoethane (EDB)106-93-4 8260B ND 1ug/L0.401.0
1,2-Dichlorobenzene 95-50-1 8260B ND 1ug/L0.401.0
1,3-Dichlorobenzene 541-73-1 8260B ND 1ug/L0.401.0
1,4-Dichlorobenzene 106-46-7 8260B ND 1ug/L0.401.0
Diisopropyl ether (IPE)108-20-3 8260B ND 1ug/L0.401.0
Ethylbenzene 100-41-4 8260B ND 1ug/L0.401.0
Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 1ug/L0.401.0
Toluene 108-88-3 8260B ND 1ug/L0.401.0
Xylenes (total)1330-20-7 8260B ND 1ug/L0.401.0
AcceptanceRun 1
Surrogate Q % Recovery Limits
1,2-Dichloroethane-d4 103 70-130
Bromofluorobenzene 105 70-130
Toluene-d8 103 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 13 of 48
Library Search
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 04/16/2018 2022 CMP2 69652
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Ethanol, 2-butoxy-625.1 20 1ug/L
Cyclopentasiloxane, decamethyl-625.1 5.3 1ug/L
Butanoic acid, butyl ester 625.1 3.5 1ug/L
9-Octadecenoic acid, (E)-625.1 16 1ug/L
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 14 of 48
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 04/16/2018 2022 CMP2 04/11/2018 1012 69222
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
Acenaphthene 83-32-9 625.1 ND 1ug/L0.111.6
Acenaphthylene 208-96-8 625.1 ND 1ug/L0.0601.6
Anthracene 120-12-7 625.1 ND 1ug/L0.0601.6
Benzo(a)anthracene 56-55-3 625.1 ND 1ug/L0.0701.6
Benzo(a)pyrene 50-32-8 625.1 ND 1ug/L0.0401.6
Benzo(b)fluoranthene 205-99-2 625.1 ND 1ug/L0.0501.6
Benzo(g,h,i)perylene 191-24-2 625.1 ND 1ug/L0.121.6
Benzo(k)fluoranthene 207-08-9 625.1 ND 1ug/L0.0701.6
Benzyl alcohol 100-51-6 625.1 ND 1ug/L2.03.2
4-Bromophenyl phenyl ether 101-55-3 625.1 ND 1ug/L0.161.6
Butyl benzyl phthalate 85-68-7 625.1 ND 1ug/L0.151.6
bis (2-Chloro-1-methylethyl) ether 108-60-1 625.1 ND 1ug/L0.491.6
4-Chloro-3-methyl phenol 59-50-7 625.1 ND 1ug/L0.401.6
bis(2-Chloroethoxy)methane 111-91-1 625.1 ND 1ug/L0.481.6
bis(2-Chloroethyl)ether 111-44-4 625.1 ND 1ug/L0.501.6
2-Chloronaphthalene 91-58-7 625.1 ND 1ug/L0.401.6
2-Chlorophenol 95-57-8 625.1 ND 1ug/L0.341.6
4-Chlorophenyl phenyl ether 7005-72-3 625.1 ND 1ug/L0.211.6
Chrysene 218-01-9 625.1 ND 1ug/L0.0501.6
Dibenzo(a,h)anthracene 53-70-3 625.1 ND 1ug/L0.111.6
Dibenzofuran 132-64-9 625.1 ND 1ug/L1.01.6
1,2-Dichlorobenzene 95-50-1 625.1 ND 1ug/L0.461.6
1,3-Dichlorobenzene 541-73-1 625.1 ND 1ug/L0.401.6
1,4-Dichlorobenzene 106-46-7 625.1 ND 1ug/L0.411.6
3,3'-Dichlorobenzidine 91-94-1 625.1 ND 1ug/L1.68.0
2,4-Dichlorophenol 120-83-2 625.1 ND 1ug/L0.701.6
Diethylphthalate 84-66-2 625.1 ND 1ug/L0.191.6
Dimethyl phthalate 131-11-3 625.1 ND 1ug/L0.211.6
2,4-Dimethylphenol 105-67-9 625.1 ND 1ug/L0.621.6
Di-n-butyl phthalate 84-74-2 625.1 ND 1ug/L0.261.6
4,6-Dinitro-2-methylphenol 534-52-1 625.1 ND 1ug/L0.698.0
2,4-Dinitrophenol 51-28-5 625.1 ND 1ug/L0.658.0
Di-n-octylphthalate 117-84-0 625.1 ND 1ug/L0.0701.6
1,2-Diphenylhydrazine(as azobenzene)103-33-3 625.1 ND 1ug/L0.121.6
bis(2-Ethylhexyl)phthalate 117-81-7 625.1 1.0 J 1ug/L0.191.6
Fluoranthene 206-44-0 625.1 ND 1ug/L0.0501.6
Fluorene 86-73-7 625.1 ND 1ug/L0.0601.6
Hexachlorobenzene 118-74-1 625.1 ND 1ug/L0.391.6
Hexachlorobutadiene 87-68-3 625.1 ND 1ug/L0.471.6
Hexachlorocyclopentadiene 77-47-4 625.1 ND 1ug/L0.148.0
Hexachloroethane 67-72-1 625.1 ND 1ug/L0.531.6
Indeno(1,2,3-c,d)pyrene 193-39-5 625.1 ND 1ug/L0.111.6
Isophorone 78-59-1 625.1 ND 1ug/L0.441.6
