WA-1016_12613_CA_RPTS_20150424_MRP

EXECUTIVE SUMMARY

The former Phelps Amoco site is located along US Highway 64 West, west of the Town of Creswell,
Washington County, North Carolina. The adjoining properties are agricultural and residential. Municipal
water is available to the surrounding properties. The risk classification is currently ranked as intermediate
due to the historical presence of free product and ground water contamination exceeding the gross
contamination level (GCL) for benzene.

Two Type II monitoring wells were installed at the site on February 24, 2015 to delineate the extent of the
contaminant plume. On April 1, 2015, seven Type II monitoring wells were gauged, purged and sampled.
Ground water flow direction was convergent at the site. Concentrations of requested method constituents
that exceeded the maximum allowable concentrations were reported in the ground water samples
collected from MW-14 and MW-21. The concentrations of benzene reported in the ground water samples
collected from MW-14 and MW-21 exceeded the GCL. Absorbent booms were replaced in MW-14 and
MW-21 upon the completion of the April 2015 sampling event.

Based on this information, the contaminant plume has been adequately defined. GRI recommends that
additional aggressive fluid vapor recovery (AFVR) events should be conducted in order to reduce
contamination levels in MW-14 and MW-21. The AFVR event(s) should be enhanced with the
installation of a recovery well between MW-14 and MW-21. Absorbent boom maintenance for MW-14
and MW-21 should continue until the next sampling event. Semi-annual ground water monitoring should
continue at the site. The next ground water monitoring event is tentatively scheduled for October 2015.

TABLE OF CONTENTS

1.0 SITE HISTORY AND CHARACTERIZATION .................................................................... 1
2.0 CURRENT SITE ACTIVITIES ............................................................................................... 1
3.0 MONITORING WELL INSTALLATION .............................................................................. 2
4.0 GROUND WATER QUALITY ................................................................................................ 2
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................................... 3
6.0 LIMITATIONS ......................................................................................................................... 3
FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Water Table Surface Map
Figure 4: Ground Water Quality Map

TABLES
Table 1: Well Construction Information
Table 2: Summary of Ground Water Sample Analytical Results

APPENDICES
Appendix A: Monitoring Well Permit, DOT Encroachment Agreement and Well Construction Records
Appendix B: Laboratory Report - Ground Water Samples

1
1.0 SITE HISTORY AND CHARACTERIZATION
The site is a former convenience store and petroleum retail facility. Soil and ground water assessment
activities commenced at the site in response to a release reported in May 1994 during the closure of three
4,000-gallon gasoline and one 1,000-gallon diesel USTs. A new UST system consisting of one 6,000-
gallon gasoline, two 4,000-gallon gasoline, one 1,000-gallon diesel and one 1,000-gallon kerosene USTs
was installed in the former UST basin in July 1994. A Corrective Action Plan (CAP) for the site
developed by TRC Triangle (TRC) proposed remediation using soil excavation followed by natural
attenuation and water supply well abandonment. The proposed remediation method was designed to
accommodate the North Carolina Department of Transportation (NCDOT) plans to raze the facility and
construct a new US Highway 64 over the site. As part of the Corrective Action Plan, the UST system
installed in July 1994, associated pumps and product piping, as well as 3,909.89 tons of contaminated soil
were removed from the site in March and April 2002 by Coastal Environmental Services, Inc. (CES).

Eleven Type II monitoring wells (MW-1 through MW-3 and MW-5 through MW-8 and MW-10 through
MW-13) and two Type III monitoring wells (MWD-4 and MWD-9) were installed at the site during
previous ground water assessment activities. Prior to excavation activities, CES abandoned monitoring
wells MW-1 through MW-5, MW-7, MW-8, MW-9, MW-12 and water supply well DW-1. Monitoring
wells MW-10 and MW-11 and water supply wells DW-2 and DW-3 were reportedly destroyed by the
NCDOT and therefore were not properly abandoned. Nine additional Type II monitoring wells (MW-14
through MW-22) were installed by Geological Resources, Inc. (GRI) to replace monitoring wells
abandoned and/or destroyed during CAP implementation activities and NCDOT construction in 2002.

Assessment activities conducted prior to the July 2008 updated receptor survey were conducted by past
consultants. Although GRI cannot verify the accuracy of information obtained from previous reports, for
the purposes of this report, it is assumed to be correct.

2.0 CURRENT SITE ACTIVITIES
The purpose of this report is to present the results of the ground water assessment activities conducted
between February and April 2015, at the former Phelps Amoco site located along US Highway 64 West,
west of the Town of Creswell, Washington County, North Carolina (Figure 1). The activities were
conducted in accordance with GRI proposal number 14-677 which was submitted to NCDENR on
November 17, 2014 and approved as Task Authorization No. 12613-24 on January 22, 2015. The

2
purpose of the activities was to further define the contaminant plume and to obtain current ground water
quality data for the site.

3.0 MONITORING WELL INSTALLATION
On February 24, 2015, two Type II monitoring wells (MW-23 and MW-24) were to total depths 12 feet
each and were completed with 10-foot screened intervals set to bracket the water table at the time of
installation. Top of casing elevations for the newly installed monitoring wells were measured on
February 24, 2015. A Site Map showing the locations of the monitoring wells and the former site
structures has been included as Figure 2. A summary of well construction information including ground
water elevation data is presented in Table 1. Copies of the monitoring well permit, DOT encroachment
agreement and well construction records are included as Appendix A.
4.0 GROUND WATER QUALITY
Seven Type II monitoring wells (MW-6, MW-14, MW-15 and MW-21 through MW-24) were gauged,
purged and sampled on April 1, 2015. No free product was observed during the April 2015 sampling
event. The depths to ground water in the Type II monitoring wells during the April 2015 sampling event
ranged from 1.30 to 2.57 feet below the top of well casings. Ground water elevations in the Type II
monitoring wells relative to a temporary benchmark assumed by the previous consultant ranged from
97.32 to 97.55 feet. Based on this information, ground water flow direction is generally convergent in the
vicinity of the former dispenser island with an average horizontal hydraulic gradient of less than 0.01 feet
per foot. A Water Table Surface Map for the April 2015 sampling event has been included as Figure 3.
A summary of well construction information including ground water elevation data is presented in Table
1.

Laboratory analyses were performed on the ground water samples collected from the monitoring wells
during the April 2015 sampling event for volatile organic compounds (VOCs) using EPA Method 6200B.

Concentrations of one or more BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, n-
propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the maximum
allowable concentrations (MACs) specified in T15A NCAC 2L.0202 were reported in the ground water
samples collected from MW-14 and MW-21. The concentrations of benzene reported in the ground water
samples collected from MW-14 and MW-21 exceeded the gross contamination level (GCL). A Ground
Water Quality Map based on data from the April 1, 2015 sampling event has been included as Figure 4.
A summary of ground water sample analytical results is presented in Table 2. A complete laboratory

3
report has been included as Appendix B. Upon completion of the April 2015 sampling event, absorbent
booms were replaced in MW-14 and MW-21.

5.0 CONCLUSIONS AND RECOMMENDATIONS
 Two Type II monitoring wells were installed at the site on February 24, 2015 to delineate the
extent of the contaminant plume.
 The average depth to water during the April 2015 sampling event was 2.01 feet. Ground water
flow in the vicinity of the former dispenser was generally convergent at the site with an average
horizontal hydraulic gradient of less than 0.01 feet per foot.
 Concentrations of one or more BTEX constituents, MTBE, naphthalene, 1,2-dichloroethane, n-
propylbenzene, 1,2,4-trimethylbenzene and/or 1,3,5-trimethylbenzene that exceeded the MACs
were reported in the ground water samples collected from MW-14 and MW-21. The
concentrations of benzene reported in the ground water samples collected from MW-14 and MW-
21 exceeded the GCL.
 Absorbent booms were re-installed in MW-14 and MW-21 following the completion of the April
2015 sampling event.
 Based on this information, the GCL contaminant plume has been adequately defined. GRI
recommends that boom maintenance at the site should continue during the next semi-annual
ground water monitoring event. Additional AFVR events should be conducted to reduce
contaminant concentrations to below GCLs. The AFVR event(s) should be enhanced with the
installation of a recovery well between MW-14 and MW-21. Semi-annual ground water
monitoring should continue at the site. The next semi-annual sampling event is tentatively
scheduled for October 2015.

6.0 LIMITATIONS
This report has been prepared for the exclusive use of North East Oil Company, Inc. for specific
application to the referenced site in Washington County, North Carolina. The assessment was conducted
based on the scope of work and level of effort specified by NCDENR and with resources adequate only
for that scope of work. Our findings have been developed in accordance with generally accepted
standards of geology and hydrogeology practices in the State of North Carolina, available information,
and our professional judgment. No other warranty is expressed or implied.