1-Methylnaphthalene 90-12-0 625.1 ND 1ug/L0.401.6
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 15 of 48
Semivolatile Organic Compounds by GC/MS
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 625.1 625.1 1 04/16/2018 2022 CMP2 04/11/2018 1012 69222
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
2-Methylnaphthalene 91-57-6 625.1 ND 1ug/L0.401.6
2-Methylphenol 95-48-7 625.1 ND 1ug/L0.671.6
3+4-Methylphenol 106-44-5 625.1 ND 1ug/L1.51.6
Naphthalene 91-20-3 625.1 ND 1ug/L0.131.6
Nitrobenzene 98-95-3 625.1 ND 1ug/L1.11.6
2-Nitrophenol 88-75-5 625.1 ND 1ug/L0.883.2
4-Nitrophenol 100-02-7 625.1 ND 1ug/L1.28.0
N-Nitrosodi-n-propylamine 621-64-7 625.1 ND 1ug/L0.151.6
N-Nitrosodiphenylamine (Diphenylamine)86-30-6 625.1 ND 1ug/L0.251.6
Pentachlorophenol 87-86-5 625.1 ND 1ug/L1.48.0
Phenanthrene 85-01-8 625.1 ND 1ug/L0.121.6
Phenol 108-95-2 625.1 ND 1ug/L0.221.6
Pyrene 129-00-0 625.1 ND 1ug/L0.0601.6
1,2,4-Trichlorobenzene 120-82-1 625.1 ND 1ug/L0.571.6
2,4,6-Trichlorophenol 88-06-2 625.1 ND 1ug/L0.441.6
AcceptanceRun 1
Surrogate Q % Recovery Limits
2-Fluorobiphenyl 69 37-129
2-Fluorophenol 50 24-127
Nitrobenzene-d5 82 38-127
Phenol-d5 58 28-128
Terphenyl-d14 100 10-148
2,4,6-Tribromophenol 72 41-144
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 16 of 48
MADEP EPH (aliphatics) - Unfractionated
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH-MADEP-EPH-04 1 04/16/2018 1951 PMS 04/12/2018 1619 69617
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C19 - C36 Aliphatics - Unfractionated MADEP-EPH-04 ND 2ug/L100100
C9 - C18 Aliphatics - Unfractionated MADEP-EPH-04 ND 2ug/L100100
AcceptanceRun 2
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) - Unfractionated 50 40-140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 17 of 48
MADEP EPH (aromatics) - Unfractionated
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH-MADEP-EPH-04 1 04/16/2018 1951 PMS 04/12/2018 1619 69618
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C11 - C22 Aromatics - Unfractionated MADEP-EPH-04 ND 2ug/L100100
AcceptanceRun 2
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) - Unfractionated 55 40-140
2-Fluorobiphenyl (fractionation 1)69 40-140
2-Bromonaphthalene (fractionation 2)70 40-140
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 18 of 48
MADEP VPH (aliphatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-04-1.1 1 04/13/2018 2022 JJG 69590
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C5 - C8 Aliphatics MADEP-VPH-ND 1ug/L1575
C9 - C12 Aliphatics MADEP-VPH-ND 1ug/L1575
AcceptanceRun 1
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)N 142 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 19 of 48
MADEP VPH (aromatics)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Blue Ridge Environmental Services
DW-1
TD09051-002
04/05/2018 1444
04/09/2018
Aqueous
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 VPH MADEP-VPH-04-1.1 1 04/18/2018 1552 JJG 69831
AnalyticalCAS
Parameter Number Method Result Q LOQ Units Run DL
C9 - C10 Aromatics MADEP-VPH-ND 2ug/L5.025
AcceptanceRun 2
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)95 70-130
J = Estimated result < LOQ and > DL_
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria
H = Out of holding time
DL = Detection Limit
W = Reported on wet weight basis
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 20 of 48