4
The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No
additional information can logically be inferred from these data. Please note that field data collected prior
to the July 2008 update receptor survey and November 2008 sampling event was not obtained under the
supervision of GRI. Although the accuracy of this information cannot be verified, for the purpose of this
report, GRI assumes that it is correct.

FIGURES

TABLES
11/11/08 7.26 0.00 92.51
06/02/09 6.21 0.00 93.56
06/08/11 6.42 0.00 93.35
06/12/12 4.12 0.00 95.65
05/07/13 3.96 0.00 95.81
10/03/13 5.28 0.00 94.49
09/11/14 2.46 0.00 97.31
04/01/15 2.41 0.00 97.36
MW-10 02/13/98 NA 1 1 - 11 11 99.10 NM NM NM Destroyed
MW-11 02/11/98 NA 1 1 - 11 11 98.72 NM NM NM Destroyed
MW-13 07/22/98 NA 3 3 - 8 8 98.32 NM NM NM Not Located
11/11/08 7.13 0.00 92.53
06/02/09 9.03 0.00 90.63
06/08/11 6.33 0.03 93.36
11/17/11 3.91 0.00 95.75
06/12/12 4.06 0.00 95.60
04/03/13 3.46 0.00 96.20 Before AFVR
04/03/13 4.80 0.00 94.86 After AFVR
05/07/13 3.80 0.00 95.86
10/03/13 5.21 0.00 94.45
07/23/14 4.44 0.00 95.22 Before AFVR
07/23/14 5.35 0.00 94.31 After AFVR
09/11/14 2.46 0.00 97.20
04/01/15 2.31 0.00 97.35
11/11/08 7.29 0.00 92.71
06/02/09 6.34 0.00 93.66
06/08/11 6.58 0.00 93.42
06/12/12 4.30 0.00 95.70
05/07/13 4.08 0.00 95.92
10/03/13 5.41 0.00 94.59
09/11/14 2.71 0.00 97.29
04/01/15 2.57 0.00 97.43
11/11/08 12.64 0.00 92.49
06/02/09 10.79 0.00 94.34
06/08/11 11.66 0.00 93.47
06/12/12 9.43 0.00 95.70
05/07/13 9.23 0.00 95.90
10/03/13 10.45 0.00 94.68
11/11/08 12.42 0.00 93.85
06/02/09 11.49 0.00 94.78
06/08/11 11.30 0.00 94.97
06/12/12 9.77 0.00 96.50
05/07/13 9.23 0.00 97.04
10/03/13 10.52 0.00 95.75
11/10/08 12.42 0.00 92.70
06/02/09 11.44 0.00 93.68
06/08/11 11.60 0.00 93.52
06/12/12 9.43 0.00 95.69
05/07/13 9.30 0.00 95.82
10/03/13 10.53 0.00 94.59
11/10/08 13.71 0.00 92.57
06/02/09 12.21 0.00 94.07
06/08/11 10.52 0.00 95.76
06/12/12 9.96 0.00 96.32
05/07/13 10.11 0.00 96.17
10/03/13 9.70 0.00 96.58
11/10/08 13.00 0.00 92.71
06/02/09 12.02 0.00 93.69
06/08/11 11.98 0.00 93.73
06/12/12 9.88 0.00 95.83
05/07/13 9.59 0.00 96.12
10/03/13 10.79 0.00 94.92
MW-17
MW-16 11/11/08
Free
Product
Thickness
(ft.)
Depth to
Ground
Water
from Top
of Casing
(ft.)
Well
ID
Date
Installed
(mm/dd/yy)
Ground
Water
Elevation*
(ft.)
Screened
Interval
(x to y
ft. BGS)
Date
Water
Level
Measured
(mm/dd/yy)
11/10/08
105.13
8 - 23
2 - 12
20
8
TABLE 1
WELL CONSTRUCTION INFORMATION
FORMER PHELPS AMOCO (INCIDENT NO. 12163)
Bottom
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Comments
Well
Casing
Depth
(ft. BGS)
10 - 20
11/11/08
Facility ID #: 0-006306
MW-20 11/10/08 10 10 - 20 20
10
MW-19
105.71
10 - 20 20
106.28
105.12
2010 - 20
12
Date: 04/08/15
106.27
MW-18 11/10/08 10
122 - 122
10
MW-15 100.00
MW-6
11/10/08MW-14
23
211/10/08
99.66
99.77133 - 13303/22/96
Page 1 of 2
Free
Product
Thickness
(ft.)
Depth to
Ground
Water
from Top
of Casing
(ft.)
Well
ID
Date
Installed
(mm/dd/yy)
Ground
Water
Elevation*
(ft.)
Screened
Interval
(x to y
ft. BGS)
Date
Water
Level
Measured
(mm/dd/yy)
TABLE 1
WELL CONSTRUCTION INFORMATION
FORMER PHELPS AMOCO (INCIDENT NO. 12163)
Bottom
of Well
(ft.
BGS)
Top of
Casing
Elevation*
(ft.)
Comments
Well
Casing
Depth
(ft. BGS)
Facility ID #: 0-006306Date: 04/08/15
05/03/10 3.88 0.00 95.31
06/08/11 5.80 0.00 93.39
06/12/12 3.10 0.00 96.09
04/03/13 3.03 0.00 96.16 Before AFVR
04/03/13 3.67 0.00 95.52 After AFVR
05/07/13 3.58 0.03 95.64
10/03/13 4.72 0.00 94.47
07/23/14 3.99 0.00 95.20 Before AFVR
07/23/14 5.10 0.00 94.09 After AFVR
09/11/14 2.11 0.00 97.08
04/01/15 1.87 0.00 97.32
05/03/10 3.50 0.00 95.52
06/08/11 5.50 0.00 93.52
06/12/12 3.25 0.00 95.77
05/07/13 2.45 0.00 96.57
10/03/13 4.36 0.00 94.66
09/11/14 1.31 0.00 97.71
04/01/15 1.50 0.00 97.52
MW-23 02/24/15 04/01/15 2 2-12 12 98.78 1.30 0.00 97.48
MW-24 02/24/15 04/01/15 2 2-12 12 99.69 2.14 0.00 97.55
Notes:
July 22, 2002 and from Corrective Action Plan dated September 2000. Top-of-casing elevations for monitoring wells MW-6 and MW-14 through
MW-20 were resurveyed on November 10-11, 2008. MW-15 was used as the reference point for elevation measurements with an assumed
elevation of 100.00 ft.
• NM: Not measured; well could not be located or was destroyed.
• *: Well construction data for monitoring wells installed prior to 2008 is reproduced from the Soil Excavation Report for March and April 2002 dated
• ft BGS: feet below ground surface
• NA: Not available.
• Monitoring wells MW-1 through MW-3, MWD-4, MW-5, MW-7, MW-8, MWD-9 and MW-10 were abandoned in 2002.
99.19123 - 123
204/27/10 99.02
04/27/10
112 - 11MW-22
MW-21
Page 2 of 2
Date: 04/10/15
EPA
504.1
EPA
6010B/
3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 3 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 3,000 28,500 25,000 50 15,000 ————
11/11/08 <0.11 <0.10 <0.13 <0.22 <0.10 <0.10 <0.10 <0.15 <0.20 <0.11 <0.13 <0.10 <0.13 <0.02017 3.4 170 <211 <111 <211
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 5 <100 <100 NR <100
06/08/11 <0.13 0.37 J <0.15 0.81 J <0.13 0.54 <0.16 <0.10 <0.11 <0.11 <0.18 0.72 J 0.21 J NR 6.3 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/08 5,400 940 550 1,700 <10 49 JB <10 30 J <20 52 J 23 J 170 78 J <0.02059 5.5 2,500 1,100 <105 1,100 E
06/02/09 14,300 15,600 1,350 7,080 <16.5 459 51.1 60 J <83.5 110 <16.5 1,210 358 NR 9.03 12,500 3,600 NR 3,820
06/08/11 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
11/17/11 8,970 7,770 1,050 6,020 <33 261 <41 46.4 J <27 109 J <45 1,200 416 NR NR NR NR NR NR
06/12/12 14,600 17,700 1,540 8,630 <33 343 <41 54.7 J <27 131 <45 1,410 438 NR NR NR NR NR NR
05/07/13 12,500 15,800 1,760 10,600 <10 483 32.9 J 92.0 <10 266 <10 2,380 699 NR NR NR NR NR NR
10/03/13 13,500 17,600 1,420 7,970 <50 275 <50 <50 <50 114 J <50 1,040 304 NR NR NR NR NR NR
09/11/14 7,030 8,080 1,150 6,750 <20 289 <20 56.2 J <20 151 <20 1,390 412 NR NR NR NR NR NR
04/01/15 8,340 9,980 1,030 6,350 <8.2 315 26.4 50.0 <8.0 124 <7.3 1,230 390 NR NR NR NR NR NR
11/11/08 2.6 4.0 0.87 J 4.6 <0.10 <0.10 <0.10 <0.15 <0.20 0.25 J <0.13 1.1 0.42 J <0.02077 19.2 <100 <211 <111 <211
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 30.2 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 48.4 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
11/11/08 <0.11 <0.10 <0.13 <0.22 <0.10 <0.10 <0.10 <0.15 <0.20 <0.11 <0.13 <0.10 <0.13 <0.02244 1.6 J <100 <205 <105 <205
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 2.01 J <100 <100 NR <100
06/08/11 <0.13 0.37 J <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 7.9 <35 <145 <110 <145
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/11/08 9.2 100 73 610 <0.50 23 B <0.50 18 <1.0 24 <0.65 100 53 <0.02047 <1.5 1,200 470 182 420 E
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 5.06 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 23.0 <35 <535 <500 <535
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
FORMER PHELPS AMOCO (INCIDENT NO. 12613)IPE1,3,5-TrimethylbenzeneLead2L Standard C9-C18 AliphaticsSUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TABLE 2
C19-C36 AliphaticsC9-C22 AromaticsMADEP VPH and/or EPH
EDBContaminant of Concern
1,2,4-TrimethylbenzeneTolueneEthylbenzeneBenzeneXylenesFacility ID # : 0-006306
MW-16 MTBETrichloroetheneC5-C8 AliphaticsAnalytical Method EPA Method 6200B/ EPA Method 610
GCL Isopropylbenzenen-PropylbenzeneNaphthalene1,2-DichloroethaneMW-15
MW-14
MW-6
MW-17
Page 1 of 3
Date: 04/10/15
EPA
504.1
EPA
6010B/
3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 3 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 3,000 28,500 25,000 50 15,000 ————
FORMER PHELPS AMOCO (INCIDENT NO. 12613)IPE1,3,5-TrimethylbenzeneLead2L Standard C9-C18 AliphaticsSUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TABLE 2
C19-C36 AliphaticsC9-C22 AromaticsMADEP VPH and/or EPH
EDBContaminant of Concern
1,2,4-TrimethylbenzeneTolueneEthylbenzeneBenzeneXylenesFacility ID # : 0-006306 MTBETrichloroetheneC5-C8 AliphaticsAnalytical Method EPA Method 6200B/ EPA Method 610
GCL Isopropylbenzenen-PropylbenzeneNaphthalene1,2-Dichloroethane11/10/08 <0.14 0.75 J <0.15 <0.12 <0.25 <0.070 <0.11 <0.12 <0.20 <0.22 <0.15 <0.14 <0.13 <0.02000 26.6 <100 <205 <105 <205
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 7.57 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 17.6 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/10/08 800 26 190 170 <0.25 65 0.47 J 13 2.3 J 21 <0.15 3.0 1.9 <0.02000 6.7 2,500 300 <105 210
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 12.5 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 59.4 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 0.12 J <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
11/10/08 0.28 J <0.19 0.18 J <0.12 3.1 0.40 J <0.11 <0.12 <0.20 <0.22 <0.15 <0.14 <0.13 <0.02000 10.0 <100 <205 <105 <205
06/02/09 <0.200 <0.330 <0.670 <1.33 <0.330 <1.00 <0.330 <1.00 <1.67 <0.330 <0.330 <0.330 <0.330 NR 10.7 <100 <100 NR <100
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR <5.0 <35 <135 <100 <135
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
06/08/11 19,400 20,900 1,300 7,400 <65 565 806 72.4 J <54 215 J <90 2,260 632 NR 98.4 78,300 84,300 1,000 33,400
06/12/12 26,000 32,000 1,780 11,800 <65 564 1,020 78.4 J <54 273 <90 3,410 1,110 NR NR NR NR NR NR
05/07/13 FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP FP
10/03/13 26,500 40,900 1,930 10,500 <100 380 J 855 <100 <100 172 J <100 1,350 386 J NR NR NR NR NR NR
09/11/14 22,800 22,800 1,880 11,500 85.1 J 622 <50 67.1 J <50 236 J <50 2,270 645 NR NR NR NR NR NR
04/01/15 26,900 36,700 1,670 11,200 191 J 1,630 1,230 <120 <160 177 J <150 2,280 601 NR NR NR NR NR NR
06/08/11 <0.13 <0.13 <0.15 <0.30 <0.13 <0.10 <0.16 <0.10 <0.11 <0.11 <0.18 <0.10 <0.10 NR 874 <35 <535 <500 <535
10/03/13 <0.10 <0.10 <0.10 <0.22 <0.10 <0.15 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
09/11/14 <0.10 <0.10 <0.10 <0.20 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 <0.10 NR NR NR NR NR NR
04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
MW-23 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
MW-20
MW-22
MW-21
MW-18
MW-19
Page 2 of 3
Date: 04/10/15
EPA
504.1
EPA
6010B/
3030C
Well
ID
Date
Collected
(mm/dd/yy)
1 600 600 500 20 6 0.4 70 70 70 3 400 400 0.02 15 400 700 10,000 200
5,000 260,000 84,500 85,500 20,000 6,000 400 25,000 70,000 30,000 3,000 28,500 25,000 50 15,000 ————
FORMER PHELPS AMOCO (INCIDENT NO. 12613)IPE1,3,5-TrimethylbenzeneLead2L Standard C9-C18 AliphaticsSUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
TABLE 2
C19-C36 AliphaticsC9-C22 AromaticsMADEP VPH and/or EPH
EDBContaminant of Concern
1,2,4-TrimethylbenzeneTolueneEthylbenzeneBenzeneXylenesFacility ID # : 0-006306 MTBETrichloroetheneC5-C8 AliphaticsAnalytical Method EPA Method 6200B/ EPA Method 610
GCL Isopropylbenzenen-PropylbenzeneNaphthalene1,2-DichloroethaneMW-24 04/01/15 <0.17 <0.17 <0.15 <0.43 <0.16 <0.12 <0.16 <0.12 <0.16 <0.16 <0.15 <0.14 <0.14 NR NR NR NR NR NR
Notes:
• GCL: Gross contamination level.
• NE: Standard not established.
• NS: Not sampled
• Concentrations in bold face type exceeded the 2L standard; concentrations in italics exceeded the GCLs.
• J: The compound is present, but the calculated result is less than the EQL.
• For other compounds reported which did not exceed the 2L Standards, refer to the laboratory reports.
• < : Less than the method detection limit specified in the analytical report.
• 2L Standard: as specified in T15A NCAC 2L.0202.
• Results reported in µg/l (micrograms per liter).
• B: Compound was also detected in the method blank.
Page 3 of 3

APPENDICES

APPENDIX A
Monitoring Well Permit, DOT Encroachment Agreement and Well Construction Records

APPENDIX B
Laboratory Report – Ground Water Samples
04/13/15
Technical Report for
GRI (Geological Resources Inc.)
Former Phelps Amoco; Hwy 64 E, Creswell, NC
2720
Accutest Job Number: FA23294
Sampling Date: 04/01/15
Report to:
GRI (Geological Resources Inc.)
[e-mail]
ATTN: Angela Roach
Total number of pages in report:
Certifications: FL (E83510), LA (03051), KS (E-10327), IA (366), IL (200063), NC (573), NJ (FL002), SC (96038001)
DoD ELAP (L-A-B L2229), CA (2937), TX (T104704404), PA (68-03573), VA (460177),
AK, AR, GA, KY, MA, NV, OK, UT, WA
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
Southeast • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone] • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Norm Farmer
Technical Director
Southeast
04/13/15
Reissue #1
e-Hardcopy 2.0
Automated Report
38
Accutest Laboratories is the sole authority for authorizing edits or modifications to this
document. Unauthorized modification of this report is strictly prohibited.
1 of 38
FA23294
Florida  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]  htpp://www.accutest.com www.accutest.com

April 10, 2015

Ms. Angela Roach
Geological Resources Inc
2301 F. Crown Point EX Dr
Charlotte, NC 28207

RE: Accutest job FA23294 Reissue

Dear Ms. Roach,

The final report for job number FA23294 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

The sample ID has been revised.

Accutest apologies for any inconvenience this may have caused. Please feel free to contact
us if we can be of further assistance.