QC Summary
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 21 of 48
Volatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Sample ID:TQ69560-001
69560 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Benzene ND 04/15/2018 22501.0 0.40 ug/L1
Chlorobenzene ND 04/15/2018 22501.0 0.40 ug/L1
1,2-Dibromoethane (EDB)ND 04/15/2018 22501.0 0.40 ug/L1
1,2-Dichlorobenzene ND 04/15/2018 22501.0 0.40 ug/L1
1,3-Dichlorobenzene ND 04/15/2018 22501.0 0.40 ug/L1
1,4-Dichlorobenzene ND 04/15/2018 22501.0 0.40 ug/L1
Diisopropyl ether (IPE)ND 04/15/2018 22501.0 0.40 ug/L1
Ethylbenzene ND 04/15/2018 22501.0 0.40 ug/L1
Methyl tertiary butyl ether (MTBE)ND 04/15/2018 22501.0 0.40 ug/L1
Toluene ND 04/15/2018 22501.0 0.40 ug/L1
Xylenes (total)ND 04/15/2018 22501.0 0.40 ug/L1
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 105 70-130
Bromofluorobenzene 105 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 22 of 48
Volatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Sample ID:TQ69560-002
69560 5030B
Analytical Method:8260B
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Benzene 49 04/15/2018 2204985070-1301
Chlorobenzene 52 04/15/2018 22041035070-1301
1,2-Dibromoethane (EDB)52 04/15/2018 22041035070-1301
1,2-Dichlorobenzene 55 04/15/2018 22041095070-1301
1,3-Dichlorobenzene 49 04/15/2018 2204995070-1301
1,4-Dichlorobenzene 47 04/15/2018 2204945070-1301
Diisopropyl ether (IPE)48 04/15/2018 2204965070-1301
Ethylbenzene 50 04/15/2018 22041005070-1301
Methyl tertiary butyl ether (MTBE)48 04/15/2018 2204955070-1301
Toluene 51 04/15/2018 22041035070-1301
Xylenes (total)100 04/15/2018 220410210070-1301
Surrogate Q % Rec
Acceptance
Limit
1,2-Dichloroethane-d4 101 70-130
Bromofluorobenzene 101 70-130
Toluene-d8 103 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 23 of 48
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ69222-001
69222 625.1
04/11/2018 1012Analytical Method:625.1
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
Acenaphthene ND 04/16/2018 11071.6 0.11 ug/L1
Acenaphthylene ND 04/16/2018 11071.6 0.060 ug/L1
Anthracene ND 04/16/2018 11071.6 0.060 ug/L1
Benzo(a)anthracene ND 04/16/2018 11071.6 0.070 ug/L1
Benzo(a)pyrene ND 04/16/2018 11071.6 0.040 ug/L1
Benzo(b)fluoranthene ND 04/16/2018 11071.6 0.050 ug/L1
Benzo(g,h,i)perylene ND 04/16/2018 11071.6 0.12 ug/L1
Benzo(k)fluoranthene ND 04/16/2018 11071.6 0.070 ug/L1
Benzyl alcohol ND 04/16/2018 11073.2 2.0 ug/L1
4-Bromophenyl phenyl ether ND 04/16/2018 11071.6 0.16 ug/L1
Butyl benzyl phthalate ND 04/16/2018 11071.6 0.15 ug/L1
bis (2-Chloro-1-methylethyl) ether ND 04/16/2018 11071.6 0.49 ug/L1
4-Chloro-3-methyl phenol ND 04/16/2018 11071.6 0.40 ug/L1
bis(2-Chloroethoxy)methane ND 04/16/2018 11071.6 0.48 ug/L1
bis(2-Chloroethyl)ether ND 04/16/2018 11071.6 0.50 ug/L1
2-Chloronaphthalene ND 04/16/2018 11071.6 0.40 ug/L1
2-Chlorophenol ND 04/16/2018 11071.6 0.34 ug/L1
4-Chlorophenyl phenyl ether ND 04/16/2018 11071.6 0.21 ug/L1
Chrysene ND 04/16/2018 11071.6 0.050 ug/L1
Dibenzo(a,h)anthracene ND 04/16/2018 11071.6 0.11 ug/L1
Dibenzofuran ND 04/16/2018 11071.6 1.0 ug/L1
1,2-Dichlorobenzene ND 04/16/2018 11071.6 0.46 ug/L1
1,3-Dichlorobenzene ND 04/16/2018 11071.6 0.40 ug/L1
1,4-Dichlorobenzene ND 04/16/2018 11071.6 0.41 ug/L1
3,3'-Dichlorobenzidine ND 04/16/2018 11078.0 1.6 ug/L1