Sincerely,

Accutest Laboratories, SE

2 of 38
FA23294
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................7
3.1: FA23294-1: MW-6 ........................................................................................................8
3.2: FA23294-2: MW-14 ......................................................................................................10
3.3: FA23294-3: MW-15 ......................................................................................................12
3.4: FA23294-4: MW-21 ......................................................................................................14
3.5: FA23294-5: MW-22 ......................................................................................................16
3.6: FA23294-6: MW-23 ......................................................................................................18
3.7: FA23294-7: MW-24 ......................................................................................................20
Section 4: Misc. Forms ............................................................................................................22
4.1: Chain of Custody ...........................................................................................................23
Section 5: GC/MS Volatiles - QC Data Summaries ..............................................................26
5.1: Method Blank Summary ................................................................................................27
5.2: Blank Spike Summary ...................................................................................................31
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................35 123453 of 38
FA23294
Accutest Laboratories
Sample Summary
GRI (Geological Resources Inc.)
Job No:FA23294
Former Phelps Amoco; Hwy 64 E, Creswell, NC
Project No: 2720
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
FA23294-1 04/01/15 13:03 HMJ 04/02/15 AQ Ground Water MW-6
FA23294-2 04/01/15 13:33 HMJ 04/02/15 AQ Ground Water MW-14
FA23294-3 04/01/15 12:56 HMJ 04/02/15 AQ Ground Water MW-15
FA23294-4 04/01/15 12:35 HMJ 04/02/15 AQ Ground Water MW-21
FA23294-5 04/01/15 12:30 HMJ 04/02/15 AQ Ground Water MW-22
FA23294-6 04/01/15 13:18 HMJ 04/02/15 AQ Ground Water MW-23
FA23294-7 04/01/15 13:24 HMJ 04/02/15 AQ Ground Water MW-24
4 of 38
FA23294 1
Summary of Hits Page 1 of 2
Job Number:FA23294
Account:GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Collected:04/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA23294-1 MW-6
No hits reported in this sample.
FA23294-2 MW-14
Benzene 8340 100 34 ug/l SM 6200B
n-Butylbenzene 18.3 J 25 7.2 ug/l SM 6200B
sec-Butylbenzene 9.9 J 25 6.9 ug/l SM 6200B
1,2-Dichloroethane 26.4 25 8.2 ug/l SM 6200B
Ethylbenzene 1030 25 7.6 ug/l SM 6200B
Isopropylbenzene 50.0 25 5.9 ug/l SM 6200B
p-Isopropyltoluene 8.9 J 25 6.1 ug/l SM 6200B
Naphthalene 315 25 6.1 ug/l SM 6200B
n-Propylbenzene 124 25 7.8 ug/l SM 6200B
Styrene 12.5 J 25 6.0 ug/l SM 6200B
Toluene 9980 100 33 ug/l SM 6200B
1,2,4-Trimethylbenzene 1230 25 6.8 ug/l SM 6200B
1,3,5-Trimethylbenzene 390 25 6.8 ug/l SM 6200B
m,p-Xylene 4340 50 15 ug/l SM 6200B
o-Xylene 2010 25 6.7 ug/l SM 6200B
Xylene (total)6350 75 22 ug/l SM 6200B
FA23294-3 MW-15
No hits reported in this sample.
FA23294-4 MW-21
Benzene 26900 500 170 ug/l SM 6200B
1,2-Dichloroethane 1230 500 160 ug/l SM 6200B
Ethylbenzene 1670 500 150 ug/l SM 6200B
Methyl Tert Butyl Ether 191 J 500 160 ug/l SM 6200B
Naphthalene 1630 500 120 ug/l SM 6200B
n-Propylbenzene 177 J 500 160 ug/l SM 6200B
Toluene 36700 500 170 ug/l SM 6200B
1,2,4-Trimethylbenzene 2280 500 140 ug/l SM 6200B
1,3,5-Trimethylbenzene 601 500 140 ug/l SM 6200B
m,p-Xylene 7720 1000 300 ug/l SM 6200B
o-Xylene 3500 500 130 ug/l SM 6200B
Xylene (total)11200 1500 430 ug/l SM 6200B
FA23294-5 MW-22
No hits reported in this sample.
5 of 38
FA23294 2
Summary of Hits Page 2 of 2
Job Number:FA23294
Account:GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Collected:04/01/15
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA23294-6 MW-23
No hits reported in this sample.
FA23294-7 MW-24
No hits reported in this sample.
6 of 38
FA23294 2
Accutest Laboratories
Sample Results
Report of Analysis
Southeast
Section 3
7 of 38
FA23294 3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-6
Lab Sample ID:FA23294-1 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193682.D 1 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 38
FA23294 33.1
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-6
Lab Sample ID:FA23294-1 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 111%70-130%
2037-26-5 Toluene-D8 92%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 38
FA23294 33.1
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-14
Lab Sample ID:FA23294-2 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193642.D 50 04/07/15 TD n/a n/a VA1681
Run #2 A0193644.D 200 04/07/15 TD n/a n/a VA1681
Purge Volume
Run #1 10.0 ml
Run #2 10.0 ml
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 8340 a 100 34 ug/l
108-86-1 Bromobenzene ND 25 8.0 ug/l
74-97-5 Bromochloromethane ND 25 8.0 ug/l
75-27-4 Bromodichloromethane ND 25 7.4 ug/l
75-25-2 Bromoform ND 25 5.5 ug/l
104-51-8 n-Butylbenzene 18.3 25 7.2 ug/l J
135-98-8 sec-Butylbenzene 9.9 25 6.9 ug/l J
98-06-6 tert-Butylbenzene ND 25 7.3 ug/l
56-23-5 Carbon Tetrachloride ND 25 7.7 ug/l
108-90-7 Chlorobenzene ND 25 7.9 ug/l
75-00-3 Chloroethane ND 25 10 ug/l
67-66-3 Chloroform ND 25 8.6 ug/l
95-49-8 o-Chlorotoluene ND 25 7.6 ug/l
106-43-4 p-Chlorotoluene ND 25 6.9 ug/l
124-48-1 Dibromochloromethane ND 25 6.2 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 25 9.9 ug/l
106-93-4 1,2-Dibromoethane ND 25 7.1 ug/l
75-71-8 Dichlorodifluoromethane ND 25 6.5 ug/l
95-50-1 1,2-Dichlorobenzene ND 25 6.5 ug/l
541-73-1 1,3-Dichlorobenzene ND 25 7.0 ug/l
106-46-7 1,4-Dichlorobenzene ND 25 7.6 ug/l
75-34-3 1,1-Dichloroethane ND 25 9.1 ug/l
107-06-2 1,2-Dichloroethane 26.4 25 8.2 ug/l
75-35-4 1,1-Dichloroethylene ND 25 8.5 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 25 9.0 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 25 8.5 ug/l
78-87-5 1,2-Dichloropropane ND 25 8.7 ug/l
142-28-9 1,3-Dichloropropane ND 25 7.3 ug/l
594-20-7 2,2-Dichloropropane ND 25 6.1 ug/l
563-58-6 1,1-Dichloropropene ND 25 7.9 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 25 6.6 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 25 6.3 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 38
FA23294 33.2
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-14
Lab Sample ID:FA23294-2 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 25 8.0 ug/l
100-41-4 Ethylbenzene 1030 25 7.6 ug/l
87-68-3 Hexachlorobutadiene ND 25 6.1 ug/l
98-82-8 Isopropylbenzene 50.0 25 5.9 ug/l
99-87-6 p-Isopropyltoluene 8.9 25 6.1 ug/l J
74-83-9 Methyl Bromide ND 25 9.1 ug/l
74-87-3 Methyl Chloride ND 25 7.9 ug/l
74-95-3 Methylene Bromide ND 25 8.5 ug/l
75-09-2 Methylene Chloride ND 100 50 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 25 8.2 ug/l
91-20-3 Naphthalene 315 25 6.1 ug/l
103-65-1 n-Propylbenzene 124 25 7.8 ug/l
100-42-5 Styrene 12.5 25 6.0 ug/l J
630-20-6 1,1,1,2-Tetrachloroethane ND 25 6.3 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 25 7.1 ug/l