2,4-Dichlorophenol ND 04/16/2018 11071.6 0.70 ug/L1
Diethylphthalate ND 04/16/2018 11071.6 0.19 ug/L1
Dimethyl phthalate ND 04/16/2018 11071.6 0.21 ug/L1
2,4-Dimethylphenol ND 04/16/2018 11071.6 0.62 ug/L1
Di-n-butyl phthalate ND 04/16/2018 11071.6 0.26 ug/L1
4,6-Dinitro-2-methylphenol ND 04/16/2018 11078.0 0.69 ug/L1
2,4-Dinitrophenol ND 04/16/2018 11078.0 0.65 ug/L1
Di-n-octylphthalate ND 04/16/2018 11071.6 0.070 ug/L1
1,2-Diphenylhydrazine(as azobenzene)ND 04/16/2018 11071.6 0.12 ug/L1
bis(2-Ethylhexyl)phthalate ND 04/16/2018 11071.6 0.19 ug/L1
Fluoranthene ND 04/16/2018 11071.6 0.050 ug/L1
Fluorene ND 04/16/2018 11071.6 0.060 ug/L1
Hexachlorobenzene ND 04/16/2018 11071.6 0.39 ug/L1
Hexachlorobutadiene ND 04/16/2018 11071.6 0.47 ug/L1
Hexachlorocyclopentadiene ND 04/16/2018 11078.0 0.14 ug/L1
Hexachloroethane ND 04/16/2018 11071.6 0.53 ug/L1
Indeno(1,2,3-c,d)pyrene ND 04/16/2018 11071.6 0.11 ug/L1
Isophorone ND 04/16/2018 11071.6 0.44 ug/L1
1-Methylnaphthalene ND 04/16/2018 11071.6 0.40 ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 24 of 48
Semivolatile Organic Compounds by GC/MS - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ69222-001
69222 625.1
04/11/2018 1012Analytical Method:625.1
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
2-Methylnaphthalene ND 04/16/2018 11071.6 0.40 ug/L1
2-Methylphenol ND 04/16/2018 11071.6 0.67 ug/L1
3+4-Methylphenol ND 04/16/2018 11071.6 1.5 ug/L1
Naphthalene ND 04/16/2018 11071.6 0.13 ug/L1
Nitrobenzene ND 04/16/2018 11071.6 1.1 ug/L1
2-Nitrophenol ND 04/16/2018 11073.2 0.88 ug/L1
4-Nitrophenol ND 04/16/2018 11078.0 1.2 ug/L1
N-Nitrosodi-n-propylamine ND 04/16/2018 11071.6 0.15 ug/L1
N-Nitrosodiphenylamine (Diphenylamine)ND 04/16/2018 11071.6 0.25 ug/L1
Pentachlorophenol ND 04/16/2018 11078.0 1.4 ug/L1
Phenanthrene ND 04/16/2018 11071.6 0.12 ug/L1
Phenol ND 04/16/2018 11071.6 0.22 ug/L1
Pyrene ND 04/16/2018 11071.6 0.060 ug/L1
1,2,4-Trichlorobenzene ND 04/16/2018 11071.6 0.57 ug/L1
2,4,6-Trichlorophenol ND 04/16/2018 11071.6 0.44 ug/L1
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 69 37-129
2-Fluorophenol 53 24-127
Nitrobenzene-d5 80 38-127
Phenol-d5 63 28-128
Terphenyl-d14 113 10-148
2,4,6-Tribromophenol 64 41-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 25 of 48
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ69222-002
69222 625.1
04/11/2018 1012Analytical Method:625.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Acenaphthene 14 04/16/2018 1131702047-1451
Acenaphthylene 14 04/16/2018 1131682033-1451
Anthracene 16 04/16/2018 1131792027-1331
Benzo(a)anthracene 17 04/16/2018 1131872033-1431
Benzo(a)pyrene 17 04/16/2018 1131832017-1631
Benzo(b)fluoranthene 20 04/16/2018 1131992024-1591
Benzo(g,h,i)perylene 17 04/16/2018 113186201-2191
Benzo(k)fluoranthene 17 04/16/2018 1131872011-1621
Benzyl alcohol 17 04/16/2018 1131862030-1301
4-Bromophenyl phenyl ether 15 04/16/2018 1131732053-1271
Butyl benzyl phthalate 19 04/16/2018 113196201-1521
bis (2-Chloro-1-methylethyl) ether 15 04/16/2018 1131762036-1661
4-Chloro-3-methyl phenol 15 04/16/2018 1131752022-1471
bis(2-Chloroethoxy)methane 14 04/16/2018 1131702033-1841
bis(2-Chloroethyl)ether 15 04/16/2018 1131752012-1581
2-Chloronaphthalene 13 04/16/2018 1131642060-1201
2-Chlorophenol 12 04/16/2018 1131612023-1341
4-Chlorophenyl phenyl ether 14 04/16/2018 1131682025-1581
Chrysene 17 04/16/2018 1131842017-1681
Dibenzo(a,h)anthracene 18 04/16/2018 113189201-2271
Dibenzofuran 13 04/16/2018 1131672048-1181
1,2-Dichlorobenzene 13 04/16/2018 1131652032-1291
1,3-Dichlorobenzene 12 04/16/2018 113161201-1721
1,4-Dichlorobenzene 12 04/16/2018 1131612020-1241
3,3'-Dichlorobenzidine 1.3 04/16/2018 11316.720 1-2621
2,4-Dichlorophenol 13 04/16/2018 1131632039-1351
Diethylphthalate 16 04/16/2018 113181201-1201
Dimethyl phthalate 15 04/16/2018 113174201-1201
2,4-Dimethylphenol 13 04/16/2018 1131672032-1201
Di-n-butyl phthalate 18 04/16/2018 113189201-1201
4,6-Dinitro-2-methylphenol 15 04/16/2018 113174201-1811
2,4-Dinitrophenol 25 04/16/2018 113163401-1911
Di-n-octylphthalate 16 04/16/2018 113181204-1461
1,2-Diphenylhydrazine(as azobenzene)15 04/16/2018 113177201-1501
bis(2-Ethylhexyl)phthalate 17 04/16/2018 113187208-1581
Fluoranthene 17 04/16/2018 1131852026-1371
Fluorene 15 04/16/2018 1131742059-1211
Hexachlorobenzene 16 04/16/2018 113178201-1521
Hexachlorobutadiene 12 04/16/2018 1131602024-1201
Hexachlorocyclopentadiene 36 04/16/2018 1131361001-1501
Hexachloroethane 12 04/16/2018 1131612040-1201
Indeno(1,2,3-c,d)pyrene 17 04/16/2018 113186201-1711
Isophorone 15 04/16/2018 1131752021-1961
1-Methylnaphthalene 13 04/16/2018 1131662042-1261
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 26 of 48
Semivolatile Organic Compounds by GC/MS - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ69222-002
69222 625.1
04/11/2018 1012Analytical Method:625.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
2-Methylnaphthalene 13 04/16/2018 1131672040-1321
2-Methylphenol 16 04/16/2018 1131782030-1301
3+4-Methylphenol 15 04/16/2018 1131752030-1301
Naphthalene 13 04/16/2018 1131662021-1331
Nitrobenzene 15 04/16/2018 1131742035-1801
2-Nitrophenol 13 04/16/2018 1131662029-1821
4-Nitrophenol 34 04/16/2018 113184401-1321
N-Nitrosodi-n-propylamine 17 04/16/2018 113183201-2301
N-Nitrosodiphenylamine (Diphenylamine)12 04/16/2018 113160201-1501
Pentachlorophenol 28 04/16/2018 1131704014-1761
Phenanthrene 15 04/16/2018 1131762054-1201
Phenol 13 04/16/2018 113163205-1201
Pyrene 18 04/16/2018 1131922052-1201
1,2,4-Trichlorobenzene 13 04/16/2018 1131632044-1421
2,4,6-Trichlorophenol 14 04/16/2018 1131692037-1441
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 69 37-129
2-Fluorophenol 46 24-127
Nitrobenzene-d5 81 38-127
Phenol-d5 66 28-128
Terphenyl-d14 98 10-148
2,4,6-Tribromophenol 74 41-144
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 27 of 48
MADEP EPH (aliphatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ69614-001
69614 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C9 - C18 Aliphatics ND 04/20/2018 2001100100ug/L1
C19 - C36 Aliphatics ND 04/20/2018 2001100100ug/L1
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)52 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 28 of 48
MADEP EPH (aliphatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ69614-002
69614 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C9 - C18 Aliphatics 120 04/20/2018 20314130040-1401
C19 - C36 Aliphatics 270 04/20/2018 20316840040-1401
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)63 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 29 of 48
MADEP EPH (aliphatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:TQ69614-003