127-18-4 Tetrachloroethylene ND 25 7.4 ug/l
108-88-3 Toluene 9980 a 100 33 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 25 6.8 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 25 6.5 ug/l
71-55-6 1,1,1-Trichloroethane ND 25 8.1 ug/l
79-00-5 1,1,2-Trichloroethane ND 25 7.0 ug/l
79-01-6 Trichloroethylene ND 25 7.3 ug/l
75-69-4 Trichlorofluoromethane ND 25 8.1 ug/l
96-18-4 1,2,3-Trichloropropane ND 25 6.4 ug/l
95-63-6 1,2,4-Trimethylbenzene 1230 25 6.8 ug/l
108-67-8 1,3,5-Trimethylbenzene 390 25 6.8 ug/l
75-01-4 Vinyl Chloride ND 25 6.5 ug/l
m,p-Xylene 4340 50 15 ug/l
95-47-6 o-Xylene 2010 25 6.7 ug/l
1330-20-7 Xylene (total)6350 75 22 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 97%101%70-130%
17060-07-0 1,2-Dichloroethane-D4 113%109%70-130%
2037-26-5 Toluene-D8 99%98%70-130%
460-00-4 4-Bromofluorobenzene 102%100%70-130%
(a) Result is from Run# 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 38
FA23294 33.2
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-15
Lab Sample ID:FA23294-3 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193683.D 1 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 38
FA23294 33.3
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-15
Lab Sample ID:FA23294-3 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%70-130%
17060-07-0 1,2-Dichloroethane-D4 112%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 38
FA23294 33.3
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-21
Lab Sample ID:FA23294-4 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193647.D 1000 04/07/15 TD n/a n/a VA1681
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene 26900 500 170 ug/l
108-86-1 Bromobenzene ND 500 160 ug/l
74-97-5 Bromochloromethane ND 500 160 ug/l
75-27-4 Bromodichloromethane ND 500 150 ug/l
75-25-2 Bromoform ND 500 110 ug/l
104-51-8 n-Butylbenzene ND 500 140 ug/l
135-98-8 sec-Butylbenzene ND 500 140 ug/l
98-06-6 tert-Butylbenzene ND 500 150 ug/l
56-23-5 Carbon Tetrachloride ND 500 150 ug/l
108-90-7 Chlorobenzene ND 500 160 ug/l
75-00-3 Chloroethane ND 500 210 ug/l
67-66-3 Chloroform ND 500 170 ug/l
95-49-8 o-Chlorotoluene ND 500 150 ug/l
106-43-4 p-Chlorotoluene ND 500 140 ug/l
124-48-1 Dibromochloromethane ND 500 120 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 500 200 ug/l
106-93-4 1,2-Dibromoethane ND 500 140 ug/l
75-71-8 Dichlorodifluoromethane ND 500 130 ug/l
95-50-1 1,2-Dichlorobenzene ND 500 130 ug/l
541-73-1 1,3-Dichlorobenzene ND 500 140 ug/l
106-46-7 1,4-Dichlorobenzene ND 500 150 ug/l
75-34-3 1,1-Dichloroethane ND 500 180 ug/l
107-06-2 1,2-Dichloroethane 1230 500 160 ug/l
75-35-4 1,1-Dichloroethylene ND 500 170 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 500 180 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 500 170 ug/l
78-87-5 1,2-Dichloropropane ND 500 170 ug/l
142-28-9 1,3-Dichloropropane ND 500 150 ug/l
594-20-7 2,2-Dichloropropane ND 500 120 ug/l
563-58-6 1,1-Dichloropropene ND 500 160 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 500 130 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 500 130 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 38
FA23294 33.4
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-21
Lab Sample ID:FA23294-4 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 500 160 ug/l
100-41-4 Ethylbenzene 1670 500 150 ug/l
87-68-3 Hexachlorobutadiene ND 500 120 ug/l
98-82-8 Isopropylbenzene ND 500 120 ug/l
99-87-6 p-Isopropyltoluene ND 500 120 ug/l
74-83-9 Methyl Bromide ND 500 180 ug/l
74-87-3 Methyl Chloride ND 500 160 ug/l
74-95-3 Methylene Bromide ND 500 170 ug/l
75-09-2 Methylene Chloride ND 2000 1000 ug/l
1634-04-4 Methyl Tert Butyl Ether 191 500 160 ug/l J
91-20-3 Naphthalene 1630 500 120 ug/l
103-65-1 n-Propylbenzene 177 500 160 ug/l J
100-42-5 Styrene ND 500 120 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 500 130 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 500 140 ug/l
127-18-4 Tetrachloroethylene ND 500 150 ug/l
108-88-3 Toluene 36700 500 170 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 500 140 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 500 130 ug/l
71-55-6 1,1,1-Trichloroethane ND 500 160 ug/l
79-00-5 1,1,2-Trichloroethane ND 500 140 ug/l
79-01-6 Trichloroethylene ND 500 150 ug/l
75-69-4 Trichlorofluoromethane ND 500 160 ug/l
96-18-4 1,2,3-Trichloropropane ND 500 130 ug/l
95-63-6 1,2,4-Trimethylbenzene 2280 500 140 ug/l
108-67-8 1,3,5-Trimethylbenzene 601 500 140 ug/l
75-01-4 Vinyl Chloride ND 500 130 ug/l
m,p-Xylene 7720 1000 300 ug/l
95-47-6 o-Xylene 3500 500 130 ug/l
1330-20-7 Xylene (total)11200 1500 430 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 95%70-130%
17060-07-0 1,2-Dichloroethane-D4 100%70-130%
2037-26-5 Toluene-D8 97%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 38
FA23294 33.4
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-22
Lab Sample ID:FA23294-5 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193684.D 1 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 38
FA23294 33.5
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-22
Lab Sample ID:FA23294-5 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 107%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 90%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 38
FA23294 33.5
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-23
Lab Sample ID:FA23294-6 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193685.D 1 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 38
FA23294 33.6
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-23
Lab Sample ID:FA23294-6 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 108%70-130%
17060-07-0 1,2-Dichloroethane-D4 117%70-130%
2037-26-5 Toluene-D8 94%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 38
FA23294 33.6
Accutest Laboratories
Report of Analysis Page 1 of 2
Client Sample ID:MW-24
Lab Sample ID:FA23294-7 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 A0193686.D 1 04/08/15 TD n/a n/a VA1682
Run #2
Purge Volume
Run #1 10.0 ml
Run #2
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 38
FA23294 33.7
Accutest Laboratories
Report of Analysis Page 2 of 2
Client Sample ID:MW-24
Lab Sample ID:FA23294-7 Date Sampled:04/01/15
Matrix:AQ - Ground Water Date Received:04/02/15
Method:SM 6200B Percent Solids:n/a
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
VOA 6200B List
CAS No.Compound Result RL MDL Units Q
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%70-130%
17060-07-0 1,2-Dichloroethane-D4 114%70-130%
2037-26-5 Toluene-D8 96%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 38
FA23294 33.7
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Southeast
Section 4
22 of 38
FA23294 4
FA23294: Chain of Custody
Page 1 of 3
23 of 38
FA23294 44.1
FA23294: Chain of Custody
Page 2 of 3
24 of 38
FA23294 44.1
FA23294: Chain of Custody
Page 3 of 3
25 of 38
FA23294 44.1
Accutest Laboratories
GC/MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Southeast
Section 5
26 of 38
FA23294 5
Method Blank Summary Page 1 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1681-MB A0193637.D 1 04/07/15 TD n/a n/a VA1681
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-2, FA23294-4
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
27 of 38
FA23294 55.1.1