69614 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C9 - C18 Aliphatics 130 04/20/2018 21014330040-1405.8 251
C19 - C36 Aliphatics 280 04/20/2018 21017140040-1403.5 251
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic)64 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 30 of 48
MADEP EPH (aromatics) - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ69616-001
69616 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C11 - C22 Aromatics ND 04/20/2018 2200100100ug/L1
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic)66 40-140
2-Fluorobiphenyl (fractionation 1)65 40-140
2-Bromonaphthalene (fractionation 2)71 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 31 of 48
MADEP EPH (aromatics) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ69616-002
69616 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C11 - C22 Aromatics 570 04/20/2018 22296785040-1401
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic)67 40-140
2-Fluorobiphenyl (fractionation 1)69 40-140
2-Bromonaphthalene (fractionation 2)57 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 32 of 48
MADEP EPH (aromatics) - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:TQ69616-003
69616 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C11 - C22 Aromatics 580 04/20/2018 22596885040-1401.7 251
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic)67 40-140
2-Fluorobiphenyl (fractionation 1)73 40-140
2-Bromonaphthalene (fractionation 2)65 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 33 of 48
MADEP EPH (aliphatics) - Unfractionated - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ69617-001
69617 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C19 - C36 Aliphatics - Unfractionated ND 04/16/2018 1822100100ug/L1
C9 - C18 Aliphatics - Unfractionated ND 04/16/2018 1822100100ug/L1
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 70 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 34 of 48
MADEP EPH (aliphatics) - Unfractionated - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ69617-002
69617 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C19 - C36 Aliphatics - Unfractionated 710 04/16/2018 18527890040-1401
C9 - C18 Aliphatics - Unfractionated 370 04/16/2018 18525665040-1401
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 74 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 35 of 48
MADEP EPH (aliphatics) - Unfractionated - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:TQ69617-003
69617 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C19 - C36 Aliphatics - Unfractionated 690 04/16/2018 19227790040-1402.0 251
C9 - C18 Aliphatics - Unfractionated 370 04/16/2018 19225765040-1400.58 251
Surrogate Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) - Unfractionated 74 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 36 of 48
MADEP EPH (aromatics) - Unfractionated - MB
Batch:Prep Method:
Prep Date:
Sample ID:TQ69618-001
69618 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C11 - C22 Aromatics - Unfractionated ND 04/16/2018 1822100100ug/L1
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) - Unfractionated 59 40-140
2-Fluorobiphenyl (fractionation 1)70 40-140
2-Bromonaphthalene (fractionation 2)71 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 37 of 48
MADEP EPH (aromatics) - Unfractionated - LCS
Batch:Prep Method:
Prep Date:
Sample ID:TQ69618-002