Method Blank Summary Page 2 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1681-MB A0193637.D 1 04/07/15 TD n/a n/a VA1681
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-2, FA23294-4
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 98%70-130%
460-00-4 4-Bromofluorobenzene 99%70-130%
28 of 38
FA23294 55.1.1
Method Blank Summary Page 1 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-MB A0193680.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-1, FA23294-3, FA23294-5, FA23294-6, FA23294-7
CAS No.Compound Result RL MDL Units Q
71-43-2 Benzene ND 0.50 0.17 ug/l
108-86-1 Bromobenzene ND 0.50 0.16 ug/l
74-97-5 Bromochloromethane ND 0.50 0.16 ug/l
75-27-4 Bromodichloromethane ND 0.50 0.15 ug/l
75-25-2 Bromoform ND 0.50 0.11 ug/l
104-51-8 n-Butylbenzene ND 0.50 0.14 ug/l
135-98-8 sec-Butylbenzene ND 0.50 0.14 ug/l
98-06-6 tert-Butylbenzene ND 0.50 0.15 ug/l
56-23-5 Carbon Tetrachloride ND 0.50 0.15 ug/l
108-90-7 Chlorobenzene ND 0.50 0.16 ug/l
75-00-3 Chloroethane ND 0.50 0.21 ug/l
67-66-3 Chloroform ND 0.50 0.17 ug/l
95-49-8 o-Chlorotoluene ND 0.50 0.15 ug/l
106-43-4 p-Chlorotoluene ND 0.50 0.14 ug/l
124-48-1 Dibromochloromethane ND 0.50 0.12 ug/l
96-12-8 1,2-Dibromo-3-chloropropane ND 0.50 0.20 ug/l
106-93-4 1,2-Dibromoethane ND 0.50 0.14 ug/l
75-71-8 Dichlorodifluoromethane ND 0.50 0.13 ug/l
95-50-1 1,2-Dichlorobenzene ND 0.50 0.13 ug/l
541-73-1 1,3-Dichlorobenzene ND 0.50 0.14 ug/l
106-46-7 1,4-Dichlorobenzene ND 0.50 0.15 ug/l
75-34-3 1,1-Dichloroethane ND 0.50 0.18 ug/l
107-06-2 1,2-Dichloroethane ND 0.50 0.16 ug/l
75-35-4 1,1-Dichloroethylene ND 0.50 0.17 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 0.50 0.18 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 0.50 0.17 ug/l
78-87-5 1,2-Dichloropropane ND 0.50 0.17 ug/l
142-28-9 1,3-Dichloropropane ND 0.50 0.15 ug/l
594-20-7 2,2-Dichloropropane ND 0.50 0.12 ug/l
563-58-6 1,1-Dichloropropene ND 0.50 0.16 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 0.50 0.13 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 0.50 0.13 ug/l
108-20-3 Di-Isopropyl Ether ND 0.50 0.16 ug/l
100-41-4 Ethylbenzene ND 0.50 0.15 ug/l
87-68-3 Hexachlorobutadiene ND 0.50 0.12 ug/l
98-82-8 Isopropylbenzene ND 0.50 0.12 ug/l
29 of 38
FA23294 55.1.2
Method Blank Summary Page 2 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-MB A0193680.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-1, FA23294-3, FA23294-5, FA23294-6, FA23294-7
CAS No.Compound Result RL MDL Units Q
99-87-6 p-Isopropyltoluene ND 0.50 0.12 ug/l
74-83-9 Methyl Bromide ND 0.50 0.18 ug/l
74-87-3 Methyl Chloride ND 0.50 0.16 ug/l
74-95-3 Methylene Bromide ND 0.50 0.17 ug/l
75-09-2 Methylene Chloride ND 2.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 0.50 0.16 ug/l
91-20-3 Naphthalene ND 0.50 0.12 ug/l
103-65-1 n-Propylbenzene ND 0.50 0.16 ug/l
100-42-5 Styrene ND 0.50 0.12 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 0.50 0.13 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 0.50 0.14 ug/l
127-18-4 Tetrachloroethylene ND 0.50 0.15 ug/l
108-88-3 Toluene ND 0.50 0.17 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 0.50 0.14 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 0.50 0.13 ug/l
71-55-6 1,1,1-Trichloroethane ND 0.50 0.16 ug/l
79-00-5 1,1,2-Trichloroethane ND 0.50 0.14 ug/l
79-01-6 Trichloroethylene ND 0.50 0.15 ug/l
75-69-4 Trichlorofluoromethane ND 0.50 0.16 ug/l
96-18-4 1,2,3-Trichloropropane ND 0.50 0.13 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 0.50 0.14 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 0.50 0.14 ug/l
75-01-4 Vinyl Chloride ND 0.50 0.13 ug/l
m,p-Xylene ND 1.0 0.30 ug/l
95-47-6 o-Xylene ND 0.50 0.13 ug/l
1330-20-7 Xylene (total)ND 1.5 0.43 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 106%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 102%70-130%
30 of 38
FA23294 55.1.2
Blank Spike Summary Page 1 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1681-BS A0193635.D 1 04/07/15 TD n/a n/a VA1681
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-2, FA23294-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 10.5 105 70-130
108-86-1 Bromobenzene 10 10.4 104 70-130
74-97-5 Bromochloromethane 10 9.9 99 70-130
75-27-4 Bromodichloromethane 10 11.0 110 70-130
75-25-2 Bromoform 10 10.7 107 70-130
104-51-8 n-Butylbenzene 10 10.8 108 70-130
135-98-8 sec-Butylbenzene 10 11.7 117 70-130
98-06-6 tert-Butylbenzene 10 11.6 116 70-130
56-23-5 Carbon Tetrachloride 10 11.5 115 70-130
108-90-7 Chlorobenzene 10 11.1 111 70-130
75-00-3 Chloroethane 10 12.8 128 60-140
67-66-3 Chloroform 10 10.7 107 70-130
95-49-8 o-Chlorotoluene 10 11.2 112 70-130
106-43-4 p-Chlorotoluene 10 11.6 116 70-130
124-48-1 Dibromochloromethane 10 11.0 110 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 10 100 70-130
106-93-4 1,2-Dibromoethane 10 10.5 105 70-130
75-71-8 Dichlorodifluoromethane 10 8.9 89 60-140
95-50-1 1,2-Dichlorobenzene 10 11.0 110 70-130
541-73-1 1,3-Dichlorobenzene 10 11.1 111 70-130
106-46-7 1,4-Dichlorobenzene 10 10.2 102 70-130
75-34-3 1,1-Dichloroethane 10 10.5 105 70-130
107-06-2 1,2-Dichloroethane 10 10.8 108 70-130
75-35-4 1,1-Dichloroethylene 10 12.0 120 70-130
156-59-2 cis-1,2-Dichloroethylene 10 10.7 107 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.0 110 70-130
78-87-5 1,2-Dichloropropane 10 10.7 107 70-130
142-28-9 1,3-Dichloropropane 10 10.5 105 70-130
594-20-7 2,2-Dichloropropane 10 11.8 118 70-130
563-58-6 1,1-Dichloropropene 10 11.5 115 70-130
10061-01-5 cis-1,3-Dichloropropene 10 10.7 107 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.5 115 70-130
108-20-3 Di-Isopropyl Ether 10 10.5 105 70-130
100-41-4 Ethylbenzene 10 10.6 106 70-130
87-68-3 Hexachlorobutadiene 10 10.8 108 70-130
98-82-8 Isopropylbenzene 10 11.8 118 70-130
* = Outside of Control Limits.
31 of 38
FA23294 55.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1681-BS A0193635.D 1 04/07/15 TD n/a n/a VA1681
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-2, FA23294-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 11.6 116 70-130
74-83-9 Methyl Bromide 10 12.5 125 60-140
74-87-3 Methyl Chloride 10 10.7 107 60-140
74-95-3 Methylene Bromide 10 10.5 105 70-130
75-09-2 Methylene Chloride 10 10.7 107 70-130
1634-04-4 Methyl Tert Butyl Ether 10 10.9 109 70-130
91-20-3 Naphthalene 10 10.7 107 70-130
103-65-1 n-Propylbenzene 10 11.7 117 70-130
100-42-5 Styrene 10 10.6 106 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 10.7 107 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.0 100 70-130
127-18-4 Tetrachloroethylene 10 10.8 108 70-130
108-88-3 Toluene 10 10.6 106 70-130
87-61-6 1,2,3-Trichlorobenzene 10 10.4 104 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.4 104 70-130
71-55-6 1,1,1-Trichloroethane 10 11.4 114 70-130
79-00-5 1,1,2-Trichloroethane 10 10.4 104 70-130
79-01-6 Trichloroethylene 10 11.0 110 70-130
75-69-4 Trichlorofluoromethane 10 10.8 108 60-140
96-18-4 1,2,3-Trichloropropane 10 10.4 104 70-130
95-63-6 1,2,4-Trimethylbenzene 10 10.7 107 70-130
108-67-8 1,3,5-Trimethylbenzene 10 10.7 107 70-130
75-01-4 Vinyl Chloride 10 11.7 117 60-140
m,p-Xylene 20 22.3 112 70-130
95-47-6 o-Xylene 10 11.5 115 70-130
1330-20-7 Xylene (total)30 33.8 113 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 104%70-130%
2037-26-5 Toluene-D8 99%70-130%
460-00-4 4-Bromofluorobenzene 100%70-130%
* = Outside of Control Limits.
32 of 38
FA23294 55.2.1
Blank Spike Summary Page 1 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-BS A0193679.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-1, FA23294-3, FA23294-5, FA23294-6, FA23294-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
71-43-2 Benzene 10 11.0 110 70-130
108-86-1 Bromobenzene 10 10.9 109 70-130
74-97-5 Bromochloromethane 10 11.1 111 70-130
75-27-4 Bromodichloromethane 10 11.5 115 70-130
75-25-2 Bromoform 10 10.9 109 70-130
104-51-8 n-Butylbenzene 10 11.5 115 70-130
135-98-8 sec-Butylbenzene 10 12.5 125 70-130
98-06-6 tert-Butylbenzene 10 12.4 124 70-130
56-23-5 Carbon Tetrachloride 10 12.1 121 70-130
108-90-7 Chlorobenzene 10 12.4 124 70-130
75-00-3 Chloroethane 10 7.7 77 60-140
67-66-3 Chloroform 10 11.2 112 70-130
95-49-8 o-Chlorotoluene 10 11.8 118 70-130
106-43-4 p-Chlorotoluene 10 12.1 121 70-130
124-48-1 Dibromochloromethane 10 11.3 113 70-130
96-12-8 1,2-Dibromo-3-chloropropane 10 9.8 98 70-130
106-93-4 1,2-Dibromoethane 10 11.0 110 70-130
75-71-8 Dichlorodifluoromethane 10 8.5 85 60-140
95-50-1 1,2-Dichlorobenzene 10 11.4 114 70-130
541-73-1 1,3-Dichlorobenzene 10 11.9 119 70-130
106-46-7 1,4-Dichlorobenzene 10 10.8 108 70-130
75-34-3 1,1-Dichloroethane 10 11.1 111 70-130
107-06-2 1,2-Dichloroethane 10 11.6 116 70-130
75-35-4 1,1-Dichloroethylene 10 12.5 125 70-130
156-59-2 cis-1,2-Dichloroethylene 10 11.1 111 70-130
156-60-5 trans-1,2-Dichloroethylene 10 11.4 114 70-130
78-87-5 1,2-Dichloropropane 10 11.1 111 70-130
142-28-9 1,3-Dichloropropane 10 10.8 108 70-130
594-20-7 2,2-Dichloropropane 10 11.7 117 70-130
563-58-6 1,1-Dichloropropene 10 12.4 124 70-130
10061-01-5 cis-1,3-Dichloropropene 10 11.0 110 70-130
10061-02-6 trans-1,3-Dichloropropene 10 11.9 119 70-130
108-20-3 Di-Isopropyl Ether 10 11.7 117 70-130
100-41-4 Ethylbenzene 10 11.2 112 70-130
87-68-3 Hexachlorobutadiene 10 10.7 107 70-130
98-82-8 Isopropylbenzene 10 12.6 126 70-130
* = Outside of Control Limits.
33 of 38
FA23294 55.2.2
Blank Spike Summary Page 2 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VA1682-BS A0193679.D 1 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-1, FA23294-3, FA23294-5, FA23294-6, FA23294-7
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
99-87-6 p-Isopropyltoluene 10 12.4 124 70-130
74-83-9 Methyl Bromide 10 8.3 83 60-140
74-87-3 Methyl Chloride 10 8.5 85 60-140
74-95-3 Methylene Bromide 10 10.9 109 70-130
75-09-2 Methylene Chloride 10 12.9 129 70-130
1634-04-4 Methyl Tert Butyl Ether 10 11.5 115 70-130
91-20-3 Naphthalene 10 10.2 102 70-130
103-65-1 n-Propylbenzene 10 12.4 124 70-130
100-42-5 Styrene 10 11.6 116 70-130
630-20-6 1,1,1,2-Tetrachloroethane 10 11.5 115 70-130
79-34-5 1,1,2,2-Tetrachloroethane 10 10.2 102 70-130
127-18-4 Tetrachloroethylene 10 11.4 114 70-130
108-88-3 Toluene 10 11.5 115 70-130
87-61-6 1,2,3-Trichlorobenzene 10 11.1 111 70-130
120-82-1 1,2,4-Trichlorobenzene 10 10.4 104 70-130
71-55-6 1,1,1-Trichloroethane 10 11.6 116 70-130
79-00-5 1,1,2-Trichloroethane 10 10.9 109 70-130
79-01-6 Trichloroethylene 10 11.9 119 70-130
75-69-4 Trichlorofluoromethane 10 7.2 72 60-140
96-18-4 1,2,3-Trichloropropane 10 10.3 103 70-130
95-63-6 1,2,4-Trimethylbenzene 10 11.2 112 70-130
108-67-8 1,3,5-Trimethylbenzene 10 11.2 112 70-130
75-01-4 Vinyl Chloride 10 8.3 83 60-140
m,p-Xylene 20 23.4 117 70-130
95-47-6 o-Xylene 10 12.3 123 70-130
1330-20-7 Xylene (total)30 35.6 119 70-130
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 101%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%70-130%
2037-26-5 Toluene-D8 100%70-130%
460-00-4 4-Bromofluorobenzene 101%70-130%
* = Outside of Control Limits.
34 of 38
FA23294 55.2.2
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23294-4MS A0193649.D 1000 04/07/15 TD n/a n/a VA1681
FA23294-4MSD A0193650.D 1000 04/07/15 TD n/a n/a VA1681
FA23294-4 A0193647.D 1000 04/07/15 TD n/a n/a VA1681
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-2, FA23294-4
FA23294-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 26900 10000 34900 80 10000 32500 56* a 7 70-130/20
108-86-1 Bromobenzene ND 10000 8610 86 10000 8040 80 7 70-130/20
74-97-5 Bromochloromethane ND 10000 8250 83 10000 7830 78 5 70-130/20
75-27-4 Bromodichloromethane ND 10000 9110 91 10000 8570 86 6 70-130/20
75-25-2 Bromoform ND 10000 8460 85 10000 8390 84 1 70-130/20
104-51-8 n-Butylbenzene ND 10000 8870 89 10000 8110 81 9 70-130/20
135-98-8 sec-Butylbenzene ND 10000 9570 96 10000 8800 88 8 70-130/20
98-06-6 tert-Butylbenzene ND 10000 9580 96 10000 8760 88 9 70-130/20
56-23-5 Carbon Tetrachloride ND 10000 9390 94 10000 8430 84 11 70-130/20
108-90-7 Chlorobenzene ND 10000 9030 90 10000 8660 87 4 70-130/20
75-00-3 Chloroethane ND 10000 9670 97 10000 8960 90 8 60-140/20
67-66-3 Chloroform ND 10000 8970 90 10000 8340 83 7 70-130/20
95-49-8 o-Chlorotoluene ND 10000 9380 94 10000 8640 86 8 70-130/20
106-43-4 p-Chlorotoluene ND 10000 9460 95 10000 8930 89 6 70-130/20
124-48-1 Dibromochloromethane ND 10000 8760 88 10000 8570 86 2 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 10000 8940 89 10000 8320 83 7 70-130/20
106-93-4 1,2-Dibromoethane ND 10000 8630 86 10000 8510 85 1 70-130/20
75-71-8 Dichlorodifluoromethane ND 10000 6780 68 10000 6180 62 9 60-140/20
95-50-1 1,2-Dichlorobenzene ND 10000 9270 93 10000 8780 88 5 70-130/20
541-73-1 1,3-Dichlorobenzene ND 10000 9340 93 10000 8770 88 6 70-130/20
106-46-7 1,4-Dichlorobenzene ND 10000 8550 86 10000 7980 80 7 70-130/20
75-34-3 1,1-Dichloroethane ND 10000 8770 88 10000 8150 82 7 70-130/20
107-06-2 1,2-Dichloroethane 1230 10000 9990 88 10000 9590 84 4 70-130/20
75-35-4 1,1-Dichloroethylene ND 10000 9820 98 10000 8950 90 9 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 10000 8710 87 10000 8280 83 5 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 10000 9070 91 10000 8240 82 10 70-130/20
78-87-5 1,2-Dichloropropane ND 10000 8800 88 10000 8380 84 5 70-130/20
142-28-9 1,3-Dichloropropane ND 10000 8640 86 10000 8400 84 3 70-130/20
594-20-7 2,2-Dichloropropane ND 10000 9340 93 10000 8620 86 8 70-130/20
563-58-6 1,1-Dichloropropene ND 10000 9430 94 10000 8540 85 10 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 10000 8670 87 10000 8250 83 5 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 10000 9300 93 10000 9070 91 3 70-130/20
108-20-3 Di-Isopropyl Ether ND 10000 8720 87 10000 8290 83 5 70-130/20
100-41-4 Ethylbenzene 1670 10000 10300 86 10000 9690 80 6 70-130/20
87-68-3 Hexachlorobutadiene ND 10000 8840 88 10000 8180 82 8 70-130/20
98-82-8 Isopropylbenzene ND 10000 9850 99 10000 9050 91 8 70-130/20
* = Outside of Control Limits.
35 of 38
FA23294 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23294-4MS A0193649.D 1000 04/07/15 TD n/a n/a VA1681
FA23294-4MSD A0193650.D 1000 04/07/15 TD n/a n/a VA1681
FA23294-4 A0193647.D 1000 04/07/15 TD n/a n/a VA1681
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-2, FA23294-4
FA23294-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene ND 10000 9570 96 10000 8710 87 9 70-130/20
74-83-9 Methyl Bromide ND 10000 9580 96 10000 9120 91 5 60-140/20
74-87-3 Methyl Chloride ND 10000 8520 85 10000 7870 79 8 60-140/20
74-95-3 Methylene Bromide ND 10000 8770 88 10000 8400 84 4 70-130/20
75-09-2 Methylene Chloride ND 10000 9290 93 10000 8820 88 5 70-130/20