69618 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C11 - C22 Aromatics - Unfractionated 770 04/16/2018 185255140040-1401
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) - Unfractionated 58 40-140
2-Fluorobiphenyl (fractionation 1)69 40-140
2-Bromonaphthalene (fractionation 2)66 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 38 of 48
MADEP EPH (aromatics) - Unfractionated - LCSD
Batch:Prep Method:
Prep Date:
Sample ID:TQ69618-003
69618 MADEP-EPH-04
04/12/2018 1619Analytical Method:MADEP-EPH-04
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C11 - C22 Aromatics - Unfractionated 760 04/16/2018 192254140040-1400.91 251
Surrogate Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) - Unfractionated 58 40-140
2-Fluorobiphenyl (fractionation 1)72 40-140
2-Bromonaphthalene (fractionation 2)69 40-140
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 39 of 48
MADEP VPH (aliphatics) - MB
Batch:Prep Method:
Sample ID:TQ69590-001
69590 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C5 - C8 Aliphatics ND 04/13/2018 19257515ug/L1
C9 - C12 Aliphatics ND 04/13/2018 19257515ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)128 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 40 of 48
MADEP VPH (aliphatics) - LCS
Batch:Prep Method:
Sample ID:TQ69590-002
69590 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 130 04/13/2018 18288715070-1301
C9 - C12 Aliphatics 180 04/13/2018 182810018070-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)117 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 41 of 48
MADEP VPH (aliphatics) - LCSD
Batch:Prep Method:
Sample ID:TQ69590-003
69590 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C5 - C8 Aliphatics 130 04/13/2018 18578715070-1300.77 251
C9 - C12 Aliphatics 170 04/13/2018 18579918070-1300.92 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID)121 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 42 of 48
MADEP VPH (aromatics) - MB
Batch:Prep Method:
Sample ID:TQ69831-001
69831 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter Result Q LOQ DL Units Analysis DateDil
C9 - C10 Aromatics ND 04/18/2018 1453255.0 ug/L1
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)102 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 43 of 48
MADEP VPH (aromatics) - LCS
Batch:Prep Method:
Sample ID:TQ69831-002
69831 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 28 04/18/2018 13561112570-1301
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)114 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 44 of 48
MADEP VPH (aromatics) - LCSD
Batch:Prep Method:
Sample ID:TQ69831-003
69831 VPH
Analytical Method:MADEP-VPH-04-1.1
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
C9 - C10 Aromatics 29 04/18/2018 14251162570-1304.2 251
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (PID)108 70-130
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
LOQ = Limit of Quantitation
ND = Not detected at or above the DL
J = Estimated result < LOQ and > DL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_DL = Detection Limit
LOD = Limit of Detection
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 45 of 48
Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 46 of 48
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 47 of 48
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 48 of 48