1634-04-4 Methyl Tert Butyl Ether 191 J 10000 8990 88 10000 8860 87 1 70-130/20
91-20-3 Naphthalene 1630 10000 9440 78 10000 9210 76 2 70-130/20
103-65-1 n-Propylbenzene 177 J 10000 9870 97 10000 9010 88 9 70-130/20
100-42-5 Styrene ND 10000 8830 88 10000 8380 84 5 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 10000 8790 88 10000 8430 84 4 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 10000 8530 85 10000 8380 84 2 70-130/20
127-18-4 Tetrachloroethylene ND 10000 8770 88 10000 8160 82 7 70-130/20
108-88-3 Toluene 36700 10000 43900 72 10000 41300 46* a 6 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 10000 8630 86 10000 8280 83 4 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 10000 8670 87 10000 8290 83 4 70-130/20
71-55-6 1,1,1-Trichloroethane ND 10000 9460 95 10000 8560 86 10 70-130/20
79-00-5 1,1,2-Trichloroethane ND 10000 8520 85 10000 8400 84 1 70-130/20
79-01-6 Trichloroethylene ND 10000 9030 90 10000 8270 83 9 70-130/20
75-69-4 Trichlorofluoromethane ND 10000 8220 82 10000 7470 75 10 60-140/20
96-18-4 1,2,3-Trichloropropane ND 10000 8640 86 10000 8590 86 1 70-130/20
95-63-6 1,2,4-Trimethylbenzene 2280 10000 10700 84 10000 9990 77 7 70-130/20
108-67-8 1,3,5-Trimethylbenzene 601 10000 9360 88 10000 8650 80 8 70-130/20
75-01-4 Vinyl Chloride ND 10000 9090 91 10000 8220 82 10 60-140/20
m,p-Xylene 7720 20000 25800 90 20000 24300 83 6 70-130/20
95-47-6 o-Xylene 3500 10000 13100 96 10000 12300 88 6 70-130/20
1330-20-7 Xylene (total)11200 30000 38900 92 30000 36600 85 6 70-130/20
CAS No.Surrogate Recoveries MS MSD FA23294-4 Limits
1868-53-7 Dibromofluoromethane 100%99%95%70-130%
17060-07-0 1,2-Dichloroethane-D4 102%102%100%70-130%
2037-26-5 Toluene-D8 98%99%97%70-130%
460-00-4 4-Bromofluorobenzene 101%99%99%70-130%
(a) Outside control limits due to high level in sample relative to spike amount.
* = Outside of Control Limits.
36 of 38
FA23294 55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23295-2MS A0193690.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2MSD A0193691.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2 A0193688.D 25 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-1, FA23294-3, FA23294-5, FA23294-6, FA23294-7
FA23295-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
71-43-2 Benzene 26.2 250 266 96 250 275 100 3 70-130/20
108-86-1 Bromobenzene ND 250 232 93 250 242 97 4 70-130/20
74-97-5 Bromochloromethane ND 250 255 102 250 257 103 1 70-130/20
75-27-4 Bromodichloromethane ND 250 261 104 250 223 89 16 70-130/20
75-25-2 Bromoform ND 250 207 83 250 175 70 17 70-130/20
104-51-8 n-Butylbenzene 8.8 J 250 255 98 250 268 104 5 70-130/20
135-98-8 sec-Butylbenzene 4.9 J 250 270 106 250 286 112 6 70-130/20
98-06-6 tert-Butylbenzene ND 250 268 107 250 278 111 4 70-130/20
56-23-5 Carbon Tetrachloride ND 250 279 112 250 234 94 18 70-130/20
108-90-7 Chlorobenzene ND 250 272 109 250 278 111 2 70-130/20
75-00-3 Chloroethane ND 250 276 110 250 293 117 6 60-140/20
67-66-3 Chloroform ND 250 258 103 250 259 104 0 70-130/20
95-49-8 o-Chlorotoluene ND 250 279 112 250 289 116 4 70-130/20
106-43-4 p-Chlorotoluene ND 250 259 104 250 271 108 5 70-130/20
124-48-1 Dibromochloromethane ND 250 232 93 250 200 80 15 70-130/20
96-12-8 1,2-Dibromo-3-chloropropane ND 250 257 103 250 250 100 3 70-130/20
106-93-4 1,2-Dibromoethane ND 250 240 96 250 249 100 4 70-130/20
75-71-8 Dichlorodifluoromethane ND 250 320 128 250 310 124 3 60-140/20
95-50-1 1,2-Dichlorobenzene ND 250 253 101 250 262 105 3 70-130/20
541-73-1 1,3-Dichlorobenzene ND 250 259 104 250 266 106 3 70-130/20
106-46-7 1,4-Dichlorobenzene ND 250 236 94 250 239 96 1 70-130/20
75-34-3 1,1-Dichloroethane ND 250 248 99 250 253 101 2 70-130/20
107-06-2 1,2-Dichloroethane ND 250 279 112 250 273 109 2 70-130/20
75-35-4 1,1-Dichloroethylene ND 250 283 113 250 291 116 3 70-130/20
156-59-2 cis-1,2-Dichloroethylene ND 250 244 98 250 248 99 2 70-130/20
156-60-5 trans-1,2-Dichloroethylene ND 250 254 102 250 247 99 3 70-130/20
78-87-5 1,2-Dichloropropane ND 250 247 99 250 254 102 3 70-130/20
142-28-9 1,3-Dichloropropane ND 250 231 92 250 245 98 6 70-130/20
594-20-7 2,2-Dichloropropane ND 250 251 100 250 242 97 4 70-130/20
563-58-6 1,1-Dichloropropene ND 250 268 107 250 269 108 0 70-130/20
10061-01-5 cis-1,3-Dichloropropene ND 250 233 93 250 202 81 14 70-130/20
10061-02-6 trans-1,3-Dichloropropene ND 250 248 99 250 217 87 13 70-130/20
108-20-3 Di-Isopropyl Ether ND 250 267 107 250 272 109 2 70-130/20
100-41-4 Ethylbenzene 88.6 250 336 99 250 348 104 4 70-130/20
87-68-3 Hexachlorobutadiene ND 250 236 94 250 239 96 1 70-130/20
98-82-8 Isopropylbenzene 6.8 J 250 284 111 250 295 115 4 70-130/20
* = Outside of Control Limits.
37 of 38
FA23294 55.3.2
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 2
Job Number:FA23294
Account:GRINCC GRI (Geological Resources Inc.)
Project:Former Phelps Amoco; Hwy 64 E, Creswell, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA23295-2MS A0193690.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2MSD A0193691.D 25 04/08/15 TD n/a n/a VA1682
FA23295-2 A0193688.D 25 04/08/15 TD n/a n/a VA1682
The QC reported here applies to the following samples:Method: SM 6200B
FA23294-1, FA23294-3, FA23294-5, FA23294-6, FA23294-7
FA23295-2 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
99-87-6 p-Isopropyltoluene 5.5 J 250 270 106 250 284 111 5 70-130/20
74-83-9 Methyl Bromide ND 250 295 118 250 306 122 4 60-140/20
74-87-3 Methyl Chloride ND 250 316 126 250 312 125 1 60-140/20
74-95-3 Methylene Bromide ND 250 256 102 250 255 102 0 70-130/20
75-09-2 Methylene Chloride ND 250 278 111 250 272 109 2 70-130/20
1634-04-4 Methyl Tert Butyl Ether ND 250 260 104 250 264 106 2 70-130/20
91-20-3 Naphthalene 109 250 341 93 250 352 97 3 70-130/20
103-65-1 n-Propylbenzene 19.6 250 283 105 250 299 112 5 70-130/20
100-42-5 Styrene ND 250 254 102 250 265 106 4 70-130/20
630-20-6 1,1,1,2-Tetrachloroethane ND 250 254 102 250 241 96 5 70-130/20
79-34-5 1,1,2,2-Tetrachloroethane ND 250 219 88 250 230 92 5 70-130/20
127-18-4 Tetrachloroethylene ND 250 243 97 250 252 101 4 70-130/20
108-88-3 Toluene 399 250 634 94 250 674 110 6 70-130/20
87-61-6 1,2,3-Trichlorobenzene ND 250 249 100 250 253 101 2 70-130/20
120-82-1 1,2,4-Trichlorobenzene ND 250 233 93 250 241 96 3 70-130/20
71-55-6 1,1,1-Trichloroethane ND 250 272 109 250 263 105 3 70-130/20
79-00-5 1,1,2-Trichloroethane ND 250 260 104 250 273 109 5 70-130/20
79-01-6 Trichloroethylene ND 250 262 105 250 257 103 2 70-130/20
75-69-4 Trichlorofluoromethane ND 250 278 111 250 272 109 2 60-140/20
96-18-4 1,2,3-Trichloropropane ND 250 237 95 250 242 97 2 70-130/20
95-63-6 1,2,4-Trimethylbenzene 641 250 865 90 250 904 105 4 70-130/20
108-67-8 1,3,5-Trimethylbenzene 201 250 442 96 250 464 105 5 70-130/20
75-01-4 Vinyl Chloride ND 250 283 113 250 295 118 4 60-140/20
m,p-Xylene 1130 500 1630 100 500 1690 112 4 70-130/20
95-47-6 o-Xylene 592 250 862 108 250 897 122 4 70-130/20
1330-20-7 Xylene (total)1720 750 2490 103 750 2580 115 4 70-130/20
CAS No.Surrogate Recoveries MS MSD FA23295-2 Limits
1868-53-7 Dibromofluoromethane 109%104%106%70-130%
17060-07-0 1,2-Dichloroethane-D4 115%107%116%70-130%
2037-26-5 Toluene-D8 95%100%99%70-130%
460-00-4 4-Bromofluorobenzene 97%100%100%70-130%
* = Outside of Control Limits.
38 of 38
FA23294 55.3.2